Investigation of a Novel NDE Method for Monitoring Thermomechanical Damage and Microstructure Evolution in Ferritic-Martensitic Steels for Generation IV Nuclear Energy Systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nagy, Peter

2013-09-30

The main goal of the proposed project is the development of validated nondestructive evaluation (NDE) techniques for in situ monitoring of ferritic-martensitic steels like Grade 91 9Cr-1Mo, which are candidate materials for Generation IV nuclear energy structural components operating at temperatures up to ~650{degree}C and for steam-generator tubing for sodium-cooled fast reactors. Full assessment of thermomechanical damage requires a clear separation between thermally activated microstructural evolution and creep damage caused by simultaneous mechanical stress. Creep damage can be classified as "negligible" creep without significant plastic strain and "ordinary" creep of the primary, secondary, and tertiary kind that is accompanied bymore » significant plastic deformation and/or cavity nucleation and growth. Under negligible creep conditions of interest in this project, minimal or no plastic strain occurs, and the accumulation of creep damage does not significantly reduce the fatigue life of a structural component so that low-temperature design rules, such as the ASME Section III, Subsection NB, can be applied with confidence. The proposed research project will utilize a multifaceted approach in which the feasibility of electrical conductivity and thermo-electric monitoring methods is researched and coupled with detailed post-thermal/creep exposure characterization of microstructural changes and damage processes using state-of-the-art electron microscopy techniques, with the aim of establishing the most effective nondestructive materials evaluation technique for particular degradation modes in high-temperature alloys that are candidates for use in the Next Generation Nuclear Plant (NGNP) as well as providing the necessary mechanism-based underpinnings for relating the two. Only techniques suitable for practical application in situ will be considered. As the project evolves and results accumulate, we will also study the use of this technique for monitoring other GEN IV materials. Through the results obtained from this integrated materials behavior and NDE study, new insight will be gained into the best nondestructive creep and microstructure monitoring methods for the particular mechanisms identified in these materials. The proposed project includes collaboration with a national laboratory partner and the results will also serve as a foundation to guide the efforts of scientists in the DOE laboratory, university, and industrial communities concerned with the technological challenges of monitoring creep and microstructural evolution in materials planned to be used in Generation IV Nuclear Energy Systems.« less

Creep-Fatigue Damage Investigation and Modeling of Alloy 617 at High Temperatures

NASA Astrophysics Data System (ADS)

Tahir, Fraaz

The Very High Temperature Reactor (VHTR) is one of six conceptual designs proposed for Generation IV nuclear reactors. Alloy 617, a solid solution strengthened Ni-base superalloy, is currently the primary candidate material for the tubing of the Intermediate Heat Exchanger (IHX) in the VHTR design. Steady-state operation of the nuclear power plant at elevated temperatures leads to creep deformation, whereas loading transients including startup and shutdown generate fatigue. A detailed understanding of the creep-fatigue interaction in Alloy 617 is necessary before it can be considered as a material for nuclear construction in ASME Boiler and Pressure Vessel Code. Current design codes for components undergoing creep-fatigue interaction at elevated temperatures require creep-fatigue testing data covering the entire range from fatigue-dominant to creep-dominant loading. Classical strain-controlled tests, which produce stress relaxation during the hold period, show a saturation in cycle life with increasing hold periods due to the rapid stress-relaxation of Alloy 617 at high temperatures. Therefore, applying longer hold time in these tests cannot generate creep-dominated failure. In this study, uniaxial isothermal creep-fatigue tests with non-traditional loading waveforms were designed and performed at 850 and 950°C, with an objective of generating test data in the creep-dominant regime. The new loading waveforms are hybrid strain-controlled and force-controlled testing which avoid stress relaxation during the creep hold. The experimental data showed varying proportions of creep and fatigue damage, and provided evidence for the inadequacy of the widely-used time fraction rule for estimating creep damage under creep-fatigue conditions. Micro-scale damage features in failed test specimens, such as fatigue cracks and creep voids, were quantified using a Scanning Electron Microscope (SEM) to find a correlation between creep and fatigue damage. Quantitative statistical imaging analysis showed that the microstructural damage features (cracks and voids) are correlated with a new mechanical driving force parameter. The results from this image-based damage analysis were used to develop a phenomenological life-prediction methodology called the effective time fraction approach. Finally, the constitutive creep-fatigue response of the material at 950°C was modeled using a unified viscoplastic model coupled with a damage accumulation model. The simulation results were used to validate an energy-based constitutive life-prediction model, as a mechanistic model for potential component and structure level creep-fatigue analysis.

Characterization of C/Enhanced SiC Composite During Creep-Rupture Tests Using an Ultrasonic Guided Wave Scan System

NASA Technical Reports Server (NTRS)

Roth, Don J.; Verrilli, Michael J.; Martin, Richard E.; Cosgriff, Laura M.

2004-01-01

An ultrasonic guided wave scan system was used to nondestructively monitor damage over time and position in a C/enhanced SiC sample that was creep tested to failure at 1200 C in air at a stress of 69 MPa (10 ksi). The use of the guided wave scan system for mapping evolving oxidation profiles (via porosity gradients resulting from oxidation) along the sample length and predicting failure location was explored. The creep-rupture tests were interrupted for ultrasonic evaluation every two hours until failure at approx. 17.5 cumulative hours.

Creep Damage Analysis of a Lattice Truss Panel Structure

NASA Astrophysics Data System (ADS)

Jiang, Wenchun; Li, Shaohua; Luo, Yun; Xu, Shugen

2017-01-01

The creep failure for a lattice truss sandwich panel structure has been predicted by finite element method (FEM). The creep damage is calculated by three kinds of stresses: as-brazed residual stress, operating thermal stress and mechanical load. The creep damage at tensile and compressive loads have been calculated and compared. The creep rate calculated by FEM, Gibson-Ashby and Hodge-Dunand models have been compared. The results show that the creep failure is located at the fillet at both tensile and creep loads. The damage rate at the fillet at tensile load is 50 times as much as that at compressive load. The lattice truss panel structure has a better creep resistance to compressive load than tensile load, because the creep and stress triaxiality at the fillet has been decreased at compressive load. The maximum creep strain at the fillet and the equivalent creep strain of the panel structure increase with the increase of applied load. Compared with Gibson-Ashby model and Hodge-Dunand models, the modified Gibson-Ashby model has a good prediction result compared with FEM. However, a more accurate model considering the size effect of the structure still needs to be developed.

Some aspects of thermomechanical fatigue of AISI 304L stainless steel: Part I. creep- fatigue damage

NASA Astrophysics Data System (ADS)

Zauter, R.; Christ, H. J.; Mughrabi, H.

1994-02-01

Thermomechanical fatigue (TMF) tests on the austenitic stainless steel AISI 304L have been conducted under “true≓ plastic-strain control in vacuum. This report considers the damage oc-curring during TMF loading. It is shown how the temperature interval and the phasing (in-phase, out-of-phase) determine the mechanical response and the lifetime of the specimens. If creep-fatigue interaction takes place during in-phase cycling, the damage occurs inside the ma-terial, leading to intergranular cracks which reduce the lifetime considerably. Out-of-phase cy-cling inhibits creep-induced damage, and no lifetime reduction occurs, even if the material is exposed periodically to temperatures in the creep regime. A formula is proposed which allows prediction of the failure mode, depending on whether creep-fatigue damage occurs or not. At a given strain rate, the formula is able to estimate the temperature of transition between pure fatigue and creep-fatigue damage.

Influence of Prior Fatigue Cycling on Creep Behavior of Reduced Activation Ferritic-Martensitic Steel

NASA Astrophysics Data System (ADS)

Sarkar, Aritra; Vijayanand, V. D.; Parameswaran, P.; Shankar, Vani; Sandhya, R.; Laha, K.; Mathew, M. D.; Jayakumar, T.; Rajendra Kumar, E.

2014-06-01

Creep tests were carried out at 823 K (550 °C) and 210 MPa on Reduced Activation Ferritic-Martensitic (RAFM) steel which was subjected to different extents of prior fatigue exposure at 823 K at a strain amplitude of ±0.6 pct to assess the effect of prior fatigue exposure on creep behavior. Extensive cyclic softening that characterized the fatigue damage was found to be immensely deleterious for creep strength of the tempered martensitic steel. Creep rupture life was reduced to 60 pct of that of the virgin steel when the steel was exposed to as low as 1 pct of fatigue life. However, creep life saturated after fatigue exposure of 40 pct. Increase in minimum creep rate and decrease in creep rupture ductility with a saturating trend were observed with prior fatigue exposures. To substantiate these findings, detailed transmission electron microscopy studies were carried out on the steel. With fatigue exposures, extensive recovery of martensitic-lath structure was distinctly observed which supported the cyclic softening behavior that was introduced due to prior fatigue. Consequently, prior fatigue exposures were considered responsible for decrease in creep ductility and associated reduction in the creep rupture strength.

Part-to-itself model inversion in process compensated resonance testing

NASA Astrophysics Data System (ADS)

Mayes, Alexander; Jauriqui, Leanne; Biedermann, Eric; Heffernan, Julieanne; Livings, Richard; Aldrin, John C.; Goodlet, Brent; Mazdiyasni, Siamack

2018-04-01

Process Compensated Resonance Testing (PCRT) is a non-destructive evaluation (NDE) method involving the collection and analysis of a part's resonance spectrum to characterize its material or damage state. Prior work used the finite element method (FEM) to develop forward modeling and model inversion techniques. In many cases, the inversion problem can become confounded by multiple parameters having similar effects on a part's resonance frequencies. To reduce the influence of confounding parameters and isolate the change in a part (e.g., creep), a part-to-itself (PTI) approach can be taken. A PTI approach involves inverting only the change in resonance frequencies from the before and after states of a part. This approach reduces the possible inversion parameters to only those that change in response to in-service loads and damage mechanisms. To evaluate the effectiveness of using a PTI inversion approach, creep strain and material properties were estimated in virtual and real samples using FEM inversion. Virtual and real dog bone samples composed of nickel-based superalloy Mar-M-247 were examined. Virtual samples were modeled with typically observed variations in material properties and dimensions. Creep modeling was verified with the collected resonance spectra from an incrementally crept physical sample. All samples were inverted against a model space that allowed for change in the creep damage state and the material properties but was blind to initial part dimensions. Results quantified the capabilities of PTI inversion in evaluating creep strain and material properties, as well as its sensitivity to confounding initial dimensions.

A continuous damage model based on stepwise-stress creep rupture tests

NASA Technical Reports Server (NTRS)

Robinson, D. N.

1985-01-01

A creep damage accumulation model is presented that makes use of the Kachanov damage rate concept with a provision accounting for damage that results from a variable stress history. This is accomplished through the introduction of an additional term in the Kachanov rate equation that is linear in the stress rate. Specification of the material functions and parameters in the model requires two types of constituting a data base: (1) standard constant-stress creep rupture tests, and (2) a sequence of two-step creep rupture tests.

Thermomechanical behavior of tin-rich (lead-free) solders

NASA Astrophysics Data System (ADS)

Sidhu, Rajen Singh

In order to adequately characterize the behavior of ball-grid-array (BGA) Pb-free solder spheres in electronic devices, the microstructure and thermomechanical behavior need to be studied. Microstructure characterization of pure Sn, Sn-0.7Cu, Sn-3.5Ag, and Sn-3.9Ag-0.7Cu alloys was conducted using optical microscopy, scanning electron microscopy, transmission electron microscopy, image analysis, and a novel serial sectioning 3D reconstruction process. Microstructure-based finite-element method (FEM) modeling of deformation in Sn-3.5Ag alloy was conducted, and it will be shown that this technique is more accurate when compared to traditional unit cell models for simulating and understanding material behavior. The effect of cooling rate on microstructure and creep behavior of bulk Sn-rich solders was studied. The creep behavior was evaluated at 25, 95, and 120°C. Faster cooling rates were found to increase the creep strength of the solders due to refinement of the solder microstructure. The creep behavior of Sn-rich single solder spheres reflowed on Cu substrates was studied at 25, 60, 95, and 130°C. Testing was conducted using a microforce testing system, with lap-shear geometry samples. The solder joints displayed two distinct creep behaviors: (a) precipitation-strengthening (Sn-3.5Ag and Sn-3.9Ag-0.7Cu) and (b) power law creep accommodated by grain boundary sliding (GBS) (Sn and Sn-0.7Cu). The relationship between microstructural features (i.e. intermetallic particle size and spacing), stress exponents, threshold stress, and activation energies are discussed. The relationship between small-length scale creep behavior and bulk behavior is also addressed. To better understand the damage evolution in Sn-rich solder joints during thermal fatigue, the local damage will be correlated to the cyclic hysteresis behavior and crystal orientations present in the Sn phase of solder joints. FEM modeling will also be utilized to better understand the macroscopic and local strain response of the lap shear geometry.

Damage Assessment of Heat Resistant Steels through Electron BackScatter Diffraction Strain Analysis under Creep and Creep-Fatigue Conditions

NASA Astrophysics Data System (ADS)

Fujiyama, Kazunari; Kimachi, Hirohisa; Tsuboi, Toshiki; Hagiwara, Hiroyuki; Ogino, Shotaro; Mizutani, Yoshiki

EBSD(Electron BackScatter Diffraction) analyses were conducted for studying the quantitative microstructural metrics of creep and creep-fatigue damage for austenitic SUS304HTB boiler tube steel and ferritic Mod.9Cr piping steel. KAM(Kernel Average Misorientation) maps and GOS(Grain Orientation Spread) maps were obtained for these samples and the area averaged values KAMave and GOSave were obtained. While the increasing trends of these misorientation metrics were observed for SUS304HTB steel, the decreasing trends were observed for damaged Mod.9Cr steel with extensive recovery of subgrain structure. To establish more universal parameter representing the accumulation of damage to compensate these opposite trends, the EBSD strain parameters were introduced for converting the misorientation changes into the quantities representing accumulated permanent strains during creep and creep-fatigue damage process. As KAM values were dependent on the pixel size (inversely proportional to the observation magnification) and the permanent strain could be expressed as the shear strain which was the product of dislocation density, Burgers vector and dislocation movement distance, two KAM strain parameters MεKAMnet and MεδKAMave were introduced as the sum of product of the noise subtracted KAMnet and the absolute change from initial value δKAMave with dislocation movement distance divided by pixel size. MεδKAMave parameter showed better relationship both with creep strain in creep tests and accumulated creep strain range in creep-fatigue tests. This parameter can be used as the strain-based damage evaluation and detector of final failure.

Failure Mechanisms and Damage Model of Ductile Cast Iron Under Low-Cycle Fatigue Conditions

NASA Astrophysics Data System (ADS)

Wu, Xijia; Quan, Guangchun; MacNeil, Ryan; Zhang, Zhong; Sloss, Clayton

2014-10-01

Strain-controlled low-cycle fatigue (LCF) tests were conducted on ductile cast iron (DCI) at strain rates of 0.02, 0.002, and 0.0002/s in the temperature range from room temperature to 1073 K (800 °C). A constitutive-damage model was developed within the integrated creep-fatigue theory (ICFT) framework on the premise of strain decomposition into rate-independent plasticity and time-dependent creep. Four major damage mechanisms: (i) plasticity-induced fatigue, (ii) intergranular embrittlement (IE), (iii) creep, and (iv) oxidation were considered in a nonlinear creep-fatigue interaction model which represents the overall damage accumulation process consisting of oxidation-assisted fatigue crack nucleation and propagation in coalescence with internally distributed damage ( e.g., IE and creep), leading to final fracture. The model was found to agree with the experimental observations of the complex DCI-LCF phenomena, for which the linear damage summation rule would fail.

Creep Behavior in Interlaminar Shear of a SiC/SiC Ceramic Composite with a Self-healing Matrix

NASA Astrophysics Data System (ADS)

Ruggles-Wrenn, M. B.; Pope, M. T.

2014-02-01

Creep behavior in interlaminar shear of a non-oxide ceramic composite with a multilayered matrix was investigated at 1,200 °C in laboratory air and in steam environment. The composite was produced via chemical vapor infiltration (CVI). The composite had an oxidation inhibited matrix, which consisted of alternating layers of silicon carbide and boron carbide and was reinforced with laminated Hi-Nicalon™ fibers woven in a five-harness-satin weave. Fiber preforms had pyrolytic carbon fiber coating with boron carbide overlay applied. The interlaminar shear properties were measured. The creep behavior was examined for interlaminar shear stresses in the 16-22 MPa range. Primary and secondary creep regimes were observed in all tests conducted in air and in steam. In air and in steam, creep run-out defined as 100 h at creep stress was achieved at 16 MPa. Larger creep strains were accumulated in steam. However, creep strain rates and creep lifetimes were only moderately affected by the presence of steam. The retained properties of all specimens that achieved run-out were characterized. Composite microstructure, as well as damage and failure mechanisms were investigated.

The strainrange conversion principle for treating cumulative fatigue damage in the creep range

NASA Technical Reports Server (NTRS)

Manson, S. S.

1983-01-01

A formula is derived for combining effects of successive hysteresis loops in the creep range of materials when one loop has excess tensile creep, while the other contains excess compressive creep. The resultant effect resembles single loops involving balanced tensile and compressive creep. The attempt to use the Interaction Damage Rule as a tool in combining loops of non-equal size and complex strainrange content has led to important new concepts useful in future studies of creep-fatigue. It turns out that the Interaction Damage Rule is basically an expression of how a set of hysteresis loops involving only single generic strains can combine to produce the same micromechanistic damage as the loop containing the combined strainranges which it analyzes. Making use of the underlying concept of Strainrange Partitioning that only the strainrange content of a hysteresis loop governs fatigue life, not order of introducing strainranges, a rational derivation of the Interaction Damage Rule is provided, showing also how it can effectively be used to synthesize independent loops and determine both damaging and healing effects.

Thermomechanical Fatigue Durability of T650-35/PMR-15 Sheet Molding Compound

NASA Technical Reports Server (NTRS)

Castelli, Michael G.; Sutter, James K.; Benson, Dianne

1998-01-01

Although polyimide based composites have been used for many years in a wide variety of elevated temperature applications, very little work has been done to examine the durability and damage behavior under more prototypical thermomechanical fatigue (TMF) loadings. Synergistic effects resulting from simultaneous temperature and load cycling can potentially lead to enhanced, if not unique, damage modes and contribute to a number of nonlinear deformation responses. The goal of this research was to examine the effects of a TMF loading spectrum, representative of a gas turbine engine compressor application, on a polyimide sheet molding compound (SMC). High performance SMCs present alternatives to prepreg forms with great potential for low cost component production through less labor intensive, more easily automated manufacturing. To examine the issues involved with TMF, a detailed experimental investigation was conducted to characterize the durability of a T650-35/PMR-15 SMC subjected to TMF mission cycle loadings. Fatigue damage progression was tracked through macroscopic deformation and elastic stiffness. Additional properties, such as the glass transition temperature (T(sub g) and dynamic mechanical properties were examined. The fiber distribution orientation was also characterized through a detailed quantitative image analysis. Damage tolerance was quantified on the basis of residual static tensile properties after a prescribed number of TMF missions. Detailed microstructural examinations were conducted using optical and scanning electron microscopy to characterize the local damage. The imposed baseline TMF missions had only a modest impact on inducing fatigue damage with no statistically significant degradation occurring in the measured macroscopic properties. Microstructural damage was, however, observed subsequent to 100 h of TMF cycling which consisted primarily of fiber debonding and transverse cracking local to predominantly transverse fiber bundles. The TMF loadings did introduce creep related effects (strain accumulation) which led to rupture in some of the more aggressive stress scenarios examined. In some cases this creep behavior occurred at temperatures in excess of 150 C below commonly cited values for T(sub g). Thermomechanical exploratory creep tests revealed that the SMC was subject to time dependent deformation at stress/temperature thresholds of 150 MPa/230 C and 170 MPa/180 C.

Process compensated resonance testing modeling for damage evolution and uncertainty quantification

NASA Astrophysics Data System (ADS)

Biedermann, Eric; Heffernan, Julieanne; Mayes, Alexander; Gatewood, Garrett; Jauriqui, Leanne; Goodlet, Brent; Pollock, Tresa; Torbet, Chris; Aldrin, John C.; Mazdiyasni, Siamack

2017-02-01

Process Compensated Resonance Testing (PCRT) is a nondestructive evaluation (NDE) method based on the fundamentals of Resonant Ultrasound Spectroscopy (RUS). PCRT is used for material characterization, defect detection, process control and life monitoring of critical gas turbine engine and aircraft components. Forward modeling and model inversion for PCRT have the potential to greatly increase the method's material characterization capability while reducing its dependence on compiling a large population of physical resonance measurements. This paper presents progress on forward modeling studies for damage mechanisms and defects in common to structural materials for gas turbine engines. Finite element method (FEM) models of single crystal (SX) Ni-based superalloy Mar-M247 dog bones and Ti-6Al-4V cylindrical bars were created, and FEM modal analyses calculated the resonance frequencies for the samples in their baseline condition. Then the frequency effects of superalloy creep (high-temperature plastic deformation) and macroscopic texture (preferred crystallographic orientation of grains detrimental to fatigue properties) were evaluated. A PCRT sorting module for creep damage in Mar-M247 was trained with a virtual database made entirely of modeled design points. The sorting module demonstrated successful discrimination of design points with as little as 1% creep strain in the gauge section from a population of acceptable design points with a range of material and geometric variation. The resonance frequency effects of macro-scale texture in Ti-6Al-4V were quantified with forward models of cylinder samples. FEM-based model inversion was demonstrated for Mar-M247 bulk material properties and variations in crystallographic orientation. PCRT uncertainty quantification (UQ) was performed using Monte Carlo studies for Mar-M247 that quantified the overall uncertainty in resonance frequencies resulting from coupled variation in geometry, material properties, crystallographic orientation and creep damage. A model calibration process was also developed that evaluates inversion fitting to differences from a designated reference sample rather than absolute property values, yielding a reduction in fit error.

The influence of temperature on brittle creep in sandstones

NASA Astrophysics Data System (ADS)

Heap, M. J.; Baud, P.; Meredith, P. G.; Vinciguerra, S.

2009-04-01

The characterization of time-dependent brittle rock deformation is fundamental to understanding the long-term evolution and dynamics of the Earth's upper crust. The presence of water promotes time-dependent deformation through environment-dependent stress corrosion cracking that allows rocks to deform at stresses far below their short-term failure stress. Here we report results from an experimental study of the influence of an elevated temperature on time-dependent brittle creep in water-saturated samples of Darley Dale (initial porosity of 13%), Bentheim (23%) and Crab Orchard (4%) sandstones. We present results from both conventional creep experiments (or ‘static fatigue' tests) and stress-stepping creep experiments performed under 20°C and 75°C and an effective confining pressure of 30 MPa (50 MPa confining pressure and a 20 MPa pore fluid pressure). The evolution of crack damage was monitored throughout each experiment by measuring the three proxies for damage (1) axial strain (2) pore volume change and (3) the output of AE energy. Conventional creep experiments have demonstrated that, for any given applied differential stress, the time-to-failure is dramatically reduced and the creep strain rate is significantly increased by application of an elevated temperature. Stress-stepping creep experiments have allowed us to investigate the influence of temperature in detail. Results from these experiments show that the creep strain rate for Darley Dale and Bentheim sandstones increases by approximately 3 orders of magnitude, and for Crab Orchard sandstone increases by approximately 2 orders of magnitude, as temperature is increased from 20°C to 75°C at a fixed effective differential stress. We discuss these results in the context of the different mineralogical and microstructural properties of the three rock types and the micro-mechanical and chemical processes operating on them.

Continuum Damage Mechanics Used to Predict the Creep Life of Monolithic Ceramics

NASA Technical Reports Server (NTRS)

Powers, Lynn M.; Jadaan, Osama M.

1998-01-01

Significant improvements in propulsion and power generation for the next century will require revolutionary advances in high-temperature materials and structural design. Advanced ceramics are candidate materials for these elevated temperature applications. High-temperature and long-duration applications of monolithic ceramics can place their failure mode in the creep rupture regime. An analytical methodology in the form of the integrated design program-Ceramics Analysis and Reliability Evaluation of Structures/Creep (CARES/Creep) has been developed by the NASA Lewis Research Center to predict the life of ceramic structural components subjected to creep rupture conditions. This program utilizes commercially available finite element packages and takes into account the transient state of stress and creep strain distributions (stress relaxation as well as the asymmetric response to tension and compression). The creep life of a component is discretized into short time steps, during which the stress distribution is assumed constant. Then, the damage is calculated for each time step on the basis of a modified Monkman-Grant (MMG) creep rupture criterion. The cumulative damage is subsequently calculated as time elapses in a manner similar to Miner's rule for cyclic fatigue loading. Failure is assumed to occur when the normalized cumulative damage at any point in the component reaches unity. The corresponding time is the creep rupture life for that component.

Creep Tests and Modeling Based on Continuum Damage Mechanics for T91 and T92 Steels

NASA Astrophysics Data System (ADS)

Pan, J. P.; Tu, S. H.; Zhu, X. W.; Tan, L. J.; Hu, B.; Wang, Q.

2017-12-01

9-11%Cr ferritic steels play an important role in high-temperature and high-pressure boilers of advanced power plants. In this paper, a continuum damage mechanics (CDM)-based creep model was proposed to study the creep behavior of T91 and T92 steels at high temperatures. Long-time creep tests were performed for both steels under different conditions. The creep rupture data and creep curves obtained from creep tests were captured well by theoretical calculation based on the CDM model over a long creep time. It is shown that the developed model is able to predict creep data for the two ferritic steels accurately up to tens of thousands of hours.

Low cycle fatigue and creep-fatigue behavior of Ni-based alloy 230 at 850 C

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, Xiang; Yang, Zhiqing; Sokolov, Mikhail A

Strain-controlled low cycle fatigue (LCF) and creep-fatigue testing of Ni-based alloy 230 were carried out at 850 C. The material creep-fatigue life decreased compared with its low cycle fatigue life at the same total strain range. Longer hold time at peak tensile strain further reduced the material creep-fatigue life. Based on the electron backscatter diffraction, a novel material deformation characterization method was applied, which revealed that in low cycle fatigue testing as the total strain range increased, the deformation was segregated to grain boundaries since the test temperature was higher than the material equicohesive temperature and grain boundaries became weakermore » regions compared with grains. Creep-fatigue tests enhanced the localized deformation, resulting in material interior intergranular cracking, and accelerated material damage. Precipitation in alloy 230 helped slip dispersion, favorable for fatigue property, but grain boundary cellular precipitates formed after material exposure to the elevated temperature had a deleterious effect on the material low cycle fatigue and creep-fatigue property.« less

NASALIFE - Component Fatigue and Creep Life Prediction Program

NASA Technical Reports Server (NTRS)

Gyekenyesi, John Z.; Murthy, Pappu L. N.; Mital, Subodh K.

2014-01-01

NASALIFE is a life prediction program for propulsion system components made of ceramic matrix composites (CMC) under cyclic thermo-mechanical loading and creep rupture conditions. Although the primary focus was for CMC components, the underlying methodologies are equally applicable to other material systems as well. The program references empirical data for low cycle fatigue (LCF), creep rupture, and static material properties as part of the life prediction process. Multiaxial stresses are accommodated by Von Mises based methods and a Walker model is used to address mean stress effects. Varying loads are reduced by the Rainflow counting method or a peak counting type method. Lastly, damage due to cyclic loading and creep is combined with Minor's Rule to determine damage due to cyclic loading, damage due to creep, and the total damage per mission and the number of potential missions the component can provide before failure.

Numerical-graphical method for describing the creep of damaged highly filled polymer materials

NASA Astrophysics Data System (ADS)

Bykov, D. L.; Martynova, E. D.; Mel'nikov, V. P.

2015-09-01

A method for describing the creep behavior until fracture of a highly filled polymer material previously damaged in preliminary tests is proposed. The constitutive relations are the relations of nonlinear endochronic theory of aging viscoelastic materials (NETAVEM) [1]. The numerical-graphical method for identifying the functions occurring in NETAVEM, which was proposed in [2] for describing loading processes at a constant strain rate, is used here for the first time in creep theory. We use the results of experiments with undamaged and preliminary damaged specimens under the action of the same constant tensile loads. The creep kernel is determined in experiments with an undamaged specimen. The reduced time function contained in NETAVEM is determined from the position of points corresponding to the same values of strain on the creep curves of the damaged and undamaged specimens. An integral equation is solved to obtain the aging function, and then the viscosity function is determined. The knowledge of all functions contained in the constitutive relations permits solving the creep problem for products manufactured from a highly filled polymer material.

Accelerated Creep Testing of High Strength Aramid Webbing

NASA Technical Reports Server (NTRS)

Jones, Thomas C.; Doggett, William R.; Stnfield, Clarence E.; Valverde, Omar

2012-01-01

A series of preliminary accelerated creep tests were performed on four variants of 12K and 24K lbf rated Vectran webbing to help develop an accelerated creep test methodology and analysis capability for high strength aramid webbings. The variants included pristine, aged, folded and stitched samples. This class of webbings is used in the restraint layer of habitable, inflatable space structures, for which the lifetime properties are currently not well characterized. The Stepped Isothermal Method was used to accelerate the creep life of the webbings and a novel stereo photogrammetry system was used to measure the full-field strains. A custom MATLAB code is described, and used to reduce the strain data to produce master creep curves for the test samples. Initial results show good correlation between replicates; however, it is clear that a larger number of samples are needed to build confidence in the consistency of the results. It is noted that local fiber breaks affect the creep response in a similar manner to increasing the load, thus raising the creep rate and reducing the time to creep failure. The stitched webbings produced the highest variance between replicates, due to the combination of higher local stresses and thread-on-fiber damage. Large variability in the strength of the webbings is also shown to have an impact on the range of predicted creep life.

Micro-Macro Analysis and Phenomenological Modelling of Salt Viscous Damage and Application to Salt Caverns

NASA Astrophysics Data System (ADS)

Zhu, Cheng; Pouya, Ahmad; Arson, Chloé

2015-11-01

This paper aims to gain fundamental understanding of the microscopic mechanisms that control the transition between secondary and tertiary creep around salt caverns in typical geological storage conditions. We use a self-consistent inclusion-matrix model to homogenize the viscoplastic deformation of halite polycrystals and predict the number of broken grains in a Representative Elementary Volume of salt. We use this micro-macro modeling framework to simulate creep tests under various axial stresses, which gives us the critical viscoplastic strain at which grain breakage (i.e., tertiary creep) is expected to occur. The comparison of simulation results for short-term and long-term creep indicates that the initiation of tertiary creep depends on the stress and the viscoplastic strain. We use the critical viscoplastic deformation as a yield criterion to control the transition between secondary and tertiary creep in a phenomenological viscoplastic model, which we implement into the Finite Element Method program POROFIS. We model a 850-m-deep salt cavern of irregular shape, in axis-symmetric conditions. Simulations of cavern depressurization indicate that a strain-dependent damage evolution law is more suitable than a stress-dependent damage evolution law, because it avoids high damage concentrations and allows capturing the formation of a damaged zone around the cavity. The modeling framework explained in this paper is expected to provide new insights to link grain breakage to phenomenological damage variables used in Continuum Damage Mechanics.

FY16 Status Report on Development of Integrated EPP and SMT Design Methods

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jetter, R. I.; Sham, T. -L.; Wang, Y.

2016-08-01

The goal of the Elastic-Perfectly Plastic (EPP) combined integrated creep-fatigue damage evaluation approach is to incorporate a Simplified Model Test (SMT) data based approach for creep-fatigue damage evaluation into the EPP methodology to avoid the separate evaluation of creep and fatigue damage and eliminate the requirement for stress classification in current methods; thus greatly simplifying evaluation of elevated temperature cyclic service. The EPP methodology is based on the idea that creep damage and strain accumulation can be bounded by a properly chosen “pseudo” yield strength used in an elastic-perfectly plastic analysis, thus avoiding the need for stress classification. The originalmore » SMT approach is based on the use of elastic analysis. The experimental data, cycles to failure, is correlated using the elastically calculated strain range in the test specimen and the corresponding component strain is also calculated elastically. The advantage of this approach is that it is no longer necessary to use the damage interaction, or D-diagram, because the damage due to the combined effects of creep and fatigue are accounted in the test data by means of a specimen that is designed to replicate or bound the stress and strain redistribution that occurs in actual components when loaded in the creep regime. The reference approach to combining the two methodologies and the corresponding uncertainties and validation plans are presented. Results from recent key feature tests are discussed to illustrate the applicability of the EPP methodology and the behavior of materials at elevated temperature when undergoing stress and strain redistribution due to plasticity and creep.« less

Engineering Property Prediction Tools for Tailored Polymer Composite Structures (49465)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nguyen, Ba Nghiep; Kunc, Vlastimil

2009-12-29

Process and constitutive models as well as characterization tools and testing methods were developed to determine stress-strain responses, damage development, strengths and creep of long-fiber thermoplastics (LFTs). The developed models were implemented in Moldflow and ABAQUS and have been validated against LFT data obtained experimentally.

Creep and Environmental Durability of EBC/CMCs Under Imposed Thermal Gradient Conditions

NASA Technical Reports Server (NTRS)

Appleby, Matthew; Morscher, Gregory N.; Zhu, Dongming

2013-01-01

Interest in SiC fiber-reinforced SiC ceramic matrix composite (CMC) environmental barrier coating (EBC) systems for use in high temperature structural applications has prompted the need for characterization of material strength and creep performance under complex aerospace turbine engine environments. Stress-rupture tests have been performed on SiC/SiC composites systems, with varying fiber types and coating schemes to demonstrate material behavior under isothermal conditions. Further testing was conducted under exposure to thermal stress gradients to determine the effect on creep resistance and material durability. In order to understand the associated damage mechanisms, emphasis is placed on experimental techniques as well as implementation of non-destructive evaluation; including electrical resistivity monitoring. The influence of environmental and loading conditions on life-limiting material properties is shown.

Evaluation of CVI SiC/SiC Composites for High Temperature Applications

NASA Technical Reports Server (NTRS)

Kiser, D.; Almansour, A.; Smith, C.; Gorican, D.; Phillips, R.; Bhatt, R.; McCue, T.

2017-01-01

Silicon carbide fiber reinforced silicon carbide (SiC/SiC) composites are candidate materials for various high temperature turbine engine applications because of their high specific strength and good creep resistance at temperatures of 1400 C (2552 F) and higher. Chemical vapor infiltration (CVI) SiC/SiC ceramic matrix composites (CMC) incorporating Sylramic-iBN SiC fiber were evaluated via fast fracture tensile tests (acoustic emission damage characterization to assess cracking behavior), tensile creep testing, and microscopy. The results of this testing and observed material behavior degradation mechanisms are reviewed.

Creep and cracking of concrete hinges: insight from centric and eccentric compression experiments.

PubMed

Schlappal, Thomas; Schweigler, Michael; Gmainer, Susanne; Peyerl, Martin; Pichler, Bernhard

2017-01-01

Existing design guidelines for concrete hinges consider bending-induced tensile cracking, but the structural behavior is oversimplified to be time-independent. This is the motivation to study creep and bending-induced tensile cracking of initially monolithic concrete hinges systematically. Material tests on plain concrete specimens and structural tests on marginally reinforced concrete hinges are performed. The experiments characterize material and structural creep under centric compression as well as bending-induced tensile cracking and the interaction between creep and cracking of concrete hinges. As for the latter two aims, three nominally identical concrete hinges are subjected to short-term and to longer-term eccentric compression tests. Obtained material and structural creep functions referring to centric compression are found to be very similar. The structural creep activity under eccentric compression is significantly larger because of the interaction between creep and cracking, i.e. bending-induced cracks progressively open and propagate under sustained eccentric loading. As for concrete hinges in frame-like integral bridge construction, it is concluded (i) that realistic simulation of variable loads requires consideration of the here-studied time-dependent behavior and (ii) that permanent compressive normal forces shall be limited by 45% of the ultimate load carrying capacity, in order to avoid damage of concrete hinges under sustained loading.

Finite strain transient creep of D16T alloy: identification and validation employing heterogeneous tests

NASA Astrophysics Data System (ADS)

Shutov, A. V.; Larichkin, A. Yu

2017-10-01

A cyclic creep damage model, previously proposed by the authors, is modified for a better description of the transient creep of D16T alloy observed in the finite strain range under rapidly changing stresses. The new model encompasses the concept of kinematic hardening, which allows us to account for the creep-induced anisotropy. The model kinematics is based on the nested multiplicative split of the deformation gradient, proposed by Lion. The damage evolution is accounted for by the classical Kachanov-Rabotnov approach. The material parameters are identified using experimental data on cyclic torsion of thick-walled samples with different holding times between load reversals. For the validation of the proposed material model, an additional experiment is analyzed. Although this additional test is not involved in the identification procedure, the proposed cyclic creep damage model describes it accurately.

Deformation analysis of polymers composites: rheological model involving time-based fractional derivative

NASA Astrophysics Data System (ADS)

Zhou, H. W.; Yi, H. Y.; Mishnaevsky, L.; Wang, R.; Duan, Z. Q.; Chen, Q.

2017-05-01

A modeling approach to time-dependent property of Glass Fiber Reinforced Polymers (GFRP) composites is of special interest for quantitative description of long-term behavior. An electronic creep machine is employed to investigate the time-dependent deformation of four specimens of dog-bond-shaped GFRP composites at various stress level. A negative exponent function based on structural changes is introduced to describe the damage evolution of material properties in the process of creep test. Accordingly, a new creep constitutive equation, referred to fractional derivative Maxwell model, is suggested to characterize the time-dependent behavior of GFRP composites by replacing Newtonian dashpot with the Abel dashpot in the classical Maxwell model. The analytic solution for the fractional derivative Maxwell model is given and the relative parameters are determined. The results estimated by the fractional derivative Maxwell model proposed in the paper are in a good agreement with the experimental data. It is shown that the new creep constitutive model proposed in the paper needs few parameters to represent various time-dependent behaviors.

Damage Characterization in SiC/SiC Composites using Electrical Resistance

NASA Technical Reports Server (NTRS)

Smith, Craig E.; Xia, Zhenhai

2011-01-01

SiC/SiC ceramic matrix composites (CMCs) under creep-rupture loading accumulate damage by means of local matrix cracks that typically form near a stress concentration, such as a 90o fiber tow or large matrix pore, and grow over time. Such damage is difficult to detect through conventional techniques. Electrical resistance changes can be correlated with matrix cracking to provide a means of damage detection. Sylramic-iBN fiber-reinforced SiC composites with both melt infiltrated (MI) and chemical vapor infiltrated (CVI) matrix types are compared here. Results for both systems exhibit an increase in resistance prior to fracture, which can be detected either in situ or post-damage.

Microtexture Analysis and Modeling of Ambient Fatigue and Creep-Fatigue Damages in Ti-6Al-4V Alloy

NASA Astrophysics Data System (ADS)

Kumar, Jalaj; Singh, A. K.; Raman, S. Ganesh Sundara; Kumar, Vikas

2017-02-01

In the present investigation, microtexture analysis using electron back-scattered diffraction technique has been performed to study fatigue- and creep-fatigue damages and associated deformation structures in Ti-6Al-4V alloy. Special emphasis has been given to low-angle grain boundary configuration and its possible application as a damage indicator. Damage is mostly present in the form of voids as investigated through scanning electron microscopy. Stored deformation energies have been evaluated for the strain-controlled fatigue-, the stress-controlled fatigue-, and the creep-fatigue-tested samples. Stored deformation energies have also been analyzed vis-à-vis total damage energies to quantify the contribution of damages to various samples. A relation between the stored deformation energy and the applied strain amplitude has been proposed in this study.

Experimental and modeling results of creep fatigue life of Inconel 617 and Haynes 230 at 850 C

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, Xiang; Sokolov, Mikhail A; Sham, Sam

Creep fatigue testing of Ni-based superalloy Inconel 617 and Haynes 230 were conducted in the air at 850 C. Tests were performed with fully reversed axial strain control at a total strain range of 0.5%, 1.0% or 1.5% and hold time at maximum tensile strain for 3, 10 or 30 min. In addition, two creep fatigue life prediction methods, i.e. linear damage summation and frequency-modified tensile hysteresis energy modeling, were evaluated and compared with experimental results. Under all creep fatigue tests, Haynes 230 performed better than Inconel 617. Compared to the low cycle fatigue life, the cycles to failure formore » both materials decreased under creep fatigue test conditions. Longer hold time at maximum tensile strain would cause a further reduction in both material creep fatigue life. The linear damage summation could predict the creep fatigue life of Inconel 617 for limited test conditions, but considerably underestimated the creep fatigue life of Haynes 230. In contrast, frequency-modified tensile hysteresis energy modeling showed promising creep fatigue life prediction results for both materials.« less

Experimental and modeling results of creep-fatigue life of Inconel 617 and Haynes 230 at 850 °C

NASA Astrophysics Data System (ADS)

Chen, Xiang; Sokolov, Mikhail A.; Sham, Sam; Erdman, Donald L., III; Busby, Jeremy T.; Mo, Kun; Stubbins, James F.

2013-01-01

Creep-fatigue testing of Ni-based superalloy Inconel 617 and Haynes 230 were conducted in the air at 850 °C. Tests were performed with fully reversed axial strain control at a total strain range of 0.5%, 1.0% or 1.5% and hold time at maximum tensile strain for 3, 10 or 30 min. In addition, two creep-fatigue life prediction methods, i.e. linear damage summation and frequency-modified tensile hysteresis energy modeling, were evaluated and compared with experimental results. Under all creep-fatigue tests, Haynes 230 performed better than Inconel 617. Compared to the low cycle fatigue life, the cycles to failure for both materials decreased under creep-fatigue test conditions. Longer hold time at maximum tensile strain would cause a further reduction in both material creep-fatigue life. The linear damage summation could predict the creep-fatigue life of Inconel 617 for limited test conditions, but considerably underestimated the creep-fatigue life of Haynes 230. In contrast, frequency-modified tensile hysteresis energy modeling showed promising creep-fatigue life prediction results for both materials.

Irradiation creep due to SIPA under cascade damage conditions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Woo, C.H.; Garner, F.A.; Holt, R.A.

1992-12-31

This paper derives the relationships between void swelling and irradiation creep due to Stress-Induced Preferred Absorption (SIPA) and SIPA-Induced Growth (SIG) under cascade damage conditions in an irradiated pressurized tube. It is found that at low swelling rates irradiation creep is a major contribution to the total diametral strain rate of the tube, whereas at high swelling rates the creep becomes a minor contribution. The anisotropy of the corresponding dislocation structure is also predicted to decline as the swelling rate increases. The theoretical predictions are found to agree very well with experimental results.

Creep of trabecular bone from the human proximal tibia

PubMed Central

Novitskaya, Ekaterina; Zin, Carolyn; Chang, Neil; Cory, Esther; Chen, Peter; D'Lima, Darryl; Sah, Robert L.; McKittrick, Joanna

2014-01-01

Creep is the deformation that occurs under a prolonged, sustained load and can lead to permanent damage in bone. Creep in bone is a complex phenomenon and varies with type of loading and local mechanical properties. Human trabecular bone samples from proximal tibia were harvested from a 71-year old female cadaver with osteoporosis. The samples were initially subjected to one cycle load up to 1% strain to determine the creep load. Samples were then loaded in compression under a constant stress for two hours and immediately unloaded. All tests were conducted with the specimens soaked in phosphate buffered saline with proteinase inhibitors at 37°C. Steady state creep rate and final creep strain were estimated from mechanical testing and compared with published data. The steady state creep rate correlated well with values obtained from bovine tibial and human vertebral trabecular bone, and was higher for lower density samples. Tissue architecture was analyzed by micro-computed tomography (μCT) both before and after creep testing to assess creep deformation and damage accumulated. Quantitative morphometric analysis indicated that creep induced changes in trabecular separation and the structural model index. A main mode of deformation was bending of trabeculae. PMID:24857486

Creep behavior and in-depth microstructural characterization of dissimilar joints

PubMed Central

Kauffmann, F; Klein, T; Klenk, A; Maile, K

2013-01-01

The 700 °C power plants currently under development will utilize Ni-base alloys such as alloy 617 for components to be operated at temperatures >650 °C. Due to economic reasons for components or parts of components which are subjected to temperatures <650 °C, 2% Cr or 9–12% Cr steels is used, depending on the required mechanical properties. This makes the dissimilar joining of Ni-base alloys and Cr steels a necessity in these plants. Experimental investigations show that these joints have to be identified as weak points with regard to damage development under creep and creep-fatigue loading. The present investigation focuses on welds between the alloy 617 and 2% Cr steel. Under creep load the fracture occurs near the fusion line between the 2% Cr steel base metal and alloy 617 weld metal. To explain the reasons for this fracture location, the microstructure of this fusion line was investigated using TEM and FIB techniques after welding and after creep loading. The TEM investigations have shown a small zone in the weld metal near the fusion line exhibiting chromium depletion and clearly reduced amounts of chromium carbides, leading to a weakening of this zone. PMID:27877551

Creep Crack Initiation and Growth Behavior for Ni-Base Superalloys

NASA Astrophysics Data System (ADS)

Nagumo, Yoshiko; Yokobori, A. Toshimitsu, Jr.; Sugiura, Ryuji; Ozeki, Go; Matsuzaki, Takashi

The structural components which are used in high temperature gas turbines have various shapes which may cause the notch effect. Moreover, the site of stress concentration might have the heterogeneous microstructural distribution. Therefore, it is necessary to clarify the creep fracture mechanism for these materials in order to predict the life of creep fracture with high degree of accuracy. In this study, the creep crack growth tests were performed using in-situ observational testing machine with microscope to observe the creep damage formation and creep crack growth behavior. The materials used are polycrystalline Ni-base superalloy IN100 and directionally solidified Ni-base superalloy CM247LC which were developed for jet engine turbine blades and gas turbine blades in electric power plants, respectively. The microstructural observation of the test specimens was also conducted using FE-SEM/EBSD. Additionally, the analyses of two-dimensional elastic-plastic creep finite element using designed methods were conducted to understand the effect of microstructural distribution on creep damage formation. The experimental and analytical results showed that it is important to determine the creep crack initiation and early crack growth to predict the life of creep fracture and it is indicated that the highly accurate prediction of creep fracture life could be realized by measuring notch opening displacement proposed as the RNOD characteristic.

A Lattice-Misfit-Dependent Damage Model for Non-linear Damage Accumulations Under Monotonous Creep in Single Crystal Superalloys

NASA Astrophysics Data System (ADS)

le Graverend, J.-B.

2018-05-01

A lattice-misfit-dependent damage density function is developed to predict the non-linear accumulation of damage when a thermal jump from 1050 °C to 1200 °C is introduced somewhere in the creep life. Furthermore, a phenomenological model aimed at describing the evolution of the constrained lattice misfit during monotonous creep load is also formulated. The response of the lattice-misfit-dependent plasticity-coupled damage model is compared with the experimental results obtained at 140 and 160 MPa on the first generation Ni-based single crystal superalloy MC2. The comparison reveals that the damage model is well suited at 160 MPa and less at 140 MPa because the transfer of stress to the γ' phase occurs for stresses above 150 MPa which leads to larger variations and, therefore, larger effects of the constrained lattice misfit on the lifetime during thermo-mechanical loading.

Creep deformation and mechanisms in Haynes 230 at 800 °C and 900 °C

NASA Astrophysics Data System (ADS)

Pataky, Garrett J.; Sehitoglu, Huseyin; Maier, Hans J.

2013-11-01

Creep was studied in Haynes 230, a material candidate for the very high temperature reactor's intermediate heat exchanger, at 800 °C and 900 °C. This study focused on the differences between the behavior at the two elevated temperature, and using the microstructure, grain boundary serrations and triple junction strain concentrations were quantitatively identified. There was significant damage in the 900 °C samples and the creep was almost entirely tertiary. In contrast, the 800 °C sample exhibited secondary creep. Using an Arrhenius equation, the minimum creep rate exponents were found to be n ≈ 3 and n ≈ 5 for 900 °C and 800 °C, respectively. The creep mechanisms were identified as solute drag for n ≈ 3 and dislocation climb for n ≈ 5. Strain concentrations were identified at triple junctions and grain boundary serrations using high resolution digital image correlation overlaid on the microstructure. The grain boundary serrations restrict grain boundary sliding which may reduce the creep damage at triple junctions and extend the creep life of Haynes 230 at elevated temperatures.

Aseismic creep along the North Anatolian Fault quantified by coupling microstructural strain and chemical analyses

NASA Astrophysics Data System (ADS)

Kaduri, Maor; Gratier, Jean-Pierre; Renard, François; Çakir, Ziyadin; Lasserre, Cécile

2017-04-01

In the last decade aseismic creep has been noted as one of the key processes along tectonic plate boundaries. It contributes to the energy budget during the seismic cycle, delaying or triggering the occurrence of large earthquakes. Several major continental active faults show spatial alternation of creeping and locked segments. A great challenge is to understand which parameters control the transition from seismic to aseismic deformation in fault zones, such as the lithology, the degree of deformation from damage rocks to gouge, and the stress driven fault architecture transformations at all scales. The present study focuses on the North Anatolian Fault (Turkey) and characterizes the mechanisms responsible for the partition between seismic and aseismic deformation. Strain values were calculated using various methods, e.g. Fry, R-φs from microstructural measurements in gouge and damage samples collected on more than 30 outcrops along the fault. Maps of mineral composition were reconstructed from microprobe measurements of gouge and damage rock microstructure, in order to calculate the relative mass changes due to stress driven processes during deformation. Strain values were extracted, in addition to the geometrical properties of grain orientation and size distribution. Our data cover subsamples in the damage zones that were protected from deformation and are reminiscent of the host rock microstructure and composition, and subsamples that were highly deformed and recorded both seismic and aseismic deformations. Increase of strain value is linked to the evolution of the orientation of the grains from random to sheared sub-parallel and may be related to various parameters: (1) relative mass transfer increase with increasing strain indicating how stress driven mass transfer processes control aseismic creep evolution with time; (2) measured strain is strongly related with the initial lithology and with the evolution of mineral composition: monomineralic rocks are stronger (less deformed) than polymineralic ones; (3) strain measurements allow to evaluate the cumulated geological displacement accommodated by aseismic creep and the relative ratio between seismic and aseismic displacement for each section of an active fault. These relations allow to quantify more accurately the aseismic creep processes and their evolution with time along the North Anatolian Fault which are controlled by a superposition of two kinds of mechanisms: (1) stress driven mass transfer (pressure solution and metamorphism) that control local and regional mass transfer and associated rheology evolution and (2) grain boundary sliding along weak mineral interfaces (initially weak minerals or more often transformed by deformation-related reactions).

Effect of Creep and Oxidation on Reduced Creep-Fatigue life of Ni-based Alloy 617 at 850 C

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, Xiang; Yang, Zhiqing; Sokolov, Mikhail A

Low cycle fatigue (LCF) and creep fatigue testing of Ni-based alloy 617 was carried out at 850 C. Compared with its LCF life, the material s creep fatigue life decreases to different extents depending on test conditions. To elucidate the microstructure-fatigue property relationship for alloy 617 and the effect of creep and oxidation on its fatigue life, systematic microstructural investigations were carried out using scanning electron microscopy, energy-dispersive X-ray spectroscopy, and electron backscatter diffraction (EBSD). In LCF tests, as the total strain range increased, deformations concentrated near high angle grain boundaries (HAGBs). The strain hold period in the creep fatiguemore » tests introduced additional creep damage to the material, which revealed the detrimental effect of the strain hold time on the material fatigue life in two ways. First, the strain hold time enhanced the localized deformation near HAGBs, resulting in the promotion of intergranular cracking of alloy 617. Second, the strain hold time encouraged grain boundary sliding, which resulted in interior intergranular cracking of the material. Oxidation accelerated the initiation of intergranular cracking in alloy 617. In the crack propagation stage, if oxidation was promoted and the cyclic oxidation damage was greater than the fatigue damage, oxidation-assisted intergranular crack growth resulted in a significant reduction in the material s fatigue life.« less

DETERMINATION OF THE CREEP–FATIGUE INTERACTION DIAGRAM FOR ALLOY 617

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wright, J. K.; Carroll, L. J.; Sham, T. -L.

Alloy 617 is the leading candidate material for an intermediate heat exchanger for the very high temperature reactor. To evaluate the behavior of this material in the expected service conditions, creep-fatigue testing was performed. Testing has been performed primarily on a single heat of material at 850 and 950°C for total strain ranges of 0.3 to 1% and tensile hold times as long as 240 minutes. At 850°C, increases in the tensile hold duration degraded the creep fatigue resistance, at least to the investigated strain-controlled hold time of up to 60 minutes at the 0.3% strain range and 240 minutesmore » at the 1.0% strain range. At 950°C, the creep-fatigue cycles to failure becomes constant with increasing hold times, indicating saturation occurs at relatively short hold times. The creep and fatigue damage fractions have been calculated and plotted on a creep-fatigue interaction D-diagram. Results from earlier creep-fatigue tests at 800 and 1000°C on an additional heat of Alloy 617 are also plotted on the D-diagram. The methodology for calculating the damage fractions will be presented, and the effects of strain rate, strain range, temperature, hold time, and strain profile (i.e. holds in tension, compression or both) on the creep-fatigue damage will be explored.« less

Sandia/Stanford Unified Creep Plasticity Damage Model for ANSYS

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pierce, David M.; Vianco, Paul T.; Fossum, Arlo F.

2006-09-03

A unified creep plasticity (UCP) model was developed, based upon the time-dependent and time-independent deformation properties of the 95.5Sn-3.9Ag-0.6Cu (wt.%) soldier that were measured at Sandia. Then, a damage parameter, D, was added to the equation to develop the unified creep plasticity damage (UCPD) model. The parameter, D, was parameterized, using data obtained at Sandia from isothermal fatigue experiments on a double-lap shear test. The softwae was validated against a BGA solder joint exposed to thermal cycling. The UCPD model was put into the ANSYS finite element as a subroutine. So, the softwae is the subroutine for ANSYS 8.1.

Creep Life Prediction of Ceramic Components Using the Finite Element Based Integrated Design Program (CARES/Creep)

NASA Technical Reports Server (NTRS)

Jadaan, Osama M.; Powers, Lynn M.; Gyekenyesi, John P.

1997-01-01

The desirable properties of ceramics at high temperatures have generated interest in their use for structural applications such as in advanced turbine systems. Design lives for such systems can exceed 10,000 hours. Such long life requirements necessitate subjecting the components to relatively low stresses. The combination of high temperatures and low stresses typically places failure for monolithic ceramics in the creep regime. The objective of this work is to present a design methodology for predicting the lifetimes of structural components subjected to multiaxial creep loading. This methodology utilizes commercially available finite element packages and takes into account the time varying creep stress distributions (stress relaxation). In this methodology, the creep life of a component is divided into short time steps, during which, the stress and strain distributions are assumed constant. The damage, D, is calculated for each time step based on a modified Monkman-Grant creep rupture criterion. For components subjected to predominantly tensile loading, failure is assumed to occur when the normalized accumulated damage at any point in the component is greater than or equal to unity.

Integrated Design Software Predicts the Creep Life of Monolithic Ceramic Components

NASA Technical Reports Server (NTRS)

1996-01-01

Significant improvements in propulsion and power generation for the next century will require revolutionary advances in high-temperature materials and structural design. Advanced ceramics are candidate materials for these elevated-temperature applications. As design protocols emerge for these material systems, designers must be aware of several innate features, including the degrading ability of ceramics to carry sustained load. Usually, time-dependent failure in ceramics occurs because of two different, delayedfailure mechanisms: slow crack growth and creep rupture. Slow crack growth initiates at a preexisting flaw and continues until a critical crack length is reached, causing catastrophic failure. Creep rupture, on the other hand, occurs because of bulk damage in the material: void nucleation and coalescence that eventually leads to macrocracks which then propagate to failure. Successful application of advanced ceramics depends on proper characterization of material behavior and the use of an appropriate design methodology. The life of a ceramic component can be predicted with the NASA Lewis Research Center's Ceramics Analysis and Reliability Evaluation of Structures (CARES) integrated design programs. CARES/CREEP determines the expected life of a component under creep conditions, and CARES/LIFE predicts the component life due to fast fracture and subcritical crack growth. The previously developed CARES/LIFE program has been used in numerous industrial and Government applications.

Creep Life of Ceramic Components Using a Finite-Element-Based Integrated Design Program (CARES/CREEP)

NASA Technical Reports Server (NTRS)

Powers, L. M.; Jadaan, O. M.; Gyekenyesi, J. P.

1998-01-01

The desirable properties of ceramics at high temperatures have generated interest in their use for structural application such as in advanced turbine engine systems. Design lives for such systems can exceed 10,000 hours. The long life requirement necessitates subjecting the components to relatively low stresses. The combination of high temperatures and low stresses typically places failure for monolithic ceramics in the creep regime. The objective of this paper is to present a design methodology for predicting the lifetimes of structural components subjected to creep rupture conditions. This methodology utilizes commercially available finite element packages and takes into account the time-varying creep strain distributions (stress relaxation). The creep life, of a component is discretized into short time steps, during which the stress and strain distributions are assumed constant. The damage is calculated for each time step based on a modified Monkman-Grant creep rupture criterion. Failure is assumed to occur when the normalized accumulated damage at any point in the component is greater than or equal to unity. The corresponding time will be the creep rupture life for that component. Examples are chosen to demonstrate the Ceramics Analysis and Reliability Evaluation of Structures/CREEP (CARES/CREEP) integrated design program, which is written for the ANSYS finite element package. Depending on the component size and loading conditions, it was found that in real structures one of two competing failure modes (creep or slow crack growth) will dominate. Applications to benchmark problems and engine components are included.

Creep Life of Ceramic Components Using a Finite-Element-Based Integrated Design Program (CARES/CREEP)

NASA Technical Reports Server (NTRS)

Gyekenyesi, J. P.; Powers, L. M.; Jadaan, O. M.

1998-01-01

The desirable properties of ceramics at high temperatures have generated interest in their use for structural applications such as in advanced turbine systems. Design lives for such systems can exceed 10,000 hours. The long life requirement necessitates subjecting the components to relatively low stresses. The combination of high temperatures and low stresses typically places failure for monolithic ceramics in the creep regime. The objective of this paper is to present a design methodology for predicting the lifetimes of structural components subjected to creep rupture conditions. This methodology utilized commercially available finite element packages and takes into account the time-varying creep strain distributions (stress relaxation). The creep life of a component is discretized into short time steps, during which the stress and strain distributions are assumed constant. The damage is calculated for each time step based on a modified Monkman-Grant creep rupture criterion. Failure is assumed to occur when the normalized accumulated damage at any point in the component is greater than or equal to unity. The corresponding time will be the creep rupture life for that component. Examples are chosen to demonstrate the CARES/CREEP (Ceramics Analysis and Reliability Evaluation of Structures/CREEP) integrated design programs, which is written for the ANSYS finite element package. Depending on the component size and loading conditions, it was found that in real structures one of two competing failure modes (creep or slow crack growth) will dominate. Applications to benechmark problems and engine components are included.

Microstructural Characterization of Alloy 617 Crept into the Tertiary Regime

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lillo, Thomas Martin; Wright, Richard Neil

2015-07-01

The microstructure of Alloy 617 was characterized following creep tests interrupted at total creep strains ranging from 2-20%. A range of creep temperatures (750-1000oC) and initial creep stresses (10-145 MPa) produced creep test durations ranging from 1 to 5800 hours. Image analysis of optical photomicrographs on longitudinal sections of the gage length was used to document the fraction of creep porosity as a function of creep parameters. Creep porosity was negligible below tertiary creep strains of 10% and increased with tertiary creep strain, thereafter. For a given temperature and total creep strain, creep porosity increased with decreasing creep stress. Creepmore » porosity increased linearly with duration of the creep experiment. TEM performed on the gage sections did not reveal significant creep cavity formation on grain boundaries at the sub-micron level. It was concluded that the onset of tertiary creep did not result from creep cavitation and more likely arose due to the formation of low energy dislocation substructures with increasing tertiary strain.« less

Life Prediction Methodologies for Aerospace Materials Annual Report, 2003

DTIC Science & Technology

2003-06-01

peening parameters are obtained using a simplified model [Cao, et al .]. The solutions ultimately will need to be fine-tuned by simulating the...clamping stress and applied axial stress, identified from prior work [Hutson, et al .]. Accumulated damage on some samples was characterized using...defined using single fiber creep data [Wilson, et al .]. A two-level Mori-Tanaka model [Mori and Tanaka] has been used to define the effective

Progress Report on Long Hold Time Creep Fatigue of Alloy 617 at 850°C

DOE Office of Scientific and Technical Information (OSTI.GOV)

Carroll, Laura Jill

Alloy 617 is the leading candidate material for an intermediate heat exchanger for the very high temperature reactor. To evaluate the behavior of this material in the expected service conditions, strain-controlled cyclic tests that include long hold times up to 240 minutes at maximum tensile strain were conducted at 850°C. In terms of the total number of cycles to failure, the fatigue resistance decreased when a hold time was added at peak tensile strain. Increases in the tensile hold duration degraded the creep-fatigue resistance, at least to the investigated strain controlled hold time of up to 60 minutes at themore » 0.3% strain range and 240 minutes at the 1.0% strain range. The creep-fatigue deformation mode is considered relative to the lack of saturation, or continually decreasing number of cycles to failure with increasing hold times. Additionally, preliminary values from the 850°C creep-fatigue data are calculated for the creep-fatigue damage diagram and have higher values of creep damage than those from tests at 950°C.« less

Fatigue Behavior of a Third Generation PM Disk Superalloy

NASA Technical Reports Server (NTRS)

Gayda, John; Gabb, Timothy P.

2008-01-01

The fatigue behavior of a 3rd generation PM disk alloy, LSHR, was studied at 1300 F. Tensile, creep, and fatigue tests were run on smooth and notched (Kt = 2) bars under a variety of conditions. Analysis of smooth bar fatigue data, run under strain and load control with R ratios of 0 and -1, showed that a stress based Smith-Watson-Topper approach could collapse the data set. While the tensile and creep data showed substantial notch strengthening at 1300 F, the fatigue data showed a life deficit for the notch specimens. A viscoplastic finite element model, which accounted for stress relaxation at the notch tip, provided the best correlation between the notched and smooth bar behavior, although the fatigue data was not fully rationalized based on this simplified viscoplastic model of the stresses at the notch tip.Inclusion of a 90 sec dwell at peak load was found to dramatically decrease notch fatigue life. This result was shown to be consistent with a simple linear creep-fatigue damage rule, where creep damage dominated at low stresses and fatigue damage was more prevalent at higher stresses.

Long-term creep characterization of Gr. 91 steel by modified creep constitutive equations

NASA Astrophysics Data System (ADS)

Kim, Woo-Gon; Kim, Sung-Ho; Lee, Chan-Bock

2011-06-01

This paper focuses on the long-term creep characterization of Gr. 91 steel using creep constitutive equations. The models of three such equations, a combination of power-law form and omega model (CPO), a combination of exponential form and omega model (CEO), and a combination of logarithmic form and omega model (CLO), which are described as sum decaying primary creep and accelerating tertiary creep, are proposed. A series of creep rupture data was obtained through creep tests with various applied loads at 600 °C. On the basis of the creep data, a nonlinear least-square fitting (NLSF) analysis was carried out to provide the best fit with the experimental data in optimizing the parameter constants of an individual equation. The results of the NLSF analysis showed that in the lower stress regions of 160 MPa (σ/σys <0.65), the CEO model showed a match with the experimental creep data comparable to those of the CPO and CLO models; however, in the higher stress regions of 160 MPa (σ/σy > 0.65), the CPO model showed better agreement than the other two models. It was found that the CEO model was superior to the CPO and CLO models in the modeling of long-term creep curves. Using the CEO model, the long-term creep curves of Gr. 91 steel were numerically characterized, and its creep life was predicted accurately.

Damage Assessment of Creep Tested and Thermally Aged Udimet 520 Using Acousto-Ultrasonics

NASA Technical Reports Server (NTRS)

Gyekenyesi, Andrew L.; Kautz, Harold E.; Cao, Wei

2001-01-01

Due to elevated temperatures and excessive stresses, turbine components may experience creep behavior. As a result, it is desirable to monitor and assess the current condition of such components. This study employed the Acousto-Ultrasonics (AU) method in an effort to monitor the state of the material at various percentages of used up creep life in the nickel base alloy, Udimet 520. A stepped specimen (i.e., varying cross sectional area) was employed which allowed for a postmortem nondestructive evaluation (NDE) analysis of the various levels of used up life. The overall objectives here were two fold: First, a user friendly, graphical interface AU system was developed, and second the new AU system was applied as an NDE tool to assess distributed damage resulting from creep. The experimental results demonstrated that the AU method shows promise as an NDE tool capable of detecting material changes as a function of used up creep life. Furthermore, the changes in the AU parameters were mainly attributed to the case of combined load and elevated temperature (i.e., creep) and not simply because of a timed exposure at elevated temperature (i.e., heat treatment or thermal aging).

Creep and creep rupture of laminated graphite/epoxy composites. Ph.D. Thesis. Final Report, 1 Oct. 1979 - 30 Sep. 1980

NASA Technical Reports Server (NTRS)

Dillard, D. A.; Morris, D. H.; Brinson, H. F.

1981-01-01

An incremental numerical procedure based on lamination theory is developed to predict creep and creep rupture of general laminates. Existing unidirectional creep compliance and delayed failure data is used to develop analytical models for lamina response. The compliance model is based on a procedure proposed by Findley which incorporates the power law for creep into a nonlinear constitutive relationship. The matrix octahedral shear stress is assumed to control the stress interaction effect. A modified superposition principle is used to account for the varying stress level effect on the creep strain. The lamina failure model is based on a modification of the Tsai-Hill theory which includes the time dependent creep rupture strength. A linear cumulative damage law is used to monitor the remaining lifetime in each ply.

Fatigue creep damage at the cement-bone interface: an experimental and a micro-mechanical finite element study

PubMed Central

Waanders, Daan; Janssen, Dennis; Miller, Mark A.; Mann, Kenneth A.; Verdonschot, Nico

2009-01-01

The goal of this study was to quantify the micromechanics of the cement-bone interface under tensile fatigue loading using finite element analysis (FEA) and to understand the underlying mechanisms that play a role in the fatigue behavior of this interface. Laboratory cement-bone specimens were subjected to a tensile fatigue load, while local displacements and crack growth on the specimen's surface were monitored. FEA models were created from these specimens based upon micro-computed tomography data. To accurately model interfacial gaps at the interface between the bone and cement, a custom-written erosion algorithm was applied to the bone model. A fatigue load was simulated in the FEA models while monitoring the local displacements and crack propagation. The results showed the FEA models were able to capture the general experimental creep damage behavior and creep stages of the interface. Consistent with the experiments, the majority of the deformation took place at the contact interface. Additionally, the FEA models predicted fatigue crack patterns similar to experimental findings. Experimental surface cracks correlated moderately with FEA surface cracks (r2=0.43), but did not correlate with the simulated crack volume fraction (r2=0.06). Although there was no relationship between experimental surface cracks and experimental creep damage displacement (r2=0.07), there was a strong relationship between the FEA crack volume fraction and the FEA creep damage displacement (r2=0.76). This study shows the additional value of FEA of the cement-bone interface relative to experimental studies and can therefore be used to optimize its mechanical properties. PMID:19682690

Effects of Multiple Rejuvenation Cycles on Mechanical Properties and Microstructure of IN-738 Superalloy

NASA Astrophysics Data System (ADS)

Monti, Cosimo; Giorgetti, Alessandro; Tognarelli, Leonardo; Mastromatteo, Francesco

2018-05-01

The scope of this work is to show the effects of multiple applications of a rejuvenation treatment studied for IN-738 on both the microstructure and the mechanical properties of the creep-damaged superalloy and to check the recovery obtained after one and two rejuvenation cycles through creep and tensile tests, whose results will be compared with the performance of the virgin material. This work will show that this rejuvenation treatment is able to recover the microstructure of creep-damaged specimens after one and two applications and that the mechanical properties of the rejuvenated alloy are very similar to the virgin material even after two rejuvenation cycles.

Correlation Between Intercritical Heat-Affected Zone and Type IV Creep Damage Zone in Grade 91 Steel

NASA Astrophysics Data System (ADS)

Wang, Yiyu; Kannan, Rangasayee; Li, Leijun

2018-04-01

A soft zone in Cr-Mo steel weldments has been reported to accompany the infamous Type IV cracking, the highly localized creep damage in the heat-affected zone of creep-resistant steels. However, the microstructural features and formation mechanism of this soft zone are not well understood. In this study, using microhardness profiling and microstructural verification, the initial soft zone in the as-welded condition was identified to be located in the intercritical heat-affected zone of P91 steel weldments. It has a mixed structure, consisting of Cr-rich re-austenitized prior austenite grains and fine Cr-depleted, tempered martensite grains retained from the base metal. The presence of these further-tempered retained grains, originating from the base metal, is directly responsible for the hardness reduction of the identified soft zone in the as-welded condition. The identified soft zone exhibits a high location consistency at three thermal stages. Local chemistry analysis and thermodynamic calculation show that the lower chromium concentrations inside these retained grains thermodynamically decrease their potentials for austenitic transformation during welding. Heterogeneous grain growth is observed in the soft zone during postweld heat treatment. The mismatch of strengths between the weak Cr-depleted grains and strong Cr-rich grains enhances the creep damage. Local deformation of the weaker Cr-depleted grains accelerates the formation of creep cavities.

Modeling Creep-Fatigue-Environment Interactions in Steam Turbine Rotor Materials for Advanced Ultra-supercritical Coal Power Plants

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shen, Chen

2014-04-01

The goal of this project is to model creep-fatigue-environment interactions in steam turbine rotor materials for advanced ultra-supercritical (A-USC) coal power Alloy 282 plants, to develop and demonstrate computational algorithms for alloy property predictions, and to determine and model key mechanisms that contribute to the damages caused by creep-fatigue-environment interactions.

Relation of structure to mechanical properties of thin thoria dispersion strengthened nickel-chromium (TD-NiCr alloy sheet

NASA Technical Reports Server (NTRS)

Whittenberger, J. D.

1975-01-01

A study of the relation between structure and mechanical properties of thin TD-NiCr sheet indicated that the elevated temperature tensile, stress-rupture, and creep strength properties depend primarily on the grain aspect ratio and sheet thickness. In general, the strength properties increased with increasing grain aspect ratio and sheet thickness. Tensile testing revealed an absence of ductility at elevated temperatures. A threshold stress for creep appears to exist. Even small amounts of prior creep deformation at elevated temperatures can produce severe creep damage.

Creep and intergranular cracking of Ni-Cr-Fe-C in 360[degree]C argon

DOE Office of Scientific and Technical Information (OSTI.GOV)

Angeliu, T.M.; Was, G.S.

1994-06-01

The influence of carbon and chromium on the creep and intergranular (IG) cracking behavior of controlled-purity Ni-xCr-9Fe-yC alloys in 360 C argon was investigated using constant extension rate tension (CERT) and constant load tension (CLT) testing. The CERT test results at 360 C show that the degree of IG cracking increases with decreasing bulk chromium or carbon content. The CLT test results at 360 C and 430 C reveal that, as the amounts of chromium and carbon in solution decrease, the steady-state creep rate increases. The occurrence of severe IG cracking correlates with a high steady-state creep rate, suggesting thatmore » creep plays a role in the IG cracking behavior in argon at 360 C. The failure mode of IG cracking and the deformation mode of creep are coupled through the formation of grain boundary voids that interlink to form grain boundary cavities, resulting in eventual failure by IG cavitation and ductile overload of the remaining ligaments. Grain boundary sliding may be enhancing grain boundary cavitation by redistributing the stress from inclined to more perpendicular boundaries and concentrating stress at discontinuities for the boundaries oriented 45 deg with respect to the tensile axis. Additions of carbon or chromium, which reduce the creep rate over all stress levels, also reduce the amount of IG fracture in CERT experiments. A damage accumulation model was formulated and applied to CERT tests to determine whether creep damage during a CERT test controls failure. Results show that, while creep plays a significant role in CERT experiments, failure is likely controlled by ductile overload caused by reduction in area resulting from grain boundary void formation and interlinkage.« less

Progress Report on Alloy 617 Notched Specimen Testing

DOE Office of Scientific and Technical Information (OSTI.GOV)

McMurtrey, Michael David; Wright, Richard Neil; Lillo, Thomas Martin

Creep behavior of Alloy 617 has been extensively characterized to support the development of a draft Code Case to qualify Alloy 617 in Section III division 5 of the ASME Boiler and Pressure Vessel Code. This will allow use of Alloy 617 in construction of nuclear reactor components at elevated temperatures and longer periods of time (up to 950°C and 100,000 hours). Prior to actual use, additional concerns not considered in the ASME code need to be addressed. Code Cases are based largely on uniaxial testing of smooth gage specimens. In service conditions, components will generally be under multi axialmore » loading. There is also the concern of the behavior at discontinuities, such as threaded components. To address the concerns of multi axial creep behavior and at geometric discontinuities, notched specimens have been designed to create conditions representative of the states that service components experience. Two general notch geometries have been used for these series of tests: U notch and V notch specimens. The notches produce a tri axial stress state, though not uniform across the specimen. Characterization of the creep behavior of the U notch specimens and the creep rupture behavior of the V notch specimens provides a good approximation of the behavior expected of actual components. Preliminary testing and analysis have been completed and are reported in this document. This includes results from V notch specimens tested at 900°C and 800°C. Failure occurred in the smooth gage section of the specimen rather than at the root of the notch, though some damage was present at the root of the notch, where initial stress was highest. This indicates notch strengthening behavior in this material at these temperatures.« less

Creep Behavior of Passive Bovine Extraocular Muscle

PubMed Central

Yoo, Lawrence; Kim, Hansang; Shin, Andrew; Gupta, Vijay; Demer, Joseph L.

2011-01-01

This paper characterized bovine extraocular muscles (EOMs) using creep, which represents long-term stretching induced by a constant force. After preliminary optimization of testing conditions, 20 fresh EOM samples were subjected to four different loading rates of 1.67, 3.33, 8.33, and 16.67%/s, after which creep was observed for 1,500 s. A published quasilinear viscoelastic (QLV) relaxation function was transformed to a creep function that was compared with data. Repeatable creep was observed for each loading rate and was similar among all six anatomical EOMs. The mean creep coefficient after 1,500 seconds for a wide range of initial loading rates was at 1.37 ± 0.03 (standard deviation, SD). The creep function derived from the relaxation-based QLV model agreed with observed creep to within 2.7% following 16.67%/s ramp loading. Measured creep agrees closely with a derived QLV model of EOM relaxation, validating a previous QLV model for characterization of EOM biomechanics. PMID:22131809

Experimental Research on Creep Characteristics of Nansha Soft Soil

PubMed Central

Luo, Qingzi; Chen, Xiaoping

2014-01-01

A series of tests were performed to investigate the creep characteristics of soil in interactive marine and terrestrial deposit of Pearl River Delta. The secondary consolidation test results show that the influence of consolidation pressure on coefficient of secondary consolidation is conditional, which is decided by the consolidation state. The ratio of coefficient of secondary consolidation and coefficient of compressibility C a/C c is almost a constant, and the value is 0.03. In the shear-box test, the direct sheer creep failure of soil is mainly controlled by shear stress rather than the accumulation of shear strain. The triaxial creep features are closely associated with the drainage conditions, and consolidation can weaken the effect of creep. When the soft soil has triaxial creep damage, the strain rate will increase sharply. PMID:24526925

Experimental research on creep characteristics of Nansha soft soil.

PubMed

Luo, Qingzi; Chen, Xiaoping

2014-01-01

A series of tests were performed to investigate the creep characteristics of soil in interactive marine and terrestrial deposit of Pearl River Delta. The secondary consolidation test results show that the influence of consolidation pressure on coefficient of secondary consolidation is conditional, which is decided by the consolidation state. The ratio of coefficient of secondary consolidation and coefficient of compressibility (Ca/Cc) is almost a constant, and the value is 0.03. In the shear-box test, the direct sheer creep failure of soil is mainly controlled by shear stress rather than the accumulation of shear strain. The triaxial creep features are closely associated with the drainage conditions, and consolidation can weaken the effect of creep. When the soft soil has triaxial creep damage, the strain rate will increase sharply.

Characterization of Time-Dependent Behavior of Ramming Paste Used in an Aluminum Electrolysis Cell

NASA Astrophysics Data System (ADS)

Orangi, Sakineh; Picard, Donald; Alamdari, Houshang; Ziegler, Donald; Fafard, Mario

2015-12-01

A new methodology was proposed for the characterization of time-dependent behavior of materials in order to develop a constitutive model. The material used for the characterization was ramming paste, a porous material used in an aluminum electrolysis cell, which is baked in place under varying loads induced by the thermal expansion of other components of the cell. In order to develop a constitutive model representing the paste mechanical behavior, it was necessary to get some insight into its behavior using samples which had been baked at different temperatures ranging from 200 to 1000 °C. Creep stages, effect of testing temperature on the creep, creep-recovery, as well as nonlinear creep were observed for designing a constitutive law. Uniaxial creep-recovery tests were carried out at two temperatures on the baked paste: ambient and higher. Results showed that the shape of creep curves was similar to a typical creep; recovery happened and the creep was shown to be nonlinear. Those experimental observations and the identification of nonlinear parameters of developed constitutive model demonstrated that the baked paste experiences nonlinear viscoelastic-viscoplastic behavior at different temperatures.

Computational simulation of the creep-rupture process in filamentary composite materials

NASA Technical Reports Server (NTRS)

Slattery, Kerry T.; Hackett, Robert M.

1991-01-01

A computational simulation of the internal damage accumulation which causes the creep-rupture phenomenon in filamentary composite materials is developed. The creep-rupture process involves complex interactions between several damage mechanisms. A statistically-based computational simulation using a time-differencing approach is employed to model these progressive interactions. The finite element method is used to calculate the internal stresses. The fibers are modeled as a series of bar elements which are connected transversely by matrix elements. Flaws are distributed randomly throughout the elements in the model. Load is applied, and the properties of the individual elements are updated at the end of each time step as a function of the stress history. The simulation is continued until failure occurs. Several cases, with different initial flaw dispersions, are run to establish a statistical distribution of the time-to-failure. The calculations are performed on a supercomputer. The simulation results compare favorably with the results of creep-rupture experiments conducted at the Lawrence Livermore National Laboratory.

NASALife-Component Fatigue and Creep Life Prediction Program and Illustrative Examples

NASA Technical Reports Server (NTRS)

Murthy, Pappu L. N.; Mital, Subodh K.; Gyekenyesi, John Z.

2005-01-01

NASALife is a life prediction program for propulsion system components made of ceramic matrix composites (CMC) under cyclic thermo-mechanical loading and creep rupture conditions. Although, the primary focus was for CMC components the underlying methodologies are equally applicable to other material systems as well. The program references data for low cycle fatigue (LCF), creep rupture, and static material properties as part of the life prediction process. Multiaxial stresses are accommodated by Von Mises based methods and a Walker model is used to address mean stress effects. Varying loads are reduced by the Rainflow counting method. Lastly, damage due to cyclic loading (Miner s rule) and creep are combined to determine the total damage per mission and the number of missions the component can survive before failure are calculated. Illustration of code usage is provided through example problem of a CMC turbine stator vane made of melt-infiltrated, silicon carbide fiber-reinforced, silicon carbide matrix composite (MI SiC/SiC)

Constitutive modelling of creep in a long fiber random glass mat thermoplastic composite

NASA Astrophysics Data System (ADS)

Dasappa, Prasad

The primary objective of this proposed research is to characterize and model the creep behaviour of Glass Mat Thermoplastic (GMT) composites under thermo-mechanical loads. In addition, tensile testing has been performed to study the variability in mechanical properties. The thermo-physical properties of the polypropylene matrix including crystallinity level, transitions and the variation of the stiffness with temperature have also been determined. In this work, the creep of a long fibre GMT composite has been investigated for a relatively wide range of stresses from 5 to 80 MPa and temperatures from 25 to 90°C. The higher limit for stress is approximately 90% of the nominal tensile strength of the material. A Design of Experiments (ANOVA) statistical method was applied to determine the effects of stress and temperature in the random mat material which is known for wild experimental scatter. Two sets of creep tests were conducted. First, preliminary short-term creep tests consisting of 30 minutes creep followed by recovery were carried out over a wide range of stresses and temperatures. These tests were carried out to determine the linear viscoelastic region of the material. From these tests, the material was found to be linear viscoelastic up-to 20 MPa at room temperature and considerable non-linearities were observed with both stress and temperature. Using Time-Temperature superposition (TTS) a long term master curve for creep compliance for up-to 185 years at room temperature has been obtained. Further, viscoplastic strains were developed in these tests indicating the need for a non-linear viscoelastic viscoplastic constitutive model. The second set of creep tests was performed to develop a general non-linear viscoelastic viscoplastic constitutive model. Long term creep-recovery tests consisting of 1 day creep followed by recovery has been conducted over the stress range between 20 and 70 MPa at four temperatures: 25°C, 40°C, 60°C and 80°C. Findley's model, which is the reduced form of the Schapery non-linear viscoelastic model, was found to be sufficient to model the viscoelastic behaviour. The viscoplastic strains were modeled using the Zapas and Crissman viscoplastic model. A parameter estimation method which isolates the viscoelastic component from the viscoplastic part of the non-linear model has been developed. The non-linear parameters in the Findley's non-linear viscoelastic model have been found to be dependent on both stress and temperature and have been modeled as a product of functions of stress and temperature. The viscoplastic behaviour for temperatures up to 40°C was similar indicating similar damage mechanisms. Moreover, the development of viscoplastic strains at 20 and 30 MPa were similar over all the entire temperature range considered implying similar damage mechanisms. It is further recommended that the material should not be used at temperature greater than 60°C at stresses over 50 MPa. To further study the viscoplastic behaviour of continuous fibre glass mat thermoplastic composite at room temperature, multiple creep-recovery experiments of increasing durations between 1 and 24 hours have been conducted on a single specimen. The purpose of these tests was to experimentally and numerically decouple the viscoplastic strains from total creep response. This enabled the characterization of the evolution of viscoplastic strains as a function of time, stress and loading cycles and also to co-relate the development of viscoplastic strains with progression of failure mechanisms such as interfacial debonding and matrix cracking which were captured in-situ. A viscoplastic model developed from partial data analysis, as proposed by Nordin, had excellent agreement with experimental results for all stresses and times considered. Furthermore, the viscoplastic strain development is accelerated with increasing number of cycles at higher stress levels. These tests further validate the technique proposed for numerical separation of viscoplastic strains employed in obtaining the non-linear viscoelastic viscoplastic model parameters. These tests also indicate that the viscoelastic strains during creep are affected by the previous viscoplastic strain history. (Abstract shortened by UMI.)

Oxidation-Assisted Crack Growth in Single-Crystal Superalloys during Fatigue with Compressive Holds

NASA Astrophysics Data System (ADS)

Lafata, M. A.; Rettberg, L. H.; He, M. Y.; Pollock, T. M.

2018-01-01

The mechanism of oxidation-assisted growth of surface cracks during fatigue with compressive holds has been studied experimentally and via a model that describes the role of oxide and substrate properties. The creep-based finite element model has been employed to examine the role of material parameters in the damage evolution in a Ni-base single-crystal superalloy René N5. Low-cycle fatigue experiments with compressive holds were conducted at 1255 K and 1366 K (982 °C and 1093 °C). Interrupted and failed specimens were characterized for crack depth and spacing, oxide thickness, and microstructural evolution. Comparison of experimental to modeled hysteresis loops indicates that transient creep drives the macroscopic stress-strain response. Crack penetration rates are strongly influenced by growth stresses in the oxide, structural evolution in the substrate, and the development of γ ^' } denuded zones. Implications for design of alloys resistant to this mode of degradation are discussed.

Draft ASME Boiler and Pressure Vessel Code Section III, Division 5, Section HB, Subsection B, Code Case for Alloy 617 and Background Documentation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wright, Julie Knibloe

2015-08-01

Alloy 617 is the leading candidate material for an intermediate heat exchanger for the very high temperature reactor. To evaluate the behavior of this material in the expected service conditions, strain controlled cyclic tests that include long hold times up to 240 minutes at maximum tensile strain were conducted at 850°C. In terms of the total number of cycles to failure, the fatigue resistance decreased when a hold time was added at peak tensile strain. Increases in the tensile hold duration degraded the creep fatigue resistance, at least to the investigated strain controlled hold time of up to 60 minutesmore » at the 0.3% strain range and 240 minutes at the 1.0% strain range. The creep fatigue deformation mode is considered relative to the lack of saturation, or continually decreasing number of cycles to failure with increasing hold times. Additionally, preliminary values from the 850°C creep fatigue data are calculated for the creep fatigue damage diagram and have higher values of creep damage than those from tests at 950°C.« less

Creep analysis of silicone for podiatry applications.

PubMed

Janeiro-Arocas, Julia; Tarrío-Saavedra, Javier; López-Beceiro, Jorge; Naya, Salvador; López-Canosa, Adrián; Heredia-García, Nicolás; Artiaga, Ramón

2016-10-01

This work shows an effective methodology to characterize the creep-recovery behavior of silicones before their application in podiatry. The aim is to characterize, model and compare the creep-recovery properties of different types of silicone used in podiatry orthotics. Creep-recovery phenomena of silicones used in podiatry orthotics is characterized by dynamic mechanical analysis (DMA). Silicones provided by Herbitas are compared by observing their viscoelastic properties by Functional Data Analysis (FDA) and nonlinear regression. The relationship between strain and time is modeled by fixed and mixed effects nonlinear regression to compare easily and intuitively podiatry silicones. Functional ANOVA and Kohlrausch-Willians-Watts (KWW) model with fixed and mixed effects allows us to compare different silicones observing the values of fitting parameters and their physical meaning. The differences between silicones are related to the variations of breadth of creep-recovery time distribution and instantaneous deformation-permanent strain. Nevertheless, the mean creep-relaxation time is the same for all the studied silicones. Silicones used in palliative orthoses have higher instantaneous deformation-permanent strain and narrower creep-recovery distribution. The proposed methodology based on DMA, FDA and nonlinear regression is an useful tool to characterize and choose the proper silicone for each podiatry application according to their viscoelastic properties. Copyright © 2016 Elsevier Ltd. All rights reserved.

Report on FY15 Alloy 617 SMT Creep-Fatigue Test Results

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Yanli; Jetter, Robert I.; Baird, Seth T.

For the temperature range of 990-950C, Alloy 617 is a candidate IHX structural material for high temperature gas reactors (HTGRs) because of its high temperature creep properties. Also, its superior strength over a broad temperature range also offers advantages for certain component applications. In order for the designers to be able to use Alloy 617 for these high temperature components, Alloy 617 has to be approved for use in Section III (the nuclear section) of the ASME (American Society of Mechanical Engineers) Boiler and Pressure Vessel Code. A plan has been developed to propose a Code Case for use ofmore » Alloy 617 at elevated temperature in Section III of the ASME Code by September 2015. There has not been a new high temperature material approved for use in Section III for almost 20 years. The Alloy 617 Code Case effort would lead the way to establish a path for Code qualification of new high temperature materials of interest to other advanced SMRs. Creep-fatigue at elevated temperatures is the most damaging structural failure mode. In the past 40 years significant efforts have been devoted to the elevated temperature Code rule development in Section III, Subsection NH* of the ASME Boiler and Pressure Vessel Code, to ascertain conservative structural designs to prevent creep-fatigue failure. The current Subsection NH creep-fatigue procedure was established by the steps of (1) analytically obtaining a detailed stress-strain history, (2) comparing the stress and strain components to cyclic test results deconstructed into stress and strain quantities, and (3) recombining the results to obtain a damage function in the form of the so-called creep-fatigue damage-diagram. The deconstruction and recombination present difficulties in evaluation of test data and determination of cyclic damage in design. The uncertainties in these steps lead to the use of overly conservative design factors in the current creep-fatigue procedure. In addition, and of major significance to the viability of the Alloy 617 Code Case, the use of the current elastic analysis based rules in Subsection NH for the evaluation of strain limits (a precursor for the creep-fatigue rules) and the creep-fatigue rules themselves have been deemed inappropriate for Alloy 617 at temperatures above 650C (Corum and Brass, 1991). The rationale for this exclusion is that at higher temperatures it is not feasible to decouple plasticity and creep, which is the basis for the current simplified rules. This temperature, 650C, is well below the temperature range of interest for this material for the High Temperature Gas Cooled Reactor (HTGR) as well as the VHTR. The only current alternative is, thus, a full inelastic analysis which requires sophisticated material models which have not yet been formulated and verified. To address the prohibition on the use of current methods at very high temperatures, proposed Code rules have been developed which are based on the use of elastic-perfectly plastic (E-PP) analysis methods and which are expected to be applicable to very high temperatures. To provide data to implement the proposed rules and to verify their application, a series of tests have been initiated. One test concept, the Simplified Model Test (SMT), takes into account the stress and strain redistribution in real structures by including representative follow-up characteristics in the test specimen. The correlation parameter between test and design is the elastically calculated strain, and the dependent test variable is the observed cycles to failure. Although the initial priority for the SMT approach is to generate data to support validation of the E-PP Code Case for evaluation of creep-fatigue damage, the broader goal of the SMT approach is to develop a methodology for evaluation of creep fatigue damage which is simpler to implement than the current complex rules and applicable to the full temperature range from ambient conditions to the very high temperature creep regime of 900-950C. Also, guidance has been received from ASME Code committees that the proposed EPP methodology for evaluation of creep-fatigue damage should be extended to the other Subsection NH materials to the extent feasible. Thus, the scope of testing has been expanded to include SS304H and SS316H. This report describes the SMT approach and the development of testing capability to conduct SMT experiments on Alloy 617 and 304H and 316H and stainless steels. These SMT specimen data are also representative of component loading conditions and have been used as part of the verification of the proposed elastic-perfectly plastic Code Cases. Results from the SMT tests on both Alloy 617 and SS316H were compared to the predictions from the EPP Creep-Fatigue Code Case. Two different comparisons were made; one based on design life equal to the test duration and the other with an acceptable design life determined from the EPP Code Case procedure. The latter approach permits the determination of...« less

Slow crack growth versus creep cavity coalescence: Competing failure mechanisms during high-temperature deformation of advanced ceramics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jenkins, M.G.; Kohles, S.S.; Stevens, T.L.

1996-12-31

Duality of failure mechanisms (slow crack growth from pre-existing defects versus cumulative creep damage) is examined in a silicon nitride advanced ceramic recently tested at elevated-temperatures. Static (constant stress over time), dynamic (monotonically-increasing stress over time), and cyclic (fluctuating stress over time) fatigue behaviors were evaluated in tension in ambient air at temperatures of 1150, 1260, and 1370{degrees}C for a hot-isostatically pressed monolithic {beta}-silicon nitride. At 1150{degrees}C, all three types of fatigue results showed the similar failure mechanism of slow crack growth (SCG). At 1260 and 1370{degrees}C the failure mechanism was more complex. Failure under static fatigue was dominated bymore » the accumulation of creep damage via diffusion-controlled cavities. In dynamic fatigue, failure occurred by SCG at high stress rates (>10{sup {minus}2}MPa/s) and by creep damage at low stress rates ({le}10{sup {minus}2} MPa/s). For cyclic fatigue, such rate effects influenced the stress rupture results in which times to failure were greater for dynamic and cyclic fatigue than for static fatigue. Elucidation of failure mechanisms is necessary for accurate prediction of long-term survivability and reliability of structural ceramics.« less

The Application of Strain Range Partitioning Method to Torsional Creep-Fatigue Interaction

NASA Technical Reports Server (NTRS)

Zamrik, S. Y.

1975-01-01

The method of strain range partitioning was applied to a series of torsional fatigue tests conducted on tubular 304 stainless steel specimens at 1200 F. Creep strain was superimposed on cycling strain, and the resulting strain range was partitioned into four components; completely reversed plastic shear strain, plastic shear strain followed by creep strain, creep strain followed by plastic strain and completely reversed creep strain. Each strain component was related to the cyclic life of the material. The damaging effects of the individual strain components were expressed by a linear life fraction rule. The plastic shear strain component showed the least detrimental factor when compared to creep strain reversed by plastic strain. In the latter case, a reduction of torsional fatigue life in the order of magnitude of 1.5 was observed.

Damage-mitigating control of a reusable rocket engine for high performance and extended life

NASA Technical Reports Server (NTRS)

Ray, Asok; Dai, Xiaowen

1995-01-01

The goal of damage mitigating control in reusable rocket engines is to achieve high performance with increased durability of mechanical structures such that functional lives of the critical components are increased. The major benefit is an increase in structural durability with no significant loss of performance. This report investigates the feasibility of damage mitigating control of reusable rocket engines. Phenomenological models of creep and thermo-mechanical fatigue damage have been formulated in the state-variable setting such that these models can be combined with the plant model of a reusable rocket engine, such as the Space Shuttle Main Engine (SSME), for synthesizing an optimal control policy. Specifically, a creep damage model of the main thrust chamber wall is analytically derived based on the theories of sandwich beam and viscoplasticity. This model characterizes progressive bulging-out and incremental thinning of the coolant channel ligament leading to its eventual failure by tensile rupture. The objective is to generate a closed form solution of the wall thin-out phenomenon in real time where the ligament geometry is continuously updated to account for the resulting deformation. The results are in agreement with those obtained from the finite element analyses and experimental observation for both Oxygen Free High Conductivity (OFHC) copper and a copper-zerconium-silver alloy called NARloy-Z. Due to its computational efficiency, this damage model is suitable for on-line applications of life prediction and damage mitigating control, and also permits parametric studies for off-line synthesis of damage mitigating control systems. The results are presented to demonstrate the potential of life extension of reusable rocket engines via damage mitigating control. The control system has also been simulated on a testbed to observe how the damage at different critical points can be traded off without any significant loss of engine performance. The research work reported here is built upon concepts derived from the disciplines of Controls, Thermo-fluids, Structures, and Materials. The concept of damage mitigation, as presented in this report, is not restricted to control of rocket engines. It can be applied to any system where structural durability is an important issue.

Long-Term Creep and Creep Rupture Behavior of Woven Ceramic Matrix Composites

NASA Technical Reports Server (NTRS)

Haque, A.; Rahman, M.; Mach, A.; Jeelani, S.; Verrilli, Michael J. (Technical Monitor)

2001-01-01

Tensile creep behavior of SiC/SiNC ceramic matrix composites at elevated temperatures and at various stress levels have been investigated for turbine engine applications. The objective of this research is to present creep behavior of SiC/SiCN composites at stress levels above and below the monotonic proportional limit strength and predict the life at creep rupture conditions. Tensile creep-rupture tests were performed on an Instron 8502 servohydraulic testing machine at constant load conditions up to a temperature limit of 1000 C. Individual creep curves indicate three stages such as primary, secondary, and tertiary. The creep rate increased linearly at an early stage and then gradually became exponential at higher strains. The stress exponent and activation energy were also obtained at 700 and 1000 C. The specimen lifetime was observed to be 55 hrs at 121 MPa and at 700 C. The life span reduced to 35 hrs at 143 MPa and at 1000 C. Scanning electron microscopy observations revealed significant changes in the crystalline phases and creep damage development. Creep failures were accompanied by extensive fiber pullout, matrix cracking, and debonding along with fiber fracture. The creep data was applied to Time-Temperature-Stress superposition model and the Manson-Haferd parametric model for long-time life prediction.

Normalized coffin-manson plot in terms of a new life function based on stress relaxation under creep-fatigue conditions

NASA Astrophysics Data System (ADS)

Jeong, Chang Yeol; Nam, Soo Woo; Lim, Jong Dae

2003-04-01

A new life prediction function based on a model formulated in terms of stress relaxation during hold time under creep-fatigue conditions is proposed. From the idea that reduction in fatigue life with hold is due to the creep effect of stress relaxation that results in additional energy dissipation in the hysteresis loop, it is suggested that the relaxed stress range may be a creep-fatigue damage function. Creep-fatigue data from the present and other investigators are used to check the validity of the proposed life prediction equation. It is shown that the data satisfy the applicability of the life relation model. Accordingly, using this life prediction model, one may realize that all the Coffin-Manson plots at various levels of hold time in strain-controlled creep-fatigue tests can be normalized to make one straight line.

Effect of welding on creep damage evolution in P91B steel

NASA Astrophysics Data System (ADS)

Baral, J.; Swaminathan, J.; Chakrabarti, D.; Ghosh, R. N.

2017-07-01

Study of creep behavior of base metal (without weld) and welded specimens of P91B steel over a range of temperatures (600-650 °C) and stresses (50-180 MPa) showed similar values of minimum creep-rates for both specimens at higher stress regime (>100 MPa) whilst, significantly higher creep rates in the case of welded specimens at lower stress regime. Considering that welded specimen is comprised of two distinct structural regimes, i.e. weld affected zone and base metal, a method has been proposed for estimating the material parameters describing creep behavior of those regimes. Stress-strain distribution across welded specimen predicted from finite element analysis based on material parameters revealed preferential accumulation of stress and creep strain at the interface between weld zone and base metal. This is in-line with the experimental finding that creep rupture preferentially occurs at inter-critical heat affected zone in welded specimens owing to ferrite-martensite structure with coarse Cr23C6 particles.

Creep fatigue life prediction for engine hot section materials (isotropic)

NASA Technical Reports Server (NTRS)

Moreno, Vito; Nissley, David; Lin, Li-Sen Jim

1985-01-01

The first two years of a two-phase program aimed at improving the high temperature crack initiation life prediction technology for gas turbine hot section components are discussed. In Phase 1 (baseline) effort, low cycle fatigue (LCF) models, using a data base generated for a cast nickel base gas turbine hot section alloy (B1900+Hf), were evaluated for their ability to predict the crack initiation life for relevant creep-fatigue loading conditions and to define data required for determination of model constants. The variables included strain range and rate, mean strain, strain hold times and temperature. None of the models predicted all of the life trends within reasonable data requirements. A Cycle Damage Accumulation (CDA) was therefore developed which follows an exhaustion of material ductility approach. Material ductility is estimated based on observed similarities of deformation structure between fatigue, tensile and creep tests. The cycle damage function is based on total strain range, maximum stress and stress amplitude and includes both time independent and time dependent components. The CDA model accurately predicts all of the trends in creep-fatigue life with loading conditions. In addition, all of the CDA model constants are determinable from rapid cycle, fully reversed fatigue tests and monotonic tensile and/or creep data.

Viscoelastic Characterization of a Nonlinear, Glass/Epoxy Composite Including the Effects of Damage

DTIC Science & Technology

1974-10-01

weasure:;ient of theseu propeetLies di rec tly or inrdirctc ly [?, 9 18, 33, 16P]. T 73 In the subsections which follow we shall discuss some of the... Thesis , Texas A & M University, August 1973. 61. J. Kabelka and J. Vejchar, "Creep in Polyester Resin Laminates at Varying Temperatures," Kunstoff-Ger...J. Farris, "Applications of Viscoclasticity to Filled Materials," Master’s Thesis , University of Utah (1969). 130. A. E. Green, R. S. Rivlin and A. J

Simulated acid rain alters litter decomposition and enhances the allelopathic potential of the invasive plant Wedelia trilobata (Creeping Daisy)

USDA-ARS?s Scientific Manuscript database

Invasive species and acid rain cause global environmental problems. Limited information exists, however, concerning the effects of acid rain on the invasiveness of these plants. For example, creeping daisy, an invasive exotic allelopathic weed, has caused great damage in southern China where acid ra...

Irradiation creep of candidate materials for advanced nuclear plants

NASA Astrophysics Data System (ADS)

Chen, J.; Jung, P.; Hoffelner, W.

2013-10-01

In the present paper, irradiation creep results of an intermetallic TiAl alloy and two ferritic oxide dispersion strengthened (ODS) steels are summarized. In situ irradiation creep measurements were performed using homogeneous implantation with α- and p-particles to maximum doses of 0.8 dpa at displacement damage rates of 2-8 × 10-6 dpa/s. The strains of miniaturized flat dog-bone specimens were monitored under uniaxial tensile stresses ranging from 20 to 400 MPa at temperatures of 573, 673 and 773 K, respectively. The effects of material composition, ODS particle size, and bombarding particle on the irradiation creep compliance was studied and results are compared to literature data. Evolution of microstructure during helium implantation was investigated in detail by TEM and is discussed with respect to irradiation creep models.

Biomechanics of the Human Posterior Sclera: Age- and Glaucoma-Related Changes Measured Using Inflation Testing

PubMed Central

Coudrillier, Baptiste; Tian, Jing; Alexander, Stephen; Myers, Kristin M.; Quigley, Harry A.; Nguyen, Thao D.

2012-01-01

Purpose. The objective of this study was to measure the biomechanical response of the human posterior sclera in vitro and to estimate the effects of age and glaucoma. Methods. Scleral specimens from 22 donors with no history of glaucoma and 11 donors with a history of glaucoma were excised 3 mm posterior to the equator and affixed to an inflation chamber. Optic nerve cross-sections were graded to determine the presence of axon loss. The time-dependent inflation response was measured in a series of pressure-controlled load–unload tests to 30 mm Hg and creep tests to 15 and 30 mm Hg. Circumferential and meridional strains were computed from the digital image correlation displacements, and midposterior stresses were determined from pressure and deformed geometry. Results. Among normal specimens, older age was predictive of a stiffer response and a thinner sclera. In the age group 75 to 93, diagnosed glaucoma eyes with axon damage were thicker than normal eyes. Both damaged and undamaged glaucoma eyes had a different strain response in the peripapillary sclera characterized by a stiffer meridional response. Undamaged glaucoma eyes had slower circumferential creep rates in the peripapillary sclera than normal eyes. Glaucoma eyes were not different from normal eyes in stresses and strains in the midposterior sclera. Conclusions. The observed differences in the biomechanical response of normal and glaucoma sclera may represent baseline properties that contribute to axon damage, or may be characteristics that result from glaucomatous disease. PMID:22395883

Shear transformation zone activation during deformation in bulk metallic glasses characterized using a new indentation creep technique

Treesearch

J.B. Puthoff; H.B. Cao; Joseph E. Jakes; P.M. Voyles; D.S. Stone

2009-01-01

We have developed a novel type of nanoindentation creep experiment, called broadband nanoindentation creep (BNC), and used it to characterize the thermal activation of shear transformation zones (STZs) in three BMGs in the Zr-Cu-Al system. Using BNC, material hardness can be determined across a wide range of strain rates (10–4 to 10 s–...

Effect of Mechanical and Thermal Loading Histories on Residual Properties of SiCf/SiC Ceramic Matrix Composites

NASA Technical Reports Server (NTRS)

Almansour, Amjad; Kiser, Doug; Smith, Craig; Bhatt, Ram; Gorican, Dan; Phillips, Ron; McCue, Terry R.

2017-01-01

Silicon Carbide based Ceramic Matrix Composites (CMCs) are attractive materials for use in high-temperature structural applications in the aerospace and nuclear industries. Under high stresses and temperatures, creep degradation is the dominant damage mechanism in CMCs. Consequently, chemical vapor infiltration (CVI) SiCf/SiC ceramic matrix composites (CMC) incorporating SylramicTM-iBN SiC fibers coated with boron nitride (BN) interphase and CVI-SiC matrix were tested to examine creep behavior in air at a range of elevated temperatures of (2200 - 2700 F). Samples that survived creep tests were evaluated via RT fast fracture tensile tests to determine residual properties, with the use of acoustic emission (AE) to assess stress dependent damage initiation and progression. Microscopy of regions within the gage section of the tested specimens was performed. Observed material degradation mechanisms are discussed.

Observations on the relationship of structure to the mechanical properties of thin TD-NiCr sheet

NASA Technical Reports Server (NTRS)

Whittenberger, J. D.

1976-01-01

A study of the relationship between structure and mechanical properties of thin TD-NiCr sheet indicated that the elevated temperature tensile, stress-rupture, and creep strength properties are dependent on grain aspect ratio and sheet thickness. In general, the strength properties increase with increasing grain aspect ratio and sheet thickness. Tensile testing revealed an absence of ductility at elevated temperatures (not less than 1144 K). Significant creep damage as determined by subsequent tensile testing at room temperature occurs after very small amounts (less than 0.1%) of prior creep deformation over the temperature range 1144-1477 K. A threshold stress for creep appears to exist. Creep exposure below the threshold stress at T not less than 1366 K results in almost full retention of room temperature tensile properties.

Dynamic responses of concrete-filled steel tubular member under axial compression considering creep effect

NASA Astrophysics Data System (ADS)

Jiang, X. T.; Wang, Y. D.; Dai, C. H.; Ding, M.

2017-08-01

The finite element model of concrete-filled steel tubular member was established by the numerical analysis software considering material nonlinearity to analyze concrete creep effect on the dynamic responses of the member under axial compression and lateral impact. In the model, the constitutive model of core concrete is the plastic damage model, that of steel is the Von Mises yield criterion and kinematic hardening model, and the creep effect at different ages is equivalent to the change of concrete elastic modulus. Then the dynamic responses of concrete-filled steel tubular member considering creep effects was simulated, and the effects of creep on contact time, impact load, deflection, stress and strain were discussed. The fruits provide a scientific basis for the design of the impact resistance of concrete filled steel tubular members.

Creep-Fatigue Relationsihps in Electroactive Polymer Systems and Predicted Effects in an Actuator Design

NASA Technical Reports Server (NTRS)

Vinogradov, Aleksandra M.; Ihlefeld, Curtis M.; Henslee, Issac

2009-01-01

The paper concerns the time-dependent behavior of electroactive polymers (EAP) and their use in advanced intelligent structures for space exploration. Innovative actuator design for low weight and low power valves required in small plants planned for use on the moon for chemical analysis is discussed. It is shown that in-depth understanding of cyclic loading effects observed through accelerated creep rates due to creep-fatigue interaction in polymers is critical in terms of proper functioning of EAP based actuator devices. In the paper, an overview of experimental results concerning the creep properties and cyclic creep response of a thin film piezoelectric polymer polyvinylidene fluoride (PVDF) is presented. The development of a constitutive creep-fatigue interaction model to predict the durability and service life of electroactive polymers is discussed. A novel method is proposed to predict damage accumulation and fatigue life of polymers under oyclic loading conditions in the presence of creep. The study provides a basis for ongoing research initiatives at the NASA Kennedy Space Center in the pursuit of new technologies using EAP as active elements for lunar exploration systems.

Creep-Fatigue Interaction and Cyclic Strain Analysis in P92 Steel Based on Test

NASA Astrophysics Data System (ADS)

Ji, Dongmei; Zhang, Lai-Chang; Ren, Jianxing; Wang, Dexian

2015-04-01

This work focused on the interaction of creep and fatigue and cyclic strain analysis in high-chromium ferritic P92 steel based on load-controlled creep-fatigue (CF) tests and conventional creep test at 873 K. Mechanical testing shows that the cyclic load inhibits the propagation of creep damage in the P92 steel and CF interaction becomes more severe with the decrease in the holding period duration and stress ratio. These results are also verified by the analysis of cyclic strain. The fatigue lifetime reduces with the increasing of the holding period duration and it does not reduce much with the increasing stress ratio especially under the conditions of long holding period duration. The cyclic strains (i.e., the strain range and creep strain) of CF tests consist of three stages, which is the same as those for the conventional creep behavior. The microscopic fracture surface observations illustrated that two different kinds of voids are observed at the fracture surfaces and Laves phase precipitates at the bottom of the voids.

Creep and fracture of a model yoghurt

NASA Astrophysics Data System (ADS)

Manneville, Sebastien; Leocmach, Mathieu; Perge, Christophe; Divoux, Thibaut

2014-11-01

Biomaterials such as protein or polysaccharide gels are known to behave qualitatively as soft solids and to rupture under an external load. Combining optical and ultrasonic imaging to shear rheology we show that the failure scenario of a model yoghurt, namely a casein gel, is reminiscent of brittle solids: after a primary creep regime characterized by a macroscopically homogeneous deformation and a power-law behavior which exponent is fully accounted for by linear viscoelasticity, fractures nucleate and grow logarithmically perpendicularly to shear, up to the sudden rupture of the gel. A single equation accounting for those two successive processes nicely captures the full rheological response. The failure time follows a decreasing power-law with the applied shear stress, similar to the Basquin law of fatigue for solids. These results are in excellent agreement with recent fiber-bundle models that include damage accumulation on elastic fibers and exemplify protein gels as model, brittle-like soft solids. Work funded by the European Research Council under Grant Agreement No. 258803.

Detection and quantification of creep strain using process compensated resonance testing (PCRT) sorting modules trained with modeled resonance spectra

NASA Astrophysics Data System (ADS)

Heffernan, Julieanne; Biedermann, Eric; Mayes, Alexander; Livings, Richard; Jauriqui, Leanne; Goodlet, Brent; Aldrin, John C.; Mazdiyasni, Siamack

2018-04-01

Process Compensated Resonant Testing (PCRT) is a full-body nondestructive testing (NDT) method that measures the resonance frequencies of a part and correlates them to the part's material and/or damage state. PCRT testing is used in the automotive, aerospace, and power generation industries via automated PASS/FAIL inspections to distinguish parts with nominal process variation from those with the defect(s) of interest. Traditional PCRT tests are created through the statistical analysis of populations of "good" and "bad" parts. However, gathering a statistically significant number of parts can be costly and time-consuming, and the availability of defective parts may be limited. This work uses virtual databases of good and bad parts to create two targeted PCRT inspections for single crystal (SX) nickel-based superalloy turbine blades. Using finite element (FE) models, populations were modeled to include variations in geometric dimensions, material properties, crystallographic orientation, and creep damage. Model results were verified by comparing the frequency variation in the modeled populations with the measured frequency variations of several physical blade populations. Additionally, creep modeling results were verified through the experimental evaluation of coupon geometries. A virtual database of resonance spectra was created from the model data. The virtual database was used to create PCRT inspections to detect crystallographic defects and creep strain. Quantification of creep strain values using the PCRT inspection results was also demonstrated.

Effect of PVA fiber content on creep property of fiber reinforced high-strength concrete columns

NASA Astrophysics Data System (ADS)

Xu, Zongnan; Wang, Tao; Wang, Weilun

2018-04-01

The effect of PVA (polyvinyl alcohol) fiber content on the creep property of fiber reinforced high-strength concrete columns was investigated. The correction factor of PVA fiber content was proposed and the creep prediction model of ACI209 was modified. Controlling the concrete strength as C80, changing the content of PVA fiber (volume fraction 0%, 0.25%, 0.5%, 1% respectively), the creep experiment of PVA fiber reinforced concrete columns was carried out, the creep coefficient of each specimen was calculated to characterize the creep property. The influence of PVA fiber content on the creep property was analyzed based on the creep coefficient and the calculation results of several frequently used creep prediction models. The correction factor of PVA fiber content was proposed to modify the ACI209 creep prediction model.

A thermodynamic approach to nonlinear ultrasonics for material state awareness and prognosis

NASA Astrophysics Data System (ADS)

Chillara, Vamshi Krishna

2017-11-01

We develop a thermodynamic framework for modeling nonlinear ultrasonic damage sensing and prognosis in materials undergoing progressive damage. The framework is based on the internal variable approach and relies on the construction of a pseudo-elastic strain energy function that captures the energetics associated with the damage progression. The pseudo-elastic strain energy function is composed of two energy functions—one that describes how a material stores energy in an elastic fashion and the other describes how material dissipates energy or stores it in an inelastic fashion. Experimental motivation for the choice of the above two functionals is discussed and some specific choices pertaining to damage progression during fatigue and creep are presented. The thermodynamic framework is employed to model the nonlinear response of material undergoing stress relaxation and creep-like degradation. For each of the above cases, evolution of the nonlinearity parameter with damage as well as with macroscopic measurables like accumulated plastic strain is obtained.

Ultrasonic characterization of engineering performanace of oriented strandboard

NASA Astrophysics Data System (ADS)

Vun, Ronnie Yunheu

Direct-contact (DC) and non-contact (NC) ultrasonic transmission (UT) methods were developed to characterize the structural performance of oriented strandboard (OSB). The UT variable velocity was shown to be sensitive to the physical impediments caused by flake interfacial boundaries and embedded voids. Both attenuation and root mean square (RMS) voltage were good indicators of the "zero void" densification level for OSB, a point of the greatest transmissivity of the stress wave energy. For both DC and NC methods, the predicted densities of the model were validated for spatial distribution over each OSB type. Based on the control limits of +/-10% of the panel average density, density prediction improved with higher resin content (RC) and higher nominal density (ND) levels. From the out-of-limits plots, the predicted in-situ densities produced a reasonably spatial coherence to the measured values. All panels made with ND 0.60 g/cm3 or greater conformed well within the limits, with declining conformity towards lower RC panels. For each composite type made of different particle sizes, the equilibrium moisture content showed a decreasing trend toward smaller particle panels. The attenuation and RMS were good indicators for moisture change and densification level for each composite type. The velocity, sensitive to physical resistance of particle sizes, increased with increasing IB strength and sample density, manifesting the positive influence of layering, resin content, and the negative effect of bark as a constituent. The results of the creep rupture tests on commercial OSB using an acoustic emission (AE) technique indicated that the cumulative AE event count parameter was highly correlated with deflection parameter and appropriately represented the accumulation of incipient damage. Under high stress levels, specimens with high moisture content (MC) sustained the worse damages having the shortest creep rupture time followed by specimens with dynamically rising MC. Defects on the compression-side of the bending specimen were found critical to creep rupture than those on the tension-side. The in-plane fracture patterns tended to follow the defect trenches of low-density valleys, and worsened with greater variability of the horizontal density, indicating the need to measure and control the horizontal density variation within reasonable limits.

Nondestructive Evaluation Approaches Developed for Material Characterization in Aeronautics and Space Applications

NASA Technical Reports Server (NTRS)

Baaklini, George Y.; Kautz, Harold E.; Gyekenyesi, Andrew L.; Abdul-Aziz, Ali; Martin, Richard E.

2001-01-01

At the NASA Glenn Research Center, nondestructive evaluation (NDE) approaches were developed or tailored for characterizing advanced material systems. The emphasis was on high-temperature aerospace propulsion applications. The material systems included monolithic ceramics, superalloys, and high-temperature composites. In the aeronautics area, the major applications were cooled ceramic plate structures for turbine applications, gamma-TiAl blade materials for low-pressure turbines, thermoelastic stress analysis for residual stress measurements in titanium-based and nickel-based engine materials, and acousto-ultrasonics for creep damage assessment in nickel-based alloys. In the space area, applications consisted of cooled carbon-carbon composites for gas generator combustors and flywheel rotors composed of carbon-fiber-reinforced polymer matrix composites for energy storage on the International Space Station.

Creep-rupture of polymer-matrix composites. [graphite-epoxy laminates

NASA Technical Reports Server (NTRS)

Brinson, H. F.; Griffith, W. I.; Morris, D. H.

1980-01-01

An accelerated characterization method for resin matrix composites is reviewed. Methods for determining modulus and strength master curves are given. Creep rupture analytical models are discussed as applied to polymers and polymer matrix composites. Comparisons between creep rupture experiments and analytical models are presented. The time dependent creep rupture process in graphite epoxy laminates is examined as a function of temperature and stress level.

A new uniformly valid asymptotic integration algorithm for elasto-plastic creep and unified viscoplastic theories including continuum damage

NASA Technical Reports Server (NTRS)

Chulya, Abhisak; Walker, Kevin P.

1991-01-01

A new scheme to integrate a system of stiff differential equations for both the elasto-plastic creep and the unified viscoplastic theories is presented. The method has high stability, allows large time increments, and is implicit and iterative. It is suitable for use with continuum damage theories. The scheme was incorporated into MARC, a commercial finite element code through a user subroutine called HYPELA. Results from numerical problems under complex loading histories are presented for both small and large scale analysis. To demonstrate the scheme's accuracy and efficiency, comparisons to a self-adaptive forward Euler method are made.

Creep fatigue life prediction for engine hot section materials (isotropic): Fourth year progress review

NASA Technical Reports Server (NTRS)

Nelson, Richard S.; Schoendorf, John F.

1986-01-01

As gas turbine technology continues to advance, the need for advanced life prediction methods for hot section components is becoming more and more evident. The complex local strain and temperature histories at critical locations must be accurately interpreted to account for the effects of various damage mechanisms (such as fatigue, creep, and oxidation) and their possible interactions. As part of the overall NASA HOST effort, this program is designed to investigate these fundamental damage processes, identify modeling strategies, and develop practical models which can be used to guide the early design and development of new engines and to increase the durability of existing engines.

A new uniformly valid asymptotic integration algorithm for elasto-plastic-creep and unified viscoplastic theories including continuum damage

NASA Technical Reports Server (NTRS)

Chulya, A.; Walker, K. P.

1989-01-01

A new scheme to integrate a system of stiff differential equations for both the elasto-plastic creep and the unified viscoplastic theories is presented. The method has high stability, allows large time increments, and is implicit and iterative. It is suitable for use with continuum damage theories. The scheme was incorporated into MARC, a commercial finite element code through a user subroutine called HYPELA. Results from numerical problems under complex loading histories are presented for both small and large scale analysis. To demonstrate the scheme's accuracy and efficiency, comparisons to a self-adaptive forward Euler method are made.

Crack initiation modeling of a directionally-solidified nickel-base superalloy

NASA Astrophysics Data System (ADS)

Gordon, Ali Page

Combustion gas turbine components designed for application in electric power generation equipment are subject to periodic replacement as a result of cracking, damage, and mechanical property degeneration that render them unsafe for continued operation. In view of the significant costs associated with inspecting, servicing, and replacing damaged components, there has been much interest in developing models that not only predict service life, but also estimate the evolved microstructural state of the material. This thesis explains manifestations of microstructural damage mechanisms that facilitate fatigue crack nucleation in a newly-developed directionally-solidified (DS) Ni-base superalloy components exposed to elevated temperatures and high stresses. In this study, models were developed and validated for damage and life prediction using DS GTD-111 as the subject material. This material, proprietary to General Electric Energy, has a chemical composition and grain structure designed to withstand creep damage occurring in the first and second stage blades of gas-powered turbines. The service conditions in these components, which generally exceed 600°C, facilitate the onset of one or more damage mechanisms related to fatigue, creep, or environment. The study was divided into an empirical phase, which consisted of experimentally simulating service conditions in fatigue specimens, and a modeling phase, which entailed numerically simulating the stress-strain response of the material. Experiments have been carried out to simulate a variety of thermal, mechanical, and environmental operating conditions endured by longitudinally (L) and transversely (T) oriented DS GTD-111. Both in-phase and out-of-phase thermo-mechanical fatigue tests were conducted. In some cases, tests in extreme environments/temperatures were needed to isolate one or at most two of the mechanisms causing damage. Microstructural examinations were carried out via SEM and optical microscopy. A continuum crystal plasticity model was used to simulate the material behavior in the L and T orientations. The constitutive model was implemented in ABAQUS and a parameter estimation scheme was developed to obtain the material constants. A physically-based model was developed for correlating crack initiation life based on the experimental life data and predictions are made using the crack initiation model. Assuming a unique relationship between the damage fraction and cycle fraction with respect to cycles to crack initiation for each damage mode, the total crack initiation life has been represented in terms of the individual damage components (fatigue, creep-fatigue, creep, and oxidation-fatigue) observed at the end state of crack initiation.

Experimental characterization and numerical modelling of polymeric film damage, constituting the stratospheric super pressurized balloons

NASA Astrophysics Data System (ADS)

Chaabane, Makram; Chaabane, Makram; Dalverny, Olivier; Deramecourt, Arnaud; Mistou, Sébastien

The super-pressure balloons developed by CNES are a great challenge in scientific ballooning. Whatever the balloon type considered (spherical, pumpkin...), it is necessary to have good knowledge of the mechanical behavior of the envelope regarding to the flight level and the lifespan of the balloon. It appears during the working stages of the super pressure balloons that these last can exploded prematurely in the course of the first hours of flight. For this reason CNES and LGP are carrying out research programs about experimentations and modelling in order to predict a good stability of the balloons flight and guarantee a life time in adequacy with the technical requirement. This study deals with multilayered polymeric film damage which induce balloons failure. These experimental and numerical study aims, are a better understanding and predicting of the damage mechanisms bringing the premature explosion of balloons. The following damages phenomena have different origins. The firsts are simple and triple wrinkles owed during the process and the stocking stages of the balloons. The second damage phenomenon is associated to the creep of the polymeric film during the flight of the balloon. The first experimental results we present in this paper, concern the mechanical characterization of three different damage phenomena. The severe damage induced by the wrinkles of the film involves a significant loss of mechanical properties. In a second part the theoretical study, concerns the choice and the development of a non linear viscoelastic coupled damage behavior model in a finite element code.

Low-Temperature Fault Creep: Strong vs. Weak, Steady vs. Episodic

NASA Astrophysics Data System (ADS)

Wang, K.; Gao, X.

2017-12-01

Unless we understand how faults creep, we do not fully understand how they produce earthquakes. However, most of the physics and geology of low-temperature creep is not known. There are two end-member types of low-temperature creep: weak creep of smooth faults and strong creep of rough faults, with a spectrum of intermediate modes in between. Most conceptual and numerical models deal with weak creep, assuming a very smooth fault with a gouge typically weakened by hydrous minerals (Harris, 2017). Less understood is strong creep. For subduction zones, strong creep appears to be common and is often associated with the subduction of large geometrical irregularities such as seamounts and aseismic ridges (Wang and Bilek, 2014). These irregularities generate fracture systems as they push against the resistance of brittle rocks. The resultant heterogeneous stress and structural environment makes it very difficult to lock the fault. The geodetically observed creep under such conditions is accomplished by the complex deformation of a 3D damage zone. Strong-creeping faults dissipate more heat than faults that produce great earthquakes (Gao and Wang, 2014). Although an integrated frictional strength of the fault is still a useful concept, the creeping mechanism is very different from frictional slip of a velocity-strengthening smooth fault. Cataclasis and pressure-solution creep in the fracture systems must be important processes in strong creep. Strong creep is necessarily non-steady and produces small and medium earthquakes. Strong creep of a megathrust can also promote the occurrence of a very special type of weak creep - episodic slow slip around the mantle wedge corner accompanied with tremor (ETS). An example is Hikurangi, where strong creep causes the frictional-viscous transition along the plate interface to occur much shallower than the mantle wedge corner, a necessary condition for ETS (Gao and Wang, 2017). Gao and Wang (2014), Strength of stick-slip and creeping subduction megathrusts from heat flow observations, Science. Gao and Wang (2017), Rheological separation of the megathrust seismogenic zone and Episodic Tremor and Slip, Nature. Harris (2017), Large earthquakes and creeping faults, Rev. Geophys. Wang and Bilek (2014), Fault creep caused by subduction of rough seafloor relief, Tectonophysics.

Monitoring microstructural evolution of alloy 617 with non-linear acoustics for remaining useful life prediction; multiaxial creep-fatigue and creep-ratcheting

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lissenden, Cliff; Hassan, Tasnin; Rangari, Vijaya

The research built upon a prior investigation to develop a unified constitutive model for design-­by-­analysis of the intermediate heat exchanger (IHX) for a very high temperature reactor (VHTR) design of next generation nuclear plants (NGNPs). Model development requires a set of failure data from complex mechanical experiments to characterize the material behavior. Therefore uniaxial and multiaxial creep-­fatigue and creep-­ratcheting tests were conducted on the nickel-­base Alloy 617 at 850 and 950°C. The time dependence of material behavior, and the interaction of time dependent behavior (e.g., creep) with ratcheting, which is an increase in the cyclic mean strain under load-­controlled cycling,more » are major concerns for NGNP design. This research project aimed at characterizing the microstructure evolution mechanisms activated in Alloy 617 by mechanical loading and dwell times at elevated temperature. The acoustic harmonic generation method was researched for microstructural characterization. It is a nonlinear acoustics method with excellent potential for nondestructive evaluation, and even online continuous monitoring once high temperature sensors become available. It is unique because it has the ability to quantitatively characterize microstructural features well before macroscale defects (e.g., cracks) form. The nonlinear acoustics beta parameter was shown to correlate with microstructural evolution using a systematic approach to handle the complexity of multiaxial creep-­fatigue and creep-­ratcheting deformation. Mechanical testing was conducted to provide a full spectrum of data for: thermal aging, tensile creep, uniaxial fatigue, uniaxial creep-­fatigue, uniaxial creep-ratcheting, multiaxial creep-fatigue, and multiaxial creep-­ratcheting. Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM), and Optical Microscopy were conducted to correlate the beta parameter with individual microstructure mechanisms. We researched application of the harmonic generation method to tubular mechanical test specimens and pipes for nondestructive evaluation. Tubular specimens and pipes act as waveguides, thus we applied the acoustic harmonic generation method to guided waves in both plates and shells. Magnetostrictive transducers were used to generate and receive guided wave modes in the shell sample and the received signals were processed to show the sensitivity of higher harmonic generation to microstructure evolution. Modeling was initiated to correlate higher harmonic generation with the microstructure that will lead to development of a life prediction model that is informed by the nonlinear acoustics measurements.« less

Time-dependent brittle deformation (creep) at Mt. Etna volcano

NASA Astrophysics Data System (ADS)

Heap, M. J.; Baud, P.; Meredith, P. G.; Vinciguerra, S.; Bell, A. F.; Main, I. G.

2009-04-01

Mt. Etna is the largest and most active volcano in Europe. Time-dependent weakening mechanisms, leading to slow fracturing, have been shown to act during pre-eruptive patterns of flank eruptions at Mt. Etna volcano. Due to the high permeability of its volcanic rocks, the volcanic edifice hosts one of the biggest hydrogeologic reservoirs of Sicily (Ogniben, 1966). The presence of a fluid phase in cracks within rock has been shown to dramatically affect both mechanical and chemical interactions. Chemically, it promotes time-dependent brittle deformation through such mechanisms as stress corrosion cracking that allows rocks to deform at stresses far below their short-term failure strength. Such crack growth is highly non-linear and accelerates towards dynamic failure over extended periods of time, even under constant applied stress; a phenomenon known as ‘brittle creep'. Here we report results from a study of time-dependent brittle creep in water-saturated samples of Etna basalt (EB) under triaxial stress conditions (confining pressure of 50 MPa and pore fluid pressure of 20 MPa). Samples of EB were loaded at a constant strain rate of 10-5 s-1 to a pre-determined percentage of the short-term strength and left to deform under constant stress until failure. Crack damage evolution was monitored throughout each experiment by measuring the independent damage proxies of axial strain, pore volume change and output of acoustic emission (AE) energy, during brittle creep of creep strain rates ranging over four orders of magnitude. Our data not only demonstrates that basalt creeps in the brittle regime but also that the applied differential stress exerts a crucial influence on both time-to-failure and creep strain rate in EB. Furthermore, stress corrosion is considered to be responsible for the acceleratory cracking and seismicity prior to volcanic eruptions and is invoked as an important mechanism in forecasting models. Stress-stepping creep experiments were then performed to allow the influence of the effective confining stress to be studied in detail. Experiments were performed under effective stress conditions of 10, 30 and 50 MPa (whilst maintaining a constant pore fluid pressure of 20 MPa). In addition to the purely mechanical influence of water, governed by the effective stress, which results in a shift of the creep strain rate curves to lower strain rates at higher effective stresses. Our results also demonstrate that the chemically-driven process of stress corrosion cracking appears to be inhibited at higher effective stress. This results in an increase in the gradient of the creep strain rate curves with increasing effective stress. We suggest that the most likely cause of this change is a decrease in water mobility due to a reduction in crack aperture and an increase in water viscosity at higher pressure. Finally, we show that a theoretical model based on mean-field damage mechanics creep laws is able to reproduce the experimental strain-time relations. Our results indicate that the local changes in the stress field and fluid circulation can have a profound impact in the time-to-failure properties of the basaltic volcanic pile.

Irradiation Creep in Graphite

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ubic, Rick; Butt, Darryl; Windes, William

2014-03-13

An understanding of the underlying mechanisms of irradiation creep in graphite material is required to correctly interpret experimental data, explain micromechanical modeling results, and predict whole-core behavior. This project will focus on experimental microscopic data to demonstrate the mechanism of irradiation creep. High-resolution transmission electron microscopy should be able to image both the dislocations in graphite and the irradiation-induced interstitial clusters that pin those dislocations. The team will first prepare and characterize nanoscale samples of virgin nuclear graphite in a transmission electron microscope. Additional samples will be irradiated to varying degrees at the Advanced Test Reactor (ATR) facility and similarlymore » characterized. Researchers will record microstructures and crystal defects and suggest a mechanism for irradiation creep based on the results. In addition, the purchase of a tensile holder for a transmission electron microscope will allow, for the first time, in situ observation of creep behavior on the microstructure and crystallographic defects.« less

Low cycle fatigue of PM/HIP astroloy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Choe, S.J.; Stoloff, N.S.; Duquette, D.J.

Low cycle fatigue and creep-fatigue-environment interactions of PM/HIP Astrology were studied at 650 C and 725 C. Total strain range was varied from 1.5% to 2.7% at a frequency of 0.3Hz. Creep-fatigue tests were performed with 2 min. or 5 min. tensile hold times. All tests were run in high purity argon in an attempt to minimize environmental effects. Employing a tensile hold was more damaging than raising temperature by 75 C. Slopes of Coffin-Manson plots were nearly independent of temperature and hold time. Raising temperature from 650 C to 725 C did not change the transgranular (TG) crack propagationmore » mode, whereas employing hold times caused TG+IG propagation. All samples displayed multiple fracture origins associated with inclusions located at the specimen surface; pre-existing pores did not affect fatigue crack initiation. Examination of secondary cracks showed no apparent creep damage. Oxidation in high purity argon appeared to be the major factor in LCF life degradation due to hold times.« less

Study of Damage and Fracture Toughness Due to Influence of Creep and Fatigue of Commercially Pure Copper by Monotonic and Cyclic Indentation

NASA Astrophysics Data System (ADS)

Ghosh, Sabita; Prakash, Raghu V.

2013-01-01

Fracture toughness is the ability of a component containing a flow to resist fracture. In the current study, the Ball indentation (BI) test technique, which is well acknowledged as an alternative approach to evaluate mechanical properties of materials due to its semi-nondestructive, fast, and high accurate qualities is used to estimate damage and the fracture toughness for copper samples subjected to varying levels of creep and fatigue. The indentation fracture toughness shows the degradation of Cu samples when they are subjected to different creep conditions. Axial fatigue cycling increases the strength at the mid-gauge section compared to other regions of the samples due to initial strain hardening. The advancement of indentation depth with indentation fatigue cycles experiences transient stage, i.e., jump in indentation depth has been observed, which may be an indication of failure and followed by a steady state with almost constant depth propagation with indentation cycles.

Assessment of surface relief and short cracks under cyclic creep in a type 316LN austenitic stainless steel

NASA Astrophysics Data System (ADS)

Sarkar, Aritra; Nagesha, A.; Parameswaran, P.; Sandhya, R.; Laha, K.

2015-12-01

Formation of surface relief and short cracks under cyclic creep (stress-controlled fatigue) in type 316LN stainless steel was studied at temperatures ranging from ambient to 923 K using scanning electron microscopy technique. The surface topography and crack distribution behaviour under cyclic creep were found to be strong functions of testing temperature due to the difference in strain accumulation. At 823 K, surface relief mainly consisted of fine slip markings due to negligible accumulation of strain as a consequence of dynamic strain ageing (DSA) which led to an increase in the cyclic life. Persistent slip markings (PSM) with distinct extrusions containing minute cracks were seen to prevail in the temperature range 873-923 K, indicating a higher slip activity causing higher strain accumulation in the absence of DSA. Besides, a large number of secondary cracks (both transgranular and intergranular) which were partially accentuated by severe oxidation, were observed. Extensive cavitation-induced grain boundary cracking took place at 923 K, which coalesced with PSM-induced transgranular cracks resulting in failure dominated by creep that in turn led to a drastic reduction in cyclic life. Investigations on the influence of stress rate were also carried out which underlined the presence of DSA at 823 K. At 923 K, lowering the stress rate caused further strengthening of the contribution from creep damage marked by a shift in the damage mechanism from cyclic slip to diffusion.

High-Temperature Creep Degradation of the AM1/NiAlPt/EBPVD YSZ System

NASA Astrophysics Data System (ADS)

Riallant, Fanny; Cormier, Jonathan; Longuet, Arnaud; Milhet, Xavier; Mendez, José

2014-01-01

The failure mechanisms of a NiAlPt/electron beam physical vapor deposition yttria-stabilized-zirconia thermal barrier coating system deposited on the AM1 single crystalline substrate have been investigated under pure creep conditions in the temperature range from 1273 K to 1373 K (1000 °C to 1100 °C) and for durations up to 1000 hours. Doubly tapered specimens were used allowing for the analysis of different stress states and different accumulated viscoplastic strains for a given creep condition. Under such experiments, two kinds of damage mechanisms were observed. Under low applied stress conditions ( i.e., long creep tests), microcracking is localized in the vicinity of the thermally grown oxide (TGO). Under high applied stress conditions, an unconventional failure mechanism at the substrate/bond coat interface is observed because of large creep strains and fast creep deformation, hence leading to a limited TGO growth. This unconventional failure mechanism is observed although the interfacial bond coat/top coat TGO thickening is accelerated by the mechanical applied stress beyond a given stress threshold.

Viscoplastic Creep Response and Microstructure of As-Fabricated Microscale Sn-3.0Ag-0.5Cu Solder Interconnects

NASA Astrophysics Data System (ADS)

Cuddalorepatta, Gayatri; Williams, Maureen; Dasgupta, Abhijit

2010-10-01

The viscoplastic behavior of as-fabricated, undamaged, microscale Sn-3.0 Ag-0.5Cu (SAC305) Pb-free solder is investigated and compared with that of eutectic Sn-37Pb solder and near-eutectic Sn-3.8Ag-0.7Cu (SAC387) solder from prior studies. Creep measurements of microscale SAC305 solder shear specimens show significant piece-to-piece variability under identical loading. Orientation imaging microscopy reveals that these specimens contain only a few, highly anisotropic Sn grains across the entire joint. For the studied loads, the coarse-grained Sn microstructure has a more significant impact on the scatter in primary creep compared to that in the secondary creep. The observed lack of statistical homogeneity (microstructure) and joint-dependent mechanical behavior of microscale SAC305 joints are consistent with those observed for functional microelectronics interconnects. Compared with SAC305 joints, microscale Sn-37Pb shear specimens exhibit more homogenous behavior and microstructure with a large number of small Sn (and Pb) grains. Creep damage in the Pb-free joint is predominantly concentrated at highly misoriented Sn grain boundaries. The coarse-grained Sn microstructure recrystallizes into new grains with high misorientation angles under creep loading. In spite of the observed joint-dependent behavior, as-fabricated SAC305 is significantly more creep resistant than Sn-37Pb solder and slightly less creep resistant than near-eutectic SAC387 solder. Average model constants for primary and secondary creep of SAC305 are presented. Since the viscoplastic measurements are averaged over a wide range of grain configurations, the creep model constants represent the effective continuum behavior in an average sense. The average secondary creep behavior suggests that the dominant creep mechanism is dislocation climb assisted by dislocation pipe diffusion.

Long-term conditioning of deep-seated rockslides in deglaciated valleys: the Spriana case study

NASA Astrophysics Data System (ADS)

Agliardi, Federico; Crosta, Giovanni B.

2015-04-01

Deep-seated rockslides in alpine valleys evolve over long time under the action of multiple triggers. Early Warning based on monitoring is often the only effective approach to cope with these landslides, but it requires an improved understanding of mechanisms interplaying over long time. Deep-seated rockslides are often characterized by long-term 'creep' and seasonal displacement components, contributing to measured displacement patterns which are often modelled as rockslide responses to hydrologic perturbations. Although this hydro-mechanical modelling approach fits the behaviour of disrupted rockslide masses with well-developed shear zones, it is often insufficient to explain the initial onset and the long-term components of creep movements of deep-seated rockslides. This outlines the need to link long-term evolution of rock slopes and their sensitivity to triggers. We discuss the Spriana rockslide, affecting the steep left-hand flank of Val Malenco (italian Central Alps). Documented instabilities date back to 1912, whereas the rockslide underwent major acceleration stages in 1960 and 1977-78 and later minor reactivations. We reviewed a large amount of data collected since 1978 by extensive geotechnical site investigation (borehole drilling, exploratory adits, and seismic refraction) and monitoring activities (ground surface and deep displacements, pore pressures) motivated by potential catastrophic collapse threatening the city of Sondrio area. We performed rock mass characterization based on laboratory studies on intact rock samples, field surveys and drillcore logging. These data allowed re-evaluating the geological model of the Spriana rockslide, which is a compound slide of up to 50 Mm3 of slope debris and fractured gneiss, with multiple shear failure zones up to 90 m deep. Two main scarps developed in different stages, suggesting progressive failure processes. The rockslide creeps at slow rates of 0.4-3 cm/a, and undergoes acceleration stages (weeks to months) during increased water recharge periods. Heavily fractured rock masses occur below rockslide base up to 150 m in depth, suggesting extensive rock mass damage pre-dating rockslide onset. Groundwater monitoring shows that this fractured layer hosts a perched water table characterized by annual fluctuations up to 3 m. To gain insights in the long-term slope evolution we performed 2D Finite-Element multi-stage stress-strain and seepage modelling, accounting for post-LGM deglaciation, damage and related changes in slope strength and hydrology. Results validated using investigation data show that rockslide onset would have been unlikely without the strong preconditioning of long-term damage related to deglaciation. This led to a two-layer hydro-mechanical slope differentiation, with a fractured upper layer hosting a perched water table that favoured rockslide onset. Once structured, the rockslide became more sensitive to short-term hydrologic triggers, with displacement rates increasing in response to groundwater recharge related to critical values of antecedent (7 to 30 days) rainfall. Our results outline the importance of accounting for long-term slope evolution when dealing with rockslides evolving over 102-103 year timescales, and point to the need of modelling approaches able to relate changing hydro-mechanical properties of slopes to long-term damage processes.

Study on creep behavior of Grade 91 heat-resistant steel using theta projection method

NASA Astrophysics Data System (ADS)

Ren, Facai; Tang, Xiaoying

2017-10-01

Creep behavior of Grade 91 heat-resistant steel used for steam cooler was characterized using the theta projection method. Creep tests were conducted at the temperature of 923K under the stress ranging from 100-150MPa. Based on the creep curve results, four theta parameters were established using a nonlinear least square fitting method. Four theta parameters showed a good linearity as a function of stress. The predicted curves coincided well with the experimental data and creep curves were also modeled to the low stress level of 60MPa.

Effect of cold work on the stress corrosion cracking behavior of Alloy 690 in supercritical water environment

NASA Astrophysics Data System (ADS)

Chen, Kai; Du, Donghai; Gao, Wenhua; Guo, Xianglong; Zhang, Lefu; Andresen, Peter L.

2018-01-01

The stress corrosion cracking (SCC) behavior of Alloy 690 with 0, 20% and 30% cold work (CW) was studied in supercritical water (SCW) environment with an emphasis on CW and creep on the CGRs (CGR). SCC and creep CGRs increased with %CW, which correlated hardness very well. Microscopic characterization of the crack tip and fracture surface showed obvious cavity-like features, which is clear evidence of creep attack. The creep CGRs in inert gas were comparable to the SCC CGRs in SCW, indicating that creep is a major factor in crack growth. Increasing level of CW was found to increase the creep susceptibility, and high activation energies for creep crack growth were observed between 500 °C and 550 °C.

Time-dependent brittle deformation at Mt. Etna volcano

NASA Astrophysics Data System (ADS)

Baud, Patrick; Heap, Michael; Meredith, Philip; Vinciguerra, Sergio; Bell, Andrew; Main, Ian

2010-05-01

Time-dependent weakening mechanisms, leading to slow fracturing, are likely to act during the build up to flank eruptions at Mt. Etna volcano and are potentially a primary control on pre-eruptive patterns of seismicity and deformation. Due to the high permeability of its volcanic rocks, the volcanic edifice hosts a large water reservoir (Ogniben, 1966). The presence of a fluid phase in cracks within rock has been shown to dramatically affect both mechanical and chemical interactions. Chemically, it promotes time-dependent brittle deformation through such mechanisms as stress corrosion cracking that allows rocks to deform at stresses far below their short-term failure strength. Such crack growth is highly non-linear and accelerates towards dynamic failure over extended periods of time, even under constant applied stress; a phenomenon known as ‘brittle creep'. Here we report results from a study of time-dependent brittle creep in water-saturated samples of Etna basalt (EB) under triaxial stress conditions (confining pressure of 50 MPa and pore fluid pressure of 20 MPa). Samples of EB were loaded at a constant strain rate of 10-5 s-1 to a pre-determined percentage of the short-term strength and left to deform under constant stress until failure. Crack damage evolution was monitored throughout each experiment by measuring the independent damage proxies of axial strain, pore volume change and output of acoustic emission (AE) energy, during brittle creep of creep strain rates ranging over four orders of magnitude. Our data not only demonstrates that basalt creeps in the brittle regime but also that the applied differential stress exerts a crucial influence on both time-to-failure and creep strain rate in EB. Furthermore, stress corrosion is considered to be responsible for the acceleratory cracking and seismicity prior to volcanic eruptions and is invoked as an important mechanism in forecasting models. Stress-stepping creep experiments were then performed to allow the influence of the effective confining stress to be studied in detail. Experiments were performed under effective stress conditions of 10, 30 and 50 MPa (whilst maintaining a constant pore fluid pressure of 20 MPa). In addition to the purely mechanical influence of water, governed by the effective stress, which results in a shift of the creep strain rate curves to lower strain rates at higher effective stresses. Our results also demonstrate that the chemically-driven process of stress corrosion cracking appears to be inhibited at higher effective stress. This results in an increase in the gradient of the creep strain rate curves with increasing effective stress. We suggest that the most likely cause of this change is a decrease in water mobility due to a reduction in crack aperture and an increase in water viscosity at higher pressure. Finally, we show that a theoretical model based on mean-field damage mechanics creep laws is able to reproduce the experimental strain-time relations and inverse seismicity plots using our experimental AE data. Our results indicate that the local changes in the stress field and fluid circulation can have a profound impact in the time-to-failure properties of the basaltic volcanic pile.

Investigation of Macroscopic Brittle Creep Failure Caused by Microcrack Growth Under Step Loading and Unloading in Rocks

NASA Astrophysics Data System (ADS)

Li, Xiaozhao; Shao, Zhushan

2016-07-01

The growth of subcritical cracks plays an important role in the creep of brittle rock. The stress path has a great influence on creep properties. A micromechanics-based model is presented to study the effect of the stress path on creep properties. The microcrack model of Ashby and Sammis, Charles' Law, and a new micro-macro relation are employed in our model. This new micro-macro relation is proposed by using the correlation between the micromechanical and macroscopic definition of damage. A stress path function is also introduced by the relationship between stress and time. Theoretical expressions of the stress-strain relationship and creep behavior are derived. The effects of confining pressure on the stress-strain relationship are studied. Crack initiation stress and peak stress are achieved under different confining pressures. The applied constant stress that could cause creep behavior is predicted. Creep properties are studied under the step loading of axial stress or the unloading of confining pressure. Rationality of the micromechanics-based model is verified by the experimental results of Jinping marble. Furthermore, the effects of model parameters and the unloading rate of confining pressure on creep behavior are analyzed. The coupling effect of step axial stress and confining pressure on creep failure is also discussed. The results provide implications on the deformation behavior and time-delayed rockburst mechanism caused by microcrack growth on surrounding rocks during deep underground excavations.

Finite Element Creep-Fatigue Analysis of a Welded Furnace Roll for Identifying Failure Root Cause

NASA Astrophysics Data System (ADS)

Yang, Y. P.; Mohr, W. C.

2015-11-01

Creep-fatigue induced failures are often observed in engineering components operating under high temperature and cyclic loading. Understanding the creep-fatigue damage process and identifying failure root cause are very important for preventing such failures and improving the lifetime of engineering components. Finite element analyses including a heat transfer analysis and a creep-fatigue analysis were conducted to model the cyclic thermal and mechanical process of a furnace roll in a continuous hot-dip coating line. Typically, the roll has a short life, <1 year, which has been a problem for a long time. The failure occurred in the weld joining an end bell to a roll shell and resulted in the complete 360° separation of the end bell from the roll shell. The heat transfer analysis was conducted to predict the temperature history of the roll by modeling heat convection from hot air inside the furnace. The creep-fatigue analysis was performed by inputting the predicted temperature history and applying mechanical loads. The analysis results showed that the failure was resulted from a creep-fatigue mechanism rather than a creep mechanism. The difference of material properties between the filler metal and the base metal is the root cause for the roll failure, which induces higher creep strain and stress in the interface between the weld and the HAZ.

Life Modeling and Design Analysis for Ceramic Matrix Composite Materials

NASA Technical Reports Server (NTRS)

2005-01-01

The primary research efforts focused on characterizing and modeling static failure, environmental durability, and creep-rupture behavior of two classes of ceramic matrix composites (CMC), silicon carbide fibers in a silicon carbide matrix (SiC/SiC) and carbon fibers in a silicon carbide matrix (C/SiC). An engineering life prediction model (Probabilistic Residual Strength model) has been developed specifically for CMCs. The model uses residual strength as the damage metric for evaluating remaining life and is posed probabilistically in order to account for the stochastic nature of the material s response. In support of the modeling effort, extensive testing of C/SiC in partial pressures of oxygen has been performed. This includes creep testing, tensile testing, half life and residual tensile strength testing. C/SiC is proposed for airframe and propulsion applications in advanced reusable launch vehicles. Figures 1 and 2 illustrate the models predictive capabilities as well as the manner in which experimental tests are being selected in such a manner as to ensure sufficient data is available to aid in model validation.

Plate-tectonic boundary formation by grain-damage and pinning

NASA Astrophysics Data System (ADS)

Bercovici, David

2015-04-01

Shear weakening in the lithosphere is an essential ingredient for understanding how and why plate tectonics is generated from mantle convection on terrestrial planets. I present continued work on a theoretical model for lithospheric shear-localization and plate generation through damage, grain evolution and Zener pinning in two-phase (polycrystalline) lithospheric rocks. Grain size evolves through the competition between coarsening, which drives grain-growth, with damage, which drives grain reduction. The interface between phases controls Zener pinning, which impedes grain growth. Damage to the interface enhances the Zener pinning effect, which then reduces grain-size, forcing the rheology into the grain-size-dependent diffusion creep regime. This process thus allows damage and rheological weakening to co-exist, providing a necessary shear-localizing feedback. Moreover, because pinning inhibits grain-growth it promotes shear-zone longevity and plate-boundary inheritance. This theory has been applied recently to the emergence of plate tectonics in the Archean by transient subduction and accumulation of plate boundaries over 1Gyr, as well as to rapid slab detachment and abrupt tectonic changes. New work explores the saturation of interface damage at low interface curvature (e.g., because it is associated with larger grains that take up more of the damage, and/or because interface area is reduced). This effect allows three possible equilibrium grain-sizes for a given stress; a small-grain-size high-shear state in diffusion creep, a large grain-size low shear state in dislocation creep, and an intermediate state (often near the deformation map phase-boundary). The low and high grain-size states are stable, while the intermediate one is unstable. This implies that a material deformed at a given stress can acquire two stable deformation regimes, a low- and high- shear state; these are indicative of plate-like flows, i.e, the coexistence of both slowly deforming plates and rapidly deforming plate boundaries.

Complexities of high temperature metal fatigue: Some steps toward understanding

NASA Technical Reports Server (NTRS)

Manson, S. S.; Halford, G. R.

1983-01-01

After pointing out many of the complexities that attend high temperature metal fatigue beyond those already studied in the sub-creep range, a description of the micromechanisms of deformation and fracture is presented for several classes of materials that were studied over the past dozen years. Strainrange Partitioning (SRP) is used as a framework for interpreting the results. Several generic types of behavior were observed with regard both to deformation and fracture and each is discussed in the context of the micromechanisms involved. Treatment of cumulative fatigue damage and the possibility of ""healing'' of damage in successive loading loops, has led to a new interpretation of the Interaction Damage Rule of SRP. Using the concept of ""equivalent micromechanistic damage'' -- that the same damage on a microscopic scale is induced if the same hysteresis loops are generated, element for element -- it turns out the Interaction Damage Rule essentially compounds a number of variants of hysteresis loops, all of which have the same damage according to SRP concepts, into a set of loops each containing only one of the generic SRP strainranges. Thus the damage associcated with complex loops comprising several types of strainrange is analyzed by considering a combination of loops each containing only one type of strainrange. This concept is expanded to show how several independent loops can combine to ""heal'' creep damage in a complex loading history.

Creep crack growth by grain boundary cavitation under monotonic and cyclic loading

NASA Astrophysics Data System (ADS)

Wen, Jian-Feng; Srivastava, Ankit; Benzerga, Amine; Tu, Shan-Tung; Needleman, Alan

2017-11-01

Plane strain finite deformation finite element calculations of mode I crack growth under small scale creep conditions are carried out. Attention is confined to isothermal conditions and two time histories of the applied stress intensity factor: (i) a monononic increase to a plateau value subsequently held fixed; and (ii) a cyclic time variation. The crack growth calculations are based on a micromechanics constitutive relation that couples creep deformation and damage due to grain boundary cavitation. Grain boundary cavitation, with cavity growth due to both creep and diffusion, is taken as the sole failure mechanism contributing to crack growth. The influence on the crack growth rate of loading history parameters, such as the magnitude of the applied stress intensity factor, the ratio of the applied minimum to maximum stress intensity factors, the loading rate, the hold time and the cyclic loading frequency, are explored. The crack growth rate under cyclic loading conditions is found to be greater than under monotonic creep loading with the plateau applied stress intensity factor equal to its maximum value under cyclic loading conditions. Several features of the crack growth behavior observed in creep-fatigue tests naturally emerge, for example, a Paris law type relation is obtained for cyclic loading.

Irradiation creep and swelling of AISI 316 to exposures of 130 dpa at 385?400$deg;C

NASA Astrophysics Data System (ADS)

Garner, F. A.; Porter, D. L.

1988-07-01

The creep and swelling of AISI 316 stainless steel have been studied at 385 to 400°C in EBR-II to doses of 130 dpa. Most creep capsules were operated at constant stress and temperature but mid-life changes in these variables were also made. This paper concentrates on the behavior of the 20% cold-worked condition but five other conditions were also studied. Swelling at ⩽ 400° C was found to lose the sensitivity to stress exhibited at higher temperatures while the creep rate was found to retain linear dependencies on both stress and swelling rate. The creep coefficients extracted at 400°C agree with those found in other experiments conducted at higher temperatures. In the temperature range of ⩽ 400° C, swelling is in the recombinationdominated regime and the swelling rate falls strongly away from the ~1%/dpa rate observed at higher temperatures. These lower rates of creep and swelling, coupled with the attainment of high damage levels without failure, encourage the use of AISI 316 in the construction of water-cooled fusion first walls operating at temperatures below 400°C.

Damage Characterization of EBC-SiCSiC Ceramic Matrix Composites Under Imposed Thermal Gradient Testing

NASA Technical Reports Server (NTRS)

Appleby, Matthew P.; Morscher, Gregory N.; Zhu, Dongming

2014-01-01

Due to their high temperature capabilities, Ceramic Matrix Composite (CMC) components are being developed for use in hot-section aerospace engine applications. Harsh engine environments have led to the development of Environmental Barrier Coatings (EBCs) for silicon-based CMCs to further increase thermal and environmental capabilities. This study aims at understanding the damage mechanisms associated with these materials under simulated operating conditions. A high heat-flux laser testing rig capable of imposing large through-thickness thermal gradients by means of controlled laser beam heating and back-side air cooling is used. Tests are performed on uncoated composites, as well as CMC substrates that have been coated with state-of-the-art ceramic EBC systems. Results show that the use of the EBCs may help increase temperature capability and creep resistance by reducing the effects of stressed oxidation and environmental degradation. Also, the ability of electrical resistance (ER) and acoustic emission (AE) measurements to monitor material condition and damage state during high temperature testing is shown; suggesting their usefulness as a valuable health monitoring technique. Micromechanics models are used to describe the localized stress state of the composite system, which is utilized along with ER modeling concepts to develop an electromechanical model capable of characterizing material behavior.

Modeling Long-term Creep Performance for Welded Nickel-base Superalloy Structures for Power Generation Systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shen, Chen

2015-01-01

We report here a constitutive model for predicting long-term creep strain evolution in’ strengthened Ni-base superalloys. Dislocation climb-bypassing’, typical in intermediate’ volume fraction (~20%) alloys, is considered as the primary deformation mechanism. Dislocation shearing’ to anti-phase boundary (APB) faults and diffusional creep are also considered for high-stress and high-temperature low-stress conditions, respectively. Additional damage mechanism is taken into account for rapid increase in tertiary creep strain. The model has been applied to Alloy 282, and calibrated in a temperature range of 1375-1450°F, and stress range of 15-45ksi. The model parameters and a MATLAB code are provided. This report is preparedmore » by Monica Soare and Chen Shen at GE Global Research. Technical discussions with Dr. Vito Cedro are greatly appreciated. This work was supported by DOE program DE-FE0005859« less

Cyclic Deformation, Damage, and Effects of Environment in the Ni3Al Ordered Alloy at Elevated Temperature

DTIC Science & Technology

1991-03-29

restricts atomic mobility leading to slower diffusion and perhaps better creep resistance. Ordered intermetallics such as aluminides and silicides are...evaluation of the mechanical properties of these materials (specifically creep , oxidation and fatigue) must be evaluated before implementation in...rate by an order of magnitude (frcm 0.001/s to 0.01/s) doubled the fatigue life at a given plastic strain range. When tested in vacuum environments

Viscoplastic Model Development with an Eye Toward Characterization

NASA Technical Reports Server (NTRS)

Freed, Alan D.; Walker, Kevin P.

1995-01-01

A viscoplastic theory is developed that reduces analytically to creep theory under steady-state conditions. A viscoplastic model is constructed within this theoretical framework by defining material functions that have close ties to the physics of inelasticity. As a consequence, this model is easily characterized-only steady-state creep data, monotonic stress-strain curves, and saturated stress-strain hysteresis loops are required.

In situ monitored in-pile creep testing of zirconium alloys

NASA Astrophysics Data System (ADS)

Kozar, R. W.; Jaworski, A. W.; Webb, T. W.; Smith, R. W.

2014-01-01

The experiments described herein were designed to investigate the detailed irradiation creep behavior of zirconium based alloys in the HALDEN Reactor spectrum. The HALDEN Test Reactor has the unique capability to control both applied stress and temperature independently and externally for each specimen while the specimen is in-reactor and under fast neutron flux. The ability to monitor in situ the creep rates following a stress and temperature change made possible the characterization of creep behavior over a wide stress-strain-rate-temperature design space for two model experimental heats, Zircaloy-2 and Zircaloy-2 + 1 wt%Nb, with only 12 test specimens in a 100-day in-pile creep test program. Zircaloy-2 specimens with and without 1 wt% Nb additions were tested at irradiation temperatures of 561 K and 616 K and stresses ranging from 69 MPa to 455 MPa. Various steady state creep models were evaluated against the experimental results. The irradiation creep model proposed by Nichols that separates creep behavior into low, intermediate, and high stress regimes was the best model for predicting steady-state creep rates. Dislocation-based primary creep, rather than diffusion-based transient irradiation creep, was identified as the mechanism controlling deformation during the transitional period of evolving creep rate following a step change to different test conditions.

Assessment of Creep Deformation, Damage, and Rupture Life of 304HCu Austenitic Stainless Steel Under Multiaxial State of Stress

NASA Astrophysics Data System (ADS)

Sahoo, K. C.; Goyal, Sunil; Parameswaran, P.; Ravi, S.; Laha, K.

2018-03-01

The role of the multiaxial state of stress on creep deformation and rupture behavior of 304HCu austenitic stainless steel was assessed by performing creep rupture tests on both smooth and notched specimens of the steel. The multiaxial state of stress was introduced by incorporating circumferential U-notches of different root radii ranging from 0.25 to 5.00 mm on the smooth specimens of the steel. Creep tests were carried out at 973 K over the stress range of 140 to 220 MPa. In the presence of notch, the creep rupture strength of the steel was found to increase with the associated decrease in rupture ductility. Over the investigated stress range and notch sharpness, the strengthening was found to increase drastically with notch sharpness and tended toward saturation. The fractographic studies revealed the mixed mode of failure consisting of transgranular dimples and intergranular creep cavitation for shallow notches, whereas the failure was predominantly intergranular for relatively sharper notches. Detailed finite element analysis of stress distribution across the notch throat plane on creep exposure was carried out to assess the creep failure of the material in the presence of notch. The reduction in von-Mises stress across the notch throat plane, which was greater for sharper notches, increased the creep rupture strength of the material. The variation in fracture behavior of the material in the presence of notch was elucidated based on the von-Mises, maximum principal, and hydrostatic stresses. Electron backscatter diffraction analysis of creep strain distribution across the notch revealed localized creep straining at the notch root for sharper notches. A master curve for predicting creep rupture life under the multiaxial state of stress was generated considering the representative stress having contributions from both the von-Mises and principal stress components of the stress field in the notch throat plane. Rupture ductility was also predicted based on the multiaxial state of stress.

A Study on Soil Movement Characteristics and Monitoring of Land creeping in the Republic of Korea

NASA Astrophysics Data System (ADS)

Kang, M.; Lee, C.; Woo, C.; Kim, D.; Seo, J.; Kim, K.

2017-12-01

In South Korea, `Landslide' is general phenomenon that the soil is saturated by rainfall and the soil is rapidly falling down at top soil. Landslide Sediment-related disaster is mainly composed of shallow landslide and debris flow in South Korea. However, land creeping is also occurring due to climate change and mountain development. Land creeping is a phenomenon in which a part of the soil layer moves due to the influence of groundwater and external impacts in the mountain slope. It is difficult to detect the phenomenon because the moving speed is very slow and it occurs even without the effect of rainfall. In case land creeping occurs, the damage appears on a large scale. Therefore, it is important to analyze the cause of the occurrence and to cope with it promptly. This study was conducted to investigation soil characteristics and cracks monitoring in order to understand the characteristics and causes of land creeping in South Korea. The crack of land creeping was found in 5ea and the total extension was about 121m. The width and depth range of the crack are each 0.2 0.5m, 0.25 0.45m. Geology, engineering and geomorphological characteristics of the ground were considered. As a result, the land creeping occurred to following reasons; (1) Characteristics of bed rock(anorthosite), (2) Relatively high groundwater level, (3) Maintenance of lower slope when reservoir build, (4) Stratum structure of thinly plied layer. In addition, stability analysis was carried out through the precision ground survey. As a result, instability was found in all sections except for some sections. The method of countermeasures was decided by opinions of field experts. As a result, a monitoring method was suggested in order to understand the change of tension cracks. Therefore, real-time monitoring of landslide early detection system is being implemented. NIFS `unmanned remote monitoring system detects the occurrence of landslides using sensor data and provides early warning information. In order to reduce damage of residents near the hazardous area, the system was introduces centered on places where it is difficult to install landslide control structures like debris control dam. Currently, the system is installed at 2 locations in the land creeping area. Monitoring is being continuously carried out to obtain useful measurement data.

A Comparison of the Irradiation Creep Behavior of Several Graphites

DOE Office of Scientific and Technical Information (OSTI.GOV)

Burchell, Timothy D; Windes, Will

2016-01-01

Graphite creep strain data from the irradiation creep capsule Advanced Graphite Creep-1 (AGC-1) are reported. This capsule was the first (prototype) of a series of five or six capsules planned as part of the AGC experiment, which was designed to fully characterize the effects of neutron irradiation and the radiation creep behavior of current nuclear graphite. The creep strain data and analysis are reported for the six graphite grades incorporated in the capsule. The AGC-1 capsule was irradiated in the Advanced Test Reactor at Idaho National Laboratory (INL) at approximately 700 C and to a peak dose of 7 dpamore » (displacements per atom). The specimen s final dose, temperature, and stress conditions have been reported by INL and were used during this analysis. The derived creep coefficients (K) were calculated for each grade and were found to compare well to literature data for the creep coefficient, even under the wide range of AGC-1 specimen temperatures. Comparisons were made between AGC-1 data and historical grade data for creep coefficients.« less

Life Assessment for Cr-Mo Steel Dissimilar Joints by Various Filler Metals Using Accelerated Creep Testing

NASA Astrophysics Data System (ADS)

Petchsang, S.; Phung-on, I.; Poopat, B.

2016-12-01

Accelerated creep rupture tests were performed on T22/T91 dissimilar metal joints to determine the fracture location and rupture time of different weldments. Four configurations of deposited filler metal were tested using gas tungsten arc welding to estimate the service life for Cr-Mo steel dissimilar joints at elevated temperatures in power plants. Results indicated that failure in all configurations occurred in the tempered original microstructure and tempered austenite transformation products (martensite or bainite structure) as type IV cracking at the intercritical area of the heat-affected zone (ICHAZ) for both T22 and T91 sides rather than as a consequence of the different filler metals. Creep damage occurred with the formation of precipitations and microvoids. The correlation between applied stress and the Larson-Miller parameter (PLM) was determined to predict the service life of each material configuration. Calculated time-to-failure based on the PLM and test results for both temperature and applied stress parameters gave a reasonable fit. The dissimilar joints exhibited lower creep rupture compared to the base material indicating creep degradation of the weldment.

Materials for a Stirling engine heater head

NASA Technical Reports Server (NTRS)

Noble, J. E.; Lehmann, G. A.; Emigh, S. G.

1990-01-01

Work done on the 25-kW advanced Stirling conversion system (ASCS) terrestrial solar program in establishing criteria and selecting materials for the engine heater head and heater tubes is described. Various mechanisms contributing to incompatibility between materials are identified and discussed. Large thermal gradients, coupled with requirements for long life (60,000 h at temperature) and a large number of heatup and cooldown cycles (20,000) drive the design from a structural standpoint. The pressurized cylinder is checked for creep rupture, localized yielding, reverse plasticity, creep and fatigue damage, and creep ratcheting, in addition to the basic requirements for bust and proof pressure. In general, creep rupture and creep and fatigue interaction are the dominant factors in the design. A wide range of materials for the heater head and tubes was evaluated. Factors involved in the assessment were strength and effect on engine efficiency, reliability, and cost. A preliminary selection of Inconel 713LC for the heater head is based on acceptable structural properties but driven mainly by low cost. The criteria for failure, the structural analysis, and the material characteristics with basis for selection are discussed.

Numerical Experiments on Ductile Fracture in Granites

NASA Astrophysics Data System (ADS)

Regenauer-Lieb, K.; Weinberg, R. F.

2006-12-01

Ceramics and, by analogy rocks, are brittle at low temperatures, however, at high temperature and high pressure a second ductile mode of fracture based on dislocation and/or diffusion processes predominates. For ceramics 0.5-0.7 times the melting temperature suffice to create creep/ductile fracture which occurs typically after long time of deformation 104-1010 s (1). Ductile creep fractures make up for the low stress by profiting from accumulated strain and diffusion during slow creep deformation. Creep fractures typically nucleate on grain or phase boundaries, rigid or soft inclusions. Ultimately, the localized inhomogeneous damaged zone, begin to spread laterally and coalesce to create or follow a propagating shear band. The creep fracture sequence of crack nucleation, growth and coalescence relies on a mechanism of self-organization of fluids into a shear band during deformation and converts macroscopically to the crack like propagation of localized shear zones. Numerical experiments are used to test the ductile fracture hypothesis for the segregation and transfer of melts in granites. Ref: (1) C. Ghandi, M. F. Ashby, Acta Metallurgica 27, 1565 (1979).

Time-dependent Brittle Deformation in Etna Basalt

NASA Astrophysics Data System (ADS)

Heap, M. J.; Baud, P.; Meredith, P. G.; Vinciguerra, S.; Bell, A. F.; Main, I. G.

2008-12-01

Mt Etna is the largest and most active volcano in Europe. Due to the high permeability of its volcanic rocks, the volcanic edifice hosts one of the biggest hydrogeologic reservoirs of Sicily (Ogniben, 1966). Pre-eruptive patterns of flank eruptions, closely monitored by means of ground deformation and seismicity, revealed the slow development of fracture systems at different altitudes, marked by repeated bursts of seismicity and accelerating/decelerating deformation patterns acting over the scale of months to days. The presence of a fluid phase in cracks within rock has been shown to dramatically affect both mechanical and chemical interactions. Chemically, it promotes time-dependent brittle deformation through such mechanisms as stress corrosion cracking that allows rocks to deform at stresses far below their short-term failure strength. Such crack growth is highly non-linear and accelerates towards dynamic failure over extended periods of time, even under constant applied stress; a phenomenon known as 'brittle creep'. Stress corrosion is considered to be responsible for the acceleratory cracking and seismicity prior to volcanic eruptions and is invoked as an important mechanism in forecasting models. Here we report results from a study of time-dependent brittle creep in water-saturated samples of Etna basalt (EB) under triaxial stress conditions (confining pressure of 50 MPa and pore fluid pressure of 20 MPa). Samples of EB were loaded at a constant strain rate of 10-5 s-1 to a pre-determined percentage of the short- term strength and left to deform under constant stress until failure. Crack damage evolution was monitored throughout each experiment by measuring the independent damage proxies of axial strain, pore volume change and output of acoustic emission (AE) energy, during brittle creep of creep strain rates ranging over four orders of magnitude. Our data demonstrate that the applied differential stress exerts a crucial influence on both time-to-failure and creep strain rate in EB. Stress-stepping creep experiments were then performed to allow the influence of the effective confining stress to be studied in detail. Experiments were performed under effective stress conditions of 10, 30 and 50 MPa (whilst maintaining a constant pore fluid pressure of 20 MPa). In addition to the purely mechanical influence of water, governed by the effective stress, which results in a shift of the creep strain rate curves to lower strain rates at higher effective stresses. Our results also demonstrate that the chemically-driven process of stress corrosion cracking appears to be inhibited at higher effective stress. This results in an increase in the gradient of the creep strain rate curves with increasing effective stress. We suggest that the most likely cause of this change is a decrease in water mobility due to a reduction in crack aperture and an increase in water viscosity at higher pressure. Finally, we show that a theoretical model based on mean-field damage mechanics creep laws is able to reproduce the experimental strain-time relations. Our results indicate that the local changes in the stress field and fluid circulation can have a profound impact in the time- to-failure properties of the basaltic volcanic pile.

Low cycle fatigue and creep fatigue interaction behavior of 9Cr-0.5Mo-1.8W-V-Nb heat-resistant steel at high temperature

NASA Astrophysics Data System (ADS)

Wang, Xiaowei; Zhang, Wei; Gong, Jianming; Wahab, Magd Abdel

2018-07-01

In this paper, Low Cycle Fatigue (LCF) and Creep-Fatigue Interaction (CFI) behavior of 9Cr-0.5Mo-1.8 W-V-Nb heat-resistant steel (ASME Grade P92 steel) at elevated temperature of 600 °C are investigated. Strain controlled LCF tests are conducted in fully reversed triangular waveform at different strain amplitudes ranging from 0.2% to 0.8%. CFI tests are conducted at 0.4% strain amplitude in trapezoid waveform with tensile hold time varying from 1 min to 60 min and compressive hold time varying from 1 min to 10 min. During LCF and CFI loadings, the evolution of cyclic stress, mean stress and stress relaxation behavior are investigated. It turns out that the softening behavior and lifetime degradation are dependent on strain amplitude, hold time and hold direction. In addition, the microstructure evolution and fracture behavior are characterized by optical, scanning and transmission electron microscope. The initial rapid softening behavior is attributed to the quick elimination of low angle boundaries, whereas no obvious microstructure alteration appears in the stable stage. Fracture behavior analysis reveals creep voids in long-term CFI tests facilitates the initiation and propagation of secondary cracks. The different responses of outer surface oxidation layer during cycling provides an explanation for severer damage of compressive hold and also accounts for the observed various fracture behavior of failed samples.

A Viscoelastic Constitutive Model Can Accurately Represent Entire Creep Indentation Tests of Human Patella Cartilage

PubMed Central

Pal, Saikat; Lindsey, Derek P.; Besier, Thor F.; Beaupre, Gary S.

2013-01-01

Cartilage material properties provide important insights into joint health, and cartilage material models are used in whole-joint finite element models. Although the biphasic model representing experimental creep indentation tests is commonly used to characterize cartilage, cartilage short-term response to loading is generally not characterized using the biphasic model. The purpose of this study was to determine the short-term and equilibrium material properties of human patella cartilage using a viscoelastic model representation of creep indentation tests. We performed 24 experimental creep indentation tests from 14 human patellar specimens ranging in age from 20 to 90 years (median age 61 years). We used a finite element model to reproduce the experimental tests and determined cartilage material properties from viscoelastic and biphasic representations of cartilage. The viscoelastic model consistently provided excellent representation of the short-term and equilibrium creep displacements. We determined initial elastic modulus, equilibrium elastic modulus, and equilibrium Poisson’s ratio using the viscoelastic model. The viscoelastic model can represent the short-term and equilibrium response of cartilage and may easily be implemented in whole-joint finite element models. PMID:23027200

Microstructure characterization in domestically-made TP310HNbN austenitic stainless steel after creep test

NASA Astrophysics Data System (ADS)

Guo, Yan; Lin, Lin; Hou, Shufang; Wang, Bohan

Microstructure characterization of domestically-made TP310HNbN austenitic stainless steel after creep test was investigated by means of transmission electron microscopy (TEM) and scanning electron microscopy (SEM). The results revealed that M23C6 carbides precipitated both inside grains and at the grain boundaries and NbCrN particles were located inside grains for creep-rupture samples. It was clear that sigma phase and NbC particles precipitated inside grains for the creep-rupture sample at 670 C. M23C6 carbides with lattice parameter of three times of the austenite matrix grow in a cube to cube orientation relationship with the matrix. The amount of M23C6 carbide particles obviously increased with the testing time prolonged. Deformation hardening induced an enhanced hardness nearby rupture surface for the creep-rupture samples with a short testing time. For the domestically-made TP310HNbN steel, great attention should be paid to the distribution, size and amount of sigma phase and M23C6 during service.

Relationship between fatigue life in the creep-fatigue region and stress-strain response

NASA Technical Reports Server (NTRS)

Berkovits, A.; Nadiv, S.

1988-01-01

On the basis of mechanical tests and metallographic studies, strainrange partitioned lives were predicted by introducing stress-strain materials parameters into the Universal Slopes Equation. This was the result of correlating fatigue damage mechanisms and deformation mechanisms operating at elevated temperatures on the basis of observed mechanical and microstructural behavior. Correlation between high temperature fatigue and stress strain properties for nickel base superalloys and stainless steel substantiated the method. Parameters which must be evaluated for PP- and CC- life are the maximum stress achievable under entirely plastic and creep conditions respectively and corresponding inelastic strains, and the elastic modulus. For plasticity/creep interaction conditions (PC and CP) two more pairs of stress strain parameters must be ascertained.

Assessment of microalloying effects on the high temperature fatigue behavior of NiAl

NASA Technical Reports Server (NTRS)

Noebe, R. D.; Lerch, B. A.; Rao, K. B. S.

1995-01-01

Binary NiAl suffers from a lack of strength and poor creep properties at and above 1000 K. Poor creep resistance in turn affects low cycle fatigue (LCF) lives at low strain ranges due to the additional interactions of creep damage. One approach for improving these properties involved microalloying with either Zr or N. As an integral part of a much larger alloying program the low cycle fatigue behavior of Zr and N doped nickel aluminides produced by extrusion of prealloyed powders has been investigated. Strain controlled LCF tests were performed in air at 1000 K. The influence of these microalloying additions on the fatigue life and cyclic stress response of polycrystalline NiAl are discussed.

Thermally activated creep and fluidization in flowing disordered materials

NASA Astrophysics Data System (ADS)

Merabia, Samy; Detcheverry, François

2016-11-01

When submitted to a constant mechanical load, many materials display power law creep followed by fluidization. A fundamental understanding of these processes is still far from being achieved. Here, we characterize creep and fluidization on the basis of a mesoscopic viscoplastic model that includes thermally activated yielding events and a broad distribution of energy barriers, which may be lowered under the effect of a local deformation. We relate the creep exponent observed before fluidization to the width of barrier distribution and to the specific form of stress redistribution following yielding events. We show that Andrade creep is accompanied by local strain hardening driven by stress redistribution and find that the fluidization time depends exponentially on the applied stress. The simulation results are interpreted in the light of a mean-field analysis, and should help in rationalizing the creep phenomenology in disordered materials.

Rate-based structural health monitoring using permanently installed sensors

PubMed Central

2017-01-01

Permanently installed sensors are becoming increasingly ubiquitous, facilitating very frequent in situ measurements and consequently improved monitoring of ‘trends’ in the observed system behaviour. It is proposed that this newly available data may be used to provide prior warning and forecasting of critical events, particularly system failure. Numerous damage mechanisms are examples of positive feedback; they are ‘self-accelerating’ with an increasing rate of damage towards failure. The positive feedback leads to a common time-response behaviour which may be described by an empirical relation allowing prediction of the time to criticality. This study focuses on Structural Health Monitoring of engineering components; failure times are projected well in advance of failure for fatigue, creep crack growth and volumetric creep damage experiments. The proposed methodology provides a widely applicable framework for using newly available near-continuous data from permanently installed sensors to predict time until failure in a range of application areas including engineering, geophysics and medicine. PMID:28989308

Low Cycle Fatigue and Creep-Fatigue Behavior of Alloy 617 at High Temperature

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cabet, Celine; Carroll, Laura; Wright, Richard

Alloy 617 is the leading candidate material for an intermediate heat exchanger (IHX) application of the Very High Temperature Nuclear Reactor (VHTR), expected to have an outlet temperature as high as 950 degrees C. Acceptance of Alloy 617 in Section III of the ASME Code for nuclear construction requires a detailed understanding of the creep-fatigue behavior. Initial creep-fatigue work on Alloy 617 suggests a more dominant role of environment with increasing temperature and/or hold times evidenced through changes in creep-fatigue crack growth mechanism/s and failure life. Continuous cycle fatigue and creep-fatigue testing of Alloy 617 was conducted at 950 degreesmore » C and 0.3% and 0.6% total strain in air to simulate damage modes expected in a VHTR application. Continuous cycle specimens exhibited transgranular cracking. Intergranular cracking was observed in the creep-fatigue specimens, although evidence of grain boundary cavitation was not observed. Despite the absence of grain boundary cavitation to accelerate crack propagation, the addition of a hold time at peak tensile strain was detrimental to cycle life. This suggests that creepfatigue interaction may occur by a different mechanism or that the environment may be partially responsible for accelerating failure.« less

Change of nonlinear acoustics in ASME grade 122 steel welded joint during creep

NASA Astrophysics Data System (ADS)

Ohtani, Toshihiro; Honma, Takumi; Ishii, Yutaka; Tabuchi, Masaaki; Hongo, Hiromichi; Hirao, Masahiko

2016-02-01

In this paper, we described the changes of two nonlinear acoustic characterizations; resonant frequency shift and three-wave interaction, with electromagnetic acoustic resonance (EMAR) throughout the creep life in the welded joints of ASME Grade 122, one of high Cr ferritic heat resisting steels. EMAR was a combination of the resonant acoustic technique with a non-contact electromagnetic acoustic transducer (EMAT). These nonlinear acoustic parameters decreased from the start to 50% of creep life. After slightly increased, they rapidly increased from 80% of creep life to rupture. We interpreted these phenomena in terms of dislocation recovery, recrystallization, and restructuring related to the initiation and growth of creep void, with support from the SEM and TEM observation.

Characterization of Wisconsin mixture low temperature properties for the AASHTO mechanistic-empirical pavement design guide.

DOT National Transportation Integrated Search

2011-12-01

This research evaluated the low temperature creep compliance and tensile strength properties of Wisconsin mixtures. : Creep compliance and tensile strength data were collected for 16 Wisconsin mixtures representing commonly used : aggregate sources a...

Microscale mechanical characterization of materials for extreme environments

NASA Astrophysics Data System (ADS)

Ozerinc, Sezer

Nanocrystalline metals are promising materials for applications that require outstanding strength and stability in extreme environments. Further improvements in the desirable mechanical properties of these materials require a better understanding of the relationship between their microstructure and grain boundary deformation behavior. Previous molecular dynamics simulations suggested that solute additions to grain boundaries can enhance the strength of nanocrystalline metals, but there has been a lack of experimental studies investigating this prediction. This dissertation presents mechanical and microstructural characterization of nanocrystalline Cu alloys and demonstrate that addition of Nb solutes to grain boundaries greatly enhances the strength of Cu. The measured hardness of Cu90Nb10 alloy is 5.6 GPa which is more than double the hardness of nanocrystalline pure Cu. Microstructural characterization through transmission electron microscopy and energy-dispersive X-ray spectroscopy on these alloys indicates a strong correlation between the grain boundary composition and the hardness. Variation of measured hardness with measured grain boundary composition is in very good agreement with previous molecular dynamics simulation predictions. The results of this work provide experimental evidence that grain boundary doping enhances the strength of nanocrystalline Cu far beyond that predicted by classical Hall-Petch strengthening and decreasing grain boundary energy through solute additions is the key to reaching theoretical strength in nanocrystalline metals. Irradiation induced creep is a deformation mechanism that takes place under combined stress and particle bombardment. Effective characterization of this phenomenon on nanostructured materials is crucial for the assessment of their potential use in next generation nuclear power plants. Direct measurements of irradiation induced creep under MeV-heavy ion bombardment have not been feasible until recently due to the requirements of micron-sized specimens, muN-level force sensitivity, and nm-level displacement sensitivity. A recently developed mechanical characterization technique, micropillar compression, has enabled the testing of miniaturized specimens; however, there has been no demonstration of the application of this technique to irradiation induced creep measurements. This dissertation presents the development of an in situ measurement apparatus for compression testing of micron-sized cylindrical specimens under MeV-heavy ion bombardment. The apparatus has a force resolution of 1 muN and a displacement resolution of 1 nm. The apparatus measured irradiation induced creep in four different amorphous materials and the findings clarified the significance of different creep mechanisms in these materials. In amorphous metals and amorphous Si, the measured irradiation induced fluidity is ≈ 3 dpa-1GPa-1 (dpa: displacements per atom). The measured fluidity is in excellent agreement with previous molecular dynamics simulation predictions, providing experimental evidence for point defect mediated plastic flow under ion bombardment. For amorphous SiO2, stress relaxation through thermal spikes further contribute to the creep response, resulting in higher fluidities up to ≈ 83 dpa-1GPa -1. Finally, this dissertation presents the further development of the creep testing apparatus for high temperature measurements. The apparatus demonstrated good thermal and mechanical stability and measured irradiation induced creep of nanocrystalline Cu at 200°C. Resulting irradiation induced fluidity is ≈ 10% of the fluidity of the amorphous metals, in agreement with previous measurements on free-standing films. Understanding the creep behavior of nanostructured metals under heavy ion bombardment at elevated temperatures is important for identifying the governing creep mechanisms in these materials. The developed apparatus provides a new and effective method of accelerated mechanical characterization of such promising materials for their potential use in future nuclear applications.

Finite element analysis of history-dependent damage in time-dependent fracture mechanics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Krishnaswamy, P.; Brust, F.W.; Ghadiali, N.D.

1993-11-01

The demands for structural systems to perform reliably under both severe and changing operating conditions continue to increase. Under these conditions time-dependent straining and history-dependent damage become extremely important. This work focuses on studying creep crack growth using finite element (FE) analysis. Two important issues, namely, (1) the use of history-dependent constitutive laws, and (2) the use of various fracture parameters in predicting creep crack growth, have both been addressed in this work. The constitutive model used here is the one developed by Murakami and Ohno and is based on the concept of a creep hardening surface. An implicit FEmore » algorithm for this model was first developed and verified for simple geometries and loading configurations. The numerical methodology developed here has been used to model stationary and growing cracks in CT specimens. Various fracture parameters such as the C[sub 1], C[sup *], T[sup *], J were used to compare the numerical predictions with experimental results available in the literature. A comparison of the values of these parameters as a function of time has been made for both stationary and growing cracks. The merit of using each of these parameters has also been discussed.« less

Generation of plate tectonics with two-phase grain-damage and pinning: Source-sink model and toroidal flow

NASA Astrophysics Data System (ADS)

Bercovici, David; Ricard, Yanick

2013-03-01

The grain-damage and pinning mechanism of Bercovici and Ricard (2012) for lithospheric shear-localization is employed in two-dimensional flow calculations to test its ability to generate toroidal (strike-slip) motion and influence plate evolution. This mechanism posits that damage to the interface between phases in a polycrystalline material like peridotite (composed primarily of olivine and pyroxene) increases the number of small Zener pinning surfaces, which then constrain mineral grains to ever smaller sizes, regardless of creep mechanism. This effect allows a self-softening feedback in which damage and grain-reduction can co-exist with a grain-size dependent diffusion creep rheology; moreover, grain growth and weak-zone healing are greatly impeded by Zener pinning thereby leading to long-lived relic weak zones. The fluid dynamical calculations employ source-sink driven flow as a proxy for convective poloidal flow (upwelling/downwelling and divergent/convergent motion), and the coupling of this flow with non-linear rheological mechanisms excites toroidal or strike-slip motion. The numerical experiments show that pure dislocation-creep rheology, and grain-damage without Zener pinning (as occurs in a single-phase assemblages) permit only weak localization and toroidal flow; however, the full grain-damage with pinning readily allows focussed localization and intense, plate-like toroidal motion and strike-slip deformation. Rapid plate motion changes are also tested with abrupt rotations of the source-sink field after a plate-like configuration is developed; the post-rotation flow and material property fields retain memory of the original configuration for extensive periods, leading to suboptimally aligned plate boundaries (e.g., strike-slip margins non-parallel to plate motion), oblique subduction, and highly localized, weak and long lived acute plate-boundary junctions such as at what is observed at the Aleutian-Kurile intersection. The grain-damage and pinning theory therefore readily satisfies key plate-tectonic metrics of localized toroidal motion and plate-boundary inheritance, and thus provides a predictive theory for the generation of plate tectonics on Earth and other planets.

Characterizing the effect of creep on stress corrosion cracking of cold worked Alloy 690 in supercritical water environment

NASA Astrophysics Data System (ADS)

Zhang, Lefu; Chen, Kai; Du, Donghai; Gao, Wenhua; Andresen, Peter L.; Guo, Xianglong

2017-08-01

The effect of creep on stress corrosion cracking (SCC) was studied by measuring crack growth rates (CGRs) of 30% cold worked (CW) Alloy 690 in supercritical water (SCW) and inert gas environments at temperatures ranging from 450 °C to 550 °C. The SCC crack growth rate under SCW environments can be regarded as the cracking induced by the combined effect of corrosion and creep, while the CGR in inert gas environment can be taken as the portion of creep induced cracking. Results showed that the CW Alloy 690 sustained high susceptibility to intergranular (IG) cracking, and creep played a dominant role in the SCC crack growth behavior, contributing more than 80% of the total crack growth rate at each testing temperature. The temperature dependence of creep induced CGRs follows an Arrhenius dependency, with an apparent activation energy (QE) of about 225 kJ/mol.

Numerical Simulation of Creep Characteristic for Composite Rock Mass with Weak Interlayer

NASA Astrophysics Data System (ADS)

Li, Jian-guang; Zhang, Zuo-liang; Zhang, Yu-biao; Shi, Xiu-wen; Wei, Jian

2017-06-01

The composite rock mass with weak interlayer is widely exist in engineering, and it’s essential to research the creep behavior which could cause stability problems of rock engineering and production accidents. However, due to it is difficult to take samples, the losses and damages in delivery and machining process, we always cannot get enough natural layered composite rock mass samples, so the indirect test method has been widely used. In this paper, we used ANSYS software (a General Finite Element software produced by American ANSYS, Inc) to carry out the numerical simulation based on the uniaxial compression creep experiments of artificial composite rock mass with weak interlayer, after experimental data fitted. The results show that the laws obtained by numerical simulations and experiments are consistent. Thus confirmed that carry out numerical simulation for the creep characteristics of rock mass with ANSYS software is feasible, and this method can also be extended to other underground engineering of simulate the weak intercalations.

Tensile and compressive creep behavior of extruded Mg–10Gd–3Y–0.5Zr (wt.%) alloy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, H.; The State Key Laboratory of Metal Matrix Composites, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240; Wang, Q.D., E-mail: wangqudong@sjtu.edu.cn

2015-01-15

The tensile and compressive creep behavior of an extruded Mg–10Gd–3Y–0.5Zr (wt.%) alloy was investigated at temperatures ranging from 200 °C to 300 °C and under stresses ranging from 30 MPa to 120 MPa. There existed an asymmetry in the tensile and compressive creep properties. The minimum creep rate of the alloy was slightly greater in tension than in compression. The measured values of the transient strain and initial creep rate in compression were greater than those in tension. The creep stress exponent was approximately 2.5 at low temperatures (T < 250 °C) and 3.4 at higher temperatures both in tensionmore » and in compression. The compression creep activation energy at low temperatures and high temperatures was 83.4 and 184.3 kJ/mol respectively, while one activation energy (184 kJ/mol) represented the tensile–creep behavior over the temperature range examined. Dislocation creep was suggested to be the main mechanism in tensile creep and in the high-temperature regime in compressive creep, while grain boundary sliding was suggested to dominate in the low-temperature regime in compressive creep. Precipitate free zones were observed near grain boundaries perpendicular to the loading direction in tension and parallel to the loading direction in compression. Electron backscattered diffraction analysis revealed that the texture changed slightly during creep. Non-basal slip was suggested to contribute to the deformation after basal slip was introduced. In the tensile–creep ruptured specimens, intergranular cracks were mainly observed at general high-angle boundaries. - Highlights: • Creep behavior of an extruded Mg–RE alloy was characterized by EBSD. • T5 aging treatment enhanced the tension–compression creep asymmetry. • The grains grew slightly during tensile creep, but not for compressive creep. • Precipitate free zones (PFZs) were observed at specific grain boundaries. • Intergranular fracture was dominant and cracks mainly originated at GHABs.« less

Viscoelastic Response of the Titanium Alloy Ti-6-4: Experimental Identification of Time- and Rate-Dependent Reversible and Irreversible Deformation Regions

NASA Technical Reports Server (NTRS)

Lerch, Bradley A.; Arnold, Steven M.

2014-01-01

In support of an effort on damage prognosis, the viscoelastic behavior of Ti-6Al-4V (Ti-6-4) was investigated. This report documents the experimental characterization of this titanium alloy. Various uniaxial tests were conducted to low load levels over the temperature range of 20 to 538 C to define tensile, creep, and relaxation behavior. A range of strain rates (6x10(exp -7) to 0.001/s) were used to document rate effects. All tests were designed to include an unloading portion, followed by a hold time at temperature to allow recovery to occur either at zero stress or strain. The titanium alloy was found to exhibit viscoelastic behavior below the "yield" point and over the entire range of temperatures (although at lower temperatures the magnitude is extremely small). These experimental data will be used for future characterization of a viscoelastic model.

Simulation-Based Extreme Value Marked Correlations in Fatigue of Advanced Engineering Alloys (PREPRINT)

DTIC Science & Technology

2010-04-01

000 the response of damage dependent processes like fatigue crack formation, a framework is needed that accounts for the extreme value life...many different damage processes (e.g. fatigue, creep, fracture). In this work, multiple material volumes for both IN100 and Ti-6Al-4V are simulated via...polycrystalline P/M Ni-base superalloy IN100 Typically, fatigue damage formation in polycrystalline superalloys has been linked to the existence of

Elevated temperature creep and fracture properties of the 62Cu-35Au-3Ni braze alloy

NASA Astrophysics Data System (ADS)

Stephens, J. J.; Greulich, F. A.

1995-06-01

The Cu-Au-Ni braze alloys are used for metal/ceramic brazes in electronic assemblies because of their good wetting characteristics and low vapor pressure. We have studied the tensile creep properties of annealed 62Cu-35Au-3Ni alloy over the temperature range 250 °C to 750 °C. Two power-law equations have been developed for the minimum creep rate as a function of true stress and temperature. At the highest temperatures studied (650 °C and 750 °C), the minimum creep rate is well described with a stress exponent of 3.0, which can be rationalized in the context of Class I solid solution strengthening. The inverted shape of the creep curves observed at these temperatures is also consistent with Class I alloy behavior. At lower temperatures, power-law creep is well described with a stress exponent of 7.5, and normal three-stage creep curves are observed. Intergranular creep damage, along with minimum values of strain to fracture, is most apparent at 450 °C and 550 °C. The lower stress exponent in the Class I alloy regime helps to increase the strain to fracture at higher temperatures (650 °C and 750 °C). The minimum creep rate behavior of the 62Cu-35Au-3Ni alloy is also compared with those of the 74.2Cu-25. 8Au alloy and pure Cu. This comparison indicates that the 62Cu-35Au-3Ni has considerably higher creep strength than pure Cu. This fact suggests that the 62Cu-35Au-3Ni braze alloy can be used in low mismatch metal-to-ceramic braze joints such as Mo to metallized alumina ceramic with few problems. However, careful joint design may be essential for the use of this alloy in high thermal mismatch metal-to-ceramic braze joints.

Technical evaluation report of the Specialists Meeting on Characterization of Low Cycle High Temperature Fatigue by the Strainrange Partitioning Method

NASA Technical Reports Server (NTRS)

Drapier, J. M.; Hirschberg, M. H.

1979-01-01

The ability of the Strainrange Partitioning Method SRP was evaluated to correlate the creep-fatigue behavior of gas turbine materials and to predict the creep fatigue life of laboratory specimens subjected to complex cycling conditions. A reference body of high temperature creep fatigue data which can be used in the evaluation of other SRP and low cycle high temperature fatigue predictive techniques was provided.

In situ nonlinear ultrasonic technique for monitoring microcracking in concrete subjected to creep and cyclic loading.

PubMed

Kim, Gun; Loreto, Giovanni; Kim, Jin-Yeon; Kurtis, Kimberly E; Wall, James J; Jacobs, Laurence J

2018-08-01

This research conducts in situ nonlinear ultrasonic (NLU) measurements for real time monitoring of load-induced damage in concrete. For the in situ measurements on a cylindrical specimen under sustained load, a previously developed second harmonic generation (SHG) technique with non-contact detection is adapted to a cylindrical specimen geometry. This new setup is validated by demonstrating that the measured nonlinear Rayleigh wave signals are equivalent to those in a flat half space, and thus the acoustic nonlinearity parameter, β can be defined and interpreted in the same way. Both the acoustic nonlinearity parameter and strain are measured to quantitatively assess the early-age damage in a set of concrete specimens subjected to either 25 days of creep, or 11 cycles of cyclic loading at room temperature. The experimental results show that the acoustic nonlinearity parameter is sensitive to early-stage microcrack formation under both loading conditions - the measured β can be directly linked to the accumulated microscale damage. This paper demonstrates the potential of NLU for the in situ monitoring of mechanical load-induced microscale damage in concrete components. Copyright © 2018 Elsevier B.V. All rights reserved.

Interconversion of dynamic modulus to creep compliance and relaxation modulus : numerical modeling and laboratory validation - final report.

DOT National Transportation Integrated Search

2016-09-01

Viscoelastic material functions such as time domain functions, such as, relaxation modulus and creep compliance, : or frequency domain function, such as, complex modulus can be used to characterize the linear viscoelastic behavior : of asphalt concre...

Validity of multiple stress creep recovery test for LADOTD asphalt binder specification.

DOT National Transportation Integrated Search

2010-09-01

The objectives of this research are to characterize the elastic response of various binders used by LADOTD to determine the feasibility of the Multiple Stress Creep Recovery (MSCR) test to be included in the LADOTD asphalt binder specification and to...

Large Engine Technology (LET) Short Haul Civil Tiltrotor Contingency Power Materials Knowledge and Lifing Methodologies

NASA Technical Reports Server (NTRS)

Spring, Samuel D.

2006-01-01

This report documents the results of an experimental program conducted on two advanced metallic alloy systems (Rene' 142 directionally solidified alloy (DS) and Rene' N6 single crystal alloy) and the characterization of two distinct internal state variable inelastic constitutive models. The long term objective of the study was to develop a computational life prediction methodology that can integrate the obtained material data. A specialized test matrix for characterizing advanced unified viscoplastic models was specified and conducted. This matrix included strain controlled tensile tests with intermittent relaxtion test with 2 hr hold times, constant stress creep tests, stepped creep tests, mixed creep and plasticity tests, cyclic temperature creep tests and tests in which temperature overloads were present to simulate actual operation conditions for validation of the models. The selected internal state variable models where shown to be capable of representing the material behavior exhibited by the experimental results; however the program ended prior to final validation of the models.

Creep Deformation, Rupture Analysis, Heat Treatment and Residual Stress Measurement of Monolithic and Welded Grade 91 Steel for Power Plant Components

NASA Astrophysics Data System (ADS)

Shrestha, Triratna

Modified 9Cr-1 Mo (Grade 91) steel is currently considered as a candidate material for reactor pressure vessels (RPVs) and reactor internals for the Very High Temperature Reactor (VHTR), and in fossil-fuel fired power plants at higher temperatures and stresses. The tensile creep behavior of Grade 91 steel was studied in the temperature range of 600°C to 750°C and stresses between 35 MPa and 350 MPa. Heat treatment of Grade 91 steel was studied by normalizing and tempering the steel at various temperatures and times. Moreover, Thermo-Ca1c(TM) calculation was used to predict the precipitate stability and their evolution, and construct carbon isopleths of Grade 91 steel. Residual stress distribution across gas tungsten arc welds (GTAW) in Grade 91 steel was measured by the time-of-flight neutron diffraction using the Spectrometer for Materials Research at Temperature and Stress (SMARTS) diffractometer at Lujan Neutron Scattering Center, Los Alamos National Laboratory, Los Alamos, NM, USA. Analysis of creep results yielded stress exponents of ˜9-11 in the higher stress regime and ˜1 in the lower stress regime. The creep behavior of Grade 91 steel was described by the modified Bird-Mukherjee-Dorn relation. The rate-controlling creep deformation mechanism in the high stress regime was identified as the edge dislocation climb with a stress exponent of n = 5. On the other hand, the deformation mechanism in the Newtonian viscous creep regime (n = 1) was identified as the Nabarro-Herring creep. Creep rupture data were analyzed in terms of Monkman-Grant relation and Larson-Miller parameter. Creep damage tolerance factor and stress exponent were used to identify the cause of creep damage. The fracture surface morphology of the ruptured specimens was studied by scanning electron microscopy to elucidate the failure mechanisms. Fracture mechanism map for Grade 91 steel was developed based on the available material parameters and experimental observations. The microstructural evolution of heat treated steel was correlated with the differential scanning calorimetric study. The combination of microstructural studies with optical microscopy, scanning and transmission electron microscopy, microhardness profiles, and calorimetric plots helped in the understanding of the evolution of microstructure and precipitates in Grade 91 steel. The residual stresses were determined at the mid-thickness of the plate, 4.35 mm and 2.35 mm below the surface of the as-welded and post-weld heat treated plate. The residual stresses of the as-welded plate were compared with the post-weld heat treated plate. The post-weld heat treatment significantly reduced the residual stress in the base metal, heat affected zone, and the weld zone. Vickers microhardness profiles of the as-welded, and post-weld heat treated specimens were also determined and correlated with the observed residual stress profile and microstructure.

Rheology of the lithosphere and the folding caused by horizontal compression

NASA Astrophysics Data System (ADS)

Birger, B. I.

2015-05-01

The laboratory tests of rock specimens show that transient creep, at which deformations increase with time whereas strain rate decreases occurs when creep strains are sufficiently small. Since plate tectonics only permits small deformations in the lithospheric plates, the creep of the lithosphere is transient (non-steady-state). In this work, we study how the rheology of the lithosphere that possesses elasticity, brittleness (pseudo-plasticity), and creep affects the folding in the Earth's crust. Folding is caused by horizontal compression that results from the collision between the lithospheric plates. The effective viscosity characterizing the transient creep is lower than in the case of a steady-state creep and depends on the characteristic time of the considered process. The allowance for transient creep gives the distribution of the rheological properties of the horizontally compressed lithosphere in which the upper crust is brittle, whereas the lower crust and mantle lithosphere are dominated by transient creep. It is shown that the flows that arise in the lithosphere due to the instability under horizontal compression and cause folding are small-scale. These flows are concentrated in the upper brittle crust, they determine the short-wave Earth's surface topography, penetrate into the lower, creep-dominated crust to a shallow depth, and do not penetrate into the mantle. Therefore, these flows do not deform the Moho.

Lattice continuum and diffusional creep.

PubMed

Mesarovic, Sinisa Dj

2016-04-01

Diffusional creep is characterized by growth/disappearance of lattice planes at the crystal boundaries that serve as sources/sinks of vacancies, and by diffusion of vacancies. The lattice continuum theory developed here represents a natural and intuitive framework for the analysis of diffusion in crystals and lattice growth/loss at the boundaries. The formulation includes the definition of the Lagrangian reference configuration for the newly created lattice, the transport theorem and the definition of the creep rate tensor for a polycrystal as a piecewise uniform, discontinuous field. The values associated with each crystalline grain are related to the normal diffusional flux at grain boundaries. The governing equations for Nabarro-Herring creep are derived with coupled diffusion and elasticity with compositional eigenstrain. Both, bulk diffusional dissipation and boundary dissipation accompanying vacancy nucleation and absorption, are considered, but the latter is found to be negligible. For periodic arrangements of grains, diffusion formally decouples from elasticity but at the cost of a complicated boundary condition. The equilibrium of deviatorically stressed polycrystals is impossible without inclusion of interface energies. The secondary creep rate estimates correspond to the standard Nabarro-Herring model, and the volumetric creep is small. The initial (primary) creep rate is estimated to be much larger than the secondary creep rate.

Lattice continuum and diffusional creep

NASA Astrophysics Data System (ADS)

Mesarovic, Sinisa Dj.

2016-04-01

Diffusional creep is characterized by growth/disappearance of lattice planes at the crystal boundaries that serve as sources/sinks of vacancies, and by diffusion of vacancies. The lattice continuum theory developed here represents a natural and intuitive framework for the analysis of diffusion in crystals and lattice growth/loss at the boundaries. The formulation includes the definition of the Lagrangian reference configuration for the newly created lattice, the transport theorem and the definition of the creep rate tensor for a polycrystal as a piecewise uniform, discontinuous field. The values associated with each crystalline grain are related to the normal diffusional flux at grain boundaries. The governing equations for Nabarro-Herring creep are derived with coupled diffusion and elasticity with compositional eigenstrain. Both, bulk diffusional dissipation and boundary dissipation accompanying vacancy nucleation and absorption, are considered, but the latter is found to be negligible. For periodic arrangements of grains, diffusion formally decouples from elasticity but at the cost of a complicated boundary condition. The equilibrium of deviatorically stressed polycrystals is impossible without inclusion of interface energies. The secondary creep rate estimates correspond to the standard Nabarro-Herring model, and the volumetric creep is small. The initial (primary) creep rate is estimated to be much larger than the secondary creep rate.

Generation of plate tectonics via grain-damage and pinning

NASA Astrophysics Data System (ADS)

Bercovici, D.; Ricard, Y. R.

2012-12-01

Weakening and shear localization in the lithosphere are essential ingredients for understanding how and whether plate tectonics is generated from mantle convection on terrestrial planets. The grain-damage and pinning mechanism of Bercovici & Ricard (2012) for lithospheric shear--localization proposes that damage to the interface between phases in a polycrystalline material like peridotite (composed primarily of olivine and pyroxene) increases the number of small Zener pinning surfaces that constrain mineral grains to ever smaller sizes regardless of creep mechanism. This effect allows a self-softening feedback in which damage and grain-reduction can co-exist with a grain-size dependent diffusion creep rheology; moreoever, grain growth and weak-zone healing are greatly impeded by Zener pinning thereby leading to long-lived relic weak zones. This mechanism is employed in two-dimensional flow calculations to test its ability to generate toroidal (strike-slip) motion from convective type flow and to influence plate evolution. The fluid dynamical calculations employ source-sink driven flow as a proxy for convective poloidal flow (upwelling/downwelling and divergent/convergent motion), and the coupling of this flow with non-linear rheological mechanisms excites toroidal or strike-slip motion. The numerical experiments show that pure dislocation-creep rheology, and grain-damage without Zener pinning (as occurs in a single-phase assemblages) permit only weak localization and toroidal flow; however, the full grain-damage with pinning readily allows focussed localization and intense, plate-like toroidal motion and strike-slip deformation. Rapid plate motion changes are also tested with abrupt rotations of the source-sink field after a plate-like configuration is developed; the post-rotation flow and material property fields are found to never recover or lose memory of the original configuration, leading to suboptimally aligned plate boundaries (e.g., strike-slip margins non-parallel to plate motion), oblique subduction and highly localized, weak and long lived acute plate-boundary junctions such as at the Aleution-Kurile intersection. The grain-damage and pinning theory therefore readily satisfies key plate-tectonic metrics of localized toroidal motion and plate-boundary inheritance, and thus provides a predictive theory for the generation of plate tectonics on Earth and other planets. References: Bercovici, D., Ricard, Y., 2012. Mechanisms for the generation of plate tectonics by two-phase grain-damage and pinning. Phys. Earth Planet. Int. 202-203, 27--55.

Creep-fatigue modelling in structural steels using empirical and constitutive creep methods implemented in a strip-yield model

NASA Astrophysics Data System (ADS)

Andrews, Benjamin J.

The phenomena of creep and fatigue have each been thoroughly studied. More recently, attempts have been made to predict the damage evolution in engineering materials due to combined creep and fatigue loading, but these formulations have been strictly empirical and have not been used successfully outside of a narrow set of conditions. This work proposes a new creep-fatigue crack growth model based on constitutive creep equations (adjusted to experimental data) and Paris law fatigue crack growth. Predictions from this model are compared to experimental data in two steels: modified 9Cr-1Mo steel and AISI 316L stainless steel. Modified 9Cr-1Mo steel is a high-strength steel used in the construction of pressure vessels and piping for nuclear and conventional power plants, especially for high temperature applications. Creep-fatigue and pure creep experimental data from the literature are compared to model predictions, and they show good agreement. Material constants for the constitutive creep model are obtained for AISI 316L stainless steel, an alloy steel widely used for temperature and corrosion resistance for such components as exhaust manifolds, furnace parts, heat exchangers and jet engine parts. Model predictions are compared to pure creep experimental data, with satisfactory results. Assumptions and constraints inherent in the implementation of the present model are examined. They include: spatial discretization, similitude, plane stress constraint and linear elasticity. It is shown that the implementation of the present model had a non-trivial impact on the model solutions in 316L stainless steel, especially the spatial discretization. Based on these studies, the following conclusions are drawn: 1. The constitutive creep model consistently performs better than the Nikbin, Smith and Webster (NSW) model for predicting creep and creep-fatigue crack extension. 2. Given a database of uniaxial creep test data, a constitutive material model such as the one developed for modified 9Cr-1Mo can be developed for other materials. 3. Due to the assumptions used to develop the strip-yield model, model predictions are expected to show some scatter, especially in some situations. Several areas of future research are proposed from these conclusions: 1. Alternative methods for predicting fatigue crack growth, especially a constitutive fatigue crack growth model, 2. Continued development of new material models and refinement the existing ones, and 3. Implementation of the present creep-fatigue model as a user-defined subroutine in a finite element solver.

Environmental degradation of 316 stainless steel in high temperature low cycle fatigue

NASA Technical Reports Server (NTRS)

Kalluri, Sreeramesh; Manson, S. Stanford; Halford, Gary R.

1987-01-01

Procedures based on modification of the conventional Strainrange Partitioning method are proposed to characterize the time-dependent degradation of engineering alloys in high-temperature, low-cycle fatigue. Creep-fatigue experiments were conducted in air using different waveforms of loading on 316 stainless steel at 816 C (1500 F) to determine the effect of exposure time on cyclic life. Reductions in the partitioned cyclic lives were observed with an increase in the time of exposure (or with the corresponding decrease in the steady-state creep rate) for all the waveforms involving creep strain. Excellent correlations of the experimental data were obtained by modifying the Conventional Strainrange Partitioning life relationships involving creep strain using a power-law term of either: (1) time of exposure, or (2) steady-state creep rate of the creep-fatigue test. Environmental degradation due to oxidation, material degradation due to the precipitation of carbides along the grain boundaries and detrimental deformation modes associated with the prolonged periods of creep were observed to be the main mechanisms responsible for life reductions at long exposure times.

DaDyn-RS: a tool for the time-dependent simulation of damage, fluid pressure and long-term instability in alpine rock slopes

NASA Astrophysics Data System (ADS)

Riva, Federico; Agliardi, Federico; Amitrano, David; Crosta, Giovanni B.

2017-04-01

Large mountain slopes in alpine environments undergo a complex long-term evolution from glacial to postglacial environments, through a transient period of paraglacial readjustment. During and after this transition, the interplay among rock strength, topographic relief, and morpho-climatic drivers varying in space and time can lead to the development of different types of slope instability, from sudden catastrophic failures to large, slow, long-lasting yet potentially catastrophic rockslides. Understanding the long-term evolution of large rock slopes requires accounting for the time-dependence of deglaciation unloading, permeability and fluid pressure distribution, displacements and failure mechanisms. In turn, this is related to a convincing description of rock mass damage processes and to their transition from a sub-critical (progressive failure) to a critical (catastrophic failure) character. Although mechanisms of damage occurrence in rocks have been extensively studied in the laboratory, the description of time-dependent damage under gravitational load and variable external actions remains difficult. In this perspective, starting from a time-dependent model conceived for laboratory rock deformation, we developed Dadyn-RS, a tool to simulate the long-term evolution of real, large rock slopes. Dadyn-RS is a 2D, FEM model programmed in Matlab, which combines damage and time-to-failure laws to reproduce both diffused damage and strain localization meanwhile tracking long-term slope displacements from primary to tertiary creep stages. We implemented in the model the ability to account for rock mass heterogeneity and property upscaling, time-dependent deglaciation, as well as damage-dependent fluid pressure occurrence and stress corrosion. We first tested DaDyn-RS performance on synthetic case studies, to investigate the effect of the different model parameters on the mechanisms and timing of long-term slope behavior. The model reproduces complex interactions between topography, deglaciation rate, mechanical properties and fluid pressure occurrence, resulting in different kinematics, damage patterns and timing of slope instabilities. We assessed the role of groundwater on slope damage and deformation mechanisms by introducing time-dependent pressure cycling within simulations. Then, we applied DaDyn-RS to real slopes located in the Italian Central Alps, affected by an active rockslide and a Deep Seated Gravitational Slope Deformation, respectively. From Last Glacial Maximum to present conditions, our model allows reproducing in an explicitly time-dependent framework the progressive development of damage-induced permeability, strain localization and shear band differentiation at different times between the Lateglacial period and the Mid-Holocene climatic transition. Different mechanisms and timings characterize different styles of slope deformations, consistently with available dating constraints. DaDyn-RS is able to account for different long-term slope dynamics, from slow creep to the delayed transition to fast-moving rockslides.

Viscous Creep in Dry Unconsolidated Gulf of Mexico Shale

NASA Astrophysics Data System (ADS)

Chang, C.; Zoback, M. D.

2002-12-01

We conducted laboratory experiments to investigate creep characteristics of dry unconsolidated shale recovered from the pathfinder well, Gulf of Mexico (GOM). We subjected jacketed cylindrical specimens (25.4 mm diameter) to hydrostatic pressure that increased from 10 to 50 MPa in steps of 5 MPa. We kept the pressure constant in each step for at least 6 hours and measured axial and lateral strains (provided by LVDTs) and ultrasonic velocities (provided by seismic-wave transducers). The dry shale exhibited pronounced creep strain at all pressure levels, indicating that the dry frame of the shale possesses an intrinsic viscous property. Interestingly, the creep behavior of the shale is different above and below 30 MPa confining pressure. Above 30 MPa, the amount of creep strain in 6 hours is nearly constant with equal pressurization steps, indicating a linear viscous rheology. Below 30 MPa, the amount of creep increases linearly as pressure is raised in constant incremental steps, suggesting that the creep deformation accelerates as pressure increases within this pressure range. Thus, the general creep behavior of the GOM shale is characterized by a bilinear dependence on pressure magnitude. This creep characteristic is quite different from that observed in unconsolidated reservoir sands (Hagin and Zoback, 2002), which exhibited nearly constant amount of creep regardless of the pressure magnitude for equal increasing steps of pressure. The shale exhibits a lack of creep (and nearly negligible strain recovery) when unloaded, suggesting that the creep strain is irrecoverable and can be considered viscoplastic deformation. SEM observations show that the major mechanism of compaction of the dry shale appears to be packing of clay and a progressive collapse of pore (void) spaces. Creep compaction is considerably more significant than compaction that occurs instantaneously, indicating that the process of shale compaction is largely time-dependent.

Damage mechanisms in alloy 800H under creep-fatigue conditions

NASA Astrophysics Data System (ADS)

Mu, Z.; Bothe, K.; Gerold, V.

1994-05-01

The interaction between fatigue damage (i.e., fatigue crack propagation) and internal grain boundary damage (i.e., cavity formation at grain boundaries) has been studied for the Alloy 800H at 750 C for constant plastic strain ranges but different experimental conditions. Most experiments were performed at constant ranges of alternating tensile/compression stresses. Symmetrical as well as asymmetrical tests (with larger compression stresses) were performed. In comparison to the former tests, asymmetrical tests led to shorter cyclic lifetimes mainly due to cavity formation which was not observed for symmetrical tests. It could be shown that a fast compressive and a slow tensile half cycle (at large compressive and low tensile stresses) are ideal conditions for the nucleation and growth of cavities. Based on quantitative measurements of the cavity density from interrupted fatigue tests, a physical model is presented which can predict the number of cycles to failure. This cycle number is determined only by fatigue crack growth which is controlled by (1) athermal plastic deformation, (2) creep deformation and (3) rate enhancement by cavitation.

Microstructural Effects on Creep-Fatigue Life of Alloy 709

DOE Office of Scientific and Technical Information (OSTI.GOV)

McMurtrey, Michael; Carroll, Laura; Wright, Jill

Creep-fatigue tests were performed on plates of Alloy 709 from various heats and processing conditions, but often with inhomogeneous microstructures. After testing, metallographic analysis was performed and the specimens were generally found to either have a uniform grain size or a bimodal grain size distribution with either isolated or groups (bands) of large grains. Creep-fatigue life was characterized with respect to the length of the grain boundary perpendicular to the stress axis, and it was found that large grains (>400 μm) tended to be detrimental to creep-fatigue life, with the exception of elongated (parallel to the stress axis) grains andmore » some specimens that underwent additional annealing.« less

Understanding the mechanisms of amorphous creep through molecular simulation

NASA Astrophysics Data System (ADS)

Cao, Penghui; Short, Michael P.; Yip, Sidney

2017-12-01

Molecular processes of creep in metallic glass thin films are simulated at experimental timescales using a metadynamics-based atomistic method. Space-time evolutions of the atomic strains and nonaffine atom displacements are analyzed to reveal details of the atomic-level deformation and flow processes of amorphous creep in response to stress and thermal activations. From the simulation results, resolved spatially on the nanoscale and temporally over time increments of fractions of a second, we derive a mechanistic explanation of the well-known variation of creep rate with stress. We also construct a deformation map delineating the predominant regimes of diffusional creep at low stress and high temperature and deformational creep at high stress. Our findings validate the relevance of two original models of the mechanisms of amorphous plasticity: one focusing on atomic diffusion via free volume and the other focusing on stress-induced shear deformation. These processes are found to be nonlinearly coupled through dynamically heterogeneous fluctuations that characterize the slow dynamics of systems out of equilibrium.

Analytical, Numerical, and Experimental Investigation on a Non-Contact Method for the Measurements of Creep Properties of Ultra-High-Temperature Materials

NASA Technical Reports Server (NTRS)

Lee, Jonghyun; Hyers, Robert W.; Rogers, Jan R.; Rathz, Thomas J.; Choo, Hahn; Liaw, Peter

2006-01-01

Responsive access to space requires re-use of components such as rocket nozzles that operate at extremely high temperatures. For such applications, new ultra-hightemperature materials that can operate over 2,000 C are required. At the temperatures higher than the fifty percent of the melting temperature, the characterization of creep properties is indispensable. Since conventional methods for the measurement of creep is limited below 1,700 C, a new technique that can be applied at higher temperatures is strongly demanded. This research develops a non-contact method for the measurement of creep at the temperatures over 2,300 C. Using the electrostatic levitator in NASA MSFC, a spherical sample was rotated to cause creep deformation by centrifugal acceleration. The deforming sample was captured with a digital camera and analyzed to measure creep deformation. Numerical and analytical analyses have also been conducted to compare the experimental results. Analytical, numerical, and experimental results showed a good agreement with one another.

Linking the fractional derivative and the Lomnitz creep law to non-Newtonian time-varying viscosity

NASA Astrophysics Data System (ADS)

Pandey, Vikash; Holm, Sverre

2016-09-01

Many of the most interesting complex media are non-Newtonian and exhibit time-dependent behavior of thixotropy and rheopecty. They may also have temporal responses described by power laws. The material behavior is represented by the relaxation modulus and the creep compliance. On the one hand, it is shown that in the special case of a Maxwell model characterized by a linearly time-varying viscosity, the medium's relaxation modulus is a power law which is similar to that of a fractional derivative element often called a springpot. On the other hand, the creep compliance of the time-varying Maxwell model is identified as Lomnitz's logarithmic creep law, making this possibly its first direct derivation. In this way both fractional derivatives and Lomnitz's creep law are linked to time-varying viscosity. A mechanism which yields fractional viscoelasticity and logarithmic creep behavior has therefore been found. Further, as a result of this linking, the curve-fitting parameters involved in the fractional viscoelastic modeling, and the Lomnitz law gain physical interpretation.

Linking the fractional derivative and the Lomnitz creep law to non-Newtonian time-varying viscosity.

PubMed

Pandey, Vikash; Holm, Sverre

2016-09-01

Many of the most interesting complex media are non-Newtonian and exhibit time-dependent behavior of thixotropy and rheopecty. They may also have temporal responses described by power laws. The material behavior is represented by the relaxation modulus and the creep compliance. On the one hand, it is shown that in the special case of a Maxwell model characterized by a linearly time-varying viscosity, the medium's relaxation modulus is a power law which is similar to that of a fractional derivative element often called a springpot. On the other hand, the creep compliance of the time-varying Maxwell model is identified as Lomnitz's logarithmic creep law, making this possibly its first direct derivation. In this way both fractional derivatives and Lomnitz's creep law are linked to time-varying viscosity. A mechanism which yields fractional viscoelasticity and logarithmic creep behavior has therefore been found. Further, as a result of this linking, the curve-fitting parameters involved in the fractional viscoelastic modeling, and the Lomnitz law gain physical interpretation.

Implications of Microstructural Studies of the SAFOD Gouge for the Strength and Deformation Mechanisms in the Creeping Segment of the San Andreas Fault

NASA Astrophysics Data System (ADS)

Hadizadeh, J.; Gratier, J. L.; Mittempergher, S.; Renard, F.; Richard, J.; di Toro, G.; Babaie, H. A.

2010-12-01

The San Andreas Fault zone (SAF) in the vicinity of the San Andreas Fault Observatory at Depth (SAFOD)in central California is characterized by an average 21 mm/year aseismic creep and strain release through repeating M<3 earthquakes. Seismic inversion studies indicate that the ruptures occur on clusters of stationary patches making up 1% or less of the total fault surface area. The existence of these so-called asperity patches, although not critical in determining the fault strength, suggests interaction of different deformation mechanisms. What are the deformation mechanisms, and how do the mechanisms couple and factor into the current strength models for the SAF? The SAFOD provides core samples and geophysical data including cores from two shear zones where the main borehole casing is deforming. The studies so far show a weak fault zone with about 200m of low-permeability damage zone without anomalous temperature or high fluid pressure (Zoback et al. EOS 2010). To answer the above questions, we studied core samples and thin sections ranging in measured depths (MD) from 3059m to 3991m including gouge from borehole casing deformation zones. The methods of study included high resolution scanning and transmission electron microscopy, cathodoluminescence imaging, X-ray fluorescence mapping, and energy dispersive X-ray spectroscopy. The microstructural and analytical data suggest that deformation is by a coupling of cataclastic flow and pressure solution accompanied by widespread alteration of feldspar to clay minerals and other neomineralizations. The clay contents of the gouge and streaks of serpentinite are not uniformly distributed, but weakness of the creeping segment is likely to be due to intrinsically low frictional strength of the fault material. This conclusion, which is based on the overall ratio of clay/non-clay constituents and the presence of talc in the actively deforming zones, is consistent with the 0.3-0.45 coefficient of friction for the drill cuttings tested by others. We also considered weakening by diffusion-accommodated grain boundary sliding. There are two main trends in the microstructural data that provide a basis for explaining the creep rate and seismic activity: 1. Clay content of the gouge including serpentinite and talc increases toward the 1-3m wide borehole casing deformation zones, which are expected to be deforming at above the average creep rate 2. Evidence of pressure solution creep and fracture sealing is more abundant in the siltstone cataclasites than in the shale. Such rocks could act as rigid inclusions that are repeatedly loaded to seismic failure by creep of the surrounding clay gouge. Regular cycles of fracture and restrengthening by fracture sealing in and around the inclusions are thus expected. The inclusions may be viewed as asperity patches (or cluster of patches) that predominantly deform by pressure solution at below the average creep rate.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wereszczak, A.A.; Ferber, M.K.; Kirkland, T.P.

Several yttria-fluxed, hot-isostatically pressed (HIPed) silicon nitrides have been tensile creep tested at temperatures representative of gas turbine engines. Creep and oxidation assisted damage mechanisms concurrently evolve when these materials are tested at high temperatures and low stresses (i.e., long exposure times at temperature). Atmospheric creep testing results in creation of oxygen and yttrium gradients across the radial dimension. High concentrations of oxygen and yttrium coincide with dense populations of lenticular-shaped cavities near the surface of crept specimens. The center of the tensile specimens was devoid of oxygen or yttrium; in addition, lenticular cavities were rare. The gradient in lenticular-cavitymore » concentration is coincident with the oxygen and yttrium gradients. Stress corrosion cracking (SCC) also occurs in these HIPed silicon nitrides when they are subjected to stress at high temperatures in ambient air. The size of this damage zone increases when the temperature is higher and/or the applied stress is lower. Stress-corrosion cracking initiates at the surface of the tensile specimen and advances radially inwards. What nucleates SCC has not yet been identified, but it is believed to result from a stress-concentrator (e.g., machining damage) at the surface and its growth is a result of coalescence of microcracks and cavities. The higher concentration of oxygen and yttrium in the grain boundaries near the specimen`s surface lessens the local high temperature mechanical integrity; this is believed to be associated with the growth of the SCC zone. This SCC zone continues to grow in size during tensile loading until it reaches a critical size which causes fracture.« less

Reliability and Creep/Fatigue Analysis of a CMC Component

NASA Technical Reports Server (NTRS)

Murthy, Pappu L. N.; Mital, Subodh K.; Gyekenyesi, John Z.; Gyekenyesi, John P.

2007-01-01

High temperature ceramic matrix composites (CMC) are being explored as viable candidate materials for hot section gas turbine components. These advanced composites can potentially lead to reduced weight and enable higher operating temperatures requiring less cooling; thus leading to increased engine efficiencies. There is a need for convenient design tools that can accommodate various loading conditions and material data with their associated uncertainties to estimate the minimum predicted life as well as the failure probabilities of a structural component. This paper presents a review of the life prediction and probabilistic analyses performed for a CMC turbine stator vane. A computer code, NASALife, is used to predict the life of a 2-D woven silicon carbide fiber reinforced silicon carbide matrix (SiC/SiC) turbine stator vane due to a mission cycle which induces low cycle fatigue and creep. The output from this program includes damage from creep loading, damage due to cyclic loading and the combined damage due to the given loading cycle. Results indicate that the trends predicted by NASALife are as expected for the loading conditions used for this study. In addition, a combination of woven composite micromechanics, finite element structural analysis and Fast Probability Integration (FPI) techniques has been used to evaluate the maximum stress and its probabilistic distribution in a CMC turbine stator vane. Input variables causing scatter are identified and ranked based upon their sensitivity magnitude. Results indicate that reducing the scatter in proportional limit strength of the vane material has the greatest effect in improving the overall reliability of the CMC vane.

Mechanisms of High-Temperature Fatigue Failure in Alloy 800H

NASA Technical Reports Server (NTRS)

BhanuSankaraRao, K.; Schuster, H.; Halford, G. R.

1996-01-01

The damage mechanisms influencing the axial strain-controlled Low-Cycle Fatigue (LCF) behavior of alloy 800H at 850 C have been evaluated under conditions of equal tension/compression ramp rates (Fast-Fast (F-F): 4 X 10(sup -3)/s and Slow-Slow (S-S): 4 X 10(sup -5)/s) and asymmetrical ramp rates (Fast-Slow (F-S): 4 x 10(sup -3)/s / 4 X 10(sup -5/s and Slow-Fast (S-F): 4 X 10(sup -5) / 4 X 10(sup -3)/s) in tension and compression. The fatigue life, cyclic stress response, and fracture modes were significantly influenced by the waveform shape. The fatigue lives displayed by different loading conditions were in the following order: F-F greater than S-S greater than F-S greater than S-F. The fracture mode was dictated by the ramp rate adopted in the tensile direction. The fast ramp rate in the tensile direction led to the occurrence of transgranular crack initiation and propagation, whereas the slow ramp rate caused intergranular initiation and propagation. The time-dependent processes and their synergistic interactions, which were at the basis of observed changes in cyclic stress response and fatigue life, were identified. Oxidation, creep damage, dynamic strain aging, massive carbide precipitation, time-dependent creep deformation, and deformation ratcheting were among the several factors influencing cyclic life. Irrespective of the loading condition, the largest effect on life was exerted by oxidation processes. Deformation ratcheting had its greatest influence on life under asymmetrical loading conditions. Creep damage accumulated the greatest amount during the slow tensile ramp under S-F conditions.

Creep of plain weave polymer matrix composites

NASA Astrophysics Data System (ADS)

Gupta, Abhishek

Polymer matrix composites are increasingly used in various industrial sectors to reduce structural weight and improve performance. Woven (also known as textile) composites are one class of polymer matrix composites with increasing market share mostly due to their lightweight, their flexibility to form into desired shape, their mechanical properties and toughness. Due to the viscoelasticity of the polymer matrix, time-dependent degradation in modulus (creep) and strength (creep rupture) are two of the major mechanical properties required by engineers to design a structure reliably when using these materials. Unfortunately, creep and creep rupture of woven composites have received little attention by the research community and thus, there is a dire need to generate additional knowledge and prediction models, given the increasing market share of woven composites in load bearing structural applications. Currently, available creep models are limited in scope and have not been validated for any loading orientation and time period beyond the experimental time window. In this thesis, an analytical creep model, namely the Modified Equivalent Laminate Model (MELM), was developed to predict tensile creep of plain weave composites for any orientation of the load with respect to the orientation of the fill and warp fibers, using creep of unidirectional composites. The ability of the model to predict creep for any orientation of the load is a "first" in this area. The model was validated using an extensive experimental involving the tensile creep of plain weave composites under varying loading orientation and service conditions. Plain weave epoxy (F263)/ carbon fiber (T300) composite, currently used in aerospace applications, was procured as fabrics from Hexcel Corporation. Creep tests were conducted under two loading conditions: on-axis loading (0°) and off-axis loading (45°). Constant load creep, in the temperature range of 80-240°C and stress range of 1-70% UTS of the composites, was experimentally evaluated for time periods ranging from 1--120 hours under both loading conditions. The composite showed increase in creep with increase in temperature and stress. Creep of composite increased with increase in angle of loading, from 1% under on-axis loading to 31% under off-axis loading, within the tested time window. The experimental creep data for plain weave composites were superposed using TTSP (Time Temperature Superposition Principle) to obtain a master curve of experimental data extending to several years and was compared with model predictions to validate the model. The experimental and model results were found in good agreement within an error range of +/-1-3% under both loading conditions. A parametric study was also conducted to understand the effect of microstructure of plain weave composites on its on-axis and off-axis creep. Generation of knowledge in this area is also "first". Additionally, this thesis generated knowledge on time-dependent damage m woven composites and its effect on creep and tensile properties and their prediction.

Results of studying creep and long-term strength of metals at the Institute of Mechanics at the Lomonosov Moscow State University (To Yu. N. Rabotnov's Anniversary)

NASA Astrophysics Data System (ADS)

Lokoshchenko, A. M.

2014-01-01

Basic results of experimental and theoretical research of creep processes and long-term strength of metals obtained by researchers of the Institute of Mechanics at the Lomonosov Moscow State University are presented. These results further develop and refine the kinetic theory of creep and long-duration strength proposed by Yu. N. Rabotnov. Some problems arising in formulating various types of kinetic equations and describing experimental data for materials that can be considered as statically homogeneous materials (in studying the process of deformation and rupture of such materials, there is no need to study the evolution of individual cracks) are considered. The main specific features of metal creep models at constant and variable stresses, in uniaxial and complex stress states, and with allowance for one or two damage parameters are described. Criterial and kinetic approaches used to determine long-term strength under conditions of a complex stress state are considered. Methods of modeling the metal behavior in an aggressive medium are described. A possibility of using these models for solving engineering problems is demonstrated.

Influence of Constituents on Creep Properties of SiC/SiC Composites

NASA Technical Reports Server (NTRS)

Bhatt, R.; DiCarlo, J.

2016-01-01

SiC-SiC composites are being considered as potential candidate materials for next generation turbine components such as combustor liners, nozzle vanes and blades because of their low density, high temperature capability, and tailorable mechanical properties. These composites are essentially fabricated by infiltrating matrix into a stacked array of fibers or fiber preform by one or a combination of manufacturing methods such as, Melt Infiltration (MI) of molten silicon metal, Chemical Vapor Infiltration (CVI), Polymer Infiltration and Pyrolysis (PIP). To understand the influence of constituents, the SiC-SiC composites fabricated by MI, CVI, and PIP methods were creep tested in air between 12000 and 14500 degrees Centigrade for up to 500 hours. The failed specimens were analyzed under a scanning electron microscope to assess damage mechanisms. Also, knowing the creep deformation parameters of the fiber and the matrix under the testing conditions, the creep behavior of the composites was modeled and compared with the measured data. The implications of the results on the long term durability of these composites will be discussed.

Damage mechanisms in bithermal and thermomechanical fatigue of Haynes 188

NASA Technical Reports Server (NTRS)

Kalluri, Sreeramesh; Halford, Gary R.

1992-01-01

Post failure fractographic and metallographic studies were conducted on Haynes 188 specimens fatigued under bithermal and thermomechanical loading conditions between 316 and 760 C. Bithermal fatigue specimens examined included those tested under high strain rate in-phase and out-phase, tensile creep in-phase, and compressive creep out-of-phase loading conditions. Specimens tested under in-phase and out-of-phase thermomechanical fatigue were also examined. The nature of failure mode (transgrandular versus intergranular), the topography of the fracture surface, and the roles of oxidation and metallurgical changes were studied for each type of bithermal and thermomechanical test.

Lattice continuum and diffusional creep

PubMed Central

2016-01-01

Diffusional creep is characterized by growth/disappearance of lattice planes at the crystal boundaries that serve as sources/sinks of vacancies, and by diffusion of vacancies. The lattice continuum theory developed here represents a natural and intuitive framework for the analysis of diffusion in crystals and lattice growth/loss at the boundaries. The formulation includes the definition of the Lagrangian reference configuration for the newly created lattice, the transport theorem and the definition of the creep rate tensor for a polycrystal as a piecewise uniform, discontinuous field. The values associated with each crystalline grain are related to the normal diffusional flux at grain boundaries. The governing equations for Nabarro–Herring creep are derived with coupled diffusion and elasticity with compositional eigenstrain. Both, bulk diffusional dissipation and boundary dissipation accompanying vacancy nucleation and absorption, are considered, but the latter is found to be negligible. For periodic arrangements of grains, diffusion formally decouples from elasticity but at the cost of a complicated boundary condition. The equilibrium of deviatorically stressed polycrystals is impossible without inclusion of interface energies. The secondary creep rate estimates correspond to the standard Nabarro–Herring model, and the volumetric creep is small. The initial (primary) creep rate is estimated to be much larger than the secondary creep rate. PMID:27274696

Diallelic nuclear microsatellites for diversity and population analyses of the allotraploid creeping bentgrass (Agrostis stolonifera)

EPA Science Inventory

Nine diallelic nuclear microsatellite loci were characterized in creeping bentgrass, Agrostis stolonifera L. (2n=4x=28, A2A2A3A3). Markers were developed for analyses of diversity and population biology of A. stolonifera. They may also help with identification of germplasm resour...

A coupled creep plasticity model for residual stress relaxation of a shot-peened nickel-based superalloy

NASA Astrophysics Data System (ADS)

Buchanan, Dennis J.; John, Reji; Brockman, Robert A.; Rosenberger, Andrew H.

2010-01-01

Shot peening is a commonly used surface treatment process that imparts compressive residual stresses into the surface of metal components. Compressive residual stresses retard initiation and growth of fatigue cracks. During component loading history, shot-peened residual stresses may change due to thermal exposure, creep, and cyclic loading. In these instances, taking full credit for compressive residual stresses would result in a nonconservative life prediction. This article describes a methodical approach for characterizing and modeling residual stress relaxation under elevated temperature loading, near and above the monotonic yield strength of INI 00. The model incorporates the dominant creep deformation mechanism, coupling between the creep and plasticity models, and effects of prior plastic strain to simulate surface treatment deformation.

FY17 Status Report on the Micromechanical Finite Element Modeling of Creep Fracture of Grade 91 Steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Messner, M. C.; Truster, T. J.; Cochran, K. B.

Advanced reactors designed to operate at higher temperatures than current light water reactors require structural materials with high creep strength and creep-fatigue resistance to achieve long design lives. Grade 91 is a ferritic/martensitic steel designed for long creep life at elevated temperatures. It has been selected as a candidate material for sodium fast reactor intermediate heat exchangers and other advanced reactor structural components. This report focuses on the creep deformation and rupture life of Grade 91 steel. The time required to complete an experiment limits the availability of long-life creep data for Grade 91 and other structural materials. Design methodsmore » often extrapolate the available shorter-term experimental data to longer design lives. However, extrapolation methods tacitly assume the underlying material mechanisms causing creep for long-life/low-stress conditions are the same as the mechanisms controlling creep in the short-life/high-stress experiments. A change in mechanism for long-term creep could cause design methods based on extrapolation to be non-conservative. The goal for physically-based microstructural models is to accurately predict material response in experimentally-inaccessible regions of design space. An accurate physically-based model for creep represents all the material mechanisms that contribute to creep deformation and damage and predicts the relative influence of each mechanism, which changes with loading conditions. Ideally, the individual mechanism models adhere to the material physics and not an empirical calibration to experimental data and so the model remains predictive for a wider range of loading conditions. This report describes such a physically-based microstructural model for Grade 91 at 600° C. The model explicitly represents competing dislocation and diffusional mechanisms in both the grain bulk and grain boundaries. The model accurately recovers the available experimental creep curves at higher stresses and the limited experimental data at lower stresses, predominately primary creep rates. The current model considers only one temperature. However, because the model parameters are, for the most part, directly related to the physics of fundamental material processes, the temperature dependence of the properties are known. Therefore, temperature dependence can be included in the model with limited additional effort. The model predicts a mechanism shift for 600° C at approximately 100 MPa from a dislocation- dominated regime at higher stress to a diffusion-dominated regime at lower stress. This mechanism shift impacts the creep life, notch-sensitivity, and, likely, creep ductility of Grade 91. In particular, the model predicts existing extrapolation methods for creep life may be non-conservative when attempting to extrapolate data for higher stress creep tests to low stress, long-life conditions. Furthermore, the model predicts a transition from notchstrengthening behavior at high stress to notch-weakening behavior at lower stresses. Both behaviors may affect the conservatism of existing design methods.« less

High temperature behavior of B2-based ruthenium aluminide systems

NASA Astrophysics Data System (ADS)

Cao, Fang

Ru-modified NiAl-based bond coats have the potential to improve the durability of Superalloy-Thermal Barrier Coating systems (TBCs) for advanced gas turbine engines. A fundamental understanding of the high temperature mechanical behavior across the Ni-Al-Ru B2 phase field can provide direction for the development of these new bond coats for TBCs. The purpose of this study has been to describe the fundamental processes of creep deformation in single phase B2 Ru-Al-Ni ternary alloys which would form the basis for the bond coats. To accomplish this, five ternary alloys with compositions located within the B2 field across the NiAl-RuAl phase region were fabricated and investigated. Special emphasis was placed on characterizing creep deformation and describing the operative creep mechanisms in these alloys. At room temperature, brittle failure was observed in the Ni-rich alloys in compression, while improved strength and ductility were displayed in two Ru-rich ternary alloys at temperatures up to 700°C. Exceptional creep strength was observed in these alloys, as compared to other high melting temperature B2 intermetallics. A continuous increase of the melting temperature and creep resistance with the increasing of the Ru/Ni ratio in these alloys was observed. Post-creep dislocation analyses identified the presence of <100> and <110> edge dislocations in the Ni-rich alloys, while uniformly distributed jogged <100> screw dislocations predominated in the Ru-rich ternary alloys. A transition of the creep mechanism from viscous glide controlled to jogged screw motion in these Ru-Al-Ni ternary B2 alloys with increasing Ru/Ni ratio is demonstrated by the characteristics of the creep deformation process, stress change creep tests, post-creep dislocation analyses, and numerical modeling. Additionally, the knowledge of the cyclic oxidation behavior of ruthenium aluminide-based alloy is essential, as many high-temperature applications for which this intermetallic might be utilized undergo repeated severe thermal cycling. Thus the second portion of this thesis focuses on the characterization of the cyclic oxidation properties of RuAl-based alloys. The cyclic oxidation behavior of six RuAl-based alloys was studied in air over the temperature range of 1000°C to 1300°C. Oxidation kinetics have been shown to be influenced by microstructure as well as the addition of platinum.

A potential drop strain sensor for in-situ power station creep monitoring

NASA Astrophysics Data System (ADS)

Corcoran, Joseph; Cawley, Peter; Nagy, Peter B.

2014-02-01

Creep is a high temperature damage mechanism of interest to the power industry and at present lacks a satisfactory inspection technique. Existing material inspection techniques are extremely laborious while strain measurements rely on often infrequent off-load measurements. A quasi-DC directional potential drop technique has been suggested that is able to suppress the effects of permeability and is primarily sensitive to changes in resistivity and also the geometry that will develop through strain. The change in creep related resistivity is shown by an equivalent effective resistivity approach to be small at <2% change when compared to the >100% change in transfer resistance that occurs due to strain as observed in laboratory tests. A biaxial inversion is then presented and demonstrated on in-lab samples showing good performance. The result is a sensor that performs as a very robust high temperature strain gauge.

Creep-Fatigue Failure Diagnosis

PubMed Central

Holdsworth, Stuart

2015-01-01

Failure diagnosis invariably involves consideration of both associated material condition and the results of a mechanical analysis of prior operating history. This Review focuses on these aspects with particular reference to creep-fatigue failure diagnosis. Creep-fatigue cracking can be due to a spectrum of loading conditions ranging from pure cyclic to mainly steady loading with infrequent off-load transients. These require a range of mechanical analysis approaches, a number of which are reviewed. The microstructural information revealing material condition can vary with alloy class. In practice, the detail of the consequent cracking mechanism(s) can be camouflaged by oxidation at high temperatures, although the presence of oxide on fracture surfaces can be used to date events leading to failure. Routine laboratory specimen post-test examination is strongly recommended to characterise the detail of deformation and damage accumulation under known and well-controlled loading conditions to improve the effectiveness and efficiency of failure diagnosis. PMID:28793676

Simulation of irradiation creep

DOE Office of Scientific and Technical Information (OSTI.GOV)

Reiley, T.C.; Jung, P.

1977-01-01

The results to date in the area of radiation enhanced deformation using beams of light ions to simulate fast neutron displacement damage are reviewed. A comparison is made between these results and those of in-reactor experiments. Particular attention is given to the displacement rate calculations for light ions and the electronic energy losses and their effect on the displacement cross section. Differences in the displacement processes for light ions and neutrons which may effect the irradiation creep process are discussed. The experimental constraints and potential problem areas associated with these experiments are compared to the advantages of simulation. Support experimentsmore » on the effect of thickness on thermal creep are presented. A brief description of the experiments in progress is presented for the following laboratories: HEDL, NRL, ORNL, PNL, U. of Lowell/MIT in the United States, AERE Harwell in the United Kingdom, CEN Saclay in France, GRK Karlsruhe and KFA Julich in West Germany.« less

Effect of tooth bleaching agents on protein content and mechanical properties of dental enamel.

PubMed

Elfallah, Hunida M; Bertassoni, Luiz E; Charadram, Nattida; Rathsam, Catherine; Swain, Michael V

2015-07-01

This study investigated the effect of two bleaching agents, 16% carbamide peroxide (CP) and 35% hydrogen peroxide (HP), on the mechanical properties and protein content of human enamel from freshly extracted teeth. The protein components of control and treated enamel were extracted and examined on sodium dodecyl sulfate polyacrylamide gel electrophoresis (SDS-PAGE). Marked reduction of the protein matrix and random fragmentation of the enamel proteins after bleaching treatments was found. The mechanical properties were analyzed with Vickers indentations to characterize fracture toughness, and nanoindentation to establish enamel hardness, elastic modulus and creep deformation. Results indicate that the hardness and elastic modulus of enamel were significantly reduced after treatment with CP and HP. After bleaching, the creep deformation at maximum load increased and the recovery upon unloading reduced. Crack lengths of CP and HP treated enamel were increased, while fracture toughness decreased. Additionally, the microstructures of fractured and indented samples were examined with field emission gun scanning electron microscopy (FEG-SEM) showing distinct differences in the fracture surface morphology between pre- and post-bleached enamel. In conclusion, tooth bleaching agents can produce detrimental effects on the mechanical properties of enamel, possibly as a consequence of damaging or denaturing of its protein components. Copyright © 2015 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

Irradiation effect on mechanical properties in structural materials of fast breeder reactor plant

NASA Astrophysics Data System (ADS)

Nagae, Yuji; Takaya, Shigeru; Wakai, Eiichi; Aoto, Kazumi

2011-07-01

The effects of displacement per atom (dpa) level, helium content, and the ratio of helium content to dpa level on the tensile and creep properties have been investigated in the assumed irradiation damage range of FBR structural materials. The assumed irradiation damage range is up to about 1 dpa and about 30 appm for helium content. Austenitic stainless steel and high-chromium martensitic steel are considered as FBR structural materials. As a result, it is shown that the dpa level is a promising index for evaluating neutron irradiation damage.

Evolution of the substructure of a novel 12% Cr steel under creep conditions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yadav, Surya Deo, E-mail: surya.yadav@tugraz.at; Kalácska, Szilvia, E-mail: kalacska@metal.elte.hu; Dománková, Mária, E-mail: maria.domankova@stuba.sk

2016-05-15

In this work we study the microstruture evolution of a newly developed 12% Cr martensitic/ferritic steel in as-received condition and after creep at 650 °C under 130 MPa and 80 MPa. The microstructure is described as consisting of mobile dislocations, dipole dislocations, boundary dislocations, precipitates, lath boundaries, block boundaries, packet boundaries and prior austenitic grain boundaries. The material is characterized employing light optical microscopy (LOM), scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). TEM is used to characterize the dislocations (mobile + dipole) inside the subgrains and XRD measurements are used tomore » the characterize mobile dislocations. Based on the subgrain boundary misorientations obtained from EBSD measurements, the boundary dislocation density is estimated. The total dislocation density is estimated for the as-received and crept conditions adding the mobile, boundary and dipole dislocation densities. Additionally, the subgrain size is estimated from the EBSD measurements. In this publication we propose the use of three characterization techniques TEM, XRD and EBSD as necessary to characterize all type of dislocations and quantify the total dislocation densty in martensitic/ferritic steels. - Highlights: • Creep properties of a novel 12% Cr steel alloyed with Ta • Experimental characterization of different types of dislocations: mobile, dipole and boundary • Characterization and interpretation of the substructure evolution using unique combination of TEM, XRD and EBSD.« less

Creep Behavior of Poly(lactic acid) Based Biocomposites

PubMed Central

Morreale, Marco; Mistretta, Maria Chiara; Fiore, Vincenzo

2017-01-01

Polymer composites containing natural fibers are receiving growing attention as possible alternatives for composites containing synthetic fibers. The use of biodegradable matrices obtained from renewable sources in replacement for synthetic ones is also increasing. However, only limited information is available about the creep behavior of the obtained composites. In this work, the tensile creep behavior of PLA based composites, containing flax and jute twill weave woven fabrics, produced through compression molding, was investigated. Tensile creep tests were performed at different temperatures (i.e., 40 and 60 °C). The results showed that the creep behavior of the composites is strongly influenced by the temperature and the woven fabrics used. As preliminary characterization, quasi-static tensile tests and dynamic mechanical tests were carried out on the composites. Furthermore, fabrics (both flax and jute) were tested as received by means of quasi-static tests and creep tests to evaluate the influence of fabrics mechanical behavior on the mechanical response of the resulting composites. The morphological analysis of the fracture surface of the tensile samples showed the better fiber-matrix adhesion between PLA and jute fabric. PMID:28772755

Creep Behavior of Poly(lactic acid) Based Biocomposites.

PubMed

Morreale, Marco; Mistretta, Maria Chiara; Fiore, Vincenzo

2017-04-08

Polymer composites containing natural fibers are receiving growing attention as possible alternatives for composites containing synthetic fibers. The use of biodegradable matrices obtained from renewable sources in replacement for synthetic ones is also increasing. However, only limited information is available about the creep behavior of the obtained composites. In this work, the tensile creep behavior of PLA based composites, containing flax and jute twill weave woven fabrics, produced through compression molding, was investigated. Tensile creep tests were performed at different temperatures (i.e., 40 and 60 °C). The results showed that the creep behavior of the composites is strongly influenced by the temperature and the woven fabrics used. As preliminary characterization, quasi-static tensile tests and dynamic mechanical tests were carried out on the composites. Furthermore, fabrics (both flax and jute) were tested as received by means of quasi-static tests and creep tests to evaluate the influence of fabrics mechanical behavior on the mechanical response of the resulting composites. The morphological analysis of the fracture surface of the tensile samples showed the better fiber-matrix adhesion between PLA and jute fabric.

Synthesis and Characterization of Liquid Crystalline Epoxy Resins

DTIC Science & Technology

2014-01-01

Temperature dependence of the four parameters in the Burgers model. ......... 81 Figure 4.7 Dependence of creep compliance on creep time at different...Kinetic parameters for LCERs. ......................................................................... 65 Table 3.4 Kinetic parameters for non-LCERs...curing in a high strength magnetic field. The orientation was quantified by an orientation parameter determined with two-dimensional X-ray diffraction

Environmental Durability and Stress Rupture of EBC/CMCs

NASA Technical Reports Server (NTRS)

Appleby, Matthew; Morscher, Gregory N.; Zhu, Dongming

2012-01-01

This research focuses on the strength and creep performance of SiC fiber-reinforced SiC ceramic matrix composite (CMC) environmental barrier coating (EBC) systems under complex simulated engine environments. Tensile-strength and stress-rupture testing was conducted to illustrate the material properties under isothermal and thermal gradient conditions. To determine material durability, further testing was conducted under exposure to thermal cycling, thermal gradients and simulated combustion environments. Emphasis is placed on experimental techniques as well as implementation of non-destructive evaluation, including modal acoustic emission and electrical resistivity monitoring, to characterize strength degradation and damage mechanisms. Currently, little is known about the behavior of EBC-CMCs under these conditions; consequently, this work will prove invaluable in the development of structural components for use in high temperature applications.

Mechanical Interferometry Imaging for Creep Modeling of the Cornea

PubMed Central

Yoo, Lawrence; Reed, Jason; Gimzewski, James K.

2011-01-01

Purpose. A novel nanoindentation technique was used to biomechanically characterize each of three main layers of the cornea by using Hertzian viscoelastic formulation of creep, the deformation resulting from sustained-force application. Methods. The nanoindentation method known as mechanical interferometry imaging (MII) with <1-nm displacement precision was used to observe indentation of bovine corneal epithelium, endothelium, and stroma by a spherical ferrous probe in a calibrated magnetic field. For each specimen, creep testing was performed using two different forces for 200 seconds. Measurements for single force were used to build a quantitative Hertzian model that was then used to predict creep behavior for another imposed force. Results. For all three layers, displacement measurements were highly repeatable and were well predicted by Hertzian models. Although short- and long-term stiffnesses of the endothelium were highest of the three layers at 339.2 and 20.2 kPa, respectively, both stromal stiffnesses were lowest at 100.4 and 3.6 kPa, respectively. Stiffnesses for the epithelium were intermediate at 264.6 and 12.2 kPa, respectively. Conclusions. Precise, repeatable measurements of corneal creep behavior can be conveniently obtained using MII at mechanical scale as small as one cell thickness. When interpreted in analytical context of Hertzian viscoelasticity, MII technique proved to be a powerful tool for biomechanical characterization of time-dependent biomechanics of corneal regions. PMID:21969299

Comparison of the dynamic fatigue behavior of two monolithic SiC and an Al{sub 2}O{sub 3}/SiC composite

DOE Office of Scientific and Technical Information (OSTI.GOV)

Breder, K.; Tennery, V.J.

1994-09-01

Two monolithic silicon carbides, NT230 siliconized SiC from Norton Saint Gobain and sintered {beta}-SiC from Coors, and a silicon carbide particulate reinforced alumina ceramic composite from Lanxide, which all are candidate materials for pressurized heat exchangers in coal-fired power plants have been evaluated. The fast fracture flexure strength was measured as a function of temperature. All candidate materials retained a sufficient strength level up to 1400C. The susceptibility to slow crack growth (SCG) was evaluated by the dynamic fatigue method at 1100C and 1400C. None of the materials exhibited SCG at 1100C. At 1400C the siliconized SiC ceramic showed limitedmore » SCG and the composite ceramic exhibited creep damage when stressed to 50% of fast fracture strength at the intermediate and slow stressing rates. This prevented the evaluation of the SCG properties of this material at 1400C. Fractography supported the mechanical observations and with the exception of the specimens which exhibited creep damage, only the siliconized SiC showed a small SCG damage zone at long times at 1400C.« less

FIB–SEM tomography of 4th generation PWA 1497 superalloy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ziętara, Maciej, E-mail: zietara@agh.edu.pl; Kruk, Adam, E-mail: kruczek@agh.edu.pl; Gruszczyński, Adam, E-mail: gruszcz@agh.edu.pl

2014-01-15

The effect of creep deformation on the microstructure of the PWA 1497 single crystal Ni-base superalloy developed for turbine blade applications was investigated. The aim of the present study was to characterize quantitatively a superalloy microstructure and subsequent development of rafted γ′ precipitates in the PWA 1497 during creep deformation at 982 °C and 248 MPa up to rupture. The PWA1497 microstructure was characterized by scanning electron microscopy and FIB–SEM electron tomography. The 3D reconstruction of the PWA1497 microstructure is presented and discussed. - Highlights: • The microstructure of PWA1497 superalloy was examined using FIB–SEM tomography. • In case ofmore » modern single crystal superalloys, measurements of A{sub A} are adequate for V{sub V}. • During creep the γ channel width increases from 65 to 193 nm for ruptured specimen. • Tomography is a useful technique for quantitative studies of material microstructure.« less

A Novel Creep-Fatigue Life Prediction Model for P92 Steel on the Basis of Cyclic Strain Energy Density

NASA Astrophysics Data System (ADS)

Ji, Dongmei; Ren, Jianxing; Zhang, Lai-Chang

2016-11-01

A novel creep-fatigue life prediction model was deduced based on an expression of the strain energy density in this study. In order to obtain the expression of the strain energy density, the load-controlled creep-fatigue (CF) tests of P92 steel at 873 K were carried out. Cyclic strain of P92 steel under CF load was divided into elastic strain, applying and unloading plastic strain, creep strain, and anelastic strain. Analysis of cyclic strain indicates that the damage process of P92 steel under CF load consists of three stages, similar to pure creep. According to the characteristics of the strains above, an expression was defined to describe the strain energy density for each cycle. The strain energy density at stable stage is inversely proportional to the total strain energy density dissipated by P92 steel. However, the total strain energy densities under different test conditions are proportional to the fatigue life. Therefore, the expression of the strain energy density at stable stage was chosen to predict the fatigue life. The CF experimental data on P92 steel were employed to verify the rationality of the novel model. The model obtained from the load-controlled CF test of P92 steel with short holding time could predict the fatigue life of P92 steel with long holding time.

Special Considerations for Qualifying Thin Films for Supper Pressure Pumpkin Ultra Long Duration Balloon (ULDB) Missions

NASA Astrophysics Data System (ADS)

Said, M.

Pumpkin type super pressure balloons require much less stringent mechanical requirements on the envelope film material when compared to spherical super pressure type balloons. However, since suitable thin films are typically viscoelastic in nature, their creep characteristics must be fully characterized and must not exceed specific and predetermined design limits. Proper assessment of materials limits to meet these design limits requires creep-load-temperature data that characterizes the performance of the material over a time that exceeds the duration of the design service life by some specified margin. Contrary to the behavior of materials with purely elastic response, visco-elastic materials such as these considered for the ULDB design, change their geometry under sustained loading over time. This change is usually reflected by exhibiting a significant visco-elastic component over the service life of the mission. For that regime of large visco-elastic response, where the material is highly nonlinear, a certain load-temperature threshold can be reached where the creep is limited by an asymptote that depends on both the temperature and load level. Such creep is recoverable, although the recovery period may be much longer than the 100 day design service life of the ULDB structure plus the factor of safety required for the design. For a typical flight, the most significant creep occurs at the highest temperature, which also produces the highest internal pressure. At mid- latitudes a significant portion of the service life is spent at night, i.e. at low temperature and low load; for the ULDB film, this nighttime contribution to creep is insignificant in comparison to any daytime contribution. By contrast, flight exposure in an Antarctic summer is at an almost constant high temperature and corresponding high pressure. This response behavior must be sufficiently characterized to serve the needs of the structural design and performance predictions of the vehicle in service. In this work, a special emphasis will be given to the creep and dynamic characteristics of selected coextruded films and their dependence on the loading level and temperature. Preliminary testing has suggested t at the creep behavior of theh coextruded linear low density resin films is highly dependent on temperature and that the dynamic response depends on the make up of the composite film. In addition, the paper will, in general, highlight the process of qualify ing thin films for the pumpkin class of super pressure balloons.

Creep avalanches on San Andreas Fault and their underlying mechanism from 19 years of InSAR and seismicity

NASA Astrophysics Data System (ADS)

Khoshmanesh, M.; Shirzaei, M.

2017-12-01

Recent seismic and geodetic observations indicate that interseismic creep rate varies in both time and space. The spatial extent of creep determines the earthquake potential, while its temporal evolution, known as slow slip events (SSE), may trigger earthquakes. Although the conditions promoting fault creep are well-established, the mechanism for initiating self-sustaining and sometimes cyclic creep events is enigmatic. Here we investigate a time series of 19 years of surface deformation measured by radar interferometry between 1992 and 2011 along the Central San Andreas Fault (CSAF) to constrain the temporal evolution of creep. We show that the creep rate along the CSAF has a sporadic behavior, quantified with a Gumbel-like probability distribution characterized by longer tail toward the extreme positive rates, which is signature of burst-like creep dynamics. Defining creep avalanches as clusters of isolated creep with rates exceeding the shearing rate of tectonic plates, we investigate the statistical properties of their size and length. We show that, similar to the frequency-magnitude distribution of seismic events, the distribution of potency estimated for creep avalanches along the CSAF follows a power law, dictated by the distribution of their along-strike lengths. We further show that an ensemble of concurrent creep avalanches which aseismically rupture isolated fault compartments form the semi-periodic SSEs observed along the CSAF. Using a rate and state friction model, we show that normal stress is temporally variable on the fault, and support this using seismic observations. We propose that, through a self-sustaining fault-valve behavior, compaction induced elevation of pore pressure within hydraulically isolated fault compartments, and subsequent frictional dilation is the cause for the observed episodic SSEs. We further suggest that the 2004 Parkfield Mw6 earthquake may have been triggered by the SSE on adjacent creeping segment, which increased Coulomb failure stress up to 0.45 bar/yr. While creeping segments are suggested to act as barriers and arrest rupture, our study implies that SSEs on these zones may trigger seismic events on adjacent locked parts.

Non-contact Creep Resistance Measurement for Ultra-high temperature Materials

NASA Technical Reports Server (NTRS)

Hyers, Robert W.; Lee, Jonghuyn; Bradshaw, Richard C.; Rogers, Jan; Rathz, Thomas J.; Wall, James J.; Choo, Hahn; Liaw, Peter K.

2005-01-01

Continuing pressures for higher performance and efficiency in propulsion are driving ever more demanding needs for high-temperature materials. Some immediate applications in spaceflight include combustion chambers for advanced chemical rockets and turbomachinery for jet engines and power conversion in nuclear-electric propulsion. In the case of rockets, the combination of high stresses and high temperatures make the characterization of creep properties very important. Creep is even more important in the turbomachinery, where a long service life is an additional constraint. Some very high-temperature materials are being developed, including platinum group metals, carbides, borides, and silicides. But the measurement of creep properties at very high temperatures is itself problematic, because the testing instrument must operate at such high temperatures. Conventional techniques are limited to about 1700 C. A new, containerless technique for measuring creep deformation has been developed. This technique is based on electrostatic levitation (ESL) of a spherical sample, which is heated to the measurement temperature and rotated at a rate such that the centrifugal acceleration causes creep deformation. Creep of samples has been demonstrated at up to 2300 C in the ESL facility at NASA MSFC, while ESL itself has been applied at over 3000 C, and has no theoretical maximum temperature. The preliminary results and future directions of this NASA-funded research collaboration will be presented.

Numerical analysis of the creeping behavior of the S. Andrea di Perarolo secondary landslide (Italian Eastern Alps)

NASA Astrophysics Data System (ADS)

Cioli, C.; Genevois, R.; Iafelice, M.; Zorzi, L.

2012-04-01

The S. Andrea landslide is a complex secondary phenomenon characterized by continuous movements causing a very high hazard condition for the near Perarolo di Cadore village (Italian Eastern Alps). A significant amount of geological and geotechnical investigations has been carried out in the past allowing the detection of the basal sliding surface. In specific, the sliding surface coincides with the contact between the bedrock and the overlying mass of an old landslides, involving a volume of about 180.000 cubic meters. A numerical approach has been adopted to analyze the stability of slope. This method is able to simulate the formation and development of shear zones as areas of strain localization in the model. Indeed, the S. Andrea landslide has been, then, investigated using FLAC, a two-dimensional explicit finite difference program, particularly useful in case of slopes with complex geometry. In order to build up a suitable model, variation of geological, hydrogeological and geotechnical parameters have been identified from the interpretation of all available data. In a preliminary stage, a Mohr-Coulomb plasticity model has been adopted except for the bedrock, which was characterized by an isotropic elastic model. Groundwater flow condition has been performed evaluating the change in pore pressure coupled to the mechanical deformation calculation. Numerical results show that this model cannot simulate real displacement behavior of the slope mainly due to both the complex material behavior and lithological heterogeneity, and due to geotechnical spatial complexity of different soils and mechanical parameters. It has been assumed that it was necessary to improve the model in the light of a time dependent behavior of existing soils. An elastic-viscoplastic model has been then used to reproduce the observed creeping behavior, and only in viscoplastic region time effects have been considered. Discussion of results points out on: i) the evolution of the ``mechanical damage'' within the moving mass; ii) the identification of possible causes of the displacements recorded in the field; iii) the utility of the computational approach for the creeping response of the soil slopes under constant load conditions and for two dimensional applications.

Life prediction technologies for aeronautical propulsion systems

NASA Technical Reports Server (NTRS)

Mcgaw, Michael A.

1987-01-01

Fatigue and fracture problems continue to occur in aeronautical gas turbine engines. Components whose useful life is limited by these failure modes include turbine hot-section blades, vanes and disks. Safety considerations dictate that catastrophic failures be avoided, while economic considerations dictate that noncatastrophic failures occur as infrequently as possible. The design decision is therefore in making the tradeoff between engine performance and durability. The NASA Lewis Research Center has contributed to the aeropropulsion industry in the areas of life prediction technology for 30 years, developing creep and fatigue life prediction methodologies for hot-section materials. Emphasis is placed on the development of methods capable of handling both thermal and mechanical fatigue under severe environments. Recent accomplishments include the development of more accurate creep-fatigue life prediction methods such as the total strain version of Lewis' Strainrange Partitioning (SRP) and the HOST-developed Cyclic Damage Accumulation (CDA) model. Other examples include the Double Damage Curve Approach (DDCA), which provides greatly improved accuracy for cumulative fatigue design rules.

Physical aging effects on the compressive linear viscoelastic creep of IM7/K3B composite

NASA Technical Reports Server (NTRS)

Veazie, David R.; Gates, Thomas S.

1995-01-01

An experimental study was undertaken to establish the viscoelastic behavior of 1M7/K3B composite in compression at elevated temperature. Creep compliance, strain recovery and the effects of physical aging on the time dependent response was measured for uniaxial loading at several isothermal conditions below the glass transition temperature (T(g)). The IM7/K3B composite is a graphite reinforced thermoplastic polyimide with a T(g) of approximately 240 C. In a composite, the two matrix dominated compliance terms associated with time dependent behavior occur in the transverse and shear directions. Linear viscoelasticity was used to characterize the creep/recovery behavior and superposition techniques were used to establish the physical aging related material constants. Creep strain was converted to compliance and measured as a function of test time and aging time. Results included creep compliance master curves, physical aging shift factors and shift rates. The description of the unique experimental techniques required for compressive testing is also given.

Modeling flow for modified concentric cylinder rheometer geometry

NASA Astrophysics Data System (ADS)

Ekeruche, Karen; Connelly, Kelly; Kavehpour, H. Pirouz

2016-11-01

Rheology experiments on biological fluids can be difficult when samples are limited in volume, sensitive to degradation, and delicate to extract from tissues. A probe-like geometry has been developed to perform shear creep experiments on biological fluids and to use the creep response to characterize fluid material properties. This probe geometry is a modified concentric cylinder setup, where the gap is large and we assume the inner cylinder rotates in an infinite fluid. To validate this assumption we perform shear creep tests with the designed probe on Newtonian and non-Newtonian fluids and vary the outer cylinder container diameter. We have also created a numerical model based on the probe geometry setup to compare with experimental results at different outer cylinder diameters. A creep test is modeled by applying rotation to the inner cylinder and solving for the deformation of the fluid throughout the gap. Steady state viscosity values are calculated from creep compliance curves and compared between experimental and numerical results.

Characterization of long-term extension of isolated cell walls from growing cucumber hypocotyls

NASA Technical Reports Server (NTRS)

Cosgrove, D. J.

1989-01-01

Walls from frozen-thawed cucumber (Cucumis sativus L.) hypocotyls extend for many hours when placed in tension under acidic conditions. This study examined whether such "creep" is a purely physical process dependent on wall viscoelasticity alone or whether enzymatic activities are needed to maintain wall extension. Chemical denaturants inhibited wall creep, some acting reversibly and others irreversibly. Brief (15 s) boiling in water irreversibly inhibited creep, as did pre-incubation with proteases. Creep exhibited a high Q10 (3.8) between 20 degrees and 30 degrees C, with slow inactivation at higher temperatures, whereas the viscous flow of pectin solutions exhibited a much lower Q10 (1.35). On the basis of its temperature sensitivity, involvement of pectic gel-sol transitions was judged to be of little importance in creep. Pre-incubation of walls in neutral pH irreversibly inactivated their ability to creep, with a half-time of about 40 min. At 1 mM, Cu2+, Hg2+ and Al3+ were strongly inhibitory whereas most other cations, including Ca2+, had little effect. Sulfhydryl-reducing agents strongly stimulated creep, apparently by stabilizing wall enzyme(s). The physical effects of these treatments on polymer interactions were examined by Instron and stress-relaxation analyses. Some treatments, such as pH and Cu2+, had significant effects on wall viscoelasticity, but others had little or no apparent effect, thus implicating an enzymatic creep mechanism. The results indicate that creep depends on relatively rugged enzymes that are firmly attached to or entangled in the wall. The sensitivity of creep to SH-reducing agents indicates that thiol reduction of wall enzymes might provide a control mechanism for endogenous cell growth.

Field and experimental evidence for coseismic ruptures along shallow creeping faults in forearc sediments of the Crotone Basin, South Italy

NASA Astrophysics Data System (ADS)

Balsamo, Fabrizio; Aldega, Luca; De Paola, Nicola; Faoro, Igor; Storti, Fabrizio

2014-05-01

Large seismic slip occurring along shallow creeping faults in tectonically active areas represents an unsolved paradox, which is largely due to our poor understanding of the mechanics governing creeping faults, and to the lack of documented geological evidence showing how coseismic rupturing overprints creep in near-surface conditions. In this contribution we integrate field, petrophysical, mineralogical and friction data to characterize the signature of coseismic ruptures propagating along shallow creeping faults affecting unconsolidated forearc sediments of the seismically active Crotone Basin, in South Italy. Field observations of fault zones show widespread foliated cataclasites in fault cores, locally overprinted by sharp slip surfaces decorated by thin (0.5-1.5 cm) black gouge layers. Compared to foliated cataclasites, black gouges have much lower grain size, porosity and permeability, which may have facilitated slip weakening by thermal fluid pressurization. Moreover, black gouges are characterized by distinct mineralogical assemblages compatible with high temperatures (180-200°C) due to frictional heating during seismic slip. Foliated cataclasites and black gouges were also produced by laboratory friction experiments performed on host sediments at sub-seismic (≤ 0.1 m/s) and seismic (1 m/s) slip rates, respectively. Black gouges display low friction coefficients (0.3) and velocity-weakening behaviours, as opposed to high friction coefficients (0.65) and velocity-strengthening behaviours shown by the foliated cataclasites. Our results show that narrow black gouges developed within foliated cataclasites represent a potential diagnostic marker for episodic seismic activity in shallow creeping faults. These findings can help understanding the time-space partitioning between aseismic and seismic slip of faults at shallow crustal levels, impacting on seismic hazard evaluation of subduction zones and forearc regions affected by destructive earthquakes and tsunamis.

Electrical Resistance of SiC/SiC Ceramic Matrix Composites for Damage Detection and Life-Prediction

NASA Technical Reports Server (NTRS)

Smith, Craig; Morscher, Gregory; Xia, Zhenhai

2009-01-01

Ceramic matrix composites (CMC) are suitable for high temperature structural applications such as turbine airfoils and hypersonic thermal protection systems due to their low density high thermal conductivity. The employment of these materials in such applications is limited by the ability to accurately monitor and predict damage evolution. Current nondestructive methods such as ultrasound, x-ray, and thermal imaging are limited in their ability to quantify small scale, transverse, in-plane, matrix cracks developed over long-time creep and fatigue conditions. CMC is a multifunctional material in which the damage is coupled with the material s electrical resistance, providing the possibility of real-time information about the damage state through monitoring of resistance. Here, resistance measurement of SiC/SiC composites under mechanical load at both room temperature monotonic and high temperature creep conditions, coupled with a modal acoustic emission technique, can relate the effects of temperature, strain, matrix cracks, fiber breaks, and oxidation to the change in electrical resistance. A multiscale model can in turn be developed for life prediction of in-service composites, based on electrical resistance methods. Results of tensile mechanical testing of SiC/SiC composites at room and high temperatures will be discussed. Data relating electrical resistivity to composite constituent content, fiber architecture, temperature, matrix crack formation, and oxidation will be explained, along with progress in modeling such properties.

Creep analysis of solid oxide fuel cell with bonded compliant seal design

NASA Astrophysics Data System (ADS)

Jiang, Wenchun; Zhang, Yucai; Luo, Yun; Gong, J. M.; Tu, S. T.

2013-12-01

Solid oxide fuel cell (SOFC) requires good sealant because it works in harsh conditions (high temperature, thermal cycle, oxidative and reducing gas environments). Bonded compliant seal (BCS) is a new sealing method for planar SOFC. It uses a thin foil metal to bond the window frame and cell, achieving the seal between window frame and cell. At high temperature, a comprehensive evaluation of its creep strength is essential for the adoption of BCS design. In order to characterize the creep behavior, the creep induced by thermal stresses in SOFC with BCS design is simulated by finite element method. The results show that the foil is compressed and large thermal stresses are generated. The initial peak thermal stress is located in the thin foil because the foil acts as a spring stores the thermal stresses by elastic and plastic deformation in itself. Serving at high temperature, initial thermal displacement is partially recovered because of the creep relaxation, which becomes a new discovered advantage for BCS design. It predicts that the failures are likely to happen in the middle of the cell edge and BNi-2 filler metal, because the maximum residual displacement and creep strain are located.

Experiment and Modeling of Simultaneous Creep, Plasticity and Transformation of High Temperature Shape Memory Alloys During Cyclic Actuation

NASA Technical Reports Server (NTRS)

Kumar, Parikshith K.; Desai, Uri; Chatzigeorgiou, George; Lagoudas, Dimitris C.; Monroe, James; Karaman, Ibrahim; Noebe, Ron; Bigelow, Glen

2010-01-01

The present work is focused on studying the cycling actuation behavior of HTSMAs undergoing simultaneous creep and transformation. For the thermomechanical testing, a high temperature test setup was assembled on a MTS frame with the capability to test up to temperatures of 600 C. Constant stress thermal cycling tests were conducted to establish the actuation characteristics and the phase diagram for the chosen HTSMA. Additionally, creep tests were conducted at constant stress levels at different test temperatures to characterize the creep behavior of the alloy over the operational range. A thermodynamic constitutive model is developed and extended to take into account a) the effect of multiple thermal cycling on the generation of plastic strains due to transformation (TRIP strains) and b) both primary and secondary creep effects. The model calibration is based on the test results. The creep tests and the uniaxial tests are used to identify the viscoplastic behavior of the material. The parameters for the SMA properties, regarding the transformation and transformation induced plastic strain evolutions, are obtained from the material phase diagram and the thermomechanical tests. The model is validated by predicting the material behavior at different thermomechanical test conditions.

Sources of Variation in Creep Testing

NASA Technical Reports Server (NTRS)

Loewenthal, William S.; Ellis, David L.

2011-01-01

Creep rupture is an important material characteristic for the design of rocket engines. It was observed during the characterization of GRCop-84 that the complete data set had nearly 4 orders of magnitude of scatter. This scatter likely confounded attempts to determine how creep performance was influenced by manufacturing. It was unclear if this variation was from the testing, the material, or both. Sources of variation were examined by conducting tests on identically processed specimens at the same specified stresses and temperatures. Significant differences existed between the five constant-load creep frames. The specimen temperature was higher than the desired temperature by as much as 43 C. It was also observed that the temperature gradient was up to 44 C. Improved specimen temperature control minimized temperature variations. The data from additional tests demonstrated that the results from all five frames were comparable. The variation decreased to 1/2 order of magnitude from 2 orders of magnitude for the baseline data set. Independent determination of creep rates in a reference load frame closely matched the creep rates determined after the modifications. Testing in helium tended to decrease the sample temperature gradient, but helium was not a significant improvement over vacuum.

Toward Improving the Type IV Cracking Resistance in Cr-Mo Steel Weld Through Thermo-Mechanical Processing

DOE PAGES

Shassere, Benjamin A.; Yamamoto, Yukinori; Babu, Sudarsanam Suresh

2016-02-23

Detailed microstructure characterization of Grade 91 (Modified 9Cr-1Mo, ASTM A387) steel subjected to a thermo-mechanical treatment (TMT) process was performed to rationalize the cross-weld creep properties. A series of thermo-mechanical processing in the austenite phase region, followed by isothermal aging at temperatures at 973 to 1173 K (700 to 900ºC) was applied to the Grade 91 steel to promote precipitation kinetics of MX (M: Nb and V, X: C and N) in the austenite matrix. Detailed characterization of the base metals after standard tempering confirmed the presence of fine MX dispersion within the tempered martensitic microstructure in steels processed at/andmore » above 1073 K (800 ºC). Relatively low volume fraction of M 23C 6 precipitates was observed after processing at 1073 K (800 ºC). The cross-weld creep strength after processing was increased with respect to the increase of MX dispersion, indicating that these MX precipitates maintained during weld thermal cycles in the fine grained heat affected zone (FGHAZ) region and thereby contribute to improved creep resistant of welds in comparison to the welds made with the standard “normalization and tempering” processes. Lastly, the steels processed in this specific processing condition showed improved cross-weld creep resistance and sufficient room-temperature toughness. The above data is also analysed based on existing theories of creep deformation based on dislocation climb mechanism.« less

Toward Improving the Type IV Cracking Resistance in Cr-Mo Steel Weld Through Thermo-Mechanical Processing

NASA Astrophysics Data System (ADS)

Shassere, Benjamin A.; Yamamoto, Yukinori; Babu, Sudarsanam Suresh

2016-05-01

Detailed microstructure characterization of Grade 91 (Modified 9Cr-1Mo, ASTM A387) steel subjected to a thermo-mechanical treatment process was performed to rationalize the cross-weld creep properties. A series of thermo-mechanical processing in the austenite phase region, followed by isothermal aging at temperatures at 973 K to 1173 K (700 °C to 900 °C), was applied to the Grade 91 steel to promote precipitation kinetics of MX (M: Nb and V, X: C and N) in the austenite matrix. Detailed characterization of the base metals after standard tempering confirmed the presence of fine MX dispersion within the tempered martensitic microstructure in steels processed at/and above 1073 K (800 °C). Relatively low volume fraction of M23C6 precipitates was observed after processing at 1073 K (800 °C). The cross-weld creep strength after processing was increased with respect to the increase of MX dispersion, indicating that these MX precipitates maintained during weld thermal cycles in the fine-grained heat-affected zone region and thereby contribute to improved creep resistant of welds in comparison to the welds made with the standard "normalization and tempering" processes. The steels processed in this specific processing condition showed improved cross-weld creep resistance and sufficient room temperature toughness. The above data are also analyzed based on existing theories of creep deformation based on dislocation climb mechanism.

Toward Improving the Type IV Cracking Resistance in Cr-Mo Steel Weld Through Thermo-Mechanical Processing

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shassere, Benjamin A.; Yamamoto, Yukinori; Babu, Sudarsanam Suresh

Detailed microstructure characterization of Grade 91 (Modified 9Cr-1Mo, ASTM A387) steel subjected to a thermo-mechanical treatment (TMT) process was performed to rationalize the cross-weld creep properties. A series of thermo-mechanical processing in the austenite phase region, followed by isothermal aging at temperatures at 973 to 1173 K (700 to 900ºC) was applied to the Grade 91 steel to promote precipitation kinetics of MX (M: Nb and V, X: C and N) in the austenite matrix. Detailed characterization of the base metals after standard tempering confirmed the presence of fine MX dispersion within the tempered martensitic microstructure in steels processed at/andmore » above 1073 K (800 ºC). Relatively low volume fraction of M 23C 6 precipitates was observed after processing at 1073 K (800 ºC). The cross-weld creep strength after processing was increased with respect to the increase of MX dispersion, indicating that these MX precipitates maintained during weld thermal cycles in the fine grained heat affected zone (FGHAZ) region and thereby contribute to improved creep resistant of welds in comparison to the welds made with the standard “normalization and tempering” processes. Lastly, the steels processed in this specific processing condition showed improved cross-weld creep resistance and sufficient room-temperature toughness. The above data is also analysed based on existing theories of creep deformation based on dislocation climb mechanism.« less

Nonlinear viscoelastic characterization of bovine trabecular bone.

PubMed

Manda, Krishnagoud; Wallace, Robert J; Xie, Shuqiao; Levrero-Florencio, Francesc; Pankaj, Pankaj

2017-02-01

The time-independent elastic properties of trabecular bone have been extensively investigated, and several stiffness-density relations have been proposed. Although it is recognized that trabecular bone exhibits time-dependent mechanical behaviour, a property of viscoelastic materials, the characterization of this behaviour has received limited attention. The objective of the present study was to investigate the time-dependent behaviour of bovine trabecular bone through a series of compressive creep-recovery experiments and to identify its nonlinear constitutive viscoelastic material parameters. Uniaxial compressive creep and recovery experiments at multiple loads were performed on cylindrical bovine trabecular bone samples ([Formula: see text]). Creep response was found to be significant and always comprised of recoverable and irrecoverable strains, even at low stress/strain levels. This response was also found to vary nonlinearly with applied stress. A systematic methodology was developed to separate recoverable (nonlinear viscoelastic) and irrecoverable (permanent) strains from the total experimental strain response. We found that Schapery's nonlinear viscoelastic constitutive model describes the viscoelastic response of the trabecular bone, and parameters associated with this model were estimated from the multiple load creep-recovery (MLCR) experiments. Nonlinear viscoelastic recovery compliance was found to have a decreasing and then increasing trend with increasing stress level, indicating possible stiffening and softening behaviour of trabecular bone due to creep. The obtained parameters from MLCR tests, expressed as second-order polynomial functions of stress, showed a similar trend for all the samples, and also demonstrate stiffening-softening behaviour with increasing stress.

Evaluation of a Linear Cumulative Damage Failure Model for Epoxy Adhesive

NASA Technical Reports Server (NTRS)

Richardson, David E.; Batista-Rodriquez, Alicia; Macon, David; Totman, Peter; McCool, Alex (Technical Monitor)

2001-01-01

Recently a significant amount of work has been conducted to provide more complex and accurate material models for use in the evaluation of adhesive bondlines. Some of this has been prompted by recent studies into the effects of residual stresses on the integrity of bondlines. Several techniques have been developed for the analysis of bondline residual stresses. Key to these analyses is the criterion that is used for predicting failure. Residual stress loading of an adhesive bondline can occur over the life of the component. For many bonded systems, this can be several years. It is impractical to directly characterize failure of adhesive bondlines under a constant load for several years. Therefore, alternative approaches for predictions of bondline failures are required. In the past, cumulative damage failure models have been developed. These models have ranged from very simple to very complex. This paper documents the generation and evaluation of some of the most simple linear damage accumulation tensile failure models for an epoxy adhesive. This paper shows how several variations on the failure model were generated and presents an evaluation of the accuracy of these failure models in predicting creep failure of the adhesive. The paper shows that a simple failure model can be generated from short-term failure data for accurate predictions of long-term adhesive performance.

Predicting knee replacement damage in a simulator machine using a computational model with a consistent wear factor.

PubMed

Zhao, Dong; Sakoda, Hideyuki; Sawyer, W Gregory; Banks, Scott A; Fregly, Benjamin J

2008-02-01

Wear of ultrahigh molecular weight polyethylene remains a primary factor limiting the longevity of total knee replacements (TKRs). However, wear testing on a simulator machine is time consuming and expensive, making it impractical for iterative design purposes. The objectives of this paper were first, to evaluate whether a computational model using a wear factor consistent with the TKR material pair can predict accurate TKR damage measured in a simulator machine, and second, to investigate how choice of surface evolution method (fixed or variable step) and material model (linear or nonlinear) affect the prediction. An iterative computational damage model was constructed for a commercial knee implant in an AMTI simulator machine. The damage model combined a dynamic contact model with a surface evolution model to predict how wear plus creep progressively alter tibial insert geometry over multiple simulations. The computational framework was validated by predicting wear in a cylinder-on-plate system for which an analytical solution was derived. The implant damage model was evaluated for 5 million cycles of simulated gait using damage measurements made on the same implant in an AMTI machine. Using a pin-on-plate wear factor for the same material pair as the implant, the model predicted tibial insert wear volume to within 2% error and damage depths and areas to within 18% and 10% error, respectively. Choice of material model had little influence, while inclusion of surface evolution affected damage depth and area but not wear volume predictions. Surface evolution method was important only during the initial cycles, where variable step was needed to capture rapid geometry changes due to the creep. Overall, our results indicate that accurate TKR damage predictions can be made with a computational model using a constant wear factor obtained from pin-on-plate tests for the same material pair, and furthermore, that surface evolution method matters only during the initial "break in" period of the simulation.

Identification of Deformation Mechanisms During Bi-Axial Straining of Superplastic AA5083 Material

DTIC Science & Technology

2004-06-01

equiaxed grain structure in FSS along with the prevalence of high - energy boundaries accommodates sliding under the proper shearing conditions. Figure...by a randomized texture and a higher concentration of high disorientation angles. Dislocation creep, which dominates at higher strain rates, is...concentration of high disorientation angles. Dislocation creep, which dominates at higher strain rates, is characterized by fiber texture formation

Robust Rocket Engine Concept

NASA Technical Reports Server (NTRS)

Lorenzo, Carl F.

1995-01-01

The potential for a revolutionary step in the durability of reusable rocket engines is made possible by the combination of several emerging technologies. The recent creation and analytical demonstration of life extending (or damage mitigating) control technology enables rapid rocket engine transients with minimum fatigue and creep damage. This technology has been further enhanced by the formulation of very simple but conservative continuum damage models. These new ideas when combined with recent advances in multidisciplinary optimization provide the potential for a large (revolutionary) step in reusable rocket engine durability. This concept has been named the robust rocket engine concept (RREC) and is the basic contribution of this paper. The concept also includes consideration of design innovations to minimize critical point damage.

Creep-Rupture Behavior of Ni-Based Alloy Tube Bends for A-USC Boilers

NASA Astrophysics Data System (ADS)

Shingledecker, John

Advanced ultrasupercritical (A-USC) boiler designs will require the use of nickel-based alloys for superheaters and reheaters and thus tube bending will be required. The American Society of Mechanical Engineers (ASME) Boiler and Pressure Vessel Code Section II PG-19 limits the amount of cold-strain for boiler tube bends for austenitic materials. In this summary and analysis of research conducted to date, a number of candidate nickel-based A-USC alloys were evaluated. These alloys include alloy 230, alloy 617, and Inconel 740/740H. Uniaxial creep and novel structural tests and corresponding post-test analysis, which included physical measurements, simplified analytical analysis, and detailed microscopy, showed that different damage mechanisms may operate based on test conditions, alloy, and cold-strain levels. Overall, creep strength and ductility were reduced in all the alloys, but the degree of degradation varied substantially. The results support the current cold-strain limits now incorporated in ASME for these alloys for long-term A-USC boiler service.

Influence of deformation behavior, oxydation, and temperature on the long time cyclic stress behavior of high temperature steels

NASA Technical Reports Server (NTRS)

Maile, K.

1982-01-01

The influence of different parameters on the creep-fatigue behavior of several steel alloys was investigated. The higher the temperature the lower the crack initiation value. Pauses during the cycle reduce the damage. Oxidation reduces and protective gas increases the lifetime. Prior loading and prior deformation reduce the lifetime. Short annealing slightly affects the cycle stress behavior. The test results do not satisfactorily agree with methods of extrapolation and damage accumulation.

Application of Radar Interferometry for Monitoring the Landslide Creeping of Jiufen Area, Northern Taiwan

NASA Astrophysics Data System (ADS)

Tai, YuHeng; Chang, ChungPai

2015-04-01

Taiwan is one of the most active landslide areas in the world because of its high precipitation and active tectonic. Landslide, which destroys buildings and human lives, causes a lot of hazard and economical loss in the recent years. Jiufen, which have been determined as a creeping area with previous studies, is one of the famous tourist place in northern Taiwan. Therefore, detection and monitoring of landslide and creeping thus play an important role in risk management and help us decrease the damage from such mass movement. In this study, we apply Interferometric Synthetic Aperture Radar (InSAR) techniques at Jiufen area to monitor the creeping of slope. InSAR observations are obtained from ERS and ENVISAT, which were launched by European Space Agency, spaning from 1994 to 2008. Persistent Scatterer InSAR (PSInSAR) method is also applied to reduce the phase contributed from atmosphere and topography and help us get more precise measurement. We compare the result with previous studies carried out by fieldwork to confirm the possibility of InSAR techniques applying on landslide monitoring. Moreover, the time-series analysis helps us to understand the motion of the creeping along with time. After completion of some amelioration measures, time-series can illustrate the effect of these structures. Then, the result combining with fieldwork survey will give good suggestion of future remediation works. Furthermore, we estimate the measuring error and possible factors, such as slope direction, dip angle, etc., affecting InSAR result and. The result helps us to verify the reliability of this method and gives us more clear deformation pattern of the creeping area.

Relationship between fatigue life in the creep-fatigue region and stress-strain response

NASA Technical Reports Server (NTRS)

Berkovits, A.; Nadiv, S.

1988-01-01

On the basis of mechanical tests and metallographic studies, strainrange partitioned lives were predicted by introducing stress-strain materials parameters into the Universal Slopes Equation. This was the result of correlating fatigue damage mechanisms and deformation mechanisms operating at elevated temperatures on the basis of observed mechanical and microstructural behavior. Correlation between high temperature fatigue and stress strain properties for nickel base superalloys and stainless steel substantiated the method. Parameters which must be evaluated for PP- and CC- life are the maximum stress achievable under entirely plastic and creep conditions respectively and corresponding inelastic strains, and the two more pairs of stress strain parameters must be ascertained.

Creep Strength of Dissimilar Welded Joints Using High B-9Cr Steel for Advanced USC Boiler

NASA Astrophysics Data System (ADS)

Tabuchi, Masaaki; Hongo, Hiromichi; Abe, Fujio

2014-10-01

The commercialization of a 973 K (700 °C) class pulverized coal power system, advanced ultra-supercritical (A-USC) pressure power generation, is the target of an ongoing research project initiated in Japan in 2008. In the A-USC boiler, Ni or Ni-Fe base alloys are used for high-temperature parts at 923 K to 973 K (650 °C to 700 °C), and advanced high-Cr ferritic steels are planned to be used at temperatures lower than 923 K (650 °C). In the dissimilar welds between Ni base alloys and high-Cr ferritic steels, Type IV failure in the heat-affected zone (HAZ) is a concern. Thus, the high B-9Cr steel developed at the National Institute for Materials Science, which has improved creep strength in weldments, is a candidate material for the Japanese A-USC boiler. In the present study, creep tests were conducted on the dissimilar welded joints between Ni base alloys and high B-9Cr steels. Microstructures and creep damage in the dissimilar welded joints were investigated. In the HAZ of the high B-9Cr steels, fine-grained microstructures were not formed and the grain size of the base metal was retained. Consequently, the creep rupture life of the dissimilar welded joints using high B-9Cr steel was 5 to 10 times longer than that of the conventional 9Cr steel welded joints at 923 K (650 °C).

A finite deformation viscoelastic-viscoplastic constitutive model for self-healing materials

NASA Astrophysics Data System (ADS)

Shahsavari, H.; Naghdabadi, R.; Baghani, M.; Sohrabpour, S.

2016-12-01

In this paper, employing the Hencky strain, viscoelastic-viscoplastic response of self-healing materials is investigated. Considering the irreversible thermodynamics and using the effective configuration in the Continuum Damage-Healing Mechanics (CDHM), a phenomenological finite strain viscoelastic-viscoplastic constitutive model is presented. Considering finite viscoelastic and viscoplastic deformations, total deformation gradient is multiplicatively decomposed into viscoelastic and viscoplastic parts. Due to mathematical advantages and physical meaning of Hencky strain, this measure of strain is employed in the constitutive model development. In this regard, defining the damage and healing variables and employing the strain equivalence hypothesis, the strain tensor is determined in the effective configuration. Satisfying the Clausius-Duhem inequality, the evolution equations are introduced for the viscoelastic and viscoplastic strains. The damage and healing variables also evolve according to two different prescribed functions. To employ the proposed model in different loading conditions, the model is discretized in the semi-implicit form. Material parameters of the model are identified employing experimental tests on asphalt mixes available in the literature. Finally, capability of the model is demonstrated comparing the model predictions in the creep-recovery and repeated creep-recovery with the experimental results available in the literature and a good agreement between predicted and test results is revealed.

Hierarchically-driven Approach for Quantifying Materials Uncertainty in Creep Deformation and Failure of Aerospace Materials

DTIC Science & Technology

2016-07-01

characteristics and to examine the sensitivity of using such techniques for evaluating microstructure. In addition to the GUI tool, a manual describing its use has... Evaluating Local Primary Dendrite Arm Spacing Characterization Techniques Using Synthetic Directionally Solidified Dendritic Microstructures, Metallurgical and...driven approach for quanti - fying materials uncertainty in creep deformation and failure of aerspace materials, Multi-scale Structural Mechanics and

Computer programs to characterize alloys and predict cyclic life using the total strain version of strainrange partitioning: Tutorial and users manual, version 1.0

NASA Technical Reports Server (NTRS)

Saltsman, James F.

1992-01-01

This manual presents computer programs for characterizing and predicting fatigue and creep-fatigue resistance of metallic materials in the high-temperature, long-life regime for isothermal and nonisothermal fatigue. The programs use the total strain version of Strainrange Partitioning (TS-SRP). An extensive database has also been developed in a parallel effort. This database is probably the largest source of high-temperature, creep-fatigue test data available in the public domain and can be used with other life prediction methods as well. This users manual, software, and database are all in the public domain and are available through COSMIC (382 East Broad Street, Athens, GA 30602; (404) 542-3265, FAX (404) 542-4807). Two disks accompany this manual. The first disk contains the source code, executable files, and sample output from these programs. The second disk contains the creep-fatigue data in a format compatible with these programs.

Accelerated viscoelastic characterization of T300-5208 graphite-epoxy laminates

NASA Technical Reports Server (NTRS)

Tuttle, M. E.; Brinson, H. F.

1985-01-01

A viscoelastic response scheme for the accelerated characterization of polymer-based composite laminates in applied to T300/5208 graphite/epoxy. The response of uni-directional specimens is modeled. The transient component of the viscoelastic creep compliance is assumed to follow a power law approximation. A recursive relationship is developed, based upon the Schapery single-integral equation, which allows approximation of a continuous time-varying uniaxial load using discrete steps in stress. The viscoelastic response of T300/5208 to transverse normal and shear stresses is determined unsing 90 deg and 10 deg off-axis tensile specimens. In each case the seven viscoelastic material parameters required in the analysis are determined experimentally using short-term creep and creep recovery tests. It is shown that an accurate measure of the power law exponent is crucial for accurate long-term prediction. A short term test cycle selection procedure is proposed, which should provide useful guidelines for the evaluation of other viscoelastic materials.

Comparison of measured temperatures, thermal stresses and creep residues with predictions on a built-up titanium structure

NASA Technical Reports Server (NTRS)

Jenkins, Jerald M.

1987-01-01

Temperature, thermal stresses, and residual creep stresses were studied by comparing laboratory values measured on a built-up titanium structure with values calculated from finite-element models. Several such models were used to examine the relationship between computational thermal stresses and thermal stresses measured on a built-up structure. Element suitability, element density, and computational temperature discrepancies were studied to determine their impact on measured and calculated thermal stress. The optimum number of elements is established from a balance between element density and suitable safety margins, such that the answer is acceptably safe yet is economical from a computational viewpoint. It is noted that situations exist where relatively small excursions of calculated temperatures from measured values result in far more than proportional increases in thermal stress values. Measured residual stresses due to creep significantly exceeded the values computed by the piecewise linear elastic strain analogy approach. The most important element in the computation is the correct definition of the creep law. Computational methodology advances in predicting residual stresses due to creep require significantly more viscoelastic material characterization.

Effect of fiber-matrix adhesion on the creep behavior of CF/PPS composites: temperature and physical aging characterization

NASA Astrophysics Data System (ADS)

Motta Dias, M. H.; Jansen, K. M. B.; Luinge, J. W.; Bersee, H. E. N.; Benedictus, R.

2016-06-01

The influence of fiber-matrix adhesion on the linear viscoelastic creep behavior of `as received' and `surface modified' carbon fibers (AR-CF and SM-CF, respectively) reinforced polyphenylene sulfide (PPS) composite materials was investigated. Short-term tensile creep tests were performed on ±45° specimens under six different isothermal conditions, 40, 50, 60, 65, 70 and 75 °C. Physical aging effects were evaluated on both systems using the short-term test method established by Struik. The results showed that the shapes of the curves were affected neither by physical aging nor by the test temperature, allowing then superposition to be made. A unified model was proposed with a single physical aging and temperature-dependent shift factor, a_{T,te}. It was suggested that the surface treatment carried out in SM-CF/PPS had two major effects on the creep response of CF/PPS composites at a reference temperature of 40 °C: a lowering of the initial compliance of about 25 % and a slowing down of the creep response of about 1.1 decade.

Overview of Strategies for High-Temperature Creep and Oxidation Resistance of Alumina-Forming Austenitic Stainless Steels

NASA Astrophysics Data System (ADS)

Yamamoto, Y.; Brady, M. P.; Santella, M. L.; Bei, H.; Maziasz, P. J.; Pint, B. A.

2011-04-01

A family of creep-resistant, alumina-forming austenitic (AFA) stainless steel alloys is under development for structural use in fossil energy conversion and combustion system applications. The AFA alloys developed to date exhibit comparable creep-rupture lives to state-of-the-art advanced austenitic alloys, and superior oxidation resistance in the ~923 K to 1173 K (650 °C to 900 °C) temperature range due to the formation of a protective Al2O3 scale rather than the Cr2O3 scales that form on conventional stainless steel alloys. This article overviews the alloy design approaches used to obtain high-temperature creep strength in AFA alloys via considerations of phase equilibrium from thermodynamic calculations as well as microstructure characterization. Strengthening precipitates under evaluation include MC-type carbides or intermetallic phases such as NiAl-B2, Fe2(Mo,Nb)-Laves, Ni3Al-L12, etc. in the austenitic single-phase matrix. Creep, tensile, and oxidation properties of the AFA alloys are discussed relative to compositional and microstructural factors.

Tectonic creep in the Hayward fault zone, California

USGS Publications Warehouse

Radbruch-Hall, Dorothy H.; Bonilla, M.G.

1966-01-01

Tectonic creep is slight apparently continuous movement along a fault. Evidence of creep has been noted at several places within the Hayward fault zone--a zone trending northwestward near the western front of the hills bordering the east side of San Francisco Bay. D. H. Radbruch of the Geological Survey and B. J. Lennert, consulting engineer, confirmed a reported cracking of a culvert under the University of California stadium. F. B. Blanchard and C. L. Laverty of the East Bay Municipal Utility District of Oakland studied cracks in the Claremont water tunnel in Berkeley. M. G. Bonilla of the Geological Survey noted deformation of railroad tracks in the Niles district of Fremont. Six sets of tracks have been bent and shifted. L. S. Cluff of Woodward-Clyde-Sherard and Associates and K. V. Steinbrugge of the Pacific Fire Rating Bureau noted that the concrete walls of a warehouse in the Irvington district of Fremont have been bent and broken, and the columns forced out of line. All the deformations noted have been right lateral and range from about 2 inches in the Claremont tunnel to about 8 inches on the railroad tracks. Tectonic creep almost certainly will continue to damage buildings, tunnels, and other structures that cross the narrow bands of active movement within the Hayward fault zone.

Study of the Elasto-plastic Properties of Mineralized Biomaterials via Synchrotron High-energy X-ray Diffraction

NASA Astrophysics Data System (ADS)

Deymier-Black, Alix Christine

Synchrotron high-energy X-ray diffraction was employed to investigate the strains in the hydroxyapatite (HAP) platelets and mineralized collagen fibrils in bovine dentin and cortical bone. The HAP and the fibrillar apparent moduli, defined as the applied stress divided by the phase strain, in dentin were measured as 27+/-7.2 and 16+/-4.9 GPa. The HAP apparent modulus ( EHAPapp ) is less than the lower bound calculated for EHAPapp from the Voigt model. This discrepancy is probably due to stress concentrators or decreases in the HAP Young's modulus due to size or composition effects. EHAPapp and Efibapp in dentin vary significantly within a single tooth in both the apical-cervical direction and the buccal-lingual direction. However, the variation between teeth is minimal. The HAP and fibrillar apparent moduli are not affected by freezing in dentin or by X-ray irradiation in bone and dentin. X-ray irradiation causes a decrease in HAP residual strain in bone. This decrease suggests the presence of HAP-collagen interfacial damage. It was determined from the HAP 00.2 peak broadening that irradiation damage mostly affects the HAP unit cells which are under the highest strain. From this it was theorized that irradiation may damage highly-strained bonds at stress concentrators and/or calcium-mediated electrostatic bonds. The fact that the apparent modulus does not change with irradiation suggests that the interfacial damage must be reversible. Bone and dentin both undergo creep when loaded to high stresses. At low irradiation doses, both the fibrillar and HAP strains increase with creep time indicating that load is being transferred from the matrix to the HAP. However, at high doses, the strain on the HAP decreases with creep time. This supports the interfacial damage theory which would allow the HAP to release its elastic load upon interfacial debonding. At -80 MPa, beyond a dose of 50 kGy, the rate of change in HAP strain with time begins to increase, becoming positive at ˜115 kGy. After 300 kGy the HAP strain rate decreases and plateaus probably due to stiffening of the matrix through cross-linking. The HAP and fibrillar strain rate in irradiated bone and dentin samples increase with increased temperature and applied load.

Tensile, Creep, and Fatigue Behaviors of 3D-Printed Acrylonitrile Butadiene Styrene

NASA Astrophysics Data System (ADS)

Zhang, Hanyin; Cai, Linlin; Golub, Michael; Zhang, Yi; Yang, Xuehui; Schlarman, Kate; Zhang, Jing

2018-01-01

Acrylonitrile butadiene styrene (ABS) is a widely used thermoplastics in 3D printing. However, there is a lack of thorough investigation of the mechanical properties of 3D-printed ABS components, including orientation-dependent tensile strength and creep fatigue properties. In this work, a systematic characterization is conducted on the mechanical properties of 3D-printed ABS components. Specifically, the effect of printing orientation on the tensile and creep properties is investigated. The results show that, in tensile tests, the 0° printing orientation has the highest Young's modulus of 1.81 GPa, and ultimate strength of 224 MPa. In the creep test, the 90° printing orientation has the lowest k value of 0.2 in the plastics creep model, suggesting 90° is the most creep resistant direction. In the fatigue test, the average cycle number under load of 30 N is 3796 cycles. The average cycle number decreases to 128 cycles when the load is 60 N. Using the Paris law, with an estimated crack size of 0.75 mm, and stress intensity factor is varied from 352 to 700 N√ m, the derived fatigue crack growth rate is 0.0341 mm/cycle. This study provides important mechanical property data that is useful for applying 3D-printed ABS in engineering applications.

Structure and creep rupture properties of directionally solidified eutectic gamma/gamma-prime-alpha alloy

NASA Technical Reports Server (NTRS)

Whittenberger, J. D.; Wirth, G.

1982-01-01

A simple ternary gamma/gamma-prime-alpha alloy of nominal composition (wt-%) Ni-32Mo-6Al has been directionally solidified at 17 mm/h and tested in creep rupture at 1073, 1173, and 1273 K. A uniform microstructure consisting of square-shaped Mo fibers in a gamma + gamma-prime matrix was found despite some variation in the molybdenum and aluminum concentrations along the growth direction. Although the steady-state creep rate is well described by the normal stress temperature equation, the stress exponent (12) and the activation energy (580 kJ/mol) are high. The rupture behavior is best characterized by the Larson-Miller parameter where the constant equals 20.

Creep rupture of polymer-matrix composites

NASA Technical Reports Server (NTRS)

Brinson, H. F.; Morris, D. H.; Griffith, W. I.

1981-01-01

The time-dependent creep-rupture process in graphite-epoxy laminates is examined as a function of temperature and stress level. Moisture effects are not considered. An accelerated characterization method of composite-laminate viscoelastic modulus and strength properties is reviewed. It is shown that lamina-modulus master curves can be obtained using a minimum of normally performed quality-control-type testing. Lamina-strength master curves, obtained by assuming a constant-strain-failure criterion, are presented along with experimental data, and reasonably good agreement is shown to exist between the two. Various phenomenological delayed failure models are reviewed and two (the modified rate equation and the Larson-Miller parameter method) are compared to creep-rupture data with poor results.

Physiological and Metabolic Effects of 5-Aminolevulinic Acid for Mitigating Salinity Stress in Creeping Bentgrass

PubMed Central

Yang, Zhimin; Chang, Zuoliang; Sun, Lihong; Yu, Jingjin; Huang, Bingru

2014-01-01

The objectives of this study were to determine whether foliar application of a chlorophyll precursor, 5-aminolevulinic acid (ALA), could mitigate salinity stress damages in perennial grass species by regulating photosynthetic activities, ion content, antioxidant metabolism, or metabolite accumulation. A salinity-sensitive perennial grass species, creeping bentgrass (Agrostis stolonifera), was irrigated daily with 200 mM NaCl for 28 d, which were foliar sprayed with water or ALA (0.5 mg L−1) weekly during the experiment in growth chamber. Foliar application of ALA was effective in mitigating physiological damage resulting from salinity stress, as manifested by increased turf quality, shoot growth rate, leaf relative water content, chlorophyll content, net photosynthetic rate, stomatal conductance and transpiration rate. Foliar application of ALA also alleviated membrane damages, as shown by lower membrane electrolyte leakage and lipid peroxidation, which was associated with increases in the activities of antioxidant enzymes. Leaf content of Na+ was reduced and the ratio of K+/Na+ was increased with ALA application under salinity stress. The positive effects of ALA for salinity tolerance were also associated with the accumulation of organic acids (α-ketoglutaric acid, succinic acid, and malic acid), amino acids (alanine, 5-oxoproline, aspartic acid, and γ -aminobutyric acid), and sugars (glucose, fructose, galactose, lyxose, allose, xylose, sucrose, and maltose). ALA-mitigation of physiological damages by salinity could be due to suppression of Na+ accumulation and enhanced physiological and metabolic activities related to photosynthesis, respiration, osmotic regulation, and antioxidant defense. PMID:25551443

Early stage fatigue damage occurs in bovine tendon fascicles in the absence of changes in mechanics at either the gross or micro-structural level

PubMed Central

Shepherd, Jennifer H.; Riley, Graham P.; Screen, Hazel R.C.

2014-01-01

Many tendon injuries are believed to result from repetitive motion or overuse, leading to the accumulation of micro-damage over time. In vitro fatigue loading can be used to characterise damage during repeated use and investigate how this may relate to the aetiology of tendinopathy. This study considered the effect of fatigue loading on fascicles from two functionally distinct bovine tendons: the digital extensor and deep digital flexor. Micro-scale extension mechanisms were investigated in fascicles before or after a period of cyclic creep loading, comparing two different measurement techniques – the displacement of a photo-bleached grid and the use of nuclei as fiducial markers. Whilst visual damage was clearly identified after only 300 cycles of creep loading, these visual changes did not affect either gross fascicle mechanics or fascicle microstructural extension mechanisms over the 900 fatigue cycles investigated. However, significantly greater fibre sliding was measured when observing grid deformation rather than the analysis of nuclei movement. Measurement of microstructural extension with both techniques was localised and this may explain the absence of change in microstructural deformation in response to fatigue loading. Alternatively, the data may demonstrate that fascicles can withstand a degree of matrix disruption with no impact on mechanics. Whilst use of a photo-bleached grid to directly measure the collagen is the best indicator of matrix deformation, nuclei tracking may provide a better measure of the strain perceived directly by the cells. PMID:25001495

Report on FY17 testing in support of integrated EPP-SMT design methods development

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Yanli .; Jetter, Robert I.; Sham, T. -L.

The goal of the proposed integrated Elastic Perfectly-Plastic (EPP) and Simplified Model Test (SMT) methodology is to incorporate a SMT data-based approach for creep-fatigue damage evaluation into the EPP methodology to avoid the separate evaluation of creep and fatigue damage and eliminate the requirement for stress classification in current methods; thus greatly simplifying evaluation of elevated temperature cyclic service. The purpose of this methodology is to minimize over-conservatism while properly accounting for localized defects and stress risers. To support the implementation of the proposed methodology and to verify the applicability of the code rules, thermomechanical tests continued in FY17. Thismore » report presents the recent test results for Type 1 SMT specimens on Alloy 617 with long hold times, pressurization SMT on Alloy 617, and two-bar thermal ratcheting test results on SS316H at the temperature range of 405 °C to 705 °C. Preliminary EPP strain range analysis on the two-bar tests are critically evaluated and compared with the experimental results.« less

Thermomechanical Fatigue of Ductile Cast Iron and Its Life Prediction

NASA Astrophysics Data System (ADS)

Wu, Xijia; Quan, Guangchun; MacNeil, Ryan; Zhang, Zhong; Liu, Xiaoyang; Sloss, Clayton

2015-06-01

Thermomechanical fatigue (TMF) behaviors of ductile cast iron (DCI) were investigated under out-of-phase (OP), in-phase (IP), and constrained strain-control conditions with temperature hold in various temperature ranges: 573 K to 1073 K, 723 K to 1073 K, and 433 K to 873 K (300 °C to 800 °C, 450 °C to 800 °C, and 160 °C to 600 °C). The integrated creep-fatigue theory (ICFT) model was incorporated into the finite element method to simulate the hysteresis behavior and predict the TMF life of DCI under those test conditions. With the consideration of four deformation/damage mechanisms: (i) plasticity-induced fatigue, (ii) intergranular embrittlement, (iii) creep, and (iv) oxidation, as revealed from the previous study on low cycle fatigue of the material, the model delineates the contributions of these physical mechanisms in the asymmetrical hysteresis behavior and the damage accumulation process leading to final TMF failure. This study shows that the ICFT model can simulate the stress-strain response and life of DCI under complex TMF loading profiles (OP and IP, and constrained with temperature hold).

Evaluation of cast creep occurring during simulated clubfoot correction

PubMed Central

Cohen, Tamara L; Altiok, Haluk; Wang, Mei; McGrady, Linda M; Krzak, Joseph; Graf, Adam; Tarima, Sergey; Smith, Peter A; Harris, Gerald, F

2016-01-01

The Ponseti method is a widely accepted and highly successful conservative treatment of pediatric clubfoot involving weekly manipulations and cast applications. Qualitative assessments have indicated the potential success of the technique with cast materials other than standard plaster of Paris. However, guidelines for clubfoot correction based on the mechanical response of these materials have yet to be investigated. The current study sought to characterize and compare the ability of three standard cast materials to maintain the Ponseti corrected foot position by evaluating cast creep response. A dynamic cast testing device, built to model clubfoot correction, was wrapped in plaster-of-Paris, semi-rigid fiberglass, and rigid fiberglass. Three-dimensional motion responses to two joint stiffnesses were recorded. Rotational creep displacement and linearity of the limb-cast composite were analyzed. Minimal change in position over time was found for all materials. Among cast materials, the rotational creep displacement was significantly different (p < 0.0001). The most creep displacement occurred in the plaster-of-Paris (2.0 degrees), then the semi-rigid fiberglass (1.0 degrees), and then the rigid fiberglass (0.4 degrees). Torque magnitude did not affect creep displacement response. Analysis of normalized rotation showed quasi—linear viscoelastic behavior. This study provided a mechanical evaluation of cast material performance as used for clubfoot correction. Creep displacement dependence on cast material and insensitivity to torque were discovered. This information may provide a quantitative and mechanical basis for future innovations for clubfoot care. PMID:23636764

Computational design and performance prediction of creep-resistant ferritic superalloys

DOE Office of Scientific and Technical Information (OSTI.GOV)

Liaw, Peter K.; Wang, Shao-Yu; Dunand, David C.

Ferritic superalloys containing the B2 phase with the parent L21 phase precipitates in a disordered solid-solution matrix, also known as a hierarchical-precipitate-strengthened ferritic alloy (HPSFA), had been developed for high-temperature structural applications in fossil-energy power plants. These alloys were designed by adding Ti into a previously-studied NiAl-strengthened ferritic alloy (denoted as FBB8 in this study). Following with the concept of HPSFAs, in the present research, a systematic investigation on adding other elements, such as Hf and Zr, and optimizing the Ti content within the alloy system, has been conducted, in order to further improve the creep resistance of the modelmore » alloys. Studies include advanced experimental techniques, first-principles calculations on thermodynamic and mechanical properties, and numerical simulations on precipitation hardening, have been integrated and conducted to characterize the complex microstructures and excellent creep resistance of alloys. The experimental techniques include transmission-electron microscopy (TEM), scanning-electron microscopy (SEM), neutron diffraction (ND), and atom-probe tomography (APT), which provide the detailed microstructural information of the model alloys. Systematic tension/compression creep tests have also been conducted in order to verify the creep resistance of the potential alloy compositions. The results show that when replacing Ti with Hf and Zr, it does not form the L21 phase. Instead, the hexagonal Laves phase forms and distributes majorly along the grain boundary, or large segregation within grains. Since the Laves phase does not form parent to the B2-phase precipitates, it cannot bring the strengthening effect of HPSFAs. As a result, the FBB8 + 2 wt. % Hf and FBB8 + 2 wt. % Zr alloys have similar mechanical properties to the original FBB8. The FBB8 + Ti series alloys had also been studied, from the creep tests and microstructural characterizations, the FBB8 + 3.5 wt.% Ti possesses the greatest creep resistance, with the L21/B2 phase ratio of 4 (80% of the precipitates is the L21 phase, and 20% is the B2 phase). First-principles calculations include thermodynamics, elastic properties, and interfacial properties, which have been conducted for the understanding of the thermodynamic and mechanical properties of HPSFAs. In addition to the systematic experimental approach and first-principles calculations, a series of numerical tools and algorithms, which assist in the optimization of creep properties of ferritic superalloys, are utilized and developed. These numerical simulation results are compared with the available experimental data and previous first-principles calculations, providing the deep insight of creep mechanisms of the creep-resistant ferritic superalloys. To conclude the present research, we’ve found that (1) only FBB8 + Ti alloys have the potential of forming HPSFA, and FBB8 + Hf and FBB8 + Zr do not work. Therefore, only FBB8 + Ti alloys have desirable creep resistance, (2) the optimum composition for the FBB8 + Ti alloys is FBB8 + 3.5% Ti, which has the greatest creep resistance (218.8 MPa as the threshold stress at 700 oC), (3) first-principle calculations obtained results that could not be obtained in experiments, which are relevant to develop ferritic superalloys with the improved creep resistance, and (4) two-dimensional dislocation-dynamics simulations investigate effects of factors like precipitate volume fractions and precipitate radii in the alloy systems, which helps in developing the most desirable microstructure with greatest strengthening.« less

NDE for Material Characterization in Aeronautic and Space Applications

NASA Technical Reports Server (NTRS)

Baaklini, George Y.; Kautz, Harold E.; Gyekenyesi, Andrew L.; Abdul-Aziz, Ali; Martin, Richard E.

2000-01-01

This paper describes selected nondestructive evaluation (NDE) approaches that were developed or tailored at the NASA Glenn Research Center for characterizing advanced material systems. The emphasis is on high-temperature aerospace propulsion applications. The material systems include monolithic ceramics, superalloys, and high temperature composites. In the aeronautic area, the highlights are cooled ceramic plate structures for turbine applications, F-TiAl blade materials for low-pressure turbines, thermoelastic stress analysis (TSA) for residual stress measurements in titanium based and nickel based engine materials, and acousto ultrasonics (AU) for creep damage assessment in nickel-based alloys. In the space area, examples consist of cooled carbon-carbon composites for gas generator combustors and flywheel rotors composed of carbon fiber reinforced polymer matrix composites for energy storage on the international space station (ISS). The role of NDE in solving manufacturing problems, the effect of defects on structural behavior, and the use of NDE-based finite element modeling are discussed. NDE technology needs for improved microelectronic and mechanical systems as well as health monitoring of micro-materials and components are briefly discussed.

Fe-Cr-Mo based ODS alloys via spark plasma sintering: A combinational characterization study by TEM and APT

DOE Office of Scientific and Technical Information (OSTI.GOV)

Y. Q. Wu; K. N. Allahar; J. Burns

2013-08-01

Nanoscale oxides play an important role in oxide dispersion strengthened (ODS) alloys for improved high temperature creep resistance and enhanced radiation damage tolerance. In this study, transmission electron microscopy (TEM) and atom probe tomography (APT) were combined to investigate two novel Fe-16Cr-3Mo (wt.%) based ODS alloys. Spark plasma sintering (SPS) was used to consolidate the ODS alloys from powders that were milled with 0.5 wt.% Y2O3 powder only or with Y2O3 powder and 1 wt.% Ti. TEM characterization revealed that both alloys have a bimodal structure of nanometer-size (~ 100 – 500 nm) and micron-size grains with nanostructured oxide precipitatesmore » formed along and close to grain boundaries with diameters ranging from five to tens of nanometers. APT provides further quantitative analyses of the oxide precipitates, and also reveals Mo segregation at grain boundaries next to oxide precipitates. The alloys with and without Ti are compared based on their microstructures.« less

Report on an Assessment of the Application of EPP Results from the Strain Limit Evaluation Procedure to the Prediction of Cyclic Life Based on the SMT Methodology

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jetter, R. I.; Messner, M. C.; Sham, T. -L.

The goal of the proposed integrated Elastic Perfectly-Plastic (EPP) and Simplified Model Test (SMT) methodology is to incorporate an SMT data based approach for creep-fatigue damage evaluation into the EPP methodology to avoid the separate evaluation of creep and fatigue damage and eliminate the requirement for stress classification in current methods; thus greatly simplifying evaluation of elevated temperature cyclic service. This methodology should minimize over-conservatism while properly accounting for localized defects and stress risers. To support the implementation of the proposed methodology and to verify the applicability of the code rules, analytical studies and evaluation of thermomechanical test results continuedmore » in FY17. This report presents the results of those studies. An EPP strain limits methodology assessment was based on recent two-bar thermal ratcheting test results on 316H stainless steel in the temperature range of 405 to 7050C. Strain range predictions from the EPP evaluation of the two-bar tests were also evaluated and compared with the experimental results. The role of sustained primary loading on cyclic life was assessed using the results of pressurized SMT data from tests on Alloy 617 at 9500C. A viscoplastic material model was used in an analytic simulation of two-bar tests to compare with EPP strain limits assessments using isochronous stress strain curves that are consistent with the viscoplastic material model. A finite element model of a prior 304H stainless steel Oak Ridge National Laboratory (ORNL) nozzle-to-sphere test was developed and used for an EPP strain limits and creep-fatigue code case damage evaluations. A theoretical treatment of a recurring issue with convergence criteria for plastic shakedown illustrated the role of computer machine precision in EPP calculations.« less

Grain boundary oxidation and its effects on high temperature fatigue life

NASA Technical Reports Server (NTRS)

Liu, H. W.; Oshida, Yoshiki

1986-01-01

Fatigue lives at elevated temperatures are often shortened by creep and/or oxidation. Creep causes grain boundary void nucleation and grain boundary cavitation. Grain boundary voids and cavities will accelerate fatigue crack nucleation and propagation, and thereby shorten fatigue life. The functional relationships between the damage rate of fatigue crack nucleation and propagation and the kinetic process of oxygen diffusion depend on the detailed physical processes. The kinetics of grain boundary oxidation penetration was investigated. The statistical distribution of grain boundary penetration depth was analyzed. Its effect on high temperature fatigue life are discussed. A model of intermittent micro-ruptures of grain boundary oxide was proposed for high temperature fatigue crack growth. The details of these studies are reported.

Durability of bends in high-temperature steam lines under the conditions of long-term operation

NASA Astrophysics Data System (ADS)

Katanakha, N. A.; Semenov, A. S.; Getsov, L. B.

2015-04-01

The article presents the results of stress-strain state computations and durability of bent and steeply curved branches of high-temperature steam lines carried out on the basis of the finite element method using the modified Soderberg formula for describing unsteady creep processes with taking the accumulation of damage into account. The computations were carried out for bends made of steel grades that are most widely used for manufacturing steam lines (12Kh1MF, 15Kh1M1F, and 10Kh9MFB) and operating at different levels of inner pressure and temperature. The solutions obtained using the developed creep model are compared with those obtained using the models widely used in practice.

Tracking and Control of Gas Turbine Engine Component Damage/Life

NASA Technical Reports Server (NTRS)

Jaw, Link C.; Wu, Dong N.; Bryg, David J.

2003-01-01

This paper describes damage mechanisms and the methods of controlling damages to extend the on-wing life of critical gas turbine engine components. Particularly, two types of damage mechanisms are discussed: creep/rupture and thermo-mechanical fatigue. To control these damages and extend the life of engine hot-section components, we have investigated two methodologies to be implemented as additional control logic for the on-board electronic control unit. This new logic, the life-extending control (LEC), interacts with the engine control and monitoring unit and modifies the fuel flow to reduce component damages in a flight mission. The LEC methodologies were demonstrated in a real-time, hardware-in-the-loop simulation. The results show that LEC is not only a new paradigm for engine control design, but also a promising technology for extending the service life of engine components, hence reducing the life cycle cost of the engine.

Indentation experiments and simulation of ovine bone using a viscoelastic-plastic damage model

PubMed Central

Zhao, Yang; Wu, Ziheng; Turner, Simon; MacLeay, Jennifer; Niebur, Glen L.; Ovaert, Timothy C.

2015-01-01

Indentation methods have been widely used to study bone at the micro- and nanoscales. It has been shown that bone exhibits viscoelastic behavior with permanent deformation during indentation. At the same time, damage due to microcracks is induced due to the stresses beneath the indenter tip. In this work, a simplified viscoelastic-plastic damage model was developed to more closely simulate indentation creep data, and the effect of the model parameters on the indentation curve was investigated. Experimentally, baseline and 2-year postovariectomized (OVX-2) ovine (sheep) bone samples were prepared and indented. The damage model was then applied via finite element analysis to simulate the bone indentation data. The mechanical properties of yielding, viscosity, and damage parameter were obtained from the simulations. The results suggest that damage develops more quickly for OVX-2 samples under the same indentation load conditions as the baseline data. PMID:26136623

The physical and mechanical metallurgy of advanced O+BCC titanium alloys

NASA Astrophysics Data System (ADS)

Cowen, Christopher John

This thesis comprises a systematic study of the microstructural evolution, phase transformation behavior, elevated-temperature creep behavior, room-temperature and elevated-temperature tensile behavior, and room-temperature fatigue behavior of advanced titanium-aluminum-niobium (Ti-Al-Nb) alloys with and without boron additions. The specific alloys studied were: Ti-5A1-45Nb (at%), Ti-15Al-33Nb (at%), Ti-15Al-33Nb-0.5B (at%), Ti-15Al-33Nb-5B (at%), Ti-21Al-29Nb (at%), Ti-22Al-26Nb (at%), and Ti-22Al-26Nb-5B (at%). The only alloy composition that had been previously studied before this thesis work began was Ti-22Al-26Nb (at%). Publication in peer-reviewed material science journals of the work performed in this thesis has made data available in the scientific literature that was previously non-existent. The knowledge gap for Ti-Al-Nb phase equilibria over the compositional range of Ti-23Al-27Nb (at%) to Ti-12Al-38Nb (at%) that existed before this work began was successfully filled. The addition of 5 at% boron to the Ti-15Al-33Nb alloy produced 5-9 volume percent boride phase needles within the microstructure. The chemical composition of the boride phase measured by electron microprobe was determined to be approximately B 2TiNb. The lattice parameters of the boride phase were simulated through density functional theory calculations by collaborators at the Air Force Research Laboratory based on the measured composition. Using the simulated lattice parameters, electron backscatter diffraction kikuchi patterns and selected area electron diffraction patterns obtained from the boride phase were successfully indexed according to the space group and site occupancies of the B27 orthorhombic crystal structure. This suggests that half the Ti (c) Wyckoff positions are occupied by Ti atoms and the other half are occupied by Nb atoms in the boride phase lattice. Creep deformation behavior is the main focus of this thesis and in particular understanding the dominant creep deformation mechanisms as a function of stress, temperature, and strain rate. Microstructure-creep relationships for Ti-Al-Nb-xB alloys were developed with the understanding gained. A rule-of-mixtures empirical model based on constituent phase volume fractions and strain rates was developed to predict the minimum creep rates of two-phase O+BCC microstructures. The most innovative results of this thesis were produced through the development of an in-situ creep testing methodology. The creep deformation evolution was chronicled in-situ during high temperature creep experiments, while creep displacement versus time data was simultaneously obtained. The in-situ experiments revealed that prior-BCC grain boundaries were the locus of damage accumulation during creep deformation. A methodology that allows in-situ observation of surface creep deformation as a function of creep displacement has yet to be presented in the literature.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Neilsen, Michael K.; Lu, Wei-Yang; Scherzinger, William M.

Numerous experiments were performed to characterize the mechanical response of several different rigid polyurethane foams (FR3712, PMDI10, PMDI20, and TufFoam35) to large deformation. In these experiments, the effects of load path, loading rate, and temperature were investigated. Results from these experiments indicated that rigid polyurethane foams exhibit significant volumetric and deviatoric plasticity when they are compressed. Rigid polyurethane foams were also found to be very strain-rate and temperature dependent. These foams are also rather brittle and crack when loaded to small strains in tension or to larger strains in compression. Thus, a new Unified Creep Plasticity Damage (UCPD) model wasmore » developed and implemented into SIERRA with the name Foam Damage to describe the mechanical response of these foams to large deformation at a variety of temperatures and strain rates. This report includes a description of recent experiments and experimental findings. Next, development of a UCPD model for rigid, polyurethane foams is described. Selection of material parameters for a variety of rigid polyurethane foams is then discussed and finite element simulations with the new UCPD model are compared with experimental results to show behavior that can be captured with this model.« less

Irradiation-induced creep in metallic nanolaminates characterized by In situ TEM pillar nanocompression

DOE PAGES

Dillon, Shen J.; Bufford, Daniel C.; Jawaharram, Gowtham S.; ...

2017-04-13

Our work reports on irradiation-induced creep (IIC) measured on nanolaminate (Cu-W and Ni-Ag) and nanocrystalline alloys (Cu-W) at room temperature using a combination of heavy ion irradiation and nanopillar compression performed concurrently in situ in a transmission electron microscope. Furthermore, we observed appreciable IIC in multilayers with 50 nm layer thicknesses at high stress, ≈½ the yield strength, but not in multilayers with only 5 nm layer thicknesses.

Early detection of materials degradation

NASA Astrophysics Data System (ADS)

Meyendorf, Norbert

2017-02-01

Lightweight components for transportation and aerospace applications are designed for an estimated lifecycle, taking expected mechanical and environmental loads into account. The main reason for catastrophic failure of components within the expected lifecycle are material inhomogeneities, like pores and inclusions as origin for fatigue cracks, that have not been detected by NDE. However, material degradation by designed or unexpected loading conditions or environmental impacts can accelerate the crack initiation or growth. Conventional NDE methods are usually able to detect cracks that are formed at the end of the degradation process, but methods for early detection of fatigue, creep, and corrosion are still a matter of research. For conventional materials ultrasonic, electromagnetic, or thermographic methods have been demonstrated as promising. Other approaches are focused to surface damage by using optical methods or characterization of the residual surface stresses that can significantly affect the creation of fatigue cracks. For conventional metallic materials, material models for nucleation and propagation of damage have been successfully applied for several years. Material microstructure/property relations are well established and the effect of loading conditions on the component life can be simulated. For advanced materials, for example carbon matrix composites or ceramic matrix composites, the processes of nucleation and propagation of damage is still not fully understood. For these materials NDE methods can not only be used for the periodic inspections, but can significantly contribute to the material scientific knowledge to understand and model the behavior of composite materials.

Superplastic Creep of Metal Nanowires From Rate-Dependent Plasticity Transition

DOE PAGES

Tao, Weiwei; Cao, Penghui; Park, Harold S.

2018-04-30

Understanding the time-dependent mechanical behavior of nanomaterials such as nanowires is essential to predict their reliability in nanomechanical devices. This understanding is typically obtained using creep tests, which are the most fundamental loading mechanism by which the time dependent deformation of materials is characterized. However, due to existing challenges facing both experimentalists and theorists, the time dependent mechanical response of nanowires is not well-understood. Here, we use atomistic simulations that can access experimental time scales to examine the creep of single-crystal face-centered cubic metal (Cu, Ag, Pt) nanowires. Here, we report that both Cu and Ag nanowires show significantly increasedmore » ductility and superplasticity under low creep stresses, where the superplasticity is driven by a rate-dependent transition in defect nucleation from twinning to trailing partial dislocations at the micro- or millisecond time scale. The transition in the deformation mechanism also governs a corresponding transition in the stress-dependent creep time at the microsecond (Ag) and millisecond (Cu) time scales. Overall, this work demonstrates the necessity of accessing time scales that far exceed those seen in conventional atomistic modeling for accurate insights into the time-dependent mechanical behavior and properties of nanomaterials.« less

Superplastic Creep of Metal Nanowires from Rate-Dependent Plasticity Transition.

PubMed

Tao, Weiwei; Cao, Penghui; Park, Harold S

2018-05-22

Understanding the time-dependent mechanical behavior of nanomaterials such as nanowires is essential to predict their reliability in nanomechanical devices. This understanding is typically obtained using creep tests, which are the most fundamental loading mechanism by which the time-dependent deformation of materials is characterized. However, due to existing challenges facing both experimentalists and theorists, the time-dependent mechanical response of nanowires is not well-understood. Here, we use atomistic simulations that can access experimental time scales to examine the creep of single-crystal face-centered cubic metal (Cu, Ag, Pt) nanowires. We report that both Cu and Ag nanowires show significantly increased ductility and superplasticity under low creep stresses, where the superplasticity is driven by a rate-dependent transition in defect nucleation from twinning to trailing partial dislocations at the micro- or millisecond time scale. The transition in the deformation mechanism also governs a corresponding transition in the stress-dependent creep time at the microsecond (Ag) and millisecond (Cu) time scales. Overall, this work demonstrates the necessity of accessing time scales that far exceed those seen in conventional atomistic modeling for accurate insights into the time-dependent mechanical behavior and properties of nanomaterials.

Superplastic Creep of Metal Nanowires From Rate-Dependent Plasticity Transition

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tao, Weiwei; Cao, Penghui; Park, Harold S.

Understanding the time-dependent mechanical behavior of nanomaterials such as nanowires is essential to predict their reliability in nanomechanical devices. This understanding is typically obtained using creep tests, which are the most fundamental loading mechanism by which the time dependent deformation of materials is characterized. However, due to existing challenges facing both experimentalists and theorists, the time dependent mechanical response of nanowires is not well-understood. Here, we use atomistic simulations that can access experimental time scales to examine the creep of single-crystal face-centered cubic metal (Cu, Ag, Pt) nanowires. Here, we report that both Cu and Ag nanowires show significantly increasedmore » ductility and superplasticity under low creep stresses, where the superplasticity is driven by a rate-dependent transition in defect nucleation from twinning to trailing partial dislocations at the micro- or millisecond time scale. The transition in the deformation mechanism also governs a corresponding transition in the stress-dependent creep time at the microsecond (Ag) and millisecond (Cu) time scales. Overall, this work demonstrates the necessity of accessing time scales that far exceed those seen in conventional atomistic modeling for accurate insights into the time-dependent mechanical behavior and properties of nanomaterials.« less

Effect of Long-Term Thermal Exposures on Microstructure and Impression Creep in 304HCu Grade Austenitic Stainless Steel

NASA Astrophysics Data System (ADS)

Dash, Manmath Kumar; Karthikeyan, T.; Mythili, R.; Vijayanand, V. D.; Saroja, S.

2017-10-01

This paper presents the results of microstructural evolution and mechanical properties in 304H Cu grade austenite stainless (SS 304HCu) during long-term exposure at high temperatures. The predicted phase composition as a function of temperature obtained using JMatPro® software was confirmed in conjunction with the microstructural evolution characterized by scanning and transmission electron microscopy. Microstructures revealed primary Nb(C,N), M23C6 precipitates at γ-grain boundaries, fine secondary Nb(C,N) intragranular carbides, and a uniform precipitation of <40-nm-sized spherical Cu-rich phase after thermal aging for 10,000 hours at 903 K (630 °C). The impression creep rate at 300 MPa increased by a factor of 20 between 873 K and 923 K (600 °C and 650 °C). The creep rate at 903 K (630 °C) was found to moderately reduce with aging time, signifying the role of Cu-rich phase in improving the creep resistance. The deformation zones and the recrystallization behavior of the plastic zone in creep tested specimen was assessed using Electron backscatter diffraction technique.

Time dependent micromechanics in continuous graphite fiber/epoxy composites with fiber breaks

NASA Astrophysics Data System (ADS)

Zhou, Chao Hui

Time dependent micromechanics in graphite fiber/epoxy composites around fiber breaks was investigated with micro Raman spectroscopy (MRS) and two shear-lag based composite models, a multi-fiber model (VBI) and a single fiber model (SFM), which aim at predicting the strain/stress evolutions in the composite from the matrix creep behavior and fiber strength statistics. This work is motivated by the need to understand the micromechanics and predict the creep-rupture of the composites. Creep of the unfilled epoxy was characterized under different stress levels and at temperatures up to 80°C, with two power law functions, which provided the modeling parameters used as input for the composite models. Both the VBI and the SFM models showed good agreement with the experimental data obtained with MRS, when inelasticity (interfacial debonding and/or matrix yielding) was not significant. The maximum shear stress near a fiber break relaxed at t-alpha/2 (or as (1+ talpha)-1/2) and the load recovery length increased at talpha/2(or (1+ talpha)1/2) following the model predictions. When the inelastic zone became non-negligible, the viscoelastic VBI model lost its competence, while the SFM with inelasticity showed good agreement with the MRS measurements. Instead of using the real fiber spacing, an effective fiber spacing was used in model predictions, taking into account of the radial decay of the interfacial shear stress from the fiber surface. The comparisons between MRS data and the SFM showed that inelastic zone would initiate when the shear strain at the fiber end exceeds a critical value gammac which was determined to be 5% for this composite system at room temperature and possibly a smaller value at elevated temperatures. The stress concentrations in neighboring intact fibers played important roles in the subsequent fiber failure and damage growth. The VBI model predicts a constant stress concentration factor, 1.33, for the 1st nearest intact fiber, which is in good agreement with MRS measurements for most cases except for those with severely debonded interfaces. However, the VBI model usually gives a stress concentration profile narrower than the measured one due to the inelasticity near the fiber break. The low average fiber volume fraction in the model composites caused small relaxation in the stress concentration, which became more obvious at elevated temperatures, especially for large fiber spacing cases. When new break(s) occurred in the original intact neighboring fibers within an effective distance from the original break, the inelastic zones grew at a faster rate due to the strong interactions. Results on the creep-rupture of the bulk composites showed that the failure probability depends on the stress level and the loading time. The time dependent failure probability data could be fitted to a power law function, which suggested a link between the matrix creep, composite short-term strength and the composite creep-rupture.

Irradiation creep and microstructural changes in an advanced ODS ferritic steel during helium implantation under stress

NASA Astrophysics Data System (ADS)

Chen, J.; Pouchon, M. A.; Kimura, A.; Jung, P.; Hoffelner, W.

2009-04-01

An advanced oxide dispersion strengthened (ODS) ferritic steel with very fine oxide particles has been homogeneously implanted with helium under uniaxial tensile stresses from 20 to 250 MPa to a maximum dose of about 0.38 dpa (1650 appm-He) with displacement damage rates of 4.4 × 10 -6 dpa/s at temperatures of 573 and 773 K. The samples were in the form of miniaturized dog-bones, where during the helium implantation the straining and the electrical resistance were monitored simultaneously. Creep compliances were measured to be 4.0 × 10 -6 and 11 × 10 -6 dpa -1 MPa -1 at 573 and 773 K, respectively. The resistivity of ODS steel samples decreased with dose, indicating segregation and/or precipitation. Evolution of microstructure during helium implantation was studied in detail by TEM. The effects of ODS particle size on irradiation creep and microstructural changes was investigated by comparing the results from the present advanced ODS (K1) to a commercial ODS ferritic steels (PM2000) with much bigger oxide particles.

Creep life prediction of super heater coils used in coal based thermal power plants subjected to fly ash erosion and oxide scale formation

NASA Astrophysics Data System (ADS)

Srinivasan, P.; Kushwaha, Shashank

2018-04-01

Super heater coils of the coal based thermal power plants and subjected to severe operating conditions from both steam side and gas side. Formation of oxide scale due to prolonged service lead to temperature raise of the tube and erosion due to fly ash present in the combusted gases leads to tube thinning. Both these factors lead to creep rupture of the coils much before the designed service life. Failure of super heater coils during service of the boiler leads to power loss and huge monitory loss to the power plants. An attempt is made to model the creep damage caused to the super heater coils using heat transfer analysis tube thinning due to erosive wear of the tubes. Combined effects of these parameters are taken into consideration to predict the life of the super heater coils. This model may be used to estimate the life of the coils operating under the severe operating conditions to prevent the unexpected failure of the coils.

Modeling the mechanical response of PBX 9501

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ragaswamy, Partha; Lewis, Matthew W; Liu, Cheng

2010-01-01

An engineering overview of the mechanical response of Plastic-Bonded eXplosives (PBXs), specifically PBX 9501, will be provided with emphasis on observed mechanisms associated with different types of mechanical testing. Mechanical tests in the form of uniaxial tension, compression, cyclic loading, creep (compression and tension), and Hopkinson bar show strain rate and temperature dependence. A range of mechanical behavior is observed which includes small strain recoverable response in the form of viscoelasticity; change in stiffness and softening beyond peak strength due to damage in the form microcracks, debonding, void formation and the growth of existing voids; inelastic response in the formmore » of irrecoverable strain as shown in cyclic tests, and viscoelastic creep combined with plastic response as demonstrated in creep and recovery tests. The main focus of this paper is to elucidate the challenges and issues involved in modeling the mechanical behavior of PBXs for simulating thermo-mechanical responses in engineering components. Examples of validation of a constitutive material model based on a few of the observed mechanisms will be demonstrated against three point bending, split Hopkinson pressure bar and Brazilian disk geometry.« less

U 3Si 2 Fabrication and Testing for Implementation into the BISON Fuel Performance Code

DOE Office of Scientific and Technical Information (OSTI.GOV)

Knight, Travis W.

A creep test stand was designed and constructed for compressive creep testing of U 3Si 2 pellets. This is described in Chapter 3. Creep testing of U 3Si 2 pellets was completed. In total, 13 compressive creep tests of U 3Si 2 pellets was successfully completed. This is reported in Chapter 3. Secondary creep model of U 3Si 2 was developed and implemented in BISON. This is described in Chapter 4. Properties of U 3Si 2 were implemented in BISON. This is described in Chapter 4. A resonant frequency and damping analyzer (RFDA) using impulse excitation technique (IET) was setup,more » tested, and used to analyze U 3Si 2 samples to measure Young’s and Shear Moduli which were then used to calculate the Poisson ratio for U 3Si 2. This is described in Chapter 5. Characterization of U 3Si 2 samples was completed. Samples were prepared and analyzed by XRD, SEM, and optical microscopy. Grain size analysis was conducted on images. SEM with EDS was used to analyze second phase precipitates. Impulse excitation technique was used to determine the Young’s and Shear Moduli of a tile specimen which allowed for the determination of the Poisson ratio. Helium pycnometry and mercury intrusion porosimetry was performed and used with image analysis to determine porosity size distribution. Vickers microindentation characterization method was used to evaluate the mechanical properties of U 3Si 2 including toughness, hardness, and Vickers hardness. Electrical resistivity measurement was done using the four-point probe method. This is reported in Chapter 5.« less

Low strain, long life creep fatigue of AF2-1DA and INCO 718

NASA Technical Reports Server (NTRS)

Thakker, A. B.; Cowles, B. A.

1983-01-01

Two aircraft turbine disk alloys, GATORIZED AF2-DA and INCO 718 were evaluated for their low strain long life creep-fatigue behavior. Static (tensile and creep rupture) and cyclic properties of both alloys were characterized. The cntrolled strain LCF tests were conducted at 760 C (1400 F) and 649 C (1200 F) for AF2-1DA and INCO 718, respectively. Hold times were varied for tensile, compressive and tensile/compressive strain dwell (relaxation) tests. Stress (creep) hold behavior of AF2-1DA was also evaluated. Generally, INCO 718 exhibited more pronounced reduction in cyclic life due to hold than AF2-1DA. The percent reduction in life for both alloys for strain dwell tests was greater at low strain ranges (longer life regime). Changing hold time from 0 to 0.5, 2.0 and 15.0 min. resulted in corresponding reductions in life. The continuous cycle and cyclic/dwell initiation failure mechanism was predominantly transgranular for AF2-1DA and intergranular for INCO 718.

Constitutive Modeling of a Glass Fiber-Reinforced PTFE Gasketed-Joint Under a Re-torque

NASA Astrophysics Data System (ADS)

Williams, James; Gordon, Ali P.

Joints gasketed with viscoelastic seals often receive an application of a secondary torque, i.e., retorque, in order to ensure joint tightness and proper sealing. The motivation of this study is to characterize and analytically model the load and deflection re-torque response of a single 25% glass-fiber reinforced polytetrafluorethylene (PTFE) gasket-bolted joint with serrated flange detail. The Burger-type viscoelastic modeling constants of the material are obtained through isolating the gasket from the bolt by performing a gasket creep test via a MTS electromechanical test frame. The re-load creep response is also investigated by re-loading the gasket after a period of initial creep to observe the response. The modeling constants obtained from the creep tests are used with a Burger-type viscoelastic model to predict the re-torque response of a single bolt-gasket test fixture in order to validate the ability of the model to simulate the re-torque response under various loading conditions and flange detail.

Deformation and crack growth response under cyclic creep conditions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Brust, F.W. Jr.

To increase energy efficiency, new plants must operate at higher and higher temperatures. Moreover, power generation equipment continues to age and is being used far beyond its intended original design life. Some recent failures which unfortunately occurred with serious consequences have clearly illustrated that current methods for insuring safety and reliability of high temperature equipment is inadequate. Because of these concerns, an understanding of the high-temperature crack growth process is very important and has led to the following studies of the high temperature failure process. This effort summarizes the results of some recent studies which investigate the phenomenon of highmore » temperature creep fatigue crack growth. Experimental results which detail the process of creep fatigue, analytical studies which investigate why current methods are ineffective, and finally, a new approach which is based on the T{sup *}-integral and its ability to characterize the creep-fatigue crack growth process are discussed. The potential validity of this new predictive methodology is illustrated.« less

Fine-pore aeration diffusers: accelerated membrane ageing studies.

PubMed

Kaliman, An; Rosso, Diego; Leu, Shao-Yuan; Stenstrom, Michael K

2008-01-01

Polymeric membranes are widely used in aeration systems for biological treatment. These membranes may degrade over time and are sensitive to fouling and scaling. Membrane degradation is reflected in a decline in operating performance and higher headloss, resulting in increased energy costs. Mechanical property parameters, such as membrane hardness, Young's modulus, and orifice creep, were used to characterize the performance of membranes over time in operation and to predict their failure. Used diffusers from municipal wastewater treatment plants were collected and tested for efficiency and headloss, and then dissected to facilitate measurements of Young's modulus, hardness, and orifice creep. Higher degree of membrane fouling corresponded consistently with larger orifice creep. A lab-scale membrane ageing simulation was performed with polyurethane and four different ethylene-propylene-diene (EPDM) membrane diffusers by subjecting them to chemical ageing cycles and periodic testing. The results confirmed full-scale plant results and showed the superiority of orifice creep over Young's modulus and hardness in predicting diffuser deterioration.

Axisymmetric thermoviscoelastoplastic state of thin laminated shells made of a damageable material

NASA Astrophysics Data System (ADS)

Galishin, A. Z.

2008-04-01

A technique for the determination of the axisymmetric thermoviscoelastoplastic state of laminated thin shells made of a damageable material is developed. The technique is based on the kinematic equations of the theory of thin shells that account for transverse shear strains. The thermoviscoplastic equations, which describe the deformation of a shell element along paths of small curvature, are used as the constitutive equations. The equivalent stress that appears in the kinetic equations of damage and creep is determined from a failure criterion that accounts for the stress mode. The thermoviscoplastic deformation of a two-layer shell that models an element of a rocket engine nozzle is considered as an example

Creep Strength Behavior of Boron Added P91 Steel and its Weld in the Temperature Range of 600-650°C

NASA Astrophysics Data System (ADS)

Swaminathan, J.; Das, C. R.; Baral, Jayashree; Phaniraj, C.; Ghosh, R. N.; Albert, S. K.; Bhaduri, A. K.

One of the promising ways for mitigation of Type IV cracking — a failure by cracking at the intercritical /fine grained heat affected zone, a life limiting problem in advanced 9-12 Cr ferritic steel weld like that of P91 is through modification of alloy composition by addition of boron. Addition of boron was observed to improve the microstructure at the weld zone and hence the creep strength. In the present work, boron (100 ppm with controlled nitrogen) added P91 steel after normalizing at 1050°C and 1150°C and tempered at 760°C were studied for the creep behavior in the base metal and welded condition in the temperature range of 600-650°C. Creep strength was characterized in terms of stress and temperature dependence of creep rate and rupture time. Weld creep life was reduced compared to the base metal with rupture occurring at the ICHAZ (Type IV crack). However at longer time (at lower stress levels) exposure creep crack moves from weld metal to HAZ (Type II crack). Rupture life was found to superior for the base and weld in the boron containing steel when higher normalizing temperature is used. Estimation of 105 h was attempted based on short term rupture data available and weld strength factors were calculated. Observed values are better for P91BH condition than the values for P91BLcondition as well as those available for P91 in open literature

Coupled modeling of a directly heated tubular solar receiver for supercritical carbon dioxide Brayton cycle: Structural and creep-fatigue evaluation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ortega, Jesus; Khivsara, Sagar; Christian, Joshua

A supercritical carbon dioxide (sCO 2) Brayton cycle is an emerging high energy-density cycle undergoing extensive research due to the appealing thermo-physical properties of sCO 2 and single phase operation. Development of a solar receiver capable of delivering sCO 2 at 20 MPa and 700 °C is required for implementation of the high efficiency (~50%) solar powered sCO 2 Brayton cycle. In this work, extensive candidate materials are review along with tube size optimization using the ASME Boiler and Pressure Vessel Code. Moreover, temperature and pressure distribution obtained from the thermal-fluid modeling (presented in a complementary publication) are used tomore » evaluate the thermal and mechanical stresses along with detailed creep-fatigue analysis of the tubes. The lifetime performance of the receiver tubes were approximated using the resulting body stresses. A cyclic loading analysis is performed by coupling the Strain-Life approach and the Larson-Miller creep model. The structural integrity of the receiver was examined and it was found that the stresses can be withstood by specific tubes, determined by a parametric geometric analysis. Furthermore, the creep-fatigue analysis displayed the damage accumulation due to cycling and the permanent deformation on the tubes showed that the tubes can operate for the full lifetime of the receiver.« less

Coupled modeling of a directly heated tubular solar receiver for supercritical carbon dioxide Brayton cycle: Structural and creep-fatigue evaluation

DOE PAGES

Ortega, Jesus; Khivsara, Sagar; Christian, Joshua; ...

2016-06-06

A supercritical carbon dioxide (sCO 2) Brayton cycle is an emerging high energy-density cycle undergoing extensive research due to the appealing thermo-physical properties of sCO 2 and single phase operation. Development of a solar receiver capable of delivering sCO 2 at 20 MPa and 700 °C is required for implementation of the high efficiency (~50%) solar powered sCO 2 Brayton cycle. In this work, extensive candidate materials are review along with tube size optimization using the ASME Boiler and Pressure Vessel Code. Moreover, temperature and pressure distribution obtained from the thermal-fluid modeling (presented in a complementary publication) are used tomore » evaluate the thermal and mechanical stresses along with detailed creep-fatigue analysis of the tubes. The lifetime performance of the receiver tubes were approximated using the resulting body stresses. A cyclic loading analysis is performed by coupling the Strain-Life approach and the Larson-Miller creep model. The structural integrity of the receiver was examined and it was found that the stresses can be withstood by specific tubes, determined by a parametric geometric analysis. Furthermore, the creep-fatigue analysis displayed the damage accumulation due to cycling and the permanent deformation on the tubes showed that the tubes can operate for the full lifetime of the receiver.« less

Investigation of Creep Processes and Microdamages in 10Kh9V2MFBR-Sh High-Chromium Steel

NASA Astrophysics Data System (ADS)

Grin', E. A.; Pchelintsev, A. V.

2018-01-01

During the modernization and the new construction of power units at TPPs in Russia, high-chromium martensitic steels with higher heat-resistant properties than the traditional perlite steels are increasingly used as structural materials. High-chromium steels have a necessary regulatory support for their use in domestic power engineering. However, up to the present time, the issue of assessing the quality of these steels at the analysis of their state during long-term operation remains open. The article proposed is one of the first attempts to create a system of quality criteria for martensitic steels based on their microdamage parameters. Tests were carried out on the long-term strength and creep of samples from 10Kh9V2MFBR-Sh steel at high temperatures with the construction of creep curves in relative coordinates "deformation related to the deformation of fracture, current time related to time to failure." For some samples, the tests were interrupted and the metal was subjected to metallographic studies consisting of the analysis of microdamage with reference to the accumulated creep strain. It has been shown experimentally that the deformation curve of high-chromium steel differs from the analogous curve of pearlitic steel by a longer and flat section of steady creep and by a sharper transition to the third accelerated creep stage, which has a very short time period (approximately 10% of the total durability). The tendency to the increase in the microdamage of the structure of steel as the accumulated creep strain increases with time was confirmed. The beginning of transition to the final creep phase is characterized by the formation of contours of future pore chains and by the appearance of individual large pores of up to 6 μm in size, the presence of which in the microstructure of the martensitic steel indicates a very significant accumulation of creep strain, and corresponds to the predestruction stage of metal. It is necessary to continue the research to obtain quantitative indicators on the accumulation of microdamage in high-chromium steel in a conjunction with the development of a metal resource under creep conditions.

Early stage fatigue damage occurs in bovine tendon fascicles in the absence of changes in mechanics at either the gross or micro-structural level.

PubMed

Shepherd, Jennifer H; Riley, Graham P; Screen, Hazel R C

2014-10-01

Many tendon injuries are believed to result from repetitive motion or overuse, leading to the accumulation of micro-damage over time. In vitro fatigue loading can be used to characterise damage during repeated use and investigate how this may relate to the aetiology of tendinopathy. This study considered the effect of fatigue loading on fascicles from two functionally distinct bovine tendons: the digital extensor and deep digital flexor. Micro-scale extension mechanisms were investigated in fascicles before or after a period of cyclic creep loading, comparing two different measurement techniques - the displacement of a photo-bleached grid and the use of nuclei as fiducial markers. Whilst visual damage was clearly identified after only 300 cycles of creep loading, these visual changes did not affect either gross fascicle mechanics or fascicle microstructural extension mechanisms over the 900 fatigue cycles investigated. However, significantly greater fibre sliding was measured when observing grid deformation rather than the analysis of nuclei movement. Measurement of microstructural extension with both techniques was localised and this may explain the absence of change in microstructural deformation in response to fatigue loading. Alternatively, the data may demonstrate that fascicles can withstand a degree of matrix disruption with no impact on mechanics. Whilst use of a photo-bleached grid to directly measure the collagen is the best indicator of matrix deformation, nuclei tracking may provide a better measure of the strain perceived directly by the cells. Copyright © 2014 The Authors. Published by Elsevier Ltd.. All rights reserved.

The Influence of Temperature on Time-Dependent Deformation and Failure in Granite: A Mesoscale Modeling Approach

NASA Astrophysics Data System (ADS)

Xu, T.; Zhou, G. L.; Heap, Michael J.; Zhu, W. C.; Chen, C. F.; Baud, Patrick

2017-09-01

An understanding of the influence of temperature on brittle creep in granite is important for the management and optimization of granitic nuclear waste repositories and geothermal resources. We propose here a two-dimensional, thermo-mechanical numerical model that describes the time-dependent brittle deformation (brittle creep) of low-porosity granite under different constant temperatures and confining pressures. The mesoscale model accounts for material heterogeneity through a stochastic local failure stress field, and local material degradation using an exponential material softening law. Importantly, the model introduces the concept of a mesoscopic renormalization to capture the co-operative interaction between microcracks in the transition from distributed to localized damage. The mesoscale physico-mechanical parameters for the model were first determined using a trial-and-error method (until the modeled output accurately captured mechanical data from constant strain rate experiments on low-porosity granite at three different confining pressures). The thermo-physical parameters required for the model, such as specific heat capacity, coefficient of linear thermal expansion, and thermal conductivity, were then determined from brittle creep experiments performed on the same low-porosity granite at temperatures of 23, 50, and 90 °C. The good agreement between the modeled output and the experimental data, using a unique set of thermo-physico-mechanical parameters, lends confidence to our numerical approach. Using these parameters, we then explore the influence of temperature, differential stress, confining pressure, and sample homogeneity on brittle creep in low-porosity granite. Our simulations show that increases in temperature and differential stress increase the creep strain rate and therefore reduce time-to-failure, while increases in confining pressure and sample homogeneity decrease creep strain rate and increase time-to-failure. We anticipate that the modeling presented herein will assist in the management and optimization of geotechnical engineering projects within granite.

Creep Behavior of a Sn-Ag-Bi Pb-Free Solder

PubMed Central

Vianco, Paul; Rejent, Jerome; Grazier, Mark; Kilgo, Alice

2012-01-01

Compression creep tests were performed on the ternary 91.84Sn-3.33Ag-4.83Bi (wt.%, abbreviated Sn-Ag-Bi) Pb-free alloy. The test temperatures were: −25 °C, 25 °C, 75 °C, 125 °C, and 160 °C (± 0.5 °C). Four loads were used at the two lowest temperatures and five at the higher temperatures. The specimens were tested in the as-fabricated condition or after having been subjected to one of two air aging conditions: 24 hours at either 125 °C or 150 °C. The strain-time curves exhibited frequent occurrences of negative creep and small-scale fluctuations, particularly at the slower strain rates, that were indicative of dynamic recrystallization (DRX) activity. The source of tertiary creep behavior at faster strain rates was likely to also be DRX rather than a damage accumulation mechanism. Overall, the strain-time curves did not display a consistent trend that could be directly attributed to the aging condition. The sinh law equation satisfactorily represented the minimum strain rate as a function of stress and temperature so as to investigate the deformation rate kinetics: dε/dtmin = Asinhn (ασ) exp (−ΔH/RT). The values of α, n, and ΔH were in the following ranges (±95% confidence interval): α, 0.010–0.015 (±0.005 1/MPa); n, 2.2–3.1 (±0.5); and ΔH, 54–66 (±8 kJ/mol). The rate kinetics analysis indicated that short-circuit diffusion was a contributing mechanism to dislocation motion during creep. The rate kinetics analysis also determined that a minimum creep rate trend could not be developed between the as-fabricated versus aged conditions. This study showed that the elevated temperature aging treatments introduced multiple changes to the Sn-Ag-Bi microstructure that did not result in a simple loss (“softening”) of its mechanical strength.

Environmental Barrier Coating Fracture, Fatigue and High-Heat-Flux Durability Modeling and Stochastic Progressive Damage Simulation

NASA Technical Reports Server (NTRS)

Zhu, Dongming; Nemeth, Noel N.

2017-01-01

Advanced environmental barrier coatings will play an increasingly important role in future gas turbine engines because of their ability to protect emerging light-weight SiC/SiC ceramic matrix composite (CMC) engine components, further raising engine operating temperatures and performance. Because the environmental barrier coating systems are critical to the performance, reliability and durability of these hot-section ceramic engine components, a prime-reliant coating system along with established life design methodology are required for the hot-section ceramic component insertion into engine service. In this paper, we have first summarized some observations of high temperature, high-heat-flux environmental degradation and failure mechanisms of environmental barrier coating systems in laboratory simulated engine environment tests. In particular, the coating surface cracking morphologies and associated subsequent delamination mechanisms under the engine level high-heat-flux, combustion steam, and mechanical creep and fatigue loading conditions will be discussed. The EBC compostion and archtechture improvements based on advanced high heat flux environmental testing, and the modeling advances based on the integrated Finite Element Analysis Micromechanics Analysis Code/Ceramics Analysis and Reliability Evaluation of Structures (FEAMAC/CARES) program will also be highlighted. The stochastic progressive damage simulation successfully predicts mud flat damage pattern in EBCs on coated 3-D specimens, and a 2-D model of through-the-thickness cross-section. A 2-parameter Weibull distribution was assumed in characterizing the coating layer stochastic strength response and the formation of damage was therefore modeled. The damage initiation and coalescence into progressively smaller mudflat crack cells was demonstrated. A coating life prediction framework may be realized by examining the surface crack initiation and delamination propagation in conjunction with environmental degradation under high-heat-flux and environment load test conditions.

Synergistic Effects of Physical Aging and Damage on Long-Term Behavior of Polymer Matrix Composites

NASA Technical Reports Server (NTRS)

Brinson, L. Cate

1999-01-01

The research consisted of two major parts, first modeling and simulation of the combined effects of aging and damage on polymer composites and secondly an experimental phase examining composite response at elevated temperatures, again activating both aging and damage. For the simulation, a damage model for polymeric composite laminates operating at elevated temperatures was developed. Viscoelastic behavior of the material is accounted for via the correspondence principle and a variational approach is adopted to compute the temporal stresses within the laminate. Also, the effect of physical aging on ply level stress and on overall laminate behavior is included. An important feature of the model is that damage evolution predictions for viscoelastic laminates can be made. This allows us to track the mechanical response of the laminate up to large load levels though within the confines of linear viscoelastic constitutive behavior. An experimental investigation of microcracking and physical aging effects in polymer matrix composites was also pursued. The goal of the study was to assess the impact of aging on damage accumulation, in ten-ns of microcracking, and the impact of damage on aging and viscoelastic behavior. The testing was performed both at room and elevated temperatures on [+/- 45/903](sub s) and [02/903](sub s) laminates, both containing a set of 90 deg plies centrally located to facilitate investigation of microcracking. Edge replication and X-ray-radiography were utilized to quantify damage. Sequenced creep tests were performed to characterize viscoelastic and aging parameters. Results indicate that while the aging times studied have limited ]Influence on damage evolution, elevated temperature and viscoelastic effects have a profound effect on the damage mode seen. Some results are counterintuitive, including the lower strain to failure for elevated temperature tests and the catastrophic failure mode observed for the [+/- 45/9O3](sub s), specimens. The fracture toughness for transverse cracks increases with increasing temperature for both systems: transverse cracking was completely absent prior to failure in [+/- 45/903](sub s), and was suppressed for [02/903](sub s). No significant effect of damage on aging or viscoelastic parameters was observed.

Irradiation creep and stress-enhanced swelling of Fe-16Cr-15Ni-Nb austenitic stainless steel in BN-350

DOE Office of Scientific and Technical Information (OSTI.GOV)

Vorobjev, A.N.; Porollo, S.I.; Konobeev, Yu.V.

1997-04-01

Irradiation creep and void swelling will be important damage processes for stainless steels when subjected to fusion neutron irradiation at elevated temperatures. The absence of an irradiation device with fusion-relevant neutron spectra requires that data on these processes be collected in surrogate devices such as fast reactors. This paper presents the response of an annealed austenitic steel when exposed to 60 dpa at 480{degrees}C and to 20 dpa at 520{degrees}C. This material was irradiated as thin-walled argon-pressurized tubes in the BN-350 reactor located in Kazakhstan. These tubes were irradiated at hoop stresses ranging from 0 to 200 MPa. After irradiationmore » both destructive and non-destructive examination was conducted.« less

FY16 Progress Report on Test Results In Support Of Integrated EPP and SMT Design Methods Development

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Yanli; Jetter, Robert I.; Sham, T. -L.

2016-08-08

The proposed integrated Elastic Perfectly-Plastic (EPP) and Simplified Model Test (SMT) methodology consists of incorporating an SMT data-based approach for creep-fatigue damage evaluation into the EPP methodology to avoid using the creep-fatigue interaction diagram (the D diagram) and to minimize over-conservatism while properly accounting for localized defects and stress risers. To support the implementation of the proposed code rules and to verify their applicability, a series of thermomechanical tests have been initiated. This report presents the recent test results for Type 2 SMT specimens on Alloy 617, Pressurization SMT on Alloy 617, Type 1 SMT on Gr. 91, and two-barmore » thermal ratcheting test results on Alloy 617 with a new thermal loading profile.« less

Utilization of fractography in the evaluations of high temperature dynamic fatigue experiments

DOE Office of Scientific and Technical Information (OSTI.GOV)

Breder, K.; Tennery, V.J.; Mroz, T.J.

1996-12-31

The slow crack growth properties of six structural ceramics were measured by dynamic fatigue in air and inert atmospheres over a range of elevated temperatures. The material response varied from no strength degradation as a function of stress and environment to significant strength degradation by slow crack growth (SCG) and by a combination of SCG and creep. The fractographic investigation showed that SCG was evidenced by growth of isolated cracks and often by an intergranular fracture mode, while creep was evidenced by accumulated damage such as void formation and opening of the microstructure at grain boundaries and triple junctions. Formore » the materials in which the strength was unaffected by the stress and environment, the fracture surfaces were essentially indistinguishable from the inert fracture surfaces.« less

Utilization of fractography in the evaluation of high temperature dynamic fatigue experiments

DOE Office of Scientific and Technical Information (OSTI.GOV)

Breder, K.; Wereszczak, A.A.; Tennery, V.J.

1995-12-31

The slow crack growth properties of six structural ceramics were measured by dynamic fatigue in air and inert atmospheres over a range of elevated temperatures. The material response varied from no strength degradation as a function of stress and environment to significant strength degradation by slow crack growth (SCG) and by a combination of SCG and creep. The fractographic investigation showed that SCG was evidenced by growth of isolated cracks and often by an intergranular fracture mode, while creep was evidenced by accumulated damage such as void formation and opening of the microstructure at grain boundaries and triple junctions. Formore » the materials in which the strength was unaffected by the stress and environment, the fracture surfaces were essentially indistinguishable from the inert fracture surfaces.« less

Grain Boundary Engineering the Mechanical Properties of Allvac 718Plus(Trademark) Superalloy

NASA Technical Reports Server (NTRS)

Gabb, Timothy P.; Telesman, Jack; Garg, Anita; Lin, Peter; Provenzano, virgil; Heard, Robert; Miller, Herbert M.

2010-01-01

Grain Boundary Engineering can enhance the population of structurally-ordered "low S" Coincidence Site Lattice (CSL) grain boundaries in the microstructure. In some alloys, these "special" grain boundaries have been reported to improve overall resistance to corrosion, oxidation, and creep resistance. Such improvements could be quite beneficial for superalloys, especially in conditions which encourage damage and cracking at grain boundaries. Therefore, the effects of GBE processing on high-temperature mechanical properties of the cast and wrought superalloy Allvac 718Plus (Allvac ATI) were screened. Bar sections were subjected to varied GBE processing, and then consistently heat treated, machined, and tested at 650 C. Creep, tensile stress relaxation, and dwell fatigue crack growth tests were performed. The influences of GBE processing on microstructure, mechanical properties, and associated failure modes are discussed.

The International Space Station Assembly on Schedule

NASA Technical Reports Server (NTRS)

1997-01-01

As engineers continue to prepare the International Space Station (ISS) for in-orbit assembly in the year 2002, ANSYS software has proven instrumental in resolving a structural problem in the project's two primary station modules -- Nodes 1 and 2. Proof pressure tests performed in May revealed "low temperature, post-yield creep" in some of the Nodes' gussets, which were designed to reinforce ports for loads from station keeping and reboost motion of the entire space station. An extensive effort was undertaken to characterize the creep behavior of the 2219-T851 aluminum forging material from which the gussets were made. Engineers at Sverdrup Technology, Inc. (Huntsville, AL) were responsible for conducting a combined elastic-plastic-creep analysis of the gussets to determine the amount of residual compressive stress which existed in the gussets following the proof pressure tests, and to determine the stress-strain history in the gussets while on-orbit. Boeing, NASA's Space Station prime contractor, supplied the Finite Element Analysis (FEA) model geometry and developed the creep equations from the experimental data taken by NASA's Marshall Space Flight Center and Langley Research Center. The goal of this effort was to implement the uniaxial creep equations into a three dimensional finite element program, and to determine analytically whether or not the creep was something that the space station program could live with. The objective was to show analytically that either the creep rate was at an acceptable level, or that the node module had to be modified to lower the stress levels to where creep did not occur. The elastic-plastic-creep analysis was performed using the ANSYS finite element program of ANSYS, Inc. (Houston, PA). The analysis revealed that the gussets encountered a compressive stress of approximately 30,000 pounds per square inch (psi) when unloaded. This compressive residual stress significantly lowered the maximum tension stress in the gussets which decreased the creep strain rate. The analysis also showed that the gussets would not experience a great deal of creep from future pressure tests if braces or struts proposed by Boeing were installed to redistribute stress away from them. Subsequent analysis of on-orbit station keeping and reboost loads convinced Boeing that the gussets should be removed altogether.

Surface/subsurface observation and removal mechanisms of ground reaction bonded silicon carbide

NASA Astrophysics Data System (ADS)

Yao, Wang; Zhang, Yu-Min; Han, Jie-cai; Zhang, Yun-long; Zhang, Jian-han; Zhou, Yu-feng; Han, Yuan-yuan

2006-01-01

Reaction Bonded Silicon Carbide (RBSiC) has long been recognized as a promising material for optical applications because of its unique combination of favorable properties and low-cost fabrication. Grinding of silicon carbide is difficult because of its high hardness and brittleness. Grinding often induces surface and subsurface damage, residual stress and other types of damage, which have great influence on the ceramic components for optical application. In this paper, surface integrity, subsurface damage and material removal mechanisms of RBSiC ground using diamond grinding wheel on creep-feed surface grinding machine are investigated. The surface and subsurface are studied with scanning electron microscopy (SEM) and optical microscopy. The effects of grinding conditions on surface and subsurface damage are discussed. This research links the surface roughness, surface and subsurface cracks to grinding parameters and provides valuable insights into the material removal mechanism and the dependence of grind induced damage on grinding conditions.

Fatigue and Creep-Fatigue Deformation of an Ultra-Fine Precipitate Strengthened Advanced Austenitic Alloy

DOE Office of Scientific and Technical Information (OSTI.GOV)

M.C. Carroll; L.J. Carroll

An advanced austenitic alloy, HT-UPS (high-temperature ultrafine-precipitation-strengthened), has been identified as an ideal candidate material for the structural components of fast reactors and energy-conversion systems. HT-UPS alloys demonstrate improved creep resistance relative to 316 stainless steel (SS) through additions of Ti and Nb, which precipitate to form a widespread dispersion of stable nanoscale metallic carbide (MC) particles in the austenitic matrix. The low-cycle fatigue and creep-fatigue behavior of an HT-UPS alloy have been investigated at 650 °C and a 1.0% total strain, with an R-ratio of -1 and hold times at peak tensile strain as long as 150 min. Themore » cyclic deformation response of HT-UPS is directly compared to that of standard 316 SS. The measured values for total cycles to failure are similar, despite differences in peak stress profiles and in qualitative observations of the deformed microstructures. Crack propagation is primarily transgranular in fatigue and creep-fatigue of both alloys at the investigated conditions. Internal grain boundary damage in the form of fine cracks resulting from the tensile hold is present for hold times of 60 min and longer, and substantially more internal cracks are quantifiable in 316 SS than in HT-UPS. The dislocation substructures observed in the deformed material differ significantly; an equiaxed cellular structure is observed in 316 SS, whereas in HT-UPS the microstructure takes the form of widespread and relatively homogenous tangles of dislocations pinned by the nanoscale MC precipitates. The significant effect of the fine distribution of precipitates on observed fatigue and creep-fatigue response is described in three distinct behavioral regions as it evolves with continued cycling.« less

Metallurgical causes for the occurrence of creep damage in longitudinally seam-welded Cr-Mo high-energy piping

NASA Astrophysics Data System (ADS)

Zhou, Gang

A continuous occurrence of catastrophic failures, leaks and cracks of the Cr-Mo steam piping has created widespread utility concern for the integrity and serviceability of the seam-welded piping systems in power plants across USA. Cr-Mo steels are the materials widely used for elevated temperature service in fossil-fired generating stations. A large percentage of the power plant units with the Cr-Mo seam-welded steam piping have been in operation for a long duration such that the critical components of the units have been employed beyond the design life (30 or 40 years). This percentage will increase even more significantly in the near future. There is a strong desire to extend and thus there is a need to assess the remaining life of these units. Thus, understanding of the metallurgical causes for the failures and damage in the Cr-Mo seam-welded piping plays a major role in estimating possible life-extension and decision making on whether to operate, repair or replace. In this study, an optical metallographic method and a Cryo-Crack fractographic method have been developed for characterization and quantification of the damage in seam-welded steam piping. More than 500 metallographic assessments, from more than 25 power plants, have been accomplished using the optical metallographic method, and more than 200 fractographic specimens from 10 power plants have been evaluated using the "Cryo-Crack" fractographic technique. For comparison, "virgin" SA welds were fabricated using the Mohave welding procedure with re-N&T Mohave base metal with both "acid" and "basic" fluxes. The damage mechanism, damage distribution pattern, damage classification, correlation of the damage with the microstructural features of these SA welds and the impurity segregation patterns have been determined. A physical model for cavitation (leading to failure) in Cr-Mo SA weld metals and evaluation methodologies for high energy piping are proposed.

Property Evaluation and Damage Evolution of Environmental Barrier Coatings and Environmental Barrier Coated SiC/SiC Ceramic Matrix Composite Sub-Elements

NASA Technical Reports Server (NTRS)

Zhu, Dongming; Halbig, Michael; Jaskowiak, Martha; Hurst, Janet; Bhatt, Ram; Fox, Dennis S.

2014-01-01

This paper describes recent development of environmental barrier coatings on SiC/SiC ceramic matrix composites. The creep and fatigue behavior at aggressive long-term high temperature conditions have been evaluated and highlighted. Thermal conductivity and high thermal gradient cyclic durability of environmental barrier coatings have been evaluated. The damage accumulation and complex stress-strain behavior environmental barrier coatings on SiCSiC ceramic matrix composite turbine airfoil subelements during the thermal cyclic and fatigue testing of have been also reported.

A Nonlinear Viscoelastic Model for Ceramics at High Temperatures

NASA Technical Reports Server (NTRS)

Powers, Lynn M.; Panoskaltsis, Vassilis P.; Gasparini, Dario A.; Choi, Sung R.

2002-01-01

High-temperature creep behavior of ceramics is characterized by nonlinear time-dependent responses, asymmetric behavior in tension and compression, and nucleation and coalescence of voids leading to creep rupture. Moreover, creep rupture experiments show considerable scatter or randomness in fatigue lives of nominally equal specimens. To capture the nonlinear, asymmetric time-dependent behavior, the standard linear viscoelastic solid model is modified. Nonlinearity and asymmetry are introduced in the volumetric components by using a nonlinear function similar to a hyperbolic sine function but modified to model asymmetry. The nonlinear viscoelastic model is implemented in an ABAQUS user material subroutine. To model the random formation and coalescence of voids, each element is assigned a failure strain sampled from a lognormal distribution. An element is deleted when its volumetric strain exceeds its failure strain. Element deletion has been implemented within ABAQUS. Temporal increases in strains produce a sequential loss of elements (a model for void nucleation and growth), which in turn leads to failure. Nonlinear viscoelastic model parameters are determined from uniaxial tensile and compressive creep experiments on silicon nitride. The model is then used to predict the deformation of four-point bending and ball-on-ring specimens. Simulation is used to predict statistical moments of creep rupture lives. Numerical simulation results compare well with results of experiments of four-point bending specimens. The analytical model is intended to be used to predict the creep rupture lives of ceramic parts in arbitrary stress conditions.

Special considerations for qualifying thin films for super pressure pumpkin ultra long duration balloon missions

NASA Astrophysics Data System (ADS)

Said, Magdi A.

2004-01-01

The assessment of creep and dynamic response behaviors on materials intended for ultra long duration balloon (ULDB) applications is essential. The first provides needed information for design and fabrication. The second ensures that the film is sufficiently tough to survive the dynamic events during launch and ascent. Characterization and assessment of these two important parameters are discussed in this paper. Visco-elastic behavior of materials in a loaded structure, such as the ULDB film change their geometry significantly over time under load causing possible changes in the load path and the stress distribution. These changes must be held in check to satisfy the functional requirements of the structure over its service life. Typically, the balloon experiences during its service life various environmental conditions each with a different creep response. These are characterized by a simplified load temperature history for the purpose of lifetime response assessment. At mid-latitudes a significant portion of the service life is spent at night, i.e., at low temperature and low load; for the ULDB film this night-time contribution to creep is negligible. By contrast, flight exposure in an Antarctic summer is at an almost constant high temperature and corresponding high pressure. This paper presents the creep behavior of the ULDB film as a function of load, temperature, and time along with an overview of its implementation in the design. In addition, it presents a quantitative assessment on the toughness of the material under dynamic "Snatch" loading.

Damage Assessment of Creep Tested and Thermally Aged Metallic Alloys Using Acousto-Ultrasonics

NASA Technical Reports Server (NTRS)

Gyekenyesi, Andrew L.; Kautz, Harold E.; Baaklini, George Y.

2001-01-01

In recent years emphasis has been placed on the early detection of material changes experienced in turbine powerplant components. During the scheduled overhaul of a turbine, the current techniques of examination of various hot section components aim to find flaws such as cracks, wear, and erosion, as well as excessive deformations. Thus far, these localized damage modes have been detected with satisfactory results. However, the techniques used to find these flaws provide no information on life until the flaws are actually detected. Major improvements in damage assessment, safety, as well as more accurate life prediction could be achieved if nondestructive evaluation (NDE) techniques could be utilized to sense material changes that occur prior to the localized defects mentioned. Because of elevated temperatures and excessive stresses, turbine components may experience creep behavior. As a result, it is desirable to monitor and access the current condition of such components. Research at the NASA Glenn Research Center involves developing and utilizing an NDE technique that discloses distributed material changes that occur prior to the localized damage detected by the current methods of inspection. In a recent study, creep processes in a nickel-base alloy were the life-limiting condition of interest, and the NDE technique was acousto-ultrasonics (AU). AU is an NDE technique that utilizes two ultrasonic transducers to interrogate the condition of a test specimen. The sending transducer introduces an ultrasonic pulse at a point on the surface of the specimen while a receiving transducer detects the signal after it has passed through the material. The goal of the method is to correlate certain parameters of the detected waveform to characteristics of the material between the two transducers. Here, the waveform parameter of interest is the attenuation due to internal damping for which information is being garnered from the frequency domain. The parameters utilized to indirectly quantify the attenuation are the ultrasonic decay rate as well as various moments of the frequency power spectrum. A new, user-friendly, graphical interface AU system was developed at NASA Glenn. This system is an all-inclusive, multifunction system that controls the sending and receiving ultrasonic transducers as well as all posttest signal analysis. The system's postprocessing software calculates the multiple parameters used to study the material of interest.

Thermomechanical fatigue life prediction for several solders

NASA Astrophysics Data System (ADS)

Wen, Shengmin

Since solder connections operate at high homologous temperature, solders are high temperature materials. This feature makes their mechanical behavior and fatigue phenomena unique. Based on experimental findings, a physical damage mechanism is introduced for solders. The mechanism views the damage process as a series of independent local damage events characterized by the failure of individual grains, while the structural damage is the eventual percolation result of such local events. Fine's dislocation energy density concept and Mura's microcrack initiation theory are adopted to derive the fatigue formula for an individual grain. A physical damage metric is introduced to describe the material with damage. A unified creep and plasticity constitutive model is adopted to simulate the mechanical behavior of solders. The model is cast into a continuum damage mechanics framework to simulate material with damage. The model gives good agreement with the experimental results of 96.5Pb-3.5Sn and 96.5Sn-3.5Ag solders under uniaxial strain-controlled cyclic loading. The model is convenient for implementation into commercial computational packages. Also presented is a fatigue theory with its failure criterion for solders based on physical damage mechanism. By introducing grain orientation into the fatigue formula, an m-N curve (m is Schmid factor) at constant loading condition is suggested for fatigue of grains with different orientations. A solder structure is defined as fatigued when the damage metric reaches a critical threshold, since at this threshold the failed grains may form a cluster and percolate through the structure according to percolation theory. Fatigue data of 96.5Pb-3.5Sn solder bulk specimens under various uniaxial tension tests were analyzed. Results show that the theory gives consistent predictions under broad conditions, while inelastic strain theory does not. The theory is anisotropic with no size limitation to its application, which could be suitable for anisotropic small-scale (micron or nano scale) solder joints. More importantly, the theory is materials science based so that the parameters of the fatigue formula can be worked out by testing of bulk specimens while the formula can be applicable to small-scale structures. The theory suggests metallurgical control in the manufacturing process to optimize the fatigue life of solder structures.

A damage mechanics based general purpose interface/contact element

NASA Astrophysics Data System (ADS)

Yan, Chengyong

Most of the microelectronics packaging structures consist of layered substrates connected with bonding materials, such as solder or epoxy. Predicting the thermomechanical behavior of these multilayered structures is a challenging task in electronic packaging engineering. In a layered structure the most complex part is always the interfaces between the strates. Simulating the thermo-mechanical behavior of such interfaces, is the main theme of this dissertation. The most commonly used solder material, Pb-Sn alloy, has a very low melting temperature 180sp°C, so that the material demonstrates a highly viscous behavior. And, creep usually dominates the failure mechanism. Hence, the theory of viscoplasticity is adapted to describe the constitutive behavior. In a multilayered assembly each layer has a different coefficient of thermal expansion. Under thermal cycling, due to heat dissipated from circuits, interfaces and interconnects experience low cycle fatigue. Presently, the state-of-the art damage mechanics model used for fatigue life predictions is based on Kachanov (1986) continuum damage model. This model uses plastic strain as a damage criterion. Since plastic strain is a stress path dependent value, the criterion does not yield unique damage values for the same state of stress. In this dissertation a new damage evolution equation based on the second law of thermodynamic is proposed. The new criterion is based on the entropy of the system and it yields unique damage values for all stress paths to the final state of stress. In the electronics industry, there is a strong desire to develop fatigue free interconnections. The proposed interface/contact element can also simulate the behavior of the fatigue free Z-direction thin film interconnections as well as traditional layered interconnects. The proposed interface element can simulate behavior of a bonded interface or unbonded sliding interface, also called contact element. The proposed element was verified against laboratory test data presented in the literature. The results demonstrate that the proposed element and the damage law perform very well. The most important scientific contribution of this dissertation is the proposed damage criterion based on second law of thermodynamic and entropy of the system. The proposed general purpose interface/contact element is another contribution of this research. Compared to the previous adhoc interface elements proposed in the literature, the new one is, much more powerful and includes creep, plastic deformations, sliding, temperature, damage, cyclic behavior and fatigue life in a unified formulation.

Some aspects of the damage kinetics at static loading of a heterogeneous solid under the conditions of constrained deformation

NASA Astrophysics Data System (ADS)

Leksovskii, A. M.; Baskin, B. L.; Yakushev, P. N.

2015-12-01

The damaging kinetics of a composite system subjected to static loading, which simulates an inhomogeneous body with microductility, and of D16T-B(43%) composite simulating a quasi-brittle solid is analyzed with the acoustic emission method. By using laser interferometry, it is shown on a model sample that mesocracking may cause a short-term change in the plastic strain rate, which two or more orders of magnitude exceeds the change in the creep rate during the usual supramolecular structure reconfiguration. Whether the object will remain functional or acquire damage of the next scale after being subjected to such local "impact" loading depends on the ability of its immediate environment to absorb released energy.

Relationships between sliding behavior and internal geometry of laboratory fault zones and some creeping and locked strike-slip faults of California

USGS Publications Warehouse

Moore, Diane E.; Byerlee, J.

1992-01-01

Moore, D.E. and Byerlee, J., 1992. Relationships between sliding behavior and internal geometry of laboratory fault zones and some creeping and locked strike-slip faults of California. In: T. Mikumo, K. Aki, M. Ohnaka, L.J. Ruff and P.K.P. Spudich (Editors), Earthquake Source Physics and Earthquake Precursors. Tectonophysics, 211: 305-316. In order to relate fault geometries to sliding behavior, maps of recently active breaks within the Hayward fault of central California, which is characterized by fault creep, have been examined and compared to maps of the San Andreas fault. The patterns of recent breaks of the Hayward fault are consistent with those found within the creeping section of the San Andreas, and they appear to have plausible physical explanations in the findings of laboratory experiments. The distinguishing geometric features of the examined locked and creeping faults are: (1) P-type second-order traces predominate over R(Riedel)-type traces in creeping sections; and (2) R-type second-order traces make smaller angles to the local fault strike in creeping sections than they do in locked sections. Two different maps of the Hayward fault gave similar results, supporting the inference that the patterns identified are basic characteristics of the fault rather than artifacts of a particular mapping procedure. P shears predominate over R shears under laboratory conditions that allow dilation within the fault zone. In our own experiments, P-shear development was favored by the generation of excess pore-fluid pressures. We propose that creep in California faults also is the result of fluid overpressures that are maintained in a low-permeability gouge zone and that significantly lower effective stresses, thus helping to stabilize slip and producing high values of the ratio P/R. Small R-trace angles may also be an indicator of low effective stresses, but the evidence for this is not conclusive because other factors can also affect the size of the angles. ?? 1992.

Measuring Aseismic Slip through Characteristically Repeating Earthquakes at the Mendocino Triple Junction, Northern California

NASA Astrophysics Data System (ADS)

Materna, K.; Taira, T.; Burgmann, R.

2016-12-01

The Mendocino Triple Junction (MTJ), at the transition point between the San Andreas fault system, the Mendocino Transform Fault, and the Cascadia Subduction Zone, undergoes rapid tectonic deformation and produces more large (M>6.0) earthquakes than any region in California. Most of the active faults of the triple junction are located offshore, making it difficult to characterize both seismic slip and aseismic creep. In this work, we study aseismic creep rates near the MTJ using characteristically repeating earthquakes (CREs) as indicators of creep rate. CREs are generally interpreted as repeated failures of the same seismic patch within an otherwise creeping fault zone; as a consequence, the magnitude and recurrence time of the CREs can be used to determine a fault's creep rate through empirically calibrated scaling relations. Using seismic data from 2010-2016, we identify CREs as recorded by an array of eight 100-Hz PBO borehole seismometers deployed in the Cape Mendocino area. For each event pair with epicenters less than 30 km apart, we compute the cross-spectral coherence of 20 seconds of data starting one second before the P-wave arrival. We then select pairs with high coherence in an appropriate frequency band, which is determined uniquely for each event pair based on event magnitude, station distance, and signal-to-noise ratio. The most similar events (with median coherence above 0.95 at two or more stations) are selected as CREs and then grouped into CRE families, and each family is used to infer a local creep rate. On the Mendocino Transform Fault, we find relatively high creep rates of >5 cm/year that increase closer to the Gorda Ridge. Closer to shore and to the MTJ itself, we find many families of repeaters on and off the transform fault with highly variable creep rates, indicative of the complex deformation that takes place there.

Modeling Long-term Creep Performance for Welded Nickel-base Superalloy Structures for Power Generation Systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shen, Chen; Gupta, Vipul; Huang, Shenyan

The goal of this project is to model long-term creep performance for nickel-base superalloy weldments in high temperature power generation systems. The project uses physics-based modeling methodologies and algorithms for predicting alloy properties in heterogeneous material structures. The modeling methodology will be demonstrated on a gas turbine combustor liner weldment of Haynes 282 precipitate-strengthened nickel-base superalloy. The major developments are: (1) microstructure-property relationships under creep conditions and microstructure characterization (2) modeling inhomogeneous microstructure in superalloy weld (3) modeling mesoscale plastic deformation in superalloy weld and (4) a constitutive creep model that accounts for weld and base metal microstructure and theirmore » long term evolution. The developed modeling technology is aimed to provide a more efficient and accurate assessment of a material’s long-term performance compared with current testing and extrapolation methods. This modeling technology will also accelerate development and qualification of new materials in advanced power generation systems. This document is a final technical report for the project, covering efforts conducted from October 2014 to December 2016.« less

Tensile and Creep Property Characterization of Potential Brayton Cycle Impeller and Duct Materials

NASA Technical Reports Server (NTRS)

Gabb, Timothy P.; Gayda, John

2006-01-01

This paper represents a status report documenting the work on creep of superalloys performed under Project Prometheus. Cast superalloys have potential applications in space as impellers within closed-loop Brayton cycle nuclear power generation systems. Likewise wrought superalloys are good candidates for ducts and heat exchangers transporting the inert working gas in a Brayton-based power plant. Two cast superalloys, Mar-M247LC and IN792, and a NASA GRC powder metallurgy superalloy, LSHR, are being screened to compare their respective capabilities for impeller applications. Several wrought superalloys including Hastelloy X, (Haynes International, Inc., Kokomo, IN), Inconel 617, Inconel 740, Nimonic 263, and Incoloy MA956 (Special Metals Corporation, Huntington, WV) are also being screened to compare their capabilities for duct applications. These proposed applications would require sufficient strength and creep resistance for long term service at temperatures up to 1200 K, with service times to 100,000 h or more. Conventional tensile and creep tests were performed at temperatures up to 1200 K on specimens extracted from the materials. Initial microstructure evaluations were also undertaken.

Effects of state recovery on creep buckling under variable loading

NASA Technical Reports Server (NTRS)

Robinson, D. N.; Arnold, S. M.

1986-01-01

Structural alloys embody internal mechanisms that allow recovery of state with varying stress and elevated temperature, i.e., they can return to a softer state following periods of hardening. Such material behavior is known to strongly influence structural response under some important thermomechanical loadings, for example, that involving thermal ratchetting. The influence of dynamic and thermal recovery on the creep buckling of a column under variable loading is investigated. The column is taken as the idealized (Shanley) sandwich column. The constitutive model, unlike the commonly employed Norton creep model, incorporates a representation of both dynamic and thermal (state) recovery. The material parameters of the constitutive model are chosen to characterize Narloy Z, a representative copper alloy used in thrust nozzle liners of reusable rocket engines. Variable loading histories include rapid cyclic unloading/reloading sequences and intermittent reductions of load for extended periods of time; these are superimposed on a constant load. The calculated results show that state recovery significantly affects creep buckling under variable loading. Structural alloys embody internal mechanisms that allow recovery of state with varying stress and time.

A damage mechanics based approach to structural deterioration and reliability

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bhattcharya, B.; Ellingwood, B.

1998-02-01

Structural deterioration often occurs without perceptible manifestation. Continuum damage mechanics defines structural damage in terms of the material microstructure, and relates the damage variable to the macroscopic strength or stiffness of the structure. This enables one to predict the state of damage prior to the initiation of a macroscopic flaw, and allows one to estimate residual strength/service life of an existing structure. The accumulation of damage is a dissipative process that is governed by the laws of thermodynamics. Partial differential equations for damage growth in terms of the Helmholtz free energy are derived from fundamental thermodynamical conditions. Closed-form solutions tomore » the equations are obtained under uniaxial loading for ductile deformation damage as a function of plastic strain, for creep damage as a function of time, and for fatigue damage as function of number of cycles. The proposed damage growth model is extended into the stochastic domain by considering fluctuations in the free energy, and closed-form solutions of the resulting stochastic differential equation are obtained in each of the three cases mentioned above. A reliability analysis of a ring-stiffened cylindrical steel shell subjected to corrosion, accidental pressure, and temperature is performed.« less

Time dependency of strainrange partitioning life relationships

NASA Technical Reports Server (NTRS)

Kalluri, S.; Manson, S. S.

1984-01-01

The effect of exposure time (or creep rate) on the CP life relationship is established by conducting isothermal CP tests at varying exposure times on 316 Ss at 1300 and 1500 F. A reduction in the CP cycle life is observed with an increase in the exposure time of the CP test at a given inelastic strain-range. This phenomenon is characterized by modifying the Manson-Coffin type of CP relationship. Two new life relationships: (1) the Steady State Creep Rate (SSRC) Modified CP life relationship, and (2) the Failure Time (FT) Modified CP life relationship, are developed in this report. They account for the effect of creep rate and exposure time within the CP type of waveform. The reduction in CP cyclic life in the long exposure time tests is attributed to oxidation and the precipitation of carbides along the grain boundaries.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Oleinikov, A. I., E-mail: a.i.oleinikov@mail.ru; Bormotin, K. S., E-mail: cvmi@knastu.ru

It is shown that inverse problems of steady-state creep bending of plates in both the geometrically linear and nonlinear formulations can be represented in a variational formulation. Steady-state values of the obtained functionals corresponding to the solutions of the problems of inelastic deformation and springback are determined by applying a finite element procedure to the functionals. Optimal laws of creep deformation are formulated using the criterion of minimizing damage in the functionals of the inverse problems. The formulated problems are reduced to the problems solved by the finite element method using MSC.Marc software. Currently, forming of light metals poses tremendousmore » challenges due to their low ductility at room temperature and their unusual deformation characteristics at hot-cold work: strong asymmetry between tensile and compressive behavior, and a very pronounced anisotropy. We used the constitutive models of steady-state creep of initially transverse isotropy structural materials the kind of the stress state has influence. The paper gives basics of the developed computer-aided system of design, modeling, and electronic simulation targeting the processes of manufacture of wing integral panels. The modeling results can be used to calculate the die tooling, determine the panel processibility, and control panel rejection in the course of forming.« less

Monitoring the mechanical behaviour of electrically conductive polymer nanocomposites under ramp and creep conditions.

PubMed

Pedrazzoli, D; Dorigato, A; Pegoretti, A

2012-05-01

Various amounts of carbon black (CB) and carbon nanofibres (CNF) were dispersed in an epoxy resin to prepare nanocomposites whose mechanical behaviour, under ramp and creep conditions, was monitored by electrical measurements. The electrical resistivity of the epoxy resin was dramatically reduced by both nanofillers after the percolation threshold (1 wt% for CB and 0.5 wt% for CNF), reaching values in the range of 10(3)-10(4) omega . cm for filler loadings higher than 2 wt%. Due to the synergistic effects between the nanofillers, an epoxy system containing a total nanofiller amount of 2 wt%, with a relative CB/CNF ratio of 90/10 was selected for the specific applications. A direct correlation between the tensile strain and the increase of the electrical resistance was observed over the whole experimental range, and also the final failure of the samples was clearly detected. Creep tests confirmed the possibility to monitor the various deformational stages under constant loads, with a strong dependency from the temperature and the applied stress. The obtained results are encouraging for a possible application of nanomodified epoxy resin as a matrix for the preparation of structural composites with sensing (i.e., damage-monitoring) capabilities.

Very High Cycle Fatigue of Ni-Based Single-Crystal Superalloys at High Temperature

NASA Astrophysics Data System (ADS)

Cervellon, A.; Cormier, J.; Mauget, F.; Hervier, Z.; Nadot, Y.

2018-05-01

Very high cycle fatigue (VHCF) properties at high temperature of Ni-based single-crystal (SX) superalloys and of a directionally solidified (DS) superalloy have been investigated at 20 kHz and a temperature of 1000 °C. Under fully reversed conditions (R = - 1), no noticeable difference in VHCF lifetimes between all investigated alloys has been observed. Internal casting pores size is the main VHCF lifetime-controlling factor whatever the chemical composition of the alloys. Other types of microstructural defects (eutectics, carbides), if present, may act as stress concentration sites when the number of cycles exceed 109 cycles or when porosity is absent by applying a prior hot isostatic pressing treatment. For longer tests (> 30 hours), oxidation also controls the main crack initiation sites leading to a mode I crack initiation from oxidized layer. Under such conditions, alloy's resistance to oxidation has a prominent role in controlling the VHCF. When creep damage is present at high ratios (R ≥ 0.8), creep resistance of SX/DS alloys governs VHCF lifetime. Under such high mean stress conditions, SX alloys developed to retard the initiation and creep propagation of mode I micro-cracks from pores have better VHCF lifetimes.

Modelling and analysis of creep deformation and fracture in a 1 Cr 1/2 Mo ferritic steel

NASA Astrophysics Data System (ADS)

Dyson, B. F.; Osgerby, D.

A quantitative model, based upon a proposed new mechanism of creep deformation in particle-hardened alloys, has been validated by analysis of creep data from a 13CrMo 4 4 (1Cr 1/2 Mo) material tested under a range of stresses and temperatures. The methodology that has been used to extract the model parameters quantifies, as a first approximation, only the main degradation (damage) processes - in the case of the 1CR 1/2 Mo steel, these are considered to be the parallel operation of particle-coarsening and a progressively increasing stress due to a constant-load boundary condition. These 'global' model parameters can then be modified (only slightly) as required to obtain a detailed description and 'fit' to the rupture lifetime and strain/time trajectory of any individual test. The global model parameter approach may be thought of as predicting average behavior and the detailed fits as taking account of uncertainties (scatter) due to variability in the material. Using the global parameter dataset, predictions have also been made of behavior under biaxial stressing; constant straining rate; constant total strain (stress relaxation) and the likely success or otherwise of metallographic and mechanical remanent lifetime procedures.

The inverse problems of wing panel manufacture processes

NASA Astrophysics Data System (ADS)

Oleinikov, A. I.; Bormotin, K. S.

2013-12-01

It is shown that inverse problems of steady-state creep bending of plates in both the geometrically linear and nonlinear formulations can be represented in a variational formulation. Steady-state values of the obtained functionals corresponding to the solutions of the problems of inelastic deformation and springback are determined by applying a finite element procedure to the functionals. Optimal laws of creep deformation are formulated using the criterion of minimizing damage in the functionals of the inverse problems. The formulated problems are reduced to the problems solved by the finite element method using MSC.Marc software. Currently, forming of light metals poses tremendous challenges due to their low ductility at room temperature and their unusual deformation characteristics at hot-cold work: strong asymmetry between tensile and compressive behavior, and a very pronounced anisotropy. We used the constitutive models of steady-state creep of initially transverse isotropy structural materials the kind of the stress state has influence. The paper gives basics of the developed computer-aided system of design, modeling, and electronic simulation targeting the processes of manufacture of wing integral panels. The modeling results can be used to calculate the die tooling, determine the panel processibility, and control panel rejection in the course of forming.

Development of GENOA Progressive Failure Parallel Processing Software Systems

NASA Technical Reports Server (NTRS)

Abdi, Frank; Minnetyan, Levon

1999-01-01

A capability consisting of software development and experimental techniques has been developed and is described. The capability is integrated into GENOA-PFA to model polymer matrix composite (PMC) structures. The capability considers the physics and mechanics of composite materials and structure by integration of a hierarchical multilevel macro-scale (lamina, laminate, and structure) and micro scale (fiber, matrix, and interface) simulation analyses. The modeling involves (1) ply layering methodology utilizing FEM elements with through-the-thickness representation, (2) simulation of effects of material defects and conditions (e.g., voids, fiber waviness, and residual stress) on global static and cyclic fatigue strengths, (3) including material nonlinearities (by updating properties periodically) and geometrical nonlinearities (by Lagrangian updating), (4) simulating crack initiation. and growth to failure under static, cyclic, creep, and impact loads. (5) progressive fracture analysis to determine durability and damage tolerance. (6) identifying the percent contribution of various possible composite failure modes involved in critical damage events. and (7) determining sensitivities of failure modes to design parameters (e.g., fiber volume fraction, ply thickness, fiber orientation. and adhesive-bond thickness). GENOA-PFA progressive failure analysis is now ready for use to investigate the effects on structural responses to PMC material degradation from damage induced by static, cyclic (fatigue). creep, and impact loading in 2D/3D PMC structures subjected to hygrothermal environments. Its use will significantly facilitate targeting design parameter changes that will be most effective in reducing the probability of a given failure mode occurring.

Life prediction technologies for aeronautical propulsion systems

NASA Technical Reports Server (NTRS)

Mcgaw, Michael A.

1990-01-01

Fatigue and fracture problems continue to occur in aeronautical gas turbine engines. Components whose useful life is limited by these failure modes include turbine hot-section blades, vanes, and disks. Safety considerations dictate that catastrophic failures be avoided, while economic considerations dictate that catastrophic failures be avoided, while economic considerations dictate that noncatastrophic failures occur as infrequently as possible. Therefore, the decision in design is making the tradeoff between engine performance and durability. LeRC has contributed to the aeropropulsion industry in the area of life prediction technology for over 30 years, developing creep and fatigue life prediction methodologies for hot-section materials. At the present time, emphasis is being placed on the development of methods capable of handling both thermal and mechanical fatigue under severe environments. Recent accomplishments include the development of more accurate creep-fatigue life prediction methods such as the total strain version of LeRC's strain-range partitioning (SRP) and the HOST-developed cyclic damage accumulation (CDA) model. Other examples include the development of a more accurate cumulative fatigue damage rule - the double damage curve approach (DDCA), which provides greatly improved accuracy in comparison with usual cumulative fatigue design rules. Other accomplishments in the area of high-temperature fatigue crack growth may also be mentioned. Finally, we are looking to the future and are beginning to do research on the advanced methods which will be required for development of advanced materials and propulsion systems over the next 10-20 years.

Coda Wave Interferometry Method Applied in Structural Monitoring to Assess Damage Evolution in Masonry and Concrete Structures

NASA Astrophysics Data System (ADS)

Masera, D.; Bocca, P.; Grazzini, A.

2011-07-01

In this experimental program the main goal is to monitor the damage evolution in masonry and concrete structures by Acoustic Emission (AE) signal analysis applying a well-know seismic method. For this reason the concept of the coda wave interferometry is applied to AE signal recorded during the tests. Acoustic Emission (AE) are very effective non-destructive techniques applied to identify micro and macro-defects and their temporal evolution in several materials. This technique permits to estimate the velocity of ultrasound waves propagation and the amount of energy released during fracture propagation to obtain information on the criticality of the ongoing process. By means of AE monitoring, an experimental analysis on a set of reinforced masonry walls under variable amplitude loading and strengthening reinforced concrete (RC) beams under monotonic static load has been carried out. In the reinforced masonry wall, cyclic fatigue stress has been applied to accelerate the static creep and to forecast the corresponding creep behaviour of masonry under static long-time loading. During the tests, the evaluation of fracture growth is monitored by coda wave interferometry which represents a novel approach in structural monitoring based on AE relative change velocity of coda signal. In general, the sensitivity of coda waves has been used to estimate velocity changes in fault zones, in volcanoes, in a mining environment, and in ultrasound experiments. This method uses multiple scattered waves, which travelled through the material along numerous paths, to infer tiny temporal changes in the wave velocity. The applied method has the potential to be used as a "damage-gauge" for monitoring velocity changes as a sign of damage evolution into masonry and concrete structures.

Structural integrity of materials in nuclear service: a bibliography

DOE Office of Scientific and Technical Information (OSTI.GOV)

Heddleson, F.A.

This report contains 679 abstracts from the Nuclear Safety Information Center (NSIC) computer file dated 1973 through 1976 covering material properties with respect to structural integrity. All materials important to the nuclear industry (except concrete) are covered for mechanical properties, chemical properties, corrosion, fracture or failure, radiation damage, creep, cracking, and swelling. Keyword, author, and permuted-title indexes are included for the convenience of the user.

Exposure damage mechanisms for KCl windows in high power laser systems

NASA Technical Reports Server (NTRS)

Blaszuk, P. R.; Woody, B. A.; Hulse, C. O.; Davis, J. W.; Waters, J. P.

1976-01-01

An experimental study of the 10.6 micrometer and 0.6328 micrometer optical properties of single crystal and europium doped polycrystal is described. Significant variations in the optical properties are observed over periods of exposure up to 100 hours. Models are proposed to predict the 10.6 micrometer absorptivity for long exposure periods. Mechanical creep has been detected in both materials at high temperature.

In situ X-ray micro-CT characterization of chemo-mechanical relaxations during Sn lithiation

NASA Astrophysics Data System (ADS)

Gonzalez, Joseph F.; Antartis, Dimitrios A.; Chasiotis, Ioannis; Dillon, Shen J.; Lambros, John

2018-03-01

Sn has been proposed for use as a high capacity anode material. Because of its ductile metallic nature, Sn may exhibit unique stress evolution during lithiation. Here, 2D radiography and 3D tomography are employed to visualize the evolution of geometry, internal structure, alloying, and damage during lithiation, delithiation, and rest of Sn wires with micron scale diameters. Lithiation proceeds isotropically, resulting in geometric and dimensional changes after 25% of total lithiation when the tensile stresses are sufficiently high to exceed the flow stress of the unlithiated Sn core and cause elongation and diameter increase. Damage occurs at later stages in the form of cracks terminating at the wire surface and voids forming in the unlithiated core. Notably, significant fragmentation occurs during delithiation which, due to void formation that accommodates the resulting stresses, does not measurably alter the wire cross-section and length. The distinguishing feature of the chemo-mechanics of Sn compared to Si or Ge is the pronounced creep rate at applied strain rates as high as 10-6 s-1, which promotes large strains in the core, eventually leading to void nucleation in the unlithiated core during lithiation, and more importantly, continues driving the deformation of the anode while at rest.

Performance characterizations of asphalt binders and mixtures incorporating silane additive ZycoTherm

NASA Astrophysics Data System (ADS)

Hasan, Mohd Rosli Mohd; Hamzah, Meor Othman; Yee, Teh Sek

2017-10-01

Experimental works were conducted to evaluate the properties of asphalt binders and mixtures produced using a relatively new silane additive, named ZycoTherm. In this study, 0.1wt% ZycoTherm was blended with asphalt binder to enable production of asphalt mixture at lower than normal temperatures, as well as improve mix workability and compactability. Asphalt mixture performances towards pavement distresses in tropical climate region were also investigated. The properties of control asphalt binders (60/70 and 80/10 penetration grade) and asphalt binders incorporating 0.1% ZycoTherm were reported based on the penetration, softening point, rotational viscosity, complex modulus and phase angle. Subsequently, to compare the performance of asphalt mixture incorporating ZycoTherm with the control asphalt mixture, cylindrical samples were prepared at recommended temperatures and air voids depending on the binder types and test requirements. The samples were tested for indirect tensile strength (ITS), resilient modulus, dynamic creep, Hamburg wheel tracking and moisture induced damage. From compaction data using the Servopak gyratory compactor, specimen prepared using ZycoTherm exhibit higher workability and compactability compared to the conventional mixture. From the mixture performance test results, mixtures prepared with ZycoTherm showed comparable if not better performance than the control sample in terms of the resistance to moisture damage, permanent deformation and cracking.

Effet de la poudre de verre sur le fluage du C-S-H

NASA Astrophysics Data System (ADS)

Danilova, Maryna

Glass is a unique inert material that could be recycled many times without changing its physical and chemical properties. Nevertheless, for some reason, large quantities of glass are still not recycled and therefore are stored as a waste. Its alternative recycling has become, since long, a major environmental problem. Moreover, glass is a potentially useful material for the development of ecological concrete, consequently, this way valorization seems to be imminent. In this research, characterization of the creep of concrete incorporating waste glass in powder form, i.e. glass powder (GP) as a supplementary cementitious material (GP-concrete) was carried out at a macro- and nanolevels. First, results from experimental study on the under load behaviour of GP-concrete are presented. Different types of strain occurring under load or after unload were discussed: quasi-instantaneous deformation, total mechanical deformation due to the maintained uniaxial compressive load during 1 year, total creep, basic creep, elastic recovery and total recovery. Shrinkage under drying conditions and endogenous shrinkage were also studied. After 1 year creep, the effects of constant load and drying on residual strength were also examined. A comparison was made concerning the final state of the porosity. Afterwards, the thesis reveals the results of tests conducted on the cement paste, going down to its composition and properties of the hydrated phases, in particular of calcium silicate hydrates (C-S-H). All of this, in order to conclude on the harmlessness use of GP regarding to the creep. Keywords : Glass powder, Air-entrained concrete, Creep, Shrinkage, C-S-H, Nanoindentation

Microstructural Evolution and Creep-Rupture Behavior of A-USC Alloy Fusion Welds

NASA Astrophysics Data System (ADS)

Bechetti, Daniel H.; DuPont, John N.; Siefert, John A.; Shingledecker, John P.

2016-09-01

Characterization of the microstructural evolution of fusion welds in alloys slated for use in advanced ultrasupercritical (A-USC) boilers during creep has been performed. Creep-rupture specimens involving INCONEL® 740, NIMONIC® 263 (INCONEL and NIMONIC are registered trademarks of Special Metals Corporation), and Haynes® 282® (Haynes and 282 are registered trademarks of Haynes International) have been analyzed via light optical microscopy, scanning electron microscopy, X-ray diffraction, and thermodynamic and kinetic modeling. Focus has been given to the microstructures that develop along the grain boundaries in these alloys during creep at temperatures relevant to the A-USC process cycle, and particular attention has been paid to any evidence of the formation of local γ'-denuded or γ'-free zones. This work has been performed in an effort to understand the microstructural changes that lead to a weld strength reduction factor (WSRF) in these alloys as compared to solution annealed and aged alloy 740 base metal. γ' precipitate-free zones have been identified in alloy 740 base metal, solution annealed alloy 740 weld metal, and alloy 263 weld metal after creep. Their development during long-term thermal exposure is correlated with the stabilization of phases that are rich in γ'-forming elements ( e.g., η and G) and is suppressed by precipitation of phases that do not contain the γ' formers ( e.g., M23C6 and μ). The location of failure and creep performance in terms of rupture life and WSRF for each welded joint is presented and discussed.

Retardations in fault creep rates before local moderate earthquakes along the San Andreas fault system, central California

USGS Publications Warehouse

Burford, R.O.

1988-01-01

Records of shallow aseismic slip (fault creep) obtained along parts of the San Andreas and Calaveras faults in central California demonstrate that significant changes in creep rates often have been associated with local moderate earthquakes. An immediate postearthquake increase followed by gradual, long-term decay back to a previous background rate is generally the most obvious earthquake effect on fault creep. This phenomenon, identified as aseismic afterslip, usually is characterized by above-average creep rates for several months to a few years. In several cases, minor step-like movements, called coseismic slip events, have occurred at or near the times of mainshocks. One extreme case of coseismic slip, recorded at Cienega Winery on the San Andreas fault 17.5 km southeast of San Juan Bautista, consisted of 11 mm of sudden displacement coincident with earthquakes of ML=5.3 and ML=5.2 that occurred 2.5 minutes apart on 9 April 1961. At least one of these shocks originated on the main fault beneath the winery. Creep activity subsequently stopped at the winery for 19 months, then gradually returned to a nearly steady rate slightly below the previous long-term average. The phenomena mentioned above can be explained in terms of simple models consisting of relatively weak material along shallow reaches of the fault responding to changes in load imposed by sudden slip within the underlying seismogenic zone. In addition to coseismic slip and afterslip phenomena, however, pre-earthquake retardations in creep rates also have been observed. Onsets of significant, persistent decreases in creep rates have occurred at several sites 12 months or more before the times of moderate earthquakes. A 44-month retardation before the 1979 ML=5.9 Coyote Lake earthquake on the Calaveras fault was recorded at the Shore Road creepmeter site 10 km northwest of Hollister. Creep retardation on the San Andreas fault near San Juan Bautista has been evident in records from one creepmeter site for the past 5 years. Retardations with durations of 21 and 19 months also occurred at Shore Road before the 1974 and 1984 earthquakes of ML=5.2 and ML=6.2, respectively. Although creep retardation remains poorly understood, several possible explanations have been discussed previously. (1) Certain onsets of apparent creep retardation may be explained as abrupt terminations of afterslip generated from previous moderate-mainshock sequences. (2) Retardations may be related to significant decreases in the rate of seismic and/or aseismic slip occurring within or beneath the underlying seismogenic zone. Such decreases may be caused by changes in local conditions related to growth of asperities, strain hardening, or dilatancy, or perhaps by passage of stress-waves or other fluctuations in driving stresses. (3) Finally, creep rates may be lowered (or increased) by stresses imposed on the fault by seismic or aseismic slip on neighboring faults. In addition to causing creep-rate increases or retardations, such fault interactions occasionally may trigger earthquakes. Regardless of the actual mechanisms involved and the current lack of understanding of creep retardation, it appears that shallow fault creep is sensitive to local and regional effects that promote or accompany intermediate-term preparation stages leading to moderate earthquakes. A strategy for more complete monitoring of fault creep, wherever it is known to occur, therefore should be assigned a higher priority in our continuing efforts to test various hypotheses concerning the mechanical relations between seismic and aseismic slip. ?? 1988 Birkha??user Verlag.

Retardations in fault creep rates before local moderate earthquakes along the San Andreas fault system, central California

NASA Astrophysics Data System (ADS)

Burford, Robert O.

1988-06-01

Records of shallow aseismic slip (fault creep) obtained along parts of the San Andreas and Calaveras faults in central California demonstrate that significant changes in creep rates often have been associated with local moderate earthquakes. An immediate postearthquake increase followed by gradual, long-term decay back to a previous background rate is generally the most obvious earthquake effect on fault creep. This phenomenon, identified as aseismic afterslip, usually is characterized by above-average creep rates for several months to a few years. In several cases, minor step-like movements, called coseismic slip events, have occurred at or near the times of mainshocks. One extreme case of coseismic slip, recorded at Cienega Winery on the San Andreas fault 17.5 km southeast of San Juan Bautista, consisted of 11 mm of sudden displacement coincident with earthquakes of M L =5.3 and M L =5.2 that occurred 2.5 minutes apart on 9 April 1961. At least one of these shocks originated on the main fault beneath the winery. Creep activity subsequently stopped at the winery for 19 months, then gradually returned to a nearly steady rate slightly below the previous long-term average. The phenomena mentioned above can be explained in terms of simple models consisting of relatively weak material along shallow reaches of the fault responding to changes in load imposed by sudden slip within the underlying seismogenic zone. In addition to coseismic slip and afterslip phenomena, however, pre-earthquake retardations in creep rates also have been observed. Onsets of significant, persistent decreases in creep rates have occurred at several sites 12 months or more before the times of moderate earthquakes. A 44-month retardation before the 1979 M L =5.9 Coyote Lake earthquake on the Calaveras fault was recorded at the Shore Road creepmeter site 10 km northwest of Hollister. Creep retardation on the San Andreas fault near San Juan Bautista has been evident in records from one creepmeter site for the past 5 years. Retardations with durations of 21 and 19 months also occurred at Shore Road before the 1974 and 1984 earthquakes of M L =5.2 and M L =6.2, respectively. Although creep retardation remains poorly understood, several possible explanations have been discussed previously. (1) Certain onsets of apparent creep retardation may be explained as abrupt terminations of afterslip generated from previous moderate-mainshock sequences. (2) Retardations may be related to significant decreases in the rate of seismic and/or aseismic slip occurring within or beneath the underlying seismogenic zone. Such decreases may be caused by changes in local conditions related to growth of asperities, strain hardening, or dilatancy, or perhaps by passage of stress-waves or other fluctuations in driving stresses. (3) Finally, creep rates may be lowered (or increased) by stresses imposed on the fault by seismic or aseismic slip on neighboring faults. In addition to causing creep-rate increases or retardations, such fault interactions occasionally may trigger earthquakes. Regardless of the actual mechanisms involved and the current lack of understanding of creep retardation, it appears that shallow fault creep is sensitive to local and regional effects that promote or accompany intermediate-term preparation stages leading to moderate earthquakes. A strategy for more complete monitoring of fault creep, wherever it is known to occur, therefore should be assigned a higher priority in our continuing efforts to test various hypotheses concerning the mechanical relations between seismic and aseismic slip.

Heterogeneous Creep Deformations and Correlation to Microstructures in Fe-30Cr-3Al Alloys Strengthened by an Fe 2Nb Laves Phase

DOE PAGES

Shassere, Benjamin; Yamamoto, Yukinori; Poplawsky, Jonathan; ...

2017-08-07

We have develooped a new Fe-Cr-Al (FCA) alloy system with good oxidation resistance and creep strength at high temperature. The alloy system is a candidate for use in future fossil-fueled power plants. The creep strength of these alloys at 973 K (700 °C) was found to be comparable with traditional 9 pct Cr ferritic–martensitic steels. A few FCA alloys with general composition of Fe-30Cr-3Al-.2Si-xNb (x = 0, 1, or 2) with a ferrite matrix and Fe 2Nb-type Laves precipitates were prepared. The detailed microstructural characterization of samples, before and after creep rupture testing, indicated precipitation of the Laves phase withinmore » the matrix, Laves phase at the grain boundaries, and a 0.5 to 1.5 μm wide precipitate-free zone (PFZ) parallel to all the grain boundaries. In these alloys, the areal fraction of grain boundary Laves phase and the width of the PFZ controlled the cavitation nucleation and eventual grain boundary ductile failure. Finally, we used a phenomenological model to compare the creep strain rates controlled by the effects of the particles on the dislocations within the grain and at grain boundaries. (The research sponsored by US-DOE, Office of Fossil Energy, the Crosscutting Research Program).« less

Microstructural Evolution and Creep-Rupture Behavior of Fusion Welds Involving Alloys for Advanced Ultrasupercritical Power Generation

NASA Astrophysics Data System (ADS)

Bechetti, Daniel H., Jr.

Projections for large increases in the global demand for electric power produced by the burning of fossil fuels, in combination with growing environmental concerns surrounding these fuel sources, have sparked initiatives in the United States, Europe, and Asia aimed at developing a new generation of coal fired power plant, termed Advanced Ultrasupercritical (A-USC). These plants are slated to operate at higher steam temperatures and pressures than current generation plants, and in so doing will offer increased process cycle efficiency and reduced greenhouse gas emissions. Several gamma' precipitation strengthened Ni-based superalloys have been identified as candidates for the hottest sections of these plants, but the microstructural instability and poor creep behavior (compared to wrought products) of fusion welds involving these alloys present significant hurdles to their implementation and a gap in knowledge that must be addressed. In this work, creep testing and in-depth microstructural characterization have been used to provide insight into the long-term performance of these alloys. First, an investigation of the weld metal microstructural evolution as it relates to creep strength reductions in A-USC alloys INCONELRTM 740, NIMONICRTM 263 (INCONEL and NIMONIC are registered trademarks of Special Metals Corporation), and HaynesRTM 282RTM (Haynes and 282 are registered trademarks of Haynes International) was performed. gamma'-precipitate free zones were identified in two of these three alloys, and their development was linked to the evolution of phases that precipitate at the expense of gamma'. Alloy 282 was shown to avoid precipitate free zone formation because the precipitates that form during long term aging in this alloy are poor in the gamma'-forming elements. Next, the microstructural evolution of INCONELRTM 740H (a compositional variant of alloy 740) during creep was investigated. Gleeble-based interrupted creep and creep-rupture testing was used to determine the correlation of discontinuous coarsening of the gamma' phase with time at temperature, creep strain, plastic prestrain, post-weld heat treatment, and compositional modification. The discontinuous coarsening reaction was shown to depend most strongly on the total strain experienced during creep. Post-weld homogenization and compositional modification had mixed effects on fusion weld rupture life and the rate of discontinuous coarsening. The differences in rupture life and discontinuous coarsening across a large matrix of creep specimens were related to the differences in strain at rupture and the relative ease of grain boundary motion in the samples. Finally, in-depth characterization of the discontinuous coarsening reaction products in alloy 740H creep specimens was performed. The effects of solute partitioning during non-equilibrium solidification on the variation in the volume fraction of strengthening precipitates along the length of the grain boundaries has been linked to the propensity for discontinuous coarsening. Evidence for the preferential development of discontinuous coarsening along grain boundary segments with sharp variations in gamma' content was presented. In addition, evidence for the preferred growth of colonies of discontinuous coarsening into regions of lower gamma' content was documented. Scanning transmission electron microscopy determined the compositions of the matrix and precipitate phases within the colonies and quantified the segregation of alloying elements to the reaction front. Thermodynamic and kinetic modeling using commercially available software packages were leaned on extensively throughout this research, both as a way to provide theoretical bases for experimental observations and as a way to design and guide experimentation. Overall, the results presented in this work offer detailed observations on the evolution of deleterious grain boundary features in A-USC alloy fusion welds and provide insight for changes that may improve their creep performance.

Application of interface waves for near surface damage detection in hybrid structures

NASA Astrophysics Data System (ADS)

Jahanbin, M.; Santhanam, S.; Ihn, J.-B.; Cox, A.

2017-04-01

Guided waves are acoustic waves that are guided by boundaries. Depending on the structural geometry, guided waves can either propagate between boundaries, known as plate waves, or propagate on the surface of the objects. Many different types of surface waves exist based on the material property of the boundary. For example Rayleigh wave in solid - air, Scholte wave in solid - liquid, Stoneley in solid - solid interface and many other different forms like Love wave on inhomogeneous surfaces, creeping waves, etc. This research work is demonstrating the application of surface and interface waves for detection of interfacial damages in hybrid bonded structures.

Accelerated Near-Threshold Fatigue Crack Growth Behavior of an Aluminum Powder Metallurgy Alloy

NASA Technical Reports Server (NTRS)

Piascik, Robert S.; Newman, John A.

2002-01-01

Fatigue crack growth (FCG) research conducted in the near threshold regime has identified a room temperature creep crack growth damage mechanism for a fine grain powder metallurgy (PM) aluminum alloy (8009). At very low DK, an abrupt acceleration in room temperature FCG rate occurs at high stress ratio (R = Kmin/Kmax). The near threshold accelerated FCG rates are exacerbated by increased levels of Kmax (Kmax less than 0.4 KIC). Detailed fractographic analysis correlates accelerated FCG with the formation of crack-tip process zone micro-void damage. Experimental results show that the near threshold and Kmax influenced accelerated crack growth is time and temperature dependent.

Monitoring the Deformation of High-Rise Buildings in Shanghai Luijiazui Zone by Tomo-Psinsar

NASA Astrophysics Data System (ADS)

Zhou, L. F.; Ma, P. F.; Xia, Y.; Xie, C. H.

2018-05-01

In this study, we utilize a Tomography-based Persistent Scatterers Interferometry (Tomo-PSInSAR) approach for monitoring the deformation performances of high-rise buildings, i.e. SWFC and Jin Mao Tower, in Shanghai Lujiazui Zone. For the purpose of this study, we use 31 Stripmap acquisitions from TerraSAR-X missions, spanning from December 2009 to February 2013. Considering thermal expansion, creep and shrinkage are two long-term movements that occur in high-rise buildings with concrete structures, we use an extended 4-D SAR phase model, and three parameters (height, deformation velocity, and thermal amplitude) are estimated simultaneously. Moreover, we apply a two-tier network strategy to detect single and double PSs with no need for preliminary removal of the atmospheric phase screen (APS) in the study area, avoiding possible error caused by the uncertainty in spatiotemporal filtering. Thermal expansion is illustrated in the thermal amplitude map, and deformation due to creep and shrinkage is revealed in the linear deformation velocity map. The thermal amplitude map demonstrates that the derived thermal amplitude of the two high-rise buildings both dilate and contract periodically, which is highly related to the building height due to the upward accumulative effect of thermal expansion. The linear deformation velocity map reveals that SWFC is subject to deformation during the new built period due to creep and shrinkage, which is height-dependent movements in the linear velocity map. It is worth mention that creep and shrinkage induces movements that increase with the increasing height in the downward direction. In addition, the deformation rates caused by creep and shrinkage are largest at the beginning and gradually decrease, and at last achieve a steady state as time goes infinity. On the contrary, the linear deformation velocity map shows that Jin Mao Tower is almost stable, and the reason is that it is an old built building, which is not influenced by creep and shrinkage as the load is relaxed and dehydration proceeds. This study underlines the potential of the Tomo-PSInSAR solution for the monitoring deformation performance of high-rise buildings, which offers a quantitative indicator to local authorities and planners for assessing potential damages.

Durability of a continuous strand mat polymeric composite for automotive structural applications

DOE Office of Scientific and Technical Information (OSTI.GOV)

Corum, J.M.; McCoy, H.E. Jr.; Ruggles, M.B.

1995-12-31

A key unanswered question that must be addressed before polymeric composites will be widely used in automotive structural components is their durability. Major durability issues are the effects of cyclic loadings, creep, automotive environments, and low-energy impacts on dimensional stability, strength, and stiffness. The U.S. Department of Energy is sponsoring a project at Oak Ridge National Laboratory to address these issues and to develop, in cooperation with the Automotive Composites Consortium, experimentally based, durability driven, design guidelines. The initial reference material is an isocyanurate reinforced with a continuous strand, swirl glass mat. This paper describes the basic deformation and failuremore » behavior of the reference material, and it presents test results illustrating the property degradations caused by loading, time, and environmental effects. The importance of characterizing and understanding damage and how it leads to failure is also discussed. The results presented are from the initial phases of an ongoing project. The ongoing effort and plans are briefly described.« less

Estimation of local stresses and elastic properties of a mortar sample by FFT computation of fields on a 3D image

DOE Office of Scientific and Technical Information (OSTI.GOV)

Escoda, J.; Departement Materiaux et Mecanique des Composants, Electricite de France, Moret-sur-Loing; Willot, F., E-mail: francois.willot@ensmp.f

2011-05-15

This study concerns the prediction of the elastic properties of a 3D mortar image, obtained by micro-tomography, using a combined image segmentation and numerical homogenization approach. The microstructure is obtained by segmentation of the 3D image into aggregates, voids and cement paste. Full-fields computations of the elastic response of mortar are undertaken using the Fast Fourier Transform method. Emphasis is made on highly-contrasted properties between aggregates and matrix, to anticipate needs for creep or damage computation. The representative volume element, i.e. the volume size necessary to compute the effective properties with a prescribed accuracy, is given. Overall, the volumes usedmore » in this work were sufficient to estimate the effective response of mortar with a precision of 5%, 6% and 10% for contrast ratios of 100, 1000 and 10,000, resp. Finally, a statistical and local characterization of the component of the stress field parallel to the applied loading is carried out.« less

Alloy and structural optimization of a directionally solidified lamellar eutectic alloy

NASA Technical Reports Server (NTRS)

Sheffler, K. D.

1976-01-01

Mechanical property characterization tests of a directionally solidified Ni-20 percent Cb-2.5 percent Al-6 percent Cr cellular eutectic turbine blade alloy demonstrated excellent long time creep stability and indicated intermediate temperature transverse tensile ductility and shear strength to be somewhat low for turbine blade applications. Alloy and structural optimization significantly improves these off-axis properties with no loss of longitudinal creep strength or stability. The optimized alloy-structure combination is a carbon modified Ni-20.1 percent Cb-2.5 percent Al-6.0 percent Cr-0.06 percent C composition processed under conditions producing plane front solidification and a fully-lamellar microstructure. With current processing technology, this alloy exhibits a creep-rupture advantage of 39 C over the best available nickel base superalloy, directionally solidified MAR M200+ Hf. While improved by about 20 percent, shear strength of the optimized alloy remains well below typical superalloy values.

Application of neutron diffraction in characterization of texture evolution during high-temperature creep in magnesium alloys

DOE Office of Scientific and Technical Information (OSTI.GOV)

Vogel, Sven C; Sediako, Dimitry; Shook, S

2010-01-01

A good combination of room-temperature and elevated temperature strength and ductility, good salt-spray corrosion resistance and exceUent diecastability are frequently among the main considerations in development of a new alloy. Unfortunately, there has been much lesser effort in development of wrought-stock alloys for high temperature applications. Extrudability and high temperature performance of wrought material becomes an important factor in an effort to develop new wrought alloys and processing technologies. This paper shows some results received in creep testing and studies of in-creep texture evolution for several wrought magnesium alloys developed for use in elevated-temperature applications. These studies were performed usingmore » E3 neutron spectrometer of the Canadian Neutron Beam Centre in Chalk River, ON, and HIPPO time-of-flight (TOF) spectrometer at Los Alamos Neutron Science Center, NM.« less

Thermal Fatigue and Fracture Behavior of Ceramic Thermal Barrier Coatings

NASA Technical Reports Server (NTRS)

Zhu, Dong-Ming; Choi, Sung R.; Miller, Robert A.

2001-01-01

Thermal fatigue and fracture behavior of plasma-sprayed ceramic thermal barrier coatings has been investigated under high heat flux and thermal cyclic conditions. The coating crack propagation is studied under laser heat flux cyclic thermal loading, and is correlated with dynamic fatigue and strength test results. The coating stress response and inelasticity, fatigue and creep interactions, and interface damage mechanisms during dynamic thermal fatigue processes are emphasized.

The development of Nb-based advanced intermetallic alloys for structural applications

NASA Astrophysics Data System (ADS)

Subramanian, P. R.; Mendiratta, M. G.; Dimiduk, D. M.

1996-01-01

A new generation of refractory material systems with significant increases in temperature capability is required to meet the demands of future aerospace applications. Such materials require a balance of properties such as low-temperature damage tolerance, high-temperature strength, creep resistance, and superior environmental stability for implementation in advanced aerospace systems. Systems incorporating niobium-based beta alloys and intermetallic compounds have the potential for meeting these requirements.

Advanced Numerical Model for Irradiated Concrete

DOE Office of Scientific and Technical Information (OSTI.GOV)

Giorla, Alain B.

In this report, we establish a numerical model for concrete exposed to irradiation to address these three critical points. The model accounts for creep in the cement paste and its coupling with damage, temperature and relative humidity. The shift in failure mode with the loading rate is also properly represented. The numerical model for creep has been validated and calibrated against different experiments in the literature [Wittmann, 1970, Le Roy, 1995]. Results from a simplified model are shown to showcase the ability of numerical homogenization to simulate irradiation effects in concrete. In future works, the complete model will be appliedmore » to the analysis of the irradiation experiments of Elleuch et al. [1972] and Kelly et al. [1969]. This requires a careful examination of the experimental environmental conditions as in both cases certain critical information are missing, including the relative humidity history. A sensitivity analysis will be conducted to provide lower and upper bounds of the concrete expansion under irradiation, and check if the scatter in the simulated results matches the one found in experiments. The numerical and experimental results will be compared in terms of expansion and loss of mechanical stiffness and strength. Both effects should be captured accordingly by the model to validate it. Once the model has been validated on these two experiments, it can be applied to simulate concrete from nuclear power plants. To do so, the materials used in these concrete must be as well characterized as possible. The main parameters required are the mechanical properties of each constituent in the concrete (aggregates, cement paste), namely the elastic modulus, the creep properties, the tensile and compressive strength, the thermal expansion coefficient, and the drying shrinkage. These can be either measured experimentally, estimated from the initial composition in the case of cement paste, or back-calculated from mechanical tests on concrete. If some are unknown, a sensitivity analysis must be carried out to provide lower and upper bounds of the material behaviour. Finally, the model can be used as a basis to formulate a macroscopic material model for concrete subject to irradiation, which later can be used in structural analyses to estimate the structural impact of irradiation on nuclear power plants.« less

Effect of high temperature creep and oxidation on residual room temperature properties for several thin sheet superalloys

NASA Technical Reports Server (NTRS)

Royster, D. M.; Lisagor, W. B.

1972-01-01

Superalloys are being considered for the primary heat shields and supports in the thermal protection system of both hypersonic transport and space shuttle vehicles. Since conservative design philosophy dictates designs based on residual material properties at the end of the service life, material characterization after exposure to the environmental conditions imposed by the flight requirements of these two classes of vehicles is needed on the candidate alloys. An investigation was conducted to provide some of the necessary data, with emphasis placed on oxidation, creep, and residual properties of thin-gage sheet material.

Effects of high power ultrasonic vibration on temperature distribution of workpiece in dry creep feed up grinding.

PubMed

Paknejad, Masih; Abdullah, Amir; Azarhoushang, Bahman

2017-11-01

Temperature history and distribution of steel workpiece (X20Cr13) was measured by a high tech infrared camera under ultrasonic assisted dry creep feed up grinding. For this purpose, a special experimental setup was designed and fabricated to vibrate only workpiece along two directions by a high power ultrasonic transducer. In this study, ultrasonic effects with respect to grinding parameters including depth of cut (a e ), feed speed (v w ), and cutting speed (v s ) has been investigated. The results indicate that the ultrasonic vibration has considerable effect on reduction of temperature, depth of thermal damage of workpiece and width of temperature contours. Maximum temperature reduction of 25.91% was reported at condition of v s =15m/s, v w =500mm/min, a e =0.4mm in the presence of ultrasonic vibration. Copyright © 2017 Elsevier B.V. All rights reserved.

High Temperature Corrosion Problem of Boiler Components in presence of Sulfur and Alkali based Fuels

NASA Astrophysics Data System (ADS)

Ghosh, Debashis; Mitra, Swapan Kumar

2011-04-01

Material degradation and ageing is of particular concern for fossil fuel fired power plant components. New techniques/approaches have been explored in recent years for Residual Life assessment of aged components and material degradation due to different damage mechanism like creep, fatigue, corrosion and erosion etc. Apart from the creep, the high temperature corrosion problem in a fossil fuel fired boiler is a matter of great concern if the fuel contains sulfur, chlorine sodium, potassium and vanadium etc. This paper discusses the material degradation due to high temperature corrosion in different critical components of boiler like water wall, superheater and reheater tubes and also remedial measures to avoid the premature failure. This paper also high lights the Residual Life Assessment (RLA) methodology of the components based on high temperature fireside corrosion. of different critical components of boiler.

Sensitivity of storage field performance to geologic and cavern design parameters in salt domes.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ehgartner, Brian L.; Park, Byoung Yoon

2009-03-01

A sensitivity study was performed utilizing a three dimensional finite element model to assess allowable cavern field sizes for strategic petroleum reserve salt domes. A potential exists for tensile fracturing and dilatancy damage to salt that can compromise the integrity of a cavern field in situations where high extraction ratios exist. The effects of salt creep rate, depth of salt dome top, dome size, caprock thickness, elastic moduli of caprock and surrounding rock, lateral stress ratio of surrounding rock, cavern size, depth of cavern, and number of caverns are examined numerically. As a result, a correlation table between the parametersmore » and the impact on the performance of storage field was established. In general, slower salt creep rates, deeper depth of salt dome top, larger elastic moduli of caprock and surrounding rock, and a smaller radius of cavern are better for structural performance of the salt dome.« less

AGC-2 Specimen Post Irradiation Data Package Report

DOE Office of Scientific and Technical Information (OSTI.GOV)

Windes, William Enoch; Swank, W. David; Rohrbaugh, David T.

This report documents results of the post-irradiation examination material property testing of the creep, control, and piggyback specimens from the irradiation creep capsule Advanced Graphite Creep (AGC)-2 are reported. This is the second of a series of six irradiation test trains planned as part of the AGC experiment to fully characterize the neutron irradiation effects and radiation creep behavior of current nuclear graphite grades. The AGC-2 capsule was irradiated in the Idaho National Laboratory Advanced Test Reactor at a nominal temperature of 600°C and to a peak dose of 5 dpa (displacements per atom). One-half of the creep specimens weremore » subjected to mechanical stresses (an applied stress of either 13.8, 17.2, or 20.7 MPa) to induce irradiation creep. All post-irradiation testing and measurement results are reported with the exception of the irradiation mechanical strength testing, which is the last destructive testing stage of the irradiation testing program. Material property tests were conducted on specimens from 15 nuclear graphite grades using a similar loading configuration as the first AGC capsule (AGC-1) to provide easy comparison between the two capsules. However, AGC-2 contained an increased number of specimens (i.e., 487 total specimens irradiated) and replaced specimens of the minor grade 2020 with the newer grade 2114. The data reported include specimen dimensions for both stressed and unstressed specimens to establish the irradiation creep rates, mass and volume data necessary to derive density, elastic constants (Young’s modulus, shear modulus, and Poisson’s ratio) from ultrasonic time-of-flight velocity measurements, Young’s modulus from the fundamental frequency of vibration, electrical resistivity, and thermal diffusivity and thermal expansion data from 100–500°C. No data outliers were determined after all measurements were completed. A brief statistical analysis was performed on the irradiated data and a limited comparison between pre- and post-irradiation properties is presented. A more complete evaluation of trends in the material property changes, as well as irradiation-induced creep due to irradiation, temperature, and applied load on specimens will be discussed in later AGC-2 post-irradiation examination analysis reports.« less

The effect of sheet processing on the microstructure, tensile, and creep behavior of INCONEL alloy 718

NASA Astrophysics Data System (ADS)

Boehlert, C. J.; Dickmann, D. S.; Eisinger, Ny. N. C.

2006-01-01

The grain size, grain boundary character distribution (GBCD), creep, and tensile behavior of INCONEL alloy 718 (IN 718) were characterized to identify processing-microstructure-property relationships. The alloy was sequentially cold rolled (CR) to 0, 10, 20, 30, 40, 60, and 80 pct followed by annealing at temperatures between 954 °C and 1050 °C and the traditional aging schedule used for this alloy. In addition, this alloy can be superplastically formed (IN 718SPF) to a significantly finer grain size and the corresponding microstructure and mechanical behavior were evaluated. The creep behavior was evaluated in the applied stress (σ a ) range of 300 to 758 MPa and the temperature range of 638 °C to 670 °C. Constant-load tensile creep experiments were used to measure the values of the steady-state creep rate and the consecutive load reduction method was used to determine the values of backstress (σ0). The values for the effective stress exponent and activation energy suggested that the transition between the rate-controlling creep mechanisms was dependent on effective stresses (σ e =σ a σ0) and the transition occurred at σ e ≅ 135 MPa. The 10 to 40 pct CR samples exhibited the greatest 650 °C strength, while IN 718SPF exhibited the greatest room-temperature (RT) tensile strength (>1550 MPa) and ductility (ɛ f >16 pct). After the 954 °C annealing treatment, the 20 pct CR and 30 pct CR microstructures exhibited the most attractive combination of elevated-temperature tensile and creep strength, while the most severely cold-rolled materials exhibited the poorest elevated-temperature properties. After the 1050 °C annealing treatment, the IN 718SPF material exhibited the greatest backstress and best creep resistance. Electron backscattered diffraction was performed to identify the GBCD as a function of CR and annealing. The data indicated that annealing above 1010 °C increased the grain size and resulted in a greater fraction of twin boundaries, which in turn increased the fraction of coincident site lattice boundaries. This result is discussed in light of the potential to grain boundary engineer this alloy.

Viscoelastic and fatigue properties of model methacrylate-based dentin adhesives

PubMed Central

Singh, Viraj; Misra, Anil; Marangos, Orestes; Park, Jonggu; Ye, Qiang; Kieweg, Sarah L.; Spencer, Paulette

2013-01-01

The objective of the current study is to characterize the viscoelastic and fatigue properties of model methacrylate-based dentin adhesives under dry and wet conditions. Static, creep, and fatigue tests were performed on cylindrical samples in a 3-point bending clamp. Static results showed that the apparent elastic modulus of the model adhesive varied from 2.56 to 3.53 GPa in the dry condition, and from 1.04 to 1.62 GPa in the wet condition, depending upon the rate of loading. Significant differences were also found for the creep behavior of the model adhesive under dry and wet conditions. A linear viscoelastic model was developed by fitting the adhesive creep behavior. The developed model with 5 Kelvin Voigt elements predicted the apparent elastic moduli measured in the static tests. The model was then utilized to interpret the fatigue test results. It was found that the failure under cyclic loading can be due to creep or fatigue, which has implications for the failure criterion that are applied for these types of tests. Finally, it was found that the adhesive samples tested under dry conditions were more durable than those tested under wet conditions. PMID:20848661

FEM simulation of the die compaction of pharmaceutical products: influence of visco-elastic phenomena and comparison with experiments.

PubMed

Diarra, Harona; Mazel, Vincent; Busignies, Virginie; Tchoreloff, Pierre

2013-09-10

This work studies the influence of visco-elastic behavior in the finite element method (FEM) modeling of die compaction of pharmaceutical products and how such a visco-elastic behavior may improve the agreement between experimental and simulated compression curves. The modeling of the process was conducted on a pharmaceutical excipient, microcrystalline cellulose (MCC), by using Drucker-Prager cap model coupled with creep behavior in Abaqus(®) software. The experimental data were obtained on a compaction simulator (STYLCAM 200R). The elastic deformation of the press was determined by performing experimental tests on a calibration disk and was introduced in the simulation. Numerical optimization was performed to characterize creep parameters. The use of creep behavior in the simulations clearly improved the agreement between the numerical and experimental compression curves (stresses, thickness), mainly during the unloading part of the compaction cycle. For the first time, it was possible to reproduce numerically the fact that the minimum tablet thickness is not obtained at the maximum compression stress. This study proves that creep behavior must be taken into account when modeling the compaction of pharmaceutical products using FEM methods. Copyright © 2013 Elsevier B.V. All rights reserved.

Effects of Aging-Time Reference on the Long Term Behavior of the IM7/K3B Composite

NASA Technical Reports Server (NTRS)

Veazie, David R.; Gates, Thomas S.

1998-01-01

An analytical study was undertaken to investigate the effects of the time-based shift reference on the long term behavior of the graphite reinforced thermoplastic polyimide composite IM7/K3B at elevated temperature. Creep compliance and the effects of physical aging on the time dependent response was measured for uniaxial loading at several isothermal conditions below the glass transition temperature (T(sub g). Two matrix dominated loading modes, shear and transverse, were investigated in tension and compression. The momentary sequenced creep/aging curves were collapsed through a horizontal (time) shift using the shortest, middle and longest aging time curve as the reference curve. Linear viscoelasticity was used to characterize the creep/recovery behavior and superposition techniques were used to establish the physical aging related material constants. The use of effective time expressions in a laminated plate model allowed for the prediction of long term creep compliance. The effect of using different reference curves with time/aging-time superposition was most sensitive to the physical aging shift rate at lower test temperatures. Depending on the loading mode, the reference curve used can result in a more accurate long term prediction, especially at lower test temperatures.

Long-term fault creep observations in central California

NASA Astrophysics Data System (ADS)

Schulz, Sandra S.; Mavko, Gerald M.; Burford, Robert O.; Stuart, William D.

1982-08-01

The U.S. Geological Survey (USGS) has been monitoring aseismic fault slip in central California for more than 10 years as part of an earthquake prediction experiment. Since 1968, the USGS creep network has grown from one creep meter at the Cienega Winery south of Hollister to a 44-station network that stretches from Hayward, east of San Francisco Bay, to Palmdale in southern California. In general, the long-term slip pattern is most variable on sections of the faults where several magnitude 4 and larger earthquakes occurred during the recording period (e.g., Calaveras fault near Hollister and San Andreas fault between San Juan Bautista and Bear Valley). These fault sections are the most difficult to characterize with a single long-term slip rate. In contrast, sections of the faults that are seismically relatively quiet (e.g., San Andreas fault between Bear Valley and Parkfield) produce the steadiest creep records and are easiest to fit with a single long-term slip rate. Appendix is available with entire article on microfiche. Order from the American Geophysical Union, 2000 Florida Avenue, N.W., Washington, D.C. 20009. Document J82-004; $1.00. Payment must accompany order.

A generalization of the Becker model in linear viscoelasticity: creep, relaxation and internal friction

NASA Astrophysics Data System (ADS)

Mainardi, Francesco; Masina, Enrico; Spada, Giorgio

2018-02-01

We present a new rheological model depending on a real parameter ν \\in [0,1], which reduces to the Maxwell body for ν =0 and to the Becker body for ν =1. The corresponding creep law is expressed in an integral form in which the exponential function of the Becker model is replaced and generalized by a Mittag-Leffler function of order ν . Then the corresponding non-dimensional creep function and its rate are studied as functions of time for different values of ν in order to visualize the transition from the classical Maxwell body to the Becker body. Based on the hereditary theory of linear viscoelasticity, we also approximate the relaxation function by solving numerically a Volterra integral equation of the second kind. In turn, the relaxation function is shown versus time for different values of ν to visualize again the transition from the classical Maxwell body to the Becker body. Furthermore, we provide a full characterization of the new model by computing, in addition to the creep and relaxation functions, the so-called specific dissipation Q^{-1} as a function of frequency, which is of particular relevance for geophysical applications.

A Study on Formation and Thermal Stability of Nano-sized Oxide Clusters in Mechanically Alloyed Nickel Aluminum for High Temperature Applications

NASA Astrophysics Data System (ADS)

Kim, Yong-Deog

The intermetallic compound, B2 NiAl, is a promising material for high temperature structural applications such as in aviation jet engines or gas turbines, provided that its high temperature mechanical properties can be improved. Although extensive efforts over the last several decades have been devoted toward enhancing ductility through alloying design and reducing impurities, as well as improving high temperature creep strength through precipitation and dispersion strengthening, these efforts have relied on traditional approaches, a combination of large grain size to limit diffusional creep and precipitation/dispersion (50 ˜ 100 nm size) strengthening to limit dislocation creep, for high temperature strengthening. While traditional approaches have shown a good improvement from a relatively high temperature strengthening point of view, the size and number density of dispersoids were not able to provide sufficient strength in the high temperature creep regime. Furthermore, details of the interaction mechanism between dislocations and dispersoids are not yet well understood. This study focuses on designing and developing advanced oxide dispersion strengthened (ODS) NiAl intermetallics with improved high temperature creep strength by incorporating a high number density (˜1024 m-3) of very thermally stable Y-Ti-O nano-clusters, akin to those recently observed to improve creep strength and radiation resistance in nano-structured ferritic alloys. Advanced ODS NiAl alloys have been produced by mechanical alloying of pre-alloyed Ni-50at%Al with Y2O3 and Ti elemental powders. The milled powders were subsequently consolidated by spark plasma sintering, with the objective of producing very high number densities of nano-sized Y-Ti-O precipitates, along with fine grain size. Advanced experimental characterization techniques, combined with microhardness strength measurement, were used to investigate the material microstructure and strength following processing and to evaluate the thermal stability during an extensive matrix of long-term thermal annealing. In particular, the size, number density and composition of nano-clusters were assessed. While improvements in strength were obtained in the advanced NiAl ODS alloys, and the higher strength persisted through thermal annealing for 100 hrs at 1723K, characterization revealed the presence of Al in the oxide precipitate phases. The Al incorporation is believed detrimental to the formation of a high density of thermally stable Y-Ti-O nanoscale precipitates.

A Continuum Damage Mechanics Model for the Static and Cyclic Fatigue of Cellular Composites

PubMed Central

Huber, Otto

2017-01-01

The fatigue behavior of a cellular composite with an epoxy matrix and glass foam granules is analyzed and modeled by means of continuum damage mechanics. The investigated cellular composite is a particular type of composite foam, and is very similar to syntactic foams. In contrast to conventional syntactic foams constituted by hollow spherical particles (balloons), cellular glass, mineral, or metal place holders are combined with the matrix material (metal or polymer) in the case of cellular composites. A microstructural investigation of the damage behavior is performed using scanning electron microscopy. For the modeling of the fatigue behavior, the damage is separated into pure static and pure cyclic damage and described in terms of the stiffness loss of the material using damage models for cyclic and creep damage. Both models incorporate nonlinear accumulation and interaction of damage. A cycle jumping procedure is developed, which allows for a fast and accurate calculation of the damage evolution for constant load frequencies. The damage model is applied to examine the mean stress effect for cyclic fatigue and to investigate the frequency effect and the influence of the signal form in the case of static and cyclic damage interaction. The calculated lifetimes are in very good agreement with experimental results. PMID:28809806

Quantifying drag on wellbore casings in moving salt sheets

NASA Astrophysics Data System (ADS)

Weijermars, R.; Jackson, M. P. A.; Dooley, T. P.

2014-08-01

Frontier hydrocarbon development projects in the deepwater slopes of the Gulf of Mexico Basin, Santos Basin and Lower Congo Basin all require wells to cross ductile layers of autochthonous or allochthonous salt moving at peak rates of 100 mm yr-1. The Couette-Poiseuille number is introduced here to help pinpoint the depth of shear stress reversal in such salt layers. For any well-planned through salt, the probable range of creep forces of moving salt needs to be taken into account when designing safety margins and load-factor tolerance of the well casing. Drag forces increase with wellbore diameter, but more significantly with effective viscosity and speed of the creeping salt layer. The potential drag forces on cased wellbores in moving salt sheets are estimated analytically using a range of salt viscosities (1015-1019 Pa s) and creep rates (0-10 mm yr-1). Drag on perfectly rigid casing of infinite strength may reach up to 13 Giga Newton per meter wellbore length in salt having a viscosity of 1019 Pa s. Well designers may delay stress accumulations due to salt drag when flexible casing accommodates some of the early displacement and strain. However, all creeping salt could displace, fracture and disconnect well casing, eventually. The shear strength of typical heavy duty well casing (about 1000 MPa) can be reached due to drag by moving salt. Internal flow of salt will then fracture the casing near salt entry and exit points, but the structural damage is likely to remain unnoticed early in the well-life when the horizontal shift of the wellbore is still negligibly small (at less than 1 cm yr-1). Disruption of casing and production flow lines within the anticipated service lifetime of a well remains a significant risk factor within distinct zones of low-viscosity salt which may reach ultrafast creep rates of 100 mm yr-1.

Constitutive Behavior of Mixed Sn-Pb/Sn-3.0Ag-0.5Cu Solder Alloys

NASA Astrophysics Data System (ADS)

Tucker, J. P.; Chan, D. K.; Subbarayan, G.; Handwerker, C. A.

2012-03-01

During the transition from Pb-containing solders to Pb-free solders, joints composed of a mixture of Sn-Pb and Sn-Ag-Cu often result from either mixed assemblies or rework. Comprehensive characterization of the mechanical behavior of these mixed solder alloys resulting in a deformationally complete constitutive description is necessary to predict failure of mixed alloy solder joints. Three alloys with 1 wt.%, 5 wt.%, and 20 wt.% Pb were selected so as to represent reasonable ranges of Pb contamination expected from different 63Sn-37Pb components mixed with Sn-3.0Ag-0.5Cu. Creep and displacement-controlled tests were performed on specially designed assemblies at temperatures of 25°C, 75°C, and 125°C using a double lap shear test setup that ensures a nearly homogeneous state of plastic strain at the joint interface. The observed changes in creep and tensile behavior with Pb additions were related to phase equilibria and microstructure differences observed through differential scanning calorimetric and scanning electron microscopic cross-sectional analysis. As Pb content increased, the steady-state creep strain rates increased, and primary creep decreased. Even 1 wt.% Pb addition was sufficient to induce substantially large creep strains relative to the Sn-3.0Ag-0.5Cu alloy. We describe rate-dependent constitutive models for Pb-contaminated Sn-Ag-Cu solder alloys, ranging from the traditional time-hardening creep model to the viscoplastic Anand model. We illustrate the utility of these constitutive models by examining the inelastic response of a chip-scale package (CSP) under thermomechanical loading through finite-element analysis. The models predict that, as Pb content increases, total inelastic dissipation decreases.

Microstructure of a Creep-Resistant 10 Pct Chromium Steel Containing 250 ppm Boron

NASA Astrophysics Data System (ADS)

Golpayegani, Ardeshir; Liu, Fang; Svensson, Henrik; Andersson, Marcus; Andrén, Hans-Olof

2011-04-01

The microstructure of a trial martensitic chromium steel containing a high content of boron (250 ppm) was characterized in detail in the as-tempered and aged conditions. This steel has a similar composition and heat treatment as the TAF steel that still is unsurpassed in creep strength among all 9 to 12 pct chromium steels. Characterization was performed by using scanning electron microscopy, energy-filtered transmission electron microscopy, secondary ion mass spectroscopy, and atom probe tomography. Focus was placed on investigating different types of precipitates that play a key role in improving the creep resistance of these steels. The low tempering temperature of 963 K (690 °C) is enough for the precipitation of the full volume fraction of both MX and M23C6. A high boron content, more than 1 at. pct, was found in M23C6 precipitates and they grow slowly during aging. The high boron level in the steel results in metal borides rather than BN with the approximate formula (Mo0.66Cr0.34)2(Fe0.75V0.25)B2. Two families of MX precipitates were found, one at lath boundaries about 35 nm in size and one dense inside the laths, only 5 to 15 nm in size.

Nonlinear viscoelastic characterization of polycarbonate

NASA Technical Reports Server (NTRS)

Caplan, E. S.; Brinson, H. F.

1982-01-01

Uniaxial tensile creep and recovery data from polycarbonate at six temperatures and six stress levels are analyzed for nonlinear viscoelastic constitutive modeling. A theory to account for combined effects of two or more accelerating factors is presented.

Equivalent damage: A critical assessment

NASA Technical Reports Server (NTRS)

Laflen, J. R.; Cook, T. S.

1982-01-01

Concepts in equivalent damage were evaluated to determine their applicability to the life prediction of hot path components of aircraft gas turbine engines. Equivalent damage was defined as being those effects which influence the crack initiation life-time beyond the damage that is measured in uniaxial, fully-reversed sinusoidal and isothermal experiments at low homologous temperatures. Three areas of equivalent damage were examined: mean stress, cumulative damage, and multiaxiality. For each area, a literature survey was conducted to aid in selecting the most appropriate theories. Where possible, data correlations were also used in the evaluation process. A set of criteria was developed for ranking the theories in each equivalent damage regime. These criteria considered aspects of engine utilization as well as the theoretical basis and correlative ability of each theory. In addition, consideration was given to the complex nature of the loading cycle at fatigue critical locations of hot path components; this loading includes non-proportional multiaxial stressing, combined temperature and strain fluctuations, and general creep-fatigue interactions. Through applications of selected equivalent damage theories to some suitable data sets it was found that there is insufficient data to allow specific recommendations of preferred theories for general applications. A series of experiments and areas of further investigations were identified.

Unusual twig "twistiness" in pawpaw (Asimina triloba) provides biomechanical protection for distal foliage in high winds.

PubMed

Goodrich, Katherine R; Ortiz, Luis A; Coughlin, David J

2016-11-01

Deciduous woody species invest considerable resources in the growth of new foliage and distal stems. This new growth is at risk for mechanical damage from high winds and storms. Pawpaw has large leaves borne distally on thin twigs. Following a storm, pawpaw branches sometimes exhibit a persistent "flipped" orientation, slowly returning upright over 24 h. We investigated biomechanical properties of pawpaw twigs, comparing them to co-occurring species with similarly high leaf areas and loads, which do not exhibit this "flipping". Our goal was to determine biomechanical and structural properties in these species and how variation in form might relate to functional differences. We measured flexural stiffness, torsional stiffness, and viscoelastic creep in pawpaw and co-occurring trees Liriodendron tulipifera and Carya cordiformis. We also recorded twig/foliage reconfiguration in high winds. We stained thin cross sections of distal twigs and recorded images using fluorescent light microscopy. Flexural and torsional stiffness increased with twig radius in pawpaw and tulip tree, although torsional stiffness increased more slowly in pawpaw. Pawpaw had a high ratio of flexural to torsional stiffness (EI/GJ) across a range of twig radii and significant viscoelastic creep compared with the other species. Biomechanical data showed that pawpaw twigs were "twistier" than the comparison species, which were shown previously to alleviate drag-induced damage by reorienting petioles and leaves. Pawpaw has an unusual strategy of low torsional stiffness in twigs, allowing for reorientation of the entire distal appendage, likely minimizing drag-induced damage in storms. © 2016 Botanical Society of America.

Effects of Amplitude Variations on Deformation and Damage Evolution in SnAgCu Solder in Isothermal Cycling

NASA Astrophysics Data System (ADS)

Wentlent, Luke; Alghoul, Thaer M.; Greene, Christopher M.; Borgesen, Peter

2018-02-01

Although apparently simpler than in thermal cycling, the behavior of SnAgCu (SAC) solder joints in cyclic bending or vibration is not currently well understood. The rate of damage has been shown to scale with the inelastic work per cycle, and excursions to higher amplitudes lead to an apparent softening, some of which remains so that damage accumulation is faster in subsequent cycling at lower amplitudes. This frequently leads to a dramatic breakdown of current damage accumulation rules. An empirical damage accumulation rule has been proposed to account for this, but any applicability to the extrapolation of accelerated test results to life under realistic long-term service conditions remains to be validated. This will require a better understanding of the underlying mechanisms. The present work provides experimental evidence to support recent suggestions that the observed behavior is a result of cycling-induced dislocation structures providing for increased diffusion creep. It is argued that this means that the measured work is an indicator of the instantaneous dislocation density, rather than necessarily reflecting the actual work involved in the creation of the damage.

Assessing the P-wave attenuation and phase velocity characteristics of fractured media based on creep and relaxation tests

NASA Astrophysics Data System (ADS)

Milani, Marco; Germán Rubino, J.; Müller, Tobias M.; Quintal, Beatriz; Holliger, Klaus

2014-05-01

Fractures are present in most geological formations and they tend to dominate not only their mechanical but also, and in particular, their hydraulic properties. For these reasons, the detection and characterization of fractures are of great interest in several fields of Earth sciences. Seismic attenuation has been recognized as a key attribute for this purpose, as both laboratory and field experiments indicate that the presence of fractures typically produces significant energy dissipation and that this attribute tends to increase with increasing fracture density. This energy loss is generally considered to be primarily due to wave-induced pressure diffusion between the fractures and the embedding porous matrix. That is, due to the strong compressibility contrast between these two domains, the propagation of seismic waves can generate a strong fluid pressure gradient and associated pressure diffusion, which leads to fluid flow and in turn results in frictional energy dissipation. Numerical simulations based on Biot's poroelastic wave equations are computationally very expensive. Alternative approaches consist in performing numerical relaxation or creep tests on representative elementary volumes (REV) of the considered medium. These tests are typically based on Biot's consolidation equations. Assuming that the heterogeneous poroelastic medium can be replaced by an effective, homogeneous viscoelastic solid, these numerical creep and relaxation tests allow for computing the equivalent seismic P-wave attenuation and phase velocity. From a practical point of view, an REV is typically characterized by the smallest volume for which rock physical properties are statistically stationary and representative of the probed medium in its entirety. A more general definition in the context of wavefield attributes is to consider an REV as the smallest volume over which the P-wave attenuation and phase velocity dispersion are independent of the applied boundary conditions. That is, the corresponding results obtained from creep and relaxation tests must be equivalent. For most analyses of media characterized by patchy saturation or double-porosity-type structures these two definitions are equivalent. It is, however, not clear whether this equivalence remains true in the presence of strong material contrasts as those prevailing in fractured rocks. In this work, we explore this question for periodically fractured media. To this end, we build a medium composed of infinite replicas of a unit volume containing one fracture. This unit volume coincides with the smallest possible volume that is statistically representative of the whole. Then, we perform several creep and relaxation tests on samples composed of an increasing number of these unit volumes. We find that the wave field signatures determined from relaxation tests are independent from the number of unit volumes. Conversely, the P-wave attenuation and phase velocity characteristics inferred from creep tests are different and vary with the number of unit volumes considered. Quite interestingly, the creep test results converge with those of the relaxation tests as the number of unit volumes increases. These findings are expected to have direct implications for corresponding laboratory measurements as well as for our understanding of seismic wave propagation in fractured media.

Comparative mineral chemistry and textures of SAFOD fault gouge and damage-zone rocks

USGS Publications Warehouse

Moore, Diane E.

2014-01-01

Creep in the San Andreas Fault Observatory at Depth (SAFOD) drillhole is localized to two foliated gouges, the central deforming zone (CDZ) and southwest deforming zone (SDZ). The gouges consist of porphyroclasts of serpentinite and sedimentary rock dispersed in a foliated matrix of Mg-smectite clays that formed as a result of shearing-enhanced reactions between the serpentinite and quartzofeldspathic rocks. The CDZ takes up most of the creep and exhibits differences in mineralogy and texture from the SDZ that are attributable to its higher shearing rate. In addition, a ∼0.2-m-wide sector of the CDZ at its northeastern margin (NE-CDZ) is identical to the SDZ and may represent a gradient in creep rate across the CDZ. The SDZ and NE-CDZ have lower clay contents and larger porphyroclasts than most of the CDZ, and they contain veinlets and strain fringes of calcite in the gouge matrix not seen elsewhere in the CDZ. Matrix clays in the SDZ and NE-CDZ are saponite and corrensite, whereas the rest of the CDZ lacks corrensite. Saponite is younger than corrensite, reflecting clay crystallization under declining temperatures, and clays in the more actively deforming portions of the CDZ have better equilibrated to the lower-temperature conditions.

Microstructure and Mechanical Properties of Extruded Gamma Met PX

NASA Technical Reports Server (NTRS)

Draper, S. L.; Das, G.; Locci, I.; Whittenberger, J. D.; Lerch, B. A.; Kestler, H.

2003-01-01

A gamma TiAl alloy with a high Nb content is being assessed as a compressor blade material. The microstructure and mechanical properties of extruded Ti-45Al-X(Nb,B,C) (at %) were evaluated in both an as-extruded condition and after a lamellar heat treatment. Tensile behavior of both as-extruded and lamellar heat treated specimens was studied in the temperature range of RT to 926 C. In general, the yield stress and ultimate tensile strength reached relatively high values at room temperature and decreased with increasing deformation temperature. The fatigue strength of both microstructures was characterized at 650 C and compared to a baseline TiAl alloy and to a Ni-base superalloy. Tensile and fatigue specimens were also exposed to 800 C for 200 h in air to evaluate the alloy's environmental resistance. A decrease in ductility was observed at room temperature due to the 800 C exposure but the 650 C fatigue properties were unaffected. Compressive and tensile creep testing between 727 and 1027 C revealed that the creep deformation was reproducible and predictable. Creep strengths reached superalloy-like levels at fast strain rates and lower temperatures but deformation at slower strain rates and/or higher temperature indicated significant weakening for the as-extruded condition. At high temperatures and low stresses, the lamellar microstructure had improved creep properties when compared to the as-extruded material. Microstructural evolution during heat treatment, identification of various phases, and the effect of microstructure on the tensile, fatigue, and creep behaviors is discussed.

Microstructure and Mechanical Properties of Extruded Gamma Microstructure Met PX

NASA Technical Reports Server (NTRS)

Draper, S. L.; Das, G.; Locci, J.; Whittenberger, J. D.; Lerch, B. A.; Kestler, H.

2003-01-01

A gamma TiAl alloy with a high Nb content is being assessed as a compressor blade material. The microstructure and mechanical properties of extruded Ti-45Al-X(Nb,B,C) (at.%) were evaluated in both an as-extruded condition and after a lamellar heat treatment. Tensile behavior of both as-extruded and lamellar heat treated specimens was studied in the temperature range of RT to 926 C. In general, the yield stress and ultimate tensile strength reached relatively high values at room temperature and decreased with increasing deformation temperature. The fatigue strength of both microstructures was characterized at 650 C and compared to a baseline TiAl alloy and to a Ni-base superalloy. Tensile and fatigue specimens were also exposed to 800 C for 200 h in air to evaluate the alloy's environmental resistance. A decrease in ductility was observed at room temperature due to the 800 C. exposure but the 650 C fatigue properties were unaffected. Compressive and tensile creep testing between 727 and 1027 C revealed that the creep deformation was reproducible and predictable. Creep strengths reached superalloy-like levels at fast strain rates and lower temperatures but deformation at slower strain rates and/or higher temperature indicated significant weakening for the as-extruded condition. At high temperatures and low stresses, the lamellar microstructure had improved creep properties when compared to the as-extruded material. Microstructural evolution during heat treatment, identification of various phases, and the effect of microstructure on the tensile, fatigue, and creep behaviors is discussed.

Analysis of pellet cladding interaction and creep of U 3SIi2 fuel for use in light water reactors

NASA Astrophysics Data System (ADS)

Metzger, Kathryn E.

Following the accident at the Fukushima plant, enhancing the accident tolerance of the light water reactor (LWR) fleet became a topic of serious discussion. Under the direction of congress, the DOE office of Nuclear Energy added accident tolerant fuel development as a primary component to the existing Advanced Fuels Program. The DOE defines accident tolerant fuels as fuels that "in comparison with the standard UO2- Zircaloy system currently used by the nuclear industry, can tolerate loss of active cooling in the reactor core for a considerably longer time period (depending on the LWR system and accident scenario) while maintaining or improving the fuel performance during normal operations, operational transients, as well as design-basis and beyond design-basis events." To be economically viable, proposed accident tolerant fuels and claddings should be backward compatible with LWR designs, provide significant operating cost improvements such as power uprates, increased fuel burnup, or increased cycle length. In terms of safety, an alternative fuel pellet must have resistance to water corrosion comparable to UO2, thermal conductivity equal to or larger than that of UO2, and a melting temperature that allows the material to remain solid under power reactor conditions. Among the candidates, U3Si2 has a number of advantageous thermophysical properties, including; high density, high thermal conductivity at room temperature, and a high melting temperature. These properties support its use as an accident tolerant fuel while its high uranium density is capable of supporting uprates to the LWR fleet. This research characterizes U3Si2 pellets and analyzes U3Si2 under light water reactor conditions using the fuel performance code BISON. While some thermophysical properties for U3Si2 have been found in the literature, the irradiation behavior is sparse and limited to experience with dispersion fuels. Accordingly, the creep behavior for U3Si2 has been unknown, making it difficult to predict fuel-cladding mechanical behavior. This information is essential for designing accident tolerant fuel systems where ceramic claddings, like silicon carbide (SiC) are proposed. This research provides a model for both the thermal and irradiation creep behavior for U3Si2. This body of research is comprised of both experimental and modeling components. Characterization of the fuel microstructure includes; optical microscopy with pore and grain size analysis, helium pycnometry for density determination, mercury intrusion porosimetry, compositional analysis in the form of XRD, second phase identification using EDX, electrical resistance measurement via four point probe, determination of hardness and toughness through Vickers indentation testing, and determination of elastic properties using the impulse excitation method. Post-sintering grain size data allowed for the determination of grain boundary activation energy and diffusion coefficients, which were used to develop creep models. This was extended to lattice and irradiation enhanced diffusion in order to develop a U3Si2 creep model over thermal and irradiation creep regimes. In addition to the creep model, thermal and swelling behavior models for U3Si2 were implemented into the BISON fuel performance code. A series of simulations evaluated the performance and behavior of U3Si2 under typical light water reactor conditions with advanced SiC ceramic cladding. Simulation results show that fuel creep relieves stress in the ceramic cladding and postpones the. moment of fuel-clad contact. However, the stress reduction to the cladding is minimal because the fuel creep rate is low while the swelling rate is high. Future work should include the investigation of monolithic U3Si2 irradiation swelling since the current model relies upon the swelling data of U3Si2 particles in a metallic dispersion fuel. Additionally, planned thermal creep testing at the University of South Carolina can provide confirmation of the U3Si2 creep model contained herein.

Laboratory tests for hot-mix asphalt characterization in Virginia.

DOT National Transportation Integrated Search

2005-01-01

This project reviewed existing laboratory methods for accurately describing the constitutive behavior of the mixes used in the Commonwealth of Virginia. Indirect tensile (IDT) strength, resilient modulus, static creep in the IDT and uniaxial modes, f...

Time dependent reliability model incorporating continuum damage mechanics for high-temperature ceramics

NASA Technical Reports Server (NTRS)

Duffy, Stephen F.; Gyekenyesi, John P.

1989-01-01

Presently there are many opportunities for the application of ceramic materials at elevated temperatures. In the near future ceramic materials are expected to supplant high temperature metal alloys in a number of applications. It thus becomes essential to develop a capability to predict the time-dependent response of these materials. The creep rupture phenomenon is discussed, and a time-dependent reliability model is outlined that integrates continuum damage mechanics principles and Weibull analysis. Several features of the model are presented in a qualitative fashion, including predictions of both reliability and hazard rate. In addition, a comparison of the continuum and the microstructural kinetic equations highlights a strong resemblance in the two approaches.

Accelerated Threshold Fatigue Crack Growth Effect-Powder Metallurgy Aluminum Alloy

NASA Technical Reports Server (NTRS)

Piascik, R. S.; Newman, J. A.

2002-01-01

Fatigue crack growth (FCG) research conducted in the near threshold regime has identified a room temperature creep crack growth damage mechanism for a fine grain powder metallurgy (PM) aluminum alloy (8009). At very low (Delta) K, an abrupt acceleration in room temperature FCG rate occurs at high stress ratio (R = K(sub min)/K(sub max)). The near threshold accelerated FCG rates are exacerbated by increased levels of K(sub max) (K(sub max) = 0.4 K(sub IC)). Detailed fractographic analysis correlates accelerated FCG with the formation of crack-tip process zone micro-void damage. Experimental results show that the near threshold and K(sub max) influenced accelerated crack growth is time and temperature dependent.

Endochronic theory of transient creep and creep recovery

NASA Technical Reports Server (NTRS)

Wu, H. C.; Chen, L.

1979-01-01

Short time creep and creep recovery were investigated by means of the endochronic theory of viscoplasticity. It is shown that the constitutive equations for constant-strain-rate stress-strain behavior, creep, creep recovery, and stress relaxation can all ber derived from the general constitutive equation by imposing appropriate constraints. In this unified approach, the effect of strain-hardening is naturally accounted for when describing creep and creep recovery. The theory predicts with reasonable accuracy the creep and creep recovery behaviors for Aluminum 1100-0 at 150 C. It was found that the strain-rate history at prestraining stage affects the subsequent creep. A critical stress was also established for creep recovery. The theory predicts a forward creep for creep recovery stress greater than the critical stress. For creep recovery stress less than the critical stress, the theory then predicts a normal strain recovery.

Ceramic Matrix Composite (CMC) Materials Characterization

NASA Technical Reports Server (NTRS)

Calomino, Anthony

2001-01-01

Under the former NASA EPM Program, much initial progress was made in identifying constituent materials and processes for SiC/SiC ceramic composite hot-section components. This presentation discusses the performance benefits of these approaches and elaborates on further constituent and property improvements made under NASA UEET. These include specific treatments at NASA that significantly improve the creep and environmental resistance of the Sylramic(TM) SiC fiber as well as the thermal conductivity and creep resistance of the CVI Sic matrix. Also discussed are recent findings concerning the beneficial effects of certain 2D-fabric architectures and carbon between the BN interphase coating and Sic matrix.

Analysis of Factors Affecting the Performance of RLV Thrust Cell Liners

NASA Technical Reports Server (NTRS)

Arnold, Steven M. (Technical Monitor); Butler, Daniel T., Jr.; Pinders, Marek-Jerzy

2004-01-01

The reusable launch vehicle (RLV) thrust cell liner, or thrust chamber, is a critical component of the Space Shuttle Main Engine (SSME). It is designed to operate in some of the most severe conditions seen in engineering practice. This requirement, in conjunction with experimentally observed 'dog-house' failure modes characterized by bulging and thinning of the cooling channel wall, provides the motivation to study the factors that influence RLV thrust cell liner performance. Factors or parameters believed to be directly related to the observed characteristic deformation modes leading to failure under in-service loading conditions are identified, and subsequently investigated using the cylindrical version of the higher-order theory for functionally graded materials in conjunction with the Robinson's unified viscoplasticity theory and the power-law creep model for modeling the response of the liner s constituents. Configurations are analyzed in which specific modifications in cooling channel wall thickness or constituent materials are made to determine the influence of these parameters on the deformations resulting in the observed failure modes in the outer walls of the cooling channel. The application of thermal barrier coatings and functional grading are also investigated within this context. Comparison of the higher-order theory results based on the Robinson and power-law creep model predictions has demonstrated that, using the available material parameters, the power-law creep model predicts more precisely the experimentally observed deformation leading to the 'dog-house' failure mode for multiple short cycles, while also providing much improved computational efficiency. However, for a single long cycle, both models predict virtually identical deformations. Increasing the power-law creep model coefficients produces appreciable deformations after just one long cycle that would normally be obtained after multiple cycles, thereby enhancing the efficiency of the analysis. This provides a basis for the development of an accelerated modeling procedure to further characterize dog-house deformation modes in RLV thrust cell liners. Additionally, the results presented herein have demonstrated that the mechanism responsible for deformation leading to 'dog-house' failure modes is driven by pressure, creep/relaxation and geometric effects.

Fluid-injection and the mechanics of frictional stability of shale-bearing faults

NASA Astrophysics Data System (ADS)

Scuderi, Marco Maria; Collettini, Cristiano; Marone, Chris

2017-04-01

Fluid overpressure is one of the primary mechanisms for triggering tectonic fault slip and human-induced seismicity. This mechanism is appealing because fluids lubricate the fault and reduce the effective normal stress that holds the fault in place. However, current models of earthquake nucleation, based on rate- and state- friction, imply that stable sliding is favored by the increase of pore fluid pressure. Despite this apparent dilemma, there are a few studies on the role of fluid pressure in frictional stability under controlled, laboratory conditions. Here, we describe laboratory experiments on shale fault gouge, conducted in the double direct shear configuration in a true-triaxial machine. To characterize frictional stability and hydrological properties we performed three types of experiments: 1) stable sliding shear experiment to determine the material failure envelope resulting in fault strength of µ=0.28 and fault zone permeability (k 10-19m2); 2) velocity step experiments to determine the rate- and state- frictional properties, characterized by a velocity strengthening behavior with a negative rate parameter b, indicative of stable aseismic creep; 3) creep experiment to study fault slip evolution with increasing pore-fluid pressure. In these creep experiments fault slip history can be divided in three main stages: a) for low fluid pressure the fault is locked and undergoes compaction; b) with increasing fluid pressurization, we observe aseismic creep (i.e. v=0.0001 µm/s) associated with fault dilation, with maintained low permeability; c) As fluid pressure is further increased and we approach the failure criteria fault begins to accelerate, the dilation rate increases causing an increase in permeability. Following the first acceleration we document complex fault slip behavior characterized by periodic accelerations and decelerations with slip velocity that remains slow (i.e. v 200 µm/s), never approaching dynamic slip rates. Surprisingly, this complex slip behavior is associated with fault zone compaction and permeability increase as opposite to the dilation hardening mechanism that is usually invoked to quench the instability. We relate this complex fault slip behaviour to the interplay between fault weakening induced by fluid pressurization and the strong rate-strengthening behaviour of shales. Our data show that fault rheology and fault stability is controlled by the coupling between fluid pressure and rate- and state- friction parameters suggesting that their comprehensive characterization is fundamental for assessing the role of fluid pressure in natural and human induced earthquakes.

Simulating subduction zone earthquakes using discrete element method: a window into elusive source processes

NASA Astrophysics Data System (ADS)

Blank, D. G.; Morgan, J.

2017-12-01

Large earthquakes that occur on convergent plate margin interfaces have the potential to cause widespread damage and loss of life. Recent observations reveal that a wide range of different slip behaviors take place along these megathrust faults, which demonstrate both their complexity, and our limited understanding of fault processes and their controls. Numerical modeling provides us with a useful tool that we can use to simulate earthquakes and related slip events, and to make direct observations and correlations among properties and parameters that might control them. Further analysis of these phenomena can lead to a more complete understanding of the underlying mechanisms that accompany the nucleation of large earthquakes, and what might trigger them. In this study, we use the discrete element method (DEM) to create numerical analogs to subduction megathrusts with heterogeneous fault friction. Displacement boundary conditions are applied in order to simulate tectonic loading, which in turn, induces slip along the fault. A wide range of slip behaviors are observed, ranging from creep to stick slip. We are able to characterize slip events by duration, stress drop, rupture area, and slip magnitude, and to correlate the relationships among these quantities. These characterizations allow us to develop a catalog of rupture events both spatially and temporally, for comparison with slip processes on natural faults.

A Generalized Maxwell Model for Creep Behavior of Artery Opening Angle

PubMed Central

Zhang, W.; Guo, X.; Kassab, G. S.

2009-01-01

An artery ring springs open into a sector after a radial cut. The opening angle characterizes the residual strain in the unloaded state, which is fundamental to understanding stress and strain in the vessel wall. A recent study revealed that the opening angle decreases with time if the artery is cut from the loaded state, while it increases if the cut is made from the no-load state due to viscoelasticity. In both cases, the opening angle approaches the same value in 3 hours. This implies that the characteristic relaxation time is about 10,000 sec. Here, the creep function of a generalized Maxwell model (a spring in series with six Voigt bodies) is used to predict the temporal change of opening angle in multiple time scales. It is demonstrated that the theoretical model captures the salient features of the experimental results. The proposed creep function may be extended to study the viscoelastic response of blood vessels under various loading conditions. PMID:19045526

Radiation and temperature effects on the time-dependent response of T300/934 graphite/epoxy

NASA Technical Reports Server (NTRS)

Yancey, Robert N.; Pindera, Marek-Jerzy

1988-01-01

A time-dependent characterization study was performed on T300/934 graphite/epoxy in a simulated space environment. Creep tests on irradiated and nonirradiated graphite/epoxy and bulk resin specimens were carried out at temperatures of 72 and 250 F. Irradiated specimens were exposed to dosages of penetrating electron radiation equal to 30 years exposure at GEO-synchronous orbit. Radiation was shown to have little effect on the creep response of both the composite and bulk resin specimens at 72 F while radiation had a significant effect at 250 F. A healing process was shown to be present in the irradiated specimens where broken bonds in the epoxy due to radiation recombined over time to form cross-links in the 934 resin structure. An analytical micromechanical model was also developed to predict the viscoelastic response of fiber reinforced composite materials. The model was shown to correlate well with experimental results for linearly viscoelastic materials with relatively small creep strains.

Damage and failure behavior of metal matrix composites under biaxial loads

NASA Astrophysics Data System (ADS)

Kirkpatrick, Steven Wayne

Metal matrix composites (MMCs) are being considered for increased use in structures that require the ductility and damage tolerance of the metal matrix and the enhanced strength and creep resistance at elevated temperatures of high performance fibers. Particularly promising for advanced aerospace engines and airframes are SiC fiber/titanium matrix composites (TMCs). A large program was undertaken in the Air Force to characterize the deformation and failure behaviors of TMCs and to develop computational models that can be used for component design. The effort reported here focused on a SiC SCS-6/Timetal 21S composite under biaxial loading conditions. Biaxial loading conditions are important because multiaxial stresses have been shown to influence the strength and ductility of engineering materials and, in general, structural components are subjected to multiaxial loads. The TMC material response, including stress-strain curves and failure surfaces, was measured using a combination of off-axis uniaxial tension and compression tests and biaxial cruciform tests. The off-axis tests produce combinations of in-plane tension, compression, and shear stresses, the mix of which are controlled by the relative angle between the fiber and specimen axes. The biaxial cruciform tests allowed independent control over the tensile or compressive loads in the fiber and transverse directions. The results of these characterization tests were used to develop a microstructural constitutive model and failure criteria. The basis of the micromechanical constitutive model is a representative unit volume of the MMC with a periodic array of fibers. The representative unit volume is divided into a fiber and three matrix cells for which the microstructural equilibrium and compatibility equations can be analyzed. The resulting constitutive model and associated failure criteria can be used to predict the material behavior under general loading conditions.

Development of Advanced 9Cr Ferritic-Martensitic Steels and Austenitic Stainless Steels for Sodium-Cooled Fast Reactor

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sham, Sam; Tan, Lizhen; Yamamoto, Yukinori

2013-01-01

Ferritic-martensitic (FM) steel Grade 92, with or without thermomechanical treatment (TMT), and austenitic stainless steels HT-UPS (high-temperature ultrafine precipitate strengthening) and NF709 were selected as potential candidate structural materials in the U.S. Sodium-cooled Fast Reactor (SFR) program. The objective is to develop advanced steels with improved properties as compared with reference materials such as Grade 91 and Type 316H steels that are currently in nuclear design codes. Composition modification and/or processing optimization (e.g., TMT and cold-work) were performed to improve properties such as resistance to thermal aging, creep, creep-fatigue, fracture, and sodium corrosion. Testings to characterize these properties for themore » advanced steels were conducted by the Idaho National Laboratory, the Argonne National Laboratory and the Oak Ridge National Laboratory under the U.S. SFR program. This paper focuses on the resistance to thermal aging and creep of the advanced steels. The advanced steels exhibited up to two orders of magnitude increase in creep life compared to the reference materials. Preliminary results on the weldment performance of the advanced steels are also presented. The superior performance of the advanced steels would improve reactor design flexibility, safety margins and economics.« less

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shassere, Benjamin; Yamamoto, Yukinori; Poplawsky, Jonathan

We have develooped a new Fe-Cr-Al (FCA) alloy system with good oxidation resistance and creep strength at high temperature. The alloy system is a candidate for use in future fossil-fueled power plants. The creep strength of these alloys at 973 K (700 °C) was found to be comparable with traditional 9 pct Cr ferritic–martensitic steels. A few FCA alloys with general composition of Fe-30Cr-3Al-.2Si-xNb (x = 0, 1, or 2) with a ferrite matrix and Fe 2Nb-type Laves precipitates were prepared. The detailed microstructural characterization of samples, before and after creep rupture testing, indicated precipitation of the Laves phase withinmore » the matrix, Laves phase at the grain boundaries, and a 0.5 to 1.5 μm wide precipitate-free zone (PFZ) parallel to all the grain boundaries. In these alloys, the areal fraction of grain boundary Laves phase and the width of the PFZ controlled the cavitation nucleation and eventual grain boundary ductile failure. Finally, we used a phenomenological model to compare the creep strain rates controlled by the effects of the particles on the dislocations within the grain and at grain boundaries. (The research sponsored by US-DOE, Office of Fossil Energy, the Crosscutting Research Program).« less

Effects of Environment on Creep Behavior of Nextel 720/Alumina-Mullite Ceramic Composite at 1200 deg C

DTIC Science & Technology

2008-03-01

creep life . This degradation increased with increasing temperatures. At 1000°, all specimens achieved creep run-out, defined as...strain measurement 29 Table 4. Summary of N720/AM creep data. Sample Environment Thermal Strain (%) E (GPa) Creep Stress (MPa) Creep Life (h...Material Creep Stress(MPa) Creep Life (h) Creep Strain (%) Secondary Creep Rate (s-1) N720/A 80 >100 0.798 1.5E-08 N720/A 100 41 1.520

Lifetime Prediction of Nano-Silica based Glass Fibre/Epoxy composite by Time Temperature Superposition Principle

NASA Astrophysics Data System (ADS)

Anand, Abhijeet; Banerjee, Poulami; Prusty, Rajesh Kumar; Ray, Bankin Chandra

2018-03-01

The incorporation of nano fillers in Fibre reinforced polymer (FRP) composites has been a source of experimentation for researchers. Addition of nano fillers has been found to improve mechanical, thermal as well as electrical properties of Glass fibre reinforced polymer (GFRP) composites. The in-plane mechanical properties of GFRP composite are mainly controlled by fibers and therefore exhibit good values. However, composite exhibits poor through-thickness properties, in which the matrix and interface are the dominant factors. Therefore, it is conducive to modify the matrix through dispersion of nano fillers. Creep is defined as the plastic deformation experienced by a material for a temperature at constant stress over a prolonged period of time. Determination of Master Curve using time-temperature superposition principle is conducive for predicting the lifetime of materials involved in naval and structural applications. This is because such materials remain in service for a prolonged time period before failure which is difficult to be kept marked. However, the failure analysis can be extrapolated from its behaviour in a shorter time at an elevated temperature as is done in master creep analysis. The present research work dealt with time-temperature analysis of 0.1% SiO2-based GFRP composites fabricated through hand-layup method. Composition of 0.1% for SiO2nano fillers with respect to the weight of the fibers was observed to provide optimized flexural properties. Time and temperature dependence of flexural properties of GFRP composites with and without nano SiO2 was determined by conducting 3-point bend flexural creep tests over a range of temperature. Stepwise isothermal creep tests from room temperature (30°C) to the glass transition temperature Tg (120°C) were performed with an alternative creep/relaxation period of 1 hour at each temperature. A constant stress of 40MPa was applied during the creep tests. The time-temperature superposition principle was followed while determining the Master Curve and cumulative damage law. The purpose of a Master Curve was to determine the variation of compliance with respect to increase in time and temperature of the specimen. The shift factors at any reference temperature were determined by Arrhenius activation energy method at a far lower temperature than Tg (Glass transition temperature) and by manual shift method at a temperature near Tg (Glass transition temperature).

Crack networks in damaged glass

NASA Astrophysics Data System (ADS)

Mallet, Celine; Fortin, Jerome; Gueguen, Yves

2013-04-01

We investigate how cracks develop and propagate in synthetic glass samples. Cracks are introduced in glass by a thermal shock of 300oC. Crack network is documented from optical and electronic microscopy on these samples that have been submitted to a thermal shock only. Samples are cylinder of 80 mm length and 40 mm diameter. Sections were cut along the cylinder axis and perpendicular to it. Using SEM, crack lengths and apertures can be measured. Optical microscopy allows to get the crack distribution over the entire sample. The sample average crack length is 3 mm. The average aperture is 6 ± 3μm. There is however a clear difference between the sample core, where the crack network has approximatively a transverse isotrope symmetry and the outer ring, where cracks are smaller and more numerous. By measuring before and after the thermal treatment the radial P and S wave velocities in room conditions, we can determine the total crack density which is 0.24. Thermally cracked samples, as described above, were submitted to creep tests. Constant axial stress and lateral stress were applied. Several experiments were performed at different stress values. Samples are saturated for 48 hours (to get an homogeneous pore fluid distribution), the axial stress is increased up to 80% of the sample strength. Stress step tests were performed in order to get creep data. The evolution of strain (axial and radial strain) is measured using strain gages, gap sensors (for the global axial strain) and pore volume change (for the volumetric strain). Creep data are interpreted as evidence of sub-critical crack growth in the cracked glass samples. The above microstructural observations are used, together with a crack propagation model, to account for the creep behavior. Assuming that (i) the observed volumetric strain rate is due to crack propagation and (ii) crack aspect ratio is constant we calculate the creep rate. We obtain some value on the crack propagation during a 24 hours of constant stress test. At each of these test, crack propagate of 0.3 to 0.4 mm. From the initial average crack length of 3 mm, the crack reach the size of 5.8 mm at the end of a complete creep test (with 8 constant stress step of 24 hours).

Boiler-turbine life extension

DOE Office of Scientific and Technical Information (OSTI.GOV)

Natzkov, S.; Nikolov, M.

1995-12-01

The design life of the main power equipment-boilers and turbines is about 105 working hours. The possibilities for life extension are after normatively regulated control tests. The diagnostics and methodology for Boilers and Turbines Elements Remaining Life Assessment using up to date computer programs, destructive and nondestructive control of metal of key elements of units equipment, metal creep and low cycle fatigue calculations. As well as data for most common damages and some technical decisions for elements life extension are presented.

Pelletized Asphalt for Airfield Damage Repair

DTIC Science & Technology

2009-08-01

The public reporting burden for this collection of information is estimated to average 1 hour per response, including the time for reviewing...terms of resistance to rutting because the binder will dissipate less energy as permanent deformation per load cycle (7). The high pavement... Vessel ) material at 10 radian/sec oscillatory shear and 31°C, and 5) a maximum stiffness of 300 MPa and a minimum creep slope of 0.3 at -12°C for the

Damage-mitigating control of aerospace systems for high performance and extended life

NASA Technical Reports Server (NTRS)

Ray, Asok; Wu, Min-Kuang; Carpino, Marc; Lorenzo, Carl F.; Merrill, Walter C.

1992-01-01

The concept of damage-mitigating control is to minimize fatigue (as well as creep and corrosion) damage of critical components of mechanical structures while simultaneously maximizing the system dynamic performance. Given a dynamic model of the plant and the specifications for performance and stability robustness, the task is to synthesize a control law that would meet the system requirements and, at the same time, satisfy the constraints that are imposed by the material and structural properties of the critical components. The authors present the concept of damage-mitigating control systems design with the following objectives: (1) to achieve high performance with a prolonged life span; and (2) to systematically update the controller as the new technology of advanced materials evolves. The major challenge is to extract the information from the material properties and then utilize this information in a mathematical form so that it can be directly applied to robust control synthesis for mechanical systems. The basic concept of damage-mitigating control is illustrated using a relatively simplified model of a space shuttle main engine.

Interdisciplinary research on the nature and properties of ceramic materials

NASA Technical Reports Server (NTRS)

1980-01-01

Several investigations concerning the properties and processing of brittle ceramic materials as related to design considerations are briefly described. Surface characterization techniques, fractography, high purity materials, creep properties, impact and thermal shock resistance, and reaction bonding are discussed.

Irradiation response of commercial, high-Tc superconducting tapes: Electromagnetic transport properties

DOE PAGES

Gapud, A. A.; Greenwood, N. T.; Alexander, J. A.; ...

2015-07-01

Effects of low dose irradiation on the electrical transport current properties of commercially available high-temperature superconducting, coated-conductor tapes were investigated, in view of potential applications in the irradiative environment of fusion reactors. Three different tapes, each with unique as-grown flux-pinning structures, were irradiated with Au and Ni ions at energies that provide a range of damage effects, with accumulated damage levels near that expected for conductors in a fusion reactor environment. Measurements using transport current determined the pre- and post-irradiation resistivity, critical current density, and pinning force density, yielding critical temperatures, irreversibility lines, and inferred vortex creep rates. Results showmore » that at the irradiation damage levels tested, any detriment to as-grown pre-irradiation properties is modest; indeed in one case already-superior pinning forces are enhanced, leading to higher critical currents.« less

A New Ductility Exhaustion Model for High Temperature Low Cycle Fatigue Life Prediction of Turbine Disk Alloys

NASA Astrophysics Data System (ADS)

Zhu, Shun-Peng; Huang, Hong-Zhong; Li, Haiqing; Sun, Rui; Zuo, Ming J.

2011-06-01

Based on ductility exhaustion theory and the generalized energy-based damage parameter, a new viscosity-based life prediction model is introduced to account for the mean strain/stress effects in the low cycle fatigue regime. The loading waveform parameters and cyclic hardening effects are also incorporated within this model. It is assumed that damage accrues by means of viscous flow and ductility consumption is only related to plastic strain and creep strain under high temperature low cycle fatigue conditions. In the developed model, dynamic viscosity is used to describe the flow behavior. This model provides a better prediction of Superalloy GH4133's fatigue behavior when compared to Goswami's ductility model and the generalized damage parameter. Under non-zero mean strain conditions, moreover, the proposed model provides more accurate predictions of Superalloy GH4133's fatigue behavior than that with zero mean strains.

Compaction of granular materials: numerical simulation of "elastic" compression and pressure solution creep

NASA Astrophysics Data System (ADS)

Bernabe, Y.; Evans, J.

2012-12-01

In a previous work we investigated stress transfer in a pair of grain contacts undergoing pressure solution (PS) creep, showed that stress transfer resulted in a significant decrease in overall strain rate, and concluded that PS creep rates of a randomly packed granular aggregate should be affected by packing evolution and the formation of new contacts during creep. To test these conclusions further, we are numerically simulating the "elastic" hydrostatic compression of a random pack of spheres, using a numerical method similar to that of Cundall and Strack [1979]. We assumed that the spheres were frictionless (i.e., spheres in contact only interacted through normal forces) and that the contact forces obeyed the non-linear Digby [1981] model. In order to determine the PS creep compression of the sphere pack subjected to a constant confining pressure pc, we calculated the thicknesses of the dissolved layers at each individual grain contact during a small time increment and, from these, the overall deformation of the sphere pack. We used an analytical expression discussed in our previous paper and originating from Lehner and Leroy [2004]. During these simulations, we also computed the mean coordination number of the grain contact z, the effective bulk modulus K of the sphere pack and others parameters characterizing the topological and mechanical properties of the sphere assembly. Our results show strong non-linear increase of z and K with pc during "elastic" compression and, with time, during PS creep. The packing rearrangements associated with PS creep produce complex time dependence of the overall deformation ɛ(t). We observed a regular transition from ɛ∝t^3/4 at early times (i.e., less than 0.1 years) and ɛ∝t^1/3 at late times (i.e., more than 1000 years). Cundall, P.A., and O.D.L. Strack (1979), A discrete numerical model for granular assemblies, Geotech., 29, 47-65. Digby, P.J. (1981), The effective elastic moduli of porous rocks, J. Appl. Mech., 48, 803-808. Lehner, F.K., and Y. Leroy (2004), Sandstone compaction by intergranular pressure solution, In Mech. Fluid Saturated Rocks (eds. Y. Guéguen and M. Boutéca), Elsevier.

Creep and Creep Recovery Response of Load Cells Tested According to U.S. and International Evaluation Procedures

PubMed Central

Bartel, Thomas W.; Yaniv, Simone L.

1997-01-01

The 60 min creep data from National Type Evaluation Procedure (NTEP) tests performed at the National Institute of Standards and Technology (NIST) on 65 load cells have been analyzed in order to compare their creep and creep recovery responses, and to compare the 60 min creep with creep over shorter time periods. To facilitate this comparison the data were fitted to a multiple-term exponential equation, which adequately describes the creep and creep recovery responses of load cells. The use of such a curve fit reduces the effect of the random error in the indicator readings on the calculated values of the load cell creep. Examination of the fitted curves show that the creep recovery responses, after inversion by a change in sign, are generally similar in shape to the creep response, but smaller in magnitude. The average ratio of the absolute value of the maximum creep recovery to the maximum creep is 0.86; however, no reliable correlation between creep and creep recovery can be drawn from the data. The fitted curves were also used to compare the 60 min creep of the NTEP analysis with the 30 min creep and other parameters calculated according to the Organization Internationale de Métrologie Légale (OIML) R 60 analysis. The average ratio of the 30 min creep value to the 60 min value is 0.84. The OIML class C creep tolerance is less than 0.5 of the NTEP tolerance for classes III and III L. PMID:27805151

Effect of misalignment on mechanical behavior of metals in creep. [computer programs

NASA Technical Reports Server (NTRS)

Wu, H. C.

1979-01-01

Application of the endochronic theory of viscoplasticity to creep, creep recovery, and stress relaxation at the small strain and short time range produced the following results: (1) The governing constitutive equations for constant-strain-rate stress-strain behavior, creep, creep recovery, and stress relaxation were derived by imposing appropriate constraints on the general constitutive equation of the endochronic theory. (2) A set of material constants was found which correlate strain-hardening, creep, creep recovery, and stress relaxation. (3) The theory predicts with reasonable accuracy the creep and creep recovery behaviors at short time. (4) The initial strain history prior to the creep stage affects the subsequent creep significantly. (5) A critical stress was established for creep recovery. A computer program, written for the misalignment problem is reported.

Irradiation creep and precipitation in a ferritic ODS steel under helium implantation

NASA Astrophysics Data System (ADS)

Chen, J.; Jung, P.; Pouchon, M. A.; Rebac, T.; Hoffelner, W.

2008-02-01

Ferritic oxide dispersion strengthened (ODS) steel, PM2000, has been homogeneously implanted with helium under uniaxial tensile stresses from 20 to 250 MPa to maximum doses of about 0.75 dpa (3000 ppm He) with displacement damage rates of 5.5 × 10 -6 dpa/s at temperatures of 573, 673 and 773 K. Straining of a miniaturized dog-bone specimen under helium implantation was monitored by linear variable displacement transformer (LVDT) and meanwhile by their resistance also measured by four-pole technique. Creep compliance was almost constant at 5.7 × 10 -6 dpa -1 MPa -1 for temperatures below 673 K and increased to 18 × 10 -6 dpa -1 MPa -1 at 773 K. The resistivity of PM2000 samples decreased with dose and showed a tendency to saturation. Subsequent transmission electron microscopy observations indicated the formation of ordered Fe 3- xCr xAl precipitates during implantation. Correlations between the microstructure and resistivity are discussed.

Atom probe tomography analysis of high dose MA957 at selected irradiation temperatures

NASA Astrophysics Data System (ADS)

Bailey, Nathan A.; Stergar, Erich; Toloczko, Mychailo; Hosemann, Peter

2015-04-01

Oxide dispersion strengthened (ODS) alloys are meritable structural materials for nuclear reactor systems due to the exemplary resistance to radiation damage and high temperature creep. Summarized in this work are atom probe tomography (APT) investigations on a heat of MA957 that underwent irradiation in the form of in-reactor creep specimens in the Fast Flux Test Facility-Materials Open Test Assembly (FFTF-MOTA) for the Liquid Metal Fast Breeder Reactor (LMFBR) program. The oxide precipitates appear stable under irradiation at elevated temperature over extended periods of time. Nominally, the precipitate chemistry is unchanged by the accumulated dose; although, evidence suggests that ballistic dissolution and reformation processes are occurring at all irradiation temperatures. At 412 °C-109 dpa, chromium enrichments - consistent with the α‧ phase - appear between the oxide precipitates, indicating radiation induced segregation. Grain boundaries, enriched with several elements including nickel and titanium, are observed at all irradiation conditions. At 412 °C-109 dpa, the grain boundaries are also enriched in molecular titanium oxide (TiO).

Interface between fatigue, creep and stress-corrosion cracking on Ti6246 titanium alloy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sarrazin-Baudoux, C.; Chabanne, Y.; Petit, J.

1999-07-01

The influence of mean stress on the fatigue crack growth behavior of a Ti6246 alloy has been studied in the near-threshold area at room temperature and at 500 C. Tests were performed at various constant K{sub max} levels in ambient air, high vacuum and humidified Argon. Conditions for the occurrence of an abnormal behavior consisting in the disappearance of the threshold for sufficiently high K{sub max} level, are discussed with respect to environment and temperature. This effect is observed in air and in vacuum for K{sub max} higher than 52 MPa{radical}m, and is related to an intrinsic creep damage processmore » which appears more efficient at room temperature than at 500 C and more accentuated in air than in vacuum. In humidified Argon, the critical Kmax level is reduced at 22 MPa{radical}m at 500 C, such a detrimental effect being related to a Stress Corrosion Cracking process induced by water vapor.« less

Creep, Fatigue and Fracture Behavior of Environmental Barrier Coating and SiC-SiC Ceramic Matrix Composite Systems: The Role of Environment Effects

NASA Technical Reports Server (NTRS)

Zhu, Dongming; Ghosn, Louis J.

2015-01-01

Advanced environmental barrier coating (EBC) systems for low emission SiCSiC CMC combustors and turbine airfoils have been developed to meet next generation engine emission and performance goals. This presentation will highlight the developments of NASAs current EBC system technologies for SiC-SiC ceramic matrix composite combustors and turbine airfoils, their performance evaluation and modeling progress towards improving the engine SiCSiC component temperature capability and long-term durability. Our emphasis has also been placed on the fundamental aspects of the EBC-CMC creep and fatigue behaviors, and their interactions with turbine engine oxidizing and moisture environments. The EBC-CMC environmental degradation and failure modes, under various simulated engine testing environments, in particular involving high heat flux, high pressure, high velocity combustion conditions, will be discussed aiming at quantifying the protective coating functions, performance and durability, and in conjunction with damage mechanics and fracture mechanics approaches.

Advances In High Temperature (Viscoelastoplastic) Material Modeling for Thermal Structural Analysis

NASA Technical Reports Server (NTRS)

Arnold, Steven M.; Saleeb, Atef F.

2005-01-01

Typical High Temperature Applications High Temperature Applications Demand High Performance Materials: 1) Complex Thermomechanical Loading; 2) Complex Material response requires Time-Dependent/Hereditary Models: Viscoelastic/Viscoplastic; and 3) Comprehensive Characterization (Tensile, Creep, Relaxation) for a variety of material systems.

Characterization of low temperature creep properties of crack sealants using bending beam rehometry.

DOT National Transportation Integrated Search

2009-11-01

Crack sealing has been widely used as a routine preventative maintenance practice. Given its proper installation, crack sealants can extend : pavement service life by three to five years. However, current specifications for the selection of crack sea...

Dislocation creep accommodated Grain Boundary Sliding: A high strain rate/low temperature deformation mechanism in calcite ultramylonites

NASA Astrophysics Data System (ADS)

Rogowitz, Anna; Grasemann, Bernhard

2014-05-01

Grain boundary sliding (GBS) is an important grain size sensitive deformation mechanism that is often associated with extreme strain localization and superplasticity. Another mechanism has to operate simultaneously to GBS in order to prevent overlaps and voids between sliding grains. One of the most common accommodating mechanisms is diffusional creep but, recently, dislocation creep has been reported to operate simultaneous to GBS. Due to the formation of a flanking structure in nearly pure calcite marble on Syros (Cyclades, Greece) at lower greenschist facies conditions, an extremely fine grained ultramylonite developed. The microstructure of the layer is characterized by (1) calcite grains with an average grain size of 3.6 µm (developed by low temperature/high strain rate grain boundary migration recrystallization, BLG), (2) grain boundary triple junctions with nearly 120° angles and (3) small cavities preferentially located at triple junctions and at grain boundaries in extension. These features suggest that the dominant deformation mechanism was GBS. In order to get more information on the accommodation mechanism detailed microstructural and textural analyses have been performed on a FEI Quanta 3D FEG instrument equipped with an EDAX Digiview IV EBSD camera. The misorientation distribution curves for correlated and uncorrelated grains follow almost perfect the calculated theoretical curve for a random distribution, which is typical for polycrystalline material deformed by GBS. However, the crystallographic preferred orientation indicates that dislocation creep might have operated simultaneously. We also report Zener-Stroh cracks resulting from dislocation pile up, indicating that dislocation movement was active. We, therefore, conclude that the dominant deformation mechanism was dislocation creep accommodated grain boundary sliding. This is consistent with the observed grain size range that plots at the field boundary between grain size insensitive and grain size sensitive creep, in a deformation mechanism map for calcite.

Creep and Creep-Fatigue Crack Growth at Structural Discontinuities and Welds

DOE Office of Scientific and Technical Information (OSTI.GOV)

Dr. F. W. Brust; Dr. G. M. Wilkowski; Dr. P. Krishnaswamy

2010-01-27

The subsection ASME NH high temperature design procedure does not admit crack-like defects into the structural components. The US NRC identified the lack of treatment of crack growth within NH as a limitation of the code and thus this effort was undertaken. This effort is broken into two parts. Part 1, summarized here, involved examining all high temperature creep-fatigue crack growth codes being used today and from these, the task objective was to choose a methodology that is appropriate for possible implementation within NH. The second part of this task, which has just started, is to develop design rules formore » possible implementation within NH. This second part is a challenge since all codes require step-by-step analysis procedures to be undertaken in order to assess the crack growth and life of the component. Simple rules for design do not exist in any code at present. The codes examined in this effort included R5, RCC-MR (A16), BS 7910, API 579, and ATK (and some lesser known codes). There are several reasons that the capability for assessing cracks in high temperature nuclear components is desirable. These include: (1) Some components that are part of GEN IV reactors may have geometries that have sharp corners - which are essentially cracks. Design of these components within the traditional ASME NH procedure is quite challenging. It is natural to ensure adequate life design by modeling these features as cracks within a creep-fatigue crack growth procedure. (2) Workmanship flaws in welds sometimes occur and are accepted in some ASME code sections. It can be convenient to consider these as flaws when making a design life assessment. (3) Non-destructive Evaluation (NDE) and inspection methods after fabrication are limited in the size of the crack or flaw that can be detected. It is often convenient to perform a life assessment using a flaw of a size that represents the maximum size that can elude detection. (4) Flaws that are observed using in-service detection methods often need to be addressed as plants age. Shutdown inspection intervals can only be designed using creep and creep-fatigue crack growth techniques. (5) The use of crack growth procedures can aid in examining the seriousness of creep damage in structural components. How cracks grow can be used to assess margins on components and lead to further safe operation. After examining the pros and cons of all these methods, the R5 code was chosen as the most up-to-date and validated high temperature creep and creep fatigue code currently used in the world at present. R5 is considered the leader because the code: (1) has well established and validated rules, (2) has a team of experts continually improving and updating it, (3) has software that can be used by designers, (4) extensive validation in many parts with available data from BE resources as well as input from Imperial college's database, and (5) was specifically developed for use in nuclear plants. R5 was specifically developed for use in gas cooled nuclear reactors which operate in the UK and much of the experience is based on materials and temperatures which are experienced in these reactors. If the next generation advanced reactors to be built in the US used these same materials within the same temperature ranges as these reactors, then R5 may be appropriate for consideration of direct implementation within ASME code NH or Section XI. However, until more verification and validation of these creep/fatigue crack growth rules for the specific materials and temperatures to be used in the GEN IV reactors is complete, ASME should consider delaying this implementation. With this in mind, it is this authors opinion that R5 methods are the best available for code use today. The focus of this work was to examine the literature for creep and creep-fatigue crack growth procedures that are well established in codes in other countries and choose a procedure to consider implementation into ASME NH. It is very important to recognize that all creep and creep fatigue crack growth procedures that are part of high temperature design codes are related and very similar. This effort made no attempt to develop a new creep-fatigue crack growth predictive methodology. Rather examination of current procedures was the only goal. The uncertainties in the R5 crack growth methods and recommendations for more work are summarized here also.« less

Characterization of the mechanical and physical properties of TD-NiCr (Ni-20Cr-2ThO2) alloy sheet

NASA Technical Reports Server (NTRS)

Fritz, L. J.; Koster, W. P.; Taylor, R. E.

1973-01-01

Sheets of TD-NiCr processed using techniques developed to produce uniform material were tested to supply mechanical and physical property data. Two heats each of 0.025 and 0.051 cm thick sheet were tested. Mechanical properties evaluated included tensile, modulus of elasticity, Poisson's Ratio, compression, creep-rupture, creep strength, bearing strength, shear strength, sharp notch and fatigue strength. Test temperatures covered the range from ambient to 1589K. Physical properties were also studied as a function of temperature. The physical properties measured were thermal conductivity, linear thermal expansion, specific heat, total hemispherical emittance, thermal diffusivity, and electrical conductivity.

Mechanical properties and XRD of Nafion modified by 2-hydroxyethylammonium ionic liquids

NASA Astrophysics Data System (ADS)

Garaev, V.; Pavlovica, S.; Reinholds, I.; Vaivars, G.

2013-12-01

In this work, the Nafion 112 membrane impregnated with 2-hydroxyethylammonium carboxylate ionic liquids have been investigated. The used ionic liquids were 2-hydroxyethylammonium formate [HEA]F, acetate [HEA]A and lactate [HEA]L. Prepared composite membranes Nafion/ionic liquid are characterized by mechanical testing, such as tensile test and creep test. It is found that ionic liquids decrease elastic modulus and creep compliance, but do not have significant effect on the tensile strength. Also, composite membranes were studied by wide angle X-ray diffraction. All ionic liquids shift the peak maximum to the lower angle. In this work, only biodegradable ionic liquids were used for composite preparation.

Mechanical Characterization of the Human Lumbar Intervertebral Disc Subjected to Impact Loading Conditions

NASA Astrophysics Data System (ADS)

Jamison, David, IV

Low back pain is a large and costly problem in the United States. Several working populations, such as miners, construction workers, forklift operators, and military personnel, have an increased risk and prevalence of low back pain compared to the general population. This is due to exposure to repeated, transient impact shocks, particularly while operating vehicles or other machinery. These shocks typically do not cause acute injury, but rather lead to pain and injury over time. The major focus in low back pain is often the intervertebral disc, due to its role as the major primary load-bearing component along the spinal column. The formation of a reliable standard for human lumbar disc exposure to repeated transient shock could potentially reduce injury risk for these working populations. The objective of this project, therefore, is to characterize the mechanical response of the lumbar intervertebral disc subjected to sub-traumatic impact loading conditions using both cadaveric and computational models, and to investigate the possible implications of this type of loading environment for low back pain. Axial, compressive impact loading events on Naval high speed boats were simulated in the laboratory and applied to human cadaveric specimen. Disc stiffness was higher and hysteresis was lower than quasi-static loading conditions. This indicates a shift in mechanical response when the disc is under impact loads and this behavior could be contributing to long-term back pain. Interstitial fluid loss and disc height changes were shown to affect disc impact mechanics in a creep study. Neutral zone increased, while energy dissipation and low-strain region stiffness decreased. This suggests that the disc has greater clinical instability during impact loading with progressive creep and fluid loss, indicating that time of day should be considered for working populations subjected to impact loads. A finite element model was developed and validated against cadaver specimen subjected to impacts in the laboratory. Analysis showed greater total von Mises stress and pore pressure in the components of the disc under transient shocks compared to static or quasi-static loading. These findings support the idea that impact shocks cause a change in mechanical response and are potentially damaging to the disc in the long term.

Magnetic evaluation of the external surface in cast heat-resistant steel tubes with different aging states

NASA Astrophysics Data System (ADS)

Arenas, Mónica P.; Silveira, Rosa M.; Pacheco, Clara J.; Bruno, Antonio C.; Araujo, Jefferson F. D. F.; Eckstein, Carlos B.; Nogueira, Laudemiro; de Almeida, Luiz H.; Rebello, João M. A.; Pereira, Gabriela R.

2018-06-01

Heat-resistant austenitic stainless steels have become the principal alloys for use in steam reformer tubes in the petrochemical industry due to its mechanical properties. These tubes are typically exposed to severe operational conditions leading to microstructural transformations such as the aging phenomenon. The combination of high temperatures and moderate stresses causes creep damages, being necessary to monitor its structural condition by non-destructive techniques. The tube external wall is also subjected to oxidizing atmospheres, favoring the formation of an external surface, composed by an oxide scale and a chromium depleted zone. This external surface is usually not taken into account in the tube evaluation, which can lead to erroneous estimations of the service life of these components. In order to observe the magnetic influence of this layer, two samples, exposed to different operational temperatures, were characterized by non-destructive eddy current testing (ECT), scanning DC-susceptometer and magnetic force microscopy (MFM). It was found that the external surface thickness influences directly in the magnetic response of the samples.

Creep deformation and rupture behavior of CLAM steel at 823 K and 873 K

NASA Astrophysics Data System (ADS)

Zhong, Boyu; Huang, Bo; Li, Chunjing; Liu, Shaojun; Xu, Gang; Zhao, Yanyun; Huang, Qunying

2014-12-01

China Low Activation Martensitic (CLAM) steel is selected as the candidate structural material in Fusion Design Study (FDS) series fusion reactor conceptual designs. The creep property of CLAM steel has been studied in this paper. Creep tests have been carried out at 823 K and 873 K over a stress range of 150-230 MPa. The creep curves showed three creep regimes, primary creep, steady-state creep and tertiary creep. The relationship between minimum creep rate (ε˙min) and the applied stress (σ) could be described by Norton power law, and the stress exponent n was decreased with the increase of the creep temperature. The creep mechanism was analyzed with the fractographes of the rupture specimens which were examined by scanning electron microscopy (SEM). The coarsening of precipitates observed with transmission electron microscope (TEM) indicated the microstructural degradation after creep test.

Ultra-High Temperature Materials Characterization for Propulsion Applications

NASA Technical Reports Server (NTRS)

Rogers, Jan; Hyers, Robert

2007-01-01

Propulsion system efficiency increases as operating temperatures are increased. Some very high-temperature materials are being developed, including refractory metal alloys, carbides, borides, and silicides. System design requires data for materials properties at operating temperatures. Materials property data are not available for many materials of interest at the desired operating temperatures (up to approx. 3000 K). The objective of this work is to provide important physical property data at ultra-high temperatures. The MSFC Electrostatic levitation (ESL) facility can provide measurements of thermophysical properties which include: creep strength, density and thermal expansion for materials being developed for propulsion applications. The ESL facility uses electrostatic fields to position samples between electrodes during processing and characterization studies. Because the samples float between the electrodes during studies, they are free from any contact with a container or test apparatus. This provides a high purity environment for the study of high-temperature, reactive materials. ESL can be used to process a wide variety of materials including metals, alloys, ceramics, glasses and semiconductors. The MSFC ESL has provided non-contact measurements of properties of materials up to 3400 C. Density and thermal expansion are measured by analyzing digital images of the sample at different temperatures. Our novel, non-contact method for measuring creep uses rapid rotation to deform the sample. Digital images of the deformed samples are analyzed to obtain the creep properties, which match those obtained using ASTM Standard E-139 for Nb at 1985 C. Data from selected ESL-based characterization studies will be presented. The ESL technique could support numerous propulsion technologies by advancing the knowledge base and the technology readiness level for ultra-high temperature materials. Applications include non-eroding nozzle materials and lightweight, high-temperature alloys for turbines and structures.

Damage Accumulation in Advanced Metal Matrix Composites Under Thermal Cycling/Creep Loadings

DTIC Science & Technology

1993-09-01

34transformation strain" (Eshelby, 1957) or * eigenstrain " (Mura, 1987). The stress-strain relation of a ccmposite predicted by the Tanaka-Mori model is given by a0o...a short fiber MMC can be calculated if the following eigenstrains are given in the domains of fiber (0l) and of the punched region encompassing the...and Mortenson modified the above model to account for partial relaxation by dislocation punching along the fiber axis. The eigenstrains based on this

Contemporary overview of soil creep phenomenon

NASA Astrophysics Data System (ADS)

Kaczmarek, Łukasz; Dobak, Paweł

2017-06-01

Soil creep deformation refers to phenomena which take place in many areas and research in this field of science is rich and constantly developing. The article presents an analysis of the literature on soil creep phenomena. In light of the complexity of the issues involved and the wide variety of perspectives taken, this attempt at systematization seeks to provide a reliable review of current theories and practical approaches concerning creep deformation. The paper deals with subjects such as definition of creep, creep genesis, basic description of soil creep dynamics deformation, estimation of creep capabilities, various fields of creep occurrence, and an introduction to creep modeling. Furthermore, based on this analysis, a new direction for research is proposed.

The Hollin Hill Landslide Observatory - a decade of geophysical characterization and monitoring

NASA Astrophysics Data System (ADS)

Uhlemann, S.; Wilkinson, P. B.; Meldrum, P.; Smith, A.; Dixon, N.; Merritt, A.; Swift, R. T.; Whiteley, J.; Gunn, D.; Chambers, J. E.

2017-12-01

Landslides are major and frequent natural hazards. They shape the Earth's surface, and endanger communities and infrastructure worldwide. Within the last decade, landslides caused more than 28,000 fatalities and direct damage exceeding $1.8 billion. Climate change, causing more frequent weather extremes, is likely to increase occurrences of shallow slope failures worldwide. Thus, there is a need to improve our understanding of these shallow, rainfall-induced landslides. In this context, integrated geophysical characterization and monitoring can play a crucial role by providing volumetric data that can be linked to the hydrological and geotechnical conditions of a slope. This enables understanding of the complex hydrological processes most-often being associated with landslides. Here we present a review of a decade of characterizing and monitoring a complex, inland, clayey landslide - forming the "Hollin Hill Landslide Observatory". Within the last decade, this landslide has experienced different activity characteristics, including creep, flow, and rotational failures - thereby providing an excellent testbed for the development of geophysical and geotechnical monitoring instrumentation and methodologies. These include developments of 4D geoelectrical monitoring techniques to estimate electrode positions from the resistivity data, incorporating these into a time-lapse inversion, and imaging moisture dynamics that control the landslide behaviour. Other developments include acoustic emission monitoring, and active and passive seismic monitoring. This work is underpinned by detailed characterization of the landslide, using geomorphological and geological mapping, geotechnical investigations, and a thorough geoelectrical and seismic characterization of the landslide mass. Hence, the data gained from the Hollin Hill landslide observatory has improved our understanding of the shallow landslide dynamics in response to climate change, their mechanics and evolution. The methodological and technical developments achieved at this site are suitable and applicable for implementation on other landslides worldwide.

Time-Dependent Behavior of Diabase and a Nonlinear Creep Model

NASA Astrophysics Data System (ADS)

Yang, Wendong; Zhang, Qiangyong; Li, Shucai; Wang, Shugang

2014-07-01

Triaxial creep tests were performed on diabase specimens from the dam foundation of the Dagangshan hydropower station, and the typical characteristics of creep curves were analyzed. Based on the test results under different stress levels, a new nonlinear visco-elasto-plastic creep model with creep threshold and long-term strength was proposed by connecting an instantaneous elastic Hooke body, a visco-elasto-plastic Schiffman body, and a nonlinear visco-plastic body in series mode. By introducing the nonlinear visco-plastic component, this creep model can describe the typical creep behavior, which includes the primary creep stage, the secondary creep stage, and the tertiary creep stage. Three-dimensional creep equations under constant stress conditions were deduced. The yield approach index (YAI) was used as the criterion for the piecewise creep function to resolve the difficulty in determining the creep threshold value and the long-term strength. The expression of the visco-plastic component was derived in detail and the three-dimensional central difference form was given. An example was used to verify the credibility of the model. The creep parameters were identified, and the calculated curves were in good agreement with the experimental curves, indicating that the model is capable of replicating the physical processes.

Compilation of Surface Creep on California Faults and Comparison of WGCEP 2007 Deformation Model to Pacific-North American Plate Motion

USGS Publications Warehouse

Wisely, Beth A.; Schmidt, David A.; Weldon, Ray J.

2008-01-01

This Appendix contains 3 sections that 1) documents published observations of surface creep on California faults, 2) constructs line integrals across the WG-07 deformation model to compare to the Pacific ? North America plate motion, and 3) constructs strain tensors of volumes across the WG-07 deformation model to compare to the Pacific ? North America plate motion. Observation of creep on faults is a critical part of our earthquake rupture model because if a fault is observed to creep the moment released as earthquakes is reduced from what would be inferred directly from the fault?s slip rate. There is considerable debate about how representative creep measured at the surface during a short time period is of the whole fault surface through the entire seismic cycle (e.g. Hudnut and Clark, 1989). Observationally, it is clear that the amount of creep varies spatially and temporally on a fault. However, from a practical point of view a single creep rate is associated with a fault section and the reduction in seismic moment generated by the fault is accommodated in seismic hazard models by reducing the surface area that generates earthquakes or by reducing the slip rate that is converted into seismic energy. WG-07 decided to follow the practice of past Working Groups and the National Seismic Hazard Map and used creep rate (where it was judged to be interseismic, see Table P1) to reduce the area of the fault surface that generates seismic events. In addition to following past practice, this decision allowed the Working Group to use a reduction of slip rate as a separate factor to accommodate aftershocks, post seismic slip, possible aseismic permanent deformation along fault zones and other processes that are inferred to affect the entire surface area of a fault, and thus are better modeled as a reduction in slip rate. C-zones are also handled by a reduction in slip rate, because they are inferred to include regions of widely distributed shear that is not completely expressed as earthquakes large enough to model. Because the ratio of the rate of creep relative to the total slip rate is often used to infer the average depth of creep, the ?depth? of creep can be calculated and used to reduce the surface area of a fault that generates earthquakes in our model. This reduction of surface area of rupture is described by an ?aseismicity factor,? assigned to each creeping fault in Appendix A. An aseismicity factor of less than 1 is only assigned to faults that are inferred to creep during the entire interseismic period. A single aseismicity factor was chosen for each section of the fault that creeps by expert opinion from the observations documented here. Uncertainties were not determined for the aseismicity factor, and thus it represents an unmodeled (and difficult to model) source of error. This Appendix simply provides the documentation of known creep, the type and precision of its measurement, and attempts to characterize the creep as interseismic, afterslip, transient or triggered. Parts 2 and 3 of this Appendix compare the WG-07 deformation model and the seismic source model it generates to the strain generated by the Pacific - North American plate motion. The concept is that plate motion generates essentially all of the elastic strain in the vicinity of the plate boundary that can be released as earthquakes. Adding up the slip rates on faults and all others sources of deformation (such as C-zones and distributed ?background? seismicity) should approximately yield the plate motion. This addition is usually accomplished by one of four approaches: 1) line integrals that sum deformation along discrete paths through the deforming zone between the two plates, 2) seismic moment tensors that add up seismic moment of a representative set of earthquakes generated by a crustal volume spanning the plate boundary, 3) strain tensors generated by adding up the strain associated with all of the faults in a crustal volume spanning the plate

CHARACTERIZATION OF AGROSTIS SPP. HABITAT IN CENTRAL OREGON

EPA Science Inventory

Creeping bentgrass, Agrostis stolonifera L., is a non-native grass commonly found at mesic sites in central Oregon. Interest in A. stolonifera plant communities and the factors that may control its distribution has increased since field trials of A. stolonifera ...