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Sample records for fusrap middlesex sampling

  1. Middlesex Sampling Plant environmental report for calendar year 1992, 239 Mountain Avenue, Middlesex, New Jersey. Formerly Utilized Sites Remedial Action Program (FUSRAP)

    SciTech Connect

    Not Available

    1993-05-01

    This report describes the environmental surveillance program at the Middlesex Sampling Plant (MSP) and provides the results for 1992. The site, in the Borough of Middlesex, New Jersey, is a fenced area and includes four buildings and two storage piles that contain 50,800 m{sup 3} of radioactive and mixed hazardous waste. More than 70 percent of the MSP site is paved with asphalt. The MSP facility was established in 1943 by the Manhattan Engineer District (MED) to sample, store, and/or ship uranium, thorium, and beryllium ores. In 1955 the Atomic Energy Commission (AEC), successor to MED, terminated the operation and later used the site for storage and limited sampling of thorium residues. In 1967 AEC activities ceased, onsite structures were decontaminated, and the site was certified for unrestricted use under criteria applicable at that time. In 1980 the US Department of Energy (DOE) initiated a multiphase remedial action project to clean up several vicinity properties onto which contamination from the plant had migrated. Material from these properties was consolidated into the storage piles onsite. Environmental surveillance of MSP began in 1980 when Congress added the site to DOE`s Formerly Utilized Sites Remedial Action Program. The environmental surveillance program at MSP includes sampling networks for radon and thoron in air; external gamma radiation exposure; and radium-226, radium-228, thorium-230, thorium-232, and total uranium in surface water, sediment, and groundwater. Additionally, chemical analyses are performed to detect metals and organic compounds in surface water and groundwater and metals in sediments. This program assists in fulfilling th DOE policy of measuring and monitoring effluents from DOE activities and calculating hypothetical doses.

  2. Middlesex FUSRAP Site - A Path to Site-Wide Closure - 13416

    SciTech Connect

    Miller, David M.; Edge, Helen

    2013-07-01

    The road-map to obtaining closure of the Middlesex Sampling Plant FUSRAP site in Middlesex, New Jersey (NJ) has required a multi-faceted approach, following the CERCLA Process. Since 1998, the US ACE, ECC, and other contractors have completed much of the work required for regulatory acceptance of site closure with unrestricted use. To date, three buildings have been decontaminated, demolished, and disposed of. Two interim storage piles have been removed and disposed of, followed by the additional removal and disposal of over 87,000 tons of radiologically and chemically-impacted subsurface soils by the summer of 2008. The US ACE received a determination from the EPA for the soils Operable Unit, (OU)-1, in September 2010 that the remedial excavations were acceptable, and meet the criteria for unrestricted use as required by the 2004 Record of Decision (ROD) for OU-1. Following the completion of OU-1, the project delivery team performed additional field investigation of the final Operable Unit for Middlesex, OU-2, Groundwater. As of December 2012, the project delivery team has completed a Supplemental Remedial Investigation, which will be followed with a streamlined Feasibility Study, Proposed Plan, and ROD. Several years of historical groundwater data was available from previous investigations and the FUSRAP Environmental Surveillance Program. Historical data indicated sporadic detections of Volatile Organic Compounds (VOCs), primarily trichloroethylene (TCE), carbon tetrachloride (CT), and methyl tert-butyl ether (MTBE), with no apparent trend or pattern indicating extent or source of the VOC impact. In 2008, the project delivery team initiated efforts to re-assess the Conceptual Site Model (CSM) for groundwater. The bedrock was re-evaluated as a leaky multi-unit aquifer, and a plan was developed for additional investigations for adequate bedrock characterization and delineation of groundwater contaminated primarily by CT, TCE, and tetrachloroethene (PCE). The

  3. Middlesex Sampling Plant environmental report for calendar year 1989, Middlesex, New Jersey

    SciTech Connect

    Not Available

    1990-05-01

    The environmental monitoring program, which began in 1980, was continued in 1989 at the former Middlesex Sampling Plant (MSP) site, located in the Borough of Middlesex, New Jersey. The MSP site is part of the Formerly Utilized Sites Remedial Action Program (FUSRAP), a Department of Energy (DOE) program to decontaminate or otherwise control sites where residual radioactive materials remain either from the early years of the nation's atomic energy program or from commercial operations causing conditions that Congress has authorized DOE to remedy. The monitoring program at MSP measures radon concentrations in air; external gamma radiation levels; and uranium and radium concentrations in surface water, groundwater, and sediment. Additionally, several nonradiological parameters are measured in groundwater samples. To verify that the site is in compliance with the DOE radiation protection standard (100 mrem/yr) and to assess its potential effect on public health, the radiation dose was calculated for a hypothetical maximally exposed individual. This report presents the findings of the environmental monitoring program conducted in the area of the Middlesex Sampling Plant (MSP) site during calendar year 1989. 17 refs., 16 figs., 16 tabs.

  4. Reducing Contingency through Sampling at the Luckey FUSRAP Site - 13186

    SciTech Connect

    Frothingham, David; Barker, Michelle; Buechi, Steve; Durham, Lisa

    2013-07-01

    Typically, the greatest risk in developing accurate cost estimates for the remediation of hazardous, toxic, and radioactive waste sites is the uncertainty in the estimated volume of contaminated media requiring remediation. Efforts to address this risk in the remediation cost estimate can result in large cost contingencies that are often considered unacceptable when budgeting for site cleanups. Such was the case for the Luckey Formerly Utilized Sites Remedial Action Program (FUSRAP) site near Luckey, Ohio, which had significant uncertainty surrounding the estimated volume of site soils contaminated with radium, uranium, thorium, beryllium, and lead. Funding provided by the American Recovery and Reinvestment Act (ARRA) allowed the U.S. Army Corps of Engineers (USACE) to conduct additional environmental sampling and analysis at the Luckey Site between November 2009 and April 2010, with the objective to further delineate the horizontal and vertical extent of contaminated soils in order to reduce the uncertainty in the soil volume estimate. Investigative work included radiological, geophysical, and topographic field surveys, subsurface borings, and soil sampling. Results from the investigative sampling were used in conjunction with Argonne National Laboratory's Bayesian Approaches for Adaptive Spatial Sampling (BAASS) software to update the contaminated soil volume estimate for the site. This updated volume estimate was then used to update the project cost-to-complete estimate using the USACE Cost and Schedule Risk Analysis process, which develops cost contingencies based on project risks. An investment of $1.1 M of ARRA funds for additional investigative work resulted in a reduction of 135,000 in-situ cubic meters (177,000 in-situ cubic yards) in the estimated base volume estimate. This refinement of the estimated soil volume resulted in a $64.3 M reduction in the estimated project cost-to-complete, through a reduction in the uncertainty in the contaminated soil

  5. Ocean FUSRAP: feasibility of ocean disposal of materials from the Formerly Utilized Sites Remedial Action Progam (FUSRAP)

    SciTech Connect

    Kupferman, S.L.; Anderson, D.R.; Brush, L.H.; Gomez, L.S.; Laul, J.C.; Shephard, L.E.

    1982-01-01

    The Formerly Utilized Sites Remedial Action Program (FUSRAP) of the Department of Energy is designed to identify and evaluate the radiological conditions at sites formerly used by the Corps of Engineers Manhattan Engineer District and the US Atomic Energy Commission. Where required, remedial action will be instituted to remove potential restrictions on the use of the sites due to residual low-level radioactive contamination. A total of 31 sites that may require remedial action has been identified. The purpose of the Ocean FUSRAP Program, which began in March 1981, is to assess the technical, environmental, and institutional feasibility of disposing, in the ocean and on the ocean floor, of FUSRAP soil and rubble which contains traces of natural radioactive materials. The initial focus has been on the Middlesex, New Jersey, Sampling Plant site and surrounding properties, which contain on the order of 100,000 metric tons of material. The Belgian Congo uranium ore and other uranium ores used by the United States were handled at the sampling plant site. In studying the feasibility of ocean disposal of FUSRAP material from Middlesex, New Jersey, we have begun to examine institutional requirements to be met, the composition of the source material with regard to its inventory of toxic chemical and radiochemical components and the impact of the source material in the marine environment. To date we have found nothing that would preclude safe and inexpensive disposal of this material in the ocean.

  6. Lessons Learned from FUSRAP

    SciTech Connect

    Castillo, Darina; Carpenter, Cliff; Miller, Michele

    2016-03-06

    The US DOE Office of Legacy Management (LM) is the long-term steward for 90 sites remediated under numerous regulatory regimes including the Formerly Utilized Sites Remedial Action Program (FUSRAP) sites. In addition, LM holds considerable historical information, gathered in the 1970s, to determine site eligibility for remediation under FUSRAP. To date, 29 FUSRAP sites are in LM’s inventory of sites for long-term surveillance and maintenance (LTS&M), and 25 are with the US Army Corps of Engineers (USACE) for remediation or in the process of being transitioned to LM. It is forecasted that 13 FUSRAP sites will transfer from the USACE to LM over the next 10 years; however, the timing of the transfers is strongly dependent upon federal funding of the ongoing remedial actions. Historically, FUSRAP sites were generally cleaned up for “unrestricted” industrial use or remediated to the “cleanup standards” at that time, and their use remained unchanged. Today, these sites as well as the adjacent properties are now changing or envisioned to have changes in land use, typically from industrial to commercial or residential uses. The implication of land-use change affects DOE’s LTS&M responsibility for the sites under LM stewardship as well as the planning for the additional sites scheduled to transition in time. Coinciding with land-use changes at or near FUSRAP sites is an increased community awareness of these sites. As property development increases near FUSRAP sites, the general public and interested stakeholders regularly inquire about the sufficiency of cleanups that impact their neighborhoods and communities. LM has used this experience to address a series of lessons learned to improve our program management in light of the changing conditions of our sites. We describe these lessons learned as (1) improved stakeholder relations, (2) enhanced LTS&M requirements for the sites, and (3) greater involvement in the transition process.

  7. St. Louis FUSRAP Lessons Learned

    SciTech Connect

    Eberlin, J.; Williams, D.; Mueller, D.

    2003-02-26

    The purpose of this paper is to present lessons learned from fours years' experience conducting Remedial Investigation and Remedial Action activities at the St. Louis Downtown Site (SLDS) under the Formerly Utilized Sites Remedial Action Program (FUSRAP). Many FUSRAP sites are experiencing challenges conducting Remedial Actions within forecasted volume and budget estimates. The St. Louis FUSRAP lessons learned provide insight to options for cost effective remediation at FUSRAP sites. The lessons learned are focused on project planning (budget and schedule), investigation, design, and construction.

  8. Middlesex Community College Geothermal Project

    SciTech Connect

    Klein, Jessie; Spaziani, Gina

    2013-03-29

    The purpose of the project was to install a geothermal system in the trustees house on the Bedford campus of Middlesex Community College. In partnership with the environmental science faculty, learning activities for environmental science courses were developed to explain geothermal energy and more specifically the newly installed system to Middlesex students. A real-time monitoring system highlights the energy use and generation.

  9. Geologic report, Middlesex Municipal Landfill site, Middlesex, New Jersey

    SciTech Connect

    Not Available

    1984-03-01

    This is a report on geologic and hydrologic investigations of the former Municipal Landfill, Middlesex, New Jersey, conducted during 1982 and 1983 by Bechtel National, Inc. for the United States Department of Energy, Oak Ridge Operations Office. The investigations were designed to assess the feasibility of stabilizing the radioactive contamination present on site. The investigations were conducted in two phases: Phase 1 consisted of permeability tests; Phase 2 consisted of tests to ascertain the extent of hydraulic interconnection between various stratigraphic units. The investigations revealed that a complete separation of bedrock and overburden did not exist and that the clay present could not be relied upon to confine vertical migration of contaminants over the long term. 6 references, 27 figures, 6 tables.

  10. Is Middlesex County College Accomplishing Its Mission?

    ERIC Educational Resources Information Center

    Balabkins, Xenia P.

    Over the past few years, New Jersey's Middlesex County College (MCC) has placed an inordinate amount of attention and effort on the issue of student transfer to four-year institutions. Although attention to traditional academic goals is important, MCC's stated mission also addresses other important segments of the college's market. The college has…

  11. Introducing RFID at Middlesex University Learning Resources

    ERIC Educational Resources Information Center

    Hopkinson, Alan; Chandrakar, Rajesh

    2006-01-01

    Purpose: To describe the first year of the implementation of radio frequency identification (RFID) in Middlesex University Learning Resources. Design/methodology/approach: The technology is explained in detail to set the scene. Information on the implementation is presented in chronological order. Findings: Problems which would generally be…

  12. Middlesex Community College Software Technical Writing Program.

    ERIC Educational Resources Information Center

    Middlesex Community Coll., Bedford, MA.

    This document describes the Software Technical Writing Program at Middlesex Community College (Massachusetts). The program is a "hands-on" course designed to develop job-related skills in three major areas: technical writing, software, and professional skills. The program was originally designed in cooperation with the Massachusetts High…

  13. Crushing leads to waste disposal savings for FUSRAP

    SciTech Connect

    Darby, J.

    1997-02-01

    In this article the author discusses the application of a rock crusher as a means of implementing cost savings in the remediation of FUSRAP sites. Transportation and offsite disposal costs are at present the biggest cost items in the remediation of FUSRAP sites. If these debris disposal problems can be handled in different manners, then remediation savings are available. Crushing can result in the ability to handle some wastes as soil disposal problems, which have different disposal regulations, thereby permitting cost savings.

  14. Remediation and Recycling of Linde FUSRAP Materials

    SciTech Connect

    Coutts, P. W.; Franz, J. P.; Rehmann, M. R.

    2002-02-27

    During World War II, the Manhattan Engineering District (MED) utilized facilities in the Buffalo, New York area to extract natural uranium from uranium-bearing ores. The Linde property is one of several properties within the Tonawanda, New York Formerly Utilized Sites Remedial Action Program (FUSRAP) site, which includes Linde, Ashland 1, Ashland 2, and Seaway. Union Carbide Corporation's Linde Division was placed under contract with the Manhattan Engineering District (MED) from 1942 to 1946 to extract uranium from seven different ore sources: four African pitchblende ores and three domestic ores. Over the years, erosion and weathering have spread contamination from the residuals handled and disposed of at Linde to adjacent soils. The U.S. Department of Energy (DOE) and the U.S. Environmental Protection Agency (EPA) negotiated a Federal Facilities Agreement (FFA) governing remediation of the Linde property. In Fiscal Year (FY) 1998, Congress transferred cleanup management responsibility for the sites in the FUSRAP program, including the Linde Site, from the DOE to the U.S. Army Corps of Engineers (USACE), with the charge to commence cleanup promptly. All actions by the USACE at the Linde Site are being conducted subject to the administrative, procedural, and regulatory provisions of the Comprehensive Environmental Response Compensation and Liability Act (CERCLA) and the existing FFA. USACE issued a Proposed Plan for the Linde Property in 1999 and a Final Record of Decision (ROD) in 2000. USACE worked with the local community near the Tonawanda site, and after considering public comment, selected the remedy calling for removing soils that exceed the site-specific cleanup standard, and transporting the contaminated material to off-site locations. The selected remedy is protective of human health and the environment, complies with Federal and State requirements, and meets commitments to the community.

  15. 7. RARITAN AVENUE BRIDGE. NEW BRUNSWICK, MIDDLESEX CO., NJ. Sec. ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    7. RARITAN AVENUE BRIDGE. NEW BRUNSWICK, MIDDLESEX CO., NJ. Sec. 1401, MP 30.92. - Northeast Railroad Corridor, Amtrak Route between Pennsylvania/New Jersey & New Jersey/New York State Lines, Newark, Essex County, NJ

  16. 8. Raritan River Bridge. New Brunswick, Middlesex Co., NJ. Sec. ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    8. Raritan River Bridge. New Brunswick, Middlesex Co., NJ. Sec. 1401, MP 30.92. - Northeast Railroad Corridor, Amtrak Route between Pennsylvania/New Jersey & New Jersey/New York State Lines, Newark, Essex County, NJ

  17. 9. Raritan River Bridge. New Brunswick, Middlesex Co., NJ. Sec. ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    9. Raritan River Bridge. New Brunswick, Middlesex Co., NJ. Sec. 1401, MP 30.92. - Northeast Railroad Corridor, Amtrak Route between Pennsylvania/New Jersey & New Jersey/New York State Lines, Newark, Essex County, NJ

  18. 6. RARITAN AVENUE BRIDGE. NEW BRUNSWICK, MIDDLESEX CO., NJ. Sec. ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    6. RARITAN AVENUE BRIDGE. NEW BRUNSWICK, MIDDLESEX CO., NJ. Sec. 1401, MP 30.92 - Northeast Railroad Corridor, Amtrak Route between Pennsylvania/New Jersey & New Jersey/New York State Lines, Newark, Essex County, NJ

  19. Development of Preliminary Remediation Goals for Indoor Dust at the Colonie FUSRAP Site - 12273

    SciTech Connect

    Watters, David J.; Opdyke, Clifford P.; Moore, James T.

    2012-07-01

    The Colonie FUSRAP Site is located in the Town of Colonie, Albany County, New York. The U.S. Army Corps of Engineers is currently addressing environmental contamination associated with the Site under the Comprehensive Environmental Response, Compensation and Liability Act (CERCLA) process as part of the Formerly Utilized Sites Remedial Action Program (FUSRAP). Soil remediation activities have been substantially completed at the Colonie FUSRAP Site and its vicinity properties under the FUSRAP. A study unrelated to FUSRAP was recently performed by an independent party to establish the distribution of DU contamination in various media in the environs of the Site. As part of this study, dust samples were collected in residencies and businesses in the immediate vicinity of the Site. These samples were collected in non-living areas such as basement window sills and garages. Many of these samples tested positive for DU. An assessment was performed to establish preliminary remediation goals (PRGs) for indoor dust in non-living areas of residential homes and businesses in the vicinity of the Site. The results of this assessment provide estimates of dose-based, carcinogenic risk-based, and noncarcinogenic-based PRGs derived from a hypothetical exposure scenario with reasonable levels of conservatism. Ultimately, the PRGs will be compared to results of dust sampling and analyses in residences and businesses in proximity of the Site to determine whether a response action is appropriate. This assessment estimates PRGs for DU contaminated dust in non-living areas of residences in the vicinity of the Colonie FUSRAP site based on a reasonably conservative exposure scenario. Estimated PRGs based on residential receptors are considered to be conservatively representative of workers in nearby businesses based on the considerably longer exposure duration of residents relative to workers. This assessment provides reasonably conservative estimates of PRGs for DU contaminated dust in non

  20. Lessons Learned from a Complex FUSRAP Site - Sylvania Corning FUSRAP Site - 12269

    SciTech Connect

    Ewy, Ann; Hays, David

    2012-07-01

    Since its addition to the Formerly Utilized Sites Remedial Action Program (FUSRAP) in 2005, the Sylvania Corning FUSRAP Site (the Site) in Hicksville, New York, has provided challenges and opportunities from which to gain lessons learned for conducting investigation work at a complex multi-contaminant FUSRAP Site. The United States Army Corps of Engineers (USACE) and its contractors conducted a Comprehensive Environmental Response, Compensation and Liability Act (CERCLA) Remedial Investigation (RI) and are currently in the Feasibility Study (FS) phase at the Site. This paper presents the planning, execution, and reporting lessons learned by USACE during the RI/FS. The Site, operated from 1952 to 1967 for the research, development, and fabrication of nuclear elements under the Atomic Energy Commission, and other government and commercial contracts. Previous investigations performed by the New York State Department of Environmental Conservation (NYSDEC) and the current property owner have identified uranium, thorium, nickel, and chlorinated solvents, as Site contaminants [1]. The property owner is currently under two separate voluntary agreements with NYSDEC to investigate and remediate the Site. USACE's work at the site has been independent of this voluntary agreement and has moved on a parallel path with any work the property owner has completed. The project at the Site is complex because of the radiological and chemical concerns in both soils and groundwater, high hydraulically conductive soils, lack of a shallow aquiclude/aquitard, and a principal water table aquifer underlying the site. Contaminants are migrating from the Site and may potentially impact local drinking water supplies (municipal wells). During the RI/FS process the project team has encountered many issues and has thus developed many resolutions. The issues are organized into three categories: Planning and Contracting, Execution, and Reporting. Planning and Contracting lessons learned include: how

  1. St. Louis FUSRAP-A Strategy for Success

    SciTech Connect

    Lyerla, M.; Fox, B.; Chinnock, J.; Haase, A.; Wojinski, S.; Bretz, M.; Cotner, S.; Dellorco, L.; Mueller, D.; Roberts, S.; Overmohle, D.

    2002-02-27

    In October 1997, Congress transferred the Formerly Utilized Sites Remedial Action Program (FUSRAP) from the Department of Energy (DOE) to the United States Army Corps of Engineers (USACE). FUSRAP addresses contamination generated by activities of the Manhattan Engineering District and the Atomic Energy Commission during the 1940's and 50's in support of the nation's nuclear weapons development program. The USACE Operation Order for FUSRAP gave responsibility for remediation of five sites in Missouri and Illinois to the USACESt. Louis District. The principal site is the St. Louis Airport Site (SLAPS), which involves the removal, transportation, disposal, and restoration of approximately 28 acres and 245,000 bank cubic yards (bcy) of contaminated soils. This paper will focus on the progress and achievements in removal action efficiencies of the SLAPS team. This team consists primarily of the USACE and Stone & Webster, Incorporated.

  2. Radiological surveys of properties in the Middlesex, New Jersey area. Final report

    SciTech Connect

    Leggett, R W; Haywood, F.F. Cottrell, W.D.

    1981-03-01

    Results of the radiological surveys conducted at three properties in the Middlesex, New Jersey area as well as one additional location downstream from the Middlesex Sampling Plant (Willow Lake), are presented. The survey revealed that the yard around the church rectory on Harris Avenue is contaminated with a /sup 226/Ra-bearing material, probably pitchblende ore from the former Middlesex Sampling Plant. The elevated /sup 226/Ra concentrations around and, to a lesser extent, underneath the rectory are leading to elevated /sup 222/Rn concentrations in air in the rectory and elevated alpha contamination levels (from radon daughters) on surfaces inside the rectory. External gamma radiation levels in the rectory yard are well above background levels, and beta-gamma dose rates at many points in the yard are above federal guidelines for the release of property for unrestricted use. The radiological survey of a parking lot at the Union Carbide plant in Bound Brook, New Jersey revealed that a nearly circular region of 50-ft diam in the lot showed above-background external gamma radiation levels. Two isolated spots within this region showed concentrations of uranium in soil above the licensable level stated in 10 CFR 40. Soil samples taken in the area of elevated gamma radiation levels generally showed nearly equal activities of /sup 226/Ra and /sup 238/U. The survey at the residences on William Street in Piscataway, revealed that the front yeard is generally contaminated from near the surface to a depth of 1.5 to 2.5 ft with /sup 226/Ra-bearing material, possibly pitchblende ore. The remainder of the yard shows scattered contaminaion. External gamma radiation levels inside the house are above the background level near some outside walls.

  3. Challenging Texts: How Teaching "Middlesex" Challenged Students' Paradigms

    ERIC Educational Resources Information Center

    Vanderburg, Robert

    2009-01-01

    "Middlesex" is a book about undiagnosed hermaphrodite coming to terms with his/her socially determined sexuality and his/her choice of sexuality. The protagonist and narrator of the novel, Calliope Stephanides, is raised as a girl because he/she presented feminine genitalia at birth. When Calliope realizes he/she is a hermaphrodite--a realization…

  4. Uptake by plants of radionuclides from FUSRAP waste materials

    SciTech Connect

    Knight, M.J.

    1983-04-01

    Radionuclides from FUSRAP wastes potentially may be taken up by plants during remedial action activities and permanent near-surface burial of contaminated materials. In order to better understand the propensity of radionuclides to accumulate in plant tissue, soil and plant factors influencing the uptake and accumulation of radionuclides by plants are reviewed. In addition, data describing the uptake of the principal radionuclides present in FUSRAP wastes (uranium-238, thorium-230, radium-226, lead-210, and polonium-210) are summarized. All five radionuclides can accumulate in plant root tissue to some extent, and there is potential for the translocation and accumulation of these radionuclides in plant shoot tissue. Of these five radionuclides, radium-226 appears to have the greatest potential for translocation and accumulation in plant shoot tissue. 28 references, 1 figure, 3 tables.

  5. Utilizing Isotopic Uranium Ratios in Groundwater Evaluations at FUSRAP Sites

    SciTech Connect

    Frederick, W.T.; Keil, K.G.; Rhodes, M.C.; Peterson, J.M.; MacDonell, M.M.

    2007-07-01

    The U.S. Army Corps of Engineers Buffalo District is evaluating environmental radioactive contamination at several Formerly Utilized Sites Remedial Action Program (FUSRAP) sites throughout New York, Pennsylvania, Ohio, and Indiana. The investigations follow the process defined in the Comprehensive Environmental Response, Compensation and Liability Act (CERCLA). Groundwater data from the Niagara Falls Storage Site (NFSS) in Lewiston, New York were evaluated for isotopic uranium ratios, specifically uranium-234 versus uranium-238 (U- 234 and U-238, respectively), and the results were presented at Waste Management 2006. Since uranium naturally occurs in all groundwater, it can be difficult to distinguish where low-concentration impacts from past releases differ from the high end of a site-specific natural background range. In natural groundwater, the ratio of U-234 to U-238 exceeds 1 (unity) due to the alpha particle recoil effect, in which U-234 is preferentially mobilized to groundwater from adjacent rock or soil. This process is very slow and may take hundreds to thousands of years before a measurable increase is seen in the natural isotopic ratio. If site releases are the source of uranium being measured in groundwater, the U-234 to U-238 ratio is commonly closer to 1, which normally reflects FUSRAP-related, uranium-contaminated wastes and soils. This lower ratio occurs because not enough residence time has elapsed since the 1940's and 1950's for the alpha particle recoil effect to have significantly altered the contamination-derived ratio. An evaluation of NFSS-specific and regional groundwater data indicate that an isotopic ratio of 1.2 has been identified as a signature value to help distinguish natural groundwater, which may have a broad background range, from zones impacted by past releases. (authors)

  6. Successful Implementation of Soil Segregation Technology at the Painesville FUSRAP Site - 12281

    SciTech Connect

    Buechi, Stephen P.; Andrews, Shawn M.; Lombardo, Andrew J.; Lively, Jeffrey W.

    2012-07-01

    Typically the highest cost component of the radiological soils remediation of Formerly Utilized Sites Remedial Action Program (FUSRAP) sites is the cost to transport and dispose of the excavated soils, typically contaminated with naturally occurring isotopes of uranium, thorium and radium, at an appropriately permitted off-site disposal facility. The heterogeneous nature of the contamination encountered at these sites makes it difficult to accurately delineate the extent of contaminated soil using the limited, discrete sampling data collected during the investigation phases; and difficult to precisely excavate only the contaminated soil that is above the established cleanup limits using standard in-field scanning and guiding methodologies. This usually results in a conservative guided excavation to ensure cleanup criteria are met, with the attendant transportation and disposal costs for the larger volumes of soil excavated. To address this issue during the remediation of the Painesville FUSRAP Site, located in Painesville, Ohio, the Buffalo District of the U.S. Army Corps of Engineers, and its contractor, Safety and Ecology Corporation (SEC), employed automatic soil segregation technology provided by MACTEC (now AMEC) to reduce the potential for transportation and disposal of soils that met the cleanup limits. This waste minimization technology utilized gamma spectroscopy of conveyor-fed soils to automatically segregate the material into above and below criteria discharge piles. Use of the soil segregation system resulted in cost savings through the significant reduction of the volume of excavated soil that required off-site transportation and disposal, and the reduction of the amount of imported clean backfill required via reuse of 'below criteria' segregated soil as place back material in restoring the excavations. Measurements taken by the soil segregation system, as well as results of quality control sampling of segregated soils, confirmed that soils segregated

  7. Comparison of Activity Determination of Radium 226 in FUSRAP Soil using Various Energy Lines - 12299

    SciTech Connect

    Tucker, Brian; Donakowski, Jough; Hays, David

    2012-07-01

    Gamma spectroscopy is used at the Formerly Utilized Sites Remedial Action Program (FUSRAP) Maywood Superfund Site as the primary radioanalytical tool for quantization of activities of the radionuclides of concern in site soil. When selecting energy lines in gamma spectroscopy, a number of factors are considered including assumptions concerning secondary equilibrium, interferences, and the strength of the lines. The case of the Maywood radionuclide of concern radium-226 (Ra-226) is considered in this paper. At the FUSRAP Maywood Superfund Site, one of the daughters produced from radioactive decay of Ra-226, lead-214 (Pb- 214), is used to quantitate Ra-226. Another Ra-226 daughter, bismuth-214 (Bi-214), also may be used to quantitate Ra-226. In this paper, a comparison of Ra-226 to Pb-214 activities and Ra-226 to Bi-214 activities, obtained using gamma spectrometry for a large number of soil samples, was performed. The Pb-214, Bi-214, and Ra-226 activities were quantitated using the 352 kilo electron volt (keV), 609 keV, and 186 keV lines, respectively. The comparisons were made after correcting the Ra-226 activities by a factor of 0.571 and both ignoring and accounting for the contribution of a U-235 interfering line to the Ra-226 line. For the Pb-214 and Bi-214 activities, a mean in-growth factor was employed. The gamma spectrometer was calibrated for efficiency and energy using a mixed gamma standard and an energy range of 59 keV to 1830 keV. The authors expect other sites with Ra-226 contamination in soil may benefit from the discussions and points in this paper. Proper use of correction factors and comparison of the data from three different gamma-emitting radionuclides revealed agreement with expectations and provided confidence that using such correction factors generates quality data. The results indicate that if contamination is low level and due to NORM, the Ra-226 can be measured directly if corrected to subtract the contribution from U-235. If there is

  8. Maywood Interim Storage Site environmental report for calendar year 1992, 100 West Hunter Avenue, Maywood, New Jersey. Formerly Utilized Sites Remedial Action Program (FUSRAP)

    SciTech Connect

    Not Available

    1993-05-01

    This report describes the environmental surveillance program at the Maywood Interim Storage Site (MISS) and provides the results for 1992. Environmental monitoring of MISS began in 1984, when the site was assigned to DOE by Congress through the Energy and Water Development Appropriations Act and was placed under DOE`s Formerly Utilized Sites Remedial Action Program (FUSRAP). FUSRAP was established to identify and decontaminate or otherwise control sites where residual radioactive materials remain from the early years of the nation`s atomic energy program or from commercial operations causing conditions that Congress has authorized DOE to remedy. MISS is part of a National Priorities List (NPL) site. The environmental surveillance program at MISS includes sampling networks for radon and thoron in air; external gamma radiation exposure; and radium-226, radium-228, thorium-232, and total uranium in surface water, sediment, and groundwater. Additionally, chemical analysis includes metals and organic compounds in surface water and groundwater and metals in sediments. This program assists in fulfilling the DOE objective of measuring and monitoring effluents from DOE activities and calculating hypothetical doses to members of the general public. Monitoring results are compared with applicable Environmental Protection Agency (EPA) and state standards, DOE derived concentration guides (DCGs), dose limits, and other DOE requirements. Environmental standards are established to protect public health and the environment. The radiological data for all media sampled support the conclusion that doses to the public are not distinguishable from natural background radiation.

  9. Towpaths to Oblivion. The Middlesex Canal and the Coming of the Railroad 1792-1853.

    ERIC Educational Resources Information Center

    Holmes, Cary W.

    This narrative history of the Middlesex Canal from 1792-1853 is designed to be used with "Canal," a role-playing, decision-making game found in SO 011 886. Economic, social, and political factors related to planning, building, and implementing the canal are considered. The document is presented in three parts. Part I states reasons for…

  10. Preliminary Bedrock Geologic Map of the Old Lyme Quadrangle, New London and Middlesex Counties, Connecticut

    USGS Publications Warehouse

    Walsh, Gregory J.; Scott, Robert B.; Aleinikoff, John N.; Armstrong, Thomas R.

    2006-01-01

    This report presents a preliminary map of the bedrock geology of the Old Lyme quadrangle, New London and Middlesex Counties, Connecticut. The map depicts contacts of bedrock geologic units, faults, outcrops, and structural geologic information. The map was published as part of a study of fractured bedrock aquifers and regional tectonics.

  11. Colonie Interim Storage Site environmental report for calendar year 1992, 1130 Central Avenue, Colonie, New York. Formerly Utilized Sites Remedial Action Program (FUSRAP)

    SciTech Connect

    Not Available

    1993-05-01

    This report describes the environmental surveillance program at the Colonie Interim Storage Site (CISS) and provides the results for 1992. The site is located in eastern New York State, approximately 6.4 km (4.0 mi) northwest of downtown Albany. From 1958 to 1984, National Lead (NL) Industries used the facility to manufacture various components from depleted and enriched uranium natural thorium. Environmental monitoring of CISS began in 1984 when Congress added, the site to the US Department of Energy`s (DOE) Formerly Utilized Sites Remedial Action Program (FUSRAP). FUSRAP is a program established to identify and decontaminate or otherwise control sites where residual radioactive materials remain from the early years of the nation`s atomic energy program or from commercial operations causing conditions that Congress has authorized DOE to remedy. The environmental surveillance program at CISS includes sampling networks for external gamma radiation exposure and for thorium-232 and total uranium concentrations in surface water, sediment, and groundwater. Several chemical parameters are also measured in groundwater, including total metals, volatile organics, and water quality parameters. This surveillance program assists in fulfilling the DOE policy of measuring and monitoring effluents from DOE activities and calculating hypothetical doses. Results are compared with applicable Environmental Protection Agency (EPA) and New York State Department of Environmental Conservation (NYSDEC) standards, DOE derived concentration guides (DCGs), dose limits, and other DOE requirements.

  12. EPA Takes Action Against Underground Petroleum Storage Tank Violations in Monmouth County, Middlesex County and Paterson, New Jersey

    EPA Pesticide Factsheets

    (New York, N.Y.) In separate agreements with the U.S. Environmental Protection Agency, Monmouth and Middlesex counties in New Jersey have settled alleged violations of federal laws regarding the proper maintenance and operation of underground petroleum sto

  13. Scoping survey of perceived concerns, issues, and problems for near-surface disposal of FUSRAP waste

    SciTech Connect

    Robinson, J.E.; Gilbert, T.L.

    1982-12-01

    This report is a scoping summary of concerns, issues, and perceived problems for near-surface disposal of radioactive waste, based on a survey of the current literature. Near-surface disposal means land burial in or within 15 to 20 m of the earth's surface. It includes shallow land burial (burial in trenches, typically about 6 m deep with a 2-m cap and cover) and some intermediate-depth land burial (e.g., trenches and cap similar to shallow land burial, but placed below 10 to 15 m of clean soil). Proposed solutions to anticipated problems also are discussed. The purpose of the report is to provide a better basis for identifying and evaluating the environmental impacts and related factors that must be analyzed and compared in assessing candidate near-surface disposal sites for FUSRAP waste. FUSRAP wastes are of diverse types, and their classification for regulatory purposes is not yet fixed. Most of it may be characterized as low-activity bulk solid waste, and is similar to mill tailings, but with somewhat lower average specific activity. It may also qualify as Class A segregated waste under the proposed 10 CFR 61 rules, but the parent radionuclides of concern in FUSRAP (primarily U-238 and Th-232) have longer half-lives than do the radionuclides of concern in most low-level waste. Most of the references reviewed deal with low-level waste or mill tailings, since there is as yet very little literature in the public domain on FUSRAP per se.

  14. Challenges in Obtaining Property Access: The FUSRAP Maywood Site Experience - 13433

    SciTech Connect

    Kollar, William

    2013-07-01

    The Formerly Utilized Sites Remedial Action Program (FUSRAP) is the US government program started in 1974 to identify, investigate and clean up or control sites that became contaminated as a result of the nation's early atomic programs. Many of these sites are not owned by the federal government and therefore require owner permission to enter. The experience in pursuing such access at the FUSRAP Maywood Superfund Site (the Maywood Site or the Site) in Bergen County, New Jersey, is extensive. Since the US Army Corps of Engineers (the Corps) assumed responsibility for the Maywood Site from the US Department of Energy in 1997, at least 186 separate property access agreements (known in FUSRAP as a Real Estate Right-of- Entry or ROE) have been executed between the Corps and approximately 55 different land owners and tenant occupants at the Maywood Site (agreement renewals with the same owners over time account for the difference). Maywood's experience during the Corps' tenure, reflected here in three case studies of representative property access efforts, offers some lessons and best practices that may apply to other remedial programs. While the Site Community Relations Manager (the author of this paper) managed the property access task, multi-disciplinary support from across the project was also critical to success in this endeavor. (authors)

  15. Comparison of Statistically Modeled Contaminated Soil Volume Estimates and Actual Excavation Volumes at the Maywood FUSRAP Site - 13555

    SciTech Connect

    Moore, James; Hays, David; Quinn, John; Johnson, Robert; Durham, Lisa

    2013-07-01

    As part of the ongoing remediation process at the Maywood Formerly Utilized Sites Remedial Action Program (FUSRAP) properties, Argonne National Laboratory (Argonne) assisted the U.S. Army Corps of Engineers (USACE) New York District by providing contaminated soil volume estimates for the main site area, much of which is fully or partially remediated. As part of the volume estimation process, an initial conceptual site model (ICSM) was prepared for the entire site that captured existing information (with the exception of soil sampling results) pertinent to the possible location of surface and subsurface contamination above cleanup requirements. This ICSM was based on historical anecdotal information, aerial photographs, and the logs from several hundred soil cores that identified the depth of fill material and the depth to bedrock under the site. Specialized geostatistical software developed by Argonne was used to update the ICSM with historical sampling results and down-hole gamma survey information for hundreds of soil core locations. The updating process yielded both a best guess estimate of contamination volumes and a conservative upper bound on the volume estimate that reflected the estimate's uncertainty. Comparison of model results to actual removed soil volumes was conducted on a parcel-by-parcel basis. Where sampling data density was adequate, the actual volume matched the model's average or best guess results. Where contamination was un-characterized and unknown to the model, the actual volume exceeded the model's conservative estimate. Factors affecting volume estimation were identified to assist in planning further excavations. (authors)

  16. Hydrogeologic Modeling at the Sylvania Corning FUSRAP Site - 13419

    SciTech Connect

    Ewy, Ann; Heim, Kenneth J.; McGonigal, Sean T.; Talimcioglu, Nazmi M.

    2013-07-01

    A comparative groundwater hydrogeologic modeling analysis is presented herein to simulate potential contaminant migration pathways in a sole source aquifer in Nassau County, Long Island, New York. The source of contamination is related to historical operations at the Sylvania Corning Plant ('Site'), a 9.49- acre facility located at 70, 100 and 140 Cantiague Rock Road, Town of Oyster Bay in the westernmost portion of Hicksville, Long Island. The Site had historically been utilized as a nuclear materials manufacturing facility (e.g., cores, slug, and fuel elements) for reactors used in both research and electric power generation in early 1950's until late 1960's. The Site is contaminated with various volatile organic and inorganic compounds, as well as radionuclides. The major contaminants of concern at the Site are tetrachloroethene (PCE), trichloroethene (TCE), nickel, uranium, and thorium. These compounds are present in soil and groundwater underlying the Site and have migrated off-site. The Site is currently being investigated as part of the Formerly Utilized Sites Remedial Action Program (FUSRAP). The main objective of the current study is to simulate the complex hydrogeologic features in the region, such as numerous current and historic production well fields; large, localized recharge basins; and, multiple aquifers, and to assess potential contaminant migration pathways originating from the Site. For this purpose, the focus of attention was given to the underlying Magothy formation, which has been impacted by the contaminants of concern. This aquifer provides more than 90% of potable water supply in the region. Nassau and Suffolk Counties jointly developed a three-dimensional regional groundwater flow model to help understand the factors affecting groundwater flow regime in the region, to determine adequate water supply for public consumption, to investigate salt water intrusion in localized areas, to evaluate the impacts of regional pumping activity, and to

  17. Relocation of on-site spoils pile materials at the Linde Fusrap Site

    SciTech Connect

    Schwippert, M.T.; Boyle, J.D.; Bousquet, S.M.

    2007-07-01

    During the 1940's, the Linde Division of Union Carbide used portions of their property in Tonawanda, New York for processing uranium ores under Federal Manhattan Engineering District (MED) contracts. These activities resulted in radiological contamination on portions of the property. The radionuclides of concern at the site are Radium, Thorium, and Uranium. The site is currently owned and operated by Praxair Inc., an industrial gas company. The U.S. Army Corps of Engineers (USACE) issued a Record of Decision to remediate the radiologically-contaminated materials associated with MED activities in March 2000 under the authority of the Formerly Utilized Sites Remedial Action Program (FUSRAP). The selected remedy is fully protective of human health and the environment and complies with Federal and State requirements that are legally applicable or relevant and appropriate and meets community commitments. The USACE - Buffalo District has been executing remedial activities at the site and has successfully addressed many challenges in a safe and cost effective manner through effective coordination, project management, and partnering with stakeholders. These efforts supported the successful relocation of approximately 29,000 cubic yards of stockpiled material (soils, concrete, steel, asphalt and miscellaneous non-soil) that had been generated by the property owner as a result of ongoing development of the facility. Relocation of the material was necessary to allow safe access to the surface and subsurface soils beneath the pile for sampling and analysis. During relocation operations, materials were evaluated for the presence of radiological contamination. The vast majority of material was relocated onsite and remained the property owner's responsibility. A small portion of the material required off-site disposal at a permitted disposal facility due to radiological contamination that exceeded site criteria. This paper presents details associated with the successful

  18. Considerations for Implementation of MARSSIM/MARSAME Surface Radioactivity Surveys within FUSRAP - 12330

    SciTech Connect

    Hay, Scott S.; Winters, Michael S.

    2012-07-01

    Surveys for residual surface radioactivity support the release of buildings under MARSSIM and the release of materials and equipment under MARSAME consensus guidance. There are a multitude of factors and conditions that must be assessed and addressed when developing a defensible survey design. ISO-7503 addresses the most basic survey considerations with consistent terminology and defensible calculation methodologies recommended for program-wide implementation by the authors. A key point of interest is the ISO-7503 approach to determining the total efficiency of the measurement system that is promoted by the authors for adoption throughout FUSRAP. (authors)

  19. Superfund Record of Decision (EPA Region 2): Chemsol, Inc. , Piscataway, Middlesex County, NJ. (First remedial action), September 1991

    SciTech Connect

    Not Available

    1991-09-20

    The 40-acre Chemsol site is a former solvent recovery and waste reprocessing facility in Piscataway Township, Middlesex County, New Jersey. Land use in the area is predominantly commercial and residential, with an onsite marshy area that may be considered a wetlands. The site overlies a bedrock aquifer that is used as a regional drinking water source. Between 1980 and 1990, sampling of residential wells indicated the presence of organic contaminants and PCBs. The Record of Decision (ROD) provides an interim remedy to restrict the offsite migration of highly contaminated ground water. The primary contaminants of concern affecting the ground water are VOCs including benzene, toluene, and xylenes; other organics including pesticides and phenols; and metals including arsenic, chromium, and lead. The selected remedial action for this interim remedy includes installing a ground water collection trench; installing three ground water extraction wells to a depth of 130 feet; constructing an onsite treatment plant and treating contaminated ground water using air stripping, biological filtration, and activated carbon adsorption.

  20. The Changing Role of Public Participation as a FUSRAP Site Moves from Characterization to Remedial Action and Closure

    SciTech Connect

    Roos, A. D.; Kollar, W.

    2006-07-01

    This paper describes a comprehensive public participation program developed by the U.S. Army Corps of Engineers (USACE, or the Corps) and its contractor, Shaw Environmental, Inc. at the Formerly Utilized Sites Remedial Action Program (FUSRAP) Maywood Superfund Site (the Site) in New Jersey, USA. It focuses on the program's evolving nature as the Site has moved through the Comprehensive Environmental, Response, Compensation and Liability Act (CERCLA) process. CERCLA is commonly referred to as the Superfund program. A principal objective of the FUSRAP Maywood Site's public involvement program is to minimize impacts to affected property owners, while keeping the broader public fully informed and involved as required under the CERCLA. The various properties comprising the Site have gone through site investigation (or characterization), remedial design, remedial action (ongoing) and, in some cases, property closeout reporting since the Corps assumed responsibility for the FUSRAP in 1997. At the outset, the Corps developed an integrated and forward-looking communication approach. As the CERCLA process drives changes in priorities, the approach has been tailored to accommodate the changing nature of the project. These changes were principally driven by the technical objectives of each project phase and, as important, by the anticipated and expressed needs of impacted property owners. This paper also notes public participation activities of the U.S. Department of Energy (DOE) during its management of the FUSRAP Maywood Site as needed, to provide context to the Corps' follow-on public participation efforts. (authors)

  1. Communicating potential risks of uncontrolled site development at a Fusrap site

    SciTech Connect

    Roos, A.D.; Kollar, W.

    2008-07-01

    This paper describes a particular risk communication challenge at the FUSRAP Maywood Superfund Site (the Site) in Maywood, New Jersey, USA. That challenge is communicating the potential human exposure risks of uncontrolled site development to landowners, tenants, private contractors and public works entities that may engage in construction activities at or adjacent to Site properties. This is of special concern because the Site does not have the authority to establish physical control over most of the properties where contamination is known or suspected to exist. Consequently, a range of communications techniques have been employed to alert property owners and others to the risks of uncontrolled site development. Each technique has its particular limitations, but collectively this multi-channel communication strategy has proved successful in delivering the risk message. (authors)

  2. Quantifying Contaminant Mass for the Feasibility Study of the DuPont Chambers Works FUSRAP Site - 13510

    SciTech Connect

    Young, Carl; Rahman, Mahmudur; Johnson, Ann; Owe, Stephan

    2013-07-01

    The U.S. Army Corps of Engineers (USACE) - Philadelphia District is conducting an environmental restoration at the DuPont Chambers Works in Deepwater, New Jersey under the Formerly Utilized Sites Remedial Action Program (FUSRAP). Discrete locations are contaminated with natural uranium, thorium-230 and radium-226. The USACE is proposing a preferred remedial alternative consisting of excavation and offsite disposal to address soil contamination followed by monitored natural attenuation to address residual groundwater contamination. Methods were developed to quantify the error associated with contaminant volume estimates and use mass balance calculations of the uranium plume to estimate the removal efficiency of the proposed alternative. During the remedial investigation, the USACE collected approximately 500 soil samples at various depths. As the first step of contaminant mass estimation, soil analytical data was segmented into several depth intervals. Second, using contouring software, analytical data for each depth interval was contoured to determine lateral extent of contamination. Six different contouring algorithms were used to generate alternative interpretations of the lateral extent of the soil contamination. Finally, geographical information system software was used to produce a three dimensional model in order to present both lateral and vertical extent of the soil contamination and to estimate the volume of impacted soil for each depth interval. The average soil volume from all six contouring methods was used to determine the estimated volume of impacted soil. This method also allowed an estimate of a standard deviation of the waste volume estimate. It was determined that the margin of error for the method was plus or minus 17% of the waste volume, which is within the acceptable construction contingency for cost estimation. USACE collected approximately 190 groundwater samples from 40 monitor wells. It is expected that excavation and disposal of

  3. Integrating intrusive and nonintrusive characterization methods to achieve a conceptual site model for the SLDA FUSRAP site - 8265.

    SciTech Connect

    Durham, L. A.; Peterson, J. M.; Frothingham, D. G.; Frederick, W. T.; Lenart, W.; Environmental Science Division; U. S. Army Corps of Engineers, Pittsburg District; U. S. Army Corps of Engineers, Buffalo District

    2008-01-01

    The US Army Corps of Engineers (USACE) is addressing radiological contamination following Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA) requirements at the Shallow Land Disposal Area (SLDA) site, which is a radiologically contaminated property that is part of the Formerly utilized Sites Remedial Action Program (FUSRAP). The SLDA is an 18-hectare (44-acre) site in Parks township, Armstrong County, Pennsylvania, about 37 kilometers (23 miles) east-northeast of Pittsburgh. According to historical record, radioactive wastes were disposed of at the SLDA in a series of trenches by the Nuclear Materials and Equipment Company (NUMEC) in the 1960s. The wastes originated from the nearby Apollo nuclear fuel fabrication facility, which began operations under NUMEC in the late 1950s and fabricated enriched uranium into naval reactor fuel elements. It is believed that the waste materials were buried in a series of pits constructed adjacent to one another in accordance with an Atomic Energy Commission (AEC) regulation that has since been rescinded. A CERCLA remedial investigation/feasibility study (RI/FS) process was completed for the SLDA site, and the results of the human health risk assessment indicated that the radiologically contaminated wastes could pose a risk to human health in the future. There are no historical records that provide the exact location of these pits. However, based on geophysical survey results conducted in the 1980s, these pits were defined by geophysical anomalies and were depicted on historical site drawings as trenches. At the SLDA site, a combination of investigative methods and tools was used in the RI/FS and site characterization activities. The SLDA site provides an excellent example of how historical documents and data, historical aerial photo analysis, physical sampling, and nonintrusive geophysical and gamma walkover surveys were used in combination to reduce the uncertainty in the location of the trenches. The

  4. Integrating Intrusive and Non-intrusive Characterization Methods To Achieve A Conceptual Site Model For The SLDA FUSRAP

    SciTech Connect

    Durham, L.A.; Peterson, J.M.; Frothingham, D.G.; Frederick, W.T.; Lenart, W.

    2008-07-01

    The U.S. Army Corps of Engineers (USACE) is addressing radiological contamination following Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA) requirements at the Shallow Land Disposal Area (SLDA) site, which is a radiologically contaminated property that is part of the Formerly Utilized Sites Remedial Action Program (FUSRAP). The SLDA is an 18-hectare (44- acre) site in Parks Township, Armstrong County, Pennsylvania, about 37 kilometers (23 miles) east-northeast of Pittsburgh. According to historical record, radioactive wastes were disposed of at the SLDA in a series of trenches by the Nuclear Materials and Equipment Company (NUMEC) in the 1960's. The wastes originated from the nearby Apollo nuclear fuel fabrication facility, which began operations under NUMEC in the late 1950's and fabricated enriched uranium into naval reactor fuel elements. It is believed that the waste materials were buried in a series of pits constructed adjacent to one another in accordance with an Atomic Energy Commission (AEC) regulation that has since been rescinded. A CERCLA remedial investigation/feasibility study (RI/FS) process was completed for the SLDA site, and the results of the human health risk assessment indicated that the radiologically contaminated wastes could pose a risk to human health in the future. There are no historical records that provide the exact location of these pits. However, based on geophysical survey results conducted in the 1980's, these pits were defined by geophysical anomalies and were depicted on historical site drawings as trenches. At the SLDA site, a combination of investigative methods and tools was used in the RI/FS and site characterization activities. The SLDA site provides an excellent example of how historical documents and data, historical aerial photo analysis, physical sampling, and non-intrusive geophysical and gamma walkover surveys were used in combination to reduce the uncertainty in the location of the

  5. USACE FUSRAP Maywood Team Develops a Mechanism to Evaluate Residual Radon Exposure Potential at Vicinity Properties Where Remediation of Accessible Contamination has been Completed

    SciTech Connect

    Winters, M.; Walnicki, S.; Hays, D.

    2008-07-01

    The Maywood FUSRAP Team is obligated, under its approved remedy selection decision document, to demonstrate substantive compliance with New Jersey Administrative Code 7:28- 12(a)2, establishing an indoor limit of three Pico-Curies per liter above background for radon-222 (Rn-222). The Maywood Team explores various avenues for dealing with the radon issue and provides an alternative for demonstrating substantive compliance with the radon remediation standard by answering the question: 'In certain conservative situations, can compliance with the radon standard be demonstrated without performing monitoring?' While monitoring may be the most definitive method for demonstrating compliance, a logical argument can be made that when radiological remediation removes the potential source for Rn-222 above background, monitoring is unnecessary. This position is defended through the use of historical physical radon measurements which illustrate that indoor radon was not a pre-remediation problem, and post-remediation soil sampling data which demonstrate that the source of the potentially elevated Rn- 222 levels have been successfully mitigated. Monitoring recommendations are made for situations where insufficient data exists to make definitive determinations or when un-remediated sources affecting habitable structures remain on a given property. Additional information regarding recommended techniques and references for effective monitoring of indoor radon are included in this paper. This paper may benefit teams that have similar regulatory commitments and/or have need to make assessments of radon exposure potential based upon historical monitoring data and available soils concentration data. (authors)

  6. New Brunswick Site annual environmental report for calendar year 1991, New Brunswick, New Jersey. Formerly Utilized Sites Remedial Action Program (FUSRAP)

    SciTech Connect

    Not Available

    1992-09-01

    This document describes the environmental monitoring program at the New Brunswick Site (NBS) and surrounding area, implementation of the program, and monitoring results for 1991. The site, near New Brunswick,, New Jersey, is a 5.6-acre vacant, fenced, and grass-covered area. Environmental monitoring of NBS began in 1981 when the site was part of the US Department of Energy`s (DOE) Surplus Facilities Management Program. In 1990 responsibility for NBS was transferred to the Formerly Utilized Sites Remedial Action Program (FUSP.4P). FUSRAP is a DOE program to identify and decontaminate or otherwise control sites where residual radioactive materials remain from the,early years of the nation`s atomic energy program or from commercial operations causing conditions that Congress has authorized DOE to remedy. The environmental monitoring program at NBS includes sampling networks for radon and thoron in air; external gamma radiation exposure; and radium-226, radium-228, thorium-228, thorium-230, thorium-232, americium-241, cesium-137, plutonium-239, and total uranium in surface water, sediment, and groundwater. Several nonradiological parameters are also measured in groundwater, surface water, and sediments. Monitoring results are compared with applicable Environmental Protection Agency standards, DOE derived concentration guides, dose limits, and other requirements in DOE orders. Environmental standards are established to protect public health and the environment.

  7. Wayne Interim Storage Site environmental report for calendar year 1992, 868 Black Oak Ridge Road, Wayne, New Jersey. Formerly Utilized Sites Remedial Action Program (FUSRAP)

    SciTech Connect

    Not Available

    1993-05-01

    This report describes the environmental surveillance program at the Wayne Interim Storage Site (WISS) and provides the results for 1992. The fenced, site, 32 km (20 mi) northwest of Newark, New Jersey, was used between 1948 and 1971 for commercial processing of monazite sand to separate natural radioisotopes - predominantly thorium. Environmental surveillance of WISS began in 1984 in accordance with Department of Energy (DOE) Order 5400.1 when Congress added the site to DOE`s Formerly Utilized Sites Remedial Action Program (FUSRAP). The environmental surveillance program at WISS includes sampling networks for radon and thoron in air; external gamma radiation exposure; radium-226, radium-228, thorium-230, thorium-232, total uranium, and several chemicals in surface water and sediment; and total uranium, radium-226, radium-228, thorium-230, thorium-232, and organic and inorganic chemicals in groundwater. Monitoring results are compared with applicable Environmental Protection Agency (EPA) and state standards, DOE derived concentration guides (DCGs), dose limits, and other DOE requirements. This monitoring program assists in fulfilling the DOE policy of measuring and monitoring effluents from DOE activities and calculating hypothetical doses. Results for environmental surveillance in 1992 show that the concentrations of all radioactive and most chemical contaminants were below applicable standards.

  8. Effect of soil erosion on the long-term stability of FUSRAP near-surface waste-burial sites

    SciTech Connect

    Knight, M.J.

    1983-04-01

    Decontamination of FUSRAP sites could result in the generation of large volumes (in excess of 400,000 m/sup 3/) of low-activity radioactive wastes (primarily contaminated soil and building materials) requiring subsequent disposal. It is likely that near-surface burial will be seriously considered as an option for disposal of these materials. A number of factors - including soil erosion - could adversely affect the long-term stability of a near-surface waste-burial site. The majority of FUSRAP sites are located in the humid eastern United States, where the principal cause of erosion is the action of water. This report examines the effect of soil erosion by water on burial-site stability based on analysis of four hypothetical near-surface burial sites. The Universal Soil Loss Equation was employed to estimate average annual soil loss from burial sites and the 1000-year effects of soil loss on the soil barrier (burial trench cap) placed over low-activity wastes. Results suggest that the land use of the burial site and the slope gradient of the burial trench cap significantly affect the rate of soil erosion. The development of measures limiting the potential land use of a burial site (e.g., mixing large rocks into the burial trench cap) may be required to preserve the integrity of a burial trench for long periods of time.

  9. Study of field assessment methods and worker risks for processing alternatives to support principles for FUSRAP waste materials. Part 1: Treatment methods and comparative risks of thorium removal from waste residues

    SciTech Connect

    Porter, R.D.; Hamby, D.M.; Martin, J.E.

    1997-07-01

    This study was done to examine the risks of remediation and the effectiveness of removal methods for thorium and its associated radioactive decay products from various soils and wastes associated with DOE`s Formerly Utilized Sites Remedial Action Program (FUSRAP). Its purpose was to provide information to the Environmental Management Advisory Board`s FUSRAP Committee for use in its deliberation of guiding principles for FUSRAP sites, in particular the degree to which treatment should be considered in the FUSRAP Committee`s recommendations. Treatment of FUSRAP wastes to remove thorium could be beneficial to management of lands that contain thorium if such treatment were effective and cost efficient. It must be recognized, however, that treatment methods invariably require workers to process residues and waste materials usually with bulk handling techniques. These processes expose workers to the radioactivity in the materials, therefore, workers would incur radiological risks in addition to industrial accident risks. An important question is whether the potential reduction of future radiological risks to members of the public justifies the risks that are incurred by remediation workers due to handling materials. This study examines, first, the effectiveness of treatment and then the risks that would be associated with remediation. Both types of information should be useful for decisions on whether and how to apply thorium removal methods to FUSRAP waste materials.

  10. Land development in Massachusetts: Its effect on the environment within Essex and Middlesex counties from 1990 to 2007

    NASA Astrophysics Data System (ADS)

    Tardie, Peter Sean

    Since the 1970's urban centers in and surrounding Essex and Middlesex Counties in Massachusetts have expanded and proliferated into adjacent communities. This expansion has led to the conversion of land for housing, businesses, schools, recreation, and parks, placing significant strain on existing land cover, land use, and available natural resources. Mounting growth pressures and a reduction of undeveloped land have raised serious concerns as cropland and forest fragmentation, wetland destruction, protected open-space infringement, pollution, and systematic losses of rural conditions have become obvious. To monitor development, the post-classification change detection method was applied to Landsat Thematic Mapper (TM) satellite data and GIS was used to detect, quantity, and document the extent of development and its effect on the environment and to assess and quantify the demographic changes that occurred within the counties from 1990 to 2007. Classification of the 1990 image resulted in 217 clusters and 214 clusters for the 2007 image The overall accuracy achieved for the 1990 image classification was 87.3% with a KHAT value of 0.848, and the overall accuracy for the 2007 classification was 86.27% with a KHAT value of 0.840. From 1990 to 2007 land cover change occurred primarily along major transportation corridors. The post-classification change detection results indicate that Essex and Middlesex County combined gained 23,435.66 "new" acres of land development from 1990 to 2007 through a loss and change in acreage from the Bareland, Forest, Grassland, Water, and Wetland land cover class categories. Results indicate that there was an approximate 0.56% overall (net) increase of newly developed land areas within the 1990 and 2007 image classifications from 415.46 acres or 0.64 square miles. In addition, there was a substantial decrease (-40.0%) within the grassland category. Land development was responsible for a portion of the decrease of grasslands (-13

  11. Linde FUSRAP Site Remediation: Engineering Challenges and Solutions of Remedial Activities on an Active Industrial Facility - 13506

    SciTech Connect

    Beres, Christopher M.; Fort, E. Joseph; Boyle, James D.

    2013-07-01

    The Linde FUSRAP Site (Linde) is located in Tonawanda, New York at a major research and development facility for Praxair, Inc. (Praxair). Successful remediation activities at Linde combines meeting cleanup objectives of radiological contamination while minimizing impacts to Praxair business operations. The unique use of Praxair's property coupled with an array of active and abandoned utilities poses many engineering and operational challenges; each of which has been overcome during the remedial action at Linde. The U.S. Army Corps of Engineers - Buffalo District (USACE) and CABRERA SERVICES, INC. (CABRERA) have successfully faced engineering challenges such as relocation of an aboveground structure, structural protection of an active water line, and installation of active mechanical, electrical, and communication utilities to perform remediation. As remediation nears completion, continued success of engineering challenges is critical as remaining activities exist in the vicinity of infrastructure essential to business operations; an electrical substation and duct bank providing power throughout the Praxair facility. Emphasis on engineering and operations through final remediation and into site restoration will allow for the safe and successful completion of the project. (authors)

  12. Derivation of guidelines for uranium residual radioactive material in soil at the New Brunswick Site, Middlesex County, New Jersey

    SciTech Connect

    Dunning, D.; Kamboj, S.; Nimmagadda, M.; Yu, C.

    1996-02-01

    Residual radioactive material guidelines for uranium in soil were derived for the New Brunswick Site, located in Middlesex County, New Jersey. This site has been designated for remedial action under the Formerly Utilized Sites Remedial Action Program of the US Department of Energy (DOE). Residual radioactive material guidelines for individual radionuclides of concern and total uranium were derived on the basis of the requirement that the 50-year committed effective dose equivalent to a hypothetical individual who lives or works in the immediate vicinity of the New Brunswick Site should not exceed a dose of 30 mrem/yr following remedial action for the current-use and likely future-use scenarios or a dose of 100 mrem/yr for less likely future-use scenarios. The DOE residual radioactive material guideline computer code, RESRAD, was used in this evaluation; RESRAD implements the methodology described in the DOE manual for establishing residual radioactive material guidelines. The guidelines derived in this report are intended to apply to the remediation of these remaining residual radioactive materials at the site. The primary radionuclides of concern in these remaining materials are expected to be radium-226 and, to a lesser extent, natural uranium and thorium. The DOE has established generic cleanup guidelines for radium and thorium in soil; however, cleanup guidelines for other radionuclides must be derived on a site-specific basis.

  13. Transition and Transfer of Remediated Formerly Utilized Sites Remedial Action Program (FUSRAP) Sites from U.S. Army Corps of Engineers (USACE) to U.S. Department of Energy (DOE)

    SciTech Connect

    Carpenter, Cliff; Castillo, Darina; Fatherly, Nicki; Miller, Michele

    2016-03-06

    The US Department of Energy (DOE) expects to receive the transfer of 10 FUSRAP Sites from the US Army Corps of Engineers (USACE) over the next 10 years; however, the timing of the transfers is highly dependent upon federal funding of the ongoing remedial actions. When remediation for each site is complete and the 2-year operations and maintenance period has concluded, each site will transfer from USACE to DOE for long-term surveillance and maintenance (LTS&M). US DOE’s Office of Legacy Management (LM) will accept program responsibility for these sites and conduct LTS&M activities required to maintain protectiveness, preserve site-specific knowledge, and retain the cleanup and stewardship records while keeping stakeholders informed. Since the last FUSRAP site transfer occurred in 2007, LM in coordination with USACE intends to establish a transition process to promote the seamless transfer of sites from the time when the first record of decision is signed to the completion of FUSRAP activities. The approach to transfer active FUSRAP sites to completed sites status has been historically outlined in foundational documents such as the 1999 Memorandum of Understanding and supporting letters of agreement between the two agencies. As more complex FUSRAP sites are completed, this transition process will provide a model between the two agencies to communicate future long-term care liabilities. Ultimately, the FUSRAP transition process is structured to acquire and preserve site knowledge and information necessary for protecting the environment and public health. As of 2015, LM has transitioned and accepted programmatic responsibility for over 90 sites. From LM’s perspective, successful transition of any site includes understanding the long-term environmental liabilities. LM uses site transition framework requirements from past transitions to develop site-specific transition plans. Site-specific transition plans are developed by LM in coordination with USACE and executed

  14. Consolidated Online Data Management Strategy in Support of Environmental Remediation Activities at the Dupont Chambers Works Formerly Utilized Sites Remedial Action Program (Fusrap) Site

    SciTech Connect

    Nelson, K.A.; Desai, N.B.; Samus, J.E.; Bock, G.O.

    2007-07-01

    The U.S. Army Corps of Engineers (USACE) has developed and implemented an innovative online data management application in support of site characterization and remediation activities at the DuPont Chambers Works Formerly Utilized Sites Remedial Action Program (FUSRAP) Site. The password-protected, web-based application was implemented to centralize project data, facilitate project communications, and provide a large and diverse group of project team members with access to the data and analytical tools they need to efficiently and effectively manage the ongoing characterization and remediation efforts. Centralizing resources using the online application and web-based strategy streamlines data access and communications, allowing the team to effectively keep the project on track while reducing the costs associated with data requests, data duplication, document review and retrieval, software requirements, and lapses in communication or data transfer. (authors)

  15. Fall Protection Procedures for Sealing Bulk Waste Shipments by Rail Cars at Formerly Utilized Sites Remedial Action Program (FUSRAP) Sites - 13509

    SciTech Connect

    Boyle, J.D.; Fort, E. Joseph; Lorenz, William; Mills, Andy

    2013-07-01

    Rail-cars loaded with radioactive materials must be closed and fastened to comply with United States Department of Transportation (DOT) requirements before they shipped. Securing waste shipments in a manner that meets these regulations typically results in the use of a sealable rail-car liner. Workers accessing the tops of the 2.74 m high rail-cars to seal and inspect liners for compliance prior to shipment may be exposed to a fall hazard. Relatively recent revisions to the Fall Protection requirements in the Safety and Health Requirements Manual (EM385-1-1, U.S. Army Corps of Engineers) have necessitated modifications to the fall protection systems previously employed for rail-car loading at Formerly Utilized Sites Remedial Action Program (FUSRAP) sites. In response these projects have developed site-specific procedures to protect workers and maintain compliance with the improved fall protection regulations. (authors)

  16. Formerly Used Sites Remedial Action Program (FUSRAP) W. R. Grace Building 23 Remedial Action-Challenges and Successes - 12247

    SciTech Connect

    Barber, Brenda; Honerlah, Hans; O'Neill, Mike; Young, Carl

    2012-07-01

    : coordination with stakeholders, coordination between multiple RA contractors, addressing unique structural challenges for Building 23, nonradiological hazards associated with the RA, weather issues, and complex final status survey (FSS) coordination. The challenges during the Phase 1 RA were handled successfully. The challenges for the Phase 2 RA, which is anticipated to be complete by late-summer of 2012, have been handled successfully so far. By fall of 2012, USACE is expecting to finalize a robust RA Closure Report, including the Final Status Survey Report, which summarizes the RA activities and documents compliance with the ROD. During the ongoing RA at Building 23, there have been and still are many challenges both technically and from a project management perspective, due in part to the nature and extent of impact at the site (residual radioactivity within an active processing building), dual oversight by the property owner and USACE, and site-specific challenges associated with a complex RA and multiple contractors. Currently, USACE and its industry partner are overseeing the completion of RA field activities. RA closure documentation for the remediation of Building 23 to address residual contamination in building materials will be reviewed/approved by USACE and its industry partner upon completion of the field activities. USACE and its industry partner are working well together, through the Settlement Agreement, to conduct a cost-efficient and effective remedial action to address the legacy issues at Building 23. This cooperative effort has set a firm foundation for achieving a successful RA at the RWDA using a 'forward think' approach, and it is a case study for other sites where an industry partner is involved. The collaborative effort led to implementation of an RA which is acceptable to the site owner, the regulators, and the public, thus allowing USACE to move this project forward successfully in the FUSRAP program. (authors)

  17. Public health assessment for JIS Landfill, South Brunswick, Middlesex County, New Jersey, Region 2. Cerclis No. NJD97400998. addendum. Final report

    SciTech Connect

    1995-08-25

    The Jones Industrial Services (JIS) Landfill site is an approximately eleven acre landfill located on a 24 acre site in South Brunswick Town, Middlesex County, New Jersey. The landfill records document that sludges, solvents, pesticides, and industrial wastes, some of which are toxic and/or hazardous substances were accepted at the landfill from the 1960`s through the early 1970`s. On-site and off-site soil and groundwater is contaminated with volatile organic compounds (VOCs), petroleum hydrocarbons, polychlorinated biphenyls, pesticides, and heavy metals. The landfill may have posed a public health hazard in the past, since the site information indicates that human exposure to volatile organic compounds (VOCs) and metals in domestic drinking water wells may have occurred. However, available data do not indicate that humans are presently being exposed to contaminants at levels expected to cause adverse health effects.

  18. Health assessment for petitioned preliminary public health assessment, Global Landfill, Old Bridge, Middlesex County, New Jersey, Region 2. CERCLIS No. NJD063160667. Preliminary report

    SciTech Connect

    Not Available

    1993-04-26

    Located in the Old Bridge Township, Middlesex County, New Jersey, the Global Landfill National Priorities List (NPL) site is situated along a tidal marsh. The 57.5-acre NPL site has about 2,400,000 cubic yards of municipal solid, bulky, vegetative, and industrial wastes. Global Landfill generates significant amounts of leachate and landfill gas. On-site environmental monitoring of leachate, surface and ground water, and soil gas indicates there is significant contamination of the environment at the Global Landfill NPL site. Based on available information, the Agency for Toxic Substances and Disease Registry (ATSDR) concludes that the Global Landfill NPL site is an indeterminate public health hazard because most of the on- and off-site data are not appropriate for determining possible health impacts for the site. Because airborne contaminants may be migrating into nearby residential areas, air monitoring is needed at the landfill and in residential areas to determine whether significant human exposure is occurring. As described in the public health assessment, the New Jersey Department of Environmental Protection and Energy (NJDEPE) is planning a number of remedial activities. When those corrective actions are complete, the potential for human exposure to Global Landfill NPL site-related contaminants should be reduced, provided operable unit 1 is appropriately designed and maintained.

  19. Superfund Record of Decision (EPA Region 2): Kin-Buc Landfill, Edison Township, Middlesex County, NJ. (Second remedial action), September 1992. Final report

    SciTech Connect

    Not Available

    1992-09-28

    The 200-acre Kin-Buc Landfill consists of several inactive disposal areas and is located in Edison Township, Middlesex County, New Jersey. Land use in the area is predominantly industrial and commercial, with some residences within 2 miles north of the site. No drinking water supply wells are located within a 2-mile radius of the site. As a result of an oil spill in 1976, EPA conducted an investigation of the property. In 1980, clean-up activities were initiated under the Clean Water Act and included removal, treatment, and disposal of leachate and drummed waste. The ROD addresses a final remedy for OU2 consisting of the sediment and groundwater in the Edmonds Creek wetlands area, Mill Brook/Martins Creek, Mound B, and the low-lying area. The primary contaminants of concern affecting the sediment and ground water are VOCs, including benzene and xylenes; other organics, including PAHs, PCBs, and pesticides; and metals, including arsenic and lead. The selected remedy for the site are included.

  20. Determination of ecologically vital groundwaters at selected sites in the Formerly Utilized Sites Remedial Action Program

    SciTech Connect

    Vinikour, W.S.; Yin, S.C.L.

    1989-08-01

    The US Department of Energy is classifying groundwaters at sites in its Formerly Utilized Sites Remedial Action Program (FUSRAP). Of particular concern is the potential presence of groundwaters that are highly vulnerable to contamination and that are either (1) irreplaceable sources of drinking water or (2) ecologically vital. Conditions at nine FUSRAP sites were evaluated to determine if ecologically vital groundwaters are present. The sites evaluated were Wayne Interim Storage Site, Maywood Interim Storage Site, and Middlesex Sampling Plant in New Jersey; Ashland 2 Site, Seaway Industrial Park, Colonie Interim storage Site, and Niagara Falls Storage Site in New York; and the St. Louis Airport Site and Hazelwood Interim Storage Site in Missouri. The analyses indicated that groundwaters are vulnerable to contamination at all but two of the sites -- the Ashland 2 and Seaway Industrial Park sites in New York. Groundwater discharge points were identified within a 2-mile radius (i.e., the classification review area) of all of the sites. No ecologically vital groundwater areas exist in the vicinities of any of the nine FUSRAP sites evaluated. 35 refs., 17 figs.

  1. Niagara Falls Storage Site environmental report for calendar year 1992, 1397 Pletcher Road, Lewiston, New York. Formerly Utilized Sites Remedial Action Program (FUSRAP)

    SciTech Connect

    Not Available

    1993-05-01

    This report describes the environmental surveillance program at the Niagara Falls Storage Site (NFSS) and provides the results for 1992. From 1944 to the present, the primary use of NFSS has been storage of radioactive residues produced as a by-product of uranium production. All onsite areas of residual radioactivity above guidelines have been remediated. Materials generated during remediation are stored onsite in the 4-ha (10-acre) waste containment structure (WCS). The WCS is a clay-lined, clay-capped, and grass-covered storage pile. The environmental surveillance program at NFSS includes sampling networks for radon concentrations in air; external gamma radiation exposure; and total uranium and radium-226 concentrations in surface water, sediments, and groundwater. Several chemical parameters, including seven metals, are also routinely measured in groundwater. This surveillance program assists in fulfilling the DOE policy of measuring and monitoring effluents from DOE activities and calculating hypothetical doses. Monitoring results are compared with applicable Environmental Protection Agency (EPA) and New York State Department of Environmental Conservation (NYSDEC) standards, DOE derived concentration guides (DCGs), dose limits, and other DOE requirements. Results of environmental monitoring during 1992 indicate that levels of the parameters measured were in compliance with all but one requirement: Concentrations of iron and manganese in groundwater were above NYSDEC groundwater quality standards. However, these elements occur naturally in the soils and groundwater associated with this region. In 1992 there were no environmental occurrences or reportable quantity releases.

  2. "Middlesex" Meditations: Understanding and Teaching Intersex

    ERIC Educational Resources Information Center

    Breu, Christopher

    2009-01-01

    Teachers who include intersex issues in their curricula can provide their intersex students with a sense of community. Intersex people, whether children, teenagers, or adults, often feel that they are going through their experiences absolutely alone. For them, realizing that there are others out there with similar experiences, facing similar…

  3. Capillary sample

    MedlinePlus

    ... repeat the test with blood drawn from a vein. Alternative Names Blood sample - capillary; Fingerstick; Heelstick Images Phenylketonuria test Phenylketonuria test Capillary sample References Garza ...

  4. Venous Sampling

    MedlinePlus

    ... parts of the body, including: Adrenal venous sampling (AVS) , in which blood samples are taken from the ... for a few days before the procedure. For AVS, you will be asked to stop taking certain ...

  5. Laser sampling

    NASA Astrophysics Data System (ADS)

    Gorbatenko, A. A.; Revina, E. I.

    2015-10-01

    The review is devoted to the major advances in laser sampling. The advantages and drawbacks of the technique are considered. Specific features of combinations of laser sampling with various instrumental analytical methods, primarily inductively coupled plasma mass spectrometry, are discussed. Examples of practical implementation of hybrid methods involving laser sampling as well as corresponding analytical characteristics are presented. The bibliography includes 78 references.

  6. Lunar Sample Quarantine & Sample Curation

    NASA Technical Reports Server (NTRS)

    Allton, Judith H.

    2000-01-01

    The main goal of this presentation is to discuss some of the responsibility of the lunar sample quarantine project. The responsibilities are: flying the mission safely, and on schedule, protect the Earth from biohazard, and preserve scientific integrity of samples.

  7. Sampling Development

    PubMed Central

    Adolph, Karen E.; Robinson, Scott R.

    2011-01-01

    Research in developmental psychology requires sampling at different time points. Accurate depictions of developmental change provide a foundation for further empirical studies and theories about developmental mechanisms. However, overreliance on widely spaced sampling intervals in cross-sectional and longitudinal designs threatens the validity of the enterprise. This article discusses how to sample development in order to accurately discern the shape of developmental change. The ideal solution is daunting: to summarize behavior over 24-hour intervals and collect daily samples over the critical periods of change. We discuss the magnitude of errors due to undersampling, and the risks associated with oversampling. When daily sampling is not feasible, we offer suggestions for sampling methods that can provide preliminary reference points and provisional sketches of the general shape of a developmental trajectory. Denser sampling then can be applied strategically during periods of enhanced variability, inflections in the rate of developmental change, or in relation to key events or processes that may affect the course of change. Despite the challenges of dense repeated sampling, researchers must take seriously the problem of sampling on a developmental time scale if we are to know the true shape of developmental change. PMID:22140355

  8. Sampling Development

    ERIC Educational Resources Information Center

    Adolph, Karen E.; Robinson, Scott R.

    2011-01-01

    Research in developmental psychology requires sampling at different time points. Accurate depictions of developmental change provide a foundation for further empirical studies and theories about developmental mechanisms. However, overreliance on widely spaced sampling intervals in cross-sectional and longitudinal designs threatens the validity of…

  9. Elevating sampling

    PubMed Central

    Labuz, Joseph M.; Takayama, Shuichi

    2014-01-01

    Sampling – the process of collecting, preparing, and introducing an appropriate volume element (voxel) into a system – is often under appreciated and pushed behind the scenes in lab-on-a-chip research. What often stands in the way between proof-of-principle demonstrations of potentially exciting technology and its broader dissemination and actual use, however, is the effectiveness of sample collection and preparation. The power of micro- and nanofluidics to improve reactions, sensing, separation, and cell culture cannot be accessed if sampling is not equally efficient and reliable. This perspective will highlight recent successes as well as assess current challenges and opportunities in this area. PMID:24781100

  10. SAMPLING SYSTEM

    DOEpatents

    Hannaford, B.A.; Rosenberg, R.; Segaser, C.L.; Terry, C.L.

    1961-01-17

    An apparatus is given for the batch sampling of radioactive liquids such as slurries from a system by remote control, while providing shielding for protection of operating personnel from the harmful effects of radiation.

  11. SAMPLING OSCILLOSCOPE

    DOEpatents

    Sugarman, R.M.

    1960-08-30

    An oscilloscope is designed for displaying transient signal waveforms having random time and amplitude distributions. The oscilloscopc is a sampling device that selects for display a portion of only those waveforms having a particular range of amplitudes. For this purpose a pulse-height analyzer is provided to screen the pulses. A variable voltage-level shifter and a time-scale rampvoltage generator take the pulse height relative to the start of the waveform. The variable voltage shifter produces a voltage level raised one step for each sequential signal waveform to be sampled and this results in an unsmeared record of input signal waveforms. Appropriate delay devices permit each sample waveform to pass its peak amplitude before the circuit selects it for display.

  12. Sampling apparatus

    DOEpatents

    Gordon, N.R.; King, L.L.; Jackson, P.O.; Zulich, A.W.

    1989-07-18

    A sampling apparatus is provided for sampling substances from solid surfaces. The apparatus includes first and second elongated tubular bodies which telescopically and sealingly join relative to one another. An absorbent pad is mounted to the end of a rod which is slidably received through a passageway in the end of one of the joined bodies. The rod is preferably slidably and rotatably received through the passageway, yet provides a selective fluid tight seal relative thereto. A recess is formed in the rod. When the recess and passageway are positioned to be coincident, fluid is permitted to flow through the passageway and around the rod. The pad is preferably laterally orientable relative to the rod and foldably retractable to within one of the bodies. A solvent is provided for wetting of the pad and solubilizing or suspending the material being sampled from a particular surface. 15 figs.

  13. Sampling apparatus

    DOEpatents

    Gordon, Norman R.; King, Lloyd L.; Jackson, Peter O.; Zulich, Alan W.

    1989-01-01

    A sampling apparatus is provided for sampling substances from solid surfaces. The apparatus includes first and second elongated tubular bodies which telescopically and sealingly join relative to one another. An absorbent pad is mounted to the end of a rod which is slidably received through a passageway in the end of one of the joined bodies. The rod is preferably slidably and rotatably received through the passageway, yet provides a selective fluid tight seal relative thereto. A recess is formed in the rod. When the recess and passageway are positioned to be coincident, fluid is permitted to flow through the passageway and around the rod. The pad is preferably laterally orientable relative to the rod and foldably retractable to within one of the bodies. A solvent is provided for wetting of the pad and solubilizing or suspending the material being sampled from a particular surface.

  14. Chain Sampling

    DTIC Science & Technology

    1972-08-01

    35609 Advanced Techniques Branch Plans and Programs Analysis Division Directorate for Product Assurance U. S. Army Missile Command Redstone Arsenal...Ray Heathcock Advanced Techniques Branch Plans and Programs Analysis Division Directorate for Product Assurance U. S. Army Missile Command...for Product Assurance has established a rather unique computer program for handling a variety of chain sampling schemes and is available for

  15. Inquests into London and Middlesex Homicides, 1675-1782

    PubMed Central

    Forbes, Thomas R.

    1977-01-01

    Depositions for coroners' inquests on 377 deaths, nearly all of them homicides, were reviewed and analyzed for reported causes and circumstances of death. The role of coroner and surgeon and the emergence of the medicolegal autopsy are considered. PMID:331696

  16. Sampling Strategy

    NASA Technical Reports Server (NTRS)

    2008-01-01

    Three locations to the right of the test dig area are identified for the first samples to be delivered to the Thermal and Evolved Gas Analyzer (TEGA), the Wet Chemistry Lab (WCL), and the Optical Microscope (OM) on NASA's Phoenix Mars Lander. These sampling areas are informally labeled 'Baby Bear', 'Mama Bear', and 'Papa Bear' respectively. This image was taken on the seventh day of the Mars mission, or Sol 7 (June 1, 2008) by the Surface Stereo Imager aboard NASA's Phoenix Mars Lander.

    The Phoenix Mission is led by the University of Arizona, Tucson, on behalf of NASA. Project management of the mission is by NASA's Jet Propulsion Laboratory, Pasadena, Calif. Spacecraft development is by Lockheed Martin Space Systems, Denver.

  17. Coring Sample Acquisition Tool

    NASA Technical Reports Server (NTRS)

    Haddad, Nicolas E.; Murray, Saben D.; Walkemeyer, Phillip E.; Badescu, Mircea; Sherrit, Stewart; Bao, Xiaoqi; Kriechbaum, Kristopher L.; Richardson, Megan; Klein, Kerry J.

    2012-01-01

    A sample acquisition tool (SAT) has been developed that can be used autonomously to sample drill and capture rock cores. The tool is designed to accommodate core transfer using a sample tube to the IMSAH (integrated Mars sample acquisition and handling) SHEC (sample handling, encapsulation, and containerization) without ever touching the pristine core sample in the transfer process.

  18. Sampling by Length.

    ERIC Educational Resources Information Center

    Handley, John C.

    1991-01-01

    Discussion of sampling methods used in information science research focuses on Fussler's method for sampling catalog cards and on sampling by length. Highlights include simple random sampling, sampling with probability equal to size without replacement, sampling with replacement, and examples of estimating the number of books on shelves in certain…

  19. A Mars Sample Return Sample Handling System

    NASA Technical Reports Server (NTRS)

    Wilson, David; Stroker, Carol

    2013-01-01

    We present a sample handling system, a subsystem of the proposed Dragon landed Mars Sample Return (MSR) mission [1], that can return to Earth orbit a significant mass of frozen Mars samples potentially consisting of: rock cores, subsurface drilled rock and ice cuttings, pebble sized rocks, and soil scoops. The sample collection, storage, retrieval and packaging assumptions and concepts in this study are applicable for the NASA's MPPG MSR mission architecture options [2]. Our study assumes a predecessor rover mission collects samples for return to Earth to address questions on: past life, climate change, water history, age dating, understanding Mars interior evolution [3], and, human safety and in-situ resource utilization. Hence the rover will have "integrated priorities for rock sampling" [3] that cover collection of subaqueous or hydrothermal sediments, low-temperature fluidaltered rocks, unaltered igneous rocks, regolith and atmosphere samples. Samples could include: drilled rock cores, alluvial and fluvial deposits, subsurface ice and soils, clays, sulfates, salts including perchlorates, aeolian deposits, and concretions. Thus samples will have a broad range of bulk densities, and require for Earth based analysis where practical: in-situ characterization, management of degradation such as perchlorate deliquescence and volatile release, and contamination management. We propose to adopt a sample container with a set of cups each with a sample from a specific location. We considered two sample cups sizes: (1) a small cup sized for samples matching those submitted to in-situ characterization instruments, and, (2) a larger cup for 100 mm rock cores [4] and pebble sized rocks, thus providing diverse samples and optimizing the MSR sample mass payload fraction for a given payload volume. We minimize sample degradation by keeping them frozen in the MSR payload sample canister using Peltier chip cooling. The cups are sealed by interference fitted heat activated memory

  20. Ranked set sampling with unequal samples.

    PubMed

    Bhoj, D S

    2001-09-01

    A ranked set sampling procedure with unequal samples (RSSU) is proposed and used to estimate the population mean. This estimator is then compared with the estimators based on the ranked set sampling (RSS) and median ranked set sampling (MRSS) procedures. It is shown that the relative precisions of the estimator based on RSSU are higher than those of the estimators based on RSS and MRSS. An example of estimating the mean diameter at breast height of longleaf-pine trees on the Wade Tract in Thomas County, Georgia, is presented.

  1. How Sample Size Affects a Sampling Distribution

    ERIC Educational Resources Information Center

    Mulekar, Madhuri S.; Siegel, Murray H.

    2009-01-01

    If students are to understand inferential statistics successfully, they must have a profound understanding of the nature of the sampling distribution. Specifically, they must comprehend the determination of the expected value and standard error of a sampling distribution as well as the meaning of the central limit theorem. Many students in a high…

  2. Fluid sampling tool

    DOEpatents

    Garcia, Anthony R.; Johnston, Roger G.; Martinez, Ronald K.

    2000-01-01

    A fluid-sampling tool for obtaining a fluid sample from a container. When used in combination with a rotatable drill, the tool bores a hole into a container wall, withdraws a fluid sample from the container, and seals the borehole. The tool collects fluid sample without exposing the operator or the environment to the fluid or to wall shavings from the container.

  3. Enhanced conformational sampling using enveloping distribution sampling.

    PubMed

    Lin, Zhixiong; van Gunsteren, Wilfred F

    2013-10-14

    To lessen the problem of insufficient conformational sampling in biomolecular simulations is still a major challenge in computational biochemistry. In this article, an application of the method of enveloping distribution sampling (EDS) is proposed that addresses this challenge and its sampling efficiency is demonstrated in simulations of a hexa-β-peptide whose conformational equilibrium encompasses two different helical folds, i.e., a right-handed 2.7(10∕12)-helix and a left-handed 3(14)-helix, separated by a high energy barrier. Standard MD simulations of this peptide using the GROMOS 53A6 force field did not reach convergence of the free enthalpy difference between the two helices even after 500 ns of simulation time. The use of soft-core non-bonded interactions in the centre of the peptide did enhance the number of transitions between the helices, but at the same time led to neglect of relevant helical configurations. In the simulations of a two-state EDS reference Hamiltonian that envelops both the physical peptide and the soft-core peptide, sampling of the conformational space of the physical peptide ensures that physically relevant conformations can be visited, and sampling of the conformational space of the soft-core peptide helps to enhance the transitions between the two helices. The EDS simulations sampled many more transitions between the two helices and showed much faster convergence of the relative free enthalpy of the two helices compared with the standard MD simulations with only a slightly larger computational effort to determine optimized EDS parameters. Combined with various methods to smoothen the potential energy surface, the proposed EDS application will be a powerful technique to enhance the sampling efficiency in biomolecular simulations.

  4. Fort Devens Sudbury Training Annex Middlesex County Massachusetts Remedial (Data Gap) Investigations of Area of Contamination A4 and Areas of Combination A7/A9 (Management-of-Migration Operable Unit) and Supplemental Site Investigation Unit) and Supplemental Site Investigations of Selected Study Areas

    DTIC Science & Technology

    1996-05-01

    exploration locations and included I mercury (0.919 tg/g from boring OHM-A7-8), and lead (160 fzg/g from test pit A7TPK). Organic compounds including...chlorinated solvents in the 3 form of a dense nonaqueous-phase liquid ( DNAPL ) may have migrated down-dip on top of the dense till layer or on top of rock...confirmatory samples will be from the two deepest sampled depths. If a well is installed, a sump will be built into the well and the presence of U DNAPL will

  5. Apollo 14 rock samples

    NASA Technical Reports Server (NTRS)

    Carlson, I. C.

    1978-01-01

    Petrographic descriptions of all Apollo 14 samples larger than 1 cm in any dimension are presented. The sample description format consists of: (1) an introductory section which includes information on lunar sample location, orientation, and return containers, (2) a section on physical characteristics, which contains the sample mass, dimensions, and a brief description; (3) surface features, including zap pits, cavities, and fractures as seen in binocular view; (4) petrographic description, consisting of a binocular description and, if possible, a thin section description; and (5) a discussion of literature relevant to sample petrology is included for samples which have previously been examined by the scientific community.

  6. Rain sampling device

    DOEpatents

    Nelson, Danny A.; Tomich, Stanley D.; Glover, Donald W.; Allen, Errol V.; Hales, Jeremy M.; Dana, Marshall T.

    1991-01-01

    The present invention constitutes a rain sampling device adapted for independent operation at locations remote from the user which allows rainfall to be sampled in accordance with any schedule desired by the user. The rain sampling device includes a mechanism for directing wet precipitation into a chamber, a chamber for temporarily holding the precipitation during the process of collection, a valve mechanism for controllably releasing samples of said precipitation from said chamber, a means for distributing the samples released from the holding chamber into vessels adapted for permanently retaining these samples, and an electrical mechanism for regulating the operation of the device.

  7. Rain sampling device

    DOEpatents

    Nelson, D.A.; Tomich, S.D.; Glover, D.W.; Allen, E.V.; Hales, J.M.; Dana, M.T.

    1991-05-14

    The present invention constitutes a rain sampling device adapted for independent operation at locations remote from the user which allows rainfall to be sampled in accordance with any schedule desired by the user. The rain sampling device includes a mechanism for directing wet precipitation into a chamber, a chamber for temporarily holding the precipitation during the process of collection, a valve mechanism for controllably releasing samples of the precipitation from the chamber, a means for distributing the samples released from the holding chamber into vessels adapted for permanently retaining these samples, and an electrical mechanism for regulating the operation of the device. 11 figures.

  8. Stardust Sample: Investigator's Guidebook

    NASA Technical Reports Server (NTRS)

    Allen, Carl

    2006-01-01

    In January 2006, the Stardust spacecraft returned the first in situ collection of samples from a comet, and the first samples of contemporary interstellar dust. Stardust is the first US sample return mission from a planetary body since Apollo, and the first ever from beyond the moon. This handbook is a basic reference source for allocation procedures and policies for Stardust samples. These samples consist of particles and particle residues in aerogel collectors, in aluminum foil, and in spacecraft components. Contamination control samples and unflown collection media are also available for allocation.

  9. GROUND WATER SAMPLING ISSUES

    EPA Science Inventory

    Obtaining representative ground water samples is important for site assessment and
    remedial performance monitoring objectives. Issues which must be considered prior to initiating a ground-water monitoring program include defining monitoring goals and objectives, sampling point...

  10. Improved Sampling Method Reduces Isokinetic Sampling Errors.

    ERIC Educational Resources Information Center

    Karels, Gale G.

    The particulate sampling system currently in use by the Bay Area Air Pollution Control District, San Francisco, California is described in this presentation for the 12th Conference on Methods in Air Pollution and Industrial Hygiene Studies, University of Southern California, April, 1971. The method represents a practical, inexpensive tool that can…

  11. Decision by Sampling

    ERIC Educational Resources Information Center

    Stewart, Neil; Chater, Nick; Brown, Gordon D. A.

    2006-01-01

    We present a theory of decision by sampling (DbS) in which, in contrast with traditional models, there are no underlying psychoeconomic scales. Instead, we assume that an attribute's subjective value is constructed from a series of binary, ordinal comparisons to a sample of attribute values drawn from memory and is its rank within the sample. We…

  12. Developing Water Sampling Standards

    ERIC Educational Resources Information Center

    Environmental Science and Technology, 1974

    1974-01-01

    Participants in the D-19 symposium on aquatic sampling and measurement for water pollution assessment were informed that determining the extent of waste water stream pollution is not a cut and dry procedure. Topics discussed include field sampling, representative sampling from storm sewers, suggested sampler features and application of improved…

  13. SAMPLING OF CONTAMINATED SITES

    EPA Science Inventory

    A critical aspect of characterization of the amount and species of contamination of a hazardous waste site is the sampling plan developed for that site. f the sampling plan is not thoroughly conceptualized before sampling takes place, then certain critical aspects of the limits o...

  14. Fluid sampling pump

    SciTech Connect

    Allen, P.V.; Nimberger, M.; Ward, R.L.

    1991-12-24

    This patent describes a fluid sampling pump for withdrawing pressurized sample fluid from a flow line and for pumping a preselected quantity of sample fluid with each pump driving stroke from the pump to a sample vessel, the sampling pump including a pump body defining a pump bore therein having a central axis, a piston slideably moveable within the pump bore and having a fluid inlet end and an opposing operator end, a fluid sample inlet port open to sample fluid in the flow line, a fluid sample outlet port for transmitting fluid from the pump bore to the sample vessel, and a line pressure port in fluid pressure sample fluid in the flow line, an inlet valve for selectively controlling sample fluid flow from the flow line through the fluid sample inlet port, an operator unit for periodically reciprocating the piston within the pump bore, and a controller for regulating the stroke of the piston within the pump bore, and thereby the quantity of fluid pumped with each pump driving stroke. It comprises a balanced check valve seat; a balanced check valve seal; a compression member; and a central plunger.

  15. Aerosol sampling system

    DOEpatents

    Masquelier, Donald A.

    2004-02-10

    A system for sampling air and collecting particulate of a predetermined particle size range. A low pass section has an opening of a preselected size for gathering the air but excluding particles larger than the sample particles. An impactor section is connected to the low pass section and separates the air flow into a bypass air flow that does not contain the sample particles and a product air flow that does contain the sample particles. A wetted-wall cyclone collector, connected to the impactor section, receives the product air flow and traps the sample particles in a liquid.

  16. Rockballer Sample Acquisition Tool

    NASA Technical Reports Server (NTRS)

    Giersch, Louis R.; Cook, Brant T.

    2013-01-01

    It would be desirable to acquire rock and/or ice samples that extend below the surface of the parent rock or ice in extraterrestrial environments such as the Moon, Mars, comets, and asteroids. Such samples would allow measurements to be made further back into the geologic history of the rock, providing critical insight into the history of the local environment and the solar system. Such samples could also be necessary for sample return mission architectures that would acquire samples from extraterrestrial environments for return to Earth for more detailed scientific investigation.

  17. Vicinity Property Assessments at Formerly Utilized Sites Remedial Action Program Project Sites in the New York District - 13420

    SciTech Connect

    Ewy, Ann; Hays, David

    2013-07-01

    The Formerly Utilized Sites Remedial Action Program (FUSRAP) has addressed sites across the nation for almost 4 decades. Multiple stake holder pressures, multiple regulations, and process changes occur over such long time periods. These result in many challenges to the FUSRAP project teams. Initial FUSRAP work was not performed under Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA) Records of Decision (ROD). The ROD identifies the remedy decision and ultimately the criteria to be used to release a site. Early FUSRAP projects used DOE Orders or the Uranium Mill Tailings Radiation Control Act (UMTRCA) standards. Under current RODs, regulations may differ, resulting in different cleanup criteria than that used in prior Vicinity Property (VP) remediation. The USACE, in preparation for closeout of Sites, conducts reviews to evaluate whether prior actions were sufficient to meet the cleanup criteria specified in the current ROD. On the basis of these reviews, USACE has conducted additional sampling, determined that prior actions were sufficient, or conducted additional remediation consistent with the selected remedy in the ROD. As the public pressures, regulations, and processes that the FUSRAP encounters continue to change, the program itself continues to evolve. Assessment of VPs at FUSRAP sites is a necessary step in the life cycle of our site management. (authors)

  18. Sample Proficiency Test exercise

    SciTech Connect

    Alcaraz, A; Gregg, H; Koester, C

    2006-02-05

    The current format of the OPCW proficiency tests has multiple sets of 2 samples sent to an analysis laboratory. In each sample set, one is identified as a sample, the other as a blank. This method of conducting proficiency tests differs from how an OPCW designated laboratory would receive authentic samples (a set of three containers, each not identified, consisting of the authentic sample, a control sample, and a blank sample). This exercise was designed to test the reporting if the proficiency tests were to be conducted. As such, this is not an official OPCW proficiency test, and the attached report is one method by which LLNL might report their analyses under a more realistic testing scheme. Therefore, the title on the report ''Report of the Umpteenth Official OPCW Proficiency Test'' is meaningless, and provides a bit of whimsy for the analyses and readers of the report.

  19. Sample size calculations.

    PubMed

    Noordzij, Marlies; Dekker, Friedo W; Zoccali, Carmine; Jager, Kitty J

    2011-01-01

    The sample size is the number of patients or other experimental units that need to be included in a study to answer the research question. Pre-study calculation of the sample size is important; if a sample size is too small, one will not be able to detect an effect, while a sample that is too large may be a waste of time and money. Methods to calculate the sample size are explained in statistical textbooks, but because there are many different formulas available, it can be difficult for investigators to decide which method to use. Moreover, these calculations are prone to errors, because small changes in the selected parameters can lead to large differences in the sample size. This paper explains the basic principles of sample size calculations and demonstrates how to perform such a calculation for a simple study design.

  20. Curation of Frozen Samples

    NASA Technical Reports Server (NTRS)

    Fletcher, L. A.; Allen, C. C.; Bastien, R.

    2008-01-01

    NASA's Johnson Space Center (JSC) and the Astromaterials Curator are charged by NPD 7100.10D with the curation of all of NASA s extraterrestrial samples, including those from future missions. This responsibility includes the development of new sample handling and preparation techniques; therefore, the Astromaterials Curator must begin developing procedures to preserve, prepare and ship samples at sub-freezing temperatures in order to enable future sample return missions. Such missions might include the return of future frozen samples from permanently-shadowed lunar craters, the nuclei of comets, the surface of Mars, etc. We are demonstrating the ability to curate samples under cold conditions by designing, installing and testing a cold curation glovebox. This glovebox will allow us to store, document, manipulate and subdivide frozen samples while quantifying and minimizing contamination throughout the curation process.

  1. The Lunar Sample Compendium

    NASA Technical Reports Server (NTRS)

    Meyer, Charles

    2009-01-01

    The Lunar Sample Compendium is a succinct summary of the data obtained from 40 years of study of Apollo and Luna samples of the Moon. Basic petrographic, chemical and age information is compiled, sample-by-sample, in the form of an advanced catalog in order to provide a basic description of each sample. The LSC can be found online using Google. The initial allocation of lunar samples was done sparingly, because it was realized that scientific techniques would improve over the years and new questions would be formulated. The LSC is important because it enables scientists to select samples within the context of the work that has already been done and facilitates better review of proposed allocations. It also provides back up material for public displays, captures information found only in abstracts, grey literature and curatorial databases and serves as a ready access to the now-vast scientific literature.

  2. Lunar Sample Compendium

    NASA Technical Reports Server (NTRS)

    Meyer, C.

    2009-01-01

    The Lunar Sample Compendium is a succinct summary of what has been learned from the study of Apollo and Luna samples of the Moon. Basic information is compiled, sample-by-sample, in the form of an advanced catalog in order to provide a basic description of each sample. Information presented is carefully attributed to the original source publication, thus the Compendium also serves as a ready access to the now vast scientific literature pertaining to lunar smples. The Lunar Sample Compendium is a work in progress (and may always be). Future plans include: adding sections on additional samples, adding new thin section photomicrographs, replacing the faded photographs with newly digitized photos from the original negatives, attempting to correct the age data using modern decay constants, adding references to each section, and adding an internal search engine.

  3. Urine sample collection protocols for bioassay samples

    SciTech Connect

    MacLellan, J.A.; McFadden, K.M.

    1992-11-01

    In vitro radiobioassay analyses are used to measure the amount of radioactive material excreted by personnel exposed to the potential intake of radioactive material. The analytical results are then used with various metabolic models to estimate the amount of radioactive material in the subject`s body and the original intake of radioactive material. Proper application of these metabolic models requires knowledge of the excretion period. It is normal practice to design the bioassay program based on a 24-hour excretion sample. The Hanford bioassay program simulates a total 24-hour urine excretion sample with urine collection periods lasting from one-half hour before retiring to one-half hour after rising on two consecutive days. Urine passed during the specified periods is collected in three 1-L bottles. Because the daily excretion volume given in Publication 23 of the International Commission on Radiological Protection (ICRP 1975, p. 354) for Reference Man is 1.4 L, it was proposed to use only two 1-L bottles as a cost-saving measure. This raised the broader question of what should be the design capacity of a 24-hour urine sample kit.

  4. Urine sample collection protocols for bioassay samples

    SciTech Connect

    MacLellan, J.A.; McFadden, K.M.

    1992-11-01

    In vitro radiobioassay analyses are used to measure the amount of radioactive material excreted by personnel exposed to the potential intake of radioactive material. The analytical results are then used with various metabolic models to estimate the amount of radioactive material in the subject's body and the original intake of radioactive material. Proper application of these metabolic models requires knowledge of the excretion period. It is normal practice to design the bioassay program based on a 24-hour excretion sample. The Hanford bioassay program simulates a total 24-hour urine excretion sample with urine collection periods lasting from one-half hour before retiring to one-half hour after rising on two consecutive days. Urine passed during the specified periods is collected in three 1-L bottles. Because the daily excretion volume given in Publication 23 of the International Commission on Radiological Protection (ICRP 1975, p. 354) for Reference Man is 1.4 L, it was proposed to use only two 1-L bottles as a cost-saving measure. This raised the broader question of what should be the design capacity of a 24-hour urine sample kit.

  5. Air Conditioning and Refrigeration. Volume XXVI. 1975 Edition of Course of Study Outlines. Middlesex County Vocational and Technical High Schools and Middlesex County Adult Technical Schools.

    ERIC Educational Resources Information Center

    Capizzi, James

    The two courses of study described and outlined here are offered at Burr D. Coe Vocational and Technical High School in East Brunswick, New Jersey, for students wishing to prepare for a career in air conditioning and refrigeration. Section 1 deals with a 4-year high school course, Section 2 with a 1-year course for those who have completed high…

  6. Sampling functions for geophysics

    NASA Technical Reports Server (NTRS)

    Giacaglia, G. E. O.; Lunquist, C. A.

    1972-01-01

    A set of spherical sampling functions is defined such that they are related to spherical-harmonic functions in the same way that the sampling functions of information theory are related to sine and cosine functions. An orderly distribution of (N + 1) squared sampling points on a sphere is given, for which the (N + 1) squared spherical sampling functions span the same linear manifold as do the spherical-harmonic functions through degree N. The transformations between the spherical sampling functions and the spherical-harmonic functions are given by recurrence relations. The spherical sampling functions of two arguments are extended to three arguments and to nonspherical reference surfaces. Typical applications of this formalism to geophysical topics are sketched.

  7. Sampling in Qualitative Research

    PubMed Central

    LUBORSKY, MARK R.; RUBINSTEIN, ROBERT L.

    2011-01-01

    In gerontology the most recognized and elaborate discourse about sampling is generally thought to be in quantitative research associated with survey research and medical research. But sampling has long been a central concern in the social and humanistic inquiry, albeit in a different guise suited to the different goals. There is a need for more explicit discussion of qualitative sampling issues. This article will outline the guiding principles and rationales, features, and practices of sampling in qualitative research. It then describes common questions about sampling in qualitative research. In conclusion it proposes the concept of qualitative clarity as a set of principles (analogous to statistical power) to guide assessments of qualitative sampling in a particular study or proposal. PMID:22058580

  8. Sample positioning in microgravity

    NASA Technical Reports Server (NTRS)

    Sridharan, Govind (Inventor)

    1993-01-01

    Repulsion forces arising from laser beams are provided to produce mild positioning forces on a sample in microgravity vacuum environments. The system of the preferred embodiment positions samples using a plurality of pulsed lasers providing opposing repulsion forces. The lasers are positioned around the periphery of a confinement area and expanded to create a confinement zone. The grouped laser configuration, in coordination with position sensing devices, creates a feedback servo whereby stable position control of a sample within microgravity environment can be achieved.

  9. Statistical distribution sampling

    NASA Technical Reports Server (NTRS)

    Johnson, E. S.

    1975-01-01

    Determining the distribution of statistics by sampling was investigated. Characteristic functions, the quadratic regression problem, and the differential equations for the characteristic functions are analyzed.

  10. National Sample Assessment Protocols

    ERIC Educational Resources Information Center

    Ministerial Council on Education, Employment, Training and Youth Affairs (NJ1), 2012

    2012-01-01

    These protocols represent a working guide for planning and implementing national sample assessments in connection with the national Key Performance Measures (KPMs). The protocols are intended for agencies involved in planning or conducting national sample assessments and personnel responsible for administering associated tenders or contracts,…

  11. Sampling system and method

    DOEpatents

    Decker, David L.; Lyles, Brad F.; Purcell, Richard G.; Hershey, Ronald Lee

    2013-04-16

    The present disclosure provides an apparatus and method for coupling conduit segments together. A first pump obtains a sample and transmits it through a first conduit to a reservoir accessible by a second pump. The second pump further conducts the sample from the reservoir through a second conduit.

  12. Implementing Teacher Work Sampling

    ERIC Educational Resources Information Center

    Kinne, Lenore J.; Watson, Dwight C.

    2005-01-01

    This article describes how the teacher work sample methodology of the Renaissance Partnership for Improving Teacher Quality was implemented within the teacher education program at a small liberal arts college. Resulting program improvements are described, as well as on-going challenges. The adapted teacher work sample prompt and scoring rubric are…

  13. Extraterrestrial Samples at JSC

    NASA Technical Reports Server (NTRS)

    Allen, Carlton C.

    2007-01-01

    A viewgraph presentation on the curation of extraterrestrial samples at NASA Johnson Space Center is shown. The topics include: 1) Apollo lunar samples; 2) Meteorites from Antarctica; 3) Cosmic dust from the stratosphere; 4) Genesis solar wind ions; 5) Stardust comet and interstellar grains; and 5) Space-Exposed Hardware.

  14. Urine sample (image)

    MedlinePlus

    A "clean-catch" urine sample is performed by collecting the sample of urine in midstream. Men or boys should wipe clean the head ... water and rinse well. A small amount of urine should initially fall into the toilet bowl before ...

  15. Biological sample collector

    DOEpatents

    Murphy, Gloria A.

    2010-09-07

    A biological sample collector is adapted to a collect several biological samples in a plurality of filter wells. A biological sample collector may comprise a manifold plate for mounting a filter plate thereon, the filter plate having a plurality of filter wells therein; a hollow slider for engaging and positioning a tube that slides therethrough; and a slide case within which the hollow slider travels to allow the tube to be aligned with a selected filter well of the plurality of filter wells, wherein when the tube is aligned with the selected filter well, the tube is pushed through the hollow slider and into the selected filter well to sealingly engage the selected filter well and to allow the tube to deposit a biological sample onto a filter in the bottom of the selected filter well. The biological sample collector may be portable.

  16. Rapid Active Sampling Package

    NASA Technical Reports Server (NTRS)

    Peters, Gregory

    2010-01-01

    A field-deployable, battery-powered Rapid Active Sampling Package (RASP), originally designed for sampling strong materials during lunar and planetary missions, shows strong utility for terrestrial geological use. The technology is proving to be simple and effective for sampling and processing materials of strength. Although this originally was intended for planetary and lunar applications, the RASP is very useful as a powered hand tool for geologists and the mining industry to quickly sample and process rocks in the field on Earth. The RASP allows geologists to surgically acquire samples of rock for later laboratory analysis. This tool, roughly the size of a wrench, allows the user to cut away swaths of weathering rinds, revealing pristine rock surfaces for observation and subsequent sampling with the same tool. RASPing deeper (.3.5 cm) exposes single rock strata in-situ. Where a geologist fs hammer can only expose unweathered layers of rock, the RASP can do the same, and then has the added ability to capture and process samples into powder with particle sizes less than 150 microns, making it easier for XRD/XRF (x-ray diffraction/x-ray fluorescence). The tool uses a rotating rasp bit (or two counter-rotating bits) that resides inside or above the catch container. The container has an open slot to allow the bit to extend outside the container and to allow cuttings to enter and be caught. When the slot and rasp bit are in contact with a substrate, the bit is plunged into it in a matter of seconds to reach pristine rock. A user in the field may sample a rock multiple times at multiple depths in minutes, instead of having to cut out huge, heavy rock samples for transport back to a lab for analysis. Because of the speed and accuracy of the RASP, hundreds of samples can be taken in one day. RASP-acquired samples are small and easily carried. A user can characterize more area in less time than by using conventional methods. The field-deployable RASP used a Ni

  17. Waste classification sampling plan

    SciTech Connect

    Landsman, S.D.

    1998-05-27

    The purpose of this sampling is to explain the method used to collect and analyze data necessary to verify and/or determine the radionuclide content of the B-Cell decontamination and decommissioning waste stream so that the correct waste classification for the waste stream can be made, and to collect samples for studies of decontamination methods that could be used to remove fixed contamination present on the waste. The scope of this plan is to establish the technical basis for collecting samples and compiling quantitative data on the radioactive constituents present in waste generated during deactivation activities in B-Cell. Sampling and radioisotopic analysis will be performed on the fixed layers of contamination present on structural material and internal surfaces of process piping and tanks. In addition, dose rate measurements on existing waste material will be performed to determine the fraction of dose rate attributable to both removable and fixed contamination. Samples will also be collected to support studies of decontamination methods that are effective in removing the fixed contamination present on the waste. Sampling performed under this plan will meet criteria established in BNF-2596, Data Quality Objectives for the B-Cell Waste Stream Classification Sampling, J. M. Barnett, May 1998.

  18. Instructions for borehole sampling

    SciTech Connect

    Reynolds, K.D.; Lindsey, K.A.

    1994-11-11

    Geologic systems generally are complex with physical properties and trends that can be difficult to predict. Subsurface geology exerts a fundamental control on groundwater flow and contaminant transport. The primary source for direct observation of subsurface geologic information is a borehole. However, direct observations from a borehole essentially are limited to the diameter and spacing of boreholes and the quality of the information derived from the drilling. Because it is impractical to drill a borehole every few feet to obtain data, it is necessary to maximize the data gathered during limited drilling operations. A technically defensible balance between the customer`s data quality objectives and control of drilling costs through limited drilling can be achieved with proper conduct of operations. This report presents the minimum criteria for geologic and hydrologic characterization and sampling that must be met during drilling. It outlines the sampling goals that need to be addressed when drilling boreholes, and the types of drilling techniques that work best to achieve these goals under the geologic conditions found at Hanford. This report provides general guidelines for: (1) how sampling methods are controlled by data needs, (2) how minimum sampling requirements change as knowledge and needs change, and (3) when drilling and sampling parameters need to be closely controlled with respect to the specific data needs. Consequently, the report is divided into two sections that center on: (1) a discussion of basic categories of subsurface characterization, sampling, and sampling techniques, and (2) guidelines for determining which drilling and sampling techniques meet required characterization and sampling objectives.

  19. Sample quality criteria.

    PubMed

    Ramsey, Charles A; Wagner, Claas

    2015-01-01

    The concept of Sample Quality Criteria (SQC) is the initial step in the scientific approach to representative sampling. It includes the establishment of sampling objectives, Decision Unit (DU), and confidence. Once fully defined, these criteria serve as input, in addition to material properties, to the Theory of Sampling for developing a representative sampling protocol. The first component of the SQC establishes these questions: What is the analyte(s) of concern? What is the concentration level of interest of the analyte(s)? How will inference(s) be made from the analytical data to the DU? The second component of the SQC establishes the DU, i.e., the scale at which decisions are to be made. On a large scale, a DU could be a ship or rail car; examples for small-scale DUs are individual beans, seeds, or kernels. A well-defined DU is critical because it defines the spatial and temporal boundaries of sample collection. SQC are not limited to a single DU; they can also include multiple DUs. The third SQC component, the confidence, establishes the desired probability that a correct inference (decision) can be made. The confidence level should typically correlate to the potential consequences of an incorrect decision (e.g., health or economic). The magnitude of combined errors in the sampling, sample processing and analytical protocols determines the likelihood of an incorrect decision. Thus, controlling error to a greater extent increases the probability of a correct decision. The required confidence level directly affects the sampling effort and QC measures.

  20. Sampling video compression system

    NASA Technical Reports Server (NTRS)

    Matsumoto, Y.; Lum, H. (Inventor)

    1977-01-01

    A system for transmitting video signal of compressed bandwidth is described. The transmitting station is provided with circuitry for dividing a picture to be transmitted into a plurality of blocks containing a checkerboard pattern of picture elements. Video signals along corresponding diagonal rows of picture elements in the respective blocks are regularly sampled. A transmitter responsive to the output of the sampling circuitry is included for transmitting the sampled video signals of one frame at a reduced bandwidth over a communication channel. The receiving station is provided with a frame memory for temporarily storing transmitted video signals of one frame at the original high bandwidth frequency.

  1. Sealed container sampling device

    NASA Technical Reports Server (NTRS)

    Hennigan, T. J.

    1969-01-01

    Sampling device, by means of a tapered needle, pierces a sealed container while maintaining the seal and either evacuates or pressurizes the container. This device has many applications in the chemical, preservative and battery-manufacturing industries.

  2. Soil Gas Sampling

    EPA Pesticide Factsheets

    Field Branches Quality System and Technical Procedures: This document describes general and specific procedures, methods and considerations to be used and observed when collecting soil gas samples for field screening or laboratory analysis.

  3. Lunar sample contracts

    NASA Technical Reports Server (NTRS)

    Walker, R. M.

    1974-01-01

    The major scientific accomplishments through 1971 are reported for the particle track studies of lunar samples. Results are discussed of nuclear track measurements by optical and electron microscopy, thermoluminescence, X-ray diffraction, and differential thermal analysis.

  4. Water Sample Concentrator

    SciTech Connect

    Idaho National Laboratory

    2009-07-21

    Automated portable device that concentrates and packages a sample of suspected contaminated water for safe, efficient transport to a qualified analytical laboratory. This technology will help safeguard against pathogen contamination or chemical and biolog

  5. Sample positioning apparatus

    DOEpatents

    Bell, Thomas H.; Johnson, Jr., Charles H.; Lane, Robert L.; Martin, Bradley E.; Tyree, William H.

    1976-01-06

    Apparatus for use in alpha particle counting with such as photomultiplier tubes, comprising a platform and linkage mechanism whereby samples are moved in linear manner toward and away from ends of the photomultiplier tubes.

  6. Water Sample Concentrator

    ScienceCinema

    Idaho National Laboratory

    2016-07-12

    Automated portable device that concentrates and packages a sample of suspected contaminated water for safe, efficient transport to a qualified analytical laboratory. This technology will help safeguard against pathogen contamination or chemical and biolog

  7. Dissolution actuated sample container

    SciTech Connect

    Nance, Thomas A.; McCoy, Frank T.

    2013-03-26

    A sample collection vial and process of using a vial is provided. The sample collection vial has an opening secured by a dissolvable plug. When dissolved, liquids may enter into the interior of the collection vial passing along one or more edges of a dissolvable blocking member. As the blocking member is dissolved, a spring actuated closure is directed towards the opening of the vial which, when engaged, secures the vial contents against loss or contamination.

  8. TANK 5 SAMPLING

    SciTech Connect

    Vrettos, N; William Cheng, W; Thomas Nance, T

    2007-11-26

    Tank 5 at the Savannah River Site has been used to store high level waste and is currently undergoing waste removal processes in preparation for tank closure. Samples were taken from two locations to determine the contents in support of Documented Safety Analysis (DSA) development for chemical cleaning. These samples were obtained through the use of the Drop Core Sampler and the Snowbank Sampler developed by the Engineered Equipment & Systems (EES) group of the Savannah River National Laboratory (SRNL).

  9. SAMPLING AND ANALYSIS PROTOCOLS

    SciTech Connect

    Jannik, T; P Fledderman, P

    2007-02-09

    Radiological sampling and analyses are performed to collect data for a variety of specific reasons covering a wide range of projects. These activities include: Effluent monitoring; Environmental surveillance; Emergency response; Routine ambient monitoring; Background assessments; Nuclear license termination; Remediation; Deactivation and decommissioning (D&D); and Waste management. In this chapter, effluent monitoring and environmental surveillance programs at nuclear operating facilities and radiological sampling and analysis plans for remediation and D&D activities will be discussed.

  10. Lunar Sample Compendium

    NASA Technical Reports Server (NTRS)

    Meyer, Charles

    2005-01-01

    The purpose of the Lunar Sample Compendium will be to inform scientists, astronauts and the public about the various lunar samples that have been returned from the Moon. This Compendium will be organized rock by rock in the manor of a catalog, but will not be as comprehensive, nor as complete, as the various lunar sample catalogs that are available. Likewise, this Compendium will not duplicate the various excellent books and reviews on the subject of lunar samples (Cadogen 1981, Heiken et al. 1991, Papike et al. 1998, Warren 2003, Eugster 2003). However, it is thought that an online Compendium, such as this, will prove useful to scientists proposing to study individual lunar samples and should help provide backup information for lunar sample displays. This Compendium will allow easy access to the scientific literature by briefly summarizing the significant findings of each rock along with the documentation of where the detailed scientific data are to be found. In general, discussion and interpretation of the results is left to the formal reviews found in the scientific literature. An advantage of this Compendium will be that it can be updated, expanded and corrected as need be.

  11. Liquid sampling system

    DOEpatents

    Larson, L.L.

    1984-09-17

    A conduit extends from a reservoir through a sampling station and back to the reservoir in a closed loop. A jet ejector in the conduit establishes suction for withdrawing liquid from the reservoir. The conduit has a self-healing septum therein upstream of the jet ejector for receiving one end of a double-ended cannula, the other end of which is received in a serum bottle for sample collection. Gas is introduced into the conduit at a gas bleed between the sample collection bottle and the reservoir. The jet ejector evacuates gas from the conduit and the bottle and aspirates a column of liquid from the reservoir at a high rate. When the withdrawn liquid reaches the jet ejector the rate of flow therethrough reduces substantially and the gas bleed increases the pressure in the conduit for driving liquid into the sample bottle, the gas bleed forming a column of gas behind the withdrawn liquid column and interrupting the withdrawal of liquid from the reservoir. In the case of hazardous and toxic liquids, the sample bottle and the jet ejector may be isolated from the reservoir and may be further isolated from a control station containing remote manipulation means for the sample bottle and control valves for the jet ejector and gas bleed. 5 figs.

  12. Liquid sampling system

    DOEpatents

    Larson, Loren L.

    1987-01-01

    A conduit extends from a reservoir through a sampling station and back to the reservoir in a closed loop. A jet ejector in the conduit establishes suction for withdrawing liquid from the reservoir. The conduit has a self-healing septum therein upstream of the jet ejector for receiving one end of a double-ended cannula, the other end of which is received in a serum bottle for sample collection. Gas is introduced into the conduit at a gas bleed between the sample collection bottle and the reservoir. The jet ejector evacuates gas from the conduit and the bottle and aspirates a column of liquid from the reservoir at a high rate. When the withdrawn liquid reaches the jet ejector the rate of flow therethrough reduces substantially and the gas bleed increases the pressure in the conduit for driving liquid into the sample bottle, the gas bleed forming a column of gas behind the withdrawn liquid column and interrupting the withdrawal of liquid from the reservoir. In the case of hazardous and toxic liquids, the sample bottle and the jet ejector may be isolated from the reservoir and may be further isolated from a control station containing remote manipulation means for the sample bottle and control valves for the jet ejector and gas bleed.

  13. Sample Return Science

    NASA Astrophysics Data System (ADS)

    Williford, K. H.; Allwood, A.; Beegle, L. W.; Bhartia, R.; Flannery, D.; Hoffmann, A.; Mora, M. F.; Orbay, J.; Petrizzo, D. A.; Tuite, M. L., Jr.; Willis, P. A.

    2014-12-01

    The first clear identification of an ancient habitable environment on Mars by the Mars Science Laboratory (MSL) rover mission relied on a synthetic analytical approach combining orbital and surface imagery and spectroscopy with sophisticated sample acquisition and handling technology including a rotary percussive drill that provided powdered rock for bulk geochemical analysis [1]. The recent announcement of the instrument package for the proposed NASA Mars2020 rover mission, including micro x-ray fluorescence (PIXL) for elemental mapping as well as scanning ultraviolet laser fluorescence and Raman (SHERLOC) suggests a shift in emphasis of Mars surface science towards spatially resolved geochemical analysis that will support the selection and acquisition of samples for coring, caching, and possible return to Earth for further analysis. During a recent field expedition to investigate Archean and Proterozoic biosignatures in the Pilbara region of Western Australia, we deployed a dry, rotary percussive coring drill with a bit assembly analogous to that being considered for Mars2020. Six targets of varying age and lithology were sampled with the coring drill, and surrounding and adjacent rock samples were collected simultaneously. These samples were subsequently prepared and subsampled for bulk and in situ, spatially resolved analysis using conventional laboratory methods as well as the existing PIXL and SHERLOC platforms currently in development. Here we present new approaches and data from this integrated and ongoing program of "sample return science" designed to simulate, and eventually reduce risk associated with a long-term effort towards Mars sample return. [1] Grotzinger, J.P. et al. 2014. Science 343 DOI: 10.1126/science.1242777.

  14. Fluid sampling system

    DOEpatents

    Houck, E.D.

    1994-10-11

    An fluid sampling system allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped upwardly into a sampling jet of a venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to be decreased, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodically leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank. 4 figs.

  15. Fluid sampling system

    DOEpatents

    Houck, Edward D.

    1994-01-01

    An fluid sampling system allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped upwardly into a sampling jet of a venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to decreased, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodically leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank.

  16. Core sample extractor

    NASA Technical Reports Server (NTRS)

    Akins, James; Cobb, Billy; Hart, Steve; Leaptrotte, Jeff; Milhollin, James; Pernik, Mark

    1989-01-01

    The problem of retrieving and storing core samples from a hole drilled on the lunar surface is addressed. The total depth of the hole in question is 50 meters with a maximum diameter of 100 millimeters. The core sample itself has a diameter of 60 millimeters and will be two meters in length. It is therefore necessary to retrieve and store 25 core samples per hole. The design utilizes a control system that will stop the mechanism at a certain depth, a cam-linkage system that will fracture the core, and a storage system that will save and catalogue the cores to be extracted. The Rod Changer and Storage Design Group will provide the necessary tooling to get into the hole as well as to the core. The mechanical design for the cam-linkage system as well as the conceptual design of the storage device are described.

  17. Experimental scattershot boson sampling

    PubMed Central

    Bentivegna, Marco; Spagnolo, Nicolò; Vitelli, Chiara; Flamini, Fulvio; Viggianiello, Niko; Latmiral, Ludovico; Mataloni, Paolo; Brod, Daniel J.; Galvão, Ernesto F.; Crespi, Andrea; Ramponi, Roberta; Osellame, Roberto; Sciarrino, Fabio

    2015-01-01

    Boson sampling is a computational task strongly believed to be hard for classical computers, but efficiently solvable by orchestrated bosonic interference in a specialized quantum computer. Current experimental schemes, however, are still insufficient for a convincing demonstration of the advantage of quantum over classical computation. A new variation of this task, scattershot boson sampling, leads to an exponential increase in speed of the quantum device, using a larger number of photon sources based on parametric down-conversion. This is achieved by having multiple heralded single photons being sent, shot by shot, into different random input ports of the interferometer. We report the first scattershot boson sampling experiments, where six different photon-pair sources are coupled to integrated photonic circuits. We use recently proposed statistical tools to analyze our experimental data, providing strong evidence that our photonic quantum simulator works as expected. This approach represents an important leap toward a convincing experimental demonstration of the quantum computational supremacy. PMID:26601164

  18. INEL Sample Management Office

    SciTech Connect

    Watkins, C.

    1994-12-31

    The Idaho National Engineering Laboratory (INEL) Sample Management Office (SMO) was formed as part of the EG&G Idaho Environmental Restoration Program (ERP) in June, 1990. Since then, the SMO has been recognized and sought out by other prime contractors and programs at the INEL. Since December 1991, the DOE-ID Division Directors for the Environmental Restoration Division and Waste Management Division supported the expansion of the INEL ERP SMO into the INEL site wide SMO. The INEL SMO serves as a point of contact for multiple environmental analytical chemistry and laboratory issues (e.g., capacity, capability). The SMO chemists work with project managers during planning to help develop data quality objectives, select appropriate analytical methods, identify special analytical services needs, identify a source for the services, and ensure that requirements for sampling and analysis (e.g., preservations, sample volumes) are clear and technically accurate. The SMO chemists also prepare work scope statements for the laboratories performing the analyses.

  19. Viscous sludge sample collector

    DOEpatents

    Beitel, George A [Richland, WA

    1983-01-01

    A vertical core sample collection system for viscous sludge. A sample tube's upper end has a flange and is attached to a piston. The tube and piston are located in the upper end of a bore in a housing. The bore's lower end leads outside the housing and has an inwardly extending rim. Compressed gas, from a storage cylinder, is quickly introduced into the bore's upper end to rapidly accelerate the piston and tube down the bore. The lower end of the tube has a high sludge entering velocity to obtain a full-length sludge sample without disturbing strata detail. The tube's downward motion is stopped when its upper end flange impacts against the bore's lower end inwardly extending rim.

  20. Thermoluminescence of lunar samples

    USGS Publications Warehouse

    Dalrymple, G.B.; Doell, Richard R.

    1970-01-01

    Appreciable natural thermoluminescence with glow curve peaks at about 350 degrees centigrade for lunar fines and breccias and above 400 degrees centigrade for crystalline rocks has been recognized in lunar samples. Plagioclase has been identified as the principal carrier of thermoluminescence, and the difference in peak temperatures indicates compositional or structural differences between the feldspars of the different rock types. The present thermoluminescence in the lunar samples is probably the result of a dynamic equilibrium between acquisition from radiation and loss in the lunar thermal environment. A progressive change in the glow curves of core samples with depth below the surface suggests the use of thermoluminescence disequilibrium to detect surfaces buried by recent surface activity, and it also indicates that the lunar diurnal temperature variation penetrates to at least 10.5 centimeters.

  1. Contamination sampling device

    NASA Technical Reports Server (NTRS)

    Delgado, Felix A. (Inventor); Stern, Susan M. (Inventor)

    1998-01-01

    A contamination sample collection device has a wooden dowel with a cotton swab at one end, the cotton being covered by a nylon cloth and the wooden dowel being encapsulated by plastic tubing which is heat shrunk onto the dowel and onto a portion of the cotton swab to secure the cotton in place. Another plastic tube is heat shrunk onto the plastic that encapsulates the dowel and a portion of the nylon cloth to secure the nylon cloth in place. The device may thereafter be covered with aluminum foil protector. The device may be used for obtaining samples of contamination in clean room environments.

  2. Returning Samples from Enceladus

    NASA Astrophysics Data System (ADS)

    Tsou, P.; Kanik, I.; Brownlee, D.; McKay, C.; Anbar, A.; Glavin, D.; Yano, H.

    2012-12-01

    From the first half century of space exploration, we have obtained samples only from the Moon, comet Wild 2, the Solar Wind and the asteroid Itokawa. The in-depth analyses of these samples in terrestrial laboratories have yielded profound knowledge that could not have been obtained without the returned samples. While obtaining samples from Solar System bodies is crucial science, it is rarely done due to cost and complexity. Cassini's discovery of geysers on Enceladus and organic materials, indicate that there is an exceptional opportunity and science rational to do a low-cost flyby sample return mission, similar to what was done by the Stardust. The earliest low cost possible flight opportunity is the next Discovery Mission [Tsou et al 2012]. Enceladus Plume Discovery - While Voyager provided evidence for young surfaces on Enceladus, the existence of Enceladus plumes was discovered by Cassini. Enceladus and comets are the only known solar system bodies that have jets enabling sample collection without landing or surface contact. Cassini in situ Findings -Cassini's made many discoveries at Saturn, including the break up of large organics in the plumes of Enceladus. Four prime criteria for habitability are liquid water, a heat source, organics and nitrogen [McKay et al. 2008, Waite et al. 2009, Postberg et al. 2011]. Out of all the NASA designated habitability targets, Enceladus is the single body that presents evidence for all four criteria. Significant advancement in the exploration of the biological potential of Enceladus can be made on returned samples in terrestrial laboratories where the full power of state-of-the-art laboratory instrumentation and procedures can be used. Without serious limits on power, mass or even cost, terrestrial laboratories provide the ultimate in analytical capability, adaptability, reproducibility and reliability. What Questions can Samples Address? - Samples collected from the Enceladus plume will enable a thorough and replicated

  3. Using Language Sample Databases

    ERIC Educational Resources Information Center

    Heilmann, John J.; Miller, Jon F.; Nockerts, Ann

    2010-01-01

    Purpose: Over the past 50 years, language sample analysis (LSA) has evolved from a powerful research tool that is used to document children's linguistic development into a powerful clinical tool that is used to identify and describe the language skills of children with language impairment. The Systematic Analysis of Language Transcripts (SALT; J.…

  4. Groundwater sampling: Chapter 5

    USGS Publications Warehouse

    Wang, Qingren; Munoz-Carpena, Rafael; Foster, Adam; Migliaccio, Kati W.; Li, Yuncong; Migliaccio, Kati

    2011-01-01

    Discussing an array of water quality topics, from water quality regulations and criteria, to project planning and sampling activities, this book outlines a framework for improving water quality programs. Using this framework, you can easily put the proper training and tools in place for better management of water resources.

  5. Adaptive Sampling Designs.

    ERIC Educational Resources Information Center

    Flournoy, Nancy

    Designs for sequential sampling procedures that adapt to cumulative information are discussed. A familiar illustration is the play-the-winner rule in which there are two treatments; after a random start, the same treatment is continued as long as each successive subject registers a success. When a failure occurs, the other treatment is used until…

  6. Proficiency Sample Project.

    ERIC Educational Resources Information Center

    Apodaca, Mary

    The instrument for Colorado's Foreign Language Proficiency Sample Project and directions for its administration are provided in this document. The project is a voluntary, teacher-designed and -administered effort to standardize high school student language proficiency assessment techniques. The materials are used in teacher workshops. The…

  7. Sampling for Chemical Analysis.

    ERIC Educational Resources Information Center

    Kratochvil, Byron; And Others

    1984-01-01

    This review, designed to make analysts aware of uncertainties introduced into analytical measurements during sampling, is organized under these headings: general considerations; theory; standards; and applications related to mineralogy, soils, sediments, metallurgy, atmosphere, water, biology, agriculture and food, medical and clinical areas, oil…

  8. Driven Boson Sampling

    NASA Astrophysics Data System (ADS)

    Barkhofen, Sonja; Bartley, Tim J.; Sansoni, Linda; Kruse, Regina; Hamilton, Craig S.; Jex, Igor; Silberhorn, Christine

    2017-01-01

    Sampling the distribution of bosons that have undergone a random unitary evolution is strongly believed to be a computationally hard problem. Key to outperforming classical simulations of this task is to increase both the number of input photons and the size of the network. We propose driven boson sampling, in which photons are input within the network itself, as a means to approach this goal. We show that the mean number of photons entering a boson sampling experiment can exceed one photon per input mode, while maintaining the required complexity, potentially leading to less stringent requirements on the input states for such experiments. When using heralded single-photon sources based on parametric down-conversion, this approach offers an ˜e -fold enhancement in the input state generation rate over scattershot boson sampling, reaching the scaling limit for such sources. This approach also offers a dramatic increase in the signal-to-noise ratio with respect to higher-order photon generation from such probabilistic sources, which removes the need for photon number resolution during the heralding process as the size of the system increases.

  9. Lunar sample analysis

    NASA Technical Reports Server (NTRS)

    Housley, R. M.

    1986-01-01

    A wide variety of lunar sample and meteorite studies were performed. Abstracts of the most recent reports are also attached. Experimental techniques employed have included scanning electron microscopy, transmission electron microscopy, Mossbauer spectroscopy, atomic absorption analysis and a variety of simulation studies.

  10. Randomization and sampling issues

    USGS Publications Warehouse

    Geissler, P.H.

    1996-01-01

    The need for randomly selected routes and other sampling issues have been debated by the Amphibian electronic discussion group. Many excellent comments have been made, pro and con, but we have not reached consensus yet. This paper brings those comments together and attempts a synthesis. I hope that the resulting discussion will bring us closer to a consensus.

  11. ANNULAR IMPACTOR SAMPLING DEVICE

    DOEpatents

    Tait, G.W.C.

    1959-03-31

    A high-rate air sampler capable of sampling alphaemitting particles as small as 0.5 microns is described. The device is a cylindrical shaped cup that fits in front of a suction tube and which has sticky grease coating along its base. Suction forces contaminated air against the periodically monitored particle absorbing grease.

  12. Color Discrimination Work Sample.

    ERIC Educational Resources Information Center

    Shawsheen Valley Regional Vocational-Technical High School, Billerica, MA.

    This manual contains a work sample intended to assess a handicapped student's ability to see likenesses or differences in colors or shades, identifying or matching certain colors, and selecting colors that go together. Section 1 describes the assessment and lists related occupations and DOT codes. Instructions to the evaluator are provided in the…

  13. Biological Sampling Variability Study

    SciTech Connect

    Amidan, Brett G.; Hutchison, Janine R.

    2016-11-08

    There are many sources of variability that exist in the sample collection and analysis process. This paper addresses many, but not all, sources of variability. The main focus of this paper was to better understand and estimate variability due to differences between samplers. Variability between days was also studied, as well as random variability within each sampler. Experiments were performed using multiple surface materials (ceramic and stainless steel), multiple contaminant concentrations (10 spores and 100 spores), and with and without the presence of interfering material. All testing was done with sponge sticks using 10-inch by 10-inch coupons. Bacillus atrophaeus was used as the BA surrogate. Spores were deposited using wet deposition. Grime was coated on the coupons which were planned to include the interfering material (Section 3.3). Samples were prepared and analyzed at PNNL using CDC protocol (Section 3.4) and then cultured and counted. Five samplers were trained so that samples were taken using the same protocol. Each sampler randomly sampled eight coupons each day, four coupons with 10 spores deposited and four coupons with 100 spores deposited. Each day consisted of one material being tested. The clean samples (no interfering materials) were run first, followed by the dirty samples (coated with interfering material). There was a significant difference in recovery efficiency between the coupons with 10 spores deposited (mean of 48.9%) and those with 100 spores deposited (mean of 59.8%). There was no general significant difference between the clean and dirty (containing interfering material) coupons or between the two surface materials; however, there was a significant interaction between concentration amount and presence of interfering material. The recovery efficiency was close to the same for coupons with 10 spores deposited, but for the coupons with 100 spores deposited, the recovery efficiency for the dirty samples was significantly larger (65

  14. Seabed observation & sampling system

    USGS Publications Warehouse

    Blackwood, D.; Parolski, K.

    2001-01-01

    SEABOSS has proved to be a valuable addition to the USGS data-acquisition and processing field program. It has allowed researchers to collect high-quality images and seabed samples in a timely manner. It is a simple, dependable and trouble-free system with a track record of over 3,000 deployments. When used as part of the USGS seafloor mapping acquisition, processing, and ground-truth program, SEABOSS has been invaluable in providing information quickly and efficiently, with a minimum of downtime. SEABOSS enables scientists to collect high-quality images and samples of the seabed, essential to the study of sedimentary environments and biological habitats and to the interpretation of side-scan sonar and multibeam imagery, the most common tools for mapping the seabed.

  15. Sampling system and method

    DOEpatents

    Decker, David L.; Lyles, Brad F.; Purcell, Richard G.; Hershey, Ronald Lee

    2017-03-07

    In one embodiment, the present disclosure provides an apparatus and method for supporting a tubing bundle during installation or removal. The apparatus includes a clamp for securing the tubing bundle to an external wireline. In various examples, the clamp is external to the tubing bundle or integral with the tubing bundle. According to one method, a tubing bundle and wireline are deployed together and the tubing bundle periodically secured to the wireline using a clamp. In another embodiment, the present disclosure provides an apparatus and method for coupling conduit segments together. A first pump obtains a sample and transmits it through a first conduit to a reservoir accessible by a second pump. The second pump further conducts the sample from the reservoir through a second conduit. In a specific example, one or more clamps are used to connect the first and/or second conduits to an external wireline.

  16. Cerenkov fiber sampling calorimeters

    SciTech Connect

    Arrington, K.; Kefford, D.; Kennedy, J.; Pisani, R.; Sanzeni, C.; Segall, K.; Wall, D.; Winn, D.R. ); Carey, R.; Dye, S.; Miller, J.; Sulak, L.; Worstell, W. ); Efremenko, Y.; Kamyshkov, Y.; Savin, A.; Shmakov, K.; Tarkovsky, E. )

    1994-08-01

    Clear optical fibers were used as a Cerenkov sampling media in Pb (electromagnetic) and Cu (hadron) absorbers in spaghetti calorimeters, for high rate and high radiation dose experiments, such as the forward region of high energy colliders. The fiber axes were aligned close to the direction of the incident particles (1[degree]--7[degree]). The 7 [lambda] deep hadron tower contained 2.8% by volume 1.5 mm diameter core clear plastic fibers. The 27 radiation length deep electromagnetic towers had packing fractions of 6.8% and 7.2% of 1 mm diameter core quartz fibers as the active Cerenkov sampling medium. The energy resolution on electrons and pions, energy response, pulse shapes and angular studies are presented.

  17. Nonadiabatic transition path sampling

    NASA Astrophysics Data System (ADS)

    Sherman, M. C.; Corcelli, S. A.

    2016-07-01

    Fewest-switches surface hopping (FSSH) is combined with transition path sampling (TPS) to produce a new method called nonadiabatic path sampling (NAPS). The NAPS method is validated on a model electron transfer system coupled to a Langevin bath. Numerically exact rate constants are computed using the reactive flux (RF) method over a broad range of solvent frictions that span from the energy diffusion (low friction) regime to the spatial diffusion (high friction) regime. The NAPS method is shown to quantitatively reproduce the RF benchmark rate constants over the full range of solvent friction. Integrating FSSH within the TPS framework expands the applicability of both approaches and creates a new method that will be helpful in determining detailed mechanisms for nonadiabatic reactions in the condensed-phase.

  18. Lunar sample analysis

    NASA Technical Reports Server (NTRS)

    Tittmann, B. R.

    1975-01-01

    Previous studies have shown that very small amounts of absorbed volatiles only removed by outgassing in high vacuum and elevated temperatures-drastically increase the internal friction in terrestrial analogs of lunar basalt. Recently room temperature Q values as high as 2000 were achieved by thorough outgassing procedures in 10 to the 8th power torr. Results are presented on Q measurements for lunar rock 70215.85, along with some data on the effect on Q of a variety of gases. Data show that substantially greater increases in Q are obtainable in a lunar rock sample than in the terrestrial analog samples studied, and that in addition to H2O other gases also can make non-negligible contributions to the internal friction.

  19. Phoenix Test Sample Site

    NASA Technical Reports Server (NTRS)

    2008-01-01

    This image, acquired by NASA's Phoenix Mars Lander's Surface Stereo Imager on Sol 7, the seventh day of the mission (June 1, 2008), shows the so-called 'Knave of Hearts' first-dig test area to the north of the lander. The Robotic Arm's scraping blade left a small horizontal depression above where the sample was taken.

    Scientists speculate that white material in the depression left by the dig could represent ice or salts that precipitated into the soil. This material is likely the same white material observed in the sample in the Robotic Arm's scoop.

    The Phoenix Mission is led by the University of Arizona, Tucson, on behalf of NASA. Project management of the mission is by NASA's Jet Propulsion Laboratory, Pasadena, Calif. Spacecraft development is by Lockheed Martin Space Systems, Denver.

  20. Advanced hierarchical distance sampling

    USGS Publications Warehouse

    Royle, Andy

    2016-01-01

    In this chapter, we cover a number of important extensions of the basic hierarchical distance-sampling (HDS) framework from Chapter 8. First, we discuss the inclusion of “individual covariates,” such as group size, in the HDS model. This is important in many surveys where animals form natural groups that are the primary observation unit, with the size of the group expected to have some influence on detectability. We also discuss HDS integrated with time-removal and double-observer or capture-recapture sampling. These “combined protocols” can be formulated as HDS models with individual covariates, and thus they have a commonality with HDS models involving group structure (group size being just another individual covariate). We cover several varieties of open-population HDS models that accommodate population dynamics. On one end of the spectrum, we cover models that allow replicate distance sampling surveys within a year, which estimate abundance relative to availability and temporary emigration through time. We consider a robust design version of that model. We then consider models with explicit dynamics based on the Dail and Madsen (2011) model and the work of Sollmann et al. (2015). The final major theme of this chapter is relatively newly developed spatial distance sampling models that accommodate explicit models describing the spatial distribution of individuals known as Point Process models. We provide novel formulations of spatial DS and HDS models in this chapter, including implementations of those models in the unmarked package using a hack of the pcount function for N-mixture models.

  1. Water sample filtration unit

    USGS Publications Warehouse

    Skougstad, M.W.; Scarbro, G.F.

    1968-01-01

    A readily portable, all plastic, pressure filtration unit is described which greatly facilitates rapid micropore membrane field filtration of up to several liters of water with a minimum risk of inorganic chemical alteration or contamination of the sample. The unit accommodates standard 10.2-cm. (4-inch) diameter filters. The storage and carrying case serves as a convenient filter stand for both field and laboratory use.

  2. Natural sampling strategy

    NASA Technical Reports Server (NTRS)

    Hallum, C. R.; Basu, J. P. (Principal Investigator)

    1979-01-01

    A natural stratum-based sampling scheme and the aggregation procedures for estimating wheat area, yield, and production and their associated prediction error estimates are described. The methodology utilizes LANDSAT imagery and agrophysical data to permit an improved stratification in foreign areas by ignoring political boundaries and restratifying along boundaries that are more homogeneous with respect to the distribution of agricultural density, soil characteristics, and average climatic conditions. A summary of test results is given including a discussion of the various problems encountered.

  3. Digital Microfluidics Sample Analyzer

    NASA Technical Reports Server (NTRS)

    Pollack, Michael G.; Srinivasan, Vijay; Eckhardt, Allen; Paik, Philip Y.; Sudarsan, Arjun; Shenderov, Alex; Hua, Zhishan; Pamula, Vamsee K.

    2010-01-01

    Three innovations address the needs of the medical world with regard to microfluidic manipulation and testing of physiological samples in ways that can benefit point-of-care needs for patients such as premature infants, for which drawing of blood for continuous tests can be life-threatening in their own right, and for expedited results. A chip with sample injection elements, reservoirs (and waste), droplet formation structures, fluidic pathways, mixing areas, and optical detection sites, was fabricated to test the various components of the microfluidic platform, both individually and in integrated fashion. The droplet control system permits a user to control droplet microactuator system functions, such as droplet operations and detector operations. Also, the programming system allows a user to develop software routines for controlling droplet microactuator system functions, such as droplet operations and detector operations. A chip is incorporated into the system with a controller, a detector, input and output devices, and software. A novel filler fluid formulation is used for the transport of droplets with high protein concentrations. Novel assemblies for detection of photons from an on-chip droplet are present, as well as novel systems for conducting various assays, such as immunoassays and PCR (polymerase chain reaction). The lab-on-a-chip (a.k.a., lab-on-a-printed-circuit board) processes physiological samples and comprises a system for automated, multi-analyte measurements using sub-microliter samples of human serum. The invention also relates to a diagnostic chip and system including the chip that performs many of the routine operations of a central labbased chemistry analyzer, integrating, for example, colorimetric assays (e.g., for proteins), chemiluminescence/fluorescence assays (e.g., for enzymes, electrolytes, and gases), and/or conductometric assays (e.g., for hematocrit on plasma and whole blood) on a single chip platform.

  4. Sustainable Mars Sample Return

    NASA Technical Reports Server (NTRS)

    Alston, Christie; Hancock, Sean; Laub, Joshua; Perry, Christopher; Ash, Robert

    2011-01-01

    The proposed Mars sample return mission will be completed using natural Martian resources for the majority of its operations. The system uses the following technologies: In-Situ Propellant Production (ISPP), a methane-oxygen propelled Mars Ascent Vehicle (MAV), a carbon dioxide powered hopper, and a hydrogen fueled balloon system (large balloons and small weather balloons). The ISPP system will produce the hydrogen, methane, and oxygen using a Sabatier reactor. a water electrolysis cell, water extracted from the Martian surface, and carbon dioxide extracted from the Martian atmosphere. Indigenous hydrogen will fuel the balloon systems and locally-derived methane and oxygen will fuel the MAV for the return of a 50 kg sample to Earth. The ISPP system will have a production cycle of 800 days and the estimated overall mission length is 1355 days from Earth departure to return to low Earth orbit. Combining these advanced technologies will enable the proposed sample return mission to be executed with reduced initial launch mass and thus be more cost efficient. The successful completion of this mission will serve as the next step in the advancement of Mars exploration technology.

  5. 76 FR 55161 - Boston and Maine Corporation-Abandonment Exemption-Middlesex County, Mass.; Springfield Terminal...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-09-06

    ... abandonment notice of exemption was inadvertently filed as Docket No. AB 1083X and the discontinuance of service notice of exemption was inadvertently filed as Docket No. AB 1084X. The correct docket numbers for these transactions are Docket No. AB 32 (Sub-No. 103X) and Docket No. AB 355 (Sub-No. 39X),...

  6. Record of Decision Operable Units 4 and 5, Sudbury Training Annex, Middlesex County, Massachusetts

    DTIC Science & Technology

    1996-09-01

    of the Devens Reserve Forces Training Area ( RFTA ), itself an installation of Fort McCoy, and includes several areas actively in use by the FEMA and...ABBREVIATIONS ROD RfD RFTA RME RI SA SARA SI TPHC TRC TRV Mg/L USAEC USCOE USEPA USFWS UST VOC Record of Decision Reference Dose Reserve

  7. Bedrock geologic map of the Nashua South quadrangle, Hillsborough County, New Hampshire, and Middlesex County, Massachusetts

    USGS Publications Warehouse

    Walsh, Gregory J.; Jahns, Richard H.; Aleinikoff, John N.

    2013-01-01

    The bedrock geology of the 7.5-minute Nashua South quadrangle consists primarily of deformed Silurian metasedimentary rocks of the Berwick Formation. The metasedimentary rocks are intruded by a Late Silurian to Early Devonian diorite-gabbro suite, Devonian rocks of the Ayer Granodiorite, Devonian granitic rocks of the New Hampshire Plutonic Suite including pegmatite and the Chelmsford Granite, and Jurassic diabase dikes. The bedrock geology was mapped to study the tectonic history of the area and to provide a framework for ongoing hydrogeologic characterization of the fractured bedrock of Massachusetts and New Hampshire. This report presents mapping by G.J. Walsh and R.H. Jahns and zircon U-Pb geochronology by J.N. Aleinikoff. The complete report consists of a map, text pamphlet, and GIS database. The map and text pamphlet are only available as downloadable files (see frame at right). The GIS database is available for download in ESRITM shapefile and Google EarthTM formats, and includes contacts of bedrock geologic units, faults, outcrops, structural geologic information, photographs, and a three-dimensional model.

  8. Surficial geologic map of the Framingham quadrangle, Middlesex and Worcester Counties, Massachusetts

    USGS Publications Warehouse

    Nelson, Arthur E.

    1974-01-01

    With the exception of a small part of the southeast corner, which is drained by the Charles River, the quadrangle is drained by the Sudbury River, whose waters eventually flow into the Merrimack River in the northeast part of the state.

  9. 76 FR 33777 - Stewart B. McKinney National Wildlife Refuge, Middlesex County, CT; Comprehensive Conservation...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2011-06-09

    ...; Comprehensive Conservation Plan and Environmental Assessment AGENCY: Fish and Wildlife Service, Interior. ACTION... to prepare a comprehensive conservation plan (CCP) for Stewart B. McKinney National Wildlife Refuge... Refuge System (NWRS), consistent with sound principles of fish and wildlife management,...

  10. A Cost Analysis Study of the Radiography Program at Middlesex Hospital Using Shock's Analysis Model.

    ERIC Educational Resources Information Center

    Spence, Weymouth

    Federal and state governments want to decrease payments for medical education, and other payers are trying to restrict payouts to direct and necessary patient care services. Teaching hospitals are increasing tuition and fees, reducing education budgets and, in many instances, closing education programs. Hospital administrators are examining the…

  11. Bedrock Geologic Map of the Old Lyme Quadrangle, New London and Middlesex Counties, Connecticut

    USGS Publications Warehouse

    Walsh, Gregory J.; Scott, Robert B.; Aleinikoff, John N.; Armstrong, Thomas R.

    2009-01-01

    The bedrock geology of the Old Lyme quadrangle consists of Neoproterozoic and Permian gneisses and granites of the Gander and Avalon terranes, Silurian metasedimentary rocks of the Merrimack terrane, and Silurian to Devonian metasedimentary rocks of uncertain origin. The Avalon terrane rocks crop out within the Selden Neck block, and the Gander terrane rocks crop out within the Lyme dome. The Silurian to Devonian rocks crop out between these two massifs. Previous mapping in the Old Lyme quadrangle includes the work by Lawrence Lundgren, Jr. Lundgren's work provides an excellent resource for rock descriptions and detailed modal analyses of rock units that will not be duplicated in this current report. New research that was not covered in detail by Lundgren is the focus of this report and includes (1) evaluation of the rocks in the core of the Lyme dome in an effort to subdivide units in this area; (2) structural analysis of foliations and folds in and around the Lyme dome; (3) geochronology of selected units within the Lyme dome; and (4) analysis of joints and the fracture properties of the rocks.

  12. 340 Representative sampling verification tank sampling and analysis plan

    SciTech Connect

    Olander, A.R., Westinghouse Hanford

    1996-08-21

    This Sampling and Analysis Plan contains requirements for characterizing the 340 vault tank 1. The objective of the sampling and characterization is to determine if the tank is homogeneous when agitated and which sampling method provides the most representative sample. A secondary objective is to collect and characterize solid samples.

  13. Germanium-76 Sample Analysis

    SciTech Connect

    Kouzes, Richard T.; Engelhard, Mark H.; Zhu, Zihua

    2011-04-01

    The MAJORANA DEMONSTRATOR is a large array of ultra-low background high-purity germanium detectors, enriched in 76Ge, designed to search for zero-neutrino double-beta decay (0νββ). The DEMONSTRATOR will utilize 76Ge from Russia, and the first one gram sample was received from the supplier for analysis on April 24, 2011. The Environmental Molecular Sciences facility, a DOE user facility at PNNL, was used to make the required isotopic and chemical purity measurements that are essential to the quality assurance for the MAJORANA DEMONSTRATOR. The results of this first analysis are reported here.

  14. Air Sampling Filter

    NASA Technical Reports Server (NTRS)

    1980-01-01

    General Metal Works' Accu-Vol is a high-volume air sampling system used by many government agencies to monitor air quality for pollution control purposes. Procedure prevents possible test-invalidating contamination from materials other than particulate pollutants, caused by manual handling or penetration of windblown matter during transit, a cassette was developed in which the filter is sealed within a metal frame and protected in transit by a snap-on aluminum cover, thus handled only under clean conditions in the laboratory.

  15. Pulsed field sample neutralization

    DOEpatents

    Appelhans, Anthony D.; Dahl, David A.; Delmore, James E.

    1990-01-01

    An apparatus and method for alternating voltage and for varying the rate of extraction during the extraction of secondary particles, resulting in periods when either positive ions, or negative ions and electrons are extracted at varying rates. Using voltage with alternating charge during successive periods to extract particles from materials which accumulate charge opposite that being extracted causes accumulation of surface charge of opposite sign. Charge accumulation can then be adjusted to a ratio which maintains a balance of positive and negative charge emission, thus maintaining the charge neutrality of the sample.

  16. Stack sampling apparatus

    DOEpatents

    Lind, Randall F; Lloyd, Peter D; Love, Lonnie J; Noakes, Mark W; Pin, Francois G; Richardson, Bradley S; Rowe, John C

    2014-09-16

    An apparatus for obtaining samples from a structure includes a support member, at least one stabilizing member, and at least one moveable member. The stabilizing member has a first portion coupled to the support member and a second portion configured to engage with the structure to restrict relative movement between the support member and the structure. The stabilizing member is radially expandable from a first configuration where the second portion does not engage with a surface of the structure to a second configuration where the second portion engages with the surface of the structure.

  17. 46. VIEW OF SAMPLING ROOM FROM SOUTHEAST. TO LEFT, SAMPLING ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    46. VIEW OF SAMPLING ROOM FROM SOUTHEAST. TO LEFT, SAMPLING ELEVATOR AND IN CENTER, SAMPLE BINS WITH DISCHARGE CHUTE AND THREE LABELS. - Bald Mountain Gold Mill, Nevada Gulch at head of False Bottom Creek, Lead, Lawrence County, SD

  18. Acclerated rare event sampling

    NASA Astrophysics Data System (ADS)

    Yevick, David

    2015-03-01

    We suggest a strategy for biased transition matrix Monte-Carlo calculations that both ensures the most rapid coverage of the entire computational window in the macroscopic variables of interest E --> and yields estimates of transition probabilities between states that are equally accurate in low and high probability regions. Further, paths between different low probability regions are sampled at regular intervals. For the case of a single E variable, a random system realization for which the value of E falls in e.g. the i:th histogram bin is generated. This state is perturbed and the resulting realization is rejected until a transition is observed to a neighboring bin, taken here as i + 1 . All accepted and rejected transitions are simultaneously employed to generate the elements of a transition matrix. Subsequently, only a transition to bin i + 2 is accepted and this procedure is continued until the last of the N bins comprising the computational window is sampled. The procedure is then repeated but in the direction of decreasing bin number. The probability distribution of E can then be obtained by e.g. repeatedly multiplying a random vector by the transition matrix.

  19. Fluid sampling tool

    DOEpatents

    Garcia, Anthony R.; Johnston, Roger G.; Martinez, Ronald K.

    1999-05-25

    A fluid sampling tool for sampling fluid from a container. The tool has a fluid collecting portion which is drilled into the container wall, thereby affixing it to the wall. The tool may have a fluid extracting section which withdraws fluid collected by the fluid collecting section. The fluid collecting section has a fluted shank with an end configured to drill a hole into a container wall. The shank has a threaded portion for tapping the borehole. The shank is threadably engaged to a cylindrical housing having an inner axial passageway sealed at one end by a septum. A flexible member having a cylindrical portion and a bulbous portion is provided. The housing can be slid into an inner axial passageway in the cylindrical portion and sealed to the flexible member. The bulbous portion has an outer lip defining an opening. The housing is clamped into the chuck of a drill, the lip of the bulbous section is pressed against a container wall until the shank touches the wall, and the user operates the drill. Wall shavings (kerf) are confined in a chamber formed in the bulbous section as it folds when the shank advances inside the container. After sufficient advancement of the shank, an o-ring makes a seal with the container wall.

  20. Fluid sampling tool

    DOEpatents

    Garcia, A.R.; Johnston, R.G.; Martinez, R.K.

    1999-05-25

    A fluid sampling tool is described for sampling fluid from a container. The tool has a fluid collecting portion which is drilled into the container wall, thereby affixing it to the wall. The tool may have a fluid extracting section which withdraws fluid collected by the fluid collecting section. The fluid collecting section has a fluted shank with an end configured to drill a hole into a container wall. The shank has a threaded portion for tapping the borehole. The shank is threadably engaged to a cylindrical housing having an inner axial passageway sealed at one end by a septum. A flexible member having a cylindrical portion and a bulbous portion is provided. The housing can be slid into an inner axial passageway in the cylindrical portion and sealed to the flexible member. The bulbous portion has an outer lip defining an opening. The housing is clamped into the chuck of a drill, the lip of the bulbous section is pressed against a container wall until the shank touches the wall, and the user operates the drill. Wall shavings (kerf) are confined in a chamber formed in the bulbous section as it folds when the shank advances inside the container. After sufficient advancement of the shank, an o-ring makes a seal with the container wall. 6 figs.

  1. Revisiting sample entropy analysis

    NASA Astrophysics Data System (ADS)

    Govindan, R. B.; Wilson, J. D.; Eswaran, H.; Lowery, C. L.; Preißl, H.

    2007-03-01

    We modify the definition of sample entropy (SaEn) by incorporating a time delay between the components of the block (from which the densities are estimated) and show that the modified method characterizes the complexity of the system better than the original version. We apply the modified SaEn to the standard deterministic systems and stochastic processes (uncorrelated and long range correlated (LRC) processes) and show that the underlying complexity of the system is better quantified by the modified method. We extend this analysis to the RR intervals of the normal and congestive heart failure (CHF) subjects (available via www.physionet.org) and show that there is a good degree of separation between the two groups.

  2. Fluid sampling tool

    DOEpatents

    Johnston, Roger G.; Garcia, Anthony R. E.; Martinez, Ronald K.

    2001-09-25

    The invention includes a rotatable tool for collecting fluid through the wall of a container. The tool includes a fluid collection section with a cylindrical shank having an end portion for drilling a hole in the container wall when the tool is rotated, and a threaded portion for tapping the hole in the container wall. A passageway in the shank in communication with at least one radial inlet hole in the drilling end and an opening at the end of the shank is adapted to receive fluid from the container. The tool also includes a cylindrical chamber affixed to the end of the shank opposite to the drilling portion thereof for receiving and storing fluid passing through the passageway. The tool also includes a flexible, deformable gasket that provides a fluid-tight chamber to confine kerf generated during the drilling and tapping of the hole. The invention also includes a fluid extractor section for extracting fluid samples from the fluid collecting section.

  3. Glass sample characterization

    NASA Technical Reports Server (NTRS)

    Ahmad, Anees

    1990-01-01

    The development of in-house integrated optical performance modelling capability at MSFC is described. This performance model will take into account the effects of structural and thermal distortions, as well as metrology errors in optical surfaces to predict the performance of large an complex optical systems, such as Advanced X-Ray Astrophysics Facility. The necessary hardware and software were identified to implement an integrated optical performance model. A number of design, development, and testing tasks were supported to identify the debonded mirror pad, and rebuilding of the Technology Mirror Assembly. Over 300 samples of Zerodur were prepared in different sizes and shapes for acid etching, coating, and polishing experiments to characterize the subsurface damage and stresses produced by the grinding and polishing operations.

  4. Samples from Asteroid Itokawa

    NASA Astrophysics Data System (ADS)

    Taylor, G. J.; Martel, L. M. V.

    2011-08-01

    The Hayabusa spacecraft, flown by the Japanese Aerospace Exploration Agency (JAXA), returned samples from asteroid 25143 Itokawa on June 13, 2010. Though the sampling device did not operate properly, the mission was able to return a couple thousand particles, from a few- to a few hundred-micrometers across. A battery of laboratory analyses (electron microscopy, elemental analysis, and oxygen isotopic measurements) shows that the particles derive from materials like those in thermally metamorphosed LL group ordinary chondrites. Astronomical observations had classified Itokawa as a stony S(IV) type of asteroid. The nature of S-type asteroids has been debated for decades; some astronomers argued that S-type asteroids are ordinary chondrites while others suggested that they were more likely to be differentiated objects (i.e., melted or partially melted to make igneous rocks). The problem was that we did not know enough about space weathering on asteroids to know how the spectra of chondritic or differentiated asteroids changed with exposure to micrometeorites and solar wind. The examinations of Hayabusa's treasure have settled the argument: S-type asteroid, Itokawa, indeed has an ordinary chondrite composition whose spectrum has been reddened by space weathering. This conclusion is supported by detailed studies of the surfaces of 10 Itokawa particles, half of which have glassy rims (5-50 nanometers thick) containing nano-sized particles of iron sulfide and metallic iron, signatures of space weathering. Analysis of noble gases in three particles from the asteroid indicate that they were exposed on the surface of Itokawa for surprisingly short times, less than 8 million years. The Hayabusa science team suggests that the short exposure time indicates loss of particles into space through small impacts at the surprisingly fast rate of tens of centimeters per million years. This might not seem fast, but the asteroid, only 535 x 294 x 209 meters in size, would become just a

  5. Sample introducing apparatus and sample modules for mass spectrometer

    DOEpatents

    Thompson, Cyril V.; Wise, Marcus B.

    1993-01-01

    An apparatus for introducing gaseous samples from a wide range of environmental matrices into a mass spectrometer for analysis of the samples is described. Several sample preparing modules including a real-time air monitoring module, a soil/liquid purge module, and a thermal desorption module are individually and rapidly attachable to the sample introducing apparatus for supplying gaseous samples to the mass spectrometer. The sample-introducing apparatus uses a capillary column for conveying the gaseous samples into the mass spectrometer and is provided with an open/split interface in communication with the capillary and a sample archiving port through which at least about 90 percent of the gaseous sample in a mixture with an inert gas that was introduced into the sample introducing apparatus is separated from a minor portion of the mixture entering the capillary discharged from the sample introducing apparatus.

  6. Sample introducing apparatus and sample modules for mass spectrometer

    DOEpatents

    Thompson, C.V.; Wise, M.B.

    1993-12-21

    An apparatus for introducing gaseous samples from a wide range of environmental matrices into a mass spectrometer for analysis of the samples is described. Several sample preparing modules including a real-time air monitoring module, a soil/liquid purge module, and a thermal desorption module are individually and rapidly attachable to the sample introducing apparatus for supplying gaseous samples to the mass spectrometer. The sample-introducing apparatus uses a capillary column for conveying the gaseous samples into the mass spectrometer and is provided with an open/split interface in communication with the capillary and a sample archiving port through which at least about 90 percent of the gaseous sample in a mixture with an inert gas that was introduced into the sample introducing apparatus is separated from a minor portion of the mixture entering the capillary discharged from the sample introducing apparatus. 5 figures.

  7. Soil sampling kit and a method of sampling therewith

    DOEpatents

    Thompson, C.V.

    1991-02-05

    A soil sampling device and a sample containment device for containing a soil sample is disclosed. In addition, a method for taking a soil sample using the soil sampling device and soil sample containment device to minimize the loss of any volatile organic compounds contained in the soil sample prior to analysis is disclosed. The soil sampling device comprises two close fitting, longitudinal tubular members of suitable length, the inner tube having the outward end closed. With the inner closed tube withdrawn a selected distance, the outer tube can be inserted into the ground or other similar soft material to withdraw a sample of material for examination. The inner closed end tube controls the volume of the sample taken and also serves to eject the sample. The soil sample containment device has a sealing member which is adapted to attach to an analytical apparatus which analyzes the volatile organic compounds contained in the sample. The soil sampling device in combination with the soil sample containment device allows an operator to obtain a soil sample containing volatile organic compounds and minimizing the loss of the volatile organic compounds prior to analysis of the soil sample for the volatile organic compounds. 11 figures.

  8. Soil sampling kit and a method of sampling therewith

    DOEpatents

    Thompson, Cyril V.

    1991-01-01

    A soil sampling device and a sample containment device for containing a soil sample is disclosed. In addition, a method for taking a soil sample using the soil sampling device and soil sample containment device to minimize the loss of any volatile organic compounds contained in the soil sample prior to analysis is disclosed. The soil sampling device comprises two close fitting, longitudinal tubular members of suitable length, the inner tube having the outward end closed. With the inner closed tube withdrawn a selected distance, the outer tube can be inserted into the ground or other similar soft material to withdraw a sample of material for examination. The inner closed end tube controls the volume of the sample taken and also serves to eject the sample. The soil sample containment device has a sealing member which is adapted to attach to an analytical apparatus which analyzes the volatile organic compounds contained in the sample. The soil sampling device in combination with the soil sample containment device allow an operator to obtain a soil sample containing volatile organic compounds and minimizing the loss of the volatile organic compounds prior to analysis of the soil sample for the volatile organic compounds.

  9. Considerations in sampling of water.

    PubMed

    Ramsey, Charles A

    2015-01-01

    Sampling water is no different than sampling any other media. It starts with the development of Sample Quality Criteria, understanding of material properties, then application of the Theory of Sampling. The main difference with sampling water as opposed to solids is the material properties. This paper addresses some of the material properties and consequences of those properties for the development of the sampling protocols. Two properties that must be addressed for water are the temporal nature and the inclusion of suspended solids. Examples are provided for three specific water sampling scenarios which may have application to other water sampling scenarios.

  10. [A comparison of convenience sampling and purposive sampling].

    PubMed

    Suen, Lee-Jen Wu; Huang, Hui-Man; Lee, Hao-Hsien

    2014-06-01

    Convenience sampling and purposive sampling are two different sampling methods. This article first explains sampling terms such as target population, accessible population, simple random sampling, intended sample, actual sample, and statistical power analysis. These terms are then used to explain the difference between "convenience sampling" and purposive sampling." Convenience sampling is a non-probabilistic sampling technique applicable to qualitative or quantitative studies, although it is most frequently used in quantitative studies. In convenience samples, subjects more readily accessible to the researcher are more likely to be included. Thus, in quantitative studies, opportunity to participate is not equal for all qualified individuals in the target population and study results are not necessarily generalizable to this population. As in all quantitative studies, increasing the sample size increases the statistical power of the convenience sample. In contrast, purposive sampling is typically used in qualitative studies. Researchers who use this technique carefully select subjects based on study purpose with the expectation that each participant will provide unique and rich information of value to the study. As a result, members of the accessible population are not interchangeable and sample size is determined by data saturation not by statistical power analysis.

  11. Variable Sampling Mapping

    NASA Technical Reports Server (NTRS)

    Smith, Jeffrey, S.; Aronstein, David L.; Dean, Bruce H.; Lyon, Richard G.

    2012-01-01

    The performance of an optical system (for example, a telescope) is limited by the misalignments and manufacturing imperfections of the optical elements in the system. The impact of these misalignments and imperfections can be quantified by the phase variations imparted on light traveling through the system. Phase retrieval is a methodology for determining these variations. Phase retrieval uses images taken with the optical system and using a light source of known shape and characteristics. Unlike interferometric methods, which require an optical reference for comparison, and unlike Shack-Hartmann wavefront sensors that require special optical hardware at the optical system's exit pupil, phase retrieval is an in situ, image-based method for determining the phase variations of light at the system s exit pupil. Phase retrieval can be used both as an optical metrology tool (during fabrication of optical surfaces and assembly of optical systems) and as a sensor used in active, closed-loop control of an optical system, to optimize performance. One class of phase-retrieval algorithms is the iterative transform algorithm (ITA). ITAs estimate the phase variations by iteratively enforcing known constraints in the exit pupil and at the detector, determined from modeled or measured data. The Variable Sampling Mapping (VSM) technique is a new method for enforcing these constraints in ITAs. VSM is an open framework for addressing a wide range of issues that have previously been considered detrimental to high-accuracy phase retrieval, including undersampled images, broadband illumination, images taken at or near best focus, chromatic aberrations, jitter or vibration of the optical system or detector, and dead or noisy detector pixels. The VSM is a model-to-data mapping procedure. In VSM, fully sampled electric fields at multiple wavelengths are modeled inside the phase-retrieval algorithm, and then these fields are mapped to intensities on the light detector, using the properties

  12. Sample Manipulation System for Sample Analysis at Mars

    NASA Technical Reports Server (NTRS)

    Mumm, Erik; Kennedy, Tom; Carlson, Lee; Roberts, Dustyn

    2008-01-01

    The Sample Analysis at Mars (SAM) instrument will analyze Martian samples collected by the Mars Science Laboratory Rover with a suite of spectrometers. This paper discusses the driving requirements, design, and lessons learned in the development of the Sample Manipulation System (SMS) within SAM. The SMS stores and manipulates 74 sample cups to be used for solid sample pyrolysis experiments. Focus is given to the unique mechanism architecture developed to deliver a high packing density of sample cups in a reliable, fault tolerant manner while minimizing system mass and control complexity. Lessons learned are presented on contamination control, launch restraint mechanisms for fragile sample cups, and mechanism test data.

  13. Subsurface Samples: Collection and Processing

    SciTech Connect

    Long, Philip E.; Griffin, W. Timothy; Phelps, Tommy J.

    2002-12-01

    Microbiological data, interpretation, and conclusions from subsurface samples ultimately depend on the quality and representative character of the samples. Subsurface samples for environmental microbiology ideally contain only the microbial community and geochemical properties that are representative of the subsurface environment from which the sample was taken. To that end, sample contamination by exogenous microorganisms or chemical constituents must be eliminated or minimized, and sample analyses need to begin before changes in the microbial community or geochemical characteristics occur. This article presents sampling methods and sample processing techniques for collecting representative samples from a range of subsurface environments. Factors that should be considered when developing a subsurface sampling program are discussed, including potential benefits, costs, and limitations enabling researchers to evaluate the techniques that are presented and match them to their project requirements. Methods and protocols to address coring, sampling, processing and quality assessment issues are presented.

  14. Sample holder with optical features

    DOEpatents

    Milas, Mirko; Zhu, Yimei; Rameau, Jonathan David

    2013-07-30

    A sample holder for holding a sample to be observed for research purposes, particularly in a transmission electron microscope (TEM), generally includes an external alignment part for directing a light beam in a predetermined beam direction, a sample holder body in optical communication with the external alignment part and a sample support member disposed at a distal end of the sample holder body opposite the external alignment part for holding a sample to be analyzed. The sample holder body defines an internal conduit for the light beam and the sample support member includes a light beam positioner for directing the light beam between the sample holder body and the sample held by the sample support member.

  15. Quantum Metropolis sampling.

    PubMed

    Temme, K; Osborne, T J; Vollbrecht, K G; Poulin, D; Verstraete, F

    2011-03-03

    The original motivation to build a quantum computer came from Feynman, who imagined a machine capable of simulating generic quantum mechanical systems--a task that is believed to be intractable for classical computers. Such a machine could have far-reaching applications in the simulation of many-body quantum physics in condensed-matter, chemical and high-energy systems. Part of Feynman's challenge was met by Lloyd, who showed how to approximately decompose the time evolution operator of interacting quantum particles into a short sequence of elementary gates, suitable for operation on a quantum computer. However, this left open the problem of how to simulate the equilibrium and static properties of quantum systems. This requires the preparation of ground and Gibbs states on a quantum computer. For classical systems, this problem is solved by the ubiquitous Metropolis algorithm, a method that has basically acquired a monopoly on the simulation of interacting particles. Here we demonstrate how to implement a quantum version of the Metropolis algorithm. This algorithm permits sampling directly from the eigenstates of the Hamiltonian, and thus evades the sign problem present in classical simulations. A small-scale implementation of this algorithm should be achievable with today's technology.

  16. Sample preparation techniques.

    PubMed

    Baumgartner, W A; Hill, V A

    1993-12-01

    Evidentiary false positives are caused by passive exposure to drugs in the environment rather than by active use of drugs. The avoidance of such positives is essential for both hair and urine analysis. Hair analysis enjoys the advantage over urinalysis in having a number of approaches for making this distinction. These include: methylene blue staining of the hair specimen for selecting the appropriate wash solvent; application of hair digestion techniques for the complete release of chemically unaltered analytes; the determination of three diagnostic ratios from wash and digestion data; the measurement of metabolite:drug ratios; the use of cut-off levels setting the limits for passive endogenous drug exposure; reproducibility of results (including segmental analysis) with a newly collected hair specimen; and the reporting of results as either negative, positive, or contaminated. Our sample preparation procedures have been effectively applied to the analyses of nearly 200,000 specimens, i.e. to approximately one million drug analyses for cocaine, opiates, methamphetamine, phencyclidine or marijuana. On the basis of this experience we conclude that hair analysis is a safe and effective method for workplace drug testing.

  17. Preservation of Liquid Biological Samples

    NASA Technical Reports Server (NTRS)

    Putcha, Lakshmi (Inventor); Nimmagudda, Ramalingeshwara R. (Inventor)

    2000-01-01

    The present invention provides a method of preserving a liquid biological sample, comprising the step of: contacting said liquid biological sample with a preservative comprising, sodium benzoate in an amount of at least about 0.15% of the sample (weight/volume) and citric acid in an amount of at least about 0.025% of the sample (weight/volume).

  18. How Many Samples are Needed

    DTIC Science & Technology

    2011-03-29

    if the sampling grid pattern or the regular frequency of taking samples coincides with any pattern of contamination 61 Example: Littlewood Site...Conclusion for Littlewood 71 Need 22 + 4 = 26 samples for Production Area Need 5 + 1 = 6 samples for Parking/Admin As the budget allowed

  19. Preservation of Liquid Biological Samples

    NASA Technical Reports Server (NTRS)

    Putcha, Lakshmi (Inventor); Nimmagudda, Ramalingeshwara (Inventor)

    2004-01-01

    The present invention related to the preservation of a liquid biological sample. The biological sample is exposed to a preservative containing at least about 0.15 g of sodium benzoate and at least about 0.025 g of citric acid per 100 ml of sample. The biological sample may be collected in a vessel or an absorbent mass. The biological sample may also be exposed to a substrate and/or a vehicle.

  20. INCORPORATING PRIOR KNOWLEDGE IN ENVIRONMENTAL SAMPLING: RANKED SET SAMPLING AND OTHER DOUBLE SAMPLING PROCEDURES

    EPA Science Inventory

    Environmental sampling can be difficult and expensive to carry out. Those taking the samples would like to integrate their knowledge of the system of study or their judgment about the system into the sample selection process to decrease the number of necessary samples. However,...

  1. The Digital Morphological Sampling Theorem

    NASA Astrophysics Data System (ADS)

    Haralick, Robert M.; Zhuang, Xinhua; Lin, Charlotte; Lee, James

    1988-02-01

    There are potential industrial applications for any methodology which inherently reduces processing time and cost and yet produces results sufficiently close to the result of full processing. It is for this reason that a morphological sampling theorem is important. The morphological sampling theorem described in this paper states: (1) how a digital image must be morphologically filtered before sampling in order to preserve the relevant information after sampling; (2) to what precision an appropriately morphologically filtered image can be reconstructed after sampling; and (3) the relationship between morphologically operating before sampling and the more computationally efficient scheme of morphologically operating on the sampled image with a sampled structuring element. The digital sampling theorem is developed first for the case of binary morphology and then it is extended to gray scale morphology through the use of the umbra homomorphism theorems.

  2. Sampling for area estimation: A comparison of full-frame sampling with the sample segment approach

    NASA Technical Reports Server (NTRS)

    Hixson, M.; Bauer, M. E.; Davis, B. J. (Principal Investigator)

    1979-01-01

    The author has identified the following significant results. Full-frame classifications of wheat and non-wheat for eighty counties in Kansas were repetitively sampled to simulate alternative sampling plans. Evaluation of four sampling schemes involving different numbers of samples and different size sampling units shows that the precision of the wheat estimates increased as the segment size decreased and the number of segments was increased. Although the average bias associated with the various sampling schemes was not significantly different, the maximum absolute bias was directly related to sampling size unit.

  3. Specified assurance level sampling procedure

    SciTech Connect

    Willner, O.

    1980-11-01

    In the nuclear industry design specifications for certain quality characteristics require that the final product be inspected by a sampling plan which can demonstrate product conformance to stated assurance levels. The Specified Assurance Level (SAL) Sampling Procedure has been developed to permit the direct selection of attribute sampling plans which can meet commonly used assurance levels. The SAL procedure contains sampling plans which yield the minimum sample size at stated assurance levels. The SAL procedure also provides sampling plans with acceptance numbers ranging from 0 to 10, thus, making available to the user a wide choice of plans all designed to comply with a stated assurance level.

  4. Sample Tube Sealing for Future Proposed Mars Sample Return Missions

    NASA Technical Reports Server (NTRS)

    Younse, P.; Aveline, D.; Bao, X.; Berisford, D.; Bhandari, P.; Budney, C.; Chen, F.; Cooper, M.; Chung, S.; Lewis, D.

    2013-01-01

    A key premise of a proposed Sample Caching Rover, a crucial element of the proposed Mars Sample Return (MSR) campaign, is that the samples could be packaged and left on Mars for an extended period of time (at least five Mars years) without loss of scientific value (Fig. 1). The MEPAG E2E-iSAG (2011) concluded that the single most important factor in preserving the scientific integrity of the samples during the interval between their collection and their analysis is effective sealing of the samples.

  5. Analysis of Pet Coke Samples

    EPA Pesticide Factsheets

    EPA required KCBX to submit samples of the petroleum coke stored at their North and South Chicago terminals to EPA's Chicago Regional Laboratory for analysis of pollutant levels. Results will be compared to coal and pet coke sampled in Detroit.

  6. Sampling properties of directed networks

    NASA Astrophysics Data System (ADS)

    Son, S.-W.; Christensen, C.; Bizhani, G.; Foster, D. V.; Grassberger, P.; Paczuski, M.

    2012-10-01

    For many real-world networks only a small “sampled” version of the original network may be investigated; those results are then used to draw conclusions about the actual system. Variants of breadth-first search (BFS) sampling, which are based on epidemic processes, are widely used. Although it is well established that BFS sampling fails, in most cases, to capture the IN component(s) of directed networks, a description of the effects of BFS sampling on other topological properties is all but absent from the literature. To systematically study the effects of sampling biases on directed networks, we compare BFS sampling to random sampling on complete large-scale directed networks. We present new results and a thorough analysis of the topological properties of seven complete directed networks (prior to sampling), including three versions of Wikipedia, three different sources of sampled World Wide Web data, and an Internet-based social network. We detail the differences that sampling method and coverage can make to the structural properties of sampled versions of these seven networks. Most notably, we find that sampling method and coverage affect both the bow-tie structure and the number and structure of strongly connected components in sampled networks. In addition, at a low sampling coverage (i.e., less than 40%), the values of average degree, variance of out-degree, degree autocorrelation, and link reciprocity are overestimated by 30% or more in BFS-sampled networks and only attain values within 10% of the corresponding values in the complete networks when sampling coverage is in excess of 65%. These results may cause us to rethink what we know about the structure, function, and evolution of real-world directed networks.

  7. Sampling and sample processing in pesticide residue analysis.

    PubMed

    Lehotay, Steven J; Cook, Jo Marie

    2015-05-13

    Proper sampling and sample processing in pesticide residue analysis of food and soil have always been essential to obtain accurate results, but the subject is becoming a greater concern as approximately 100 mg test portions are being analyzed with automated high-throughput analytical methods by agrochemical industry and contract laboratories. As global food trade and the importance of monitoring increase, the food industry and regulatory laboratories are also considering miniaturized high-throughput methods. In conjunction with a summary of the symposium "Residues in Food and Feed - Going from Macro to Micro: The Future of Sample Processing in Residue Analytical Methods" held at the 13th IUPAC International Congress of Pesticide Chemistry, this is an opportune time to review sampling theory and sample processing for pesticide residue analysis. If collected samples and test portions do not adequately represent the actual lot from which they came and provide meaningful results, then all costs, time, and efforts involved in implementing programs using sophisticated analytical instruments and techniques are wasted and can actually yield misleading results. This paper is designed to briefly review the often-neglected but crucial topic of sample collection and processing and put the issue into perspective for the future of pesticide residue analysis. It also emphasizes that analysts should demonstrate the validity of their sample processing approaches for the analytes/matrices of interest and encourages further studies on sampling and sample mass reduction to produce a test portion.

  8. Mars Sample Quarantine Protocol Workshop

    NASA Technical Reports Server (NTRS)

    DeVincenzi, Donald L. (Editor); Bagby, John (Editor); Race, Margaret (Editor); Rummel, John (Editor)

    1999-01-01

    The Mars Sample Quarantine Protocol (QP) Workshop was convened to deal with three specific aspects of the initial handling of a returned Mars sample: 1) biocontainment, to prevent uncontrolled release of sample material into the terrestrial environment; 2) life detection, to examine the sample for evidence of live organisms; and 3) biohazard testing, to determine if the sample poses any threat to terrestrial life forms and the Earth's biosphere. During the first part of the Workshop, several tutorials were presented on topics related to the workshop in order to give all participants a common basis in the technical areas necessary to achieve the objectives of the Workshop.

  9. Rotary Percussive Sample Acquisition Tool

    NASA Technical Reports Server (NTRS)

    Klein, K.; Badescu, M.; Haddad, N.; Shiraishi, L.; Walkemeyer, P.

    2012-01-01

    As part of a potential Mars Sample Return campaign NASA is studying a sample caching mission to Mars, with a possible 2018 launch opportunity. As such, a Sample Acquisition Tool (SAT) has been developed in support of the Integrated Mars Sample Acquisition and Handling (IMSAH) architecture as it relates to the proposed Mars Sample Return (MSR) campaign. The tool allows for core generation and capture directly into a sample tube. In doing so, the sample tube becomes the fundamental handling element within the IMSAH sample chain reducing the risk associated with sample contamination as well as the need to handle a sample of unknown geometry. The tool's functionality was verified utilizing a proposed rock test suite that encompasses a series of rock types that have been utilized in the past to qualify Martian surface sampling hardware. The corresponding results have shown the tool can effectively generate, fracture, and capture rock cores while maintaining torque margins of no less than 50% with an average power consumption of no greater than 90W and a tool mass of less than 6kg.

  10. Adaptive sampling for noisy problems

    SciTech Connect

    Cantu-Paz, E

    2004-03-26

    The usual approach to deal with noise present in many real-world optimization problems is to take an arbitrary number of samples of the objective function and use the sample average as an estimate of the true objective value. The number of samples is typically chosen arbitrarily and remains constant for the entire optimization process. This paper studies an adaptive sampling technique that varies the number of samples based on the uncertainty of deciding between two individuals. Experiments demonstrate the effect of adaptive sampling on the final solution quality reached by a genetic algorithm and the computational cost required to find the solution. The results suggest that the adaptive technique can effectively eliminate the need to set the sample size a priori, but in many cases it requires high computational costs.

  11. On-board sample cleaver.

    PubMed

    Månsson, Martin; Claesson, Thomas; Karlsson, Ulf O; Tjernberg, Oscar; Pailhés, Stéphane; Chang, Johan; Mesot, Joël; Shi, Ming; Patthey, Luc; Momono, Naoki; Oda, Migaku; Ido, Masayuki

    2007-07-01

    An on-board sample cleaver has been developed in order to cleave small and hard-to-cleave samples. To acquire good cleaves from rigid samples the alignment of the cleaving blade with respect to the internal crystallographic planes is crucial. To have the opportunity to mount the sample and align it to the blade ex situ has many advantages. The design presented has allowed us to cleave very tiny and rigid samples, e.g., the high-temperature superconductor La((2-x))Sr(x)CuO(4). Further, in this design the sample and the cleaver will have the same temperature, allowing us to cleave and keep the sample at low temperature. This is a big advantage over prior cleaver systems. As a result, better surfaces and alignments can be realized, which considerably simplifies and improves the experiments.

  12. Clean and Cold Sample Curation

    NASA Technical Reports Server (NTRS)

    Allen, C. C.; Agee, C. B.; Beer, R.; Cooper, B. L.

    2000-01-01

    Curation of Mars samples includes both samples that are returned to Earth, and samples that are collected, examined, and archived on Mars. Both kinds of curation operations will require careful planning to ensure that the samples are not contaminated by the instruments that are used to collect and contain them. In both cases, sample examination and subdivision must take place in an environment that is organically, inorganically, and biologically clean. Some samples will need to be prepared for analysis under ultra-clean or cryogenic conditions. Inorganic and biological cleanliness are achievable separately by cleanroom and biosafety lab techniques. Organic cleanliness to the <50 ng/sq cm level requires material control and sorbent removal - techniques being applied in our Class 10 cleanrooms and sample processing gloveboxes.

  13. Obstructions to Sampling Qualitative Properties

    PubMed Central

    Reimers, Arne C.

    2015-01-01

    Background Sampling methods have proven to be a very efficient and intuitive method to understand properties of complicated spaces that cannot easily be computed using deterministic methods. Therefore, sampling methods became a popular tool in the applied sciences. Results Here, we show that sampling methods are not an appropriate tool to analyze qualitative properties of complicated spaces unless RP = NP. We illustrate these results on the example of the thermodynamically feasible flux space of genome-scale metabolic networks and show that with artificial centering hit and run (ACHR) not all reactions that can have variable flux rates are sampled with variables flux rates. In particular a uniform sample of the flux space would not sample the flux variabilities completely. Conclusion We conclude that unless theoretical convergence results exist, qualitative results obtained from sampling methods should be considered with caution and if possible double checked using a deterministic method. PMID:26287384

  14. Sub-sampling and preparing forensic samples for pollen analysis.

    PubMed

    Horrocks, Mark

    2004-09-01

    The main forensic application of palynology is in providing associative evidence, assisting to prove or disprove a link between people and objects with places or with other people. Although identification and interpretation of pollen is a specialist job, sub-sampling and preparing pollen samples for analysis may be carried out by non-specialists. As few forensic laboratories have residing palynologists, laboratories may wish to reduce the cost of analysis or risk of contamination by doing their own sub-sampling and preparation. Presented is a practical guide for sub-sampling and preparing forensic samples for pollen analysis, providing a complete standard procedure for both the palynologist and non-specialist. Procedures for sub-sampling include a wide variety of materials commonly collected for forensic analysis (soil, clothing and other fabrics, footwear, twine and rope, firearms, granulated materials, plant and animal material, and illicit drugs), many of which palynologists will not be familiar with. Procedures for preparation of samples (pollen concentration) are presented as a detailed, step-by-step method. Minimizing the risks of laboratory and cross-sample contamination during sub-sampling and preparation is emphasized.

  15. Sampling almonds for aflatoxin, part I: estimation of uncertainty associated with sampling, sample preparation, and analysis.

    PubMed

    Whitaker, Thomas B; Slate, Andrew B; Jacobs, Merle; Hurley, J Michael; Adams, Julie G; Giesbrecht, Francis G

    2006-01-01

    Domestic and international regulatory limits have been established for aflatoxin in almonds and other tree nuts. It is difficult to obtain an accurate and precise estimate of the true aflatoxin concentration in a bulk lot because of the uncertainty associated with the sampling, sample preparation, and analytical steps of the aflatoxin test procedure. To evaluate the performance of aflatoxin sampling plans, the uncertainty associated with sampling lots of shelled almonds for aflatoxin was investigated. Twenty lots of shelled almonds were sampled for aflatoxin contamination. The total variance associated with measuring B1 and total aflatoxins in bulk almond lots was estimated and partitioned into sampling, sample preparation, and analytical variance components. All variances were found to increase with an increase in aflatoxin concentration (both B1 and total). By using regression analysis, mathematical expressions were developed to predict the relationship between each variance component (total, sampling, sample preparation, and analysis variances) and aflatoxin concentration. Variance estimates were the same for B1 and total aflatoxins. The mathematical relationships can be used to estimate each variance for a given sample size, subsample size, and number of analyses other than that measured in the study. When a lot with total aflatoxins at 15 ng/g was tested by using a 10 kg sample, a vertical cutter mixer type of mill, a 100 g subsample, and high-performance liquid chromatography analysis, the sampling, sample preparation, analytical, and total variances (coefficient of variation, CV) were 394.7 (CV, 132.4%), 14.7 (CV, 25.5%), 0.8 (CV, 6.1%), and 410.2 (CV, 135.0%), respectively. The percentages of the total variance associated with sampling, sample preparation, and analytical steps were 96.2, 3.6, and 0.2, respectively.

  16. Comet coma sample return instrument

    NASA Technical Reports Server (NTRS)

    Albee, A. L.; Brownlee, Don E.; Burnett, Donald S.; Tsou, Peter; Uesugi, K. T.

    1994-01-01

    The sample collection technology and instrument concept for the Sample of Comet Coma Earth Return Mission (SOCCER) are described. The scientific goals of this Flyby Sample Return are to return to coma dust and volatile samples from a known comet source, which will permit accurate elemental and isotopic measurements for thousands of individual solid particles and volatiles, detailed analysis of the dust structure, morphology, and mineralogy of the intact samples, and identification of the biogenic elements or compounds in the solid and volatile samples. Having these intact samples, morphologic, petrographic, and phase structural features can be determined. Information on dust particle size, shape, and density can be ascertained by analyzing penetration holes and tracks in the capture medium. Time and spatial data of dust capture will provide understanding of the flux dynamics of the coma and the jets. Additional information will include the identification of cosmic ray tracks in the cometary grains, which can provide a particle's process history and perhaps even the age of the comet. The measurements will be made with the same equipment used for studying micrometeorites for decades past; hence, the results can be directly compared without extrapolation or modification. The data will provide a powerful and direct technique for comparing the cometary samples with all known types of meteorites and interplanetary dust. This sample collection system will provide the first sample return from a specifically identified primitive body and will allow, for the first time, a direct method of matching meteoritic materials captured on Earth with known parent bodies.

  17. Comet coma sample return instrument

    NASA Astrophysics Data System (ADS)

    Albee, A. L.; Brownlee, Don E.; Burnett, Donald S.; Tsou, Peter; Uesugi, K. T.

    The sample collection technology and instrument concept for the Sample of Comet Coma Earth Return Mission (SOCCER) are described. The scientific goals of this Flyby Sample Return are to return to coma dust and volatile samples from a known comet source, which will permit accurate elemental and isotopic measurements for thousands of individual solid particles and volatiles, detailed analysis of the dust structure, morphology, and mineralogy of the intact samples, and identification of the biogenic elements or compounds in the solid and volatile samples. Having these intact samples, morphologic, petrographic, and phase structural features can be determined. Information on dust particle size, shape, and density can be ascertained by analyzing penetration holes and tracks in the capture medium. Time and spatial data of dust capture will provide understanding of the flux dynamics of the coma and the jets. Additional information will include the identification of cosmic ray tracks in the cometary grains, which can provide a particle's process history and perhaps even the age of the comet. The measurements will be made with the same equipment used for studying micrometeorites for decades past; hence, the results can be directly compared without extrapolation or modification. The data will provide a powerful and direct technique for comparing the cometary samples with all known types of meteorites and interplanetary dust. This sample collection system will provide the first sample return from a specifically identified primitive body and will allow, for the first time, a direct method of matching meteoritic materials captured on Earth with known parent bodies.

  18. SALTSTONE PROCESSING FACILITY TRANSFER SAMPLE

    SciTech Connect

    Cozzi, A.; Reigel, M.

    2010-08-04

    On May 19, 2010, the Saltstone Production Facility inadvertently transferred 1800 gallons of untreated waste from the salt feed tank to Vault 4. During shut down, approximately 70 gallons of the material was left in the Saltstone hopper. A sample of the slurry in the hopper was sent to Savannah River National Laboratory (SRNL) to analyze the density, pH and the eight Resource Conservation and Recovery Act (RCRA) metals. The sample was hazardous for chromium, mercury and pH. The sample received from the Saltstone hopper was analyzed visually while obtaining sample aliquots and while the sample was allowed to settle. It was observed that the sample contains solids that settle in approximately 20 minutes (Figure 3-1). There is a floating layer on top of the supernate during settling and disperses when the sample is agitated (Figure 3-2). The untreated waste inadvertently transferred from the SFT to Vault 4 was toxic for chromium and mercury. In addition, the pH of the sample is at the regulatory limit. Visually inspecting the sample indicates solids present in the sample.

  19. Sampling hazelnuts for aflatoxin: uncertainty associated with sampling, sample preparation, and analysis.

    PubMed

    Ozay, Guner; Seyhan, Ferda; Yilmaz, Aysun; Whitaker, Thomas B; Slate, Andrew B; Giesbrecht, Francis

    2006-01-01

    The variability associated with the aflatoxin test procedure used to estimate aflatoxin levels in bulk shipments of hazelnuts was investigated. Sixteen 10 kg samples of shelled hazelnuts were taken from each of 20 lots that were suspected of aflatoxin contamination. The total variance associated with testing shelled hazelnuts was estimated and partitioned into sampling, sample preparation, and analytical variance components. Each variance component increased as aflatoxin concentration (either B1 or total) increased. With the use of regression analysis, mathematical expressions were developed to model the relationship between aflatoxin concentration and the total, sampling, sample preparation, and analytical variances. The expressions for these relationships were used to estimate the variance for any sample size, subsample size, and number of analyses for a specific aflatoxin concentration. The sampling, sample preparation, and analytical variances associated with estimating aflatoxin in a hazelnut lot at a total aflatoxin level of 10 ng/g and using a 10 kg sample, a 50 g subsample, dry comminution with a Robot Coupe mill, and a high-performance liquid chromatographic analytical method are 174.40, 0.74, and 0.27, respectively. The sampling, sample preparation, and analytical steps of the aflatoxin test procedure accounted for 99.4, 0.4, and 0.2% of the total variability, respectively.

  20. Chemical analyses of provided samples

    NASA Technical Reports Server (NTRS)

    Becker, Christopher H.

    1993-01-01

    Two batches of samples were received and chemical analysis was performed of the surface and near surface regions of the samples by the surface analysis by laser ionization (SALI) method. The samples included four one-inch optics and several paint samples. The analyses emphasized surface contamination or modification. In these studies, pulsed sputtering by 7 keV Ar+ and primarily single-photon ionization (SPI) by coherent 118 nm radiation (at approximately 5 x 10(exp 5) W/cm(sup 2) were used. For two of the samples, also multiphoton ionization (MPI) at 266 nm (approximately 5 x 10(exp 11) W/cm(sup 2) was used. Most notable among the results was the silicone contamination on Mg2 mirror 28-92, and that the Long Duration Exposure Facility (LDEF) paint sample had been enriched in K and Na and depleted in Zn, Si, B, and organic compounds relative to the control paint.

  1. Acceptance sampling using judgmental and randomly selected samples

    SciTech Connect

    Sego, Landon H.; Shulman, Stanley A.; Anderson, Kevin K.; Wilson, John E.; Pulsipher, Brent A.; Sieber, W. Karl

    2010-09-01

    We present a Bayesian model for acceptance sampling where the population consists of two groups, each with different levels of risk of containing unacceptable items. Expert opinion, or judgment, may be required to distinguish between the high and low-risk groups. Hence, high-risk items are likely to be identifed (and sampled) using expert judgment, while the remaining low-risk items are sampled randomly. We focus on the situation where all observed samples must be acceptable. Consequently, the objective of the statistical inference is to quantify the probability that a large percentage of the unsampled items in the population are also acceptable. We demonstrate that traditional (frequentist) acceptance sampling and simpler Bayesian formulations of the problem are essentially special cases of the proposed model. We explore the properties of the model in detail, and discuss the conditions necessary to ensure that required samples sizes are non-decreasing function of the population size. The method is applicable to a variety of acceptance sampling problems, and, in particular, to environmental sampling where the objective is to demonstrate the safety of reoccupying a remediated facility that has been contaminated with a lethal agent.

  2. Study of sample drilling techniques for Mars sample return missions

    NASA Technical Reports Server (NTRS)

    Mitchell, D. C.; Harris, P. T.

    1980-01-01

    To demonstrate the feasibility of acquiring various surface samples for a Mars sample return mission the following tasks were performed: (1) design of a Mars rover-mounted drill system capable of acquiring crystalline rock cores; prediction of performance, mass, and power requirements for various size systems, and the generation of engineering drawings; (2) performance of simulated permafrost coring tests using a residual Apollo lunar surface drill, (3) design of a rock breaker system which can be used to produce small samples of rock chips from rocks which are too large to return to Earth, but too small to be cored with the Rover-mounted drill; (4)design of sample containers for the selected regolith cores, rock cores, and small particulate or rock samples; and (5) design of sample handling and transfer techniques which will be required through all phase of sample acquisition, processing, and stowage on-board the Earth return vehicle. A preliminary design of a light-weight Rover-mounted sampling scoop was also developed.

  3. Microwave sample preparation for analysis of metals in environmental samples

    SciTech Connect

    Collins, L.W.

    1996-10-01

    The unique nature of microwave energy enhances heating efficiency and improves acid digestion sample preparation. Faster sample preparation and improved precision of the analysis occur. These results will be illustrated in this presentation using various standard reference materials and environmentally important samples. The analytical microwave system used offers accurate temperature and pressure feedback control through the use of a hand-held controller or PC-based control. Digestions are performed in patented, user-friendly microwave vessels. USEPA Method 3015, {open_quotes}Microwave-Assisted Acid Digestion of Aqueous Samples and Extracts,{close_quotes} is properly performed when the sample is heated to 170{degrees}C within 10 minutes, and maintained for an additional 10 minutes. USEPA Method 3051, {open_quotes}Microwave-Assisted Acid Digestion of Sediments, Sludges, Soils, and Oils,{close_quotes} is properly performed when the sample is heated to 175{degrees}C within 5.5 minutes, and maintained at 175{degrees}C for an additional 4.5 minutes. After the timesaving microwave digestion period, the samples were analyzed for metals by ICP-AES. Excellent accuracy and precision were obtained, in addition to 90% time reduction when using microwave sample preparation.

  4. 16. DETAILED VIEW OF SAMPLING EQUIPMENT. SAMPLED OFFGAS IS SENT ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    16. DETAILED VIEW OF SAMPLING EQUIPMENT. SAMPLED OFF-GAS IS SENT THROUGH A FOUR - STAGE COLD WATER TRAP. COOLING OF THE GAS ALLOWS A CONDENSATE TO FORM. THE CONDENSATE IS ANALYZED FOR CHEMICAL CONTENT. (6/2/80) - Rocky Flats Plant, Plutonium Fabrication, Central section of Plant, Golden, Jefferson County, CO

  5. Sampling and sample processing in pesticide residue analysis

    Technology Transfer Automated Retrieval System (TEKTRAN)

    Proper sampling and sample processing in pesticide residue analysis of food and soil has always been essential to obtain accurate results, but the subject is becoming a greater concern as approximately 100 mg test portions are being analyzed with automated high-throughput analytical methods by agroc...

  6. Image correlation and sampling study

    NASA Technical Reports Server (NTRS)

    Popp, D. J.; Mccormack, D. S.; Sedwick, J. L.

    1972-01-01

    The development of analytical approaches for solving image correlation and image sampling of multispectral data is discussed. Relevant multispectral image statistics which are applicable to image correlation and sampling are identified. The general image statistics include intensity mean, variance, amplitude histogram, power spectral density function, and autocorrelation function. The translation problem associated with digital image registration and the analytical means for comparing commonly used correlation techniques are considered. General expressions for determining the reconstruction error for specific image sampling strategies are developed.

  7. Adaptive sampling in convergent beams.

    PubMed

    Espinosa, Julián; Mas, David; Pérez, Jorge; Illueca, Carlos

    2008-09-01

    Numerical calculation of convergent Fresnel patterns through fast Fourier transform usually requires a large number of samples to fulfill the Nyquist sampling condition around the focus. From polynomial decomposition of the wavefront it is possible to determine which polynomial orders are the main contributors to the number of samples. This information can be used to properly modify the initial wavefront and relax the Nyquist condition thus giving a more efficient numerical algorithm.

  8. Development of Sample Verification System for Sample Return Missions

    NASA Technical Reports Server (NTRS)

    Toda, Risaku; McKinney, Colin; Jackson, Shannon P.; Mojarradi, Mohammad; Trebi-Ollennu, Ashitey; Manohara, Harish

    2011-01-01

    This paper describes the development of a proof of-concept sample verification system (SVS) for in-situ mass measurement of planetary rock and soil sample in future robotic sample return missions. Our proof-of-concept SVS device contains a 10 cm diameter pressure sensitive elastic membrane placed at the bottom of a sample canister. The membrane deforms under the weight of accumulating planetary sample. The membrane is positioned in proximity to an opposing substrate with a narrow gap. The deformation of the membrane makes the gap to be narrower, resulting in increased capacitance between the two nearly parallel plates. Capacitance readout circuitry on a nearby printed circuit board (PCB) transmits data via a low-voltage differential signaling (LVDS) interface. The fabricated SVS proof-of-concept device has successfully demonstrated approximately 1pF/gram capacitance change

  9. Mars sample return: Site selection and sample acquisition study

    NASA Technical Reports Server (NTRS)

    Nickle, N. (Editor)

    1980-01-01

    Various vehicle and mission options were investigated for the continued exploration of Mars; the cost of a minimum sample return mission was estimated; options and concepts were synthesized into program possibilities; and recommendations for the next Mars mission were made to the Planetary Program office. Specific sites and all relevant spacecraft and ground-based data were studied in order to determine: (1) the adequacy of presently available data for identifying landing sities for a sample return mission that would assure the acquisition of material from the most important geologic provinces of Mars; (2) the degree of surface mobility required to assure sample acquisition for these sites; (3) techniques to be used in the selection and drilling of rock a samples; and (4) the degree of mobility required at the two Viking sites to acquire these samples.

  10. IWTU Process Sample Analysis Report

    SciTech Connect

    Nick Soelberg

    2013-04-01

    CH2M-WG Idaho (CWI) requested that Battelle Energy Alliance (BEA) analyze various samples collected during June – August 2012 at the Integrated Waste Treatment Facility (IWTU). Samples of IWTU process materials were collected from various locations in the process. None of these samples were radioactive. These samples were collected and analyzed to provide more understanding of the compositions of various materials in the process during the time of the process shutdown that occurred on June 16, 2012, while the IWTU was in the process of nonradioactive startup.

  11. The alteration of icy samples during sample acquisition

    NASA Astrophysics Data System (ADS)

    Mungas, G.; Bearman, G.; Beegle, L. W.; Hecht, M.; Peters, G. H.; Glucoft, J.; Strothers, K.

    2006-12-01

    Valid in situ scientific studies require both that samples be analyzed in as pristine condition as possible and that any modification from the pristine to the sampled state be well understood. While samples with low to high ice concentration are critical for the study of astrobiology and geology, they pose problems with respect to the sample acquisition, preparation and distribution systems (SPAD) upon which the analytical instruments depend. Most significant of the processes that occur during SPAD is sublimation or melting caused by thermal loading from drilling, coring, etc. as well as exposure to a dry low pressure ambient environment. These processes can alter the sample, as well as generating, meta-stable liquid water that can refreeze in the sample transfer mechanisms, interfering with proper operation and creating cross-contamination. We have investigated and quantified loss of volatiles such as H2O, CO, CO2, and organics contained within icy and powdered samples when acquired, processed and transferred. During development of the MSL rock crusher, for example, ice was observed to pressure-fuse and stick to the side even at -70C. We have investigated sublimation from sample acquisition at Martian temperature and pressure for a samples ranging from 10 to 100 water/dirt ratios. Using the RASP that will be on Phoenix, we have measured sublimation of ice during excavation at Martian pressure and find that the sublimation losses can range from 10 to 50 percent water. It is the thermal conductivity of the soil that determines local heat transport, and how much of the sample acquisition energy is wicked away into the soil and how much goes into the sample. Modeling of sample acquisition methods requires measurement of these parameters. There is a two phase model for thermal conductivity as a function of dirt/ice ratio but it needed to be validated. We used an ASTM method for measuring thermal conductivity and implemented it in the laboratory. The major conclusion is

  12. Environmental surveillance master sampling schedule

    SciTech Connect

    Bisping, L.E.

    1995-02-01

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest Laboratory (PNL) for the U.S. Department of Energy (DOE). This document contains the planned 1994 schedules for routine collection of samples for the Surface Environmental Surveillance Project (SESP), Drinking Water Project, and Ground-Water Surveillance Project. Samples are routinely collected for the SESP and analyzed to determine the quality of air, surface water, soil, sediment, wildlife, vegetation, foodstuffs, and farm products at Hanford Site and surrounding communities. The responsibility for monitoring onsite drinking water falls outside the scope of the SESP. PNL conducts the drinking water monitoring project concurrent with the SESP to promote efficiency and consistency, utilize expertise developed over the years, and reduce costs associated with management, procedure development, data management, quality control, and reporting. The ground-water sampling schedule identifies ground-water sampling .events used by PNL for environmental surveillance of the Hanford Site. Sampling is indicated as annual, semi-annual, quarterly, or monthly in the sampling schedule. Some samples are collected and analyzed as part of ground-water monitoring and characterization programs at Hanford (e.g. Resources Conservation and Recovery Act (RCRA), Comprehensive Environmental Response, Compensation, and Liability Act (CERCLA), or Operational). The number of samples planned by other programs are identified in the sampling schedule by a number in the analysis column and a project designation in the Cosample column. Well sampling events may be merged to avoid redundancy in cases where sampling is planned by both-environmental surveillance and another program.

  13. Bioaerosol sampling: sampling mechanisms, bioefficiency and field studies.

    PubMed

    Haig, C W; Mackay, W G; Walker, J T; Williams, C

    2016-07-01

    Investigations into the suspected airborne transmission of pathogens in healthcare environments have posed a challenge to researchers for more than a century. With each pathogen demonstrating a unique response to environmental conditions and the mechanical stresses it experiences, the choice of sampling device is not obvious. Our aim was to review bioaerosol sampling, sampling equipment, and methodology. A comprehensive literature search was performed, using electronic databases to retrieve English language papers on bioaerosol sampling. The review describes the mechanisms of popular bioaerosol sampling devices such as impingers, cyclones, impactors, and filters, explaining both their strengths and weaknesses, and the consequences for microbial bioefficiency. Numerous successful studies are described that point to best practice in bioaerosol sampling, from the use of small personal samplers to monitor workers' pathogen exposure through to large static samplers collecting airborne microbes in various healthcare settings. Of primary importance is the requirement that studies should commence by determining the bioefficiency of the chosen sampler and the pathogen under investigation within laboratory conditions. From such foundations, sampling for bioaerosol material in the complexity of the field holds greater certainty of successful capture of low-concentration airborne pathogens. From the laboratory to use in the field, this review enables the investigator to make informed decisions about the choice of bioaerosol sampler and its application.

  14. Rock Sample Destruction Limits for the Mars Sample Return Mission

    NASA Astrophysics Data System (ADS)

    Weiss, D. K.; Budney, C. J.; Shiraishi, L.; Klein, K.; Gilbert, J.

    2012-12-01

    Sample return missions, including the proposed Mars Sample Return (MSR) mission, propose to collect core samples from scientifically valuable sites on Mars. These core samples would undergo extreme forces during the drilling process, and during the reentry process if the Earth Entry Vehicle (EEV) performs a hard landing on Earth. Because of the foreseen damage to the cores, it is important to evaluate each core for rock quality. However, because no planetary core sample return mission has yet been conducted, it remains unclear as to how to assess the cores for rock quality. In this report, we describe the development of a metric designed to quantitatively assess the quality of the rock cores returned from MSR. We report on the process by which we tested the metric on core samples of Mars analogue materials, and the effectiveness of the core assessment metric (CAM) in assessing rock core quality before and after the cores were subjected to shocking (g forces representative of an EEV landing). Mars-analogue Basalt rock core. Cores like this one are being used to develop a metric with which to assess rock quality before and after shock-testing. The sample canister that houses the cores during shock-testing. SolidWorks design by James Gilbert.

  15. A Demonstration of Sample Segregation

    ERIC Educational Resources Information Center

    Fritz, Mark D.; Brumbach, Stephen B.; Hartman, JudithAnn R.

    2005-01-01

    The demonstration of sample segregation, which is simple, and visually compelling illustrates the importance of sample handling for students studying analytical chemistry and environmental chemistry. The mixture used in this demonstration has two components, which have big particle size, and different colors, which makes the segregation graphic.

  16. Gamma spectroscopy of environmental samples

    NASA Astrophysics Data System (ADS)

    Siegel, P. B.

    2013-05-01

    We describe experiments for the undergraduate laboratory that use a high-resolution gamma detector to measure radiation in environmental samples. The experiments are designed to instruct the students in the quantitative analysis of gamma spectra and secular equilibrium. Experiments include the radioactive dating of Brazil nuts, determining radioisotope concentrations in natural samples, and measurement of the 235U abundance in uranium rich rocks.

  17. FIELD SAMPLING PROTOCOLS AND ANALYSIS

    EPA Science Inventory

    I have been asked to speak again to the environmental science class regarding actual research scenarios related to my work at Kerr Lab. I plan to discuss sampling protocols along with various field analyses performed during sampling activities. Many of the students have never see...

  18. Simulated Sampling of Estuary Plankton

    ERIC Educational Resources Information Center

    Fortner, Rosanne W.; Jenkins, Deborah Bainer

    2009-01-01

    To find out about the microscopic life in the valuable estuary environment, it is usually necessary to be near the water. This dry lab offers an alternative, using authentic data and a simulation of plankton sampling. From the types of organisms found in the sample, middle school students can infer relationships in the biological and physical…

  19. Learning about Sampling with Boxer.

    ERIC Educational Resources Information Center

    Picciotto, Henri; Ploger, Don

    1991-01-01

    Described is an introductory probability and statistics class focused on teaching the concepts of sampling and binomial distributions through a strategy based on teacher and student generated simulation using the Boxer computer language. The value of integrating programing with teaching subject matter is demonstrated, and sample student work is…

  20. Sample Size for Correlation Estimates

    DTIC Science & Technology

    1989-09-01

    graphs, and computer programs are developed to find the sample number needed for a desired confidence interval size. Nonparametric measures of...correlation (Spearman’s ra and Kendall’s tau) are also examined for appropriate sample numbers when a specific confidence interval size desired.

  1. Learning to Reason from Samples

    ERIC Educational Resources Information Center

    Ben-Zvi, Dani; Bakker, Arthur; Makar, Katie

    2015-01-01

    The goal of this article is to introduce the topic of "learning to reason from samples," which is the focus of this special issue of "Educational Studies in Mathematics" on "statistical reasoning." Samples are data sets, taken from some wider universe (e.g., a population or a process) using a particular procedure…

  2. Sampling stratospheric aerosols with impactors

    NASA Technical Reports Server (NTRS)

    Oberbeck, Verne R.

    1989-01-01

    Derivation of statistically significant size distributions from impactor samples of rarefield stratospheric aerosols imposes difficult sampling constraints on collector design. It is shown that it is necessary to design impactors of different size for each range of aerosol size collected so as to obtain acceptable levels of uncertainty with a reasonable amount of data reduction.

  3. Insights into Cruciform Sample Design

    NASA Astrophysics Data System (ADS)

    Creuziger, A.; Iadicola, M. A.; Foecke, T.; Rust, E.; Banerjee, D.

    2017-01-01

    Four different cruciform sample designs, based on the work of Abu-Farha et al. (JOM 61:48, 2009) were studied. Key features of these designs are a recessed pocket with fillet and re-entrant corners. These samples were shown via digital image correlation to achieve widely differing strain values inside and outside the pocket. From the results of these tests, there are two competing failure mechanisms in the sample. The pocket region is affected by stress concentrations caused by the fillet, and re-entrant notches lead to strain-limited constraints similar to diffuse and localized necks in uniaxial samples. Balancing these two constraints determines the success or premature failure of the sample.

  4. Sample collection, biobanking, and analysis.

    PubMed

    Ahsman, Maurice J; Tibboel, Dick; Mathot, Ron A A; de Wildt, Saskia N

    2011-01-01

    Pediatric pharmacokinetic studies require sampling of biofluids from neonates and children. Limitations on sampling frequency and sample volume complicate the design of these studies. In addition, strict guidelines, designed to guarantee patient safety, are in place. This chapter describes the practical implications of sample collection and their storage, with special focus on the selection of the appropriate type of biofluid and withdrawal technique. In addition, we describe appropriate measures for storage of these specimens, for example, in the context of biobanking, and the requirements on drug assay methods that they pose. Pharmacokinetic studies in children are possible, but they require careful selection of an appropriate sampling method, specimen volume, and assay method. The checklist provided could help prospective researchers with the design of an appropriate study protocol and infrastructure.

  5. Sample push-out fixture

    DOEpatents

    Biernat, John L.

    2002-11-05

    This invention generally relates to the remote removal of pelletized samples from cylindrical containment capsules. V-blocks are used to receive the samples and provide guidance to push out rods. Stainless steel liners fit into the v-channels on the v-blocks which permits them to be remotely removed and replaced or cleaned to prevent cross contamination between capsules and samples. A capsule holder securely holds the capsule while allowing manual up/down and in/out movement to align each sample hole with the v-blocks. Both end sections contain identical v-blocks; one that guides the drive out screw and rods or manual push out rods and the other to receive the samples as they are driven out of the capsule.

  6. BACTERIOLOGICAL ANALYSIS WITH SAMPLING AND SAMPLE PRESERVATION SPECIFICS

    EPA Science Inventory

    Current federal regulations (40CFR 503) specify that under certain conditions treated municipal biosolids must be analyzed for fecal coliform or salmonellae. The regulations state that representative samples of biosolids must be collected and analyzed using standard methods. Th...

  7. Sample Results From Routine Salt Batch 7 Samples

    SciTech Connect

    Peters, T.

    2016-01-14

    Strip Effluent Hold Tank (SEHT) and Decontaminated Salt Solution Hold Tank (DSSHT) samples from several of the “microbatches” of Integrated Salt Disposition Project (ISDP) Salt Batch (“Macrobatch”) 7B have been analyzed for 238Pu, 90Sr, 137Cs, cations (Inductively Coupled Plasma Emission Spectroscopy - ICPES), and anions (Ion Chromatography Anions - IC-A). The analytical results from the current microbatch samples are similar to those from previous macrobatch samples. The Actinide Removal Process (ARP) and the Modular Caustic-Side Solvent Extraction Unit (MCU) continue to show more than adequate Pu and Sr removal, and there is a distinct positive trend in Cs removal (increasing cesium decontamination), due to the use of the Next Generation Solvent (NGS). The bulk chemistry of the DSSHT and SEHT samples do not show any signs of unusual behavior.

  8. Curation of Samples from Mars

    NASA Astrophysics Data System (ADS)

    Lindstrom, D.; Allen, C.

    One of the strong scientific reasons for returning samples from Mars is to search for evidence of current or past life in the samples. Because of the remote possibility that the samples may contain life forms that are hazardous to the terrestrial biosphere, the National Research Council has recommended that all samples returned from Mars be kept under strict biological containment until tests show that they can safely be released to other laboratories. It is possible that Mars samples may contain only scarce or subtle traces of life or prebiotic chemistry that could readily be overwhelmed by terrestrial contamination. Thus, the facilities used to contain, process, and analyze samples from Mars must have a combination of high-level biocontainment and organic / inorganic chemical cleanliness that is unprecedented. We have been conducting feasibility studies and developing designs for a facility that would be at least as capable as current maximum containment BSL-4 (BioSafety Level 4) laboratories, while simultaneously maintaining cleanliness levels exceeding those of the cleanest electronics manufacturing labs. Unique requirements for the processing of Mars samples have inspired a program to develop handling techniques that are much more precise and reliable than the approach (currently used for lunar samples) of employing gloved human hands in nitrogen-filled gloveboxes. Individual samples from Mars are expected to be much smaller than lunar samples, the total mass of samples returned by each mission being 0.5- 1 kg, compared with many tens of kg of lunar samples returned by each of the six Apollo missions. Smaller samp les require much more of the processing to be done under microscopic observation. In addition, the requirements for cleanliness and high-level containment would be difficult to satisfy while using traditional gloveboxes. JSC has constructed a laboratory to test concepts and technologies important to future sample curation. The Advanced Curation

  9. Sampling of illicit drugs for quantitative analysis--part III: sampling plans and sample preparations.

    PubMed

    Csesztregi, T; Bovens, M; Dujourdy, L; Franc, A; Nagy, J

    2014-08-01

    The findings in this paper are based on the results of our drug homogeneity studies and particle size investigations. Using that information, a general sampling plan (depicted in the form of a flow-chart) was devised that could be applied to the quantitative instrumental analysis of the most common illicit drugs: namely heroin, cocaine, amphetamine, cannabis resin, MDMA tablets and herbal cannabis in 'bud' form (type I). Other more heterogeneous forms of cannabis (type II) were found to require alternative, more traditional sampling methods. A table was constructed which shows the sampling uncertainty expected when a particular number of random increments are taken and combined to form a single primary sample. It also includes a recommended increment size; which is 1 g for powdered drugs and cannabis resin, 1 tablet for MDMA and 1 bud for herbal cannabis in bud form (type I). By referring to that table, individual laboratories can ensure that the sampling uncertainty for a particular drug seizure can be minimised, such that it lies in the same region as their analytical uncertainty for that drug. The table shows that assuming a laboratory wishes to quantitatively analyse a seizure of powdered drug or cannabis resin with a 'typical' heterogeneity, a primary sample of 15×1 g increments is generally appropriate. The appropriate primary sample for MDMA tablets is 20 tablets, while for herbal cannabis (in bud form) 50 buds were found to be appropriate. Our study also showed that, for a suitably homogenised primary sample of the most common powdered drugs, an analytical sample size of between 20 and 35 mg was appropriate and for herbal cannabis the appropriate amount was 200 mg. The need to ensure that the results from duplicate or multiple incremental sampling were compared, to demonstrate whether or not a particular seized material has a 'typical' heterogeneity and that the sampling procedure applied has resulted in a 'correct sample', was highlighted and the setting

  10. Dried saliva spot as a sampling technique for saliva samples.

    PubMed

    Abdel-Rehim, Abbi; Abdel-Rehim, Mohamed

    2014-06-01

    For the first time, dried saliva spot (DSS) was used as a sampling technique for saliva samples. In the DSS technique 50 μL of saliva was collected on filter paper and the saliva was then extracted with an organic solvent. The local anesthetic lidocaine was used as a model compound, which was determined in the DSS using liquid chromatography and mass spectrometry. The results obtained for the determination of lidocaine in saliva using DSS were compared with those from a previous study using a microextraction by packed sorbent syringe as the sampling method for saliva. This study shows that DSS can be used for the analysis of saliva samples. The method is promising and very easy in terms of sampling and extraction procedures. The results from this study are in good agreement with those from our previous work on the determination of lidocaine in saliva. DSS can open a new dimension in the saliva handling process in terms of sampling, storing and transport.

  11. Duplex sampling apparatus and method

    DOEpatents

    Brown, Paul E.; Lloyd, Robert

    1992-01-01

    An improved apparatus is provided for sampling a gaseous mixture and for measuring mixture components. The apparatus includes two sampling containers connected in series serving as a duplex sampling apparatus. The apparatus is adapted to independently determine the amounts of condensable and noncondensable gases in admixture from a single sample. More specifically, a first container includes a first port capable of selectively connecting to and disconnecting from a sample source and a second port capable of selectively connecting to and disconnecting from a second container. A second container also includes a first port capable of selectively connecting to and disconnecting from the second port of the first container and a second port capable of either selectively connecting to and disconnecting from a differential pressure source. By cooling a mixture sample in the first container, the condensable vapors form a liquid, leaving noncondensable gases either as free gases or dissolved in the liquid. The condensed liquid is heated to drive out dissolved noncondensable gases, and all the noncondensable gases are transferred to the second container. Then the first and second containers are separated from one another in order to separately determine the amount of noncondensable gases and the amount of condensable gases in the sample.

  12. Environmental surveillance master sampling schedule

    SciTech Connect

    Bisping, L.E.

    1991-01-01

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest Laboratory (PNL) for the US Department of Energy (DOE). This document contains the planned schedule for routine sample collection for the Surface Environmental Surveillance Project (SESP) and Ground-Water Monitoring Project. The routine sampling plan for the SESP has been revised this year to reflect changing site operations and priorities. Some sampling previously performed at least annually has been reduced in frequency, and some new sampling to be performed at a less than annual frequency has been added. Therefore, the SESP schedule reflects sampling to be conducted in calendar year 1991 as well as future years. The ground-water sampling schedule is for 1991. This schedule is subject to modification during the year in response to changes in Site operation, program requirements, and the nature of the observed results. Operational limitations such as weather, mechanical failures, sample availability, etc., may also require schedule modifications. Changes will be documented in the respective project files, but this plan will not be reissued. The purpose of these monitoring projects is to evaluate levels of radioactive and nonradioactive pollutants in the Hanford evirons.

  13. Rapid Sampling from Sealed Containers

    SciTech Connect

    Johnston, R.G.; Garcia, A.R.E.; Martinez, R.K.; Baca, E.T.

    1999-02-28

    The authors have developed several different types of tools for sampling from sealed containers. These tools allow the user to rapidly drill into a closed container, extract a sample of its contents (gas, liquid, or free-flowing powder), and permanently reseal the point of entry. This is accomplished without exposing the user or the environment to the container contents, even while drilling. The entire process is completed in less than 15 seconds for a 55 gallon drum. Almost any kind of container can be sampled (regardless of the materials) with wall thicknesses up to 1.3 cm and internal pressures up to 8 atm. Samples can be taken from the top, sides, or bottom of a container. The sampling tools are inexpensive, small, and easy to use. They work with any battery-powered hand drill. This allows considerable safety, speed, flexibility, and maneuverability. The tools also permit the user to rapidly attach plumbing, a pressure relief valve, alarms, or other instrumentation to a container. Possible applications include drum venting, liquid transfer, container flushing, waste characterization, monitoring, sampling for archival or quality control purposes, emergency sampling by rapid response teams, counter-terrorism, non-proliferation and treaty verification, and use by law enforcement personnel during drug or environmental raids.

  14. Biological Environmental Sampling Technologies Assessment

    DTIC Science & Technology

    2015-12-01

    sa ti li ty Types of surfaces Info only Can the device support all types of surface sampling to include but not limited to tile, concrete ...sampling to include but not limited to tile, concrete , wood, glass, stone, plastic, etc. Yes/no Informational only Yes N/A N/A Info only...include but not limited to tile, concrete , wood, glass, stone, plastic, etc. Yes/no Informational only Yes N/A N/A Info only Sampling area size

  15. Air sampling of smallpox virus

    PubMed Central

    Thomas, G.

    1974-01-01

    Airborne smallpox virus has been recovered in an isolation hospital using an adhesive surface sampling technique in the presence of very low aerosol concentrations. Previous work in this field is reviewed. Successful recovery of airborne virus depends on sampling large volumes of air with a suitable sampler and thorough investigation of the whole sample taken for the presence of viable virus. More information on the characteristics and behaviour of airborne smallpox virus is needed in particular with regard to the future design and siting of smallpox isolation units. PMID:4371586

  16. Contactless Calorimetry for Levitated Samples

    NASA Technical Reports Server (NTRS)

    Lee, M. C.; Dokko, W.

    1986-01-01

    Temperature and specific heat of hot sample measured with pyrometer in proposed experimental technique. Technique intended expecially for contactless calorimetry of such materials as undercooled molten alloys, samples of which must be levitated to prevent contamination and premature crystallization. Contactless calorimetry technique enables data to be taken over entire undercooling temperature range with only one sample. Technique proves valuable in study of undercooling because difference in specific heat between undercooled-liquid and crystalline phases at same temperature provides driving force to convert metastable undercooled phase to stable crystalline phase.

  17. Defining And Characterizing Sample Representativeness For DWPF Melter Feed Samples

    SciTech Connect

    Shine, E. P.; Poirier, M. R.

    2013-10-29

    Representative sampling is important throughout the Defense Waste Processing Facility (DWPF) process, and the demonstrated success of the DWPF process to achieve glass product quality over the past two decades is a direct result of the quality of information obtained from the process. The objective of this report was to present sampling methods that the Savannah River Site (SRS) used to qualify waste being dispositioned at the DWPF. The goal was to emphasize the methodology, not a list of outcomes from those studies. This methodology includes proven methods for taking representative samples, the use of controlled analytical methods, and data interpretation and reporting that considers the uncertainty of all error sources. Numerous sampling studies were conducted during the development of the DWPF process and still continue to be performed in order to evaluate options for process improvement. Study designs were based on use of statistical tools applicable to the determination of uncertainties associated with the data needs. Successful designs are apt to be repeated, so this report chose only to include prototypic case studies that typify the characteristics of frequently used designs. Case studies have been presented for studying in-tank homogeneity, evaluating the suitability of sampler systems, determining factors that affect mixing and sampling, comparing the final waste glass product chemical composition and durability to that of the glass pour stream sample and other samples from process vessels, and assessing the uniformity of the chemical composition in the waste glass product. Many of these studies efficiently addressed more than one of these areas of concern associated with demonstrating sample representativeness and provide examples of statistical tools in use for DWPF. The time when many of these designs were implemented was in an age when the sampling ideas of Pierre Gy were not as widespread as they are today. Nonetheless, the engineers and

  18. PPIS Information and Report Samples

    EPA Pesticide Factsheets

    Technical information about the Pesticide Product Information System and its downloadable file formats, and sample reporting for Federal Insecticide Fungicide and Rodenticide Act (FIFRA) section 3 and section 24(c).

  19. Microfluidic Sample Preparation for Immunoassays

    SciTech Connect

    Visuri, S; Benett, W; Bettencourt, K; Chang, J; Fisher, K; Hamilton, J; Krulevitch, P; Park, C; Stockton, C; Tarte, L; Wang, A; Wilson, T

    2001-08-09

    Researchers at Lawrence Livermore National Laboratory are developing means to collect and identify fluid-based biological pathogens in the forms of proteins, viruses, and bacteria. to support detection instruments, they are developing a flexible fluidic sample preparation unit. The overall goal of this Microfluidic Module is to input a fluid sample, containing background particulates and potentially target compounds, and deliver a processed sample for detection. They are developing techniques for sample purification, mixing, and filtration that would be useful to many applications including immunologic and nucleic acid assays. Many of these fluidic functions are accomplished with acoustic radiation pressure or dielectrophoresis. They are integrating these technologies into packaged systems with pumps and valves to control fluid flow through the fluidic circuit.

  20. Proposal for Microwave Boson Sampling

    NASA Astrophysics Data System (ADS)

    Peropadre, Borja; Guerreschi, Gian Giacomo; Huh, Joonsuk; Aspuru-Guzik, Alán

    2016-09-01

    Boson sampling, the task of sampling the probability distribution of photons at the output of a photonic network, is believed to be hard for any classical device. Unlike other models of quantum computation that require thousands of qubits to outperform classical computers, boson sampling requires only a handful of single photons. However, a scalable implementation of boson sampling is missing. Here, we show how superconducting circuits provide such platform. Our proposal differs radically from traditional quantum-optical implementations: rather than injecting photons in waveguides, making them pass through optical elements like phase shifters and beam splitters, and finally detecting their output mode, we prepare the required multiphoton input state in a superconducting resonator array, control its dynamics via tunable and dispersive interactions, and measure it with nondemolition techniques.

  1. Air Sampling System Evaluation Template

    SciTech Connect

    Blunt, Brent

    2000-05-09

    The ASSET1.0 software provides a template with which a user can evaluate an Air Sampling System against the latest version of ANSI N13.1 "Sampling and Monitoring Releases of Airborne Radioactive Substances from the Stacks and Ducts of Nuclear Facilities". The software uses the ANSI N13.1 PIC levels to establish basic design criteria for the existing or proposed sampling system. The software looks at such criteria as PIC level, type of radionuclide emissions, physical state of the radionuclide, nozzle entrance effects, particulate transmission effects, system and component accuracy and precision evaluations, and basic system operations to provide a detailed look at the subsystems of a monitoring and sampling system/program. A GAP evaluation can then be completed which leads to identification of design and operational flaws in the proposed systems. Corrective measures can then be limited to the GAPs.

  2. Mossbauer spectroscopy of moon samples.

    PubMed

    Muir, A H; Housley, R M; Grant, R W; Abdel-Gawad, M; Blander, M

    1970-01-30

    Lunar bulk sample 10084,85 (< 1 mm size dust), and samples from rocks 10017,17 (fine grained, vesicular), 10046,17 (breccia), 10057,59 (fine grained, vesicular, top surface), 10057,60 (fine grained, vesicular, interior), and 10058,24 (medium grained, not vesicular) have been investigated by (57)Fe Mössbauer spectroscopy. Iron metal and the Fe(2+) minerals ilmenite, pyroxene, troilite, and iron containing glass have been identified. An iron line of sample 10084,85 (originally sealed in nitrogen) showed no significant intensity change when the sample was exposed to air. The antiferromagnetic transition in several lunar ilmenites at 57(0) +/- 2 degrees K corresponds to stoichiometric FeTiO,. Magneticallv separated 10057 showed troilite and somne metallic iron.

  3. Death anxiety among Lebanese samples.

    PubMed

    Abdel-Khalek, A M

    1991-06-01

    An Arabic version of the Templer Death Anxiety Scale was administered to 673 Lebanese volunteer subjects (164 boys, 165 girls in secondary school, 170 men, 174 women undergraduates). Females attained higher mean death anxiety scores than males. The Lebanese samples had either the same or a lower mean score on death anxiety than their Arab peers, that is, Egyptians and Kuwaitians and also US samples. Split-half reliabilities ranged from .57 to .68.

  4. Gibbs Sampling for the Uninitiated

    DTIC Science & Technology

    2010-04-01

    CS-TR-4956 UMIACS-TR-2010-04 LAMP-TR-153 April 2010 GIBBS SAMPLING FOR THE UNINITIATED Philip Resnik Eric Hardisty Department of Linguistics...Institute for Advanced Computer Studies University of Maryland College Park, MD 20742-3275 resnik AT umd.edu Department of Computer Science Institute for...Prescribed by ANSI Std Z39-18 Gibbs Sampling for the Uninitiated Philip Resnik Department of Linguistics and Institute for Advanced Computer Studies

  5. Depth-discrete sampling port

    DOEpatents

    Pemberton, Bradley E.; May, Christopher P.; Rossabi, Joseph; Riha, Brian D.; Nichols, Ralph L.

    1999-01-01

    A sampling port is provided which has threaded ends for incorporating the port into a length of subsurface pipe. The port defines an internal receptacle which is in communication with subsurface fluids through a series of fine filtering slits. The receptacle is in further communication through a bore with a fitting carrying a length of tubing there which samples are transported to the surface. Each port further defines an additional bore through which tubing, cables, or similar components of adjacent ports may pass.

  6. Environmental surveillance master sampling schedule

    SciTech Connect

    Bisping, L.E.

    1993-01-01

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest Laboratory (PNL) for the US Department of Energy (DOE). Samples are routinely collected and analyzed to determine the quality of air, surface water, ground water, soil, sediment, wildlife, vegetation, foodstuffs, and farm products at Hanford Site and surrounding communities. This document contains the planned schedule for routine sample collection for the Surface Environmental Surveillance Project (SESP) and Drinking Water Project, and Ground-Water Surveillance Project.

  7. Sample-Based Surface Coloring

    PubMed Central

    Bürger, Kai; Krüger, Jens; Westermann, Rüdiger

    2011-01-01

    In this paper, we present a sample-based approach for surface coloring, which is independent of the original surface resolution and representation. To achieve this, we introduce the Orthogonal Fragment Buffer (OFB)—an extension of the Layered Depth Cube—as a high-resolution view-independent surface representation. The OFB is a data structure that stores surface samples at a nearly uniform distribution over the surface, and it is specifically designed to support efficient random read/write access to these samples. The data access operations have a complexity that is logarithmic in the depth complexity of the surface. Thus, compared to data access operations in tree data structures like octrees, data-dependent memory access patterns are greatly reduced. Due to the particular sampling strategy that is employed to generate an OFB, it also maintains sample coherence, and thus, exhibits very good spatial access locality. Therefore, OFB-based surface coloring performs significantly faster than sample-based approaches using tree structures. In addition, since in an OFB, the surface samples are internally stored in uniform 2D grids, OFB-based surface coloring can efficiently be realized on the GPU to enable interactive coloring of high-resolution surfaces. On the OFB, we introduce novel algorithms for color painting using volumetric and surface-aligned brushes, and we present new approaches for particle-based color advection along surfaces in real time. Due to the intermediate surface representation we choose, our method can be used to color polygonal surfaces as well as any other type of surface that can be sampled. PMID:20616392

  8. Onsite testing of pressure sampling

    NASA Technical Reports Server (NTRS)

    Mallory, R.

    1980-01-01

    Portable test instrument containing controller, pressure port identification, 5-V power source for transducer excitation, and digital voltmeter to test pressure sampling valves completely, including leak and plug check before, during, or after installation in any location or environment. Controller comprises 117/24-Vac 100-watt transformer, bridge rectifier, capacitive-discharge stepper, and constant voltage source for homing sampling valve. It also includes 5-V regulated power supply and bipolar digital voltmeter having 10-uV resolution.

  9. Depth-discrete sampling port

    DOEpatents

    Pemberton, Bradley E.; May, Christopher P.; Rossabi, Joseph; Riha, Brian D.; Nichols, Ralph L.

    1998-07-07

    A sampling port is provided which has threaded ends for incorporating the port into a length of subsurface pipe. The port defines an internal receptacle which is in communication with subsurface fluids through a series of fine filtering slits. The receptacle is in further communication through a bore with a fitting carrying a length of tubing there which samples are transported to the surface. Each port further defines an additional bore through which tubing, cables, or similar components of adjacent ports may pass.

  10. Sample Return: What Happens to the Samples on Earth?

    NASA Technical Reports Server (NTRS)

    McNamara, Karen

    2010-01-01

    As space agencies throughout the world turn their attention toward human exploration of the Moon, Mars, and the solar system beyond, there has been an increase in the number of robotic sample return missions proposed as precursors to these human endeavors. In reality, however, we, as a global community, have very little experience with robotic sample return missions: 3 of the Russian Luna Missions successfully returned lunar material in the 1970s; 28 years later, in 2004, NASA s Genesis Mission returned material from the solar wind; and in 2006, NASA s Stardust Mission returned material from the Comet Wild2. [Note: The Japanese Hyabusa mission continues in space with the hope of returning material from the asteroid 25143 Itokawa.] We launch many spacecraft to LEO and return them to Earth. We also launch spacecraft beyond LEO to explore the planets, our solar system, and beyond. Some even land on these bodies. But these do not return. So as we begin to contemplate the sample return missions of the future, some common questions arise: "What really happens when the capsule returns?" "Where does it land?" "Who retrieves it and just how do they do that?" "Where does it go after that?" "How do the scientists get the samples?" "Do they keep them?" "Who is in charge?" The questions are nearly endless. The goal of this paper/presentation is to uncover many of the mysteries of the post-return phase of a mission - from the time the return body enters the atmosphere until the mission ends and the samples become part of a long term collection. The discussion will be based largely on the author s own experience with both the Genesis and Stardust missions. Of course, these two missions have a great deal in common, being funded by the same NASA Program (Discovery) and having similar team composition. The intent, however, is to use these missions as examples in order to highlight the general requirements and the challenges in defining and meeting those requirements for the final

  11. Biofouling development on plasma treated samples versus layers coated samples

    NASA Astrophysics Data System (ADS)

    Hnatiuc, B.; Exnar, P.; Sabau, A.; Spatenka, P.; Dumitrache, C. L.; Hnatiuc, M.; Ghita, S.

    2016-12-01

    Biofouling is the most important cause of naval corrosion. In order to reduce the Biofouling development on naval materials as steel or resin, different new methods have been tested. These methods could help to follow the new IMO environment reglementations and they could replace few classic operations before the painting of the small ships. The replacement of these operations means a reduction in maintenance costs. Their action must influence especially the first two steps of the Biofouling development, called Microfouling, that demand about 24 hours. This work presents the comparative results of the Biofouling development on two different classic naval materials, steel and resin, for three treated samples, immersed in sea water. Non-thermal plasma, produced by GlidArc technology, is applied to the first sample, called GD. The plasma treatment was set to 10 minutes. The last two samples, called AE9 and AE10 are covered by hydrophobic layers, prepared from a special organic-inorganic sol synthesized by sol-gel method. Theoretically, because of the hydrophobic properties, the Biofouling formation must be delayed for AE9 and AE10. The Biofouling development on each treated sample was compared with a witness non-treated sample. The microbiological analyses have been done for 24 hours by epifluorescence microscopy, available for one single layer.

  12. Improving Lab Sample Management - POS/MCEARD

    EPA Science Inventory

    "Scientists face increasing challenges in managing their laboratory samples, including long-term storage of legacy samples, tracking multiple aliquots of samples for many experiments, and linking metadata to these samples. Other factors complicating sample management include the...

  13. GEOSTATISTICAL SAMPLING DESIGNS FOR HAZARDOUS WASTE SITES

    EPA Science Inventory

    This chapter discusses field sampling design for environmental sites and hazardous waste sites with respect to random variable sampling theory, Gy's sampling theory, and geostatistical (kriging) sampling theory. The literature often presents these sampling methods as an adversari...

  14. Precision of circular systematic sampling.

    PubMed

    Cruz-Orive, L M; Gual-Arnau, X

    2002-09-01

    In design stereology, many estimators require isotropic orientation of a test probe relative to the object in order to attain unbiasedness. In such cases, systematic sampling of orientations becomes imperative on grounds of efficiency and practical applicability. For instance, the planar nucleator and the vertical rotator imply systematic sampling on the circle, whereas the Buffon-Steinhaus method to estimate curve length in the plane, or the vertical designs to estimate surface area and curve length, imply systematic sampling on the semicircle. This leads to the need for predicting the precision of systematic sampling on the circle and the semicircle from a single sample. There are two main prediction approaches, namely the classical one of G. Matheron for non-necessarily periodic measurement functions, and a recent approach based on a global symmetric model of the covariogram, more specific for periodic measurement functions. The latter approach seems at least as satisfactory as the former for small sample sizes, and it is developed here incorporating local errors. Detailed examples illustrating common stereological tools are included.

  15. Sampling characteristics of satellite orbits

    NASA Technical Reports Server (NTRS)

    Wunsch, Carl

    1989-01-01

    The irregular space-time sampling of any finite region by an orbiting satellite raises difficult questions as to which frequencies and wavenumbers can be determined and which will alias into others. Conventional sampling theorems must be extended to account for both irregular data distributions and observational noise - the sampling irregularity making the system much more susceptible to noise than in regularly sampled cases. The problem is formulated here in terms of least-squares and applied to spacecraft in 10-day and 17-day repeating orbits. The 'diamond-pattern' laid down spatially in such repeating orbits means that either repeat period adequately samples the spatial variables, but the slow overall temporal coverage in the 17-day pattern leads to much greater uncertainty than in the shorter repeat cycle. The result is not definitive and it is not concluded that a 10-day orbit repeat is the most appropriate one. A major conclusion, however, is that different orbital choices have potentially quite different sampling characteristics which need to be analyzed in terms of the spectral characteristics of the moving sea surface.

  16. Improved sample size determination for attributes and variables sampling

    SciTech Connect

    Stirpe, D.; Picard, R.R.

    1985-01-01

    Earlier INMM papers have addressed the attributes/variables problem and, under conservative/limiting approximations, have reported analytical solutions for the attributes and variables sample sizes. Through computer simulation of this problem, we have calculated attributes and variables sample sizes as a function of falsification, measurement uncertainties, and required detection probability without using approximations. Using realistic assumptions for uncertainty parameters of measurement, the simulation results support the conclusions: (1) previously used conservative approximations can be expensive because they lead to larger sample sizes than needed; and (2) the optimal verification strategy, as well as the falsification strategy, are highly dependent on the underlying uncertainty parameters of the measurement instruments. 1 ref., 3 figs.

  17. Chemical Data for Precipitate Samples

    USGS Publications Warehouse

    Foster, Andrea L.; Koski, Randolph A.

    2008-01-01

    During studies of sulfide oxidation in coastal areas of Prince William Sound in 2005, precipitate samples were collected from onshore and intertidal locations near the Ellamar, Threeman, and Beatson mine sites (chapter A, fig. 1; table 7). The precipitates include jarosite and amorphous Fe oxyhydroxide from Ellamar, amorphous Fe oxyhydroxide from Threeman, and amorphous Fe oxyhydroxide, ferrihydrite, and schwertmannite from Beatson. Precipitates occurring in the form of loose, flocculant coatings were harvested using a syringe and concentrated in the field by repetitive decanting. Thicker accumulations were either scraped gently from rocks using a stainless steel spatula or were scooped directly into receptacles (polyethylene jars or plastic heavy-duty zippered bags). Most precipitate samples contain small amounts of sedimentary detritus. With three jarosite-bearing samples from Ellamar, an attempt was made to separate the precipitate from the heavy-mineral fraction of the sediment. In this procedure, the sample was stirred in a graduated cylinder containing deionized water. The jarosite-rich suspension was decanted onto analytical filter paper and air dried before analysis. Eleven precipitate samples from the three mine sites were analyzed in laboratories of the U.S. Geological Survey (USGS) in Denver, Colorado (table 8). Major and trace elements were determined by inductively coupled plasma-mass spectrometry following multiacid (HCl-HNO3-HClO4-HF) digestion (Briggs and Meier, 2002), except for mercury, which was analyzed by cold-vapor atomic absorption spectroscopy (Brown and others, 2002a). X-ray diffraction (XRD) analyses were performed on powdered samples (<200 mesh) by S. Sutley of the USGS. Additional details regarding sample preparation and detection limits are found in Taggert (2002). Discussions of the precipitate chemistry and associated microbial communities are presented in Koski and others (2008) and Foster and others (2008), respectively.

  18. Ball assisted device for analytical surface sampling

    SciTech Connect

    ElNaggar, Mariam S; Van Berkel, Gary J; Covey, Thomas R

    2015-11-03

    A system for sampling a surface includes a sampling probe having a housing and a socket, and a rolling sampling sphere within the socket. The housing has a sampling fluid supply conduit and a sampling fluid exhaust conduit. The sampling fluid supply conduit supplies sampling fluid to the sampling sphere. The sampling fluid exhaust conduit has an inlet opening for receiving sampling fluid carried from the surface by the sampling sphere. A surface sampling probe and a method for sampling a surface are also disclosed.

  19. Estimating regression coefficients from clustered samples: Sampling errors and optimum sample allocation

    NASA Technical Reports Server (NTRS)

    Kalton, G.

    1983-01-01

    A number of surveys were conducted to study the relationship between the level of aircraft or traffic noise exposure experienced by people living in a particular area and their annoyance with it. These surveys generally employ a clustered sample design which affects the precision of the survey estimates. Regression analysis of annoyance on noise measures and other variables is often an important component of the survey analysis. Formulae are presented for estimating the standard errors of regression coefficients and ratio of regression coefficients that are applicable with a two- or three-stage clustered sample design. Using a simple cost function, they also determine the optimum allocation of the sample across the stages of the sample design for the estimation of a regression coefficient.

  20. Compact drilling and sample system

    NASA Technical Reports Server (NTRS)

    Gillis-Smith, Greg R.; Petercsak, Doug

    1998-01-01

    The Compact Drilling and Sample System (CDSS) was developed to drill into terrestrial, cometary, and asteroid material in a cryogenic, vacuum environment in order to acquire subsurface samples. Although drills were used by the Apollo astronauts some 20 years ago, this drill is a fraction of the mass and power and operates completely autonomously, able to drill, acquire, transport, dock, and release sample containers in science instruments. The CDSS has incorporated into its control system the ability to gather science data about the material being drilled by measuring drilling rate per force applied and torque. This drill will be able to optimize rotation and thrust in order to achieve the highest drilling rate possible in any given sample. The drill can be commanded to drill at a specified force, so that force imparted on the rover or lander is limited. This paper will discuss the cryo dc brush motors, carbide gears, cryogenic lubrication, quick-release interchangeable sampling drill bits, percussion drilling and the control system developed to achieve autonomous, cryogenic, vacuum, lightweight drilling.

  1. Sample Results from Routine Salt Batch 7 Samples

    SciTech Connect

    Peters, T.

    2015-05-13

    Strip Effluent Hold Tank (SEHT) and Decontaminated Salt Solution Hold Tank (DSSHT) samples from several of the “microbatches” of Integrated Salt Disposition Project (ISDP) Salt Batch (“Macrobatch”) 7B have been analyzed for 238Pu, 90Sr, 137Cs, Inductively Coupled Plasma Emission Spectroscopy (ICPES), and Ion Chromatography Anions (IC-A). The results from the current microbatch samples are similar to those from earlier samples from this and previous macrobatches. The Actinide Removal Process (ARP) and the Modular Caustic-Side Solvent Extraction Unit (MCU) continue to show more than adequate Pu and Sr removal, and there is a distinct positive trend in Cs removal, due to the use of the Next Generation Solvent (NGS). The Savannah River National Laboratory (SRNL) notes that historically, most measured Concentration Factor (CF) values during salt processing have been in the 12-14 range. However, recent processing gives CF values closer to 11. This observation does not indicate that the solvent performance is suffering, as the Decontamination Factor (DF) has still maintained consistently high values. Nevertheless, SRNL will continue to monitor for indications of process upsets. The bulk chemistry of the DSSHT and SEHT samples do not show any signs of unusual behavior.

  2. Hermetic Seal Designs for Sample Return Sample Tubes

    NASA Technical Reports Server (NTRS)

    Younse, Paulo J.

    2013-01-01

    Prototypes have been developed of potential hermetic sample sealing techniques for encapsulating samples in a ˜1-cm-diameter thin-walled sample tube that are compatible with IMSAH (Integrated Mars Sample Acquisition and Handling) architecture. Techniques include a heat-activated, finned, shape memory alloy plug; a contracting shape memory alloy activated cap; an expanding shape memory alloy plug; and an expanding torque plug. Initial helium leak testing of the shape memory alloy cap and finned shape memory alloy plug seals showed hermetic- seal capability compared against an industry standard of <1×10-8 atm-cc/s He. These tests were run on both clean tubes and dirty tubes dipped in MMS (Mojave Mars Simulant). The leak tests were also performed after thermal cycling between -135 and +55 ºC to ensure seal integrity after Martian diurnal cycles. Developmental testing is currently being done on the expanding torque plug, and expanding shape memory alloy plug seal designs. The finned shape memory alloy (SMA) plug currently shows hermetic sealing capability based on preliminary tests.

  3. Environmental surveillance master sampling schedule

    SciTech Connect

    Bisping, L.E.

    1997-01-01

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest National Laboratory (PNNL)(a) for the US Department of Energy (DOE). This document contains the planned 1997 schedules for routine collection of samples for the Surface Environmental Surveillance Project (SESP) and Drinking Water Monitoring Project. In addition, Section 3.0, Biota, also reflects a rotating collection schedule identifying the year a specific sample is scheduled for collection. The purpose of these monitoring projects is to evaluate levels of radioactive and nonradioactive pollutants in the Hanford environs, as required in DOE Order 5400.1, General Environmental Protection Program, and DOE Order 5400.5, Radiation Protection of the Public and the Environment. The sampling methods will be the same as those described in the Environmental Monitoring Plan, US Department of Energy, Richland Operations Office, DOE/RL91-50, Rev. 1, US Department of Energy, Richland, Washington.

  4. Sample mounts for microcrystal crystallography

    NASA Technical Reports Server (NTRS)

    Thorne, Robert E. (Inventor); Stum, Zachary (Inventor); O'Neill, Kevin (Inventor); Kmetko, Jan (Inventor)

    2007-01-01

    Sample mounts (10) for mounting microcrystals of biological macromolecules for X-ray crystallography are prepared by using patterned thin polyimide films (12) that have curvature imparted thereto, for example, by being attached to a curved outer surface of a small metal rod (16). The patterned film (12) preferably includes a tapered tip end (24) for holding a crystal. Preferably, a small sample aperture is disposed in the film for reception of the crystal. A second, larger aperture can also be provided that is connected to the sample aperture by a drainage channel, allowing removal of excess liquid and easier manipulation in viscous solutions. The curvature imparted to the film (12) increases the film's rigidity and allows a convenient scoop-like action for retrieving crystals. The polyimide contributes minimally to background and absorption, and can be treated to obtain desired hydrophobicity or hydrophilicity.

  5. Sample preparation for STED microscopy.

    PubMed

    Wurm, Christian A; Neumann, Daniel; Schmidt, Roman; Egner, Alexander; Jakobs, Stefan

    2010-01-01

    Since the discovery of the diffraction barrier in the late nineteenth century, it has been commonly accepted that with far-field optical microscopy it is not possible to resolve structural details considerably finer than half the wavelength of light. The emergence of STED microscopy showed that, at least for fluorescence imaging, these limits can be overcome. Since STED microscopy is a far-field technique, in principle, the same sample preparation as for conventional confocal microscopy may be utilized. The increased resolution, however, requires additional precautions to ensure the structural preservation of the specimen. We present robust protocols to generate test samples for STED microscopy. These protocols for bead samples and immunolabeled mammalian cells may be used as starting points to adapt existing labeling strategies for the requirements of sub-diffraction resolution microscopy.

  6. Sample mounts for microcrystal crystallography

    NASA Technical Reports Server (NTRS)

    Thorne, Robert E. (Inventor); Stum, Zachary (Inventor); O'Neill, Kevin (Inventor); Kmetko, Jan (Inventor)

    2009-01-01

    Sample mounts (10) for mounting microcrystals of biological macromolecules for X-ray crystallography are prepared by using patterned thin polyimide films (12) that have curvature imparted thereto, for example, by being attached to a curved outer surface of a small metal rod (16). The patterned film (12) preferably includes a tip end (24) for holding a crystal. Preferably, a small sample aperture is disposed in the film for reception of the crystal. A second, larger aperture can also be provided that is connected to the sample aperture by a drainage channel, allowing removal of excess liquid and easier manipulation in viscous solutions. The curvature imparted to the film (12) increases the film's rigidity and allows a convenient scoop-like action for retrieving crystals. The polyimide contributes minimally to background and absorption, and can be treated to obtain desired hydrophobicity or hydrophilicity.

  7. 19 CFR 151.52 - Sampling procedures.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... composite sample of the shipment shall be drawn for assay, providing composite sampling is feasible and... composite sample shall consist of proportional parts by weight of the prepared sample drawn from the various... address of the sampling concern. (c) Samples taken by Customs. Where no commercial samples have been...

  8. 19 CFR 151.52 - Sampling procedures.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... composite sample of the shipment shall be drawn for assay, providing composite sampling is feasible and... composite sample shall consist of proportional parts by weight of the prepared sample drawn from the various... address of the sampling concern. (c) Samples taken by Customs. Where no commercial samples have been...

  9. 19 CFR 151.52 - Sampling procedures.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... composite sample of the shipment shall be drawn for assay, providing composite sampling is feasible and... composite sample shall consist of proportional parts by weight of the prepared sample drawn from the various... address of the sampling concern. (c) Samples taken by Customs. Where no commercial samples have been...

  10. 19 CFR 151.52 - Sampling procedures.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... composite sample of the shipment shall be drawn for assay, providing composite sampling is feasible and... composite sample shall consist of proportional parts by weight of the prepared sample drawn from the various... address of the sampling concern. (c) Samples taken by Customs. Where no commercial samples have been...

  11. Statistical Efficiency in Distance Sampling

    PubMed Central

    Clark, Robert Graham

    2016-01-01

    Distance sampling is a technique for estimating the abundance of animals or other objects in a region, allowing for imperfect detection. This paper evaluates the statistical efficiency of the method when its assumptions are met, both theoretically and by simulation. The theoretical component of the paper is a derivation of the asymptotic variance penalty for the distance sampling estimator arising from uncertainty about the unknown detection parameters. This asymptotic penalty factor is tabulated for several detection functions. It is typically at least 2 but can be much higher, particularly for steeply declining detection rates. The asymptotic result relies on a model which makes the strong assumption that objects are uniformly distributed across the region. The simulation study relaxes this assumption by incorporating over-dispersion when generating object locations. Distance sampling and strip transect estimators are calculated for simulated data, for a variety of overdispersion factors, detection functions, sample sizes and strip widths. The simulation results confirm the theoretical asymptotic penalty in the non-overdispersed case. For a more realistic overdispersion factor of 2, distance sampling estimation outperforms strip transect estimation when a half-normal distance function is correctly assumed, confirming previous literature. When the hazard rate model is correctly assumed, strip transect estimators have lower mean squared error than the usual distance sampling estimator when the strip width is close enough to its optimal value (± 75% when there are 100 detections; ± 50% when there are 200 detections). Whether the ecologist can set the strip width sufficiently accurately will depend on the circumstances of each particular study. PMID:26950934

  12. Sampled Longest Common Prefix Array

    NASA Astrophysics Data System (ADS)

    Sirén, Jouni

    When augmented with the longest common prefix (LCP) array and some other structures, the suffix array can solve many string processing problems in optimal time and space. A compressed representation of the LCP array is also one of the main building blocks in many compressed suffix tree proposals. In this paper, we describe a new compressed LCP representation: the sampled LCP array. We show that when used with a compressed suffix array (CSA), the sampled LCP array often offers better time/space trade-offs than the existing alternatives. We also show how to construct the compressed representations of the LCP array directly from a CSA.

  13. Inertial impaction air sampling device

    SciTech Connect

    Dewhurst, K.H.

    1987-12-10

    An inertial impactor to be used in an air sampling device for collection of respirable size particles in ambient air which may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry. 3 figs.

  14. Inertial impaction air sampling device

    SciTech Connect

    Dewhurst, K.H.

    1990-05-22

    An inertial impactor is designed which is to be used in an air sampling device for collection of respirable size particles in ambient air. The device may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry. 3 figs.

  15. GET electronics samples data analysis

    NASA Astrophysics Data System (ADS)

    Giovinazzo, J.; Goigoux, T.; Anvar, S.; Baron, P.; Blank, B.; Delagnes, E.; Grinyer, G. F.; Pancin, J.; Pedroza, J. L.; Pibernat, J.; Pollacco, E.; Rebii, A.; Roger, T.; Sizun, P.

    2016-12-01

    The General Electronics for TPCs (GET) has been developed to equip a generation of time projection chamber detectors for nuclear physics, and may also be used for a wider range of detector types. The goal of this paper is to propose first analysis procedures to be applied on raw data samples from the GET system, in order to correct for systematic effects observed on test measurements. We also present a method to estimate the response function of the GET system channels. The response function is required in analysis where the input signal needs to be reconstructed, in terms of time distribution, from the registered output samples.

  16. Amniocentesis and chorionic villus sampling.

    PubMed Central

    Shulman, L P; Elias, S

    1993-01-01

    Amniocentesis and chorionic villus sampling have been shown through prospective, multicenter trials to be safe and effective methods of prenatal diagnosis; accordingly, a knowledge of these tests is important for those physicians who care for women during their childbearing years. We review the indications, techniques, safety, accuracy, and efficacy of amniocentesis and chorionic villus sampling and compare the advantages and disadvantages of each diagnostic test. This review should enable physicians to provide appropriate counseling and information to women at increased risk for fetal abnormalities detectable by either of these procedures. Images PMID:8236967

  17. Sample Return Primer and Handbook

    NASA Technical Reports Server (NTRS)

    Barrow, Kirk; Cheuvront, Allan; Faris, Grant; Hirst, Edward; Mainland, Nora; McGee, Michael; Szalai, Christine; Vellinga, Joseph; Wahl, Thomas; Williams, Kenneth; Lee, Gentry; Duxbury, Thomas

    2007-01-01

    This three-part Sample Return Primer and Handbook provides a road map for conducting the terminal phase of a sample return mission. The main chapters describe element-by-element analyses and trade studies, as well as required operations plans, procedures, contingencies, interfaces, and corresponding documentation. Based on the experiences of the lead Stardust engineers, the topics include systems engineering (in particular range safety compliance), mission design and navigation, spacecraft hardware and entry, descent, and landing certification, flight and recovery operations, mission assurance and system safety, test and training, and the very important interactions with external support organizations (non-NASA tracking assets, landing site support, and science curation).

  18. Population samples and genotyping technology.

    PubMed

    Mack, S J; Sanchez-Mazas, A; Single, R M; Meyer, D; Hill, J; Dron, H A; Jani, A J; Thomson, G; Erlich, H A

    2007-04-01

    The 14th International HLA (human leukocyte antigen) Immunogenetics Workshop (14th-IHIWS) Biostatistics and Anthropology/Human Genetic Diversity project continues the population sampling, genotype data generation, and biostatistic analyses of the 13th International Histocompatibility Workshop Anthropology/Human Genetic Diversity Component, with the overall goal of further characterizing global HLA allele and haplotype diversity and better describing the relationships between major histocompatibility complex diversity, geography, linguistics, and population history. Since the 13th Workshop, new investigators have and continue to be recruited to the project and new high-resolution class I and class II genotype data are being generated for 112 population samples from around the world.

  19. Gaussian-mixture umbrella sampling

    PubMed Central

    van der Vaart, Arjan; Karplus, Martin

    2009-01-01

    We introduce the Gaussian-mixture umbrella sampling method (GAMUS), a biased molecular dynamics technique based on adaptive umbrella sampling that efficiently escapes free energy minima in multi-dimensional problems. The prior simulation data are reweighted with a maximum likelihood formulation, and the new approximate probability density is fit to a Gaussian-mixture model, augmented by information about the unsampled areas. The method can be used to identify free energy minima in multi-dimensional reaction coordinates. To illustrate GAMUS, we apply it to the alanine dipeptide (2D reaction coordinate) and tripeptide (4D reaction coordinate). PMID:19284746

  20. Sample acquisition and instrument deployment

    NASA Technical Reports Server (NTRS)

    Boyd, Robert C.

    1995-01-01

    Progress is reported in developing the Sample Acquisition and Instrument Deployment (SAID) system, a robotic system for deploying science instruments and acquiring samples for analysis. The system is a conventional four degree of freedom manipulator 2 meters in length. A baseline design has been achieved through analysis and trade studies. The design considers environmental operating conditions on the surface of Mars, as well as volume constraints on proposed Mars landers. Control issues have also been studied, and simulations of joint and tip movements have been performed. The systems have been fabricated and tested in environmental chambers, as well as soil testing and robotic control testing.

  1. The Ocean Sampling Day Consortium

    SciTech Connect

    Kopf, Anna; Bicak, Mesude; Kottmann, Renzo; Schnetzer, Julia; Kostadinov, Ivaylo; Lehmann, Katja; Fernandez-Guerra, Antonio; Jeanthon, Christian; Rahav, Eyal; Ullrich, Matthias; Wichels, Antje; Gerdts, Gunnar; Polymenakou, Paraskevi; Kotoulas, Giorgos; Siam, Rania; Abdallah, Rehab Z.; Sonnenschein, Eva C.; Cariou, Thierry; O’Gara, Fergal; Jackson, Stephen; Orlic, Sandi; Steinke, Michael; Busch, Julia; Duarte, Bernardo; Caçador, Isabel; Canning-Clode, João; Bobrova, Oleksandra; Marteinsson, Viggo; Reynisson, Eyjolfur; Loureiro, Clara Magalhães; Luna, Gian Marco; Quero, Grazia Marina; Löscher, Carolin R.; Kremp, Anke; DeLorenzo, Marie E.; Øvreås, Lise; Tolman, Jennifer; LaRoche, Julie; Penna, Antonella; Frischer, Marc; Davis, Timothy; Katherine, Barker; Meyer, Christopher P.; Ramos, Sandra; Magalhães, Catarina; Jude-Lemeilleur, Florence; Aguirre-Macedo, Ma Leopoldina; Wang, Shiao; Poulton, Nicole; Jones, Scott; Collin, Rachel; Fuhrman, Jed A.; Conan, Pascal; Alonso, Cecilia; Stambler, Noga; Goodwin, Kelly; Yakimov, Michael M.; Baltar, Federico; Bodrossy, Levente; Van De Kamp, Jodie; Frampton, Dion M. F.; Ostrowski, Martin; Van Ruth, Paul; Malthouse, Paul; Claus, Simon; Deneudt, Klaas; Mortelmans, Jonas; Pitois, Sophie; Wallom, David; Salter, Ian; Costa, Rodrigo; Schroeder, Declan C.; Kandil, Mahrous M.; Amaral, Valentina; Biancalana, Florencia; Santana, Rafael; Pedrotti, Maria Luiza; Yoshida, Takashi; Ogata, Hiroyuki; Ingleton, Tim; Munnik, Kate; Rodriguez-Ezpeleta, Naiara; Berteaux-Lecellier, Veronique; Wecker, Patricia; Cancio, Ibon; Vaulot, Daniel; Bienhold, Christina; Ghazal, Hassan; Chaouni, Bouchra; Essayeh, Soumya; Ettamimi, Sara; Zaid, El Houcine; Boukhatem, Noureddine; Bouali, Abderrahim; Chahboune, Rajaa; Barrijal, Said; Timinouni, Mohammed; El Otmani, Fatima; Bennani, Mohamed; Mea, Marianna; Todorova, Nadezhda; Karamfilov, Ventzislav; ten Hoopen, Petra; Cochrane, Guy; L’Haridon, Stephane; Bizsel, Kemal Can; Vezzi, Alessandro; Lauro, Federico M.; Martin, Patrick; Jensen, Rachelle M.; Hinks, Jamie; Gebbels, Susan; Rosselli, Riccardo; De Pascale, Fabio; Schiavon, Riccardo; dos Santos, Antonina; Villar, Emilie; Pesant, Stéphane; Cataletto, Bruno; Malfatti, Francesca; Edirisinghe, Ranjith; Silveira, Jorge A. Herrera; Barbier, Michele; Turk, Valentina; Tinta, Tinkara; Fuller, Wayne J.; Salihoglu, Ilkay; Serakinci, Nedime; Ergoren, Mahmut Cerkez; Bresnan, Eileen; Iriberri, Juan; Nyhus, Paul Anders Fronth; Bente, Edvardsen; Karlsen, Hans Erik; Golyshin, Peter N.; Gasol, Josep M.; Moncheva, Snejana; Dzhembekova, Nina; Johnson, Zackary; Sinigalliano, Christopher David; Gidley, Maribeth Louise; Zingone, Adriana; Danovaro, Roberto; Tsiamis, George; Clark, Melody S.; Costa, Ana Cristina; El Bour, Monia; Martins, Ana M.; Collins, R. Eric; Ducluzeau, Anne-Lise; Martinez, Jonathan; Costello, Mark J.; Amaral-Zettler, Linda A.; Gilbert, Jack A.; Davies, Neil; Field, Dawn; Glöckner, Frank Oliver

    2015-06-19

    In this study, Ocean Sampling Day was initiated by the EU-funded Micro B3 (Marine Microbial Biodiversity, Bioinformatics, Biotechnology) project to obtain a snapshot of the marine microbial biodiversity and function of the world’s oceans. It is a simultaneous global mega-sequencing campaign aiming to generate the largest standardized microbial data set in a single day. This will be achievable only through the coordinated efforts of an Ocean Sampling Day Consortium, supportive partnerships and networks between sites. This commentary outlines the establishment, function and aims of the Consortium and describes our vision for a sustainable study of marine microbial communities and their embedded functional traits.

  2. The ocean sampling day consortium.

    PubMed

    Kopf, Anna; Bicak, Mesude; Kottmann, Renzo; Schnetzer, Julia; Kostadinov, Ivaylo; Lehmann, Katja; Fernandez-Guerra, Antonio; Jeanthon, Christian; Rahav, Eyal; Ullrich, Matthias; Wichels, Antje; Gerdts, Gunnar; Polymenakou, Paraskevi; Kotoulas, Giorgos; Siam, Rania; Abdallah, Rehab Z; Sonnenschein, Eva C; Cariou, Thierry; O'Gara, Fergal; Jackson, Stephen; Orlic, Sandi; Steinke, Michael; Busch, Julia; Duarte, Bernardo; Caçador, Isabel; Canning-Clode, João; Bobrova, Oleksandra; Marteinsson, Viggo; Reynisson, Eyjolfur; Loureiro, Clara Magalhães; Luna, Gian Marco; Quero, Grazia Marina; Löscher, Carolin R; Kremp, Anke; DeLorenzo, Marie E; Øvreås, Lise; Tolman, Jennifer; LaRoche, Julie; Penna, Antonella; Frischer, Marc; Davis, Timothy; Katherine, Barker; Meyer, Christopher P; Ramos, Sandra; Magalhães, Catarina; Jude-Lemeilleur, Florence; Aguirre-Macedo, Ma Leopoldina; Wang, Shiao; Poulton, Nicole; Jones, Scott; Collin, Rachel; Fuhrman, Jed A; Conan, Pascal; Alonso, Cecilia; Stambler, Noga; Goodwin, Kelly; Yakimov, Michael M; Baltar, Federico; Bodrossy, Levente; Van De Kamp, Jodie; Frampton, Dion Mf; Ostrowski, Martin; Van Ruth, Paul; Malthouse, Paul; Claus, Simon; Deneudt, Klaas; Mortelmans, Jonas; Pitois, Sophie; Wallom, David; Salter, Ian; Costa, Rodrigo; Schroeder, Declan C; Kandil, Mahrous M; Amaral, Valentina; Biancalana, Florencia; Santana, Rafael; Pedrotti, Maria Luiza; Yoshida, Takashi; Ogata, Hiroyuki; Ingleton, Tim; Munnik, Kate; Rodriguez-Ezpeleta, Naiara; Berteaux-Lecellier, Veronique; Wecker, Patricia; Cancio, Ibon; Vaulot, Daniel; Bienhold, Christina; Ghazal, Hassan; Chaouni, Bouchra; Essayeh, Soumya; Ettamimi, Sara; Zaid, El Houcine; Boukhatem, Noureddine; Bouali, Abderrahim; Chahboune, Rajaa; Barrijal, Said; Timinouni, Mohammed; El Otmani, Fatima; Bennani, Mohamed; Mea, Marianna; Todorova, Nadezhda; Karamfilov, Ventzislav; Ten Hoopen, Petra; Cochrane, Guy; L'Haridon, Stephane; Bizsel, Kemal Can; Vezzi, Alessandro; Lauro, Federico M; Martin, Patrick; Jensen, Rachelle M; Hinks, Jamie; Gebbels, Susan; Rosselli, Riccardo; De Pascale, Fabio; Schiavon, Riccardo; Dos Santos, Antonina; Villar, Emilie; Pesant, Stéphane; Cataletto, Bruno; Malfatti, Francesca; Edirisinghe, Ranjith; Silveira, Jorge A Herrera; Barbier, Michele; Turk, Valentina; Tinta, Tinkara; Fuller, Wayne J; Salihoglu, Ilkay; Serakinci, Nedime; Ergoren, Mahmut Cerkez; Bresnan, Eileen; Iriberri, Juan; Nyhus, Paul Anders Fronth; Bente, Edvardsen; Karlsen, Hans Erik; Golyshin, Peter N; Gasol, Josep M; Moncheva, Snejana; Dzhembekova, Nina; Johnson, Zackary; Sinigalliano, Christopher David; Gidley, Maribeth Louise; Zingone, Adriana; Danovaro, Roberto; Tsiamis, George; Clark, Melody S; Costa, Ana Cristina; El Bour, Monia; Martins, Ana M; Collins, R Eric; Ducluzeau, Anne-Lise; Martinez, Jonathan; Costello, Mark J; Amaral-Zettler, Linda A; Gilbert, Jack A; Davies, Neil; Field, Dawn; Glöckner, Frank Oliver

    2015-01-01

    Ocean Sampling Day was initiated by the EU-funded Micro B3 (Marine Microbial Biodiversity, Bioinformatics, Biotechnology) project to obtain a snapshot of the marine microbial biodiversity and function of the world's oceans. It is a simultaneous global mega-sequencing campaign aiming to generate the largest standardized microbial data set in a single day. This will be achievable only through the coordinated efforts of an Ocean Sampling Day Consortium, supportive partnerships and networks between sites. This commentary outlines the establishment, function and aims of the Consortium and describes our vision for a sustainable study of marine microbial communities and their embedded functional traits.

  3. Inertial impaction air sampling device

    DOEpatents

    Dewhurst, Katharine H.

    1990-01-01

    An inertial impactor to be used in an air sampling device for collection of respirable size particles in ambient air which may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry.

  4. DNest3: Diffusive Nested Sampling

    NASA Astrophysics Data System (ADS)

    Brewer, Brendon

    2016-04-01

    DNest3 is a C++ implementation of Diffusive Nested Sampling (ascl:1010.029), a Markov Chain Monte Carlo (MCMC) algorithm for Bayesian Inference and Statistical Mechanics. Relative to older DNest versions, DNest3 has improved performance (in terms of the sampling overhead, likelihood evaluations still dominate in general) and is cleaner code: implementing new models should be easier than it was before. In addition, DNest3 is multi-threaded, so one can run multiple MCMC walkers at the same time, and the results will be combined together.

  5. Sampling Errors of Variance Components.

    ERIC Educational Resources Information Center

    Sanders, Piet F.

    A study on sampling errors of variance components was conducted within the framework of generalizability theory by P. L. Smith (1978). The study used an intuitive approach for solving the problem of how to allocate the number of conditions to different facets in order to produce the most stable estimate of the universe score variance. Optimization…

  6. Sample processor for chemical analysis

    NASA Technical Reports Server (NTRS)

    Boettger, Heinz G. (Inventor)

    1980-01-01

    An apparatus is provided which can process numerous samples that must be chemically analyzed by the application of fluids such as liquid reagents, solvents and purge gases, as well as the application of dumps for receiving the applied fluid after they pass across the sample, in a manner that permits numerous samples to be processed in a relatively short time and with minimal manpower. The processor includes a rotor which can hold numerous cartridges containing inert or adsorbent material for holding samples, and a pair of stators on opposite sides of the rotor. The stators form stations spaced along the path of the cartridges which lie in the rotor, and each station can include an aperture in one stator through which a fluid can be applied to a cartridge resting at that station, and an aperture in the other stator which can receive the fluid which has passed through the cartridge. The stators are sealed to the ends of the cartridges lying on the rotor, to thereby isolate the stations from one another.

  7. [Clinical research V. Sample size].

    PubMed

    Talavera, Juan O; Rivas-Ruiz, Rodolfo; Bernal-Rosales, Laura Paola

    2011-01-01

    In clinical research it is impossible and inefficient to study all patients with a specific pathology, so it is necessary to study a sample of them. The estimation of the sample size before starting a study guarantees the stability of the results and allows us to foresee the feasibility of the study depending on the availability of patients and cost. The basic structure of sample size estimation is based on the premise that seeks to demonstrate, among other cases, that the observed difference between two or more maneuvers in the subsequent state is real. Initially, it requires knowing the value of the expected difference (δ) and its data variation (standard deviation). These data are usually obtained from previous studies. Then, other components must be considered: a (alpha), percentage of error in the assertion that the difference between means is real, usually 5 %; and β, error rate accepting the claim that the no-difference between the means is real, usually ranging from 15 to 20 %. Finally, these values are substituted into the formula or in an electronic program for estimating sample size. While summary and dispersion measures vary with the type of variable according to the outcome, the basic structure is the same.

  8. Environmental surveillance master sampling schedule

    SciTech Connect

    Bisping, L.E.

    1996-02-01

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest National Laboratory (PNNL) for the US Department of Energy (DOE). This document contains the planned 1996 schedules for routine collection of samples for the Surface Environmental Surveillance Project (SESP), Drinking Water Project, and Ground-Water Surveillance Project.

  9. Environmental surveillance master sampling schedule

    SciTech Connect

    Bisping, L.E.

    1994-02-01

    This document contains the planned 1994 schedules for routine collection of samples for the Surface Environmental Surveillance Project (SESP), Drinking Water Project, and Ground-Water Surveillance Project. Samples are routinely collected for the SESP and analyzed to determine the quality of air, surface water, soil, sediment, wildlife, vegetation, foodstuffs, and farm products at Hanford Site and surrounding communities. The responsibility for monitoring the onsite drinking water falls outside the scope of the SESP. The Hanford Environmental Health Foundation is responsible for monitoring the nonradiological parameters as defined in the National Drinking Water Standards while PNL conducts the radiological monitoring of the onsite drinking water. PNL conducts the drinking water monitoring project concurrent with the SESP to promote efficiency and consistency, utilize the expertise developed over the years, and reduce costs associated with management, procedure development, data management, quality control and reporting. The ground-water sampling schedule identifies ground-water sampling events used by PNL for environmental surveillance of the Hanford Site.

  10. Workplace Education Sample Evaluation Report.

    ERIC Educational Resources Information Center

    Bozarjian, Bob; Uvin, Johan

    This sample evaluation report is part of a series of resources developed for and by workplace education practitioners in business, education, and labor partnerships funded through the Massachusetts Department of Education's Workplace Literacy Program. Data included in the report are based on Project Health, which integrates the experiences from…

  11. Elaborating transition interface sampling methods

    SciTech Connect

    Erp, Titus S. van . E-mail: bolhuis@science.uva.nl

    2005-05-01

    We review two recently developed efficient methods for calculating rate constants of processes dominated by rare events in high-dimensional complex systems. The first is transition interface sampling (TIS), based on the measurement of effective fluxes through hypersurfaces in phase space. TIS improves efficiency with respect to standard transition path sampling (TPS) rate constant techniques, because it allows a variable path length and is less sensitive to recrossings. The second method is the partial path version of TIS. Developed for diffusive processes, it exploits the loss of long time correlation. We discuss the relation between the new techniques and the standard reactive flux methods in detail. Path sampling algorithms can suffer from ergodicity problems, and we introduce several new techniques to alleviate these problems, notably path swapping, stochastic configurational bias Monte Carlo shooting moves and order-parameter free path sampling. In addition, we give algorithms to calculate other interesting properties from path ensembles besides rate constants, such as activation energies and reaction mechanisms.

  12. Sampling Assumptions in Inductive Generalization

    ERIC Educational Resources Information Center

    Navarro, Daniel J.; Dry, Matthew J.; Lee, Michael D.

    2012-01-01

    Inductive generalization, where people go beyond the data provided, is a basic cognitive capability, and it underpins theoretical accounts of learning, categorization, and decision making. To complete the inductive leap needed for generalization, people must make a key "sampling" assumption about how the available data were generated.…

  13. Micropaleontological studies of lunar samples.

    PubMed

    Schopf, J W

    1970-01-30

    Optical and electron microscopic studies of rock chips and dust from the bulk sample box returned by Apollo 11 and of petrographic thin sections and acid-resistant residues of lunar material have yielded no evidence of indigenous biological activity. vestigations.

  14. Curiosity analyzes Martian soil samples

    NASA Astrophysics Data System (ADS)

    Showstack, Randy; Balcerak, Ernie

    2012-12-01

    NASA's Mars Curiosity rover has conducted its first analysis of Martian soil samples using multiple instruments, the agency announced at a 3 December news briefing at the AGU Fall Meeting in San Francisco. "These results are an unprecedented look at the chemical diversity in the area," said NASA's Michael Meyer, program scientist for Curiosity.

  15. More about sampling and estimation of mercaptans in air samples.

    PubMed

    Moliner-Martínez, Y; Herráez-Hernández, R; Molins-Legua, C; Verdú-Andrés, J; Avella-Oliver, M; Campíns-Falcó, P

    2013-03-15

    Several strategies have been developed for sampling and determination of volatile thiols. The selectivity and sensitivity of the proposed methodologies are achieved by using a specific derivatizing reagent. The different procedures assayed are based on air sampling followed by derivatization of the analytes with OPA and isoleucine in alkaline solution. The derivatization products are separated and determined by liquid chromatography and fluorescence detection. To start, the derivatization conditions and stability of the derivates have been studied in order to establish the storage conditions. In general, the strategies studied consisted on trapping and detivatization the thiol compound on different support; a solution (Impinger) or sorbent (C₁₈ cartridges or glass fiber filter). The analytical properties of the different strategies have been obtained and compared. Procedures are recommended upon specific situations.

  16. Sample size and optimal sample design in tuberculosis surveys

    PubMed Central

    Sánchez-Crespo, J. L.

    1967-01-01

    Tuberculosis surveys sponsored by the World Health Organization have been carried out in different communities during the last few years. Apart from the main epidemiological findings, these surveys have provided basic statistical data for use in the planning of future investigations. In this paper an attempt is made to determine the sample size desirable in future surveys that include one of the following examinations: tuberculin test, direct microscopy, and X-ray examination. The optimum cluster sizes are found to be 100-150 children under 5 years of age in the tuberculin test, at least 200 eligible persons in the examination for excretors of tubercle bacilli (direct microscopy) and at least 500 eligible persons in the examination for persons with radiological evidence of pulmonary tuberculosis (X-ray). Modifications of the optimum sample size in combined surveys are discussed. PMID:5300008

  17. AUTOMATING GROUNDWATER SAMPLING AT HANFORD

    SciTech Connect

    CONNELL CW; HILDEBRAND RD; CONLEY SF; CUNNINGHAM DE

    2009-01-16

    Until this past October, Fluor Hanford managed Hanford's integrated groundwater program for the U.S. Department of Energy (DOE). With the new contract awards at the Site, however, the CH2M HILL Plateau Remediation Company (CHPRC) has assumed responsibility for the groundwater-monitoring programs at the 586-square-mile reservation in southeastern Washington State. These programs are regulated by the Resource Conservation and Recovery Act (RCRA) and the Comprehensive Environmental Response Compensation and Liability Act (CERCLA). The purpose of monitoring is to track existing groundwater contamination from past practices, as well as other potential contamination that might originate from RCRA treatment, storage, and disposal (TSD) facilities. An integral part of the groundwater-monitoring program involves taking samples of the groundwater and measuring the water levels in wells scattered across the site. More than 1,200 wells are sampled each year. Historically, field personnel or 'samplers' have been issued pre-printed forms that have information about the well(s) for a particular sampling evolution. This information is taken from the Hanford Well Information System (HWIS) and the Hanford Environmental Information System (HEIS)--official electronic databases. The samplers used these hardcopy forms to document the groundwater samples and well water-levels. After recording the entries in the field, the samplers turned the forms in at the end of the day and the collected information was posted onto a spreadsheet that was then printed and included in a log book. The log book was then used to make manual entries of the new information into the software application(s) for the HEIS and HWIS databases. This is a pilot project for automating this tedious process by providing an electronic tool for automating water-level measurements and groundwater field-sampling activities. The automation will eliminate the manual forms and associated data entry, improve the accuracy of the

  18. Apparatus for Sampling Surface Contamination

    NASA Technical Reports Server (NTRS)

    Wells, Mark

    2008-01-01

    An apparatus denoted a swab device has been developed as a convenient means of acquiring samples of contaminants from surfaces and suspending the samples in liquids. (Thereafter, the liquids can be dispensed, in controlled volumes, into scientific instruments for analysis of the contaminants.) The swab device is designed so as not to introduce additional contamination and to facilitate, simplify, and systematize the dispensing of controlled volumes of liquid into analytical instruments. The swab device is a single apparatus into which are combined all the equipment and materials needed for sampling surface contamination. The swab device contains disposable components stacked together on a nondisposable dispensing head. One of the disposable components is a supply cartridge holding a sufficient volume of liquid for one complete set of samples. (The liquid could be clean water or another suitable solvent, depending on the application.) This supply of liquid is sealed by Luer valves. At the beginning of a sampling process, the user tears open a sealed bag containing the supply cartridge. A tip on the nondisposable dispensing head is engaged with a Luer valve on one end of the supply cartridge and rotated, locking the supply cartridge on the dispensing head and opening the valve. The swab tip includes a fabric swab that is wiped across the surface of interest to acquire a sample. A sealed bag containing a disposable dispensing tip is then opened, and the swab tip is pushed into the dispensing tip until seated. The dispensing head contains a piston that passes through a spring-loaded lip seal. The air volume displaced by this piston forces the liquid out of the supply cartridge, over the swab, and into the dispensing tip. The piston is manually cycled to enforce oscillation of the air volume and thereby to cause water to flow to wash contaminants from the swab and cause the resulting liquid suspension of contaminants to flow into the dispensing tip. After several cycles

  19. Phobos Sample Return: Next Approach

    NASA Astrophysics Data System (ADS)

    Zelenyi, Lev; Martynov, Maxim; Zakharov, Alexander; Korablev, Oleg; Ivanov, Alexey; Karabadzak, George

    The Martian moons still remain a mystery after numerous studies by Mars orbiting spacecraft. Their study cover three major topics related to (1) Solar system in general (formation and evolution, origin of planetary satellites, origin and evolution of life); (2) small bodies (captured asteroid, or remnants of Mars formation, or reaccreted Mars ejecta); (3) Mars (formation and evolution of Mars; Mars ejecta at the satellites). As reviewed by Galimov [2010] most of the above questions require the sample return from the Martian moon, while some (e.g. the characterization of the organic matter) could be also answered by in situ experiments. There is the possibility to obtain the sample of Mars material by sampling Phobos: following to Chappaz et al. [2012] a 200-g sample could contain 10-7 g of Mars surface material launched during the past 1 mln years, or 5*10-5 g of Mars material launched during the past 10 mln years, or 5*1010 individual particles from Mars, quantities suitable for accurate laboratory analyses. The studies of Phobos have been of high priority in the Russian program on planetary research for many years. Phobos-88 mission consisted of two spacecraft (Phobos-1, Phobos-2) and aimed the approach to Phobos at 50 m and remote studies, and also the release of small landers (long-living stations DAS). This mission implemented the program incompletely. It was returned information about the Martian environment and atmosphere. The next profect Phobos Sample Return (Phobos-Grunt) initially planned in early 2000 has been delayed several times owing to budget difficulties; the spacecraft failed to leave NEO in 2011. The recovery of the science goals of this mission and the delivery of the samples of Phobos to Earth remain of highest priority for Russian scientific community. The next Phobos SR mission named Boomerang was postponed following the ExoMars cooperation, but is considered the next in the line of planetary exploration, suitable for launch around 2022. A

  20. Authentication of forensic DNA samples.

    PubMed

    Frumkin, Dan; Wasserstrom, Adam; Davidson, Ariane; Grafit, Arnon

    2010-02-01

    Over the past twenty years, DNA analysis has revolutionized forensic science, and has become a dominant tool in law enforcement. Today, DNA evidence is key to the conviction or exoneration of suspects of various types of crime, from theft to rape and murder. However, the disturbing possibility that DNA evidence can be faked has been overlooked. It turns out that standard molecular biology techniques such as PCR, molecular cloning, and recently developed whole genome amplification (WGA), enable anyone with basic equipment and know-how to produce practically unlimited amounts of in vitro synthesized (artificial) DNA with any desired genetic profile. This artificial DNA can then be applied to surfaces of objects or incorporated into genuine human tissues and planted in crime scenes. Here we show that the current forensic procedure fails to distinguish between such samples of blood, saliva, and touched surfaces with artificial DNA, and corresponding samples with in vivo generated (natural) DNA. Furthermore, genotyping of both artificial and natural samples with Profiler Plus((R)) yielded full profiles with no anomalies. In order to effectively deal with this problem, we developed an authentication assay, which distinguishes between natural and artificial DNA based on methylation analysis of a set of genomic loci: in natural DNA, some loci are methylated and others are unmethylated, while in artificial DNA all loci are unmethylated. The assay was tested on natural and artificial samples of blood, saliva, and touched surfaces, with complete success. Adopting an authentication assay for casework samples as part of the forensic procedure is necessary for maintaining the high credibility of DNA evidence in the judiciary system.

  1. Sampling honeybee colonies for brood production: a double sampling technique

    SciTech Connect

    Rogers, L.E.; Gilbert, R.O.; Burgett, M.

    1983-01-01

    A procedure is described for estimating numbers of capped brood cells by double sampling combined with linear regression. A complete census of capped brood cells is better than an estimate, provided it is possible to count all brood cells directly or from photographs of brood frames. The double sampling technique, however, has the advantage of enabling data to be collected more quickly and at a lower cost than for a complete count. It also provides an estimate of the approximate variability associated with brood estimates and a mechanism for correcting biases associated with different investigators or with estimates by the same individual at different times or under different conditions. The technique is easy to apply in the field and involves minimal disturbance to the colony. A disadvantage is that the calculations associated with estimates of brood area are more arduous, estimates of variability are approximate, and brood estimates may be biased if the data are too few. All calculations can be easily adapted to a programmable calculator or small computer. Linear calibration, an alternative to the use of double sampling, is briefly discussed.

  2. Optical Spectroscopy of Stardust Samples

    NASA Technical Reports Server (NTRS)

    Keller, Lindsay P.

    2006-01-01

    The Stardust spacecraft collected dust samples of the Kuiper belt comet 81P Wild-2 in aerogel and returned them to Earth January 15, 2006. Preliminary examination (PE) of the collected dust includes teams focused on mineralogy, chemical composition, isotopic measurements, organic analysis, cratering and spectroscopic properties. The main PE science goals are to provide an initial characterization of the returned samples with an emphasis on the capture process and its effects on the samples, a comparison of Stardust samples to other meteoritic materials, and the abundance of presolar materials in the Stardust samples. The science objectives of the Spectroscopy team are to obtain spectroscopic data on Stardust particles through infrared (IR), UV/Vis and Raman measurements of particles in aerogel, extracted particles, keystones, and microtome thin sections. These data will be used to answer fundamental science questions about the nature of the samples, but will also serve as preliminary mineralogical data to guide follow-on measurements that will be performed in the other preliminary examination teams. The IR characteristics of Stardust particles are measured to determine: 1) the nature of the indigenous 3.4 micron organic feature, is it detected and can it be differentiated/deconvolved from the contaminated aerogel? How does it compare to features observed in interplanetary dust particles (IDPs) and to astronomical measurements of comets and interstellar dust? 2) the shape and fine structure within the 10 micron silicate feature. Overlap with the strong Si-O stretching vibration from the aerogel complicates this analysis, but we hope to determine if the feature is dominated by amorphous silicates such as those observed in IDPs and comets and whether or not crystalline silicates (e.g. olivine, pyroxene, clays) are present, 3) the presence of secondary (alteration) phases. Deep Impact results suggest that IR observations of Stardust particles should be evaluated for

  3. Sample rotating turntable kit for infrared spectrometers

    DOEpatents

    Eckels, Joel Del; Klunder, Gregory L.

    2008-03-04

    An infrared spectrometer sample rotating turntable kit has a rotatable sample cup containing the sample. The infrared spectrometer has an infrared spectrometer probe for analyzing the sample and the rotatable sample cup is adapted to receive the infrared spectrometer probe. A reflectance standard is located in the rotatable sample cup. A sleeve is positioned proximate the sample cup and adapted to receive the probe. A rotator rotates the rotatable sample cup. A battery is connected to the rotator.

  4. Ground Water Sampling at ISCO Sites - Residual Oxidant Impact on Sample Quality and Sample Preservation Guideline

    EPA Science Inventory

    In-situ chemical oxidation (ISCO) involves the delivery of a chemical oxidant into the subsurface where oxidative reactions transform ground water contaminants into less toxic or harmless byproducts. Due to oxidant persistence, ground water samples collected at hazardous waste si...

  5. 40 CFR 1065.1107 - Sample media and sample system preparation; sample system assembly.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... number of repeat tests. Note that when repeating test cycles to increase sample mass, you may replace the... with methylene chloride for 24 hours and dry over dry nitrogen in a low-temperature vacuum oven. (2... methanol, 22 hours with methylene chloride, and 22 hours with toluene, followed by drying with nitrogen....

  6. Retrieving samples from comet nuclei

    NASA Astrophysics Data System (ADS)

    Stuhlinger, Ernst; Bassner, Helmut; Fechtig, Hugo; Igenbergs, Eduard; Kuczera, Heribert; Loeb, Horst; Schobert, Detlef

    1987-09-01

    A comet nucleus sampling scenario is proposed. Material samples for analysis in earth-based laboratories should be collected continuously to a depth of 3 m below the surface, and at a solar distance of at least 2.5 AU where the comet surface is inactive. The spacecraft is propelled by chemical and electric thrusters. While hovering above the comet nucleus at an altitude of 500 to 1000 m, the spacecraft will dispatch a rotating drill on a tether. The drill pipe will be driven into the nucleus by a rocket-powered reaction wheel. The inner pipe of the drill, when filled with cometary material, will be withdrawn by the tether, stored on the spacecraft, and transported back to Earth.

  7. Environmental surveillance master sampling schedule

    SciTech Connect

    Bisping, L E

    1992-01-01

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest Laboratory (PNL) for the US Department of Energy (DOE). This document contains the planned schedule for routine sample collection for the Surface Environmental Surveillance Project (SESP) and Ground-Water Monitoring Project. Samples for radiological analyses include Air-Particulate Filter, gases and vapor; Water/Columbia River, Onsite Pond, Spring, Irrigation, and Drinking; Foodstuffs/Animal Products including Whole Milk, Poultry and Eggs, and Beef; Foodstuffs/Produce including Leafy Vegetables, Vegetables, and Fruit; Foodstuffs/Farm Products including Wine, Wheat and Alfalfa; Wildlife; Soil; Vegetation; and Sediment. Direct Radiation Measurements include Terrestrial Locations, Columbia River Shoreline Locations, and Onsite Roadway, Railway and Aerial, Radiation Surveys.

  8. Adaptive Sampling in Hierarchical Simulation

    SciTech Connect

    Knap, J; Barton, N R; Hornung, R D; Arsenlis, A; Becker, R; Jefferson, D R

    2007-07-09

    We propose an adaptive sampling methodology for hierarchical multi-scale simulation. The method utilizes a moving kriging interpolation to significantly reduce the number of evaluations of finer-scale response functions to provide essential constitutive information to a coarser-scale simulation model. The underlying interpolation scheme is unstructured and adaptive to handle the transient nature of a simulation. To handle the dynamic construction and searching of a potentially large set of finer-scale response data, we employ a dynamic metric tree database. We study the performance of our adaptive sampling methodology for a two-level multi-scale model involving a coarse-scale finite element simulation and a finer-scale crystal plasticity based constitutive law.

  9. Passive Optical Sample Assembly (POSA)

    NASA Technical Reports Server (NTRS)

    Linton, R. C.; Miller, E. R.; Susko, M.

    1981-01-01

    A Passive Optical Sample Assembly (POSA) unit was mounted and flown in the cargo bay of the space shuttle Columbia during the first Orbital Flight Test (OFT-1). A similar unit was mounted in a different location in the cargo bay during the postflight operations. The samples in both POSA arrays were subjected to a series of optical and analytical measurements prior to delivery for installation in the cargo bay and after retrieval of the flight hardware. The final results of a comparison of the two series of measurements are presented. These STS-1 results are based on data obtained from only a portion of one of the ten Induced Environment Contamination Monitor instruments to be flown on several shuttle flights beginning with STS-2. These limited results do not indicate shuttle contamination levels in excess of those anticipated.

  10. The Ocean Sampling Day Consortium

    DOE PAGES

    Kopf, Anna; Bicak, Mesude; Kottmann, Renzo; ...

    2015-06-19

    In this study, Ocean Sampling Day was initiated by the EU-funded Micro B3 (Marine Microbial Biodiversity, Bioinformatics, Biotechnology) project to obtain a snapshot of the marine microbial biodiversity and function of the world’s oceans. It is a simultaneous global mega-sequencing campaign aiming to generate the largest standardized microbial data set in a single day. This will be achievable only through the coordinated efforts of an Ocean Sampling Day Consortium, supportive partnerships and networks between sites. This commentary outlines the establishment, function and aims of the Consortium and describes our vision for a sustainable study of marine microbial communities and theirmore » embedded functional traits.« less

  11. Replica trick for rare samples

    NASA Astrophysics Data System (ADS)

    Rizzo, Tommaso

    2014-05-01

    In the context of disordered systems with quenched Hamiltonians I address the problem of characterizing rare samples where the thermal average of a specific observable has a value different from the typical one. These rare samples can be selected through a variation of the replica trick which amounts to replicating the system and dividing the replicas intwo two groups containing, respectively, M and -M replicas. Replicas in the first (second) group experience a positive (negative) small field O (1/M) conjugate to the observable considered and the M →∞ limit is to be taken in the end. Applications to the random-field Ising model and to the Sherrington-Kirkpatrick model are discussed.

  12. Organics in APOLLO Lunar Samples

    NASA Technical Reports Server (NTRS)

    Allen, C. C.; Allton, J. H.

    2007-01-01

    One of many unknowns prior to the Apollo landings concerned the possibility of life, its remains, or its organic precursors on the surface of the Moon. While the existence of lunar organisms was considered highly unlikely, a program of biological quarantine and testing for the astronauts, the Apollo Command Modules, and the lunar rock and soil samples, was instituted in the Lunar Receiving Laboratory (LRL). No conclusive evidence of lunar organisms, was detected and the quarantine program was ended after Apollo 14. Analyses for organic compounds were also con-ducted. Considerable effort was expended, during lunar surface operations and in the LRL, to minimize and quantify organic contamination. Post-Apollo curatorial operations and cleaning minimize contamination from particulates, oxygen, and water but no longer specifically address organic contamination. The organic compounds measured in Apollo samples are generally consistent with known sources of contamination.

  13. Apparatus and method for handheld sampling

    DOEpatents

    Staab, Torsten A.

    2005-09-20

    The present invention includes an apparatus, and corresponding method, for taking a sample. The apparatus is built around a frame designed to be held in at least one hand. A sample media is used to secure the sample. A sample media adapter for securing the sample media is operated by a trigger mechanism connectively attached within the frame to the sample media adapter.

  14. Melting a Sample within TEMPUS

    NASA Technical Reports Server (NTRS)

    2003-01-01

    One of the final runs of the TEMPUS experiment shows heating of a sample on STS-94, July 15, 1997, MET:14/11:01 (approximate) and the flows on the surface. At the point this image was taken, the sample was in the process of melting. The surface of the sample is begirning to flow, looking like the motion of plate tectonics on the surface of a planet. During this mission, TEMPUS was able to run than 120 melting cycles with zirconium, with a maximum temperature of 2,000 degrees C, and was able to undercool by 340 degrees -- the highest temperature and largest undercooling ever achieved in space. The TEMPUS investigators also have provided the first measurements of viscosity of palladium-silicon alloys in the undercooled liquid alloy which are not possible on Earth. TEMPUS (stands for Tiegelfreies Elektromagnetisches Prozessiere unter Schwerelosigkeit (containerless electromagnetic processing under weightlessness). It was developed by the German Space Agency (DARA) for flight aboard Spacelab. The DARA project scientist was Igon Egry. The experiment was part of the space research investigations conducted during the Microgravity Science Laboratory-1R mission (STS-94, July 1-17 1997). DARA and NASA are exploring the possibility of flying an advanced version of TEMPUS on the International Space Station.(176KB JPEG, 1350 x 1516 pixels; downlinked video, higher quality not available) The MPG from which this composite was made is available at http://mix.msfc.nasa.gov/ABSTRACTS/MSFC-0300193.html.

  15. Laser comminution of submerged samples

    SciTech Connect

    Mariella, R. Jr.; Rubenchik, A.; Norton, M.; Donohue, G.

    2013-07-07

    With the long-term goal in mind of investigating possible designs for a 'universal, solid-sample comminution technique' for elemental analysis of debris and rubble, we have studied pulsed-laser ablation of solid samples that were submerged in water. Using 351-nm, 15-ns laser pulses with energy between 1 J and 0.35 J, intensities between 500 MW/cm{sup 2} and 30 MW/cm{sup 2}, and samples of broken rock [quartzite] and concrete debris, we have observed conditions in which the laser-driven process can remove material from the solid target substrate, dissolving it and/or converting it into ultrafine particles in a controlled manner. Our study used impure, non-metallic substrates and investigated both the rate of material removal as well as the size distribution of particles that were ablated from the process. We studied ablation at lower regimes of intensity and fluence [below 100 MW/cm{sup 2} and 0.4 J/cm{sup 2}, respectively] than has previously attracted attention and discovered that there appears to be a new regime for energy-efficient material removal [Q* < 4000 J/g, for quartzite and <2000 J/g for concrete] and for the generation of ultrafine particles.

  16. Sample Handling in Extreme Environments

    NASA Technical Reports Server (NTRS)

    Avellar, Louisa; Badescu, Mircea; Sherrit, Stewart; Bar-Cohen, Yoseph

    2013-01-01

    Harsh environments, such as that on Venus, preclude the use of existing equipment for functions that involve interaction with the environment. The operating limitations of current high temperature electronics are well below the actual temperature and pressure found on Venus (460 deg C and 92 atm), so proposed lander configurations typically include a pressure vessel where the science instruments are kept at Earth-like temperature and pressure (25 deg C and 1 atm). The purpose of this project was to develop and demonstrate a method for sample transfer from an external drill to internal science instruments for a lander on Venus. The initial concepts were string and pneumatically driven systems; and the latter system was selected for its ability to deliver samples at very high speed. The pneumatic system was conceived to be driven by the pressure difference between the Venusian atmosphere and the inside of the lander. The pneumatic transfer of a small capsule was demonstrated, and velocity data was collected from the lab experiment. The sample transfer system was modeled using CAD software and prototyped using 3D printing. General structural and thermal analyses were performed to approximate the proposed system's mass and effects on the temperature and pressure inside of the lander. Additionally, a sampler breadboard for use on Titan was tested and functionality problems were resolved.

  17. Remanent magnetization of lunar samples.

    NASA Technical Reports Server (NTRS)

    Strangway, D. W.; Pearce, G. W.; Gose, W. A.; Timme, R. W.

    1971-01-01

    The remanent magnetization of samples returned from the moon by the Apollo 11 and 12 missions consists, in most cases, of two distinct components. An unstable component is readily removed upon alternating field (AF) demagnetization in fields less than 100 Oe and is considered to be an isothermal remanence acquired during or after return to earth. The second component is unaltered by demagnetization in fields up to 400 Oe. It is probably a thermoremanent magnetization due to cooling from above 800 C in the presence of a field of a few thousand gammas. Chips from individual rocks have the same direction of magnetization after demagnetization, while the directions of different samples are random. This again demonstrates the high stability. Our data imply that the moon experienced a magnetic field that lasted at least from about 3.0 to 3.8 b.y., which is the age of Apollo 11 and 12 samples. One explanation of the origin of this field is that the moon had a liquid core and a self-exciting dynamo early in its history.

  18. Synchronized sampling improves fault location

    SciTech Connect

    Kezunovic, M.; Perunicic, B.

    1995-04-01

    Transmission line faults must be located accurately to allow maintenance crews to arrive at the scene and repair the faulted section as soon as possible. Rugged terrain and geographical layout cause some sections of power transmission lines to be difficult to reach. In the past, a variety of fault location algorithms were introduced as either an add-on feature in protective relays or stand-alone implementation in fault locators. In both cases, the measurements of current and voltages were taken at one terminal of a transmission line only. Under such conditions, it may become difficult to determine the fault location accurately, since data from other transmission line ends are required for more precise computations. In the absence of data from the other end, existing algorithms have accuracy problems under several circumstances, such as varying switching and loading conditions, fault infeed from the other end, and random value of fault resistance. Most of the one-end algorithms were based on estimation of voltage and current phasors. The need to estimate phasors introduces additional difficulty in high-speed tripping situations where the algorithms may not be fast enough in determining fault location accurately before the current signals disappear due to the relay operation and breaker opening. This article introduces a unique concept of high-speed fault location that can be implemented either as a simple add-on to the digital fault recorders (DFRs) or as a stand-alone new relaying function. This advanced concept is based on the use of voltage and current samples that are synchronously taken at both ends of a transmission line. This sampling technique can be made readily available in some new DFR designs incorporating receivers for accurate sampling clock synchronization using the satellite Global Positioning System (GPS).

  19. Nuclear tracks in lunar samples

    NASA Technical Reports Server (NTRS)

    Price, P. B.

    1971-01-01

    An attempt is made to relate the appearance of an etched tract to the atomic number and velocity of the ion that left it using 10 MeV/nucleon Kr beams and 6 MeV/nucleon Zn beams. It was found that the etching rate along a tract in minerals and glass is a monototonic function of ionization rate thus, making particle identification possible. Results show the following were present in lunar samples: superheavy elements, cosmic rays with z greater than 26, and solar flare particles in Surveyor glass.

  20. Magnetic studies of lunar samples

    USGS Publications Warehouse

    Doell, Richard R.; Gromme, S.C.; Thorpe, A.N.; Senftle, F.E.

    1970-01-01

    The remanent magnetism of a lunar type C breccia sample includes a large viscous component with a time constant of several hours, and a high coercivity remanence, possibly acquired by impact processes on the lunar surface. Ilmenite(?) and metallic iron in breccias, and ferrous and metallic iron in glass beads separated from lunar fines (type D) were identified by high-field and low-temperature experiments. The iron appears to occur in a wide range of grain sizes including the single domain and multidomain states.

  1. Mars 2005 Sample Return Workshop

    NASA Technical Reports Server (NTRS)

    Gulick, V. C. (Editor)

    1997-01-01

    Convened at the request of Dr. Jurgen Rahe of the NASA Office of Space Science, the purpose of this workshop was to reexamine the science issues that will determine how an optimum sample return mission would be carried out in 2005 given the new context that has emerged for Mars exploration since the last such workshop was held (in 1987). The results and summary of discussion that took place at the meeting are contained in this volume. The community was invited to participate in the preparation of the final written report by browsing through the agenda and reading the text and viewgraphs provided by workshop participants and submitting comments for that section.

  2. Posterior sampling with improved efficiency

    SciTech Connect

    Hanson, K.M.; Cunningham, G.S.

    1998-12-01

    The Markov Chain Monte Carlo (MCMC) technique provides a means to generate a random sequence of model realizations that sample the posterior probability distribution of a Bayesian analysis. That sequence may be used to make inferences about the model uncertainties that derive from measurement uncertainties. This paper presents an approach to improving the efficiency of the Metropolis approach to MCMC by incorporating an approximation to the covariance matrix of the posterior distribution. The covariance matrix is approximated using the update formula from the BFGS quasi-Newton optimization algorithm. Examples are given for uncorrelated and correlated multidimensional Gaussian posterior distributions.

  3. Automatic diluter for bacteriological samples.

    PubMed Central

    Trinel, P A; Bleuze, P; Leroy, G; Moschetto, Y; Leclerc, H

    1983-01-01

    The described apparatus, carrying 190 tubes, allows automatic and aseptic dilution of liquid or suspended-solid samples. Serial 10-fold dilutions are programmable from 10(-1) to 10(-9) and are carried out in glass tubes with screw caps and split silicone septa. Dilution assays performed with strains of Escherichia coli and Bacillus stearothermophilus permitted efficient conditions for sterilization of the needle to be defined and showed that the automatic dilutions were as accurate and as reproducible as the most rigorous conventional dilutions. Images PMID:6338826

  4. Cold SQUIDs and hot samples

    SciTech Connect

    Lee, T.S.C. |

    1997-05-01

    Low transition temperature (low-{Tc}) and high-{Tc} Superconducting QUantum Interference Devices (SQUIDs) have been used to perform high-resolution magnetic measurements on samples whose temperatures are much higher than the operating temperatures of the devices. Part 1 of this work focuses on measurements of the rigidity of flux vortices in high-{Tc} superconductors using two low-{Tc} SQUIDs, one on either side of a thermally-insulated sample. The correlation between the signals of the SQUIDs is a direct measure of the extent of correlation between the movements of opposite ends of vortices. These measurements were conducted under the previously-unexplored experimental conditions of nominally-zero applied magnetic field, such that vortex-vortex interactions were unimportant, and with zero external current. At specific temperatures, the authors observed highly-correlated noise sources, suggesting that the vortices moved as rigid rods. At other temperatures, the noise was mostly uncorrelated, suggesting that the relevant vortices were pinned at more than one point along their length. Part 2 describes the design, construction, performance, and applications of a scanning high-{Tc} SQUID microscope optimized for imaging room-temperature objects with very high spatial resolution and magnetic source sensitivity.

  5. TRU waste-sampling program

    SciTech Connect

    Warren, J.L.; Zerwekh, A.

    1985-08-01

    As part of a TRU waste-sampling program, Los Alamos National Laboratory retrieved and examined 44 drums of /sup 238/Pu- and /sup 239/Pu-contaminated waste. The drums ranged in age from 8 months to 9 years. The majority of drums were tested for pressure, and gas samples withdrawn from the drums were analyzed by a mass spectrometer. Real-time radiography and visual examination were used to determine both void volumes and waste content. Drum walls were measured for deterioration, and selected drum contents were reassayed for comparison with original assays and WIPP criteria. Each drum tested at atmospheric pressure. Mass spectrometry revealed no problem with /sup 239/Pu-contaminated waste, but three 8-month-old drums of /sup 238/Pu-contaminated waste contained a potentially hazardous gas mixture. Void volumes fell within the 81 to 97% range. Measurements of drum walls showed no significant corrosion or deterioration. All reassayed contents were within WIPP waste acceptance criteria. Five of the drums opened and examined (15%) could not be certified as packaged. Three contained free liquids, one had corrosive materials, and one had too much unstabilized particulate. Eleven drums had the wrong (or not the most appropriate) waste code. In many cases, disposal volumes had been inefficiently used. 2 refs., 23 figs., 7 tabs.

  6. Restricted sample variance reduces generalizability.

    PubMed

    Lakes, Kimberley D

    2013-06-01

    One factor that affects the reliability of observed scores is restriction of range on the construct measured for a particular group of study participants. This study illustrates how researchers can use generalizability theory to evaluate the impact of restriction of range in particular sample characteristics on the generalizability of test scores and to estimate how changes in measurement design could improve the generalizability of the test scores. An observer-rated measure of child self-regulation (Response to Challenge Scale; Lakes, 2011) is used to examine scores for 198 children (Grades K through 5) within the generalizability theory (GT) framework. The generalizability of ratings within relatively developmentally homogeneous samples is examined and illustrates the effect of reduced variance among ratees on generalizability. Forecasts for g coefficients of various D study designs demonstrate how higher generalizability could be achieved by increasing the number of raters or items. In summary, the research presented illustrates the importance of and procedures for evaluating the generalizability of a set of scores in a particular research context.

  7. NASA's Aerosol Sampling Experiment Summary

    NASA Technical Reports Server (NTRS)

    Meyer, Marit E.

    2016-01-01

    In a spacecraft cabin environment, the size range of indoor aerosols is much larger and they persist longer than on Earth because they are not removed by gravitational settling. A previous aerosol experiment in 1991 documented that over 90 of the mass concentration of particles in the NASA Space Shuttle air were between 10 m and 100 m based on measurements with a multi-stage virtual impactor and a nephelometer (Liu et al. 1991). While the now-retired Space Shuttle had short duration missions (less than two weeks), the International Space Station (ISS) has been continually inhabited by astronauts for over a decade. High concentrations of inhalable particles on ISS are potentially responsible for crew complaints of respiratory and eye irritation and comments about 'dusty' air. Air filtration is the current control strategy for airborne particles on the ISS, and filtration modeling, performed for engineering and design validation of the air revitalization system in ISS, predicted that PM requirements would be met. However, aerosol monitoring has never been performed on the ISS to verify PM levels. A flight experiment is in preparation which will provide data on particulate matter in ISS ambient air. Particles will be collected with a thermophoretic sampler as well as with passive samplers which will extend the particle size range of sampling. Samples will be returned to Earth for chemical and microscopic analyses, providing the first aerosol data for ISS ambient air.

  8. Sampling and monitoring for closure

    USGS Publications Warehouse

    McLemore, V.T.; Russell, C.C.; Smith, K.S.

    2004-01-01

    The Metals Mining Sector of the Acid Drainage Technology Initiative (ADTI-MMS) addresses technical drainage-quality issues related to metal mining and related metallurgical operations, for future and active mines, as well as, for historical mines and mining districts. One of the first projects of ADTI-MMS is to develop a handbook describing the best sampling, monitoring, predicting, mitigating, and modeling of drainage from metal mines, pit lakes and related metallurgical facilities based upon current scientific and engineering practices. One of the important aspects of planning a new mine in today's regulatory environment is the philosophy of designing a new or existing mine or expansion of operations for ultimate closure. The holistic philosophy taken in the ADTI-MMS handbook maintains that sampling and monitoring programs should be designed to take into account all aspects of the mine-life cycle. Data required for the closure of the operation are obtained throughout the mine-life cycle, from exploration through post-closure.

  9. Biobanking and international interoperability: samples.

    PubMed

    Kiehntopf, Michael; Krawczak, Michael

    2011-09-01

    In terms of sample exchange, international collaborations between biobanks, or between biobanks and their research partners, have two important aspects. First, the donors' consent usually implies that the scope and purpose of any sample transfer to third parties is subject to major constraints. Since the legal, ethical and political framework of biobanking may differ substantially, even between countries of comparable jurisdictional systems, general rules for the international sharing of biomaterial are difficult, if not impossible, to define. Issues of uncertainty include the right to transfer the material, the scope of research allowed, and intellectual property rights. Since suitable means of international law enforcement may not be available in the context of biobanking, collaborators are advised to clarify any residual uncertainty by means of bilateral contracts, for example, in the form of material transfer agreements. Second, biobank partners may rightly expect that the biomaterial they receive for further analysis attains a certain level of quality. This implies that a biobank has to implement stringent quality control measures covering, in addition to the material transfer itself, the whole process of material acquisition, transport, pre-analytical handling and storage. Again, it may be advisable for biobank partners to claim contractual warranties for the type and quality of the biomaterial they wish to acquire.

  10. Sampled-data controller implementation

    NASA Astrophysics Data System (ADS)

    Wang, Yu; Leduc, Ryan J.

    2012-09-01

    The setting of this article is the implementation of timed discrete-event systems (TDES) as sampled-data (SD) controllers. An SD controller is driven by a periodic clock and sees the system as a series of inputs and outputs. On each clock edge (tick event), it samples its inputs, changes states and updates its outputs. In this article, we establish a formal representation of an SD controller as a Moore synchronous finite state machine (FSM). We describe how to translate a TDES supervisor to an FSM, as well as necessary properties to be able to do so. We discuss how to construct a single centralised controller as well as a set of modular controllers, and show that they will produce equivalent output. We briefly discuss how the recently introduced SD controllability definition relates to our translation method. SD controllability is an extension of TDES controllability which captures several new properties that are useful in dealing with concurrency issues, as well as make it easier to translate a TDES supervisor into an SD controller. We next discuss the application of SD controllability to a small flexible manufacturing system (FMS) from the literature. The example demonstrates the successful application of the new SD properties. We describe the design of the system in detail to illustrate the new conditions and to provide designers with guidance on how to apply the properties. We also present some FSM translation issues encountered, as well as the FSM version of the system's supervisors.

  11. Public health assessment for Nyanza Chemical Waste Dump, Ashland, Middlesex County, Massachusetts, Region 1. Cerclis No. MAD990685422. Final report

    SciTech Connect

    Not Available

    1994-06-29

    The Nyanza site is located in Ashland, Massachusetts, approximately 22 miles west of Boston. More than 100 different chemicals (mainly dyes, but additionally a number of semi-volatiles including benzidine, dianisidine, o-tolidine, and 2-napthylamine) have been detected at the site, which encompasses a 35-acre area. Liquid wastes from Nyanza have been discharged into the environment in several different ways including into the underground vault, unlined lagoons, and nearby brooks and wetlands. Surface water and soil on-site are known to have been contaminated. Groundwater beneath and downgradient of the site is known to be contaminated. Releases into the ambient air are known to have occurred historically. These releases have included oleum, bromine, and nitric acid. Opportunity for human exposure in the past was high and included exposures to children playing in the soils and lagoons on-site as well as in the Chemical Brook.

  12. 78 FR 14300 - Proposed CERCLA Settlement Relating to the 1244 White Drive Site in North Brunswick, Middlesex...

    Federal Register 2010, 2011, 2012, 2013, 2014

    2013-03-05

    ... Agreement, the Settling Parties will pay EPA 10% ($42,978.35) of the total leaving a balance of $386,805.19... properties until the balance of $386,805.19 is paid in full. In the event that any balance remains due after the sale of the seven properties the remaining balance will be paid out of the Settling...

  13. 75 FR 42814 - Boston & Maine Corporation―Abandonment Exemption―in Essex, Middlesex, and Suffolk Counties, MA

    Federal Register 2010, 2011, 2012, 2013, 2014

    2010-07-22

    ... years; (2) there is no overhead traffic on the line; (3) no formal complaint filed by a user of rail service on the line (or by a State or local government entity acting on behalf of such user) regarding...) must be filed. Provided no formal expression of intent to file an offer of financial assistance...

  14. Offline solid phase microextraction sampling system

    DOEpatents

    Harvey, Chris A.

    2008-12-16

    An offline solid phase microextraction (SPME) sampling apparatus for enabling SPME samples to be taken a number of times from a previously collected fluid sample (e.g. sample atmosphere) stored in a fused silica lined bottle which keeps volatile organics in the fluid sample stable for weeks at a time. The offline SPME sampling apparatus has a hollow body surrounding a sampling chamber, with multiple ports through which a portion of a previously collected fluid sample may be (a) released into the sampling chamber, (b) SPME sampled to collect analytes for subsequent GC analysis, and (c) flushed/purged using a fluidically connected vacuum source and purging fluid source to prepare the sampling chamber for additional SPME samplings of the same original fluid sample, such as may have been collected in situ from a headspace.

  15. Methodology Series Module 5: Sampling Strategies.

    PubMed

    Setia, Maninder Singh

    2016-01-01

    Once the research question and the research design have been finalised, it is important to select the appropriate sample for the study. The method by which the researcher selects the sample is the ' Sampling Method'. There are essentially two types of sampling methods: 1) probability sampling - based on chance events (such as random numbers, flipping a coin etc.); and 2) non-probability sampling - based on researcher's choice, population that accessible & available. Some of the non-probability sampling methods are: purposive sampling, convenience sampling, or quota sampling. Random sampling method (such as simple random sample or stratified random sample) is a form of probability sampling. It is important to understand the different sampling methods used in clinical studies and mention this method clearly in the manuscript. The researcher should not misrepresent the sampling method in the manuscript (such as using the term ' random sample' when the researcher has used convenience sample). The sampling method will depend on the research question. For instance, the researcher may want to understand an issue in greater detail for one particular population rather than worry about the ' generalizability' of these results. In such a scenario, the researcher may want to use ' purposive sampling' for the study.

  16. Micro-organism distribution sampling for bioassays

    NASA Technical Reports Server (NTRS)

    Nelson, B. A.

    1975-01-01

    Purpose of sampling distribution is to characterize sample-to-sample variation so statistical tests may be applied, to estimate error due to sampling (confidence limits) and to evaluate observed differences between samples. Distribution could be used for bioassays taken in hospitals, breweries, food-processing plants, and pharmaceutical plants.

  17. Sampling for area estimation: A comparison of full-frame sampling with the sample segment approach. [Kansas

    NASA Technical Reports Server (NTRS)

    Hixson, M. M.; Bauer, M. E.; Davis, B. J.

    1979-01-01

    The effect of sampling on the accuracy (precision and bias) of crop area estimates made from classifications of LANDSAT MSS data was investigated. Full-frame classifications of wheat and non-wheat for eighty counties in Kansas were repetitively sampled to simulate alternative sampling plants. Four sampling schemes involving different numbers of samples and different size sampling units were evaluated. The precision of the wheat area estimates increased as the segment size decreased and the number of segments was increased. Although the average bias associated with the various sampling schemes was not significantly different, the maximum absolute bias was directly related to sampling unit size.

  18. Sampling of respirable isocyanate particles.

    PubMed

    Gylestam, Daniel; Gustavsson, Marcus; Karlsson, Daniel; Dalene, Marianne; Skarping, Gunnar

    2014-04-01

    An advanced design of a denuder impactor (DI) sampler has been developed for characterization of possible airborne isocyanate exposure in different particle size fractions. The sampler is equipped with 12 different parallel denuder tubes, 4 impaction stages with the cut-off values (d50) of: 9.5, 4, 2.5 and 1 µm, and an end filter that collects particles < 1 µm. All collecting parts were impregnated with di-n-butylamine DBA as the reagent in a mixture with acetic acid. The performance of the DI sampler was studied on a standard atmosphere containing gas and particulate isocyanates. The isocyanate atmosphere was generated by liquid permeation of 2,4-, 2,6-Toluene Diisocyanate (TDI), 1,6-Hexamethylene Diisocyanate (HDI) and Isophorone Diisocyanate (IPDI). 4,4'-Methylene Diphenyl Diisocyanate (MDI) particles were generated by heating of technical MDI and condensing the mixture of gas and particle-borne MDI in an atmosphere containing mixed salt particles. The study was performed in a 0.85 m3 environmental chamber with stainless steel walls. With the advancement of the DI sampler it is now possible to collect isocyanate particle samples for up to 320 min. The performance of the DI sampler is essentially unaffected by the humidity. The DI sampler and the ASSET EZ4-NCO sampler (Sigma-Aldrich/Supelco, Bellefonte, PA, USA) gave similar results. Sample losses within the DI sampler are low. In the environmental chamber it was observed that the particle distribution may be affected by the humidity and ageing. A scanning mobility particle sizer (SMPS) was used to separate a flow of selected fractions containing MDI particles from mixed MDI and salt particles. The particle-size distribution had a maximum at about 300 nm, but later in the environmental chamber 1 µm dominated. The distribution was very different as compared to with only NaCl or MDI present. The biological relevance for studying isocyanate nano particles is significant as these have the possibility to reach the

  19. Heuristic-biased stochastic sampling

    SciTech Connect

    Bresina, J.L.

    1996-12-31

    This paper presents a search technique for scheduling problems, called Heuristic-Biased Stochastic Sampling (HBSS). The underlying assumption behind the HBSS approach is that strictly adhering to a search heuristic often does not yield the best solution and, therefore, exploration off the heuristic path can prove fruitful. Within the HBSS approach, the balance between heuristic adherence and exploration can be controlled according to the confidence one has in the heuristic. By varying this balance, encoded as a bias function, the HBSS approach encompasses a family of search algorithms of which greedy search and completely random search are extreme members. We present empirical results from an application of HBSS to the realworld problem of observation scheduling. These results show that with the proper bias function, it can be easy to outperform greedy search.

  20. Sampling and handling of desert soils

    NASA Technical Reports Server (NTRS)

    Blank, G. B.; Cameron, R. E.

    1969-01-01

    Report on sampling and handling desert soils includes sections on selection, characterization, and photography of area, site, and soil, sterilization of sampling equipment and containers, and soil sample collection, transport, storage, and dispersal.

  1. Hanford Site Environmental Surveillance Master Sampling Schedule

    SciTech Connect

    Bisping, Lynn E.

    2000-01-27

    This document contains the CY2000 schedules for the routine collection of samples for the Surface Environmental Surveillance Project (SESP) and Drinking Water Monitoring Project. Each section includes sampling locations, sample types, and analyses to be performed.

  2. 77 FR 37471 - National Automotive Sampling System

    Federal Register 2010, 2011, 2012, 2013, 2014

    2012-06-21

    ... National Highway Traffic Safety Administration National Automotive Sampling System AGENCY: National Highway... comments. SUMMARY: The NHTSA is conducting a comprehensive review of the National Automotive Sampling... undertaking a modernization effort to upgrade the National Automotive Sampling System (NASS) by improving...

  3. Hanford analytical sample projections 1996 - 2000

    SciTech Connect

    Joyce, S.M.

    1996-02-02

    Sample projections are compiled for the Hanford site based on inputs from the major programs for the years 1996 through 2000. Sample projections are categorized by radiation level, protocol, sample matrix and Program. Analyses requirements are also presented.

  4. Methodology Series Module 5: Sampling Strategies

    PubMed Central

    Setia, Maninder Singh

    2016-01-01

    Once the research question and the research design have been finalised, it is important to select the appropriate sample for the study. The method by which the researcher selects the sample is the ‘ Sampling Method’. There are essentially two types of sampling methods: 1) probability sampling – based on chance events (such as random numbers, flipping a coin etc.); and 2) non-probability sampling – based on researcher's choice, population that accessible & available. Some of the non-probability sampling methods are: purposive sampling, convenience sampling, or quota sampling. Random sampling method (such as simple random sample or stratified random sample) is a form of probability sampling. It is important to understand the different sampling methods used in clinical studies and mention this method clearly in the manuscript. The researcher should not misrepresent the sampling method in the manuscript (such as using the term ‘ random sample’ when the researcher has used convenience sample). The sampling method will depend on the research question. For instance, the researcher may want to understand an issue in greater detail for one particular population rather than worry about the ‘ generalizability’ of these results. In such a scenario, the researcher may want to use ‘ purposive sampling’ for the study. PMID:27688438

  5. Physical sampling for site and waste characterization

    SciTech Connect

    Bonnough, T.L.

    1996-08-01

    Physical sampling plays a basic role in high-level radioactive waste management program effort. The term ``physical sampling`` used here means collecting tangible, physical samples of soil, water, air, waste streams, or other materials. The industry defines the term ``physical sampling`` broadly to include measurements of physical conditions such as temperature, wind conditions, and pH, which are also often taken in a sample collection effort. Most environmental compliance actions are supported by the results of taking, recording, and analyzing physical samples and the measurements of physical conditions taken in association with sample collecting. Therefore, the when and how to take samples is needed to be known and planned.

  6. [Sampling and conveyance of mail testing].

    PubMed

    Higashino, Kouji

    2005-12-01

    In mail testing, a testee collects samples at home from his or her own body, and mails them to the medical institution. Because the testee does not need to attend the medical institution, an advantage of mail testing is that it is not time-consuming. Because the amount of sample is small and time from sampling to measurement is long, the manner of collecting and transporting samples are important factors affecting the precision of the result. There is the risk that inappropriate sample picking can occur, as the testee, who is not skilled in medical testing, may obtain the sample. Moreover, the samples may include blood, urine, secretions, and so on. Depending on the purpose of the test, the transport and sampling method varies, and the character of the sampling device and transport method influence the procedure required. I describe collection methods and other issues in this paper according to medical examination item, sample, and sampling.

  7. Apparatus for sectioning demountable semiconductor samples

    DOEpatents

    Sopori, Bhushan L.; Wolf, Abraham

    1984-01-01

    Apparatus for use during polishing and sectioning operations of a ribbon sample is described. The sample holder includes a cylinder having an axially extending sample cavity terminated in a first funnel-shaped opening and a second slot-like opening. A spring-loaded pressure plunger is located adjacent the second opening of the sample cavity for frictional engagement of the sample prior to introduction of a molding medium in the sample cavity. A heat softenable molding medium is inserted in the funnel-shaped opening, to surround the sample. After polishing, the heater is energized to allow draining of the molding medium from the sample cavity. During manual polishing, the second end of the sample holder is inserted in a support ring which provides mechanical support as well as alignment of the sample holder during polishing. A gauge block for measuring the protrusion of a sample beyond the second wall of the holder is also disclosed.

  8. Bilateral inferior petrosal sinus sampling.

    PubMed

    Zampetti, Benedetta; Grossrubatscher, Erika; Dalino Ciaramella, Paolo; Boccardi, Edoardo; Loli, Paola

    2016-07-01

    Simultaneous bilateral inferior petrosal sinus sampling (BIPSS) plays a crucial role in the diagnostic work-up of Cushing's syndrome. It is the most accurate procedure in the differential diagnosis of hypercortisolism of pituitary or ectopic origin, as compared with clinical, biochemical and imaging analyses, with a sensitivity and specificity of 88-100% and 67-100%, respectively. In the setting of hypercortisolemia, ACTH levels obtained from venous drainage of the pituitary are expected to be higher than the levels of peripheral blood, thus suggesting pituitary ACTH excess as the cause of hypercortisolism. Direct stimulation of the pituitary corticotroph with corticotrophin-releasing hormone enhances the sensitivity of the procedure. The procedure must be undertaken in the presence of hypercortisolemia, which suppresses both the basal and stimulated secretory activity of normal corticotrophic cells: ACTH measured in the sinus is, therefore, the result of the secretory activity of the tumor tissue. The poor accuracy in lateralization of BIPSS (positive predictive value of 50-70%) makes interpetrosal ACTH gradient alone not sufficient for the localization of the tumor. An accurate exploration of the gland is recommended if a tumor is not found in the predicted area. Despite the fact that BIPSS is an invasive procedure, the occurrence of adverse events is extremely rare, particularly if it is performed by experienced operators in referral centres.

  9. Bilateral inferior petrosal sinus sampling

    PubMed Central

    Grossrubatscher, Erika; Dalino Ciaramella, Paolo; Boccardi, Edoardo

    2016-01-01

    Simultaneous bilateral inferior petrosal sinus sampling (BIPSS) plays a crucial role in the diagnostic work-up of Cushing’s syndrome. It is the most accurate procedure in the differential diagnosis of hypercortisolism of pituitary or ectopic origin, as compared with clinical, biochemical and imaging analyses, with a sensitivity and specificity of 88–100% and 67–100%, respectively. In the setting of hypercortisolemia, ACTH levels obtained from venous drainage of the pituitary are expected to be higher than the levels of peripheral blood, thus suggesting pituitary ACTH excess as the cause of hypercortisolism. Direct stimulation of the pituitary corticotroph with corticotrophin-releasing hormone enhances the sensitivity of the procedure. The procedure must be undertaken in the presence of hypercortisolemia, which suppresses both the basal and stimulated secretory activity of normal corticotrophic cells: ACTH measured in the sinus is, therefore, the result of the secretory activity of the tumor tissue. The poor accuracy in lateralization of BIPSS (positive predictive value of 50–70%) makes interpetrosal ACTH gradient alone not sufficient for the localization of the tumor. An accurate exploration of the gland is recommended if a tumor is not found in the predicted area. Despite the fact that BIPSS is an invasive procedure, the occurrence of adverse events is extremely rare, particularly if it is performed by experienced operators in referral centres. PMID:27352844

  10. Sample concentration using optical chromatography

    NASA Astrophysics Data System (ADS)

    Hart, Sean J.; Terray, Alex; Arnold, Jonathan; Leski, Tomasz A.

    2007-03-01

    Optical chromatography is a technique for the separation of particles that capitalizes on the balance between optic and fluidic forces. When microscopic particles in a fluid flow encounter a laser beam propagating in the opposite direction, they are trapped axially along the beam. They are then optically pushed upstream from the laser focal point to rest at a point where the optic and fluidic forces on the particle balance. Because optical and fluid forces are sensitive to differences in the physical and chemical properties of a particle, both coarse and fine separations are possible. We describe how an optical chromatography beam directed into a tailored flow environment, has been adapted to operate as an optical filter for the concentration / bioenrichment of colloidal and biological samples. In this work, the demonstrated ability to concentrate spores of the biowarfare agent, Bacillus anthracis, may have significant impact in the biodefense arena. Application of these techniques and further design of fluidic and optical environments will allow for more specific identification, concentration and separation of many more microscopic particle and biological suspensions.

  11. Mars sample return power supply

    NASA Technical Reports Server (NTRS)

    Hoang, Don; Ludwigs, Sharon; Schmitz, Paul; Wright, John

    1988-01-01

    A power supply is designed for a vehicle able to operate on the surface of Mars for a period of 5 to 10 years. This vehicle will be used for sample and data collection. The design is based on the assumption that the vehicle will be unmanned. Also, there will be no means by which components could be repaired or replaced while on the Martian surface. A consequence of this is that all equipment must meet high standards of reliability and, if possible, redundancy. Power will be supplied to the vehicle by means of a General Purpose Heat Source capable of producing a minimum of 7 kW of thermal power. The heat generated from the General Purpose Heat Source will be transferred to a Stirling engine via hot side heat pipes. The Stirling engine will then convert this heat into 2 kW of electrical power. Cold side heat pipes will be used to carry away waste heat, which will be released to the Martian environment via radiators connected to the end of the cold side heat pipes.

  12. Mars sample return power supply

    NASA Astrophysics Data System (ADS)

    Hoang, Don; Ludwigs, Sharon; Schmitz, Paul; Wright, John

    A power supply is designed for a vehicle able to operate on the surface of Mars for a period of 5 to 10 years. This vehicle will be used for sample and data collection. The design is based on the assumption that the vehicle will be unmanned. Also, there will be no means by which components could be repaired or replaced while on the Martian surface. A consequence of this is that all equipment must meet high standards of reliability and, if possible, redundancy. Power will be supplied to the vehicle by means of a General Purpose Heat Source capable of producing a minimum of 7 kW of thermal power. The heat generated from the General Purpose Heat Source will be transferred to a Stirling engine via hot side heat pipes. The Stirling engine will then convert this heat into 2 kW of electrical power. Cold side heat pipes will be used to carry away waste heat, which will be released to the Martian environment via radiators connected to the end of the cold side heat pipes.

  13. Electrphoretic Sample Excitation Light Assembly.

    SciTech Connect

    Li, Qingbo; Liu, Changsheng

    2002-04-02

    An automated electrophoretic system is disclosed. The system employs a capillary cartridge having a plurality of capillary tubes. The cartridge has a first array of capillary ends projecting from one side of a plate. The first array of capillary ends are spaced apart in substantially the same manner as the wells of a microtitre tray of standard size. This allows one to simultaneously perform capillary electrophoresis on samples present in each of the wells of the tray. The system includes a stacked, dual carrousel arrangement to eliminate cross-contamination resulting from reuse of the same buffer tray on consecutive executions from electrophoresis. The system also has a gel delivery module containing a gel syringe/a stepper motor or a high pressure chamber with a pump to quickly and uniformly deliver gel through the capillary tubes. The system further includes a multi-wavelength beam generator to generate a laser beam which produces a beam with a wide range of wavelengths. An off-line capillary reconditioner thoroughly cleans a capillary cartridge to enable simultaneous execution of electrophoresis with another capillary cartridge. The streamlined nature of the off-line capillary reconditioner offers the advantage of increased system throughput with a minimal increase in system cost.

  14. 40 CFR 761.323 - Sample preparation.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 761.323 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) TOXIC SUBSTANCES CONTROL... Remediation Waste Samples § 761.323 Sample preparation. (a) The comparison study requires analysis of a minimum of 10 samples weighing at least 300 grams each. Samples of PCB remediation waste used in...

  15. A Primer on Sampling for Statewide Assessment.

    ERIC Educational Resources Information Center

    Jaeger, Richard M.

    This paper is a primer on sampling procedures for statewide assessment. The careful reader should gain substantial knowledge about the promises and pitfalls of sampling for assessment. The primer has three basic objectives: (1) to define terms and concepts basic to sampling theory and its application, including population, sampling unit, sampling…

  16. 42 CFR 402.109 - Statistical sampling.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 42 Public Health 2 2011-10-01 2011-10-01 false Statistical sampling. 402.109 Section 402.109... Statistical sampling. (a) Purpose. CMS or OIG may introduce the results of a statistical sampling study to... or caused to be presented. (b) Prima facie evidence. The results of the statistical sampling...

  17. 42 CFR 402.109 - Statistical sampling.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 42 Public Health 2 2013-10-01 2013-10-01 false Statistical sampling. 402.109 Section 402.109... Statistical sampling. (a) Purpose. CMS or OIG may introduce the results of a statistical sampling study to... or caused to be presented. (b) Prima facie evidence. The results of the statistical sampling...

  18. 42 CFR 402.109 - Statistical sampling.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 42 Public Health 2 2014-10-01 2014-10-01 false Statistical sampling. 402.109 Section 402.109... Statistical sampling. (a) Purpose. CMS or OIG may introduce the results of a statistical sampling study to... or caused to be presented. (b) Prima facie evidence. The results of the statistical sampling...

  19. 42 CFR 402.109 - Statistical sampling.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 42 Public Health 2 2012-10-01 2012-10-01 false Statistical sampling. 402.109 Section 402.109... Statistical sampling. (a) Purpose. CMS or OIG may introduce the results of a statistical sampling study to... or caused to be presented. (b) Prima facie evidence. The results of the statistical sampling...

  20. Fluid sample collection and storage device

    NASA Technical Reports Server (NTRS)

    Cohen, D.; Stone, S. E.

    1969-01-01

    Fluid sampling device collects a sample from a low-pressure fluid system and stores it for an indefinite period, with little risk of contamination of either the sample or the surrounding environment. The collector /a plastic bladder/ is separated from the sampler after a sample is collected.

  1. Modification to Tracerlab Automatic Sample Changer

    USGS Publications Warehouse

    Flanegan, F.J.; Nelson, J.M.; Warr, J.J.

    1950-01-01

    The U.S. Geological Survey has recently modified the Tracerlab Automatic Sample Changer so that the geometry is greatly improved for counting larger low-activity samples in finely ground form. The larger sample and larger Geiger Mueller tubes allow a greater number of samples to be counted per hour with the same statistical accuracy.

  2. Tank 12H residuals sample analysis report

    SciTech Connect

    Oji, L. N.; Shine, E. P.; Diprete, D. P.; Coleman, C. J.; Hay, M. S.

    2015-06-11

    The Savannah River National Laboratory (SRNL) was requested by Savannah River Remediation (SRR) to provide sample preparation and analysis of the Tank 12H final characterization samples to determine the residual tank inventory prior to grouting. Eleven Tank 12H floor and mound residual material samples and three cooling coil scrape samples were collected and delivered to SRNL between May and August of 2014.

  3. Computer Graphics Simulations of Sampling Distributions.

    ERIC Educational Resources Information Center

    Gordon, Florence S.; Gordon, Sheldon P.

    1989-01-01

    Describes the use of computer graphics simulations to enhance student understanding of sampling distributions that arise in introductory statistics. Highlights include the distribution of sample proportions, the distribution of the difference of sample means, the distribution of the difference of sample proportions, and the distribution of sample…

  4. Physical sampling for site and waste characterization

    SciTech Connect

    Bonnough, T.L.

    1994-06-01

    Physical sampling plays a basic role in site and waste characterization program effort. The term ``physical sampling`` used here means collecting tangible, physical samples of soil, water, air, waste streams, or other materials. The industry defines the term ``physical sampling`` broadly to include measurements of physical conditions such as temperature, wind conditions, and pH which are also often taken in a sample collection effort. Most environmental compliance actions are supported by the results of taking, recording, and analyzing physical samples and the measuring of physical conditions taken in association with sample collecting.

  5. Stability of multirate sampled-data systems

    NASA Technical Reports Server (NTRS)

    Stanford, D. P.; Caglayan, A. K.

    1975-01-01

    Current adaptive sampling schemes that can be used in sampled-data systems with variable rate sampling does not guarantee the stability of the resulting closed-loop system. A study was undertaken with the objective of finding a stable control law for multirate sampled-data systems. The problem is formulated such that the sampling interval is selected from a set of fixed number of sample intervals. A necessary and sufficient condition under which these types of systems can be stabilized is given. For a certain subclass of these types of systems, a sampling selection algorithm is given which results in a stable closed-loop system.

  6. Sample introduction system for a flow cytometer

    DOEpatents

    Van den Engh, Ger

    1997-01-01

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning, HPLC tubing and fittings may be used in a manner which facilitates removing of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it.

  7. Sample introduction apparatus for a flow cytometer

    DOEpatents

    Van den Engh, Ger

    1998-01-01

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning HPLC tubing and fittings may be used in a manner which facilitates removable of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it.

  8. Sample introduction apparatus for a flow cytometer

    DOEpatents

    Van den Engh, G.

    1998-03-10

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning HPLC tubing and fittings may be used in a manner which facilitates removable of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it. 3 figs.

  9. Sample introduction system for a flow cytometer

    DOEpatents

    Engh, G. van den

    1997-02-11

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning, HPLC tubing and fittings may be used in a manner which facilitates removing of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it. 3 figs.

  10. Apparatus for sectioning demountable semiconductor samples

    DOEpatents

    Sopori, B.L.; Wolf, A.

    1984-01-01

    Apparatus for use during polishing and sectioning operations of a ribbon sample is described. The sample holder includes a cylinder having an axially extending sample cavity terminated in a first funnel-shaped opening and a second slot-like opening. A spring-loaded pressure plunger is located adjacent the second opening of the sample cavity for frictional engagement of the sample cavity. A heat softenable molding medium is inserted in the funnel-shaped opening, to surround the sample. After polishing, the heater is energized to allow draining of the molding medium from the sample cavity. During manual polishing, the second end of the sample holder is inserted in a support ring which provides mechanical support as well as alignment of the sample holder during polishing. A gauge block for measuring the protrusion of a sample beyond the second wall of the holder is also disclosed.

  11. Concrete samples for organic samples, data package and 222-S validation summary report. Addendum 1A

    SciTech Connect

    Vogel, R.E.

    1994-11-01

    This document is in two parts: the first is the data package entitled ``Concrete Samples for Organic Samples`` and the second is entitled ``Concrete Samples for Organic Samples -- Addendum 1A`` which is the 222-S validation summary report.

  12. 40 CFR 761.286 - Sample size and procedure for collecting a sample.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ..., DISTRIBUTION IN COMMERCE, AND USE PROHIBITIONS Sampling To Verify Completion of Self-Implementing Cleanup and...) § 761.286 Sample size and procedure for collecting a sample. At each selected sampling location for...

  13. Markovian Time-Delay Sampling Policies.

    DTIC Science & Technology

    1980-08-01

    Markovian sampling policy for water quality monitoring. Biometrics 33: 41-46. Wald , A. and Wolfowitz , J. (1945). Sampling inspection plans for...to remain in control. This idea is not new. Sampling plans for the percent defective were devised along these lines by Dodge (1943), Wald and... Wolfowitz (1945), and Dodge and Torrey (1951), who gave rules for switching from 100% sampling to sampling a fraction f. Multi-level inspec- tion plans having

  14. Sampling bacteria with a laser

    NASA Astrophysics Data System (ADS)

    Schwarzwälder, Kordula; Rutschmann, Peter

    2014-05-01

    also compared these data to samples of usual collection and filtering. The results of these laser measurements are very promising.

  15. Sample vial inserts: A better approach for sampling heterogeneous slurry samples in the SRS Defense Waste Processing Facility

    SciTech Connect

    Coleman, C.J.; Goode, S.R.

    1996-05-01

    A convenient and effective new approach for analyzing DWPF samples involves the use of inserts with volumes of 1.5--3 ml placed in the neck of 14 ml sample vials. The inserts have rims that conform to the rim of the vials so that they sit straight and stable in the vial. The DWPF tank sampling system fills the pre-weighed insert rather than the entire vial, so the vial functions only as the insert holder. The shielded cell operator then removes the vial cap and decants the insert containing the sample into a plastic bottle, crucible, etc., for analysis. Inert materials such as Teflon, plastic, and zirconium are used for the insert so it is unnecessary to separate the insert from the sample for most analyses. The key technique advantage of using inserts to take DWPF samples versus filling sample vials is that it provides a convenient and almost foolproof way of obtaining and handling small volumes of slurry samples in a shielded cell without corrupting the sample. Since the insert allows the entire sample to be analyzed, this approach eliminates the errors inherent with subsampling heterogeneous slurries that comprise DWPF samples. Slurry samples can then be analyzed with confidence. Analysis times are dramatically reduced by eliminating the drying and vitrification steps normally used to produce a homogeneous solid sample. Direct dissolution and elemental analysis of slurry samples are achieved in 8 hours or less compared with 40 hours for analysis of vitrified slurry samples. Comparison of samples taken in inserts versus full vials indicate that the insert does not significantly affect sample composition.

  16. Using Inverse Probability Bootstrap Sampling to Eliminate Sample Induced Bias in Model Based Analysis of Unequal Probability Samples.

    PubMed

    Nahorniak, Matthew; Larsen, David P; Volk, Carol; Jordan, Chris E

    2015-01-01

    In ecology, as in other research fields, efficient sampling for population estimation often drives sample designs toward unequal probability sampling, such as in stratified sampling. Design based statistical analysis tools are appropriate for seamless integration of sample design into the statistical analysis. However, it is also common and necessary, after a sampling design has been implemented, to use datasets to address questions that, in many cases, were not considered during the sampling design phase. Questions may arise requiring the use of model based statistical tools such as multiple regression, quantile regression, or regression tree analysis. However, such model based tools may require, for ensuring unbiased estimation, data from simple random samples, which can be problematic when analyzing data from unequal probability designs. Despite numerous method specific tools available to properly account for sampling design, too often in the analysis of ecological data, sample design is ignored and consequences are not properly considered. We demonstrate here that violation of this assumption can lead to biased parameter estimates in ecological research. In addition, to the set of tools available for researchers to properly account for sampling design in model based analysis, we introduce inverse probability bootstrapping (IPB). Inverse probability bootstrapping is an easily implemented method for obtaining equal probability re-samples from a probability sample, from which unbiased model based estimates can be made. We demonstrate the potential for bias in model-based analyses that ignore sample inclusion probabilities, and the effectiveness of IPB sampling in eliminating this bias, using both simulated and actual ecological data. For illustration, we considered three model based analysis tools--linear regression, quantile regression, and boosted regression tree analysis. In all models, using both simulated and actual ecological data, we found inferences to be

  17. Using Inverse Probability Bootstrap Sampling to Eliminate Sample Induced Bias in Model Based Analysis of Unequal Probability Samples

    PubMed Central

    Nahorniak, Matthew

    2015-01-01

    In ecology, as in other research fields, efficient sampling for population estimation often drives sample designs toward unequal probability sampling, such as in stratified sampling. Design based statistical analysis tools are appropriate for seamless integration of sample design into the statistical analysis. However, it is also common and necessary, after a sampling design has been implemented, to use datasets to address questions that, in many cases, were not considered during the sampling design phase. Questions may arise requiring the use of model based statistical tools such as multiple regression, quantile regression, or regression tree analysis. However, such model based tools may require, for ensuring unbiased estimation, data from simple random samples, which can be problematic when analyzing data from unequal probability designs. Despite numerous method specific tools available to properly account for sampling design, too often in the analysis of ecological data, sample design is ignored and consequences are not properly considered. We demonstrate here that violation of this assumption can lead to biased parameter estimates in ecological research. In addition, to the set of tools available for researchers to properly account for sampling design in model based analysis, we introduce inverse probability bootstrapping (IPB). Inverse probability bootstrapping is an easily implemented method for obtaining equal probability re-samples from a probability sample, from which unbiased model based estimates can be made. We demonstrate the potential for bias in model-based analyses that ignore sample inclusion probabilities, and the effectiveness of IPB sampling in eliminating this bias, using both simulated and actual ecological data. For illustration, we considered three model based analysis tools—linear regression, quantile regression, and boosted regression tree analysis. In all models, using both simulated and actual ecological data, we found inferences to be

  18. Method and apparatus for data sampling

    DOEpatents

    Odell, D.M.C.

    1994-04-19

    A method and apparatus for sampling radiation detector outputs and determining event data from the collected samples is described. The method uses high speed sampling of the detector output, the conversion of the samples to digital values, and the discrimination of the digital values so that digital values representing detected events are determined. The high speed sampling and digital conversion is performed by an A/D sampler that samples the detector output at a rate high enough to produce numerous digital samples for each detected event. The digital discrimination identifies those digital samples that are not representative of detected events. The sampling and discrimination also provides for temporary or permanent storage, either serially or in parallel, to a digital storage medium. 6 figures.

  19. Method and apparatus for data sampling

    DOEpatents

    Odell, Daniel M. C.

    1994-01-01

    A method and apparatus for sampling radiation detector outputs and determining event data from the collected samples. The method uses high speed sampling of the detector output, the conversion of the samples to digital values, and the discrimination of the digital values so that digital values representing detected events are determined. The high speed sampling and digital conversion is performed by an A/D sampler that samples the detector output at a rate high enough to produce numerous digital samples for each detected event. The digital discrimination identifies those digital samples that are not representative of detected events. The sampling and discrimination also provides for temporary or permanent storage, either serially or in parallel, to a digital storage medium.

  20. Fluid sampling system for a nuclear reactor

    DOEpatents

    Lau, Louis K.; Alper, Naum I.

    1994-01-01

    A system of extracting fluid samples, either liquid or gas, from the interior of a nuclear reactor containment utilizes a jet pump. To extract the sample fluid, a nonradioactive motive fluid is forced through the inlet and discharge ports of a jet pump located outside the containment, creating a suction that draws the sample fluid from the containment through a sample conduit connected to the pump suction port. The mixture of motive fluid and sample fluid is discharged through a return conduit to the interior of the containment. The jet pump and means for removing a portion of the sample fluid from the sample conduit can be located in a shielded sample grab station located next to the containment. A non-nuclear grade active pump can be located outside the grab sampling station and the containment to pump the nonradioactive motive fluid through the jet pump.

  1. Fluid sampling system for a nuclear reactor

    DOEpatents

    Lau, L.K.; Alper, N.I.

    1994-11-22

    A system of extracting fluid samples, either liquid or gas, from the interior of a nuclear reactor containment utilizes a jet pump. To extract the sample fluid, a nonradioactive motive fluid is forced through the inlet and discharge ports of a jet pump located outside the containment, creating a suction that draws the sample fluid from the containment through a sample conduit connected to the pump suction port. The mixture of motive fluid and sample fluid is discharged through a return conduit to the interior of the containment. The jet pump and means for removing a portion of the sample fluid from the sample conduit can be located in a shielded sample grab station located next to the containment. A non-nuclear grade active pump can be located outside the grab sampling station and the containment to pump the nonradioactive motive fluid through the jet pump. 1 fig.

  2. A Sample Return Container with Hermetic Seal

    NASA Technical Reports Server (NTRS)

    Kong, Kin Yuen; Rafeek, Shaheed; Sadick, Shazad; Porter, Christopher C.

    2000-01-01

    A sample return container is being developed by Honeybee Robotics to receive samples from a derivative of the Champollion/ST4 Sample Acquisition and Transfer Mechanism or other samplers and then hermetically seal samples for a sample return mission. The container is enclosed in a phase change material (PCM) chamber to prevent phase change during return and re-entry to earth. This container is designed to operate passively with no motors and actuators. Using the sampler's featured drill tip for interfacing, transfer-ring and sealing samples, the container consumes no electrical power and therefore minimizes sample temperature change. The circular container houses a few isolated canisters, which will be sealed individually for samples acquired from different sites or depths. The drill based sampler indexes each canister to the sample transfer position, below the index interface for sample transfer. After sample transfer is completed, the sampler indexes a seal carrier, which lines up seals with the openings of the canisters. The sampler moves to the sealing interface and seals the sample canisters one by one. The sealing interface can be designed to work with C-seals, knife edge seals and cup seals. Again, the sampler provides all sealing actuation. This sample return container and co-engineered sample acquisition system are being developed by Honeybee Robotics in collaboration with the JPL Exploration Technology program.

  3. Options in Extraterrestrial Sample Handling and Study

    NASA Technical Reports Server (NTRS)

    Papanastassiou, Dimitri A.

    2000-01-01

    This presentation mentions important service functions such as: sample preservation, hazard assessment, and handling. It also discuss how preliminary examination of samples is necessary for sample hazard assessment and for sample allocations. Clean facilities and clean sample handling are required. Conflicts, cross contamination issues will be present and need to be resolved. Extensive experience is available for extraterrestrial samples and must be sought and applied. Extensive experience is available in studies of pathogenicity and must be sought and applied as necessary. Advisory and oversight structures must also be in place

  4. Sampling considerations for health care improvement.

    PubMed

    Perla, Rocco J; Provost, Lloyd P; Murray, Sandra K

    2014-01-01

    Sampling in improvement work can pose challenges. How is it different from the sampling strategies many use with research, clinical trials, or regulatory programs? What should improvement teams consider when determining a useful approach to sampling and a useful sample size? The aim of this article is to introduce some of the concepts related to sampling for improvement. We give specific guidance related to determining a useful sample size to a wider health care audience so that it can be applied to improvement projects in hospitals and health systems.

  5. Sampling considerations for health care improvement.

    PubMed

    Perla, Rocco J; Provost, Lloyd P; Murray, Sandra K

    2013-01-01

    Sampling in improvement work can pose challenges. How is it different from the sampling strategies many use with research, clinical trials, or regulatory programs? What should improvement teams consider when determining a useful approach to sampling and a useful sample size? The aim of this article is to introduce some of the concepts related to sampling for improvement. We give specific guidance related to determining a useful sample size to a wider health care audience so that it can be applied to improvement projects in hospitals and health systems.

  6. ALARA ASSESSMENT OF SETTLER SLUDGE SAMPLING METHODS

    SciTech Connect

    NELSEN LA

    2009-01-30

    The purpose of this assessment is to compare underwater and above water settler sludge sampling methods to determine if the added cost for underwater sampling for the sole purpose of worker dose reductions is justified. Initial planning for sludge sampling included container, settler and knock-out-pot (KOP) sampling. Due to the significantly higher dose consequence of KOP sludge, a decision was made to sample KOP underwater to achieve worker dose reductions. Additionally, initial plans were to utilize the underwater sampling apparatus for settler sludge. Since there are no longer plans to sample KOP sludge, the decision for underwater sampling for settler sludge needs to be revisited. The present sampling plan calls for spending an estimated $2,500,000 to design and construct a new underwater sampling system (per A21 C-PL-001 RevOE). This evaluation will compare and contrast the present method of above water sampling to the underwater method that is planned by the Sludge Treatment Project (STP) and determine if settler samples can be taken using the existing sampling cart (with potentially minor modifications) while maintaining doses to workers As Low As Reasonably Achievable (ALARA) and eliminate the need for costly redesigns, testing and personnel retraining.

  7. Dynamic Method for Identifying Collected Sample Mass

    NASA Technical Reports Server (NTRS)

    Carson, John

    2008-01-01

    G-Sample is designed for sample collection missions to identify the presence and quantity of sample material gathered by spacecraft equipped with end effectors. The software method uses a maximum-likelihood estimator to identify the collected sample's mass based on onboard force-sensor measurements, thruster firings, and a dynamics model of the spacecraft. This makes sample mass identification a computation rather than a process requiring additional hardware. Simulation examples of G-Sample are provided for spacecraft model configurations with a sample collection device mounted on the end of an extended boom. In the absence of thrust knowledge errors, the results indicate that G-Sample can identify the amount of collected sample mass to within 10 grams (with 95-percent confidence) by using a force sensor with a noise and quantization floor of 50 micrometers. These results hold even in the presence of realistic parametric uncertainty in actual spacecraft inertia, center-of-mass offset, and first flexibility modes. Thrust profile knowledge is shown to be a dominant sensitivity for G-Sample, entering in a nearly one-to-one relationship with the final mass estimation error. This means thrust profiles should be well characterized with onboard accelerometers prior to sample collection. An overall sample-mass estimation error budget has been developed to approximate the effect of model uncertainty, sensor noise, data rate, and thrust profile error on the expected estimate of collected sample mass.

  8. Small Sample Whole-Genome Amplification

    SciTech Connect

    Hara, C A; Nguyen, C P; Wheeler, E K; Sorensen, K J; Arroyo, E S; Vrankovich, G P; Christian, A T

    2005-09-20

    Many challenges arise when trying to amplify and analyze human samples collected in the field due to limitations in sample quantity, and contamination of the starting material. Tests such as DNA fingerprinting and mitochondrial typing require a certain sample size and are carried out in large volume reactions; in cases where insufficient sample is present whole genome amplification (WGA) can be used. WGA allows very small quantities of DNA to be amplified in a way that enables subsequent DNA-based tests to be performed. A limiting step to WGA is sample preparation. To minimize the necessary sample size, we have developed two modifications of WGA: the first allows for an increase in amplified product from small, nanoscale, purified samples with the use of carrier DNA while the second is a single-step method for cleaning and amplifying samples all in one column. Conventional DNA cleanup involves binding the DNA to silica, washing away impurities, and then releasing the DNA for subsequent testing. We have eliminated losses associated with incomplete sample release, thereby decreasing the required amount of starting template for DNA testing. Both techniques address the limitations of sample size by providing ample copies of genomic samples. Carrier DNA, included in our WGA reactions, can be used when amplifying samples with the standard purification method, or can be used in conjunction with our single-step DNA purification technique to potentially further decrease the amount of starting sample necessary for future forensic DNA-based assays.

  9. Small sample whole-genome amplification

    NASA Astrophysics Data System (ADS)

    Hara, Christine; Nguyen, Christine; Wheeler, Elizabeth; Sorensen, Karen; Arroyo, Erin; Vrankovich, Greg; Christian, Allen

    2005-11-01

    Many challenges arise when trying to amplify and analyze human samples collected in the field due to limitations in sample quantity, and contamination of the starting material. Tests such as DNA fingerprinting and mitochondrial typing require a certain sample size and are carried out in large volume reactions; in cases where insufficient sample is present whole genome amplification (WGA) can be used. WGA allows very small quantities of DNA to be amplified in a way that enables subsequent DNA-based tests to be performed. A limiting step to WGA is sample preparation. To minimize the necessary sample size, we have developed two modifications of WGA: the first allows for an increase in amplified product from small, nanoscale, purified samples with the use of carrier DNA while the second is a single-step method for cleaning and amplifying samples all in one column. Conventional DNA cleanup involves binding the DNA to silica, washing away impurities, and then releasing the DNA for subsequent testing. We have eliminated losses associated with incomplete sample release, thereby decreasing the required amount of starting template for DNA testing. Both techniques address the limitations of sample size by providing ample copies of genomic samples. Carrier DNA, included in our WGA reactions, can be used when amplifying samples with the standard purification method, or can be used in conjunction with our single-step DNA purification technique to potentially further decrease the amount of starting sample necessary for future forensic DNA-based assays.

  10. Environmental sampling for spores of Bacillus anthracis.

    PubMed

    Teshale, Eyasu H; Painter, John; Burr, Gregory A; Mead, Paul; Wright, Scott V; Cseh, Larry F; Zabrocki, Ronald; Collins, Rick; Kelley, Kathy A; Hadler, James L; Swerdlow, David L

    2002-10-01

    On November 11, 2001, following the bioterrorism-related anthrax attacks, the U.S. Postal Service collected samples at the Southern Connecticut Processing and Distribution Center; all samples were negative for Bacillus anthracis. After a patient in Connecticut died from inhalational anthrax on November 19, the center was sampled again on November 21 and 25 by using dry and wet swabs. All samples were again negative for B. anthracis. On November 28, guided by information from epidemiologic investigation, we sampled the site extensively with wet wipes and surface vacuum sock samples (using HEPA vacuum). Of 212 samples, 6 (3%) were positive, including one from a highly contaminated sorter. Subsequently B. anthracis was also detected in mail-sorting bins used for the patient's carrier route. These results suggest cross-contaminated mail as a possible source of anthrax for the inhalational anthrax patient in Connecticut. In future such investigations, extensive sampling guided by epidemiologic data is imperative.

  11. 21 CFR 1230.44 - Samples.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... POISON ACT Imports § 1230.44 Samples. On the same day that samples are requested by the district, the... the containers do not comply with the requirements of the Federal Caustic Poison Act, they must...

  12. 21 CFR 1230.44 - Samples.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... POISON ACT Imports § 1230.44 Samples. On the same day that samples are requested by the district, the... the containers do not comply with the requirements of the Federal Caustic Poison Act, they must...

  13. 21 CFR 1230.44 - Samples.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... POISON ACT Imports § 1230.44 Samples. On the same day that samples are requested by the district, the... the containers do not comply with the requirements of the Federal Caustic Poison Act, they must...

  14. 21 CFR 1230.44 - Samples.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... POISON ACT Imports § 1230.44 Samples. On the same day that samples are requested by the district, the... the containers do not comply with the requirements of the Federal Caustic Poison Act, they must...

  15. 21 CFR 1230.44 - Samples.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... POISON ACT Imports § 1230.44 Samples. On the same day that samples are requested by the district, the... the containers do not comply with the requirements of the Federal Caustic Poison Act, they must...

  16. 19 CFR 151.51 - Sampling requirements.

    Code of Federal Regulations, 2013 CFR

    2013-04-01

    ... warehousing at the port of first arrival, they shall be sampled for assay and moisture purposes in accordance... of any available sample, knowledge of prior importations of similar materials, and other data,...

  17. 19 CFR 151.51 - Sampling requirements.

    Code of Federal Regulations, 2011 CFR

    2011-04-01

    ... warehousing at the port of first arrival, they shall be sampled for assay and moisture purposes in accordance... of any available sample, knowledge of prior importations of similar materials, and other data,...

  18. 19 CFR 151.51 - Sampling requirements.

    Code of Federal Regulations, 2010 CFR

    2010-04-01

    ... warehousing at the port of first arrival, they shall be sampled for assay and moisture purposes in accordance... of any available sample, knowledge of prior importations of similar materials, and other data,...

  19. 19 CFR 151.51 - Sampling requirements.

    Code of Federal Regulations, 2014 CFR

    2014-04-01

    ... warehousing at the port of first arrival, they shall be sampled for assay and moisture purposes in accordance... of any available sample, knowledge of prior importations of similar materials, and other data,...

  20. 19 CFR 151.51 - Sampling requirements.

    Code of Federal Regulations, 2012 CFR

    2012-04-01

    ... warehousing at the port of first arrival, they shall be sampled for assay and moisture purposes in accordance... of any available sample, knowledge of prior importations of similar materials, and other data,...

  1. ADVANCES IN GROUND WATER SAMPLING PROCEDURES

    EPA Science Inventory

    Obtaining representative ground water samples is important for site assessment and remedial performance monitoring objectives. Issues which must be considered prior to initiating a ground-water monitoring program include defining monitoring goals and objectives, sampling point...

  2. Phootprint: A European Phobos Sample Return Mission

    NASA Astrophysics Data System (ADS)

    Barraclough, S.; Ratcliffe, A.; Buchwald, R.; Scheer, H.; Chapuy, M.; Garland, M.; Rebuffat, D.

    2014-06-01

    Phootprint is an ESA funded feasibility study for a European Phobos Sample Return Mission. A complete system design has been performed including ERC, Landing Leg, Sample Acquisition System and GNC Proximity Operations.

  3. Principles for Sampling Airborne Radioactivity from Stacks

    SciTech Connect

    Glissmeyer, John A.

    2010-10-18

    This book chapter describes the special processes involved in sampling the airborne effluents from nuclear faciities. The title of the book is Radioactive Air Sampling Methods. The abstract for this chapter was cleared as PNNL-SA-45941.

  4. REPRESENTATIVE SAMPLING AND ANALYSIS OF HETEROGENEOUS SOILS

    EPA Science Inventory

    Standard sampling and analysis methods for hazardous substances in contaminated soils currently are available and routinely employed. Standard methods inherently assume a homogeneous soil matrix and contaminant distribution; therefore only small sample quantities typically are p...

  5. 40 CFR 761.130 - Sampling requirements.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... sampling scheme and the guidance document are available on EPA's PCB Web site at http://www.epa.gov/pcb, or... sampling scheme is that it is designed to characterize the degree of contamination within the...

  6. 40 CFR 761.130 - Sampling requirements.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... sampling scheme and the guidance document are available on EPA's PCB Web site at http://www.epa.gov/pcb, or... sampling scheme is that it is designed to characterize the degree of contamination within the...

  7. Petrological studies on lunar rock samples

    NASA Technical Reports Server (NTRS)

    Kushiro, I.

    1974-01-01

    Petrological studies were made on Apollo 14, 15, 16, and 17 lunar samples. High-pressure melting experiments were conducted, along with electron microprobe analyses. The composition of the samples is reported.

  8. Lab Analyses of Pet Coke Samples

    EPA Pesticide Factsheets

    April 2014: the EPA Chicago Regional Laboratory analyzed samples taken from petroleum coke (petcoke) storage piles at KCBX facilities in southeast Chicago. The samples were analyzed for metals, radionuclides and PAHs.

  9. Subrandom methods for multidimensional nonuniform sampling

    NASA Astrophysics Data System (ADS)

    Worley, Bradley

    2016-08-01

    Methods of nonuniform sampling that utilize pseudorandom number sequences to select points from a weighted Nyquist grid are commonplace in biomolecular NMR studies, due to the beneficial incoherence introduced by pseudorandom sampling. However, these methods require the specification of a non-arbitrary seed number in order to initialize a pseudorandom number generator. Because the performance of pseudorandom sampling schedules can substantially vary based on seed number, this can complicate the task of routine data collection. Approaches such as jittered sampling and stochastic gap sampling are effective at reducing random seed dependence of nonuniform sampling schedules, but still require the specification of a seed number. This work formalizes the use of subrandom number sequences in nonuniform sampling as a means of seed-independent sampling, and compares the performance of three subrandom methods to their pseudorandom counterparts using commonly applied schedule performance metrics. Reconstruction results using experimental datasets are also provided to validate claims made using these performance metrics.

  10. Molecular-beam gas-sampling system

    NASA Technical Reports Server (NTRS)

    Young, W. S.; Knuth, E. L.

    1972-01-01

    A molecular beam mass spectrometer system for rocket motor combustion chamber sampling is described. The history of the sampling system is reviewed. The problems associated with rocket motor combustion chamber sampling are reported. Several design equations are presented. The results of the experiments include the effects of cooling water flow rates, the optimum separation gap between the end plate and sampling nozzle, and preliminary data on compositions in a rocket motor combustion chamber.

  11. Acoustic Translation of an Acoustically Levitated Sample

    NASA Technical Reports Server (NTRS)

    Barmatz, M. B.; Allen, J. L.

    1986-01-01

    Acoustic-levitation apparatus uses only one acoustic mode to move sample from one region of chamber to another. Sample heated and cooled quickly by translation between hot and cold regions of levitation chamber. Levitated sample is raised into furnace region by raising plunger. Frequency of sound produced by transducers adjusted by feedback system to maintain (102) resonant mode, which levitates sample midway between transducers and plunger regardless of plunger position.

  12. Illustration of Launching Samples Home from Mars

    NASA Technical Reports Server (NTRS)

    2005-01-01

    One crucial step in a Mars sample return mission would be to launch the collected sample away from the surface of Mars. This artist's concept depicts a Mars ascent vehicle for starting a sample of Mars rocks on their trip to Earth.

  13. Lunar and Meteorite Sample Disk for Educators

    NASA Technical Reports Server (NTRS)

    Foxworth, Suzanne; Luckey, M.; McInturff, B.; Allen, J.; Kascak, A.

    2015-01-01

    NASA Johnson Space Center (JSC) has the unique responsibility to curate NASA's extraterrestrial samples from past and future missions. Curation includes documentation, preservation, preparation and distribution of samples for research, education and public outreach. Between 1969 and 1972 six Apollo missions brought back 382 kilograms of lunar rocks, core and regolith samples, from the lunar surface. JSC also curates meteorites collected from a US cooperative effort among NASA, the National Science Foundation (NSF) and the Smithsonian Institution that funds expeditions to Antarctica. The meteorites that are collected include rocks from Moon, Mars, and many asteroids including Vesta. The sample disks for educational use include these different samples. Active relevant learning has always been important to teachers and the Lunar and Meteorite Sample Disk Program provides this active style of learning for students and the general public. The Lunar and Meteorite Sample Disks permit students to conduct investigations comparable to actual scientists. The Lunar Sample Disk contains 6 samples; Basalt, Breccia, Highland Regolith, Anorthosite, Mare Regolith and Orange Soil. The Meteorite Sample Disk contains 6 samples; Chondrite L3, Chondrite H5, Carbonaceous Chondrite, Basaltic Achondrite, Iron and Stony-Iron. Teachers are given different activities that adhere to their standards with the disks. During a Sample Disk Certification Workshop, teachers participate in the activities as students gain insight into the history, formation and geologic processes of the moon, asteroids and meteorites.

  14. 7 CFR 29.33 - Official sample.

    Code of Federal Regulations, 2010 CFR

    2010-01-01

    ... 7 Agriculture 2 2010-01-01 2010-01-01 false Official sample. 29.33 Section 29.33 Agriculture Regulations of the Department of Agriculture AGRICULTURAL MARKETING SERVICE (Standards, Inspections, Marketing... INSPECTION Regulations Definitions § 29.33 Official sample. A sample selected, tagged, and signed by...

  15. 45 CFR 1356.84 - Sampling.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ...(e) of this part on a sample of the baseline population consistent with the sampling requirements... population consistent with 45 CFR 1356.81(b) who participated in the State agency's data collection at age 17. (c) The sample size is based on the number of youth in the baseline population who participated...

  16. 45 CFR 1356.84 - Sampling.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ...(e) of this part on a sample of the baseline population consistent with the sampling requirements... population consistent with 45 CFR 1356.81(b) who participated in the State agency's data collection at age 17. (c) The sample size is based on the number of youth in the baseline population who participated...

  17. 45 CFR 1356.84 - Sampling.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ...(e) of this part on a sample of the baseline population consistent with the sampling requirements... population consistent with 45 CFR 1356.81(b) who participated in the State agency's data collection at age 17. (c) The sample size is based on the number of youth in the baseline population who participated...

  18. 42 CFR 1003.133 - Statistical sampling.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 42 Public Health 5 2014-10-01 2014-10-01 false Statistical sampling. 1003.133 Section 1003.133... AUTHORITIES CIVIL MONEY PENALTIES, ASSESSMENTS AND EXCLUSIONS § 1003.133 Statistical sampling. (a) In meeting... statistical sampling study as evidence of the number and amount of claims and/or requests for payment...

  19. 45 CFR 160.536 - Statistical sampling.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 45 Public Welfare 1 2011-10-01 2011-10-01 false Statistical sampling. 160.536 Section 160.536... REQUIREMENTS GENERAL ADMINISTRATIVE REQUIREMENTS Procedures for Hearings § 160.536 Statistical sampling. (a) In... statistical sampling study as evidence of the number of violations under § 160.406 of this part, or...

  20. 42 CFR 1003.133 - Statistical sampling.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 42 Public Health 5 2012-10-01 2012-10-01 false Statistical sampling. 1003.133 Section 1003.133... AUTHORITIES CIVIL MONEY PENALTIES, ASSESSMENTS AND EXCLUSIONS § 1003.133 Statistical sampling. (a) In meeting... statistical sampling study as evidence of the number and amount of claims and/or requests for payment...

  1. 45 CFR 160.536 - Statistical sampling.

    Code of Federal Regulations, 2012 CFR

    2012-10-01

    ... 45 Public Welfare 1 2012-10-01 2012-10-01 false Statistical sampling. 160.536 Section 160.536... REQUIREMENTS GENERAL ADMINISTRATIVE REQUIREMENTS Procedures for Hearings § 160.536 Statistical sampling. (a) In... statistical sampling study as evidence of the number of violations under § 160.406 of this part, or...

  2. 42 CFR 1003.133 - Statistical sampling.

    Code of Federal Regulations, 2011 CFR

    2011-10-01

    ... 42 Public Health 5 2011-10-01 2011-10-01 false Statistical sampling. 1003.133 Section 1003.133... AUTHORITIES CIVIL MONEY PENALTIES, ASSESSMENTS AND EXCLUSIONS § 1003.133 Statistical sampling. (a) In meeting... statistical sampling study as evidence of the number and amount of claims and/or requests for payment...

  3. 42 CFR 1003.133 - Statistical sampling.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... 42 Public Health 5 2010-10-01 2010-10-01 false Statistical sampling. 1003.133 Section 1003.133... AUTHORITIES CIVIL MONEY PENALTIES, ASSESSMENTS AND EXCLUSIONS § 1003.133 Statistical sampling. (a) In meeting... statistical sampling study as evidence of the number and amount of claims and/or requests for payment...

  4. 45 CFR 160.536 - Statistical sampling.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 45 Public Welfare 1 2013-10-01 2013-10-01 false Statistical sampling. 160.536 Section 160.536... REQUIREMENTS GENERAL ADMINISTRATIVE REQUIREMENTS Procedures for Hearings § 160.536 Statistical sampling. (a) In... statistical sampling study as evidence of the number of violations under § 160.406 of this part, or...

  5. 45 CFR 160.536 - Statistical sampling.

    Code of Federal Regulations, 2014 CFR

    2014-10-01

    ... 45 Public Welfare 1 2014-10-01 2014-10-01 false Statistical sampling. 160.536 Section 160.536... REQUIREMENTS GENERAL ADMINISTRATIVE REQUIREMENTS Procedures for Hearings § 160.536 Statistical sampling. (a) In... statistical sampling study as evidence of the number of violations under § 160.406 of this part, or...

  6. 42 CFR 1003.133 - Statistical sampling.

    Code of Federal Regulations, 2013 CFR

    2013-10-01

    ... 42 Public Health 5 2013-10-01 2013-10-01 false Statistical sampling. 1003.133 Section 1003.133... AUTHORITIES CIVIL MONEY PENALTIES, ASSESSMENTS AND EXCLUSIONS § 1003.133 Statistical sampling. (a) In meeting... statistical sampling study as evidence of the number and amount of claims and/or requests for payment...

  7. Social network sampling using spanning trees

    NASA Astrophysics Data System (ADS)

    Jalali, Zeinab S.; Rezvanian, Alireza; Meybodi, Mohammad Reza

    2016-12-01

    Due to the large scales and limitations in accessing most online social networks, it is hard or infeasible to directly access them in a reasonable amount of time for studying and analysis. Hence, network sampling has emerged as a suitable technique to study and analyze real networks. The main goal of sampling online social networks is constructing a small scale sampled network which preserves the most important properties of the original network. In this paper, we propose two sampling algorithms for sampling online social networks using spanning trees. The first proposed sampling algorithm finds several spanning trees from randomly chosen starting nodes; then the edges in these spanning trees are ranked according to the number of times that each edge has appeared in the set of found spanning trees in the given network. The sampled network is then constructed as a sub-graph of the original network which contains a fraction of nodes that are incident on highly ranked edges. In order to avoid traversing the entire network, the second sampling algorithm is proposed using partial spanning trees. The second sampling algorithm is similar to the first algorithm except that it uses partial spanning trees. Several experiments are conducted to examine the performance of the proposed sampling algorithms on well-known real networks. The obtained results in comparison with other popular sampling methods demonstrate the efficiency of the proposed sampling algorithms in terms of Kolmogorov-Smirnov distance (KSD), skew divergence distance (SDD) and normalized distance (ND).

  8. 30 CFR 15.5 - Test samples.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 30 Mineral Resources 1 2010-07-01 2010-07-01 false Test samples. 15.5 Section 15.5 Mineral... § 15.5 Test samples. (a) Submission of test samples. (1) The applicant shall not submit explosives or... magazine for at least 30 days before gallery tests are conducted....

  9. 30 CFR 15.5 - Test samples.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 30 Mineral Resources 1 2013-07-01 2013-07-01 false Test samples. 15.5 Section 15.5 Mineral... § 15.5 Test samples. (a) Submission of test samples. (1) The applicant shall not submit explosives or... magazine for at least 30 days before gallery tests are conducted....

  10. 30 CFR 15.5 - Test samples.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 30 Mineral Resources 1 2011-07-01 2011-07-01 false Test samples. 15.5 Section 15.5 Mineral... § 15.5 Test samples. (a) Submission of test samples. (1) The applicant shall not submit explosives or... magazine for at least 30 days before gallery tests are conducted....

  11. Wastewater Sampling Methodologies and Flow Measurement Techniques.

    ERIC Educational Resources Information Center

    Harris, Daniel J.; Keffer, William J.

    This document provides a ready source of information about water/wastewater sampling activities using various commercial sampling and flow measurement devices. The report consolidates the findings and summarizes the activities, experiences, sampling methods, and field measurement techniques conducted by the Environmental Protection Agency (EPA),…

  12. 31 CFR 515.547 - Research samples.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 31 Money and Finance: Treasury 3 2010-07-01 2010-07-01 false Research samples. 515.547 Section 515..., Authorizations, and Statements of Licensing Policy § 515.547 Research samples. Specific licenses are issued for importation of Cuban-origin commodities for bona-fide research purposes in sample quantities only....

  13. 31 CFR 500.552 - Research samples.

    Code of Federal Regulations, 2010 CFR

    2010-07-01

    ... 31 Money and Finance: Treasury 3 2010-07-01 2010-07-01 false Research samples. 500.552 Section 500..., Authorizations and Statements of Licensing Policy § 500.552 Research samples. Specific licenses are issued for importation of commodities subject to § 500.204 for bona fide research purposes in sample quantities only....

  14. 40 CFR 141.703 - Sampling locations.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... samples prior to the point of filter backwash water addition. (d) Bank filtration. (1) Systems that... applicable, must collect source water samples in the surface water prior to bank filtration. (2) Systems that use bank filtration as pretreatment to a filtration plant must collect source water samples from...

  15. 40 CFR 141.703 - Sampling locations.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... samples prior to the point of filter backwash water addition. (d) Bank filtration. (1) Systems that... applicable, must collect source water samples in the surface water prior to bank filtration. (2) Systems that use bank filtration as pretreatment to a filtration plant must collect source water samples from...

  16. 40 CFR 141.703 - Sampling locations.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... samples prior to the point of filter backwash water addition. (d) Bank filtration. (1) Systems that... applicable, must collect source water samples in the surface water prior to bank filtration. (2) Systems that use bank filtration as pretreatment to a filtration plant must collect source water samples from...

  17. 40 CFR 141.703 - Sampling locations.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... samples prior to the point of filter backwash water addition. (d) Bank filtration. (1) Systems that... applicable, must collect source water samples in the surface water prior to bank filtration. (2) Systems that use bank filtration as pretreatment to a filtration plant must collect source water samples from...

  18. 42 CFR 402.109 - Statistical sampling.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... Statistical sampling. (a) Purpose. CMS or OIG may introduce the results of a statistical sampling study to... or caused to be presented. (b) Prima facie evidence. The results of the statistical sampling study... § 402.1. (c) Burden of proof. Once CMS or OIG has made a prima facie case, the burden is on...

  19. 45 CFR 160.536 - Statistical sampling.

    Code of Federal Regulations, 2010 CFR

    2010-10-01

    ... statistical sampling study as evidence of the number of violations under § 160.406 of this part, or the... statistical sampling study, if based upon an appropriate sampling and computed by valid statistical methods... prima facie case, as described in paragraph (a) of this section, the burden of going forward shifts...

  20. 40 CFR 1065.1111 - Sample analysis.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 40 Protection of Environment 33 2014-07-01 2014-07-01 false Sample analysis. 1065.1111 Section... § 1065.1111 Sample analysis. This subpart does not specify chromatographic or analytical methods to... process by verifying the volume of sample injected for analysis....

  1. 31 CFR 515.547 - Research samples.

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ... 31 Money and Finance:Treasury 3 2011-07-01 2011-07-01 false Research samples. 515.547 Section 515..., Authorizations, and Statements of Licensing Policy § 515.547 Research samples. Specific licenses are issued for importation of Cuban-origin commodities for bona-fide research purposes in sample quantities only....

  2. 31 CFR 515.547 - Research samples.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... 31 Money and Finance:Treasury 3 2013-07-01 2013-07-01 false Research samples. 515.547 Section 515..., Authorizations, and Statements of Licensing Policy § 515.547 Research samples. Specific licenses are issued for importation of Cuban-origin commodities for bona-fide research purposes in sample quantities only....

  3. 31 CFR 515.547 - Research samples.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... 31 Money and Finance:Treasury 3 2012-07-01 2012-07-01 false Research samples. 515.547 Section 515..., Authorizations, and Statements of Licensing Policy § 515.547 Research samples. Specific licenses are issued for importation of Cuban-origin commodities for bona-fide research purposes in sample quantities only....

  4. 31 CFR 515.547 - Research samples.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... 31 Money and Finance:Treasury 3 2014-07-01 2014-07-01 false Research samples. 515.547 Section 515..., Authorizations, and Statements of Licensing Policy § 515.547 Research samples. Specific licenses are issued for importation of Cuban-origin commodities for bona-fide research purposes in sample quantities only....

  5. Mixed Methods Sampling: A Typology with Examples

    ERIC Educational Resources Information Center

    Teddlie, Charles; Yu, Fen

    2007-01-01

    This article presents a discussion of mixed methods (MM) sampling techniques. MM sampling involves combining well-established qualitative and quantitative techniques in creative ways to answer research questions posed by MM research designs. Several issues germane to MM sampling are presented including the differences between probability and…

  6. 40 CFR 761.292 - Chemical extraction and analysis of individual samples and composite samples.

    Code of Federal Regulations, 2012 CFR

    2012-07-01

    ... individual samples and composite samples. 761.292 Section 761.292 Protection of Environment ENVIRONMENTAL....61(a)(6) § 761.292 Chemical extraction and analysis of individual samples and composite samples. Use... individual and composite samples of PCB remediation waste. Use Method 8082 from SW-846, or a method...

  7. 40 CFR 761.292 - Chemical extraction and analysis of individual samples and composite samples.

    Code of Federal Regulations, 2014 CFR

    2014-07-01

    ... individual samples and composite samples. 761.292 Section 761.292 Protection of Environment ENVIRONMENTAL....61(a)(6) § 761.292 Chemical extraction and analysis of individual samples and composite samples. Use... individual and composite samples of PCB remediation waste. Use Method 8082 from SW-846, or a method...

  8. 40 CFR 761.292 - Chemical extraction and analysis of individual samples and composite samples.

    Code of Federal Regulations, 2013 CFR

    2013-07-01

    ... individual samples and composite samples. 761.292 Section 761.292 Protection of Environment ENVIRONMENTAL....61(a)(6) § 761.292 Chemical extraction and analysis of individual samples and composite samples. Use... individual and composite samples of PCB remediation waste. Use Method 8082 from SW-846, or a method...

  9. [Variance estimation considering multistage sampling design in multistage complex sample analysis].

    PubMed

    Li, Yichong; Zhao, Yinjun; Wang, Limin; Zhang, Mei; Zhou, Maigeng

    2016-03-01

    Multistage sampling is a frequently-used method in random sampling survey in public health. Clustering or independence between observations often exists in the sampling, often called complex sample, generated by multistage sampling. Sampling error may be underestimated and the probability of type I error may be increased if the multistage sample design was not taken into consideration in analysis. As variance (error) estimator in complex sample is often complicated, statistical software usually adopt ultimate cluster variance estimate (UCVE) to approximate the estimation, which simply assume that the sample comes from one-stage sampling. However, with increased sampling fraction of primary sampling unit, contribution from subsequent sampling stages is no more trivial, and the ultimate cluster variance estimate may, therefore, lead to invalid variance estimation. This paper summarize a method of variance estimation considering multistage sampling design. The performances are compared with UCVE and the method considering multistage sampling design by simulating random sampling under different sampling schemes using real world data. Simulation showed that as primary sampling unit (PSU) sampling fraction increased, UCVE tended to generate increasingly biased estimation, whereas accurate estimates were obtained by using the method considering multistage sampling design.

  10. The Effect of Asymmetrical Sample Training on Retention Functions for Hedonic Samples in Rats

    ERIC Educational Resources Information Center

    Simmons, Sabrina; Santi, Angelo

    2012-01-01

    Rats were trained in a symbolic delayed matching-to-sample task to discriminate sample stimuli that consisted of the presence of food or the absence of food. Asymmetrical sample training was provided in which one group was initially trained with only the food sample and the other group was initially trained with only the no-food sample. In…

  11. Global Unique Identification of Geoscience Samples: The International Geo Sample Number (IGSN) and the System for Earth Sample Registration (SESAR)

    NASA Astrophysics Data System (ADS)

    Lehnert, K. A.; Goldstein, S. L.; Vinayagamoorthy, S.; Lenhardt, W. C.

    2005-12-01

    Data on samples represent a primary foundation of Geoscience research across disciplines, ranging from the study of climate change, to biogeochemical cycles, to mantle and continental dynamics and are key to our knowledge of the Earth's dynamical systems and evolution. Different data types are generated for individual samples by different research groups, published in different papers, and stored in different databases on a global scale. The utility of these data is critically dependent on their integration. Such integration can be achieved within a Geoscience Cyberinfrastructure, but requires unambiguous identification of samples. Currently, naming of samples is arbitrary and inconsistent and therefore severely limits our ability to share, link, and integrate sample-based data. Major problems include name duplication, and changing of names as a sample is passed along over many years to different investigators. SESAR, the System for Earth Sample Registration (http://www.geosamples.org), addresses this problem by building a registry that generates and administers globally unique identifiers for Geoscience samples: the International Geo Sample Number (IGSN). Implementation of the IGSN in data publication and digital data management will dramatically advance interoperability among information systems for sample-based data, opening an extensive range of new opportunities for discovery and for interdisciplinary approaches in research. The IGSN will also facilitate the ability of investigators to build on previously collected data on samples as new measurements are made or new techniques are developed. With potentially broad application to all types of Geoscience samples, SESAR is global in scope. It is a web-based system that can be easily accessed by individual users through an interactive web interface and by distributed client systems via standard web services. Samples can be registered individually or in batches and at various levels of granularity from entire cores

  12. Statistical aspects of food safety sampling.

    PubMed

    Jongenburger, I; den Besten, H M W; Zwietering, M H

    2015-01-01

    In food safety management, sampling is an important tool for verifying control. Sampling by nature is a stochastic process. However, uncertainty regarding results is made even greater by the uneven distribution of microorganisms in a batch of food. This article reviews statistical aspects of sampling and describes the impact of distributions on the sampling results. Five different batch contamination scenarios are illustrated: a homogeneous batch, a heterogeneous batch with high- or low-level contamination, and a batch with localized high- or low-level contamination. These batch contamination scenarios showed that sampling results have to be interpreted carefully, especially when heterogeneous and localized contamination in food products is expected.

  13. Technology for return of planetary samples, 1977

    NASA Technical Reports Server (NTRS)

    1978-01-01

    Recent progress on the development of a basic warning system (BWS) proposed to assess the biohazard of a Mars sample returned to earth, an earth orbiting spacecraft, or to a moon base was presented. The BWS package consists of terrestrial microorganisms representing major metabolic pathways. A vital processes component of the BWS will examine the effects of a Mars sample at terrestrial atmospheric conditions while a hardy organism component will examine the effects of a Mars sample under conditions approaching those of the Martian environment. Any deleterious insult on terrestrial metabolism effected by the Mars sample could be indicated long before the sample reached earth proximity.

  14. Thermoluminescence of Apollo 12 lunar samples

    USGS Publications Warehouse

    Doell, Richard R.; Brent, Dalrymple G.

    1971-01-01

    Thermoluminescence (TL) glow curve and decay characteristics of Apollo 12 fines and soil samples are similar to those from Apollo 11. Interpretation of the results from the core sample is difficult because of inadequate sample, spacing, but it appears that the part of the core below about 8 cm has been undisturbed for about 104 years whereas the part of the core above 10 cm may have been disturbed by recent surface activity. TL in the Apollo 12 samples is about twice that in the Apollo 11 samples, suggesting a lower mean daytime surface temperature of a few degrees at the Apollo 12 site. ?? 1971.

  15. Odour sampling 1: Physical chemistry considerations.

    PubMed

    Hudson, N; Ayoko, G A

    2008-07-01

    The selection of an odour sampling device may influence the composition of the resulting odour sample. Limited comparison of emission rates derived from turbulent and essentially quiescent sampling devices confirms that the emission rates derived from these devices are quite different. There is therefore compelling evidence that current odour sampling practice should have greater regard for fundamental physical and chemical principles, the nature of the odour source and the conditions created by the sampling device. Such consideration may identify the most appropriate situations under which the use of these devices may or may not be correct.

  16. Artifacts in magnetic measurements of fluid samples

    NASA Astrophysics Data System (ADS)

    Boekelheide, Z.; Dennis, C. L.

    2016-08-01

    Applications of magnetic fluids are ever increasing, as well as the corresponding need to be able to characterize these fluids in situ. Commercial magnetometers are accurate and well-characterized for solid and powder samples, but their use with fluid samples is more limited. Here, we describe artifacts which can occur in magnetic measurements of fluid samples and their impact. The most critical problem in the measurement of fluid samples is the dynamic nature of the sample position and size/shape. Methods to reduce these artifacts are also discussed, such as removal of air bubbles and dynamic centering.

  17. A New Technique for Sampling Firn Air

    NASA Astrophysics Data System (ADS)

    Perron, F. E.; Dibb, J. E.; Albert, M. R.

    2004-12-01

    The discovery and subsequent interest in photochemical interactions between the polar snowpack and the atmosphere has spawned interest in reliable methods of measuring chemical concentrations in interstitial air. Consistent sampling of the interstitial air in the snowpack had been problematic due to great chemical differences possible from sampling different layers in the snow and the difficulties in acquiring a sample that could serve multiple investigators at the same time. This paper describes a new air sampling device that was developed to solve many of the sampling problems. This new system allows multiple simultaneous chemical analysis of air contained in the pore spaces of the arctic snowpack at unlimited increments from depths of 0 to 150 cm. The three major components are a 4 ft diameter highly UV transmittent acrylic "hood" with a 10 cm rim, a 10 cm diameter casing barrel, and an air probe head. These components operate along with a variety of sub-components that supplement the sampling process. The technique provides for a common sample collection, use for a variety of gases to be sampled, it eliminates short circuit air sampling, provides undisturbed snow for in-situ sampling at multiple sample depths in the same location. The design is discussed and possible extension as a platform for other sensors is described.

  18. Automated sample preparation for CE-SDS.

    PubMed

    Le, M Eleanor; Vizel, Alona; Hutterer, Katariina M

    2013-05-01

    Traditionally, CE with SDS (CE-SDS) places many restrictions on sample composition. Requirements include low salt content, known initial sample concentration, and a narrow window of final sample concentration. As these restrictions require buffer exchange for many sample types, sample preparation is often tedious and yields poor sample recoveries. To improve capacity and streamline sample preparation, an automated robotic platform was developed using the PhyNexus Micro-Extractor Automated Instrument (MEA) for both the reduced and nonreduced CE-SDS assays. This automated sample preparation normalizes sample concentration, removes salts and other contaminants, and adds the required CE-SDS reagents, essentially eliminating manual steps during sample preparation. Fc-fusion proteins and monoclonal antibodies were used in this work to demonstrate benefits of this approach when compared to the manual method. With optimized conditions, this application has demonstrated decreased analyst "hands on" time and reduced total assay time. Sample recovery greater than 90% can be achieved, regardless of initial composition and concentration of analyte.

  19. Materials properties: heterogeneity and appropriate sampling modes.

    PubMed

    Esbensen, Kim H

    2015-01-01

    The target audience for this Special Section comprises parties related to the food and feed sectors, e.g., field samplers, academic and industrial scientists, laboratory personnel, companies, organizations, regulatory bodies, and agencies who are responsible for sampling, as well as project leaders, project managers, quality managers, supervisors, and directors. All these entities face heterogeneous materials, and the characteristics of heterogeneous materials needs to be competently understood by all of them. Before delivering analytical results for decision-making, one form or other of primary sampling is always necessary, which must counteract the effects of the sampling target heterogeneity. Up to five types of sampling error may arise as a specific sampling process interacts with a heterogeneous material; two sampling errors arise because of the heterogeneity of the sampling target, and three additional sampling errors are produced by the sampling process itself-if not properly understood, reduced, and/or eliminated, which is the role of Theory of Sampling. This paper discusses the phenomenon and concepts involved in understanding, describing, and managing the adverse effects of heterogeneity in sampling.

  20. Considerations for sampling contaminants in agricultural soils.

    PubMed

    Ramsey, Charles A

    2015-01-01

    Sampling agricultural soils for contaminants is relatively new. Existing standard sampling protocols used for the evaluation of soil nutrients are likely insufficient for contaminants. The main reasons are the very low analyte levels and differences in heterogeneity between nutrients and contaminants. To evaluate the adequacy of existing sampling protocols or to develop new protocols, a systematic scientific approach is needed. This approach begins with the development of the Sample Quality Criteria followed by a realistic understanding of the properties of the material to be sampled, most notably its heterogeneity. The Sample Quality Criteria and material properties are inputs into the Theory of Sampling. With these inputs, the Theory of Sampling can be used to determine the specifics of the sampling protocol (e.g., mass, number of increments, tool selection) that must be implemented to control error to reliably estimate the concentration of the analyte(s) of interest. Development of sampling protocols in this manner will ensure sample representativeness and therefore improve data equivalency among various parties involved. This is the only way to provide a sound technical basis for defensible decision making to ensure increased safety of food and feed, specifically with respect to contaminants in agricultural soils.

  1. Rotary Mode Core Sample System availability improvement

    SciTech Connect

    Jenkins, W.W.; Bennett, K.L.; Potter, J.D.; Cross, B.T.; Burkes, J.M.; Rogers, A.C.

    1995-02-28

    The Rotary Mode Core Sample System (RMCSS) is used to obtain stratified samples of the waste deposits in single-shell and double-shell waste tanks at the Hanford Site. The samples are used to characterize the waste in support of ongoing and future waste remediation efforts. Four sampling trucks have been developed to obtain these samples. Truck I was the first in operation and is currently being used to obtain samples where the push mode is appropriate (i.e., no rotation of drill). Truck 2 is similar to truck 1, except for added safety features, and is in operation to obtain samples using either a push mode or rotary drill mode. Trucks 3 and 4 are now being fabricated to be essentially identical to truck 2.

  2. Uniform sampling table method and its applications: establishment of a uniform sampling method.

    PubMed

    Chen, Yibin; Chen, Jiaxi; Wang, Wei

    2013-01-01

    A novel uniform sampling method is proposed in this paper. According to the requirements of uniform sampling, we propose the properties that must be met by analyzing the distribution of samples. Based on this, the proposed uniform sampling method is demonstrated and evaluated strictly by mathematical means such as inference. The uniform sampling tables with respect to Cn(t2) and Cn(t3) are established. Furthermore, a one-dimension uniform sampling method and a multidimension method are proposed. The proposed novel uniform sampling method, which is guided by uniform design theory, enjoys the advantages of simplified use and good representativeness of the whole sample.

  3. Air sampling in the workplace. Final report

    SciTech Connect

    Hickey, E.E.; Stoetzel, G.A.; Strom, D.J.; Cicotte, G.R.; Wiblin, C.M.; McGuire, S.A.

    1993-09-01

    This report provides technical information on air sampling that will be useful for facilities following the recommendations in the NRC`s Regulatory Guide 8.25, Revision 1, ``Air sampling in the Workplace.`` That guide addresses air sampling to meet the requirements in NRC`s regulations on radiation protection, 10 CFR Part 20. This report describes how to determine the need for air sampling based on the amount of material in process modified by the type of material, release potential, and confinement of the material. The purposes of air sampling and how the purposes affect the types of air sampling provided are discussed. The report discusses how to locate air samplers to accurately determine the concentrations of airborne radioactive materials that workers will be exposed to. The need for and the methods of performing airflow pattern studies to improve the accuracy of air sampling results are included. The report presents and gives examples of several techniques that can be used to evaluate whether the airborne concentrations of material are representative of the air inhaled by workers. Methods to adjust derived air concentrations for particle size are described. Methods to calibrate for volume of air sampled and estimate the uncertainty in the volume of air sampled are described. Statistical tests for determining minimum detectable concentrations are presented. How to perform an annual evaluation of the adequacy of the air sampling is also discussed.

  4. Preferential sampling in veterinary parasitological surveillance.

    PubMed

    Cecconi, Lorenzo; Biggeri, Annibale; Grisotto, Laura; Berrocal, Veronica; Rinaldi, Laura; Musella, Vincenzo; Cringoli, Giuseppe; Catelan, Dolores

    2016-04-18

    In parasitological surveillance of livestock, prevalence surveys are conducted on a sample of farms using several sampling designs. For example, opportunistic surveys or informative sampling designs are very common. Preferential sampling refers to any situation in which the spatial process and the sampling locations are not independent. Most examples of preferential sampling in the spatial statistics literature are in environmental statistics with focus on pollutant monitors, and it has been shown that, if preferential sampling is present and is not accounted for in the statistical modelling and data analysis, statistical inference can be misleading. In this paper, working in the context of veterinary parasitology, we propose and use geostatistical models to predict the continuous and spatially-varying risk of a parasite infection. Specifically, breaking with the common practice in veterinary parasitological surveillance to ignore preferential sampling even though informative or opportunistic samples are very common, we specify a two-stage hierarchical Bayesian model that adjusts for preferential sampling and we apply it to data on Fasciola hepatica infection in sheep farms in Campania region (Southern Italy) in the years 2013-2014.

  5. Representing and publishing physical sample descriptions

    NASA Astrophysics Data System (ADS)

    Devaraju, Anusuriya; Klump, Jens; Cox, Simon J. D.; Golodoniuc, Pavel

    2016-11-01

    This paper presents a metadata model for physical samples, developed by CSIRO for its role as an allocating agent. The model is essential for connecting various samples to the Web in a systematic manner. It serves as a basis for registering and publishing samples from researchers and laboratories in CSIRO with the International Geo Sample Number (IGSN). The model is simple, extensible and publicly available. We specify how existing controlled vocabularies are incorporated into the model development, and discuss their relevance and limitations. We also describe the mappings between the developed model and existing standards. This is necessary to extend the model's adoption across various science domains. The model has been implemented and tested in the context of two large sample repositories in CSIRO. The results demonstrate the effectiveness of the metadata model while maintaining its flexibility to adapt to various sample types.

  6. Reconstruction of Intensity From Covered Samples

    SciTech Connect

    Barabash, Rozaliya; Watkins, Thomas R; Meisner, Roberta Ann; Burchell, Timothy D; Rosseel, Thomas M

    2015-01-01

    The safe handling of activated samples requires containment and covering the sample to eliminate any potential for contamination. Subsequent characterization of the surface with x-rays ideally necessitates a thin film. While many films appear visually transparent, they are not necessarily x-ray transparent. Each film material has a unique beam attenuation and sometimes have amorphous peaks that can superimpose with those of the sample. To reconstruct the intensity of the underlying activated sample, the x-ray attenuation and signal due to the film needs to be removed from that of the sample. This requires the calculation of unique deconvolution parameters for the film. The development of a reconstruction procedure for a contained/covered sample is described.

  7. Generalized Sampling Theorem for Bandpass Signals

    NASA Astrophysics Data System (ADS)

    Prokes, Ales

    2006-12-01

    The reconstruction of an unknown continuously defined function[InlineEquation not available: see fulltext.] from the samples of the responses of[InlineEquation not available: see fulltext.] linear time-invariant (LTI) systems sampled by the[InlineEquation not available: see fulltext.]th Nyquist rate is the aim of the generalized sampling. Papoulis (1977) provided an elegant solution for the case where[InlineEquation not available: see fulltext.] is a band-limited function with finite energy and the sampling rate is equal to[InlineEquation not available: see fulltext.] times cutoff frequency. In this paper, the scope of the Papoulis theory is extended to the case of bandpass signals. In the first part, a generalized sampling theorem (GST) for bandpass signals is presented. The second part deals with utilizing this theorem for signal recovery from nonuniform samples, and an efficient way of computing images of reconstructing functions for signal recovery is discussed.

  8. Nuclear magnetic resonance properties of lunar samples.

    NASA Technical Reports Server (NTRS)

    Kline, D.; Weeks, R. A.

    1972-01-01

    Nuclear magnetic resonance spectra of Na-23, Al-27, and P-31 in fines samples 10084,60 and 14163,168 and in crystalline rock samples 12021,55 and 14321,166, have been recorded over a range of frequencies up to 20 MHz. A shift in the field at which maximum absorption occurs for all of the spectra relative to the field at which maximum absorption occurs for terrestrial analogues is attributed to a sample-dependent magnetic field at the Na, Al, and P sites opposing the laboratory field. The magnitude of these fields internal to the samples is sample dependent and varies from 5 to 10 G. These fields do not correlate with the iron content of the samples. However, the presence of single-domain particles of iron distributed throughout the plagioclase fraction that contains the principal fraction of Na and Al is inferred from electron magnetic resonance spectra shapes.

  9. Texture synthesis and transfer from multiple samples

    NASA Astrophysics Data System (ADS)

    Qi, Yue; Zhao, Qinping

    2003-09-01

    Texture Mapping plays a very important role in Computer Graphics. Texture Synthesis is one of the main methods to obtain textures, it makes use of sample textures to generate new textures. Texture Transfer is based on Texture Synthesis, it renders objects with textures taken from different objects. Currently, most of Texture Synthesis and Transfer methods use a single sample texture. A method for Texture Synthesis adn Transfer from multi samples was presented. For texture synthesis, the L-shaped neighborhood seaching approach was used. Users specify the proportion of each sample, the number of seed points, and these seed points are scattered randomly according to their samples in horizontal and vertical direction synchronously to synthesize textures. The synthesized textures are very good. For texture transfer, the luminance of the target image and the sample textures are analyzed. This procedure is from coarse to fine, and can produce a visually pleasing result.

  10. Lipid Removal from Human Serum Samples

    PubMed Central

    Castro, Arnold R.; Morrill, William E.; Pope, Victoria

    2000-01-01

    The efficacy of lipid removal from human serum samples obtained by using Cleanascite HC, a commercially available product, was compared to that obtained by the standard chloroform method. Separate samples of 21 frozen, banked human serum samples used in the preparation of samples for proficiency testing were treated with either Cleanascite HC or chloroform. The lipid content was measured before and after treatment. The total percentages of lipid removed ranged from 61 to 70% with Cleanascite HC and from 60 to 62% with chloroform. The advantage of Cleanascite HC over chloroform is based on the simplicity of the procedure with Cleanascite HC without the environmental concerns inherent in the use of chloroform. In 15 serum samples known to contain antibodies to treponemal and nontreponemal syphilis antigens, Cleanascite HC bound some immunoglobulin, but with only minimal loss of reactivity in the serologic tests for syphilis. Cleanascite HC is therefore an acceptable alternative to chloroform for lipid reduction in human serum samples. PMID:10702492

  11. 100 Area Columbia River sediment sampling

    SciTech Connect

    Weiss, S.G.

    1993-09-08

    Forty-four sediment samples were collected from 28 locations in the Hanford Reach of the Columbia River to assess the presence of metals and man-made radionuclides in the near shore and shoreline settings of the Hanford Site. Three locations were sampled upriver of the Hanford Site plutonium production reactors. Twenty-two locations were sampled near the reactors. Three locations were sampled downstream of the reactors near the Hanford Townsite. Sediment was collected from depths of 0 to 6 in. and between 12 to 24 in. below the surface. Samples containing concentrations of metals exceeding the 95 % upper threshold limit values (DOE-RL 1993b) are considered contaminated. Contamination by arsenic, chromium, copper, lead, and zinc was found. Man-made radionuclides occur in all samples except four collected opposite the Hanford Townsite. Man-made radionuclide concentrations were generally less than 1 pCi/g.

  12. Sample Curation at a Lunar Outpost

    NASA Technical Reports Server (NTRS)

    Allen, Carlton C.; Lofgren, Gary E.; Treiman, A. H.; Lindstrom, Marilyn L.

    2007-01-01

    The six Apollo surface missions returned 2,196 individual rock and soil samples, with a total mass of 381.6 kg. Samples were collected based on visual examination by the astronauts and consultation with geologists in the science back room in Houston. The samples were photographed during collection, packaged in uniquely-identified containers, and transported to the Lunar Module. All samples collected on the Moon were returned to Earth. NASA's upcoming return to the Moon will be different. Astronauts will have extended stays at an out-post and will collect more samples than they will return. They will need curation and analysis facilities on the Moon in order to carefully select samples for return to Earth.

  13. Sample Acquisition Techniques for Exobiology Flight Experiments

    NASA Technical Reports Server (NTRS)

    Kojiro, Daniel R.; Carle, Glenn C.; Stratton, David M.; Valentin, Jose R.; DeVincenzi, Donald (Technical Monitor)

    1999-01-01

    Exobiology Flight Experiments involve complex analyses conducted in environments far different than those encountered in terrestrial applications. A major part of the analytical challenge is often the selection, acquisition, delivery and, in some cases, processing of a sample suitable for the analytical requirements of the mission. The added complications of severely limited resources and sometimes rigid time constraints combine to make sample acquisition potentially a major obstacle for successful analyses. Potential samples come in a wide range including planetary atmospheric gas and aerosols (from a wide variety of pressures), planetary soil or rocks, dust and ice particles streaming off of a comet, and cemetery surface ice and rocks. Methods to collect and process sample are often mission specific, requiring continual development of innovative concepts and mechanisms. These methods must also maintain the integrity of the sample for the experimental results to be meaningful. We present here sample acquisition systems employed from past missions and proposed for future missions.

  14. Direct impact aerosol sampling by electrostatic precipitation

    SciTech Connect

    Braden, Jason D.; Harter, Andrew G.; Stinson, Brad J.; Sullivan, Nicholas M.

    2016-02-02

    The present disclosure provides apparatuses for collecting aerosol samples by ionizing an air sample at different degrees. An air flow is generated through a cavity in which at least one corona wire is disposed and electrically charged to form a corona therearound. At least one grounded sample collection plate is provided downstream of the at least one corona wire so that aerosol ions generated within the corona are deposited on the at least one grounded sample collection plate. A plurality of aerosol samples ionized to different degrees can be generated. The at least one corona wire may be perpendicular to the direction of the flow, or may be parallel to the direction of the flow. The apparatus can include a serial connection of a plurality of stages such that each stage is capable of generating at least one aerosol sample, and the air flow passes through the plurality of stages serially.

  15. Ultrahigh density microarrays of solid samples.

    PubMed

    LeBaron, Matthew J; Crismon, Heidi R; Utama, Fransiscus E; Neilson, Lynn M; Sultan, Ahmed S; Johnson, Kevin J; Andersson, Eva C; Rui, Hallgeir

    2005-07-01

    We present a sectioning and bonding technology to make ultrahigh density microarrays of solid samples, cutting edge matrix assembly (CEMA). Maximized array density is achieved by a scaffold-free, self-supporting construction with rectangular array features that are incrementally scalable. This platform technology facilitates arrays of >10,000 tissue features on a standard glass slide, inclusion of unique sample identifiers for improved manual or automated tracking, and oriented arraying of stratified or polarized samples.

  16. Terrestrial contamination in Apollo lunar samples.

    NASA Technical Reports Server (NTRS)

    Flory, D. A.; Simoneit, B. R.

    1972-01-01

    The contamination prevention procedures adopted for controlling the collection, processing, and analysis of the Apollo lunar samples in order to keep them free of significant levels of terrestrial organic matter are described. The organic contaminants actually found in the samples by the various investigators are summarized. It is shown that the program succeeded in providing investigators with samples containing less than 0.1 ppm total contamination.

  17. Innovative methods for inorganic sample preparation

    SciTech Connect

    Essling, A.M.; Huff, E.A.; Graczyk, D.G.

    1992-04-01

    Procedures and guidelines are given for the dissolution of a variety of selected materials using fusion, microwave, and Parr bomb techniques. These materials include germanium glass, corium-concrete mixtures, and zeolites. Emphasis is placed on sample-preparation approaches that produce a single master solution suitable for complete multielement characterization of the sample. In addition, data are presented on the soil microwave digestion method approved by the Environmental Protection Agency (EPA). Advantages and disadvantages of each sample-preparation technique are summarized.

  18. Hanford Sampling Quality Management Plan (HSQMP)

    SciTech Connect

    Hyatt, J.E.

    1995-06-01

    HSQMP establishes quality requirements in response to DOE Order 5700. 6C and to 10 Code of Federal Regulations 830.120. HSQMP is designed to meet the needs of Richland Operations Office for controlling the quality of services provided by sampling operations. It is issued through the Analytical Services Program of the Waste Programs Division. This document describes the Environmental Sampling and Analysis Program activities considered to represent the best management activities necessary to achieve a sampling program with adequate control.

  19. Space X1 First Entry Sample

    NASA Technical Reports Server (NTRS)

    James, John T.

    2012-01-01

    One mini-grab sample container (m-GSC) was returned aboard Space X1 because of the importance of quickly knowing first-entry conditions in this new commercial module. This sample was analyzed alongside samples of the portable clean room (PCR) used in the Space X complex at KSC. The recoveries of C-13-acetone, fluorobenzene, and chlorobenzene from the GSCs averaged 130, 129, and 132 %, respectively.

  20. Apollo-11 lunar sample information catalogue

    NASA Technical Reports Server (NTRS)

    Kramer, F. E. (Compiler); Twedell, D. B. (Compiler); Walton, W. J. A., Jr. (Compiler)

    1977-01-01

    The Apollo 11 mission is reviewed with emphasis on the collection of lunar samples, their geologic setting, early processing, and preliminary examination. The experience gained during five subsequent missions was applied to obtain physical-chemical data for each sample using photographic and binocular microscope techniques. Topics discussed include: binocular examination procedure; breccia clast dexrriptuons, thin section examinations procedure typical breccia in thin section, typical basalt in thin section, sample histories, and chemical and age data. An index to photographs is included.