grain surface roughness: Topics by Science.gov

Sample records for grain surface roughness

Effect of deformation on the thermal conductivity of granular porous media with rough grain surface

NASA Astrophysics Data System (ADS)

Askari, Roohollah; Hejazi, S. Hossein; Sahimi, Muhammad

2017-08-01

Heat transfer in granular porous media is an important phenomenon that is relevant to a wide variety of problems, including geothermal reservoirs and enhanced oil recovery by thermal methods. Resistance to flow of heat in the contact area between the grains strongly influences the effective thermal conductivity of such porous media. Extensive experiments have indicated that the roughness of the grains' surface follows self-affine fractal stochastic functions, and thus, the contact resistance cannot be accounted for by models based on smooth surfaces. Despite the significance of rough contact area, the resistance has been accounted for by a fitting parameter in the models of heat transfer. In this Letter we report on a study of conduction in a packing of particles that contains a fluid of a given conductivity, with each grain having a rough self-affine surface, and is under an external compressive pressure. The deformation of the contact area depends on the fractal dimension that characterizes the grains' rough surface, as well as their Young's modulus. Excellent qualitative agreement is obtained with experimental data. Deformation of granular porous media with grains that have rough self-affine fractal surface is simulated. Thermal contact resistance between grains with rough surfaces is incorporated into the numerical simulation of heat conduction under compressive pressure. By increasing compressive pressure, thermal conductivity is enhanced more in the grains with smoother surfaces and lower Young's modulus. Excellent qualitative agreement is obtained with the experimental data.
The balance between keystone clustering and bed roughness in experimental step-pool stabilization

NASA Astrophysics Data System (ADS)

Johnson, J. P.

2016-12-01

Predicting how mountain channels will respond to environmental perturbations such as floods requires an improved quantitative understanding of morphodynamic feedbacks among bed topography, surface grain size and sediment sorting. In boulder-rich gravel streams, transport and sorting often lead to the development of step pool morphologies, which are expressed both in bed topography and coarse grain clustering. Bed stability is difficult to measure, and is sometimes inferred from the presence of step pools. I use scaled flume experiments to explore feedbacks among surface grain sizes, coarse grain clustering, bed roughness and hydraulic roughness during progressive bed stabilization and over a range of sediment transport rates. While grain clusters are sometimes identified by subjective interpretation, I quantify the degree of coarse surface grain clustering using spatial statistics, including a novel normalization of Ripley's K function. This approach is objective and provides information on the strength of clustering over a range of length scales. Flume experiments start with an initial bed surface with a broad grain size distribution and spatially random positions. Flow causes the bed surface to progressively stabilize in response to erosion, surface coarsening, roughening and grain reorganization. At 95% confidence, many but not all beds stabilized with coarse grains becoming more clustered than complete spatial randomness (CSR). I observe a tradeoff between topographic roughness and clustering. Beds that stabilized with higher degrees of coarse-grain clustering were topographically smoother, and vice-versa. Initial conditions influenced the degree of clustering at stability: Beds that happened to have fewer initial coarse grains had more coarse grain reorganization during stabilization, leading to more clustering. Finally, regressions demonstrate that clustering statistics actually predict hydraulic roughness significantly better than does D84 (the size at which 84% of grains are smaller). In the experimental data, the spatial organization of surface grains is a stronger control on flow characteristics than the size of surface grains.
Plastic strain and grain size effects in the surface roughening of a model aluminum alloy

NASA Astrophysics Data System (ADS)

Moore, Eric Joseph

To address issues surrounding improved automotive fuel economy, an experiment was designed to study the effect of uniaxial plastic tensile deformation on surface roughness and on slip and grain rotation. Electron backscatter diffraction (EBSD) and scanning laser confocal microscopy (SLCM) were used to track grain size, crystallographic texture, and surface topography as a function of incremental true strain for a coarse-grained binary alloy that is a model for AA5xxx series aluminum alloys. One-millimeter thick sheets were heat treated at 425°C to remove previous rolling texture and to grow grains to sizes in the range ˜10-8000 mum. At five different strain levels, 13 sample regions, containing 43 grains, were identified in both EBSD and SLCM micrographs, and crystallographic texture and surface roughness were measured. After heat treatment, a strong cube texture matrix emerged, with bands of generally non-cube grains embedded parallel to the rolling direction (RD). To characterize roughness, height profiles from SLCM micrographs were extracted and a filtered Fourier transform approach was used to separate the profiles into intergranular (long wavelength) and intragranular (short wavelength) signatures. The commonly-used rms roughness parameter (Rq) characterized intragranular results. Two important parameters assess intergranular results in two grain size regimes: surface tilt angle (Deltatheta) and surface height discontinuity (DeltazH) between neighboring grains at a boundary. In general, the magnitude of Rq and Deltatheta increase monotonically with strain and indicate that intergranular roughness is the major contributor to overall surface roughness for true strains up to epsilon = 0.12. Surface height discontinuity DeltazH is defined due to exceptions in surface tilt angle analyses. The range of observed Deltatheta= 1-10° are consistent with the observed 3-12° rotation of individual grains as measured with EBSD. For some grain boundaries with Deltatheta< 4°, the surface height discontinuity DeltazH characterizes the response of adjacent grains in which one or more are large (˜1000-2000 mum), making a 3-12° rotation of the grain highly unlikely. This can be understood by postulating that the energy associated with rotating large grains would exceed the energy to shear along the boundary. Slip and grain boundary shearing are the active mechanisms in these instances.
Surface Roughening Behavior of 6063 Aluminum Alloy during Bulging by Spun Tubes

PubMed Central

Cai, Yang; Wang, Xiaosong; Yuan, Shijian

2017-01-01

Severe surface roughening during the hydroforming of aluminum alloy parts can produce surface defects that severely restrict their application in the automobile and aerospace industry. To understand the relation between strain, grain size and surface roughness under biaxial stress conditions, hydro-bulging tests of aluminum alloy tubes were carried out, and the tubes with different grain sizes were prepared by a spinning and annealing process. The surface roughness was measured by a laser scanning confocal microscope to evaluate the surface roughening macroscopical behavior, and the corresponding microstructures were observed using electron back-scattered diffraction (EBSD) to reveal the roughening microscopic behavior. The results obtained show that the surface roughness increased with both strain and grain size under biaxial stress. No surface defects were observed on the surface when the grain size was less than 105 μm if the strain was less than 18%, or when the grain size was between 130 and 175 μm if the strain was less than 15.88% and 7.15%, respectively. The surface roughening microscopic behavior was identified as an inhomogeneous grain size distribution, which became more pronounced with increasing grain size and resulted in greater local deformation. Concentrated grain orientation also results in severe inhomogeneous deformation during plastics deformation, and serious surface roughening. PMID:28772658
Laser Surface Modification of H13 Die Steel using Different Laser Spot Sizes

NASA Astrophysics Data System (ADS)

Aqida, S. N.; Naher, S.; Brabazon, D.

2011-05-01

This paper presents a laser surface modification process of AISI H13 tool steel using three sizes of laser spot with an aim to achieve reduced grain size and surface roughness. A Rofin DC-015 diffusion-cooled CO2 slab laser was used to process AISI H13 tool steel samples. Samples of 10 mm diameter were sectioned to 100 mm length in order to process a predefined circumferential area. The parameters selected for examination were laser peak power, overlap percentage and pulse repetition frequency (PRF). Metallographic study and image analysis were done to measure the grain size and the modified surface roughness was measured using two-dimensional surface profilometer. From metallographic study, the smallest grain sizes measured by laser modified surface were between 0.51 μm and 2.54 μm. The minimum surface roughness, Ra, recorded was 3.0 μm. This surface roughness of the modified die steel is similar to the surface quality of cast products. The grain size correlation with hardness followed the findings correlate with Hall-Petch relationship. The potential found for increase in surface hardness represents an important method to sustain tooling life.
Modeling and evaluating of surface roughness prediction in micro-grinding on soda-lime glass considering tool characterization

NASA Astrophysics Data System (ADS)

Cheng, Jun; Gong, Yadong; Wang, Jinsheng

2013-11-01

The current research of micro-grinding mainly focuses on the optimal processing technology for different materials. However, the material removal mechanism in micro-grinding is the base of achieving high quality processing surface. Therefore, a novel method for predicting surface roughness in micro-grinding of hard brittle materials considering micro-grinding tool grains protrusion topography is proposed in this paper. The differences of material removal mechanism between convention grinding process and micro-grinding process are analyzed. Topography characterization has been done on micro-grinding tools which are fabricated by electroplating. Models of grain density generation and grain interval are built, and new predicting model of micro-grinding surface roughness is developed. In order to verify the precision and application effect of the surface roughness prediction model proposed, a micro-grinding orthogonally experiment on soda-lime glass is designed and conducted. A series of micro-machining surfaces which are 78 nm to 0.98 μm roughness of brittle material is achieved. It is found that experimental roughness results and the predicting roughness data have an evident coincidence, and the component variable of describing the size effects in predicting model is calculated to be 1.5×107 by reverse method based on the experimental results. The proposed model builds a set of distribution to consider grains distribution densities in different protrusion heights. Finally, the characterization of micro-grinding tools which are used in the experiment has been done based on the distribution set. It is concluded that there is a significant coincidence between surface prediction data from the proposed model and measurements from experiment results. Therefore, the effectiveness of the model is demonstrated. This paper proposes a novel method for predicting surface roughness in micro-grinding of hard brittle materials considering micro-grinding tool grains protrusion topography, which would provide significant research theory and experimental reference of material removal mechanism in micro-grinding of soda-lime glass.
The Relationship Between Microscopic Grain Surface Structure and the Dynamic Capillary-Driven Advance of Water Films over Individual Dry Natural Sand Grains

NASA Astrophysics Data System (ADS)

Kibbey, T. C. G.; Adegbule, A.; Yan, S.

2017-12-01

The movement of nonvolatile solutes in unsaturated porous media at low water contents depends on transport in surface-associated water films. The focus of the work described here was on studying solute movement in water films advancing by capillary forces over initially-dry grain surfaces, to understand how microscopic surface roughness features influence the initial velocity of water film advance. For this work, water containing a non-adsorbing conservative tracer was used to track the movement of advancing water films. A stainless steel capillary tube connected to an external reservoir a fixed distance below the grain surface was used to transmit solution to the grain surface under negative pressure (positive capillary pressure), consistent with conditions that might be expected in the unsaturated zone. The small internal diameter of the capillary prevents solution from draining out of the capillary back into the reservoir. When the capillary is contacted with a grain surface, capillary forces that result from contact between the fluid and the rough grain surface cause water films to wick across the grain surface. Multiple experiments were conducted on the same grain, rotating the grain and varying the capillary contact point around the circumference of the grain. Imaging was conducted at fixed intervals using an automated Extended Depth of Field (EDF) imaging system, and images were analyzed to determine initial velocity. Grain surfaces were then characterized through scanning electron microscope (SEM) imaging, using a hybrid stereoscopic reconstruction method designed to extract maximum detail in creating elevation maps of geologic surfaces from tilted pairs of SEM images. The resulting elevation maps were used to relate surface roughness profiles around the grain with initial velocities. Results suggest that velocity varies significant with contact point around an individual grain, and correlates quantitatively with the local grain surface structure. Preliminary simulation results will also be discussed.
The coevolution of bed roughness, grain clustering, surface armoring, hydraulic roughness, and sediment transport rate in experimental coarse alluvial channels: implications for long-term effects of gravel augmentation

NASA Astrophysics Data System (ADS)

Johnson, J. P.; Aronovitz, A. C.

2012-12-01

We conducted laboratory flume experiments to quantify changes in multiple factors leading to mountain river bed stability (i.e., minimal bed changes in space and time), and to understand how stable beds respond to perturbations in sediment supply. Experiments were run in a small flume 4 m long by 0.1 m wide. We imposed an initial well-graded size distribution of sediment (from coarse sand to up to 4 cm clasts), a steady water discharge (0.9 L/s), and initial bed surface slopes (8% and 12%). We measured outlet sediment flux and size distribution, bed topography and surface size distributions, and water depths; from these we calculated total shear stress, form drag and skin friction stress partitioning, and hydraulic roughness. The bed was initially allowed to stabilize with no imposed upstream sediment flux. This stabilization occurred due to significant changes in all of the factors listed in the title, and resulted in incipient step-pool like bed morphologies. In addition, this study was designed to explore possible long-term effects of gravel augmentation on mountain channel morphology and surface grain size. While the short-term goal of gravel augmentation is usually to cause fining of surface sediment patches, we find that the long-term effects may be opposite. We perturbed the stabilized channels by temporarily imposing an upstream sediment flux of the finest sediment size fraction (sand to granules). Median surface sizes initially decreased due to fine sediment deposition, although transport rates of intermediate-sized grains increased. When the fine sediment supply was stopped, beds evolved to be both rougher and coarser than they had been previously, because the largest grains remained on the bed but intermediate-sized grains were preferentially transported out, leaving higher fractions of larger grains on the surface. Existing models for mixed grain size transport actually predict changes in mobilization reasonably well, but do not explicity account for surface roughness evolution. Our results indicate a nonlinear relationship between surface median grain size and bed roughness.
Can high resolution topographic surveys provide reliable grain size estimates?

NASA Astrophysics Data System (ADS)

Pearson, Eleanor; Smith, Mark; Klaar, Megan; Brown, Lee

2017-04-01

High resolution topographic surveys contain a wealth of information that is not always exploited in the generation of Digital Elevation Models (DEMs). In particular, several authors have related sub-grid scale topographic variability (or 'surface roughness') to particle grain size by deriving empirical relationships between the two. Such relationships would permit rapid analysis of the spatial distribution of grain size over entire river reaches, providing data to drive distributed hydraulic models and revolutionising monitoring of river restoration projects. However, comparison of previous roughness-grain-size relationships shows substantial variability between field sites and do not take into account differences in patch-scale facies. This study explains this variability by identifying the factors that influence roughness-grain-size relationships. Using 275 laboratory and field-based Structure-from-Motion (SfM) surveys, we investigate the influence of: inherent survey error; irregularity of natural gravels; particle shape; grain packing structure; sorting; and form roughness on roughness-grain-size relationships. A suite of empirical relationships is presented in the form of a decision tree which improves estimations of grain size. Results indicate that the survey technique itself is capable of providing accurate grain size estimates. By accounting for differences in patch facies, R2 was seen to improve from 0.769 to R2 > 0.9 for certain facies. However, at present, the method is unsuitable for poorly sorted gravel patches. In future, a combination of a surface roughness proxy with photosieving techniques using SfM-derived orthophotos may offer improvements on using either technique individually.
Controlling Surface Chemistry to Deconvolute Corrosion Benefits Derived from SMAT Processing

NASA Astrophysics Data System (ADS)

Murdoch, Heather A.; Labukas, Joseph P.; Roberts, Anthony J.; Darling, Kristopher A.

2017-07-01

Grain refinement through surface plastic deformation processes such as surface mechanical attrition treatment has shown measureable benefits for mechanical properties, but the impact on corrosion behavior has been inconsistent. Many factors obfuscate the particular corrosion mechanisms at work, including grain size, but also texture, processing contamination, and surface roughness. Many studies attempting to link corrosion and grain size have not been able to decouple these effects. Here we introduce a preprocessing step to mitigate the surface contamination effects that have been a concern in previous corrosion studies on plastically deformed surfaces; this allows comparison of corrosion behavior across grain sizes while controlling for texture and surface roughness. Potentiodynamic polarization in aqueous NaCl solution suggests that different corrosion mechanisms are responsible for samples prepared with the preprocessing step.
Effects of hydraulic roughness on surface textures of gravel-bed rivers

Treesearch

John M. Buffington; David R. Montgomery

1999-01-01

Field studies of forest gravel-bed rivers in northwestern Washington and southeastern Alaska demonstrate that bed-surface grain size is responsive to hydraulic roughness caused by bank irregularities, bars, and wood debris. We evaluate textural response by comparing reach-average median grain size (D50) to that predicted from the total bank-full boundary shear stress (...
Interactions of light with rough dielectric surfaces - Spectral reflectance and polarimetric properties

NASA Technical Reports Server (NTRS)

Yon, S. A.; Pieters, C. M.

1988-01-01

The nature of the interactions of visible and NIR radiation with the surfaces of rock and mineral samples was investigated by measuring the reflectance and the polarization properties of scattered and reflected light for slab samples of obsidian and fine-grained basalt, prepared to controlled surface roughness. It is shown that the degree to which radiation can penetrate a surface and then scatter back out, an essential criterion for mineralogic determinations based on reflectance spectra, depends not only upon the composition of the material, but also on its physical condition such as sample grain size and surface roughness. Comparison of the experimentally measured reflectance and polarization from smooth and rough slab materials with the predicted models indicates that single Fresnel reflections are responsible for the largest part of the reflected intensity resulting from interactions with the surfaces of dielectric materials; multiple Fresnel reflections are much less important for such surfaces.
Effect of Young's Modulus and Surface Roughness on the Inter-Particle Friction of Granular Materials.

PubMed

Sandeep, Chitta Sai; Senetakis, Kostas

2018-01-31

In the study we experimentally examine the influence of elastic properties and surface morphology on the inter-particle friction of natural soil grains. The experiments are conducted with a custom-built micromechanical apparatus and the database is enhanced by testing engineered-reference grains. Naturally-occurring geological materials are characterized by a wide spectrum of mechanical properties (e.g., Young's modulus) and surface morphology (e.g., roughness), whereas engineered grains have much more consistent characteristics. Comparing to engineered materials, geological materials are found to display more pronounced initial plastic behavior during compression. Under the low normal load range applied in the study, between 1 and 5 N, we found that the frictional force is linearly correlated with the applied normal load, but we acknowledge that the data are found more scattered for natural soil grains, especially for rough and weathered materials which have inconsistent characteristics. The inter-particle coefficient of friction is found to be inversely correlated with the Young's modulus and the surface roughness. These findings are important in geophysical and petroleum engineering contents, since a number of applications, such as landslides and granular flows, hydraulic fracturing using proppants, and weathering process of cliffs, among others, can be simulated using discrete numerical methods. These methods employ contact mechanics properties at the grain scale and the inter-particle friction is one of these critical components. It is stressed in our study that friction is well correlated with the elastic and morphological characteristics of the grains.
Effect of Process Variables on the Grain Size and Crystallographic Texture of Hot-Dip Galvanized Coatings

NASA Astrophysics Data System (ADS)

Kaboli, Shirin; McDermid, Joseph R.

2014-08-01

A galvanizing simulator was used to determine the effect of galvanizing bath antimony (Sb) content, substrate surface roughness, and cooling rate on the microstructural development of metallic zinc coatings. Substrate surface roughness was varied through the use of relatively rough hot-rolled and relatively smooth bright-rolled steels, cooling rates were varied from 0.1 to 10 K/s, and bulk bath Sb levels were varied from 0 to 0.1 wt pct. In general, it was found that increasing bath Sb content resulted in coatings with a larger grain size and strongly promoted the development of coatings with the close-packed {0002} basal plane parallel to the substrate surface. Increasing substrate surface roughness tended to decrease the coating grain size and promoted a more random coating crystallographic texture, except in the case of the highest Sb content bath (0.1 wt pct Sb), where substrate roughness had no significant effect on grain size except at higher cooling rates (10 K/s). Increased cooling rates tended to decrease the coating grain size and promote the {0002} basal orientation. Calculations showed that increasing the bath Sb content from 0 to 0.1 wt pct Sb increased the dendrite tip growth velocity from 0.06 to 0.11 cm/s by decreasing the solid-liquid interface surface energy from 0.77 to 0.45 J/m2. Increased dendrite tip velocity only partially explains the formation of larger zinc grains at higher Sb levels. It was also found that the classic nucleation theory cannot completely explain the present experimental observations, particularly the effect of increasing the bath Sb, where the classical theory predicts increased nucleation and a finer grain size. In this case, the "poisoning" theory of nucleation sites by segregated Sb may provide a partial explanation. However, any analysis is greatly hampered by the lack of fundamental thermodynamic information such as partition coefficients and surface energies and by a lack of fundamental structural studies. Overall, it was concluded that the fundamental mechanisms behind the microstructural development of solidified metallic zinc coatings have yet to be completely elucidated and require further investigation.
An Explanation for Bends of 1-Dimensional Nanorods

NASA Astrophysics Data System (ADS)

Mukaida, Masashi; Ichinose, Ataru; Mele, Paolo; Mtsumoto, Kaname; Horii, Shigeru; Yoshida, Yutaka

Growth of artificial pinning centers (APCs) in YBa2Cu3O7-J (YBCO) films are discussed. The APCs used in this research are BaZrO3 and BaSnO3 nanorods which are reported by Mele et al. TEM images show these nanorods graduallybend accordinglywith approachingtoasurfaceof films. This featureshowedagrowth patternlikeafirework. Weexplainthe featureofthe nanorodsas follows;Atanearlygrowth stage, filmsgrowinalayerbylayergrowth mode. The surface of the films is flat and very smooth. After the early growth stage, the film surface gradually becomes rough, indicating the film grows in a Stranski-Krastanov growth mode. This roughness was caused by a spiral growth of films with manysteps. At the step of YBCO films, nanorod materials such as BaZrO3 are supplied from one direction. Then, the center of nanorods sifts to the same direction of the step flow. Then, the nanorods bend to the edge of the grains in the films. As a grain in spiral growth had a convex surface, nanorods bent to the direction perpendicular to the grain surface. Finally, nanorods in rough grains form firework structures.
The evolution of fracture surface roughness and its dependence on slip

NASA Astrophysics Data System (ADS)

Wells, Olivia L.

Under effective compression, impingement of opposing rough surfaces of a fracture can force the walls of the fracture apart during slip. Therefore, a fracture's surface roughness exerts a primary control on the amount of dilation that can be sustained on a fracture since the opposing surfaces need to remain in contact. Previous work has attempted to characterize fracture surface roughness through topographic profiles and power spectral density analysis, but these metrics describing the geometry of a fracture's surface are often non-unique when used independently. However, when combined these metrics are affective at characterizing fracture surface roughness, as well as the mechanisms affecting changes in roughness with increasing slip, and therefore changes in dilation. These mechanisms include the influence of primary grains and pores on initial fracture roughness, the effect of linkage on locally increasing roughness, and asperity destruction that limits the heights of asperities and forms gouge. This analysis reveals four essential stages of dilation during the lifecycle of a natural fracture, whereas previous slip-dilation models do not adequately address the evolution of fracture surface roughness: (1) initial slip companied by small dilation is mediated by roughness controlled by the primary grain and pore dimensions; (2) rapid dilation during and immediately following fracture growth by linkage of formerly isolated fractures; (3) wear of the fracture surface and gouge formation that minimizes dilation; and (4) between slip events cementation that modifies the mineral constituents in the fracture. By identifying these fundamental mechanisms that influence fracture surface roughness, this new conceptual model relating dilation to slip has specific applications to Enhanced Geothermal Systems (EGS), which attempt to produce long-lived dilation in natural fractures by inducing slip.
Effects of hydraulic roughness on surface textures of gravel‐bed rivers

USGS Publications Warehouse

Buffington, John M.; Montgomery, David R.

1999-01-01

Field studies of forest gravel‐bed rivers in northwestern Washington and southeastern Alaska demonstrate that bed‐surface grain size is responsive to hydraulic roughness caused by bank irregularities, bars, and wood debris. We evaluate textural response by comparing reach‐average median grain size (D50) to that predicted from the total bank‐full boundary shear stress (т0bf), representing a hypothetical reference condition of low hydraulic roughness. For a given т0bf, channels with progressively greater hydraulic roughness have systematically finer bed surfaces, presumably due to reduced bed shear stress, resulting in lower channel competence and diminished bed load transport capacity, both of which promote textural fining. In channels with significant hydraulic roughness, observed values D50 can be up to 90% smaller than those predicted from т0bf. We find that wood debris plays an important role at our study sites, not only providing hydraulic roughness but also influencing pool spacing, frequency of textural patches, and the amplitude and wavelength of bank and bar topography and their consequent roughness. Our observations also have biological implications. We find that textural fining due to hydraulic roughness can create usable salmonid spawning gravels in channels that otherwise would be too coarse.
The evolution of slip surface roughness during earthquake propagation in carbonate faults

NASA Astrophysics Data System (ADS)

Zhu, B.; De Paola, N.; Llewellin, E. W.; Holdsworth, R.

2014-12-01

Slip surface roughness is understood to control the dynamics of earthquake propagation. Quantifying the micro- and nano-scale roughness of slip surfaces can give insight into the grain-scale processes controlling the strength of faults during earthquake propagation. Friction experiments were performed on fine-grained calcite gouges, at speed 1 ms-1, normal stress 18 MPa, displacements 0.009-1.46 m, and room temperature and humidity. Results show a two stage-evolution (S1-2) of the fault strength, with an initial increase up to peak value 0.82 (S1), followed by a sudden decrease to a low, steady-state value 0.18 (S2). Samples retrieved at the end of S1 show the development of a cohesive slip zone (SZ), made of micron-scale, angular clasts formed by brittle fracturing and cataclasis. The SZ of samples deformed up to S2, is composed of nanograin aggregates which exhibit polygonal grain boundaries indicating high temperature grain boundary sliding creep deformation. In both cases, the SZ is bounded by a sharply defined slip surface. The 3-D geometry of seven experimental slip surfaces (40μm×40μm) has been reconstructed by digital processing of sets of 1800 images of SZ cross sections acquired at 20 nm intervals perpendicular to the slip direction, using a slicing (Focussed Ion Beam) and viewing (Field Emission Scanning Electron Microscope) technique. Spectrum power density analyses show that nano- and micron-scale slip surface roughness is anisotropic for both S1 and S2 slip surfaces. At the nano- and micron-scale, root mean square values decrease with length for S1 slip surfaces, but only slightly for S2 surfaces, and are anisotropic in the slip-normal and slip-parallel directions. The anisotropy is reduced at the nano-scale, although S2 slip surfaces are still smoother parallel to slip than normal to slip. Hurst exponents vary through scales, and are anisotropic in the directions parallel and normal to slip. Variable Hurst exponents indicate that slip surface roughness is scale-dependent with anisotropic, not self-affine behaviour at the micro/nano-scale, in contrast to the self-affine behaviour inferred at the mm to km scales. Dynamic weakening and creep deformation, observed during S2, coincide with an evolution towards less anisotropic and scale-dependent slip surface roughness at the nanoscale.
Addressing scale dependence in roughness and morphometric statistics derived from point cloud data.

NASA Astrophysics Data System (ADS)

Buscombe, D.; Wheaton, J. M.; Hensleigh, J.; Grams, P. E.; Welcker, C. W.; Anderson, K.; Kaplinski, M. A.

2015-12-01

The heights of natural surfaces can be measured with such spatial density that almost the entire spectrum of physical roughness scales can be characterized, down to the morphological form and grain scales. With an ability to measure 'microtopography' comes a demand for analytical/computational tools for spatially explicit statistical characterization of surface roughness. Detrended standard deviation of surface heights is a popular means to create continuous maps of roughness from point cloud data, using moving windows and reporting window-centered statistics of variations from a trend surface. If 'roughness' is the statistical variation in the distribution of relief of a surface, then 'texture' is the frequency of change and spatial arrangement of roughness. The variance in surface height as a function of frequency obeys a power law. In consequence, roughness is dependent on the window size through which it is examined, which has a number of potential disadvantages: 1) the choice of window size becomes crucial, and obstructs comparisons between data; 2) if windows are large relative to multiple roughness scales, it is harder to discriminate between those scales; 3) if roughness is not scaled by the texture length scale, information on the spacing and clustering of roughness `elements' can be lost; and 4) such practice is not amenable to models describing the scattering of light and sound from rough natural surfaces. We discuss the relationship between roughness and texture. Some useful parameters which scale vertical roughness to characteristic horizontal length scales are suggested, with examples of bathymetric point clouds obtained using multibeam from two contrasting riverbeds, namely those of the Colorado River in Grand Canyon, and the Snake River in Hells Canyon. Such work, aside from automated texture characterization and texture segmentation, roughness and grain size calculation, might also be useful for feature detection and classification from point clouds.
Roughness topographical effects on mean momentum and stress budgets in developed turbulent channel flows

NASA Astrophysics Data System (ADS)

Aghaei Jouybari, Mostafa; Yuan, Junlin

2017-11-01

Direct numerical simulations of turbulent channel flows are carried out over two surfaces: a synthesized sand-grain surface and a realistic turbine roughness that is characterized by more prominent large-scale surface features. To separate the effects of wall-normal variation of the roughness area fraction from the (true) variation of flow statistics, the governing equations are area-averaged using intrinsic averaging, contrary to the usually practice based on the total area (i.e., superficial averaging). Additional terms appear in the mean-momentum equation resulted from the wall-normal variation of the solid fraction and play a role in the near-wall balance. Results from surfaces with a step solidity function (e.g., cubes) will also be discussed. Compared to the sand grains, the turbine surface generates stronger form-induced fluctuations, despite weaker dispersive shear stress. This is associated with more significant form-induced productions (comparable to shear production) in Reynolds stress budgets, weaker pressure work, and, consequently, more anisotropic redistribution of turbulent kinetic energy in the roughness sublayer, which potentially leads to different turbulent responses between the two surfaces in non-equilibrium flows.

Numerical analysis of the effect of surface roughness on mechanical fields in polycrystalline aggregates

NASA Astrophysics Data System (ADS)

Guilhem, Yoann; Basseville, Stéphanie; Curtit, François; Stéphan, Jean-Michel; Cailletaud, Georges

2018-06-01

This paper is dedicated to the study of the influence of surface roughness on local stress and strain fields in polycrystalline aggregates. Finite element computations are performed with a crystal plasticity model on a 316L stainless steel polycrystalline material element with different roughness states on its free surface. The subsequent analysis of the plastic strain localization patterns shows that surface roughness strongly affects the plastic strain localization induced by crystallography. Nevertheless, this effect mainly takes place at the surface and vanishes under the first layer of grains, which implies the existence of a critical perturbed depth. A statistical analysis based on the plastic strain distribution obtained for different roughness levels provides a simple rule to define the size of the affected zone depending on the rough surface parameters.
The Effect of Humidity and Particle Characteristics on Friction and Stick-slip Instability in Granular Fault Gouge

NASA Astrophysics Data System (ADS)

Anthony, J. L.; Marone, C. J.

2003-12-01

Previous studies have shown that particle characteristics such as shape, dimension, and roughness affect friction in granular shear zones. Other work shows that humidity plays a key role in frictional healing and rate/state dependence within granular gouge. In order to improve our understanding of grain-scale deformation mechanisms within fault gouge, we performed laboratory experiments using a double-direct-shear testing apparatus. This assembly includes three rigid forcing blocks with two gouge layers sandwiched between rough or smooth surfaces. Roughened surfaces were triangular grooves 0.8 mm deep and 1 mm wavelength. These promote distributed shear throughout the layer undergoing cataclastic deformation. Smooth surfaces were mirror-finished hardened steel and were used to promote and isolate grain boundary sliding. The center block is forced at controlled displacement rate between the two side blocks to create frictional shear. We studied gouge layers 3-7 mm thick, consisting of either quartz rods sheared in 1-D and 2-D configurations and smooth glass beads mixed with varying amounts of rough sand particles. We report on particle diameters that range from 0.050-0.210 mm, and quartz rods 1 mm in diameter and 100 mm long. The experiments are run at room temperature, controlled relative humidity ranging from 5 to 100%, and shear displacement rates from 0.1 to 300 microns per second. Experiments are carried out under a normal stress of 5 MPa, a non-fracture loading regime where sliding friction for smooth spherical particles is measurably lower than for rough angular particles. We compare results from shear between smooth boundaries, where we hypothesize that grain boundary sliding is the mechanism influencing granular friction, to rough sample experiments where shear undergoes a transition from distributed, pervasive shear to progressively localized as a function of increasing strain. For shear within rough surfaces, stick-slip instability occurs in gouge that consists of less than 30% angular grains and begins once the coefficient of friction (shear stress divided by normal stress) reaches a value of 0.35-0.40. Peak friction during stick-slip cycles is 0.40-0.45. Each stick-slip event involves a small amount of quasi-static displacement prior to failure, which we refer to as pre-seismic slip. For unstable sliding regimes, we measure the amount of pre-seismic slip and the magnitude of dynamic stress drop. These parameters vary systematically with sliding velocity, particle characteristics, and bounding roughness. For shear within smooth surfaces, friction is very low (0.15-0.16 for spherical particles) and sliding is stable, without stick-slip instability. As more angular grains are mixed with spherical beads the coefficient of friction increases. This holds true for both the rough and smooth sample experiments. We expand on previous work done by Frye and Marone 2002 (JGR) to study the effect of humidity on 1-D, 2-D, and 3-D gouge layer configurations. Our data show that humidity has a significant effect on frictional strength and stability and that this effect is observed for both smooth surfaces, where grain boundary sliding is the dominant deformation mechanisms, and for shear within rough surfaces where gouge deformation occurs by rolling, dilation, compaction, and grain boundary sliding.
Investigation of quartz grain surface textures by atomic force microscopy for forensic analysis.

PubMed

Konopinski, D I; Hudziak, S; Morgan, R M; Bull, P A; Kenyon, A J

2012-11-30

This paper presents a study of quartz sand grain surface textures using atomic force microscopy (AFM) to image the surface. Until now scanning electron microscopy (SEM) has provided the primary technique used in the forensic surface texture analysis of quartz sand grains as a means of establishing the provenance of the grains for forensic reconstructions. The ability to independently corroborate the grain type classifications is desirable and provides additional weight to the findings of SEM analysis of the textures of quartz grains identified in forensic soil/sediment samples. AFM offers a quantitative means of analysis that complements SEM examination, and is a non-destructive technique that requires no sample preparation prior to scanning. It therefore has great potential to be used for forensic analysis where sample preservation is highly valuable. By taking quantitative topography scans, it is possible to produce 3D representations of microscopic surface textures and diagnostic features for examination. Furthermore, various empirical measures can be obtained from analysing the topography scans, including arithmetic average roughness, root-mean-square surface roughness, skewness, kurtosis, and multiple gaussian fits to height distributions. These empirical measures, combined with qualitative examination of the surfaces can help to discriminate between grain types and provide independent analysis that can corroborate the morphological grain typing based on the surface textures assigned using SEM. Furthermore, the findings from this study also demonstrate that quartz sand grain surfaces exhibit a statistically self-similar fractal nature that remains unchanged across scales. This indicates the potential for a further quantitative measure that could be utilised in the discrimination of quartz grains based on their provenance for forensic investigations. Copyright © 2012 Elsevier Ireland Ltd. All rights reserved.
Can high resolution 3D topographic surveys provide reliable grain size estimates in gravel bed rivers?

NASA Astrophysics Data System (ADS)

Pearson, E.; Smith, M. W.; Klaar, M. J.; Brown, L. E.

2017-09-01

High resolution topographic surveys such as those provided by Structure-from-Motion (SfM) contain a wealth of information that is not always exploited in the generation of Digital Elevation Models (DEMs). In particular, several authors have related sub-metre scale topographic variability (or 'surface roughness') to sediment grain size by deriving empirical relationships between the two. In fluvial applications, such relationships permit rapid analysis of the spatial distribution of grain size over entire river reaches, providing improved data to drive three-dimensional hydraulic models, allowing rapid geomorphic monitoring of sub-reach river restoration projects, and enabling more robust characterisation of riverbed habitats. However, comparison of previously published roughness-grain-size relationships shows substantial variability between field sites. Using a combination of over 300 laboratory and field-based SfM surveys, we demonstrate the influence of inherent survey error, irregularity of natural gravels, particle shape, grain packing structure, sorting, and form roughness on roughness-grain-size relationships. Roughness analysis from SfM datasets can accurately predict the diameter of smooth hemispheres, though natural, irregular gravels result in a higher roughness value for a given diameter and different grain shapes yield different relationships. A suite of empirical relationships is presented as a decision tree which improves predictions of grain size. By accounting for differences in patch facies, large improvements in D50 prediction are possible. SfM is capable of providing accurate grain size estimates, although further refinement is needed for poorly sorted gravel patches, for which c-axis percentiles are better predicted than b-axis percentiles.
Rough SERS substrate based on gold coated porous silicon layer prepared on the silicon backside surface

NASA Astrophysics Data System (ADS)

Dridi, H.; Haji, L.; Moadhen, A.

2017-04-01

We report in this paper a novel method to elaborate rough Surface Enhanced Raman Scattering (SERS) substrate. A single layer of porous silicon was formed on the silicon backside surface. Morphological characteristics of the porous silicon layer before and after gold deposition were influenced by the rough character (gold size). The reflectance measurements showed a dependence of the gold nano-grains size on the surface nature, through the Localized Surface Plasmon (LSP) band properties. SERS signal of Rhodamine 6G used as a model analyte, adsorbed on the rough porous silicon layer revealed a marked enhancement of its vibrational modes intensities.
Resistivity scaling and electron relaxation times in metallic nanowires

DOE Office of Scientific and Technical Information (OSTI.GOV)

Moors, Kristof, E-mail: kristof@itf.fys.kuleuven.be; Imec, Kapeldreef 75, B-3001 Leuven; Sorée, Bart

2014-08-14

We study the resistivity scaling in nanometer-sized metallic wires due to surface roughness and grain-boundaries, currently the main cause of electron scattering in nanoscaled interconnects. The resistivity has been obtained with the Boltzmann transport equation, adopting the relaxation time approximation of the distribution function and the effective mass approximation for the conducting electrons. The relaxation times are calculated exactly, using Fermi's golden rule, resulting in a correct relaxation time for every sub-band state contributing to the transport. In general, the relaxation time strongly depends on the sub-band state, something that remained unclear with the methods of previous work. The resistivitymore » scaling is obtained for different roughness and grain-boundary properties, showing large differences in scaling behavior and relaxation times. Our model clearly indicates that the resistivity is dominated by grain-boundary scattering, easily surpassing the surface roughness contribution by a factor of 10.« less
Using UAS optical imagery and SfM photogrammetry to characterize the surface grain size of gravel bars in a braided river (Vénéon River, French Alps)

NASA Astrophysics Data System (ADS)

Vázquez-Tarrío, Daniel; Borgniet, Laurent; Liébault, Frédéric; Recking, Alain

2017-05-01

This paper explores the potential of unmanned aerial system (UAS) optical aerial imagery to characterize grain roughness and size distribution in a braided, gravel-bed river (Vénéon River, French Alps). With this aim in view, a Wolman field campaign (19 samples) and five UAS surveys were conducted over the Vénéon braided channel during summer 2015. The UAS consisted of a small quadcopter carrying a GoPro camera. Structure-from-Motion (SfM) photogrammetry was used to extract dense and accurate three-dimensional point clouds. Roughness descriptors (roughness heights, standard deviation of elevation) were computed from the SfM point clouds and were correlated with the median grain size of the Wolman samples. A strong relationship was found between UAS-SfM-derived grain roughness and Wolman grain size. The procedure employed has potential for the rapid and continuous characterization of grain size distribution in exposed bars of gravel-bed rivers. The workflow described in this paper has been successfully used to produce spatially continuous grain size information on exposed gravel bars and to explore textural changes following flow events.
Influence of Structural Features and Fracture Processes on Surface Roughness: A Case Study from the Krosno Sandstones of the Górka-Mucharz Quarry (Little Beskids, Southern Poland)

NASA Astrophysics Data System (ADS)

Pieczara, Łukasz

2015-09-01

The paper presents the results of analysis of surface roughness parameters in the Krosno Sandstones of Mucharz, southern Poland. It was aimed at determining whether these parameters are influenced by structural features (mainly the laminar distribution of mineral components and directional distribution of non-isometric grains) and fracture processes. The tests applied in the analysis enabled us to determine and describe the primary statistical parameters used in the quantitative description of surface roughness, as well as specify the usefulness of contact profilometry as a method of visualizing spatial differentiation of fracture processes in rocks. These aims were achieved by selecting a model material (Krosno Sandstones from the Górka-Mucharz Quarry) and an appropriate research methodology. The schedule of laboratory analyses included: identification analyses connected with non-destructive ultrasonic tests, aimed at the preliminary determination of rock anisotropy, strength point load tests (cleaved surfaces were obtained due to destruction of rock samples), microscopic analysis (observation of thin sections in order to determine the mechanism of inducing fracture processes) and a test method of measuring surface roughness (two- and three-dimensional diagrams, topographic and contour maps, and statistical parameters of surface roughness). The highest values of roughness indicators were achieved for surfaces formed under the influence of intragranular fracture processes (cracks propagating directly through grains). This is related to the structural features of the Krosno Sandstones (distribution of lamination and bedding).
Size effects and charge transport in metals: Quantum theory of the resistivity of nanometric metallic structures arising from electron scattering by grain boundaries and by rough surfaces

NASA Astrophysics Data System (ADS)

Munoz, Raul C.; Arenas, Claudio

2017-03-01

We discuss recent progress regarding size effects and their incidence upon the coefficients describing charge transport (resistivity, magnetoresistance, and Hall effect) induced by electron scattering from disordered grain boundaries and from rough surfaces on metallic nanostructures; we review recent measurements of the magneto transport coefficients that elucidate the electron scattering mechanisms at work. We review as well theoretical developments regarding quantum transport theories that allow calculating the increase in resistivity induced by electron-rough surface scattering (in the absence of grain boundaries) from first principles—from the parameters that describe the surface roughness that can be measured with a Scanning Tunnelling Microscope (STM). We evaluate the predicting power of the quantum version of the Fuchs-Sondheimer theory and of the model proposed by Calecki, abandoning the method of parameter fitting used for decades, but comparing instead theoretical predictions with resistivity measured in thin films where surface roughness has also been measured with a STM, and where electron-grain boundary scattering can be neglected. We also review the theory of Mayadas and Shatzkes (MS) [Phys. Rev. B 1, 1382 (1970)] used for decades, and discuss its severe conceptual difficulties that arise out of the fact that: (i) MS employed plane waves to describe the electronic states within the metal sample having periodic grain boundaries, rather than the Bloch states known since the thirties to be the solutions of the Schrödinger equation describing electrons propagating through a Krönig-Penney [Proc. R. Soc. London Ser. A 130, 499 (1931)] periodic potential; (ii) MS ignored the fact that the wave functions describing electrons propagating through a 1-D disordered potential are expected to decay exponentially with increasing distance, a fact known since the work of Anderson [Phys. Rev. 109, 1492 (1958)] in 1958 for which he was awarded the Nobel Prize in 1977; (iii) The current in the sample should be proportional to TN, the probability that an electron traverses N consecutive (disordered) grains found along a mean free path; MS assumed that TN = 1. We review unpublished details of a quantum transport theory based upon a model of diffusive transport and Kubo's linear response formalism recently published [Arenas et al., Appl. Surf. Sci. 329, 184 (2015)], which permits estimating the increase in resistivity of a metallic specimen (over the bulk resistivity) under the combined effects of electron scattering by phonons, impurities, disordered grain boundaries, and rough surfaces limiting the sample. We evaluate the predicting power of both the MS theory and of the new quantum model on samples where the temperature dependence of the resistivity has been measured between 4 K and 300 K, and where surface roughness and grain size distribution has been measured on each sample via independent experiments. We find that the quantum theory does exhibit a predicting power, whereas the predicting power of the MS model as well as the significance and reliability of its fitting parameters seems questionable. We explore the power of the new theory by comparing, for the first time, the resistivity predicted and measured on nanometric Cu wires of (approximately) rectangular cross section employed in building integrated circuits, based upon a quantum description of electron motion.
Atomic force microscopy studies of homoepitaxial GaN layers grown on GaN template by laser MBE

DOE Office of Scientific and Technical Information (OSTI.GOV)

Choudhary, B. S.; Rajasthan Technical University, Rawatbhata Road, Kota 324010; Singh, A.

We have grown homoepitaxial GaN films on metal organic chemical vapor deposition (MOCVD) grown 3.5 µm thick GaN on sapphire (0001) substrate (GaN template) using an ultra-high vacuum (UHV) laser assisted molecular beam epitaxy (LMBE) system. The GaN films were grown by laser ablating a polycrystalline solid GaN target in the presence of active r.f. nitrogen plasma. The influence of laser repetition rates (10-30 Hz) on the surface morphology of homoepitaxial GaN layers have been studied using atomic force microscopy. It was found that GaN layer grown at 10 Hz shows a smooth surface with uniform grain size compared to the rough surfacemore » with irregular shape grains obtained at 30 Hz. The variation of surface roughness of the homoepitaxial GaN layer with and without wet chemical etching has been also studied and it was observed that the roughness of the film decreased after wet etching due to the curved structure/rough surface.« less
Influence of Surface Roughness on Polymer Drag Reduction

DTIC Science & Technology

2007-11-30

paint (High Build Semi-Gloss 97-130, Aquapon ) with glass bead grit. The particles were tightly packed producing a sand grain type roughness. Based on the... Aquapon High Build Semi-Gloss Epoxy 97-130) with glass bead grit blown into the epoxy. The particles were tightly packed giving an average roughness height
Experimental study of crack initiation and propagation in high- and gigacycle fatigue in titanium alloys

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bannikov, Mikhail, E-mail: mbannikov@icmm.ru, E-mail: oborin@icmm.ru, E-mail: naimark@icmm.ru; Oborin, Vladimir, E-mail: mbannikov@icmm.ru, E-mail: oborin@icmm.ru, E-mail: naimark@icmm.ru; Naimark, Oleg, E-mail: mbannikov@icmm.ru, E-mail: oborin@icmm.ru, E-mail: naimark@icmm.ru

Fatigue (high- and gigacycle) crack initiation and its propagation in titanium alloys with coarse and fine grain structure are studied by fractography analysis of fracture surface. Fractured specimens were analyzed by interferometer microscope and SEM to improve methods of monitoring of damage accumulation during fatigue test and to verify the models for fatigue crack kinetics. Fatigue strength was estimated for high cycle fatigue regime using the Luong method [1] by “in-situ” infrared scanning of the sample surface for the step-wise loading history for different grain size metals. Fine grain alloys demonstrated higher fatigue resistance for both high cycle fatigue andmore » gigacycle fatigue regimes. Fracture surface analysis for plane and cylindrical samples was carried out using optical and electronic microscopy method. High resolution profilometry (interferometer-profiler New View 5010) data of fracture surface roughness allowed us to estimate scale invariance (the Hurst exponent) and to establish the existence of two characteristic areas of damage localization (different values of the Hurst exponent). Area 1 with diameter ∼300 μm has the pronounced roughness and is associated with damage localization hotspot. Area 2 shows less amplitude roughness, occupies the rest fracture surface and considered as the trace of the fatigue crack path corresponding to the Paris kinetics.« less
A numerical investigation of the crystallographic texture effect on the surface roughening in aluminum polycrystals

NASA Astrophysics Data System (ADS)

Romanova, V.; Balokhonov, R.; Batukhtina, E.; Zinovieva, O.; Bezmozgiy, I.

2015-10-01

The results of a numerical analysis of the mesoscale surface roughening in a polycrystalline aluminum alloy exposed to uniaxial tension are presented. A 3D finite-element model taking an explicit account of grain structure is developed. The model describes a constitutive behavior of the material on the grain scale, using anisotropic elasticity and crystal plasticity theory. The effects of the grain shape and texture on the deformation-induced roughening are investigated. Calculation results have shown that surface roughness is much higher and develops at the highest rate in a polycrystal with equiaxed grains where both the micro- and mesoscale surface displacements are observed.
The influence of nanostructured features on bacterial adhesion and bone cell functions on severely shot peened 316L stainless steel.

PubMed

Bagherifard, Sara; Hickey, Daniel J; de Luca, Alba C; Malheiro, Vera N; Markaki, Athina E; Guagliano, Mario; Webster, Thomas J

2015-12-01

Substrate grain structure and topography play major roles in mediating cell and bacteria activities. Severe plastic deformation techniques, known as efficient metal-forming and grain refining processes, provide the treated material with novel mechanical properties and can be adopted to modify nanoscale surface characteristics, possibly affecting interactions with the biological environment. This in vitro study evaluates the capability of severe shot peening, based on severe plastic deformation, to modulate the interactions of nanocrystallized metallic biomaterials with cells and bacteria. The treated 316L stainless steel surfaces were first investigated in terms of surface topography, grain size, hardness, wettability and residual stresses. The effects of the induced surface modifications were then separately studied in terms of cell morphology, adhesion and proliferation of primary human osteoblasts (bone forming cells) as well as the adhesion of multiple bacteria strains, specifically Staphylococcus aureus, Staphylococcus epidermidis, Pseudomonas aeruginosa, and ampicillin-resistant Escherichia coli. The results indicated a significant enhancement in surface work hardening and compressive residual stresses, maintenance of osteoblast adhesion and proliferation as well as a remarkable decrease in the adhesion and growth of gram-positive bacteria (S. aureus and S. epidermidis) compared to non-treated and conventionally shot peened samples. Impressively, the decrease in bacteria adhesion and growth was achieved without the use of antibiotics, for which bacteria can develop a resistance towards anyway. By slightly grinding the surface of severe shot peened samples to remove differences in nanoscale surface roughness, the effects of varying substrate grain size were separated from those of varying surface roughness. The expression of vinculin focal adhesions from osteoblasts was found to be singularly and inversely related to grain size, whereas the attachment of gram-positive bacteria (S. aureus and S. epidermidis) decreased with increasing nanoscale surface roughness, and was not affected by grain refinement. Ultimately, this study demonstrated the advantages of the proposed shot peening treatment to produce multifunctional 316L stainless steel materials for improved implant functions without necessitating the use of drugs. Copyright © 2015 Elsevier Ltd. All rights reserved.
Coevolution of bed surface patchiness and channel morphology: 2. Numerical experiments

USGS Publications Warehouse

Nelson, Peter A.; McDonald, Richard R.; Nelson, Jonathan M.; Dietrich, William E.

2015-01-01

In gravel bed rivers, bed topography and the bed surface grain size distribution evolve simultaneously, but it is not clear how feedbacks between topography and grain sorting affect channel morphology. In this, the second of a pair of papers examining interactions between bed topography and bed surface sorting in gravel bed rivers, we use a two-dimensional morphodynamic model to perform numerical experiments designed to explore the coevolution of both free and forced bars and bed surface patches. Model runs were carried out on a computational grid simulating a 200 m long, 2.75 m wide, straight, rectangular channel, with an initially flat bed at a slope of 0.0137. Over five numerical experiments, we varied (a) whether an obstruction was present, (b) whether the sediment was a gravel mixture or a single size, and (c) whether the bed surface grain size feeds back on the hydraulic roughness field. Experiments with channel obstructions developed a train of alternate bars that became stationary and were connected to the obstruction. Freely migrating alternate bars formed in the experiments without channel obstructions. Simulations incorporating roughness feedbacks between the bed surface and flow field produced flatter, broader, and longer bars than simulations using constant roughness or uniform sediment. Our findings suggest that patches are not simply a by-product of bed topography, but they interact with the evolving bed and influence morphologic evolution.
The effects of ultrasonic agitation on supercritical CO2 copper electroplating.

PubMed

Chuang, Ho-Chiao; Yang, Hsi-Min; Wu, Guan-Lin; Sánchez, Jorge; Shyu, Jenq-Huey

2018-01-01

Applying ultrasound to the electroplating process can improve mechanical properties and surface roughness of the coating. Supercritical electroplating process can refine grain to improve the surface roughness and hardness. However, so far there is no research combining the above two processes to explore its effect on the coating. This study aims to use ultrasound (42kHz) in supercritical CO 2 (SC-CO 2 ) electroplating process to investigate the effect of ultrasonic powers and supercritical pressures on the properties of copper films. From the results it was clear that higher ultrasonic irradiation resulted in higher current efficiency, grain refinement, higher hardness, better surface roughness and higher internal stress. SEM was also presented to verify the correctness of the measured data. The optimal parameters were set to obtain the deposit at pressure of 2000psi and ultrasonic irradiation of 0.157W/cm 3 . Compared with SC-CO 2 electroplating process, the current efficiency can be increased from 77.57% to 93.4%, the grain size decreases from 24.34nm to 22.45nm, the hardness increases from 92.87Hv to 174.18Hv, and the surface roughness decreases from 0.83μm to 0.28μm. Therefore, this study has successfully integrated advantages of ultrasound and SC-CO 2 electroplating, and proved that applied ultrasound to SC-CO 2 electroplating process can significantly improve the mechanical properties of the coating. Copyright © 2017 Elsevier B.V. All rights reserved.
Effects of size reduction on deformation, microstructure, and surface roughness of micro components for micro metal injection molding

NASA Astrophysics Data System (ADS)

Liu, Lin; Wang, Xin-da; Li, Xiang; Qi, Xiao-tong; Qu, Xuan-hui

2017-09-01

The fabrication of 17-4PH micro spool mandrils by micro metal injection molding was described here. The effects of size reduction on deformation, microstructure and surface roughness were studied by comparing a ϕ500 μm micro post and a ϕ1.7 mm cylinder after debinding and sintering. Experimental results show that slumping of the micro posts occurred due to a dramatic increase in outlet vapor pressure initiated at the thermal degradation onset temperature and the moment of gravity. Asymmetrical stress distribution within the micro component formed during the cooling stage may cause warping. Prior solvent debinding and adjustment in a thermal debinding scheme were useful for preventing the deformation of the micro components. Smaller grain size and higher micro hardness due to impeded grain growth were observed for the micro posts compared with the ϕ1.7 mm cylinder. Surface roughness increased with distance from the gate of the micro spool mandril due to melt front advancement during mold filling and the ensuing pressure distribution. At each position, surface roughness was dictated by injection molding and increased slightly after sintering.
Enhanced endothelial cell density on NiTi surfaces with sub-micron to nanometer roughness

PubMed Central

Samaroo, Harry D; Lu, Jing; Webster, Thomas J

2008-01-01

The shape memory effect and superelastic properties of NiTi (or Nitinol, a nickel-titanium alloy) have already attracted much attention for various biomedical applications (such as vascular stents, orthodontic wires, orthopedic implants, etc). However, for vascular stents, conventional approaches have required coating NiTi with anti-thrombogenic or anti-inflammatory drug-eluting polymers which as of late have proven problematic for healing atherosclerotic blood vessels. Instead of focusing on the use of drug-eluting anti-thrombogenic or anti-inflammatory proteins, this study focused on promoting the formation of a natural anti-thrombogenic and anti-inflammatory surface on metallic stents: the endothelium. In this study, we synthesized various NiTi substrates with different micron to nanometer surface roughness by using dissimilar dimensions of constituent NiTi powder. Endothelial cell adhesion on these compacts was compared with conventional commercially pure (cp) titanium (Ti) samples. The results after 5 hrs showed that endothelial cells adhered much better on fine grain (<60 μm) compared with coarse grain NiTi compacts (<100 μm). Coarse grain NiTi compacts and conventional Ti promoted similar levels of endothelial cell adhesion. In addition, cells proliferated more after 5 days on NiTi with greater sub-micron and nanoscale surface roughness compared with coarse grain NiTi. In this manner, this study emphasized the positive pole that NiTi with sub-micron to nanometer surface features can play in promoting a natural anti-thrombogenic and anti-inflammatory surface (the endothelium) on a vascular stent and, thus, suggests that more studies should be conducted on NiTi with sub-micron to nanometer surface features. PMID:18488418
Sub-discretized surface model with application to contact mechanics in multi-body simulation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Johnson, S; Williams, J

2008-02-28

The mechanics of contact between rough and imperfectly spherical adhesive powder grains are often complicated by a variety of factors, including several which vary over sub-grain length scales. These include several traction factors that vary spatially over the surface of the individual grains, including high energy electron and acceptor sites (electrostatic), hydrophobic and hydrophilic sites (electrostatic and capillary), surface energy (general adhesion), geometry (van der Waals and mechanical), and elasto-plastic deformation (mechanical). For mechanical deformation and reaction, coupled motions, such as twisting with bending and sliding, as well as surface roughness add an asymmetry to the contact force which invalidatesmore » assumptions for popular models of contact, such as the Hertzian and its derivatives, for the non-adhesive case, and the JKR and DMT models for adhesive contacts. Though several contact laws have been offered to ameliorate these drawbacks, they are often constrained to particular loading paths (most often normal loading) and are relatively complicated for computational implementation. This paper offers a simple and general computational method for augmenting contact law predictions in multi-body simulations through characterization of the contact surfaces using a hierarchically-defined surface sub-discretization. For the case of adhesive contact between powder grains in low stress regimes, this technique can allow a variety of existing contact laws to be resolved across scales, allowing for moments and torques about the contact area as well as normal and tangential tractions to be resolved. This is especially useful for multi-body simulation applications where the modeler desires statistical distributions and calibration for parameters in contact laws commonly used for resolving near-surface contact mechanics. The approach is verified against analytical results for the case of rough, elastic spheres.« less
Mechanisms of dust grain charging in plasma with allowance for electron emission processes

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mol’kov, S. I.; Savin, V. N., E-mail: moped@onego.ru

2017-02-15

The process of dust grain charging is described with allowance for secondary, ion-induced, photoelectric, and thermal electron emission from the grain surface. The roughness of the grain surface is taken into account. An intermediate charging regime involving ion–atom collisions and electron ionization in the perturbed plasma region is analyzed using the moment equations and Poisson’s equation. A calculation method is proposed that allows one to take into account the influence of all the above effects and determine the radius of the plasma region perturbed by the dust grain.

Surface correlations of hydrodynamic drag for transitionally rough engineering surfaces

NASA Astrophysics Data System (ADS)

Thakkar, Manan; Busse, Angela; Sandham, Neil

2017-02-01

Rough surfaces are usually characterised by a single equivalent sand-grain roughness height scale that typically needs to be determined from laboratory experiments. Recently, this method has been complemented by a direct numerical simulation approach, whereby representative surfaces can be scanned and the roughness effects computed over a range of Reynolds number. This development raises the prospect over the coming years of having enough data for different types of rough surfaces to be able to relate surface characteristics to roughness effects, such as the roughness function that quantifies the downward displacement of the logarithmic law of the wall. In the present contribution, we use simulation data for 17 irregular surfaces at the same friction Reynolds number, for which they are in the transitionally rough regime. All surfaces are scaled to the same physical roughness height. Mean streamwise velocity profiles show a wide range of roughness function values, while the velocity defect profiles show a good collapse. Profile peaks of the turbulent kinetic energy also vary depending on the surface. We then consider which surface properties are important and how new properties can be incorporated into an empirical model, the accuracy of which can then be tested. Optimised models with several roughness parameters are systematically developed for the roughness function and profile peak turbulent kinetic energy. In determining the roughness function, besides the known parameters of solidity (or frontal area ratio) and skewness, it is shown that the streamwise correlation length and the root-mean-square roughness height are also significant. The peak turbulent kinetic energy is determined by the skewness and root-mean-square roughness height, along with the mean forward-facing surface angle and spanwise effective slope. The results suggest feasibility of relating rough-wall flow properties (throughout the range from hydrodynamically smooth to fully rough) to surface parameters.
A Transport Equation Approach to Modeling the Influence of Surface Roughness on Boundary Layer Transition

NASA Astrophysics Data System (ADS)

Langel, Christopher Michael

A computational investigation has been performed to better understand the impact of surface roughness on the flow over a contaminated surface. This thesis highlights the implementation and development of the roughness amplification model in the flow solver OVERFLOW-2. The model, originally proposed by Dassler, Kozulovic, and Fiala, introduces an additional scalar field roughness amplification quantity. This value is explicitly set at rough wall boundaries using surface roughness parameters and local flow quantities. This additional transport equation allows non-local effects of surface roughness to be accounted for downstream of rough sections. This roughness amplification variable is coupled with the Langtry-Menter model and used to modify the criteria for transition. Results from flat plate test cases show good agreement with experimental transition behavior on the flow over varying sand grain roughness heights. Additional validation studies were performed on a NACA 0012 airfoil with leading edge roughness. The computationally predicted boundary layer development demonstrates good agreement with experimental results. New tests using varying roughness configurations are being carried out at the Texas A&M Oran W. Nicks Low Speed Wind Tunnel to provide further calibration of the roughness amplification method. An overview and preliminary results are provided of this concurrent experimental investigation.
Percolation characteristics of solvent invasion in rough fractures under miscible conditions

NASA Astrophysics Data System (ADS)

Korfanta, M.; Babadagli, T.; Develi, K.

2017-10-01

Surface roughness and flow rate effects on the solvent transport under miscible conditions in a single fracture are studied. Surface replicas of seven different rocks (marble, granite, and limestone) are used to represent different surface roughness characteristics each described by different mathematical models including three fractal dimensions. Distribution of dyed solvent is investigated at various flow rate conditions to clarify the effect of roughness on convective and diffusive mixing. After a qualitative analysis using comparative images of different rocks, the area covered by solvent with respect to time is determined to conduct a semi-quantitative analysis. In this exercise, two distinct zones are identified, namely the straight lines obtained for convective (early times) and diffusive (late times) flow. The bending point between these two lines is used to point the transition between the two zones. Finally, the slopes of the straight lines and the bending points are correlated to five different roughness parameters and the rate (Peclet number). It is observed that both surface roughness and flow rate have significant effect on solvent spatial distribution. The largest area covered is obtained at moderate flow rates and hence not only the average surface roughness characteristic is important, but coessentially total fracture surface area needs to be considered when evaluating fluid distribution. It is also noted that the rate effect is critically different for the fracture samples of large grain size (marbles and granite) compared to smaller grain sizes (limestones). Variogram fractal dimension exhibits the strongest correlation with the maximum area covered by solvent, and display increasing trend at the moderate flow rates. Equations with variogram surface fractal dimension in combination with any other surface fractal parameter coupled with Peclet number can be used to predict maximum area covered by solvent in a single fracture, which in turn can be utilized to model oil recovery, waste disposal, and groundwater contamination processes in the presence of fractures.
Copper foils with gradient structure in thickness direction and different roughnesses on two surfaces fabricated by double rolling

NASA Astrophysics Data System (ADS)

Wang, Xi-yong; Liu, Xue-feng; Zou, Wen-jiang; Xie, Jian-xin

2013-12-01

Copper foils with gradient structure in thickness direction and different roughnesses on two surfaces were fabricated by double rolling. The two surface morphologies of double-rolled copper foils are quite different, and the surface roughness values are 61 and 1095 nm, respectively. The roughness value of matt surface can meet the requirement for bonding the resin matrix with copper foils used for flexible printed circuit boards, thus may omit traditional roughening treatment; the microstructure of double-rolled copper foils demonstrates an obviously asymmetric gradient feature. From bright surface to matt surface in thickness direction, the average grain size first increases from 2.3 to 7.4 μm and then decreases to 3.6 μm; compared with conventional rolled copper foils, the double-rolled copper foils exhibit a remarkably increased bending fatigue life, and the increased range is about 16.2%.
Permeability-porosity relationships in sedimentary rocks

USGS Publications Warehouse

Nelson, Philip H.

1994-01-01

In many consolidated sandstone and carbonate formations, plots of core data show that the logarithm of permeability (k) is often linearly proportional to porosity (??). The slope, intercept, and degree of scatter of these log(k)-?? trends vary from formation to formation, and these variations are attributed to differences in initial grain size and sorting, diagenetic history, and compaction history. In unconsolidated sands, better sorting systematically increases both permeability and porosity. In sands and sandstones, an increase in gravel and coarse grain size content causes k to increase even while decreasing ??. Diagenetic minerals in the pore space of sandstones, such as cement and some clay types, tend to decrease log(k) proportionately as ?? decreases. Models to predict permeability from porosity and other measurable rock parameters fall into three classes based on either grain, surface area, or pore dimension considerations. (Models that directly incorporate well log measurements but have no particular theoretical underpinnings from a fourth class.) Grain-based models show permeability proportional to the square of grain size times porosity raised to (roughly) the fifth power, with grain sorting as an additional parameter. Surface-area models show permeability proportional to the inverse square of pore surface area times porosity raised to (roughly) the fourth power; measures of surface area include irreducible water saturation and nuclear magnetic resonance. Pore-dimension models show permeability proportional to the square of a pore dimension times porosity raised to a power of (roughly) two and produce curves of constant pore size that transgress the linear data trends on a log(k)-?? plot. The pore dimension is obtained from mercury injection measurements and is interpreted as the pore opening size of some interconnected fraction of the pore system. The linear log(k)-?? data trends cut the curves of constant pore size from the pore-dimension models, which shows that porosity reduction is always accompanied by a reduction in characteristic pore size. The high powers of porosity of the grain-based and surface-area models are required to compensate for the inclusion of the small end of the pore size spectrum.
A scanning electron microscope study of olivine crystal surfaces

NASA Technical Reports Server (NTRS)

Olsen, E. J.; Grossman, L.

1974-01-01

SEM photographs were taken of euhedral olivine grains from the Murchison C2 chondrite and several terrestrial and lunar occurrences. In general, the crystal faces of the meteorite grains are rough and uneven, with irregular growth patterns. They are very similar to crystal faces on terrestrial olivine grains that formed by sublimation from a vapor phase. They are very different from the relatively smooth and featureless surfaces of magmatic olivine crystals that precipitated from igneous melts. Qualitatively, the surface morphology of the crystal supports the contention that many euhedral crystals of olivine in C2 meteorites condensed from a gas phase.
The Effect of Surface Irregularities on Wing Drag. 3; Roughness

NASA Technical Reports Server (NTRS)

Hood, Manley J.

1938-01-01

Tests have been made in the N.A.C.A. 8-foot high-speed wind tunnel of the drag caused by roughness on the surface of an airfoil of N.A.C.A. 23012 section and 5-foot chord. The tests were made at speeds from 80 t o 500 miles per hour at lift coefficients from 0 to 0.30. For conditions corresponding to high-speed flight, the increase in the drag was 30 percent of the profile drag of the smooth airfoil for the roughness produced by spray painting and 63 percent for the roughness produced. by 0.0037-inch carborundum grains. About one-half the drag increase was caused by the roughness on the forward one-fourth of the airfoil. Sandpapering the painted surface with No. 400 sandpaper made it sufficiently smooth that the drag was no greater than when the surface was polished. In the lower part of the range investigated the drag due to roughness increased rapidly with Reynolds Number.
DOE Office of Scientific and Technical Information (OSTI.GOV)

Yadav, Praveen Kumar, E-mail: praveenyadav@rrcat.gov.in; Nayak, Maheswar; Rai, Sanjay Kumar

The authors report the effect of argon ion to molybdenum atom ratio (r) on the microstructure of low energy (70 eV) argon ion assisted electron beam evaporated Mo thin films. Surface roughness, morphology, and crystallinity of Mo films are found to strongly depend on “r.” Increase of “r” from 0 to 100 induces gradual loss in crystallinity, reduction in surface roughness and systematic increase in density of the film. For “r” ∼ 100, average atomic density of the film approaches the bulk value (97%) with lowest surface roughness. Further, increasing “r” up to 170 reduces the atomic density, increases roughness, and increase inmore » crystallinity induced by low energy Ar ion beam. The observed surface roughness and grain size determined by x-ray reflectivity and glancing incidence x-ray diffraction correlate well with atomic force microscopy measurements. This study demonstrates that for r = 100 one gets lowest roughness Mo film with highest density and nearly amorphous microstructure. The growth model is discussed by structural zone model.« less
Thermophysical Characteristics of OSIRIS-REx Target Asteroid (101955) Bennu

NASA Astrophysics Data System (ADS)

Yu, Liangliang; Ji, Jianghui

2016-01-01

In this work, we investigate the thermophysical properties, including thermal inertia, roughness fraction and surface grain size of OSIRIS-REx target asteroid (101955) Bennu by using a thermophysical model with the recently updated 3D radar-derived shape model (Nolan et al., 2013) and mid-infrared observations (Müller et al. 2012, Emery et al., 2014). We find that the asteroid bears an effective diameter of 510+6 -40 m, a geometric albedo of 0.047+0.0083 -0.0011, a roughness fraction of 0.04+0.26 -0.04, and thermal inertia of 240+440 -60 Jm-2s-0.5K-1 for our best-fit solution. The best-estimate thermal inertia suggests that fine-grained regolith may cover a large portion of Bennu's surface, where a grain size may vary from 1.3 to 31 mm. Our outcome suggests that Bennu is suitable for the OSIRIS-REx mission to return samples to Earth.
Study the Formation of H2, HD and D2 under Various Interstellar Conditions

NASA Astrophysics Data System (ADS)

Sahu, Dipen; Chakrabarti, Sandip Kumar; Das, Ankan

2016-07-01

Hydrogen is the most abundant molecule in the Interstellar medium (ISM). Formation of gas phase hydrogen molecule is inefficient; perhaps grain surface acts as a necessary ingredients for the formation of H_2 molecule. H atoms accrete on the grain surface, recombine there and desorb in the gas phase. Similarly, deuterium accretion on grain surfaces can produce simple dueterated molecules (HD and D_2) on the ISM. Unlike gas phase reactions, rate equations can not yield accurate result for grain surface reactions due to inherent randomness of surface species. We use Monte-Carlo method to follow this surface chemistry which effectively take care of this randomness. We use square grids and impose periodic boundary condition on them to mimic the spherical nature of grains. Various types of rough surfaces are considered to study the impact on effective production rates. We found that these simple but most important molecules are produced in low temperature (physisorption sites) as well as in high temperature (chemisorption sites) regions.
Effect of Shot Peening in Different Shot Distance and Shot Angle on Surface Morphology, Surface Roughness and Surface Hardness of 316L Biomaterial

NASA Astrophysics Data System (ADS)

Umbu Kondi Maliwemu, Erich; Malau, Viktor; Iswanto, Priyo Tri

2018-01-01

Shot peening is a mechanical surface treatment with a beneficial effect to generate compressive residual stress caused by plastic deformation on the surface of material. This plastic deformation can improve the surface characteristics of metallic materials, such as modification of surface morphology, surface roughness, and surface hardness. The objective of this study is to investigate the effect of shot peening in different shot distance and shot angle on surface morphology, surface roughness, and surface hardness of 316L biomaterial. Shot distance was varied at 6, 8, 10, and 12 cm and shot angle at 30, 60, and 90°, working pressure at 7 kg/cm2, shot duration for 20 minutes, and using steel balls S-170 with diameter of 0.6 mm. The results present that the shot distance and shot angle of shot peening give the significant effect to improve the surface morphology, surface roughness, and surface hardness of 316 L biomaterial. Shot peening can increase the surface roughness by the increasing of shot distance and by the decreasing of shot angle. The nearest shot distance (6 cm) and the largest shot angle (90°) give the best results on the grain refinement with the surface roughness of 1.04 μm and surface hardness of 534 kg/mm2.
A note on ``critical roughness height'' and ``transitional roughness''

NASA Astrophysics Data System (ADS)

Bradshaw, P.

2000-06-01

An unrigorous but plausible analysis suggests that the concept of a critical roughness height, below which roughness does not affect a turbulent wall flow, is erroneous. The Oseen approximation implies that the effect of roughness on the additive constant in the logarithmic law of the wall should vary as the square of the roughness Reynolds number (specifically the roughness height in "wall units"). This is an important point in determining whether surfaces used in experiments at high unit Reynolds number can be regarded as hydraulically smooth. Attention is also called to the qualitative difference between Nikuradse's measurements of friction factor in pipe flow with uniform-size sand-grain roughness in the "transitional" range of Reynolds number and the data correlation in the Moody chart of 1944; the latter was derived from tests on miscellaneous real-life rough surfaces in the 1930s. Nearly all textbooks on elementary fluid dynamics present, but practically none discuss, this difference. Nikuradse's monodisperse roughness is a very rare case with untypical behavior in the transitional range.
Transgenic cry1C(⁎) gene rough rice line T1C-19 does not change the host preferences of the non-target stored product pest, Rhyzopertha dominica (Fabricius) (Coleoptera: Bostrichidae), and its parasitoid wasp, Anisopteromalus calandrae (Howard) (Hymenoptera: Pteromalidae).

PubMed

Sun, Xiao; Yan, Miao-Jun; Zhang, Aijun; Wang, Man-Qun

2015-10-01

Rough rice grains are often stored for extended periods before they are used or consumed. However, during storage, the rough rice is vulnerable to insect infestation, resulting in significant economic loss. Previous studies have shown that volatiles cues, physical characteristics, and taste chemicals on the grains could be the important key behavior factors for storage insect pests to locate the hosts and select oviposition sites. It is also well known that the transgenic Bt rough rice line T1C-19, which expresses a cry1C(⁎) gene has a high resistance to Lepidoptera pests. However, there were no evidences to show the consequences of host preference for non-target insect pests after growing Bt transgenic rice. In this study, the potential key factors of Bt rough rice were investigated for their impacts on the behaviors of non-target pest lesser grain borer Rhyzopertha dominica, the main weevil pest of grain and its parasitic wasps Anisopteromalus calandrae, the natural enemy of the beetle. Both electronic nose and electronic tongue analyses showed that the parameters of Bt rough rice were analogous to those of the non-Bt rough rice. The volatile profiles of Bt and non-Bt rough rice examined by gas chromatographic mass spectrometry (GC-MS) were similar. For most volatile compounds, there were no significantly quantitative differences in compound quantities between Bt and non-Bt rough rice. The densities of sclereids and trichomes on the rough rice husk surface were statistically equal in Bt and non-Bt rough rice. The non-target pest, R. dominica, and its parasitoid wasp, A. calandrae, were attracted to both rough rice and could not distinguish the transgenic T1C-19 from the isogenic rough rice. These results demonstrated that Bt rough rice has no negative impacts on the host preference behaviors of non-target stored product pest R. dominica and its parasitoid A. calandrae. Copyright © 2015 Elsevier Inc. All rights reserved.
Erosion of phosphor bronze under cavitation attack in a mineral oil

NASA Technical Reports Server (NTRS)

Rao, B. C. S.; Buckley, D. H.

1986-01-01

Experimental investigations on erosion of a copper alloy, phosphor bronze, under cavitation attack in a viscous mineral oil are presented. The details of pit formation and erosion were studied using scanning electron microscopy. The mean depth of penetration, the variations in surface roughness, and the changes in erosion pit size were studied. Cavitation pits formed initially over the grain boundaries while the surface grains were plastically deformed. Erosion of surface grains occurred largely by ductile fracture involving microcracking and removal in layers. The ratio h/a of the depth h to half width a of cavitation pits increased with test duration from 0.047 to 0.55.
Correlation between substratum roughness and wettability, cell adhesion, and cell migration.

PubMed

Lampin, M; Warocquier-Clérout; Legris, C; Degrange, M; Sigot-Luizard, M F

1997-07-01

Cell adhesion and spreading of chick embryo vascular and corneal explants grown on rough and smooth poly (methyl methacrylate) (PMMA) were analyzed to test the cell response specificity to substratum surface properties. Different degrees of roughness were obtained by sand-blasting PMMA with alumina grains. Hydrophilic and hydrophobic components of the surface free energy (SFE) were calculated according to Good-van Oss's model. Contact angles were determined using a computerized angle meter. The apolar component of the SFE gamma s(LW), increased with a slight roughness whereas the basic component, gamma s-, decreased. The acido-basic properties disappeared as roughness increased. Incubation of PMMA in culture medium, performed to test the influence if the biological environment, allowed surface adsorption of medium proteins which annihilated roughness effect and restored hydrophilic properties. An organotypic culture assay was carried out in an attempt to relate the biocompatibility to substratum surface state. Cell migration was calculated from the area of cell layer. Cellular adhesion was determined by measuring the kinetic of release of enzymatically dissociated cells. A slight roughness raised the migration are to an upper extent no matter which cell type. Enhancement of the cell adhesion potential was related to the degree of roughness and the hydrophobicity.
Nanostructures on fused silica surfaces produced by ion beam sputtering with Al co-deposition

NASA Astrophysics Data System (ADS)

Liu, Ying; Hirsch, Dietmar; Fechner, Renate; Hong, Yilin; Fu, Shaojun; Frost, Frank; Rauschenbach, Bernd

2018-01-01

The ion beam sputtering (IBS) of smooth mono-elemental Si with impurity co-deposition is extended to a pre-rippled binary compound surface of fused silica (SiO2). The dependence of the rms roughness and the deposited amount of Al on the distance from the Al source under Ar+ IBS with Al co-deposition was investigated on smooth SiO2, pre-rippled SiO2, and smooth Si surfaces, using atomic force microscopy and X-ray photoelectron spectroscopy. Although the amounts of Al deposited on these three surfaces all decreased with increasing distance from the Al target, the morphology and rms roughness of the smooth Si surface did not demonstrate a strong distance dependence. In contrast to smooth Si, the rms roughness of both the smooth and pre-rippled SiO2 surfaces exhibited a similar distance evolution trend of increasing, decreasing, and final stabilization at the distance where the results were similar to those obtained without Al co-deposition. However, the pre-rippled SiO2 surfaces showed a stronger modulation of rms roughness than the smooth surfaces. At the incidence angles of 60° and 70°, dot-decorated ripples and roof-tiles were formed on the smooth SiO2 surfaces, respectively, whereas nanostructures of closely aligned grains and blazed facets were generated on the pre-rippled SiO2, respectively. The combination of impurity co-deposition with pre-rippled surfaces was found to facilitate the formation of novel types of nanostructures and morphological growth. The initial ripples act as a template to guide the preferential deposition of Al on the tops of the ripples or the ripple sides facing the Al wedge, but not in the valleys between the ripples, leading to 2D grains and quasi-blazed grating, which offer significant promise in optical applications. The rms roughness enhancement is attributed not to AlSi, but to AlOxFy compounds originating mainly from the Al source.
Influence of microstructure and surface topography on the electrical conductivity of Cu and Ag thin films obtained by magnetron sputtering

NASA Astrophysics Data System (ADS)

Polonyankin, D. A.; Blesman, A. I.; Postnikov, D. V.

2017-05-01

Conductive thin films formation by copper and silver magnetron sputtering is one of high technological areas for industrial production of solar energy converters, energy-saving coatings, flat panel displays and touch control panels because of their high electrical and optical properties. Surface roughness and porosity, average grain size, internal stresses, orientation and crystal lattice type, the crystallinity degree are the main physical properties of metal films affecting their electrical resistivity and conductivity. Depending on the film thickness, the dominant conduction mechanism can affect bulk conductivity due to the flow of electron gas, and grain boundary conductivity. The present investigation assesses the effect of microstructure and surface topography on the electrical conductivity of magnetron sputtered Cu and Ag thin films using X-ray diffraction analysis, scanning electron and laser interference microscopy. The highest specific conductivity (78.3 MS m-1 and 84.2 MS m-1, respectively, for copper and silver films at the thickness of 350 nm) were obtained with the minimum values of roughness and grain size as well as a high degree of lattice structuredness.
The influence of surface roughness and high pressure torsion on the growth of anodic titania nanotubes on pure titanium

NASA Astrophysics Data System (ADS)

Hu, Nan; Gao, Nong; Starink, Marco J.

2016-11-01

Anodic titanium dioxide nanotube (TNT) arrays have wide applications in photocatalytic, catalysis, electronics, solar cells and biomedical implants. When TNT coatings are combined with severe plastic deformation (SPD), metal processing techniques which efficiently improve the strength of metals, a new generation of biomedical implant is made possible with both improved bulk and surface properties. This work investigated the effect of processing by high pressure torsion (HPT) and different mechanical preparations on the substrate and subsequently on the morphology of TNT layers. HPT processing was applied to refine the grain size of commercially pure titanium samples and substantially improved their strength and hardness. Subsequent anodization at 30 V in 0.25 wt.% NH4F for 2 h to form TNT layers on sample surfaces prepared with different mechanical preparation methods was carried out. It appeared that the local roughness of the titanium surface on a microscopic level affected the TNT morphology more than the macroscopic surface roughness. For HPT-processed sample, the substrate has to be pre-treated by a mechanical preparation finer than 4000 grit for HPT to have a significant influence on TNTs. During the formation of TNT layers the oxide dissolution rate was increased for the ultrafine-grained microstructure formed due to HPT processing.
Laser melting of groove defect repair on high thermal conductivity steel (HTCS-150)

NASA Astrophysics Data System (ADS)

Norhafzan, B.; Aqida, S. N.; Fazliana, F.; Reza, M. S.; Ismail, I.; Khairil, C. M.

2018-02-01

This paper presents laser melting repair of groove defect on HTCS-150 surface using Nd:YAG laser system. Laser melting process was conducted using JK300HPS Nd:YAG twin lamp laser source with 1064 nm wavelength and pulsed mode. The parameters are pulse repetition frequency (PRF) that is set from 70 to 100 Hz, average power ( P A) of 50-70 W, and laser spot size of 0.7 mm. HTCS-150 samples were prepared with groove dimension of 0.3 mm width and depths of 0.5 mm using EDM wire cut. Groove defect repaired using laser melting process on groove surface area with various parameters' process. The melted surface within the groove was characterized for subsurface hardness profile, roughness, phase identification, chemical composition, and metallographic study. The roughness analysis indicates high PRF at large spot size caused high surface roughness and low surface hardness. Grain refinement of repaired layer was analyzed within the groove as a result of rapid heating and cooling. The hardness properties of modified HTCS inside the groove and the bulk surface increased two times from as received HTCS due to grain refinement which is in agreement with Hall-Petch equation. These findings are significant to parameter design of die repair for optimum surface integrity and potential for repairing crack depth and width of less than 0.5 and 0.3 mm, respectively.
Small scale variability of snow properties on Antarctic sea ice

NASA Astrophysics Data System (ADS)

Wever, Nander; Leonard, Katherine; Paul, Stephan; Jacobi, Hans-Werner; Proksch, Martin; Lehning, Michael

2016-04-01

Snow on sea ice plays an important role in air-ice-sea interactions, as snow accumulation may for example increase the albedo. Snow is also able to smooth the ice surface, thereby reducing the surface roughness, while at the same time it may generate new roughness elements by interactions with the wind. Snow density is a key property in many processes, for example by influencing the thermal conductivity of the snow layer, radiative transfer inside the snow as well as the effects of aerodynamic forcing on the snowpack. By comparing snow density and grain size from snow pits and snow micro penetrometer (SMP) measurements, highly resolved density and grain size profiles were acquired during two subsequent cruises of the RV Polarstern in the Weddell Sea, Antarctica, between June and October 2013. During the first cruise, SMP measurements were done along two approximately 40 m transects with a horizontal resolution of approximately 30 cm. During the second cruise, one transect was made with approximately 7.5 m resolution over a distance of 500 m. Average snow densities are about 300 kg/m3, but the analysis also reveals a high spatial variability in snow density on sea ice in both horizontal and vertical direction, ranging from roughly 180 to 360 kg/m3. This variability is expressed by coherent snow structures over several meters. On the first cruise, the measurements were accompanied by terrestrial laser scanning (TLS) on an area of 50x50 m2. The comparison with the TLS data indicates that the spatial variability is exhibiting similar spatial patterns as deviations in surface topology. This suggests a strong influence from surface processes, for example wind, on the temporal development of density or grain size profiles. The fundamental relationship between variations in snow properties, surface roughness and changes therein as investigated in this study is interpreted with respect to large-scale ice movement and the mass balance.

Surface roughness retrieval by inversion of the Hapke model: A multiscale approach

NASA Astrophysics Data System (ADS)

Labarre, S.; Ferrari, C.; Jacquemoud, S.

2017-07-01

Surface roughness is a key property of soils that controls many surface processes and influences the scattering of incident electromagnetic waves at a wide range of scales. Hapke (2012b) designed a photometric model providing an approximate analytical solution of the Bidirectional Reflectance Distribution Function (BRDF) of a particulate medium: he introduced the effect of surface roughness as a correction factor of the BRDF of a smooth surface. This photometric roughness is defined as the mean slope angle of the facets composing the surface, integrated over all scales from the grain size to the local topography. Yet its physical meaning is still a question at issue, as the scale at which it occurs is not clearly defined. This work aims at better understanding the relative influence of roughness scales on soil BRDF and to test the ability of the Hapke model to retrieve a roughness that depicts effectively the ground truth. We apply a wavelet transform on millimeter digital terrain models (DTM) acquired over volcanic terrains. This method allows splitting the frequency band of a signal in several sub-bands, each corresponding to a spatial scale. We demonstrate that sub-centimeter surface features dominate both the integrated roughness and the BRDF shape. We investigate the suitability of the Hapke model for surface roughness retrieval by inversion on optical data. A global sensitivity analysis of the model shows that soil BRDF is very sensitive to surface roughness, nearly as much as the single scattering albedo according to the phase angle, but also that these two parameters are strongly correlated. Based on these results, a simplified two-parameter model depending on surface albedo and roughness is proposed. Inversion of this model on BRDF data simulated by a ray-tracing code over natural targets shows a good estimation of surface roughness when the assumptions of the model are verified, with a priori knowledge on surface albedo.
Tin doped indium oxide anodes with artificially controlled nano-scale roughness using segregated Ag nanoparticles for organic solar cells

NASA Astrophysics Data System (ADS)

Kim, Hyo-Joong; Ko, Eun-Hye; Noh, Yong-Jin; Na, Seok-In; Kim, Han-Ki

2016-09-01

Nano-scale surface roughness in transparent ITO films was artificially formed by sputtering a mixed Ag and ITO layer and wet etching of segregated Ag nanoparticles from the surface of the ITO film. Effective removal of self-segregated Ag particles from the grain boundaries and surface of the crystalline ITO film led to a change in only the nano-scale surface morphology of ITO film without changes in the sheet resistance and optical transmittance. A nano-scale rough surface of the ITO film led to an increase in contact area between the hole transport layer and the ITO anode, and eventually increased the hole extraction efficiency in the organic solar cells (OSCs). The heterojunction OSCs fabricated on the ITO anode with a nano-scale surface roughness exhibited a higher power conversion efficiency of 3.320%, than that (2.938%) of OSCs made with the reference ITO/glass. The results here introduce a new method to improve the performance of OSCs by simply modifying the surface morphology of the ITO anodes.
Modeling interface shear behavior of granular materials using micro-polar continuum approach

NASA Astrophysics Data System (ADS)

Ebrahimian, Babak; Noorzad, Ali; Alsaleh, Mustafa I.

2018-01-01

Recently, the authors have focused on the shear behavior of interface between granular soil body and very rough surface of moving bounding structure. For this purpose, they have used finite element method and a micro-polar elasto-plastic continuum model. They have shown that the boundary conditions assumed along the interface have strong influences on the soil behavior. While in the previous studies, only very rough bounding interfaces have been taken into account, the present investigation focuses on the rough, medium rough and relatively smooth interfaces. In this regard, plane monotonic shearing of an infinite extended narrow granular soil layer is simulated under constant vertical pressure and free dilatancy. The soil layer is located between two parallel rigid boundaries of different surface roughness values. Particular attention is paid to the effect of surface roughness of top and bottom boundaries on the shear behavior of granular soil layer. It is shown that the interaction between roughness of bounding structure surface and the rotation resistance of bounding grains can be modeled in a reasonable manner through considered Cosserat boundary conditions. The influence of surface roughness is investigated on the soil shear strength mobilized along the interface as well as on the location and evolution of shear localization formed within the layer. The obtained numerical results have been qualitatively compared with experimental observations as well as DEM simulations, and acceptable agreement is shown.
Oxidation behavior of grain boundary engineered alloy 690 in supercritical water environment

NASA Astrophysics Data System (ADS)

Xu, P.; Zhao, L. Y.; Sridharan, K.; Allen, T. R.

2012-03-01

Nickel-base alloy is an important structural material that is known for its exceptional high temperature oxidation resistance. Oxidation in this alloy at high temperatures occurs to a greater extent along the grain boundaries. Grain boundary engineering (GBE) was applied to modify the grain boundary characteristics of this alloy to affect its oxidation resistance. Specimens with both low level and high level cold works showed a high fraction of special grain boundaries, and were tested for supercritical water oxidation resistance at 500 °C and 24 MPa. Both GBE and as-received samples exhibited mass gain followed by mass loss during 10 weeks of exposure, but the normalized mass change was small and less than 0.12 mg/cm2. GBE samples showed better oxide layer retention compared to the as-received sample. XRD results indicate that nickel oxide, chromium oxide, and spinel oxide were the three main types of oxides that form on as-received and GBE alloy 690. Three distinct regions were identified on the oxidized surface: a flat region with oxide flakes aligning relatively parallel to the surface, a rough region with polygon-type oxide particles randomly distributed on the surface, and a region with aggregated oxide flakes perpendicular to the surface. The flat region of oxidation consisted of (1 1 1) orientated oxide spinel flakes formed on (1 1 1) oriented alloy 690 grains. The flat oxide region was thinner and showed better oxide adhesion compared to the rough region. Chromium oxidation was found only at random grain boundaries, leading to formation of thick Cr2O3 layer on the surface and chromium depletion underneath. None of this oxidation was found at low angle or special boundaries. The chromium oxidation was attributed to fast chromium diffusion through random boundaries and mechanically deformed regions such as scratches left after polishing. It is envisioned that the oxidation behavior of alloy 690 in supercritical water can be tailored by microstructure engineering that involves changes in grain orientation and grain boundary character distribution.
The variation of riverbed material due to tropical storms in Shi-Wen River, Taiwan.

PubMed

Lin, Chin-Ping; Wang, Yu-Min; Tfwala, Samkele S; Chen, Ching-Nuo

2014-01-01

Taiwan, because of its location, is a flood prone region and is characterised by typhoons which brings about two-thirds to three quarters of the annual rainfall amount. Consequently, enormous flows result in rivers and entrain some fractions of the grains that constitute the riverbed. Hence, the purpose of the study is to quantify the impacts of these enormous flows on the distribution of grain size in riverbeds. The characteristics of riverbed material prior to and after the typhoon season are compared in Shi-Wen River located at southern Taiwan. These include grain size variation, bimodality, and roughness coefficient. A decrease (65%) and increase (50%) in geometric mean size of grains were observed for subsurface and surface bed material, respectively. Geometric standard deviation decreased in all sites after typhoon. Subsurface material was bimodal prior to typhoons and polymodal after. For surface material, modal class is in the gravel class, while after typhoons it shifts towards cobble class. The reduction in geometric mean resulted to a decrease in roughness coefficient by up to 30%. Finally, the relationship of Shields and Froude numbers are studied and a change in the bed form to antidunes and transition form is observed, respectively.
The Variation of Riverbed Material due to Tropical Storms in Shi-Wen River, Taiwan

PubMed Central

Lin, Chin-Ping; Tfwala, Samkele S.; Chen, Ching-Nuo

2014-01-01

Taiwan, because of its location, is a flood prone region and is characterised by typhoons which brings about two-thirds to three quarters of the annual rainfall amount. Consequently, enormous flows result in rivers and entrain some fractions of the grains that constitute the riverbed. Hence, the purpose of the study is to quantify the impacts of these enormous flows on the distribution of grain size in riverbeds. The characteristics of riverbed material prior to and after the typhoon season are compared in Shi-Wen River located at southern Taiwan. These include grain size variation, bimodality, and roughness coefficient. A decrease (65%) and increase (50%) in geometric mean size of grains were observed for subsurface and surface bed material, respectively. Geometric standard deviation decreased in all sites after typhoon. Subsurface material was bimodal prior to typhoons and polymodal after. For surface material, modal class is in the gravel class, while after typhoons it shifts towards cobble class. The reduction in geometric mean resulted to a decrease in roughness coefficient by up to 30%. Finally, the relationship of Shields and Froude numbers are studied and a change in the bed form to antidunes and transition form is observed, respectively. PMID:24526910
Dust Grain Charge above the Lunar terminator

NASA Astrophysics Data System (ADS)

Vaverka, Jakub; Richterova, Ivana; Nemecek, Zdenek; Safrankova, Jana; Pavlu, Jiri; Vysinka, Marek

Interaction of a lunar surface with the solar wind and magnetosphere leads to its charging by several processes as photoemission, a collection of primary particles, and secondary electron emission. Nevertheless, charging of the lunar surface is complicated by a shielding of solar light and solar wind ions by hills, craters, and boulders that can locally influence the surface potential. Moreover, a presence of a plasma wake can strongly affect this potential at the night side of the Moon. A typical surface potential varies from slightly positive (dayside) to negative values of the order of several hundred volts (night side). An electric field above the charged surface can lead to a levitation of dust grains as it has been observed by several spacecraft and by astronauts during Apollo missions. Although charging and transport of dust grains above the lunar surface are in the center of interest for many years, these phenomena are not still completely understood. We present calculation of an equilibrium potential of dust grains above the lunar surface. We focus on a terminator area during the Earth’s plasma sheet crossing. We use the secondary electron emission model for dust grains which takes into account an influence of the grain size, material, and surface roughness and findings from laboratory experiments with charging of lunar dust simulants by an electron beam.
Engineered plant biomass feedstock particles

DOEpatents

Dooley, James H [Federal Way, WA; Lanning, David N [Federal Way, WA; Broderick, Thomas F [Lake Forest Park, WA

2011-10-11

A novel class of flowable biomass feedstock particles with unusually large surface areas that can be manufactured in remarkably uniform sizes using low-energy comminution techniques. The feedstock particles are roughly parallelepiped in shape and characterized by a length dimension (L) aligned substantially with the grain direction and defining a substantially uniform distance along the grain, a width dimension (W) normal to L and aligned cross grain, and a height dimension (H) normal to W and L. The particles exhibit a disrupted grain structure with prominent end and surface checks that greatly enhances their skeletal surface area as compared to their envelope surface area. The L.times.H dimensions define a pair of substantially parallel side surfaces characterized by substantially intact longitudinally arrayed fibers. The W.times.H dimensions define a pair of substantially parallel end surfaces characterized by crosscut fibers and end checking between fibers. The L.times.W dimensions define a pair of substantially parallel top surfaces characterized by some surface checking between longitudinally arrayed fibers. The feedstock particles are manufactured from a variety of plant biomass materials including wood, crop residues, plantation grasses, hemp, bagasse, and bamboo.
Lycus Sulci

NASA Image and Video Library

2003-03-14

This NASA Mars Odyssey image shows Lycus Sulci, a region of ridges and hills located north-northwest of the volcano Olympus Mons. Several dust avalanches on the flanks of the roughly textured surfaces suggest a thick coating of fine-grained materials.
Surface Roughness Investigation of Ultrafine-Grained Aluminum Alloy Subjected to High-Speed Erosion

NASA Astrophysics Data System (ADS)

Kazarinov, N. A.; Evstifeev, A. D.; Petrov, Y. V.; Atroshenko, S. A.; Lashkov, V. A.; Valiev, R. Z.; Bondarenko, A. S.

2016-09-01

This study is the first attempt to investigate the influence of severe plastic deformation (SPD) treatment on material surface behavior under intensive erosive conditions. Samples of aluminum alloy 1235 (99.3 Al) before and after high-pressure torsion (HPT) were subjected to intensive erosion by corundum particles accelerated via air flow in a small-scale wind tunnel. Velocity of particles varied from 40 to 200 m/s, while particle average diameter was around 100 μm. Surface roughness measurements provided possibility to compare surface properties of both materials after erosion tests. Moreover, SPD processing appeared to increase noticeably the threshold velocity of the surface damaging process. Additionally, structural analysis of the fracture surfaces of the tested samples was carried out.
Microstructure and magnetism of Co2FeAl Heusler alloy prepared by arc and induction melting compared with planar flow casting

NASA Astrophysics Data System (ADS)

Titov, A.; Jiraskova, Y.; Zivotsky, O.; Bursik, J.; Janickovic, D.

2018-04-01

This paper is devoted to investigations of the structural and magnetic properties of the Co2FeAl Heusler alloy produced by three technologies. The alloys prepared by arc and induction melting have resulted in coarse-grained samples in contrast to the fine-grained ribbon-type sample prepared by planar flow casting. Scanning electron microscopy completed by energy dispersive X-ray spectroscopy, X-ray diffraction, Mössbauer spectroscopy, and magnetic methods sensitive to both bulk and surface were applied. The chemical composition was slightly different from the nominal only for the ribbon sample. From the viewpoint of magnetic properties, the bulk coercivity and remnant magnetization have followed the structure influenced by the technology used. Saturation magnetization was practically the same for samples prepared by arc and induction melting, whereas the magnetization of ribbon is slightly lower due to a higher Al content at the expense of iron and cobalt. The surface magnetic properties were markedly influenced by anisotropy, grain size, and surface roughness of the samples. The surface roughness and brittleness of the ribbon-type sample did not make domain structure observation possible. The other two samples could be well polished and their highly smooth surface has enabled domain structure visualization by both magneto-optical Kerr microscopy and magnetic force microscopy.
A systematic analysis of eight decades of incipient motion studies, with special reference to gravel-bedded rivers

Treesearch

John M. Buffington; David R. Montgomery

1997-01-01

Data compiled from eight decades of incipient motion studies were used to calculate dimensionless critical shear stress values of the median grain size, T*c50. Calculated T*c50 values were stratified by initial motion definition, median grain size type (surface, subsurface, or laboratory mixture), relative roughness, and flow regime. A traditional Shields plot...
Effects of Sediment Patches on Sediment Transport Predictions in Steep Mountain Channels

NASA Astrophysics Data System (ADS)

Monsalve Sepulveda, A.; Yager, E.

2013-12-01

Bed surface patches occur in most gravel-bedded rivers and in steep streams can be divided between relatively immobile boulders and more mobile patches of cobbles and gravel. This spatial variability in grain size, roughness and sorting impact bed load transport by altering the relative local mobility of different grain sizes and creating complex local flow fields. Large boulders also bear a significant part of the total shear stress and we hypothesize that the remaining shear stress on a given mobile patch is a distribution of values that depend on the local topography, patch type and location relative to the large roughness elements and thalweg. Current sediment transport equations do not account for the variation in roughness, local flow and grain size distributions on and between patches and often use an area-weighted approach to obtain a representative grain size distribution and reach-averaged shear stress. Such equations also do not distinguish between active (patches where at least one grain size is in motion) and inactive patches or include the difference in mobility between patch classes as result of spatial shear stress distributions. To understand the effects of sediment patches on sediment transport in steep channels, we calculated the shear stress distributions over a range of patch classes in a 10% gradient step-pool stream. We surveyed the bed with a high density resolution (every 5 cm in horizontal and vertical directions over a 40 m long reach) using a total station and terrestrial LiDAR, mapped and classified patches by their grain size distributions, and measured water surface elevations and mean velocities for low to moderate flow events. Using these data we calibrated a quasi-three dimensional model (FaSTMECH) to obtain shear stress distributions over each patch for a range of flow discharges. We modified Parker's (1990) equations to use the calculated shear stress distribution, measured grain sizes, and a specific hiding function for each patch class, and then added the bedload fluxes for each patch to calculate the reach-averaged sediment transport rate. Sediment mobility in patches was highly dependent on the patch's class and location relative to the thalweg and large roughness elements. Compared to deterministic formulations, the use of distributions of shear stress improved predictions of bedload transport in steep mountain channels.
Wear of sharp aggregates in a rotating drum

NASA Astrophysics Data System (ADS)

Deiros Quintanilla, Ivan; Combe, Gaël; Emeriault, Fabrice; Toni, Jean-Benoît; Voivret, Charles; Ferellec, Jean François

2017-06-01

Aggregates constituting ballast layer wear due to the continuous passage of trains and during the necessary maintenance operations of the track. In order to develop efficient solutions for ballasted tracks design and maintenance, a proper knowledge of the degradation laws of ballast grains is needed. In tribology, the amount of wear due to friction when two surfaces are in contact is classically predicted by Archard's equation. However, due to the continuous evolution of grain angularity and roughness, at the macro-scale wear coefficient cannot be assumed to remain constant, but will depend on the state of degradation of the grain surface. In order to adjust the model to this particular case, the Micro-Deval Attrition test is used. The rotating drum is stopped at intermediate stages and the amount of generated fine particles is measured. Thus the curve of mass loss along time is built. These results are then linked to Archard's model using the values of contact forces and relative displacements extracted from discrete element simulations. Finally, a morphology analysis is performed tracking shape and roughness parameters at different stages of degradation using X-ray tomography and a laser profilometer.
Electro and Magneto-Electropolished Surface Micro-Patterning on Binary and Ternary Nitinol

PubMed Central

Munroe, Norman; McGoron, Anthony

2012-01-01

In this study, an Atomic Force Microscopy (AFM) roughness analysis was performed on non-commercial Nitinol alloys with Electropolished (EP) and Magneto-Electropolished (MEP) surface treatments and commercially available stents by measuring Root-Mean-Square (RMS), Average Roughness (Ra), and Surface Area (SA) values at various dimensional areas on the alloy surfaces, ranging from (800 × 800 nm) to (115 × 115μm), and (800 × 800 nm) to (40 × 40 μm) on the commercial stents. Results showed that NiTi-Ta 10 wt% with an EP surface treatment yielded the highest overall roughness, while the NiTi-Cu 10 wt% alloy had the lowest roughness when analyzed over (115 × 115 μm). Scanning Electron Microscopy (SEM) and Energy Dispersive Spectroscopy (EDS) analysis revealed unique surface morphologies for surface treated alloys, as well as an aggregation of ternary elements Cr and Cu at grain boundaries in MEP and EP surface treated alloys, and non-surface treated alloys. Such surface micro-patterning on ternary Nitinol alloys could increase cellular adhesion and accelerate surface endothelialization of endovascular stents, thus reducing the likelihood of in-stent restenosis and provide insight into hemodynamic flow regimes and the corrosion behavior of an implantable device influenced from such surface micro-patterns. PMID:22754200
Slippery surfaces of pitcher plants: Nepenthes wax crystals minimize insect attachment via microscopic surface roughness.

PubMed

Scholz, I; Bückins, M; Dolge, L; Erlinghagen, T; Weth, A; Hischen, F; Mayer, J; Hoffmann, S; Riederer, M; Riedel, M; Baumgartner, W

2010-04-01

Pitcher plants of the genus Nepenthes efficiently trap and retain insect prey in highly specialized leaves. Besides a slippery peristome which inhibits adhesion of insects they employ epicuticular wax crystals on the inner walls of the conductive zone of the pitchers to hamper insect attachment by adhesive devices. It has been proposed that the detachment of individual crystals and the resulting contamination of adhesive organs is responsible for capturing insects. However, our results provide evidence in favour of a different mechanism, mainly based on the stability and the roughness of the waxy surface. First, we were unable to detect a large quantity of crystal fragments on the pads of insects detached from mature pitcher surfaces of Nepenthes alata. Second, investigation of the pitcher surface by focused ion beam treatment showed that the wax crystals form a compact 3D structure. Third, atomic force microscopy of the platelet-shaped crystals revealed that the crystals are mechanically stable, rendering crystal detachment by insect pads unlikely. Fourth, the surface profile parameters of the wax layer showed striking similarities to those of polishing paper with low grain size. By measuring friction forces of insects on this artificial surface we demonstrate that microscopic roughness alone is sufficient to minimize insect attachment. A theoretical model shows that surface roughness within a certain length scale will prevent adhesion by being too rough for adhesive pads but not rough enough for claws.
Structure evolution of zinc oxide thin films deposited by unbalance DC magnetron sputtering

DOE Office of Scientific and Technical Information (OSTI.GOV)

Aryanto, Didik, E-mail: didi027@lipi.go.id; Materials Research Group, Physics Department, Universitas Negeri Semarang, Gunungpati, Semarang 50229 Jawa Tengah; Marwoto, Putut

Zinc oxide (ZnO) thin films are deposited on corning glass substrates using unbalanced DC magnetron sputtering. The effect of growth temperature on surface morphology and crystallographic orientation of ZnO thin film is studied using atomic force microscopy (AFM) and X-ray diffraction (XRD) techniques. The surface morphology and crystallographic orientation of ZnO thin film are transformed against the increasing of growth temperature. The mean grain size of film and the surface roughness are inversely and directly proportional towards the growth temperature from room temperature to 300 °C, respectively. The smaller grain size and finer roughness of ZnO thin film are obtainedmore » at growth temperature of 400 °C. The result of AFM analysis is in good agreement with the result of XRD analysis. ZnO thin films deposited in a series of growth temperatures have hexagonal wurtzite polycrystalline structures and they exhibit transformations in the crystallographic orientation. The results in this study reveal that the growth temperature strongly influences the surface morphology and crystallographic orientation of ZnO thin film.« less
Phase-field study of grain boundary tracking behavior in crack-seal microstructures

NASA Astrophysics Data System (ADS)

Ankit, Kumar; Nestler, Britta; Selzer, Michael; Reichardt, Mathias

2013-12-01

In order to address the growth of crystals in veins, a multiphase-field model is used to capture the dynamics of crystals precipitating from a super-saturated solution. To gain a detailed understanding of the polycrystal growth phenomena in veins, we investigate the influence of various boundary conditions on crystal growth. In particular, we analyze the formation of vein microstructures resulting from the free growth of crystals as well as crack-sealing processes. We define the crystal symmetry by considering the anisotropy in surface energy to simulate crystals with flat facets and sharp corners. The resulting growth competition of crystals with different orientations is studied to deduce a consistent orientation selection rule in the free-growth regime. Using crack-sealing simulations, we correlate the grain boundary tracking behavior depending on the relative rate of crack opening, opening trajectory, initial grain size, and wall roughness. Further, we illustrate how these parameters induce the microstructural transition between blocky (crystals growing anisotropically) to fibrous morphology (isotropic) and formation of grain boundaries. The phase-field simulations of crystals in the free-growth regime (in 2D and 3D) indicate that the growth or consumption of a crystal is dependent on the orientation difference with neighboring crystals. The crack-sealing simulation results (in 2D and 3D) reveal that crystals grow isotropically and grain boundaries track the opening trajectory if the wall roughness is high, opening increments are small, and crystals touch the wall before the next crack increment starts. Further, we find that within the complete crack-seal regime, anisotropy in surface energy results in the formation of curved/oscillating grain boundaries (instead of straight) when the crack-opening velocity is increased and wall roughness is not sufficiently high. Additionally, the overall capability of phase-field method to simulate large-scale polycrystal growth in veins (in 3D) is demonstrated enumerating the main advantages of adopting the novel approach.
On the surface roughness of a braidplain in an Alpine proglacial area

NASA Astrophysics Data System (ADS)

Baewert, H.; Morche, D.; Culha, C.

2014-12-01

Surface roughness is a crucial parameter of studies concerning (paleo) flood peak discharge estimation and related factors (cf. stream power). Usually, the analysis requires preliminary knowledge of grain size distribution of the study site. However, in some cases this is impractical, especially when investigating large areas, or even impossible due to inaccessibility. In addition, the particles in the channel are usually hidden by other particles or incorporated into finer sediment. Therefore, removing particles from the channel bottom is not suitable, because it falsifies the results. Here, the application of noninvasive terrestrial laser scanning (TLS) offers new possibilities. The indirect recording of the surface leads to a significant reduction of the workload. Furthermore, form roughness and burial/imbrication are taken into account. However, there are some disadvantages in using TLS. The resolution of the TLS data is a limiting factor when defining surface roughness, because coarseness at finer detail will not be captured at lower resolution (Baewert et al. 2014). There are numerous other factors, which may alter the results. We would like to further understand how the noise associated with TLS data alters the outcome and whether the interpolation method has an influence. This study focuses on the latter two issues. For this purpose, a braidplain in the forefield of the glacier Gepatschferner in Austria was surveyed using a terrestrial laser scanner. The images were taken from different angles and with different resolutions. Subsequently, the outliers are removed from the point cloud in order to investigate the influence of the noise. Thinning the point cloud is another method used to understand the effects of the point density. References Baewert, H., Bimböse, M., Bryk, A., Rascher, E., Schmidt, K.-H. & Morche, D. (2014): Roughness determination of coarse grained alpine river bed surfaces using Terrestrial Laser Scanning data. - Zeitschrift für Geomorphologie N.F. 58(1): 81-95. Doi: 10.1127/0372-8854/2013/S-00127 .
Effect of Machining Parameters on Oxidation Behavior of Mild Steel

NASA Astrophysics Data System (ADS)

Majumdar, P.; Shekhar, S.; Mondal, K.

2015-01-01

This study aims to find out a correlation between machining parameters, resultant microstructure, and isothermal oxidation behavior of lathe-machined mild steel in the temperature range of 660-710 °C. The tool rake angles "α" used were +20°, 0°, and -20°, and cutting speeds used were 41, 232, and 541 mm/s. Under isothermal conditions, non-machined and machined mild steel samples follow parabolic oxidation kinetics with activation energy of 181 and ~400 kJ/mol, respectively. Exaggerated grain growth of the machined surface was observed, whereas, the center part of the machined sample showed minimal grain growth during oxidation at higher temperatures. Grain growth on the surface was attributed to the reduction of strain energy at high temperature oxidation, which was accumulated on the sub-region of the machined surface during machining. It was also observed that characteristic surface oxide controlled the oxidation behavior of the machined samples. This study clearly demonstrates the effect of equivalent strain, roughness, and grain size due to machining, and subsequent grain growth on the oxidation behavior of the mild steel.

Origins of Folding Instabilities on Polycrystalline Metal Surfaces

NASA Astrophysics Data System (ADS)

Beckmann, N.; Romero, P. A.; Linsler, D.; Dienwiebel, M.; Stolz, U.; Moseler, M.; Gumbsch, P.

2014-12-01

Wear and removal of material from polycrystalline metal surfaces is inherently connected to plastic flow. Here, plowing-induced unconstrained surface plastic flow on a nanocrystalline copper surface has been studied by massive molecular dynamics simulations and atomic force microscopy scratch experiments. In agreement with experimental findings, bulges in front of a model asperity develop into vortexlike fold patterns that mark the disruption of laminar flow. We identify dislocation-mediated plastic flow in grains with suitably oriented slip systems as the basic mechanism of bulging and fold formation. The observed folding can be fundamentally explained by the inhomogeneity of plasticity on polycrystalline surfaces which favors bulge formation on grains with suitably oriented slip system. This process is clearly distinct from Kelvin-Helmholtz instabilities in fluids, which have been previously suggested to resemble the formed surface fold patterns. The generated prow grows into a rough chip with stratified lamellae that are identified as the precursors of wear debris. Our findings demonstrate the importance of surface texture and grain structure engineering to achieve ultralow wear in metals.
Nanoscale Investigation of Grain Growth in RF-Sputtered Indium Tin Oxide Thin Films by Scanning Probe Microscopy

NASA Astrophysics Data System (ADS)

Lamsal, B. S.; Dubey, M.; Swaminathan, V.; Huh, Y.; Galipeau, D.; Qiao, Q.; Fan, Q. H.

2014-11-01

This work studied the electronic characteristics of the grains and grain boundaries of indium tin oxide (ITO) thin films using electrostatic and Kelvin probe force microscopy. Two types of ITO films were compared, deposited using radiofrequency magnetron sputtering in pure argon or 99% argon + 1% oxygen, respectively. The average grain size and surface roughness increased with substrate temperature for the films deposited in pure argon. With the addition of 1% oxygen, the increase in the grain size was inhibited above 150°C, which was suggested to be due to passivation of the grains by the excess oxygen. Electrostatic force microscopy and Kelvin probe force microscopy (KPFM) images confirmed that the grain growth was defect mediated and occurred at defective interfaces at high temperatures. Films deposited at room temperature with 1% oxygen showed crystalline nature, while films deposited with pure argon at room temperature were amorphous as observed from KPFM images. The potential drop across the grain and grain boundary was determined by taking surface potential line profiles to evaluate the electronic properties.
Structural properties 3,16-bis triisopropylsilylethynyl (pentacene) (TIPS-pentacene) thin films onto organic dielectric layer using slide coating method

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rusnan, Fara Naila; Mohamad, Khairul Anuar; Seria, Dzul Fahmi Mohd Husin

3,16-bis triisopropylsilylethynyl (Pentacene) (TIPS-Pentacene) compactable interface property is important in order to have a good arrangement of molecular structure. Comparison for TIPS-Pentacene deposited between two different surface layers conducted. 0.1wt% TIPS-Pentacene diluted in chloroform were deposited onto poly(methylmeaclyrate) (PMMA) layered transparent substrates using slide coating method. X-ray diffraction (XRD) used to determine crystallinity of thin films. Series of (00l) diffraction peaks obtained with sharp first peaks (001) for TIPS-Pentacene deposited onto PMMA layer at 5.35° and separation of 16.3 Å. Morphology and surface roughness were carried out using scanning electron microscope (SEM) and surface profilemeter LS500, respectively.TIPS-Pentacene deposited onto PMMAmore » layer formed needled-like-shape grains with 10.26 nm surface roughness. These properties were related as thin film formed and its surface roughness plays important role towards good mobility devices.« less
Oxidant effect of La(NO3)3·6H2O solution on the crystalline characteristics of nanocrystalline ZrO2 films grown by atomic layer deposition

NASA Astrophysics Data System (ADS)

Oh, Nam Khen; Kim, Jin-Tae; Kang, Goru; An, Jong-Ki; Nam, Minwoo; Kim, So Yeon; Park, In-Sung; Yun, Ju-Young

2017-02-01

Nanocrystalline ZrO2 films were synthesized by atomic layer deposition method using CpZr[N(CH3)2]3 (Cp = C5H5) as the metal precursor and La(NO3)3·6H2O solution as the oxygen source. La element in the deposited ZrO2 films could not be detected as its content was below the resolution limit of the X-ray photoelectron spectroscopy. The alternative introduction of La(NO3)3·6H2O solution to conventionally used H2O as the oxidant effectively altered the crystalline structure, grain size, and surface roughness of the grown ZrO2 films. Specifically, the crystalline structure of the ZrO2 film changed from a mixture of tetragonal and monoclinic phases to monoclinic phase. The average grain size also increased, and the resulting film surface became rougher. The average grain sizes of the ZrO2 films prepared from La(NO3)3·6H2O solution at concentrations of 10, 20, 30, and 40% were 280, 256, 208, and 200 nm, respectively, whereas that prepared using H2O oxidant was 142 nm. However, the concentration of La(NO3)3·6H2O solution minimally influenced the crystalline characteristics of the nanocrystalline ZrO2 films i.e., the crystalline structure, grain size, and surface roughness except for crystallite size.
Experimental and Numerical Analysis of Microstructures and Stress States of Shot-Peened GH4169 Superalloys

NASA Astrophysics Data System (ADS)

Hu, Dianyin; Gao, Ye; Meng, Fanchao; Song, Jun; Wang, Rongqiao

2018-04-01

Combining experiments and finite element analysis (FEA), a systematic study was performed to analyze the microstructural evolution and stress states of shot-peened GH4169 superalloy over a variety of peening intensities and coverages. A dislocation density evolution model was integrated into the representative volume FEA model to quantitatively predict microstructural evolution in the surface layers and compared with experimental results. It was found that surface roughness and through-depth residual stress profile are more sensitive to shot-peening intensity compared to coverage due to the high kinetic energy involved. Moreover, a surface nanocrystallization layer was discovered in the top surface region of GH4169 for all shot-peening conditions. However, the grain refinement was more intensified under high shot-peening coverage, under which enough time was permitted for grain refinement. The grain size gradient predicted by the numerical framework showed good agreement with experimental observations.
Uncertainty quantification-based robust aerodynamic optimization of laminar flow nacelle

NASA Astrophysics Data System (ADS)

Xiong, Neng; Tao, Yang; Liu, Zhiyong; Lin, Jun

2018-05-01

The aerodynamic performance of laminar flow nacelle is highly sensitive to uncertain working conditions, especially the surface roughness. An efficient robust aerodynamic optimization method on the basis of non-deterministic computational fluid dynamic (CFD) simulation and Efficient Global Optimization (EGO)algorithm was employed. A non-intrusive polynomial chaos method is used in conjunction with an existing well-verified CFD module to quantify the uncertainty propagation in the flow field. This paper investigates the roughness modeling behavior with the γ-Ret shear stress transport model including modeling flow transition and surface roughness effects. The roughness effects are modeled to simulate sand grain roughness. A Class-Shape Transformation-based parametrical description of the nacelle contour as part of an automatic design evaluation process is presented. A Design-of-Experiments (DoE) was performed and surrogate model by Kriging method was built. The new design nacelle process demonstrates that significant improvements of both mean and variance of the efficiency are achieved and the proposed method can be applied to laminar flow nacelle design successfully.
Influence of Under-layer Morphology on Structural and Magnetic Properties of Sputtered Co81Pd19 Films

NASA Astrophysics Data System (ADS)

Ponchaiya, Pairin; Rattanasakulthong, Watcharee

2017-09-01

Sputtered Co81Pd19 films with thickness of about 60 nm were deposited on various under-layers (Co, Ni, Cr and Al) and on glass substrate. Structural, morphological and magnetic properties of Co81Pd19 films were investigated. All of prepared Co81Pd19 film showed CoPd-FCC phase in (111) direction on CoO-FCC (111), NiO-FCC (200), Cr-BCC (200) and (201) and AlO-FCC (200) phases of Co, Ni, Cr and Al under-layer, respectively. AFM images revealed that the film on Cr under-layers and glass substrate exhibited the maximum roughness with the highest grain size and the minimum roughness with the continuous grain size, respectively. Both parallel and perpendicular maximum coercive field were found in the film on glass under-layer and the film on Co-under-layer film showed the highest saturation magnetization from both in-plane and out-of-plane measurements. These results confirmed that the structural and magnetic properties of sputtered Co81Pd19 films were affected by under-layer surface roughness and morphology by the virtue of particle size and distribution on the under-layer film surface.
Simplified Approach to Predicting Rough Surface Transition

NASA Technical Reports Server (NTRS)

Boyle, Robert J.; Stripf, Matthias

2009-01-01

Turbine vane heat transfer predictions are given for smooth and rough vanes where the experimental data show transition moving forward on the vane as the surface roughness physical height increases. Consiste nt with smooth vane heat transfer, the transition moves forward for a fixed roughness height as the Reynolds number increases. Comparison s are presented with published experimental data. Some of the data ar e for a regular roughness geometry with a range of roughness heights, Reynolds numbers, and inlet turbulence intensities. The approach ta ken in this analysis is to treat the roughness in a statistical sense , consistent with what would be obtained from blades measured after e xposure to actual engine environments. An approach is given to determ ine the equivalent sand grain roughness from the statistics of the re gular geometry. This approach is guided by the experimental data. A roughness transition criterion is developed, and comparisons are made with experimental data over the entire range of experimental test co nditions. Additional comparisons are made with experimental heat tran sfer data, where the roughness geometries are both regular as well a s statistical. Using the developed analysis, heat transfer calculatio ns are presented for the second stage vane of a high pressure turbine at hypothetical engine conditions.
A Numerical Wind Tunnel Study of Viscous-Inviscid Interaction

DTIC Science & Technology

1992-01-01

partially successful. In Task 1 we devised surface boundary conditions for the multiscale model including effects of roughness and blowing. This work tied up ...directed at cleaning up some loose ends in de- veloping the Wilcox multiscale model (see Appendix R). The most significant issue was the development of...the following correlation between SR and k , will reproduce measured effects of sand-grain roughness for values of k up to about 400. ( k, ញ SiR (42
Enhanced Hydrogen Transport over Palladium Ultrathin Films through Surface Nanostructure Engineering.

PubMed

Abate, Salvatore; Giorgianni, Gianfranco; Gentiluomo, Serena; Centi, Gabriele; Perathoner, Siglinda

2015-11-01

Palladium ultrathin films (around 2 μm) with different surface nanostructures are characterized by TEM, SEM, AFM, and temperature programmed reduction (TPR), and evaluated in terms of H2 permeability and H2-N2 separation. A change in the characteristics of Pd seeds by controlled oxidation-reduction treatments produces films with the same thickness, but different surface and bulk nanostructure. In particular, the films have finer and more homogeneous Pd grains, which results in lower surface roughness. Although all samples show high permeo-selectivity to H2 , the samples with finer grains exhibit enhanced permeance and lower activation energy for H2 transport. The analysis of the data suggests that grain boundaries between the Pd grains at the surface favor H2 transfer from surface to subsurface. Thus, the surface nanostructure plays a relevant role in enhancing the transport of H2 over the Pd ultrathin film, which is an important aspect to develop improved membranes that function at low temperatures and toward new integrated process architectures in H2 and syngas production with enhanced sustainability. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
Microstructural Evolution at Micro/Meso-Scale in an Ultrafine-Grained Pure Aluminum Processed by Equal-Channel Angular Pressing with Subsequent Annealing Treatment.

PubMed

Xu, Jie; Li, Jianwei; Zhu, Xiaocheng; Fan, Guohua; Shan, Debin; Guo, Bin

2015-11-04

Micro-forming with ultrafine-grained (UFG) materials is a promising direction for the fabrication of micro-electro-mechanical systems (MEMS) components due to the improved formability, good surface quality, and excellent mechanical properties it provides. In this paper, micro-compression tests were performed using UFG pure aluminum processed by equal-channel angular pressing (ECAP) with subsequent annealing treatment. Microstructural evolution was investigated by electron back-scattered diffraction (EBSD) and transmission electron microscopy (TEM). The results show that microstructural evolutions during compression tests at the micro/meso-scale in UFG pure Al are absolutely different from the coarse-grained (CG) materials. A lot of low-angle grain boundaries (LAGBs) and recrystallized fine grains are formed inside of the original large grains in CG pure aluminum after micro-compression. By contrast, ultrafine grains are kept with few sub-grain boundaries inside the grains in UFG pure aluminum, which are similar to the original microstructure before micro-compression. The surface roughness and coordinated deformation ability can be signmicrostructure; micro/meso-forming; ultrafine grains; ECAP; aluminumificantly improved with UFG pure aluminum, which demonstrates that the UFG materials have a strong potential application in micro/meso-forming.
Estimating Discharge, Depth and Bottom Friction in Sand Bed Rivers Using Surface Currents and Water Surface Elevation Observations

NASA Astrophysics Data System (ADS)

Simeonov, J.; Czapiga, M. J.; Holland, K. T.

2017-12-01

We developed an inversion model for river bathymetry estimation using measurements of surface currents, water surface elevation slope and shoreline position. The inversion scheme is based on explicit velocity-depth and velocity-slope relationships derived from the along-channel momentum balance and mass conservation. The velocity-depth relationship requires the discharge value to quantitatively relate the depth to the measured velocity field. The ratio of the discharge and the bottom friction enter as a coefficient in the velocity-slope relationship and is determined by minimizing the difference between the predicted and the measured streamwise variation of the total head. Completing the inversion requires an estimate of the bulk friction, which in the case of sand bed rivers is a strong function of the size of dune bedforms. We explored the accuracy of existing and new empirical closures that relate the bulk roughness to parameters such as the median grain size diameter, ratio of shear velocity to sediment fall velocity or the Froude number. For given roughness parameterization, the inversion solution is determined iteratively since the hydraulic roughness depends on the unknown depth. We first test the new hydraulic roughness parameterization using estimates of the Manning roughness in sand bed rivers based on field measurements. The coupled inversion and roughness model is then tested using in situ and remote sensing measurements of the Kootenai River east of Bonners Ferry, ID.
NASA Cold Land Processes Experiment (CLPX 2002/03): Field measurements of snowpack properties and soil moisture

Treesearch

Kelly Elder; Don Cline; Glen E. Liston; Richard Armstrong

2009-01-01

A field measurement program was undertaken as part NASA's Cold Land Processes Experiment (CLPX). Extensive snowpack and soil measurements were taken at field sites in Colorado over four study periods during the two study years (2002 and 2003). Measurements included snow depth, density, temperature, grain type and size, surface wetness, surface roughness, and...
RANS Based Methodology for Predicting the Influence of Leading Edge Erosion on Airfoil Performance

DOE Office of Scientific and Technical Information (OSTI.GOV)

Langel, Christopher M.; Chow, Raymond C.; van Dam, C. P.

The impact of surface roughness on flows over aerodynamically designed surfaces is of interested in a number of different fields. It has long been known the surface roughness will likely accelerate the laminar- turbulent transition process by creating additional disturbances in the boundary layer. However, there are very few tools available to predict the effects surface roughness will have on boundary layer flow. There are numerous implications of the premature appearance of a turbulent boundary layer. Increases in local skin friction, boundary layer thickness, and turbulent mixing can impact global flow properties compounding the effects of surface roughness. With thismore » motivation, an investigation into the effects of surface roughness on boundary layer transition has been conducted. The effort involved both an extensive experimental campaign, and the development of a high fidelity roughness model implemented in a R ANS solver. Vast a mounts of experimental data was generated at the Texas A&M Oran W. Nicks Low Speed Wind Tunnel for the calibration and validation of the roughness model described in this work, as well as future efforts. The present work focuses on the development of the computational model including a description of the calibration process. The primary methodology presented introduces a scalar field variable and associated transport equation that interacts with a correlation based transition model. The additional equation allows for non-local effects of surface roughness to be accounted for downstream of rough wall sections while maintaining a "local" formulation. The scalar field is determined through a boundary condition function that has been calibrated to flat plate cases with sand grain roughness. The model was initially tested on a NACA 0012 airfoil with roughness strips applied to the leading edge. Further calibration of the roughness model was performed using results from the companion experimental study on a NACA 63 3 -418 airfoil. The refined model demonstrates favorable agreement predicting changes to the transition location, as well as drag, for a number of different leading edge roughness configurations on the NACA 63 3-418 airfoil. Additional tests were conducted on a thicker S814 airfoil, with similar roughness configurations to the NACA 63 3-418. Simulations run with the roughness model compare favorably with the results obtained in the experimental study for both airfoils.« less
How does substrate roughness affect the service life of a superhydrophobic coating?

NASA Astrophysics Data System (ADS)

Zhang, Xin; Mo, Jiliang; Si, Yifan; Guo, Zhiguang

2018-05-01

Although the development of superhydrophobic coatings is rapidly maturing, issues related to their low mechanical durability persist. In this context, the effect of substrate roughness on the service life of superhydrophobic coatings was studied. In this study, superhydrophobic coatings were fabricated on sandpapers of different roughness and reciprocating wear tests were conducted. The wear-resistance number of the superhydrophobic coating, defined as the maximum number of friction cycles after which the superhydrophobic surface started to lose its superhydrophobicity, increased from 50 to 24,000 with an increase in the substrate roughness from 2000 CW to 240 CW (CW is defined as the number of particles arranged in an inch), while it decreased from 24,000 to 17,000 with a further increase in the substrate roughness from 240 CW to 60 CW. Observations of the surface structure and wear analyses indicated that the superhydrophobic material infiltrated the spaces between the sand grains, and the rough peaks could consequently protect the superhydrophobic material during the wear tests. However, this protection weakens when the substrate roughness increases or decreases beyond certain values. Furthermore, these phenomena and results were also verified by applying the superhydrophobic coatings to different types of common substrates.
The effect of copper substrate’s roughness on graphene growth process via PECVD

NASA Astrophysics Data System (ADS)

Fan, Tengfei; Yan, Cuixia; Lu, Jianchen; Zhang, Lianchang; Cai, Jinming

2018-04-01

Despite many excellent properties, the synthesis of high quality graphene with low-cost way is still a challenge, thus many different factors have been researched. In this work, the effect of surface roughness to the graphene quality was studied. Graphene was synthesized by plasma enhanced chemical vapor deposition (PECVD) method on copper substrates with different roughness from 0.074 μm to 0.339 μm, which were prepared via annealing, corrosion or polishing, respectively. Ar+ plasma cleaning was applied before graphene growth in order to accommodate similar surface chemical reactivity to each other. Scanning electron microscope and Raman spectroscope were employed to investigate the effect of surface roughness, which reveals that the graphene quality decrease first and then increase again according to the ratio of ID/IG in Raman spectroscopy. When the ratio of ID/IG reaches the largest number, the substrate roughness is 0.127 μm, where is the graphene quality changing point. First principle calculation was applied to explain the phenomenon and revealed that it is strongly affected by the graphene grain size and quantity which can induce defects. This strategy is expected to guide the industrial production of graphene.
Chemical weathering rates of a soil chronosequence on granitic alluvium: I. Quantification of mineralogical and surface area changes and calculation of primary silicate reaction rates

USGS Publications Warehouse

White, A.F.; Blum, A.E.; Schulz, M.S.; Bullen, T.D.; Harden, J.W.; Peterson, M.L.

1996-01-01

Mineral weathering rates are determined for a series of soils ranging in age from 0.2-3000 Ky developed on alluvial terraces near Merced in the Central Valley of California. Mineralogical and elemental abundances exhibit time-dependent trends documenting the chemical evolution of granitic sand to residual kaolinite and quartz. Mineral losses with time occur in the order: hornblende > plagioclase > K-feldspar. Maximum volume decreases of >50% occur in the older soils. BET surface areas of the bulk soils increase with age, as do specific surface areas of aluminosilicate mineral fractions such as plagioclase, which increases from 0.4-1.5 m2 g-1 over 600 Ky. Quartz surface areas are lower and change less with time (0.11-0.23 m2 g-1). BET surface areas correspond to increasing external surface roughness (?? = 10-600) and relatively constant internal surface area (??? 1.3 m2 g-1). SEM observations confirm both surface pitting and development of internal porosity. A numerical model describes aluminosilicate dissolution rates as a function of changes in residual mineral abundance, grain size distributions, and mineral surface areas with time. A simple geometric treatment, assuming spherical grains and no surface roughness, predicts average dissolution rates (plagioclase, 10-17.4; K-feldspar, 10-17.8; and hornblende, 10-17.5 mol cm-1 s-1) that are constant with time and comparable to previous estimates of soil weathering. Average rates, based on BET surface area measurements and variable surface roughnesses, are much slower (plagioclase, 10-19.9; K-feldspar, 10-20.5; and hornblende 10-20.1 mol cm-2 s-1). Rates for individual soil horizons decrease by a factor of 101.5 over 3000 Ky indicating that the surface reactivities of minerals decrease as the physical surface areas increase. Rate constants based on BET estimates for the Merced soils are factors of 103-104 slower than reported experimental dissolution rates determined from freshly prepared silicates with low surface roughness (?? <10). This study demonstrates that the utility of experimental rate constants to predict weathering in soils is limited without consideration of variable surface areas and processes that control the evolution of surface reactivity with time.
Variations in Surface Texture of the North Polar Residual Cap of Mars

NASA Technical Reports Server (NTRS)

Milkovich, S. M.; Byrne, S.; Russell, P. S.

2011-01-01

The northern polar residual cap (NPRC) of Mars is a water ice deposit with a rough surface made up of pits, knobs, and linear depressions on scales of tens of meters. This roughness manifests as a series of bright mounds and dark hollows in visible images; these bright and dark patches have a characteristic wavelength and orientation. Spectral data indicate that the surface of the NPRC is composed of large-grained (and therefore old) water ice. Due to the presence of this old ice, it is thought that the NPRC is in a current state of net loss of material a result potentially at odds with impact crater statistics, which suggest ongoing deposition over the past 10-20 Kyr.
High Stability Pentacene Transistors Using Polymeric Dielectric Surface Modifier.

PubMed

Wang, Xiaohong; Lin, Guangqing; Li, Peng; Lv, Guoqiang; Qiu, Longzhen; Ding, Yunsheng

2015-08-01

1,6-bis(trichlorosilyl)hexane (C6Cl), polystyrene (PS), and cross-linked polystyrene (CPS) were investigated as gate dielectric modified layers for high performance organic transistors. The influence of the surface energy, roughness and morphology on the charge transport of the organic thin-film transistors (OTFTs) was investigated. The surface energy and roughness both affect the grain size of the pentacene films which will control the charge carrier mobility of the devices. Pentacene thin-film transistors fabricated on the CPS modified dielectric layers exhibited charge carrier mobility as high as 1.11 cm2 V-1 s-1. The bias stress stability for the CPS devices shows that the drain current only decays 1% after 1530 s and the mobility never decreases until 13530 s.
The Effects of Acid Etching on the Nanomorphological Surface Characteristics and Activation Energy of Titanium Medical Materials.

PubMed

Hung, Kuo-Yung; Lin, Yi-Chih; Feng, Hui-Ping

2017-10-11

The purpose of this study was to characterize the etching mechanism, namely, the etching rate and the activation energy, of a titanium dental implant in concentrated acid and to construct the relation between the activation energy and the nanoscale surface topographies. A commercially-pure titanium (CP Ti) and Ti-6Al-4V ELI surface were tested by shot blasting (pressure, grain size, blasting distance, blasting angle, and time) and acid etching to study its topographical, weight loss, surface roughness, and activation energy. An Arrhenius equation was applied to derive the activation energy for the dissolution of CP Ti/Ti-6Al-4V ELI in sulfuric acid (H₂SO₄) and hydrochloric acid (HCl) at different temperatures. In addition, white-light interferometry was applied to measure the surface nanomorphology of the implant to obtain 2D or 3D roughness parameters (Sa, Sq, and St). The nanopore size that formed after etching was approximately 100-500 nm. The surface roughness of CP Ti and Ti-6Al-4V ELI decreased as the activation energy decreased but weight loss increased. Ti-6Al-4V ELI has a higher level of activation energy than Ti in HCl, which results in lower surface roughness after acid etching. This study also indicates that etching using a concentrated hydrochloric acid provided superior surface modification effects in titanium compared with H₂SO₄.

Engineered plant biomass feedstock particles

DOEpatents

Dooley, James H [Federal Way, WA; Lanning, David N [Federal Way, WA; Broderick, Thomas F [Lake Forest Park, WA

2011-10-18

A novel class of flowable biomass feedstock particles with unusually large surface areas that can be manufactured in remarkably uniform sizes using low-energy comminution techniques. The feedstock particles are roughly parallelepiped in shape and characterized by a length dimension (L) aligned substantially with the grain direction and defining a substantially uniform distance along the grain, a width dimension (W) normal to L and aligned cross grain, and a height dimension (H) normal to W and L. The particles exhibit a disrupted grain structure with prominent end and surface checks that greatly enhances their skeletal surface area as compared to their envelope surface area. The L.times.H dimensions define a pair of substantially parallel side surfaces characterized by substantially intact longitudinally arrayed fibers. The W.times.H dimensions define a pair of substantially parallel end surfaces characterized by crosscut fibers and end checking between fibers. The L.times.W dimensions define a pair of substantially parallel top surfaces characterized by some surface checking between longitudinally arrayed fibers. At least 80% of the particles pass through a 1/4 inch screen having a 6.3 mm nominal sieve opening but are retained by a No. 10 screen having a 2 mm nominal sieve opening. The feedstock particles are manufactured from a variety of plant biomass materials including wood, crop residues, plantation grasses, hemp, bagasse, and bamboo.
Surface roughness of zirconia for full-contour crowns after clinically simulated grinding and polishing.

PubMed

Hmaidouch, Rim; Müller, Wolf-Dieter; Lauer, Hans-Christoph; Weigl, Paul

2014-12-01

The aim of this study was to evaluate the effect of controlled intraoral grinding and polishing on the roughness of full-contour zirconia compared to classical veneered zirconia. Thirty bar-shaped zirconia specimens were fabricated and divided into two groups (n=15). Fifteen specimens (group 1) were glazed and 15 specimens (group 2) were veneered with feldspathic ceramic and then glazed. Prior to grinding, maximum roughness depth (Rmax) values were measured using a profilometer, 5 times per specimen. Simulated clinical grinding and polishing were performed on the specimens under water coolant for 15 s and 2 N pressure. For grinding, NTI diamonds burs with grain sizes of 20 µm, 10 µm, and 7.5 µm were used sequentially. The ground surfaces were polished using NTI kits with coarse, medium and fine polishers. After each step, Rmax values were determined. Differences between groups were examined using one-way analysis of variance (ANOVA). The roughness of group 1 was significantly lower than that of group 2. The roughness increased significantly after coarse grinding in both groups. The results after glazing were similar to those obtained after fine grinding for non-veneered zirconia. However, fine-ground veneered zirconia had significantly higher roughness than venerred, glazed zirconia. No significant difference was found between fine-polished and glazed zirconia, but after the fine polishing of veneered zirconia, the roughness was significantly higher than after glazing. It can be concluded that for full-contour zirconia, fewer defects and lower roughness values resulted after grinding and polishing compared to veneered zirconia. After polishing zirconia, lower roughness values were achieved compared to glazing; more interesting was that the grinding of glazed zirconia using the NTI three-step system could deliver smooth surfaces comparable to untreated glazed zirconia surfaces.
Surface roughness of zirconia for full-contour crowns after clinically simulated grinding and polishing

PubMed Central

Hmaidouch, Rim; Müller, Wolf-Dieter; Lauer, Hans-Christoph; Weigl, Paul

2014-01-01

The aim of this study was to evaluate the effect of controlled intraoral grinding and polishing on the roughness of full-contour zirconia compared to classical veneered zirconia. Thirty bar-shaped zirconia specimens were fabricated and divided into two groups (n=15). Fifteen specimens (group 1) were glazed and 15 specimens (group 2) were veneered with feldspathic ceramic and then glazed. Prior to grinding, maximum roughness depth (Rmax) values were measured using a profilometer, 5 times per specimen. Simulated clinical grinding and polishing were performed on the specimens under water coolant for 15 s and 2 N pressure. For grinding, NTI diamonds burs with grain sizes of 20 µm, 10 µm, and 7.5 µm were used sequentially. The ground surfaces were polished using NTI kits with coarse, medium and fine polishers. After each step, Rmax values were determined. Differences between groups were examined using one-way analysis of variance (ANOVA). The roughness of group 1 was significantly lower than that of group 2. The roughness increased significantly after coarse grinding in both groups. The results after glazing were similar to those obtained after fine grinding for non-veneered zirconia. However, fine-ground veneered zirconia had significantly higher roughness than venerred, glazed zirconia. No significant difference was found between fine-polished and glazed zirconia, but after the fine polishing of veneered zirconia, the roughness was significantly higher than after glazing. It can be concluded that for full-contour zirconia, fewer defects and lower roughness values resulted after grinding and polishing compared to veneered zirconia. After polishing zirconia, lower roughness values were achieved compared to glazing; more interesting was that the grinding of glazed zirconia using the NTI three-step system could deliver smooth surfaces comparable to untreated glazed zirconia surfaces. PMID:25059249
An intermittency model for predicting roughness induced transition

NASA Astrophysics Data System (ADS)

Ge, Xuan; Durbin, Paul

2014-11-01

An extended model for roughness-induced transition is proposed based on an intermittency transport equation for RANS modeling formulated in local variables. To predict roughness effects in the fully turbulent boundary layer, published boundary conditions for k and ω are used, which depend on the equivalent sand grain roughness height, and account for the effective displacement of wall distance origin. Similarly in our approach, wall distance in the transition model for smooth surfaces is modified by an effective origin, which depends on roughness. Flat plate test cases are computed to show that the proposed model is able to predict the transition onset in agreement with a data correlation of transition location versus roughness height, Reynolds number, and inlet turbulence intensity. Experimental data for a turbine cascade are compared with the predicted results to validate the applicability of the proposed model. Supported by NSF Award Number 1228195.
Grain-Boundary Roughening in Colloidal Crystals

NASA Astrophysics Data System (ADS)

Liao, Maijia; Xiao, Xiao; Chui, Siu Tat; Han, Yilong

2018-04-01

In polycrystals, faceted grains may become round and rough at high temperatures. Such a roughening phenomenon remains poorly understood, partly because of the lack of experimental observations. Here, we directly visualize the roughening dynamics of grain boundaries inside thin-film colloidal crystals at the single-particle level using video microscopy. The thermal fluctuations of grain boundaries appear to exhibit both static and dynamic critical-like behaviors, in contrast to the Kosterlitz-Thouless transition in typical free surface roughening. The roughening point shifts towards the melting point as the grain boundary's mismatch angle θ decreases and is preempted by melting when θ <18 ° . Counterintuitively, the amplitude of grain-boundary fluctuations decreases above the roughening point. This could be attributed to the observed widening of the grain boundary. The roughening strongly affects the mobility of the grain boundary but not the stiffness. These results provide new guidance for the control of microstructures in polycrystals and further development of roughening theory.
Surface optical properties of geological materials: a new look at the regolith of the Moon, Mercury and asteroids

NASA Astrophysics Data System (ADS)

Souchon, Audrey; Pinet, Patrick; Chevrel, Serge; Daydou, Yves; Josset, Jean-Luc; Beauvivre, Stephane

2010-05-01

With the exception of the lunar samples brought back to Earth, the only way to study the surface of a planet so far remains the use of remote-sensing techniques. Among them photometry can be used to determine the physical properties of surface particles (e.g., grain size, roughness…). Laboratory measurements with the spectro-imaging instrument at the DTP laboratory (Toulouse, France) have been made to determine the photometric parameters of natural samples (e.g., basalts, pyroclastics and olivine grains). Each one has been sieved either into natural grain sizes or ground to get particles from 45 microns to 2 mm. Multiangular data spanning the phase range between 20 and 130° have been acquired and Hapke's photometric parameters b, c, theta and w have been determined by means of a dedicated genetic algorithm [Cord, Icarus, 2003]. The modelled phase functions match satisfactorily the observations, and the parameters show very different behaviours depending on the sample and grain size. For non glassy materials, such as fresh basalt or pyroclastics, surface roughness parameter theta ranges from 12° to 25° with an increase seemingly correlated with the grain size, while for glassy materials, such as olivine or Hawaiian basalt, this parameter is much lower (about 4 to 10°) and shows no increase with grain size. Phase parameters b and c estimates displayed on a double Henyey-Greenstein graph (c vs. b) [see McGuire & Hapke, Icarus, 1995] fall on the expected trend, with glassy materials becoming more and more forward-scattering when grain size increases. Non glassy samples display more variability when particle size increases, and generally show a more backward-scattering behaviour. These results show that a characterization of a surface state in terms of physical properties is possible from multiangular datasets using Hapke's photometric model. The combination of photometric results with spectroscopic analyses could thus lead to more thorough understanding of remotely observed surfaces, as these techniques give access to complementary information. To date, few multiangular orbital datasets are available, with the additional difficulties that phase angles larger than 100° and less than 20° are more difficult to acquire than in laboratory experiments. In addition, high resolution topographic information is requested for this type of investigation. A study of multiangular imaging observations of the lunar crater Lavoisier recently made by the AMIE camera onboard the European spacecraft SMART-1 has been undertaken, with phase angles ranging from 26° to 83°. Despite this limited phase coverage, a first-order photometric survey has been carried out. Dark patches believed to be pyroclastic deposits [Gaddis, Icarus, 2003] show similar photometric behaviour (backward scattering, high surface roughness); another dark region within Lavoisier F crater appears to display an even higher surface roughness, associated with a less pronounced backward scattering. The fact that both the modelled phase curves match well the observation and the retrieved parameters are physically plausible, suggests that Hapke's model not only can be applied to laboratory data, but also to orbital imaging datasets. As more complete sets will be produced from ongoing or soon-to-come observations (e.g., Kaguya/Selene, Chandra'yaan, LRO for the Moon, Messenger, Bepi-Colombo for Mercury, Dawn for Vesta and Ceres, …), a more precise characterization of planetary surfaces should be achieved.
The use of the durometer to measure rock hardness in geomorphology. Advantages and limitations.

NASA Astrophysics Data System (ADS)

Feal-Pérez, Alejandra; Blanco-Chao, Ramón; Valcarcel-Díaz, Marcos; Combes, Martín. A.

2010-05-01

The durometer is a hardness tester developed to measure hardness of metallic materials that has been recently introduced to measure rock hardness in weathering studies. Aoki & Matsukura (2007) highlight some advantages of the durometer compared with the Schmidt Rock Test Hammer: the smaller plunge allows measurements in small surfaces such as taffoni or rock carvings, the wider measurement range and the lower impact energy. This last makes it a non destructive method that can be used on relatively soft rocks. In this work the durometer Equotip (©) has been tested in different environments in the field and in the laboratory to explore its applicability and limitations. We applied the device on small rock samples of granite and limestone and a T-test showed that smaller sample size gave smaller hardness values (p < 0.01). Testing the effects of water content, there were no statistically significant differences between water saturated and dry samples. The influence of rock surface roughness was evaluated applying the durometer in ancient rock carvings in medium to coarse grain granites. We compared the values obtained inside and outside the grooves of the carvings using two different support rings, one flat and one concave. The flat ring was not able to reach the bottom of the groove, meanwhile the concave ring adjusts fairly well given its semi spherical section. A t-test confirmed the difference (p < 0.01) between lower rebound values obtained in the grooves using the flat ring and the higher and less scattered values obtained when the concave ring is used. As a very sensitive device, there are some problems in the use related with rock roughness and rock grain size. In weathered medium to coarse grained rocks, with very irregular surfaces, is not easy to get a good contact between the plunge and the rock surface. A poor contact caused by surface roughness causes the scattering and lowering of rebound values. On the contrary, in homogeneous fine grained rocks and in uniform rock surfaces the device gave very good results. The data obtained in glacial, nival and rock coastal environments showed the potential of the device in the identification of changes in rock hardness. We were able to asses the changes in the weathering degree of glacial striations and marked differences in the rock surfaces subjected or not to abrasion. A. Feal-Pérez is supported by the grant AP2006-03854 (Spanish Ministry of Education)
Microscopic observation of laser glazed yttria-stabilized zirconia coatings

NASA Astrophysics Data System (ADS)

Morks, M. F.; Berndt, C. C.; Durandet, Y.; Brandt, M.; Wang, J.

2010-08-01

Thermal barrier coatings (TBCs) are frequently used as insulation system for hot components in gas-turbine, combustors and power plant industries. The corrosive gases which come from combustion of low grade fuels can penetrate into the TBCs and reach the metallic components and bond coat and cause hot corrosion and erosion damage. Glazing the top coat by laser beam is advanced approach to seal TBCs surface. The laser beam has the advantage of forming a dense thin layer composed of micrograins. Plasma-sprayed yttria-stabilized zirconia (YSZ) coating was glazed with Nd-YAG laser at different operating conditions. The surface morphologies, before and after laser treatment, were investigated by scanning electron microscopy. Laser beam assisted the densification of the surface by remelting a thin layer of the exposed surface. The laser glazing converted the rough surface of TBCs into smooth micron-size grains with size of 2-9 μm and narrow grain boundaries. The glazed surfaces showed higher Vickers hardness compared to as-sprayed coatings. The results revealed that the hardness increases as the grain size decreases.
Using LIDAR and UAV-derived point clouds to evaluate surface roughness in a gravel-bed braided river (Vénéon river, French Alps)

NASA Astrophysics Data System (ADS)

Vázquez Tarrío, Daniel; Borgniet, Laurent; Recking, Alain; Liebault, Frédéric; Vivier, Marie

2016-04-01

The present research is focused on the Vénéon river at Plan du Lac (Massif des Ecrins, France), an alpine braided gravel bed stream with a glacio-nival hydrological regime. It drains a catchment area of 316 km2. The present research is focused in a 2.5 km braided reach placed immediately upstream of a small hydropower dam. An airbone LIDAR survey was accomplished in October, 2014 by EDF (the company managing the small hydropower dam), and data coming from this LIDAR survey were available for the present research. Point density of the LIDAR-derived 3D-point cloud was between 20-50 points/m2, with a vertical precision of 2-3 cm over flat surfaces. Moreover, between April and Juin, 2015, we carried out a photogrammetrical campaign based in aerial images taken with an UAV-drone. The UAV-derived point-cloud has a point density of 200-300 points/m2, and a vertical precision over flat control surfaces comparable to that of the LIDAR point cloud (2-3 cm). Simultaneously to the UAV campaign, we took several Wolman samples with the aim of characterizing the grain size distribution of bed sediment. Wolman samples were taken following a geomorphological criterion (unit bars, head/tail of compound bars). Furthermore, some of the Wolman samples were repeated with the aim of defining the uncertainty of our sampling protocol. LIDAR and UAV-derived point clouds were treated in order to check whether both point-clouds were correctly co-aligned. After that, we estimated bed roughness using the detrended standard deviation of heights, in a 40-cm window. For all this data treatment we used CloudCompare. Then, we measured the distribution of roughness in the same geomorphological units where we took the Wolman samples, and we compared with the grain size distributions measured in the field: differences between UAV-point cloud roughness distributions and measured-grain size distribution (~1-2 cm) are in the same order of magnitude of the differences found between the repeated Wolman samples (~0.5-1.5 cm). Differences with LIDAR-derived roughness distributions are only slightly higher, which could be due to the lower point density of the LIDAR point clouds.
Bulk and Interface Thermodynamics of Calcia-, and Yttria-doped Zirconia Ceramics: Nanograined Phase Stability

NASA Astrophysics Data System (ADS)

Drazin, John Walter

Calcia-, and yttria- doped zirconia powders and samples are essential systems in academia and industry due to their observed bulk polymorphism. Pure zirconia manifests as Baddeleyite, a monoclinic structured mineral with 7-fold coordination. This bulk form of zirconia has little application due to its asymmetry. Therefore dopants are added to the grain in-order to induce phase transitions to either a tetragonal or cubic polymorph with the incorporation of oxygen vacancies due to the dopant charge mis-match with the zirconia matrix. The cubic polymorph has cubic symmetry such that these samples see applications in solid oxide fuel cells (SOFCs) due to the high oxygen vacancy concentrations and high ionic mobility at elevated temperatures. The tetragonal polymorph has slight asymmetry in the c-axis compared to the a-axis such that the tetragonal samples have increased fracture toughness due to an impact induced phase transformation to a cubic structure. These ceramic systems have been extensively studied in academia and used in various industries, but with the advent of nanotechnology one can wonder whether smaller grain samples will see improved characteristics similar to their bulk grain counterparts. However, there is a lack of data and knowledge of these systems in the nano grained region which provides us with an opportunity to advance the theory in these systems. The polymorphism seen in the bulk grains samples is also seen in the nano-grained samples, but at slightly distinct dopant concentrations. The current theory hypothesizes that a surface excess, gamma (J/m 2), can be added to the Gibbs Free energy equation to account for the additional free energy of the nano-grain atoms. However, these surface energies have been difficult to measure and therefore thermodynamic data on these nano-grained samples have been sparse. Therefore, in this work, I will use a well established water adsorption microcalorimetry apparatus to measure the water coverage isotherms while simultaneously collecting the energetic contribution of the adsorbing water vapor. With this data and apparatus, I have derived a 2nd order differential equation that relates the surface energy to the measured quantities such that I collected surfaces energies for over 35 specimens in the calcia-zirconia and yttria-zirconia systems for the first time. From the results, it was found that the monoclinic polymorph had the largest surface energy in the range of 1.9 - 2.1 ( J/m2) while the tetragonal surface energies were roughly 1.4 - 1.6 (J/m2), the cubic surface energies were roughly 0.8 - 1.0 (J/m2), and the amorphous surface energies were the smallest at roughly 0.7 - 0.8 (J/m 2). With the measured surface energy data, collected for the first time, we can create a nano-grain phase diagram similar to a bulk phase diagram that shows the stable polymorph as a function of dopant concentration and grain size using the bulk enthalpy data collected from high temperature oxide melt drop solution calorimetry. The phase diagrams show that pure zirconia will transform into tetragonal and cubic polymorphs from the monoclinic one at 7 and 5 nm respectively which confirms the experimental observations. The results are powerful predictive tools successfully applied in the nCZ and nYZ systems to a high degree of accuracy and adds a new development to conventional bulk phase diagrams. These diagrams should be the basis for nanotechnological efforts in nCZ and nYZ based systems, and suggest similar efforts are needed in other nano systems to pursue an in depth understanding and optimization of nanomaterials. After working on the theoretical aspects of phase stability, the focus of the research will shift to producing dense samples to measure observable quantities such as oxygen conduction and mechanical hardness. However, producing said samples with the nanocrystalline grain sizes has also been challenging as conventional sintering requires high temperatures which, as a consequence, induces grain growth of the samples limiting the minimum grain size of the samples. Therefore, in this work, we have developed a Pressure Assisted Rapid Sintering Technique (PARS) that uses high currents to Joule heat the samples to moderate temperatures (650-900 °C) for short durations (5-10 min) under large compressive pressures (600-2200 MPa). With this new technique, atomic level grain sizes (sub-10nm) can be easily achieved at high relative densities (>98 %). Using the PARS setup, multiple 3nYZ samples were produced with varied grain sizes down to 9 nm and as large as 5mum. The mechanical hardness of these samples were tested using a Vicker's microhardness indentation apparatus. The hardness of the "bulk" grains was roughly 12.9 GPa while the smallest grain size pellet had a hardness approaching 15 GPa. All of the 3nYZ pellets had a higher hardness with diminishing grain size, thereby extending the Hall-Petch relationship to 9 nm in the 3YZ system. This is an amazing and unprecedented result to date. After producing the extreme nano-grained samples (15nCZ and 17.5nYSZ), they were tested for inter- and intragranular oxygen ion conduction as well. The results showed that the smaller grained samples have increased levels of oxygen ion conduction from both inter- and intragranular diffusion regardless of the operating temperatures. In addition, it was seen that the activation energies for both modes of oxygen ion diffusion were lowered for the nCZ system while a plateaued effect was seen in the nYZ system. A new theoretical formulation was proposed to explain the trends such that there are two modifiable parameters to exploit; activation energy and grain size. With the lowering of the grain size, the number of interconnected grain boundaries would increase dramatically allowing for more efficient travel around and through the grains. The activation energy can be lowered by modifying the chemistry of the grain boundary by specifically choosing larger dopants with a positive enthalpy of segregation such the concentration of the dopants on the grain boundary would increase, spacing the unattached bonds further apart and reducing their number. Therefore, one can use an engineered nanograined SOFC to decrease the operating temperature of the device without altering the output power density; significantly improving safety and economics.
Characterization on White Etching Layer Formed During Ceramic Milling of Inconel 718

NASA Astrophysics Data System (ADS)

Kruk, A.; Wusatowska-Sarnek, A. M.; Ziętara, M.; Jemielniak, K.; Siemiątkowski, Z.; Czyrska-Filemonowicz, A.

2018-03-01

A comprehensive characterization of the near surface formed during the interrupted high-speed dry ceramic milling of IN718 was performed using light imaging, SEM/EDX, TEM and nano-hardness methods. It was found out that even an initial cut by a fresh tool creates a sub-surface alteration roughly 20 µm deep. The depth of altered sub-surface progressively changed to a roughly 40 µm when the tool reached an approximately half of its life, and almost 60 µm at the tool's end of the life. In the last two cases, the visible WEL (utilizing a light microscope) of the thickness roughly 6 and 15 µm was created, respectively. The outermost layer of the deformed subsurface was found to be for all three cases approximately 1.5 µm thick and composed of dynamically recrystallized γ phase grains with the average diameter of approximately 150 nm. This layer was free of δ phase and γ' or γ″ precipitates. It was followed by a plastically deformed zone.
Dissolution of minerals with rough surfaces

NASA Astrophysics Data System (ADS)

de Assis, Thiago A.; Aarão Reis, Fábio D. A.

2018-05-01

We study dissolution of minerals with initial rough surfaces using kinetic Monte Carlo simulations and a scaling approach. We consider a simple cubic lattice structure, a thermally activated rate of detachment of a molecule (site), and rough surface configurations produced by fractional Brownian motion algorithm. First we revisit the problem of dissolution of initial flat surfaces, in which the dissolution rate rF reaches an approximately constant value at short times and is controlled by detachment of step edge sites. For initial rough surfaces, the dissolution rate r at short times is much larger than rF ; after dissolution of some hundreds of molecular layers, r decreases by some orders of magnitude across several time decades. Meanwhile, the surface evolves through configurations of decreasing energy, beginning with dissolution of isolated sites, then formation of terraces with disordered boundaries, their growth, and final smoothing. A crossover time to a smooth configuration is defined when r = 1.5rF ; the surface retreat at the crossover is approximately 3 times the initial roughness and is temperature-independent, while the crossover time is proportional to the initial roughness and is controlled by step-edge site detachment. The initial dissolution process is described by the so-called rough rates, which are measured for fixed ratios between the surface retreat and the initial roughness. The temperature dependence of the rough rates indicates control by kink site detachment; in general, it suggests that rough rates are controlled by the weakest microscopic bonds during the nucleation and formation of the lowest energy configurations of the crystalline surface. Our results are related to recent laboratory studies which show enhanced dissolution in polished calcite surfaces. In the application to calcite dissolution in alkaline environment, the minimal values of recently measured dissolution rate spectra give rF ∼10-9 mol/(m2 s), and the calculated rate laws of our model give rough rates in the range 10-6 -10-5 mol/(m2 s). This estimate is consistent with the range of calcite dissolution rates obtained in a recent work after treatment of literature data, which suggests the universal control of kink site dissolution in short term laboratory works. The weak effects of lattice size on our results also suggest that smoothing of mineral grain surfaces across geological times may be a microscopic explanation for the difference of chemical weathering rate of silicate minerals in laboratory and in the environment.
THE EFFECTS OF CRACKING ON THE SURFACE POTENTIAL OF ICY GRAINS IN SATURN’S E-RING: LABORATORY STUDIES

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bu, Caixia; Bahr, David A.; Dukes, Catherine A.

2016-07-10

Within Saturn's E-ring, dust grains are coated by water vapor co-released with ice grains from the geyser-like eruptions of Enceladus. These ice-coated grains have intrinsic surface potential and interact synergistically with the ions and electrons of Saturn's magnetospheric plasmas. We perform laboratory experiments to investigate the effects of water-ice growth on the surface potential, using amorphous solid water (ASW) films. We estimate the growth of the surface potential to be ∼ 2.5 mV (Earth) yr{sup 1} and 112 mV yr{sup 1} for E-ring grains at ∼4.5 R {sub s} and 3.95 R {sub s} outside Enceladus’s plume, respectively. In addition,more » our measurements show that the linear relationship between the surface potential and the film thickness, as described in previous studies, has an upper limit, where the film spontaneously cracks above a porosity-dependent critical thickness. Heating of the cracked films with (and without) deposited charge shows that significant positive (and negative) surface potentials are retained at temperatures above 110 K, contrary to the minimal values (roughly zero) for thin, transparent ASW films. The significant surface potentials observed on micron-scale cracked ice films after thermal cycling, (5–20) V, are consistent with Cassini measurements, which indicate a negative charge of up to 5 V for E-ring dust particles at ∼5 R {sub s}. Therefore, the native grain surface potential resulting from water-vapor coating must be included in modeling studies of interactions between E-ring icy surfaces and Saturn's magnetospheric plasma.« less
Surface integrity and fatigue behaviour of electric discharged machined and milled austenitic stainless steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lundberg, Mattias, E-mail: mattias.lundberg@liu.se

Machining of austenitic stainless steels can result in different surface integrities and different machining process parameters will have a great impact on the component fatigue life. Understanding how machining processes affect the cyclic behaviour and microstructure are of outmost importance in order to improve existing and new life estimation models. Milling and electrical discharge machining (EDM) have been used to manufacture rectangular four-point bend fatigue test samples; subjected to high cycle fatigue. Before fatigue testing, surface integrity characterisation of the two surface conditions was conducted using scanning electron microscopy, surface roughness, residual stress profiles, and hardness profiles. Differences in cyclicmore » behaviour were observed between the two surface conditions by the fatigue testing. The milled samples exhibited a fatigue limit. EDM samples did not show the same behaviour due to ratcheting. Recrystallized nano sized grains were identified at the severely plastically deformed surface of the milled samples. Large amounts of bent mechanical twins were observed ~ 5 μm below the surface. Grain shearing and subsequent grain rotation from milling bent the mechanical twins. EDM samples showed much less plastic deformation at the surface. Surface tensile residual stresses of ~ 500 MPa and ~ 200 MPa for the milled and EDM samples respectively were measured. - Highlights: •Milled samples exhibit fatigue behaviour, but not EDM samples. •Four-point bending is not suitable for materials exhibiting pronounced ratcheting. •LAGB density can be used to quantitatively measure plastic deformation. •Grain shearing and rotation result in bent mechanical twins. •Nano sized grains evolve due to the heat of the operation.« less
The Effects of Acid Etching on the Nanomorphological Surface Characteristics and Activation Energy of Titanium Medical Materials

PubMed Central

Hung, Kuo-Yung; Lin, Yi-Chih; Feng, Hui-Ping

2017-01-01

The purpose of this study was to characterize the etching mechanism, namely, the etching rate and the activation energy, of a titanium dental implant in concentrated acid and to construct the relation between the activation energy and the nanoscale surface topographies. A commercially-pure titanium (CP Ti) and Ti-6Al-4V ELI surface were tested by shot blasting (pressure, grain size, blasting distance, blasting angle, and time) and acid etching to study its topographical, weight loss, surface roughness, and activation energy. An Arrhenius equation was applied to derive the activation energy for the dissolution of CP Ti/Ti-6Al-4V ELI in sulfuric acid (H2SO4) and hydrochloric acid (HCl) at different temperatures. In addition, white-light interferometry was applied to measure the surface nanomorphology of the implant to obtain 2D or 3D roughness parameters (Sa, Sq, and St). The nanopore size that formed after etching was approximately 100–500 nm. The surface roughness of CP Ti and Ti-6Al-4V ELI decreased as the activation energy decreased but weight loss increased. Ti-6Al-4V ELI has a higher level of activation energy than Ti in HCl, which results in lower surface roughness after acid etching. This study also indicates that etching using a concentrated hydrochloric acid provided superior surface modification effects in titanium compared with H2SO4. PMID:29019926
Characterizing the effects of regolith surface roughness on photoemission from surfaces in space

NASA Astrophysics Data System (ADS)

Dove, A.; Horanyi, M.; Wang, X.

2017-12-01

Surfaces of airless bodies and spacecraft in space are exposed to a variety of charging environments. A balance of currents due to plasma bombardment, photoemission, electron and ion emission and collection, and secondary electron emission determines the surface's charge. Photoelectron emission is the dominant charging process on sunlit surfaces in the inner solar system due to the intense solar UV radiation. This can result in a net positive surface potential, with a cloud of photoelectrons immediately above the surface, called the photoelectron sheath. Conversely, the unlit side of the body will charge negatively due the collection of the fast-moving solar wind electrons. The interaction of charged dust grains with these positively and negatively charged surfaces, and within the photoelectron and plasma sheaths may explain the occurrence of dust lofting, levitation and transport above the lunar surface. The surface potential of exposed objects is also dependent on the material properties of their surfaces. Composition and particle size primarily affect the quantum efficiency of photoelectron generation; however, surface roughness can also control the charging process. In order to characterize these effects, we have conducted laboratory experiments to examine the role of surface roughness in generating photoelectrons in dedicated laboratory experiments using solid and dusty surfaces of the same composition (CeO2), and initial comparisons with JSC-1 lunar simulant. Using Langmuir probe measurements, we explore the measured potentials above insulating surfaces exposed to UV and an electric field, and we show that the photoemission current from a dusty surface is largely reduced due to its higher surface roughness, which causes a significant fraction of the emitted photoelectrons to be re-absorbed within the surface. We will discuss these results in context of similar situations on planetary surfaces.
Aerodynamic performance of transonic and subsonic airfoils: Effects of surface roughness, turbulence intensity, Mach number, and streamline curvature-airfoil shape

NASA Astrophysics Data System (ADS)

Zhang, Qiang

The effects of surface roughness, turbulence intensity, Mach number, and streamline curvature-airfoil shape on the aerodynamic performance of turbine airfoils are investigated in compressible, high speed flows. The University of Utah Transonic Wind Tunnel is employed for the experimental part of the study. Two different test sections are designed to produce Mach numbers, Reynolds numbers, passage mass flow rates, and physical dimensions, which match values along turbine blades in operating engines: (i) a nonturning test section with a symmetric airfoil, and (ii) a cascade test section with a cambered turbine vane. The nonuniform, irregular, three-dimensional surface roughness is characterized using the equivalent sand grain roughness size. Changing the airfoil surface roughness condition has a substantial effect on wake profiles of total pressure loss coefficients, normalized Mach number, normalized kinetic energy, and on the normalized and dimensional magnitudes of Integrated Aerodynamic Losses produced by the airfoils. Comparisons with results for a symmetric airfoil and a cambered vane show that roughness has more substantial effects on losses produced by the symmetric airfoil than the cambered vane. Data are also provided that illustrate the larger loss magnitudes are generally present with flow turning and cambered airfoils, than with symmetric airfoils. Wake turbulence structure of symmetric airfoils and cambered vanes are also studied experimentally. The effects of surface roughness and freestream turbulence levels on wake distributions of mean velocity, turbulence intensity, and power spectral density profiles and vortex shedding frequencies are quantified one axial chord length downstream of the test airfoils. As the level of surface roughness increases, all wake profile quantities broaden significantly and nondimensional vortex shedding frequencies decrease. Wake profiles produced by the symmetric airfoil are more sensitive to variations of surface roughness and freestream turbulence, compared with data from the cambered vane airfoil. Stanton numbers, skin friction coefficients, aerodynamic losses, and Reynolds analogy behavior are numerically predicted for a turbine vane using the FLUENT with a k-epsilon RNG model to show the effects of Mach number, mainstream turbulence level, and surface roughness. Comparisons with wake aerodynamic loss experimental data are made. Numerically predicted skin friction coefficients and Stanton numbers are also used to deduce Reynolds analogy behavior on the vane suction and pressure sides.
Wettability of Y2O3: A Relative Analysis of Thermally Oxidized, Reactively Sputtered and Template Assisted Nanostructured Coatings

PubMed Central

Barshilia, Harish C.; Chaudhary, Archana; Kumar, Praveen; Manikandanath, Natarajan T.

2012-01-01

The wettability of reactively sputtered Y2O3, thermally oxidized Y-Y2O3 and Cd-CdO template assisted Y2O3 coatings has been studied. The wettability of as-deposited Y2O3 coatings was determined by contact angle measurements. The water contact angles for reactively sputtered, thermally oxidized and template assisted Y2O3 nanostructured coatings were 99°, 117° and 155°, respectively. The average surface roughness values of reactively sputtered, thermally oxidized and template assisted Y2O3 coatings were determined by using atomic force microscopy and the corresponding values were 3, 11 and 180 nm, respectively. The low contact angle of the sputter deposited Y2O3 and thermally oxidized Y-Y2O3 coatings is attributed to a densely packed nano-grain like microstructure without any void space, leading to low surface roughness. A water droplet on such surfaces is mostly in contact with a solid surface relative to a void space, leading to a hydrophobic surface (low contact angle). Surface roughness is a crucial factor for the fabrication of a superhydrophobic surface. For Y2O3 coatings, the surface roughness was improved by depositing a thin film of Y2O3 on the Cd-CdO template (average roughness = 178 nm), which resulted in a contact angle greater than 150°. The work of adhesion of water was very high for the reactively sputtered Y2O3 (54 mJ/m2) and thermally oxidized Y-Y2O3 coatings (43 mJ/m2) compared to the Cd-CdO template assisted Y2O3 coating (7 mJ/m2). PMID:28348296
Ion-Implanted Diamond Films and Their Tribological Properties

NASA Technical Reports Server (NTRS)

Wu, Richard L. C.; Miyoshi, Kazuhisa; Korenyi-Both, Andras L.; Garscadden, Alan; Barnes, Paul N.

1993-01-01

This paper reports the physical characterization and tribological evaluation of ion-implanted diamond films. Diamond films were produced by microwave plasma, chemical vapor deposition technique. Diamond films with various grain sizes (0.3 and 3 microns) and roughness (9.1 and 92.1 nm r.m.s. respectively) were implanted with C(+) (m/e = 12) at an ion energy of 160 eV and a fluence of 6.72 x 10(exp 17) ions/sq cm. Unidirectional sliding friction experiments were conducted in ultrahigh vacuum (6.6 x 10(exp -7)Pa), dry nitrogen and humid air (40% RH) environments. The effects of C(+) ion bombardment on fine and coarse-grained diamond films are as follows: the surface morphology of the diamond films did not change; the surface roughness increased (16.3 and 135.3 nm r.m.s.); the diamond structures were damaged and formed a thin layer of amorphous non-diamond carbon; the friction coefficients dramatically decreased in the ultrahigh vacuum (0.1 and 0.4); the friction coefficients decreased slightly in the dry nitrogen and humid air environments.
Photopolarimetric Retrievals of Snow Properties

NASA Technical Reports Server (NTRS)

Ottaviani, M.; van Diedenhoven, B.; Cairns, B.

2015-01-01

Polarimetric observations of snow surfaces, obtained in the 410-2264 nm range with the Research Scanning Polarimeter onboard the NASA ER-2 high-altitude aircraft, are analyzed and presented. These novel measurements are of interest to the remote sensing community because the overwhelming brightness of snow plagues aerosol and cloud retrievals based on airborne and spaceborne total reflection measurements. The spectral signatures of the polarized reflectance of snow are therefore worthwhile investigating in order to provide guidance for the adaptation of algorithms currently employed for the retrieval of aerosol properties over soil and vegetated surfaces. At the same time, the increased information content of polarimetric measurements allows for a meaningful characterization of the snow medium. In our case, the grains are modeled as hexagonal prisms of variable aspect ratios and microscale roughness, yielding retrievals of the grains' scattering asymmetry parameter, shape and size. The results agree with our previous findings based on a more limited data set, with the majority of retrievals leading to moderately rough crystals of extreme aspect ratios, for each scene corresponding to a single value of the asymmetry parameter.

Surface damage and structure evolution of recrystallized tungsten exposed to ELM-like transient loads

NASA Astrophysics Data System (ADS)

Yuan, Y.; Du, J.; Wirtz, M.; Luo, G.-N.; Lu, G.-H.; Liu, W.

2016-03-01

Surface damage and structure evolution of the full tungsten ITER divertor under transient heat loads is a key concern for component lifetime and plasma operations. Recrystallization caused by transients and steady-state heat loads can lead to degradation of the material properties and is therefore one of the most serious issues for tungsten armor. In order to investigate the thermal response of the recrystallized tungsten under edge localized mode-like transient thermal loads, fully recrystallized tungsten samples with different average grain sizes are exposed to cyclic thermal shocks in the electron beam facility JUDITH 1. The results indicate that not only does the microstructure change due to recrystallization, but that the surface residual stress induced by mechanical polishing strongly influences the surface cracking behavior. The stress-free surface prepared by electro-polishing is shown to be more resistant to cracking than the mechanically polished one. The resulting surface roughness depends largely on the loading conditions instead of the recrystallized-grain size. As the base temperature increases from room temperature to 400 °C, surface roughening mainly due to the shear bands in each grain becomes more pronounced, and sub-grains (up to 3 μm) are simultaneously formed in the sub-surface. The directions of the shear bands exhibit strong grain-orientation dependence, and they are generally aligned with the traces of {1 1 2} twin habit planes. The results suggest that twinning deformation and dynamic recrystallization represent the predominant mechanism for surface roughening and related microstructure evolution.
Enhanced in vitro biocompatibility of ultrafine-grained biomedical NiTi alloy with microporous surface

NASA Astrophysics Data System (ADS)

Zheng, C. Y.; Nie, F. L.; Zheng, Y. F.; Cheng, Y.; Wei, S. C.; Valiev, R. Z.

2011-08-01

Bulk ultrafine-grained Ni 50.8Ti 49.2 alloy (UFG-NiTi) was successfully fabricated by equal-channel angular pressing (ECAP) technique in the present study, and to further improve its surface biocompatibility, surface modification techniques including sandblasting, acid etching and alkali treatment were employed to produce either irregularly roughened surface or microporous surface or hierarchical porous surface with bioactivity. The effect of the above surface treatments on the surface roughness, wettability, corrosion behavior, ion release, apatite forming ability and cytocompatibility of UFG-NiTi alloy were systematically investigated with the coarse-grained NiTi alloy as control. The pitting corrosion potential ( Epit) was increased from 393 mV (SCE) to 704 mV (SCE) with sandblasting and further increased to 1539 mV (SCE) with following acid etching in HF/HNO 3 solution. All the above surface treatment increased the apatite forming ability of UFG-NiTi in varying degrees when soaked them in simulated body fluid (SBF). Meanwhile, both sandblasting and acid etching could promote the cytocompatibility for osteoblasts: sandblasting enhanced cell attachment and acid etching increased cell proliferation. The different corrosion behavior, apatite forming ability and cellular response of UFG-NiTi after different surface modifications are attributed to the topography and wettability of the resulting surface oxide layer.
Surface morphological evolution of epitaxial CrN(001) layers

NASA Astrophysics Data System (ADS)

Frederick, J. R.; Gall, D.

2005-09-01

CrN layers, 57 and 230 nm thick, were grown on MgO(001) at Ts=600-800 °C by ultrahigh-vacuum magnetron sputter deposition in pure N2 discharges from an oblique deposition angle α=80°. Layers grown at 600 °C nucleate as single crystals with a cube-on-cube epitaxial relationship with the substrate. However, rough surfaces with cauliflower-type morphologies cause the nucleation of misoriented CrN grains that develop into cone-shaped grains that protrude out of the epitaxial matrix to form triangular faceted surface mounds. The surface morphology of epitaxial CrN(001) grown at 700 °C is characterized by dendritic ridge patterns extending along the orthogonal <110> directions superposed by square-shaped super mounds with <100> edges. The ridge patterns are attributed to a Bales-Zangwill instability while the supermounds form due to atomic shadowing which leads to the formation of epitaxial inverted pyramids that are separated from the surrounding layer by tilted nanovoids. Growth at 800 °C yields complete single crystals with smooth surfaces. The root-mean-square surface roughness for 230-nm-thick layers decreases from 18.8 to 9.3 to 1.1 nm as Ts is raised from 600 to 700 to 800 °C. This steep decrease is due to a transition in the roughening mechanism from atomic shadowing to kinetic roughening. Atomic shadowing is dominant at 600 and 700 °C, where misoriented grains and supermounds, respectively, capture a larger fraction of the oblique deposition flux in comparison to the surrounding epitaxial matrix, resulting in a high roughening rate that is described by a power law with an exponent β>0.5. In contrast, kinetic roughening controls the surface morphology for Ts=800 °C, as well as the epitaxial fraction of the layers grown at 600 and 700 °C, yielding relatively smooth surfaces and β<=0.27.
Characteristic of Low Temperature Carburized Austenitic Stainless Steel

NASA Astrophysics Data System (ADS)

Istiroyah; Pamungkas, M. A.; Saroja, G.; Ghufron, M.; Juwono, A. M.

2018-01-01

Low temperature carburizing process has been carried out on austenitic stainless steel (ASS) type AISI 316L, that contain chromium in above 12 at%. Therefore, conventional heat treatment processes that are usually carried out at high temperatures are not applicable. The sensitization process due to chromium migration from the grain boundary will lead to stress corrosion crack and decrease the corrosion resistance of the steel. In this study, the carburizing process was carried out at low temperatures below 500 °C. Surface morphology and mechanical properties of carburized specimens were investigated using optical microscopy, non destructive profilometer, and Vicker microhardness. The surface roughness analysis show the carburising process improves the roughness of ASS surface. This improvement is due to the adsorption of carbon atoms on the surface of the specimen. Likewise, the hardness test results indicate the carburising process increases the hardness of ASS.
Hydrocarbon-Fuel/Combustion-Chamber-Liner Materials Compatibility

DTIC Science & Technology

1991-04-01

Grains, Leaving a Rough, Highly Pitted Surface 13 V (a) (b) ALA " I~ 4~ (0) (d) Figure 7. Cooling Channel Surface Features Resulting From the Overall...Canada or Terrell County, Texas as compared to natural gas from Rio Arriba County, New Mexico. Thus, the viability of using field gas feedstock...possible source of higher volumes in the more distant future. TABLE.14 COMPOSITION OF VARIOUS NATURAL GAS FIELDS Rio Olds Cliffside Arriba Terrel
SRF Cavity Surface Topography Characterization Using Replica Techniques

DOE Office of Scientific and Technical Information (OSTI.GOV)

C. Xu, M.J. Kelley, C.E. Reece

2012-07-01

To better understand the roll of topography on SRF cavity performance, we seek to obtain detailed topographic information from the curved practical cavity surfaces. Replicas taken from a cavity interior surface provide internal surface molds for fine Atomic Force Microscopy (AFM) and stylus profilometry. In this study, we confirm the replica resolution both on surface local defects such as grain boundary and etching pits and compare the surface uniform roughness with the aid of Power Spectral Density (PSD) where we can statistically obtain roughness parameters at different scales. A series of sampling locations are at the same magnetic field chosenmore » at the same latitude on a single cell cavity to confirm the uniformity. Another series of sampling locations at different magnetic field amplitudes are chosen for this replica on the same cavity for later power loss calculation. We also show that application of the replica followed by rinsing does not adversely affect the cavity performance.« less
Effect of surface treatments on shear bond strength of resin composite bonded to CAD/CAM resin-ceramic hybrid materials

PubMed Central

Güngör, Merve Bankoğlu; Bal, Bilge Turhan; Ünver, Senem; Doğan, Aylin

2016-01-01

PURPOSE The purpose of this study was to assess the effect of surface treatments on shear bond strength of resin composite bonded to thermocycled and non-thermocycled CAD/CAM resin-ceramic hybrid materials. MATERIALS AND METHODS 120 specimens (10×10×2 mm) from each material were divided into 12 groups according to different surface treatments in combination with thermal aging procedures. Surface treatment methods were airborne-particle abrasion (abraded with 50 micron alumina particles), dry grinding (grinded with 125 µm grain size bur), and hydrofluoric acid (9%) and silane application. According to the thermocycling procedure, the groups were assigned as non-thermocycled, thermocycled after packing composites, and thermocycled before packing composites. The average surface roughness of the non-thermocycled specimens were measured after surface treatments. After packing composites and thermocycling procedures, shear bond strength (SBS) of the specimens were tested. The results of surface roughness were statistically analyzed by 2-way Analysis of Variance (ANOVA), and SBS results were statistically analyzed by 3-way ANOVA. RESULTS Surface roughness of GC were significantly lower than that of LU and VE (P<.05). The highest surface roughness was observed for dry grinding group, followed by airborne particle abraded group (P<.05). Comparing the materials within the same surface treatment method revealed that untreated surfaces generally showed lower SBS values. The values of untreated LU specimens showed significantly different SBS values compared to those of other surface treatment groups (P<.05). CONCLUSION SBS was affected by surface treatments. Thermocycling did not have any effect on the SBS of the materials except acid and silane applied GC specimens, which were subjected to thermocycling before packing of the composite resin. PMID:27555894
Coarse-graining of proteins based on elastic network models

NASA Astrophysics Data System (ADS)

Sinitskiy, Anton V.; Voth, Gregory A.

2013-08-01

To simulate molecular processes on biologically relevant length- and timescales, coarse-grained (CG) models of biomolecular systems with tens to even hundreds of residues per CG site are required. One possible way to build such models is explored in this article: an elastic network model (ENM) is employed to define the CG variables. Free energy surfaces are approximated by Taylor series, with the coefficients found by force-matching. CG potentials are shown to undergo renormalization due to roughness of the energy landscape and smoothing of it under coarse-graining. In the case study of hen egg-white lysozyme, the entropy factor is shown to be of critical importance for maintaining the native structure, and a relationship between the proposed ENM-mode-based CG models and traditional CG-bead-based models is discussed. The proposed approach uncovers the renormalizable character of CG models and offers new opportunities for automated and computationally efficient studies of complex free energy surfaces.
The perfect debris flow? Aggregated results from 28 large-scale experiments

USGS Publications Warehouse

Iverson, Richard M.; Logan, Matthew; LaHusen, Richard G.; Berti, Matteo

2010-01-01

Aggregation of data collected in 28 controlled experiments reveals reproducible debris-flow behavior that provides a clear target for model tests. In each experiment ∼10 m3 of unsorted, water-saturated sediment composed mostly of sand and gravel discharged from behind a gate, descended a steep, 95-m flume, and formed a deposit on a nearly horizontal runout surface. Experiment subsets were distinguished by differing basal boundary conditions (1 versus 16 mm roughness heights) and sediment mud contents (1 versus 7 percent dry weight). Sensor measurements of evolving flow thicknesses, basal normal stresses, and basal pore fluid pressures demonstrate that debris flows in all subsets developed dilated, coarse-grained, high-friction snouts, followed by bodies of nearly liquefied, finer-grained debris. Mud enhanced flow mobility by maintaining high pore pressures in flow bodies, and bed roughness reduced flow speeds but not distances of flow runout. Roughness had these effects because it promoted debris agitation and grain-size segregation, and thereby aided growth of lateral levees that channelized flow. Grain-size segregation also contributed to development of ubiquitous roll waves, which had diverse amplitudes exhibiting fractal number-size distributions. Despite the influence of these waves and other sources of dispersion, the aggregated data have well-defined patterns that help constrain individual terms in a depth-averaged debris-flow model. The patterns imply that local flow resistance evolved together with global flow dynamics, contradicting the hypothesis that any consistent rheology applied. We infer that new evolution equations, not new rheologies, are needed to explain how characteristic debris-flow behavior emerges from the interactions of debris constituents.
From smooth to rough, from water to air: the intertidal habitat of Northern clingfish ( Gobiesox maeandricus)

NASA Astrophysics Data System (ADS)

Ditsche, Petra; Hicks, Madeline; Truong, Lisa; Linkem, Christina; Summers, Adam

2017-04-01

The Northern clingfish is a small, Eastern North Pacific fish that can attach to rough, fouled rocks in the intertidal. Their ability to attach to surfaces has been measured previously in the laboratory, and in this study, we show the roughness and fouling of the natural habitat of these fish. We introduce a new method for measuring surface roughness of natural substrates with time-limited accessibility. We expect this method to be broadly applicable in studies of animal/substrate surface interactions in habitats difficult to characterize. Our roughness measurements demonstrate that the fish's ability to attach to very coarse roughness is required in its natural environment. Some of the rocks showed even coarser roughness than the fish could attach to in the lab setting. We also characterized the clingfish's preference for other habitat descriptors such as the size of the rocks, biofilm, and Aufwuchs (macroalgae, encrusting invertebrates) cover, as well as grain size of underlying substrate. Northern clingfish seek shelter under rocks of 15-45 cm in size. These rocks have variable Aufwuchs cover, and gravel is the main underlying substrate type. In the intertidal, environmental conditions change with the tides, and for clingfish, the daily time under water (DTUW%) was a key parameter explaining distribution. Rather than location being determined by intertidal zonation, an 80% DTUW, a finer scale concept of tidal inundation, was required by the fish. We expect that this is likely because the mobility of the fish allows them to more closely track the ideal inundation in the marine intertidal.
Scattering by inhomogeneous systems with rough internal surfaces: Porous solids and random-field Ising systems

NASA Astrophysics Data System (ADS)

Wong, Po-Zen

1985-12-01

For a two-component inhomogeneous system consisting of compact domains of characteristic size R, I show that if the domain walls are ``rough'' and their root-mean-square fluctuation w over a distance r obeys a power law w=b(r/a)x (a is the lattice constant and x>0), then the geometrical correlation function γ(r) has leading terms proportional to rx and r for r<>R-1, where d is the dimension of the system. Two possible applications of this result are discussed. (i) In granular porous solids which have a minimum grain size Rmin, the above result implies that surface roughness can cause I(q) to fall off like 1/qα for q>>Rmin-1, where α=3+x>3 for d=3. In particular, when x>1, the surface becomes a fractal with dimension D=1+x=α-2, which can be extracted from the scattering data. On the other hand, if the grains are smooth and their size distribution obeys a power law dN(R)/dR~R-β over a range Rmin
Growth mechanism of surface roughed platinum nanowires through electrodeposition current control and their electrochemical applications

NASA Astrophysics Data System (ADS)

Ruan, Dajiang

The aim of this work is to investigate the effect of current density on the grain size and surface morphology of electrodeposited platinum nanowires and their applications. Platinum (Pt) nanowires were fabricated by a galvanostatic electrodeposition method in a porous anodic alumina oxide (AAO) template with different current densities. Both direct current and pulse current electrodeposition were used to synthesize the Pt nanowires. The grain size and surface morphology of the Pt nanowires were studied by field emission scanning electron microscopy (FE-SEM), transmission electron microcopy (TEM) and X-ray diffraction (XRD). The experimental results showed that the current density was the key factor to control the surface roughness. The surface of the Pt nanowires became rougher and the grain sizes were increased by increasing the current densities. From the experimental results, a growth mechanism of Pt nanowires based on progressive nucleation and crystallization was proposed in order to find out the relationship between the surface morphology and current density. The electrochemical properties and catalytic activities of these surface roughed Pt nanowires were investigated in the detection of H20 2 and for the methanol oxidation. Cyclic voltammograms of Pt nanowire modified electrodes were obtained using a potentiostat, which showed that rougher Pt nanowires have higher response and better activity than that of smooth nanowires. For H202 detection, the effect of scan rate and H202 concentration were studied and it was found that the peak current for hydrogen peroxide reduction became larger with the increasing of either scan rate or H202 concentration. It can be inferred that the process of electrocatalytic hydrogen peroxide reduction may be controlled by diffusion of hydrogen peroxide and the Pt nanowire modified glassy carbon electrode (GCE) is well suited for the detection of H202. From the relationship between the peak current and square root of scan rates for methanol oxidation, it can be inferred that the process of electrocatalytic methanol oxidation was controlled by diffusion of methanol. To understand the effect of the morphological feature on the electrocatalytic activity of the Pt nanowire catalysts, the electrochemically active surface area (ECSA) as a function of deposited current density was investigated, which suggests that Pt nanowire catalysts deposited at highest current density had the most ECSA surface morphology of the Pt nanowires. The chronoamperometric curves and electrochemical impedance spectroscopy (EIS) results confirmed that the Pt nanowire catalyst synthesized at higher current density possessed longer durability and gave more efficient electrochemical performance.
Machinability of IPS Empress 2 framework ceramic.

PubMed

Schmidt, C; Weigl, P

2000-01-01

Using ceramic materials for an automatic production of ceramic dentures by CAD/CAM is a challenge, because many technological, medical, and optical demands must be considered. The IPS Empress 2 framework ceramic meets most of them. This study shows the possibilities for machining this ceramic with economical parameters. The long life-time requirement for ceramic dentures requires a ductile machined surface to avoid the well-known subsurface damages of brittle materials caused by machining. Slow and rapid damage propagation begins at break outs and cracks, and limits life-time significantly. Therefore, ductile machined surfaces are an important demand for machine dental ceramics. The machining tests were performed with various parameters such as tool grain size and feed speed. Denture ceramics were machined by jig grinding on a 5-axis CNC milling machine (Maho HGF 500) with a high-speed spindle up to 120,000 rpm. The results of the wear test indicate low tool wear. With one tool, you can machine eight occlusal surfaces including roughing and finishing. One occlusal surface takes about 60 min machining time. Recommended parameters for roughing are middle diamond grain size (D107), cutting speed v(c) = 4.7 m/s, feed speed v(ft) = 1000 mm/min, depth of cut a(e) = 0.06 mm, width of contact a(p) = 0.8 mm, and for finishing ultra fine diamond grain size (D46), cutting speed v(c) = 4.7 m/s, feed speed v(ft) = 100 mm/min, depth of cut a(e) = 0.02 mm, width of contact a(p) = 0.8 mm. The results of the machining tests give a reference for using IPS Empress(R) 2 framework ceramic in CAD/CAM systems. Copyright 2000 John Wiley & Sons, Inc.
Mechanisms by which oxygen acts as a surfactant in giant magnetoresistance film growth

NASA Astrophysics Data System (ADS)

Larson, D. J.; Petford-Long, A. K.; Cerezo, A.; Bozeman, S. P.; Morrone, A.; Ma, Y. Q.; Georgalakis, A.; Clifton, P. H.

2003-04-01

The mechanisms by which oxygen acts as a surfactant in giant magnetoresistance multilayers have been elucidated for the first time. Three-dimensional atom probe analysis of Cu/CoFe multilayers reveals the elemental distributions at the atomic level. Interfacial intermixing and oxygen impurity levels have been quantified for the first time. Both with and without oxygen the intermixing is greater at the CoFe-on-Cu interface than at the Cu-on-CoFe one and for both interfaces, oxygen reduced the intermixing. The oxygen largely floats to the growing surface and is incorporated at grain boundaries. The oxygen also reduces conformal roughness and grain boundary grooving, indicating a reduction in long-range surface diffusion.
Nanoscale imaging of photocurrent and efficiency in CdTe solar cells

DOE PAGES

Leite, Marina S.; National Inst. of Standards and Technology; Abashin, Maxim; ...

2014-10-15

The local collection characteristics of grain interiors and grain boundaries in thin film CdTe polycrystalline solar cells are investigated using scanning photocurrent microscopy. The carriers are locally generated by light injected through a small aperture (50-300 nm) of a near-field scanning optical microscope in an illumination mode. Possible influence of rough surface topography on light coupling is examined and eliminated by sculpting smooth wedges on the granular CdTe surface. By varying the wavelength of light, nanoscale spatial variations in external quantum efficiency are mapped. We find that the grain boundaries (GBs) are better current collectors than the grain interiors (GIs).more » The increased collection efficiency is caused by two distinct effects associated with the material composition of GBs. First, GBs are charged, and the corresponding built-in field facilitates the separation and the extraction of the photogenerated carriers. Second, the GB regions generate more photocurrent at long wavelength corresponding to the band edge, which can be caused by a smaller local band gap. As a result, resolving carrier collection with nanoscale resolution in solar cell materials is crucial for optimizing the polycrystalline device performance through appropriate thermal processing and passivation of defect and surfaces.« less
Residual Stress Distribution and Microstructure of a Multiple Laser-Peened Near-Alpha Titanium Alloy

NASA Astrophysics Data System (ADS)

Umapathi, A.; Swaroop, S.

2018-04-01

Laser peening without coating (LPwC) was performed on a Ti-2.5 Cu alloy with multiple passes (1, 3 and 5), using a Nd:YAG laser (1064 nm) at a constant overlap rate of 70% and power density of 6.7 GW cm-2. Hardness and residual stress profiles indicated thermal softening near the surface (< 100 μm) and bulk softening due to adiabatic heating. Maximum hardness (235 HV at 500 μm) and maximum residual stress (- 890 MPa at 100 μm) were observed for LPwC with 1 pass. Surface roughness and surface 3-D topography imaging showed that the surface roughness increased with the increase in the number of passes. XRD results indicated no significant β phases. However, peak shifts, broadening and asymmetry were observed and interpreted based on dislocation activity. Microstructures indicated no melting or resolidification or refinement of grains at the surface. Twin density was found to increase with the increase in the number of passes.
Residual Stress Distribution and Microstructure of a Multiple Laser-Peened Near-Alpha Titanium Alloy

NASA Astrophysics Data System (ADS)

Umapathi, A.; Swaroop, S.

2018-05-01

Laser peening without coating (LPwC) was performed on a Ti-2.5 Cu alloy with multiple passes (1, 3 and 5), using a Nd:YAG laser (1064 nm) at a constant overlap rate of 70% and power density of 6.7 GW cm-2. Hardness and residual stress profiles indicated thermal softening near the surface (< 100 μm) and bulk softening due to adiabatic heating. Maximum hardness (235 HV at 500 μm) and maximum residual stress (- 890 MPa at 100 μm) were observed for LPwC with 1 pass. Surface roughness and surface 3-D topography imaging showed that the surface roughness increased with the increase in the number of passes. XRD results indicated no significant β phases. However, peak shifts, broadening and asymmetry were observed and interpreted based on dislocation activity. Microstructures indicated no melting or resolidification or refinement of grains at the surface. Twin density was found to increase with the increase in the number of passes.
Underestimated role of the secondary electron emission in the space

NASA Astrophysics Data System (ADS)

Nemecek, Zdenek; Richterova, Ivana; Safrankova, Jana; Pavlu, Jiri; Vaverka, Jakub; Nouzak, Libor

2016-07-01

Secondary electron emission (SEE) is one of many processes that charges surfaces of bodies immersed into a plasma. Until present, a majority of considerations in theories and experiments is based on the sixty year old description of an interaction of planar metallic surfaces with electrons, thus the effects of a surface curvature, roughness, presence of clusters as well as an influence of the material conductance on different aspects of this interaction are neglected. Dust grains or their clusters can be frequently found in many space environments - interstellar clouds, atmospheres of planets, tails of comets or planetary rings are only typical examples. The grains are exposed to electrons of different energies and they can acquire positive or negative charge during this interaction. We review the progress in experimental investigations and computer simulations of the SEE from samples relevant to space that was achieved in course of the last decade. We present a systematic study of well-defined systems that starts from spherical grains of various diameters and materials, and it continues with clusters consisting of different numbers of small spherical grains that can be considered as examples of real irregularly shaped space grains. The charges acquired by investigated objects as well as their secondary emission yields are calculated using the SEE model. We show that (1) the charge and surface potential of clusters exposed to the electron beam are influenced by the number of grains and by their geometry within a particular cluster, (2) the model results are in an excellent agreement with the experiment, and (3) there is a large difference between charging of a cluster levitating in the free space and that attached to a planar surface. The calculation provides a reduction of the secondary electron emission yield of the surface covered by dust clusters by a factor up to 1.5 with respect to the yield of a smooth surface. (4) These results are applied on charging of the lunar surface and the dust grains levitating above it, and it is shown that the SEE is more important for isolated dust grains than for the lunar surface covered by them.
Carbon storage potential of Columbia River flood basalt

NASA Astrophysics Data System (ADS)

Wells, R. K.; Xiong, W.; Giammar, D.; Skemer, P. A.

2017-12-01

Basalt reservoirs are an important option for sequestering carbon through dissolution of host rock and precipitation of stable carbonate minerals. This study seeks to understand the nature of dissolution and surface roughening processes and their influence on the timing and spatial distribution of carbonation, in static experiments at 150 °C and 100 bar CO2. Intact samples and cores with milled pathways from Ca-rich and Fe-rich Columbia River flood basalt formations were reacted for up to 40 weeks. Experimental specimens were analyzed using SEM-EDS, microprobe, and μCT scanning, Raman spectroscopy, and 2D profilometer to characterize changes in composition and surface roughness. ICP-MS was used to examine bulk fluid chemistry. Initial dissolution of olivine grains results in higher Mg2+ and Fe2+ concentrations within the bulk solution in the first week of reaction. However, once available olivine grains are gone, Ca-rich pyroxene becomes the primary contributor of Ca2+, Mg2+, and Fe2+ within the bulk solution. The complete dissolution of olivine grains resulted in pits up to 200 μm deep. Dissolution of other minerals resulted in the formation of microscale textures, primarily along grain boundaries and fractures. The surface roughness increased by factors of up to 42, while surface area increased 20%. Based on these results, pyroxene is the sustaining contributor of divalent metal cations during dissolution of basalt, and the limited connectivity of olivine and pyroxene grains limits the exposure of new reactive surface areas. Within 6 weeks, aragonite precipitated in Ca-rich basalt samples, while Fe-rich samples precipitated of siderite. The highest concentration of carbonates occurs 1/3 into milled pathways, which simulate dead-end fractures, in low porosity basalts, and near the fracture tip in high porosity basalts. Even at elevated temperatures, the fractures are not blocked nor filled within 40 weeks of reaction. When vesicles are present, carbonates can precipitate within these pores even when the pores do not appear to connect to the main fracture pathway. Based on our experimental results, we estimate the carbon storage potential of the Ca-rich formations within the Columbia River flood basalt to be 47 kg CO2/m3, which could be reached in 38 years at a constant carbonation rate of 1.24 ± 0.54 kg CO2/m3yr.
An experimental assessment of the size effects on the strength and ductility of freestanding copper films under macroscopically homogenous deformation

NASA Astrophysics Data System (ADS)

Chauhan, Shakti Singh

Metallic interconnects and circuitry has been experiencing excessive deformation beyond their elastic limits in many applications, ranging from micro-electromechanical systems (MEMS) to flexible electronics. These broad applications are creating needs to understand the extent of strength and ductility of freestanding metallic films at scales approaching the micron and sub micron range. This work aims to elucidate the effects of microstructural constraint as well as geometric dimensional constraint on the strength and ductility of freestanding Cu films under uniaxial tension. Two types of films are tested (i) high purity rolled films of 12.5-100microm thickness and average grain sizes of 11-47microm and (ii) electroplated films of 2-50 microm thickness and average grain sizes of 1.8-5microm. Several experimental tools including residual electrical resistivity measurements, surface strain measurements and surface roughness measurements are employed to highlight the underlying deformation mechanisms leading to the observed size effects. With respect to the strength of the specimens, we find that the nature and magnitude of thickness effects is very sensitive to the average grain size. In all cases, coupled thickness and grain size effects were observed. This study shows that this observed coupling, unique to the case of freestanding specimen, arises because the observed size effects are an outcome of the size dependence of two fundamental microstructural parameters i.e. volume fraction of surface grains and grain boundary area per unit specimen volume. For films having thickness and grain sizes greater than 5microm, thickness dependent weakening is observed for a constant grain size. Reducing thickness results in an increase in the volume fraction of grains exposed to the free surface as well as a reduction in the grain boundary area per unit specimen volume. The former effect leads to a reduction in the effective microstructural constraint on the intragranular dislocation activity in individual grains. This free surface related effect is the origin of a weakening contribution to the overall specimen strength with reducing thickness. For specimens with grain sizes ˜ O (10-50microm), this effect was found to be dominating i.e. reducing thickness resulted in reducing strength. A phenomenological model employing the flow strength of surface and bulk grains is proposed to model the observed trends. For films having thickness and grain sizes smaller than 5microm, size dependent strengthening is observed for a constant grain size. At this scale, grain boundary dislocations dominate. As a consequence, thickness effects arise because grain boundary dislocation source density per unit specimen volume reduces with reducing specimen thickness. This statistical reduction in dislocation source density leads to increasing specimen strength via source starvation strengthening. Our results show that such increasing specimen strength with reducing thickness, which has only been observed previously for nanocrystalline thin films, first appears at average grain size of ˜5microm or xx smaller. The measurements showed a characteristic length scale of about 5microm, which defines the size dependent strengthening or weakening of the film. With respect to the thickness effects on ductility, it was found that both thickness and average grain size affect ductility. While prominent thickness effects persist at larger grain sizes, for specimens with grain size approaching 1microm, the loss of strain hardening ability at such fine microstructures dominates and a limiting ductility of ˜2% is seen irrespective of the thickness. The observed thickness effects on ductility were investigated via surface roughness measurements that allow the characterization of initiation and evolution of deformation heterogeneities. It was found that thickness has a strong influence on the characteristic heterogeneity of deformation. At small specimen thicknesses, the deformation was found to be highly localized i.e. widely spaced regions showing substantial thickness reduction, hence increasing the vulnerability to the onset of plastic instabilities. At larger thicknesses, however, the increasing microstructural constraint delocalizes the strain and thereby precludes the early onset of instability, leading to enhanced ductility.

Corrosion resistant surface for vanadium nitride and hafnium nitride layers as function of grain size

NASA Astrophysics Data System (ADS)

Escobar, C. A.; Caicedo, J. C.; Aperador, W.

2014-01-01

In this research it was studied vanadium nitride (VN) and hafnium nitride (HfN) film, which were deposited onto silicon (Si (100)) and AISI 4140 steel substrates via r.f. magnetron sputtering technique in Ar/N2 atmosphere with purity at 99.99% for both V and Hf metallic targets. Both films were approximately 1.2±0.1 μm thick. The crystallography structures that were evaluated via X-ray diffraction analysis (XRD) showed preferential orientations in the Bragg planes VN (200) and HfN (111). The chemical compositions for both films were characterized by EDX. Atomic Force Microscopy (AFM) was used to study the morphology; the results reveal grain sizes of 78±2 nm for VN and 58±2 nm for HfN and roughness values of 4.2±0.1 nm for VN and 1.5±0.1 nm for HfN films. The electrochemical performance in VN and HfN films deposited onto steel 4140 were studied by Tafel polarization curves and impedance spectroscopy methods (EIS) under contact with sodium chloride at 3.5 wt% solution, therefore, it was found that the corrosion rate decreased about 95% in VN and 99% for HfN films in relation to uncoated 4140 steel, thus demonstrating, the protecting effect of VN and HfN films under a corrosive environment as function of morphological characteristics (grain size). VN(grain size)=78±2.0 nm, VN(roughness)=4.2±0.1 nm, VN(corrosion rate)=40.87 μmy. HfN(grain size)=58±2.0 nm, HfN(roughness)=1.5±0.1 nm, HfN(corrosion rate)=0.205 μmy. It was possible to analyze that films with larger grain size, can be observed smaller grain boundary thus generating a higher corrosion rate, therefore, in this work it was found that the HfN layer has better corrosion resistance (low corrosion rate) in relation to VN film which presents a larger grain size, indicating that the low grain boundary in (VN films) does not restrict movement of the Cl- ion and in this way the corrosion rate increases dramatically.
Characterization of self-affinity in the global regime

NASA Astrophysics Data System (ADS)

Neimark, Alexander V.

1994-11-01

Methods for characterization of self-affine surfaces and measurements of their roughness exponents H are developed. It is shown that for smoothed surfaces, which underwent particular coarse graining or averaging of the small-scale fluctuations, the excess surface area Sex and the mean square root radius of curvature ac are related by two distinct asymptotic power laws if ac is well below or well above a certain crossover scale acr. In the local regime of self-affinity, when ac<>acr, Sex~(ac/acr)-2(1-H)/(2-H). The former scaling relationship is consistent with the well known definition of local fractal dimensions dloc=dtop+1-H. The latter scaling relationship offers alternatives for characterization of self-affinity over large scales by means of excess dimensions defined as dex=dtop+2(1-H)/(2-H) and can be used for determination of roughness exponents from the measurements provided in the global regime. The thermodynamic method of fractal analysis, proposed earlier for self-similar surfaces (A.V. Neimark, Pis'ma Zh. Eksp. Teor. Fiz. 51, 535 (1990) [JETP Lett. 51, 607 (1990)]; Physica A 191, 258 (1992)), is extended for self-affine surfaces for determination of fractal dimensions and roughness exponents from adsorption and capillary experimental data.
Ultrasonic impact peening for the surface properties’ management

NASA Astrophysics Data System (ADS)

Mordyuk, Bohdan N.; Prokopenko, Georgiy I.

2007-12-01

It is demonstrated that the ultrasonic impact peening (UIP) technique is a beneficial method for essential increase in the fatigue durability of metallic materials due to the surface nanocrystallization and hardening process provided for severe plastic deformation of surface via multiple impacts of high velocity impact pins. Nano-scale grain structures were obtained in the surface layers of stainless steel, low carbon steel weld and different titanium alloys using developed equipment for the UIP. Both the surface nanostructure and compressive residual stresses are shown to attribute to the essential hardness increase. It is revealed experimentally using profilometry that new modification of the UIP apparatus providing high velocity "sliding" impacts leads to marked diminution of the surface roughness, which is another important factor affecting to the fatigue cracks initiation process. The two-dimensional finite element model is used to simulate the indent formation process during single impaction. The solid steel pin and the Al alloy plate are modeled as a rigid material and an elasto-plastic material, respectively. It is shown that the surface roughness magnitude depends on the correlation of the vertical and lateral load components.
Direct laser metal sintering as a new approach to fabrication of an isoelastic functionally graded material for manufacture of porous titanium dental implants.

PubMed

Traini, T; Mangano, C; Sammons, R L; Mangano, F; Macchi, A; Piattelli, A

2008-11-01

This work focuses on a titanium alloy implants incorporating a gradient of porosity, from the inner core to the outer surface, obtained by laser sintering of metal powder. Surface appearance, microstructure, composition, mechanical properties and fractography were evaluated. All the specimens were prepared by a selective laser sintering procedure using a Ti-6Al-4V alloy powder with a particle size of 1-10 microm. The morphological and chemical analyses were performed by SEM and energy dispersive X-ray spectroscopy. The flexure strength was determined by a three-point bend test using a universal testing machine. The surface roughness was investigated using a confocal scanning laser microscope. The surface roughness variation was statistically evaluated by use of a Chi square test. A p value of <0.05 was considered statistically significant. The original surface microstructure consisted of roughly spherical particles, diameter range 5-50 microm. After exposure to hydrofluoric acid some of these were removed and the microsphere diameter then ranged from 5.1 microm to 26.8 microm. Following an organic acid treatment, particles were replaced by grooves 14.6-152.5 microm in width and 21.4-102.4 microm depth. The metal core consisted of columnar beta grains with alpha and beta laths within the grains. The alloy was composed of 90.08% Ti, 5.67% Al and 4.25% V. The Young's modulus of the inner core material was 104+/-7.7 GPa; while that of the outer porous material was 77+/-3.5 GPa. The fracture face showed a dimpled appearance typical of ductile fracture. In conclusion, laser metal sintering proved to be an efficient means of construction of dental implants with a functionally graded material which is better adapted to the elastic properties of the bone. Such implants should minimize stress shielding effects and improve long-term performance.
A theoretical analysis of colloid attachment and straining in chemically heterogeneous porous media.

PubMed

Bradford, Scott A; Torkzaban, Saeed; Shapiro, Alexander

2013-06-11

A balance of applied hydrodynamic (T(H)) and resisting adhesive (T(A)) torques was conducted over a chemically heterogeneous porous medium that contained random roughness of height h(r) to determine the fraction of the solid surface area that contributes to colloid immobilization (S(f)*) under unfavorable attachment conditions. This model considers resistance due to deformation and the horizontal component of the adhesive force (F(AT)), spatial variations in the pore scale velocity distribution, and the influence of hr on lever arms for T(H) and T(A). Values of S(f)* were calculated for a wide range of physicochemical properties to gain insight into mechanisms and factors influencing colloid immobilization. Colloid attachment processes were demonstrated to depend on solution ionic strength (IS), the colloid radius (r(c)), the Young's modulus (K), the amount of chemical heterogeneity (P+), and the Darcy velocity (q). Colloid immobilization was also demonstrated to occur on a rough surface in the absence of attachment. In this case, S(f)* depended on IS, r(c), the roughness fraction (f0), h(r), and q. Roughness tended to enhance T(A) and diminish T(H). Consequently, the effect of IS on S(f)* was enhanced by h(r) relative to attachment. In contrast, the effects of r(c) and q on S(f)* were diminished by hr in comparison to attachment. Colloid immobilization adjacent to macroscopic roughness locations shares many similarities to grain-grain contact points and may be viewed as a type of straining process. In general, attachment was more important for higher IS and variance in the secondary minimum, and for smaller r(c), q, and K, but diffusion decreased these values. Conversely, straining was dominant for the opposite conditions. Discrepancies in the literature on mechanisms of colloid retention are likely due to a lack of consideration of all of these factors.
The nanostructure and microstructure of SiC surface layers deposited by MWCVD and ECRCVD

NASA Astrophysics Data System (ADS)

Dul, K.; Jonas, S.; Handke, B.

2017-12-01

Scanning electron microscopy (SEM) and Atomic force microscopy (AFM) have been used to investigate ex-situ the surface topography of SiC layers deposited on Si(100) by Microwave Chemical Vapour Deposition (MWCVD) -S1,S2 layers and Electron Cyclotron Resonance Chemical Vapor Deposition (ECRCVD) - layers S3,S4, using silane, methane, and hydrogen. The effects of sample temperature and gas flow on the nanostructure and microstructure have been investigated. The nanostructure was described by three-dimensional surface roughness analysis based on digital image processing, which gives a tool to quantify different aspects of surface features. A total of 13 different numerical parameters used to describe the surface topography were used. The scanning electron image (SEM) of the microstructure of layers S1, S2, and S4 was similar, however, layer S3 was completely different; appearing like grains. Nonetheless, it can be seen that no grain boundary structure is present in the AFM images.
Verification of roughness coefficients for selected natural and constructed stream channels in Arizona

USGS Publications Warehouse

Phillips, Jeff V.; Ingersoll, Todd L.

1998-01-01

Physical and hydraulic characteristics are presented for 14 river and canal reaches in Arizona for which 37 roughness coefficients have been determined. The verified roughness coefficients which ranged from 0.017 to 0.067, were computed from discharges, channel geometry, and water-surface profiles measured at each of the sites. The information given for each stream segment includes bed and bank descriptions, data tables showing hydraulic components, a plan view, cross-section plots, and color photographs that can be used as a comparison aid in determining roughness coefficients for similarly channeled streams. Relations derived from the data presented relate Manning's roughness coefficient (n) to various hydraulic components. For gravel-bed streams, verified roughness coefficients are related to median grain size of the bed material and hydraulic radius resulting in an equation that can be used to transfer results to similar dry-land channels. The equation developed for base values of n for gravel-bed channels in Arizona is significantly different from similarly derived equations for other regions of the United States and the world.
Effect of roughness formulation on the performance of a coupled wave, hydrodynamic, and sediment transport model

USGS Publications Warehouse

Ganju, Neil K.; Sherwood, Christopher R.

2010-01-01

A variety of algorithms are available for parameterizing the hydrodynamic bottom roughness associated with grain size, saltation, bedforms, and wave–current interaction in coastal ocean models. These parameterizations give rise to spatially and temporally variable bottom-drag coefficients that ostensibly provide better representations of physical processes than uniform and constant coefficients. However, few studies have been performed to determine whether improved representation of these variable bottom roughness components translates into measurable improvements in model skill. We test the hypothesis that improved representation of variable bottom roughness improves performance with respect to near-bed circulation, bottom stresses, or turbulence dissipation. The inner shelf south of Martha’s Vineyard, Massachusetts, is the site of sorted grain-size features which exhibit sharp alongshore variations in grain size and ripple geometry over gentle bathymetric relief; this area provides a suitable testing ground for roughness parameterizations. We first establish the skill of a nested regional model for currents, waves, stresses, and turbulent quantities using a uniform and constant roughness; we then gauge model skill with various parameterization of roughness, which account for the influence of the wave-boundary layer, grain size, saltation, and rippled bedforms. We find that commonly used representations of ripple-induced roughness, when combined with a wave–current interaction routine, do not significantly improve skill for circulation, and significantly decrease skill with respect to stresses and turbulence dissipation. Ripple orientation with respect to dominant currents and ripple shape may be responsible for complicating a straightforward estimate of the roughness contribution from ripples. In addition, sediment-induced stratification may be responsible for lower stresses than predicted by the wave–current interaction model.
SEM and AFM studies of dip-coated CuO nanofilms.

PubMed

Dhanasekaran, V; Mahalingam, T; Ganesan, V

2013-01-01

Cupric oxide (CuO) semiconducting thin films were prepared at various copper sulfate concentrations by dip coating. The copper sulfate concentration was varied to yield films of thicknesses in the range of 445-685 nm by surface profilometer. X-ray diffraction patterns revealed that the deposited films were polycrystalline in nature with monoclinic structure of (-111) plane. The surface morphology and topography of monoclinic-phase CuO thin films were examined using scanning electron microscopy (SEM) and atomic force microscopy (AFM), respectively. Surface roughness profile was plotted using WSxM software and the estimated surface roughness was about ∼19.4 nm at 30 mM molar concentration. The nanosheets shaped grains were observed by SEM and AFM studies. The stoichiometric compound formation was observed at 30 mM copper sulfate concentration prepared film by EDX. The indirect band gap energy of CuO films was increased from 1.08 to 1.20 eV with the increase of copper sulfate concentrations. Copyright © 2012 Wiley Periodicals, Inc.
Creep shear behavior of the oxide dispersion strengthened superalloy MA 6000E

NASA Technical Reports Server (NTRS)

Glasgow, T. K.

1981-01-01

The shear rupture life of the oxide dispersion strengthened (ODS) superalloy MA 6000E was determined at 650 and 760 C was 250 MPa. Comparisons were made at 760 C with the conventional cast superalloy B-1900+Hf, the ODS alloy MA 754, and the directionally solidified eutectic alloy gamma/gamma prime-delta was 170 MPa, and for B-1900+Hf was 360 MPa. The ODS alloy MA 6000E and gamma/gamma prime-delta failed with very little indication of ductile accommodation. Both MA 754 and B-1900+Hf showed some ductile tearing. Fracture surfaces of the ODS alloy MA 754 showed discontinuities similar size, shape, and roughness to its grain structure, but the fracture surfaces of MA 6000E were much smoother than its grain boundaries.
Thermal Emission Spectroscopy of 1 Ceres: Evidence for Olivine

NASA Technical Reports Server (NTRS)

Witteborn, F. C.; Roush, T. L.; Cohen, M.

1999-01-01

Thermal emission spectra of the largest asteroid 1 Ceres obtained from the Kuiper Airborne Observatory display features that may provide information on its surface mineralogy. A plot of the Ceres spectrum (calibrated using alpha Boo as a standard) divided by a standard thermal model (STM) is shown. Also shown is the emissivity spectrum deduced from reflectivity measurements for olivine grains <5 microns in diameter. The general shape of the Ceres and the olivine curves agree in essential details, such as the maxima from 8 to 12 microns, the minimum between 12 and 14 microns, the broad peak near 17.5 micron, and the slope beyond 22 micron. (Use of the 10 to 15-micron grain reflectivities provides a better match to the 12- to 14-micron dip. We used a value of unity for beta, the beaming factor associated with small-scale surface roughness in our STM. Adjustment of beta to a lower value raises the long-wavelength side of the Ceres spectrum, providing an even better match to the olivine curve.) The emissivity behavior roughly matches the emission coefficients which were calculated for olivine particles with a particle radius of 3 microns. Their calculations show not only the negative slope from 23 to 25 pm, but a continued decrease past 30 micron. The Ceres emissivity is thus similar to that of small olivine grains from 8 to 30 micron, but olivine's emissivity is lower from 5 to 8 pm.
Surface scanning inspection system particle detection dependence on aluminum film morphology

NASA Astrophysics Data System (ADS)

Prater, Walter; Tran, Natalie; McGarvey, Steve

2012-03-01

Physical vapor deposition (PVD) aluminum films present unique challenges when detecting particulate defects with a Surface Scanning Inspection System (SSIS). Aluminum (Al) films 4500Å thick were deposited on 300mm particle grade bare Si wafers at two temperatures using a Novellus Systems INOVA® NExT,.. Film surface roughness and morphology measurements were performed using a Veeco Vx310® atomic force microscope (AFM). AFM characterization found the high deposition temperature (TD) Al roughness (Root Mean Square 16.5 nm) to be five-times rougher than the low-TD Al roughness (rms 3.7 nm). High-TD Al had grooves at the grain boundaries that were measured to be 20 to 80 nm deep. Scanning electron microscopy (SEM) examination, with a Hitachi RS6000 defect review SEM, confirmed the presence of pronounced grain grooves. SEM images established that the low-TD filmed wafers have fine grains (0.1 to 0.3 um diameter) and the high-TD film wafers have fifty-times larger equiaxed plateletshape grains (5 to 15 um diameter). Calibrated Poly-Styrene Latex (PSL) spheres ranging in size from 90 nm to 1 μm were deposited in circular patterns on the wafers using an aerosol deposition chamber. PSL sphere depositions at each spot were controlled to yield 2000 to 5000 counts. A Hitachi LS9100® dark field full wafer SSIS was used to experimentally determine the relationship of the PSL sphere scattered light intensity with S-polarized light, a measure of scattering cross-section, with respect to the calibrated PSL sphere diameter. Comparison of the SSIS scattered light versus PSL spot size calibration curves shows two distinct differences. Scattering cross-section (intensity) of the PSL spheres increased on the low-TD Al film with smooth surface roughness and the low-TD Al film defect detection sensitivity was 126 nm compared to 200 nm for the rougher high- TD Al film. This can be explained by the higher signal to noise attributed to the smooth low-TD Al. Dark field defect detection on surface scanning inspection systems is used to rapidly measure defectivity data. The user generates a calibration curve on the SSIS to plot the intensity of the light scattering derived at each National Institute of Standards and Technology (NIST) certified PSL deposition spot that was deposited. It is not uncommon for the end user to embark upon the time consuming process of attempting to "push" the maximal SSIS film specific sensitivity curve beyond the optical performance capability of the SSIS. Bidirectional reflectance distribution function (BRDF) light scattering modeling was utilized as a means of determining the most appropriate polarity prior to the SSIS recipe creation process. The modeling utilized the Al refractive index (n) and extinction coefficient (k) and the SSIS detector angles and laser wavelength. The modeling results allowed predetermination of the maximal sensitivity for each different Al thickness and eliminate unnecessary recipe modification trial-and-error in search of the SSIS maximal sensitivity. The modeling accurately forecasted the optimal polarization and maximal sensitivity of the SSIS recipe, which, by avoiding a trial and error approach, can result in a substantial savings in time and resources.
Suppressed Superconductivity on the Surface of Superconducting RF Quality Niobium for Particle Accelerating Cavities

NASA Astrophysics Data System (ADS)

Sung, Z. H.; Polyanskii, A. A.; Lee, P. J.; Gurevich, A.; Larbalestier, D. C.

2011-03-01

Significant performance degradation of superconducting RF (radio frequency) niobium cavities in high RF field is strongly associated with the breakdown of superconductivity on localized multi-scale surface defects lying within the 40 nm penetration depth. These defects may be on the nanometer scale, like grain boundaries and dislocations or even at the much larger scale of surface roughness and welding pits. By combining multiple superconducting characterization techniques including magneto-optical (MO) imaging and direct transport measurement with non-contact characterization of the surface topology using scanning confocal microscopy, we were able to show clear evidence of suppression of surface superconductivity at chemically treated RF-quality niobium. We found that pinning of vortices along GBs is weaker than pinning of vortices in the grains, which may indicate suppressed superfluid density on GBs. We also directly measured the local magnetic characteristics of BCP-treated Nb sample surface using a micro-Hall sensor in order to further understanding of the effect of surface topological features on the breakdown of superconducting state in RF mode.
Increasing the hydrophobicity degree of stonework by means of laser surface texturing: An application on Zimbabwe black granites

NASA Astrophysics Data System (ADS)

Chantada, A.; Penide, J.; Riveiro, A.; del Val, J.; Quintero, F.; Meixus, M.; Soto, R.; Lusquiños, F.; Pou, J.

2017-10-01

Tailoring the wetting characteristics of materials has gained much interest in applications related to surface cleaning in both industry and home. Zimbabwe black granite is a middle-to-fine-grained natural stone commonly used as countertops in kitchens and bathrooms. In this study, the laser texturing of Zimbabwe black granite surfaces is investigated with the aim to enhance its hydrophobic character, thus reducing the attachment of contaminants on the surface. Two laser sources (λ = 1064 and 532 nm) were used for this purpose. The treatment is based on the irradiation of the stone by a laser focused on the surface of the targeting sample. The influence of different laser processing parameters on the surface characteristics of granite (wettability, roughness, and chemistry) was statistically assessed. Most suitable laser processing parameters required to obtain the highest hydrophobicity degree were identified. It has been possible to identify the 532 nm laser wavelength as the most effective one to increase the hydrophobic degree of Zimbabwe black granite surface. The phenomenon governing wettability changes was found to be the surface roughness patterns, given the unaltered chemical surface composition after laser processing.
Characteristics of Iron-Palladium alloy thin films deposited by magnetron sputtering

NASA Astrophysics Data System (ADS)

Chiu, Y.-J.; Shen, C.-Y.; Chang, H.-W.; Jian, S.-R.

2018-06-01

The microstructural features, magnetic, nanomechanical properties and wettability behaviors of Iron-Palladium (FePd) alloy thin films are investigated by using X-ray diffraction (XRD), atomic force microscopy (AFM), vibrating sample magnetometer (VSM), nanoindentation and water contact angle (CA) techniques, respectively. The FePd alloy thin films were deposited on glass substrates using a magnetron sputtering system. The post-annealing processes of FePd alloy thin films were carried out at 400 °C and 750 °C and resulted in a significant increase of both the average grain size and surface roughness. The XRD analysis showed that FePd alloy thin films exhibited a predominant (1 1 1) orientation. The magnetic field dependence of magnetization of all FePd thin films are measured at room temperature showed the ferromagnetic characteristics. The nanoindentation with continuous stiffness measurement (CSM) is used to measure the hardness and Young's modulus of present films. The contact angle (θCA) increased with increasing surface roughness. The maximum θCA of 75° was achieved for the FePd alloy thin film after annealing at 750 °C and a surface roughness of 4.2 nm.
In situ study on surface roughening in radiation-resistant Ag nanowires

NASA Astrophysics Data System (ADS)

Shang, Z.; Li, Jin; Fan, C.; Chen, Y.; Li, Q.; Wang, H.; Shen, T. D.; Zhang, X.

2018-05-01

Metallic materials subjected to heavy ion irradiation experience significant radiation damage. Free surface is a type of effective defect sinks to improve the radiation resistance in metallic materials. However, the radiation resistance of metallic nanowires (NWs) is largely unknown. Here we show, via in situ Kr ion irradiations in a transmission electron microscope, Ag NWs exhibited much better radiation resistance than coarse-grained Ag. Irradiation-induced prominent surface roughening in Ag NWs provides direct evidence for interaction between defect clusters and free surface. Diameter dependent variation of the surface roughness in irradiated Ag NWs has also been observed. This study provides insight on mechanisms of enhanced radiation resistance via free surfaces in metallic NWs.
In situ study on surface roughening in radiation-resistant Ag nanowires.

PubMed

Shang, Z; Li, Jin; Fan, C; Chen, Y; Li, Q; Wang, H; Shen, T D; Zhang, X

2018-05-25

Metallic materials subjected to heavy ion irradiation experience significant radiation damage. Free surface is a type of effective defect sinks to improve the radiation resistance in metallic materials. However, the radiation resistance of metallic nanowires (NWs) is largely unknown. Here we show, via in situ Kr ion irradiations in a transmission electron microscope, Ag NWs exhibited much better radiation resistance than coarse-grained Ag. Irradiation-induced prominent surface roughening in Ag NWs provides direct evidence for interaction between defect clusters and free surface. Diameter dependent variation of the surface roughness in irradiated Ag NWs has also been observed. This study provides insight on mechanisms of enhanced radiation resistance via free surfaces in metallic NWs.
Characterization of erosion of metallic materials under cavitation attack in a mineral oil

NASA Technical Reports Server (NTRS)

Rao, B. C. S.; Buckley, D. H.

1985-01-01

Cavitation erosion and erosion rates of eight metallic materials representing three crystal structures were studied. The erosion experiments were conducted with a 20-kHz ultrasonic magnetostrictive oscillator in a viscous mineral oil. The erosion rates of the metals with an fcc matrix were 10 to 100 times higher than that of an hop-matrix titanium alloy. The erosion rates of iron and molybdenum, with bcc matrices, were higher than that of the titanium alloy but lower than those of those of the fcc materials. Studies with scanning electron microscopy indicated that the cavitation pits were initially formed at the grain boundaries and precipitates and that the pits formed at the junction of grain boundaries grew faster than the others. Transcrystalline craters formed by cavitation attack over the surface of grains and roughened the surfaces by multiple slip and twinning. Surface roughness measurements showed that the pits that formed over the grain boundaries deepened faster than pits. Computer analysis revealed that a geometric expression describes the nondimensional erosion curves during the time period 0.5 t (sub 0) t 2.5 t (sub 0), where t (sub 0) is the incubation period. The fcc metals had very short incubation periods; the titanium alloy had the longest incubation period.
Surface polishing of niobium for superconducting radio frequency (SRF) cavity applications

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhao, Liang

2014-08-01

Niobium cavities are important components in modern particle accelerators based on superconducting radio frequency (SRF) technology. The interior of SRF cavities are cleaned and polished in order to produce high accelerating field and low power dissipation on the cavity wall. Current polishing methods, buffered chemical polishing (BCP) and electro-polishing (EP), have their advantages and limitations. We seek to improve current methods and explore laser polishing (LP) as a greener alternative of chemical methods. The topography and removal rate of BCP at different conditions (duration, temperature, sample orientation, flow rate) was studied with optical microscopy, scanning electron microscopy (SEM), and electronmore » backscatter diffraction (EBSD). Differential etching on different crystal orientations is the main contributor to fine grain niobium BCP topography, with gas evolution playing a secondary role. The surface of single crystal and bi-crystal niobium is smooth even after heavy BCP. The topography of fine grain niobium depends on total removal. The removal rate increases with temperature and surface acid flow rate within the rage of 0~20 °C, with chemical reaction being the possible dominate rate control mechanism. Surface flow helps to regulate temperature and avoid gas accumulation on the surface. The effect of surface flow rate on niobium EP was studied with optical microscopy, atomic force microscopy (AFM), and power spectral density (PSD) analysis. Within the range of 0~3.7 cm/s, no significant difference was found on the removal rate and the macro roughness. Possible improvement on the micro roughness with increased surface flow rate was observed. The effect of fluence and pulse accumulation on niobium topography during LP was studied with optical microscopy, SEM, AFM, and PSD analysis. Polishing on micro scale was achieved within fluence range of 0.57~0.90 J/cm2, with pulse accumulation adjusted accordingly. Larger area treatment was proved possible by overlapping laser tracks at proper ratio. Comparison of topography and PSD indicates that LP smooths the surface in a way similar to EP. The optimized LP parameters were applied to different types of niobium surfaces representing different stages in cavity fabrication. LP reduces the sharpness on rough surfaces effectively, while doing no harm to smooth surfaces. Secondary ion mass spectrometer (SIMS) analysis showed that LP reduces the oxide layer slightly and no contamination occurred from LP. EBSD showed no significant change on crystal structure after LP.« less
Correlation between surface morphology and electrical properties of VO2 films grown by direct thermal oxidation method

NASA Astrophysics Data System (ADS)

Yoon, Joonseok; Park, Changwoo; Park, Sungkyun; Mun, Bongjin Simon; Ju, Honglyoul

2015-10-01

We investigate surface morphology and electrical properties of VO2 films fabricated by direct thermal oxidation method. The VO2 film prepared with oxidation temperature at 580 °C exhibits excellent qualities of VO2 characteristics, e.g. a metal-insulator transition (MIT) near 67 °C, a resistivity ratio of ∼2.3 × 104, and a bandgap of 0.7 eV. The analysis of surface morphology with electrical resistivity of VO2 films reveals that the transport properties of VO2 films are closely related to the grain size and surface roughness that vary with oxidation annealing temperatures.

Structural and electrical properties of sputter deposited ZnO thin films

NASA Astrophysics Data System (ADS)

Muhammed Shameem P., V.; Mekala, Laxman; Kumar, M. Senthil

2018-05-01

The growth of zinc oxide thin films having different oxygen content was achieved at ambient temperature by reactive dc magnetron sputtering technique and their structural and electrical properties are studied. The structural studies show that the films are polycrystalline with a preferential orientation of the grains along the c-axis [002], which increases with increase in oxygen partial pressure. The grain size and the surface roughness of the zinc oxide films are found to decrease with increasing oxygen partial pressure. It is observed that the resistivity of the zinc oxide films can be tuned from semiconducting to insulating regime by varying the oxygen content.
Surface Modification of Solution-Processed ZrO2 Films through Double Coating for Pentacene Thin-Film Transistors

NASA Astrophysics Data System (ADS)

Kwon, Jin-Hyuk; Bae, Jin-Hyuk; Lee, Hyeonju; Park, Jaehoon

2018-03-01

We report the modification of surface properties of solution-processed zirconium oxide (ZrO2) dielectric films achieved by using double-coating process. It is proven that the surface properties of the ZrO2 film are modified through the double-coating process; the surface roughness decreases and the surface energy increases. The present surface modification of the ZrO2 film contributes to an increase in grain size of the pentacene film, thereby increasing the field-effect mobility and decreasing the threshold voltage of the pentacene thin-film transistors (TFTs) having the ZrO2 gate dielectric. Herein, the molecular orientation of pentacene film is also studied based on the results of contact angle and X-ray diffraction measurements. Pentacene molecules on the double-coated ZrO2 film are found to be more tilted than those on the single-coated ZrO2 film, which is attributed to the surface modification of the ZrO2 film. However, no significant differences are observed in insulating properties between the single-and the double-coated ZrO2 dielectric films. Consequently, the characteristic improvements of the pentacene TFTs with the double-coated ZrO2 gate dielectric film can be understood through the increase in pentacene grain size and the reduction in grain boundary density.
Classification Scheme for Diverse Sedimentary and Igneous Rocks Encountered by MSL in Gale Crater

NASA Technical Reports Server (NTRS)

Schmidt, M. E.; Mangold, N.; Fisk, M.; Forni, O.; McLennan, S.; Ming, D. W.; Sumner, D.; Sautter, V.; Williams, A. J.; Gellert, R.

2015-01-01

The Curiosity Rover landed in a lithologically and geochemically diverse region of Mars. We present a recommended rock classification framework based on terrestrial schemes, and adapted for the imaging and analytical capabilities of MSL as well as for rock types distinctive to Mars (e.g., high Fe sediments). After interpreting rock origin from textures, i.e., sedimentary (clastic, bedded), igneous (porphyritic, glassy), or unknown, the overall classification procedure (Fig 1) involves: (1) the characterization of rock type according to grain size and texture; (2) the assignment of geochemical modifiers according to Figs 3 and 4; and if applicable, in depth study of (3) mineralogy and (4) geologic/stratigraphic context. Sedimentary rock types are assigned by measuring grains in the best available resolution image (Table 1) and classifying according to the coarsest resolvable grains as conglomerate/breccia, (coarse, medium, or fine) sandstone, silt-stone, or mudstone. If grains are not resolvable in MAHLI images, grains in the rock are assumed to be silt sized or smaller than surface dust particles. Rocks with low color contrast contrast between grains (e.g., Dismal Lakes, sol 304) are classified according to minimum size of apparent grains from surface roughness or shadows outlining apparent grains. Igneous rocks are described as intrusive or extrusive depending on crystal size and fabric. Igneous textures may be described as granular, porphyritic, phaneritic, aphyric, or glassy depending on crystal size. Further descriptors may include terms such as vesicular or cumulate textures.
Character of the opposition effect and negative polarization

NASA Technical Reports Server (NTRS)

Pieters, Carle M.; Shkuratov, Yu. G.; Stankevich, D. G.

1991-01-01

Photometric and polarimetric properties at small phase angles were measured for silicates with controlled surface properties in order to distinguish properties that are associated with surface reflection from those that are associated with multiple scattering from internal grain boundaries. These data provide insight into the causes and conditions of photometric properties observed at small phase angles for dark bodies of the solar system. Obsidian was chosen to represent a silicate dielectric with no internal scattering boundaries. Because obsidian is free of internal scatterers, light reflected from both the rough and smooth obsidian samples is almost entirely single and multiple Fresnel reflections form surface facets with no body component. Surface structure alone cannot produce an opposition effect. Comparison of the obsidian and basalt results indicates that for an opposition effect to occur, surface texture must be both rough and contain internal scattering interfaces. Although the negative polarization observed for the obsidian samples indicates single and multiple reflections are part of negative polarization, the longer inversion angle of the multigrain inversion samples implies that internal reflections must also contribute a significant negative polarization component.
A multi-topographical-instrument analysis: the breast implant texture measurement

NASA Astrophysics Data System (ADS)

Garabédian, Charles; Delille, Rémi; Deltombe, Raphaël; Anselme, Karine; Atlan, Michael; Bigerelle, Maxence

2017-06-01

Capsular contracture is a major complication after implant-based breast augmentation. To address this tissue reaction, most manufacturers texture the outer breast implant surfaces with calibrated salt grains. However, the analysis of these surfaces on sub-micron scales has been under-studied. This scale range is of interest to understand the future of silicone particles potentially released from the implant surface and the aetiology of newly reported complications, such as Anaplastic Large Cell Lymphoma. The surface measurements were accomplished by tomography and by two optical devices based on interferometry and on focus variation. The robustness of the measurements was investigated from the tissue scale to the cellular scale. The macroscopic pore-based structure of the textured implant surfaces is consistently measured by the three instruments. However, the multi-scale analyses start to be discrepant in a scale range between 50 µm and 500 µm characteristic of a finer secondary roughness regardless of the pore shape. The focus variation and the micro-tomography would fail to capture this roughness regime because of a focus-related optical artefact and of step-shaped artefact respectively.
Rough-surface model for surface temperature calculations on Vesta

NASA Astrophysics Data System (ADS)

Palmer, E.; Sykes, M.

2014-07-01

We model observations by the Dawn Visual and Infrared spectrometer (VIR) [1] to reproduce the observed surface temperature of Vesta. The VIR instrument has collected over 3,700 spectral cubes of Vesta out to 5.1 microns. The observed surface temperature is derived by matching the irradiance near 5 microns with a grey body, the Planck function after removing a reflected-light component per previous procedures [2--5] with similar results. We noted that the observed surface temperatures are significantly hotter than what simple theoretical models would predict [2]. To better understand this, we used a high-resolution topographic model of Vesta [6] that provided exact phase, incidence, and emission angles for every VIR pixel. We assume an emissivity of 0.9, Bond albedo of between 0.16 and 0.22 [5], and a variety of thermal inertia values for a low-contrast, highly degraded, homogenous crater. We have created a ''rough-surface'' thermal model that takes into account how irregular grains create sub-pixel variations in the thermal spectrum and describe the effect it has on the observed surface temperatures of Vesta. We have applied this method to the VIR observations of Vesta, which produced a high level of agreement with the observed surface temperatures.
Is fault surface roughness indicative of fault mechanisms? Observations from experimental Limestone faults

NASA Astrophysics Data System (ADS)

Sagy, A.; Tesei, T.; Collettini, C.

2016-12-01

Geometrical irregularity of contacting surfaces is a fundamental factor controlling friction and energy dissipation during sliding. We performed direct shear experiments on 20x20 cm limestone surfaces by applying constant normal load (40-200 kN) and sliding velocity 1-300 µm/s. Before shearing, the surfaces were polished with maximal measured amplitudes of less than 0.1 mm. After shear, elongated islands of shear zones are observed, characterized by grooves ploughed into the limestone surfaces and by layers of fine grain wear. These structures indicate that the contact areas during shear are scattered and occupy a limited portion of the entire surface area. The surfaces was scanned by a laser profilometer that measures topography using 640 parallel beams in a single run, offer up to 10 µm accuracy and working ranges of 200 mm. Two distinctive types of topographical end members are defined: rough wavy sections and smooth polished ones. The rough zones display ridges with typical amplitudes of 0.1-1 mm that cross the grooves perpendicular to the slip direction. These features are associated with penetrative brittle damage and with fragmentation. The smoother zones display reflective mirror-like surfaces bordered by topographical sharp steps at heights of 0.3-0.5 mm. These sections are localized inside the wear layer or between the wear layer and the host rock, and are not associated with observed penetrative damage. Preliminary statistical analysis suggests that the roughness of the ridges zones can be characterized using a power-low relationship between profile length and mean roughness, with relatively high values of Hurst exponents (e.g. H > 0.65) parallel to the slip direction. The polished zones, on the other hand, corresponded to lower values of Hurst exponents (e.g. H ≤ 0.6). Both structural and roughness measurements indicate that the distinctive topographic variations on the surfaces reflect competing mechanical processes which occur simultaneously during shear. The wavy ridged zone is the surface expression of penetrative cracking and fragmentation which widen the shear zone, while the smooth zones reflect localized flow and plastic deformation of the wear material. The similarity in topography of shear structures between experimental and natural faults suggests similar mechanical processes.
Exploration on Wire Discharge Machining Added Powder for Metal-Based Diamond Grinding Wheel on Wire EDM Dressing and Truing of Grinding Tungsten Carbide Material

NASA Astrophysics Data System (ADS)

Chow, H. M.; Yang, L. D.; Lin, Y. C.; Lin, C. L.

2017-12-01

In this paper, the effects of material removal rate and abrasive grain protrusion on the metal-based diamond grinding wheel were studied to find the optimal parameters for adding powder and wire discharge. In addition, this kind of electric discharge method to add powder on the metal-based diamond grinding wheel on line after dressing and truing will be applied on tungsten carbide to study the grinding material removal rate, grinding wheel wear, surface roughness, and surface micro-hardness.
DOE Office of Scientific and Technical Information (OSTI.GOV)

Lyazgin, Alexander, E-mail: lyazgin@list.ru; Shugurov, Artur, E-mail: shugurov@ispms.tsc.ru; Sergeev, Viktor, E-mail: retc@ispms.tsc.ru

The effect of bombardment of the Ni-B sublayer by Zr ion beams on the surface morphology and tribomechanical properties of Au-Ni coatings was investigated. It was found that the treatment has no significant effect on the surface roughness and grain size of the Au-Ni coatings, while it provides essential reducing of their friction coefficient and improvement of wear resistance. It is shown that increased wear resistance of these coatings was caused by their strain hardening resulted from localization of plastic strain. The optimal Zr fluence were determined that provide the maximum reduction of linear wear of the coatings.
A hybrid 3D SEM reconstruction method optimized for complex geologic material surfaces.

PubMed

Yan, Shang; Adegbule, Aderonke; Kibbey, Tohren C G

2017-08-01

Reconstruction methods are widely used to extract three-dimensional information from scanning electron microscope (SEM) images. This paper presents a new hybrid reconstruction method that combines stereoscopic reconstruction with shape-from-shading calculations to generate highly-detailed elevation maps from SEM image pairs. The method makes use of an imaged glass sphere to determine the quantitative relationship between observed intensity and angles between the beam and surface normal, and the detector and surface normal. Two specific equations are derived to make use of image intensity information in creating the final elevation map. The equations are used together, one making use of intensities in the two images, the other making use of intensities within a single image. The method is specifically designed for SEM images captured with a single secondary electron detector, and is optimized to capture maximum detail from complex natural surfaces. The method is illustrated with a complex structured abrasive material, and a rough natural sand grain. Results show that the method is capable of capturing details such as angular surface features, varying surface roughness, and surface striations. Copyright © 2017 Elsevier Ltd. All rights reserved.
Nanostructured magnesium has fewer detrimental effects on osteoblast function.

PubMed

Weng, Lucy; Webster, Thomas J

2013-01-01

Efforts have been made recently to implement nanoscale surface features on magnesium, a biodegradable metal, to increase bone formation. Compared with normal magnesium, nanostructured magnesium has unique characteristics, including increased grain boundary properties, surface to volume ratio, surface roughness, and surface energy, which may influence the initial adsorption of proteins known to promote the function of osteoblasts (bone-forming cells). Previous studies have shown that one way to increase nanosurface roughness on magnesium is to soak the metal in NaOH. However, it has not been determined if degradation of magnesium is altered by creating nanoscale features on its surface to influence osteoblast density. The aim of the present in vitro study was to determine the influence of degradation of nanostructured magnesium, created by soaking in NaOH, on osteoblast density. Our results showed a less detrimental effect of magnesium degradation on osteoblast density when magnesium was treated with NaOH to create nanoscale surface features. The detrimental degradation products of magnesium are of significant concern when considering use of magnesium as an orthopedic implant material, and this study identified a surface treatment, ie, soaking in NaOH to create nanoscale features for magnesium that can improve its use in numerous orthopedic applications.
Nanostructured magnesium has fewer detrimental effects on osteoblast function

PubMed Central

Weng, Lucy; Webster, Thomas J

2013-01-01

Efforts have been made recently to implement nanoscale surface features on magnesium, a biodegradable metal, to increase bone formation. Compared with normal magnesium, nanostructured magnesium has unique characteristics, including increased grain boundary properties, surface to volume ratio, surface roughness, and surface energy, which may influence the initial adsorption of proteins known to promote the function of osteoblasts (bone-forming cells). Previous studies have shown that one way to increase nanosurface roughness on magnesium is to soak the metal in NaOH. However, it has not been determined if degradation of magnesium is altered by creating nanoscale features on its surface to influence osteoblast density. The aim of the present in vitro study was to determine the influence of degradation of nanostructured magnesium, created by soaking in NaOH, on osteoblast density. Our results showed a less detrimental effect of magnesium degradation on osteoblast density when magnesium was treated with NaOH to create nanoscale surface features. The detrimental degradation products of magnesium are of significant concern when considering use of magnesium as an orthopedic implant material, and this study identified a surface treatment, ie, soaking in NaOH to create nanoscale features for magnesium that can improve its use in numerous orthopedic applications. PMID:23674891
Cosmological simulation with dust formation and destruction

NASA Astrophysics Data System (ADS)

Aoyama, Shohei; Hou, Kuan-Chou; Hirashita, Hiroyuki; Nagamine, Kentaro; Shimizu, Ikkoh

2018-06-01

To investigate the evolution of dust in a cosmological volume, we perform hydrodynamic simulations, in which the enrichment of metals and dust is treated self-consistently with star formation and stellar feedback. We consider dust evolution driven by dust production in stellar ejecta, dust destruction by sputtering, grain growth by accretion and coagulation, and grain disruption by shattering, and treat small and large grains separately to trace the grain size distribution. After confirming that our model nicely reproduces the observed relation between dust-to-gas ratio and metallicity for nearby galaxies, we concentrate on the dust abundance over the cosmological volume in this paper. The comoving dust mass density has a peak at redshift z ˜ 1-2, coincident with the observationally suggested dustiest epoch in the Universe. In the local Universe, roughly 10 per cent of the dust is contained in the intergalactic medium (IGM), where only 1/3-1/4 of the dust survives against dust destruction by sputtering. We also show that the dust mass function is roughly reproduced at ≲ 108 M⊙, while the massive end still has a discrepancy, which indicates the necessity of stronger feedback in massive galaxies. In addition, our model broadly reproduces the observed radial profile of dust surface density in the circum-galactic medium (CGM). While our model satisfies the observational constraints for the dust extinction on cosmological scales, it predicts that the dust in the CGM and IGM is dominated by large (>0.03 μm) grains, which is in tension with the steep reddening curves observed in the CGM.
Effect of Electropulsing-Assisted Ultrasonic Nanocrystalline Surface Modification on the Surface Mechanical Properties and Microstructure of Ti-6Al-4V Alloy

NASA Astrophysics Data System (ADS)

Ye, Yongda; Wang, Haibo; Tang, Guoyi; Song, Guolin

2018-05-01

The effect of electropulsing-assisted ultrasonic nanocrystalline surface modification (EP-UNSM) on surface mechanical properties and microstructure of Ti-6Al-4V alloy is investigated. Compared to conventional ultrasonic nanocrystalline surface modification (UNSM), EP-UNSM can effectively facilitate surface roughness and morphology, leading to excellent surface roughness (reduced from Ra 0.918 to Ra 0.028 μm by UNSM and Ra 0.019 μm by EP-UNSM) and smoother morphology with less cracks and defects. Surface friction coefficients are enhanced, resulting in lower and smoother friction coefficients. In addition, the surface-strengthened layer and ultra-refined grains are significantly enhanced with more severe plastic deformation and a greater surface hardness (a maximum hardness value of 407 HV and an effective depth of 550 μm, in comparison with the maximum hardness value of 364 HV and effective depth of 300 μm obtained by conventional UNSM). Remarkable enhancement of surface mechanical properties can be attributed to the refined gradient microstructure and the enhanced severe plastic deformation layer induced by coupling the effects of UNSM and electropulsing. The accelerated dislocation mobility and atom diffusion caused by the thermal and athermal effects of electropulsing treatment may be the primary intrinsic reasons for these improvements.
Characterization of N-doped polycrystalline diamond films deposited on microgrinding tools

NASA Astrophysics Data System (ADS)

Jackson, M. J.; Ahmed, W.

2005-10-01

Chemical vapor deposited diamond films have many industrial applications but are assuming increasing importance in the area of microengineering, most notably in the development of diamond coated microgrinding tools. For these applications the control of structure and morphology is of critical importance. The crystallite size, orientation, surface roughness, and the degree of sp 3 character have a profound effect on the tribological properties of the films deposited. In this article, we present experimental results on the effects of nitrogen doping on the surface morphology, crystallite size, and wear of microgrinding tools. The sp 3 character optimizes at 200 ppm nitrogen, and above this value the surface becomes much smoother and crystal sizes decrease considerably. Fracture-induced wear of the diamond grain is the most important mechanism of material removal from a microgrinding tool during the grinding process. Fracture occurs as a consequence of tensile stresses induced into diamond grains by grinding forces to which they are subjected. The relationship between the wear of diamond coated grinding tools, component grinding forces, and induced stresses in the model diamond grains is described in detail. A significant correlation was found between the maximum value of tensile stress induced in the diamond grain and the appropriate wheel-wear parameter (grinding ratio). It was concluded that the magnitude of tensile stresses induced in the diamond grain by grinding forces at the rake face is the best indicator of tool wear during the grinding process.
Mechanism of room temperature oxygen sensor based on nanocrystalline TiO2 film

NASA Astrophysics Data System (ADS)

Bakri, A. S.; Sahdan, M. Z.; Nafarizal, N.; Abdullah, S. A.; Said, N. D. M.; Raship, N. A.; Sari, Y.

2018-04-01

A titanium dioxide (TiO2) thin film is proposed as the active layer for the detection of oxygen gas. The sensor is fabricated on silicon wafer using sol-gel dip coating technique with a constant withdrawal speed. The field emission scanning electron microscope image reveals that the film has a uniform structure while the x-ray diffraction analysis indicates that the film is anatase phase with tetragonal lattice structure. The film exhibit the highest intensity peak at (101) plane. The surface roughness measurement shows that the film has low surface roughness with small grain size. The electrical studies revealed that the resistivity is about 4.02 x 10-3 Ω.cm and the thickness of TiO2 film is 127.44 nm. The gas sensor measurement showed that the sensor response of the film is about 4.21% at room temperature.
Characterization of erosion of metallic materials under cavitation attack in a mineral oil

NASA Technical Reports Server (NTRS)

Rao, B. C. S.; Buckley, D. H.

1984-01-01

Cavitation erosion and erosion rates of eight metallic materials representing three crystal structures were studied using a 20-kHz ultrasonic magnetostrictive oscillator in viscous mineral oil. The erosion rates of the metals with an fcc matrix were 10 to 100 times higher than that of an hcp-matrix titanium alloy. The erosion rates of iron and molybdenum, with bcc matrices, were higher than that of the titanium alloy but lower than those of the fcc metals. Scanning electron microscopy indicates that the cavitation pits are initially formed at the grain boundaries and precipitates and that the pits that formed at the triple points grew faster than the others. Transcrystalline craters formed by cavitation attack over the surface of grains and roughened the surfaces by multiple slip and twinning. Surface roughness measurements show that the pits that formed over the grain boundaries deepended faster than other pits. Computer analysis revealed that a geometric expression describes the nondimensional erosion curves during the time period 0.5 t(0) t 2.5 t(0), where t(0) is the incubation period. The fcc metals had very short incubation periods; the titanium alloy had the longest incubation period.
Geometrical and Structural Asperities on Fault Surfaces

NASA Astrophysics Data System (ADS)

Sagy, A.; Brodsky, E. E.; van der Elst, N.; Agosta, F.; di Toro, G.; Collettini, C.

2007-12-01

Earthquake dynamics are strongly affected by fault zone structure and geometry. Fault surface irregularities and the nearby structure control the rupture nucleation and propagation, the fault strength, the near-field stress orientations and the hydraulic properties. New field observations demonstrate the existence of asperities in faults as displayed by topographical bumps on the fault surface and hardening of the internal structure near them. Ground-based LIDAR measurements on more than 30 normal and strike slip faults in different lithologies demonstrate that faults are not planar surfaces and roughness is strongly dependent on fault displacement. In addition to the well-understood roughness exemplified by abrasive striations and fracture segmentation, we found semi-elliptical topographical bumps with wavelengths of a few meters. In many faults the bumps are not spread equally on the surface and zones can be bumpier than others. The bumps are most easily identified on faults with total displacement of dozens to hundreds of meters. Smaller scale roughness on these faults is smoothed by abrasive processes. A key site in southern Oregon shows that the topographic bumps are closely tied to the internal structure of the fault zone. At this location, we combine LiDAR data with detailed structural analysis of the fault zone embedded in volcanic rocks. Here the bumps correlate with an abrupt change in the width of the cohesive cataclasite layer that is exposed under a thin ultracataclasite zone. In most of the exposures the cohesive layer thickness is 10-20 cm. However, under protruding bumps the layer is always thickened and the width can locally exceed one meter. Field and microscopic analyses show that the layer contains grains with dimensions ranging from less than 10 μ up to a few centimeters. There is clear evidence of internal flow, rotation and fracturing of the grains in the layer. X-Ray diffraction measurements of samples from the layer show that the bulk mineralogy is identical to that of the host rock, although thin section analysis suggests that some alteration and secondary mineralization of the grains also occurs. We infer that the cohesiveness of the layer is a consequence of repacking and cementation similar to deformation bands in granular material. By comparing the thickness of the cohesive layer on several secondary faults in this fault area we found that the average thickness of the layer increases with total slip. The correlation is nonlinear and the thickening rate decreases with increasing slip. We conclude that granular flow decreasing with increasing slip and thus the deformation is continually localized.
Effect of Multi-Pass Ultrasonic Surface Rolling on the Mechanical and Fatigue Properties of HIP Ti-6Al-4V Alloy

PubMed Central

Li, Gang; Qu, Shengguan; Xie, Mingxin; Ren, Zhaojun; Li, Xiaoqiang

2017-01-01

The main purpose of this paper was to investigate the effect of a surface plastic deformation layer introduced by multi-pass ultrasonic surface rolling (MUSR) on the mechanical and fatigue properties of HIP Ti-6Al-4V alloys. Some microscopic analysis methods (SEM, TEM and XRD) were used to characterize the modified microstructure in the material surface layer. The results indicated that the material surface layer experienced a certain extent plastic deformation, accompanied by some dense dislocations and twin generation. Moreover, surface microhardness, residual stress and roughness values of samples treated by MUSR were also greatly improved compared with that of untreated samples. Surface microhardness and compressive residual stress were increased to 435 HV and −1173 MPa, respectively. The minimum surface roughness was reduced to 0.13 μm. The maximum depth of the surface hardening layer was about 55 μm. However, the practical influence depth was about 450 μm judging from the tensile and fatigue fracture surfaces. The ultimate tensile strength of the MUSR-treated sample increased to 990 MPa from the initial 963 MPa. The fatigue strength of the MUSR-treated sample was increased by about 25% on the base of 107 cycles, and the lifetime was prolonged from two times to two orders of magnitude at the applied stress amplitudes of 650–560 MPa. The improved mechanical and fatigue properties of MUSR-treated samples should be attributed to the combined effects of the increased microhardness and compressive residual stress, low surface roughness, grain refinement and micro-pore healing in the material surface-modified layer. PMID:28772494
Re-analysis of previous laboratory phase curves: 1. Variations of the opposition effect morphology with the textural properties, and an application to planetary surfaces

NASA Astrophysics Data System (ADS)

Déau, Estelle; Flandes, Alberto; Spilker, Linda J.; Petazzoni, Jérôme

2013-11-01

Typical variations in the opposition effect morphology of laboratory samples at optical wavelengths are investigated to probe the role of the textural properties of the surface (roughness, porosity and grain size). A previously published dataset of 34 laboratory phase curves is re-analyzed and fit with several morphological models. The retrieved morphological parameters that characterize the opposition surge, amplitude, width and slope (A, HWHM and S respectively) are correlated to the single scattering albedo, the roughness, the porosity and the grain size of the samples. To test the universality of the laboratory samples’ trends, we use previously published phase curves of planetary surfaces, including the Moon, satellites and rings of the giant planets. The morphological parameters of the surge (A and HWHM) for planetary surfaces are found to have a non-monotonic variation with the single scattering albedo, similar to that observed in asteroids (Belskaya, I.N., Shevchenko, V.G. [2000]. Icarus 147, 94-105), which is unexplained so far. The morphological parameters of the surge (A and HWHM) for laboratory samples seem to exhibit the same non-monotonic variation with single scattering albedo. While the non-monotonic variation with albedo was already observed by Nelson et al. (Nelson, R.M., Hapke, B.W., Smythe, W.D., Hale, A.S., Piatek, J.L. [2004]. Planetary regolith microstructure: An unexpected opposition effect result. In: Mackwell, S., Stansbery, E. (Eds.), Proc. Lunar Sci. Conf. 35, p. 1089), we report here the same variation for the angular width.

Development and characterization of food-grade tracers for the global grain tracing and recall system.

PubMed

Lee, Kyung-Min; Armstrong, Paul R; Thomasson, J Alex; Sui, Ruixiu; Casada, Mark; Herrman, Timothy J

2010-10-27

Tracing grain from the farm to its final processing destination as it moves through multiple grain-handling systems, storage bins, and bulk carriers presents numerous challenges to existing record-keeping systems. This study examines the suitability of coded caplets to trace grain, in particular, to evaluate methodology to test tracers' ability to withstand the rigors of a commercial grain handling and storage systems as defined by physical properties using measurement technology commonly applied to assess grain hardness and end-use properties. Three types of tracers to dispense into bulk grains for tracing the grain back to its field of origin were developed using three food-grade substances [processed sugar, pregelatinized starch, and silicified microcrystalline cellulose (SMCC)] as a major component in formulations. Due to a different functionality of formulations, the manufacturing process conditions varied for each tracer type, resulting in unique variations in surface roughness, weight, dimensions, and physical and spectroscopic properties before and after coating. The applied two types of coating [pregelatinized starch and hydroxypropylmethylcellulose (HPMC)] using an aqueous coating system containing appropriate plasticizers showed uniform coverage and clear coating. Coating appeared to act as a barrier against moisture penetration, to protect against mechanical damage of the surface of the tracers, and to improve the mechanical strength of tracers. The results of analysis of variance (ANOVA) tests showed the type of tracer, coating material, conditioning time, and a theoretical weight gain significantly influenced the morphological and physical properties of tracers. Optimization of these factors needs to be pursued to produce desirable tracers with consistent quality and performance when they flow with bulk grains throughout the grain marketing channels.
Oxygen plasma ashing effects on aluminum and titanium space protective coatings

NASA Technical Reports Server (NTRS)

Synowicki, R.; Kubik, R. D.; Hale, J. S.; Peterkin, Jane; Nafis, S.; Woollam, John A.; Zaat, S.

1991-01-01

Using variable angle spectroscopic ellipsometry and atomic force microscopy (AFM), the surface roughness and oxidation of aluminum and titanium thin films have been studied as a function of substrate deposition temperature and oxygen plasma exposure. Increasing substrate deposition temperatures affect film microstructure by greatly increasing grain size. Short exposures to an oxygen plasma environment produce sharp spikes rising rapidly above the surface as seen by AFM. Ellipsometric measurements were made over a wide range of plasma exposure times, and results at longer exposure times suggest that the surface is greater than 30% void. This is qualitatively verified by the AFM images.
Ductile mode grinding of reaction-bonded silicon carbide mirrors.

PubMed

Dong, Zhichao; Cheng, Haobo

2017-09-10

The demand for reaction-bonded silicon carbide (RB-SiC) mirrors has escalated recently with the rapid development of space optical remote sensors used in astronomy or Earth observation. However, RB-SiC is difficult to machine due to its high hardness. This study intends to perform ductile mode grinding to RB-SiC, which produces superior surface integrity and fewer subsurface damages, thus minimizing the workload of subsequent lapping and polishing. For this purpose, a modified theoretical model for grain depth of cut of grinding wheels is presented, which correlates various processing parameters and the material characteristics (i.e., elastic module) of a wheel's bonding matrix and workpiece. Ductile mode grinding can be achieved as the grain depth of cut of wheels decreases to be less than the critical cut depth of workpieces. The theoretical model gives a roadmap to optimize the grinding parameters for ductile mode grinding of RB-SiC and other ultra-hard brittle materials. Its feasibility was validated by experiments. With the optimized grinding parameters for RB-SiC, the ductile mode grinding produced highly specular surfaces (with roughness of ∼2.2-2.8 nm Ra), which means the material removal mechanism of RB-SiC is dominated by plastic deformation rather than brittle fracture. Contrast experiments were also conducted on fused silica, using the same grinding parameters; this produced only very rough surfaces, which further validated the feasibility of the proposed model.
Topography evolution of rough-surface metallic substrates by solution deposition planarization method

NASA Astrophysics Data System (ADS)

Chu, Jingyuan; Zhao, Yue; Liu, Linfei; Wu, Wei; Zhang, Zhiwei; Hong, Zhiyong; Li, Yijie; Jin, Zhijian

2018-01-01

As an emerging technique for surface smoothing, solution deposition planarization (SDP) has recently drawn more attention on the fabrication of the second generation high temperature superconducting (2G-HTS) tapes. In our work, a number of amorphous oxide layers were deposited on electro-polished or mirror-rolled metallic substrates by chemical solution route. Topography evolution of surface defects on these two types of metallic substrates was thoroughly investigated by atomic force microscopy (AFM). It was showed that root mean square roughness values (at 50 × 50 μm2 scanning scale) on both rough substrates reduced to ∼5 nm after coating with SDP-layer. The smoothing effect was mainly attributed to decrease of the depth at grain boundary grooving on the electro-polished metallic substrate. On the mirror-rolled metallic substrates, the amplitude and frequency of the height fluctuation perpendicular to the rolling direction were gradually reduced as depositing more numbers of SDP-layer. A high Jc value of 4.17 MA cm-2 (at 77 K, s.f.) was achieved on a full stack of YBCO/CeO2/IBAD-MgO/SDP-layer/C276 sample. This study enhanced understanding of the topography evolution on the surface defects covered by the SDP-layer, and demonstrated a low-cost route for fabricating IBAD-MgO based YBCO templates with a simplified architecture.
Ice sintering timescales at the surface of Europa and implications for surface properties

NASA Astrophysics Data System (ADS)

Phillips, C. B.; Molaro, J.; Meirion-Griffith, G.

2017-12-01

The planned exploration of Europa by NASA's Europa Clipper Mission and the possibility of a future Europa lander have driven the need to characterize its surface strength, roughness, porosity, thermal conductivity, and regolith depth in order to accurately interpret remote sensing data and develop appropriate spacecraft landing systems. Many processes contribute to Europa's landscape evolution, such as sputtering, mass wasting, thermal segregation, and impact gardening, driving the creation and distribution of icy regolith across the surface. While the efficacy of these processes are not well constrained, any amount of regolith emplaced at the surface will undergo subsequent processing due to sintering. Ice sintering is a form of frost metamorphism whereby contacting ice grains experience the diffusion of material into their contact region, forming a "neck" between them and densifying over time. Over long enough timescales, ice aggregates will sinter into solid material, which may contribute to the incorporation of non-ice material into Europa's subsurface and help to drive subsurface chemistry. Sintering also interacts with other processes, adding to the complexity of icy surface evolution. For example, sputtering preferentially removes larger grains and may enhance sintering rates, and changes in ice porosity may affect the response of the surface to micrometeorite impacts. Quantifying the effects of ice sintering will allow us to predict the microstructural properties of Europa's surface at spacecraft scales. To this end, we have modeled pressure-less (no overburden) sintering of spherical water-ice grains and validated the results with a laboratory experiment. We also modeled ice at the surface of Europa to obtain a first-order approximation of the sintering timescale and surface properties. Preliminary results indicate that ice grains will experience neck growth but not significant densification over Europa's surface age, suggesting that loose surface ice forms a weak and porous crust. Furthermore, our results suggest that existing models do not accurately quantify all stages of the sintering process for ice, emphasizing the need for more laboratory studies on this topic.
Encapsulated Annealing: Enhancing the Plasmon Quality Factor in Lithographically–Defined Nanostructures

PubMed Central

Bosman, Michel; Zhang, Lei; Duan, Huigao; Tan, Shu Fen; Nijhuis, Christian A.; Qiu, Cheng–Wei; Yang, Joel K. W.

2014-01-01

Lithography provides the precision to pattern large arrays of metallic nanostructures with varying geometries, enabling systematic studies and discoveries of new phenomena in plasmonics. However, surface plasmon resonances experience more damping in lithographically–defined structures than in chemically–synthesized nanoparticles of comparable geometries. Grain boundaries, surface roughness, substrate effects, and adhesion layers have been reported as causes of plasmon damping, but it is difficult to isolate these effects. Using monochromated electron energy–loss spectroscopy (EELS) and numerical analysis, we demonstrate an experimental technique that allows the study of these effects individually, to significantly reduce the plasmon damping in lithographically–defined structures. We introduce a method of encapsulated annealing that preserves the shape of polycrystalline gold nanostructures, while their grain-boundary density is reduced. We demonstrate enhanced Q–factors in lithographically–defined nanostructures, with intrinsic damping that matches the theoretical Drude damping limit. PMID:24986023
Directional bottom roughness associated with waves, currents, and ripples

USGS Publications Warehouse

Sherwood, Christopher R.; Rosati, Julie D.; Wang, Ping; Roberts, Tiffany M.

2011-01-01

Roughness lengths are used in wave-current bottom boundary layer models to parameterize drag associated with grain roughness, the effect of saltating grains during sediment transport, and small-scale bottom topography (ripples and biogenic features). We made field measurements of flow parameters and recorded sonar images of ripples at the boundary of a sorted-bedform at ~12-m depth on the inner shelf for a range of wave and current conditions over two months. We compared estimates of apparent bottom roughness inferred from the flow measurements with bottom roughness calculated using ripple geometry and the Madsen (1994) one-dimensional (vertical) wave-current bottom boundary layer model. One result of these comparisons was that the model over predicted roughness of flow from the dormant large ripples when waves were small. We developed a correction to the ripple-roughness model that incorporates an apparent ripple wavelength related to the combined wave-current flow direction. This correction provides a slight improvement for low-wave conditions, but does not address several other differences between observations and the modeled roughness.
Artificial Niches for Stromal Stem Cells as a Potential Instrument for the Design of the Surface of Biomimetic Osteogenic Materials

NASA Astrophysics Data System (ADS)

Khlusov, I. A.; Khlusova, M. Yu.; Pichugin, V. F.; Sharkeev, Yu. P.; Legostaeva, E. V.

2014-02-01

A relationship between the topography of rough calcium phosphate surfaces having osteogenic niche-reliefs and the electrostatic potential of these surfaces as a possible instrument to control stromal stem cells has been investigated. The in vitro culture of human lung prenatal stromal cells on nanostructured/ultrafine-grained VT1.0 titanium alloy plates with bilateral rough calcium phosphate (CaP) microarc coating was used. It was established that the amplitude of the electret CaP surface potential linearly increased with increasing area of valleys (sockets), and the negative charge is formed on the socket surface. The area of alkaline phosphatase staining (the marker of osteoblast maturation and differentiation) of adherent CD34- CD44+ cells increases linearly with increasing area of artificial microterritory (socket) of the CaP surface occupied with each cell. The negative electret potential in valleys (sockets) of microarc CaP coatings can be the physical mechanism mediating the influence of the surface topography on osteogenic maturation and differentiation of cells in vitro. This mechanism can be called "niche-potential" and can be used as an instrument for biomimetic modification of smooth CaP surfaces to strengthen their integration with the bone tissue.
Determination of maize hardness by biospeckle and fuzzy granularity.

PubMed

Weber, Christian; Dai Pra, Ana L; Passoni, Lucía I; Rabal, Héctor J; Trivi, Marcelo; Poggio Aguerre, Guillermo J

2014-09-01

In recent years there has been renewed interest in the development of novel grain classification methods that could complement traditional empirical tests. A speckle pattern occurs when a laser beam illuminates an optically rough surface that flickers when the object is active and is called biospeckle. In this work, we use laser biospeckle to classify maize (Zea mays L.) kernel hardness. A series of grains of three types of maize were cut and illuminated by a laser. A series of images were then registered, stored, and processed. These were compared with results obtained by floating test. The laser speckle technique was effective in discriminating the grains based on the presence of floury or vitreous endosperm and could be considered a feasible alternative to traditional floating methods. The results indicate that this methodology can distinguish floury and vitreous grains. Moreover, the assay showed higher discrimination capability than traditional tests. It could be potentially useful for maize classification and to increase the efficiency of processing dry milling corn.
Lasing of surface-polished polycrystalline Ho: YAG (yttrium aluminum garnet) fiber.

PubMed

Kim, Hyunjun; Hay, Randall S; McDaniel, Sean A; Cook, Gary; Usechak, Nicholas G; Urbas, Augustine M; Shugart, Kathleen N; Lee, HeeDong; Kadhim, Ali H; Brown, Dean P; Griffin, Benjamin; Fair, Geoff E; Corns, Randall G; Potticary, Santeri A; Hopkins, Frank K; Averett, Kent L; Zelmon, David E; Parthasarathy, Triplicane A; Keller, Kristin A

2017-03-20

A polycrystalline 1.5% Ho: YAG fiber with a diameter of 31 µm was prepared. Surface roughness from grain boundary grooving was reduced by polishing, which decreased the fiber scattering coefficient from 76 m^-1 to 35 m^-1. Lasing tests were done on this fiber with a SF57 Schott glass cladding. Lasing was confirmed by spectrum narrowing with threshold pump power lower than 500 mW and a slope efficiency of 7%. To our knowledge, this is the first lasing demonstration from a small diameter polycrystalline ceramic fiber.
Results of the Imager for Mars Pathfinder windsock experiment

USGS Publications Warehouse

Sullivan, R.; Greeley, R.; Kraft, M.; Wilson, G.; Golombek, M.; Herkenhoff, K.; Murphy, J.; Smith, P.

2000-01-01

The Imager for Mars Pathfinder (IMP) windsock experiment measured wind speeds at three heights within 1.2 m of the Martian surface during Pathfinder landed operations. These wind data allowed direct measurement of near-surface wind profiles on Mars for the first time, including determination of aerodynamic roughness length and wind friction speeds. Winds were light during periods of windsock imaging, but data from the strongest breezes indicate aerodynamic roughness length of 3 cm at the landing site, with wind friction speeds reaching 1 m/s. Maximum wind friction speeds were about half of the threshold-of-motion friction speeds predicted for loose, fine-grained materials on smooth Martian terrain and about one third of the threshold-of-motion friction speeds predicted for the same size particles over terrain with aerodynamic roughness of 3 cm. Consistent with this, and suggesting that low wind speeds prevailed when the windsock array was not imaged and/or no particles were available for aeolian transport, no wind-related changes to the surface during mission operations have been recognized. The aerodynamic roughness length reported here implies that proposed deflation of fine particles around the landing site, or activation of duneforms seen by IMP and Sojourner, would require wind speeds >28 m/s at the Pathfinder top windsock height (or >31 m/s at the equivalent Viking wind sensor height of 1.6 m) and wind speeds >45 m/s above 10 m. These wind speeds would cause rock abrasion if a supply of durable particles were available for saltation. Previous analyses indicate that the Pathfinder landing site probably is rockier and rougher than many other plains units on Mars, so aerodynamic roughness length elsewhere probably is less than the 3-cm value reported for the Pathfinder site. Copyright 2000 by the American Geophysical Union.
Smoothing and roughening of slip surfaces in direct shear experiments

NASA Astrophysics Data System (ADS)

Sagy, Amir; Badt, Nir; Hatzor, Yossef H.

2015-04-01

Faults in the upper crust contain discrete slip surfaces which have absorbed a significant part of the shear displacement along them. Field measurements demonstrate that these surfaces are rough at all measurable scales and indicate that surfaces of relatively large-slip faults are statistically smoother than those of small-slip faults. However, post faulting and surface erosion process that might affect the geometry of outcrops cannot be discounted in such measurements. Here we present experimental results for the evolution of shear surface topography as function of slip distance and normal stress in direct shear experiments. A single prismatic fine grain limestone block is first fractured in tension mode using the four-point bending test methodology and then the fracture surface topography is scanned using a laser profilometer. We then shear the obtained tensile fracture surfaces in direct shear, ensuring the original fracture surfaces are in a perfectly matching configuration at the beginning of the shear test. First, shearing is conducted to distances varying from 5 to 15 mm under constant normal stress of 2MPa and a constant displacement rate of 0.05 mm/s using two closed-loop servo controlled hydraulic pistons, supplying normal and shear forces (Davidesko et al., 2014). In the tested configuration peak shear stress is typically attained after a shear displacement of about 2-3 mm, beyond which lower shear stress is required to continue shearing at the preset displacement rate of 0.05 mm/s as is typical for initially rough joints. Following some initial compression the interface begins to dilate and continues to do so until the end of the test. The sheared tensile fracture surface is then scanned again and the geometrical evolution, in term of RMS roughness and power spectral density (PSD) is analyzed. We show that shearing smooth the surface along all our measurements scales. The roughness ratio, measured by initial PSD / final PSD for each wavelength, increases as a function of slip amount. The roughness measured after slip can be fitted by a power-law similar to that of the initial tensile surface. In the next series of experiments a similar procedure is applied when the roughness evolution is measured as a function of increasing normal stress for a fixed displacement amount of 10 mm. While samples sheared under a constant normal stress of 5 MPa generated surface smoothing, shearing under normal stress of 7.5 MPa to 15 MPa exhibited surface roughening at the measured range of scales. We find that roughening is correlated with the attained peak shear stress values, stress drop (peak shear stress minus residual shear stress) and with wear accumulation, a novel measurement procedure of which is developed here. Analysis of the sheared samples shows that roughening is generated by sets of dense fractures that significantly damaged the sample in the immediate proximity to large asperities. This roughening is related to penetrative damage during transient wear in rough surfaces.
Comparative Laboratory and Numerical Simulations of Shearing Granular Fault Gouge: Micromechanical Processes

NASA Astrophysics Data System (ADS)

Morgan, J. K.; Marone, C. J.; Guo, Y.; Anthony, J. L.; Knuth, M. W.

2004-12-01

Laboratory studies of granular shear zones have provided significant insight into fault zone processes and the mechanics of earthquakes. The micromechanisms of granular deformation are more difficult to ascertain, but have been hypothesized based on known variations in boundary conditions, particle properties and geometries, and mechanical behavior. Numerical simulations using particle dynamics methods (PDM) can offer unique views into deforming granular shear zones, revealing the precise details of granular microstructures, particle interactions, and packings, which can be correlated with macroscopic mechanical behavior. Here, we describe a collaborative program of comparative laboratory and numerical experiments of granular shear using idealized materials, i.e., glass beads, glass rods or pasta, and angular sand. Both sets of experiments are carried out under similar initial and boundary conditions in a non-fracturing stress regime. Phenomenologically, the results of the two sets of experiments are very similar. Peak friction values vary as a function of particle dimensionality (1-D vs. 2-D vs. 3-D), particle angularity, particle size and size distributions, boundary roughness, and shear zone thickness. Fluctuations in shear strength during an experiment, i.e., stick-slip events, can be correlated with distinct changes in the nature, geometries, and durability of grain bridges that support the shear zone walls. Inclined grain bridges are observed to form, and to support increasing loads, during gradual increases in assemblage strength. Collapse of an individual grain bridge leads to distinct localization of strain, generating a rapidly propagating shear surface that cuts across multiple grain bridges, accounting for the sudden drop in strength. The distribution of particle sizes within an assemblage, along with boundary roughness and its periodicity, influence the rate of formation and dissipation of grain bridges, thereby controlling friction variations during shear.
Flow Resistance Interactions on Hillslopes With Heterogeneous Attributes: Effects on Runoff Hydrograph Characteristics

NASA Astrophysics Data System (ADS)

Papanicolaou, Athanasios N.; Abban, Benjamin K. B.; Dermisis, Dimitrios C.; Giannopoulos, Christos P.; Flanagan, Dennis C.; Frankenberger, James R.; Wacha, Kenneth M.

2018-01-01

An improved modeling framework for capturing the effects of space and time-variant resistance to overland flow is developed for intensively managed landscapes. The framework builds on the WEPP model but it removes the limitations of the "equivalent" plane and time-invariant roughness assumption. The enhanced model therefore accounts for spatiotemporal changes in flow resistance along a hillslope due to changes in roughness, in profile curvature, and downslope variability. The model is used to quantify the degree of influence—from individual soil grains to aggregates, "isolated roughness elements," and vegetation—on overland flow characteristics under different storm magnitudes, downslope gradients, and profile curvatures. It was found that the net effects of land use change from vegetation to a bare surface resulted in hydrograph peaks that were up to 133% larger. Changes in hillslope profile curvature instead resulted in peak runoff rate changes that were only up to 16%. The stream power concept is utilized to develop a taxonomy that relates the influence of grains, isolated roughness elements, and vegetation, on overland flow under different storm magnitudes and hillslope gradients. Critical storm magnitudes and hillslope gradients were found beyond which the effects of these landscape attributes on the peak stream power were negligible. The results also highlight weaknesses of the space/time-invariant flow resistance assumption and demonstrate that assumptions on landscape terrain characteristics exert a strong control both on the shape and magnitude of hydrographs, with deviations reaching 65% in the peak runoff when space/time-variant resistance effects are ignored in some cases.
Characterization of surface roughness effects on pressure drop in single-phase flow in minichannels

NASA Astrophysics Data System (ADS)

Kandlikar, Satish G.; Schmitt, Derek; Carrano, Andres L.; Taylor, James B.

2005-10-01

Roughness features on the walls of a channel wall affect the pressure drop of a fluid flowing through that channel. This roughness effect can be described by (i) flow area constriction and (ii) increase in the wall shear stress. Replotting the Moody's friction factor chart with the constricted flow diameter results in a simplified plot and yields a single asymptotic value of friction factor for relative roughness values of ɛ /D>0.03 in the fully developed turbulent region. After reviewing the literature, three new roughness parameters are proposed (maximum profile peak height Rp, mean spacing of profile irregularities RSm, and floor distance to mean line Fp). Three additional parameters are presented to consider the localized hydraulic diameter variation (maximum, minimum, and average) in future work. The roughness ɛ is then defined as Rp+Fp. This definition yields the same value of roughness as obtained from the sand-grain roughness [H. Darcy, Recherches Experimentales Relatives au Mouvement de L'Eau dans les Tuyaux (Mallet-Bachelier, Paris, France, 1857); J. T. Fanning, A Practical Treatise on Hydraulic and Water Supply Engineering (Van Nostrand, New York, 1877, revised ed. 1886); J. Nikuradse, "Laws of flow in rough pipes" ["Stromungsgesetze in Rauen Rohren," VDI-Forschungsheft 361 (1933)]; Beilage zu "Forschung auf dem Gebiete des Ingenieurwesens," Ausgabe B Band 4, English translation NACA Tech. Mem. 1292 (1937)]. Specific experiments are conducted using parallel sawtooth ridge elements, placed normal to the flow direction, in aligned and offset configurations in a 10.03mm wide rectangular channel with variable gap (resulting hydraulic diameters of 325μm-1819μm with Reynolds numbers ranging from 200 to 7200 for air and 200 to 5700 for water). The use of constricted flow diameter extends the applicability of the laminar friction factor equations to relative roughness values (sawtooth height) up to 14%. In the turbulent region, the aligned and offset roughness arrangements yield different results indicating a need to further characterize the surface features. The laminar to turbulent transition is also seen to occur at lower Reynolds numbers with an increase in the relative roughness.
Effect of surface nanostructuring on corrosion behavior of Ti–6Al–4V alloy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kumar, Sanjeev, E-mail: sanjeevphy85@gmail.com; Ch

Surface nanostructure was induced in Ti–6Al–4V alloy by ultrasonic shot peening (USSP) for different durations, from 15 s to 30 min, and the modified surface was characterized by optical, scanning, atomic force and transmission electron microscopy. Nano size grains were observed to form on surface of the USSPed samples and surface roughness was increased with duration of USSP. Polarization study was carried out in Ringer's solution to examine the effect of surface nanostructuring on corrosion resistance of this alloy. Electrochemical corrosion was carried out for all the USSPed specimens as well as the non-USSPed sample in Ringer's solution. Surface morphologymore » of the corroded samples was examined by SEM. In general, corrosion resistance was improved by USSP up to the duration of 15 min and there was maximum improvement in the specimen USSPed for 1 min. However, corrosion resistance was drastically reduced due to USSP for long duration of 30 min. - Highlights: •Nanostructure was induced by USSP on alloy Ti–6Al–4V of about 28 nm. •Grain refinement was confirmed by XRD and TEM. •USSP is an effective technique for the improvement in corrosion resistance. •Nanostructured surface promotes formation of protective surface layer of TiO{sub 2}.« less
Acceptor-modulated optical enhancements and band-gap narrowing in ZnO thin films

NASA Astrophysics Data System (ADS)

Hassan, Ali; Jin, Yuhua; Irfan, Muhammad; Jiang, Yijian

2018-03-01

Fermi-Dirac distribution for doped semiconductors and Burstein-Moss effect have been correlated first time to figure out the conductivity type of ZnO. Hall Effect in the Van der Pauw configuration has been applied to reconcile our theoretical estimations which evince our assumption. Band-gap narrowing has been found in all p-type samples, whereas blue Burstein-Moss shift has been recorded in the n-type films. Atomic Force Microscopic (AFM) analysis shows that both p-type and n-type films have almost same granular-like structure with minor change in average grain size (˜ 6 nm to 10 nm) and surface roughness rms value 3 nm for thickness ˜315 nm which points that grain size and surface roughness did not play any significant role in order to modulate the conductivity type of ZnO. X-ray diffraction (XRD), Energy Dispersive X-ray Spectroscopy (EDS) and X-ray Photoelectron Spectroscopy (XPS) have been employed to perform the structural, chemical and elemental analysis. Hexagonal wurtzite structure has been observed in all samples. The introduction of nitrogen reduces the crystallinity of host lattice. 97% transmittance in the visible range with 1.4 × 107 Ω-1cm-1 optical conductivity have been detected. High absorption value in the ultra-violet (UV) region reveals that NZOs thin films can be used to fabricate next-generation high-performance UV detectors.
The Influence of Interfacial Roughness on Fiber Sliding in Oxide Composites with La-Monazite Interphases

NASA Technical Reports Server (NTRS)

Davis, J. B.; Hay, R. S.; Marshall, D. B.; Morgan, P. E. D.; Sayir, A.; Gray, Hugh R. (Technical Monitor); Farmer, Serene C. (Technical Monitor)

2002-01-01

Room temperature debonding and sliding of La-Monazite coated fibers is assessed using a composite with a polycrystalline alumina matrix and fibers of several different single crystal (mullite, sapphire) and directionally solidified eutectic (Al2O3/Y3Al5O12 and Al2O3/Y-ZrO2) compositions. These fibers provide a range of residual stresses and interfacial roughnesses. Sliding occurred over a debond crack at the fiber-coating interface when the sliding displacement and surface roughness were relatively small. At large sliding displacements with relatively rough interfaces, the monazite coatings were deformed extensively by fracture, dislocations and occasional twinning, whereas the fibers were undamaged. Dense, fine-grained (10 nm) microstructures suggestive of dynamic recrystallization were also observed in the coatings. Frictional heating during sliding is assessed. The possibility of low temperature recrystallization is discussed in the light of the known resistance of monazite to radiation damage. The ability of La-Monazite to undergo plastic deformation relatively easily at low temperatures may be enabling for its use as a composite interface.
Impact of dissolution and carbonate precipitation on carbon storage in basalt

NASA Astrophysics Data System (ADS)

Wells, R. K.; Xiong, W.; Tadeoye, J.; Menefee, A.; Ellis, B. R.; Skemer, P. A.; Giammar, D.

2016-12-01

The spatial evolution of silicate mineral dissolution, carbonate precipitation, and the transport of fluids influence the viability of carbon storage in basalt reservoirs. Dissolution of natural basalt and subsequent carbonate precipitation in systems with different transport processes operating were characterized using static and flow-through (5 mL/hr) experiments at 50, 100, and 150 °C, and 100 bar CO2. Intact samples and cores with milled pathways that simulate fractures were tested. Spatial and mineralogical patterns in dissolution and precipitation were analyzed using optical and electron microscopy, microCT scanning, and surface roughness data. Precipitates and fluid chemistry were analyzed using Raman spectroscopy, SEM-EDS, and ICP-MS. Analysis of the bulk solution and surface topography suggests dissolution of olivine and pyroxene grains begins within hours of the start of the experiments. In flow-through experiments, total effluent cation concentrations reach a peak concentration within a few hours then drop towards a steady state within a few days. In static experiments, the initial rate of cation release is faster than it is after several weeks. In both cases Ca2+, Mg2+, and Fe2+ are the dominant cations in solution in the initial stages of reaction. Lower concentrations of Na2+, K+, and Al3+, and the preservation of feldspar and matrix grains after several weeks of reaction indicate the slow reactivity of these minerals. As the reaction progresses, the surface roughness increases steadily with cavities developing at the sites of olivine and pyroxene grains. Post-reaction analysis of basalt samples reacted at static conditions with milled pathways reveals that both siderite and amorphous silica precipitated within diffusion-limited zones as early as 4-6 weeks. Siderite abundance varies with distance along the pathway with the highest concentration of carbonates 1-2 cm below the fracture opening. Siderite precipitates are large enough to fill fracture opening 100 μm wide within 4-6 weeks.
The development of manganese oxide coated ceramic membranes for combined catalytic ozonation and ultrafiltration of drinking water

NASA Astrophysics Data System (ADS)

Corneal, Lindsay Marie

A novel method for the preparation of hydrated MnO2 by the ozonation of MnCl2 in water is described. The hydrated MnO 2 was used to coat titania water filtration membranes using a layer-by-layer technique. The coated membranes were then sintered in air at 500°C for 45 minutes. Upon sintering, the MnO2 is converted to alpha-Mn 2O3 (as characterized by x-ray and electron diffraction). Atomic force microscopy (AFM) imaging showed no significant change in the roughness or height of the surface features of coated membranes, while scanning electron microscopy (SEM) imaging showed an increase in grain size with increasing number of coating layers. Energy dispersive x-ray spectroscopy (EDS) mapping and line scans revealed manganese present throughout the membrane, indicating that manganese dispersed into the porous membrane during the coating process and diffused into the titania grains during sintering. Selected area diffraction (SAD) of the coated and sintered membrane was used to index the surface layer as alpha-Mn2O3. The surface layer was uneven, although there was a trend of increasing thickness with increasing coating layers. The coating acts as a catalyst for the oxidation of organic matter when coated membranes are used in a hybrid ozonation-membrane filtration system. A trend of decreasing total organic carbon (TOC) in the permeate water was observed with increasing number of coating layers. The catalytic activity also manifests itself as improved recovery of the water flux due to oxidation of foulants on the membrane surface. Ceramic nanoparticle coatings on ceramic water filtration membranes must undergo high temperature sintering. However, this means that the underlying membrane, which has been engineered for a given molecular weight cut-off (MWCO), also undergoes a high temperature heat treatment that serves to increase pore size that have resulted in increases in permeability of titania membranes. Coating the titania membrane with manganese oxide followed by sintering in air at 500°C maintains the MWCO of the membranes, with high DI water permeability, which may be favorable in terms of membrane use. SEM micrographs of titania membrane samples sintered between 500°C to 900°C were analyzed to identify a statistically significant increase in grain size with increasing sintering temperature. The grains however, generally retain a uniform shape until the 900°C sintering temperature, where large, irregularly shaped grains were observed. AFM analysis showed a corresponding increase in the surface roughness of the membrane for the sample sintered at 900°C.

The Effect of Surfactant Content over Cu-Ni Coatings Electroplated by the sc-CO₂ Technique.

PubMed

Chuang, Ho-Chiao; Sánchez, Jorge; Cheng, Hsiang-Yun

2017-04-19

Co-plating of Cu-Ni coatings by supercritical CO₂ (sc-CO₂) and conventional electroplating processes was studied in this work. 1,4-butynediol was chosen as the surfactant and the effects of adjusting the surfactant content were described. Although the sc-CO₂ process displayed lower current efficiency, it effectively removed excess hydrogen that causes defects on the coating surface, refined grain size, reduced surface roughness, and increased electrochemical resistance. Surface roughness of coatings fabricated by the sc-CO₂ process was reduced by an average of 10%, and a maximum of 55%, compared to conventional process at different fabrication parameters. Cu-Ni coatings produced by the sc-CO₂ process displayed increased corrosion potential of ~0.05 V over Cu-Ni coatings produced by the conventional process, and 0.175 V over pure Cu coatings produced by the conventional process. For coatings ~10 µm thick, internal stress developed from the sc-CO₂ process were ~20 MPa lower than conventional process. Finally, the preferred crystal orientation of the fabricated coatings remained in the (111) direction regardless of the process used or surfactant content.
Swift heavy ion induced topography changes of Tin oxide thin films

NASA Astrophysics Data System (ADS)

Jaiswal, Manoj K.; Kumar, Avesh; Kanjilal, D.; Mohanty, T.

2012-12-01

Monodisperse tin oxide nanocrystalline thin films are grown on silicon substrates by electron beam evaporation method followed by 100 MeV silver ion bombardment with varying ion fluence from 5 × 1011 ions cm-2 to 1 × 1013 ions cm-2 at constant ion flux. Enhancement of crystallinity of thin films with fluence is observed from glancing angle X-ray diffraction studies. Morphological studies by atomic force microscopy reveal the changes in grain size from 25 nm to 44 nm with variation in ion fluence. The effect of initial surface roughness and adatom mobility on topography is reported. In this work correlation between ion beam induced defect concentration with topography and grain size distribution is emphasized.
Smooth- and rough-wall boundary layer structure from high spatial range particle image velocimetry

NASA Astrophysics Data System (ADS)

Squire, D. T.; Morrill-Winter, C.; Hutchins, N.; Marusic, I.; Schultz, M. P.; Klewicki, J. C.

2016-10-01

Two particle image velocimetry arrangements are used to make true spatial comparisons between smooth- and rough-wall boundary layers at high Reynolds numbers across a very wide range of streamwise scales. Together, the arrangements resolve scales ranging from motions on the order of the Kolmogorov microscale to those longer than twice the boundary layer thickness. The rough-wall experiments were obtained above a continuous sandpaper sheet, identical to that used by Squire et al. [J. Fluid Mech. 795, 210 (2016), 10.1017/jfm.2016.196], and cover a range of friction and equivalent sand-grain roughness Reynolds numbers (12 000 ≲δ+≲ 18000, 62 ≲ks+≲104 ). The smooth-wall experiments comprise new and previously published data spanning 6500 ≲δ+≲17 000 . Flow statistics from all experiments show similar Reynolds number trends and behaviors to recent, well-resolved hot-wire anemometry measurements above the same rough surface. Comparisons, at matched δ+, between smooth- and rough-wall two-point correlation maps and two-point magnitude-squared coherence maps demonstrate that spatially the outer region of the boundary layer is the same between the two flows. This is apparently true even at wall-normal locations where the total (inner-normalized) energy differs between the smooth and rough wall. Generally, the present results provide strong support for Townsend's [The Structure of Turbulent Shear Flow (Cambridge University Press, Cambridge, 1956), Vol. 1] wall-similarity hypothesis in high Reynolds number fully rough boundary layer flows.
Effect of Fe- and Si-Enriched Secondary Precipitates and Surface Roughness on Pore Formation on Aluminum Plate Surfaces During Anodizing

NASA Astrophysics Data System (ADS)

Zhu, Yuanzhi; Wang, Shizhi; Yang, Qingda; Zhou, Feng

2014-09-01

Two twin roll casts (TRCs) and one hot rolled (HR) AA 1235 aluminum alloy plates with different microstructures are prepared. The plates were electrolyzed in a 1.2 wt% HCl solution with a voltage of 21 V and a current of 1.9 mA. The shape, size, and number of pores formed on the surfaces of these plates were analyzed and correlated with the microstructures of the plates. It is found that pores are easier to form on the alloy plates containing subgrains with a lower dislocation density inside the subgrains, rather than along the grain boundaries. Furthermore, Fe- and Si-enriched particles in the AA1235 aluminum alloys lead to the formation of pores on the surface during electrolyzing; the average precipitate sizes of 4, 3.5, and 2 μm in Alloy 1#, Alloy 2# and Alloy 3# result in the average pore sizes of 3.78, 2.76, and 1.9 μm on the surfaces of the three alloys, respectively; The G.P zone in the alloy also facilitates the surface pore formation. High-surface roughness enhances the possibility of entrapping more lubricants into the plate surface, which eventually blocks the formation of the pores on the surface of the aluminum plates in the following electrolyzing process.
Radar, visual and thermal characteristics of Mars: Rough planar surfaces

USGS Publications Warehouse

Schaber, G.G.

1980-01-01

High-resolution Viking Orbiter images (10 to 15 m/pixel) contain significant information on Martian surface roughness at 25- to 100-m lateral scales, whereas Earth-based radar observations of Mars are sensitive to roughness at lateral scales of 1 to 30 m, or more. High-rms slopes predicted for the Tharsis-Memnonia-Amazonis volcanic plains from extremely weak radar returns (low peak radar cross section) are qualitatively confirmed by the Viking image data. Large-scale, curvilinear (but parallel) ridges on lava flows in the Memnonia Fossae region are interpreted as innate flow morphology caused by compressional foldover of moving lava sheets of possible rhyolite-dacite composition. The presence or absence of a recent mantle of fine-grained eolian material on the volcanic surfaces studied was determined by the visibility of fresh impact craters with diameters less than 50 m. Lava flows south and west of Arsia Mons, and within the large region of low thermal inertia centered on Tharsis Montes (H. H. Kieffer et al., 1977, J. Geophys. Res.82, 4249-4291), were found to possess such a recent mantle. At predawn residual temperatures ??? -10K (south boundary of this low-temperature region), lava flows are shown to have relatively old eolian mantles. Lava flows with surfaces modified by eolian erosion and deposition occur west-northwest of Apollinaris Patera at the border of the cratered equatorial uplands and southern Elysium Planitia. Nearby yardangs, for which radar observations indicate very high-rms slopes, are similar to terrestrial features of similar origin. ?? 1980.
Effect of surface texture and structure on the development of stable fluvial armors

NASA Astrophysics Data System (ADS)

Bertin, Stephane; Friedrich, Heide

2018-04-01

Stable fluvial armors are found in river systems under conditions of partial sediment transport and limited sediment supply, a common occurrence in nature. Stable armoring is also readily recreated in experimental flumes. Initially, this bed stabilizing phenomenon was examined for different flow discharges and solely related to surface coarsening and bedload transport reduction. The models developed suggest a specific armor composition (i.e., texture) dependent on the parent bed material and formative discharge. Following developments in topographic remote sensing, recent research suggests that armor structure is an important control on bed stability and roughness. In this paper, replicated flume runs during which digital elevation models (DEMs) were collected from both exposed and flooded gravel beds are used to interpret armoring manifestations and to assess their replicability. A range of methodologies was used for the analysis, providing information on (i) surface grain size and orientation, (ii) bed-elevation distributions, (iii) the spatial coherence of the elevations at the grain-scale, (iv) surface slope and aspect, (v) grain imbrication and (vi) the spatial variability in DEM properties. The bed-surface topography was found to be more responsive than bed-material size to changes in flow strength. Our experimental results also provide convincing evidence that gravel-beds' response to water-work during parallel degradation is unique (i.e., replicable) given the formative parameters. Based on this finding, relationships between the armors' properties and formative parameters are proposed, and are supported by adding extensive data from previous research.
First Photograph Taken On Mars Surface

NASA Image and Video Library

1996-12-12

This is the first photograph ever taken on the surface of the planet Mars. It was obtained by Viking 1 just minutes after the spacecraft landed successfully early today [July 20, 1976]. The center of the image is about 1.4 meters (five feet) from Viking Lander camera #2. We see both rocks and finely granulated material--sand or dust. Many of the small foreground rocks are flat with angular facets. Several larger rocks exhibit irregular surfaces with pits and the large rock at top left shows intersecting linear cracks. Extending from that rock toward the camera is a vertical linear dark band which may be due to a one-minute partial obscuration of the landscape due to clouds or dust intervening between the sun and the surface. Associated with several of the rocks are apparent signs of wind transport of granular material. The large rock in the center is about 10 centimeters (4 inches) across and shows three rough facets. To its lower right is a rock near a smooth portion of the Martian surface probably composed of very fine-grained material. It is possible that the rock was moved during Viking 1 descent maneuvers, revealing the finer-grained basement substratum; or that the fine-grained material has accumulated adjacent to the rock. There are a number of other furrows and depressions and places with fine-grained material elsewhere in the picture. At right is a portion of footpad #2. Small quantities of fine grained sand and dust are seen at the center of the footpad near the strut and were deposited at landing. The shadow to the left of the footpad clearly exhibits detail, due to scattering of light either from the Martian atmosphere or from the spacecraft, observable because the Martian sky scatters light into shadowed areas. http://photojournal.jpl.nasa.gov/catalog/PIA00381
Carbon black retention in saturated natural soils: Effects of flow conditions, soil surface roughness and soil organic matter.

PubMed

Lohwacharin, J; Takizawa, S; Punyapalakul, P

2015-10-01

We evaluated factors affecting the transport, retention, and re-entrainment of carbon black nanoparticles (nCBs) in two saturated natural soils under different flow conditions and input concentrations using the two-site transport model and Kelvin probe force microscopy (KPFM). Soil organic matter (SOM) was found to create unfavorable conditions for the retention. Despite an increased flow velocity, the relative stability of the estimated maximum retention capacity in soils may suggest that flow-induced shear stress forces were insufficient to detach nCB. The KPFM observation revealed that nCBs were retained at the grain boundary and on surface roughness, which brought about substantial discrepancy between theoretically-derived attachment efficiency factors and the ones obtained by the experiments using the two-site transport model. Thus, decreasing ionic strength and increasing solution pH caused re-entrainment of only a small fraction of retained nCB in the soil columns. Copyright © 2015 Elsevier Ltd. All rights reserved.
A Review of Australian and New Zealand Investigations on Aeronautical Fatigue During the Period April 2011 to March 2013

DTIC Science & Technology

2013-04-01

properties in high-strength coarse grain titanium alloy with rough and torturous fatigue surfaces - Kevin Walker, (DSTO and RMIT University Australia), and...Wanhill, R. J. H. (1995) Damage tolerance engineering property evaluations of aerospace aluminium alloys with emphasis on fatigue crack growth. National...T6/T651 alloys . The testing of 7075-T6 C(T) coupons confirmed that the properties are very similar to the 7075-T651 material. Baseline
Milk kefir: ultrastructure, antimicrobial activity and efficacy on aflatoxin B1 production by Aspergillus flavus.

PubMed

Ismaiel, Ahmed A; Ghaly, Mohamed F; El-Naggar, Ayman K

2011-05-01

The association of kefir microbiota was observed by electron microscopic examination. Scanning electron microscopic (SEM) observations revealed that kefir grain surface is very rough and the inner portions had scattered irregular holes on its surface. The interior of the grain comprised fibrillar materials which were interpreted as protein, lipid and a soluble polysaccharide, the kefiran complex that surrounds yeast and bacteria in the grain. Yeast was observed more clearly than bacteria on the outer portion of the grain. Transmission electron microscopic (TEM) observations of kefir revealed that the grain comprised a mixed culture of yeast and bacteria growing in close association with each other. Microbiota is dominated by budded and long-flattened yeast cells growing together with lactobacilli and lactococci bacteria. Bacterial cells with rounded ends were also observed in this mixed culture. Kefir grains, kefir suspensions, and kefiran were tested for antimicrobial activities against several bacterial and fungal species. The highest activity was obtained against Streptococcus faecalis KR6 and Fusarium graminearum CZ1. Growth of Aspergillus flavus AH3 producing for aflatoxin B1 for 10 days in broth medium supplemented with varying concentrations of kefir filtrate (%, v/v) showed that sporulation was completely inhibited at the higher concentrations of kefir filtrate (7-10%, v/v). The average values of both mycelial dry weights and aflatoxin B1 were completely inhibited at 10% (v/v). This is the first in vitro study about the antifungal characteristics of kefir against filamentous fungi which was manifested by applying its inhibitory effect on the productivity of aflatoxin B1 by A. flavus AH3.
Surface Morphology of Liquid and Solid Thin Films via X-Ray Reflectivity.

NASA Astrophysics Data System (ADS)

Shindler, Joseph Daniel

X-ray reflectivity can be used to measure the spatial variations in the electron density on length scales from Angstroms to microns. It is sensitive to atomic scale roughness, interdiffusion in buried layers, the thickness of multilayer stacks, and in-plane correlations in each of these cases. We have pioneered the use of a high intensity, moderate resolution configuration for x-ray reflectivity which utilizes a bent crystal graphite monochromator. With this technique we can obtain a beam intensity one hundred times greater than is possible using the high resolution rotating anode configuration, while we have shown that the resulting instrumental resolution is appropriate for the vast majority of thin film work. For all of the systems studied, we were able to measure the weak diffuse scattering signal to probe the in-plane length scales of interfacial roughness, a measurement which had previously only been attempted at synchrotron sources. Studied systems include thin films and surfaces with a wide range of structural order and surface morphologies. Interest in liquid films has been of a fundamental nature. Theories on the expected film evolution with changing thickness and temperature are currently being tested with scattering experiments. We have pursued the issues of film/substrate wetting and conformality, focussing on the temperature dependence of these phenomena near the triple point. Despite the heterogeneity of the substrate potential, we see a very sharp wetting transition at or near the triple point, although below the triple point the film is still smooth, consistent with a uniform layer. We also see a loss of conformality as the fluid films thicken; this is consistent with theory and with other recent experiments. The properties of a multilayer solid film depend not only on the magnitude of the roughness of each interface, but also on the conformality between interfaces and the length scales of the roughness--i.e., whether the roughness is on the atomic lengths of interdiffusion, crystalline order lengths of faceting, or even longer lengths due to other processes. In a joint project with Alcoa, we combined the methods of x-ray Bragg diffraction and small angle reflectivity to probe aluminum thin films as precursors to true multilayer films, correlating grain size and orientation with the magnitude and length-scales of surface roughness. We also correlated all film properties with such parameters as the deposition method, substrate roughness, and film thickness.
Effect of the surface roughness on the seismic signal generated by a single rock impact: insight from laboratory experiments

NASA Astrophysics Data System (ADS)

Bachelet, Vincent; Mangeney, Anne; de Rosny, Julien; Toussaint, Renaud

2016-04-01

The seismic signal generated by rockfalls, landslides or avalanches is a unique tool to detect, characterize and monitor gravitational flow activity, with strong implication in terms of natural hazard monitoring. Indeed, as natural flows travel down the slope, they apply stresses on the ground, generating seismic waves in a wide frequency band. Our ultimate objective is to relate the granular flow properties to the generated signals that result from the different physical processes involved. We investigate here the more simple process: the impact of a single bead on a rough surface. Farin et al. [2015] have already shown theoretically and experimentally the existence of a link between the properties of an impacting bead (mass and velocity) on smooth surfaces, and the emitted signal (radiated elastic energy and mean frequency). This demonstrates that the single impactor properties can be deduced from the form of the emitted signal. We extend this work here by investigating the impact of single beads and gravels on rough and erodible surfaces. Experimentally, we drop glass and steel beads of diameters from 2 mm to 10 mm on a PMMA plate. The roughness of this last is obtained by gluing 3mm-diameter glass beads on one of its face. Free beads have been also added to get erodible beds. We track the dropped impactor motion, times between impacts and the generated acoustic waves using two fast cameras and 8 accelerometers. Cameras are used in addition to estimate the impactor rotation. We investigate the energy balance during the impact process, especially how the energy restitution varies as a function of the energy lost through acoustic waves. From these experiments, we clearly observe that even if more dissipative processes are involved (friction, grain reorganization, etc.), the single bead scaling laws obtained on smooth surfaces remain valid. A main result of this work is to quantify the fluctuations of the characteristic quantities such as the bounce angle, the seismic energy and frequency induced by the plate roughness.
Ice sintering timescales at the surface of Europa and implications for surface properties

NASA Astrophysics Data System (ADS)

Molaro, Jamie; Phillips, Cynthia B.; Meirion-Griffith, Gareth

2017-10-01

The planned exploration of Europa by NASA’s Europa Clipper Mission and the possibility of a future Europa lander have driven the need to characterize its surface strength, roughness, porosity, thermal conductivity, and regolith depth in order to accurately interpret remote sensing data and develop appropriate spacecraft landing systems. Many processes contribute to Europa’s landscape evolution, such as sputtering, mass wasting, thermal segregation, and impact gardening, driving the creation and distribution of icy regolith across the surface. While the efficacy of these processes are not well constrained, any amount of regolith emplaced at the surface will undergo subsequent processing due to sintering. Ice sintering is a form of frost metamorphism whereby contacting ice grains experience the diffusion of material into their contact region, forming a “neck” between them and densifying over time. Over long enough timescales, ice aggregates will sinter into solid material, which may contribute to the incorporation of non-ice material into Europa’s subsurface and help to drive subsurface chemistry. Sintering also interacts with other processes, adding to the complexity of icy surface evolution. For example, sputtering preferentially removes larger grains and may enhance sintering rates, and changes in ice porosity may affect the response of the surface to micrometeorite impacts.Quantifying the effects of ice sintering will allow us to predict the microstructural properties of Europa’s surface at spacecraft scales. To this end, we have modeled pressure-less (no overburden) sintering of spherical water-ice grains and validated the results with a laboratory experiment. We also modeled ice at the surface of Europa to obtain a first-order approximation of the sintering timescale and surface properties. Preliminary results indicate that ice grains will experience neck growth but not significant densification over Europa’s surface age, suggesting that loose surface ice forms a weak and porous crust. Furthermore, our results suggest that existing models do not accurately quantify all stages of the sintering process for ice, emphasizing the need for more laboratory studies on this topic.
Growth evolution of AlN films on silicon (111) substrates by pulsed laser deposition

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Haiyan; Wang, Wenliang; Yang, Weijia

2015-05-14

AlN films with various thicknesses have been grown on Si(111) substrates by pulsed laser deposition (PLD). The surface morphology and structural property of the as-grown AlN films have been investigated carefully to comprehensively explore the epitaxial behavior. The ∼2 nm-thick AlN film initially grown on Si substrate exhibits an atomically flat surface with a root-mean-square surface roughness of 0.23 nm. As the thickness increases, AlN grains gradually grow larger, causing a relatively rough surface. The surface morphology of ∼120 nm-thick AlN film indicates that AlN islands coalesce together and eventually form AlN layers. The decreasing growth rate from 240 to 180 nm/h is amore » direct evidence that the growth mode of AlN films grown on Si substrates by PLD changes from the islands growth to the layer growth. The evolution of AlN films throughout the growth is studied deeply, and its corresponding growth mechanism is hence proposed. These results are instructional for the growth of high-quality nitride films on Si substrates by PLD, and of great interest for the fabrication of AlN-based devices.« less
The Effect of Grain Refinement on Solid Particle Erosion of Grade 5 Ti Alloy

NASA Astrophysics Data System (ADS)

Kazarinov, N. A.; Evstifeev, A. D.; Petrov, Y. V.; Atroshenko, S. A.; Valiev, R. R.

2018-04-01

In this work, the results on solid particle erosion of an ultrafine-grained Grade 5 titanium alloy, which was produced using high-pressure torsion (HPT) technique, are presented. In order to assess influence of the HPT treatment on material's behavior in erosive conditions, special experimental procedures were developed. The ultrafine-grained (UFG) alloy was tested alongside with a conventional coarse-grained (CG) Grade 5 titanium alloy in equal conditions. The experiments were conducted in a small-scale wind tunnel with corundum particles as an abrasive material. Both particle dimensions and particle velocities were varied in course of the experiments. Erosion resistance of the samples was evaluated in two ways—mass reduction measurements with subsequent gravimetric erosion rate calculations and investigation of samples' surface roughness after erosion tests. The UFG titanium alloy demonstrated considerable improvement of static mechanical properties (ultimate tensile strength, microhardness), whereas its CG counterpart appeared to be slightly more resistant to solid particle erosion, which might indicate the drop of dynamic strength properties for the HPT-processed material.
Quantifying grain shape with MorpheoLV: A case study using Holocene glacial marine sediments

NASA Astrophysics Data System (ADS)

Charpentier, Isabelle; Staszyc, Alicia B.; Wellner, Julia S.; Alejandro, Vanessa

2017-06-01

As demonstrated in earlier works, quantitative grain shape analysis has revealed to be a strong proxy for determining sediment transport history and depositional environments. MorpheoLV, devoted to the calculation of roughness coefficients from pictures of unique clastic sediment grains using Fourier analysis, drives computations for a collection of samples of grain images. This process may be applied to sedimentary deposits assuming core/interval/image archives for the storage of samples collected along depth. This study uses a 25.8 m jumbo piston core, NBP1203 JPC36, taken from a 100 m thick sedimentary drift deposit from Perseverance Drift on the northern Antarctic Peninsula continental shelf. Changes in ocean and ice conditions throughout the Holocene recorded in this sedimentary archive can be assessed by studying grain shape, grain texture, and other proxies. Ninety six intervals were sampled and a total of 2319 individual particle images were used. Microtextures of individual grains observed by SEM show a very high abundance of authigenically precipitated silica that obscures the original grain shape. Grain roughness, computed along depth with MorpheoLV, only shows small variation confirming the qualitative observation deduced from the SEM. Despite this, trends can be seen confirming the reliability of MorpheoLV as a tool for quantitative grain shape analysis.
Dense Suspension Splash

NASA Astrophysics Data System (ADS)

Zhang, Wendy; Dodge, Kevin M.; Peters, Ivo R.; Ellowitz, Jake; Klein Schaarsberg, Martin H.; Jaeger, Heinrich M.

2014-03-01

Upon impact onto a solid surface at several meters-per-second, a dense suspension plug splashes by ejecting liquid-coated particles. We study the mechanism for splash formation using experiments and a numerical model. In the model, the dense suspension is idealized as a collection of cohesionless, rigid grains with finite surface roughness. The grains also experience lubrication drag as they approach, collide inelastically and rebound away from each other. Simulations using this model reproduce the measured momentum distribution of ejected particles. They also provide direct evidence supporting the conclusion from earlier experiments that inelastic collisions, rather than viscous drag, dominate when the suspension contains macroscopic particles immersed in a low-viscosity solvent such as water. Finally, the simulations reveal two distinct routes for splash formation: a particle can be ejected by a single high momentum-change collision. More surprisingly, a succession of small momentum-change collisions can accumulate to eject a particle outwards. Supported by NSF through its MRSEC program (DMR-0820054) and fluid dynamics program (CBET-1336489).
A Rapid Method for Deposition of Sn-Doped GaN Thin Films on Glass and Polyethylene Terephthalate Substrates

NASA Astrophysics Data System (ADS)

Pat, Suat; Özen, Soner; Korkmaz, Şadan

2018-01-01

We report the influence of Sn doping on microstructure, surface, and optical properties of GaN thin films deposited on glass and polyethylene terephthalate (PET) substrate. Sn-doped GaN thin films have been deposited by thermionic vacuum arc (TVA) at low temperature. TVA is a rapid deposition technology for thin film growth. Surface and optical properties of the thin films were presented. Grain size, height distribution, roughness values were determined. Grain sizes were calculated as 20 nm and 13 nm for glass and PET substrates, respectively. Nano crystalline forms were shown by field emission scanning electron microscopy. Optical band gap values were determined by optical methods and photoluminescence measurement. The optical band gap values of Sn doped GaN on glass and PET were determined to be approximately ˜3.40 eV and ˜3.47 eV, respectively. As a result, TVA is a rapid and low temperature deposition technology for the Sn doped GaN deposited on glass and PET substrate.
The Role of Grain Dynamics in the Onset of Sediment Transport

NASA Astrophysics Data System (ADS)

Clark, A., IV; Shattuck, M. D.; Ouellette, N. T.; O'Hern, C.

2016-12-01

Despite decades of research, the grain-scale mechanisms that control the onset of sediment transport are still not well understood. A large collection of data, known as the Shields curve, shows that Θ c, which is the minimum dimensionless shear stress at the bed for grains to move, is primarily a function of the shear Reynolds number Re*. To understand this collapse, it is typically assumed that the onset of grain motion is determined by the conditions at which fluid forces violate static equilibrium for surface grains. Re* compares the grain size to the size of the viscous sublayer in the fluid flow, so the relevant fluid lift and drag forces vary with Re*. A complimentary approach, which remains relatively unexplored, is to ask instead when mobilized grains can stop. In this case, Re* is the ratio of two important time scales related to grain motion: (1) the time for a grain to equilibrate to the fluid flow and (2) the time for the shear stress to accelerate a grain over the characteristic bed roughness. Thus, Re* controls whether grains are accelerated significantly between collisions with the bed. To test how this effect relates to the Shields curve, we perform simulations of granular beds sheared by a model fluid flow, where Re* is varied only through the fluid-grain coupling, which alters the grain dynamics. We find good qualitative agreement with the Shields curve, and the quantitative discrepancies are consistent with lift forces calculations at varying Re*. Our results suggest that the onset of sediment transport may be better described as when mobile grains are able to stop, which varies significantly with Re*, and theoretical descriptions that account for this effect may be more successful than those that consider only static equilibrium.
Quantitative Mapping of Surface Texture on the Northern Polar Residual Cap of Mars

NASA Astrophysics Data System (ADS)

Milkovich, S. M.; Byrne, S.; Russell, P. S.

2010-12-01

The northern polar residual cap (NPRC) of Mars is a water ice deposit with a rough surface made up of pits, knobs, and linear depressions on scales of tens of meters [1]. This roughness manifests as a series of bright and dark patches in visible images. Spectral data indicate that the surface of the NPRC is composed of large-grained (and therefore old) water ice. Due to the presence of this old ice, it is thought that the NPRC is in a current state of net loss of material [2]. The NPRC provides a link between the current martian climate and the historical climate recorded within the layers of the underlying north polar layered deposits. By characterizing and mapping the variations in surface texture of the NPRC, we seek to understand what factors (distance from the pole, GCM and mesoscale wind direction predictions, etc) are currently at work in resurfacing the deposit, and may have been at work in shaping the layers below. Maps of NPRC texture wavelength and orientation are being produced from HiRISE images. Two-dimensional Fourier analysis is performed upon a 256 meter x 256 meter region (corresponding to 512 x 512 pixels in 0.5 cm/pxl images, or 1024 x 1024 pixels in 0.25 cm/pxl images) within each image analyzed. The dominant wavelength of the resulting peak power spectrum corresponds to the average size of a pit-knob pair in the image, and so is a proxy for the scale of the surface roughness. The orientation of the surface roughness (i.e., the orientation of a chain of pits and mounds) is measured from a narrow range of wavelengths encompassing the dominant wavelength. We will report on how the dominant wavelengths and orientations of this surface texture vary with location and what that implies for the processes currently shaping this landscape. [1] P. C. Thomas et al, Nature 404, 161-164, 2000 [2]Y. Langevin et al, Science 307, 5715, 1581-1584, 2005.

Periodic grain-boundary formation in a poly-Si thin film crystallized by linearly polarized Nd:YAG pulse laser with an oblique incident angle

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kaki, Hirokazu; Horita, Susumu

2005-01-01

We investigated the periodic grain-boundary formation in the polycrystalline silicon film crystallized by a linearly polarized Nd:YAG (where YAG is yttrium aluminum garnet) pulse laser with an oblique incident angle {theta}{sub i}=25 deg. , compared with the normal incident angle {theta}{sub i}=0. The alignment of the grain boundary was uncontrollable and fluctuated in the case of the oblique incident and large irradiation pulse number while that in the case of the normal incident was performed stably. It was found that the main cause for its low controllability was the nonphase matching between the periodic surface corrugation of the crystallized siliconmore » film and the periodic temperature profile induced by the laser irradiation. Also, it was found that, in the case of {theta}{sub i}=25 deg. , the dominant periodic width of the grain boundary depended on the pulse number N. That is, it was around {lambda}/(1+sin {theta}{sub i}) for small N{approx_equal}10 and {lambda}/(1-sin {theta}{sub i}) for large N{approx_equal}100 at the laser wavelength of {lambda}=532 nm. In order to explain this dependence, we proposed a model to take into account the periodic corrugation height proportional to the molten volume of the silicon film, the impediment in interference between the incident beam and diffracted beam on the irradiated surface due to the corrugation height, and the reduction of the liquid surface roughness during melting-crystallization process due to liquid-silicon viscosity.« less
Localized melt-scan strategy for site specific control of grain size and primary dendrite arm spacing in electron beam additive manufacturing

DOE Office of Scientific and Technical Information (OSTI.GOV)

Raghavan, Narendran; Simunovic, Srdjan; Dehoff, Ryan

In addition to design geometry, surface roughness, and solid-state phase transformation, solidification microstructure plays a crucial role in controlling the performance of additively manufactured components. Crystallographic texture, primary dendrite arm spacing (PDAS), and grain size are directly correlated to local solidification conditions. We have developed a new melt-scan strategy for inducing site specific, on-demand control of solidification microstructure. We were able to induce variations in grain size (30 μm–150 μm) and PDAS (4 μm - 10 μm) in Inconel 718 parts produced by the electron beam additive manufacturing system (Arcam®). A conventional raster melt-scan resulted in a grain size ofmore » about 600 μm. The observed variations in grain size with different melt-scan strategies are rationalized using a numerical thermal and solidification model which accounts for the transient curvature of the melt pool and associated thermal gradients and liquid-solid interface velocities. The refinement in grain size at high cooling rates (>104 K/s) is also attributed to the potential heterogeneous nucleation of grains ahead of the epitaxially growing solidification front. The variation in PDAS is rationalized using a coupled numerical-theoretical model as a function of local solidification conditions (thermal gradient and liquid-solid interface velocity) of the melt pool.« less
DOE Office of Scientific and Technical Information (OSTI.GOV)

Rani, R.; Kumar, N., E-mail: niranjan@igcar.gov.in; Lin, I-Nan

Nanostructured diamond films are having numerous unique properties including superior tribological behavior which is promising for enhancing energy efficiency and life time of the sliding devices. High wear resistance is the principal criterion for the smooth functioning of any sliding device. Such properties are achievable by tailoring the grain size and grain boundary volume fraction in nanodiamond film. Ultra-nanocrystalline diamond (UNCD) film was attainable using optimized gas plasma condition in a microwave plasma enhanced chemical vapor deposition (MPECVD) system. Crystalline phase of ultra-nanodiamond grains with matrix phase of amorphous carbon and short range ordered graphite are encapsulated in nanowire shapedmore » morphology. Film showed ultra-high wear resistance and frictional stability in micro-tribological contact conditions. The negligible wear of film at the beginning of the tribological contact was later transformed into the wearless regime for prolonged sliding cycles. Both surface roughness and high contact stress were the main reasons of wear at the beginning of sliding cycles. However, the interface gets smoothened due to continuous sliding, finally leaded to the wearless regime.« less
Extraction of He and NE from Individual Lunar Ilmenite Grains by Pulse Heating

NASA Astrophysics Data System (ADS)

Nier, A. O.; Schlutter, D. J.

1993-07-01

The pulse-heating technique employed for extracting helium and neon from individual interplanetary dust particles [1] has been extended to a similar study of individual lunar grains. A succession of 5-s constant power pulses is applied to the oven holding the particle. The power is increased in 0.25-W increments until all the gas is removed. The peak temperature reached during a pulse lasts about 2 s and increases by roughly 75 degrees C for each 0.25-W increment in power. In the present investigation six individual ilmenite grains of lunar soil 71501 and of breccia 79035 were studied. It was felt that this method of extracting the gas might help in distinguishing between surface embedded solar wind (SW) particles and more deeply embedded constituents such as solar energetic particles (SEP) [2], or gas of trapped or primordial origin. Although only six particles of each type have been studied to date, interesting results are beginning to emerge. For example, for both types of particles, for the initial low power pulses where the maximum pulse temperature does not exceed 500 degrees C, the ^3He/^4He ratio falls near 4 x 10^-4, as expected, if the helium is primarily unfractionated solar wind implanted near the surface. As the pulse temperature is increased to around 1000 degrees C and the solar wind gas presumably has been removed, the ^3He/^4He ratio falls to around 2.5 x 10^-4, in rough agreement with the layer etching results [2]. Likewise, the ^20Ne/^22Ne ratio falls from around 14 to a value near 12, as in the etching experiments [2]. In the case of ^4He/^20Ne ratios there appears to be a real difference between the particles from the two ilmenites. For the 79035 grains, the ratio falls from around 600 for the surface gas to around 150 for the later high-temperature extractions. On the other hand, for the 71501 grains, the ratio starts somewhat lower, near 400, and drops below 100 as the pulse temperature is raised. A qualitatively similar difference was observed in the total gas released by laser beam extractions performed on single grains from the same lunar ilmenite samples [3]. While there is considerable scatter in the data, the overall results are gratifying, and should become more definitive as more particles are investigated. The initial releases, almost certainly from the surfaces of the particles, come closer to the solar wind values [4] than generally reported for lunar grains. It will be interesting to see whether or not the differences observed are real and have a bearing on the general problem of the variation of the solar wind with time [5]. Acknowledgment: We are indebted to R. Wieler for the ilmenite grains used in the investigation. References: [1] Nier A. O. and Schlutter D. J. (1993) LPS XXIV, 1075-1076.[2] Wieler R. et al. (1986) GCA, 50, 1997-2017. [3] Olinger C. T. et al. (1990) Meteoritics, 25, 394. [4] Geiss J. et al. (1972) Apollo 16 Prelim. Sci. Rept., 14-1 to 14-10, NASA SP 315. [5] Becker R. H. and Pepin R. O. (1989) GCA, 53, 1135-1146.
Investigation of rapidly solidified aluminum by using diamond turning and a magnetorheological finishing process

NASA Astrophysics Data System (ADS)

Cheng, Yuan-Chieh; Hsu, Wei-Yao; Kuo, Ching-Hsiang; Abou-El-Hossein, Khaled; Otieno, Timothy

2015-08-01

The metal mirror has been widely used in optical application for a longtime. Especially the aluminum 6061 is often considered the preferred material for manufacturing optical components for ground-based astronomical applications. One reason for using this material is its high specific stiffness and excellent thermal properties. However, a large amount of data exists for this material and commercially available aluminum 6061 using single point diamond turning (SPDT) and polishing process can achieve surface roughness values of approximately 2 to 4 nm, which is adequate for applications that involve the infrared spectral range, but not for the shorter spectral range. A novel aluminum material, fabricated using a rapid solidification process that is equivalent to the conventional aluminum 6061 alloy grade has been used in optical applications in recent years because of its smaller grain size. In this study, the surface quality of the rapid solidification aluminum after single point diamond turning and followed by magnetorheological finish (MRF) process is investigated and compared with conventional aluminum 6061. Both the surface roughness Ra was evaluated using white light interferometers. Finally, indicators such as optimal fabrication parameter combination and optical performance are discussed.
The Effect of Surfactant Content over Cu-Ni Coatings Electroplated by the sc-CO2 Technique

PubMed Central

Chuang, Ho-Chiao; Sánchez, Jorge; Cheng, Hsiang-Yun

2017-01-01

Co-plating of Cu-Ni coatings by supercritical CO2 (sc-CO2) and conventional electroplating processes was studied in this work. 1,4-butynediol was chosen as the surfactant and the effects of adjusting the surfactant content were described. Although the sc-CO2 process displayed lower current efficiency, it effectively removed excess hydrogen that causes defects on the coating surface, refined grain size, reduced surface roughness, and increased electrochemical resistance. Surface roughness of coatings fabricated by the sc-CO2 process was reduced by an average of 10%, and a maximum of 55%, compared to conventional process at different fabrication parameters. Cu-Ni coatings produced by the sc-CO2 process displayed increased corrosion potential of ~0.05 V over Cu-Ni coatings produced by the conventional process, and 0.175 V over pure Cu coatings produced by the conventional process. For coatings ~10 µm thick, internal stress developed from the sc-CO2 process were ~20 MPa lower than conventional process. Finally, the preferred crystal orientation of the fabricated coatings remained in the (111) direction regardless of the process used or surfactant content. PMID:28772787
Rheology of ice I at low stress and elevated confining pressure

USGS Publications Warehouse

Durham, W.B.; Stern, L.A.; Kirby, S.H.

2001-01-01

Triaxial compression testing of pure, polycrystalline water ice I at conditions relevant to planetary interiors and near-surface environments (differential stresses 0.45 to 10 MPa, temperatures 200 to 250 K, confining pressure 50 MPa) reveals that a complex variety of rheologies and grain structures may exist for ice and that rheology of ice appears to depend strongly on the grain structures. The creep of polycrystalline ice I with average grain size of 0.25 mm and larger is consistent with previously published dislocation creep laws, which are now extended to strain rates as low as 2 ?? 10-8s-1. When ice I is reduced to very fine and uniform grain size by rapid pressure release from the ice II stability field, the rheology changes dramatically. At 200 and 220 K the rheology matches the grain-size-sensitive rheology measured by Goldsby and Kohlstedt [1997, this issue] at 1 atm. This finding dispels concerns that the Goldsby and Kohlstedt results were influenced by mechanisms such as microfracturing and cavitation, processes not expected to operate at elevated pressures in planetary interiors. At 233 K and above, grain growth causes the fine-grained ice to become more creep resistant. Scanning electron microscopy investigation of some of these deformed samples shows that grains have markedly coarsened and the strain hardening can be modeled by normal grain growth and the Goldsby and Kohlstedt rheology. Several samples also displayed very heterogeneous grain sizes and high aspect ratio grain shapes. Grain-size-sensitive creep and dislocation creep coincidentally contribute roughly equal amounts of strain rate at conditions of stress, temperature, and grain size that are typical of terrestrial and planetary settings, so modeling ice dynamics in these settings must include both mechanisms. Copyright 2001 by the American Geophysical Union.
Microfabricated Amorphous Silicon Nanopillars on an Ultrasmooth 500-nm-thick Titanium Adhesion Layer

DTIC Science & Technology

2012-09-01

After Ti deposition, the wafers were pretreated with 10 ml of liquid hexamethyldisilazane ( HMDS ) to promote adhesion by photoresist. The HMDS was...film with a high flux of Ti atoms and shows large grains and a rough surface. In figure 2b, some residue can be seen near the 1000-nm pillars on the...closely to the SEM image shown in appendix B, which has a measured angle near 51°. In the future, a more vertical sidewall is likely to be desired
Effectiveness of pulsed light treatment for degradation and detoxification of aflatoxin B1 and B2 in rough rice and rice bran

USDA-ARS?s Scientific Manuscript database

Aflatoxins primarily accumulate in the hull and bran layers of rough rice making these by-products of rice milling unsuitable for animal feed or human consumption. Contaminated rough rice is also a potential source of aflatoxin exposure to workers handling the grain during post-harvest storage and p...
YSZ thin films with minimized grain boundary resistivity

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mills, Edmund M.; Kleine-Boymann, Matthias; Janek, Juergen

2016-03-31

In recent years, interface engineering of solid electrolytes has been explored to increase their ionic conductivity and improve the performance of solid oxide fuel cells and other electrochemical power sources. It has been observed that the ionic conductivity of epitaxially grown thin films of some electrolytes is dramatically enhanced, which is often attributed to effects (e. g. strain-induced mobility changes) at the heterophase boundary with the substrate. Still largely unexplored is the possibility of manipulation of grain boundary resistivity in polycrystalline solid electrolyte films, clearly a limiting factor in their ionic conductivity. Here we report that the ionic conductivity ofmore » yttria stabilized zirconia thin films with nano- columnar grains grown on a MgO substrate nearly reaches that of the corresponding single crystal when the thickness of the films becomes less than roughly 8 nm (smaller by a factor of three at 500°C). Using impedance spectroscopy, the grain boundary resistivity was probed as a function of film thickness. The resistivity of the grain boundaries near the film- substrate interface and film surface (within 4 nm of each) was almost entirely eliminated. This minimization of grain boundary resistivity is attributed to Mg2+ diffusion from the MgO substrate into the YSZ grain boundaries, which is supported by time of flight secondary ion mass spectroscopy measurements. We suggest grain boundary “design” as an attractive method to obtain highly conductive solid electrolyte thin films.« less
YSZ thin films with minimized grain boundary resistivity

DOE PAGES

Mills, Edmund M.; Kleine-Boymann, Matthias; Janek, Juergen; ...

2016-03-31

In recent years, interface engineering of solid electrolytes has been explored to increase their ionic conductivity and improve the performance of solid oxide fuel cells and other electrochemical power sources. It has been observed that the ionic conductivity of epitaxially grown thin films of some electrolytes is dramatically enhanced, which is often attributed to effects (e.g. strain-induced mobility changes) at the heterophase boundary with the substrate. Still largely unexplored is the possibility of manipulation of grain boundary resistivity in polycrystalline solid electrolyte films, clearly a limiting factor in their ionic conductivity. Here in this paper, we report that the ionicmore » conductivity of yttria stabilized zirconia thin films with nano-columnar grains grown on a MgO substrate nearly reaches that of the corresponding single crystal when the thickness of the films becomes less than roughly 8 nm (smaller by a factor of three at 500 °C). Using impedance spectroscopy, the grain boundary resistivity was probed as a function of film thickness. The resistivity of the grain boundaries near the film–substrate interface and film surface (within 4 nm of each) was almost entirely eliminated. This minimization of grain boundary resistivity is attributed to Mg 2+ diffusion from the MgO substrate into the YSZ grain boundaries, which is supported by time of flight secondary ion mass spectroscopy measurements. We suggest grain boundary “design” as an attractive method to obtain highly conductive solid electrolyte thin films.« less
Grain-size-dependent diamond-nondiamond composite films: characterization and field-emission properties.

PubMed

Pradhan, Debabrata; Lin, I Nan

2009-07-01

Diamond films with grain sizes in the range of 5-1000 nm and grain boundaries containing nondiamond carbon are deposited on a silicon substrate by varying the deposition parameters. The overall morphologies of the as-deposited diamond-nondiamond composite films are examined by scanning electron microscopy and atomic force microscopy, which show a decrease in the surface roughness with a decrease in the diamond grain size. Although the Raman spectra show predominately nondiamond carbon features in the diamond films with smaller grain sizes, glancing-angle X-ray diffraction spectra show the absence of graphitic carbon features and the presence of very small amorphous carbon diffraction features. The CH4 percentage (%) in Ar and H2 plasma during deposition plays a crucial role in the formation of diamond films with different grain sizes and nondiamond carbon contents, which, in turn, determines the field-emission behavior of the corresponding diamond films. The smaller the grain size of the diamond, the lower is the turn-on field for electron emission. A lower turn-on field is obtained from the diamond films deposited with 2-5% CH4 than from the films deposited with either 1% or 7.5% CH4 in the Ar medium. A current density greater than 1 mA/cm2 (at 50 V/microm) is obtained from diamond films deposited with a higher percentage of CH4. A model is suggested for the field-emission mechanism from the diamond-nondiamond composite films with different diamond grain sizes and nondiamond contents.
Biological half-life of gaseous elemental iodine deposited onto rice grains

DOE Office of Scientific and Technical Information (OSTI.GOV)

Uchida, S.; Muramatsu, Y.; Sumiya, M.

In order to obtain the biological half-life (Tb) of iodine deposited on rough rice grains, rice plants of four different growing stages--heading, milky, dough, and yellow ripe--were exposed to elemental gaseous iodine. After the exposure, the rough rice samples were collected at different intervals and analyzed for iodine to estimate the value of Tb. The average value of Tb obtained by the experiments at the dough and yellow ripe stages was about 200 d. This value is considerably larger than those for pasture grass and leafy vegetables.
Micro-mechanisms of Surface Defects Induced on Aluminum Alloys during Plastic Deformation at Elevated Temperatures

NASA Astrophysics Data System (ADS)

Gali, Olufisayo A.

Near-surface deformed layers developed on aluminum alloys significantly influence the corrosion and tribological behavior as well as reduce the surface quality of the rolled aluminum. The evolution of the near-surface microstructures induced on magnesium containing aluminum alloys during thermomechanical processing has been investigated with the aim generating an understanding of the influence of individual forming parameters on its evolution and examine the microstructure of the roll coating induced on the mating steel roll through material transfer during rolling. The micro-mechanisms related to the various features of near-surface microstructure developed during tribological conditions of the simulated hot rolling process were identified. Thermomechanical processing experiments were performed with the aid of hot rolling (operating temperature: 550 to 460 °C, 4, 10 and 20 rolling pass schedules) and hot forming (operating temperature: 350 to 545 °C, strain rate: 4 x 10-2 s-1) tribo-simulators. The surface, near-surface features and material transfer induced during the elevated temperature plastic deformation were examined and characterized employing optical interferometry, SEM/EDS, FIB and TEM. Near-surface features characterized on the rolled aluminum alloys included; cracks, fractured intermetallic particles, aluminum nano-particles, oxide decorated grain boundaries, rolled-in oxides, shingles and blisters. These features were related to various individual rolling parameters which included, the work roll roughness, which induced the formation of shingles, rolling marks and were responsible for the redistribution of surface oxide and the enhancements of the depth of the near-surface damage. The enhanced stresses and strains experienced during rolling were related to the formation and propagation of cracks, the nanocrystalline structure of the near-surface layers and aluminum nano-particles. The mechanism of the evolution of the near-surface microstructure were determined to include grain boundary sliding which induced the cracks at the surface and subsurface of the alloy, magnesium diffusion to free surfaces, crack propagation from shear stresses and the shear strains inducing the nanocrystalline grain structure, the formation of shingles by the shear deformation of micro-wedges induced by the work roll grooves, and the deformation of this oxide covered micro-wedges inducing the rolled-in oxides. Magnesium diffusion to free surfaces was identified as inducing crack healing due to the formation of MgO within cracks and was responsible for the oxide decorated grain boundaries. An examination of the roll coating revealed a complex layered microstructure that was induced through tribo-chemical and mechanical entrapment mechanisms. The microstructure of the roll coating suggested that the work roll material and the rolled aluminum alloy were essential in determining its composition and structure. Subsequent hot forming processes revealed the rich oxide-layer of the near-surface microstructure was beneficial for reducing the coefficient of friction during tribological contact with the steel die. Damage to the microstructure include cracks induced from grain boundary sliding of near-surface grains and the formation of oxide fibres within cracks of the near-surface deformed layers.
How does sediment affect the hydraulics of bedrock-alluvial rivers?

NASA Astrophysics Data System (ADS)

Hodge, Rebecca; Hoey, Trevor; Maniatis, George; Leprêtre, Emilie

2016-04-01

Relationships between flow, sediment transport and channel morphology are relatively well established in coarse-grained alluvial channels. Developing equivalent relationships for bedrock-alluvial channels is complicated by the two different components that comprise the channel morphology: bedrock and sediment. These two components usually have very different response times to hydraulic forcing, meaning that the bedrock morphology may be inherited from previous conditions. The influence of changing sediment cover on channel morphology and roughness will depend on the relative magnitudes of the sediment size and the spatial variations in bedrock elevation. We report results from experiments in a 0.9m wide flume designed to quantify the interactions between flow and sediment patch morphology using two contrasting bedrock topographies. The first topography is a plane bed with sand-scale roughness, and the second is a 1:10 scale, 3D printed, model of a bedrock channel with spatially variable roughness (standard deviation of elevations = 12 mm in the flume). In all experiments, a sediment pulse was added to the flume (D50 between 7 and 15 mm) and sediment patches were allowed to stabilise under constant flow conditions. The flow was then incrementally increased in order to identify the discharges at which sediment patches and isolated grains were eroded. In the plane bed experiments ˜20% sediment cover is sufficient to alter the channel hydraulics through the increased roughness of the bed; this impact is expressed as the increased discharge at which isolated grains are entrained. In the scaled bed experiments, partial sediment cover decreased local flow velocities on a relatively smooth area of the bed. At the scale of the entire channel, the bed morphology, and the hydraulics induced by it, was a primary control on sediment cover stability at lower sediment inputs. At higher inputs, where sediment infilled the local bed topography, patches were relatively more stable, suggesting an increased impact on the hydraulics and the role of grain-grain interactions. We draw together these experiments using a theoretical framework to express the impact of sediment cover on channel roughness and hence hydraulics.
Temperature induced CuInSe2 nanocrystal formation in the Cu2Se-In3Se2 multilayer thin films

NASA Astrophysics Data System (ADS)

Mohan, A.; Rajesh, S.

2017-04-01

The paper deals with the impact of annealing on Cu2Se-In3Se2 multilayer structure and discusses the quantum confinements. Thermal evaporation technique was used to prepare multilayer films over the glass substrates. The films were annealed at different temperatures (150 °C-350 °C) under vacuum atmosphere. The XRD pattern reveals that the films exhibit (112) peaks with CuInSe2 Chalcopyrite structure and upon annealing crystallinity improved. The grain size comes around 13-19 nm. The optical band gap value was found to be 2.21 to 2.09 eV and band gap splitting was observed for higher annealing temperatures. The increase in the band gap is related to quantum confinement effect. SEM image shows nano crystals spread over the entire surface for higher annealing temperatures. Optical absorption and PL spectra shows the blue shift during annealing. The HR-TEM shows the particle size in the nano range and which confirms the CuInSe2 nanocrystal formation. AFM image shows the rough surface with homogenous grains for the as deposited films and smooth surface for annealed films.
Simulation model of erosion and deposition on a barchan dune

NASA Technical Reports Server (NTRS)

Howard, A. D.; Morton, J. B.; Gal-El-hak, M.; Pierce, D. B.

1977-01-01

Erosion and deposition over a barchan dune near the Salton Sea, California, are modeled by bookkeeping the quantity of sand in saltation following streamlines of transport. Field observations of near surface wind velocity and direction plus supplemental measurements of the velocity distribution over a scale model of the dune are combined as input to Bagnold type sand transport formulas corrected for slope effects. A unidirectional wind is assumed. The resulting patterns of erosion and deposition compare closely with those observed in the field and those predicted by the assumption of equilibrium (downwind translation of the dune without change in size or geometry). Discrepancies between the simulated results and the observed or predicted erosional patterns appear to be largely due to natural fluctuations in the wind direction. The shape of barchan dunes is a function of grain size, velocity, degree of saturation of the oncoming flow, and the variability in the direction of the oncoming wind. The size of the barchans may be controlled by natural atmospheric scales, by the age of the dunes, or by the upwind roughness. The upwind roughness can be controlled by fixed elements or by sand in the saltation. In the latter case, dune scale is determined by grain size and wind velocity.
Effect of surface roughness on droplet splashing

NASA Astrophysics Data System (ADS)

Hao, Jiguang

2017-12-01

It is well known that rough surfaces trigger prompt splashing and suppress corona splashing on droplet impact. Upon water droplet impact, we experimentally found that a slightly rough substrate triggers corona splashing which is suppressed to prompt splashing by both further increase and further decrease of surface roughness. The nonmonotonic effect of surface roughness on corona splashing weakens with decreasing droplet surface tension. The threshold velocities for prompt splashing and corona splashing are quantified under different conditions including surface roughness, droplet diameter, and droplet surface tension. It is determined that slight roughness significantly enhances both prompt splashing and corona splashing of a water droplet, whereas it weakly affects low-surface-tension droplet splashing. Consistent with previous studies, high roughness triggers prompt splashing and suppresses corona splashing. Further experiments on droplet spreading propose that the mechanism of slight roughness enhancing water droplet splashing is due to the decrease of the wetted area with increasing surface roughness.
Characterization of LANDSAT-4 TM and MSS Image Quality for Interpretation of Agricultural and Forest Resources

NASA Technical Reports Server (NTRS)

Degloria, S. D.; Colwell, R. N.

1984-01-01

Systematic analysis of both image and numeric data shows that the overall spectral, spatial, and radiometric quality of the TM data are excellent. Spectral variations in fallow fields are due to the vaiability in soil moisture and surface roughness resulting from the various stages of field preparation for small grains production. Spectrally, the addition of the first TM short wave infrared band (Band 5) significantly enhanced ability to discriminate different crop types. Bands 1, 5, and 6 contain saturated pixels due to high albedo effects, low moisture conditions, and high radiant temperatures of granite and dry, bare soil on south facing slopes, respectively. Spatially, the two fold decrease in interpixel distance and four fold decrease in area per pixel between the TM and MSS allow for improved discrimination of small fields, boundary conditions, road and stream networks in rough terrain, and small forest clearings resulting from various forest management practices.
Friction force microscopy: a simple technique for identifying graphene on rough substrates and mapping the orientation of graphene grains on copper

NASA Astrophysics Data System (ADS)

Marsden, A. J.; Phillips, M.; Wilson, N. R.

2013-06-01

At a single atom thick, it is challenging to distinguish graphene from its substrate using conventional techniques. In this paper we show that friction force microscopy (FFM) is a simple and quick technique for identifying graphene on a range of samples, from growth substrates to rough insulators. We show that FFM is particularly effective for characterizing graphene grown on copper where it can correlate the graphene growth to the three-dimensional surface topography. Atomic lattice stick-slip friction is readily resolved and enables the crystallographic orientation of the graphene to be mapped nondestructively, reproducibly and at high resolution. We expect FFM to be similarly effective for studying graphene growth on other metal/locally crystalline substrates, including SiC, and for studying growth of other two-dimensional materials such as molybdenum disulfide and hexagonal boron nitride.

Lacunarity study of speckle patterns produced by rough surfaces

NASA Astrophysics Data System (ADS)

Dias, M. R. B.; Dornelas, D.; Balthazar, W. F.; Huguenin, J. A. O.; da Silva, L.

2017-11-01

In this work we report on the study of Lacunarity of digital speckle patterns generated by rough surfaces. The study of Lacunarity of speckle patterns was performed on both static and moving rough surfaces. The results show that the Lacunarity is sensitive to the surface roughness, which suggests that it can be used to perform indirect measurement of surface roughness as well as to monitor defects, or variations of roughness, of metallic moving surfaces. Our results show the robustness of this statistical tool applied to speckle pattern in order to study surface roughness.
Relative roughness controls on incipient sediment motion in steep channels

NASA Astrophysics Data System (ADS)

Prancevic, J.; Lamb, M. P.; Fuller, B. M.

2012-12-01

For over eight decades, researchers have noted an appreciable increase in the nondimensional shear stress (Shields number) at initiation of fluvial bedload transport with increasing bed slope. The precise cause of the trend, however, is obscured by the covariance of several factors with increased slope: a greater downstream component of the gravity acting on the grains and fluid, changes in bed morphology, increased grainsize relative to the channel width that may lead to grain bridging, and increased grainsize relative to flow depth (relative roughness) that may change flow hydraulics and particle buoyancy. Here, we report on ongoing laboratory experiments spanning a wide range of bed slopes (2% to 67%) designed to isolate these variables and determine the true cause of heightened critical Shields numbers on steep slopes. First, we eliminated bed morphology as a factor by using only planar beds. To investigate the effect of grain bridging, we used two different channel widths, representing width-to-grainsize ratios of 23:1 and 9:1. Finally, to separate the effects of slope from relative roughness, we compared incipient motion conditions for acrylic particles (submerged specific gravity of 0.15) to natural siliciclastic gravel (submerged specific gravity of 1.65). Different particle densities allowed us to explore incipient motion as a function of relative roughness, independent of channel slope, because lighter particles move at shallower flow depths than heavier ones of the same size. Results show that both materials exhibit a positive trend between bed slope and critical Shields number despite the existence of planar beds for all slopes. Furthermore, changing the grainsize-to-width ratio had a negligible effect on this trend. For all slopes, the critical Shields number for bedload transport was higher for the acrylic particles than for gravel, indicating that relative roughness has a strong control on incipient sediment motion independent of channel slope. These results are consistent with a simple force balance model that considers the effect of relative roughness on flow hydraulics and particle buoyancy, and neglects grain bridging and particle wedging. Together, our results indicate that heightened critical Shields number on steep planar beds is fundamentally due to the increase in relative roughness with increasing slope at the onset of sediment motion.
Effect of Sn Content in a CuSnZn Metal Precursor on Formation of MoSe2 Film during Selenization in Se+SnSe Vapor

PubMed Central

Yao, Liyong; Ao, Jianping; Jeng, Ming-Jer; Bi, Jinlian; Gao, Shoushuai; Sun, Guozhong; He, Qing; Zhou, Zhiqiang; Sun, Yun; Chang, Liann-Be

2016-01-01

The preparation of Cu2ZnSnSe4 (CZTSe) thin films by the selenization of an electrodeposited copper–tin–zinc (CuSnZn) precursor with various Sn contents in low-pressure Se+SnSex vapor was studied. Scanning electron microscope (SEM) and energy dispersive spectroscopy (EDS) measurements revealed that the Sn content of the precursor that is used in selenization in a low-pressure Se+SnSex vapor atmosphere only slightly affects the elemental composition of the formed CZTSe films. However, the Sn content of the precursor significantly affects the grain size and surface morphology of CZTSe films. A metal precursor with a very Sn-poor composition produces CZTSe films with large grains and a rough surface, while a metal precursor with a very Sn-rich composition procures CZTSe films with small grains and a compact surface. X-ray diffraction (XRD) and SEM revealed that the metal precursor with a Sn-rich composition can grow a thicker MoSe2 thin film at CZTSe/Mo interface than one with a Sn-poor composition, possibly because excess Sn in the precursor may catalyze the formation of MoSe2 thin film. A CZTSe solar cell with an efficiency of 7.94%was realized by using an electrodeposited metal precursor with a Sn/Cu ratio of 0.5 in selenization in a low-pressure Se+SnSex vapor. PMID:28773366
Evaluation of Advanced Reactive Surface Area Estimates for Improved Prediction of Mineral Reaction Rates in Porous Media

NASA Astrophysics Data System (ADS)

Beckingham, L. E.; Mitnick, E. H.; Zhang, S.; Voltolini, M.; Yang, L.; Steefel, C. I.; Swift, A.; Cole, D. R.; Sheets, J.; Kneafsey, T. J.; Landrot, G.; Anovitz, L. M.; Mito, S.; Xue, Z.; Ajo Franklin, J. B.; DePaolo, D.

2015-12-01

CO2 sequestration in deep sedimentary formations is a promising means of reducing atmospheric CO2 emissions but the rate and extent of mineral trapping remains difficult to predict. Reactive transport models provide predictions of mineral trapping based on laboratory mineral reaction rates, which have been shown to have large discrepancies with field rates. This, in part, may be due to poor quantification of mineral reactive surface area in natural porous media. Common estimates of mineral reactive surface area are ad hoc and typically based on grain size, adjusted several orders of magnitude to account for surface roughness and reactivity. This results in orders of magnitude discrepancies in estimated surface areas that directly translate into orders of magnitude discrepancies in model predictions. Additionally, natural systems can be highly heterogeneous and contain abundant nano- and micro-porosity, which can limit connected porosity and access to mineral surfaces. In this study, mineral-specific accessible surface areas are computed for a sample from the reservoir formation at the Nagaoka pilot CO2 injection site (Japan). Accessible mineral surface areas are determined from a multi-scale image analysis including X-ray microCT, SEM QEMSCAN, XRD, SANS, and SEM-FIB. Powder and flow-through column laboratory experiments are performed and the evolution of solutes in the aqueous phase is tracked. Continuum-scale reactive transport models are used to evaluate the impact of reactive surface area on predictions of experimental reaction rates. Evaluated reactive surface areas include geometric and specific surface areas (eg. BET) in addition to their reactive-site weighted counterparts. The most accurate predictions of observed powder mineral dissolution rates were obtained through use of grain-size specific surface areas computed from a BET-based correlation. Effectively, this surface area reflects the grain-fluid contact area, or accessible surface area, in the powder dissolution experiment. In the model of the flow-through column experiment, the accessible mineral surface area, computed from the multi-scale image analysis, is evaluated in addition to the traditional surface area estimates.
Enhancement of Electrical Properties of Nanostructured Polysilicon Layers Through Hydrogen Passivation.

PubMed

Zhou, D; Xu, T; Lambert, Y; Cristini-Robbe; Stiévenard, D

2015-12-01

The light absorption of polysilicon planar junctions can be improved using nanostructured top surfaces due to their enhanced light harvesting properties. Nevertheless, associated with the higher surface, the roughness caused by plasma etching and defects located at the grain boundary in polysilicon, the concentration of the recombination centers increases, leading to electrical performance deterioration. In this work, we demonstrate that wet oxidation combined with hydrogen passivation using SiN(x):H are the key technological processes to significantly decrease the surface recombination and improve the electrical properties of nanostructured n(+)-i-p junctions. Nanostructured surface is fabricated by nanosphere lithography in a low-cost and controllable approach. Furthermore, it has been demonstrated that the successive annealing of silicon nitride films has significant effect on the passivation quality, resulting in some improvements on the efficiency of the Si nanostructure-based solar cell device.
Surface analysis of Fe-Co-Mo electrolytic coatings

NASA Astrophysics Data System (ADS)

Yar-Mukhamedova, G. Sh; Sakhnenko, N. D.; Ved', M. V.; Yermolenko, I. Yu; Zyubanova, S. I.

2017-06-01

Coatings Fe-Co-Mo with a composition of 47 at.% iron, 28 at.% Cobalt and 25 at.% Molybdenum were deposited from citrate electrolyte using pulse electrolysis mode. Scanning electron and atomic force microscopy have established the surface morphology and topography. It was identified the parts with a globular structure which have an average size of 0.2-0.5μm and singly located sharp grains. Within the same scan area sites with developed surface were detected the topography of which is identical to the crystal structure of cobalt with the crystallites size of 0.2-1.75μm. The parameters Ra and Rq for parts with different morphology as well as average characteristics of coatings demonstrated the low roughness of the surface. It is found that the coercive force of Fe-Co-Mo films is 7-10 Oe, which allow us to classify the Fe-Co-Mo coatings as soft magnetic materials.
Surface roughness: A review of its measurement at micro-/nano-scale

NASA Astrophysics Data System (ADS)

Gong, Yuxuan; Xu, Jian; Buchanan, Relva C.

2018-01-01

The measurement of surface roughness at micro-/nano-scale is of great importance to metrological, manufacturing, engineering, and scientific applications given the critical roles of roughness in physical and chemical phenomena. The surface roughness of materials can significantly change the way of how they interact with light, phonons, molecules, and so forth, thus surface roughness ultimately determines the functionality and property of materials. In this short review, the techniques of measuring micro-/nano-scale surface roughness are discussed with special focus on the limitations and capabilities of each technique. In addition, the calculations of surface roughness and their theoretical background are discussed to offer readers a better understanding of the importance of post-measurement analysis. Recent progress on fractal analysis of surface roughness is discussed to shed light on the future efforts in surface roughness measurement.
Were lakes on early Mars perennially were ice-covered?

NASA Astrophysics Data System (ADS)

Sumner, D. Y.; Rivera-Hernandez, F.; Mackey, T. J.

2016-12-01

Paleo-lake deposits indicate that Mars once sustained liquid water, supporting the idea of an early "wet and warm" Mars. However, liquid water can be sustained under ice in cold conditions as demonstrated by perennially ice-covered lakes (PICLs) in Antarctica. If martian lakes were ice-covered, the global climate on early Mars could have been much colder and dryer than if the atmosphere was in equilibrium with long-lived open water lakes. Modern PICLs on Earth have diagnostic sedimentary features. Unlike open water lakes that are dominated by mud, and drop stones or tills if icebergs are present, previous studies determined that deposits in PICLs can include coarser grains that are transported onto the ice cover, where they absorb solar radiation, melt through the ice and are deposited with lacustrine muds. In Lake Hoare, Antarctica, these coarse grains form conical sand mounds and ridges. Our observations of ice-covered lakes Joyce, Fryxell, Vanda and Hoare, Antarctica suggest that the distributions of grains depend significantly on ice characteristics. Deposits in these lakes contain moderately well to moderately sorted medium to very coarse sand grains, which preferentially melt through the ice whereas granules and larger grains remain on the ice surface. Similarly, high albedo grains are concentrated on the ice surface, whereas low albedo grains melt deeper into the ice, demonstrating a segregation of grains due to ice-sediment interactions. In addition, ice cover thickness may determine the spatial distribution of sand deposited in PICLs. Localized sand mounds and ridges composed of moderately sorted sand are common in PICLs with rough ice covers greater than 3 m thick. In contrast, lakes with smooth and thinner ice have disseminated sand grains and laterally extensive sand layers but may not have sand mounds. At Gale Crater, Mars, the Murray formation consists of sandy lacustrine mudstones, but the depositional process for the sand is unknown. The presence of a perennial ice-cover could explain the sand, but no definitive ice-related deposits have been identified to date. The Murray formation is an ideal target to start analyzing for evidence of ancient PICL deposits on Mars.
NASA Astrophysics Data System (ADS)

Wang, Mao-Hua; Ma, Xiao-Yu; Zhang, Bo; Zhou, Fu

2014-11-01

CaCu3Ti4O12 (CCTO) powders coated with carbon were synthesized by using a high-energy ball milling method. The obtained samples were characterized by x-ray diffraction, transmission electron microscopy and scanning electron microscopy. The carbon-coated CCTO particles had a rough surface, which resulted from the growth of the carbon coating on the CCTO particles. It was found that the CCTO phase was observed as the major phase and no reaction occurred between the carbon and CCTO during the sintering process. The grain size of the CCTO ceramics decreased with the increase in carbon content, which indicated that carbon inhibits grain growth of CCTO ceramics. Specially, the dielectric constant decreased with the increase in carbon content. And CCTO1 ceramic (mass ratio of CCTO: carbon = 10:1) showed a lower dielectric constant (3.74 × 104), with the dielectric loss value (0.04) much lower than that of CCTO at 20°C (10 k Hz).
The frictional properties of a simulated gouge having a fractal particle distribution

USGS Publications Warehouse

Biegel, R.L.; Sammis, C.G.; Dieterich, J.H.

1989-01-01

The frictional properties of a layer of simulated Westerly granite fault gouge sandwiched between sliding blocks of Westerly granite have been measured in a high-speed servo-controlled double-direct shear apparatus. Most gouge layers were prepared to have a self-similar particle distribution with a fractal dimension of 2.6. The upper fractal limit was varied between 45 and 710 ??m. Some gouges were prepared with all particles in the range between 360 and 710 ??m. In each experiment the sliding velocity was cyclically alternated between 1 and 10 ??ms-1 and the coefficient of friction ??m and its transient parameters a, b and Dc were measured as functions of displacement. In addition to the particle size distribution, the following experimental variables were also investigated: the layer thickness (1 and 3 mm), the roughness of the sliding surfaces (Nos 60 and 600 grit) and the normal stress (10 and 25 MPa). Some of the sample assemblies were epoxy impregnated following a run so the gouge structure could be microscopically examined in thin section. We observed that gouges which were initially non-fractal evolved to a fractal distribution with dimension 2.6. Gouges which had an initial fractal distribution remained fractal. When the sliding blocks had smooth surfaces, the coefficient of friction was relatively low and was independent of the particle distribution. In these cases, strong velocity weakening was observed throughout the experiment and the transient parameters a, b and Dc, remained almost constant. When the sliding blocks had rough surfaces, the coefficient of friction was larger and more dependent on the particle distribution. Velocity strengthening was observed initially but evolved to velocity weakening with increased sliding displacement. All three transient parameters changed with increasing displacement. The a and b values were about three times as large for rough surfaces as for smooth. The characteristic displacement Dc was not sensitive to surface roughness but was the only transient parameter which was sensitive to the normal stress. For the case of rough surfaces, the coefficient of friction of the 1 mm thick gouge was significantly larger than that for the 3 mm thick layers. Many of these observations can be explained by a micromechanical model in which the stress in the gouge layer is heterogeneous. The applied normal and shear stresses are supported by 'grain bridges' which span the layer and which are continually forming and failing. In this model, the frictional properties of the gouge are largely determined by the dominant failure mode of the bridging structures. ?? 1989.
Identification of quantitative trait loci for grain quality in an advanced backcross population derived from the Oryza sativa variety IR64 and the wild relative O. rufipogon.

PubMed

Septiningsih, E M; Trijatmiko, K R; Moeljopawiro, S; McCouch, S R

2003-11-01

The objective of this study was to identify quantitative trait loci (QTLs) associated with grain quality in rice. Two hundred eighty-five BC(2)F(2 )families developed from an interspecific cross between cv IR64 and Oryza rufipogon (IRGC 105491) were evaluated for 14 seed quality traits. A total of 165 markers consisting of 131 single sequence repeats and 34 restriction fragment length polymorphism markers were used to create a genetic linkage map spanning the 12 rice chromosomes. Twenty-three independent QTLs were identified using single point analysis, interval mapping, and composite interval mapping. These loci consisted of one QTL for filled rough/total rough rice ratio, two for grain density, one for percentage of de-husked rice grains, two for percentage of green rice grains, three for percentage of damaged-yellow rice grains, two for percentage of red rice grains, one for milled rice recovery, three for head rice recovery, four for broken rice grains, two for crushed rice grains, one for amylose content, and one for gel consistency. For most of the QTLs identified in this study, the O. rufipogon-derived allele contributed an undesirable effect. For amylose content and gel consistency, the O. rufipogon allele may be useful in an IR64 background, depending on the cultural preferences of the consumer. Careful selection against the regions associated with negative effects will be required to avoid unwanted grain quality characteristics during the development of improved varieties for yield and yield components using introgressions from O. rufipogon.
Surface Roughness of the Moon Derived from Multi-frequency Radar Data

NASA Astrophysics Data System (ADS)

Fa, W.

2011-12-01

Surface roughness of the Moon provides important information concerning both significant questions about lunar surface processes and engineering constrains for human outposts and rover trafficabillity. Impact-related phenomena change the morphology and roughness of lunar surface, and therefore surface roughness provides clues to the formation and modification mechanisms of impact craters. Since the Apollo era, lunar surface roughness has been studied using different approaches, such as direct estimation from lunar surface digital topographic relief, and indirect analysis of Earth-based radar echo strengths. Submillimeter scale roughness at Apollo landing sites has been studied by computer stereophotogrammetry analysis of Apollo Lunar Surface Closeup Camera (ALSCC) pictures, whereas roughness at meter to kilometer scale has been studied using laser altimeter data from recent missions. Though these studies shown lunar surface roughness is scale dependent that can be described by fractal statistics, roughness at centimeter scale has not been studied yet. In this study, lunar surface roughnesses at centimeter scale are investigated using Earth-based 70 cm Arecibo radar data and miniature synthetic aperture radar (Mini-SAR) data at S- and X-band (with wavelengths 12.6 cm and 4.12 cm). Both observations and theoretical modeling show that radar echo strengths are mostly dominated by scattering from the surface and shallow buried rocks. Given the different penetration depths of radar waves at these frequencies (< 30 m for 70 cm wavelength, < 3 m at S-band, and < 1 m at X-band), radar echo strengths at S- and X-band will yield surface roughness directly, whereas radar echo at 70-cm will give an upper limit of lunar surface roughness. The integral equation method is used to model radar scattering from the rough lunar surface, and dielectric constant of regolith and surface roughness are two dominate factors. The complex dielectric constant of regolith is first estimated globally using the regolith composition and the relation among the dielectric constant, bulk density, and regolith composition. The statistical properties of lunar surface roughness are described by the root mean square (RMS) height and correlation length, which represent the vertical and horizontal scale of the roughness. The correlation length and its scale dependence are studied using the topography data from laser altimeter observations from recent lunar missions. As these two parameters are known, surface roughness (RMS slope) can be estimated by minimizing the difference between the observed and modeled radar echo strength. Surface roughness of several regions over Oceanus Procellarum and southeastern highlands on lunar nearside are studied, and preliminary results show that maira is smoother than highlands at 70 cm scale, whereas the situation turns opposite at 12 and 4 cm scale. Surface roughness of young craters is in general higher than that of maria and highlands, indicating large rock population produced during impacting process.
The VHCF experimental investigation of FV520B-I with surface roughness Ry

NASA Astrophysics Data System (ADS)

Wang, J. L.; Zhang, Y. L.; Ding, M. C.; Zhao, Q. C.

2018-05-01

Different surface roughness type (Ra and Ry) has different effect on the VHCF failure and life. Ra is widely employed as the quantitative expression of the surface roughness, but there are few fatigue failure mechanism analysis and experimental study under surface roughness Ry. The VHCF experiment is conducted out using the specimen with different surface roughness values. The surface roughness Ry is employed as the major research object to investigate the relationship and distribution tendency between the Ry, fatigue life and the distance between internal inclusion and surface, and a new VHCF failure character is proposed.
Smoothed particle hydrodynamics study of the roughness effect on contact angle and droplet flow

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shigorina, Elena; Kordilla, Jannes; Tartakovsky, Alexandre M.

We employ a pairwise force Smoothed Particle Hydrodynamics (PF-SPH) model to simulate sessile and transient droplets on rough hydrophobic and hydrophilic surfaces. PF-SPH allows for modeling of free surface flow without discretizing the air phase, which is achieved by imposing the surface tension and dynamic contact angles with pairwise interaction forces. We use the PF-SPH model to study the effect of surface roughness and microscopic contact angle on the effective contact angle and droplet dynamics. In the first part of this work, we investigate static contact angles of sessile droplets on rough surfaces in a shape of a sinusoidal functionmore » and made of rectangular bars placed on top of a flat surface. We find that the effective static contact angles of Cassie and Wenzel droplets on a rough surface are greater than the corresponding microscale static contact angles. As a result, microscale hydrophobic rough surfaces also show effective hydrophobic behavior. On the other hand, microscale hydrophilic surfaces may be macroscopically hydrophilic or hydrophobic, depending on the type of roughness. Next, we study the impact of the roughness orientation (i.e., an anisotropic roughness) and surface inclination on droplet flow velocities. Simulations show that droplet flow velocities are lower if the surface roughness is oriented perpendicular to the flow direction. If the predominant elements of surface roughness are in alignment with the flow direction, the flow velocities increase compared to smooth surfaces, which can be attributed to the decrease in fluid-solid contact area similar to the classical lotus effect. We demonstrate that linear scaling relationships between Bond and capillary number for droplet flow on flat surfaces also hold for flow on rough surfaces.« less
Role of rough surface topography on gas slip flow in microchannels.

PubMed

Zhang, Chengbin; Chen, Yongping; Deng, Zilong; Shi, Mingheng

2012-07-01

We conduct a lattice Boltzmann simulation of gas slip flow in microchannels incorporating rough surface effects as characterized by fractal geometry with a focus on gas-solid interaction. The gas slip flow in rough microchannels, which is characterized by Poiseuille number and mass flow rate, is evaluated and compared with smooth microchannels. The effects of roughness height, surface fractal dimension, and Knudsen number on slip behavior of gas flow in microchannels are all investigated and discussed. The results indicate that the presence of surface roughness reduces boundary slip for gas flow in microchannels with respect to a smooth surface. The gas flows at the valleys of rough walls are no-slip while velocity slips are observed over the top of rough walls. We find that the gas flow behavior in rough microchannels is insensitive to the surface topography irregularity (unlike the liquid flow in rough microchannels) but is influenced by the statistical height of rough surface and rarefaction effects. In particular, decrease in roughness height or increase in Knudsen number can lead to large wall slip for gas flow in microchannels.
75 FR 56911 - Request for Public Comment on the United States Standards for Rough Rice, Brown Rice for...

Federal Register 2010, 2011, 2012, 2013, 2014

2010-09-17

... DEPARTMENT OF AGRICULTURE Grain Inspection, Packers and Stockyards Administration 7 CFR Part 868... Department of Agriculture's (USDA) Grain Inspection, Packers, and Stockyards Administration (GIPSA) is... Milled Rice under the Agriculture Marketing Act of 1946 (AMA). Since the standards were last revised...
Nutritional quality of eggs from hens fed distillers' dried grains with solubles

USDA-ARS?s Scientific Manuscript database

Distiller grains with soluble (DDGS) have roughly three times the amount of oil as regular corn used in feeds, and several studies have shown that DDGS also have higher concentrations of lipophilic bioactives such as tocopherols, tocotrienols, and xanthophylls, because the levels found in whole corn...
Investigation of laser ablation of CVD diamond film

NASA Astrophysics Data System (ADS)

Chao, Choung-Lii; Chou, W. C.; Ma, Kung-Jen; Chen, Ta-Tung; Liu, Y. M.; Kuo, Y. S.; Chen, Ying-Tung

2005-04-01

Diamond, having many advanced physical and mechanical properties, is one of the most important materials used in the mechanical, telecommunication and optoelectronic industry. However, high hardness value and extreme brittleness have made diamond extremely difficult to be machined by conventional mechanical grinding and polishing. In the present study, the microwave CVD method was employed to produce epitaxial diamond films on silicon single crystal. Laser ablation experiments were then conducted on the obtained diamond films. The underlying material removal mechanisms, microstructure of the machined surface and related machining conditions were also investigated. It was found that during the laser ablation, peaks of the diamond grains were removed mainly by the photo-thermal effects introduced by excimer laser. The diamond structures of the protruded diamond grains were transformed by the laser photonic energy into graphite, amorphous diamond and amorphous carbon which were removed by the subsequent laser shots. As the protruding peaks gradually removed from the surface the removal rate decreased. Surface roughness (Ra) was improved from above 1μm to around 0.1μm in few minutes time in this study. However, a scanning technique would be required if a large area was to be polished by laser and, as a consequence, it could be very time consuming.
Role of substrate in the surface diffusion and kinetic roughening of nanocrystallised nickel electrodeposits

NASA Astrophysics Data System (ADS)

Nzoghe-Mendome, L.; Aloufy, A.; Ebothé, J.; El Messiry, M.; Hui, D.

2009-02-01

The surface growth and roughening of nano-crystallised Ni electrodeposits prepared at the same conditions have been studied on Cu, Au and ITO substrates. The Ni films obtained are characterised by the same face-centred cubic structure with a texture affected by the substrate chemical nature. Practically, the same small-sized grains of 83 nm mean height depicting a statistical mono-mode feature grow on Cu. A three-modal feature corresponding to the biggest and compact crystallites of 335, 368 and 400 nm mean height is obtained with Au. Two typical modes, respectively, linked to isolated big crystallites of 343 nm mean height and large zones of small grains of 170 nm height, result from the ITO effect. The surface transport properties of Ni ad-atoms on each substrate have been studied from the theoretical approach including the film global roughness measured by AFM. It is shown that the ad-atom diffusion coefficients ( D s) ranged in the interval 10 -10-10 -9 cm 2 s -1 are greatly affected by the non-equilibrium conditions of the film formation. Cu and ITO, respectively, lead to Λ s=11.92 and 14.30 nm, while the higher D s value and diffusion length Λ s=37.32 nm are obtained with Au substrate.
Study of thickness dependent sputtering in gold thin films by swift heavy ion irradiation

NASA Astrophysics Data System (ADS)

Dash, P.; Sahoo, P. K.; Solanki, V.; Singh, U. B.; Avasthi, D. K.; Mishra, N. C.

2015-12-01

Gold thin films of varying thickness (10-100 nm) grown on silica substrates by e-beam evaporation method were irradiated by 120 MeV Au ions at 3 × 1012 and 1 × 1013 ions cm-2 fluences. Irradiation induced modifications of these films were probed by glancing angle X-ray diffraction (GAXRD), atomic force microscopy (AFM), Rutherford backscattering spectrometry (RBS) and surface enhanced Raman scattering (SERS). Irradiation didn't affect the structure, the lattice parameter or the crystallite size, but modified the texturing of grains from [1 1 1] to [2 2 0]. RBS indicated thickness dependent sputtering on irradiation. The sputtering yield was found to decrease with increasing thickness. AFM indicated increase of roughness with increasing irradiation fluence for films of all thickness. In agreement with the AFM observation, the gold nanostructures on the surface of 20 nm thick film were found to increase the SERS signal of acridine orange dye attached to these structures. The SERS peaks were amplified by many fold with increasing ion fluence. The effect of 120 MeV Au ion irradiation on the grain texture, surface morphology and SERS activity in addition to the thickness dependent sputtering in gold thin films are explained by the thermal spike model of ion-matter interaction.

Surface roughness measurement in the submicrometer range using laser scattering

NASA Astrophysics Data System (ADS)

Wang, S. H.; Quan, Chenggen; Tay, C. J.; Shang, H. M.

2000-06-01

A technique for measuring surface roughness in the submicrometer range is developed. The principle of the method is based on laser scattering from a rough surface. A telecentric optical setup that uses a laser diode as a light source is used to record the light field scattered from the surface of a rough object. The light intensity distribution of the scattered band, which is correlated to the surface roughness, is recorded by a linear photodiode array and analyzed using a single-chip microcomputer. Several sets of test surfaces prepared by different machining processes are measured and a method for the evaluation of surface roughness is proposed.
Optical properties of nanocrystalline Y2O3 thin films grown on quartz substrates by electron beam deposition

NASA Astrophysics Data System (ADS)

Wiktorczyk, Tadeusz; Biegański, Piotr; Serafińczuk, Jarosław

2016-09-01

Yttrium oxide thin films of a thickness 221-341 nm were formed onto quartz substrates by reactive physical vapor deposition in an oxygen atmosphere. An electron beam gun was applied as a deposition source. The effect of substrate temperature during film deposition (in the range of 323-673 K) on film structure, surface morphology and optical properties was investigated. The surface morphology studies (with atomic force microscopy and diffuse spectra reflectivity) show that the film surface was relatively smooth with RMS surface roughness in the range of 1.7-3.8 nm. XRD analysis has revealed that all diffraction lines belong to a cubic Y2O3 structure. The films consisted of small nanocrystals. Their average grain size increases from 1.6 nm to 22 nm, with substrate temperature rising from 323 K to 673 K. Optical examinations of transmittance and reflectance were performed in the spectral range of 0.2-2.5 μm. Optical constants and their dispersion curves were determined. Values of the refractive index of the films were in the range of n = 1.79-1.90 (at 0.55 μm) for substrate temperature during film deposition of 323-673 K. The changes in the refractive index upon substrate temperature correspond very well with the increase in the nanocrystals grain diameter and with film porosity.
Influence of Roughness-Induced Slip on Colloid Transport: Experimental and Modelling Insights

NASA Astrophysics Data System (ADS)

Rasmuson, J. A.; Johnson, W. P.

2017-12-01

A limitation of classic colloid filtration theory is that it applies only to smooth surfaces, yet most natural surfaces present some degree of nano- to micro-scale roughness. A large volume of research has been dedicated to understanding the effects of roughness on particle attachment at the nano-scale since these interactions dictate field scale transport behavior. It has been previously demonstrated that roughness imposes a finite slip vector at the surface that causes particles to experience higher near-surface velocities than would be expected over a smooth surface. Slip near a rough surface can affect two primary mechanisms of particle attenuation: 1) interception of the surface (finding a landing spot) and 2) arrest on the surface (sticking the landing). However, a clear designation on how slip affects particle transport near rough surfaces is missing. The goal of this study was to provide a guide for the height of the slip layer and contact surface in reference to the mean-plane for rough surfaces. Direct observation was used to measure near-surface velocities of particles translating near surfaces of varying roughness spanning three orders of magnitude. The influence of roughness on particle transport was investigated using computational fluid dynamics (CFD) modeling with rough surfaces measured with atomic force microscopy (AFM). The CFD and experimental results were used to calibrate a Lagrangian particle transport model that utilizes simple modifications to the flow field for a smooth surface using statistically based roughness parameters. Advantages of the Lagrangian model are significantly decreased computation times and applicability to a wide range of natural surfaces without explicitly simulating individual asperities. The results suggest that the no-slip boundary should be placed at the bottom of the maximum asperity valleys, and that the contact surface should be placed at the root mean square (RMS) roughness above the mean plane. Collector surfaces with the greatest RMS roughness had the highest sensitivity to the placement of the contact surface. These findings highlight the need for accurate and representative AFM measurements and have important implications for future transport models.
Optical properties and surface topography of CdCl2 activated CdTe thin films

NASA Astrophysics Data System (ADS)

Patel, S. L.; Purohit, A.; Chander, S.; Dhaka, M. S.

2018-05-01

The effect of post-CdCl2 heat treatment on optical properties and surface topography of evaporated CdTe thin films is investigated. The pristine and thermally annealed films were subjected to UV-Vis spectrophotometer and atomic force microscopy (AFM) to investigate the optical properties and surface topography, respectively. The absorbance is found to be maximum (˜90%) at 320°C temperature and transmittance found to be minimum and almost constant in ultraviolet and visible regions. The direct band gap is increased from 1.42 eV to 2.12 eV with post-CdCl2 annealing temperature. The surface topography revealed that the uniformity is improved with annealing temperature and average surface roughness is found in the range of 83.3-144.3 nm as well as grains have cylindrical hill-like shapes. The investigated results indicate that the post-CdCl2 treated films annealed at 320°C may be well-suitable for thin film solar cells as an absorber layer.
Understanding EUV mask blank surface roughness induced LWR and associated roughness requirement

NASA Astrophysics Data System (ADS)

Yan, Pei-Yang; Zhang, Guojing; Gullikson, Eric M.; Goldberg, Ken A.; Benk, Markus P.

2015-03-01

Extreme ultraviolet lithography (EUVL) mask multi-layer (ML) blank surface roughness specification historically comes from blank defect inspection tool requirement. Later, new concerns on ML surface roughness induced wafer pattern line width roughness (LWR) arise. In this paper, we have studied wafer level pattern LWR as a function of EUVL mask surface roughness via High-NA Actinic Reticle Review Tool. We found that the blank surface roughness induced LWR at current blank roughness level is in the order of 0.5nm 3σ for NA=0.42 at the best focus. At defocus of ±40nm, the corresponding LWR will be 0.2nm higher. Further reducing EUVL mask blank surface roughness will increase the blank cost with limited benefit in improving the pattern LWR, provided that the intrinsic resist LWR is in the order of 1nm and above.
Research of Surface Roughness Anisotropy

NASA Astrophysics Data System (ADS)

Bulaha, N.; Rudzitis, J.; Lungevics, J.; Linins, O.; Krizbergs, J.

2017-04-01

The authors of the paper have investigated surfaces with irregular roughness for the purpose of determination of roughness spacing parameters perpendicularly to machining traces - RSm1 and parallel to them - RSm2, as well as checking the relationship between the surface anisotropy coefficient c and surface aspect ratio Str from the standard LVS EN ISO 25178-2. Surface roughness measurement experiments with 11 surfaces show that measuring equipment values of mean spacing of profile irregularities in the longitudinal direction are not reliable due to the divergence of surface mean plane and roughness profile mean line. After the additional calculations it was stated that parameter Str can be used for determination of parameter RSm2 and roughness anisotropy evaluation for grinded, polished, friction surfaces and other surfaces with similar characteristics.
Smoothed particle hydrodynamics study of the roughness effect on contact angle and droplet flow.

PubMed

Shigorina, Elena; Kordilla, Jannes; Tartakovsky, Alexandre M

2017-09-01

We employ a pairwise force smoothed particle hydrodynamics (PF-SPH) model to simulate sessile and transient droplets on rough hydrophobic and hydrophilic surfaces. PF-SPH allows modeling of free-surface flows without discretizing the air phase, which is achieved by imposing the surface tension and dynamic contact angles with pairwise interaction forces. We use the PF-SPH model to study the effect of surface roughness and microscopic contact angle on the effective contact angle and droplet dynamics. In the first part of this work, we investigate static contact angles of sessile droplets on different types of rough surfaces. We find that the effective static contact angles of Cassie and Wenzel droplets on a rough surface are greater than the corresponding microscale static contact angles. As a result, microscale hydrophobic rough surfaces also show effective hydrophobic behavior. On the other hand, microscale hydrophilic surfaces may be macroscopically hydrophilic or hydrophobic, depending on the type of roughness. We study the dependence of the transition between Cassie and Wenzel states on roughness and droplet size, which can be linked to the critical pressure for the given fluid-substrate combination. We observe good agreement between simulations and theoretical predictions. Finally, we study the impact of the roughness orientation (i.e., an anisotropic roughness) and surface inclination on droplet flow velocities. Simulations show that droplet flow velocities are lower if the surface roughness is oriented perpendicular to the flow direction. If the predominant elements of surface roughness are in alignment with the flow direction, the flow velocities increase compared to smooth surfaces, which can be attributed to the decrease in fluid-solid contact area similar to the lotus effect. We demonstrate that classical linear scaling relationships between Bond and capillary numbers for droplet flow on flat surfaces also hold for flow on rough surfaces.
Non-linear boundary-layer receptivity due to distributed surface roughness

NASA Technical Reports Server (NTRS)

Amer, Tahani Reffet

1995-01-01

The process by which a laminar boundary layer internalizes the external disturbances in the form of instability waves is known as boundary-layer receptivity. The objective of the present research was to determine the effect of acoustic excitation on boundary-layer receptivity for a flat plate with distributed variable-amplitude surface roughness through measurements with a hot-wire probe. Tollmien-Schlichting mode shapes due to surface roughness receptivity have also been determined, analyzed, and shown to be in agreement with theory and other experimental work. It has been shown that there is a linear relationship between the surface roughness and receptivity for certain roughness configurations with constant roughness wavelength. In addition, strong non-linear receptivity effects exist for certain surface roughness configurations over a band where the surface roughness and T-S wavelength are matched. The results from the present experiment follow the trends predicted by theory and other experimental work for linear receptivity. In addition, the results show the existence of non-linear receptivity effects for certain combinations of surface roughness elements.
Role of urban surface roughness in road-deposited sediment build-up and wash-off

NASA Astrophysics Data System (ADS)

Zhao, Hongtao; Jiang, Qian; Xie, Wenxia; Li, Xuyong; Yin, Chengqing

2018-05-01

Urban road surface roughness is one of the most important factors in estimation of surface runoff loads caused by road-deposited sediment (RDS) wash-off and design of its control measures. However, because of a lack of experimental data to distinguish the role of surface roughness, the effects of surface roughness on RDS accumulation and release are not clear. In this study, paired asphalt and concrete road surfaces and rainfall simulation designs were used to distinguish the role of surface roughness in RDS build-up and wash-off. Our results showed that typical asphalt surfaces often have higher depression depths than typical concrete surfaces, indicating that asphalt surfaces are relatively rougher than concrete surface. Asphalt surfaces can retain a larger RDS amount, relative higher percentage of coarser particles, larger RDS wash-off loads, and lower wash-off percentage, than concrete surfaces. Surface roughness has different effects in RDS motilities with different particle sizes during rainfall runoff, and the settleable particles (44-149 μm) were notably influenced by it. Furthermore, the first flush phenomenon tended to be greater on relatively smooth surfaces than relatively rough surfaces. Overall, surface roughness plays an important role in influencing the complete process of RDS build-up and wash-off on different road characteristics.
AFM Studies of Lunar Soils and Application to the Mars 2001 Mission

NASA Technical Reports Server (NTRS)

Weitz, C. M.; Anderson, M. S.; Marshall, J.

1999-01-01

The upcoming Mars 01 mission will carry an Atomic Force Microscope (AFM) as part of the Mars Environmental Compatibility Assessment (MECA) instrument. By operating in a tapping mode, the AFM is capable of sub-nanometer resolution in three dimensions and can distinguish between substances of different compositions by employing phase contrast imaging. To prepare for the Mars 01 mission, we are testing the AFM on a lunar soil to determine its ability to define particle shapes and sizes and grain-surface textures. The test materials are from the Apollo 17 soil 79221, which is a mixture of agglutinates, impact and volcanic beads, and mare and highland rock and mineral fragments. The majority of the lunar soil particles are less than 100 microns in size, comparable to the sizes estimated for martian dust. We have used the AFM to examine several different soil particles at various resolutions. The instrument has demonstrated the ability to identify parallel ridges characteristic of twinning on a 150 micron plagioclase feldspar particle. Extremely small (10-100 nanometer) adhering particles are visible on the surface of the feldspar grain, and they appear elongate with smooth surfaces. Phase contrast imaging of the nanometer particles shows several compositions to be present. When the AFM was applied to a 100 micron glass spherule, it was possible to define an extremely smooth surface; this is in clear contrast to results from a basalt fragment which exhibited a rough surface texture. Also visible on the surface of the glass spherule were chains of 100 nanometer and smaller impact melt droplets. For the '01 Mars mission, the AFM is intended to define the size and shape distributions of soil particles, in combination with the NMCA optical microscope system and images from the Robot Arm Camera (RAC). These three data sets will provide a means of assessing potentially hazardous soil and dust properties. The study that we have conducted on the lunar soils now suggests that the NMCA experiment will be able to define grain transport and weathering processes. For example, it should be possible to determine if Martian grains have been subjected to aeolian or water transport, volcanic activity, impact melting processes, in-situ weathering, and a host of other processes. Additionally, textural maturity could be assessed (via freshness and form of fracture patterns and grain shapes). Thus, the AFM has the potential to shed new light on Martian surface processes by adding the submicroscopic dimension to planetary investigations.
Methods for providing ceramic matrix composite components with increased thermal capacity

NASA Technical Reports Server (NTRS)

Steibel, James Dale (Inventor); Utah, David Alan (Inventor)

2001-01-01

A method for enhancing the cooling capability of a turbine component made from a ceramic matrix composite. The method improves the thermal performance of the component by producing a surface having increased cooling capacity, thereby allowing the component to operate at a higher temperature. The method tailors the available surface area on the cooling surface of the composite component by depositing a particulate layer of coarse grained ceramic powders of preselected size onto the surface of the ceramic matrix composite component. The size of the particulate is selectively tailored to match the desired surface finish or surface roughness of the article. The article may be designed to have different surface finishes for different locations, so that the application of different sized powders can provide different cooling capabilities at different locations, if desired. The compositions of the particulates are chemically compatible with the ceramic material comprising the outer surface or portion of the ceramic matrix composite. The particulates are applied using a slurry and incorporated into the article by heating to an elevated temperature without melting the matrix, the particulates or the fiber reinforcement.
Poly-Gaussian model of randomly rough surface in rarefied gas flow

DOE Office of Scientific and Technical Information (OSTI.GOV)

Aksenova, Olga A.; Khalidov, Iskander A.

2014-12-09

Surface roughness is simulated by the model of non-Gaussian random process. Our results for the scattering of rarefied gas atoms from a rough surface using modified approach to the DSMC calculation of rarefied gas flow near a rough surface are developed and generalized applying the poly-Gaussian model representing probability density as the mixture of Gaussian densities. The transformation of the scattering function due to the roughness is characterized by the roughness operator. Simulating rough surface of the walls by the poly-Gaussian random field expressed as integrated Wiener process, we derive a representation of the roughness operator that can be appliedmore » in numerical DSMC methods as well as in analytical investigations.« less
Microstructural investigation of a locally mirror-like surface collected at 4 km depth in a Pomeranian shale sample

NASA Astrophysics Data System (ADS)

Pluymakers, Anne; Renard, Francois

2016-04-01

The presence of shiny sliding surfaces, or mirror surfaces, is sometimes thought to have been caused by slip at seismic velocities. Many fault mirrors reported so far are described to occur in carbonate-rich rocks. Here we present microstructural data on a mirror-like slip surface in the Pomeranian shale, recovered from approximately 4 km depth. The accommodated sliding of this fault is probably small, not more than one or two centimeter. The Pomeranian shale is a dark-grey to black shale, composed of 40-60% illite plus mica, 1-10% organic matter, 10% chlorite, and 10 % carbonates plus minor amounts of K-feldspar, plagioclase and kaolinite. In this sample, the surface is optically smooth with striations and some patches that reflect light. Observations using a Hitachi TM3000 (table-top) SEM show that the striations are omnipresent, though more prominent in the carbonate patches (determined using EDS analysis). The smooth surface is locally covered by granular material with a grain size up to 10 μm. This is shown to consist of a mixture of elements and thus likely locally derived fault gouge. The clay-rich parts of the smooth surface are equidimensional grains, with sub-micron grain sizes, whereas in the unperturbed part of the shale core the individual clay platelets are easy to distinguish, with lengths up to 10 μm. The striated calcite-rich patches appear as single grains with sizes up to several millimeters, though they occasionally are smeared out in a direction parallel to the striations. We have analyzed surface roughness at magnifications of 2.5x to 100x using a standard White Light Interferometer, parallel and perpendicular to slip. At low magnifications, 2.5x and 5x, Hurst exponents were anomalously low, around 0.1 to 0.2, interpreted to be related to a lack of sufficient resolution to pick up the striations. At higher magnification the Hurst exponent is 0.34 to 0.43 parallel to the striation, and 0.44 to 0.61 perpendicular to the striation. This relatively low Hurst exponent suggests that this surface has not experienced high strains, even though it locally exhibits mirror-like properties. As such, this data supports the notion that the formation of shiny surfaces is related to grain size reduction, but does not necessarily indicate major slip events. Additionally, the more strongly visible striation in the carbonate-rich parts indicates that some mineralogies are more prone to the formation of striations than others. A full interpretation of this sample is of course complicated by its small size, but these data suggest that when examining fault mirrors and the presence of striations spatial difference in mineralogy need to be taken into account.
Analogies to Demonstrate the Effect of Roughness on Surface Wettability

ERIC Educational Resources Information Center

Yolcu, Hasan

2017-01-01

This article presents an analogy to illustrate the effect of surface roughness on surface wettability. I used a water-filled balloon to represent water droplet, a toothpick to represent surface roughness and Styrofoam as the surface. The analogies presented in this article will help visualize how roughness affects the wettability of the surface…
Quantifying microbe-mineral interactions leading to remotely detectable induced polarization signals

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ntarlagiannis, Dimitrios; Moysey, Stephen; Dean, Delphine

2013-11-14

The objective of this project was to investigate controls on induced polarization responses in porous media. The approach taken in the project was to compare electrical measurements made on mineral surfaces with atomic force microscopy (AFM) techniques to observations made at the column-scale using traditional spectral induced polarization measurements. In the project we evaluated a number of techniques for investigating the surface properties of materials, including the development of a new AFM measurement protocol that utilizes an external electric field to induce grain-scale polarizations that can be probed using a charged AFM tip. The experiments we performed focused on idealizedmore » systems (i.e., glass beads and silica gel) where we could obtain the high degree of control needed to understand how changes in the pore environment, which are determined by biogeochemical controls in the subsurface, affect mechanisms contributing to complex electrical conductivity, i.e., conduction and polarization, responses. The studies we performed can be classified into those affecting the chemical versus physical properties of the grain surface and pore space. Chemical alterations of the surface focused on evaluating how changes in pore fluid pH and ionic composition control surface conduction. These were performed as column flow through experiments where the pore fluid was exchanged in a column of silica gel. Given that silica gel has a high surface area due to internal grain porosity, high-quality data could be obtained where the chemical influences on the surface are clearly apparent and qualitatively consistent with theories of grain (i.e., Stern layer) polarization controlled by electrostatic surface sorption processes (i.e., triple layer theory). Quantitative fitting of the results by existing process-based polarization models (e.g., Leroy et al., 2008) has been less successful, however, due to what we have attributed to differences between existing models developed for spherical grains versus the actual geometry associated with the nano-pores in the silica gel, though other polarization processes, e.g., proton hopping along the surface (Skold et al., 2013), may also be a contributing factor. As an alternative model-independent approach to confirming the link between surface sorption and SIP we initiated a study that will continue (unfunded) beyond the completion of this project to independently measure the accumulation of gamma emitting isotopes on the silica gel during the SIP monitoring experiments. Though our analyses of the project data are ongoing, our preliminary analyses are generally supportive of the grain (Stern layer) polarization theory of SIP. Experiments focused on evaluating the impact of physical modifications of the medium on polarization included etching and biotic and abiotic facilitated precipitation of carbonate and iron oxides to alter the roughness and electrical conductivity of the surfaces. These experiments were performed for both silica gel and glass beads, the latter of which lacked the interior porosity and high surface area of the silica gel. The results appear to be more nuanced that the chemical modifications of the system. In general, however, it was found that deposition of iron oxides and etching had relatively minimal or negative impacts on the polarization response of the medium, whereas carbonate coatings increased the polarization response. These results were generally consistent with changes in surface charge observed via AFM. Abiotic and biotic column flow through experiments demonstrated that precipitation of carbonate within the medium significantly impacted the real and imaginary conductivity over time in a manner generally consistent with the carbonate precipitation as observed from the batch grain coating experiments. Biotic effects were not observed to provide distinctly different signatures, but may have contributed to differences in the rate of changes observed with SIP. AFM was used in a variety of different ways to investigate the grain surfaces throughout the course of the project. Standard imaging methods were used to evaluate surface roughness and charge density, which showed that these data could provide qualitative insights about consistency between surface trends and the electrical behavior at the column scale (for the case of glass beads). Polarization and conductive force microscopy (PCFM) measurements were developed by the original project PI (Treavor Kendall), which illustrated the importance of the initial few monolayers of water on the mineral surface for producing surface conductivity. The technique allowed for initial local estimates of complex electrical conductivity on mineral surfaces, but could not be pursued after Kendall left the project due to phase locking limitations with the AFM instrument at Clemson and an inability to perform measurements in solution, which limited their value for linking the measurements to column-scale SIP responses. As a result, co-PI Dean developed a new methodology for making AFM measurements within an externally applied electric field. In this method, the charged tip of an AFM probe is brought within the proximity of a polarization domain while an external electric field is applied to the sample. The premise of the approach is that the tip will be attracted to or rebound from charge accumulations on the surface, which allow for detection of the local polarization response. Initial experiments showed promise in terms of the general trends of responses observed, though we have not yet been able to develop a quantitative interpretation technique that can be applied to predicting column scale responses.« less
Quantifying Microbe-Mineral Interactions Leading to Remotely Detectable Induced Polarization Signals (Final Project Report)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Moysey, Stephen; Dean, Delphine; Dimitrios, Ntarlagiannis

2013-11-13

The objective of this project was to investigate controls on induced polarization responses in porous media. The approach taken in the project was to compare electrical measurements made on mineral surfaces with atomic force microscopy (AFM) techniques to observations made at the column-scale using traditional spectral induced polarization measurements. In the project we evaluated a number of techniques for investigating the surface properties of materials, including the development of a new AFM measurement protocol that utilizes an external electric field to induce grain-scale polarizations that can be probed using a charged AFM tip. The experiments we performed focused on idealizedmore » systems (i.e., glass beads and silica gel) where we could obtain the high degree of control needed to understand how changes in the pore environment, which are determined by biogeochemical controls in the subsurface, affect mechanisms contributing to complex electrical conductivity, i.e., conduction and polarization, responses. The studies we performed can be classified into those affecting the chemical versus physical properties of the grain surface and pore space. Chemical alterations of the surface focused on evaluating how changes in pore fluid pH and ionic composition control surface conduction. These were performed as column flow through experiments where the pore fluid was exchanged in a column of silica gel. Given that silica gel has a high surface area due to internal grain porosity, high-quality data could be obtained where the chemical influences on the surface are clearly apparent and qualitatively consistent with theories of grain (i.e., Stern layer) polarization controlled by electrostatic surface sorption processes (i.e., triple layer theory). Quantitative fitting of the results by existing process-based polarization models (e.g., Leroy et al., 2008) has been less successful, however, due to what we have attributed to differences between existing models developed for spherical grains versus the actual geometry associated with the nano-pores in the silica gel, though other polarization processes, e.g., proton hopping along the surface (Skold et al., 2013), may also be a contributing factor. As an alternative model-independent approach to confirming the link between surface sorption and SIP we initiated a study that will continue (unfunded) beyond the completion of this project to independently measure the accumulation of gamma emitting isotopes on the silica gel during the SIP monitoring experiments. Though our analyses of the project data are ongoing, our preliminary analyses are generally supportive of the grain (Stern layer) polarization theory of SIP. Experiments focused on evaluating the impact of physical modifications of the medium on polarization included etching and biotic and abiotic facilitated precipitation of carbonate and iron oxides to alter the roughness and electrical conductivity of the surfaces. These experiments were performed for both silica gel and glass beads, the latter of which lacked the interior porosity and high surface area of the silica gel. The results appear to be more nuanced that the chemical modifications of the system. In general, however, it was found that deposition of iron oxides and etching had relatively minimal or negative impacts on the polarization response of the medium, whereas carbonate coatings increased the polarization response. These results were generally consistent with changes in surface charge observed via AFM. Abiotic and biotic column flow through experiments demonstrated that precipitation of carbonate within the medium significantly impacted the real and imaginary conductivity over time in a manner generally consistent with the carbonate precipitation as observed from the batch grain coating experiments. Biotic effects were not observed to provide distinctly different signatures, but may have contributed to differences in the rate of changes observed with SIP. AFM was used in a variety of different ways to investigate the grain surfaces throughout the course of the project. Standard imaging methods were used to evaluate surface roughness and charge density, which showed that these data could provide qualitative insights about consistency between surface trends and the electrical behavior at the column scale (for the case of glass beads). Polarization and conductive force microscopy (PCFM) measurements were developed by the original project PI (Treavor Kendall), which illustrated the importance of the initial few monolayers of water on the mineral surface for producing surface conductivity. The technique allowed for initial local estimates of complex electrical conductivity on mineral surfaces, but could not be pursued after Kendall left the project due to phase locking limitations with the AFM instrument at Clemson and an inability to perform measurements in solution, which limited their value for linking the measurements to column-scale SIP responses. As a result, co-PI Dean developed a new methodology for making AFM measurements within an externally applied electric field. In this method, the charged tip of an AFM probe is brought within the proximity of a polarization domain while an external electric field is applied to the sample. The premise of the approach is that the tip will be attracted to or rebound from charge accumulations on the surface, which allow for detection of the local polarization response. Initial experiments showed promise in terms of the general trends of responses observed, though we have not yet been able to develop a quantitative interpretation technique that can be applied to predicting column scale responses.« less
Manual modification and plasma exposure of boron nitride ceramic to study Hall effect thruster plasma channel material erosion

NASA Astrophysics Data System (ADS)

Satonik, Alexander J.

Worn Hall effect thrusters (HET) show a variety of unique microstructures and elemental compositions in the boron nitride thruster channel walls. Worn thruster channels are typically created by running test thrusters in vacuum chambers for hundreds of hours. Studies were undertaken to manually modify samples of boron nitride without the use of a hall effect thruster. Samples were manually abraded with an abrasive blaster and sandpaper, in addition to a vacuum heater. Some of these samples were further exposed to a xenon plasma in a magnetron sputter device. Sandpaper and abrasive blaster tests were used to modify surface roughness values of the samples from 10,000 A to 150,000 A, matching worn thruster values. Vacuum heat treatments were performed on samples. These treatments showed the ability to modify chemical compositions of boron nitride samples, but not in a manner matching changes seen in worn thruster channels. Plasma erosion rate was shown to depend on the grade of the BN ceramic and the preparation of the surface prior to plasma exposure. Abraded samples were shown to erode 43% more than their pristine counterparts. Unique surface features and elemental compositions on the worn thruster channel samples were overwritten by new surface features on the ceramic grains. The microscope images of the ceramic surface show that the magnetron plasma source rounded the edges of the ceramic grains to closely match the worn HET surface. This effect was not as pronounced in studies of ion beam bombardment of the surface and appears to be a result of the quasi-neutral plasma environment.
Roughness evolution of metallic implant surfaces under contact loading and nanometer-scale chemical etching.

PubMed

Ryu, J J; Letchuman, S; Shrotriya, P

2012-10-01

Surface damage of metallic implant surface at taper lock and clamped interfaces may take place through synergistic interactions between repeated contact loading and corrosion. In the present research, we investigated the influence of surface roughness and contact loading on the mechanical and chemical damage phenomena. Cobalt-chromium (CoCrMo) specimens with two different roughness configurations created by milling and grinding process were subjected to normal and inclined contact loading. During repeated contact loading, amplitude of surface roughness reached a steady value after decreasing during the first few cycles. During the second phase, the alternating experiment of rough surface contact and micro-etching was conducted to characterize surface evolution behavior. As a result, surface roughness amplitude continuously evolved-decreasing during contact loading due to plastic deformation of contacting asperities and increasing on exposure to corrosive environment by the preferential corrosion attack on stressed area. Two different instabilities could be identified in the surface roughness evolution during etching of contact loaded surfaces: increase in the amplitude of dominant wavenumber and increase in amplitude of a small group of roughness modes. A damage mechanism that incorporates contact-induced residual stress development and stress-assisted dissolution is proposed to elucidate the measured instabilities in surface roughness evolution. Copyright © 2012 Elsevier Ltd. All rights reserved.
Interfacial phonon scattering and transmission loss in >1 μm thick silicon-on-insulator thin films

NASA Astrophysics Data System (ADS)

Jiang, Puqing; Lindsay, Lucas; Huang, Xi; Koh, Yee Kan

2018-05-01

Scattering of phonons at boundaries of a crystal (grains, surfaces, or solid/solid interfaces) is characterized by the phonon wavelength, the angle of incidence, and the interface roughness, as historically evaluated using a specularity parameter p formulated by Ziman [Electrons and Phonons (Clarendon Press, Oxford, 1960)]. This parameter was initially defined to determine the probability of a phonon specularly reflecting or diffusely scattering from the rough surface of a material. The validity of Ziman's theory as extended to solid/solid interfaces has not been previously validated. To better understand the interfacial scattering of phonons and to test the validity of Ziman's theory, we precisely measured the in-plane thermal conductivity of a series of Si films in silicon-on-insulator (SOI) wafers by time-domain thermoreflectance (TDTR) for a Si film thickness range of 1-10 μm and a temperature range of 100-300 K. The Si /SiO2 interface roughness was determined to be 0.11 ±0.04 nm using transmission electron microscopy (TEM). Furthermore, we compared our in-plane thermal conductivity measurements to theoretical calculations that combine first-principles phonon transport with Ziman's theory. Calculations using Ziman's specularity parameter significantly overestimate values from the TDTR measurements. We attribute this discrepancy to phonon transmission through the solid/solid interface into the substrate, which is not accounted for by Ziman's theory for surfaces. The phonons that are specularly transmitted into an amorphous layer will be sufficiently randomized by the time they come back to the crystalline Si layer, the effect of which is practically equivalent to a diffuse reflection at the interface. We derive a simple expression for the specularity parameter at solid/amorphous interfaces and achieve good agreement between calculations and measurement values.
Thermal Cycling Behavior of Thermal Barrier Coatings with MCrAlY Bond Coat Irradiated by High-Current Pulsed Electron Beam.

PubMed

Cai, Jie; Lv, Peng; Guan, Qingfeng; Xu, Xiaojing; Lu, Jinzhong; Wang, Zhiping; Han, Zhiyong

2016-11-30

Microstructural modifications of a thermally sprayed MCrAlY bond coat subjected to high-current pulsed electron beam (HCPEB) and their relationships with thermal cycling behavior of thermal barrier coatings (TBCs) were investigated. Microstructural observations revealed that the rough surface of air plasma spraying (APS) samples was significantly remelted and replaced by many interconnected bulged nodules after HCPEB irradiation. Meanwhile, the parallel columnar grains with growth direction perpendicular to the coating surface were observed inside these bulged nodules. Substantial Y-rich Al 2 O 3 bubbles and varieties of nanocrystallines were distributed evenly on the top of the modified layer. A physical model was proposed to describe the evaporation-condensation mechanism taking place at the irradiated surface for generating such surface morphologies. The results of thermal cycling test showed that HCPEB-TBCs presented higher thermal cycling resistance, the spalling area of which after 200 cycles accounted for only 1% of its total area, while it was about 34% for APS-TBCs. The resulting failure mode, i.e., in particular, a mixed delamination crack path, was shown and discussed. The irradiated effects including compact remelted surface, abundant nanoparticles, refined columnar grains, Y-rich alumina bubbles, and deformation structures contributed to the formation of a stable, continuous, slow-growing, and uniform thermally grown oxide with strong adherent ability. It appeared to be responsible for releasing stress and changing the cracking paths, and ultimately greatly improving the thermal cycling behavior of HCPEB-TBCs.

EM Bias-Correction for Ice Thickness and Surface Roughness Retrievals over Rough Deformed Sea Ice

NASA Astrophysics Data System (ADS)

Li, L.; Gaiser, P. W.; Allard, R.; Posey, P. G.; Hebert, D. A.; Richter-Menge, J.; Polashenski, C. M.

2016-12-01

The very rough ridge sea ice accounts for significant percentage of total ice areas and even larger percentage of total volume. The commonly used Radar altimeter surface detection techniques are empirical in nature and work well only over level/smooth sea ice. Rough sea ice surfaces can modify the return waveforms, resulting in significant Electromagnetic (EM) bias in the estimated surface elevations, and thus large errors in the ice thickness retrievals. To understand and quantify such sea ice surface roughness effects, a combined EM rough surface and volume scattering model was developed to simulate radar returns from the rough sea ice `layer cake' structure. A waveform matching technique was also developed to fit observed waveforms to a physically-based waveform model and subsequently correct the roughness induced EM bias in the estimated freeboard. This new EM Bias Corrected (EMBC) algorithm was able to better retrieve surface elevations and estimate the surface roughness parameter simultaneously. In situ data from multi-instrument airborne and ground campaigns were used to validate the ice thickness and surface roughness retrievals. For the surface roughness retrievals, we applied this EMBC algorithm to co-incident LiDAR/Radar measurements collected during a Cryosat-2 under-flight by the NASA IceBridge missions. Results show that not only does the waveform model fit very well to the measured radar waveform, but also the roughness parameters derived independently from the LiDAR and radar data agree very well for both level and deformed sea ice. For sea ice thickness retrievals, validation based on in-situ data from the coordinated CRREL/NRL field campaign demonstrates that the physically-based EMBC algorithm performs fundamentally better than the empirical algorithm over very rough deformed sea ice, suggesting that sea ice surface roughness effects can be modeled and corrected based solely on the radar return waveforms.
Improvement in shelf life of rough and brown rice using infrared radiation heating

USDA-ARS?s Scientific Manuscript database

The objective of this study was to investigate the effect of IR heating and tempering treatments on storage stability of rough and brown rice. Samples of freshly harvested medium grain rice variety M206 with initial moisture content of 25.03±0.21% (d.b.) were used. They were dried using infrared (IR...
Modeling Surface Roughness to Estimate Surface Moisture Using Radarsat-2 Quad Polarimetric SAR Data

NASA Astrophysics Data System (ADS)

Nurtyawan, R.; Saepuloh, A.; Budiharto, A.; Wikantika, K.

2016-08-01

Microwave backscattering from the earth's surface depends on several parameters such as surface roughness and dielectric constant of surface materials. The two parameters related to water content and porosity are crucial for estimating soil moisture. The soil moisture is an important parameter for ecological study and also a factor to maintain energy balance of land surface and atmosphere. Direct roughness measurements to a large area require extra time and cost. Heterogeneity roughness scale for some applications such as hydrology, climate, and ecology is a problem which could lead to inaccuracies of modeling. In this study, we modeled surface roughness using Radasat-2 quad Polarimetric Synthetic Aperture Radar (PolSAR) data. The statistical approaches to field roughness measurements were used to generate an appropriate roughness model. This modeling uses a physical SAR approach to predicts radar backscattering coefficient in the parameter of radar configuration (wavelength, polarization, and incidence angle) and soil parameters (surface roughness and dielectric constant). Surface roughness value is calculated using a modified Campbell and Shepard model in 1996. The modification was applied by incorporating the backscattering coefficient (σ°) of quad polarization HH, HV and VV. To obtain empirical surface roughness model from SAR backscattering intensity, we used forty-five sample points from field roughness measurements. We selected paddy field in Indramayu district, West Java, Indonesia as the study area. This area was selected due to intensive decreasing of rice productivity in the Northern Coast region of West Java. Third degree polynomial is the most suitable data fitting with coefficient of determination R2 and RMSE are about 0.82 and 1.18 cm, respectively. Therefore, this model is used as basis to generate the map of surface roughness.
Numerical analysis of the bucket surface roughness effects in Pelton turbine

NASA Astrophysics Data System (ADS)

Xiao, Y. X.; Zeng, C. J.; Zhang, J.; Yan, Z. G.; Wang, Z. W.

2013-12-01

The internal flow of a Pelton turbine is quite complex. It is difficult to analyse the unsteady free water sheet flow in the rotating bucket owing to the lack of a sound theory. Affected by manufacturing technique and silt abrasion during the operation, the bucket surface roughness of Pelton turbine may be too great, and thereby influence unit performance. To investigate the effect of bucket roughness on Pelton turbine performance, this paper presents the numerical simulation of the interaction between the jet and the bucket in a Pelton turbine. The unsteady three-dimensional numerical simulations were performed with CFX code by using the SST turbulence model coupling the two-phase flow volume of fluid method. Different magnitude orders of bucket surface roughness were analysed and compared. Unsteady numerical results of the free water sheet flow patterns on bucket surface, torque and unit performance for each bucket surface roughness were generated. The total pressure distribution on bucket surface is used to show the free water sheet flow pattern on bucket surface. By comparing the variation of water sheet flow patterns on bucket surface with different roughness, this paper qualitatively analyses how the bucket surface roughness magnitude influences the impeding effect on free water sheet flow. Comparison of the torque variation of different bucket surface roughness highlighted the effect of the bucket surface roughness on the Pelton turbine output capacity. To further investigate the effect of bucket surface roughness on Pelton turbine performance, the relation between the relative efficiency loss rate and bucket surface roughness magnitude is quantitatively analysed. The result can be used to predict and evaluate the Pelton turbine performance.
Wetting properties of molecularly rough surfaces

DOE Office of Scientific and Technical Information (OSTI.GOV)

Svoboda, Martin; Lísal, Martin, E-mail: lisal@icpf.cas.cz; Department of Physics, Institute of Science, J. E. Purkinje University, 400 96 Ústí n. Lab.

2015-09-14

We employ molecular dynamics simulations to study the wettability of nanoscale rough surfaces in systems governed by Lennard-Jones (LJ) interactions. We consider both smooth and molecularly rough planar surfaces. Solid substrates are modeled as a static collection of LJ particles arranged in a face-centered cubic lattice with the (100) surface exposed to the LJ fluid. Molecularly rough solid surfaces are prepared by removing several strips of LJ atoms from the external layers of the substrate, i.e., forming parallel nanogrooves on the surface. We vary the solid-fluid interactions to investigate strongly and weakly wettable surfaces. We determine the wetting properties bymore » measuring the equilibrium droplet profiles that are in turn used to evaluate the contact angles. Macroscopic arguments, such as those leading to Wenzel’s law, suggest that surface roughness always amplifies the wetting properties of a lyophilic surface. However, our results indicate the opposite effect from roughness for microscopically corrugated surfaces, i.e., surface roughness deteriorates the substrate wettability. Adding the roughness to a strongly wettable surface shrinks the surface area wet with the liquid, and it either increases or only marginally affects the contact angle, depending on the degree of liquid adsorption into the nanogrooves. For a weakly wettable surface, the roughness changes the surface character from lyophilic to lyophobic due to a weakening of the solid-fluid interactions by the presence of the nanogrooves and the weaker adsorption of the liquid into the nanogrooves.« less
Numerical simulation of electroosmotic flow in rough microchannels using the lattice Poisson-Nernst-Planck methods

NASA Astrophysics Data System (ADS)

Kamali, Reza; Soloklou, Mohsen Nasiri; Hadidi, Hooman

2018-05-01

In this study, coupled Lattice Boltzmann method is applied to solve the dynamic model for an electroosmotic flow and investigate the effects of roughness in a 2-D flat microchannel. In the present model, the Poisson equation is solved for the electrical potential, the Nernst- Planck equation is solved for the ion concentration. In the analysis of electroosmotic flows, when the electric double layers fully overlap or the convective effects are not negligible, the Nernst-Planck equation must be used to find the ionic distribution throughout the microchannel. The effects of surface roughness height, roughness interval spacing and roughness surface potential on flow conditions are investigated for two different configurations of the roughness, when the EDL layers fully overlap through the microchannel. The results show that in both arrangements of roughness in homogeneously charged rough channels, the flow rate decreases by increasing the roughness height. A discrepancy in the mass flow rate is observed when the roughness height is about 0.15 of the channel width, which its average is higher for the asymmetric configuration and this difference grows by increasing the roughness height. In the symmetric roughness arrangement, the mass flow rate increases until the roughness interval space is almost 1.5 times the roughness width and it decreases for higher values of the roughness interval space. For the heterogeneously charged rough channel, when the roughness surface potential ψr is less than channel surface potential ψs , the net charge density increases by getting far from the roughness surface, while in the opposite situation, when ψs is more than ψr , the net charge density decreases from roughness surface to the microchannel middle center. Increasing the roughness surface potential induces stronger electric driving force on the fluid which results in larger velocities in the flow.
The improvement of surface roughness by polishing method of arcylic door panel at Taishi Tech Sdn Bhd

NASA Astrophysics Data System (ADS)

Basirin, Hammadi bin Mohd; Nawi, Ismail bin Haji Mohd

2017-04-01

This research is an approach to improve the surface roughness for acrylic door panel by using polishing process. The polishing process involve is sanding process by 3 types of sand paper. The sanding process used to improve the surface roughness by using the different grit sizes of sand paper. The experiment was done by using two types of material s, that is plywood and medium density board (MDF). These two materials are the main materials in producing the arcrylic door panel. The surface roughness of these two materials affects the qualities and quantities of the acrylic door panel. The surface structure was measured by using Optical Microscope and Scanning Electron Microscope (SEM) and the surface roughness was measured by using Mitutoyo surfest SJ 400 Tester. Results indicates that using the different types of grit are influence the surface roughness of the material. When the higher types of grit sizes had been used, the average roughness of the surface are decrease. In summary, a good surface roughness condition produced when using the higher types of grit sizes sand paper.
Clouds Versus Carbon: Predicting Vegetation Roughness by Maximizing Productivity

NASA Technical Reports Server (NTRS)

Olsen, Lola M.

2004-01-01

Surface roughness is one of the dominant vegetation properties that affects land surface exchange of energy, water, carbon, and momentum with the overlying atmosphere. We hypothesize that the canopy structure of terrestrial vegetation adapts optimally to climate by maximizing productivity, leading to an optimum surface roughness. An optimum should exist because increasing values of surface roughness cause increased surface exchange, leading to increased supply of carbon dioxide for photosynthesis. At the same time, increased roughness enhances evapotranspiration and cloud cover, thereby reducing the supply of photosynthetically active radiation. We demonstrate the optimum through sensitivity simulations using a coupled dynamic vegetation-climate model for present day conditions, in which we vary the value of surface roughness for vegetated surfaces. We find that the maximum in productivity occurs at a roughness length of 2 meters, a value commonly used to describe the roughness of today's forested surfaces. The sensitivity simulations also illustrate the strong climatic impacts of vegetation roughness on the energy and water balances over land: with increasing vegetation roughness, solar radiation is reduced by up to 20 W/sq m in the global land mean, causing shifts in the energy partitioning and leading to general cooling of the surface by 1.5 K. We conclude that the roughness of vegetated surfaces can be understood as a reflection of optimum adaptation, and it is associated with substantial changes in the surface energy and water balances over land. The role of the cloud feedback in shaping the optimum underlines the importance of an integrated perspective that views vegetation and its adaptive nature as an integrated component of the Earth system.
Mapping water surface roughness in a shallow, gravel-bed river using hyperspectral imagery

NASA Astrophysics Data System (ADS)

Overstreet, B. T.; Legleiter, C. J.

2014-12-01

Rapid advances in remote sensing are narrowing the gap between the data available for characterizing physical and biological processes in rivers and the information needed to guide river management decisions. The availability and quality of hyperspectral imagery have increased drastically over the past 20 years and hyperspectral data is now used in a number of different capacities that range from classifying riverine environments to measuring river bathymetry. A fundamental challenge in relating the spectral data from images to biophysical processes is the difficulty of isolating individual contributions to the at-sensor radiance, each associated with a different component of the fluvial environment. In this presentation we describe a method for isolating the contribution of light reflected from the water surface, or sun glint, from a hyperspectral image of a shallow gravel-bed river. We show that isolation and removal of sun glint can improve the accuracy of spectrally-based depth retrieval in cases where sun glint dominates the at-sensor radiance. Observed-vs.-predicted R2 values for depth retrieval improved from 0.56 to 0.68 following sun glint removal. In addition to clarifying the signal associated with the water column and bed, isolating sun glint could unlock important hydraulic information contained within the topography of the water surface. We present data from flume and field experiments suggesting that the intensity of sun glint is a function of water surface roughness. In rivers, water surface roughness depends on local flow hydraulics: depth, velocity, and bed material grain size. To explore this relationship, we coupled maps of image-derived sun glint with hydraulic measurements collected with a kayak-borne acoustic Doppler current profiler along 2 km of the Snake River in Grand Teton National Park. Spatial patterns of sun glint are spatially correlated with field observations of near-surface velocity and depth, suggesting that reach scale hydraulics could be mapped from hyperspectral images. These findings also suggest that aquatic habitats, which are often associated with specific hydraulic conditions and manifested as distinct surface textures, could be mapped quantitatively over large areas using hyperspectral imagery.
Stopping dynamics of a steady uniform granular flow over a rough incline

NASA Astrophysics Data System (ADS)

Deboeuf, Stéphanie; Saingier, Guillaume; Thiruvalluvar, Nitharshini; Lagrée, Pierre-Yves; Popinet, Stéphane; Staron, Lydie

2017-06-01

Granular material flowing on complex topographies are ubiquitous in industrial and geophysical situations. Even model granular flows are difficult to understand and predict. Recently, the frictional rheology μ(I) -describing the ratio of the shear stress to the normal stress as a function of the inertial number I, that compares inertial and confinement effects- allows unifying different configurations of granular flows. However it does not succeed in describing some phenomenologies, such as creep flow, deposit height, … Is it attributable to the rheology, to non-local effects, ...? Here, we consider a thin layer of grains flowing steadily and uniformly on a rough incline, when the input mass flow rate is suddenly stopped. We focus on the arrest dynamics by using both experimental and numerical approaches. We measure the height and surface velocities of the granular layer during the long-time stopping dynamics and we compare our experimental results with computations of depthaveraged equations for a fluid of rheology μ(I).
Structural and magnetic analysis of Cu, Co substituted NiFe2O4 thin films

NASA Astrophysics Data System (ADS)

Sharma, Hakikat; Bala, Kanchan; Negi, N. S.

2016-05-01

In the present work we prepared NiFe2O4, Ni0.95Cu0.05Fe2O4 and Ni0.94Cu0.05Co0.01 Fe2O4 thin films by metallo-organic decomposition method (MOD) using spin coating technique. The thin films were analyzed by X-ray diffractometer (XRD) and Atomic force microscope (AFM) for structural studies. The XRD patterns confirmed the ferrite phase of thin films. From AFM, we analyzed surface morphology, calculated grain size (GS) and root mean square roughness (RMSR). Room temperature magnetic properties were investigated by vibrating sample magnetometer (VSM).
Machinability of hypereutectic silicon-aluminum alloys

NASA Astrophysics Data System (ADS)

Tanaka, T.; Akasawa, T.

1999-08-01

The machinability of high-silicon aluminum alloys made by a P/M process and by casting was compared. The cutting test was conducted by turning on lathes with the use of cemented carbide tools. The tool wear by machining the P/M alloy was far smaller than the tool wear by machining the cast alloy. The roughness of the machined surface of the P/M alloy is far better than that of the cast alloy, and the turning speed did not affect it greatly at higher speeds. The P/M alloy produced long chips, so the disposal can cause trouble. The size effect of silicon grains on the machinability is discussed.
Effect of engraving speeds of CO₂ laser irradiation on In-Ceram Alumina roughness: a pilot study.

PubMed

Ersu, Bahadır; Ersoy, Orkun; Yuzugullu, Bulem; Canay, Senay

2015-05-01

The aim of the study was to determine the effect of CO₂ laser on surface roughness of In-Ceram-Alumina-ceramic. Four aluminum-oxide ceramic disc specimens were prepared of In-Ceram Alumina. Discs received CO₂ laser irradiation with different engraving speeds (100, 400, 600 and 800 mm/min) as a surface treatment. The roughness of the surfaces was measured on digital elevation models reconstructed from stereoscopic images acquired by scanning-electron-microscope. Surface roughness data were analyzed with One-Way-Analysis-of-Variance at a significance level of p<0.05. There was no significant difference between the roughness values (p=0.82). Due to higher laser durations, partial melting signs were observed on the surfaces. Tearing, smearing and swelling occurred on melted surfaces. Swelling accompanying melting increased the surface roughness, while laser power was fixed and different laser engraving speeds were applied. Although different laser irradiation speeds did not affect the roughness of ceramic surfaces, swelling was observed which led to changes on surfaces.
Rock discontinuity surface roughness variation with scale

NASA Astrophysics Data System (ADS)

Bitenc, Maja; Kieffer, D. Scott; Khoshelham, Kourosh

2017-04-01

ABSTRACT: Rock discontinuity surface roughness refers to local departures of the discontinuity surface from planarity and is an important factor influencing the shear resistance. In practice, the Joint Roughness Coefficient (JRC) roughness parameter is commonly relied upon and input to a shear strength criterion such as developed by Barton and Choubey [1977]. The estimation of roughness by JRC is hindered firstly by the subjective nature of visually comparing the joint profile to the ten standard profiles. Secondly, when correlating the standard JRC values and other objective measures of roughness, the roughness idealization is limited to a 2D profile of 10 cm length. With the advance of measuring technologies that provide accurate and high resolution 3D data of surface topography on different scales, new 3D roughness parameters have been developed. A desirable parameter is one that describes rock surface geometry as well as the direction and scale dependency of roughness. In this research a 3D roughness parameter developed by Grasselli [2001] and adapted by Tatone and Grasselli [2009] is adopted. It characterizes surface topography as the cumulative distribution of local apparent inclination of asperities with respect to the shear strength (analysis) direction. Thus, the 3D roughness parameter describes the roughness amplitude and anisotropy (direction dependency), but does not capture the scale properties. In different studies the roughness scale-dependency has been attributed to data resolution or size of the surface joint (see a summary of researches in [Tatone and Grasselli, 2012]). Clearly, the lower resolution results in lower roughness. On the other hand, have the investigations of surface size effect produced conflicting results. While some studies have shown a decrease in roughness with increasing discontinuity size (negative scale effect), others have shown the existence of positive scale effects, or both positive and negative scale effects. We hypothesize that roughness can increase or decrease with the joint size, depending on the large scale roughness (or waviness), which is entering the roughness calculation once the discontinuity size increases. Therefore, our objective is to characterize roughness at various spatial scales, rather than at changing surface size. Firstly, the rock surface is interpolated into a grid on which a Discrete Wavelet Transform (DWT) is applied. The resulting surface components have different frequencies, or in other words, they have a certain physical scale depending on the decomposition level and input grid resolution. Secondly, the Grasselli Parameter is computed for the original and each decomposed surface. Finally, the relative roughness change is analyzed with respect to increasing roughness wavelength for four different rock samples. The scale variation depends on the sample itself and thus indicates its potential mechanical behavior. References: - Barton, N. and V. Choubey (1977). "The shear strength of rock joints in theory and practice." Rock Mechanics and Rock Engineering 10(1): 1-54. - Grasselli, G. (2001). Shear strength of rock joints based on quantified surface description. École Polytechnique Fédérale de Lausanne. Lausanne, EPFL. - Tatone, B. S. A. and G. Grasselli (2009). "A method to evaluate the three-dimensional roughness of fracture surfaces in brittle geomaterials." Review of Scientific Instruments 80(12) - Tatone, B. and G. Grasselli (2012). "An Investigation of Discontinuity Roughness Scale Dependency Using High-Resolution Surface Measurements." Rock Mechanics and Rock Engineering: 1-25.
Determining Surface Roughness in Urban Areas Using Lidar Data

NASA Technical Reports Server (NTRS)

Holland, Donald

2009-01-01

An automated procedure has been developed to derive relevant factors, which can increase the ability to produce objective, repeatable methods for determining aerodynamic surface roughness. Aerodynamic surface roughness is used for many applications, like atmospheric dispersive models and wind-damage models. For this technique, existing lidar data was used that was originally collected for terrain analysis, and demonstrated that surface roughness values can be automatically derived, and then subsequently utilized in disaster-management and homeland security models. The developed lidar-processing algorithm effectively distinguishes buildings from trees and characterizes their size, density, orientation, and spacing (see figure); all of these variables are parameters that are required to calculate the estimated surface roughness for a specified area. By using this algorithm, aerodynamic surface roughness values in urban areas can then be extracted automatically. The user can also adjust the algorithm for local conditions and lidar characteristics, like summer/winter vegetation and dense/sparse lidar point spacing. Additionally, the user can also survey variations in surface roughness that occurs due to wind direction; for example, during a hurricane, when wind direction can change dramatically, this variable can be extremely significant. In its current state, the algorithm calculates an estimated surface roughness for a square kilometer area; techniques using the lidar data to calculate the surface roughness for a point, whereby only roughness elements that are upstream from the point of interest are used and the wind direction is a vital concern, are being investigated. This technological advancement will improve the reliability and accuracy of models that use and incorporate surface roughness.
Effect of surface roughness of trench sidewalls on electrical properties in 4H-SiC trench MOSFETs

NASA Astrophysics Data System (ADS)

Kutsuki, Katsuhiro; Murakami, Yuki; Watanabe, Yukihiko; Onishi, Toru; Yamamoto, Kensaku; Fujiwara, Hirokazu; Ito, Takahiro

2018-04-01

The effects of the surface roughness of trench sidewalls on electrical properties have been investigated in 4H-SiC trench MOSFETs. The surface roughness of trench sidewalls was well controlled and evaluated by atomic force microscopy. The effective channel mobility at each measurement temperature was analyzed on the basis of the mobility model including optical phonon scattering. The results revealed that surface roughness scattering had a small contribution to channel mobility, and at the arithmetic average roughness in the range of 0.4-1.4 nm, there was no correlation between the experimental surface roughness and the surface roughness scattering mobility. On the other hand, the characteristics of the gate leakage current and constant current stress time-dependent dielectric breakdown tests demonstrated that surface morphology had great impact on the long-term reliability of gate oxides.
A new fiber optic sensor for inner surface roughness measurement

NASA Astrophysics Data System (ADS)

Xu, Xiaomei; Liu, Shoubin; Hu, Hong

2009-11-01

In order to measure inner surface roughness of small holes nondestructively, a new fiber optic sensor is researched and developed. Firstly, a new model for surface roughness measurement is proposed, which is based on intensity-modulated fiber optic sensors and scattering modeling of rough surfaces. Secondly, a fiber optical measurement system is designed and set up. Under the help of new techniques, the fiber optic sensor can be miniaturized. Furthermore, the use of micro prism makes the light turn 90 degree, so the inner side surface roughness of small holes can be measured. Thirdly, the fiber optic sensor is gauged by standard surface roughness specimens, and a series of measurement experiments have been done. The measurement results are compared with those obtained by TR220 Surface Roughness Instrument and Form Talysurf Laser 635, and validity of the developed fiber optic sensor is verified. Finally, precision and influence factors of the fiber optic sensor are analyzed.
Roughness Effects on Fretting Fatigue

NASA Astrophysics Data System (ADS)

Yue, Tongyan; Abdel Wahab, Magd

2017-05-01

Fretting is a small oscillatory relative motion between two normal loaded contact surfaces. It may cause fretting fatigue, fretting wear and/or fretting corrosion damage depending on various fretting couples and working conditions. Fretting fatigue usually occurs at partial slip condition, and results in catastrophic failure at the stress levels below the fatigue limit of the material. Many parameters may affect fretting behaviour, including the applied normal load and displacement, material properties, roughness of the contact surfaces, frequency, etc. Since fretting damage is undesirable due to contacting, the effect of rough contact surfaces on fretting damage has been studied by many researchers. Experimental method on this topic is usually focusing on rough surface effects by finishing treatment and random rough surface effects in order to increase fretting fatigue life. However, most of numerical models on roughness are based on random surface. This paper reviewed both experimental and numerical methodology on the rough surface effects on fretting fatigue.
Characterization of Cu(In,Ga)Se 2 (CIGS) films with varying gallium ratios

DOE PAGES

Claypoole, Jesse; Peace, Bernadette; Sun, Neville; ...

2015-09-05

Cu(In 1–x,Ga x)Se 2 (CIGS) absorber layers were deposited on molybdenum (Mo) coated soda-lime glass substrates with varying Ga content (described as Ga/(In + Ga) ratios) with respect to depth. As the responsible mechanisms for the limitation of the performance of the CIGS solar cells with high Ga contents are not well understood, the goal of this work was to investigate different properties of CIGS absorber films with Ga/(In + Ga) ratios varied between 0.29 and 0.41 (as determined by X-ray florescence spectroscopy (XRF)) in order to better understand the role that the Ga content has on film quality. Themore » Ga grading in the CIGS layer has the effect causing a higher band gap toward the surface and Mo contact while the band gap in the middle of the CIGS layer is lower. Also, a wider and larger Ga/(In + Ga) grading dip located deeper in the CIGS absorber layers tend to produce larger grains in the regions of the films that have lower Ga/(In + Ga) ratios. Moreover, it was found that surface roughness decreases from 51.2 nm to 41.0 nm with increasing Ga/(In + Ga) ratios. Furthermore, the surface roughness generally decreases if the Ga grading occurs deeper in the absorber layer.« less
Pulse electro-deposition of copper on molybdenum for Cu(In,Ga)Se2 and Cu2ZnSnSe4 solar cell applications

NASA Astrophysics Data System (ADS)

Bi, Jinlian; Yao, Liyong; Ao, Jianping; Gao, Shoushuai; Sun, Guozhong; He, Qing; Zhou, Zhiqiang; Sun, Yun; Zhang, Yi

2016-09-01

The issues of rough surface morphology and the incorporated additives of the electro-deposited Cu layers, which exists in electrodeposition-based processes, is one of the major obstacles to improve the efficiency of Cu(In,Ga)Se2 (CIGSe) and Cu2ZnSnSe4 (CZTSe) solar cells. In this study, the pulse current electro-deposition method is employed to deposit smooth Cu film on Mo substrate in CuSO4 solution without any additives. Grain size of the deposited Cu film is decreased by high cathode polarization successfully. And the concentration polarization, which results from high pulse current density, is controlled successfully by adjusting the pulse frequency. Flat Cu film with smooth surface and compact structure is deposited as pulse current density @ 62.5 mA cm-2, pulse frequency @100,000 Hz, and duty cycle @ 25%. CIGSe and CZTSe absorber films with flat surface and uniform elemental distribution are prepared by selenizing the stacking metal layers electro-deposited by pulse current method. Finally, the CIGSe and CZTSe solar cells with conversion efficiency of 10.39% and 7.83% respectively are fabricated based on the smooth Cu films, which are better than the solar cells fabricated by the rough Cu film deposited by direct current electro-deposition method.

Towards predictive models for transitionally rough surfaces

NASA Astrophysics Data System (ADS)

Abderrahaman-Elena, Nabil; Garcia-Mayoral, Ricardo

2017-11-01

We analyze and model the previously presented decomposition for flow variables in DNS of turbulence over transitionally rough surfaces. The flow is decomposed into two contributions: one produced by the overlying turbulence, which has no footprint of the surface texture, and one induced by the roughness, which is essentially the time-averaged flow around the surface obstacles, but modulated in amplitude by the first component. The roughness-induced component closely resembles the laminar steady flow around the roughness elements at the same non-dimensional roughness size. For small - yet transitionally rough - textures, the roughness-free component is essentially the same as over a smooth wall. Based on these findings, we propose predictive models for the onset of the transitionally rough regime. Project supported by the Engineering and Physical Sciences Research Council (EPSRC).
Investigation of ellipsometric parameters of 2D microrough surfaces by FDTD.

PubMed

Qiu, J; Ran, D F; Liu, Y B; Liu, L H

2016-07-10

Ellipsometry is a powerful method for measuring the optical constants of materials and is very sensitive to surface roughness. In previous ellipsometric measurement of optical constants of solid materials with rough surfaces, researchers frequently used effective medium approximation (EMA) with roughness already known to fit the complex refractive index of the material. However, the ignored correlation length, the other important parameter of rough surfaces, will definitely result in fitting errors. Hence it is necessary to consider the influence of surface roughness and correlation length on the ellipsometric parameters Δ (phase difference) and Ψ (azimuth) characterizing practical systems. In this paper, the influence of roughness of two-dimensional randomly microrough surfaces (relative roughness σ/λ ranges from 0.001 to 0.025) of silicon on ellipsometric parameters was simulated by the finite-difference time-domain method which was validated with experimental results. The effects of incident angle, relative roughness, and correlation length were numerically investigated for two-dimensional Gaussian distributed randomly microrough surfaces, respectively. The simulated results showed that compared with the smooth surface, only tiny changes of the ellipsometric parameter Δ could be observed for microrough silicon surface in the vicinity of the Brewster angle, but obviously changes of Ψ occur especially in the vicinity of the Brewster angle. More differences between the ellipsometric parameters of the rough surface and smooth surface can been seen especially in the vicinity of the Brewster angle as the relative roughness σ/λ increases or correlation length τ decreases. The results reveal that when we measure the optical constants of solid materials by ellipsometry, the smaller roughness, larger correlation length and larger incident wavelength will lead to the higher precision of measurements.
Aquifer modification: an approach to improve the mobility of nanoscale zero-valent iron particles used for in situ groundwater remediation

NASA Astrophysics Data System (ADS)

MicicBatka, Vesna; Schmid, Doris; Marko, Florian; Velimirovic, Milica; Wagner, Stephan; von der Kammer, Frank; Hofmann, Thilo

2015-04-01

Successful emplacement of nanoscale zero-valent iron (nZVI) within the contaminated source zone is a prerequisite for the use of nZVI technology in groundwater remediation. Emplacement of nZVI is influenced i.e., by the injection technique and the injection velocity applied, as well as by the mobility of nZVI in the subsurface. Whereas processes linked to the injection can be controlled by the remediation practitioners, the mobility of nZVI in the subsurface remains limited. Even though mobility of nZVI is somewhat improved by surface coating with polyelectrolytes, it is still greatly affected by the groundwater composition and physical and chemical heterogeneities of aquifer grains. In order to promote mobility of nZVI it is needed to alter the surface charge heterogeneities of aquifer grains. Modifying the aquifer grain's surfaces by means of polyelectrolyte coating is an approach proposed to increase the overall negative surface charge of the aquifer grain surfaces, hinder deposition of nZVI onto aquifer grains, and finally promote nZVI mobility. In this study the effect of different polyelectrolytes on the nZVI mobility is tested in natural sands deriving from real brownfield sites that are proposed to be remediated using the nZVI technology. Sands collected from brownfield sites were characterized in terms of grain size distribution, mineralogical and chemical composition, and organic carbon content. Furthermore, surface charge of these sands was determined in both, low- and high ionic strength background solutions. Finally, changes of the sand's surface charges were examined after addition of the proposed aquifer modifiers, lignin sulfonate and humic acid. Surface charge of brownfield sands in low ionic strength background solution is more negative compared to that in high ionic strength background solution. An increase in negative surface potential of brownfield sand was recorded when aquifer modifiers were applied in a background solution with low ionic strength, indicating their potential to improve nZVI mobility under comparable environmental conditions. In contrast, no significant change of the surface potential of brownfield sand was observed when aquifer modifiers were applied in a background solution with high ionic strength. The potential of the aquifer modifiers to promote the mobility of nZVI was furthermore tested in flow-through columns, starting with the one filled with natural quartz sand with rough surface, low ionic strength background solutions and pre-injecting lignin sulfonate in concentration of 50 mg/L. The preliminary results showed that the pre-injection of lignin sulfonate does increase mobility of nZVI under this experimental condition. Further mobility tests will be carried out in order to elucidate the potential of the aquifer modifiers to promote the mobility of nZVI in sands with a complex mineralogy and in the background solutions with varying ionic strength, in order to account for the condition that resemble those at polluted sites. This research receives funding from the European Union's Seventh Framework Programme FP7/2007-2013 under grant agreement n°309517.
Cellular Behavior of Human Adipose-Derived Stem Cells on Wettable Gradient Polyethylene Surfaces

PubMed Central

Ahn, Hyun Hee; Lee, Il Woo; Lee, Hai Bang; Kim, Moon Suk

2014-01-01

Appropriate surface wettability and roughness of biomaterials is an important factor in cell attachment and proliferation. In this study, we investigated the correlation between surface wettability and roughness, and biological response in human adipose-derived stem cells (hADSCs). We prepared wettable and rough gradient polyethylene (PE) surfaces by increasing the power of a radio frequency corona discharge apparatus with knife-type electrodes over a moving sample bed. The PE changed gradually from hydrophobic and smooth surfaces to hydrophilic (water contact angle, 90º to ~50º) and rough (80 to ~120 nm) surfaces as the power increased. We found that hADSCs adhered better to highly hydrophilic and rough surfaces and showed broadly stretched morphology compared with that on hydrophobic and smooth surfaces. The proliferation of hADSCs on hydrophilic and rough surfaces was also higher than that on hydrophobic and smooth surfaces. Furthermore, integrin beta 1 gene expression, an indicator of attachment, and heat shock protein 70 gene expression were high on hydrophobic and smooth surfaces. These results indicate that the cellular behavior of hADSCs on gradient surface depends on surface properties, wettability and roughness. PMID:24477265
Barium ferrite thin-film recording media

NASA Astrophysics Data System (ADS)

Sui, Xiaoyu; Scherge, Matthias; Kryder, Mark H.; Snyder, John E.; Harris, Vincent G.; Koon, Norman C.

1996-03-01

Both longitudinal and perpendicular barium ferrite thin films are being pursued as overcoatless magnetic recording media. In this paper, prior research on thin-film Ba ferrite is reviewed and the most recent results are presented. Self-textured high-coercivity longitudinal Ba ferrite thin films have been achieved using conventional rf diode sputtering. Microstructural studies show that c-axis in-plane oriented grains have a characteristic acicular shape, while c-axis perpendicularly oriented grains have a platelet shape. Extended X-ray absorption fine structure (EXAFS) measurements indicate that the crystal orientations are predetermined by the structural anisotropy in the as-sputtered 'amorphous' state. Recording tests on 1500 Oe coercivity longitudinal Ba ferrite disks show performance comparable with that of a 1900 Oe Co alloy disk. To further improve the recording performance, both grain size and aspect ratio need to be reduced. Initial tribological tests indicate high hardness of Ba ferrite thin films. However, surface roughness needs to be reduced. For future ultrahigh-density contact recording, it is believed that perpendicular recording may be used. A thin Pt underlayer has been found to be capable of producing Ba ferrite thin films with excellent c-axis perpendicular orientation.
Properties of nanostructured undoped ZrO{sub 2} thin film electrolytes by plasma enhanced atomic layer deposition for thin film solid oxide fuel cells

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cho, Gu Young; Noh, Seungtak; Lee, Yoon Ho

2016-01-15

Nanostructured ZrO{sub 2} thin films were prepared by thermal atomic layer deposition (ALD) and by plasma-enhanced atomic layer deposition (PEALD). The effects of the deposition conditions of temperature, reactant, plasma power, and duration upon the physical and chemical properties of ZrO{sub 2} films were investigated. The ZrO{sub 2} films by PEALD were polycrystalline and had low contamination, rough surfaces, and relatively large grains. Increasing the plasma power and duration led to a clear polycrystalline structure with relatively large grains due to the additional energy imparted by the plasma. After characterization, the films were incorporated as electrolytes in thin film solidmore » oxide fuel cells, and the performance was measured at 500 °C. Despite similar structure and cathode morphology of the cells studied, the thin film solid oxide fuel cell with the ZrO{sub 2} thin film electrolyte by the thermal ALD at 250 °C exhibited the highest power density (38 mW/cm{sup 2}) because of the lowest average grain size at cathode/electrolyte interface.« less
Effective-Medium Models for Marine Gas Hydrates, Mallik Revisited

NASA Astrophysics Data System (ADS)

Terry, D. A.; Knapp, C. C.; Knapp, J. H.

2011-12-01

Hertz-Mindlin type effective-medium dry-rock elastic models have been commonly used for more than three decades in rock physics analysis, and recently have been applied to assessment of marine gas hydrate resources. Comparisons of several effective-medium models with derivative well-log data from the Mackenzie River Valley, Northwest Territories, Canada (i.e. Mallik 2L-38 and 5L-38) were made several years ago as part of a marine gas hydrate joint industry project in the Gulf of Mexico. The matrix/grain supporting model (one of the five models compared) was clearly a better representation of the Mallik data than the other four models (2 cemented sand models; a pore-filling model; and an inclusion model). Even though the matrix/grain supporting model was clearly better, reservations were noted that the compressional velocity of the model was higher than the compressional velocity measured via the sonic logs, and that the shear velocities showed an even greater discrepancy. Over more than thirty years, variations of Hertz-Mindlin type effective medium models have evolved for unconsolidated sediments and here, we briefly review their development. In the past few years, the perfectly smooth grain version of the Hertz-Mindlin type effective-medium model has been favored over the infinitely rough grain version compared in the Gulf of Mexico study. We revisit the data from the Mallik wells to review assertions that effective-medium models with perfectly smooth grains are a better predictor than models with infinitely rough grains. We briefly review three Hertz-Mindlin type effective-medium models, and standardize nomenclature and notation. To calibrate the extended effective-medium model in gas hydrates, we use a well accepted framework for unconsolidated sediments through Hashin-Shtrikman bounds. We implement the previously discussed effective-medium models for saturated sediments with gas hydrates and compute theoretical curves of seismic velocities versus gas hydrate saturation to compare with well log data available from the Canadian gas hydrates research site. By directly comparing the infinitely rough and perfectly smooth grain versions of the Hertz-Mindlin type effective-medium model, we provide additional insight to the discrepancies noted in the Gulf of Mexico study.
Measuring Skew in Average Surface Roughness as a Function of Surface Preparation

NASA Technical Reports Server (NTRS)

Stahl, Mark

2015-01-01

Characterizing surface roughness is important for predicting optical performance. Better measurement of surface roughness reduces polishing time, saves money and allows the science requirements to be better defined. This study characterized statistics of average surface roughness as a function of polishing time. Average surface roughness was measured at 81 locations using a Zygo white light interferometer at regular intervals during the polishing process. Each data set was fit to a normal and Largest Extreme Value (LEV) distribution; then tested for goodness of fit. We show that the skew in the average data changes as a function of polishing time.
Emulation of Forward-looking Radar Technology for Threat Detection in Rough Terrain Environments: A Scattering and Imaging Study

DTIC Science & Technology

2012-12-01

a) Ground with flat surface; (b) Ground with randomly rough surface, hrms =1.2 cm, lc=14.93 cm; (c) Ground with randomly rough surface, hrms =1.6 cm...horizontal-horizontal (hh)-polarized images for 20 m×10 m scene: (a) Ground with flat surface; (b) Ground with randomly rough surface, hrms =1.2 cm...lc=14.93 cm; (c) Ground with randomly rough surface, hrms =1.6 cm, lc=14.93 cm. Ground electrical properties: εr=6, σd=10 mS/m. Frequency span: 0.3
Does mere exposure mediate sensitivity to bitter taste on consumer liking and acceptability of whole grain foods?

USDA-ARS?s Scientific Manuscript database

Health benefits of whole grains (WG) are well known, yet consumption by Americans falls far short of recommended amounts. Roughly 75% of Americans are sensitive to bitter taste, and WG are known to contain bitter tasting phenolic compounds. It has been reported that individuals with the highest se...
Basin-scale availability of salmonid spawning gravel as influenced by channel type and hydraulic roughness in mountain catchments.

Treesearch

John M. Buffington; David R. Montgomery; Harvey M. Greenberg

2004-01-01

A general framework is presented for examining the effects of channel type and associated hydraulic roughness on salmonid spawning-gravel availability in mountain catchments. Digital elevation models are coupled with grain-size predictions to provide basin-scale assessments of the potential extent and spatial pattern of spawning gravels. To demonstrate both the model...
HST-STIS Spectra of Saturn's Rings and Implications for Their Reddening Agent

NASA Technical Reports Server (NTRS)

Cuzzi, Jeff

2016-01-01

We obtained HST-STIS spectra of Saturn's main rings in May 2011, using the G230L (and G430L) gratings, with final averaged radial resolution of 160 (and 330) km/pixel. The dataset filled a previous 200-330nm "spectral gap" between Cassini and ground-based spectra. The data provide radial profiles as a function of wavelength, but our most basic product at this point is a set of very low-noise spectra, radially averaged over broad regions of the rings (A, B, C, and Cassini Division). The raw spectra required special processing to remove artifacts due to extended-source grating scatter. We have modeled the spectra using a new particle surface model, which corrects for on-surface shadowing due to the likely very rough ring particle surfaces, and avoids overestimation of intra-mixed "neutral absorber". We correct for non-classical layer effects and finite ring optical depth, and relate our observed reflectivities to the spherical albedos of individual smooth particles. We model these smooth particle albedos using standard Hapke theory for regolith grain mixtures that are either homogeneous and "intramixed" (nonicy absorbers dispersed in water ice regolith grains) or heterogeneous "intimate" mixtures. As candidates for the nonicy contaminants we have considered amorphous carbon, aromatic-rich and aliphatic-rich organic tholins, silicates, hematite and iron metal. For the A and B rings, we find that iron metal (including a new theoretical estimate of the refractive indices of nanometer-sized grains of iron) is not spectrally steep enough in the 200-300nm range, and that aliphatic-rich tholins are either too steep at short wavelengths or too flat at long wavelengths. However, less than 1% by mass of aromatic-rich tholins provides a very good fit across the entire spectral range with no gratuitous "neutral absorber" needed, and a minimum of additional free parameters. The best fits require forward-scattering regolith grains. For the C Ring and Cassini Division, additional absorbers are needed (updated results will be given).
Modeling and simulation of the deposition/relaxation processes of polycrystalline diatomic structures of metallic nitride films

NASA Astrophysics Data System (ADS)

García, M. F.; Restrepo-Parra, E.; Riaño-Rojas, J. C.

2015-05-01

This work develops a model that mimics the growth of diatomic, polycrystalline thin films by artificially splitting the growth into deposition and relaxation processes including two stages: (1) a grain-based stochastic method (grains orientation randomly chosen) is considered and by means of the Kinetic Monte Carlo method employing a non-standard version, known as Constant Time Stepping, the deposition is simulated. The adsorption of adatoms is accepted or rejected depending on the neighborhood conditions; furthermore, the desorption process is not included in the simulation and (2) the Monte Carlo method combined with the metropolis algorithm is used to simulate the diffusion. The model was developed by accounting for parameters that determine the morphology of the film, such as the growth temperature, the interacting atomic species, the binding energy and the material crystal structure. The modeled samples exhibited an FCC structure with grain formation with orientations in the family planes of < 111 >, < 200 > and < 220 >. The grain size and film roughness were analyzed. By construction, the grain size decreased, and the roughness increased, as the growth temperature increased. Although, during the growth process of real materials, the deposition and relaxation occurs simultaneously, this method may perhaps be valid to build realistic polycrystalline samples.
Cheap and fast measuring roughness on big surfaces with an imprint method

NASA Astrophysics Data System (ADS)

Schopf, C.; Liebl, J.; Rascher, R.

2017-10-01

Roughness, shape and structure of a surface offer information on the state, shape and surface characteristics of a component. Particularly the roughness of the surface dictates the subsequent polishing of the optical surface. The roughness is usually measured by a white light interferometer, which is limited by the size of the components. Using a moulding method of surfaces that are difficult to reach, an imprint is taken and analysed regarding to roughness and structure. This moulding compound method is successfully used in dental technology. In optical production, the moulding compound method is advantageous in roughness determination in inaccessible spots or on large components (astrological optics). The "replica method" has been around in metal analysis and processing. Film is used in order to take an impression of a surface. Then, it is analysed for structures. In optical production, compound moulding seems advantageous in roughness determination in inaccessible spots or on large components (astrological optics). In preliminary trials, different glass samples with different roughness levels were manufactured. Imprints were taken from these samples (based on DIN 54150 "Abdruckverfahren für die Oberflächenprüfung"). The objective of these feasibility tests was to determine the limits of this method (smallest roughness determinable / highest roughness). The roughness of the imprint was compared with the roughness of the glass samples. By comparing the results, the uncertainty of the measuring method was determined. The spectrum for the trials ranged from rough grind (0.8 μm rms), over finishing grind (0.6 μm rms) to polishing (0.1 μm rms).
Using quantitative analysis to understand the current and past physical processes that sculpted the Philae landing site

NASA Astrophysics Data System (ADS)

Poulet, Francois; Lucchetti, Alice; Bibring, Jean-Pierre; Langevin, Yves; Carter, John; Delbo, Marco; Eng, Pascal; Gondet, Brigitte; Jorda, Laurent; Le Mouélic, Stéphane; Mottola, Stefano; Pilorget, Cédric; Vincendon, Mathieu; Cremonese, Gabriele

2015-11-01

The CIVA cameras onboard PHILAE provided the first ever in situ images of the surface of a comet (Bibring et al., Science, 2015). The panorama acquired by CIVA at the landing site on the 67P comet reveals a rough terrain dominated by fractures and agglomerates of consolidated materials. While the composition of these materials is unknown, they provide unique structures to constrain the conditions prevailing at the surface of a comet. A quantitative analysis of the microscopic structures (grains that look like pebbles and fractures) will be presented. The pebble size distribution will be compared to the size distribution of other cometary materials such as boulders at the touchdown site (Mottola et al. Science, 2015), boulders surrounding the landing site (Lucchetti et al., A&A, submitted), >7m sized boulders globally distributed on the comet (Pajola et al., A&A, 2015), grains collected by the COSIMA experiment onboard Rosetta (Langevin et al., JGR, submitted) as well as population of grains remotely observed in coma and jets of other comets. The nature of the pebbles will be then discussed in relation to both endogenic and exogenic processes that could explain their formation. The fractures exhibit two different size distributions that are correlated to the texture of the landscape. Among different physical processes, we will evaluate whether thermal fatigue induced by diurnal temperature variations (Delbo et al. Nature, 2014) could be a mechanism of surficial fragmentation.
Numerical investigation of roughness effects in aircraft icing calculations

NASA Astrophysics Data System (ADS)

Matheis, Brian Daniel

2008-10-01

Icing codes are playing a role of increasing significance in the design and certification of ice protected aircraft surfaces. However, in the interest of computational efficiency certain small scale physics of the icing problem are grossly approximated by the codes. One such small scale phenomena is the effect of ice roughness on the development of the surface water film and on the convective heat transfer. This study uses computational methods to study the potential effect of ice roughness on both of these small scale phenomena. First, a two-dimensional condensed layer code is used to examine the effect of roughness on surface water development. It is found that the Couette approximation within the film breaks down as the wall shear goes to zero, depending on the film thickness. Roughness elements with initial flow separation in the air induce flow separation in the water layer at steady state, causing a trapping of the film. The amount of trapping for different roughness configurations is examined. Second, a three-dimensional incompressible Navier-Stokes code is developed to examine large scale ice roughness on the leading edge. The effect on the convective heat transfer and potential effect on the surface water dynamics is examined for a number of distributed roughness parameters including Reynolds number, roughness height, streamwise extent, roughness spacing and roughness shape. In most cases the roughness field increases the net average convective heat transfer on the leading edge while narrowing surface shear lines, indicating a choking of the surface water flow. Both effects show significant variation on the scale of the ice roughness. Both the change in heat transfer as well as the potential change in surface water dynamics are presented in terms of the development of singularities in the surface shear pattern. Of particular interest is the effect of the smooth zone upstream of the roughness which shows both a relatively large increase in convective heat transfer as well as excessive choking of the surface shear lines at the upstream end of the roughness field. A summary of the heat transfer results is presented for both the averaged heat transfer as well as the maximum heat transfer over each roughness element, indicating that the roughness Reynolds number is the primary parameter which characterizes the behavior of the roughness for the problem of interest.
Critical surface roughness for wall bounded flow of viscous fluids in an electric submersible pump

NASA Astrophysics Data System (ADS)

Deshmukh, Dhairyasheel; Siddique, Md Hamid; Kenyery, Frank; Samad, Abdus

2017-11-01

Surface roughness plays a vital role in the performance of an electric submersible pump (ESP). A 3-D numerical analysis has been carried out to find the roughness effect on ESP. The performance of pump for steady wall bounded turbulent flows is evaluated at different roughness values and compared with smooth surface considering a non-dimensional roughness factor K. The k- ω SST turbulence model with fine mesh at near wall region captures the rough wall effects accurately. Computational results are validated with experimental results of water (1 cP), at a design speed (3000 RPM). Maximum head is observed for a hydraulically smooth surface (K=0). When roughness factor is increased, the head decreases till critical roughness factor (K=0.1) due to frictional loss. Further increase in roughness factor (K>0.1) increases the head due to near wall turbulence. The performance of ESP is analyzed for turbulent kinetic energy and eddy viscosity at different roughness values. The wall disturbance over the rough surface affects the pressure distribution and velocity field. The roughness effect is predominant for high viscosity oil (43cP) as compared to water. Moreover, the study at off-design conditions showed that Reynolds number influences the overall roughness effect.
Skin friction measurements of systematically-varied roughness: Probing the role of roughness amplitude and skewness

NASA Astrophysics Data System (ADS)

Barros, Julio; Flack, Karen; Schultz, Michael

2017-11-01

Real-world engineering systems which feature either external or internal wall-bounded turbulent flow are routinely affected by surface roughness. This gives rise to performance degradation in the form of increased drag or head loss. However, at present there is no reliable means to predict these performance losses based upon the roughness topography alone. This work takes a systematic approach by generating random surface roughness in which the surface statistics are closely controlled. Skin friction and roughness function results will be presented for two groups of these rough surfaces. The first group is Gaussian (i.e. zero skewness) in which the root-mean-square roughness height (krms) is varied. The second group has a fixed krms, and the skewness is varied from approximately -1 to +1. The effect of the roughness amplitude and skewness on the skin friction will be discussed. Particular attention will be paid to the effect of these parameters on the roughness function in the transitionally-rough flow regime. For example, the role these parameters play in the monotonic or inflectional nature of the roughness function will be addressed. Future research into the details of the turbulence structure over these rough surfaces will also be outlined. Research funded by U.S. Office of Naval Research (ONR).
Spin relaxation in graphene nanoribbons in the presence of substrate surface roughness

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chaghazardi, Zahra; Faez, Rahim; Touski, Shoeib Babaee

2016-08-07

In this work, spin transport in corrugated armchair graphene nanoribbons (AGNRs) is studied. We survey combined effects of spin-orbit interaction and surface roughness, employing the non-equilibrium Green's function formalism and multi-orbitals tight-binding model. Rough substrate surfaces have been statistically generated and the hopping parameters are modulated based on the bending and distance of corrugated carbon atoms. The effects of surface roughness parameters, such as roughness amplitude and correlation length, on spin transport in AGNRs are studied. The increase of surface roughness amplitude results in the coupling of σ and π bands in neighboring atoms, leading to larger spin flipping ratemore » and therefore reduction of the spin-polarization, whereas a longer correlation length makes AGNR surface smoother and increases spin-polarization. Moreover, spin diffusion length of carriers is extracted and its dependency on the roughness parameters is investigated. In agreement with experimental data, the spin diffusion length for various substrate ranges between 2 and 340 μm. Our results indicate the importance of surface roughness on spin-transport in graphene.« less
Surface texture of Vesta from optical polarimetry

NASA Technical Reports Server (NTRS)

Le Bertre, T.; Zellner, B.

1980-01-01

Polarimetric, photometric, and reflective spectroscopic properties of asteroid 4 Vesta are simulated in the laboratory by a preparation of eucrite Bereba consisting of a broad mixture of particle sizes (mainly greater than 50-micron) mixed and partially coated with particles of size 10 microns and less. Coarse grains are necessary for producing the same albedo and a very fine dust coating is necessary for producing the same polarization inversion angle as observed for Vesta. There are less small grains and fine dust in this sample than in lunar soils. Photometrically, if coating a sphere, this sample shows a constant brightness on the sunward half of the observed hemisphere, the brightness being given on the other half by the Minnaert reciprocity principle. With such a photometric behavior, the global geometric albedo and the sub-earth point geometric albedo differ by no more than 5%. The microscopic phase coefficient is 0.021 magnitude per degree for the sample; the larger value, 0.025, observed telescopically for Vesta, indicates that large-scale roughness is present on this asteroid.

Effects of choline chloride on electrodeposited Ni coating from a Watts-type bath

NASA Astrophysics Data System (ADS)

Wang, Yurong; Yang, Caihong; He, Jiawei; Wang, Wenchang; Mitsuzak, Naotoshi; Chen, Zhidong

2016-05-01

Electrodeposition of bright nickel (Ni) was carried out in a Watts-type bath. Choline chloride (ChCl) was applied as a multifunctional additive and substitute for nickel chloride (NiCl2) in a Watts-type bath. The function of ChCl was investigated through conductivity tests, anodic polarization, and cathodic polarization experiments. The studies revealed that ChCl performed well as a conducting salt, anodic activator, and cathodic inhibitor. The effects of ChCl on deposition rate, preferred orientation, grain size, surface morphology, and microhardness of Ni coatings were also studied. The deposition rate reached a maximum value of greater than 27 μm h-1 when 20 g L-1 ChCl was introduced to the bath. Using X-ray diffraction, it was confirmed that progressive addition of ChCl promoted the preferred crystal orientation modification from (2 0 0) and (2 2 0) to (1 1 1), refined grain size, and enhanced microhardness. The presence of ChCl lowered the roughness of the coating.
Experimental Research on Fatigue Failure for 2219-T6 Aluminum Alloy Friction Stir-Welded Joints

NASA Astrophysics Data System (ADS)

Sun, Guo-Qin; Niu, Jiang-Pei; Chen, Ya-Jing; Sun, Feng-Yang; Shang, De-Guang; Chen, Shu-Jun

2017-08-01

The fatigue experiment was executed for the 2219-T6 aluminum alloy friction stir-welded joints at the rotation speed of 800 r/min and the welding velocity of 150 mm/min. Most fatigue failures occurred in the weld nugget zone (WNZ), the thermo-mechanical affected zone and the nearby areas. The experimental results demonstrated that the sudden hardness gradient increases sites corresponding to the fatigue failure locations. The high-angle grain boundaries with the highest concentration were scattered within the WNZ. The microcracks initiated at the intersection of the soft grains. More than one crack initiation site was observed within the WNZ and the thermo-mechanical affected zone, when the fracture occurred in these areas. The rough surface of the welding area should be one of the main reasons for the fatigue failure occurrence. The fatigue crack growth rate in the WNZ at the first stage was fastest in comparison with the fatigue crack growth rate in the other areas of the joint.
Recrystallization and modification of the stainless-steel surface relief under photonic heat load in powerful plasma discharges

DOE Office of Scientific and Technical Information (OSTI.GOV)

Budaev, V. P., E-mail: budaev@mail.ru; Martynenko, Yu. V.; Khimchenko, L. N.

Targets made of ITER-grade 316L(N)-IG stainless steel and Russian-grade 12Cr18Ni10Ti stainless steel with a close composition were exposed at the QSPA-T plasma gun to plasma photonic radiation pulses simulating conditions of disruption mitigation in ITER. After a large number of pulses, modification of the stainless-steel surface was observed, such as the formation of a wavy structure, irregular roughness, and cracks on the target surface. X-ray and optic microscopic analyses of targets revealed changes in the orientation and dimensions of crystallites (grains) over a depth of up to 20 μm for 316L(N)-IG stainless steel after 200 pulses and up to 40more » μm for 12Cr18Ni10Ti stainless steel after 50 pulses, which is significantly larger than the depth of the layer melted in one pulse (∼10 μm). In a series of 200 tests of ITER-grade 316L(N)-IG ITER stainless steel, a linear increase in the height of irregularity (roughness) with increasing number of pulses at a rate of up to ∼1 μm per pulse was observed. No alteration in the chemical composition of the stainless-steel surface in the series of tests was revealed. A model is developed that describes the formation of wavy irregularities on the melted metal surface with allowance for the nonlinear stage of instability of the melted layer with a vapor/plasma flow above it. A decisive factor in this case is the viscous flow of the melted metal from the troughs to tops of the wavy structure. The model predicts saturation of the growth of the wavy structure when its amplitude becomes comparable with its wavelength. Approaches to describing the observed stochastic relief and roughness of the stainless-steel surface formed in the series of tests are considered. The recurrence of the melting-solidification process in which mechanisms of the hill growth compete with the spreading of the material from the hills can result in the formation of a stochastic relief.« less
Graphene thickness dependent adhesion force and its correlation to surface roughness

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pourzand, Hoorad; Tabib-Azar, Massood, E-mail: azar.m@utah.edu; Biomedical Engineering, University of Utah, Salt Lake City, Utah 84112

2014-04-28

In this paper, adhesion force of graphene layers on 300 nm silicon oxide is studied. A simple model for measuring adhesion force for a flat surface with sub-nanometer roughness was developed and is shown that small surface roughness decreases adhesion force while large roughness results in an effectively larger adhesion forces. We also show that surface roughness over scales comparable to the tip radius increase by nearly a factor of two, the effective adhesion force measured by the atomic force microscopy. Thus, we demonstrate that surface roughness is an important parameter that should be taken into account in analyzing the adhesionmore » force measurement results.« less
Optimum surface roughness prediction for titanium alloy by adopting response surface methodology

NASA Astrophysics Data System (ADS)

Yang, Aimin; Han, Yang; Pan, Yuhang; Xing, Hongwei; Li, Jinze

Titanium alloy has been widely applied in industrial engineering products due to its advantages of great corrosion resistance and high specific strength. This paper investigated the processing parameters for finish turning of titanium alloy TC11. Firstly, a three-factor central composite design of experiment, considering the cutting speed, feed rate and depth of cut, are conducted in titanium alloy TC11 and the corresponding surface roughness are obtained. Then a mathematic model is constructed by the response surface methodology to fit the relationship between the process parameters and the surface roughness. The prediction accuracy was verified by the one-way ANOVA. Finally, the contour line of the surface roughness under different combination of process parameters are obtained and used for the optimum surface roughness prediction. Verification experimental results demonstrated that material removal rate (MRR) at the obtained optimum can be significantly improved without sacrificing the surface roughness.
Radiometric Measurements of the Thermal Conductivity of Complex Planetary-like Materials

NASA Astrophysics Data System (ADS)

Piqueux, S.; Christensen, P. R.

2012-12-01

Planetary surface temperatures and thermal inertias are controlled by the physical and compositional characteristics of the surface layer material, which result from current and past geological activity. For this reason, temperature measurements are often acquired because they provide fundamental constraints on the geological history and habitability. Examples of regolith properties affecting surface temperatures and inertias are: grain sizes and mixture ratios, solid composition in the case of ices, presence of cement between grains, regolith porosity, grain roughness, material layering etc.. Other important factors include volatile phase changes, and endogenic or exogenic heat sources (i.e. geothermal heat flow, impact-related heat, biological activity etc.). In the case of Mars, the multitude of instruments observing the surface temperature at different spatial and temporal resolutions (i.e. IRTM, Thermoskan, TES, MiniTES, THEMIS, MCS, REMS, etc.) in conjunction with other instruments allows us to probe and characterize the thermal properties of the surface layer with an unprecedented resolution. While the derivation of thermal inertia values from temperature measurements is routinely performed by well-established planetary regolith numerical models, constraining the physical properties of the surface layer from thermal inertia values requires the additional step of laboratory measurements. The density and specific heat are usually constant and sufficiently well known for common geological materials, but the bulk thermal conductivity is highly variable as a function of the physical characteristics of the regolith. Most laboratory designs do not allow an investigation of the thermal conductivity of complex regolith configurations similar to those observed on planetary surfaces (i.e. cemented material, large grains, layered material, and temperature effects) because the samples are too small and need to be soft to insert heating or measuring devices. For this reason, we have built a new type of apparatus to measure the thermal conductivity of sample significantly larger than previous apparatus under planetary conditions of atmosphere and gas composition. Samples' edges are cooled down from room to LN2 temperature and the surface material temperature is recorded by an infrared camera without inserting thermocouples or heat sources. Sample surface cooling trends are fit with finite element models of heat transfer to retrieve the material thermal conductivity. Preliminary results confirm independent numerical modeling results predicting the thermal conductivity of complex materials: the thermal inertia of particulate material under Mars conditions is temperature-dependent, small amounts of cements significantly increase the bulk conductivity and inertia of particulate material, and one-grain-thick armors similar to those observed by the Mars Exploration Rovers behave like a thin highly conductive layer that does not significantly influence apparent thermal inertias. These results are used to further our interpretation of Martian temperature observations. For example local amounts of subsurface water ice or the fraction of cementing phase in the global Martian duricrust can be constrained; the search for subtle changes in near-surface heat flow can be performed more accurately, and surface thermal inertias under various atmospheric conditions of pressure and gas composition can be predicted.
Monitoring of Surface Roughness in Aluminium Turning Process

NASA Astrophysics Data System (ADS)

Chaijareenont, Atitaya; Tangjitsitcharoen, Somkiat

2018-01-01

As the turning process is one of the most necessary process. The surface roughness has been considered for the quality of workpiece. There are many factors which affect the surface roughness. Hence, the objective of this research is to monitor the relation between the surface roughness and the cutting forces in aluminium turning process with a wide range of cutting conditions. The coated carbide tool and aluminium alloy (Al 6063) are used for this experiment. The cutting parameters are investigated to analyze the effects of them on the surface roughness which are the cutting speed, the feed rate, the tool nose radius and the depth of cut. In the case of this research, the dynamometer is installed in the turret of CNC turning machine to generate a signal while turning. The relation between dynamic cutting forces and the surface roughness profile is examined by applying the Fast Fourier Transform (FFT). The experimentally obtained results showed that the cutting force depends on the cutting condition. The surface roughness can be improved when increasing the cutting speed and the tool nose radius in contrast to the feed rate and the depth of cut. The relation between the cutting parameters and the surface roughness can be explained by the in-process cutting forces. It is understood that the in-process cutting forces are able to predict the surface roughness in the further research.
Numerical Simulations of Granular Physics in the Solar System

NASA Astrophysics Data System (ADS)

Ballouz, Ronald

2017-08-01

Granular physics is a sub-discipline of physics that attempts to combine principles that have been developed for both solid-state physics and engineering (such as soil mechanics) with fluid dynamics in order to formulate a coherent theory for the description of granular materials, which are found in both terrestrial (e.g., earthquakes, landslides, and pharmaceuticals) and extra-terrestrial settings (e.g., asteroids surfaces, asteroid interiors, and planetary ring systems). In the case of our solar system, the growth of this sub-discipline has been key in helping to interpret the formation, structure, and evolution of both asteroids and planetary rings. It is difficult to develop a deterministic theory for granular materials due to the fact that granular systems are composed of a large number of elements that interact through a non-linear combination of various forces (mechanical, gravitational, and electrostatic, for example) leading to a high degree of stochasticity. Hence, we study these environments using an N-body code, pkdgrav, that is able to simulate the gravitational, collisional, and cohesive interactions of grains. Using pkdgrav, I have studied the size segregation on asteroid surfaces due to seismic shaking (the Brazil-nut effect), the interaction of the OSIRIS-REx asteroid sample-return mission sampling head, TAGSAM, with the surface of the asteroid Bennu, the collisional disruptions of rubble-pile asteroids, and the formation of structure in Saturn's rings. In all of these scenarios, I have found that the evolution of a granular system depends sensitively on the intrinsic properties of the individual grains (size, shape, sand surface roughness). For example, through our simulations, we have been able to determine relationships between regolith properties and the amount of surface penetration a spacecraft achieves upon landing. Furthermore, we have demonstrated that this relationship also depends on the strength of the local gravity. By comparing our numerical results to laboratory experiments and observations by spacecraft we can begin to understand which microscopic properties (i.e., grain properties) control the macroscopic properties of the system. For example, we can compare the mechanical response of a spacecraft to landing or Cassini observations of Saturn's ring to understand how the penetration depth of a spacecraft or the complex optical depth structure of a ring system depends on the size and surface properties of the grains in those systems.
Super Water-Repellent Fractal Surfaces of a Photochromic Diarylethene Induced by UV Light

NASA Astrophysics Data System (ADS)

Izumi, Norikazu; Minami, Takayuki; Mayama, Hiroyuki; Takata, Atsushi; Nakamura, Shinichiro; Yokojima, Satoshi; Tsujii, Kaoru; Uchida, Kingo

2008-09-01

Photochromic diarylethene forms super water-repellent surfaces upon irradiation with UV light. Microfibril-like crystals grow on the solid diarylethene surface after UV irradiation, and the contact angle of water on the surface becomes larger with increasing surface roughness with time. The fractal analysis was made by the box-counting method for the rough surfaces. There are three regions in the roughness size having the fractal dimension of ca. 2.4 (size of roughness smaller than 5 µm), of ca. 2.2 (size of roughness between 5-40 µm), and of ca. 2.0 (size of roughness larger than 40 µm). The fractal dimension of ca. 2.4 was due to the fibril-like structures generated gradually by UV irradiation on diarylethene surfaces accompanied with an increase in the contact angle. The surface structure with larger fractal dimension mainly contributes to realizing the super water-repellency of the diarylethene surfaces. This mechanism of spontaneous formation of fractal surfaces is similar to that for triglyceride and alkylketene dimer waxes.
Measuring skew in average surface roughness as a function of surface preparation

NASA Astrophysics Data System (ADS)

Stahl, Mark T.

2015-08-01

Characterizing surface roughness is important for predicting optical performance. Better measurement of surface roughness reduces polishing time, saves money and allows the science requirements to be better defined. This study characterized statistics of average surface roughness as a function of polishing time. Average surface roughness was measured at 81 locations using a Zygo® white light interferometer at regular intervals during the polishing process. Each data set was fit to a normal and Largest Extreme Value (LEV) distribution; then tested for goodness of fit. We show that the skew in the average data changes as a function of polishing time.
Passive microwave sensing of soil moisture content: Soil bulk density and surface roughness

NASA Technical Reports Server (NTRS)

Wang, J. R.

1982-01-01

Microwave radiometric measurements over bare fields of different surface roughnesses were made at the frequencies of 1.4 GHz, 5 GHz, and 10.7 GHz to study the frequency dependence as well as the possible time variation of surface roughness. The presence of surface roughness was found to increase the brightness temperature of soils and reduce the slope of regression between brightness temperature and soil moisture content. The frequency dependence of the surface roughness effect was relatively weak when compared with that of the vegetation effect. Radiometric time series observation over a given field indicated that field surface roughness might gradually diminish with time, especially after a rainfall or irrigation. This time variation of surface roughness served to enhance the uncertainty in remote soil moisture estimate by microwave radiometry. Three years of radiometric measurements over a test site revealed a possible inconsistency in the soil bulk density determination, which turned out to be an important factor in the interpretation of radiometric data.
Passive microwave sensing of soil moisture content - The effects of soil bulk density and surface roughness

NASA Technical Reports Server (NTRS)

Wang, J. R.

1983-01-01

Microwave radiometric measurements over bare fields of different surface roughness were made at frequencies of 1.4 GHz, 5 GHz, and 10.7 GHz to study the frequency dependence, as well as the possible time variation, of surface roughness. An increase in surface roughness was found to increase the brightness temperature of soils and reduce the slope of regression between brightness temperature and soil moisture content. The frequency dependence of the surface roughness effect was relatively weak when compared with that of the vegetation effect. Radiometric time-series observations over a given field indicate that field surface roughness might gradually diminish with time, especially after a rainfall or irrigation. The variation of surface roughness increases the uncertainty of remote soil moisture estimates by microwave radiometry. Three years of radiometric measurements over a test site revealed a possible inconsistency in the soil bulk density determination, which is an important factor in the interpretation of radiometric data.
DOE Office of Scientific and Technical Information (OSTI.GOV)

Holesinger, T. G.; Carpenter, J. S.; Lienert, T. J.

The ability of additive manufacturing to directly fabricate complex shapes provides characterization challenges for part qualification. The orientation of the microstructures produced by these processes will change relative to the surface normal of a complex part. In this work, the microscopy and x-ray tomography of an AlSi10Mg alloy hemispherical shell fabricated using powder bed metal additive manufacturing are used to illustrate some of these challenges. The shell was manufactured using an EOS M280 system in combination with EOS-specified powder and process parameters. The layer-by-layer process of building the shell with the powder bed additive manufacturing approach results in a position-dependentmore » microstructure that continuously changes its orientation relative to the shell surface normal. X-ray tomography was utilized to examine the position-dependent size and distribution of porosity and surface roughness in the 98.6% dense part. Optical and electron microscopy were used to identify global and local position-dependent structures, grain morphologies, chemistry, and precipitate sizes and distributions. The rapid solidification processes within the fusion zone (FZ) after the laser transit results in a small dendrite size. Cell spacings taken from the structure in the middle of the FZ were used with published relationships to estimate a cooling rate of ~9 × 10 5 K/s. Uniformly-distributed, nanoscale Si precipitates were found within the primary α-Al grains. A thin, distinct boundary layer containing larger α-Al grains and extended regions of the nanocrystalline divorced eutectic material surrounds the FZ. Moreover, subtle differences in the composition between the latter layer and the interior of the FZ were noted with scanning transmission electron microscopy (STEM) spectral imaging.« less
Characterization of an aluminum alloy hemispherical shell fabricated via direct metal laser melting

DOE PAGES

Holesinger, T. G.; Carpenter, J. S.; Lienert, T. J.; ...

2016-01-11

The ability of additive manufacturing to directly fabricate complex shapes provides characterization challenges for part qualification. The orientation of the microstructures produced by these processes will change relative to the surface normal of a complex part. In this work, the microscopy and x-ray tomography of an AlSi10Mg alloy hemispherical shell fabricated using powder bed metal additive manufacturing are used to illustrate some of these challenges. The shell was manufactured using an EOS M280 system in combination with EOS-specified powder and process parameters. The layer-by-layer process of building the shell with the powder bed additive manufacturing approach results in a position-dependentmore » microstructure that continuously changes its orientation relative to the shell surface normal. X-ray tomography was utilized to examine the position-dependent size and distribution of porosity and surface roughness in the 98.6% dense part. Optical and electron microscopy were used to identify global and local position-dependent structures, grain morphologies, chemistry, and precipitate sizes and distributions. The rapid solidification processes within the fusion zone (FZ) after the laser transit results in a small dendrite size. Cell spacings taken from the structure in the middle of the FZ were used with published relationships to estimate a cooling rate of ~9 × 10 5 K/s. Uniformly-distributed, nanoscale Si precipitates were found within the primary α-Al grains. A thin, distinct boundary layer containing larger α-Al grains and extended regions of the nanocrystalline divorced eutectic material surrounds the FZ. Moreover, subtle differences in the composition between the latter layer and the interior of the FZ were noted with scanning transmission electron microscopy (STEM) spectral imaging.« less
Characterization of an Aluminum Alloy Hemispherical Shell Fabricated via Direct Metal Laser Melting

NASA Astrophysics Data System (ADS)

Holesinger, T. G.; Carpenter, J. S.; Lienert, T. J.; Patterson, B. M.; Papin, P. A.; Swenson, H.; Cordes, N. L.

2016-03-01

The ability of additive manufacturing to directly fabricate complex shapes provides characterization challenges for part qualification. The orientation of the microstructures produced by these processes will change relative to the surface normal of a complex part. In this work, the microscopy and x-ray tomography of an AlSi10Mg alloy hemispherical shell fabricated using powder bed metal additive manufacturing are used to illustrate some of these challenges. The shell was manufactured using an EOS M280 system in combination with EOS-specified powder and process parameters. The layer-by-layer process of building the shell with the powder bed additive manufacturing approach results in a position-dependent microstructure that continuously changes its orientation relative to the shell surface normal. X-ray tomography was utilized to examine the position-dependent size and distribution of porosity and surface roughness in the 98.6% dense part. Optical and electron microscopy were used to identify global and local position-dependent structures, grain morphologies, chemistry, and precipitate sizes and distributions. The rapid solidification processes within the fusion zone (FZ) after the laser transit results in a small dendrite size. Cell spacings taken from the structure in the middle of the FZ were used with published relationships to estimate a cooling rate of ~9 × 105 K/s. Uniformly-distributed, nanoscale Si precipitates were found within the primary α-Al grains. A thin, distinct boundary layer containing larger α-Al grains and extended regions of the nanocrystalline divorced eutectic material surrounds the FZ. Subtle differences in the composition between the latter layer and the interior of the FZ were noted with scanning transmission electron microscopy (STEM) spectral imaging.
Numerical reproduction and explanation of road surface mirages under grazing-angle scattering.

PubMed

Lu, Jia; Zhou, Huaichun

2017-07-01

The mirror-like reflection image of the road surface under grazing-angle scattering can be easily observed in daily life. It was suggested that road surface mirages may occur due to a light-enhancing effect of the rough surface under grazing-angle scattering. The main purpose of this work is to explain the light-enhancing mechanism of rough surfaces under grazing-angle scattering. The off-specular reflection from a random rough magnesium oxide ceramic surface is analyzed by using the geometric optics approximation method. Then, the geometric optics approximation method is employed to develop a theoretical model to predict the observation effect of the grazing-angle scattering phenomenon of the road surface. The rough surface is assumed to consist of small-scale rough surface facets. The road surface mirage is reproduced from a large number of small-scale rough surface facets within the eye's resolution limit at grazing scattering angles, as the average bidirectional reflectance distribution function value at the bright location is about twice that of the surface in front of the mirage. It is suggested that the light-enhancing effect of the rough surface under grazing-angle scattering is not proper to be termed as "off-specular reflection," since it has nothing to do with the "specular" direction with respect to the incident direction.
Limitations to the Measurement of Oxygen Concentrations by HRTEM Imposed by Surface Roughness

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lupini, Andrew R; Chisholm, Matthew F; van Benthem, Klaus

2005-01-01

In an article published in Microscopy and Microanalysis recently (Jia et al., 2004), it was claimed that aberration-corrected high resolution transmission electron microscopy (HRTEM) allows the quantitative measurement of oxygen concentrations in ceramic materials with atomic resolution. Similar claims have recently appeared elsewhere, based on images obtained through aberration correction (Jia et al., 2003; Jia & Urban, 2004) or very high voltages (Zhang et al., 2003). Seeing oxygen columns is a significant achievement of great importance (Spence, 2003) that will doubtlessly allow some exciting new science; however, other models could provide a better explanation for some of the experimental datamore » than variations in the oxygen concentration. Quantification of the oxygen concentrations was attempted by comparing experimental images with simulations in which the fractional occupancy in individual oxygen columns was reduced. The results were interpreted as representing nonstoichiometry within the bulk and at grain boundaries. This is plausible because previous studies have shown that grain boundaries can be nonstoichiometric (Kim et al., 2001), and it is indeed possible that oxygen vacancies are present at boundaries or in the bulk. However, is this the only possible interpretation? We show that for the thicknesses considered a better match to the images is obtained using a simple model of surface damage in which atoms are removed from the surface, which would usually be interpreted as surface damage or local thickness variation (from ion milling, for example).« less
Characteristics of surface roughness associated with leading edge ice accretion

NASA Technical Reports Server (NTRS)

Shin, Jaiwon

1994-01-01

Detailed size measurements of surface roughness associated with leading edge ice accretions are presented to provide information on characteristics of roughness and trends of roughness development with various icing parameters. Data was obtained from icing tests conducted in the Icing Research Tunnel (IRT) at NASA Lewis Research Center (LeRC) using a NACA 0012 airfoil. Measurements include diameters, heights, and spacing of roughness elements along with chordwise icing limits. Results confirm the existence of smooth and rough ice zones and that the boundary between the two zones (surface roughness transition region) moves upstream towards stagnation region with time. The height of roughness grows as the air temperature and the liquid water content increase, however, the airspeed has little effect on the roughness height. Results also show that the roughness in the surface roughness transition region grows during a very early stage of accretion but reaches a critical height and then remains fairly constant. Results also indicate that a uniformly distributed roughness model is only valid at a very initial stage of the ice accretion process.
Incorporating Skew into RMS Surface Roughness Probability Distribution

NASA Technical Reports Server (NTRS)

Stahl, Mark T.; Stahl, H. Philip.

2013-01-01

The standard treatment of RMS surface roughness data is the application of a Gaussian probability distribution. This handling of surface roughness ignores the skew present in the surface and overestimates the most probable RMS of the surface, the mode. Using experimental data we confirm the Gaussian distribution overestimates the mode and application of an asymmetric distribution provides a better fit. Implementing the proposed asymmetric distribution into the optical manufacturing process would reduce the polishing time required to meet surface roughness specifications.
Experimental Measurements of Permeability Evolution along Faults during Progressive Slip

NASA Astrophysics Data System (ADS)

Strutz, M.; Mitchell, T. M.; Renner, J.

2010-12-01

Little is currently known about the dynamic changes in fault-parallel permeability along rough faults during progressive slip. With increasing slip, asperities are worn to produce gouge which can dramatically reduce along fault permeability within the slip zone. However, faults can have a range of roughness which can affect both the porosity and both the amount and distribution of fault wear material produced in the slipping zone during the early stages of fault evolution. In this novel study we investigate experimentally the evolution of permeability along a fault plane in granite sawcut sliding blocks with a variety of intial roughnesses in a triaxial apparatus. Drillholes in the samples allow the permeability to be measured along the fault plane during loading and subsequent fault displacement. Use of the pore pressure oscillation technique (PPO) allows the continuous measurement of permeability without having to stop loading. To achieve a range of intial starting roughnesses, faults sawcut surfaces were prepared using a variety of corundum powders ranging from 10 µm to 220 µm, and for coarser roughness were air-blasted with glass beads up to 800µm in size. Fault roughness has been quantified with a laser profileometer. During sliding, we measure the acoustic emissions in order to detect grain cracking and asperity shearing which may relate to both the mechanical and permeability data. Permeability shows relative reductions of up to over 4 orders of magnitude during stable sliding as asperities are sheared to produce a fine fault gouge. This variation in permeability is greatest for the roughest faults, reducing as fault roughness decreases. The onset of permeability reduction is contemporaneous with a dramatic reduction in the amount of detected acoustic emissions, where a continuous layer of fault gouge has developed. The amount of fault gouge produced is related to the initial roughness, with the rough faults showing larger fault gouge layers at the end of slip. Following large stress drops and stick slip events, permeability can both increase and decrease due to dynamic changes in pore pressure during fast sliding events. We present a summary of preliminary data to date, and discuss some of the problems and unknowns when using the PPO method to measure permeability.

Investigation of rough surfaces on Cu2ZnSn(SxSe1-x)4 monograin layers using light beam induced current measurements

NASA Astrophysics Data System (ADS)

Neubauer, Christian; Babatas, Ertug; Meissner, Dieter

2017-11-01

Monograin technology has proven to be a successful way of manufacturing low cost photovoltaic applications using the pentanary Cu2ZnSn(SxSe1-x)4 (CZTSSe) as an absorber material in an industrial roll-to-roll process. For high efficient CZTSSe monograin device fabrication a thorough understanding of the impacts of the device characteristics and surface structure is important. A new evaluation method of Light Beam Induced Current (LBIC) images had to be developed to distinguish between different effects resulting from different surface orientations, grain sizes, packing densities and contacting areas. In this work we will show that with LBIC measurements it is possible to evaluate the quality and differences in produced CZTSSe monograin cells in a post-production and non-destructive step. The high spatial resolution evaluation allows investigating the homogeneity of single crystalline grains as well as certain areas of a CZTSSe device. By introducing a statistical method the active area as a major factor for the current density of a device will be calculated and evaluated. The results show that with LBIC measurements the active area can be quantified, which differs for the investigated cells up to 9%. Additionally, the homogeneity of short circuit current densities of the monograins and also of certain areas of a cell can be detected and quantified.
Soil roughness, slope and surface storage relationship for impervious areas

NASA Astrophysics Data System (ADS)

Borselli, Lorenzo; Torri, Dino

2010-11-01

SummaryThe study of the relationships between surface roughness, local slope gradient and maximum volume of water storage in surface depressions is a fundamental element in the development of hydrological models to be used in soil and water conservation strategies. Good estimates of the maximum volume of water storage are important for runoff assessment during rainfall events. Some attempts to link surface storage to parameters such as indices of surface roughness and, more rarely, local gradient have been proposed by several authors with empirical equations often conflicting between them and usually based on a narrow range of slope gradients. This suggests care in selecting any of the proposed equations or models and invites one to verify the existence of more realistic experimental relationships, based on physical models of the surfaces and valid for a larger range of gradients. The aim of this study is to develop such a relation for predicting/estimating the maximum volume of water that a soil surface, with given roughness characteristics and local slope gradient, can store. Experimental work has been carried out in order to reproduce reliable rough surfaces able to maintain the following properties during the experimental activity: (a) impervious surface to avoid biased storage determination; (b) stable, un-erodible surfaces to avoid changes of retention volume during tests; (c) absence of hydrophobic behaviour. To meet the conditions a-c we generate physical surfaces with various roughness magnitude using plasticine (emulsion of non-expansible clay and oil). The plasticine surface, reproducing surfaces of arable soils, was then wetted and dirtied with a very fine timber sawdust. This reduced the natural hydrophobic behaviour of the plasticine to an undetectable value. Storage experiments were conducted with plasticine rough surfaces on top of large rigid polystyrene plates inclined at different slope gradient: 2%, 5%, 10%, 20%, 30%. Roughness data collected on the generated plasticine surfaces were successfully compared with roughness data collected on real soil surfaces for similar conditions. A set of roughness indices was computed for each surface using roughness profiles measured with a laser profile meter. Roughness indices included quantiles of the Abbot-Firestone curve, which is used in surface metrology for industrial application to characterize surface roughness in a non-parametric approach ( Whitehouse, 1994). Storage data were fitted with an empirical equation (double negative exponential of roughness and slope). Several roughness indices resulted well related to storage. The better results were obtained using the Abbot-Firestone curve parameter P100. Beside this storage empirical model (SEM) a geometrical model was also developed, trying to give a more physical basis to the result obtained so far. Depression geometry was approximated with spherical cups. A general physical model was derived (storage cup model - SCM). The cup approximation identifies where roughness elevation comes in and how it relates to slope gradient in defining depression volume. Moreover, the exponential decay used for assessing slope effect on storage volume in the empirical model of Eqs. (8) and (9) emerges as consistent with distribution of cup sizes.
Shear enhanced compaction-solution bands in quartz-rich calcarenites of the Cotiella Massif (Spanish Pyrennes)

NASA Astrophysics Data System (ADS)

Tavani, Stefano; Granado, Pablo; Cantanero, Irene; Balsamo, Fabrizio; Corradetti, Amerigo; Muñoz, Josep

2017-04-01

In this contribution we describe deformation bands developed due to the interplay between shearing and mechanical and chemical compaction in Paleocene quartz-rich calcarenites. The studied structures are located in the footwall of the Cotiella Thrust (Spanish Pyrennes) and form anastomosed, mm-thick tabular bands, composed of high concentration of quartz grains. The bands strike perpendicular to the local transport direction of the regional thrust sheet, thus indicating a tectonic origin, and are organized in three sets. One set is perpendicular to the shallow-dipping bedding surface, while the other two are roughly perpendicular to each other and form an angle of 45°, in opposite directions, with the bedding. No macroscopic evidence of shearing is found along these bands. Optical microscope and SEM investigations on both undeformed and deformed rocks indicate that the high concentration of quartz within the deformation bands was caused by the localized pressure-enhanced dissolution of calcite grains, which determined the enrichment of the less soluble quartz grains. Quartz grains fracturing, fragmentation and crushing was observed along in all deformation bands, whereas cataclasis and shear occurs only along oblique oblique-to-bedding sets. All these features indicate that studied deformation bands are hybrid structures most likely developed during layer-parallel shortening. In detail, bedding perpendicular and bedding oblique structures can be interpreted as pure compaction and shear-enhanced compaction bands, respectively.
Cemented fixation with PMMA or Bis-GMA resin hydroxyapatite cement: effect of implant surface roughness.

PubMed

Walsh, W R; Svehla, M J; Russell, J; Saito, M; Nakashima, T; Gillies, R M; Bruce, W; Hori, R

2004-09-01

Implant surface roughness is an important parameter governing the overall mechanical properties at the implant-cement interface. This study investigated the influence of surface roughness using polymethylmethcrylate (PMMA) and a Bisphenol-a-glycidylmethacyrlate resin-hydroxyapatite cement (CAP). Mechanical fixation at the implant-cement interface was evaluated in vitro using static shear and fatigue loading with cobalt chrome alloy (CoCr) dowels with different surface roughness preparations. Increasing surface roughness improved the mechanical properties at the implant-cement interface for both types of cement. CAP cement fixation was superior to PMMA under static and dynamic loading.
Aerodynamics of a finite wing with simulated ice

NASA Technical Reports Server (NTRS)

Bragg, M. B.; Khodadoust, A.; Kerho, M.

1992-01-01

The effect of a simulated glaze ice accretion on the aerodynamic performance of a three-dimensional wing is studied experimentally. Results are reviewed from earlier two-dimensional tests which show the character of the large leading-edge separation bubbles caused by the simulated ice accretion. The 2-D bubbles are found to closely resemble well known airfoil laminar separation bubbles. For the 3-D experiments a semispan wing of effective aspect ratio five was mounted from the sidewall of the UIUC subsonic wind tunnel. The model uses a NACA 0012 airfoil section on a rectangular planform with interchangeable tip and root sections to allow for 0- and 30-degree sweep. A three-component sidewall balance was used to measure lift, drag and pitching moment on the clean and iced model. Fluorescent oil flow visualization has been performed on the iced model and reveals extensive spanwise and vortical flow in the separation bubble aft of the upper surface horn. Sidewall interaction and spanwise nonuniformity are also seen on the unswept model. Comparisons to the computed flow fields are shown. Results are also shown for roughness effects on the straight wing. Sand grain roughness on the ice shape is seen to have a different effect than isolated 3-D roughness elements.
Growth of porous anodized alumina on the sputtered aluminum films with 2D-3D morphology for high specific surface area

NASA Astrophysics Data System (ADS)

Liao, M. W.; Chung, C. K.

2014-08-01

The porous anodic aluminum oxide (AAO) with high-aspect-ratio pore channels is widely used as a template for fabricating nanowires or other one-dimensional (1D) nanostructures. The high specific surface area of AAO can also be applied to the super capacitor and the supporting substrate for catalysis. The rough surface could be helpful to enhance specific surface area but it generally results in electrical field concentration even to ruin AAO. In this article, the aluminum (Al) films with the varied 2D-3D morphology on Si substrates were prepared using magnetron sputtering at a power of 50 W-185 W for 1 h at a working pressure of 2.5 × 10-1 Pa. Then, AAO was fabricated from the different Al films by means of one-step hybrid pulse anodizing (HPA) between the positive 40 V and the negative -2 V (1 s:1 s) for 3 min in 0.3 M oxalic acid at a room temperature. The microstructure and morphology of Al films were characterized by X-ray diffraction, scanning electron microscope and atomic force microscope, respectively. Some hillocks formed at the high target power could be attributed to the grain texture growth in the normal orientation of Al(1 1 1). The 3D porous AAO structure which is different from the conventional 2D planar one has been successfully demonstrated using HPA on the film with greatly rough hillock-surface formed at the highest power of 185 W. It offers a potential application of the new 3D AAO to high specific surface area devices.
Optimization of Surface Roughness and Wall Thickness in Dieless Incremental Forming Of Aluminum Sheet Using Taguchi

NASA Astrophysics Data System (ADS)

Hamedon, Zamzuri; Kuang, Shea Cheng; Jaafar, Hasnulhadi; Azhari, Azmir

2018-03-01

Incremental sheet forming is a versatile sheet metal forming process where a sheet metal is formed into its final shape by a series of localized deformation without a specialised die. However, it still has many shortcomings that need to be overcome such as geometric accuracy, surface roughness, formability, forming speed, and so on. This project focus on minimising the surface roughness of aluminium sheet and improving its thickness uniformity in incremental sheet forming via optimisation of wall angle, feed rate, and step size. Besides, the effect of wall angle, feed rate, and step size to the surface roughness and thickness uniformity of aluminium sheet was investigated in this project. From the results, it was observed that surface roughness and thickness uniformity were inversely varied due to the formation of surface waviness. Increase in feed rate and decrease in step size will produce a lower surface roughness, while uniform thickness reduction was obtained by reducing the wall angle and step size. By using Taguchi analysis, the optimum parameters for minimum surface roughness and uniform thickness reduction of aluminium sheet were determined. The finding of this project helps to reduce the time in optimising the surface roughness and thickness uniformity in incremental sheet forming.
Investigation of the influence of a step change in surface roughness on turbulent heat transfer

NASA Technical Reports Server (NTRS)

Taylor, Robert P.; Coleman, Hugh W.; Taylor, J. Keith; Hosni, M. H.

1991-01-01

The use is studied of smooth heat flux gages on the otherwise very rough SSME fuel pump turbine blades. To gain insights into behavior of such installations, fluid mechanics and heat transfer data were collected and are reported for a turbulent boundary layer over a surface with a step change from a rough surface to a smooth surface. The first 0.9 m length of the flat plate test surface was roughened with 1.27 mm hemispheres in a staggered, uniform array spaced 2 base diameters apart. The remaining 1.5 m length was smooth. The effect of the alignment of the smooth surface with respect to the rough surface was also studied by conducting experiments with the smooth surface aligned with the bases or alternatively with the crests of the roughness elements. Stanton number distributions, skin friction distributions, and boundary layer profiles of temperature and velocity are reported and are compared to previous data for both all rough and all smooth wall cases. The experiments show that the step change from rough to smooth has a dramatic effect on the convective heat transfer. It is concluded that use of smooth heat flux gages on otherwise rough surfaces could cause large errors.
DOE Office of Scientific and Technical Information (OSTI.GOV)

Yan, Pei-Yang; Zhang, Guojing; Gullickson, Eric M.

Extreme ultraviolet lithography (EUVL) mask multi-layer (ML) blank surface roughness specification historically comes from blank defect inspection tool requirement. Later, new concerns on ML surface roughness induced wafer pattern line width roughness (LWR) arise. In this paper, we have studied wafer level pattern LWR as a function of EUVL mask surface roughness via High-NA Actinic Reticle Review Tool. We found that the blank surface roughness induced LWR at current blank roughness level is in the order of 0.5nm 3σ for NA=0.42 at the best focus. At defocus of ±40nm, the corresponding LWR will be 0.2nm higher. Further reducing EUVL maskmore » blank surface roughness will increase the blank cost with limited benefit in improving the pattern LWR, provided that the intrinsic resist LWR is in the order of 1nm and above.« less
Investigations of grain size dependent sediment transport phenomena on multiple scales

NASA Astrophysics Data System (ADS)

Thaxton, Christopher S.

Sediment transport processes in coastal and fluvial environments resulting from disturbances such as urbanization, mining, agriculture, military operations, and climatic change have significant impact on local, regional, and global environments. Primarily, these impacts include the erosion and deposition of sediment, channel network modification, reduction in downstream water quality, and the delivery of chemical contaminants. The scale and spatial distribution of these effects are largely attributable to the size distribution of the sediment grains that become eligible for transport. An improved understanding of advective and diffusive grain-size dependent sediment transport phenomena will lead to the development of more accurate predictive models and more effective control measures. To this end, three studies were performed that investigated grain-size dependent sediment transport on three different scales. Discrete particle computer simulations of sheet flow bedload transport on the scale of 0.1--100 millimeters were performed on a heterogeneous population of grains of various grain sizes. The relative transport rates and diffusivities of grains under both oscillatory and uniform, steady flow conditions were quantified. These findings suggest that boundary layer formalisms should describe surface roughness through a representative grain size that is functionally dependent on the applied flow parameters. On the scale of 1--10m, experiments were performed to quantify the hydrodynamics and sediment capture efficiency of various baffles installed in a sediment retention pond, a commonly used sedimentation control measure in watershed applications. Analysis indicates that an optimum sediment capture effectiveness may be achieved based on baffle permeability, pond geometry and flow rate. Finally, on the scale of 10--1,000m, a distributed, bivariate watershed terain evolution module was developed within GRASS GIS. Simulation results for variable grain sizes and for distributed rainfall infiltration and land cover matched observations. Although a unique set of governing equations applies to each scale, an improved physics-based understanding of small and medium scale behavior may yield more accurate parameterization of key variables used in large scale predictive models.
Flow resistance in open channels with fixed movable bed

USGS Publications Warehouse

Simoes, Francisco J.

2010-01-01

In spite of an increasingly large body of research by many investigators, accurate quantitative prediction of open channel flow resistance remains a challenge. In general, the relations between the elements influencing resistance (turbulence, boundary roughness, and channel shape features, such as discrete obstacles, bars, channel curvature, recirculation areas, secondary circulation, etc.) and mean flow variables are complex and poorly understood. This has resulted in numerous approaches to compute friction using many and diverse variables and equally diverse prescriptions for their use. In this paper, a new resistance law for surface (grain) resistance, the resistance due to the flow viscous effects on the channel boundary roughness elements, is presented for the cases of flow in the transition (5 < Re* <70) and fully rough (Re* ≥ 70) turbulent flow regimes, where Re* is the Reynolds number based on shear velocity and sediment particle mean diameter. It is shown that the new law is sensitive to bed movement without requiring previous knowledge of sediment transport conditions. Comparisons between computation and measurements, as well as comparisons with other well-known existing roughness predictors, are presented to demonstrate its accuracy and range of application. It is shown that the method accurately predicts total friction losses in channels and natural rivers with plane beds, regardless of sediment transport conditions. This work is useful to hydraulic engineers involved with the derivation of depth-discharge relations in open channel flow and with the estimation of sediment transport rates for the case of bedload transport.
Efficacy of methoprene for multi-year protection of stored wheat, brown rice, rough rice and corn

USDA-ARS?s Scientific Manuscript database

Hard red winter wheat, brown rice, rough rice, and corn were treated with the insect growth regulator (IGR) at rates of 1.25 and 2.5 ppm, held for 24 months at ambient conditions at the floor of a grain bin, and sampled every two months. Bioassays were done by exposing 10 mixed-sex adults of Rhyzope...
Reducing the influence of the surface roughness on the hardness measurement using instrumented indentation test

NASA Astrophysics Data System (ADS)

Maslenikov, I.; Useinov, A.; Birykov, A.; Reshetov, V.

2017-10-01

The instrumented indentation method requires the sample surface to be flat and smooth; thus, hardness and elastic modulus values are affected by the roughness. A model that accounts for the isotropic surface roughness and can be used to correct the data in two limiting cases is proposed. Suggested approach requires the surface roughness parameters to be known.
Role of Integrin Subunits in Mesenchymal Stem Cell Differentiation and Osteoblast Maturation on Graphitic Carbon-coated Microstructured Surfaces

PubMed Central

Olivares-Navarrete, Rene; Rodil, Sandra E.; Hyzy, Sharon L.; Dunn, Ginger R.; Almaguer-Flores, Argelia; Schwartz, Zvi; Boyan, Barbara D.

2015-01-01

Surface roughness, topography, chemistry, and energy promote osteoblast differentiation and increase osteogenic local factor production in vitro and bone-to-implant contact in vivo, but the mechanisms involved are not well understood. Knockdown of integrin heterodimer alpha2beta1 (α2β1) blocks the osteogenic effects of the surface, suggesting signaling by this integrin homodimer is required. The purpose of the present study was to separate effects of surface chemistry and surface structure on integrin expression by coating smooth or rough titanium (Ti) substrates with graphitic carbon, retaining surface morphology but altering surface chemistry. Ti surfaces (smooth [Ra<0.4μm], rough [Ra≥3.4μm]) were sputter-coated using a magnetron sputtering system with an ultrapure graphite target, producing a graphitic carbon thin film. Human mesenchymal stem cells and MG63 osteoblast-like cells had higher mRNA for integrin subunits α1, α2, αv, and β1 on rough surfaces in comparison to smooth, and integrin αv on graphitic-carbon-coated rough surfaces in comparison to Ti. Osteogenic differentiation was greater on rough surfaces in comparison to smooth, regardless of chemistry. Silencing integrins β1, α1, or α2 decreased osteoblast maturation on rough surfaces independent of surface chemistry. Silencing integrin αv decreased maturation only on graphitic carbon-coated surfaces, not on Ti. These results suggest a major role of the integrin β1 subunit in roughness recognition, and that integrin alpha subunits play a major role in surface chemistry recognition. PMID:25770999
Expading fluvial remote sensing to the riverscape: Mapping depth and grain size on the Merced River, California

NASA Astrophysics Data System (ADS)

Richardson, Ryan T.

This study builds upon recent research in the field of fluvial remote sensing by applying techniques for mapping physical attributes of rivers. Depth, velocity, and grain size are primary controls on the types of habitat present in fluvial ecosystems. This thesis focuses on expanding fluvial remote sensing to larger spatial extents and sub-meter resolutions, which will increase our ability to capture the spatial heterogeneity of habitat at a resolution relevant to individual salmonids and an extent relevant to species. This thesis consists of two chapters, one focusing on expanding the spatial extent over which depth can be mapped using Optimal Band Ratio Analysis (OBRA) and the other developing general relations for mapping grain size from three-dimensional topographic point clouds. The two chapters are independent but connected by the overarching goal of providing scientists and managers more useful tools for quantifying the amount and quality of salmonid habitat via remote sensing. The OBRA chapter highlights the true power of remote sensing to map depths from hyperspectral images as a central component of watershed scale analysis, while also acknowledging the great challenges involved with increasing spatial extent. The grain size mapping chapter establishes the first general relations for mapping grain size from roughness using point clouds. These relations will significantly reduce the time needed in the field by eliminating the need for independent measurements of grain size for calibrating the roughness-grain size relationship and thus making grain size mapping with SFM more cost effective for river restoration and monitoring. More data from future studies are needed to refine these relations and establish their validity and generality. In conclusion, this study adds to the rapidly growing field of fluvial remote sensing and could facilitate river research and restoration.
Effects of Surface Roughness on Conical Squeeze Film Bearings with Micropolar fluid

NASA Astrophysics Data System (ADS)

Rajani, C. B.; Hanumagowda, B. N.; Shigehalli, Vijayalaxmi S.

2018-04-01

In the current paper, a hypothetical analysis of the impact of surface roughness on squeeze film lubrication of rough conical bearing using Micropolar fluid is examined using Eringen’sMicropolar fluid model. The generalized averaged Reynolds type equation for roughness has been determined analytically using the Christensen’s stochastic theory of roughness effects and the closed form expressions are obtained for the fluid film pressure, load carrying capacity and squeezing time. Further, the impacts of surface roughness using micropolar fluids on the squeeze film lubrication of rough conical bearings has been discussed and according to the outcomes arrived, pressure, load carrying capacity and squeezing time increases for azimuthal roughness pattern and decreases for radial roughness patterns comparatively to the smooth case.
Modeling photopolarimetric characteristics of comet dust as a polydisperse mixture of polyshaped rough spheroids

NASA Astrophysics Data System (ADS)

Kolokolova, L.; Das, H.; Dubovik, O.; Lapyonok, T.

2013-12-01

It is widely recognized now that the main component of comet dust is aggregated particles that consist of submicron grains. It is also well known that cometary dust obey a rather wide size distribution with abundant particles whose size reaches dozens of microns. However, numerous attempts of computer simulation of light scattering by comet dust using aggregated particles have not succeeded to consider particles larger than a couple of microns due to limitations in the memory and speed of available computers. Attempts to substitute aggregates by polydisperse solid particles (spheres, spheroids, cylinders) could not consistently reproduce observed angular and spectral characteristics of comet brightness and polarization even in such a general case as polyshaped (i.e. containing particles of a variety of aspect ratios) mixture of spheroids (Kolokolova et al., In: Photopolarimetry in Remote Sensing, Kluwer Acad. Publ., 431, 2004). In this study we are checking how well cometary dust can be modeled using modeling tools for rough spheroids. With this purpose we use the software package described in Dubovik et al. (J. Geophys. Res., 111, D11208, doi:10.1029/2005JD006619d, 2006) that allows for a substantial reduction of computer time in calculating scattering properties of spheroid mixtures by means of using pre-calculated kernels - quadrature coefficients employed in the numerical integration of spheroid optical properties over size and shape. The kernels were pre-calculated for spheroids of 25 axis ratios, ranging from 0.3 to 3, and 42 size bins within the size parameter range 0.01 - 625. This software package has been recently expanded with the possibility of simulating not only smooth but also rough spheroids that is used in present study. We consider refractive indexes of the materials typical for comet dust: silicate, carbon, organics, and their mixtures. We also consider porous particles accounting on voids in the spheroids through effective medium approach. The roughness of the spheroids is considered as a normal distribution of particle surface slopes and can be of different degree depending on the standard deviation of the distribution, σ, where σ=0 corresponds to smooth surface and σ=0.5 describes severely rough surface (see Young et al., J. Atm. Sci., 70, 330, 2012). We perform computations for two wavelengths, typical for blue (447nm) and red (640nm) cometary continuum filters. We compare phase angle dependence of polarization and brightness and their spectral change obtained with the rough-spheroid model with those observed for comets (e.g. Kolokolova et al., In: Comets 2, Arizona Press, 577, 2004) to see how well rough spheroids can reproduce cometary low albedo, red color, red polarimetric color, negative polarization at small phase angles and polarization maximum at medium phase angles.
The grain-size distribution of pyroclasts: Primary fragmentation, conduit sorting or abrasion?

NASA Astrophysics Data System (ADS)

Kueppers, U.; Schauroth, J.; Taddeucci, J.

2013-12-01

Explosive volcanic eruptions expel a mixture of pyroclasts and lithics. Pyroclasts, fragments of the juvenile magma, record the state of the magma at fragmentation in terms of porosity and crystallinity. The grain size distribution of pyroclasts is generally considered to be a direct consequence of the conditions at magma fragmentation that is mainly driven by gas overpressure in bubbles, high shear rates, contact with external water or a combination of these factors. Stress exerted by any of these processes will lead to brittle fragmentation by overcoming the magma's relaxation timescale. As a consequence, most pyroclasts exhibit angular shapes. Upon magma fragmentation, the gas pyroclast mixture is accelerated upwards and eventually ejected from the vent. The total grain size distribution deposited is a function of fragmentation conditions and transport related sorting. Porous pyroclasts are very susceptible to abrasion by particle-particle or particle-conduit wall interaction. Accordingly, pyroclastic fall deposits with angular clasts should proof a low particle abrasion upon contact to other surfaces. In an attempt to constrain the degree of particle interaction during conduit flow, monomodal batches of washed pyroclasts have been accelerated upwards by rapid decompression and subsequently investigated for their grain size distribution. In our set-up, we used a vertical cylindrical tube without surface roughness as conduit. We varied grain size (0.125-0.25; 0.5-1; 1-2 mm), porosity (0; 10; 30 %), gas-particle ratio (10 and 40%), conduit length (10 and 28 cm) and conduit diameter (2.5 and 6 cm). All ejected particles were collected after settling at the base of a 3.3 m high tank and sieved at one sieve size below starting size (half-Φ). Grain size reduction showed a positive correlation with starting grain size, porosity and overpressure at the vent. Although milling in a volcanic conduit may take place, porous pyroclasts are very likely to be a primary product of magma fragmentation at or close to the fragmentation level. Given the high abrasiveness of pumice, hemispherical clasts should be observed if clast break-up followed efficient clast abrasion. As a consequence, finer grained pyroclastic fall deposits do not necessarily proof efficient secondary fragmentation in the conduit but may rather reveal the influence of conduit length on 'What size of pyroclasts can be erupted'?
Generalizing roughness: experiments with flow-oriented roughness

NASA Astrophysics Data System (ADS)

Trevisani, Sebastiano

2015-04-01

Surface texture analysis applied to High Resolution Digital Terrain Models (HRDTMs) improves the capability to characterize fine-scale morphology and permits the derivation of useful morphometric indexes. An important indicator to be taken into account in surface texture analysis is surface roughness, which can have a discriminant role in the detection of different geomorphic processes and factors. The evaluation of surface roughness is generally performed considering it as an isotropic surface parameter (e.g., Cavalli, 2008; Grohmann, 2011). However, surface texture has often an anisotropic character, which means that surface roughness could change according to the considered direction. In some applications, for example involving surface flow processes, the anisotropy of roughness should be taken into account (e.g., Trevisani, 2012; Smith, 2014). Accordingly, we test the application of a flow-oriented directional measure of roughness, computed considering surface gravity-driven flow. For the calculation of flow-oriented roughness we use both classical variogram-based roughness (e.g., Herzfeld,1996; Atkinson, 2000) as well as an ad-hoc developed robust modification of variogram (i.e. MAD, Trevisani, 2014). The presented approach, based on a D8 algorithm, shows the potential impact of considering directionality in the calculation of roughness indexes. The use of flow-oriented roughness could improve the definition of effective proxies of impedance to flow. Preliminary results on the integration of directional roughness operators with morphometric-based models, are promising and can be extended to more complex approaches. Atkinson, P.M., Lewis, P., 2000. Geostatistical classification for remote sensing: an introduction. Computers & Geosciences 26, 361-371. Cavalli, M. & Marchi, L. 2008, "Characterization of the surface morphology of an alpine alluvial fan using airborne LiDAR", Natural Hazards and Earth System Science, vol. 8, no. 2, pp. 323-333. Grohmann, C.H., Smith, M.J., Riccomini, C., 2011. Multiscale Analysis of Topographic Surface Roughness in the Midland Valley, Scotland. IEEE Transactions on Geoscience and Remote Sensing 49, 1220-1213. Herzfeld, U.C., Higginson, C.A., 1996. Automated geostatistical seafloor classification - Principles, parameters, feature vectors, and discrimination criteria. Computers and Geosciences, 22 (1), pp. 35-52. Smith, M.W. 2014, "Roughness in the Earth Sciences", Earth-Science Reviews, vol. 136, pp. 202-225. Trevisani, S., Cavalli, M. & Marchi, L. 2012, "Surface texture analysis of a high-resolution DTM: Interpreting an alpine basin", Geomorphology, vol. 161-162, pp. 26-39. Trevisani S., Rocca M., 2014. Geomorphometric analysis of fine-scale morphology for extensive areas: a new surface-texture operator. Geophysical Research Abstracts, Vol. 16, EGU2014-5612, 2014. EGU General Assembly 2014.
Comparison of four methods of surface roughness assessment of corneal stromal bed after lamellar cutting

PubMed Central

Jumelle, Clotilde; Hamri, Alina; Egaud, Gregory; Mauclair, Cyril; Reynaud, Stephanie; Dumas, Virginie; Pereira, Sandrine; Garcin, Thibaud; Gain, Philippe; Thuret, Gilles

2017-01-01

Corneal lamellar cutting with a blade or femtosecond laser (FSL) is commonly used during refractive surgery and corneal grafts. Surface roughness of the cutting plane influences postoperative visual acuity but is difficult to assess reliably. For the first time, we compared chromatic confocal microscopy (CCM) with scanning electron microscopy, atomic force microscopy (AFM) and focus-variation microscopy (FVM) to characterize surfaces of variable roughness after FSL cutting. The small area allowed by AFM hinders conclusive roughness analysis, especially with irregular cuts. FVM does not always differentiate between smooth and rough surfaces. Finally, CCM allows analysis of large surfaces and differentiates between surface states. PMID:29188095

Analysis of multi lobe journal bearings with surface roughness using finite difference method

NASA Astrophysics Data System (ADS)

PhaniRaja Kumar, K.; Bhaskar, SUdaya; Manzoor Hussain, M.

2018-04-01

Multi lobe journal bearings are used for high operating speeds and high loads in machines. In this paper symmetrical multi lobe journal bearings are analyzed to find out the effect of surface roughnessduring non linear loading. Using the fourth order RungeKutta method, time transient analysis was performed to calculate and plot the journal centre trajectories. Flow factor method is used to evaluate the roughness and the finite difference method (FDM) is used to predict the pressure distribution over the bearing surface. The Transient analysis is done on the multi lobe journal bearings for threedifferent surface roughness orientations. Longitudinal surface roughness is more effective when compared with isotopic and traverse surface roughness.
Pressure variation of developed lapping tool on surface roughness

NASA Astrophysics Data System (ADS)

Hussain, A. K.; Lee, K. Q.; Aung, L. M.; Abu, A.; Tan, L. K.; Kang, H. S.

2018-01-01

Improving the surface roughness is always one of the major concerns in the development of lapping process as high precision machining caters a great demand in manufacturing process. This paper aims to investigate the performance of a newly designed lapping tool in term of surface roughness. Polypropylene is used as the lapping tool head. The lapping tool is tested for different pressure to identify the optimum working pressure for lapping process. The theoretical surface roughness is also calculated using Vickers Hardness. The present study shows that polypropylene is able to produce good quality and smooth surface roughness. The optimum lapping pressure in the present study is found to be 45 MPa. By comparing the theoretical and experimental values, the present study shows that the newly designed lapping tool is capable to produce finer surface roughness.
Universal emulsion stabilization from the arrested adsorption of rough particles at liquid-liquid interfaces

PubMed Central

Zanini, Michele; Marschelke, Claudia; Anachkov, Svetoslav E.; Marini, Emanuele; Synytska, Alla; Isa, Lucio

2017-01-01

Surface heterogeneities, including roughness, significantly affect the adsorption, motion and interactions of particles at fluid interfaces. However, a systematic experimental study, linking surface roughness to particle wettability at a microscopic level, is currently missing. Here we synthesize a library of all-silica microparticles with uniform surface chemistry, but tuneable surface roughness and study their spontaneous adsorption at oil–water interfaces. We demonstrate that surface roughness strongly pins the particles' contact lines and arrests their adsorption in long-lived metastable positions, and we directly measure the roughness-induced interface deformations around isolated particles. Pinning imparts tremendous contact angle hysteresis, which can practically invert the particle wettability for sufficient roughness, irrespective of their chemical nature. As a unique consequence, the same rough particles stabilize both water-in-oil and oil-in-water emulsions depending on the phase they are initially dispersed in. These results both shed light on fundamental phenomena concerning particle adsorption at fluid interfaces and indicate future design rules for particle-based emulsifiers. PMID:28589932
Universal emulsion stabilization from the arrested adsorption of rough particles at liquid-liquid interfaces

NASA Astrophysics Data System (ADS)

Zanini, Michele; Marschelke, Claudia; Anachkov, Svetoslav E.; Marini, Emanuele; Synytska, Alla; Isa, Lucio

2017-06-01

Surface heterogeneities, including roughness, significantly affect the adsorption, motion and interactions of particles at fluid interfaces. However, a systematic experimental study, linking surface roughness to particle wettability at a microscopic level, is currently missing. Here we synthesize a library of all-silica microparticles with uniform surface chemistry, but tuneable surface roughness and study their spontaneous adsorption at oil-water interfaces. We demonstrate that surface roughness strongly pins the particles' contact lines and arrests their adsorption in long-lived metastable positions, and we directly measure the roughness-induced interface deformations around isolated particles. Pinning imparts tremendous contact angle hysteresis, which can practically invert the particle wettability for sufficient roughness, irrespective of their chemical nature. As a unique consequence, the same rough particles stabilize both water-in-oil and oil-in-water emulsions depending on the phase they are initially dispersed in. These results both shed light on fundamental phenomena concerning particle adsorption at fluid interfaces and indicate future design rules for particle-based emulsifiers.
A lattice Boltzmann simulation of coalescence-induced droplet jumping on superhydrophobic surfaces with randomly distributed structures

NASA Astrophysics Data System (ADS)

Zhang, Li-Zhi; Yuan, Wu-Zhi

2018-04-01

The motion of coalescence-induced condensate droplets on superhydrophobic surface (SHS) has attracted increasing attention in energy-related applications. Previous researches were focused on regularly rough surfaces. Here a new approach, a mesoscale lattice Boltzmann method (LBM), is proposed and used to model the dynamic behavior of coalescence-induced droplet jumping on SHS with randomly distributed rough structures. A Fast Fourier Transformation (FFT) method is used to generate non-Gaussian randomly distributed rough surfaces with the skewness (Sk), kurtosis (K) and root mean square (Rq) obtained from real surfaces. Three typical spreading states of coalesced droplets are observed through LBM modeling on various rough surfaces, which are found to significantly influence the jumping ability of coalesced droplet. The coalesced droplets spreading in Cassie state or in composite state will jump off the rough surfaces, while the ones spreading in Wenzel state would eventually remain on the rough surfaces. It is demonstrated that the rough surfaces with smaller Sks, larger Rqs and a K at 3.0 are beneficial to coalescence-induced droplet jumping. The new approach gives more detailed insights into the design of SHS.
Dynamic evolution of interface roughness during friction and wear processes.

PubMed

Kubiak, K J; Bigerelle, M; Mathia, T G; Dubois, A; Dubar, L

2014-01-01

Dynamic evolution of surface roughness and influence of initial roughness (S(a) = 0.282-6.73 µm) during friction and wear processes has been analyzed experimentally. The mirror polished and rough surfaces (28 samples in total) have been prepared by surface polishing on Ti-6Al-4V and AISI 1045 samples. Friction and wear have been tested in classical sphere/plane configuration using linear reciprocating tribometer with very small displacement from 130 to 200 µm. After an initial period of rapid degradation, dynamic evolution of surface roughness converges to certain level specific to a given tribosystem. However, roughness at such dynamic interface is still increasing and analysis of initial roughness influence revealed that to certain extent, a rheology effect of interface can be observed and dynamic evolution of roughness will depend on initial condition and history of interface roughness evolution. Multiscale analysis shows that morphology created in wear process is composed from nano, micro, and macro scale roughness. Therefore, mechanical parts working under very severe contact conditions, like rotor/blade contact, screws, clutch, etc. with poor initial surface finishing are susceptible to have much shorter lifetime than a quality finished parts. © Wiley Periodicals, Inc.
Sustaining dry surfaces under water

PubMed Central

Jones, Paul R.; Hao, Xiuqing; Cruz-Chu, Eduardo R.; Rykaczewski, Konrad; Nandy, Krishanu; Schutzius, Thomas M.; Varanasi, Kripa K.; Megaridis, Constantine M.; Walther, Jens H.; Koumoutsakos, Petros; Espinosa, Horacio D.; Patankar, Neelesh A.

2015-01-01

Rough surfaces immersed under water remain practically dry if the liquid-solid contact is on roughness peaks, while the roughness valleys are filled with gas. Mechanisms that prevent water from invading the valleys are well studied. However, to remain practically dry under water, additional mechanisms need consideration. This is because trapped gas (e.g. air) in the roughness valleys can dissolve into the water pool, leading to invasion. Additionally, water vapor can also occupy the roughness valleys of immersed surfaces. If water vapor condenses, that too leads to invasion. These effects have not been investigated, and are critically important to maintain surfaces dry under water. In this work, we identify the critical roughness scale, below which it is possible to sustain the vapor phase of water and/or trapped gases in roughness valleys – thus keeping the immersed surface dry. Theoretical predictions are consistent with molecular dynamics simulations and experiments. PMID:26282732
Membrane fouling in a submerged membrane bioreactor: An unified approach to construct topography and to evaluate interaction energy between two randomly rough surfaces.

PubMed

Cai, Xiang; Shen, Liguo; Zhang, Meijia; Chen, Jianrong; Hong, Huachang; Lin, Hongjun

2017-11-01

Quantitatively evaluating interaction energy between two randomly rough surfaces is the prerequisite to quantitatively understand and control membrane fouling in membrane bioreactors (MBRs). In this study, a new unified approach to construct rough topographies and to quantify interaction energy between a randomly rough particle and a randomly rough membrane was proposed. It was found that, natural rough topographies of both foulants and membrane could be well constructed by a modified two-variable Weierstrass-Mandelbrot (WM) function included in fractal theory. Spatial differential relationships between two constructed surfaces were accordingly established. Thereafter, a new approach combining these relationships, surface element integration (SEI) approach and composite Simpson's rule was deduced to calculate the interaction energy between two randomly rough surfaces in a submerged MBR. The obtained results indicate the profound effects of surface morphology on interaction energy and membrane fouling. This study provided a basic approach to investigate membrane fouling and interface behaviors. Copyright © 2017 Elsevier Ltd. All rights reserved.
Ultra-Smooth Nanostructured Diamond Films Deposited from He/H2/CH4/N2 Microwave Plasmas

PubMed Central

Konovalov, Valery V.; Melo, Andrew; Catledge, Shane A.; Chowdhury, Shafiul

2008-01-01

Addition of He to a high CH4 content (10.7 vol%) H2/CH4/N2 feedgas mixture for microwave plasma chemical vapor deposition produced hard (56–72 GPa), ultra-smooth nanostructured diamond films on Ti-6Al-4V alloy substrates. Upon increase in He content up to 71 vol%, root mean squared (RMS) surface roughness of the film decreased to 9–10 nm and average diamond grain size to 5–6 nm. Our studies show that increased nanocrystallinity with He addition in plasma is related to plasma dilution, enhanced fragmentation of carbon containing species, and enhanced formation of CN radical. PMID:16573106
Pentacene-based low voltage organic field-effect transistors with anodized Ta2O5 gate dielectric

NASA Astrophysics Data System (ADS)

Jeong, Yeon Taek; Dodabalapur, Ananth

2007-11-01

Pentacene-based low voltage organic field-effect transistors were realized using an anodized Ta2O5 gate dielectric. The Ta2O5 gate dielectric layer with a surface roughness of 1.3Å was obtained by anodizing an e-beam evaporated Ta film. The device exhibited values of saturation mobility, threshold voltage, and Ion/Ioff ratio of 0.45cm2/Vs, 0.56V, and 7.5×101, respectively. The gate leakage current was reduced by more than 70% with a hexamethyldisilazane (HMDS) treatment on the Ta2O5 layer. The HMDS treatment also resulted in enhanced mobility values and a larger pentacene grain size.
In situ evaluation of surface roughness and micromorphology of temporary soft denture liner materials at different time intervals.

PubMed

Araújo, Célio U; Basting, Roberta T

2018-03-01

To perform an in situ evaluation of surface roughness and micromorphology of two soft liner materials for dentures at different time intervals. The surface roughness of materials may influence the adhesion of micro-organisms and inflammation of the mucosal tissues. The in situ evaluation of surface roughness and the micromorphology of soft liner materials over the course of time may present results different from those of in vitro studies, considering the constant presence of saliva and food, the changes in temperature and the pH level in the oral cavity. Forty-eight rectangular specimens of each of the two soft liner materials were fabricated: a silicone-based material (Mucopren Soft) and an acrylic resin-based material (Trusoft). The specimens were placed in the dentures of 12 participants (n = 12), and the materials were evaluated for surface roughness and micromorphology at different time intervals: 0, 7, 30 and 60 days. Roughness (Ra) was evaluated by means of a roughness tester. Surface micromorphology was evaluated by scanning electron microscopy. Analysis of variance for randomised block design and Tukey's test showed that surface roughness values were lower in the groups using the silicone-based material at all the time intervals (P < .0001). The average surface roughness was higher at time interval 0 than at the other intervals, for both materials (P < .0001). The surface micromorphology showed that the silicone material presented a more regular and smoother surface than the acrylic resin-based material. The surface roughness of acrylic resin-based and silicone-based denture soft liner materials decreased after 7 days of evaluation, leading to a smoother surface over time. The silicone-based material showed lower roughness values and a smoother surface than the acrylic resin-based material, thereby making it preferred when selecting more appropriate material, due its tendency to promote less biofilm build-up. © 2017 John Wiley & Sons A/S and The Gerodontology Association. Published by John Wiley & Sons Ltd.
2D scaling behavior of nanotextured GaN surfaces: A case study of hillocked and terraced surfaces

NASA Astrophysics Data System (ADS)

Mutta, Geeta Rani; Carapezzi, Stefania

2018-07-01

The 2D scaling properties of GaN surfaces have been studied by means of the 2D height-height correlation function (HHCF). The GaN layers under investigation presented exemplar morphologies, generated by distinct growth methods: a molecular beam epitaxy (MBE) grown surface decorated by hillocks and a metal organic vapor phase epitaxy (MOVPE) grown surface with terraced structure. The 2D statistical analysis of these surfaces has allowed assessing quantitatively the degree of morphological variability along all the different directions across each surface, their corresponding roughness exponents and correlation lengths. A scaling anisotropy as well as correlation length anisotropy has been detected for both hillocked and terraced surfaces. Especially, a marked dependence of correlation length from the direction across the terraced surface has been observed. Additionally, the terraced surfaces showed the lower root mean square (RMS) roughness value and at the same time, the lower roughness exponent value. This could appear as a contradiction, given that a low RMS value is associated to a smooth surface, and usually the roughness exponent is interpreted as a "measure" of the smoothness of the surface, the smoother the surface, the higher (approaching the unity) is the roughness exponent. Our case study is an experimental demonstration in which the roughness exponent should be, more appropriately, interpreted as a quantification of how the roughness changes with length scale.
Surface roughness analysis of fiber post conditioning processes.

PubMed

Mazzitelli, C; Ferrari, M; Toledano, M; Osorio, E; Monticelli, F; Osorio, R

2008-02-01

The chemo-mechanical surface treatment of fiber posts increases their bonding properties. The combined use of atomic force and confocal microscopy allows for the assessment and quantification of the changes on surface roughness that justify this behavior. Quartz fiber posts were conditioned with different chemicals, as well as by sandblasting, and by an industrial silicate/silane coating. We analyzed post surfaces by atomic force microscopy, recording average roughness (R(a)) measurements of fibers and resin matrix. A confocal image profiler allowed for the quantitative assessment of the average superficial roughness (R(a)). Hydrofluoric acid, potassium permanganate, sodium ethoxide, and sandblasting increased post surface roughness. Modifications of the epoxy resin matrix occurred after the surface pre-treatments. Hydrofluoric acid affected the superficial texture of quartz fibers. Surface-conditioning procedures that selectively react with the epoxy-resin matrix of the fiber post enhance roughness and improve the surface area available for adhesion by creating micro-retentive spaces without affecting the post's inner structure.
Grain size mapping in shallow rivers using spectral information: a lab spectroradiometry perspective

NASA Astrophysics Data System (ADS)

Niroumand-Jadidi, Milad; Vitti, Alfonso

2017-10-01

Every individual attribute of a riverine environment defines the overall spectral signature to be observed by an optical sensor. The spectral characteristic of riverbed is influenced not only by the type but also the roughness of substrates. Motivated by this assumption, potential of optical imagery for mapping grain size of shallow rivers (< 1 m deep) is examined in this research. The previous studies concerned with grain size mapping are all built upon the texture analysis of exposed bed material using very high resolution (i.e. cm resolution) imagery. However, the application of texturebased techniques is limited to very low altitude sensors (e.g. UAVs) to ensure the sufficient spatial resolution. Moreover, these techniques are applicable only in the presence of exposed substrates along the river channel. To address these drawbacks, this study examines the effectiveness of spectral information to make distinction among grain sizes for submerged substrates. Spectroscopic experiments are performed in controlled condition of a hydraulic lab. The spectra are collected over a water flume in a range of water depths and bottoms with several grain sizes. A spectral convolution is performed to match the spectra to WorldView-2 spectral bands. The material type of substrates is considered the same for all the experiments with only variable roughness/size of grains. The spectra observed over dry beds revealed that the brightness/reflectance increases with the grain size across all the spectral bands. Based on this finding, the above-water spectra over a river channel are simulated considering different grain sizes in the bottom. A water column correction method is then used to retrieve the bottom reflectances. Then the inferred bottom reflectances are clustered to segregate among grain sizes. The results indicate high potential of the spectral approach for clustering grain sizes (overall accuracy of 92%) which opens up some horizons for mapping this valuable attribute of rivers using remotely sensed data.
Influence of Surface Texture and Roughness of Softer and Harder Counter Materials on Friction During Sliding

NASA Astrophysics Data System (ADS)

Menezes, Pradeep L.; Kishore; Kailas, Satish V.; Lovell, Michael R.

2015-01-01

Surface texture influences friction during sliding contact conditions. In the present investigation, the effect of surface texture and roughness of softer and harder counter materials on friction during sliding was analyzed using an inclined scratch testing system. In the experiments, two test configurations, namely (a) steel balls against aluminum alloy flats of different surface textures and (b) aluminum alloy pins against steel flats of different surface textures, are utilized. The surface textures were classified into unidirectionally ground, 8-ground, and randomly polished. For a given texture, the roughness of the flat surfaces was varied using grinding or polishing methods. Optical profilometer and scanning electron microscope were used to characterize the contact surfaces before and after the experiments. Experimental results showed that the surface textures of both harder and softer materials are important in controlling the frictional behavior. The softer material surface textures showed larger variations in friction between ground and polished surfaces. However, the harder material surface textures demonstrated a better control over friction among the ground surfaces. Although the effect of roughness on friction was less significant when compared to textures, the harder material roughness showed better correlations when compared to the softer material roughness.
Effect of surface topographic features on the optical properties of skin: a phantom study

NASA Astrophysics Data System (ADS)

Liu, Guangli; Chen, Jianfeng; Zhao, Zuhua; Zhao, Gang; Dong, Erbao; Chu, Jiaru; Xu, Ronald X.

2016-10-01

Tissue-simulating phantoms are used to validate and calibrate optical imaging systems and to understand light transport in biological tissue. Light propagation in a strongly turbid medium such as skin tissue experiences multiple scattering and diffuse reflection from the surface. Surface roughness introduces phase shifts and optical path length differences for light which is scattered within the skin tissue and reflected from the surface. In this paper, we study the effect of mismatched surface roughness on optical measurement and subsequent determination of optical properties of skin tissue. A series of phantoms with controlled surface features and optical properties corresponding to normal human skin are fabricated. The fabrication of polydimethylsiloxane (PDMS) phantoms with known surface roughness follows a standard soft lithography process. Surface roughness of skin-simulating phantoms are measured with Bruker stylus profiler. The diffuse reflectance of the phantom is validated by a UV/VIS spectrophotometer. The results show that surface texture and roughness have considerable influence on the optical characteristics of skin. This study suggests that surface roughness should be considered as an important contributing factor for the determination of tissue optical properties.
The effect of toothbrush bristle stiffness on nanohybrid surface roughness

NASA Astrophysics Data System (ADS)

Zairani, O.; Irawan, B.; Damiyanti, M.

2017-08-01

The surface of a restoration can be affected by toothpaste containing abrasive agents and the stiffness of toothbrush bristles. Objective: To identify the effect of toothbrush bristle stiffness on nanohybrid surface roughness. Methods: Sixteen nanohybrid specimens were separated into two groups. The first group was brushed using soft-bristle toothbrushes, and the second group was brushed using medium-bristle toothbrushes. Media such as aqua bides was used for brushing in both groups. Brushing was done 3 times for 5 minutes. Surface roughness was measured initially and at 5, 10, and 15 minutes using a surface roughness tester. Results: The results, tested with One-Way ANOVA and Independent Samples t Test, demonstrated that after brushing for 15 minutes, the soft-bristle toothbrush group showed a significantly different value (p < 0.05) of nanohybrid surface roughness. The group using medium-bristle toothbrushes showed the value of nano hybrid surface roughness significant difference after brushing for 10 minutes. Conclusion: Roughness occurs more rapidly when brushing with medium-bristle tooth brushes than when brushing with soft-bristle toothbrushes.
The Backscattering Phase Function for a Sphere with a Two-Scale Relief of Rough Surface

NASA Astrophysics Data System (ADS)

Klass, E. V.

2017-12-01

The backscattering of light from spherical surfaces characterized by one and two-scale roughness reliefs has been investigated. The analysis is performed using the three-dimensional Monte-Carlo program POKS-RG (geometrical-optics approximation), which makes it possible to take into account the roughness of objects under study by introducing local geometries of different levels. The geometric module of the program is aimed at describing objects by equations of second-order surfaces. One-scale roughness is set as an ensemble of geometric figures (convex or concave halves of ellipsoids or cones). The two-scale roughness is modeled by convex halves of ellipsoids, with surface containing ellipsoidal pores. It is shown that a spherical surface with one-scale convex inhomogeneities has a flatter backscattering phase function than a surface with concave inhomogeneities (pores). For a sphere with two-scale roughness, the dependence of the backscattering intensity is found to be determined mostly by the lower-level inhomogeneities. The influence of roughness on the dependence of the backscattering from different spatial regions of spherical surface is analyzed.
The importance of media roughness considerations for describing particle deposition in porous media

NASA Astrophysics Data System (ADS)

Jin, C.; Emelko, M.

2016-12-01

The morphology of media/collector surfaces (i.e., roughness) is one of the most important factors that has been recognized for decades; however, literature has been, for the most part, contradictory, non-mechanistic, and non-quantitative. A one-site kinetic model for attachment/detachment using a convection-diffusion model was used to evaluate particle deposition on collector surfaces in the packed beds. Rigorous controlled experiments addressing the impacts of surface roughness on particle deposition were conducted in parallel plate and packed bed systems; they demonstrated that a) surface roughness consistently influenced colloid deposition in a nonlinear, non-monotonic manner such that a critical roughness size associated with minimum particle deposition could be identified and b) collector surface roughness and background ionic strength concurrently influenced particle deposition. Excellent agreement between experimental data and numerical simulations was found when the most current knowledge representing hydrodynamic and interfacial forces associated with collector media roughness was represented. Although surface roughness also had a non-linear, non-monotonic impact on DLVO interaction energy at all separation distances, it was inadequate for describing and simulating particle deposition on surfaces with variable roughness. Notably, this work demonstrates that hydrodynamic effects can significantly alter particle deposition relative to expectations when only the DLVO force is considered. Moreover, the combined effects of hydrodynamics and interaction forces on particle deposition on rough, spherical media are not additive, but synergistic. Consideration of hydrodynamic contributions to particle deposition may help to explain discrepancies between model-based expectations and experimental outcomes and improve descriptions of particle deposition during physicochemical filtration in systems with non-smooth collector surfaces.
Estimation of surface soil moisture and roughness from multi-angular ASAR imagery in the Watershed Allied Telemetry Experimental Research (WATER)

NASA Astrophysics Data System (ADS)

Wang, S. G.; Li, X.; Han, X. J.; Jin, R.

2010-06-01

Radar remote sensing has demonstrated its applicability to the retrieval of basin-scale soil moisture. The mechanism of radar backscattering from soils is complicated and strongly influenced by surface roughness. Furthermore, retrieval of soil moisture using AIEM-like models is a classic example of the underdetermined problem due to a lack of credible known soil roughness distributions at a regional scale. Characterization of this roughness is therefore crucial for an accurate derivation of soil moisture based on backscattering models. This study aims to directly obtain surface roughness information along with soil moisture from multi-angular ASAR images. The method first used a semi-empirical relationship that connects the roughness slope (Zs) and the difference in backscattering coefficient (Δσ) from ASAR data in different incidence angles, in combination with an optimal calibration form consisting of two roughness parameters (the standard deviation of surface height and the correlation length), to estimate the roughness parameters. The deduced surface roughness was then used in the AIEM model for the retrieval of soil moisture. An evaluation of the proposed method was performed in a grassland site in the middle stream of the Heihe River Basin, where the Watershed Allied Telemetry Experimental Research (WATER) was taken place. It has demonstrated that the method is feasible to achieve reliable estimation of soil water content. The key challenge to surface soil moisture retrieval is the presence of vegetation cover, which significantly impacts the estimates of surface roughness and soil moisture.

Modeling of surface roughness effects on Stokes flow in circular pipes

NASA Astrophysics Data System (ADS)

Song, Siyuan; Yang, Xiaohu; Xin, Fengxian; Lu, Tian Jian

2018-02-01

Fluid flow and pressure drop across a channel are significantly influenced by surface roughness on a channel wall. The present study investigates the effects of periodically structured surface roughness upon flow field and pressure drop in a circular pipe at low Reynolds numbers. The periodic roughness considered exhibits sinusoidal, triangular, and rectangular morphologies, with the relative roughness (i.e., ratio of the amplitude of surface roughness to hydraulic diameter of the pipe) no more than 0.2. Based upon a revised perturbation theory, a theoretical model is developed to quantify the effect of roughness on fully developed Stokes flow in the pipe. The ratio of static flow resistivity and the ratio of the Darcy friction factor between rough and smooth pipes are expressed in four-order approximate formulations, which are validated against numerical simulation results. The relative roughness and the wave number are identified as the two key parameters affecting the static flow resistivity and the Darcy friction factor.
Studies of SERS efficiency of gold coated porous silicon formed on rough silicon backside

NASA Astrophysics Data System (ADS)

Dridi, H.; Haji, L.; Moadhen, A.

2017-12-01

Starting from a rough backside of silicon wafer, we have formed a porous layer by electrochemical anodization and then coated by a thin film of gold. The morphological characteristics of the porous silicon and in turn the metal film are governed by the anodization process and also by the starting surface. So, in order to investigate the Plasmonic aspect of such rough surface which combines roughness inherent to the porous nature and that due to rough starting surface, we have used a dye target molecule to study its SERS signal using a porous silicon layer obtained on the rough backside surface. The use of unusual backside of silicon wafer could be, beside the others, an interesting way to made SERS effective substrate thanks to reproducible rough porous gold on porous layer from this starting face. The morphological results correspond to the silicon rough surface as a function of the crystallographic orientation showed the presence of two different substrate structure. The optical reflectivity results obtained of gold deposited on oxidized porous silicon showed a dependence of its Localized Surface Plasmon band frequency of the deposit time. SERS results, obtained for a dye target molecule (Rhodamine 6G), show a higher intensities in the case of the 〈110〉 orientation, which characterized by the higher roughness surface. Voici "the most relevant and important aspects of our work".
Sensitivity analysis of observed reflectivity to ice particle surface roughness using MISR satellite observations

NASA Astrophysics Data System (ADS)

Bell, A.; Hioki, S.; Wang, Y.; Yang, P.; Di Girolamo, L.

2016-12-01

Previous studies found that including ice particle surface roughness in forward light scattering calculations significantly reduces the differences between observed and simulated polarimetric and radiometric observations. While it is suggested that some degree of roughness is desirable, the appropriate degree of surface roughness to be assumed in operational cloud property retrievals and the sensitivity of retrieval products to this assumption remains uncertain. In an effort to extricate this ambiguity, we will present a sensitivity analysis of space-borne multi-angle observations of reflectivity, to varying degrees of surface roughness. This process is two fold. First, sampling information and statistics of Multi-angle Imaging SpectroRadiometer (MISR) sensor data aboard the Terra platform, will be used to define the most coming viewing observation geometries. Using these defined geometries, reflectivity will be simulated for multiple degrees of roughness using results from adding-doubling radiative transfer simulations. Sensitivity of simulated reflectivity to surface roughness can then be quantified, thus yielding a more robust retrieval system. Secondly, sensitivity of the inverse problem will be analyzed. Spherical albedo values will be computed by feeding blocks of MISR data comprising cloudy pixels over ocean into the retrieval system, with assumed values of surface roughness. The sensitivity of spherical albedo to the inclusion of surface roughness can then be quantified, and the accuracy of retrieved parameters can be determined.
Optical mapping of surface roughness by implementation of a spatial light modulator

NASA Astrophysics Data System (ADS)

Aulbach, Laura; Pöller, Franziska; Lu, Min; Wang, Shengjia; Koch, Alexander W.

2017-08-01

It is well-known that the surface roughness of materials plays an important role in the operation and performance of technological systems. The roughness influences key parameters, such as friction and wear, and is directly connected to the functionality and durability of the respective system. Tactile methods are widely used for the measurement of surface roughness, but a destructive measurement procedure and the lack of feasibility of online monitoring are crucial drawbacks. In the last decades, several non-contact, usually optical systems for surface roughness measurements have been developed, e.g., white light interferometry, light scatter analysis, or speckle correlation. These techniques are in turn often unable to assign the roughness to a certain surface area or involve inappropriate adjustment procedures. One promising and straightforward optical measurement method is the surface roughness measurement by analyzing the fringe visibility of an interferometric fringe pattern. In our work, we employed a spatial light modulator in the interferometric setup to vary the fringe visibility and provide a stable and reliable measurement system. In previous research, either the averaged fringe visibility or the fringe visibility along a defined observation profile were analyzed. In this article, the analysis of the fringe visibility is extended to generate a complete roughness map of the measurement target. Thus, surface defects or areas of different roughness can be easily located.
Surface and Basal Roughness in Radar Sounding Data: Obstacle and Opportunity

NASA Astrophysics Data System (ADS)

Schroeder, D. M.; Grima, C.; Haynes, M.

2015-12-01

The surface and basal roughness of glaciers, ice sheets, and ice shelves can pose a significant obstacle to the visual interpretation and quantitative analysis of radar sounding data. Areas of high surface roughness - including grounding zones, shear margins, and crevasse fields - can produce clutter and side-lobe signals that obscure the interpretation of englacial and subglacial features. These areas can also introduce significant variation in bed echo strength profiles as a result of losses from two-way propagation through rough ice surfaces. Similarly, reflections from rough basal interfaces beneath ice sheets and ice shelves can also result in large, spatially variable losses in bed echo power. If unmitigated and uncorrected, these effects can degrade or prevent the definitive interpretation of material and geometric properties at the base of ice sheets and ice shelves using radar reflectivity and bed echo character. However, these effects also provide geophysical signatures of surface and basal interface character - including surface roughness, firn density, subglacial bedform geometry, ice shelf basal roughness, marine-ice/brine detection, and crevasse geometry - that can be observed and constrained by exploiting roughness effects in radar sounding data. We present a series of applications and approaches for characterizing and correcting surface and basal roughness effects for airborne radar sounding data collected in Antarctica. We also present challenges, insights, and opportunities for extending these techniques to the orbital radar sounding of Europa's ice shell.
Investigation of Wall Shear Stress Behavior for Rough Surfaces with Blowing

NASA Astrophysics Data System (ADS)

Helvey, Jacob; Borchetta, Colby; Miller, Mark; Martin, Alexandre; Bailey, Sean

2014-11-01

We present an experimental study conducted in a turbulent channel flow wind tunnel to determine the modifications made to the turbulent flow over rough surfaces with flow injection through the surfaces. Hot-wire profile results from a quasi-two-dimensional, sinusoidally-rough surface indicate that the effects of roughness are enhanced by momentum injection through the surface. In particular, the wall shear stress was found to show behavior consistent with increased roughness height when surface blowing was increased. This observed behavior contradicts previously reported results for regular three-dimensional roughness which show a decrease in wall shear stress with additional blowing. It is unclear whether this discrepancy is due to differences in the roughness geometry under consideration or the use of the Clauser fit to estimate wall shear stress. Additional PIV experiments are being conducted for a three-dimensional fibrous surface to obtain Reynolds shear stress profiles. These results provide an additional method for estimation of wall-shear stress and thus allow verification of the use of the Clauser chart approach for flows with momentum injection through the surface. This research is supported by NASA Kentucky EPSCoR Award NNX10AV39A, and NASA RA Award NNX13AN04A.
Preliminary Examination of Particles Recovered from the Surface of the Asteroid Itokawa by the Hayabusa Mission

NASA Technical Reports Server (NTRS)

Tsuchiyama, A.; Ebihara, M.; Kimura, M.; Kitajima, F.; Kotsugi, M.; Ito, S.; Nagao, K.; Nakamura, T.; Naraoka, H.; Noguchi, T.;

2011-01-01

The Hayabusa spacecraft arrived at S-type Asteroid 25143 Itokawa in November 2006, and reveal astounding features of the small asteroid (535 x 294 x 209 m). Near-infrared spectral shape indicates that the surface of this body has an olivinerich mineral assemblage potentially similar to that of LL5 or LL6 chondrites with different degrees of space weathering. Based on the surface morphological features observed in high-resolution images of Itokawa s surface, two major types of boulders were distinguished: rounded and angular boulders. Rounded boulders seem to be breccias, while angular boulders seem to have severe impact origin. Although the sample collection did not be made by normal operations, it was considered that some amount of samples, probably small particles of regolith, was collected from MUSES-C regio on the Itokawa s surface. The sample capsule was successfully recovered on the earth on June 13, 2010, and was opened at curation facility of JAXA (Japan Aerospace Exploration Agency), Sagamihara, Japan. A large number of small particles were found in the sample container. Preliminary analysis with SEM/EDX at the curation facility showed that at least more than 1500 grains were identified as rocky particles, and most of them were judged to be of extraterrestrial origin, and definitely from Asteroid Itokawa. Minerals (olivine, low-Ca pyroxene, high-Ca pyroxene, plagioclase, Fe sulfide, Fe-Ni metal, chromite, Ca phosphate), roughly estimated mode the minerals and rough measurement of the chemical compositions of the silicates show that these particles are roughly similar to LL chondrites. Although their size are mostly less than 10 m, some larger particles of about 100 m or larger were also identified. A part of the sample (probably several tens particles) will be selected by Hayabusa sample curation team and examined preliminary in Japan within one year after the sample recovery in prior to detailed analysis phase. Hayabusa Asteroidal Sample Preliminary Examination Team (HASPET) has been preparing for the preliminary examination with close cooperation with the curation team.

In vivo surface roughness evolution of a stressed metallic implant

NASA Astrophysics Data System (ADS)

Tan, Henry

2016-10-01

Implant-associated infection, a serious medical issue, is caused by the adhesion of bacteria to the surface of biomaterials; for this process the surface roughness is an important property. Surface nanotopography of medical implant devices can control the extent of bacterial attachment by modifying the surface morphology; to this end a model is introduced to facilitate the analysis of a nanoscale smooth surface subject to mechanical loading and in vivo corrosion. At nanometre scale rough surface promotes friction, hence reduces the mobility of the bacteria; this sessile environment expedites the biofilm growth. This manuscript derives the controlling equation for surface roughness evolution for metallic implant subject to in-plane stresses, and predicts the in vivo roughness changes within 6 h of continued mechanical loading at different stress level. This paper provides analytic tool and theoretical information for surface nanotopography of medical implant devices.
Investigating the Formation of Mars Recurring Slope Lineae through Laboratory Experiments

NASA Astrophysics Data System (ADS)

Cantillo, D. C.; Hibbitts, C.; Wing, B. R.; Mushkin, A.; Stockstill-Cahill, K.; Viviano-Beck, C. E.

2017-12-01

The presence of low-albedo streaks on crater slopes, Recurring Slope Lineae (RSLs), may be evidence for present-day intermittent and repeated flow of water or brine on the surface of Mars. RSLs grow, fade, and can grow again seasonally as surface temperatures change [e.g. 1,2]. Although distinguishable by being darker than the surrounding terrain, they have no diagnostic absorption features [3] with the exception of a ferric feature that may be related to grain size [4] and the notable discovery of hydrated perchlorates at the base of one set of RSLs [5]. To explore liquid-based hypotheses for the formation of RSLs, we have constructed an environmental chamber that can simulate Martian surface conditions. The development of this chamber follows upon the successful completion of preliminary tests under a terrestrial atmosphere [6] to prove the optical design and subsequently under Mars pressure to verify the technical approach [7]. The Mars Analog Reflectance Spectroscopy (MARS) chamber is capable of exposing soils to brines from underneath, simulating possible subsurface wetting that could result in RSL formation. While maintaining Mars pressure and similar oxygen fugacity, the chamber will also allow the collection of spectra from 0.4 to 2.4 microns. Various brine compositions can be investigated, including solutions of iron chlorides. These unique salts can lower the soil albedo without inducing a spectral absorption feature, whereas other salts brighten the surface after drying or retain significant water [8]. Another possible darkening mechanism is also being explored within the MARS chamber. Experiments have shown that evaporation of liquid from palagonitic soils under Mars pressure create ubiquitous grain scale cavities within the surface [7]. This micro-roughness increases shadowing and darkens the surface, indicating it may be a process of darkening that is independent of brine composition.
Molecular dynamics simulation of nanobubble nucleation on rough surfaces

NASA Astrophysics Data System (ADS)

Liu, Yawei; Zhang, Xianren

2017-04-01

Here, we study how nanobubbles nucleate on rough hydrophobic surfaces, using long-time standard simulations to directly observe the kinetic pathways and using constrained simulations combined with the thermodynamic integration approach to quantitatively evaluate the corresponding free energy changes. Both methods demonstrate that a two-step nucleation route involving the formation of an intermediate state is thermodynamically favorable: at first, the system transforms from the Wenzel state (liquid being in full contact with the solid surface) to the Cassie state (liquid being in contact with the peaks of the rough surface) after gas cavities occur in the grooves (i.e., the Wenzel-to-Cassie transition); then, the gas cavities coalesce and form a stable surface nanobubble with pinned contact lines (i.e., the Cassie-to-nanobubble transition). Additionally, the free energy barriers for the two transitions show opposing dependencies on the degree of surface roughness, indicating that the surfaces with moderate roughness are favorable for forming stable surface nanobubbles. Moreover, the simulation results also reveal the coexistence and transition between the Wenzel, Cassie, and nanobubble states on rough surfaces.
Calculations of microwave brightness temperature of rough soil surfaces: Bare field

NASA Technical Reports Server (NTRS)

Mo, T.; Schmugge, T. J.; Wang, J. R.

1985-01-01

A model for simulating the brightness temperatures of soils with rough surfaces is developed. The surface emissivity of the soil media is obtained by the integration of the bistatic scattering coefficients for rough surfaces. The roughness of a soil surface is characterized by two parameters, the surface height standard deviation sigma and its horizontal correlation length l. The model calculations are compared to the measured angular variations of the polarized brightness temperatures at both 1.4 GHz and 5 GHz frequences. A nonlinear least-squares fitting method is used to obtain the values of delta and l that best characterize the surface roughness. The effect of shadowing is incorporated by introducing a function S(theta), which represents the probability that a point on a rough surface is not shadowed by other parts of the surface. The model results for the horizontal polarization are in excellent agreement with the data. However, for the vertical polarization, some discrepancies exist between the calculations and data, particularly at the 1.4 GHz frequency. Possible causes of the discrepancy are discussed.
Characterization of titanyl phthalocyanine (TiOPc) thin films by microscopic and spectroscopic method

NASA Astrophysics Data System (ADS)

Skonieczny, R.; Makowiecki, J.; Bursa, B.; Krzykowski, A.; Szybowicz, M.

2018-02-01

The titanyl phthalocyanine (TiOPc) thin film deposited on glass, silicon and gold substrate have been studied using Raman spectroscopy, atomic force microscopy (AFM), absorption and profilometry measurements. The TiOPc thin layers have been deposited at room temperature by the quasi-molecular beam evaporation technique. The Raman spectra have been recorded using micro Raman system equipped with a confocal microscope. Using surface Raman mapping techni que with polarized Raman spectra the polymorphic forms of the TiOPc thin films distribution have been obtained. The AFM height and phase image were examined in order to find surface features and morphology of the thin films. Additionally to compare experimental results, structure optimization and vibrational spectra calculation of single TiOPc molecule were performed using DFT calculations. The received results showed that the parameters like polymorphic form, grain size, roughness of the surface in TiOPc thin films can well characterize the obtained organic thin films structures in terms of their use in optoelectronics and photovoltaics devices.
DOE Office of Scientific and Technical Information (OSTI.GOV)

Napari, Mari, E-mail: mari.napari@jyu.fi; Malm, Jari; Lehto, Roope

ZnO films were grown by atomic layer deposition at 35 °C on poly(methyl methacrylate) substrates using diethylzinc and water precursors. The film growth, morphology, and crystallinity were studied using Rutherford backscattering spectrometry, time-of-flight elastic recoil detection analysis, atomic force microscopy, scanning electron microscopy, and x-ray diffraction. The uniform film growth was reached after several hundreds of deposition cycles, preceded by the precursor penetration into the porous bulk and island-type growth. After the full surface coverage, the ZnO films were stoichiometric, and consisted of large grains (diameter 30 nm) with a film surface roughness up to 6 nm (RMS). The introduction of Al{sub 2}O{submore » 3} seed layer enhanced the initial ZnO growth substantially and changed the surface morphology as well as the crystallinity of the deposited ZnO films. Furthermore, the water contact angles of the ZnO films were measured, and upon ultraviolet illumination, the ZnO films on all the substrates became hydrophilic, independent of the film crystallinity.« less
The microstructural changes of Ge2Sb2Te5 thin film during crystallization process

NASA Astrophysics Data System (ADS)

Xu, Jingbo; Qi, Chao; Chen, Limin; Zheng, Long; Xie, Qiyun

2018-05-01

Phase change memory is known as the most promising candidate for the next generation nonvolatile memory technology. In this paper, the microstructural changes of Ge2Sb2Te5 film, which is the most common choice of phase change memory material, has been carefully studied by the combination of several characterization techniques. The combination of resistance measurements, X-ray diffraction, Raman spectroscopy and X-ray reflectivity allows us to simultaneously extract the characteristics of microstructural changes during crystallization process. The existence of surface/interface Ge2Sb2Te5 layer has been proposed here based on X-ray reflectivity measurements. Although the total film thickness decreases, as a result of the phase transition from amorphous to metastable crystalline cubic and then to the stable hexagonal phase, the surface/interface thickness increases after crystallization. Moreover, the increase of average grain size, density and surface roughness has been confirmed during thermal annealing process.
Quantification of soil surface roughness evolution under simulated rainfall

USDA-ARS?s Scientific Manuscript database

Soil surface roughness is commonly identified as one of the dominant factors governing runoff and interrill erosion. The objective of this study was to compare several existing soil surface roughness indices and to test the Revised Triangular Prism surface area Method (RTPM) as a new approach to cal...
Effect of surface roughness on osteogenesis in vitro and osseointegration in vivo of carbon fiber-reinforced polyetheretherketone–nanohydroxyapatite composite

PubMed Central

Deng, Yi; Liu, Xiaochen; Xu, Anxiu; Wang, Lixin; Luo, Zuyuan; Zheng, Yunfei; Deng, Feng; Wei, Jie; Tang, Zhihui; Wei, Shicheng

2015-01-01

As United States Food and Drug Administration-approved implantable material, carbon fiber-reinforced polyetheretherketone (CFRPEEK) possesses an adjustable elastic modulus similar to cortical bone and is a prime candidate to replace surgical metallic implants. The bioinertness and inferior osteogenic properties of CFRPEEK, however, limit its clinical application as orthopedic/dental implants. In this study, CFRPEEK–nanohydroxyapatite ternary composites (PEEK/n-HA/CF) with variable surface roughness have been successfully fabricated. The effect of surface roughness on their in vitro cellular responses of osteoblast-like MG-63 cells (attachment, proliferation, apoptosis, and differentiation) and in vivo osseointegration is evaluated. The results show that the hydrophilicity and the amount of Ca ions on the surface are significantly improved as the surface roughness of composite increases. In cell culture tests, the results reveal that the cell proliferation rate and the extent of osteogenic differentiation of cells are a function of the size of surface roughness. The composite with moderate surface roughness significantly increases cell attachment/proliferation and promotes the production of alkaline phosphatase (ALP) activity and calcium nodule formation compared with the other groups. More importantly, the PEEK/n-HA/CF implant with appropriate surface roughness exhibits remarkably enhanced bioactivity and osseointegration in vivo in the animal experiment. These findings will provide critical guidance for the design of CFRPEEK-based implants with optimal roughness to regulate cellular behaviors, and to enhance biocompability and osseointegration. Meanwhile, the PEEK/n-HA/CF ternary composite with optimal surface roughness might hold great potential as bioactive biomaterial for bone grafting and tissue engineering applications. PMID:25733834
Effects of ice crystal surface roughness and air bubble inclusions on cirrus cloud radiative properties from remote sensing perspective

NASA Astrophysics Data System (ADS)

Tang, Guanglin; Panetta, R. Lee; Yang, Ping; Kattawar, George W.; Zhai, Peng-Wang

2017-07-01

We study the combined effects of surface roughness and inhomogeneity on the optical scattering properties of ice crystals and explore the consequent implications to remote sensing of cirrus cloud properties. Specifically, surface roughness and inhomogeneity are added to the Moderate Resolution Imaging Spectroradiometer (MODIS) collection 6 (MC6) cirrus cloud particle habit model. Light scattering properties of the new habit model are simulated using a modified version of the Improved Geometric Optics Method (IGOM). Both inhomogeneity and surface roughness affect the single scattering properties significantly. In visible bands, inhomogeneity and surface roughness both tend to smooth the phase function and eliminate halos and the backscattering peak. The asymmetry parameter varies with the degree of surface roughness following a U shape - decreases and then increases - with a minimum at around 0.15, whereas it decreases monotonically with the air bubble volume fraction. Air bubble inclusions significantly increase phase matrix element -P12 for scattering angles between 20°-120°, whereas surface roughness has a much weaker effect, increasing -P12 slightly from 60°-120°. Radiative transfer simulations and cirrus cloud property retrievals are conducted by including both the factors. In terms of surface roughness and air bubble volume fraction, retrievals of cirrus cloud optical thickness or the asymmetry parameter using solar bands show similar patterns of variation. Polarimetric simulations using the MC6 cirrus cloud particle habit model are shown to be more consistent with observations when both surface roughness and inhomogeneity are simultaneously considered.
The physics of water droplets on surfaces: exploring the effects of roughness and surface chemistry

NASA Astrophysics Data System (ADS)

Eid, K. F.; Panth, M.; Sommers, A. D.

2018-03-01

This paper explores the fluid property commonly called surface tension, its effect on droplet shape and contact angle, and the major influences of contact angle behaviour (i.e. surface roughness and surface chemistry). Images of water droplets placed on treated copper surfaces are used to measure the contact angles between the droplets and the surface. The surface wettability is manipulated either by growing a self-assembled monolayer on the surface to make it hydrophobic or by changing the surface roughness. The main activities in this experiment, then, are (1) preparing and studying surfaces with different surface wettability and roughness; (2) determining the shape and contact angles of water droplets on these surfaces; and (3) demonstrating the spontaneous motion of water droplets using surface tension gradients.
Comparative histomorphometry and resonance frequency analysis of implants with moderately rough surfaces in a loaded animal model.

PubMed

Al-Nawas, B; Groetz, K A; Goetz, H; Duschner, H; Wagner, W

2008-01-01

Test of favourable conditions for osseointegration with respect to optimum bone-implant contact (BIC) in a loaded animal model. The varied parameters were surface roughness and surface topography of commercially available dental implants. Thirty-two implants of six types of macro and microstructure were included in the study (total 196). The different types were: minimally rough control: Branemark machined Mk III; oxidized surface: TiUnite MkIII and MkIV; ZL Ticer; blasted and etched surface: Straumann SLA; rough control: titanium plasma sprayed (TPS). Sixteen beagle dogs were implanted with the whole set of the above implants. After a healing period of 8 weeks, implants were loaded for 3 months. For the evaluation of the BIC areas, adequately sectioned biopsies were visualized by subsurface scans with confocal laser scanning microscopy (CLSM). The primary statistical analysis testing BIC of the moderately rough implants (mean 56.1+/-13.0%) vs. the minimally rough and the rough controls (mean 53.9+/-11.2%) does not reveal a significant difference (P=0.57). Mean values of 50-70% BIC were found for all implant types. Moderately rough oxidized implants show a median BIC, which is 8% higher than their minimally rough turned counterpart. The intraindividual difference between the TPS and the blasted and etched counterparts revealed no significant difference. The turned and the oxidized implants show median values of the resonance frequency [implant stability quotients (ISQ)] over 60; the nonself-tapping blasted and etched and TPS implants show median values below 60. In conclusion, the benefit of rough surfaces relative to minimally rough ones in this loaded animal model was confirmed histologically. The comparison of different surface treatment modalities revealed no significant differences between the modern moderately rough surfaces. Resonance frequency analysis seems to be influenced in a major part by the transducer used, thus prohibiting the comparison of different implant systems.
Comparative Study of Lunar Roughness from Multi - Source Data

NASA Astrophysics Data System (ADS)

Lou, Y.; Kang, Z.

2017-07-01

The lunar terrain can show its collision and volcanic history. The lunar surface roughness can give a deep indication of the effects of lunar surface magma, sedimentation and uplift. This paper aims to get different information from the roughness through different data sources. Besides introducing the classical Root-mean-square height method and Morphological Surface Roughness (MSR) algorithm, this paper takes the area of the Jurassic mountain uplift in the Sinus Iridum and the Plato Crater area as experimental areas. And then make the comparison and contrast of the lunar roughness derived from LRO's DEM and CE-2 DOM. The experimental results show that the roughness obtained by the traditional roughness calculation method reflect the ups and downs of the topography, while the results obtained by morphological surface roughness algorithm show the smoothness of the lunar surface. So, we can first use the surface fluctuation situation derived from RMSH to select the landing area range which ensures the lands are gentle. Then the morphological results determine whether the landing area is suitable for the detector walking and observing. The results obtained at two different scales provide a more complete evaluation system for selecting the landing site of the lunar probe.

The effect of brushing with nano calcium carbonate and calcium carbonate toothpaste on the surface roughness of nano-ionomer

NASA Astrophysics Data System (ADS)

Anisja, D. H.; Indrani, D. J.; Herda, E.

2017-08-01

Nanotechnology developments in dentistry have resulted in the development of nano-ionomer, a new restorative material. The surface roughness of restorative materials can increase bacteria adhesion and lead to poor oral hygiene. Abrasive agents in toothpaste can alter tooth and restorative material surfaces. The aim of this study is to identify the effect of brushing with nano calcium carbonate, and calcium carbonate toothpaste on surface roughness of nano-ionomer. Eighteen nano-ionomer specimens were brushed with Aquabidest (doubledistilled water), nano calcium carbonate and calcium carbonate toothpaste. Brushing lasted 30 minutes, and the roughness value (Ra) was measured after each 10 minute segment using a surface roughness tester. The data was analyzed using repeated ANOVA and one-way ANOVA test. The value of nano-ionomer surface roughness increased significantly (p<0.05) after 20 minutes of brushing with the nano calcium carbonate toothpaste. Brushing with calcium carbonate toothpaste leaves nano-ionomer surfaces more rugged than brushing with nano calcium carbonate toothpaste.
Influence of surface roughness and waviness on film thickness and pressure distribution in elastohydrodynamic contacts

NASA Technical Reports Server (NTRS)

Chow, L. S. H.; Cheng, H. S.

1976-01-01

The Christensen theory of a stochastic model for hydrodynamic lubrication of rough surfaces was extended to elastohydrodynamic lubrication between two rollers. Solutions for the reduced pressure at the entrance as a function of the ratio of the average nominal film thickness to the rms surface roughness, were obtained numerically. Results were obtained for purely transverse as well as purely longitudinal surface roughness for cases with or without slip. The reduced pressure was shown to decrease slightly by considering longitudinal surface roughness. The same approach was used to study the effect of surface roughness on lubrication between rigid rollers and lubrication of an infinitely wide slider bearing. Using the flow balance concept, the perturbed Reynolds equation, was derived and solved for the perturbed pressure distribution. In addition, Cheng's numerical scheme was modified to incorporate a single two-dimensional elastic asperity on the stationary surface. The perturbed pressures obtained by these three different models were compared.
Effects of SiO2 substitution on wettability of laser deposited Ca-P biocoating on Ti-6Al-4V.

PubMed

Yang, Yuling; Paital, Sameer R; Dahotre, Narendra B

2010-09-01

Silicon (Si) substitution in the crystal structure of calcium phosphate (CaP) ceramics has proved to generate materials with improved bioactivity than their stoichiometric counterpart. In light of this, in the current work, 100 wt% hydroxyapatite (HA) precursor and 25 wt% SiO(2)-HA precursors were used to prepare bioactive coatings on Ti-6Al-4V substrates by a laser cladding technique. The effects of SiO(2) on phase constituents, crystallite size, surface roughness, and surface energy of the CaP coatings were studied. Furthermore, on the basis of these results, the effects and roles of SiO(2) substitution in HA were systematically discussed. X-ray diffraction analysis of the coated samples indicated the presence of various phases such as CaTiO(3), Ca(2)SiO(4), Ca(3)(PO(4))(2), TiO(2) (Anatase), and TiO(2) (Rutile). The addition of SiO(2) in the HA precursor resulted in the refinement of grain size. Confocal laser microscopy characterization of the surface morphology demonstrated an improved surface roughness for samples with 25 wt% SiO(2)-HA precursor compared to the samples with 100 wt% HA precursor processed at 125 cm/min laser speed. The addition of SiO(2) in the HA precursor resulted in the highest surface energy, increased hydrophilicity, and improved biomineralization as compared to the control (untreated Ti-6Al-4V) and the sample with 100 wt% HA as precursor. The microstructural evolution observed using a scanning electron microscopy indicated that the addition of SiO(2) in the HA precursor resulted in the presence of reduced cracking across the cross-section of the bioceramic coating.
On a grain of sand - a microhabitat for the opportunistic agglutinated foraminifera Hemisphaerammina apta n. sp., from the early Eocene Arctic Ocean

NASA Astrophysics Data System (ADS)

McNeil, David H.; Neville, Lisa A.

2018-02-01

Hemisphaerammina apta n. sp. is an attached monothalamous agglutinated foraminifera discovered in shelf sediments of the early Eocene Arctic Ocean. It is a simple yet distinctive component of the endemic agglutinated foraminiferal assemblage that colonized the Arctic Ocean after the microfaunal turnover caused by the Paleocene-Eocene Thermal Maximum. Associated foraminifera are characterized by a high percentage of monothalamous species (up to 60 %) and are entirely agglutinated indicating a brackish (mesohaline) early Eocene Arctic Ocean. Hemisphaerammina apta occurs exclusively as individuals attached to fine detrital grains (0.2 to 1.8 mm) of sediment. It is a small species (0.06 to 0.2 mm in diameter), fine-grained, with a low hemispherical profile, no floor across the attachment area, no substantive marginal flange, no internal structures, and no aperture. Lacking an aperture, it apparently propagated and fed through minute (micrometre-sized) interstitial pores in the test wall. Attachment surfaces vary from concave to convex and rough to smooth. Grains for attachment are diverse in shape and type but are predominantly of quartz and chert. The presence of H. apta in the early Eocene was an opportunistic response to an environment with an active hydrological system (storm events). Attachment to grains of sand would provide a more stable base on a sea floor winnowed by storm-generated currents. Active transport is indicated by the relative abundance of reworked foraminifera mixed with in situ species. Contemporaneous reworking and colonization by H. apta is suggested by its attachment to a reworked specimen of Cretaceous foraminifera.
Influence of Starting Powders on Hydroxyapatite Coatings Fabricated by Room Temperature Spraying Method.

PubMed

Seo, Dong Seok; Lee, Jong Kook; Hwang, Kyu Hong; Hahn, Byung Dong; Yoon, Seog Young

2015-08-01

Three types of raw materials were used for the fabrication of hydroxyapatite coatings by using the room temperature spraying method and their influence on the microstructure and in vitro characteristics were investigated. Starting hydroxyapatite powders for coatings on titanium substrate were prepared by a heat treatment at 1100 °C for 2 h of bovine bone, bone ash, and commercial hydroxyapatite powders. The phase compositions and Ca/P ratios of the three hydroxyapatite coatings were similar to those of the raw materials without decomposition or formation of a new phase. All hydroxyapatite coatings showed a honeycomb structure, but their surface microstructures revealed different features in regards to surface morphology and roughness, based on the staring materials. All coatings consisted of nano-sized grains and had dense microstructure. Inferred from in vitro experiments in pure water, all coatings have a good dissolution-resistance and biostability in water.
Growth and structure of Bi 0.5(Na 0.7K 0.2Li 0.1) 0.5TiO 3 thin films prepared by pulsed laser deposition technique

NASA Astrophysics Data System (ADS)

Lu, Lei; Xiao, Dingquan; Lin, Dunmin; Zhang, Yongbin; Zhu, Jianguo

2009-02-01

Bi 0.5(Na 0.7K 0.2Li 0.1) 0.5TiO 3 (BNKLT) thin films were prepared on Pt/Ti/SiO 2/Si substrates by pulsed laser deposition (PLD) technique. The films prepared were examined by using X-ray diffraction (XRD), scanning electron microscopy (SEM) and atomic force microscopy (AFM). The effects of the processing parameters, such as oxygen pressure, substrate temperature and laser power, on the crystal structure, surface morphology, roughness and deposition rates of the thin films were investigated. It was found that the substrate temperature of 600 °C and oxygen pressure of 30 Pa are the optimized technical parameters for the growth of textured film, and all the thin films prepared have granular structure, homogeneous grain size and smooth surfaces.
Microstructural studies by TEM of diamond films grown by combustion flame

NASA Astrophysics Data System (ADS)

Ma, G.-H. M.; Hirose, Y.; Amanuma, S.; McClure, M.; Prater, J. T.; Glass, J. T.

Microstructures of diamond films grown in an oxygen-acetylene combustion flame were studied by TEM. The O2/C2H2 gas ratio was fixed and the substrate materials and temperature were varied. High quality diamond films were grown by this method at high growth rates of about 30 micron/hr. A rough surface and high density of secondary nucleation sites and microtwins were observed in the diamond grains grown on molybdenum (Mo) at a substrate temperature of 500 C. When the substrate temperature wass raised to between 500 and 870 C, the defect density was greatly reduced, revealing a low density of stacking faults and dislocations. Diamond films grown on Si substrates did not show the same substrate temperature dependence on defect density, at least not over the same temperature range. However, the same correlation between defect density, secondary nucleation, and surface morphology was observed.
Surface and magnetic characteristics of Ni-Mn-Ga/Si (100) thin film

NASA Astrophysics Data System (ADS)

Kumar, S. Vinodh; Raja, M. Manivel; Pandi, R. Senthur; Pandyan, R. Kodi; Mahendran, M.

2016-05-01

Polycrystalline Ni-Mn-Ga thin films have been deposited on Si (100) substrate with different film thickness. The influence of film thickness on the phase structure and magnetic domain of the films has been examined by scanning electron microscope, atomic force microscopy and magnetic force microscopy. Analysis of structural parameters indicates that the film at lower thickness exhibits the coexistence of both austenite and martensite phase, whereas at higher thickness L12 cubic non magnetic phase is noticed. The grains size and the surface roughness increase along with the film thickness and attain the maximum of 45 nm and 34.96 nm, respectively. At lower film thickness, the magnetic stripe domain is found like maze pattern with dark and bright images, while at higher thickness the absence of stripe domains is observed. The magnetic results reveal that the films strongly depend on their phase structure and microstructure which influence by the film thickness.
Influence of the three-dimensional heterogeneous roughness on electrokinetic transport in microchannels.

PubMed

Hu, Yandong; Werner, Carsten; Li, Dongqing

2004-12-15

Surface roughness has been considered as a passive means of enhancing species mixing in electroosmotic flow through microfluidic systems. It is highly desirable to understand the synergetic effect of three-dimensional (3D) roughness and surface heterogeneity on the electrokinetic flow through microchannels. In this study, we developed a three-dimensional finite-volume-based numerical model to simulate electroosmotic transport in a slit microchannel (formed between two parallel plates) with numerous heterogeneous prismatic roughness elements arranged symmetrically and asymmetrically on the microchannel walls. We consider that all 3D prismatic rough elements have the same surface charge or zeta potential, the substrate (the microchannel wall) surface has a different zeta potential. The results showed that the rough channel's geometry and the electroosmotic mobility ratio of the roughness elements' surface to that of the substrate, epsilon(mu), have a dramatic influence on the induced-pressure field, the electroosmotic flow patterns, and the electroosmotic flow rate in the heterogeneous rough microchannels. The associated sample-species transport presents a tidal-wave-like concentration field at the intersection between four neighboring rough elements under low epsilon(mu) values and has a concentration field similar to that of the smooth channels under high epsilon(mu) values.
Prediction of an internal boundary layer on a flat plate after a step change in roughness using a near-wall RANS model

NASA Astrophysics Data System (ADS)

Chu, Minghan; Meng, Fanxiao; Bergstrom, Donald J.

2017-11-01

An in-house computational fluid dynamics code was used to simulate turbulent flow over a flat plate with a step change in roughness, exhibiting a smooth-rough-smooth configuration. An internal boundary layer (IBL) is formed at the transition from the smooth to rough (SR) and then the rough to smooth (RS) surfaces. For an IBL the flow far above the surface has experienced a wall shear stress that is different from the local value. Within a Reynolds-Averaged-Navier-Stokes (RANS) formulation, the two-layer k- ɛ model of Durbin et al. (2001) was implemented to analyze the response of the flow to the change in surface condition. The numerical results are compared to experimental data, including some in-house measurements and the seminal work of Antonia and Luxton (1971,72). This problem captures some aspects of roughness in industrial and environmental applications, such as corrosion and the earth's surface heterogeneity, where the roughness is often encountered as discrete distributions. It illustrates the challenge of incorporating roughness models in RANS that are capable of responding to complex surface roughness profiles.
Surface roughness mediated adhesion forces between borosilicate glass and gram-positive bacteria.

PubMed

Preedy, Emily; Perni, Stefano; Nipiĉ, Damijan; Bohinc, Klemen; Prokopovich, Polina

2014-08-12

It is well-known that a number of surface characteristics affect the extent of adhesion between two adjacent materials. One of such parameters is the surface roughness as surface asperities at the nanoscale level govern the overall adhesive forces. For example, the extent of bacterial adhesion is determined by the surface topography; also, once a bacteria colonizes a surface, proliferation of that species will take place and a biofilm may form, increasing the resistance of bacterial cells to removal. In this study, borosilicate glass was employed with varying surface roughness and coated with bovine serum albumin (BSA) in order to replicate the protein layer that covers orthopedic devices on implantation. As roughness is a scale-dependent process, relevant scan areas were analyzed using atomic force microscope (AFM) to determine Ra; furthermore, appropriate bacterial species were attached to the tip to measure the adhesion forces between cells and substrates. The bacterial species chosen (Staphylococci and Streptococci) are common pathogens associated with a number of implant related infections that are detrimental to the biomedical devices and patients. Correlation between adhesion forces and surface roughness (Ra) was generally better when the surface roughness was measured through scanned areas with size (2 × 2 μm) comparable to bacteria cells. Furthermore, the BSA coating altered the surface roughness without correlation with the initial values of such parameter; therefore, better correlations were found between adhesion forces and BSA-coated surfaces when actual surface roughness was used instead of the initial (nominal) values. It was also found that BSA induced a more hydrophilic and electron donor characteristic to the surfaces; in agreement with increasing adhesion forces of hydrophilic bacteria (as determined through microbial adhesion to solvents test) on BSA-coated substrates.
Interfacial fluctuations of block copolymers: a coarse-grain molecular dynamics simulation study.

PubMed

Srinivas, Goundla; Swope, William C; Pitera, Jed W

2007-12-13

The lamellar and cylindrical phases of block copolymers have a number of technological applications, particularly when they occur in supported thin films. One such application is block copolymer lithography, the use of these materials to subdivide or enhance submicrometer patterns defined by optical or electron beam methods. A key parameter of all lithographic methods is the line edge roughness (LER), because the electronic or optical activities of interest are sensitive to small pattern variations. While mean-field models provide a partial picture of the LER and interfacial width expected for the block interface in a diblock copolymer, these models lack chemical detail. To complement mean-field approaches, we have carried out coarse-grain molecular dynamics simulations on model poly(ethyleneoxide)-poly(ethylethylene) (PEO-PEE) lamellae, exploring the influence of chain length and hypothetical chemical modifications on the observed line edge roughness. As expected, our simulations show that increasing chi (the Flory-Huggins parameter) is the most direct route to decreased roughness, although the addition of strong specific interactions at the block interface can also produce smoother patterns.
Wetting failure of hydrophilic surfaces promoted by surface roughness

PubMed Central

Zhao, Meng-Hua; Chen, Xiao-Peng; Wang, Qing

2014-01-01

Wetting failure is of vital importance to many physical phenomena, such as industrial coating and drop emission. Here we show when and how the surface roughness promotes the destabilization of a moving contact line on a hydrophilic surface. Beyond the balance of the driving force and viscous resistance where a stable wetting interface is sustained, wetting failure occurs and is modified by the roughness of the surface. The promoting effect arises only when the wetting velocity is high enough to create a gas-liquid-solid composite interface in the vicinity of the moving contact line, and it is a function of the intrinsic contact angle and proportion of solid tops. We propose a model to explain splashes of rough solid spheres impacting into liquids. It reveals a novel concept that dynamic wetting on hydrophilic rough surfaces can be similar to that on hydrophobic surfaces, and brings a new way to design surfaces with specific wetting properties. PMID:24948390
A square-force cohesion model and its extraction from bulk measurements

NASA Astrophysics Data System (ADS)

Liu, Peiyuan; Lamarche, Casey; Kellogg, Kevin; Hrenya, Christine

2017-11-01

Cohesive particles remain poorly understood, with order of magnitude differences exhibited for prior, physical predictions of agglomerate size. A major obstacle lies in the absence of robust models of particle-particle cohesion, thereby precluding accurate prediction of the behavior of cohesive particles. Rigorous cohesion models commonly contain parameters related to surface roughness, to which cohesion shows extreme sensitivity. However, both roughness measurement and its distillation into these model parameters are challenging. Accordingly, we propose a ``square-force'' model, where cohesive force remains constant until a cut-off separation. Via DEM simulations, we demonstrate validity of the square-force model as surrogate of more rigorous models, when its two parameters are selected to match the two key quantities governing dense and dilute granular flows, namely maximum cohesive force and critical cohesive energy, respectively. Perhaps more importantly, we establish a method to extract the parameters in the square-force model via defluidization, due to its ability to isolate the effects of the two parameters. Thus, instead of relying on complicated scans of individual grains, determination of particle-particle cohesion from simple bulk measurements becomes feasible. Dow Corning Corporation.
Comparison of Predicted and Measured Turbine Vane Rough Surface Heat Transfer

NASA Technical Reports Server (NTRS)

Boyle, R. J.; Spuckler, C. M.; Lucci, B. L.

2000-01-01

The proposed paper compares predicted turbine vane heat transfer for a rough surface over a wide range of test conditions with experimental data. Predictions were made for the entire vane surface. However, measurements were made only over the suction surface of the vane, and the leading edge region of the pressure surface. Comparisons are shown for a wide range of test conditions. Inlet pressures varied between 3 and 15 psia, and exit Mach numbers ranged between 0.3 and 0.9. Thus, while a single roughened vane was used for the tests, the effective rougness,(k(sup +)), varied by more than a factor of ten. Results were obtained for freestream turbulence levels of 1 and 10%. Heat transfer predictions were obtained using the Navier-Stokes computer code RVCQ3D. Two turbulence models, suitable for rough surface analysis, are incorporated in this code. The Cebeci-Chang roughness model is part of the algebraic turbulence model. The k-omega turbulence model accounts for the effect of roughness in the application of the boundary condition. Roughness causes turbulent flow over the vane surface. Even after accounting for transition, surface roughness significantly increased heat transfer compared to a smooth surface. The k-omega results agreed better with the data than the Cebeci-Chang model. However, the low Reynolds number k-omega model did not accurately account for roughness when the freestream turbulence level was low. The high Reynolds number version of this model was more suitable when the freestream turbulence was low.
Study on Surface Roughness of Modified Silicon Carbide Mirrors polished by Magnetorheological Finishing

NASA Astrophysics Data System (ADS)

Du, Hang; Song, Ci; Li, Shengyi

2018-01-01

In order to obtain high precision and high surface quality silicon carbide mirrors, the silicon carbide mirror substrate is subjected to surface modification treatment. In this paper, the problem of Silicon Carbide (SiC) mirror surface roughness deterioration by MRF is studied. The reasons of surface flaws of “Comet tail” are analyzed. Influence principle of MRF polishing depth and the surface roughness of modified SiC mirrors is obtained by experiments. On this basis, the united process of modified SiC mirrors is proposed which is combined MRF with the small grinding head CCOS. The united process makes improvement in the surface accuracy and surface roughness of modified SiC mirrors.
Nanocrystalline diamond thin films on titanium-6 aluminum-4 vanadium alloy temporomandibular joint prosthesis simulants by microwave plasma chemical vapor deposition

NASA Astrophysics Data System (ADS)

Fries, Marc Douglas

A course of research has been performed to assess the suitability of nanocrystal-line diamond (NCD) films on Ti-6Al-4V alloy as wear-resistant coatings in biomedical implant use. A series of temporomandibular (TMJ) joint condyle simulants were polished and acid-passivated as per ASTM F86 standard for surface preparation of implants. A 3-mum-thick coating of NCD film was deposited by microwave plasma chemical vapor deposition (MPCVD) over the hemispherical articulation surfaces of the simulants. Plasma chemistry conditions were measured and monitored by optical emission spectroscopy (OES), using hydrogen as a relative standard. The films consist of diamond grains around 20 nm in diameter embedded in an amorphous carbon matrix, free of any detectable film stress gradient. Hardness averages 65 GPa and modulus measures 600 GPa at a depth of 250 nm into the film surface. A diffuse film/substrate boundary produces a minimal film adhesion toughness (GammaC) of 158 J/m2. The mean RMS roughness is 14.6 +/- 4.2 nm, with an average peak roughness of 82.6 +/- 65.9 nm. Examination of the surface morphology reveals a porous, dendritic surface. Wear testing resulted in two failed condylar coatings out of three tests. No macroscopic delamination was found on any sample, but micron-scale film pieces broke away, exposing the substrate. Electrochemical corrosion testing shows a seven-fold reduction in corrosion rate with the application of an NCD coating as opposed to polished, passivated Ti-6Al-4V, producing a corrosion rate comparable to wrought Co-Cr-Mo. In vivo biocompatibility testing indicates that implanted NCD films did not elicit an immune response in the rabbit model, and osteointegration was apparent for both compact and trabecular bone on both NCD film and bare Ti-6Al-4V. Overall, NCD thin film material is reasonably smooth, biocompatible, and very well adhered. Wear testing indicates that this material is unacceptable for use in demanding TMJ applications without improvements to wear resistance behavior. Identified problems include high surface roughness due to an inadequate seeding procedure and a porous film surface. It is believed that these problems can be solved by future research, in which case NCD thin films should prove to-be well-suited as wear resistant coatings in biomedical applications.
Unraveling the complexities of the velocity dependency of E. coli retention and release parameters in saturated porous media.

PubMed

Sasidharan, Salini; Bradford, Scott A; Torkzaban, Saeed; Ye, Xueyan; Vanderzalm, Joanne; Du, Xinqiang; Page, Declan

2017-12-15

Escherichia coli transport and release experiments were conducted to investigate the pore-water velocity (v) dependency of the sticking efficiency (α), the fraction of the solid surface area that contributed to retention (S f ), the percentage of injected cells that were irreversibly retained (M irr ), and cell release under different (10-300mM) ionic strength (IS) conditions. Values of α, S f , and M irr increased with increasing IS and decreasing v, but the dependency on v was greatest at intermediate IS (30 and 50mM). Following the retention phase, successive increases in v up to 100 or 150mday -1 and flow interruption of 24h produced negligible amounts of cell release. However, excavation of the sand from the columns in excess electrolyte solution resulted in the release of >80% of the retained bacteria. These observations were explained by: (i) extended interaction energy calculations on a heterogeneous sand collector; (ii) an increase in adhesive strength with the residence time; and (iii) torque balance consideration on rough surfaces. In particular, α, S f , and M irr increased with IS due to lower energy barriers and stronger primary minima. The values of α, S f , and M irr also increased with decreasing v because the adhesive strength increased with the residence time (e.g., an increased probability to diffuse over the energy barrier) and lower hydrodynamic forces diminished cell removal. The controlling influence of lever arms at microscopic roughness locations and grain-grain contacts were used to explain negligible cell removal with large increases in v and large amounts of cell recovery following sand excavation. Results reveal the underlying causes (interaction energy, torque balance, and residence time) of the velocity dependency of E. coli retention and release parameters (k sw , α, and S f ) that are not accounted for in colloid filtration theory. Copyright © 2017 Elsevier B.V. All rights reserved.
Study on Plastic Deformation Characteristics of Shot Peening of Ni-Based Superalloy GH4079

NASA Astrophysics Data System (ADS)

Zhong, L. Q.; Liang, Y. L.; Hu, H.

2017-09-01

In this paper, the X-ray stress diffractometer, surface roughness tester, field emission scanning electron microscope(SEM), dynamic ultra-small microhardness tester were used to measure the surface residual stress and roughness, topography and surface hardness changes of GH4079 superalloy, which was processed by metallographic grinding, turning, metallographic grinding +shot peening and turning + shot peening. Analysized the effects of shot peening parameters on shot peening plastic deformation features; and the effects of the surface state before shot peening on shot peening plastic deformation characteristics. Results show that: the surface residual compressive stress, surface roughness and surface hardness of GH4079 superalloy were increased by shot peening, in addition, the increment of the surface residual compressive stress, surface roughness and surface hardness induced by shot peening increased with increasing shot peening intensity, shot peening time, shot peening pressure and shot hardness, but harden layer depth was not affected considerably. The more plastic deformation degree of before shot peening surface state, the less increment of the surface residual compressive stress, surface roughness and surface hardness induced by shot peening.
Characterization, modeling and simulation of fused deposition modeling fabricated part surfaces

NASA Astrophysics Data System (ADS)

Taufik, Mohammad; Jain, Prashant K.

2017-12-01

Surface roughness is generally used for characterization, modeling and simulation of fused deposition modeling (FDM) fabricated part surfaces. But the average surface roughness is not able to provide the insight of surface characteristics with sharp peaks and deep valleys. It deals in the average sense for all types of surfaces, including FDM fabricated surfaces with distinct surface profile features. The present research work shows that kurtosis and skewness can be used for characterization, modeling and simulation of FDM surfaces because these roughness parameters have the ability to characterize a surface with sharp peaks and deep valleys. It can be critical in certain application areas in tribology and biomedicine, where the surface profile plays an important role. Thus, in this study along with surface roughness, skewness and kurtosis are considered to show a novel strategy to provide new transferable knowledge about FDM fabricated part surfaces. The results suggest that the surface roughness, skewness and kurtosis are significantly different at 0° and in the range (0°, 30°], [30°, 90°] of build orientation.

The effect of brushing with toothpaste containing nano calcium carbonate upon nanofill composite resin surface roughness

NASA Astrophysics Data System (ADS)

Ramadhani, A. M.; Herda, E.; Triaminingsih, S.

2017-08-01

This study aims to determine the effect of brushing with toothpaste containing nanocalcium carbonate on the roughness of nanofill composite resin surface. Brushing was conducted with 3 types of materials for 3 consecutive brushing periods of 10 minutes each. Surface roughness was measured using a surface-roughness tester and the results were analyzed using the repeated ANOVA and the one-way ANOVA test. The surface morphology was observed using SEM after 3 months’ worth of brushing with the 3 materials. It was found that the nanofill composite resin surface-roughness value increased significantly (p<0.005) after brushing with toothpaste containing nano calcium carbonate for 3 months, but the value was not as high as that obtained when brushing with other types of toothpaste.
Spin Hall effect originated from fractal surface

NASA Astrophysics Data System (ADS)

Hajzadeh, I.; Mohseni, S. M.; Movahed, S. M. S.; Jafari, G. R.

2018-05-01

The spin Hall effect (SHE) has shown promising impact in the field of spintronics and magnonics from fundamental and practical points of view. This effect originates from several mechanisms of spin scatterers based on spin–orbit coupling (SOC) and also can be manipulated through the surface roughness. Here, the effect of correlated surface roughness on the SHE in metallic thin films with small SOC is investigated theoretically. Toward this, the self-affine fractal surface in the framework of the Born approximation is exploited. The surface roughness is described by the k-correlation model and is characterized by the roughness exponent H , the in-plane correlation length ξ and the rms roughness amplitude δ. It is found that the spin Hall angle in metallic thin film increases by two orders of magnitude when H decreases from H = 1 to H = 0. In addition, the source of SHE for surface roughness with Gaussian profile distribution function is found to be mainly the side jump scattering while that with a non-Gaussian profile suggests both of the side jump and skew scatterings are present. Our achievements address how details of the surface roughness profile can adjust the SHE in non-heavy metals.
Low-Temperature Friction-Stir Welding of 2024 Aluminum

NASA Technical Reports Server (NTRS)

Benavides, S.; Li, Y.; Murr, L. E.; Brown, D.; McClure, J. C.

1998-01-01

Solid state friction-stir welding (FSW) has been demonstrated to involve dynamic recrystallization producing ultra-fine, equiaxed grain structures to facilitate superplastic deformation as the welding or joining mechanism. However, the average residual, equiaxed, grain size in the weld zone has ranged from roughly 0.5 micron to slightly more than 10 micron, and the larger weld zone grain sizes have been characterized as residual or static grain growth as a consequence of the temperatures in the weld zone (where center-line temperatures in the FSW of 6061 Al have been shown to be as high as 480C or -0.8 T(sub M) where T(sub M) is the absolute melting temperature)). In addition, the average residual weld zone grain size has been observed to increase near the top of the weld, and to decrease with distance on either side of the weld-zone centerline, an d this corresponds roughly to temperature variations within the weld zone. The residual grain size also generally decreases with decreasing FSW tool rotation speed. These observations are consistent with the general rules for recrystallization where the recrystallized grain size decreases with increasing strain (or deformation) at constant strain rate, or with increasing strain-rate, or with increasing strain rate at constant strain; especially at lower ambient temperatures, (or annealing temperatures). Since the recrystallization temperature also decreases with increasing strain rate, the FSW process is somewhat complicated because the ambient temperature, the frictional heating fraction, and the adiabatic heating fraction )proportional to the product of strain and strain-rate) will all influence both the recrystallization and growth within the FSW zone. Significantly reducing the ambient temperature of the base metal or work pieces to be welded would be expected to reduce the residual weld-zone grain size. The practical consequences of this temperature reduction would be the achievement of low temperature welding. This study compares the residual grain sizes and microstructures in 2024 Al friction-stir welded at room temperature (about 30C and low temperature (-30C).
Rough surface reconstruction for ultrasonic NDE simulation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Choi, Wonjae; Shi, Fan; Lowe, Michael J. S.

2014-02-18

The reflection of ultrasound from rough surfaces is an important topic for the NDE of safety-critical components, such as pressure-containing components in power stations. The specular reflection from a rough surface of a defect is normally lower than it would be from a flat surface, so it is typical to apply a safety factor in order that justification cases for inspection planning are conservative. The study of the statistics of the rough surfaces that might be expected in candidate defects according to materials and loading, and the reflections from them, can be useful to develop arguments for realistic safety factors.more » This paper presents a study of real rough crack surfaces that are representative of the potential defects in pressure-containing power plant. Two-dimensional (area) values of the height of the roughness have been measured and their statistics analysed. Then a means to reconstruct model cases with similar statistics, so as to enable the creation of multiple realistic realizations of the surfaces, has been investigated, using random field theory. Rough surfaces are reconstructed, based on a real surface, and results for these two-dimensional descriptions of the original surface have been compared with those from the conventional model based on a one-dimensional correlation coefficient function. In addition, ultrasonic reflections from them are simulated using a finite element method.« less
Relationships between aerodynamic roughness and land use and land cover in Baltimore, Maryland

USGS Publications Warehouse

Nicholas, F.W.; Lewis, J.E.

1980-01-01

Urbanization changes the radiative, thermal, hydrologic, and aerodynamic properties of the Earth's surface. Knowledge of these surface characteristics, therefore, is essential to urban climate analysis. Aerodynamic or surface roughness of urban areas is not well documented, however, because of practical constraints in measuring the wind profile in the presence of large buildings. Using an empirical method designed by Lettau, and an analysis of variance of surface roughness values calculated for 324 samples averaging 0.8 hectare (ha) of land use and land cover sample in Baltimore, Md., a strong statistical relation was found between aerodynamic roughness and urban land use and land cover types. Assessment of three land use and land cover systems indicates that some of these types have significantly different surface roughness characteristics. The tests further indicate that statistically significant differences exist in estimated surface roughness values when categories (classes) from different land use and land cover classification systems are used as surrogates. A Level III extension of the U.S. Geological Survey Level II land use and land cover classification system provided the most reliable results. An evaluation of the physical association between the aerodynamic properties of land use and land cover and the surface climate by numerical simulation of the surface energy balance indicates that changes in surface roughness within the range of values typical of the Level III categories induce important changes in the surface climate.
Direct numerical simulation of flow over dissimilar, randomly distributed roughness elements: A systematic study on the effect of surface morphology on turbulence

NASA Astrophysics Data System (ADS)

Forooghi, Pourya; Stroh, Alexander; Schlatter, Philipp; Frohnapfel, Bettina

2018-04-01

Direct numerical simulations are used to investigate turbulent flow in rough channels, in which topographical parameters of the rough wall are systematically varied at a fixed friction Reynolds number of 500, based on a mean channel half-height h and friction velocity. The utilized roughness generation approach allows independent variation of moments of the surface height probability distribution function [thus root-mean-square (rms) surface height, skewness, and kurtosis], surface mean slope, and standard deviation of the roughness peak sizes. Particular attention is paid to the effect of the parameter Δ defined as the normalized height difference between the highest and lowest roughness peaks. This parameter is used to understand the trends of the investigated flow variables with departure from the idealized case where all roughness elements have the same height (Δ =0 ). All calculations are done in the fully rough regime and for surfaces with high slope (effective slope equal to 0.6-0.9). The rms roughness height is fixed for all cases at 0.045 h and the skewness and kurtosis of the surface height probability density function vary in the ranges -0.33 to 0.67 and 1.9 to 2.6, respectively. The goal of the paper is twofold: first, to investigate the possible effect of topographical parameters on the mean turbulent flow, Reynolds, and dispersive stresses particularly in the vicinity of the roughness crest, and second, to investigate the possibility of using the wall-normal turbulence intensity as a physical parameter for parametrization of the flow. Such a possibility, already suggested for regular roughness in the literature, is here extended to irregular roughness.
Assessing and Mapping of Road Surface Roughness based on GPS and Accelerometer Sensors on Bicycle-Mounted Smartphones

PubMed Central

Shen, Jie; Wan, Mi; Shi, Jiafeng

2018-01-01

The surface roughness of roads is an essential road characteristic. Due to the employed carrying platforms (which are often cars), existing measuring methods can only be used for motorable roads. Until now, there has been no effective method for measuring the surface roughness of un-motorable roads, such as pedestrian and bicycle lanes. This hinders many applications related to pedestrians, cyclists and wheelchair users. In recognizing these research gaps, this paper proposes a method for measuring the surface roughness of pedestrian and bicycle lanes based on Global Positioning System (GPS) and accelerometer sensors on bicycle-mounted smartphones. We focus on the International Roughness Index (IRI), as it is the most widely used index for measuring road surface roughness. Specifically, we analyzed a computing model of road surface roughness, derived its parameters with GPS and accelerometers on bicycle-mounted smartphones, and proposed an algorithm to recognize potholes/humps on roads. As a proof of concept, we implemented the proposed method in a mobile application. Three experiments were designed to evaluate the proposed method. The results of the experiments show that the IRI values measured by the proposed method were strongly and positively correlated with those measured by professional instruments. Meanwhile, the proposed algorithm was able to recognize the potholes/humps that the bicycle passed. The proposed method is useful for measuring the surface roughness of roads that are not accessible for professional instruments, such as pedestrian and cycle lanes. This work enables us to further study the feasibility of crowdsourcing road surface roughness with bicycle-mounted smartphones. PMID:29562731
Estimating small-scale roughness of a rock joint using TLS data

NASA Astrophysics Data System (ADS)

Bitenc, Maja; Kieffer, D. Scott; Khoshelham, Kourosh

2016-04-01

Roughness of a rock joint is an important parameter influencing rock mass stability. Besides the surface amplitude, also the roughness direction- and scale-dependency should be observed (i.e. 3D roughness). Up to now most of roughness measurements and parameters rely on point or profile data obtained on small samples, mostly in a laboratory. State-of-the-art remote sensing technologies supply 3D measurements of an in-situ rock surface and therefore enable a 3D roughness parameterization. Detailed morphology of a remote large-scale vertical structure can be best observed by Terrestrial Laser Scanning (TLS). In a short time and from distances of a few hundred meters, TLS provides relatively dense and precise point cloud. Sturzenegger and Stead [2009] showed that the TLS technology and careful fieldwork allow the extraction of first-order roughness profiles, i.e. the surface irregularities with a wavelength greater than about 10 cm. Our goal is to find the lower limit; this is, to define the smallest discernible detail, and appropriate measuring and processing steps to extract this detail from the TLS data. The smallest observable roughness amplitude depends on the TLS data precision, which is limited mostly by an inherent range error (noise). An influence of the TLS noise on the rock joint roughness was analyzed using highly precise reference data acquired by Advanced TOpometric Sensor (ATOS) on a 20x30 cm rock joint sample. ATOS data were interpolated into 1 mm grid, to which five levels (0.5, 1, 1.5, 2, 2.5 mm) of normally distributed noise were added. The 3D surfaces entered direction-dependent roughness parameter computation after Grasselli [2001]. Average roughness of noisy surfaces logarithmically increase with the noise level and is already doubled for 1 mm noise. Performing Monte Carlo simulation roughness parameter noise sensitivity was investigated. Distribution of roughness differences (roughness of noisy surfaces minus roughness of reference ATOS surface) is approximately normal. Standard deviation of differences on average slightly increases with the noise level, but is strongly dependent on the analysis direction. As proved by different researches within the field of signal, image and also TLS data processing, noise can be, to a certain extent, removed by a post-processing step called denoising. In this research, four denoising methods, namely discrete WT (DWT) and stationary WT (SWT), and classic NLM (NLM) and probabilistic NLM (PNLM), were used on noisy ATOS data. Results were compared based on the (i) height and (ii) roughness differences between denoised surfaces and reference ATOS surface, (iii) the peak signal-to-noise ratio (PSNR) and (iv) the visual check of denoised surface. Increased PSNRs and reduced roughness differences prove the importance of the TLS data denoising procedure. In case of SWT, NLM and PNLM the surface is mostly over smoothed, whereas in case of DWT some noise remains. References: - Grasselli, G. (2001). Shear strength of rock joints based on quantified surface description. École Polytechnique Fédérale de Lausanne. Lausanne, EPFL. - Sturzenegger, M. and D. Stead (2009). "Close-range terrestrial digital photogrammetry and terrestrial laser scanning for discontinuity characterization on rock cuts." Engineering Geology 106(3-4): 163-182.
Bacterial plaque retention on oral hard materials: effect of surface roughness, surface composition, and physisorbed polycarboxylate.

PubMed

McConnell, Marla D; Liu, Yu; Nowak, Andrew P; Pilch, Shira; Masters, James G; Composto, Russell J

2010-03-15

Bacterial adhesion to oral hard materials is dependent on various factors, for example, surface roughness and surface composition. In this study, bacteria retention on three oral hard substrates, hydroxyapatite (HAP), enamel, and polished enamel (p-enamel) were investigated. The surface morphology and roughness of the three substrates were measured by scanning probe microscopy. HAP had the roughest surface, followed by enamel and polished enamel. For each individual substrate type, the roughness was shown to increase with scan size up to 50 microm x 50 microm. For HAP and enamel, roughness decreased considerably after formation of a pellicle, while addition of polymer coating to the pellicle layer reduced roughness much less in comparison. Bacterial surface coverage was measured at 30 min, 3 h, and 24 h on both native and surface-modified substrates, which were coated with two different polycarboxylate-based polymers, Gantrez S97 and Carbopol 940. As a result, the polymer coated surfaces had reduced bacteria coverage compared with the native surfaces over all time points and substrates measured. The reduction is the combined effect of electrostatic repulsion and sequestering of Ca(2+) ions at the surface, which plays a key role in the initial adhesion of bacteria to enamel surfaces in models of plaque formation. (c) 2009 Wiley Periodicals, Inc.
Assessment of physiological performance and perception of pushing different wheelchairs on indoor modular units simulating a surface roughness often encountered in under-resourced settings.

PubMed

Sasaki, Kotaro; Rispin, Karen

2017-01-01

In under-resourced settings where motorized wheelchairs are rarely available, manual wheelchair users with limited upper-body strength and functionalities need to rely on assisting pushers for their mobility. Because traveling surfaces in under-resourced settings are often unpaved and rough, wheelchair pushers could experience high physiological loading. In order to evaluate pushers' physiological loading and to improve wheelchair designs, we built indoor modular units that simulate rough surface conditions, and tested a hypothesis that pushing different wheelchairs would result in different physiological performances and pushers' perception of difficulty on the simulated rough surface. Eighteen healthy subjects pushed two different types of pediatric wheelchairs (Moti-Go manufactured by Motivation, and KidChair by Hope Haven) fitted with a 50-kg dummy on the rough and smooth surfaces at self-selected speeds. Oxygen uptake, traveling distance for 6 minutes, and the rating of difficulty were obtained. The results supported our hypothesis, showing that pushing Moti-Go on the rough surface was physiologically less loading than KidChair, but on the smooth surface, the two wheelchairs did not differ significantly. These results indicate wheelchair designs to improve pushers' performance in under-resourced settings should be evaluated on rough surfaces.
Correlation of bond strength with surface roughness using a new roughness measurement technique.

PubMed

Winkler, M M; Moore, B K

1994-07-01

The correlation between shear bond strength and surface roughness was investigated using new surface measurement methods. Bonding agents and associated resin composites were applied to set amalgam after mechanically roughening its surface. Surface treatments were noe (as set against glass), 80 grit, and 600 grit abrasive paper. Surface roughness (R(a) as measured parallel and perpendicular (+) to the direction of the polishing scratches and true profile length were measured. A knife-edge was applied (rate = 2.54 mm/min) at the bonding agent/amalgam interface of each sample until failure. Coefficients of determination for mean bond strength vs either roughness (R(a), of profile length were significantly higher for measurements in parallel directions than for those measurements in (+) directions. The shear bond strength to set amalgam for a PENTA-containing adhesives system (L.D. Caulk Division) was not significantly different from that of a PENTA-free adhesive (3M Dental Products Division), even though PENTA has been reported to increase bond strength to nonprecious metals. The shear bond strength of resin composite to amalgam is correlated to surface roughness when it is measured parallel to the polishing scratches. This correlation is significantly lower when surface roughness is measured in the typical manner, perpendicular to the polishing scratches.
Fast, Statistical Model of Surface Roughness for Ion-Solid Interaction Simulations and Efficient Code Coupling

NASA Astrophysics Data System (ADS)

Drobny, Jon; Curreli, Davide; Ruzic, David; Lasa, Ane; Green, David; Canik, John; Younkin, Tim; Blondel, Sophie; Wirth, Brian

2017-10-01

Surface roughness greatly impacts material erosion, and thus plays an important role in Plasma-Surface Interactions. Developing strategies for efficiently introducing rough surfaces into ion-solid interaction codes will be an important step towards whole-device modeling of plasma devices and future fusion reactors such as ITER. Fractal TRIDYN (F-TRIDYN) is an upgraded version of the Monte Carlo, BCA program TRIDYN developed for this purpose that includes an explicit fractal model of surface roughness and extended input and output options for file-based code coupling. Code coupling with both plasma and material codes has been achieved and allows for multi-scale, whole-device modeling of plasma experiments. These code coupling results will be presented. F-TRIDYN has been further upgraded with an alternative, statistical model of surface roughness. The statistical model is significantly faster than and compares favorably to the fractal model. Additionally, the statistical model compares well to alternative computational surface roughness models and experiments. Theoretical links between the fractal and statistical models are made, and further connections to experimental measurements of surface roughness are explored. This work was supported by the PSI-SciDAC Project funded by the U.S. Department of Energy through contract DOE-DE-SC0008658.
Aerodynamic Surface Stress Intermittency and Conditionally Averaged Turbulence Statistics

NASA Astrophysics Data System (ADS)

Anderson, W.

2015-12-01

Aeolian erosion of dry, flat, semi-arid landscapes is induced (and sustained) by kinetic energy fluxes in the aloft atmospheric surface layer. During saltation -- the mechanism responsible for surface fluxes of dust and sediment -- briefly suspended sediment grains undergo a ballistic trajectory before impacting and `splashing' smaller-diameter (dust) particles vertically. Conceptual models typically indicate that sediment flux, q (via saltation or drift), scales with imposed aerodynamic (basal) stress raised to some exponent, n, where n > 1. Since basal stress (in fully rough, inertia-dominated flows) scales with the incoming velocity squared, u^2, it follows that q ~ u^2n (where u is some relevant component of the above flow field, u(x,t)). Thus, even small (turbulent) deviations of u from its time-averaged value may play an enormously important role in aeolian activity on flat, dry landscapes. The importance of this argument is further augmented given that turbulence in the atmospheric surface layer exhibits maximum Reynolds stresses in the fluid immediately above the landscape. In order to illustrate the importance of surface stress intermittency, we have used conditional averaging predicated on aerodynamic surface stress during large-eddy simulation of atmospheric boundary layer flow over a flat landscape with momentum roughness length appropriate for the Llano Estacado in west Texas (a flat agricultural region that is notorious for dust transport). By using data from a field campaign to measure diurnal variability of aeolian activity and prevailing winds on the Llano Estacado, we have retrieved the threshold friction velocity (which can be used to compute threshold surface stress under the geostrophic balance with the Monin-Obukhov similarity theory). This averaging procedure provides an ensemble-mean visualization of flow structures responsible for erosion `events'. Preliminary evidence indicates that surface stress peaks are associated with the passage of inclined, high-momentum regions flanked by adjacent low-momentum regions. We will characterize geometric attributes of such structures and explore streamwise and vertical vorticity distribution within the conditionally averaged flow field.
Flow resistance dynamics in step‐pool channels: 2. Partitioning between grain, spill, and woody debris resistance

USGS Publications Warehouse

Wilcox, Andrew C.; Nelson, Jonathan M.; Wohl, Ellen E.

2006-01-01

In step‐pool stream channels, flow resistance is created primarily by bed sediments, spill over step‐pool bed forms, and large woody debris (LWD). In order to measure resistance partitioning between grains, steps, and LWD in step‐pool channels we completed laboratory flume runs in which total resistance was measured with and without grains and steps, with various LWD configurations, and at multiple slopes and discharges. Tests of additive approaches to resistance partitioning found that partitioning estimates are highly sensitive to the order in which components are calculated and that such approaches inflate the values of difficult‐to‐measure components that are calculated by subtraction from measured components. This effect is especially significant where interactions between roughness features create synergistic increases in resistance such that total resistance measured for combinations of resistance components greatly exceeds the sum of those components measured separately. LWD contributes large proportions of total resistance by creating form drag on individual pieces and by increasing the spill resistance effect of steps. The combined effect of LWD and spill over steps was found to dominate total resistance, whereas grain roughness on step treads was a small component of total resistance. The relative contributions of grain, spill, and woody debris resistance were strongly influenced by discharge and to a lesser extent by LWD density. Grain resistance values based on published formulas and debris resistance values calculated using a cylinder drag approach typically underestimated analogous flume‐derived values, further illustrating sources of error in partitioning methods and the importance of accounting for interaction effects between resistance components.
Flow resistance dynamics in step-pool channels: 2. Partitioning between grain, spill, and woody debris resistance

NASA Astrophysics Data System (ADS)

Wilcox, Andrew C.; Nelson, Jonathan M.; Wohl, Ellen E.

2006-05-01

In step-pool stream channels, flow resistance is created primarily by bed sediments, spill over step-pool bed forms, and large woody debris (LWD). In order to measure resistance partitioning between grains, steps, and LWD in step-pool channels we completed laboratory flume runs in which total resistance was measured with and without grains and steps, with various LWD configurations, and at multiple slopes and discharges. Tests of additive approaches to resistance partitioning found that partitioning estimates are highly sensitive to the order in which components are calculated and that such approaches inflate the values of difficult-to-measure components that are calculated by subtraction from measured components. This effect is especially significant where interactions between roughness features create synergistic increases in resistance such that total resistance measured for combinations of resistance components greatly exceeds the sum of those components measured separately. LWD contributes large proportions of total resistance by creating form drag on individual pieces and by increasing the spill resistance effect of steps. The combined effect of LWD and spill over steps was found to dominate total resistance, whereas grain roughness on step treads was a small component of total resistance. The relative contributions of grain, spill, and woody debris resistance were strongly influenced by discharge and to a lesser extent by LWD density. Grain resistance values based on published formulas and debris resistance values calculated using a cylinder drag approach typically underestimated analogous flume-derived values, further illustrating sources of error in partitioning methods and the importance of accounting for interaction effects between resistance components.
Surface roughness manifestations of deep-seated landslide processes

NASA Astrophysics Data System (ADS)

Booth, A. M.; Roering, J. J.; Lamb, M. P.

2012-12-01

In many mountainous drainage basins, deep-seated landslides evacuate large volumes of sediment from small surface areas, leaving behind a strong topographic signature that sets landscape roughness over a range of spatial scales. At long spatial wavelengths of hundreds to thousands of meters, landslides tend to inhibit channel incision and limit topographic relief, effectively smoothing the topography at this length scale. However, at short spatial wavelengths on the order of meters, deformation of deep-seated landslides generates surface roughness that allows expert mappers or automated algorithms to distinguish landslides from the surrounding terrain. Here, we directly connect the characteristic spatial wavelengths and amplitudes of this fine scale surface roughness to the underlying landslide deformation processes. We utilize the two-dimensional wavelet transform with high-resolution, airborne LiDAR-derived digital elevation models to systematically document the characteristic length scales and amplitudes of different kinematic units within slow moving earthflows, a common type of deep-seated landslide. In earthflow source areas, discrete slumped blocks generate high surface roughness, reflecting an extensional deformation regime. In earthflow transport zones, where material translates with minimal surface deformation, roughness decreases as other surface processes quickly smooth short wavelength features. In earthflow depositional toes, compression folds and thrust faults again increase short wavelength surface roughness. When an earthflow becomes inactive, roughness in all of these kinematic zones systematically decreases with time, allowing relative dating of earthflow deposits. We also document how each of these roughness expressions depends on earthflow velocity, using sub-pixel change detection software (COSI-Corr) and pairs of orthorectified aerial photographs to determine spatially extensive landslide surface displacements. In source areas, the wavelength of slumped blocks tends to correlate with velocity as predicted by a simple sliding block model, but the amplitude is insensitive to velocity, suggesting that landslide depth rather than velocity sets this characteristic block amplitude. In both transport zones and depositional toes, the amplitude of the surface roughness is higher where the longitudinal gradient in velocity is higher, confirming that differential movement generates and maintains this fine scale roughness.
Using Multi-Dimensional Microwave Remote Sensing Information for the Retrieval of Soil Surface Roughness

NASA Astrophysics Data System (ADS)

Marzahn, P.; Ludwig, R.

2016-06-01

In this Paper the potential of multi parametric polarimetric SAR (PolSAR) data for soil surface roughness estimation is investigated and its potential for hydrological modeling is evaluated. The study utilizes microwave backscatter collected from the Demmin testsite in the North-East Germany during AgriSAR 2006 campaign using fully polarimetric L-Band airborne SAR data. For ground truthing extensive soil surface roughness in addition to various other soil physical properties measurements were carried out using photogrammetric image matching techniques. The correlation between ground truth roughness indices and three well established polarimetric roughness estimators showed only good results for Re[ρRRLL] and the RMS Height s. Results in form of multitemporal roughness maps showed only satisfying results due to the fact that the presence and development of particular plants affected the derivation. However roughness derivation for bare soil surfaces showed promising results.
Analysis of Surface Roughness at Overlapping Laser Shock Peening

NASA Astrophysics Data System (ADS)

Dai, F. Z.; Zhang, Z. D.; Zhou, J. Z.; Lu, J. Z.; Zhang, Y. K.

2016-02-01

The overlapping effects on surface roughness are studied when samples are treated by laser shock peening (LSP). Surface roughness of overlapped circular laser spot is calculated by ISO 25178 height parameters. The usually used overlapping styles namely isosceles-right-triangle-style (AAP) and equilateral-triangle-style (AAA) are carefully investigated when the overlapping degree in x-axis (ηx) is below 50%. Surface roughness of isosceles-right-triangle-style attains its minimum value at ηx of 29.3%, and attains its maximum value at ηx of 43.6%. Surface roughness of equilateral-triangle-style attains its minimum value at ηx of 42.3%, and attains its maximum value at ηx of 32%. Experimental results are well consistent with theoretical analysis.
Pre-coalescence scaling of graphene island sizes

NASA Astrophysics Data System (ADS)

Das, Shantanu; Drucker, Jeff

2018-05-01

Graphene grown using cold-wall chemical vapor deposition on Cu surfaces follows a classical nucleation and growth mechanism. Following nucleation at the earliest growth stages, isolated crystallites grow, impinge, and coalesce to form a continuous layer. During the pre-coalescence growth regime, the size distributions of graphene crystallites exhibit scaling of the form N(s) = θ/⟨s⟩2 g(s/⟨s⟩), where s is the island area, θ is the graphene coverage, ⟨s⟩ is the average island area, N is the areal density, and g(x) is a scaling function. For graphene grown on Cu surfaces that have been annealed in a reducing Ar + H2 ambient, excellent data collapse onto a universal Avrami scaling function is observed irrespective of graphene coverage, surface roughness, or Cu grain size. This result is interpreted to indicate attachment-limited growth and desorption of diffusing C-containing species. Graphene grown on Cu surfaces that were annealed in a non-reducing environment exhibits a qualitatively different scaling function, indicating diffusion-limited growth with a lower attachment barrier combined with C detachment from the graphene edges.
Orbital SAR and Ground-Penetrating Radar for Mars: Complementary Tools in the Search for Water

NASA Technical Reports Server (NTRS)

Campbell, B. A.; Grant, J. A.

2000-01-01

The physical structure and compositional variability of the upper martian crust is poorly understood. Optical and infrared measurements probe at most the top few cm of the surface layer and indicate the presence of layered volcanics and sediments, but it is likely that permafrost, hydrothermal deposits, and transient liquid water pockets occur at depths of meters to kilometers within the crust. An orbital synthetic aperture radar (SAR) can provide constraints on surface roughness, the depth of fine-grained aeolian or volcanic deposits, and the presence of strongly absorbing near-surface deposits such as carbonates. This information is crucial to the successful landing and operation of any rover designed to search for subsurface water. A rover-based ground-penetrating radar (GPR) can reveal layering in the upper crust, the presence of erosional or other subsurface horizons, depth to a permafrost layer, and direct detection of near-surface transient liquid water. We detail here the radar design parameters likely to provide the best information for Mars, based on experience with SAR and GPR in analogous terrestrial or planetary environments.

Electrodeposited Ni nanowires-track etched P.E.T. composites as selective solar absorbers

NASA Astrophysics Data System (ADS)

Lukhwa, R.; Sone, B.; Kotsedi, L.; Madjoe, R.; Maaza, M.

2018-05-01

This contribution reports on the structural, optical and morphological properties of nanostructured flexible solar-thermal selective absorber composites for low temperature applications. The candidate material in the system is consisting of electrodeposited nickel nano-cylinders embedded in track-etched polyethylene terephthalate (PET) host membrane of pore sizes ranging between 0.3-0.8µm supported by conductive nickel thin film of about 0.5µm. PET were irradiated with 11MeV/u high charged xenon (Xe) ions at normal incidence. The tubular and metallic structure of the nickel nano-cylinders within the insulator polymeric host forms a typical ceramic-metal nano-composite "Cermet". The produced material was characterized by the following techniques: X-ray diffraction (XRD) for structural characterization to determine preferred crystallographic structure, and grain size of the materials; Scanning electron microscopy (SEM) to determine surface morphology, particle size, and visual imaging of distribution of structures on the surface of the substrate; Atomic force microscopy (AFM) to characterize surface roughness, surface morphology, and film thickness, and UV-Vis-NIR spectrophotometer to measure the reflectance, then to determine solar absorption
Effect of sandblasting on surface roughness of zirconia-based ceramics and shear bond strength of veneering porcelain.

PubMed

He, Min; Zhang, Zutai; Zheng, Dongxiang; Ding, Ning; Liu, Yan

2014-01-01

This study aims to investigate the effect of sandblasting on the surface roughness of zirconia and the shear bond strength of the veneering porcelain. Pre-sintered zirconia plates were prepared and divided into four groups. Group A were not treated at all; group B were first sandblasted under 0.2 MPa pressure and then densely sintered; group C and D were sintered first, and then sandblasted under 0.2 MPa and 0.4 MPa pressures respectively. Surface roughness was measured and 3D roughness was reconstructed for the specimens, which were also analyzed with X-ray diffractometry. Finally after veneering porcelain sintering, shear bond tests were conducted. Sandblasting zirconia before sintering significantly increased surface roughness and the shear bond strength between zirconia and veneering porcelain (p<0.05). Sandblasting zirconia before sintering is a useful method to increase surface roughness and could successfully improve the bonding strength of veneering porcelain.
Comparison of aerodynamically and model-derived roughness lengths (zo) over diverse surfaces, central Mojave Desert, California, USA

USGS Publications Warehouse

MacKinnon, D.J.; Clow, G.D.; Tigges, R.K.; Reynolds, R.L.; Chavez, P.S.

2004-01-01

The vulnerability of dryland surfaces to wind erosion depends importantly on the absence or the presence and character of surface roughness elements, such as plants, clasts, and topographic irregularities that diminish wind speed near the surface. A model for the friction velocity ratio has been developed to account for wind sheltering by many different types of co-existing roughness elements. Such conditions typify a monitored area in the central Mojave Desert, California, that experiences frequent sand movement and dust emission. Two additional models are used to convert the friction velocity ratio to the surface roughness length (zo) for momentum. To calculate roughness lengths from these models, measurements were made at 11 sites within the monitored area to characterize the surface roughness element. Measurements included (1) the number of roughness species (e.g., plants, small-scale topography, clasts), and their associated heights and widths, (2) spacing among species, and (3) vegetation porosity (a measurement of the spatial distribution of woody elements of a plant). Documented or estimated values of drag coefficients for different species were included in the modeling. At these sites, wind-speed profiles were measured during periods of neutral atmospheric stability using three 9-m towers with three or four calibrated anemometers on each. Modeled roughness lengths show a close correspondence (correlation coefficient, 0.84-0.86) to the aerodynamically determined values at the field sites. The geometric properties of the roughness elements in the model are amenable to measurement at much higher temporal and spatial resolutions using remote-sensing techniques than can be accomplished through laborious ground-based methods. A remote-sensing approach to acquire values of the modeled roughness length is particularly important for the development of linked surface/atmosphere wind-erosion models sensitive to climate variability and land-use changes in areas such as the southwestern United States, where surface roughness has large spatial and temporal variations. ?? 2004 Elsevier B.V. All rights reserved.
Interfacial phonon scattering and transmission loss in > 1 µm thick silicon-on-insulator thin films

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jiang, Puqing; Lindsay, Lucas R.; Huang, Xi

Scattering of phonons at boundaries of a crystal (grains, surfaces, or solid/solid interfaces) is characterized by the phonon wavelength, the angle of incidence, and the interface roughness, as historically evaluated using a specularity parameter p formulated by Ziman [Electrons and Phonons (Clarendon Press, Oxford, 1960)]. This parameter was initially defined to determine the probability of a phonon specularly reflecting or diffusely scattering from the rough surface of a material. The validity of Ziman's theory as extended to solid/solid interfaces has not been previously validated. Here, to better understand the interfacial scattering of phonons and to test the validity of Ziman'smore » theory, we precisely measured the in-plane thermal conductivity of a series of Si films in silicon-on-insulator (SOI) wafers by time-domain thermoreflectance (TDTR) for a Si film thickness range of 1–10 μm and a temperature range of 100–300 K. The Si/SiO 2 interface roughness was determined to be 0.11±0.04nm using transmission electron microscopy (TEM). Furthermore, we compared our in-plane thermal conductivity measurements to theoretical calculations that combine first-principles phonon transport with Ziman's theory. Calculations using Ziman's specularity parameter significantly overestimate values from the TDTR measurements. We attribute this discrepancy to phonon transmission through the solid/solid interface into the substrate, which is not accounted for by Ziman's theory for surfaces. The phonons that are specularly transmitted into an amorphous layer will be sufficiently randomized by the time they come back to the crystalline Si layer, the effect of which is practically equivalent to a diffuse reflection at the interface. Finally, we derive a simple expression for the specularity parameter at solid/amorphous interfaces and achieve good agreement between calculations and measurement values.« less
Interfacial phonon scattering and transmission loss in > 1 µm thick silicon-on-insulator thin films

DOE PAGES

Jiang, Puqing; Lindsay, Lucas R.; Huang, Xi; ...

2018-05-17

Scattering of phonons at boundaries of a crystal (grains, surfaces, or solid/solid interfaces) is characterized by the phonon wavelength, the angle of incidence, and the interface roughness, as historically evaluated using a specularity parameter p formulated by Ziman [Electrons and Phonons (Clarendon Press, Oxford, 1960)]. This parameter was initially defined to determine the probability of a phonon specularly reflecting or diffusely scattering from the rough surface of a material. The validity of Ziman's theory as extended to solid/solid interfaces has not been previously validated. Here, to better understand the interfacial scattering of phonons and to test the validity of Ziman'smore » theory, we precisely measured the in-plane thermal conductivity of a series of Si films in silicon-on-insulator (SOI) wafers by time-domain thermoreflectance (TDTR) for a Si film thickness range of 1–10 μm and a temperature range of 100–300 K. The Si/SiO 2 interface roughness was determined to be 0.11±0.04nm using transmission electron microscopy (TEM). Furthermore, we compared our in-plane thermal conductivity measurements to theoretical calculations that combine first-principles phonon transport with Ziman's theory. Calculations using Ziman's specularity parameter significantly overestimate values from the TDTR measurements. We attribute this discrepancy to phonon transmission through the solid/solid interface into the substrate, which is not accounted for by Ziman's theory for surfaces. The phonons that are specularly transmitted into an amorphous layer will be sufficiently randomized by the time they come back to the crystalline Si layer, the effect of which is practically equivalent to a diffuse reflection at the interface. Finally, we derive a simple expression for the specularity parameter at solid/amorphous interfaces and achieve good agreement between calculations and measurement values.« less
How surface mounds and depressions change during rainfall events

USDA-ARS?s Scientific Manuscript database

The soil roughness, or microrelief, controls processes occurring on the surface. Although there are numerous studies on how soil roughness affects soil erosion processes, little are focused on quantifying different roughness functions on surface hydrology and erosion, i.e., water diverging and soil...
Intense deformation field at oceanic front inferred from directional sea surface roughness observations

NASA Astrophysics Data System (ADS)

Rascle, Nicolas; Molemaker, Jeroen; Marié, Louis; Nouguier, Frédéric; Chapron, Bertrand; Lund, Björn; Mouche, Alexis

2017-06-01

Fine-scale current gradients at the ocean surface can be observed by sea surface roughness. More specifically, directional surface roughness anomalies are related to the different horizontal current gradient components. This paper reports results from a dedicated experiment during the Lagrangian Submesoscale Experiment (LASER) drifter deployment. A very sharp front, 50 m wide, is detected simultaneously in drifter trajectories, sea surface temperature, and sea surface roughness. A new observational method is applied, using Sun glitter reflections during multiple airplane passes to reconstruct the multiangle roughness anomaly. This multiangle anomaly is consistent with wave-current interactions over a front, including both cross-front convergence and along-front shear with cyclonic vorticity. Qualitatively, results agree with drifters and X-band radar observations. Quantitatively, the sharpness of roughness anomaly suggests intense current gradients, 0.3 m s-1 over the 50 m wide front. This work opens new perspectives for monitoring intense oceanic fronts using drones or satellite constellations.
Quantifying surface roughness effects on phonon transport in silicon nanowires.

PubMed

Lim, Jongwoo; Hippalgaonkar, Kedar; Andrews, Sean C; Majumdar, Arun; Yang, Peidong

2012-05-09

Although it has been qualitatively demonstrated that surface roughness can reduce the thermal conductivity of crystalline Si nanowires (SiNWs), the underlying reasons remain unknown and warrant quantitative studies and analysis. In this work, vapor-liquid-solid (VLS) grown SiNWs were controllably roughened and then thoroughly characterized with transmission electron microscopy to obtain detailed surface profiles. Once the roughness information (root-mean-square, σ, correlation length, L, and power spectra) was extracted from the surface profile of a specific SiNW, the thermal conductivity of the same SiNW was measured. The thermal conductivity correlated well with the power spectra of surface roughness, which varies as a power law in the 1-100 nm length scale range. These results suggest a new realm of phonon scattering from rough interfaces, which restricts phonon transport below the Casimir limit. Insights gained from this study can help develop a more concrete theoretical understanding of phonon-surface roughness interactions as well as aid the design of next generation thermoelectric devices.
Influence of polishing on surface roughness following toothbrushing wear of composite resins.

PubMed

Dalla-Vecchia, Karine Battestin; Taborda, Talita Damas; Stona, Deborah; Pressi, Heloísa; Burnett Júnior, Luiz Henrique; Rodrigues-Junior, Sinval Adalberto

2017-01-01

This study aimed to evaluate the influence of different polishing systems on the surface roughness of composite resins following procedures to simulate the effects of toothbrushing over time. Four currently available commercial composites were used to make 128 cylindrical specimens. The specimens were randomly allocated to polishing with a 1-step polisher or 1 of 3 multistep polishers (n = 8 per group). The baseline surface roughness was measured, and the specimens were submitted to 5000, 10,000, and 20,000 brushing cycles to represent toothbrushing throughout 6, 12, and 24 months, respectively. Results showed that surface roughness was influenced by the type of composite and polishing system and was not influenced by the simulated toothbrushing time. However, the surface roughness, as challenged by toothbrushing wear, was affected by the interaction among the composite, the polisher, and the toothbrushing time. The 1-step polisher produced the highest surface roughness and influenced toothbrushing wear resistance of some composites.
Surface roughness model based on force sensors for the prediction of the tool wear.

PubMed

de Agustina, Beatriz; Rubio, Eva María; Sebastián, Miguel Ángel

2014-04-04

In this study, a methodology has been developed with the objective of evaluating the surface roughness obtained during turning processes by measuring the signals detected by a force sensor under the same cutting conditions. In this way, the surface quality achieved along the process is correlated to several parameters of the cutting forces (thrust forces, feed forces and cutting forces), so the effect that the tool wear causes on the surface roughness is evaluated. In a first step, the best cutting conditions (cutting parameters and radius of tool) for a certain quality surface requirement were found for pieces of UNS A97075. Next, with this selection a model of surface roughness based on the cutting forces was developed for different states of wear that simulate the behaviour of the tool throughout its life. The validation of this model reveals that it was effective for approximately 70% of the surface roughness values obtained.
Surface roughness effects on bidirectional reflectance

NASA Technical Reports Server (NTRS)

Smith, T. F.; Hering, R. G.

1972-01-01

An experimental study of surface roughness effects on bidirectional reflectance of metallic surfaces is presented. A facility capable of irradiating a sample from normal to grazing incidence and recording plane of incidence bidirectional reflectance measurements was developed. Samples consisting of glass, aluminum alloy, and stainless steel materials were selected for examination. Samples were roughened using standard grinding techniques and coated with a radiatively opaque layer of pure aluminum. Mechanical surface roughness parameters, rms heights and rms slopes, evaluated from digitized surface profile measurements are less than 1.0 micrometers and 0.28, respectively. Rough surface specular, bidirectional, and directional reflectance measurements for selected values of polar angle of incidence and wavelength of incident energy within the spectral range of 1 to 14 micrometers are reported. The Beckmann bidirectional reflectance model is compared with reflectance measurements to establish its usefulness in describing the magnitude and spatial distribution of energy reflected from rough surfaces.
Shear Model Development of Limestone Joints with Incorporating Variations of Basic Friction Coefficient and Roughness Components During Shearing

NASA Astrophysics Data System (ADS)

Mehrishal, Seyedahmad; Sharifzadeh, Mostafa; Shahriar, Korosh; Song, Jae-Jon

2017-04-01

In relation to the shearing of rock joints, the precise and continuous evaluation of asperity interlocking, dilation, and basic friction properties has been the most important task in the modeling of shear strength. In this paper, in order to investigate these controlling factors, two types of limestone joint samples were prepared and CNL direct shear tests were performed on these joints under various shear conditions. One set of samples were travertine and another were onyx marble with slickensided surfaces, surfaces ground to #80, and rough surfaces were tested. Direct shear experiments conducted on slickensided and ground surfaces of limestone indicated that by increasing the applied normal stress, under different shearing rates, the basic friction coefficient decreased. Moreover, in the shear tests under constant normal stress and shearing rate, the basic friction coefficient remained constant for the different contact sizes. The second series of direct shear experiments in this research was conducted on tension joint samples to evaluate the effect of surface roughness on the shear behavior of the rough joints. This paper deals with the dilation and roughness interlocking using a method that characterizes the surface roughness of the joint based on a fundamental combined surface roughness concept. The application of stress-dependent basic friction and quantitative roughness parameters in the continuous modeling of the shear behavior of rock joints is an important aspect of this research.
Surface roughness estimation by inversion of the Hapke photometric model on optical data simulated using a ray tracing code

NASA Astrophysics Data System (ADS)

Champion, J.; Ristorcelli, T.; Ferrari, C. C.; Briottet, X.; Jacquemoud, S.

2013-12-01

Surface roughness is a key physical parameter that governs various processes (incident radiation distribution, temperature, erosion,...) on Earth and other Solar System objects. Its impact on the scattering function of incident electromagnetic waves is difficult to model. In the 80's, Hapke provided an approximate analytic solution for the bidirectional reflectance distribution function (BRDF) of a particulate medium and, later on, included the effect of surface roughness as a correction factor for the BRDF of a smooth surface. This analytical radiative transfer model is widely used in solar system science whereas its ability to remotely determine surface roughness is still a question at issue. The validation of the Hapke model has been only occasionally undertaken due to the lack of radiometric data associated with field measurement of surface roughness. We propose to validate it on Earth, on several volcanic terrains for which very high resolution digital elevation models are available at small scale. We simulate the BRDF of these DEMs thanks to a ray-tracing code and fit them with the Hapke model to retrieve surface roughness. The mean slope angle of the facets, which quantifies surface roughness, can be fairly well retrieved when most conditions are met, i.e. a random-like surface and little multiple scattering between the facets. A directional sensitivity analysis of the Hapke model confirms that both surface intrinsic optical properties (facet's reflectance or single scattering albedo) and roughness are the most influential variables on ground BRDFs. Their interactions in some directions explain why their separation may be difficult, unless some constraints are introduced in the inversion process. Simulation of soil surface BRDF at different illumination and viewing angles
Specular Reflection from Rough Surfaces Revisited

NASA Astrophysics Data System (ADS)

Yasuda, Kensei; Kim, Alvin; Cho, Hayley; Timofejev, Timofej; Walecki, Wojciech J.; Klep, James; Edelson, Amy S.; Walecki, Abigail S.; Walecki, Eve S.; Walecki, Peter S.

2016-10-01

In his beautiful paper, Hasan Fakhruddin reported observations of mirror-like reflections in the rough surface of a ground glass plate. Similar effects have been recently employed for metrology of the roughness of optical diffusers used in modern light emitting device illumination systems. We report the observations of specular reflection in nontransparent rough surfaces at oblique angles, where roughness was treated as a variable. We present a simple trigonometry-based model explaining the observed phenomenon, which we experimentally validated using aluminum surfaces that have controlled roughness. The reported demonstration requires no special equipment, other than cellphone cameras, dielectric or metal plate, and sandpaper, and serves as an introduction to wave optics. This activity can be used to get further insight into everyday applications of wave optics for students already familiar with wave optics fundamentals.
Surface roughness scattering of electrons in bulk mosfets

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zuverink, Amanda Renee

2015-11-01

Surface-roughness scattering of electrons at the Si-SiO 2 interface is a very important consideration when analyzing Si metal-oxide-semiconductor field-effect transistors (MOSFETs). Scattering reduces the mobility of the electrons and degrades the device performance. 250-nm and 50-nm bulk MOSFETs were simulated with varying device parameters and mesh sizes in order to compare the effects of surface-roughness scattering in multiple devices. The simulation framework includes the ensemble Monte Carlo method used to solve the Boltzmann transport equation coupled with a successive over-relaxation method used to solve the two-dimensional Poisson's equation. Four methods for simulating the surface-roughness scattering of electrons were implemented onmore » both devices and compared: the constant specularity parameter, the momentum-dependent specularity parameter, and the real-space-roughness method with both uniform and varying electric fields. The specularity parameter is the probability of an electron scattering speculariy from a rough surface. It can be chosen as a constant, characterizing partially diffuse scattering of all electrons from the surface the same way, or it can be momentum dependent, where the size of rms roughness and the normal component of the electron wave number determine the probability of electron-momentum randomization. The real-space rough surface method uses the rms roughness height and correlation length of an actual MOSFET to simulate a rough interface. Due to their charge, electrons scatter from the electric field and not directly from the surface. If the electric field is kept uniform, the electrons do not perceive the roughness and scatter as if from a at surface. However, if the field is allowed to vary, the electrons scatter from the varying electric field as they would in a MOSFET. These methods were implemented for both the 50-nm and 250-nm MOSFETs, and using the rms roughness heights and correlation lengths for real devices. The current-voltage and mobility-electric field curves were plotted for each method on the two devices and compared. The conclusion is that the specularity-parameter methods are valuable as simple models for relatively smooth interfaces. However, they have limitations, as they cannot accurately describe the drastic reduction in the current and the electron mobility that occur in MOSFETs with very rough Si-SiO 2 interfaces.« less
[Effect of SiO₂-ZrO₂slurry coating on surface performance of zirconia ceramic].

PubMed

Du, Qiao; Niu, Guangliang; Lin, Hong; Jiang, Ruodan

2015-11-01

To evaluate the effect of SiO₂-ZrO₂slurry coating on surface performance of zirconia ceramic. Seventy pre-sintered zirconia discs were randomly divided into seven groups with 10 discs per group. Sample discs in each group received one of the following seven different surface treatments, namely, sintered (group AS), sand blasting after sintered (group SB), coated with slurry of mole ratio of SiO₂to ZrO₂2:1 (group 2SiO₂-1ZrO₂), coated with slurry of mole ratio of SiO₂to ZrO₂1:1 (group 1SiO₂-1ZrO₂), coated with slurry of mole ratio of SiO₂to ZrO₂1:2 (group 1SiO₂-2ZrO₂), coated with slurry of mole ratio of SiO₂to ZrO₂1:3 (group 1SiO₂-3ZrO₂), coated with slurry of mole ratio of SiO₂to ZrO₂1:4 (group 1SiO₂-4ZrO₂). Profilometer, X-ray diffractometer (XRD), energy dispersive spectrometer, scanning electron microscopy (SEM) were used to analyze surface performance. The surface roughness of the discs in group AS was lower than those in the other groups [(0.33 ± 0.03) µm] (P < 0.05), there was no statistically significant difference (P > 0.05) among group 2SiO₂-1ZrO₂[(3.85 ± 0.38) µm], group 1SiO₂-1ZrO₂[(3.78 ± 0.56) µm] and group 1SiO₂-2ZrO₂[(4.06 ± 0.48) µm], and no difference (P > 0.05) was observed between group 1SiO₂-3ZrO₂[(1.02 ± 0.09) µm] and group 1SiO₂-4ZrO₂[(1.53 ± 0.23) µm] either. However, surface roughness in all coating groups was higher than those in group SB [(0.86 ± 0.05) µm] (P < 0.05). According to the XRD pattern, group AS and all coating groups consisted of 100% tetragonal airconia and monoclinic zirconia was detected at surface of group SB. Contents of surface silicon of coating groups increased significantly, however, no silicon was detected at sample surface of group AS and group SB. SEM showed that zirconia grains of coating exposed since part of silicon was etched by hydrofluoric acid, a three-dimensional network of intergrain nano-spaces was created. SiO₂-ZrO₂slurry coating could make surface of zirconia rough and increase Si content without creating monoclinic zirconia.
Atomic force microscopy analysis of different surface treatments of Ti dental implant surfaces

NASA Astrophysics Data System (ADS)

Bathomarco, Ti R. V.; Solorzano, G.; Elias, C. N.; Prioli, R.

2004-06-01

The surface of commercial unalloyed titanium, used in dental implants, was analyzed by atomic force microscopy. The morphology, roughness, and surface area of the samples, submitted to mechanically-induced erosion, chemical etching and a combination of both, were compared. The results show that surface treatments strongly influence the dental implant physical and chemical properties. An analysis of the length dependence of the implant surface roughness shows that, for scan sizes larger than 50 μm, the average surface roughness is independent of the scanning length and that the surface treatments lead to average surface roughness in the range of 0.37 up to 0.48 μm. It is shown that the implant surface energy is sensitive to the titanium surface area. As the area increases there is a decrease in the surface contact angle.
Modeling of surface roughness effects on glaze ice accretion

NASA Technical Reports Server (NTRS)

Hansman, R. John, Jr.; Yamaguchi, Keiko; Berkowitz, Brian M.; Potapczuk, Mark

1990-01-01

A series of experimental investigations focused on studying the cause and effect of roughness on accreting glaze ice surfaces were conducted. Detailed microvideo observations were made of glaze ice accretions on 1 to 4 inch diameter cylinders in three icing wind tunnels (the Data Products of New England six inch test facility, the NASA Lewis Icing Research Tunnel, and the B. F. Goodrich Ice Protection Research Facility). Infrared thermal video recordings were made of accreting ice surfaces in the Goodrich facility. Distinct zones of surface water behavior were observed; a smooth wet zone in the stagnation region with a uniform water film; a rough zone where surface tension effects caused coalescence of surface water into stationary beads; a horn zone where roughness elements grow into horn shapes; a runback zone where surface water ran back as rivulets; and a dry zone where rime feathers formed. The location of the transition from the smooth to the rough zone was found to migrate with time towards the stagnation point. The behavior of the transition appeared to be controlled by boundary layer transition and bead formation mechanisms at the interface between the smooth and rough zones. Regions of wet ice growth and enhanced heat transfer were clearly visible in the infrared video recordings of glaze ice surfaces. A simple multi-zone modification to the current glaze ice accretion model was proposed to include spatial variability in surface roughness.
Effect of denture cleansers on color stability, surface roughness, and hardness of different denture base resins

PubMed Central

Porwal, Anand; Khandelwal, Meenakshi; Punia, Vikas; Sharma, Vivek

2017-01-01

Aim: The purpose of this study was to evaluate the effect of different denture cleansers on the color stability, surface hardness, and roughness of different denture base resins. Materials and Methods: Three denture base resin materials (conventional heat cure resin, high impact resin, and polyamide denture base resin) were immersed for 180 days in commercially available two denture cleansers (sodium perborate and sodium hypochlorite). Color, surface roughness, and hardness were measured for each sample before and after immersion procedure. Statistical Analysis: One-way analysis of variance and Tukey's post hoc honestly significant difference test were used to evaluate color, surface roughness, and hardness data before and after immersion in denture cleanser (α =0.05). Results: All denture base resins tested exhibited a change in color, surface roughness, and hardness to some degree in both denture cleansers. Polyamides resin immersed in sodium perborate showed a maximum change in color after immersion for 180 days. Conventional heat cure resin immersed in sodium hypochlorite showed a maximum change in surface roughness and conventional heat cure immersed in sodium perborate showed a maximum change in hardness. Conclusion: Color changes of all denture base resins were within the clinically accepted range for color difference. Surface roughness change of conventional heat cure resin was not within the clinically accepted range of surface roughness. The choice of denture cleanser for different denture base resins should be based on the chemistry of resin and cleanser, denture cleanser concentration, and duration of immersion. PMID:28216847
Examination of Surface Roughness on Light Scattering by Long Ice Columns by Use of a Two-Dimensional Finite-Difference Time-Domain Algorithm

NASA Technical Reports Server (NTRS)

Sun, W.; Loeb, N. G.; Videen, G.; Fu, Q.

2004-01-01

Natural particles such as ice crystals in cirrus clouds generally are not pristine but have additional micro-roughness on their surfaces. A two-dimensional finite-difference time-domain (FDTD) program with a perfectly matched layer absorbing boundary condition is developed to calculate the effect of surface roughness on light scattering by long ice columns. When we use a spatial cell size of 1/120 incident wavelength for ice circular cylinders with size parameters of 6 and 24 at wavelengths of 0.55 and 10.8 mum, respectively, the errors in the FDTD results in the extinction, scattering, and absorption efficiencies are smaller than similar to 0.5%. The errors in the FDTD results in the asymmetry factor are smaller than similar to 0.05%. The errors in the FDTD results in the phase-matrix elements are smaller than similar to 5%. By adding a pseudorandom change as great as 10% of the radius of a cylinder, we calculate the scattering properties of randomly oriented rough-surfaced ice columns. We conclude that, although the effect of small surface roughness on light scattering is negligible, the scattering phase-matrix elements change significantly for particles with large surface roughness. The roughness on the particle surface can make the conventional phase function smooth. The most significant effect of the surface roughness is the decay of polarization of the scattered light.

Comparison of two metrological approaches for the prediction of human haptic perception

NASA Astrophysics Data System (ADS)

Neumann, Annika; Frank, Daniel; Vondenhoff, Thomas; Schmitt, Robert

2016-06-01

Haptic perception is regarded as a key component of customer appreciation and acceptance for various products. The prediction of customers’ haptic perception is of interest both during product development and production phases. This paper presents the results of a multivariate analysis between perceived roughness and texture related surface measurements, to examine whether perceived roughness can be accurately predicted using technical measurements. Studies have shown that standardized measurement parameters, such as the roughness coefficients (e.g. Rz or Ra), do not show a one-dimensional linear correlation with the human perception (of roughness). Thus, an alternative measurement method was compared to standard measurements of roughness, in regard to its capability of predicting perceived roughness through technical measurements. To estimate perceived roughness, an experimental study was conducted in which 102 subjects evaluated four sets of 12 different geometrical surface structures regarding their relative perceived roughness. The two different metrological procedures were examined in relation to their capability to predict the perceived roughness of the subjects stated within the study. The standardized measurements of the surface roughness were made using a structured light 3D-scanner. As an alternative method, surface induced vibrations were measured by a finger-like sensor during robot-controlled traverse over a surface. The presented findings provide a better understanding of the predictability of human haptic perception using technical measurements.
Radiographic evaluation of marginal bone level around implants with different neck designs after 1 year.

PubMed

Shin, Young-Kyu; Han, Chong-Hyun; Heo, Seong-Joo; Kim, Sunjai; Chun, Heoung-Jae

2006-01-01

To evaluate the influence of macro- and microstructure of the implant surface at the marginal bone level after functional loading. Sixty-eight patients were randomly assigned to 1 of 3 groups. The first group received 35 implants with a machined neck (Ankylos); the second group, 34 implants with a rough-surfaced neck (Stage 1); and the third, 38 implants with a rough-surfaced neck with microthreads (Oneplant). Clinical and radiographic examinations were conducted at baseline (implant loading) and 3, 6, and 12 months postloading. Two-way repeated analysis of variance (ANOVA) was used to test the significance of marginal bone change of each tested group at baseline, 3, 6, and 12 month follow-ups and 1-way ANOVA was also used to compare the bone loss of each time interval within the same implant group (P < .05). At 12 months, significant differences were noted in the amount of alveolar bone loss recorded for the 3 groups (P < .05). The group with the rough-surfaced microthreaded neck had a mean crestal bone loss of 0.18 +/- 0.16 mm; the group with the rough-surfaced neck, 0.76 +/- 0.21 mm; and the group with the machined neck, 1.32 +/- 0.27 mm. In the rough-surfaced group and the rough-surfaced microthreaded group, no statistically significant changes were observed after 3 months, whereas the machined-surface group showed significant bone loss for every interval (P < .05). To minimize marginal bone loss, in addition to the use of a rough surface at the marginal bone level, a macroscopic modification such as the addition of microthreads could be recommended. A rough surface and microthreads at the implant neck not only reduce crestal bone loss but also help with early biomechanical adaptation against loading in comparison to the machined neck design. A rough surface with microthreads at the implant neck was the most effective design to maintain the marginal bone level against functional loading.
The machined surface of magnesium AZ31 after rotary turning at air cooling condition

NASA Astrophysics Data System (ADS)

Akhyar, G.; Purnomo, B.; Hamni, A.; Harun, S.; Burhanuddin, Y.

2018-04-01

Magnesium is a lightweight metal that is widely used as an alternative to iron and steel. Magnesium has been applied in the automotive industry to reduce the weight of a component, but the machining process has the disadvantage that magnesium is highly flammable because it has a low flash point. High temperature can cause the cutting tool wear and contributes to the quality of the surface roughness. The purpose of this study is to obtain the value of surface roughness and implement methods of rotary cutting tool and air cooling output vortex tube cooler to minimize the surface roughness values. Machining parameters that is turning using rotary cutting tool at speed the workpiece of (Vw) 50, 120, 160 m/min, cutting speed of rotary tool of (Vt) 25, 50, 75 m/min, feed rate of (f) 0.1, 0.15, 0.2 mm/rev, and depth of cut of 0.3 mm. Type of tool used is a carbide tool diameter of 16 mm and air cooling pressure of 6 bar. The results show the average value of the lowest surface roughness on the speed the workpiece of 80 m/min, cutting speed of rotary tool of 50 m/min, feed rate of 0.2 mm/rev, and depth of cut of 0.3 mm. While the average value of the highest surface roughness on the speed the workpiece of 160 m/min, cutting speed of rotary tool of 50 m/min, feed rate of 0.2 mm/rev, and depth of cut of 0.3 mm. The influence of machining parameters concluded the higher the speed of the workpiece the surface roughness value higher. Otherwise the higher cutting speed of rotary tool then the lower the surface roughness value. The observation on the surface of the rotary tool, it was found that no uniform tool wear which causes non-uniform surface roughness. The use of rotary cutting tool contributing to lower surface roughness values generated.
Effects of surface roughness and electrokinetic heterogeneity on electroosmotic flow in microchannel

NASA Astrophysics Data System (ADS)

Masilamani, Kannan; Ganguly, Suvankar; Feichtinger, Christian; Bartuschat, Dominik; Rüde, Ulrich

2015-06-01

In this paper, a hybrid lattice-Boltzmann and finite-difference (LB-FD) model is applied to simulate the effects of three-dimensional surface roughness and electrokinetic heterogeneity on electroosmotic flow (EOF) in a microchannel. The lattice-Boltzmann (LB) method has been employed to obtain the flow field and a finite-difference (FD) method is used to solve the Poisson-Boltzmann (PB) equation for the electrostatic potential distribution. Numerical simulation of flow through a square cross-section microchannel with designed roughness is conducted and the results are critically analysed. The effects of surface heterogeneity on the electroosmotic transport are investigated for different roughness height, width, roughness interval spacing, and roughness surface potential. Numerical simulations reveal that the presence of surface roughness changes the nature of electroosmotic transport through the microchannel. It is found that the electroosmotic velocity decreases with the increase in roughness height and the velocity profile becomes asymmetric. For the same height of the roughness elements, the EOF velocity rises with the increase in roughness width. For the heterogeneously charged rough channel, the velocity profile shows a distinct deviation from the conventional plug-like flow pattern. The simulation results also indicate locally induced flow vortices which can be utilized to enhance the flow and mixing within the microchannel. The present study has important implications towards electrokinetic flow control in the microchannel, and can provide an efficient way to design a microfluidic system of practical interest.
Influence of Wire Electrical Discharge Machining (WEDM) process parameters on surface roughness

NASA Astrophysics Data System (ADS)

Yeakub Ali, Mohammad; Banu, Asfana; Abu Bakar, Mazilah

2018-01-01

In obtaining the best quality of engineering components, the quality of machined parts surface plays an important role. It improves the fatigue strength, wear resistance, and corrosion of workpiece. This paper investigates the effects of wire electrical discharge machining (WEDM) process parameters on surface roughness of stainless steel using distilled water as dielectric fluid and brass wire as tool electrode. The parameters selected are voltage open, wire speed, wire tension, voltage gap, and off time. Empirical model was developed for the estimation of surface roughness. The analysis revealed that off time has a major influence on surface roughness. The optimum machining parameters for minimum surface roughness were found to be at a 10 V open voltage, 2.84 μs off time, 12 m/min wire speed, 6.3 N wire tension, and 54.91 V voltage gap.
Osteoblast response to magnesium ion-incorporated nanoporous titanium oxide surfaces.

PubMed

Park, Jin-Woo; Kim, Youn-Jeong; Jang, Je-Hee; Song, Hwangjun

2010-11-01

This study investigated the surface characteristics and in vitro osteoconductivity of a titanium (Ti) surface incorporated with the magnesium ions (Mg) produced by hydrothermal treatment for future application as an endosseous implant surface. Mg-incorporated Ti oxide surfaces were produced by hydrothermal treatment using Mg-containing solution on two different microstructured surfaces--abraded minimally rough (Ma) or grit-blasted moderately rough (RBM) samples. The surface characteristics were evaluated using scanning electron microscopy, thin-film X-ray diffractometry, X-ray photoelectron spectroscopy, optical profilometry, and inductively coupled plasma atomic emission spectroscopy (ICP-AES). MC3T3-E1 pre-osteoblast cell attachment, proliferation, alkaline phosphatase (ALP) activity, and quantitative analysis of osteoblastic gene expression on Ma, RBM, Mg-incorporated Ma (Mg), and Mg-incorporated grit-blasted (RBM/Mg) Ti surfaces were evaluated. Hydrothermal treatment produced an Mg-incorporated Ti oxide layer with nanoporous surface structures. Mg-incorporated surfaces showed surface morphologies and surface roughness values almost identical to those of untreated smooth or micro-rough surfaces at the micron scale. ICP-AES analysis showed Mg ions released from treated surfaces into the solution. Mg incorporation significantly increased cellular attachment (P=0 at 0.5 h, P=0.01 at 1 h) on smooth surfaces, but no differences were found on micro-rough surfaces. Mg incorporation further increased ALP activity in cells grown on both smooth and micro-rough surfaces at 7 and 14 days of culture (P=0). Real-time polymerase chain reaction analysis showed higher mRNA expressions of the osteoblast transcription factor gene (Dlx5), various integrins, and the osteoblast phenotype genes (ALP, bone sialoprotein and osteocalcin) in cells grown on micro-rough (RBM) and Mg-incorporated (Mg and RBM/Mg) surfaces than those on Ma surfaces. Mg incorporation further increased the mRNA expressions of key osteoblast genes and integrins (α1, α2, α5, and β1) in cells grown on both the smooth and the micro-rough surfaces. These results indicate that an Mg-incorporated nanoporous Ti oxide surface produced by hydrothermal treatment may improve implant bone healing by enhancing the attachment and differentiation of osteoblastic cells. © 2010 John Wiley & Sons A/S.
Factors Affecting Optimal Surface Roughness of AISI 4140 Steel in Turning Operation Using Taguchi Experiment

NASA Astrophysics Data System (ADS)

Novareza, O.; Sulistiyarini, D. H.; Wiradmoko, R.

2018-02-01

This paper presents the result of using Taguchi method in turning process of medium carbon steel of AISI 4140. The primary concern is to find the optimal surface roughness after turning process. The taguchi method is used to get a combination of factors and factor levels in order to get the optimum surface roughness level. Four important factors with three levels were used in experiment based on Taguchi method. A number of 27 experiments were carried out during the research and analysed using analysis of variance (ANOVA) method. The result of surface finish was determined in Ra type surface roughness. The depth of cut was found to be the most important factors for reducing the surface roughness of AISI 4140 steel. On the contrary, the other important factors i.e. spindle speed and rake side angle of the tool were proven to be less factors that affecting the surface finish. It is interesting to see the effect of coolant composition that gained the second important factors to reduce the roughness. It may need further research to explain this result.
Ion radiation albedo effect: influence of surface roughness on ion implantation and sputtering of materials

NASA Astrophysics Data System (ADS)

Li, Yonggang; Yang, Yang; Short, Michael P.; Ding, Zejun; Zeng, Zhi; Li, Ju

2017-01-01

In fusion devices, ion retention and sputtering of materials are major concerns in the selection of compatible plasma-facing materials (PFMs), especially in the context of their microstructural conditions and surface morphologies. We demonstrate how surface roughness changes ion implantation and sputtering of materials under energetic ion irradiation. Using a new, sophisticated 3D Monte Carlo (MC) code, IM3D, and a random rough surface model, ion implantation and the sputtering yields of tungsten (W) with a surface roughness varying between 0-2 µm have been studied for irradiation by 0.1-1 keV D+, He+ and Ar+ ions. It is found that both ion backscattering and sputtering yields decrease with increasing roughness; this is hereafter called the ion radiation albedo effect. This effect is mainly dominated by the direct, line-of-sight deposition of a fraction of emitted atoms onto neighboring asperities. Backscattering and sputtering increase with more oblique irradiation angles. We propose a simple analytical formula to relate rough-surface and smooth-surface results.
Simple model of surface roughness for binary collision sputtering simulations

NASA Astrophysics Data System (ADS)

Lindsey, Sloan J.; Hobler, Gerhard; Maciążek, Dawid; Postawa, Zbigniew

2017-02-01

It has been shown that surface roughness can strongly influence the sputtering yield - especially at glancing incidence angles where the inclusion of surface roughness leads to an increase in sputtering yields. In this work, we propose a simple one-parameter model (the "density gradient model") which imitates surface roughness effects. In the model, the target's atomic density is assumed to vary linearly between the actual material density and zero. The layer width is the sole model parameter. The model has been implemented in the binary collision simulator IMSIL and has been evaluated against various geometric surface models for 5 keV Ga ions impinging an amorphous Si target. To aid the construction of a realistic rough surface topography, we have performed MD simulations of sequential 5 keV Ga impacts on an initially crystalline Si target. We show that our new model effectively reproduces the sputtering yield, with only minor variations in the energy and angular distributions of sputtered particles. The success of the density gradient model is attributed to a reduction of the reflection coefficient - leading to increased sputtering yields, similar in effect to surface roughness.
Effects of soil surface roughness on interrill erosion processes and sediment particle size distribution

USDA-ARS?s Scientific Manuscript database

Soil surface roughness significantly impacts runoff and erosion under rainfall. Few previous studies on runoff generation focused on the effects of soil surface roughness on the sediment particle size distribution (PSD), which greatly affects interrill erosion and sedimentation processes. To address...
Lithological and textural controls on radar and diurnal thermal signatures of weathered volcanic deposits, Lunar Crater region, Nevada

NASA Technical Reports Server (NTRS)

Plaut, Jeffrey J.; Rivard, Benoit

1992-01-01

Radar backscatter intensity as measured by calibrated synthetic aperture radar (SAR) systems is primarily controlled by three factors: local incidence angle, wavelength-scale roughness, and dielectric permittivity of surface materials. Radar observations may be of limited use for geological investigations of surface composition, unless the relationships between lithology and the above characteristics can be adequately understood. In arid terrains, such as the Southwest U.S., weathering signatures (e.g. soil development, fracturing, debris grain size and shape, and hill slope characteristics) are controlled to some extent by lithologic characteristics of the parent bedrock. These textural features of outcrops and their associated debris will affect radar backscatter to varying degrees, and the multiple-wavelength capability of the JPL Airborne SAR (AIRSAR) system allows sampling of textures at three distinct scales. Diurnal temperature excursions of geologic surfaces are controlled primarily by the thermal inertia of surface materials, which is a measure of the resistance of a material to a change in temperature. Other influences include albedo, surface slopes affecting insolation, local meteorological conditions and surface emissivity at the relevant thermal wavelengths. To first order, thermal inertia variations on arid terrain surfaces result from grain size distribution and porosity differences, at scales ranging from micrometers to tens of meters. Diurnal thermal emission observations, such as those made by the JPL Thermal Infrared Multispectral Scanner (TIMS) airborne instrument, are thus influenced by geometric surface characteristics at scales comparable to those controlling radar backscatter. A preliminary report on a project involving a combination of field, laboratory and remote sensing observations of weathered felsic-to basaltic volcanic rock units exposed in the southern part of the Lunar Crater Volcanic Field, in the Pancake Range of central Nevada is presented. Focus is on the relationship of radar backscatter cross sections at multiple wavelengths, apparent diurnal temperature excursions identified in multi-temporal TIMS images, surface geometries related to weathering style, and parent bedrock lithology.
Roughness based perceptual analysis towards digital skin imaging system with haptic feedback.

PubMed

Kim, K

2016-08-01

To examine psoriasis or atopic eczema, analyzing skin roughness by palpation is essential to precisely diagnose skin diseases. However, optical sensor based skin imaging systems do not allow dermatologists to touch skin images. To solve the problem, a new haptic rendering technology that can accurately display skin roughness must be developed. In addition, the rendering algorithm must be able to filter spatial noises created during 2D to 3D image conversion without losing the original roughness on the skin image. In this study, a perceptual way to design a noise filter that will remove spatial noises and in the meantime recover maximized roughness is introduced by understanding human sensitivity on surface roughness. A visuohaptic rendering system that can provide a user with seeing and touching digital skin surface roughness has been developed including a geometric roughness estimation method from a meshed surface. In following, a psychophysical experiment was designed and conducted with 12 human subjects to measure human perception with the developed visual and haptic interfaces to examine surface roughness. From the psychophysical experiment, it was found that touch is more sensitive at lower surface roughness, and vice versa. Human perception with both senses, vision and touch, becomes less sensitive to surface distortions as roughness increases. When interact with both channels, visual and haptic interfaces, the performance to detect abnormalities on roughness is greatly improved by sensory integration with the developed visuohaptic rendering system. The result can be used as a guideline to design a noise filter that can perceptually remove spatial noises while recover maximized roughness values from a digital skin image obtained by optical sensors. In addition, the result also confirms that the developed visuohaptic rendering system can help dermatologists or skin care professionals examine skin conditions by using vision and touch at the same time. © 2015 John Wiley & Sons A/S. Published by John Wiley & Sons Ltd.
Effect of sealer coating and storage methods on the surface roughness of soft liners.

PubMed

Usta Kutlu, Ilknur; Yanikoğlu, Nuran Dinckal; Kul, Esra; Duymuş, Zeynep Yesïl; Sağsöz, Nurdan Polat

2016-03-01

A soft lining is applied under a removable prosthesis for various reasons. The porosity of the lining material may increase colonization by microorganisms and cause tissue inflammation. The purpose of this in vitro study was to evaluate the effect of sealer coating on the surface roughness of soft lining materials under 4 different conditions. A total of 125 specimens were prepared. One high-temperature silicone-based soft lining material and 2 room-temperature-polymerized soft lining materials (1 silicone-based and 1 methacrylate-based) were used. Twenty-five specimens of each room-temperature soft lining material were coated with 2 layers of surface sealer. Additionally, 5 specimens of each material were stored in either distilled water, Coca-Cola, denture cleanser, saliva, or air. The surface roughness was measured at baseline and after 1, 7, 14, and 28 days. Surface roughness values were analyzed with repeated measures analysis of variance, and the Bonferroni multiple comparison test was performed using time-dependent groups and storage methods. In the time-dependent groups, methacrylate-based sealer-coated soft liners exhibited a significant increase in roughness (1.74-2.09 μm, P<.001), and silicone-based sealer-coated soft liners exhibited a decrease in roughness, but it was not significant (2.16-2.02 μm, P>.05). Therefore, the sealer coating was not effective in reducing surface roughness. Among the time-dependent storage methods, the denture cleanser exhibited an almost significant increase in roughness (1.83-1.99 μm, P=.054). Coca-Cola and artificial saliva did not show a significant difference (P>.05). However, a significant decrease in roughness was found with distilled water (P=.02) and air (P<.001). Statistically significant differences in surface roughness were found among the different types of soft liners. The sealer coating had no significant effect, and denture cleanser slightly increased the surface roughness. Contrary to expectations, the roughness did not increase in all groups over time. Copyright © 2016 Editorial Council for the Journal of Prosthetic Dentistry. Published by Elsevier Inc. All rights reserved.
[Modeling and Simulation of Spectral Polarimetric BRDF].

PubMed

Ling, Jin-jiang; Li, Gang; Zhang, Ren-bin; Tang, Qian; Ye, Qiu

2016-01-01

Under the conditions of the polarized light, The reflective surface of the object is affected by many factors, refractive index, surface roughness, and so the angle of incidence. For the rough surface in the different wavelengths of light exhibit different reflection characteristics of polarization, a spectral polarimetric BRDF based on Kirchhof theory is proposee. The spectral model of complex refraction index is combined with refraction index and extinction coefficient spectral model which were got by using the known complex refraction index at different value. Then get the spectral model of surface roughness derived from the classical surface roughness measuring method combined with the Fresnel reflection function. Take the spectral model of refraction index and roughness into the BRDF model, then the spectral polarimetirc BRDF model is proposed. Compare the simulation results of the refractive index varies with wavelength, roughness is constant, the refraction index and roughness both vary with wavelength and origin model with other papers, it shows that, the spectral polarimetric BRDF model can show the polarization characteristics of the surface accurately, and can provide a reliable basis for the application of polarization remote sensing, and other aspects of the classification of substances.
Eggshell structure in Caiman latirostris eggs improves embryo survival during nest inundation.

PubMed

Cedillo-Leal, César; Simoncini, Melina S; Leiva, Pamela M L; Larriera, Alejandro; Lang, Jeffrey W; Piña, Carlos I

2017-05-17

Egg inundation often results in poor hatching success in crocodylians. However, how tolerant eggs are to submergence, and/or how eggshell ultrastructure may affect embryo survival when inundated, are not well understood. In this study, our objective was to determine if embryo survival in Caiman latirostris is affected by eggshell surface roughness, when eggs are submerged under water. Tolerance to inundation was tested early (day 30) versus late (day 60) in development, using eight clutches (four per time treatments), subdivided into four groups: ( N = 9 per clutch per treatment; 9 × 4 = 36 eggs per group). 'Rough' eggshell represented the natural, unmodified eggshell surface structure. 'Smooth' eggshell surface structure was created by mechanically sanding the natural rough surface to remove surface columnar elements and secondary layer features, e.g. irregularities that result in 'roughness'. When inundated by submerging eggs under water for 10 h at day 30, 'smooth' eggshell structure resulted in more than twice as many dead embryos (16 versus 6, smooth versus rough; N = 36), and fewer than half as many healthy embryos (6 versus 13, smooth versus rough, respectively; N = 36). By contrast, at day 60, inundation resulted in very low hatching success, regardless of eggshell surface structure. Only two hatchlings survived the inundation, notably in the untreated group with intact, rough eggshells. Inundation produced a high rate of malformations (58% at day 30), but did not affect hatchling size. Our results indicate that eggshell roughness enhances embryo survival when eggs are inundated early in development, but not late in development. Apparently, the natural surface 'roughness' entraps air bubbles at the eggshell surface during inundation, thereby facilitating gas exchange through the eggshell even when the egg is submerged under water. © 2017 The Author(s).
Development of the Navy’s Next-Generation Nonhydrostatic Modeling System

DTIC Science & Technology

2013-09-30

e.g. surface roughness, land- sea mask, surface albedo ) are needed by physical parameterizations. The surface values will be read and interpolated...characteristics (e.g. albedo , surface roughness) is now available to the model during the initialization stage. We have added infrastructure to the...six faces (Fig 3). 4 Figure 3: Topography (top left, in meters), surface roughness (top right, in meters), albedo (bottom left, no units
Gloss measurements and rugometric inspection in dental biomaterials

NASA Astrophysics Data System (ADS)

Fernández-Oliveras, Alicia; Costa, Manuel F. M.; Yebra, Ana; Rubiño, Manuel; Pérez, María. M.

2013-11-01

In dental applications, optimizing appearance is desirable and increasingly demanded by patients. The specular gloss is among the major appearance properties of dental biomaterials, and its relationship with surface roughness has been reported. Roughness and gloss are key surface aspects that complement each other. We have experimentally analyzed the specular gloss and surface roughness of two different types of dental-resin composites and pre-sintered and sintered zirconia ceramics. We have studied two shades of both composite types and two sintered zirconia ceramics: colored and uncolored. Moreover, a surface treatment was applied to one specimen of each dental resin. Gloss measurements were performed with a standardized reflectometer and the corresponding gloss percentages were calculated. All the samples were submitted to rugometric non-invasive inspection with the MICROTOP.06.MFC laser microtopographer in order to determine meaningful statistical parameters such as the average roughness (Ra) and the root-mean-square deviation (Rq). For a comparison of the different biomaterials, the uncertainties associated to the measure of the surface gloss and roughness were also determined. The differences between the two shades of both kinds of composites proved significant in the case of the roughness parameters but not for the specular gloss. The surface treatment applied to the dental-resin composites increased the average roughness but the changes in the specular gloss were significant only for the A2 enamel nano-composite. For the zirconia ceramic the sintered process resulted in an increase in the surface roughness with a decrease of the specular gloss, corroborating that the relationship between the gloss and the roughness shows the expected behavior.
Surface Roughness and Gloss of Actual Composites as Polished With Different Polishing Systems.

PubMed

Rodrigues-Junior, S A; Chemin, P; Piaia, P P; Ferracane, J L

2015-01-01

This in vitro study evaluated the effect of polishing with different polishing systems on the surface roughness and gloss of commercial composites. One hundred disk-shaped specimens (10 mm in diameter × 2 mm thick) were made with Filtek P-90, Filtek Z350 XT, Opallis, and Grandio. The specimens were manually finished with #400 sandpaper and polished by a single operator using three multistep systems (Superfix, Diamond Pro, and Sof-lex), one two-step system (Polidores DFL), and one one-step system (Enhance), following the manufacturer's instructions. The average surface roughness (μm) was measured with a surface profilometer (TR 200 Surface Roughness Tester), and gloss was measured using a small-area glossmeter (Novo-Curve, Rhopoint Instrumentation, East Sussex, UK). Data were analyzed by two-way analysis of variance and Tukey's test (α=0.05). Statistically significant differences in surface roughness were identified by varying the polishing systems (p<0.0001) and by the interaction between polishing system and composite (p<0.0001). Pairwise comparisons revealed higher surface roughness for Grandio when polished with Sof-Lex and Filtek Z250 and Opallis when polished with Enhance. Gloss was influenced by the composites (p<0.0001), the polishing systems (p<0.0001), and the interaction between them (p<0.0001). The one-step system, Enhance, produced the lowest gloss for all composites. Surface roughness and gloss were affected by composites and polishing systems. The interaction between both also influenced these surface characteristics, meaning that a single polishing system will not behave similarly for all composites. The multistep systems produced higher gloss, while the one-step system produced the highest surface roughness and the lowest gloss of all.
Analysis of composite/difference field scattering properties between a slightly rough optical surface and multi-body defects.

PubMed

Gong, Lei; Wu, Zhensen; Gao, Ming; Qu, Tan

2018-03-20

The effective extraction of optical surface roughness and defect characteristic provide important realistic values to improve optical system efficiency. Based on finite difference time domain/multi-resolution time domain (FDTD/MRTD) mixed approach, composite scattering between a slightly rough optical surface and multi-body defect particles with different positions is investigated. The scattering contribution of defect particles or the slightly rough optical surface is presented. Our study provides a theoretical and technological basis for the nondestructive examination and optical performance design of nanometer structures.
Electron Scattering at Surfaces of Epitaxial Metal Layers

NASA Astrophysics Data System (ADS)

Chawla, Jasmeet Singh

In the field of electron transport in metal films and wires, the 'size effect' refers to the increase in the resistivity of the films and wires as their critical dimensions (thickness of film, width and height of wires) approach or become less than the electron mean free path lambda, which is, for example, 39 nm for bulk copper at room temperature. This size-effect is currently of great concern to the semiconductor industry because the continued downscaling of feature sizes has already lead to Cu interconnect wires in this size effect regime, with a reported 2.5 times higher resistivity for 40 nm wide Cu wires than for bulk Cu. Silver is a possible alternate material for interconnect wires and titanium nitride is proposed as a gate metal in novel field-effect-transistors. Therefore, it is important to develop an understanding of how the growth, the surface morphology, and the microstructure of ultrathin (few nanometers) Cu, Ag and TiN layers affect their electrical properties. This dissertation aims to advance the scientific knowledge of electron scattering at surfaces (external surfaces and grain boundaries), that are, the primary reasons for the size-effect in metal conductors. The effect of surface and grain boundary scattering on the resistivity of Cu thin films and nanowires is separately quantified using (i) in situ transport measurements on single-crystal, atomically smooth Cu(001) layers, (ii) textured polycrystalline Cu(111) layers and patterned wires with independently varying grain size, thickness and line width, and (iii) in situ grown interfaces including Cu-Ta, Cu-MgO, Cu-vacuum and Cu-oxygen. In addition, the electron surface scattering is also measured in situ for single-crystal Ag(001), (111) twinned epitaxial Ag(001), and single-crystal TiN(001) layers. Cu(001), Ag(001), and TiN(001) layers with a minimum continuous thickness of 4, 3.5 and 1.8 nm, respectively, are grown by ultra-high vacuum magnetron sputter deposition on MgO(001) substrates with and without thin epitaxial TiN(001) wetting layers and are studied for structure, crystalline quality, surface morphology, density and composition by a combination of x-ray diffraction theta-2theta scans, o-rocking curves, pole figures, reciprocal space mapping, Rutherford backscattering, x-ray reflectometry and transmission electron microscopy. The TiN(001) surface suppresses Cu and Ag dewetting, yielding lower defect density, no twinning, and smaller surface roughness than if grown on MgO(001). Textured polycrystalline Cu(111) layers 25-50-nm-thick are deposited on a stack of 7.5-nm-Ta on SiO2/Si(001), and subsequent in situ annealing at 350°C followed by sputter etching in Ar plasma yields Cu layers with independently variable thickness and grain size. Cu nanowires, 75 to 350 nm wide, are fabricated from Cu layers with different average grain size using a subtractive patterning process. In situ electron transport measurements at room temperature in vacuum and at 77 K in liquid nitrogen for single-crystal Cu and Ag layers is consistent with the Fuchs-Sondheimer (FS) model and indicates specular scattering at the metal-vacuum boundary with an average specularity parameter p = 0.8 and 0.6, respectively. In contrast, layers measured ex situ show diffuse surface scattering due to sub-monolayer oxidation. Also, addition of Ta atoms on Cu(001) surface perturbs the smooth interface potential and results in completely diffuse scattering at the Cu-Ta interface, and in turn, a higher resistivity of single-crystal Cu layers. In situ exposure of Cu(001) layers to O2 between 10 -3 and 105 Pa-s results in a sequential increase, decrease and increase of the electrical resistance which is attributed to specular surface scattering for clean Cu(001) and for surfaces with a complete adsorbed monolayer, but diffuse scattering at partial coverage and after chemical oxidation. Electron transport measurements for polycrystalline Cu layers and wires show a 10-15% and 7-9% decrease in resistivity, respectively, when increasing the average lateral grain size by a factor of 1.8. The maximum resistivity decrease that can be achieved by increasing the grain size of polycrystalline Cu layers with an average grain size approximately ˜2.5x the layer thickness is 20-26%.

Surface Roughness Measurement on a Wing Aircraft by Speckle Correlation

PubMed Central

Salazar, Félix; Barrientos, Alberto

2013-01-01

The study of the damage of aeronautical materials is important because it may change the microscopic surface structure profiles. The modification of geometrical surface properties can cause small instabilities and then a displacement of the boundary layer. One of the irregularities we can often find is surface roughness. Due to an increase of roughness and other effects, there may be extra momentum losses in the boundary layer and a modification in the parasite drag. In this paper we present a speckle method for measuring the surface roughness on an actual unmanned aircraft wing. The results show an inhomogeneous roughness distribution on the wing, as expected according to the anisotropic influence of the winds over the entire wing geometry. A calculation of the uncertainty of the technique is given. PMID:24013488
Surface changes of enamel after brushing with charcoal toothpaste

NASA Astrophysics Data System (ADS)

Pertiwi, U. I.; Eriwati, Y. K.; Irawan, B.

2017-08-01

The aim of this study was to determine the surface roughness changes of tooth enamel after brushing with charcoal toothpaste. Thirty specimens were brushed using distilled water (the first group), Strong® Formula toothpaste (the second group), and Charcoal® Formula toothpaste for four minutes and 40 seconds (equivalent to one month) and for 14 minutes (equivalent to three months) using a soft fleece toothbrush with a mass of 150 gr. The roughness was measured using a surface roughness tester, and the results were tested with repeated ANOVA test and one-way ANOVA. The value of the surface roughness of tooth enamel was significantly different (p<0.05) after brushing for an equivalent of one month and an equivalent of three months. Using toothpaste containing charcoal can increase the surface roughness of tooth enamel.
Surface roughness measurement on a wing aircraft by speckle correlation.

PubMed

Salazar, Félix; Barrientos, Alberto

2013-09-05

The study of the damage of aeronautical materials is important because it may change the microscopic surface structure profiles. The modification of geometrical surface properties can cause small instabilities and then a displacement of the boundary layer. One of the irregularities we can often find is surface roughness. Due to an increase of roughness and other effects, there may be extra momentum losses in the boundary layer and a modification in the parasite drag. In this paper we present a speckle method for measuring the surface roughness on an actual unmanned aircraft wing. The results show an inhomogeneous roughness distribution on the wing, as expected according to the anisotropic influence of the winds over the entire wing geometry. A calculation of the uncertainty of the technique is given.
Evaluation of Surface Roughness and Tensile Strength of Base Metal Alloys Used for Crown and Bridge on Recasting (Recycling).

PubMed

Agrawal, Amit; Hashmi, Syed W; Rao, Yogesh; Garg, Akanksha

2015-07-01

Dental casting alloys play a prominent role in the restoration of the partial dentition. Casting alloys have to survive long term in the mouth and also have the combination of structure, molecules, wear resistance and biologic compatibility. According to ADA system casting alloys were divided into three groups (wt%); high noble, Noble and predominantly base metal alloys. To evaluate the mechanical properties such as tensile strength and surface roughness of the new and recast base metal (nickel-chromium) alloys. Recasting of the base metal alloys derived from sprue and button, to make it reusable has been done. A total of 200 test specimens were fabricated using specially fabricated jig of metal and divided into two groups- 100 specimens of new alloy and 100 specimens of recast alloys, which were tested for tensile strength on universal testing machine and surface roughness on surface roughness tester. Tensile strength of new alloy showed no statistically significant difference (p-value>0.05) from recast alloy whereas new alloy had statistically significant surface roughness (Maximum and Average surface roughness) difference (p-value<0.01) as compared to recast alloy. Within the limitations of the study it is concluded that the tensile strength will not be affected by recasting of nickel-chromium alloy whereas surface roughness increases markedly.
Effect finishing and polishing procedures on the surface roughness of IPS Empress 2 ceramic.

PubMed

Boaventura, Juliana Maria Capelozza; Nishida, Rodrigo; Elossais, André Afif; Lima, Darlon Martins; Reis, José Mauricio Santos Nunes; Campos, Edson Alves; de Andrade, Marcelo Ferrarezi

2013-01-01

To evaluate the surface roughness of IPS Empress 2 ceramic when treated with different finishing/polishing protocols. Sixteen specimens of IPS Empress 2 ceramic were made from wax patterns obtained using a stainless steel split mold. The specimens were glazed (Stage 0-S0, control) and divided into two groups. The specimens in Group 1 (G1) were finished/polished with a KG Sorensen diamond point (S1), followed by KG Sorensen siliconized points (S2) and final polishing with diamond polish paste (S3). In Group 2 (G2), the specimens were finished/polished using a Shofu diamond point (S1), as well as Shofu siliconized points (S2) and final polishing was performed using Porcelize paste (S3). After glazing (S0) and following each polishing procedure (S1, S2 or S3), the surface roughness was measured using TALYSURF Series 2. The average surface roughness results were analyzed using ANOVA followed by Tukey post-hoc tests (α = 0.01) RESULTS: All of the polishing procedures yielded higher surface roughness values when compared to the control group (S0). S3 yielded lower surface roughness values when compared to S1 and S2. The proposed treatments negatively affected the surface roughness of the glazed IPS Empress 2 ceramic.
Femtosecond laser-induced surface wettability modification of polystyrene surface

NASA Astrophysics Data System (ADS)

Wang, Bing; Wang, XinCai; Zheng, HongYu; Lam, YeeCheong

2016-12-01

In this paper, we demonstrated a simple method to create either a hydrophilic or hydrophobic surface. With femtosecond laser irradiation at different laser parameters, the water contact angle (WCA) on polystyrene's surface can be modified to either 12.7° or 156.2° from its original WCA of 88.2°. With properly spaced micro-pits created, the surface became hydrophilic probably due to the spread of the water droplets into the micro-pits. While with properly spaced micro-grooves created, the surface became rough and more hydrophobic. We investigated the effect of laser parameters on WCAs and analyzed the laser-treated surface roughness, profiles and chemical bonds by surface profilometer, scanning electron microscope (SEM) and X-ray photoelectron spectroscopy (XPS). For the laser-treated surface with low roughness, the polar (such as C—O, C=O, and O—C=O bonds) and non-polar (such as C—C or C—H bonds) groups were found to be responsible for the wettability changes. While for a rough surface, the surface roughness or the surface topography structure played a more significant role in the changes of the surface WCA. The mechanisms involved in the laser surface wettability modification process were discussed.
Technological support of tool wear resistant qualities and cost saving of process of planetary grinding of flat parts

NASA Astrophysics Data System (ADS)

Ivanova, T. N.; Lyupa, D. C.; Revenko, N. F.; Berkutova, T. A.; Silivanova, O. A.

2018-03-01

A lot of factors varied in time lead to instability of the grinding process. Besides, the method of grinding influences significantly the productivity and quality of processing. In this regard a creation of processes of intensive defect-free grinding on the basis of new constructive and technology solutions represents the scientific problem which is of great importance. One of such solutions is application of planetary face grinding which allows simultaneously changing the kinematics of movement, implementing discontinuous grinding. The distinctive features of such grinding are decreasing the heat release rate in a contact zone; ensuring intermittence of the process with a solid grinding wheel; reverse grinding; cutting by different edges of an abrasive grain; stabilization of working parameters of a grinding wheel; ensuring work of a grinding wheel in a self-sharpening mode. The design of the planetary grinding tool was developed for plane surface processing for implementation of the specified distinctive features of planetary grinding. The kinematics of shaping a surface by flat face diamond grinding has been investigated; manufacturing capabilities of planetary face grinding have been revealed, and ways of improvement of quality and productivity have been offered. The algorithm and the program to define the motion path of a grain depending on the given set of grinding factors were received. Optimization of the process of face diamond grinding using the planetary grinding device has been confirmed with the developed program and techniques to choose cutting conditions of planetary grinding and characteristics of grinding wheels for processing different materials. While studying the process of planetary grinding, special attention was paid to the research how processing conditions influence microgeometry of the processed surface made of steel 4X5M (Russian State Standard (GOST)). As a result of the executed research, it was established that surface roughness parameter Ra during the processing using the planetary grinding device is 35 - 40% less than when using the tool with the solid cutting surface. This phenomenon can be accounted for more uniform work of the cutting grains of the planetary grinding tool as the number of meetings of diamond grains with the surface being processed increases. At the same time, it should be noted that during the planetary grinding more intensive smoothing of tops of microroughnesses is observed that provides the creation of steadier cutting shape. The given method of calculation of cost value of grinding operation allows solving various manufacturing problems: to compare cost value of grinding different materials, grinding wheels of different parameters; to define the optimum grinding conditions.
Validity criteria for Fermi's golden rule scattering rates applied to metallic nanowires.

PubMed

Moors, Kristof; Sorée, Bart; Magnus, Wim

2016-09-14

Fermi's golden rule underpins the investigation of mobile carriers propagating through various solids, being a standard tool to calculate their scattering rates. As such, it provides a perturbative estimate under the implicit assumption that the effect of the interaction Hamiltonian which causes the scattering events is sufficiently small. To check the validity of this assumption, we present a general framework to derive simple validity criteria in order to assess whether the scattering rates can be trusted for the system under consideration, given its statistical properties such as average size, electron density, impurity density et cetera. We derive concrete validity criteria for metallic nanowires with conduction electrons populating a single parabolic band subjected to different elastic scattering mechanisms: impurities, grain boundaries and surface roughness.
Mechanical Properties of TiTaHfNbZr High-Entropy Alloy Coatings Deposited on NiTi Shape Memory Alloy Substrates

NASA Astrophysics Data System (ADS)

Motallebzadeh, A.; Yagci, M. B.; Bedir, E.; Aksoy, C. B.; Canadinc, D.

2018-04-01

TiTaHfNbZr high-entropy alloy (HEA) thin films with thicknesses of about 750 and 1500 nm were deposited on NiTi substrates by RF magnetron sputtering using TiTaHfNbZr equimolar targets. The thorough experimental analysis on microstructure and mechanical properties of deposited films revealed that the TiTaHfNbZr films exhibited amorphous and cauliflower-like structure, where grain size and surface roughness increased concomitant with film thickness. More importantly, the current findings demonstrate that the TiTaHfNbZr HEA films with mechanical properties of the same order as those of the NiTi substrate constitute promising biomedical coatings effective in preventing Ni release.
Theory and experimental technique for nondestructive evaluation of ceramic composites

NASA Technical Reports Server (NTRS)

Generazio, Edward R.

1990-01-01

The important ultrasonic scattering mechanisms for SiC and Si3N4 ceramic composites were identified by examining the interaction of ultrasound with individual fibers, pores, and grains. The dominant scattering mechanisms were identified as asymmetric refractive scattering due to porosity gradients in the matrix material, and symmetric diffractive scattering at the fiber-to-matrix interface and at individual pores. The effect of the ultrasonic reflection coefficient and surface roughness in the ultrasonic evaluation was highlighted. A new nonintrusive ultrasonic evaluation technique, angular power spectrum scanning (APSS), was presented that is sensitive to microstructural variations in composites. Preliminary results indicate that APSS will yield information on the composite microstructure that is not available by any other nondestructive technique.
Structural and magnetic analysis of Cu, Co substituted NiFe{sub 2}O{sub 4} thin films

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sharma, Hakikat; Bala, Kanchan; Negi, N. S.

2016-05-23

In the present work we prepared NiFe{sub 2}O{sub 4}, Ni{sub 0.95}Cu{sub 0.05}Fe{sub 2}O{sub 4} and Ni{sub 0.94}Cu{sub 0.05}Co{sub 0.01} Fe{sub 2}O{sub 4} thin films by metallo-organic decomposition method (MOD) using spin coating technique. The thin films were analyzed by X-ray diffractometer (XRD) and Atomic force microscope (AFM) for structural studies. The XRD patterns confirmed the ferrite phase of thin films. From AFM, we analyzed surface morphology, calculated grain size (GS) and root mean square roughness (RMSR). Room temperature magnetic properties were investigated by vibrating sample magnetometer (VSM).
Mechanical Properties of TiTaHfNbZr High-Entropy Alloy Coatings Deposited on NiTi Shape Memory Alloy Substrates

NASA Astrophysics Data System (ADS)

Motallebzadeh, A.; Yagci, M. B.; Bedir, E.; Aksoy, C. B.; Canadinc, D.

2018-06-01

TiTaHfNbZr high-entropy alloy (HEA) thin films with thicknesses of about 750 and 1500 nm were deposited on NiTi substrates by RF magnetron sputtering using TiTaHfNbZr equimolar targets. The thorough experimental analysis on microstructure and mechanical properties of deposited films revealed that the TiTaHfNbZr films exhibited amorphous and cauliflower-like structure, where grain size and surface roughness increased concomitant with film thickness. More importantly, the current findings demonstrate that the TiTaHfNbZr HEA films with mechanical properties of the same order as those of the NiTi substrate constitute promising biomedical coatings effective in preventing Ni release.
Structural Changes and Material Transport in Al2O3-Supported Cu/Fe Spinel Particles in a Simulated Chemical Looping Combustion Environment

NASA Astrophysics Data System (ADS)

Nealley, W. H. Harrison; Nakano, Anna; Nakano, Jinichiro; Bennett, James P.

2018-05-01

Alumina-supported Cu/Fe spinel particles were exposed to oxidation/reduction atmospheres at 800°C. Structural changes of the particles subjected to gas cycles between air and 10 vol.% CO-90 vol.% Ar were studied from physical data and real-time images collected using a confocal scanning laser microscope equipped with a heating chamber. Overall particle volume slowly expanded with cycles while surface roughness decreased. Cross-sections of the exposed particles showed segregation of Cu and Fe to the edges of inner grains, which may have acted as oxygen carriers during the exposures. The particles remained whole during the cyclic exposures without any noticeable structural breakdown.
Structural, morphological and optical studies of F doped SnO2 thin films

NASA Astrophysics Data System (ADS)

Chandel, Tarun; Thakur, Vikas; Dwivedi, Shailendra Kumar; Zaman, M. Burhanuz; Rajaram, Poolla

2018-05-01

Highly conducting and transparent FTO (flourine doped tin Oxide) thin films were grown on the glass substrates using a low cost spray pyrolysis technique. The films were characterized for their structural, morphological and optical studies using XRD, SEM and UV-Vis spectroscopy. XRD studies show that the FTO films crystallize in Tetragonal cassiterite structure. Morphological analysis using SEM show that the films are uniformly covered with spherical grains albeit high in surface roughness. The average optical transmission greater than 80% in the visible region along with the appearance of interference fringes in the transmission curves confirms the high quality of the films. Electrical studies show that the films exhibit sheet resistance below 10 Ω ϒ-1.
Influence of surface roughness on the oxidation behavior of a Ni-4.0Cr-5.7Al single crystal superalloy

NASA Astrophysics Data System (ADS)

Pei, Haiqing; Wen, Zhixun; Li, Zhenwei; Zhang, Yamin; Yue, Zhufeng

2018-05-01

The high-temperature oxidation dynamics and mechanisms of a Ni-based single crystal superalloy with four kinds of surface roughnesses were investigated by virtue of XRD, OM, SEM and EDS at 1000 °C. In the initial oxidation stage, outer (Ni, Co)O was mainly produced on the surfaces of the samples with Ra = 90 nm and 19 nm. Correspondingly, outer Cr2O3 and transient θ-Al2O3 were mainly formed on the surfaces with Ra = 509 nm and 182 nm. After 180 min oxidation, the values of instantaneous parabolic mass gain coefficients (kp) of the samples with all surface roughnesses were gradually consistent with the data of the growth parabolic coefficient of α-Al2O3. The oxidation mechanisms of Ni-based superalloy with different surface roughnesses were discussed by a model. The external diffusion flux of Al (DAl) increases with the increases of surface roughness. Thus, the required Al concentration decreases with the increases of surface roughness when the selective oxidation of Al occurrs to form a protective single α-Al2O3 film.
Molecular dynamics analysis of a equilibrium nanoscale droplet on a solid surface with periodic roughness

NASA Astrophysics Data System (ADS)

Furuta, Yuma; Surblys, Donatas; Yamaguchi, Yastaka

2016-11-01

Molecular dynamics simulations of the equilibrium wetting behavior of hemi-cylindrical argon droplets on solid surfaces with a periodic roughness were carried out. The rough solid surface is located at the bottom of the calculation cell with periodic boundary conditions in surface lateral directions and mirror boundary condition at the top boundary. Similar to on a smooth surface, the change of the cosine of the droplet contact angle was linearly correlated to the potential well depth of the inter-atomic interaction between liquid and solid on a surface with a short roughness period while the correlation was deviated on one with a long roughness period. To further investigate this feature, solid-liquid, solid-vapor interfacial free energies per unit projected area of solid surface were evaluated by using the thermodynamic integration method in independent quasi-one-dimensional simulation systems with a liquid-solid interface or vapor-solid interface on various rough solid surfaces at a constant pressure. The cosine of the apparent contact angles estimated from the density profile of the droplet systems corresponded well with ones calculated from Young's equation using the interfacial energies evaluated in the quasi-one dimensional systems.
Skin friction measurements of mathematically generated roughness in the transitionally- to fully-rough regimes

NASA Astrophysics Data System (ADS)

Barros, Julio; Schultz, Michael; Flack, Karen

2016-11-01

Engineering systems are affected by surface roughness which cause an increase in drag leading to significant performance penalties. One important question is how to predict frictional drag purely based upon surface topography. Although significant progress has been made in recent years, this has proven to be challenging. The present work takes a systematic approach by generating surface roughness in which surfaces parameters, such as rms , skewness, can be controlled. Surfaces were produced using the random Fourier modes method with enforced power-law spectral slopes. The surfaces were manufactured using high resolution 3D-printing. In this study three surfaces with constant amplitude and varying slope, P, were investigated (P = - 0 . 5 , - 1 . 0 , - 1 . 5). Skin-friction measurements were conducted in a high Reynolds number turbulent channel flow facility, covering a wide range of Reynolds numbers, from hydraulic-smooth to fully-rough regimes. Results show that some long wavelength roughness scales do not contribute significantly to the frictional drag, thus highlighting the need for filtering in the calculation of surface statistics. Upon high-pass filtering, it was found that krms is highly correlated with the measured ks.
Modelling of surface roughness effects on impurity erosion and deposition in TEXTOR with a code package SURO/ERO/SDPIC

NASA Astrophysics Data System (ADS)

Dai, Shuyu; Kirschner, A.; Sun, Jizhong; Tskhakaya, D.; Wang, Dezhen

2014-12-01

The roughness-induced uneven erosion-deposition behaviour is widely observed on plasma-wetted surfaces in tokamaks. The three-dimensional (3D) angular distribution of background plasma and impurities is expected to have an impact on the local erosion-deposition characteristic on rough surfaces. The investigations of 13C deposition on rough surfaces in TEXTOR experiments have been re-visited by 3D treatment of surface morphology to evaluate the effect of 3D angular distribution and its connection with surface topography by the code package SURO/ERO/SDPIC. The simulation results show that the erosion/deposition patterns and evolution of surface topography are strongly affected by the azimuthal direction of incident flux. A reduced aspect ratio of rough surface leads to an increase in 13C deposition due to the enhanced trapping ability at surface recessions. The shadowing effect of rough surface has been revealed based on the relationship between 3D incident direction and surface topography properties. The more realistic surface structures used by 3D SURO can well reproduce the experimental results of the increase in the 13C deposition efficiency by a factor of 3-5 on a rough surface compared with a smooth one. The influence of sheath electric field on the local impact angle and resulting 13C deposition has been studied, which indicates that the difference in 13C deposition caused by sheath electric field can be alleviated by the use of more realistic surface structures. The difference in 13C deposition on smooth graphite and tungsten substrates has been specified by consideration of effects of kinetic reflection, enhanced physical sputtering and nucleation.
Comparative study on deposition of fluorine-doped tin dioxide thin films by conventional and ultrasonic spray pyrolysis methods for dye-sensitized solar modules

NASA Astrophysics Data System (ADS)

Icli, Kerem Cagatay; Kocaoglu, Bahadir Can; Ozenbas, Macit

2018-01-01

Fluorine-doped tin dioxide (FTO) thin films were produced via conventional spray pyrolysis and ultrasonic spray pyrolysis (USP) methods using alcohol-based solutions. The prepared films were compared in terms of crystal structure, morphology, surface roughness, visible light transmittance, and electronic properties. Upon investigation of the grain structures and morphologies, the films prepared using ultrasonic spray method provided relatively larger grains and due to this condition, carrier mobilities of these films exhibited slightly higher values. Dye-sensitized solar cells and 10×10 cm modules were prepared using commercially available and USP-deposited FTO/glass substrates, and solar performances were compared. It is observed that there exists no remarkable efficiency difference for both cells and modules, where module efficiency of the USP-deposited FTO glass substrates is 3.06% compared to commercial substrate giving 2.85% under identical conditions. We demonstrated that USP deposition is a low cost and versatile method of depositing commercial quality FTO thin films on large substrates employed in large area dye-sensitized solar modules or other thin film technologies.
Surface roughness and packaging tightness affect calcium lactate crystallization on Cheddar cheese.

PubMed

Rajbhandari, P; Kindstedt, P S

2014-01-01

Calcium lactate crystals that sometimes form on Cheddar cheese surfaces are a significant expense to manufacturers. Researchers have identified several postmanufacture conditions such as storage temperature and packaging tightness that contribute to crystal formation. Anecdotal reports suggest that physical characteristics at the cheese surface, such as roughness, cracks, and irregularities, may also affect crystallization. The aim of this study was to evaluate the combined effects of surface roughness and packaging tightness on crystal formation in smoked Cheddar cheese. Four 20-mm-thick cross-section slices were cut perpendicular to the long axis of a retail block (~300g) of smoked Cheddar cheese using a wire cutting device. One cut surface of each slice was lightly etched with a cheese grater to create a rough, grooved surface; the opposite cut surface was left undisturbed (smooth). The 4 slices were vacuum packaged at 1, 10, 50, and 90kPa (very tight, moderately tight, loose, very loose, respectively) and stored at 1°C. Digital images were taken at 1, 4, and 8 wk following the first appearance of crystals. The area occupied by crystals and number of discrete crystal regions (DCR) were quantified by image analysis. The experiment was conducted in triplicate. Effects of storage time, packaging tightness, surface roughness, and their interactions were evaluated by repeated-measures ANOVA. Surface roughness, packaging tightness, storage time, and their 2-way interactions significantly affected crystal area and DCR number. Extremely heavy crystallization occurred on both rough and smooth surfaces when slices were packaged loosely or very loosely and on rough surfaces with moderately tight packaging. In contrast, the combination of rough surface plus very tight packaging resulted in dramatic decreases in crystal area and DCR number. The combination of smooth surface plus very tight packaging virtually eliminated crystal formation, presumably by eliminating available sites for nucleation. Cut-and-wrap operations may significantly influence the crystallization behavior of Cheddar cheeses that are saturated with respect to calcium lactate and thus predisposed to form crystals. Copyright © 2014 American Dairy Science Association. Published by Elsevier Inc. All rights reserved.

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