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Sample records for hardened high strength

  1. Anisotropy of high temperature strength in precipitation-hardened nickel-base superalloy single crystals

    NASA Technical Reports Server (NTRS)

    Nakagawa, Y. G.; Terashima, H.; Yoshizawa, H.; Ohta, Y.; Murakami, K.

    1986-01-01

    The anisotropy of high temperature strength of nickel-base superalloy, Alloy 454, in service for advanced jet engine turbine blades and vanes, was investigated. Crystallographic orientation dependence of tensile yield strength, creep and creep rupture strength was found to be marked at about 760C. In comparison with other single crystal data, a larger allowance in high strength off-axial orientation from the 001 axis, and relatively poor strength at near the -111 axis were noted. From transmission electron microscopy the anisotropic characteristics of this alloy were explained in terms of available slip systems and stacking geometries of gamma-prime precipitate cuboids which are well hardened by a large tantalum content. 100 cube slip was considered to be primarily responsible for the poor strength of the -111 axis orientation replacing the conventional 111 plane slip systems.

  2. The development of high strength corrosion resistant precipitation hardening cast steels

    NASA Astrophysics Data System (ADS)

    Abrahams, Rachel A.

    Precipitation Hardened Cast Stainless Steels (PHCSS) are a corrosion resistant class of materials which derive their properties from secondary aging after a normalizing heat treatment step. While PHCSS materials are available in austenitic and semi-austenitic forms, the martensitic PHCSS are most widely used due to a combination of high strength, good toughness, and corrosion resistance. If higher strength levels can be achieved in these alloys, these materials can be used as a lower-cost alternative to titanium for high specific strength applications where corrosion resistance is a factor. Although wrought precipitation hardened materials have been in use and specified for more than half a century, the specification and use of PHCSS has only been recent. The effects of composition and processing on performance have received little attention in the cast steel literature. The work presented in these investigations is concerned with the experimental study and modeling of microstructural development in cast martensitic precipitation hardened steels at high strength levels. Particular attention is focused on improving the performance of the high strength CB7Cu alloy by control of detrimental secondary phases, notably delta ferrite and retained austenite, which is detrimental to strength, but potentially beneficial in terms of fracture and impact toughness. The relationship between age processing and mechanical properties is also investigated, and a new age hardening model based on simultaneous precipitation hardening and tempering has been modified for use with these steels. Because the CB7Cu system has limited strength even with improved processing, a higher strength prototype Fe-Ni-Cr-Mo-Ti system has been designed and adapted for use in casting. This prototype is expected to develop high strengths matching or exceed that of cast Ti-6Al-4V alloys. Traditional multicomponent constitution phase diagrams widely used for phase estimation in conventional stainless steels

  3. Issues associated with the use of Yoshida nonlinear isotropic/kinematic hardening material model in Advanced High Strength Steels

    NASA Astrophysics Data System (ADS)

    Shi, Ming F.; Zhang, Li; Zhu, Xinhai

    2016-08-01

    The Yoshida nonlinear isotropic/kinematic hardening material model is often selected in forming simulations where an accurate springback prediction is required. Many successful application cases in the industrial scale automotive components using advanced high strength steels (AHSS) have been reported to give better springback predictions. Several issues have been raised recently in the use of the model for higher strength AHSS including the use of two C vs. one C material parameters in the Armstrong and Frederick model (AF model), the original Yoshida model vs. Original Yoshida model with modified hardening law, and constant Young's Modulus vs. decayed Young's Modulus as a function of plastic strain. In this paper, an industrial scale automotive component using 980 MPa strength materials is selected to study the effect of two C and one C material parameters in the AF model on both forming and springback prediction using the Yoshida model with and without the modified hardening law. The effect of decayed Young's Modulus on the springback prediction for AHSS is also evaluated. In addition, the limitations of the material parameters determined from tension and compression tests without multiple cycle tests are also discussed for components undergoing several bending and unbending deformations.

  4. Double Sided Irradiation for Laser-assisted Shearing of Ultra High Strength Steels with Process Integrated Hardening

    NASA Astrophysics Data System (ADS)

    Brecher, Christian; Emonts, Michael; Eckert, Markus; Weinbach, Matthias

    Most small or medium sized parts produced in mass production are made by shearing and forming of sheet metal. This technology is cost effective, but the achievable quality and geometrical complexity are limited when working high and highest strength steel. Based on the requirements for widening the process limits of conventional sheet metal working the Fraunhofer IPT has developed the laser-assisted sheet metal working technology. With this enhancement it is possible to produce parts made of high and highest strength steel with outstanding quality, high complexity and low tool wear. Additionally laser hardening has been implemented to adjust the mechanical properties of metal parts within the process. Currently the process is limited to lower sheet thicknesses (<2 mm) to maintain short cycle times. To enable this process for larger geometries and higher sheet thicknesses the Fraunhofer IPT developed a system for double sided laser-assisted sheet metal working within progressive dies.

  5. Group precipitation and age hardening of nanostructured Fe-based alloys with ultra-high strengths

    DOE PAGES

    Jiao, Z. B.; Luan, J. H.; Miller, M. K.; Yu, C. Y.; Liu, C. T.

    2016-02-19

    The precipitation of nanoparticles plays a key role in determining the properties of many structural materials, and the understanding of their formation and stabilization mechanisms has been a long standing interest in the material field. However, the critical issues involving the group precipitation of various nanoparticles and their cooperative hardening mechanism remain elusive in the newly discovered Fe-based alloys with nanostructures. Here we quantitatively elucidate the nucleation mechanism, evolution kinetics and hardening effects of the group-precipitated nanoparticles in the Fe-Cu-Ni-Al-based alloys by atom probe tomography together with both first-principles and thermodynamic calculations. Our results provide the compelling evidence for twomore » interesting but complex group precipitation pathways of nanoparticles, i.e., the Cu-rich and NiAl-based precipitations. Lastly, the co-existence of the two precipitation pathways plays a key role in age hardening kinetics and ultimately enhances the hardening response, as compared to the single particle type of strengthening, therefore providing an effective new approach for strengthening materials for structural applications.« less

  6. Group precipitation and age hardening of nanostructured Fe-based alloys with ultra-high strengths.

    PubMed

    Jiao, Z B; Luan, J H; Miller, M K; Yu, C Y; Liu, C T

    2016-02-19

    The precipitation of nanoparticles plays a key role in determining the properties of many structural materials, and the understanding of their formation and stabilization mechanisms has been a long standing interest in the material field. However, the critical issues involving the group precipitation of various nanoparticles and their cooperative hardening mechanism remain elusive in the newly discovered Fe-based alloys with nanostructures. Here we quantitatively elucidate the nucleation mechanism, evolution kinetics and hardening effects of the group-precipitated nanoparticles in the Fe-Cu-Ni-Al-based alloys by atom probe tomography together with both first-principles and thermodynamic calculations. Our results provide the compelling evidence for two interesting but complex group precipitation pathways of nanoparticles, i.e., the Cu-rich and NiAl-based precipitations. The co-existence of the two precipitation pathways plays a key role in age hardening kinetics and ultimately enhances the hardening response, as compared to the single particle type of strengthening, therefore providing an effective new approach for strengthening materials for structural applications.

  7. Group precipitation and age hardening of nanostructured Fe-based alloys with ultra-high strengths

    NASA Astrophysics Data System (ADS)

    Jiao, Z. B.; Luan, J. H.; Miller, M. K.; Yu, C. Y.; Liu, C. T.

    2016-02-01

    The precipitation of nanoparticles plays a key role in determining the properties of many structural materials, and the understanding of their formation and stabilization mechanisms has been a long standing interest in the material field. However, the critical issues involving the group precipitation of various nanoparticles and their cooperative hardening mechanism remain elusive in the newly discovered Fe-based alloys with nanostructures. Here we quantitatively elucidate the nucleation mechanism, evolution kinetics and hardening effects of the group-precipitated nanoparticles in the Fe-Cu-Ni-Al-based alloys by atom probe tomography together with both first-principles and thermodynamic calculations. Our results provide the compelling evidence for two interesting but complex group precipitation pathways of nanoparticles, i.e., the Cu-rich and NiAl-based precipitations. The co-existence of the two precipitation pathways plays a key role in age hardening kinetics and ultimately enhances the hardening response, as compared to the single particle type of strengthening, therefore providing an effective new approach for strengthening materials for structural applications.

  8. Group precipitation and age hardening of nanostructured Fe-based alloys with ultra-high strengths

    PubMed Central

    Jiao, Z. B.; Luan, J. H.; Miller, M. K.; Yu, C. Y.; Liu, C. T.

    2016-01-01

    The precipitation of nanoparticles plays a key role in determining the properties of many structural materials, and the understanding of their formation and stabilization mechanisms has been a long standing interest in the material field. However, the critical issues involving the group precipitation of various nanoparticles and their cooperative hardening mechanism remain elusive in the newly discovered Fe-based alloys with nanostructures. Here we quantitatively elucidate the nucleation mechanism, evolution kinetics and hardening effects of the group-precipitated nanoparticles in the Fe-Cu-Ni-Al-based alloys by atom probe tomography together with both first-principles and thermodynamic calculations. Our results provide the compelling evidence for two interesting but complex group precipitation pathways of nanoparticles, i.e., the Cu-rich and NiAl-based precipitations. The co-existence of the two precipitation pathways plays a key role in age hardening kinetics and ultimately enhances the hardening response, as compared to the single particle type of strengthening, therefore providing an effective new approach for strengthening materials for structural applications. PMID:26892834

  9. Conservation Research and Development/ New Ultra-Low Carbon High Strength Steels with Improved Bake Hardenability for Enhanced Stretch Formability and Dent Resistance

    SciTech Connect

    Anthony J. DeArdo; C. Isaac Garcia

    2003-12-15

    Conservation Research and Development/New Ultra-Low Carbon High Strength Steels with Improved Bake Hardenability for Enhanced Stretch Formability and Dent Resistance. The experimental work can be divided into four phases. In each phase, the materials were received or designed, processed and tested, to evaluate the BH increment or response, as a function of compositions and processing conditions. Microstructural characterization by various techniques was performed in order to gain insights into the mechanisms of flow stress increment by bake hardening.

  10. Intergranular cracking in high-strength, cold-rolled, and precipitation-hardened austenitic stainless steel UNS S35500

    SciTech Connect

    Pednekar, S.P.; Champagne, V.K.; Pepi, M.S.; Grendahl, S.

    1999-11-01

    When quench annealed, stainless steel UNS35500 (C 0.12, Cr 15.5, Ni 4.5, Mo 3, N O.1%) is austenitic and soft. In cold-rolled-and-tempered condition heavy cold rolling followed by precipitation hardening considerably strengthens the material (UTS 220 ksi (1517 MPa), elongation 10%). Its strength combined with good corrosion resistance make the material attractive for use in critical load-bearing applications. In one application, rotor blades of a helicopter are attached to the drive shaft with a component, strap pack, assembled from 0.014 inch (O.36 mm) thick material. Premature fatigue failures of strap packs have occurred starting from intergranular cracks in single laminae. Chloride salts were detected at crack origins. This intergranular stress corrosion cracking was reproduced under crevices in slow strain rate tests conducted in 3.5% NaCl solution at 0.1 V (Ag/AgCl 4M Kcl). The potential is typical of those attained by the material under thin, chloride-bearing condensate films exposed to air. Cracking did not occur when crevices were absent. Electrolytic polishing in chloride-free acids combined with a standard overpassivation treatment in nitric acid improved the resistance to crevice corrosion. This treatment slowed, but did not prevent, the onset of stress corrosion cracking (SCC) in slow strain rate tests conducted with an artificial crevice on the specimen surface.

  11. Multiscale Modeling of Inclusions and Precipitation Hardening in Metal Matrix Composites: Application to Advanced High-Strength Steels

    SciTech Connect

    Askari, Hesam A.; Zbib, Hussein M.; Sun, Xin

    2013-06-30

    In this study, the strengthening effect of inclusions and precipitates in metals is investigated within a multiscale approach that utilizes models at various length scales, namely, Molecular Mechanics (MM), discrete Dislocation Dynamics (DD), and an Eigenstrain Inclusion Method (EIM). Particularly, precipitates are modeled as hardsoft particles whose stress fields interact with dislocations. The stress field resulting from the elastic mismatch between the particles and the matrix is accounted for through the EIM. While the MM method is employed for the purpose of developing rules for DD for short range interaction between a single dislocation and an inclusion, the DD method is used to predict the strength of the composite resulting from the interaction between ensembles of dislocations and particles. As an application to this method, the mechanical behavior of Advanced High Strength Steel (AHSS) is investigated and the results are then compared to the experimental data. The results show that the finely dispersive precipitates can strengthen the material by pinning the dislocations up to a certain shear stress and retarding the recovery, as well as annihilation of dislocations. The DD results show that strengthening due to nano sized particles is a function of the density and size of the precipitates. This size effect is then explained using a mechanistic model developed based on dislocation-particle interaction.

  12. Method for increasing the rate of compressive strength gain in hardenable mixtures containing fly ash

    DOEpatents

    Liskowitz, J.W.; Wecharatana, M.; Jaturapitakkul, C.; Cerkanowicz, A.E.

    1997-10-28

    The present invention relates to concrete, mortar and other hardenable mixtures comprising cement and fly ash for use in construction. The invention provides a method for increasing the rate of strength gain of a hardenable mixture containing fly ash by exposing the fly ash to an aqueous slurry of calcium oxide (lime) prior to its incorporation into the hardenable mixture. The invention further relates to such hardenable mixtures, e.g., concrete and mortar, that contain fly ash pre-reacted with calcium oxide. In particular, the fly ash is added to a slurry of calcium oxide in water, prior to incorporating the fly ash in a hardenable mixture. The hardenable mixture may be concrete or mortar. In a specific embodiment, mortar containing fly ash treated by exposure to an aqueous lime slurry are prepared and tested for compressive strength at early time points. 2 figs.

  13. Method for increasing the rate of compressive strength gain in hardenable mixtures containing fly ash

    DOEpatents

    Liskowitz, John W.; Wecharatana, Methi; Jaturapitakkul, Chai; Cerkanowicz, deceased, Anthony E.

    1997-01-01

    The present invention relates to concrete, mortar and other hardenable mixtures comprising cement and fly ash for use in construction. The invention provides a method for increasing the rate of strength gain of a hardenable mixture containing fly ash by exposing the fly ash to an aqueous slurry of calcium oxide (lime) prior to its incorporation into the hardenable mixture. The invention further relates to such hardenable mixtures, e.g., concrete and mortar, that contain fly ash pre-reacted with calcium oxide. In particular, the fly ash is added to a slurry of calcium oxide in water, prior to incorporating the fly ash in a hardenable mixture. The hardenable mixture may be concrete or mortar. In a specific embodiment, mortar containing fly ash treated by exposure to an aqueous lime slurry are prepared and tested for compressive strength at early time points.

  14. Hardening and welding with high-power diode lasers

    NASA Astrophysics Data System (ADS)

    Ehlers, Bodo; Herfurth, Hans-Joachim; Heinemann, Stefan

    2000-03-01

    Commercially available high power diode lasers (HPDLs) with output powers of up to 6 kW have been recognized as an interesting tool for industrial applications. In certain fields of application they offer many advantages over Nd:YAG and CO2 lasers because of their low maintenance, compact design and low capital costs. Examples of successful industrial implementation of HPDLs include plastic welding, surface hardening and heat conduction welding of stainless steel and aluminum. The joining of plastics with an HPDL offers the advantages of producing a weld seam with high strength, high consistency and superior appearance. One example is the keyless entry system introduced with the Mercedes E-class where the microelectronic circuits are embedded in a plastic housing. Other applications include instrument panels, cell phones, headlights and tail lights. Applications in the field of surface treatment of metals profit from the HPDL's inherent line-shaped focus and the homogeneous intensity distribution across this focus. An HPDL system is used within the industry to harden rails for coordinate measurement machines. This system contains a customized zoom optic to focus the laser light onto the rails. With the addition of a temperature control, even complex shapes can be hardened with a constant depth and minimum distortion.

  15. Comparative Structural Strength Research of Hardened Carbon Steel and Hot-Rolled Alloy Steel

    NASA Astrophysics Data System (ADS)

    Bogomolov, A. V.; Zhakupov, A. N.; Kanayev, A. T.; Sikach, I. A.; Tugumov, K. K.

    2016-08-01

    Experiments on quantitative evaluation of fatigue strength showed that St5ps and St5sp carbon steels with A400 strength class can be fully applied for erection of constructions and buildings having cyclical loads during operation. Study of corrosion resistance of hardened carbon steel in comparison with hot-rolled alloy steel consists in difference in structures and hence, difference in intensity of electric and chemical processes featuring presence of steel in concrete. Structure of St5sp steel with A400 strength class in surface area has significantly less corrosion rate than ferritic-perlitic structure of 35GS steel with A400 strength class.

  16. YIELD STRENGTH PREDICTION FOR RAPID AGE-HARDENING HEAT TREATMENT OF ALUMINUM ALLOYS

    SciTech Connect

    Yin, Hebi; Sabau, Adrian S; Ludtka, Gerard Michael; Skszek, Timothy; Niu, X

    2013-01-01

    A constitutive model has been developed to predict the yield strength aging curves for aluminum casting alloys during non-isothermal age-hardening processes. The model provides the specific relationship between the process variables and yield strength. Several aging heat treatment scenarios have been investigated using the proposed model, including two-step aging recipes. Two-step aging heat treatments involve a low temperature regime to promote nucleation of secondary phases and a second step at higher temperature for the growth of the secondary phases. The predicted results show that yield strength of approximately 300MPa might be obtained in shorter aging time, of approximately 30 minutes. Thus, better mechanical properties can be obtained by optimizing the time-temperature schedules for the precipitation hardening process of heat treatable aluminum alloys.

  17. High-Performance, Radiation-Hardened Electronics for Space Environments

    NASA Technical Reports Server (NTRS)

    Keys, Andrew S.; Watson, Michael D.; Frazier, Donald O.; Adams, James H.; Johnson, Michael A.; Kolawa, Elizabeth A.

    2007-01-01

    The Radiation Hardened Electronics for Space Environments (RHESE) project endeavors to advance the current state-of-the-art in high-performance, radiation-hardened electronics and processors, ensuring successful performance of space systems required to operate within extreme radiation and temperature environments. Because RHESE is a project within the Exploration Technology Development Program (ETDP), RHESE's primary customers will be the human and robotic missions being developed by NASA's Exploration Systems Mission Directorate (ESMD) in partial fulfillment of the Vision for Space Exploration. Benefits are also anticipated for NASA's science missions to planetary and deep-space destinations. As a technology development effort, RHESE provides a broad-scoped, full spectrum of approaches to environmentally harden space electronics, including new materials, advanced design processes, reconfigurable hardware techniques, and software modeling of the radiation environment. The RHESE sub-project tasks are: SelfReconfigurable Electronics for Extreme Environments, Radiation Effects Predictive Modeling, Radiation Hardened Memory, Single Event Effects (SEE) Immune Reconfigurable Field Programmable Gate Array (FPGA) (SIRF), Radiation Hardening by Software, Radiation Hardened High Performance Processors (HPP), Reconfigurable Computing, Low Temperature Tolerant MEMS by Design, and Silicon-Germanium (SiGe) Integrated Electronics for Extreme Environments. These nine sub-project tasks are managed by technical leads as located across five different NASA field centers, including Ames Research Center, Goddard Space Flight Center, the Jet Propulsion Laboratory, Langley Research Center, and Marshall Space Flight Center. The overall RHESE integrated project management responsibility resides with NASA's Marshall Space Flight Center (MSFC). Initial technology development emphasis within RHESE focuses on the hardening of Field Programmable Gate Arrays (FPGA)s and Field Programmable Analog

  18. High Strength Stainless Steel Properties that Affect Resistance Welding

    SciTech Connect

    Kanne, W.R.

    2001-08-01

    This report discusses results of a study on selected high strength stainless steel alloy properties that affect resistance welding. The austenitic alloys A-286, JBK-75 (Modified A-286), 21-6-9, 22-13-5, 316 and 304L were investigated and compared. The former two are age hardenable, and the latter four obtain their strength through work hardening. Properties investigated include corrosion and its relationship to chemical cleaning, the effects of heat treatment on strength and surface condition, and the effect of mechanical properties on strength and weldability.

  19. Hardening electronic devices against very high total dose radiation environments

    NASA Technical Reports Server (NTRS)

    Buchanan, B.; Shedd, W.; Roosild, S.; Dolan, R.

    1972-01-01

    The possibilities and limitations of hardening silicon semiconductor devices to the high neutron and gamma radiation levels and greater than 10 to the eighth power rads required for the NERVA nuclear engine development are discussed. A comparison is made of the high dose neutron and gamma hardening potential of bipolar, metal insulator semiconductors and junction field effect transistors. Experimental data is presented on device degradation for the high neutron and gamma doses. Previous data and comparisons indicate that the JFET is much more immune to the combined neutron displacement and gamma ionizing effects than other transistor types. Experimental evidence is also presented which indicates that p channel MOS devices may be able to meet the requirements.

  20. Precipitation Hardenable High Temperature Shape Memory Alloy

    NASA Technical Reports Server (NTRS)

    Noebe, Ronald Dean (Inventor); Draper, Susan L. (Inventor); Nathal, Michael V. (Inventor); Crombie, Edwin A. (Inventor)

    2010-01-01

    A composition of the invention is a high temperature shape memory alloy having high work output, and is made from (Ni+Pt+Y),Ti(100-x) wherein x is present in a total amount of 49-55 atomic % Pt is present in a total amount of 10-30 atomic %, Y is one or more of Au, Pd. and Cu and is present in a total amount of 0 to 10 atomic %. The alloy has a matrix phase wherein the total concentration of Ni, Pt, and the one or more of Pd. Au, and Cu is greater than 50 atomic %.

  1. High strength alloys

    DOEpatents

    Maziasz, Phillip James [Oak Ridge, TN; Shingledecker, John Paul [Knoxville, TN; Santella, Michael Leonard [Knoxville, TN; Schneibel, Joachim Hugo [Knoxville, TN; Sikka, Vinod Kumar [Oak Ridge, TN; Vinegar, Harold J [Bellaire, TX; John, Randy Carl [Houston, TX; Kim, Dong Sub [Sugar Land, TX

    2010-08-31

    High strength metal alloys are described herein. At least one composition of a metal alloy includes chromium, nickel, copper, manganese, silicon, niobium, tungsten and iron. System, methods, and heaters that include the high strength metal alloys are described herein. At least one heater system may include a canister at least partially made from material containing at least one of the metal alloys. At least one system for heating a subterranean formation may include a tubular that is at least partially made from a material containing at least one of the metal alloys.

  2. High strength alloys

    DOEpatents

    Maziasz, Phillip James; Shingledecker, John Paul; Santella, Michael Leonard; Schneibel, Joachim Hugo; Sikka, Vinod Kumar; Vinegar, Harold J.; John, Randy Carl; Kim, Dong Sub

    2012-06-05

    High strength metal alloys are described herein. At least one composition of a metal alloy includes chromium, nickel, copper, manganese, silicon, niobium, tungsten and iron. System, methods, and heaters that include the high strength metal alloys are described herein. At least one heater system may include a canister at least partially made from material containing at least one of the metal alloys. At least one system for heating a subterranean formation may include a tublar that is at least partially made from a material containing at least one of the metal alloys.

  3. Effects of welding and post-weld heat treatments on nanoscale precipitation and mechanical properties of an ultra-high strength steel hardened by NiAl and Cu nanoparticles

    DOE PAGES

    Jiao, Z. B.; Luan, J. H.; Guo, W.; Poplawsky, J. D.; Liu, C. T.

    2016-09-01

    The effects of welding and post-weld heat treatment (PWHT) on nanoscale co-precipitation, grain structure, and mechanical properties of an ultra-high strength steel were studied through a combination of atom probe tomography (APT) and mechanical tests. Our results indicate that the welding process dissolves all pre-existing nanoparticles and causes grain coarsening in the fusion zone, resulting in a soft and ductile weld without any cracks in the as-welded condition. A 550 °C PWHT induces fine-scale re-precipitation of NiAl and Cu co-precipitates with high number densities and ultra-fine sizes, leading to a large recovery of strength but a loss of ductility withmore » intergranular failure, whereas a 600 °C PWHT gives rise to coarse-scale re-precipitation of nanoparticles together with the formation of a small amount of reverted austenite, resulting in a great recovery in both strength and ductility. Our analysis indicates that the degree of strength recovery is dependent mainly upon the re-precipitation microstructure of nanoparticles, together with grain size and reversion of austenite, while the ductility recovery is sensitive to the grain-boundary structure. In conclusion, APT reveals that the grain-boundary segregation of Mn and P may be the main reason for the 550 °C embrittlement, and the enhanced ductility at 600 °C is ascribed to a possible reduction of the segregation and reversion of austenite.« less

  4. High strength composites evaluation

    SciTech Connect

    Marten, S.M.

    1992-02-01

    A high-strength, thick-section, graphite/epoxy composite was identified. The purpose of this development effort was to evaluate candidate materials and provide LANL with engineering properties. Eight candidate materials (Samples 1000, 1100, 1200, 1300, 1400, 1500, 1600, and 1700) were chosen for evaluation. The Sample 1700 thermoplastic material was the strongest overall.

  5. High-strength magnetic materials

    NASA Technical Reports Server (NTRS)

    Detert, K.

    1970-01-01

    Two new precipitation-hardened magnetic alloys are suitable for operation in 800 to 1600 deg F range. One is a martensitic alloy and the other a cobalt-based alloy. They possess improved creep resistance and have application in high temperature inductors and alternators.

  6. The Bendability of Ultra High strength Steels

    NASA Astrophysics Data System (ADS)

    Hazra, S. K.; Efthymiadis, P.; Alamoudi, A.; Kumar, R. L. V.; Shollock, B.; Dashwood, R.

    2016-08-01

    Automotive manufacturers have been reducing the weight of their vehicles to meet increasingly stringent environmental legislation that reflects public demand. A strategy is to use higher strength materials for parts with reduced cross-sections. However, such materials are less formable than traditional grades. The frequent result is increased processing and piece costs. 3D roll forming is a novel and flexible process: it is estimated that a quarter of the structure of a vehicle can be made with a single set of tooling. Unlike stamping, this process requires material with low work hardening rates. In this paper, we present results of ultra high strength steels that have low elongation in a tension but display high formability in bending through the suppression of the necking response.

  7. High strength ferritic alloy

    DOEpatents

    Hagel, William C.; Smidt, Frederick A.; Korenko, Michael K.

    1977-01-01

    A high-strength ferritic alloy useful for fast reactor duct and cladding applications where an iron base contains from about 9% to about 13% by weight chromium, from about 4% to about 8% by weight molybdenum, from about 0.2% to about 0.8% by weight niobium, from about 0.1% to about 0.3% by weight vanadium, from about 0.2% to about 0.8% by weight silicon, from about 0.2% to about 0.8% by weight manganese, a maximum of about 0.05% by weight nitrogen, a maximum of about 0.02% by weight sulfur, a maximum of about 0.02% by weight phosphorous, and from about 0.04% to about 0.12% by weight carbon.

  8. High-strength alloy with resistance to hydrogen-environment embrittlement

    NASA Technical Reports Server (NTRS)

    Mcnamara, T. G.

    1975-01-01

    Alloy is precipitation-hardened, high-strength, and low-thermal-expansion materials. It is iron-based and contains nickel and chromium at lower levels than high-strength alloys. It is readily welded and brazed and has good oxidation resistance. Tests indicated there was no reduction of notched or smooth strength.

  9. Strength, Hardening, and Failure Observed by In Situ TEM Tensile Testing.

    PubMed

    Kiener, Daniel; Kaufmann, Petra; Minor, Andrew M

    2012-11-01

    We present in situ transmission electron microscope tensile tests on focused ion beam fabricated single and multiple slip oriented Cu tensile samples with thicknesses in the range of 100-200 nm. Both crystal orientations fail by localized shear. While failure occurs after a few percent plastic strain and limited hardening in the single slip case, the multiple slip samples exhibit extended homogenous deformation and necking due to the activation of multiple dislocation sources in conjunction with significant hardening. The hardening behavior at 1% plastic strain is even more pronounced compared to compression samples of the same orientation due to the absence of sample taper and the interface to the compression platen. Moreover, we show for the first time that the strain rate sensitivity of such FIB prepared samples is an order of magnitude higher than that of bulk Cu.

  10. Radiation Hardened, Modulator ASIC for High Data Rate Communications

    NASA Technical Reports Server (NTRS)

    McCallister, Ron; Putnam, Robert; Andro, Monty; Fujikawa, Gene

    2000-01-01

    Satellite-based telecommunication services are challenged by the need to generate down-link power levels adequate to support high quality (BER approx. equals 10(exp 12)) links required for modem broadband data services. Bandwidth-efficient Nyquist signaling, using low values of excess bandwidth (alpha), can exhibit large peak-to-average-power ratio (PAPR) values. High PAPR values necessitate high-power amplifier (HPA) backoff greater than the PAPR, resulting in unacceptably low HPA efficiency. Given the high cost of on-board prime power, this inefficiency represents both an economical burden, and a constraint on the rates and quality of data services supportable from satellite platforms. Constant-envelope signals offer improved power-efficiency, but only by imposing a severe bandwidth-efficiency penalty. This paper describes a radiation- hardened modulator which can improve satellite-based broadband data services by combining the bandwidth-efficiency of low-alpha Nyquist signals with high power-efficiency (negligible HPA backoff).

  11. The origins of high hardening and low ductility in magnesium.

    PubMed

    Wu, Zhaoxuan; Curtin, W A

    2015-10-01

    Magnesium is a lightweight structural metal but it exhibits low ductility-connected with unusual, mechanistically unexplained, dislocation and plasticity phenomena-which makes it difficult to form and use in energy-saving lightweight structures. We employ long-time molecular dynamics simulations utilizing a density-functional-theory-validated interatomic potential, and reveal the fundamental origins of the previously unexplained phenomena. Here we show that the key 〈c + a〉 dislocation (where 〈c + a〉 indicates the magnitude and direction of slip) is metastable on easy-glide pyramidal II planes; we find that it undergoes a thermally activated, stress-dependent transition to one of three lower-energy, basal-dissociated immobile dislocation structures, which cannot contribute to plastic straining and that serve as strong obstacles to the motion of all other dislocations. This transition is intrinsic to magnesium, driven by reduction in dislocation energy and predicted to occur at very high frequency at room temperature, thus eliminating all major dislocation slip systems able to contribute to c-axis strain and leading to the high hardening and low ductility of magnesium. Enhanced ductility can thus be achieved by increasing the time and temperature at which the transition from the easy-glide metastable dislocation to the immobile basal-dissociated structures occurs. Our results provide the underlying insights needed to guide the design of ductile magnesium alloys.

  12. Cold-rolled, high-strength sheet steels for auto applications

    NASA Astrophysics Data System (ADS)

    Bleck, Wolfgang

    1996-07-01

    Several groups of cold-rolled, high-strength sheet steels have been developed to optimize the required strength and formability levels for automotive applications. Multiphase steels offer new opportunities where high-strength levels are demanded. The future in steel development will be determined by the physical modeling of properties and by adapting new process routes such as thin slab casting and in-line rolling. In this article, developments in traditional strengthening concepts (e.g., microalloying and substitutional hardening with phosphorus) and more recently developed concepts (e.g., bake hardening and strengthening of interstitial-free steels) are reviewed.

  13. Metastable high-entropy dual-phase alloys overcome the strength-ductility trade-off

    NASA Astrophysics Data System (ADS)

    Li, Zhiming; Pradeep, Konda Gokuldoss; Deng, Yun; Raabe, Dierk; Tasan, Cemal Cem

    2016-06-01

    Metals have been mankind’s most essential materials for thousands of years; however, their use is affected by ecological and economical concerns. Alloys with higher strength and ductility could alleviate some of these concerns by reducing weight and improving energy efficiency. However, most metallurgical mechanisms for increasing strength lead to ductility loss, an effect referred to as the strength-ductility trade-off. Here we present a metastability-engineering strategy in which we design nanostructured, bulk high-entropy alloys with multiple compositionally equivalent high-entropy phases. High-entropy alloys were originally proposed to benefit from phase stabilization through entropy maximization. Yet here, motivated by recent work that relaxes the strict restrictions on high-entropy alloy compositions by demonstrating the weakness of this connection, the concept is overturned. We decrease phase stability to achieve two key benefits: interface hardening due to a dual-phase microstructure (resulting from reduced thermal stability of the high-temperature phase); and transformation-induced hardening (resulting from the reduced mechanical stability of the room-temperature phase). This combines the best of two worlds: extensive hardening due to the decreased phase stability known from advanced steels and massive solid-solution strengthening of high-entropy alloys. In our transformation-induced plasticity-assisted, dual-phase high-entropy alloy (TRIP-DP-HEA), these two contributions lead respectively to enhanced trans-grain and inter-grain slip resistance, and hence, increased strength. Moreover, the increased strain hardening capacity that is enabled by dislocation hardening of the stable phase and transformation-induced hardening of the metastable phase produces increased ductility. This combined increase in strength and ductility distinguishes the TRIP-DP-HEA alloy from other recently developed structural materials. This metastability-engineering strategy should

  14. Metastable high-entropy dual-phase alloys overcome the strength-ductility trade-off.

    PubMed

    Li, Zhiming; Pradeep, Konda Gokuldoss; Deng, Yun; Raabe, Dierk; Tasan, Cemal Cem

    2016-06-01

    Metals have been mankind's most essential materials for thousands of years; however, their use is affected by ecological and economical concerns. Alloys with higher strength and ductility could alleviate some of these concerns by reducing weight and improving energy efficiency. However, most metallurgical mechanisms for increasing strength lead to ductility loss, an effect referred to as the strength-ductility trade-off. Here we present a metastability-engineering strategy in which we design nanostructured, bulk high-entropy alloys with multiple compositionally equivalent high-entropy phases. High-entropy alloys were originally proposed to benefit from phase stabilization through entropy maximization. Yet here, motivated by recent work that relaxes the strict restrictions on high-entropy alloy compositions by demonstrating the weakness of this connection, the concept is overturned. We decrease phase stability to achieve two key benefits: interface hardening due to a dual-phase microstructure (resulting from reduced thermal stability of the high-temperature phase); and transformation-induced hardening (resulting from the reduced mechanical stability of the room-temperature phase). This combines the best of two worlds: extensive hardening due to the decreased phase stability known from advanced steels and massive solid-solution strengthening of high-entropy alloys. In our transformation-induced plasticity-assisted, dual-phase high-entropy alloy (TRIP-DP-HEA), these two contributions lead respectively to enhanced trans-grain and inter-grain slip resistance, and hence, increased strength. Moreover, the increased strain hardening capacity that is enabled by dislocation hardening of the stable phase and transformation-induced hardening of the metastable phase produces increased ductility. This combined increase in strength and ductility distinguishes the TRIP-DP-HEA alloy from other recently developed structural materials. This metastability-engineering strategy should

  15. Material Strength at High Pressure LDRD Strategic Initiative Final Report

    SciTech Connect

    Lassila, D H; Bonner, B P; Bulatov, V V; Cazamias, J U; Chandler, E A; Farber, D L; Moriarty, J A; Zaug, J M

    2004-03-02

    Various aspects of the Laboratory's national security mission are now highly dependent on accurate computer code simulations of plastic flow (i.e., non-reversible deformation) of materials under conditions of high hydrostatic pressure. Strength models are typically dependent on pressure, temperature, and strain rate. Current strength models can not be extrapolated to high pressure because they are not based on the underlying mechanisms of plastic deformation. The critical need for predictive models of material strength, which describe flow stress in computer code simulations, has motivated LLNL's multiscale modeling efforts. Over the past three years, the ''Material Strength at High Pressure'' LDRD Strategic Initiative has established a framework for the development of predictive strength models for deformation of metals under conditions of high hydrostatic pressure. Deformation experiments have been developed to measure the effect of high pressure on the yield strength and work hardening behavior of high purity Mo and Ta single crystals. The over arching goal of the SI is to experimentally validate multiscale-modeling capabilities for deformation of metals under conditions of high pressure. The work performed and accomplished is a necessary next step in the development of predictive strength models. Our initial experimental results show that the influence of pressure is to dramatically increase the work hardening rate of Ta. Bridgman also observed this in experiments performed in the 1950's. Currently there is very little modern data on this phenomena, or theoretical understanding. The work started by this SI is a first step in a comprehensive understanding of plasticity under conditions of high pressure and we expect eventually to be able to incorporate the proper physics into dislocation dynamics (DD) simulations to capture the increase in work hardening that we observe experimentally. In the following sections we briefly describe the work that was performed in

  16. Strength, thermal defects, and solid solution hardening in nickel-containing B2 iron aluminides

    SciTech Connect

    Schneibel, J.H.; Munroe, P.R.; Pike, L.M.

    1996-12-31

    Nickel-containing ternary iron aluminides with an aluminum concentration of 45 at.% were investigated with respect to room temperature strength, equilibrium vacancy concentration, and the kinetics of vacancy removal. As compared to binary iron aluminides with the same Al concentration, nickel additions reduce the thermal equilibrium vacancy concentration at 1,273 K, whereas they increase this concentration at 973 K. Furthermore, at low temperatures such as 673 K, nickel additions increase dramatically the time needed to reach vacancy equilibrium. During prolonged annealing at 673 K, the density of <001> dislocations in Fe-45Al-3Ni (at.%) increased by an order of magnitude. This suggests that dislocations act as sinks for vacancies. At the same time, the number density of small (20--50 nm) voids decreased, indicating that they were not stable in the absence of substantial vacancy supersaturations. The findings show also that the solid solution strengthening of iron aluminides due to Ni is much weaker than previously thought.

  17. Development of high strength, high temperature ceramics

    NASA Technical Reports Server (NTRS)

    Hall, W. B.

    1982-01-01

    Improvement in the high-pressure turbopumps, both fuel and oxidizer, in the Space Shuttle main engine were considered. The operation of these pumps is limited by temperature restrictions of the metallic components used in these pumps. Ceramic materials that retain strength at high temperatures and appear to be promising candidates for use as turbine blades and impellers are discussed. These high strength materials are sensitive to many related processing parameters such as impurities, sintering aids, reaction aids, particle size, processing temperature, and post thermal treatment. The specific objectives of the study were to: (1) identify and define the processing parameters that affect the properties of Si3N4 ceramic materials, (2) design and assembly equipment required for processing high strength ceramics, (3) design and assemble test apparatus for evaluating the high temperature properties of Si3N4, and (4) conduct a research program of manufacturing and evaluating Si3N4 materials as applicable to rocket engine applications.

  18. Strength Development of High-Strength Ductile Concrete Incorporating Metakaolin and PVA Fibers

    PubMed Central

    Nuruddin, Muhammad Fadhil; Shafiq, Nasir

    2014-01-01

    The mechanical properties of high-strength ductile concrete (HSDC) have been investigated using Metakaolin (MK) as the cement replacing material and PVA fibers. Total twenty-seven (27) mixes of concrete have been examined with varying content of MK and PVA fibers. It has been found that the coarser type PVA fibers provide strengths competitive to control or higher than control. Concrete with coarser type PVA fibers has also refined microstructure, but the microstructure has been undergone with the increase in aspect ratio of fibers. The microstructure of concrete with MK has also more refined and packing of material is much better with MK. PVA fibers not only give higher stiffness but also showed the deflection hardening response. Toughness Index of HSDC reflects the improvement in flexural toughness over the plain concrete and the maximum toughness indices have been observed with 10% MK and 2% volume fraction of PVA fibers. PMID:24707202

  19. Strength development of high-strength ductile concrete incorporating Metakaolin and PVA fibers.

    PubMed

    Nuruddin, Muhammad Fadhil; Khan, Sadaqat Ullah; Shafiq, Nasir; Ayub, Tehmina

    2014-01-01

    The mechanical properties of high-strength ductile concrete (HSDC) have been investigated using Metakaolin (MK) as the cement replacing material and PVA fibers. Total twenty-seven (27) mixes of concrete have been examined with varying content of MK and PVA fibers. It has been found that the coarser type PVA fibers provide strengths competitive to control or higher than control. Concrete with coarser type PVA fibers has also refined microstructure, but the microstructure has been undergone with the increase in aspect ratio of fibers. The microstructure of concrete with MK has also more refined and packing of material is much better with MK. PVA fibers not only give higher stiffness but also showed the deflection hardening response. Toughness Index of HSDC reflects the improvement in flexural toughness over the plain concrete and the maximum toughness indices have been observed with 10% MK and 2% volume fraction of PVA fibers.

  20. Strength development of high-strength ductile concrete incorporating Metakaolin and PVA fibers.

    PubMed

    Nuruddin, Muhammad Fadhil; Khan, Sadaqat Ullah; Shafiq, Nasir; Ayub, Tehmina

    2014-01-01

    The mechanical properties of high-strength ductile concrete (HSDC) have been investigated using Metakaolin (MK) as the cement replacing material and PVA fibers. Total twenty-seven (27) mixes of concrete have been examined with varying content of MK and PVA fibers. It has been found that the coarser type PVA fibers provide strengths competitive to control or higher than control. Concrete with coarser type PVA fibers has also refined microstructure, but the microstructure has been undergone with the increase in aspect ratio of fibers. The microstructure of concrete with MK has also more refined and packing of material is much better with MK. PVA fibers not only give higher stiffness but also showed the deflection hardening response. Toughness Index of HSDC reflects the improvement in flexural toughness over the plain concrete and the maximum toughness indices have been observed with 10% MK and 2% volume fraction of PVA fibers. PMID:24707202

  1. Development of third generation advanced high strength steels

    NASA Astrophysics Data System (ADS)

    McGrath, Meghan Colleen

    Lightweight duplex steels with combinations of either bainite, acicular ferrite, and austenite or martensite and austenite were investigated as third generation advanced high strength steels targeted for automotive applications. Large additions of manganese (> 13 wt%) and carbon (<0.2wt%) were employed to stabilize the austenite phase. Silicon additions between 1 and 2 wt% were added to suppress cementite formation. Strength and ductility were increased while density was decreased with aluminum additions between 2.4 and 5.5 wt% to the steel. This research addressed the dependence of alloying on microstructures and mechanical behavior for high manganese and aluminum duplex steels that were cast and subsequently hot rolled. Duplex steels with different volume fractions of primary delta-ferrite were used to study the crystallography of austenite fanned during the peritectic reaction. Solute profiles across the peritectic interface showed aluminum segregated near the interface which promoted bainitic ferrite formation. Thermal treatments were used to manipulate the concentration and type of oxides and the ferrite plate density was found to correlate with inclusions of low misfit in steels with austenite grain size of 16.5 microm. A steel with bainite and acicular ferrite produced an ultimate tensile strength of 970 MPa and elongation of 40%. The mechanical prope1iies depended on the strengths and size of the microstructural constituents. Work hardening behavior was examined in a steel exhibiting multiple martensitic transformation induced plasticity (gamma-austenite→epsilon-smartensite→alpha-martensite). A strain hardening exponent as high as 1.4 was observed with ultimate tensile strength and elongation as high as 1,165 MPa and 34%.

  2. High strength high modulus ceramic fiber

    NASA Technical Reports Server (NTRS)

    Fetterolf, R. N.

    1972-01-01

    Low cost method was developed for producing high strength, high modulus, continuous ceramic oxide fibers. Process transforms inexpensive metallic salts into syrup-like liquids that can be fiberized at room temperatures. Resulting salt fibers are then converted to oxides by calcination at relatively low temperatures.

  3. High strength, tough alloy steel

    DOEpatents

    Thomas, Gareth; Rao, Bangaru V. N.

    1979-01-01

    A high strength, tough alloy steel is formed by heating the steel to a temperature in the austenite range (1000.degree.-1100.degree. C.) to form a homogeneous austenite phase and then cooling the steel to form a microstructure of uniformly dispersed dislocated martensite separated by continuous thin boundary films of stabilized retained austenite. The steel includes 0.2-0.35 weight % carbon, at least 1% and preferably 3-4.5% chromium, and at least one other substitutional alloying element, preferably manganese or nickel. The austenite film is stable to subsequent heat treatment as by tempering (below 300.degree. C.) and reforms to a stable film after austenite grain refinement.

  4. Finite-Element Simulation of Conventional and High-Speed Peripheral Milling of Hardened Mold Steel

    NASA Astrophysics Data System (ADS)

    Tang, D. W.; Wang, C. Y.; Hu, Y. N.; Song, Y. X.

    2009-12-01

    A finite-element model (FEM) with the flow stress and typical fracture is used to simulate a hard machining process, which before this work could not adequately represent the constitutive behavior of workpiece material that is usually heat treated to hardness levels above 50 Rockwell C hardness (HRC). Thus, a flow stress equation with a variation in hardness is used in the computer simulation of hard machining. In this article, the influence of the milling speed on the cutting force, chip morphology, effective stress, and cutting temperature in the deformation zones of both conventional and high-speed peripheral milling hardened mold steel is systematically studied by finite-element analysis (FEA). By taking into consideration the importance of material characteristics during the milling process, the similar Johnson-Cook’s constitutive equation with hardened mold steel is introduced to the FEM to investigate the peripheral milling of hardened mold steel. In comparison with the experimental data of the cutting force at various cutting speeds, the simulation result is identical with the measured data. The results indicate that the model can be used to accurately predict the behavior of hardened mold steel in both conventional and high-speed milling.

  5. High strength, high ductility low carbon steel

    DOEpatents

    Koo, Jayoung; Thomas, Gareth

    1978-01-01

    A high strength, high ductility low carbon steel consisting essentially of iron, 0.05-0.15 wt% carbon, and 1-3 wt% silicon. Minor amounts of other constituents may be present. The steel is characterized by a duplex ferrite-martensite microstructure in a fibrous morphology. The microstructure is developed by heat treatment consisting of initial austenitizing treatment followed by annealing in the (.alpha. + .gamma.) range with intermediate quenching.

  6. High strength and high toughness steel

    DOEpatents

    Parker, Earl R.; Zackay, Victor F.

    1979-01-01

    A structural steel which possess both high strength and high toughness and has particular application of cryogenic uses. The steel is produced by the utilization of thermally induced phase transformation following heating in a three-phase field in iron-rich alloys of the Fe-Ni-Ti system, with a preferred composition of 12% nickel, 0.5% titanium, the remainder being iron.

  7. Constitutive equation for hardened SKD11 steel at high temperature and high strain rate using the SHPB technique

    NASA Astrophysics Data System (ADS)

    Tang, D. W.; Wang, C. Y.; Hu, Y. N.; Song, Y. X.

    2010-03-01

    In this present work, dynamic tests have been performed on hardened SKD11 steel (62 Rockwell C hardness) specimens by means of a high temperature split Hopkinson pressure bar (SHPB) test system. Effects of temperature as well as those of strain and strain rate for the hardened steel are taken into account by using two ellipsoidal radiant heating reflectors with two halogen lamps and magnetic valve. The result obtained at high stain rates were compared with those at low strain rates under the different temperature. It was seen that the flow stress curves are found to include a work hardening region and a work softening region and the mechanical behavior of the hardened steel is highly sensitive to both the strain rate and the temperature. To determine the true flow stress- true strain, temperature relationship, specimens are tested from room temperature to 1073K at a strain rate form 0.01 s-1 to 104 s-1: The parameters for a Johnson-Cook constitutive equation and a modified Johnson-Cook constitutive equation are determined from the test results by fitting the data from both quasi-static compression and high temperature-dynamic compression tests. The modified Johnson-Cook constitutive equation is more suitable for expressing the dynamic behavior of the hardened SKD11 steel above the vicinity of the recrystallization temperature.

  8. Constitutive equation for hardened SKD11 steel at high temperature and high strain rate using the SHPB technique

    NASA Astrophysics Data System (ADS)

    Tang, D. W.; Wang, C. Y.; Hu, Y. N.; Song, Y. X.

    2009-12-01

    In this present work, dynamic tests have been performed on hardened SKD11 steel (62 Rockwell C hardness) specimens by means of a high temperature split Hopkinson pressure bar (SHPB) test system. Effects of temperature as well as those of strain and strain rate for the hardened steel are taken into account by using two ellipsoidal radiant heating reflectors with two halogen lamps and magnetic valve. The result obtained at high stain rates were compared with those at low strain rates under the different temperature. It was seen that the flow stress curves are found to include a work hardening region and a work softening region and the mechanical behavior of the hardened steel is highly sensitive to both the strain rate and the temperature. To determine the true flow stress- true strain, temperature relationship, specimens are tested from room temperature to 1073K at a strain rate form 0.01 s-1 to 104 s-1: The parameters for a Johnson-Cook constitutive equation and a modified Johnson-Cook constitutive equation are determined from the test results by fitting the data from both quasi-static compression and high temperature-dynamic compression tests. The modified Johnson-Cook constitutive equation is more suitable for expressing the dynamic behavior of the hardened SKD11 steel above the vicinity of the recrystallization temperature.

  9. Hardening behavior after high-temperature solution treatment of Ag-20Pd-12Au-xCu alloys with different Cu contents for dental prosthetic restorations.

    PubMed

    Kim, Yonghwan; Niinomi, Mitsuo; Hieda, Junko; Nakai, Masaaki; Cho, Ken; Fukui, Hisao

    2014-07-01

    Ag-Pd-Au-Cu alloys have been used widely for dental prosthetic applications. Significant enhancement of the mechanical properties of the Ag-20Pd-12Au-14.5Cu alloy as a result of the precipitation of the β' phase through high-temperature solution treatment (ST), which is different from conventional aging treatment in these alloys, has been reported. The relationship between the unique hardening behavior and precipitation of the β' phase in Ag-20Pd-12Au-xCu alloys (x=6.5, 13, 14.5, 17, and 20mass%) subjected to the high-temperature ST at 1123K for 3.6ks was investigated in this study. Unique hardening behavior after the high-temperature ST also occurs in Ag-20Pd-12Au-xCu alloys (x=13, 17, and 20) with precipitation of the β' phase. However, hardening is not observed and the β' phase does not precipitate in the Ag-20Pd-12Au-6.5Cu alloy after the same ST. The tensile strength and 0.2% proof stress also increase in Ag-20Pd-12Au-xCu alloys (x=13, 14.5, 17, and 20) after the high-temperature ST. In addition, these values after the high-temperature ST increase with increasing Cu content in Ag-20Pd-12Au-xCu alloys (x=14.5, 17, and 20). The formation process of the β' phase can be explained in terms of diffusion of Ag and Cu atoms and precipitation of the β' phase. Clarification of the relationship between hardening and precipitation of the β' phase via high-temperature ST is expected to help the development of more effective heat treatments for hardening in Ag-20Pd-12Au-xCu alloys.

  10. Hardening of the surface plasma jet high-frequency induction discharge of low pressure

    NASA Astrophysics Data System (ADS)

    Kashapov, N. F.; Sharifullin, S. N.

    2015-06-01

    The work presents results of research on the hardening surfaces of the products and increase their roughness class of plasma jet of high-frequency induction discharge of low pressure. It is shown that such processing allows to clear at the same time a surface of all types of pollution, to remove a defective layer after its machining, to receive a uniform microstructure, to raise a roughness class on 2 - 3 units.

  11. Solution hardening and strain hardening at elevated temperatures

    SciTech Connect

    Kocks, U.F.

    1982-10-01

    Solutes can significantly increase the rate of strain hardening; as a consequence, the saturation stress, at which strain hardening tends to cease for a given temperature and strain rate, is increased more than the yield stress: this is the major effect of solutes on strength at elevated temperatures, especially in the regime where dynamic strain-aging occurs. It is shown that local solute mobility can affect both the rate of dynamic recovery and the dislocation/dislocation interaction strength. The latter effect leads to multiplicative solution strengthening. It is explained by a new model based on repeated dislocation unlocking, in a high-temperature limit, which also rationalizes the stress dependence of static and dynamic strain-aging, and may help explain the plateau of the yield stress at elevated temperatures. 15 figures.

  12. High-Performance, Radiation-Hardened Electronics for Space and Lunar Environments

    NASA Technical Reports Server (NTRS)

    Keys, Andrew S.; Adams, James H.; Cressler, John D.; Darty, Ronald C.; Johnson, Michael A.; Patrick, Marshall C.

    2008-01-01

    The Radiation Hardened Electronics for Space Environments (RHESE) project develops advanced technologies needed for high performance electronic devices that will be capable of operating within the demanding radiation and thermal extremes of the space, lunar, and Martian environment. The technologies developed under this project enhance and enable avionics within multiple mission elements of NASA's Vision for Space Exploration. including the Constellation program's Orion Crew Exploration Vehicle. the Lunar Lander project, Lunar Outpost elements, and Extra Vehicular Activity (EVA) elements. This paper provides an overview of the RHESE project and its multiple task tasks, their technical approaches, and their targeted benefits as applied to NASA missions.

  13. Influence of slip system hardening assumptions on modeling stress dependence of work hardening

    NASA Astrophysics Data System (ADS)

    Miller, Matthew; Dawson, Paul

    1997-11-01

    Due to the discrete directional nature of processes such as crystallographic slip, the orientation of slip planes relative to a fixed set of loading axes has a direct effect on the magnitude of the external load necessary to induce dislocation motion (yielding). The effect such geometric or textural hardening has on the macroscopic flow stress can be quantified in a polycrystal by the average Taylor factor M¯. Sources of resistance to dislocation motion such as interaction with dislocation structures, precipitates, and grain boundaries, contribute to the elevation of the critically resolved shear strength τcrss. In continuum slip polycrystal formulations, material hardening phenomena are reflected in the slip system hardness equations. Depending on the model, the hardening equations and the mean field assumption can both affect geometric hardening through texture evolution. In this paper, we examine continuum slip models and focus on how the slip system hardening model and the mean field assumption affect the stress-strain response. Texture results are also presented within the context of how the texture affects geometric hardening. We explore the effect of employing slip system hardnesses averaged over different size scales. We first compare a polycrystal simulation employing a single hardness per crystal to one using a latent hardening formulation producing distinct slip system hardnesses. We find little difference between the amplitude of the single hardness and a crystal-average of the latent hardening values. The geometric hardening is different due to the differences in the textures predicted by each model. We also find that due to the high degree of symmetry in an fcc crystal, macroscopic stress-strain predictions using simulations employing crystal- and aggregateaveraged hardnesses are nearly identical. We find this to be true for several different mean field assumptions. An aggregate-averaged hardness may be preferred in light of the difficulty

  14. Tailoring the strength and porosity of rapid-hardening magnesia phosphate paste via the pre-foaming method.

    PubMed

    Liu, Li-Jie; Li, Jin-Hong; Wang, Xiang; Qian, Ting-Ting; Li, Xiao-Hui

    2015-08-13

    High-porosity magnesia phosphate paste (HPMPP) was prepared via the pre-foaming method. In the pre-foaming method, sintering treatment was not required. The bulk density and maximum compressive strength of the HPMPP prepared according to the ratio of water to solids (W/So) of 0.32 reached 464.00 ± 5.00 Kg/m(3) and 0.30 ± 0.05 MPa, respectively. The compressive strength increased with the increases in the addition amounts of sodium silicate and polypropylene fibers. The bulk density of HPMPP increased with the increase in the addition of sodium silicate and decreased with the increase in the addition of polypropylene fibers. Besides, the porosity of the magnesia phosphate paste increased from 79.85% to 81.27% and from 80.31% to 83.75% after the addition of sodium silicate and polypropylene fibers respectively. The highest porosity (83.75%) of the prepared HPMPP was realized under the addition proportion (sodium silicate: polypropylene fibers: solids = 0.06:0.0025:1). The average pore size of the prepared HPMPP is about 180 μm and the pore distribution range is relatively narrow. The hydration product (struvite) is combined with MgO particle one by one and then coated on the surface of bubbles. With the decrease of the water content, after breaking bubbles, the porous structure can be achieved.

  15. Tailoring the strength and porosity of rapid-hardening magnesia phosphate paste via the pre-foaming method

    NASA Astrophysics Data System (ADS)

    Liu, Li-Jie; Li, Jin-Hong; Wang, Xiang; Qian, Ting-Ting; Li, Xiao-Hui

    2015-08-01

    High-porosity magnesia phosphate paste (HPMPP) was prepared via the pre-foaming method. In the pre-foaming method, sintering treatment was not required. The bulk density and maximum compressive strength of the HPMPP prepared according to the ratio of water to solids (W/So) of 0.32 reached 464.00 ± 5.00 Kg/m3 and 0.30 ± 0.05 MPa, respectively. The compressive strength increased with the increases in the addition amounts of sodium silicate and polypropylene fibers. The bulk density of HPMPP increased with the increase in the addition of sodium silicate and decreased with the increase in the addition of polypropylene fibers. Besides, the porosity of the magnesia phosphate paste increased from 79.85% to 81.27% and from 80.31% to 83.75% after the addition of sodium silicate and polypropylene fibers respectively. The highest porosity (83.75%) of the prepared HPMPP was realized under the addition proportion (sodium silicate: polypropylene fibers: solids = 0.06:0.0025:1). The average pore size of the prepared HPMPP is about 180 μm and the pore distribution range is relatively narrow. The hydration product (struvite) is combined with MgO particle one by one and then coated on the surface of bubbles. With the decrease of the water content, after breaking bubbles, the porous structure can be achieved.

  16. Dry and clean age hardening of aluminum alloys by high-pressure gas quenching

    NASA Astrophysics Data System (ADS)

    Irretier, A.; Kessler, O.; Hoffmann, F.; Mayr, P.

    2004-10-01

    When precipitation-hardenable aluminum parts are water quenched, distortion occurs due to thermal stresses. Thereby, a costly reworking is necessary, and for this reason polymer quenchants are often used to reduce distortion, with the disadvantage that the quenched parts have to be cleaned after quenching. In opposition to liquid quenchants, gas quenching may decrease distortion due to the better temperature uniformity during quenching. Furthermore, cleaning of the quenched parts can be avoided because it is a dry process. For this purpose, a heat-treating process was evaluated that included a high-pressure gasquenching step. Gas quenching was applied to different aluminum alloys (i.e., 2024, 6013, 7075, and A357.0), and tensile tests have been carried out to determine the mechanical properties after solution annealing, gas quenching, and aging. Besides high-pressure gas quenching, alloy 2024 was quenched at ambient pressure in a gas nozzle field. The high velocity at the gas outlet leads to an accelerated cooling of the aluminum alloy in this case. Aluminum castings and forgings can be classified as an interesting field of application of these quenching methods due to their near-net shape before the heat treatment. Cost savings would be possible due to the reduced distortion, and therefore, less reworking after the precipitation hardening.

  17. High strength and high ductility behavior of 6061-T6 alloy after laser shock processing

    NASA Astrophysics Data System (ADS)

    Gencalp Irizalp, Simge; Saklakoglu, Nursen

    2016-02-01

    The plastic deformation behavior of 6061-T6 alloy which was subjected to severe plastic deformation (SPD) at high strain rates during laser shock processing (LSP) was researched. In LSP-treated materials, the near surface microstructural change was examined by TEM and fracture surfaces after tensile testing were examined by SEM. An increase in strength of metallic materials brings about the decrease in ductility. In this study, the results showed that LSP-treated 6061-T6 alloy exhibited both high strength and high ductility. TEM observation showed that stacking fault (SF) ribbon enlarged, deformation twins formed and twin boundary increased in LSP-treated 6061-T6 alloy. This observation was an indication of stacking fault energy (SFE) decrease. Work hardening capability was recovered after LSP impacts.

  18. Gradient twinned 304 stainless steels for high strength and high ductility

    DOE PAGES

    Chen, Aiying; Liu, Jiabin; Wang, Hongtao; Lu, Jian; Wang, Y. Morris

    2016-04-23

    Gradient materials often have attractive mechanical properties that outperform uniform microstructure counterparts. It remains a difficult task to investigate and compare the performance of various gradient microstructures due to the difficulty of fabrication, the wide range of length scales involved, and their respective volume percentage variations. We have investigated four types of gradient microstructures in 304 stainless steels that utilize submicrotwins, nanotwins, nanocrystalline-, ultrafine- and coarse-grains as building blocks. Tensile tests reveal that the gradient microstructure consisting of submicrotwins and nanotwins has a persistent and stable work hardening rate and yields an impressive combination of high strength and high ductility,more » leading to a toughness that is nearly 50% higher than that of the coarse-grained counterpart. Ex- and in-situ transmission electron microscopy indicates that nanoscale and submicroscale twins help to suppress and limit martensitic phase transformation via the confinement of martensite within the twin lamellar. Twinning and detwinning remain active during tensile deformation and contribute to the work hardening behavior. We discuss the advantageous properties of using submicrotwins as the main load carrier and nanotwins as the strengthening layers over those coarse and nanocrystalline grains. Furthermore, our work uncovers a new gradient design strategy to help metals and alloys achieve high strength and high ductility.« less

  19. Development of ductile high-strength chromium alloys, phase 2

    NASA Technical Reports Server (NTRS)

    Filippi, A. M.

    1973-01-01

    Strength and ductility were evaluated for chromium alloys dispersion hardened with the putative TaC, TaB, CbC, and CbB compounds. TaC and TaB proved to be the most potent strengtheners, but when combined, their effect far outweighed that produced individually. Tests at 1422 K (2100 F) on an alloy containing these two compounds at the combined level of 0.5 m/o revealed a 495 MN/sq m (70 ksi) tensile strength for wrought material, and a 100 hour rupture strength of 208 MN/sq m (30 ksi) when solution annealed and aged to maximize creep resistance. These levels of high temperature strength greatly exceed that reported for any other chromium-base alloy. The ductile-to-brittle transition temperature (DBTT) of the two phase strengthened alloy occurred at approximately 588 K (600 F) when heat treated to optimize creep strength and was not improved by fabrication to produce a wrought and recovered microstructure. The lowest DBTT measured on any of the alloys investigated was 422 K (300 F). Strengthening phases actually formed in Cr-Ta-B and Cr-Cb-B compositions are probable M2CrB2 (M=Ta or Cb) compounds of tetragonal crystal structure. The likely habit relationship between these compounds and chromium is postulated. Cube habit coherency was identified for TaC precipitation in chromium by electron microscopy. In another study, the maximum solubility of carbon in chromium was indicated to lie between 3/4 and 1 a/o and that of boron to be 1/2 a/o.

  20. High-Hot-Strength Ceramic Fibers

    NASA Technical Reports Server (NTRS)

    Sayir, Ali; Matson, Lawrence E.

    1994-01-01

    Continuous fibers consisting of laminae of alumina and yttrium aluminum garnet offer exceptionally high strength, resistance to creep, and chemical stability at high temperatures. These fibers exceed tensile strength of sapphire fibers. Leading candidates for reinforcement of intermetallic-matrix composites in exhaust nozzles of developmental high-speed civil transport aircraft engines. Other applications are in aerospace, automotive, chemical-process, and power-generation industries.

  1. High-Strength, Superelastic Compounds

    NASA Technical Reports Server (NTRS)

    Stanford, Malcolm; Noebe, Ronald; Dellacorte, Christopher; Bigelow, Glen; Thomas, Fransua

    2013-01-01

    can be used in the heat treatment process, less energy will be consumed, and there will be less dimensional distortion and quench cracking. This results in fewer scrap parts, less material waste from large amounts of material removal, and fewer machining steps to rework parts that are out of specification. This material has a combination of properties that have been previously unobtainable. The material has a Young s modulus of approximately 95 GPa (about half that of conventional steels), moderate density (10 to 15% lower than conventional steels), excellent corrosion resistance, and high hardness (58 to 62 HRC). These properties make this material uniquely suited for advanced bearings.

  2. High toughness-high strength iron alloy

    NASA Technical Reports Server (NTRS)

    Stephens, J. R.; Witzke, W. R. (Inventor)

    1980-01-01

    An iron alloy is provided which exhibits strength and toughness characteristics at cryogenic temperatures. The alloy consists essentially of about 10 to 16 percent by weight nickel, about 0.1 to 1.0 percent by weight aluminum, and 0 to about 3 percent by weight copper, with the balance being essentially iron. The iron alloy is produced by a process which includes cold rolling at room temperature and subsequent heat treatment.

  3. Development of High Specific Strength Envelope Materials

    NASA Astrophysics Data System (ADS)

    Komatsu, Keiji; Sano, Masa-Aki; Kakuta, Yoshiaki

    Progress in materials technology has produced a much more durable synthetic fabric envelope for the non-rigid airship. Flexible materials are required to form airship envelopes, ballonets, load curtains, gas bags and covering rigid structures. Polybenzoxazole fiber (Zylon) and polyalirate fiber (Vectran) show high specific tensile strength, so that we developed membrane using these high specific tensile strength fibers as a load carrier. The main material developed is a Zylon or Vectran load carrier sealed internally with a polyurethane bonded inner gas retention film (EVOH). The external surface provides weather protecting with, for instance, a titanium oxide integrated polyurethane or Tedlar film. The mechanical test results show that tensile strength 1,000 N/cm is attained with weight less than 230g/m2. In addition to the mechanical properties, temperature dependence of the joint strength and solar absorptivity and emissivity of the surface are measured. 

  4. Change in high-temperature strength properties of 12Kh1MF steel in long-term loading under creep conditions

    SciTech Connect

    Shron, R.Z.; Mints, I.I.; Shul`gina, N.G.

    1995-01-01

    Stress-rupture strength tests were made of metal steam pipe (12Kh1MF steel) in various conditions, the original, after aging under laboratory conditions (580{degrees}C, 10,000 h), and after long service. It was shown that the more the steel is hardened by heat treatment or cold plastic working in the original condition, the less it hardens in creep. It was established that softening in creep of steel with a moderate yield strength is caused primarily by aging and with a high yield strength by pore formation.

  5. Work-Hardening Induced Tensile Ductility of Bulk Metallic Glasses via High-Pressure Torsion

    NASA Astrophysics Data System (ADS)

    Joo, Soo-Hyun; Pi, Dong-Hai; Setyawan, Albertus Deny Heri; Kato, Hidemi; Janecek, Milos; Kim, Yong Chan; Lee, Sunghak; Kim, Hyoung Seop

    2015-04-01

    The mechanical properties of engineering materials are key for ensuring safety and reliability. However, the plastic deformation of BMGs is confined to narrow regions in shear bands, which usually result in limited ductilities and catastrophic failures at low homologous temperatures. The quasi-brittle failure and lack of tensile ductility undercut the potential applications of BMGs. In this report, we present clear tensile ductility in a Zr-based BMG via a high-pressure torsion (HPT) process. Enhanced tensile ductility and work-hardening behavior after the HPT process were investigated, focusing on the microstructure, particularly the changed free volume, which affects deformation mechanisms (i.e., initiation, propagation, and obstruction of shear bands). Our results provide insights into the basic functions of hydrostatic pressure and shear strain in the microstructure and mechanical properties of HPT-processed BMGs.

  6. Work-hardening induced tensile ductility of bulk metallic glasses via high-pressure torsion.

    PubMed

    Joo, Soo-Hyun; Pi, Dong-Hai; Setyawan, Albertus Deny Heri; Kato, Hidemi; Janecek, Milos; Kim, Yong Chan; Lee, Sunghak; Kim, Hyoung Seop

    2015-04-23

    The mechanical properties of engineering materials are key for ensuring safety and reliability. However, the plastic deformation of BMGs is confined to narrow regions in shear bands, which usually result in limited ductilities and catastrophic failures at low homologous temperatures. The quasi-brittle failure and lack of tensile ductility undercut the potential applications of BMGs. In this report, we present clear tensile ductility in a Zr-based BMG via a high-pressure torsion (HPT) process. Enhanced tensile ductility and work-hardening behavior after the HPT process were investigated, focusing on the microstructure, particularly the changed free volume, which affects deformation mechanisms (i.e., initiation, propagation, and obstruction of shear bands). Our results provide insights into the basic functions of hydrostatic pressure and shear strain in the microstructure and mechanical properties of HPT-processed BMGs.

  7. 'Work-Hardenable' Ductile Bulk Metallic Glass

    SciTech Connect

    Das, Jayanta; Eckert, Juergen; Tang Meibo; Wang Weihua; Kim, Ki Buem; Baier, Falko; Theissmann, Ralf

    2005-05-27

    Usually, monolithic bulk metallic glasses undergo inhomogeneous plastic deformation and exhibit poor ductility (<1%) at room temperature. We present a new class of bulk metallic glass, which exhibits high strength of up to 2265 MPa together with extensive 'work hardening' and large ductility of 18%. Significant increase in the flow stress was observed during deformation. The 'work-hardening' capability and ductility of this class of metallic glass is attributed to a unique structure correlated with atomic-scale inhomogeneity, leading to an inherent capability of extensive shear band formation, interactions, and multiplication of shear bands.

  8. Yield strength of molybdenum at high pressures.

    PubMed

    Jing, Qiumin; Bi, Yan; Wu, Qiang; Jing, Fuqian; Wang, Zhigang; Xu, Jian; Jiang, Sheng

    2007-07-01

    In the diamond anvil cell technology, the pressure gradient approach is one of the three major methods in determining the yield strength for various materials at high pressures. In the present work, by in situ measuring the thickness of the sample foil, we have improved the traditional technique in this method. Based on this modification, the yield strength of molybdenum at pressures has been measured. Our main experimental conclusions are as follows: (1) The measured yield strength data for three samples with different initial thickness (100, 250, and 500 microm) are in good agreement above a peak pressure of 10 GPa. (2) The measured yield strength can be fitted into a linear formula Y=0.48(+/-0.19)+0.14(+/-0.01)P (Y and P denote the yield strength and local pressure, respectively, both of them are in gigapascals) in the local pressure range of 8-21 GPa. This result is in good agreement with both Y=0.46+0.13P determined in the pressure range of 5-24 GPa measured by the radial x-ray diffraction technique and the previous shock wave data below 10 GPa. (3) The zero-pressure yield strength of Mo is 0.5 GPa when we extrapolate our experimental data into the ambient pressure. It is close to the tensile strength of 0.7 GPa determined by Bridgman [Phys. Rev. 48, 825 (1934)] previously. The modified method described in this article therefore provides the confidence in determination of the yield strength at high pressures. PMID:17672772

  9. Effect of Strain-Induced Age Hardening on Yield Strength Improvement in Ferrite-Austenite Duplex Lightweight Steels

    NASA Astrophysics Data System (ADS)

    Song, Hyejin; Lee, Seok Gyu; Sohn, Seok Su; Kwak, Jai-Hyun; Lee, Sunghak

    2016-11-01

    Ferrite-austenite lightweight steels showing TRansformation-induced plasticity were developed by varying the aging temperature with or without prestraining, and their effects on tensile properties were investigated in relation with microstructural evolution of carbide formation. The aged steels contained austenite, pearlite, and martensite in the ferrite matrix, and the austenite volume fraction decreased with the increasing aging temperature because some austenite grains decomposed to pearlites. This austenite decomposition to pearlite was favorable for the improvement of yield strength, but negatively influenced overall tensile properties. The prestraining promoted the austenite decomposition by a diffusion-controlled phase transformation, and changed the morphology of the cementite from a long lamellar shape to a densely agglomerated particle shape. In order to obtain the large increase in yield strength as well as excellent combination of strength and ductility, the strain-induced aging treatment, i.e., prestraining followed by aging, is important like in the prestrained and 673 K (400 °C)-aged steel. This large increase in yield strength, in spite of a reduction of elongation (65 to 43 pct), was basically attributed to an appropriate amount of decomposition of austenite to pearlite ( e.g., 4 vol pct), while having sufficient austenite to martensite transformation ( e.g., 14.5 vol pct martensite).

  10. Development of high strength high toughness third generation advanced high strength steels

    NASA Astrophysics Data System (ADS)

    Martis, Codrick John

    Third generation advanced high strength steels (AHSS's) are emerging as very important engineering materials for structural applications. These steels have high specific strength and thus will contribute significantly to weight reduction in automotive and other structural component. In this investigation two such low carbon low alloy steels (LCLA) with high silicon content (1.6-2wt %) has been developed. These two steel alloys were subjected to single step and two step austempering in the temperature range of 260-399°C to obtain desired microstructures and mechanical properties. Austempering heat treatment was carried out for 2 hours in a molten salt bath. The microstructures were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy and optical metallography. Quantitative analysis was carried out by image analysis technique. The effect of austempering temperature on the mechanical properties of these two alloys was examined. The influence of microstructures on the mechanical properties of alloys was also studied. Austempering heat treatment resulted in fine carbide free bainitic ferrite and high carbon austenite microstructure in the samples austempered above Ms temperature, whereas tempered martensite and austenite microstructure was obtained in samples austempered below Ms temperature. Yield strength, tensile strength and fracture toughness were found to increase as the austempering temperature decreases, whereas ductility increases as the austempering temperature increases. Tensile strength in the range of 1276MPa -1658 MPa and the fracture toughness in the range of 80-141MPa√m were obtained in these two steels. Volume fractions of different phases present and their lath sizes are related to the mechanical properties. Austempered samples consisting of mixed microstructure of bainitic ferrite and tempered martensite phases resulted in the exceptional combination of strength and toughness.

  11. Method for producing high dielectric strength microvalves

    DOEpatents

    Kirby, Brian J.; Reichmuth, David S.; Shepodd, Timothy J.

    2006-04-04

    A microvalve having a cast-in-place and lithographically shaped mobile, polymer monolith for fluid flow control in microfluidic devices and method of manufacture. The microvalve contains a porous fluorinated polymer monolithic element whose pores are filled with an electrically insulating, high dielectric strength fluid, typically a perfluorinated liquid. This combination provides a microvalve that combines high dielectric strength with extremely low electrical conductivity. These microvalves have been shown to have resistivities of at least 100 G.OMEGA. and are compatible with solvents such as water at a pH between 2.7 and 9.0, 1-1 propanol, acetonitrile, and acetone.

  12. Laser beam welding of new ultra-high strength and supra-ductile steels

    NASA Astrophysics Data System (ADS)

    Dahmen, Martin

    2015-03-01

    Ultra-high strength and supra-ductile are entering fields of new applications. Those materials are excellent candidates for modern light-weight construction and functional integration. As ultra-high strength steels the stainless martensitic grade 1.4034 and the bainitic steel UNS 53835 are investigated. For the supra-ductile steels stand two high austenitic steels with 18 and 28 % manganese. As there are no processing windows an approach from the metallurgical base on is required. Adjusting the weld microstructure the Q+P and the QT steels require weld heat treatment. The HSD steel is weldable without. Due to their applications the ultra-high strength steels are welded in as-rolled and strengthened condition. Also the reaction of the weld on hot stamping is reflected for the martensitic grades. The supra-ductile steels are welded as solution annealed and work hardened by 50%. The results show the general suitability for laser beam welding.

  13. An Anisotropic Hardening Model for Springback Prediction

    NASA Astrophysics Data System (ADS)

    Zeng, Danielle; Xia, Z. Cedric

    2005-08-01

    As more Advanced High-Strength Steels (AHSS) are heavily used for automotive body structures and closures panels, accurate springback prediction for these components becomes more challenging because of their rapid hardening characteristics and ability to sustain even higher stresses. In this paper, a modified Mroz hardening model is proposed to capture realistic Bauschinger effect at reverse loading, such as when material passes through die radii or drawbead during sheet metal forming process. This model accounts for material anisotropic yield surface and nonlinear isotropic/kinematic hardening behavior. Material tension/compression test data are used to accurately represent Bauschinger effect. The effectiveness of the model is demonstrated by comparison of numerical and experimental springback results for a DP600 straight U-channel test.

  14. Springback analysis of ultra high strength steel

    NASA Astrophysics Data System (ADS)

    Tenma, Kenji; Kina, Futoshi; Suzuki, Wataru

    2013-12-01

    It is an inevitable trend in the automotive industry to apply more and more high strength steels and even ultra-high strength steels. Even though these materials are more difficult to process the development time of forming tools must be reduced. In order to keep the development time under control, simulation tools are used to verify the forming process in advance. At Aoi Machine Industry a project has been executed to accurately simulate springback of ultra-high strength steels in order to reduce the tool tryout time. In the first phase of the project the simulation settings were optimized based on B-Pillar model A made of Dual Phase 980. In the second phase, it was verified with B-Pillar model B whether these simulation settings were usable as general setting. Results showed that with the right settings it is very well possible to accurately simulate springback of ultra-high strength steels. In the third phase the project the stamping of a B-Pillar of Dual Phase 1180 was studied.

  15. High strength composites evaluation. Final report

    SciTech Connect

    Marten, S.M.

    1992-02-01

    A high-strength, thick-section, graphite/epoxy composite was identified. The purpose of this development effort was to evaluate candidate materials and provide LANL with engineering properties. Eight candidate materials (Samples 1000, 1100, 1200, 1300, 1400, 1500, 1600, and 1700) were chosen for evaluation. The Sample 1700 thermoplastic material was the strongest overall.

  16. Bulk metallic glass composite with good tensile ductility, high strength and large elastic strain limit

    PubMed Central

    Wu, Fu-Fa; Chan, K. C.; Jiang, Song-Shan; Chen, Shun-Hua; Wang, Gang

    2014-01-01

    Bulk metallic glasses exhibit high strength and large elastic strain limit but have no tensile ductility. However, bulk metallic glass composites reinforced by in-situ dendrites possess significantly improved toughness but at the expense of high strength and large elastic strain limit. Here, we report a bulk metallic glass composite with strong strain-hardening capability and large elastic strain limit. It was found that, by plastic predeformation, the bulk metallic glass composite can exhibit both a large elastic strain limit and high strength under tension. These unique elastic mechanical properties are attributed to the reversible B2↔B19′ phase transformation and the plastic-predeformation-induced complicated stress state in the metallic glass matrix and the second phase. These findings are significant for the design and application of bulk metallic glass composites with excellent mechanical properties. PMID:24931632

  17. Induction Hardening vs Conventional Hardening of a Heat Treatable Steel

    NASA Astrophysics Data System (ADS)

    Sackl, Stephanie; Leitner, Harald; Zuber, Michael; Clemens, Helmut; Primig, Sophie

    2014-11-01

    This study focuses on the comparison of mechanical and microstructural properties of induction and conventionally heat-treated steels in the as-quenched state. The investigated steel is a heat treatable 42CrMo4 steel. In order to characterize the mechanical properties, tensile tests and Vickers hardness tests are performed. The yield strength and hardness of the induction hardened condition turn out to be slightly lower compared to the conventionally hardened one. Light optical and scanning electron microscopy show no differences in the martensitic structure of the induction and conventionally hardened condition. However, electron back scatter diffraction investigations reveal a smaller block size within the conventionally hardened specimen. Carbon mappings by electron probe micro analysis show a homogenous carbon concentration in the conventionally hardened and a non-uniform distribution in the induction-hardened case. The segregation of the carbon exhibits line-type features in the induction hardened condition, lowering the total amount of carbon in the matrix. Therefore, the carbon content in the matrix of the conventionally hardened condition is slightly higher, which causes a smaller block size. The smaller block size is believed to be the reason for the higher hardness and yield strength.

  18. Improvement in surface fatigue life of hardened gears by high-intensity shot peening

    NASA Technical Reports Server (NTRS)

    Townsend, Dennis P.

    1992-01-01

    Two groups of carburized, hardened, and ground spur gears that were manufactured from the same heat vacuum induction melted vacuum arc melted (VIM VAR) AISI 9310 steel were endurance tested for surface fatigue. Both groups were manufactured with a standard ground 16 rms surface finish. One group was subjected to a shot peening (SP) intensity of 7 to 9A, and the second group was subjected to a SP intensity of 15 to 17A. All gears were honed after SP to a surface finish of 16 rms. The gear pitch diameter was 8.89 cm. Test conditions were a maximum Hertz stress of 1.71 GPa, a gear temperature of 350 K, and a speed of 10000 rpm. The lubricant used for the tests was a synthetic paraffinic oil with an additive package. The following results were obtained: The 10 pct. surface fatigue (pitting) life of the high intensity (15 to 17A) SPed gears was 2.15 times that of the medium intensity (7 to 9A) SPed gears, the same as that calculated from measured residual stress at a depth of 127 microns. The measured residual stress for the high intensity SPed gears was 57 pct. higher than that for the medium intensity SPed gears at a depth of 127 microns and 540 pct. higher at a depth of 51 microns.

  19. High-strength mineralized collagen artificial bone

    NASA Astrophysics Data System (ADS)

    Qiu, Zhi-Ye; Tao, Chun-Sheng; Cui, Helen; Wang, Chang-Ming; Cui, Fu-Zhai

    2014-03-01

    Mineralized collagen (MC) is a biomimetic material that mimics natural bone matrix in terms of both chemical composition and microstructure. The biomimetic MC possesses good biocompatibility and osteogenic activity, and is capable of guiding bone regeneration as being used for bone defect repair. However, mechanical strength of existing MC artificial bone is too low to provide effective support at human load-bearing sites, so it can only be used for the repair at non-load-bearing sites, such as bone defect filling, bone graft augmentation, and so on. In the present study, a high strength MC artificial bone material was developed by using collagen as the template for the biomimetic mineralization of the calcium phosphate, and then followed by a cold compression molding process with a certain pressure. The appearance and density of the dense MC were similar to those of natural cortical bone, and the phase composition was in conformity with that of animal's cortical bone demonstrated by XRD. Mechanical properties were tested and results showed that the compressive strength was comparable to human cortical bone, while the compressive modulus was as low as human cancellous bone. Such high strength was able to provide effective mechanical support for bone defect repair at human load-bearing sites, and the low compressive modulus can help avoid stress shielding in the application of bone regeneration. Both in vitro cell experiments and in vivo implantation assay demonstrated good biocompatibility of the material, and in vivo stability evaluation indicated that this high-strength MC artificial bone could provide long-term effective mechanical support at human load-bearing sites.

  20. Making High-Tensile-Strength Amalgam Components

    NASA Technical Reports Server (NTRS)

    Grugel, Richard

    2008-01-01

    Structural components made of amalgams can be made to have tensile strengths much greater than previously known to be possible. Amalgams, perhaps best known for their use in dental fillings, have several useful attributes, including room-temperature fabrication, corrosion resistance, dimensional stability, and high compressive strength. However, the range of applications of amalgams has been limited by their very small tensile strengths. Now, it has been discovered that the tensile strength of an amalgam depends critically on the sizes and shapes of the particles from which it is made and, consequently, the tensile strength can be greatly increased through suitable choice of the particles. Heretofore, the powder particles used to make amalgams have been, variously, in the form of micron-sized spheroids or flakes. The tensile reinforcement contributed by the spheroids and flakes is minimal because fracture paths simply go around these particles. However, if spheroids or flakes are replaced by strands having greater lengths, then tensile reinforcement can be increased significantly. The feasibility of this concept was shown in an experiment in which electrical copper wires, serving as demonstration substitutes for copper powder particles, were triturated with gallium by use of a mortar and pestle and the resulting amalgam was compressed into a mold. The tensile strength of the amalgam specimen was then measured and found to be greater than 10(exp 4) psi (greater than about 69 MPa). Much remains to be done to optimize the properties of amalgams for various applications through suitable choice of starting constituents and modification of the trituration and molding processes. The choice of wire size and composition are expected to be especially important. Perusal of phase diagrams of metal mixtures could give insight that would enable choices of solid and liquid metal constituents. Finally, whereas heretofore, only binary alloys have been considered for amalgams

  1. Tailored work hardening descriptions in simulation of sheet metal forming

    NASA Astrophysics Data System (ADS)

    Vegter, Henk; Mulder, Hans.; van Liempt, Peter; Heijne, Jan

    2013-12-01

    In the previous decades much attention has been given on an accurate material description, especially for simulations at the design stage of new models in the automotive industry. Improvements lead to shorter design times and a better tailored use of material. It also contributed to the design and optimization of new materials. The current description of plastic material behaviour in simulation models of sheet metal forming is covered by a hardening curve and a yield surface. In this paper the focus will be on modelling of work hardening for advanced high strength steels considering the requirements of present applications. Nowadays work hardening models need to include the effect of hard phases in a soft matrix and the effect of strain rate and temperature on work hardening. Most material tests to characterize work hardening are only applicable to low strains whereas many practical applications require hardening data at relatively high strains. Therefore, physically based hardening descriptions are needed allowing reliable extensions to high strain values.

  2. High-Strength Bolt Corrosion Fatigue Life Model and Application

    PubMed Central

    Hui-li, Wang; Si-feng, Qin

    2014-01-01

    The corrosion fatigue performance of high-strength bolt was studied. Based on the fracture mechanics theory and the Gerberich-Chen formula, the high-strength bolt corrosion fracture crack model and the fatigue life model were established. The high-strength bolt crack depth and the fatigue life under corrosion environment were quantitatively analyzed. The factors affecting high-strength bolt corrosion fatigue life were discussed. The result showed that the high-strength bolt corrosion fracture biggest crack depth reduces along with the material yield strength and the applied stress increases. The material yield strength was the major factor. And the high-strength bolt corrosion fatigue life reduced along with the increase of material strength, the applied stress or stress amplitude. The stress amplitude influenced the most, and the material yield strength influenced the least. Low bolt strength and a low stress amplitude level could extend high-strength bolt corrosion fatigue life. PMID:25152916

  3. High-strength bolt corrosion fatigue life model and application.

    PubMed

    Hui-li, Wang; Si-feng, Qin

    2014-01-01

    The corrosion fatigue performance of high-strength bolt was studied. Based on the fracture mechanics theory and the Gerberich-Chen formula, the high-strength bolt corrosion fracture crack model and the fatigue life model were established. The high-strength bolt crack depth and the fatigue life under corrosion environment were quantitatively analyzed. The factors affecting high-strength bolt corrosion fatigue life were discussed. The result showed that the high-strength bolt corrosion fracture biggest crack depth reduces along with the material yield strength and the applied stress increases. The material yield strength was the major factor. And the high-strength bolt corrosion fatigue life reduced along with the increase of material strength, the applied stress or stress amplitude. The stress amplitude influenced the most, and the material yield strength influenced the least. Low bolt strength and a low stress amplitude level could extend high-strength bolt corrosion fatigue life.

  4. High-throughput design of low-activation, high-strength creep-resistant steels for nuclear-reactor applications

    NASA Astrophysics Data System (ADS)

    Lu, Qi; van der Zwaag, Sybrand; Xu, Wei

    2016-02-01

    Reduced-activation ferritic/martensitic steels are prime candidate materials for structural applications in nuclear power reactors. However, their creep strength is much lower than that of creep-resistant steel developed for conventional fossil-fired power plants as alloying elements with a high neutron activation cannot be used. To improve the creep strength and to maintain a low activation, a high-throughput computational alloy design model coupling thermodynamics, precipitate-coarsening kinetics and an optimization genetic algorithm, is developed. Twelve relevant alloying elements with either low or high activation are considered simultaneously. The activity levels at 0-10 year after the end of irradiation are taken as optimization parameter. The creep-strength values (after exposure for 10 years at 650 °C) are estimated on the basis of the solid-solution strengthening and the precipitation hardening (taking into account precipitate coarsening). Potential alloy compositions leading to a high austenite fraction or a high percentage of undesirable second phase particles are rejected automatically in the optimization cycle. The newly identified alloys have a much higher precipitation hardening and solid-solution strengthening at the same activity level as existing reduced-activation ferritic/martensitic steels.

  5. Two-surface plasticity Model and Its Application to Spring-back Simulation of Automotive Advanced High Strength Steel Sheets

    NASA Astrophysics Data System (ADS)

    Park, Taejoon; Seok, Dong-Yoon; Lee, Chul-Hwan; Noma, Nobuyasu; Kuwabara, Toshihiko; Stoughton, Thomas B.; Chung, Kwansoo

    2011-08-01

    A two-surface isotropic-kinematic hardening law was developed based on a two-surface plasticity model previously proposed by Lee et al., (2007, Int. J. Plast. 23, 1189-1212). In order to properly represent the Bauschinger and transient behaviors as well as permanent softening during reverse loading with various pre-strains, both the inner yield surface and the outer bounding surface expand (isotropic hardening) and translate (kinematic hardening) in this two-surface model. As for the permanent softening, both the isotropic hardening and the kinematic hardening evolution of the outer bounding surface were modified by introducing softening parameters. The numerical formulation was also developed based on the incremental plasticity theory and the developed constitutive law was implemented into the commercial finite element program, ABAQUS/Explicit and ABAQUS/Standard using the user-defined material subroutines. In this work, a dual phase (DP) steel was considered as an advanced high strength steel sheet and uni-axial tension tests and uni-axial tension-compression-tension tests were performed for the characterization of the material property. For a validation purpose, the developed two-surface plasticity model was applied to the 2-D draw bending test proposed as a benchmark problem of the NUMISHEET 2011 conference and successfully validated with experiments.

  6. Understanding the Behavior of Advanced High-Strength Steels Using Atom Probe Tomography

    NASA Astrophysics Data System (ADS)

    Pereloma, Elena; Beladi, Hossein; Zhang, Laichang; Timokhina, Ilana

    2012-11-01

    The key evidence for understanding the mechanical behavior of advanced high strength steels was provided by atom probe tomography (APT). Chemical overstabilization of retained austenite (RA) leading to the limited transformation-induced plasticity (TRIP) effect was deemed to be the main factor responsible for the low ductility of nanostructured bainitic steel. Appearance of the yield point on the stress-strain curve of prestrained and bake-hardened transformation-induced plasticity steel is due to the unlocking from weak carbon atmospheres of newly formed during prestraining dislocations.

  7. High-strength iron aluminide alloys

    SciTech Connect

    McKamey, C.G.; Maziasz, P.J.

    1996-06-01

    Past studies have shown that binary Fe{sub 3}Al possesses low creep-rupture strength compared to many other alloys, with creep-rupture lives of less than 5 h being reported for tests conducted at 593{degrees}C and 207 MPa. The combination of poor creep resistance and low room-temperature tensile ductility due to a susceptibility to environmentally-induced dynamic hydrogen embrittlement has limited use of these alloys for structural applications despite their excellent corrosion properties. With regard to the ductility problem, alloy development efforts have produced significant improvements, with ductilities of 10-20% and tensile yield strengths as high as 500 MPa being reported. Likewise, initial improvements in creep resistance have been realized through small additions of Mo, Nb, and Zr.

  8. Thermophilic anaerobic digestion of high strength wastewaters

    SciTech Connect

    Wiegant, W.M.; Claassen, J.A.; Lettinga, G.

    1985-09-01

    Investigations on the thermophilic anaerobic treatment of high-strength wastewaters (14-65 kg COD/mT) are presented. Vinasse, the wastewater of alcohol distilleries, was used as an example of such wastewaters. Semicontinuously fed digestion experiments at high retention times revealed that the effluent quality of digestion at 55C is comparable with that at 30C at similar loading rates. The amount of methane formed per kilogram of vinasse drops almost linearly with increasing vinasse concentrations. The treatment of vinasse was also investigated using upflow anaerobic sludge blanket (UASB) reactors.

  9. HIGH STRENGTH CONTROL RODS FOR NEUTRONIC REACTORS

    DOEpatents

    Lustman, B.; Losco, E.F.; Cohen, I.

    1961-07-11

    Nuclear reactor control rods comprised of highly compressed and sintered finely divided metal alloy panticles and fine metal oxide panticles substantially uniformly distributed theretbrough are described. The metal alloy consists essentially of silver, indium, cadmium, tin, and aluminum, the amount of each being present in centain percentages by weight. The oxide particles are metal oxides of the metal alloy composition, the amount of oxygen being present in certain percentages by weight and all the oxygen present being substantially in the form of metal oxide. This control rod is characterized by its high strength and resistance to creep at elevated temperatures.

  10. High-strength iron aluminide alloys

    SciTech Connect

    McKamey, C.G.; Marrero-Santos, Y.; Maziasz, P.J.

    1995-06-01

    Past studies have shown that binary Fe{sub 3}Al possesses low creep-rupture strength compared to many other alloys, with creep-rupture lives of less than 5 h being reported for tests conducted at 593{degrees}C and 207 MPa. The combination of poor creep resistance and low room-temperature tensile density due to a susceptibility to environmentally-induced dynamic hydrogen embrittlement has limited use of these alloys for structural applications, despite their excellent corrosion properties. Improvements in room temperature tensile ductility have been realized mainly through alloying effects, changes in thermomechanical processing to control microstructure, and by control of the specimen`s surface condition. Ductilities of 10-20% and tensile yield strengths as high as 500 MPa have been reported. In terms of creep-rupture strength, small additions of Mo, Nb, and Zr have produced significant improvements, but at the expense of weldability and room-temperature tensile ductility. Recently an alloy containing these additions, designated FA-180, was shown to exhibit a creep-rupture life of over 2000 h after a heat treatment of 1 h at 1150{degrees}C. This study presents the results of creep-rupture tests at various test temperatures and stresses and discusses the results as part of our effort to understand the strengthening mechanisms involved with heat treatment at 1150{degrees}C.

  11. RHOBOT: Radiation hardened robotics

    SciTech Connect

    Bennett, P.C.; Posey, L.D.

    1997-10-01

    A survey of robotic applications in radioactive environments has been conducted, and analysis of robotic system components and their response to the varying types and strengths of radiation has been completed. Two specific robotic systems for accident recovery and nuclear fuel movement have been analyzed in detail for radiation hardness. Finally, a general design approach for radiation-hardened robotics systems has been developed and is presented. This report completes this project which was funded under the Laboratory Directed Research and Development program.

  12. The effect of hydrogen on strain hardening and fracture mechanism of high-nitrogen austenitic steel

    NASA Astrophysics Data System (ADS)

    Maier, G. G.; Astafurova, E. G.; Melnikov, E. V.; Moskvina, V. A.; Vojtsik, V. F.; Galchenko, N. K.; Zakharov, G. N.

    2016-07-01

    High-nitrogen austenitic steels are perspective materials for an electron-beam welding and for producing of wear-resistant coatings, which can be used for application in aggressive atmospheres. The tensile behavior and fracture mechanism of high-nitrogen austenitic steel Fe-20Cr-22Mn-1.5V-0.2C-0.6N (in wt.%) after electrochemical hydrogen charging for 2, 10 and 40 hours have been investigated. Hydrogenation of steel provides a loss of yield strength, uniform elongation and tensile strength. The degradation of tensile properties becomes stronger with increase in charging duration - it occurs more intensive in specimens hydrogenated for 40 hours as compared to ones charged for 2-10 hours. Fracture analysis reveals a hydrogen-induced formation of brittle surface layers up to 6 μm thick after 40 hours of saturation. Hydrogenation changes fracture mode of steel from mixed intergranular-transgranular to mainly transgranular one.

  13. Application of steel 40Kh surface hardened by high-frequency currents in the production of gate valve parts

    SciTech Connect

    Veliev, T.K.; Arifulin, R.K.; Fataliev, N.S.; Safarov, R.S.

    1986-09-01

    Bench tests were performed to determine the change in roughness, planeness, and hardness of the sealing surfaces of parts of gate valves made with steel 40Kh surface-hardened by high-frequency currents (HFC). Most parts of the gate valves for oil wells are now made of steel 38Kh2MYuA containing molybdenum. It was of interest to conduct tests to find another steel (40Kh) with less precious alloying elements and to increase the hardness of the sealing surfaces. The tests showed that steel 40Kh with HFC surface hardening may be recommended for gate parts of straight-through gate valves with specific contact pressure of up to 70 MPa. The torque for controlling the gate must be 0.8-1kN. Tests were also conducted on an experimental batch of Christmas trees and tubing heads; those results are presented.

  14. Protective claddings for high strength chromium alloys

    NASA Technical Reports Server (NTRS)

    Collins, J. F.

    1971-01-01

    The application of a Cr-Y-Hf-Th alloy as a protective cladding for a high strength chromium alloy was investigated for its effectiveness in inhibiting nitrogen embrittlement of a core alloy. Cladding was accomplished by a combination of hot gas pressure bonding and roll cladding techniques. Based on bend DBTT, the cladding alloy was effective in inhibiting nitrogen embrittlement of the chromium core alloy for up to 720 ks (200hours) in air at 1422 K (2100 F). A significant increase in the bend DBTT occurred with longer time exposures at 1422 K or short time exposures at 1589 K (2400 F).

  15. Constitutive Modeling of Hot Deformation Behavior of High-Strength Armor Steel

    NASA Astrophysics Data System (ADS)

    Bobbili, Ravindranadh; Madhu, Vemuri

    2016-05-01

    The hot isothermal compression tests of high-strength armor steel under a wide range of deformation temperatures (1100-1250 °C) and strain rates of (0.001-1/s) were performed. Based on the experimental data, constitutive models were established using the original Johnson-Cook (JC) model, modified JC model, and strain-compensated Arrhenius model, respectively. The modified JC model considers the coupled effects of strain hardening, strain rate hardening, and thermal softening. Moreover, the prediction accuracy of these developed models was determined by estimating the correlation coefficient ( R) and average absolute relative error (AARE). The results demonstrate that the flow behavior of high-strength armor steel is considerably influenced by the strain rate and temperature. The original JC model is inadequate to provide good description on the flow stress at evaluated temperatures. The modified JC model and strain-compensated Arrhenius model significantly enhance the predictability. It is also observed from the microstructure study that at low strain rates (0.001-0.01/s) and high temperatures (1200-1250 °C), a typical dynamic recrystallization (DRX) occurs.

  16. Optimization of Process Parameters for High Efficiency Laser Forming of Advanced High Strength Steels within Metallurgical Constraints

    NASA Astrophysics Data System (ADS)

    Sheikholeslami, Ghazal; Griffiths, Jonathan; Dearden, Geoff; Edwardson, Stuart P.

    Laser forming (LF) has been shown to be a viable alternative to form automotive grade advanced high strength steels (AHSS). Due to their high strength, heat sensitivity and low conventional formability show early fractures, larger springback, batch-to-batch inconsistency and high tool wear. In this paper, optimisation of the LF process parameters has been conducted to further understand the impact of a surface heat treatment on DP1000. A FE numerical simulation has been developed to analyse the dynamic thermo-mechanical effects. This has been verified against empirical data. The goal of the optimisation has been to develop a usable process window for the LF of AHSS within strict metallurgical constraints. Results indicate it is possible to LF this material, however a complex relationship has been found between the generation and maintenance of hardness values in the heated zone. A laser surface hardening effect has been observed that could be beneficial to the efficiency of the process.

  17. High strength ferritic alloy-D53

    DOEpatents

    Hagel, William C.; Smidt, Frederick A.; Korenko, Michael K.

    1977-01-01

    A high strength ferritic alloy is described having from about 0.2% to about 0.8% by weight nickel, from about 2.5% to about 3.6% by weight chromium, from about 2.5% to about 3.5% by weight molybdenum, from about 0.1% to about 0.5% by weight vanadium, from about 0.1% to about 0.5% by weight silicon, from about 0.1% to about 0.6% by weight manganese, from about 0.12% to about 0.20% by weight carbon, from about 0.02% to about 0.1% by weight boron, a maximum of about 0.05% by weight nitrogen, a maximum of about 0.02% by weight phosphorous, a maximum of about 0.02% by weight sulfur, and the balance iron.

  18. High strength air-dried aerogels

    SciTech Connect

    Coronado, Paul R.; Satcher, Jr., Joe H.

    2012-11-06

    A method for the preparation of high strength air-dried organic aerogels. The method involves the sol-gel polymerization of organic gel precursors, such as resorcinol with formaldehyde (RF) in aqueous solvents with R/C ratios greater than about 1000 and R/F ratios less than about 1:2.1. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be air dried at ambient temperatures and pressures. The method significantly reduces the time and/or energy required to produce a dried aerogel compared to conventional methods using either supercritical solvent extraction. The air dried gel exhibits typically less than 5% shrinkage.

  19. Surface Fatigue Resistance with Induction Hardening

    NASA Technical Reports Server (NTRS)

    Townsend, Dennis; Turza, Alan; Chapman, Mike

    1996-01-01

    Induction hardening has been used for some years to harden the surface and improve the strength and service life of gears and other components. Many applications that employ induction hardening require a relatively long time to finish the hardening process and controlling the hardness of the surface layer and its depth often was a problem. Other surface hardening methods, ie., carbonizing, take a very long time and tend to cause deformations of the toothing, whose elimination requires supplementary finishing work. In double-frequency induction hardening, one uses a low frequency for the preheating of the toothed wheel and a much higher frequency for the purpose of rapidly heating the surface by way of surface hardening.

  20. Electrostatic precipitator having high strength discharge electrode

    SciTech Connect

    Bakke, E.; Willett, H.P.

    1983-06-21

    There is disclosed an electrostatic precipitator with a discharge electrode having dimensional and configuration characteristics which provide high field strength and high current density particularly in a wet electrostatic precipitator. The round cylindrical collector tube of length (L) and with an inner diameter (D) has a coaxially positioned discharge electrode having an electrode supporting mast of a diameter from 0.25 to 40 D with an electrically conducting closed screw fli secured to the mast. The screw flight has an overall diameter (D) of from 0.33 to 0.67 D with a pitch of from d-d/2 to d-d and an overall length of from one screw revolution to l-(D-d), preferably one-half L or less and most preferably one to two revolutions. The short screw flight is economical and readily adjusted. The screw flight has a thickness of from about 0.05 to 15 inch and has a symmetrically curved outer edge. Collector tube is flared at its lower end to direct water away from the electrode mast as the water is discharged from the tube. The discharge electrode is supported from above and centered by means of adjustable tie rods at its lower end.

  1. Strength analysis of laser welded lap joint for ultra high strength steel

    NASA Astrophysics Data System (ADS)

    Jeong, Young Cheol; Kim, Cheol Hee; Cho, Young Tae; Jung, Yoon Gyo

    2013-12-01

    Several industries including the automotive industry have recently applied the process of welding high strength steel. High strength steel is steel that is harder than normal high strength steel, making it much stronger and stiffer. HSS can be formed in pieces that can be up to 10 to 15 percent thinner than normal steel without sacrificing strength, which enables weight reduction and improved fuel economy. Furthermore, HSS can be formed into complex shapes that can be welded into structural areas. This study is based on previous experiments and is aimed at establishing the stress distribution for laser welded high strength steel. Research on the stress distribution for laser welded high strength steel is conducted by using Solid Works, a program that analyzes the stress of a virtual model. In conclusion, we found that the stress distribution is changed depending on the shape of welded lap joint. In addition, the Influence of the stress distribution on welded high strength steel can be used to standard for high energy welding of high strength steel, and we can also predict the region in welded high strength steel that may cracked.

  2. Process design of press hardening with gradient material property influence

    SciTech Connect

    Neugebauer, R.; Schieck, F.; Rautenstrauch, A.

    2011-05-04

    Press hardening is currently used in the production of automotive structures that require very high strength and controlled deformation during crash tests. Press hardening can achieve significant reductions of sheet thickness at constant strength and is therefore a promising technology for the production of lightweight and energy-efficient automobiles. The manganese-boron steel 22MnB5 have been implemented in sheet press hardening owing to their excellent hot formability, high hardenability, and good temperability even at low cooling rates. However, press-hardened components have shown poor ductility and cracking at relatively small strains. A possible solution to this problem is a selective increase of steel sheet ductility by press hardening process design in areas where the component is required to deform plastically during crash tests. To this end, process designers require information about microstructure and mechanical properties as a function of the wide spectrum of cooling rates and sequences and austenitizing treatment conditions that can be encountered in production environments. In the present work, a Continuous Cooling Transformation (CCT) diagram with corresponding material properties of sheet steel 22MnB5 was determined for a wide spectrum of cooling rates. Heating and cooling programs were conducted in a quenching dilatometer. Motivated by the importance of residual elasticity in crash test performance, this property was measured using a micro-bending test and the results were integrated into the CCT diagrams to complement the hardness testing results. This information is essential for the process design of press hardening of sheet components with gradient material properties.

  3. Direct observation of Lomer-Cottrell locks during strain hardening in nanocrystalline nickel by in situ TEM.

    PubMed

    Lee, Joon Hwan; Holland, Troy B; Mukherjee, Amiya K; Zhang, Xinghang; Wang, Haiyan

    2013-01-01

    Strain hardening capability is critical for metallic materials to achieve high ductility during plastic deformation. A majority of nanocrystalline metals, however, have inherently low work hardening capability with few exceptions. Interpretations on work hardening mechanisms in nanocrystalline metals are still controversial due to the lack of in situ experimental evidence. Here we report, by using an in situ transmission electron microscope nanoindentation tool, the direct observation of dynamic work hardening event in nanocrystalline nickel. During strain hardening stage, abundant Lomer-Cottrell (L-C) locks formed both within nanograins and against twin boundaries. Two major mechanisms were identified during interactions between L-C locks and twin boundaries. Quantitative nanoindentation experiments recorded show an increase of yield strength from 1.64 to 2.29 GPa during multiple loading-unloading cycles. This study provides both the evidence to explain the roots of work hardening at small length scales and the insight for future design of ductile nanocrystalline metals.

  4. Development of a Press-Hardened Steel Suitable for Thin Slab Direct Rolling Processing

    NASA Astrophysics Data System (ADS)

    Lee, Jewoong; De Cooman, Bruno C.

    2015-01-01

    The thin slab casting and direct rolling process is a hot-rolled strip production method which has maintained commercial quality steel grades as a major material in many industrial applications due to its low processing cost. Few innovative products have however been developed specifically for production by thin slab direct rolling. Press hardening or hot press forming steel grades which are now widely used to produce structural automotive steel parts requiring ultra-high strength and formability may however offer an opportunity for thin slab direct rolling-specific ultra-high strength products. In this work, a newly designed press hardening steel grade developed specifically for thin slab direct rolling processing is presented. The press hardening steel has a high nitrogen content compared with press hardening steel grades produced by conventional steelmaking routes. Boron and titanium which are key alloying additions in conventional press hardening steel such as the 22MnB5 press hardening steel grade are not utilized. Cr is added in the press hardening steel to obtain the required hardenability. The properties of the new thin slab direct rolling-specific 22MnCrN5 press hardening steel grade are reviewed. The evolution of the microstructure and mechanical properties with increasing amounts of Cr additions from 0.6 to 1.4 wt pct and the effect of the cooling rate during die-quenching were studied by means of laboratory simulations. The selection of the optimum chemical composition range for the thin slab direct rolling-specific 22MnCrN5 steel in press hardening heat treatment conditions is discussed.

  5. Evaluation of Springback for DP980 S Rail Using Anisotropic Hardening Models

    NASA Astrophysics Data System (ADS)

    Choi, Jisik; Lee, Jinwoo; Bae, Gihyun; Barlat, Frederic; Lee, Myoung-Gyu

    2016-07-01

    The effect of anisotropic hardening models on springback of an S-rail part was investigated. Two advanced constitutive models based on distortional and kinematic hardening, which captured the Bauschinger effect, transient hardening, and permanent softening during strain path change, were implemented in a finite element (FE) code. In-plane compression-tension tests were performed to identify the model parameters. The springback of the S-rail after forming a 980 MPa dual-phase steel sheet sample was measured and analyzed using different hardening models. The comparison between experimental and FE results demonstrated that the advanced anisotropic hardening models, which are particularly suitable for non-proportional loading, significantly improved the springback prediction capability of an advanced high strength steel.

  6. Microstructure evolution and mechanical behavior of a high strength dual-phase steel under monotonic loading

    SciTech Connect

    Nesterova, E.V.; Bouvier, S.; Bacroix, B.

    2015-02-15

    Transmission electron microscopy (TEM) microstructures of a high-strength dual-phase steel DP800 have been examined after moderate plastic deformations in simple shear and uniaxial tension. Special attention has been paid to the effect of the intergranular hard phase (martensite) on the microstructure evolution in the near-grain boundary regions. Quantitative parameters of dislocation patterning have been determined and compared with the similar characteristics of previously examined single-phase steels. The dislocation patterning in the interiors of the ferrite grains in DP800 steel is found to be similar to that already observed in the single-phase IF (Interstitial Free) steel whereas the martensite-affected zones present a delay in patterning and display very high gradients of continuous (gradual) disorientations associated with local internal stresses. The above stresses are shown to control the work-hardening of dual-phase materials at moderate strains for monotonic loading and are assumed to influence their microstructure evolution and mechanical behavior under strain-path changes. - Highlights: • The microstructure evolution has been studied by TEM in a DP800 steel. • It is influenced by both martensite and dislocations in the initial state. • The DP800 steel presents a high work-hardening rate due to internal stresses.

  7. Local heat treatment of high strength steels with zoom-optics and 10kW-diode laser

    NASA Astrophysics Data System (ADS)

    Baumann, Markus; Krause, Volker; Bergweiler, Georg; Flaischerowitz, Martin; Banik, Janko

    2012-03-01

    High strength steels enable new solutions for weight optimized car bodies without sacrificing crash safety. However, cold forming of these steels is limited due to the need of high press capacity, increased tool wear, and limitations in possible geometries. One can compensate for these drawbacks by local heat treatment of the blanks. In high-deformation areas the strength of the material is reduced and the plasticity is increased by diode laser irradiation. Local heat treatment with diode laser radiation could also yield key benefits for the applicability of press hardened parts. High strength is not desired all over the part. Joint areas or deformation zones for requested crash properties require locally reduced strength. In the research project "LOKWAB" funded by the German Federal Ministry of Education and Research (BMBF), heat treatment of high strength steels was investigated in cooperation with Audi, BMW, Daimler, ThyssenKrupp, Fraunhofer- ILT, -IWU and others. A diode laser with an output power of 10 kW was set up to achieve acceptable process speed. Furthermore a homogenizing zoom-optics was developed, providing a rectangular focus with homogeneous power density. The spot size in x- and y-direction can be changed independently during operation. With pyrometer controlled laser power the surface temperature is kept constant, thus the laser treated zone can be flexibly adapted to the needs. Deep-drawing experiments show significant improvement in formability. With this technique, parts can be manufactured, which can conventionally only be made of steel with lower strength. Locally reduced strength of press hardened serial parts was demonstrated.

  8. Friction Stir Spot Welding (FSSW) of Advanced High Strength Steel (AHSS)

    SciTech Connect

    Santella, M. L.; Hovanski, Yuri; Pan, Tsung-Yu

    2012-04-16

    Friction stir spot welding (FSSW) is applied to join advanced high strength steels (AHSS): galvannealed dual phase 780 MPa steel (DP780GA), transformation induced plasticity 780 MPa steel (TRIP780), and hot-stamped boron steel (HSBS). A low-cost Si3N4 ceramic tool was developed and used for making welds in this study instead of polycrystalline cubic boron nitride (PCBN) material used in earlier studies. FSSW has the advantages of solid-state, low-temperature process, and the ability of joining dissimilar grade of steels and thicknesses. Two different tool shoulder geometries, concave with smooth surface and convex with spiral pattern, were used in the study. Welds were made by a 2-step displacement control process with weld time of 4, 6, and 10 seconds. Static tensile lap-shear strength achieved 16.4 kN for DP780GA-HSBS and 13.2kN for TRIP780-HSBS, above the spot weld strength requirements by AWS. Nugget pull-out was the failure mode of the joint. The joining mechanism was illustrated from the cross-section micrographs. Microhardness measurement showed hardening in the upper sheet steel (DP780GA or TRIP780) in the weld, but softening of HSBS in the heat-affect zone (HAZ). The study demonstrated the feasibility of making high-strength AHSS spot welds with low-cost tools.

  9. Structural application of high strength, high temperature ceramics

    NASA Technical Reports Server (NTRS)

    Hall, W. B.

    1982-01-01

    The operation of rocket engine turbine pumps is limited by the temperature restrictions of metallic components used in the systems. Mechanical strength and stability of these metallic components decrease drastically at elevated temperatures. Ceramic materials that retain high strength at high temperatures appear to be a feasible alternate material for use in the hot end of the turbopumps. This project identified and defined the processing parameters that affected the properties of Si3N4, one of candidate ceramic materials. Apparatus was assembled and put into operation to hot press Si3N4 powders into bulk material for in house evaluation. A work statement was completed to seek outside contract services to design, manufacture, and evaluate Si3N4 components in the service environments that exists in SSME turbopumps.

  10. Crystal Plasticity Constitutive Model for Multiphase Advanced High Strength Steels to Account for Phase Transformation and Yield Point Elongation

    NASA Astrophysics Data System (ADS)

    Park, Taejoon; Pourboghrat, Farhang

    2016-08-01

    A constitutive law was developed based on a rate-independent crystal plasticity to account for the mechanical behavior of multiphase advanced high strength steels. Martensitic phase transformation induced by the plastic deformation of the retained austenite was represented by considering the lattice invariant shear deformation and the orientation relationship between parent austenite and transformed martensite. The stress dependent transformation kinetics were represented by adopting the stress state dependent volume fraction evolution law. The plastic deformation of the austenite was determined to have the minimum- energy associated with the work during the phase transformation. In addition to the martensitic phase transformation, yield point elongation and subsequent hardening along with inhomogeneous plastic deformation were also represented by developing a hardening stagnation model induced by the delayed dislocation density evolution.

  11. Achieving high strength and high ductility in magnesium alloy using hard-plate rolling (HPR) process.

    PubMed

    Wang, Hui-Yuan; Yu, Zhao-Peng; Zhang, Lei; Liu, Chun-Guo; Zha, Min; Wang, Cheng; Jiang, Qi-Chuan

    2015-01-01

    Magnesium alloys are highly desirable for a wide range of lightweight structural components. However, rolling Mg alloys can be difficult due to their poor plasticity, and the strong texture yielded from rolling often results in poor plate forming ability, which limits their further engineering applications. Here we report a new hard-plate rolling (HPR) route which achieves a large reduction during a single rolling pass. The Mg-9Al-1Zn (AZ91) plates processed by HPR consist of coarse grains of 30-60 μm, exhibiting a typical basal texture, fine grains of 1-5 μm and ultrafine (sub) grains of 200-500 nm, both of the latter two having a weakened texture. More importantly, the HPR was efficient in gaining a simultaneous high strength and uniform ductility, i.e., ~371 MPa and ~23%, respectively. The superior properties should be mainly attributed to the cooperation effect of the multimodal grain structure and weakened texture, where the former facilitates a strong work hardening while the latter promotes the basal slip. The HPR methodology is facile and effective, and can avoid plate cracking that is prone to occur during conventional rolling processes. This strategy is applicable to hard-to-deform materials like Mg alloys, and thus has a promising prospect for industrial application. PMID:26603776

  12. Achieving high strength and high ductility in magnesium alloy using hard-plate rolling (HPR) process.

    PubMed

    Wang, Hui-Yuan; Yu, Zhao-Peng; Zhang, Lei; Liu, Chun-Guo; Zha, Min; Wang, Cheng; Jiang, Qi-Chuan

    2015-11-25

    Magnesium alloys are highly desirable for a wide range of lightweight structural components. However, rolling Mg alloys can be difficult due to their poor plasticity, and the strong texture yielded from rolling often results in poor plate forming ability, which limits their further engineering applications. Here we report a new hard-plate rolling (HPR) route which achieves a large reduction during a single rolling pass. The Mg-9Al-1Zn (AZ91) plates processed by HPR consist of coarse grains of 30-60 μm, exhibiting a typical basal texture, fine grains of 1-5 μm and ultrafine (sub) grains of 200-500 nm, both of the latter two having a weakened texture. More importantly, the HPR was efficient in gaining a simultaneous high strength and uniform ductility, i.e., ~371 MPa and ~23%, respectively. The superior properties should be mainly attributed to the cooperation effect of the multimodal grain structure and weakened texture, where the former facilitates a strong work hardening while the latter promotes the basal slip. The HPR methodology is facile and effective, and can avoid plate cracking that is prone to occur during conventional rolling processes. This strategy is applicable to hard-to-deform materials like Mg alloys, and thus has a promising prospect for industrial application.

  13. Achieving high strength and high ductility in magnesium alloy using hard-plate rolling (HPR) process

    PubMed Central

    Wang, Hui–Yuan; Yu, Zhao–Peng; Zhang, Lei; Liu, Chun–Guo; Zha, Min; Wang, Cheng; Jiang, Qi–Chuan

    2015-01-01

    Magnesium alloys are highly desirable for a wide range of lightweight structural components. However, rolling Mg alloys can be difficult due to their poor plasticity, and the strong texture yielded from rolling often results in poor plate forming ability, which limits their further engineering applications. Here we report a new hard-plate rolling (HPR) route which achieves a large reduction during a single rolling pass. The Mg-9Al-1Zn (AZ91) plates processed by HPR consist of coarse grains of 30–60 μm, exhibiting a typical basal texture, fine grains of 1–5 μm and ultrafine (sub) grains of 200–500 nm, both of the latter two having a weakened texture. More importantly, the HPR was efficient in gaining a simultaneous high strength and uniform ductility, i.e., ~371 MPa and ~23%, respectively. The superior properties should be mainly attributed to the cooperation effect of the multimodal grain structure and weakened texture, where the former facilitates a strong work hardening while the latter promotes the basal slip. The HPR methodology is facile and effective, and can avoid plate cracking that is prone to occur during conventional rolling processes. This strategy is applicable to hard-to-deform materials like Mg alloys, and thus has a promising prospect for industrial application. PMID:26603776

  14. Gaseous hydrogen embrittlement of high strength steels

    NASA Technical Reports Server (NTRS)

    Gangloff, R. P.; Wei, R. P.

    1977-01-01

    The effects of temperature, hydrogen pressure, stress intensity, and yield strength on the kinetics of gaseous hydrogen assisted crack propagation in 18Ni maraging steels were investigated experimentally. It was found that crack growth rate as a function of stress intensity was characterized by an apparent threshold for crack growth, a stage where the growth rate increased sharply, and a stage where the growth rate was unchanged over a significant range of stress intensity. Cracking proceeded on load application with little or no detectable incubation period. Gaseous hydrogen embrittlement susceptibility increased with increasing yield strength.

  15. Development of K-Basin High-Strength Homogeneous Sludge Simulants and Correlations Between Unconfined Compressive Strength and Shear Strength

    SciTech Connect

    Onishi, Yasuo; Baer, Ellen BK; Chun, Jaehun; Yokuda, Satoru T.; Schmidt, Andrew J.; Sande, Susan; Buchmiller, William C.

    2011-02-20

    K-Basin sludge will be stored in the Sludge Transport and Storage Containers (STSCs) at an interim storage location on Central Plateau before being treated and packaged for disposal. During the storage period, sludge in the STSCs may consolidate/agglomerate, potentially resulting in high-shear-strength material. The Sludge Treatment Project (STP) plans to use water jets to retrieve K-Basin sludge after the interim storage. STP has identified shear strength to be a key parameter that should be bounded to verify the operability and performance of sludge retrieval systems. Determining the range of sludge shear strength is important to gain high confidence that a water-jet retrieval system can mobilize stored K-Basin sludge from the STSCs. The shear strength measurements will provide a basis for bounding sludge properties for mobilization and erosion. Thus, it is also important to develop potential simulants to investigate these phenomena. Long-term sludge storage tests conducted by Pacific Northwest National Laboratory (PNNL) show that high-uranium-content K-Basin sludge can self-cement and form a strong sludge with a bulk shear strength of up to 65 kPa. Some of this sludge has 'paste' and 'chunks' with shear strengths of approximately 3-5 kPa and 380-770 kPa, respectively. High-uranium-content sludge samples subjected to hydrothermal testing (e.g., 185 C, 10 hours) have been observed to form agglomerates with a shear strength up to 170 kPa. These high values were estimated by measured unconfined compressive strength (UCS) obtained with a pocket penetrometer. Due to its ease of use, it is anticipated that a pocket penetrometer will be used to acquire additional shear strength data from archived K-Basin sludge samples stored at the PNNL Radiochemical Processing Laboratory (RPL) hot cells. It is uncertain whether the pocket penetrometer provides accurate shear strength measurements of the material. To assess the bounding material strength and potential for erosion, it

  16. Silicon nitride having a high tensile strength

    DOEpatents

    Pujari, Vimal K.; Tracey, Dennis M.; Foley, Michael R.; Paille, Norman I.; Pelletier, Paul J.; Sales, Lenny C.; Willkens, Craig A.; Yeckley, Russell L.

    1996-01-01

    A silicon nitride ceramic comprising: a) inclusions no greater than 25 microns in length, b) agglomerates no greater than 20 microns in diameter, and c) a surface finish of less than about 8 microinches, said ceramic having a four-point flexural strength of at least about 900 MPa.

  17. Silicon nitride having a high tensile strength

    DOEpatents

    Pujari, V.K.; Tracey, D.M.; Foley, M.R.; Paille, N.I.; Pelletier, P.J.; Sales, L.C.; Willkens, C.A.; Yeckley, R.L.

    1996-11-05

    A silicon nitride ceramic is disclosed comprising: (a) inclusions no greater than 25 microns in length, (b) agglomerates no greater than 20 microns in diameter, and (c) a surface finish of less than about 8 microinches, said ceramic having a four-point flexural strength of at least about 900 MPa. 4 figs.

  18. System-Level Radiation Hardening

    NASA Technical Reports Server (NTRS)

    Ladbury, Ray

    2014-01-01

    Although system-level radiation hardening can enable the use of high-performance components and enhance the capabilities of a spacecraft, hardening techniques can be costly and can compromise the very performance designers sought from the high-performance components. Moreover, such techniques often result in a complicated design, especially if several complex commercial microcircuits are used, each posing its own hardening challenges. The latter risk is particularly acute for Commercial-Off-The-Shelf components since high-performance parts (e.g. double-data-rate synchronous dynamic random access memories - DDR SDRAMs) may require other high-performance commercial parts (e.g. processors) to support their operation. For these reasons, it is essential that system-level radiation hardening be a coordinated effort, from setting requirements through testing up to and including validation.

  19. A New Perspective on Fatigue Performance of Advanced High- Strength Steels (AHSS) GMAW Joints

    SciTech Connect

    Feng, Zhili; Chiang, Dr. John; Kuo, Dr. Min; Jiang, Cindy; Sang, Yan

    2008-01-01

    Weld fatigue performance is a critical aspect for application of advanced high-strength steels (AHSS) in automotive body structures. A comparative study has been conducted to evaluate the fatigue life of AHSS welds. The material studied included seven AHSS of various strength levels - DP 600, DP 780, DP 980, M130, M220, solution annealed boron and fully hardened boron steels. Two conventional steels, HSLA 590 and DR 210, were also included for baseline comparison. Lap fillet welds were made on 2-mm nominal thick sheets by the gas metal arc welding process (GMAW). Fatigue test was conducted under a number of stress levels to obtain the S/N curves of the weld joints. It was found that, unlike in the static and impact loading conditions, the fatigue performance of AHSS is not influenced by the HAZ softening in AHSS. There are appreciable differences in the fatigue lives among different AHSS. Changes in weld parameters can influence the fatigue life of the weld joints, particularly of these of higher strength AHSS. A model is developed to predict the fatigue performance of AHSS welds. The validity of the model is benchmarked with the experimental results. This model is capable to capture the effects of weld geometry and weld microstructure and strength on the fatigue performance experimentally observed. The theoretical basis and application of the newly developed fatigue modeling methodology will be discussed.

  20. Evaluation of high strength, high conductivity CuNiBe alloys for fusion energy applications

    SciTech Connect

    Zinkle, Steven J

    2014-06-01

    The unirradiated tensile properties for several different heats and thermomechanical treatment conditions of precipitation strengthened Hycon 3HPTM CuNiBe (Cu-2%Ni-0.35%Be in wt.%) have been measured over the temperature range of 20-500 C for longitudinal and long transverse orientations. The room temperature electrical conductivity has also been measured for several heats, and the precipitate microstructure was characterized using transmission electron microscopy. The CuNiBe alloys exhibit very good combination of strength and conductivity at room temperature, with yield strengths of 630-725 MPa and electrical conductivities of 65-72% International Annealed Copper Standard (IACS). The strength remained relatively high at all test temperatures, with yield strengths of 420-520 MPa at 500 C. However, low levels of ductility (<5% uniform elongation) were observed at test temperatures above 200-250 C, due to flow localization near grain boundaries (exacerbated by having only 10-20 grains across the gage thickness of the miniaturized sheet tensile specimens). Scanning electron microscopy observation of the fracture surfaces found a transition from ductile transgranular to ductile intergranular fracture with increasing test temperature. Fission neutron irradiation to a dose of ~0.7 displacements per atom (dpa) at temperatures between 100 and 240 C produced a slight increase in strength and a significant decrease in ductility. The measured tensile elongation increased with increasing irradiation temperature, with a uniform elongation of ~3.3% observed at 240 C. The electrical conductivity decreased slightly following irradiation, due to the presence of defect clusters and Ni, Zn, Co transmutation products. Considering also previously published fracture toughness data, this indicates that CuNiBe alloys have irradiated tensile and electrical properties comparable or superior to CuCrZr and oxide dispersion strengthened copper at temperatures <250 C, and may be an attractive

  1. Mechanical behavior of high strength ceramic fibers at high temperatures

    NASA Technical Reports Server (NTRS)

    Tressler, R. E.; Pysher, D. J.

    1991-01-01

    The mechanical behavior of commercially available and developmental ceramic fibers, both oxide and nonoxide, has been experimentally studied at expected use temperatures. In addition, these properties have been compared to results from the literature. Tensile strengths were measured for three SiC-based and three oxide ceramic fibers for temperatures from 25 C to 1400 C. The SiC-based fibers were stronger but less stiff than the oxide fibers at room temperature and retained more of both strength and stiffness to high temperatures. Extensive creep and creep-rupture experiments have been performed on those fibers from this group which had the best strengths above 1200 C in both single filament tests and tests of fiber bundles. The creep rates for the oxides are on the order of two orders of magnitude faster than the polymer derived nonoxide fibers. The most creep resistant filaments available are single crystal c-axis sapphire filaments. Large diameter CVD fabricated SiC fibers are the most creep and rupture resistant nonoxide polycrystalline fibers tested to date.

  2. Extracellular bone matrix exhibits hardening elastoplasticity and more than double cortical strength: Evidence from homogeneous compression of non-tapered single micron-sized pillars welded to a rigid substrate.

    PubMed

    Luczynski, Krzysztof W; Steiger-Thirsfeld, Andreas; Bernardi, Johannes; Eberhardsteiner, Josef; Hellmich, Christian

    2015-12-01

    We here report an improved experimental technique for the determination of Young׳s modulus and uniaxial strength of extracellular bone matrix at the single micrometer scale, giving direct access to the (homogeneous) deformation (or strain) states of the tested samples and to the corresponding mechanically recoverable energy, called potential or elastic energy. Therefore, a new protocol for Focused Ion Beam milling of prismatic non-tapered micropillars, and attaching them to a rigid substrate, was developed. Uniaxial strength turns out as at least twice that measured macroscopically, and respective ultimate stresses are preceded by hardening elastoplastic states, already at very low load levels. The unloading portion of quasi-static load-displacement curves revealed Young׳s modulus of 29GPa in bovine extracellular bone matrix. This value is impressively confirmed by the corresponding prediction of a multiscale mechanics model for bone, which has been comprehensively validated at various other observation scales, across tissues from the entire vertebrate animal kingdom.

  3. Reduction of work hardening rate in low-carbon steels

    NASA Astrophysics Data System (ADS)

    Yalamanchili, Bhaskar Rao

    Low carbon grades of steel rods are used to produce finished products such as fine wire, coat hangers, staples, and roofing nails. These products are subject to ductility failures during production due to excessively high work hardening rates during wire drawing. The high work hardening rates are attributed to the presence of residuals, free nitrogen, or combinations thereof. This research concludes that the most cost-effective way to reduce the work hardening rate during wire drawing is to combine boron with nitrogen to form boron nitride, and thus reducing its work hardening contribution. The results of this study also conclude the following: (1) Boron/Nitrogen ratio is the more significant factor than rod tensile strength, which affects work hardening rate. Higher ratio is better in the 0.79 to 1.19 range. (2) Maintaining this narrow B/N range requires precise process control. (3) Process conditions such as dissolved oxygen (<25 ppm), carbon (≤0.05%) and ladle refining temperature (<2930°F) are necessary for optimizing boron recovery. (4) An average of 89% boron recovery is obtained with the above controlled process conditions. (5) Use of Boron has no adverse effects on the several metallurgical properties tested except with minor difficulty with scale for descaling. North Star Steel Texas (North Star) benefited from this research by being able to provide a competitive edge in both quality and cost of its low carbon boron grades thus making North Star a preferred supplier of wire rod for these products.

  4. Fatigue crack initiation and strain-controlled fatigue of some high strength low alloy steels

    NASA Astrophysics Data System (ADS)

    Kim, Y. H.; Fine, M. E.

    1982-01-01

    Initiation and growth of fatigue microcracks were investigated in several Nb and V alloyed high strength low alloy steels, including conventional and dual phase microstructures. Fatigue microcracks initiated along prominent slip bands. Macrocracks formed by linking up of small microcracks. At low applied stress or strain, the number of cycles to crack initiation increased with the cyclic yield stress. Comparing the cyclic stress-strain curves to the monotonie stress-strain curves, cyclic hardening or softening occurred, depending upon strain amplitude. Plateau regions were observed in plots of cyclic stress amplitude vs cyclic plastic strain amplitude obtained by increasing the total strain amplitude in steps after 30 cycles at each step. In polycrystalline 0.03 pct Nb steel, the plateau region was identified with prominent slip band formation, as others have observed in single crystals of copper, C-doped iron, and other metals.

  5. Friction Stir Spot Welding of Advanced High Strength Steels

    SciTech Connect

    Hovanski, Yuri; Grant, Glenn J.; Santella, M. L.

    2009-11-13

    Friction stir spot welding techniques were developed to successfully join several advanced high strength steels. Two distinct tool materials were evaluated to determine the effect of tool materials on the process parameters and joint properties. Welds were characterized primarily via lap shear, microhardness, and optical microscopy. Friction stir spot welds were compared to the resistance spot welds in similar strength alloys by using the AWS standard for resistance spot welding high strength steels. As further comparison, a primitive cost comparison between the two joining processes was developed, which included an evaluation of the future cost prospects of friction stir spot welding in advanced high strength steels.

  6. PHETS (Permanent High Explosive Test Site) lightning hardening program: Misty Picture Event. Final report, January-November 1987

    SciTech Connect

    Chapman, G.P.; Gardner, R.L.; Lu, G.S.; Rison, W.; Gurbaxani, S.H.

    1988-06-01

    The Permanent High Explosive Test Site (PHETS) test-bed electrical topology and data flow are presented along with various equipments used in the topology. Using this information, recommendations are made to harden the test-bed instrumentation to electrical transients. These transients may be caused by lightning or electrostatic discharge. Specific attention is given to the junction box design, the shorting blocks, use of shielded cables, protection of the sensors, and the instrumentation bunker/container. Additional attention is given to the protection of personnel from lightning effects. Also, it is recommended the optimum design is of a Faraday-cage concept that completely encases the instrumentation from sensor to permanent recording medium. The optimum design should be prototyped and tested using the Precision Test bed and current injection before general application to the PHETS.

  7. A One Chip Hardened Solution for High Speed SpaceWire System Implementations. Session: Components

    NASA Technical Reports Server (NTRS)

    Marshall, Joseph R.; Berger, Richard W.; Rakow, Glenn P.

    2007-01-01

    An Application Specific Integrated Circuit (ASIC) that implements the SpaceWire protocol has been developed in a radiation hardened 0.25 micron CMOS technology. This effort began in March 2003 as a joint development between the NASA Goddard Space Flight Center (GSFC) and BAE Systems. The BAE Systems SpaceWire ASIC is comprised entirely of reusable core elements, many of which are already flight-proven. It incorporates a router with 4 SpaceWire ports and two local ports, dual PC1 bus interfaces, a microcontroller, 32KB of internal memory, and a memory controller for additional external memory use. The SpaceWire cores are also reused in other ASICs under development. The SpaceWire ASIC is planned for use on the Geostationary Operational Environmental Satellites (GOES)-R, the Lunar Reconnaissance Orbiter (LRO) and other missions. Engineering and flight parts have been delivered to programs and users. This paper reviews the SpaceWire protocol and those elements of it that have been built into the current and next SpaceWire reusable cores and features within the core that go beyond the current standard and can be enabled or disabled by the user. The adaptation of SpaceWire to BAE Systems' On Chip Bus (OCB) for compatibility with the other reusable cores will be reviewed and highlighted. Optional configurations within user systems and test boards will be shown. The physical implementation of the design will be described and test results from the hardware will be discussed. Application of this ASIC and other ASICs containing the SpaceWire cores and embedded microcontroller to Plug and Play and reconfigurable implementations will be described. Finally, the BAE Systems roadmap for SpaceWire developments will be updated, including some products already in design as well as longer term plans.

  8. EFFECTS OF LASER RADIATION ON MATTER. LASER PLASMA: Surface hardening of steels with a strip-shaped beam of a high-power CO2 laser

    NASA Astrophysics Data System (ADS)

    Dubovskii, P. E.; Kovsh, Ivan B.; Strekalova, M. S.; Sisakyan, I. N.

    1994-12-01

    A comparative analysis was made of the surface hardening of steel 45 by high-power CO2 laser beams with a rectangular strip-like cross section and a traditional circular cross section. This was done under various conditions. The treatment with the strip-like beam ensured a higher homogeneity of the hardened layer and made it possible to increase the productivity by a factor of 2-4 compared with the treatment by a beam of the same power but with a circular cross section.

  9. Intelligent systems for induction hardening processes

    SciTech Connect

    Kelley, J.B.; Adkins, D.R.; Robino, C.V.

    1994-12-31

    Induction hardening is widely used to provide enhanced strength, wear resistance, and toughness in components made from medium and high carbon steels. Current limitations of the process include the lack of closed-loop process control, previously unidentified process and material variations which cause continual adjustment of the process parameters, coil and process development by trial and error, and an instability to monitor coil condition. Improvement of the induction hardening process is limited by an inadequate understanding of process fundamentals and material/process interactions. A multidisciplinary team from Sandia National Laboratories and Delphi Saginaw Steering Systems is investigating the induction hardening process under a Cooperative Research and Development Agreement (CRADA). The application of intelligent control algorithms has led to the development of a closed-loop process controller for the combination of one material, one geometry, single frequency, single shot, process that controls to {plus_minus} 0.1mm. This controller will be demonstrated on the production floor this year. Our approach and the opportunities for expanding the usefulness of this technology will be described.

  10. Experience of high-nitrogenous steel powder application in repairs and surface hardening of responsible parts for power equipment by plasma spraying

    NASA Astrophysics Data System (ADS)

    Kolpakov, A. S.; Kardonina, N. I.

    2016-02-01

    The questions of the application of novel diffusion-alloying high-nitrogenous steel powders for repair and surface hardening of responsible parts of power equipment by plasma spraying are considered. The appropriateness of the method for operative repair of equipment and increasing its service life is justified. General data on the structure, properties, and manufacture of nitrogen-, aluminum-, and chromium-containing steel powders that are economically alloyed using diffusion are described. It is noted that the nitrogen release during the decomposition of iron nitrides, when heating, protects the powder particles from oxidation in the plasma jet. It is shown that the coating retains 50% of nitrogen that is contained in the powder. Plasma spraying modes for diffusion-alloying high-nitrogenous steel powders are given. The service properties of plasma coatings based on these powders are analyzed. It is shown that the high-nitrogenous steel powders to a nitrogen content of 8.9 wt % provide the necessary wear resistance and hardness of the coating and the strength of its adhesion to the substrate and corrosion resistance to typical aggressive media. It is noted that increasing the coating porosity promotes stress relaxation and increases its thickness being limited with respect to delamination conditions in comparison with dense coatings on retention of the low defectiveness of the interface and high adhesion to the substrate. The examples of the application of high-nitrogenous steel powders in power engineering during equipment repairs by service companies and overhaul subdivisions of heat power plants are given. It is noted that the plasma spraying of diffusion-alloyed high-nitrogenous steel powders is a unique opportunity to restore nitrided steel products.

  11. Single event upset hardening techniques

    SciTech Connect

    Weaver, H.T.; Corbett, W.T.

    1990-01-01

    Integrated circuit logic states are maintained by virtue of specific transistor combinations being either on'' (conducting) or off'' (nonconducting). High energy ion strikes on the microcircuit generate photocurrents whose primary detrimental effect is to make off'' transistors appear on,'' confusing the logic state and leading to single event upset (SEU). Protection against these soft errors is accomplished using either technology or circuit techniques, actions that generally impact yield and performance relative to unhardened circuits. We describe, and using circuit simulations analyze, a technique for hardening latches which requires combinations of technology and circuit modifications, but which provides SEU immunity without loss of speed. Specifically, a single logic state is hardened against SEU using technology methods and the information concerning valid states is then used to simplify hardened circuit design. The technique emphasizes some basic hardening concepts, ideas for which will be reviewed. 3 refs., 2 figs.

  12. Quantitative analysis of artifacts in 4D DSA: the relative contributions of beam hardening and scatter to vessel dropout behind highly attenuating structures

    NASA Astrophysics Data System (ADS)

    Hermus, James; Szczykutowicz, Timothy P.; Strother, Charles M.; Mistretta, Charles

    2014-03-01

    When performing Computed Tomographic (CT) image reconstruction on digital subtraction angiography (DSA) projections, loss of vessel contrast has been observed behind highly attenuating anatomy, such as dental implants and large contrast filled aneurysms. Because this typically occurs only in a limited range of projection angles, the observed contrast time course can potentially be altered. In this work, we have developed a model for acquiring DSA projections that models both the polychromatic nature of the x-ray spectrum and the x-ray scattering interactions to investigate this problem. In our simulation framework, scatter and beam hardening contributions to vessel dropout can be analyzed separately. We constructed digital phantoms with large clearly defined regions containing iodine contrast, bone, soft issue, titanium (dental implants) or combinations of these materials. As the regions containing the materials were large and rectangular, when the phantoms were forward projected, the projections contained uniform regions of interest (ROI) and enabled accurate vessel dropout analysis. Two phantom models were used, one to model the case of a vessel behind a large contrast filled aneurysm and the other to model a vessel behind a dental implant. Cases in which both beam hardening and scatter were turned off, only scatter was turned on, only beam hardening was turned on, and both scatter and beam hardening were turned on, were simulated for both phantom models. The analysis of this data showed that the contrast degradation is primarily due to scatter. When analyzing the aneurysm case, 90.25% of the vessel contrast was lost in the polychromatic scatter image, however only 50.5% of the vessel contrast was lost in the beam hardening only image. When analyzing the teeth case, 44.2% of the vessel contrast was lost in the polychromatic scatter image and only 26.2% of the vessel contrast was lost in the beam hardening only image.

  13. Increasing Lean Mass and Strength: A Comparison of High Frequency Strength Training to Lower Frequency Strength Training

    PubMed Central

    THOMAS, MICHAEL H.; BURNS, STEVE P.

    2016-01-01

    The purpose of this study was to determine the effect strength training frequency has on improvements in lean mass and strength. Participants were 7 women and 12 men, age (χ̄= 34.64 years ± 6.91 years), with strength training experience, training age (χ̄= 51.16 months ± 39.02 months). Participants were assigned to one of two groups to equal baseline group demographics. High frequency training group (HFT) trained each muscle group as the agonist, 3 times per week, exercising with 3 sets per muscle group per session (3 total body workouts). Low frequency training group (LFT) trained each muscle group as the agonist one time per week, completing all 9 sets during that one workout. LFT consisted of a routine split over three days: 1) pectoralis, deltoids, and triceps; 2) upper back and biceps; 3) quadriceps, hamstrings, calves, and abdominals. Following eight weeks of training, HFT increased lean mass by 1.06 kg ± 1.78 kg, (1.9%), and LFT increased lean mass by .99 kg ± 1.31 kg, (2.0%). HFT strength improvements on the chest press was 9.07 kg ± 6.33 kg, (11%), and hack squat 20.16 kg ± 11.59 kg, (21%). LFT strength improvements on chest press was 5.80kg ± 4.26 kg, (7.0%), and hack squat 21.83 kg ± 11.17 kg, (24 %). No mean differences between groups were significant. These results suggest that HFT and LFT of equal set totals result in similar improvements in lean mass and strength, following 8 weeks of strength training. PMID:27182422

  14. High-strength silicon carbides by hot isostatic pressing

    NASA Technical Reports Server (NTRS)

    Dutta, Sunil

    1989-01-01

    Silicon carbide has strong potential for heat engine hardware and other high-temperature applications because of its low density, good strength, high oxidation resistance, and good high-temperature creep resistance. Hot isostatic pressing (HIP) was used for producing alpha and beta silicon carbide (SiC) bodies with near-theoretical density, ultrafine grain size, and high strength at processing temperatures of 1900 to 2000 C. The HIPed materials exhibited ultrafine grain size. Furthermore, no phase transformation from beta to alpha was observed in HIPed beta-SiC. Both materials exhibited very high average flexural strength. It was also shown that alpha-SiC bodies without any sintering aids, when HIPed to high final density, can exhibit very high strength. Fracture toughness K (sub C) values were determined to be 3.6 to 4.0 MPa m (sup 1/2) for HIPed alpha-SiC and 3.7 to 4.1 MPa m (sup 1/2) for HIPed beta-SiC. In the HIPed specimens strength-controlling flaws were typically surface related. In spite of improvements in material properties such as strength and fracture toughness by elimination of the larger strength-limiting flaws and by grain size refinement, HIPing has no effect on the Weibull modulus.

  15. High-strength silicon carbides by hot isostatic pressing

    NASA Technical Reports Server (NTRS)

    Dutta, Sunil

    1988-01-01

    Silicon carbide has strong potential for heat engine hardware and other high-temperature applications because of its low density, good strength, high oxidation resistance, and good high-temperature creep resistance. Hot isostatic pressing (HIP) was used for producing alpha and beta silicon carbide (SiC) bodies with near-theoretical density, ultrafine grain size, and high strength at processing temperatures of 1900 to 2000 C. The HIPed materials exhibited ultrafine grain size. Furthermore, no phase transformation from beta to alpha was observed in HIPed beta-SiC. Both materials exhibited very high average flexural strength. It was also shown that alpha-SiC bodies without any sintering aids, when HIPed to high final density, can exhibit very high strength. Fracture toughness K (sub C) values were determined to be 3.6 to 4.0 MPa m (sup 1/2) for HIPed alpha-SiC and 3.7 to 4.1 MPa m (sup 1/2) for HIPed beta-SiC. In the HIPed specimens strength-controlling flaws were typically surface related. In spite of improvements in material properties such as strength and fracture toughness by elimination of the larger strength-limiting flaws and by grain size refinement, HIPing has no effect on the Weibull modulus.

  16. Friction Stir Spot Welding of Advanced High Strength Steels

    SciTech Connect

    Santella, M. L.; Hovanski, Yuri; Grant, Glenn J.; Carpenter, Joseph A.; Warren, C. D.; Smith, Mark T.

    2008-12-28

    Experiments are continuing to evaluate the feasibility of friction stir spot welding advanced high-strength steels including, DP780, martensitic hot-stamp boron steel, and TRIP steels. Spot weld lap-shear strengths can exceed those required by industry standards such as AWS D8.1.

  17. The High School Strength and Conditioning Professional: A Job Description.

    ERIC Educational Resources Information Center

    Best, Randy

    2001-01-01

    Presents a job description for the high school strength and conditioning professional, who is in a unique position to integrate athletics and academics, highlighting: minimum qualifications; school-related benefits derived from employing a strength and conditioning professional; whom the professional reports to and works with; job…

  18. Investigation of the plastic fracture of high strength steels

    NASA Technical Reports Server (NTRS)

    Cox, T. B.; Low, J. R., Jr.

    1972-01-01

    This investigation deals in detail with the three recognized stages of plastic fracture in high strength steels, namely, void initiation, void growth, and void coalescence. The particular steels under investigation include plates from both commercial purity and high purity heats of AISI 4340 and 18 Ni, 200 grade maraging steels. A scanning electron microscope equipped with an X-ray energy dispersive analyzer, together with observations made using light microscopy, revealed methods of improving the resistance of high strength steels to plastic fracture.

  19. High strength forgeable tantalum base alloy

    NASA Technical Reports Server (NTRS)

    Buckman, R. W., Jr.

    1975-01-01

    Increasing tungsten content of tantalum base alloy to 12-15% level will improve high temperature creep properties of existing tantalum base alloys while retaining their excellent fabrication and welding characteristics.

  20. Evaluation of a low temperature hardening Inorganic Phosphate Cement for high-temperature applications

    SciTech Connect

    Alshaaer, M.; Cuypers, H.; Mosselmans, G.; Rahier, H.; Wastiels, J.

    2011-01-15

    Phase and mechanical changes of Inorganic Phosphate Cement (IPC) are identified along with changes in macro properties as functions of temperature and time. In addition to amorphous phases, the presence of significant amounts of brushite and wollastonite in the reference IPC is confirmed using X-ray diffraction. The thermal behavior of IPC up to 1000 {sup o}C shows that contraction of the solid phase in IPC due to chemical transformations causes reduction in the volume of the material. Also the ongoing meta-stable calcium phosphate transformations and reactions over a long time contribute significantly to the phase instability of the material at ambient conditions. It is found that the strength of IPC increases with ageing at ambient conditions but the formation microcracks below 105 {sup o}C causes a sharp reduction in the mechanical performance of IPC. According to the results obtained by Mercury intrusion porosimetry, the pore system of the reference IPC is dominated by mesopores.

  1. Formability Characterization of a New Generation High Strength Steels

    SciTech Connect

    Sriram Sadagopan; Dennis Urban; Chris Wong; Mai Huang; Benda Yan

    2003-05-16

    Advanced high strength steels (AHSS) are being progressively explored by the automotive industry all around the world for cost-effective solutions to accomplish vehicle lightweighting, improve fuel economy, and consequently reduce greenhouse emissions. Because of their inherent high strength, attractive crash energy management properties, and good formability, the effective use of AHSS such as Duel Phase and TRIP (Transformation Induced Plasticity) steels, will significantly contribute to vehicle lightweighting and fuel economy. To further the application of these steels in automotive body and structural parts, a good knowledge and experience base must be developed regarding the press formability of these materials. This project provides data on relevant intrinsic mechanical behavior, splitting limits, and springback behavior of several lots of mild steel, conventional high strength steel (HSS), advanced high strength steel (AHSS) and ultra-high strength steel (UHSS), supplied by the member companies of the Automotive Applications Committee (AAC) of the American Iron and Steel Institute (AISI). Two lots of TRIP600, which were supplied by ThyssenKrupp Stahl, were also included in the study. Since sheet metal forming encompasses a very diverse range of forming processes and deformation modes, a number of simulative tests were used to characterize the forming behavior of these steel grades. In general, it was found that formability, as determined by the different tests, decreased with increased tensile strength. Consistant with previous findings, the formability of TRIP600 was found to be exceptionally good for its tensile strength.

  2. Transformation hardening of steel sheet for automotive applications

    NASA Astrophysics Data System (ADS)

    Takechi, H.

    2008-12-01

    Among high-strength steels, transformation hardening steels such as dual-phase (DP) steel and transformation-induced plasticity (TRIP) steel offer a superior relationship between tensile strength (TS) and elongation (El) on a commercial scale. As demand has grown for lighter-weight automobiles, so also has the demand for higher TS, lower yield ratio, and higher hole expansion ratio grown. Recently DP steel has been developed with precipitation hardening and grain refining by TiC. A new TRIP steel composed of 5Mn-2Si and control-rolled with niobium addition suggests the formation of retained austenite ( γ R ) as much as 30% and TS × El = 3,000 kgf/mm2·%.

  3. Survey of Processing Methods for High Strength High Conductivity Wires for High Field Magnet Applications

    SciTech Connect

    Han, K.; Embury, J.D.

    1998-10-01

    This paper will deal with the basic concepts of attaining combination of high strength and high conductivity in pure materials, in-situ composites and macrocomposites. It will survey current attainments, and outline where some future developments may lie in developing wire products that are close to the theoretical strength of future magnet applications.

  4. Investigating strength of materials at very high strain rates using magnetically driven expanding cylinders

    NASA Astrophysics Data System (ADS)

    Lovinger, Zev; Nemirovsky, Ron; Avriel, Eyal; Dorogoy, Avraham; Ashuach, Yehezkel; Rittel, Daniel

    2015-09-01

    Dynamic characterization of strength properties is done, in common practice by the means of a Split-Hopkinson Pressure Bar (also named Kolsky-Bar) apparatus. In such systems, strain rates are limited up to ˜ 5 ṡ 103 sec-1. For higher strain rates, the strain rate hardening is assumed to be the same as that measured at lower rates, with no direct measurement to validate the assumptions used for this extrapolation. In this work we are using a pulsed current generator (PCG) to create electro-magnetic (EM) driving forces on expanding cylinders. Most standard techniques for creating EM driving forces on cylinders or rings, as reported in the literature, reach strain rates of 1e3-1e4. Using our PCG, characterized by a fast rise time, we reach strain rates of ˜1e5, thus paving the way to a standard technique to measure strength at very high strain rates. To establish the experimental technique, we conducted a numerical study of the expanding cylinder set up using 2D hydrodynamic simulations to reach the desired high strain rates.

  5. Hydrogen trapping sites in high-strength steels at delayed fracture

    SciTech Connect

    Takai, Kenichi; Seki, Junichi; Homma, Yoshikazu

    1996-12-01

    Hydrogen trapping sites in high-strength steels hardened by cold drawing (PC Wire) and heat treatment (PC Bar) were investigated using thermal desorption spectroscopy (TDS) and secondary ion mass spectrometry (SIMS). Both steels were stressed and dipped in 20% NH{sub 4}SCN solution at 323 K to occlude hydrogen for TDS analysis, whereas they were stressed and dipped in D{sub 2}O and 20% NH{sub 4}SCN solution at 323 K to occlude deuterium for SIMS analysis. TDS analysis shows that PC Wire occludes hydrogen at the peaks of 470 K and 630 K, whereas PC Bar mainly occludes hydrogen at 470 K and slightly at 630 K. SIMS analysis makes it possible to observe the trapping sites of deuterium instead of hydrogen in high-strength steels. PC Wire traps deuterium along the drawing direction. PC Bar traps deuterium at the grain boundaries and on the inclusions. The correspondence between TDS and SIMS shows that hydrogen at 470 K is evolved from the matrix that includes dislocations and grain boundaries. In contrast, hydrogen at 630 K is evolved from inclusions and segregation of P.

  6. High-strength braze joints between copper and steel

    NASA Technical Reports Server (NTRS)

    Kuhn, R. F.

    1967-01-01

    High-strength braze joints between copper and steel are produced by plating the faying surface of the copper with a layer of gold. This reduces porosity in the braze area and strengthens the resultant joint.

  7. Investigation of the plastic fracture of high strength steels

    NASA Technical Reports Server (NTRS)

    Cox, T. B.; Low, J. R., Jr.

    1972-01-01

    An investigation of the plastic fracture process to improve tensile strength in high strength steels is presented. Two generic types of steels are considered: a quenched and tempered grade and a maraging grade, in order to compare two different matrix microstructures. Each type of steel was studied in commercial grade purity and in special melted high purity form, low in residual and impurity elements. The specific alloys dealt with include AISI 4340 and 18 Ni, 200 grade maraging steel, both heat treated to the same yield strength level of approximately 200 ksi.

  8. IR and NMR analyses of hardening and maturation of glass-ionomer cement.

    PubMed

    Matsuya, S; Maeda, T; Ohta, M

    1996-12-01

    It has been reported that the silicate phase as well as the cross-linking of the polycarboxylic acid by aluminum and calcium ions played an important role in the hardening of glass-ionomer cement. The objective of this study was to investigate the structural change during hardening of the cements by means of infrared (IR) spectroscopy and solid-state nuclear magnetic resonance (NMR) spectroscopy and to confirm the role of the silica phase in the hardening of the cement. For that purpose, we measured the change in compressive strength of an experimental glass-ionomer cement, two commercial glass-ionomer cements, and a polycarboxylate cement and carried out 29Si and 27Al NMR analyses of the cement samples after the strength measurement. In the IR spectra during hardening, a characteristic band of the silicate network around 1000 cm-1 shifted toward high frequency with time. The spectrum after hardening was similar to that for a hydrated amorphous silica structure. The 27Al NMR analysis showed that Al3+ ion was tetrahedrally coordinated by oxygen in the original glass, but a part of the Al3+ ion was octahedrally coordinated after hardening to form Al polyacrylate gel. The chemical shift of Si in the 29Si NMR spectra also changed during hardening. The variation in the chemical shift reflected the structural change in the silicate network. The initial increase in compressive strength of the cement was mainly caused by polycarboxylate gel formation. However, it was concluded that the reconstruction of the silicate network contributed to the increase in strength with time during the period after the gelation by cross-linking was completed.

  9. Stress corrosion of high strength aluminum alloys.

    NASA Technical Reports Server (NTRS)

    Cocks, F. H.; Brummer, S. B.

    1972-01-01

    An investigation has been carried out to examine the relationship of the observed chemical and mechanical properties of Al-Cu and Al-Zn-Mg alloys to the stress corrosion mechanisms which dominate in each case. Two high purity alloys and analogous commercial alloys were selected. Fundamental differences between the behavior of Al-Cu and of Al-Zn-Mg alloys were observed. These differences in the corrosion behavior of the two types of alloys are augmented by substantial differences in their mechanical behavior. The relative cleavage energy of the grain boundaries is of particular importance.

  10. Physical processes at high field strengths

    SciTech Connect

    Rhodes, C.K.

    1986-01-01

    Measurements of the radiation produced by the high field interaction with the rare gases have revealed the presence of both copious harmonic production and fluorescence. The highest harmonic observed was the seventeenth (14.6 rm) in Ne, the shortest wavelength ever produced by that means. Strong fluorescence was seen in Ar, Kr, and Xe with the shortest wavelengths observed being below 10 nm. Furthermore, radiation from inner-shell excited configurations in Xe, specifically the 4d/sup 9/5s5p ..-->.. 4d/sup 10/5s manifold at approx. 17.7 nm, was detected. The behaviors of the rare gases with respect to multiquantum ionization, harmonic production, and fluorescence were found to be correlated so that the materials fell into two groups, He and Ne in one and Ar, Kr, and Xe in the other. These experimental findings, in alliance with other studies on inner-shell decay processes, give evidence for a role of atomic correlations in a direct nonlinear process of inner-shell excitation. It is expected that an understanding of these high-field processes will enable the generation of stimulated emission in the x-ray range. 59 refs., 6 figs., 5 tabs.

  11. Investigation of ultra violet (UV) resistance for high strength fibers

    NASA Astrophysics Data System (ADS)

    Said, M. A.; Dingwall, Brenda; Gupta, A.; Seyam, A. M.; Mock, G.; Theyson, T.

    Ultra long duration balloons (ULDB), currently under development by the National Aeronautics and Space Administration (NASA), requires the use of high strength fibers in the selected super-pressure pumpkin design. The pumpkin shape balloon concept allows clear separation of the load transferring functions of the major structural elements of the pneumatic envelope, the tendons and the film. Essentially, the film provides the gas barrier and transfers only local pressure load to the tendons. The tendons, in the mean time, provide the global pressure containing strength. In that manner, the strength requirement for the film only depends on local parameters. The tendon is made of p-phenylene-2,6-benzobisoxazole (PBO) fibers, which is selected due to its high strength to weight ratio when compared to other high performance, commercially available, fibers. High strength fibers, however, are known to degrade upon exposure to light, particularly at short wavelengths. This paper reports the results of an investigation of the resistance of four commercial high strength fibers to ultra violet (UV) exposure. The results indicate that exposing high strength fibers in continuous yarn form to UV led to serious loss in strength of the fibers except for Spectra® fibers. The adverse changes in mechanical behavior occurred over short duration of exposure compared to the 100 day duration targeted for these missions. UV blocking finishes to improve the UV resistance of these fibers are being investigated. The application of these specially formulated coatings is expected to lead to significant improvement of the UV resistance of these high performance fibers. In this publication, we report on the mechanical behavior of the fibers pre- and post-exposure to UV, but without application of the blocking finishes.

  12. Factors Affecting the Inclusion Potency for Acicular Ferrite Nucleation in High-Strength Steel Welds

    NASA Astrophysics Data System (ADS)

    Kang, Yongjoon; Jeong, Seonghoon; Kang, Joo-Hee; Lee, Changhee

    2016-06-01

    Factors affecting the inclusion potency for acicular ferrite nucleation in high-strength weld metals were investigated and the contribution of each factor was qualitatively evaluated. Two kinds of weld metals with different hardenabilities were prepared, in both, MnTi2O4-rich spinel formed as the predominant inclusion phase. To evaluate the factors determining the inclusion potency, the inclusion characteristics of size, phase distribution in the multiphase inclusion, orientation relationship with ferrite, and Mn distribution near the inclusion were analyzed. Three factors affecting the ferrite nucleation potency of inclusions were evaluated: the Baker-Nutting (B-N) orientation relationship between ferrite and the inclusion; the formation of an Mn-depleted zone (MDZ) near the inclusion; and the strain energy around the inclusion. Among these, the first two factors were found to be the most important. In addition, it was concluded that the increased chemical driving force brought about by the formation of an MDZ contributed more to the formation of acicular ferrite in higher-strength weld metals, because the B-N orientation relationship between ferrite and the inclusion was less likely to form as the transformation temperature decreased.

  13. Fatigue Performance of Advanced High-Strength Steels (AHSS) GMAW Joints

    SciTech Connect

    Feng, Zhili; Sang, Yan; Jiang, Cindy; Chiang, Dr. John; Kuo, Dr. Min

    2009-01-01

    The fatigue performance of gas metal arc welding (GMAW) joints of advanced high strength steels (AHSS) are compared and analyzed. The steel studied included a number of different grades of AHSS and baseline mild steels: DP600, DP780, DP980, M130, M220, solution annealed boron steel, fully hardened boron steels, HSLA690 and DR210 (a mild steel). Fatigue testing was conducted under a number of nominal stress ranges to obtain the S/N curves of the weld joints. A two-phase analytical model is developed to predict the fatigue performance of AHSS welds. It was found that there are appreciable differences in the fatigue S/N curves among different AHSS joints made using the same welding practices, suggesting that the local microstructure in the weld toe and root region plays non-negligible role in the fatigue performance of AHSS welds. Changes in weld parameters can influence the joint characteristics which in turn influence fatigue life of the weld joints, particularly of those of higher strength AHSS. The analytical model is capable of reasonably predicting the fatigue performance of welds made with various steel grades in this study.

  14. Radiation-hardened asphaltite composites

    SciTech Connect

    Persinen, A.A.; Trubyatchinskaya, V.N.; Tolmacheva, T.P.

    1981-07-20

    A method is proposed for the production of an asphaltite block material with good physical and mechanical properties. The composite contains epoxide resin, acrylic acid, and asphaltite and radiation or radiation - thermal hardening was used. ED-16 epoxide resin with 490 molecular weight and 17.6% epoxide groups or EBF-23 epoxide resin produced from water-soluble shale phenols with 750 to 800 molecular weight and 21 to 22% epoxide groups was used as the epoxide resin. Analysis of the IR spectra showed that a rapid reaction of acrylic acid with epoxide resin occurs upon the action of ionizing radiation. The mechanical testing showed that the uniform samples obtained had rather high strength and hardness; high heat resistance and low water absorption was noted. The composites are chemically resistant towards concentrated HCl, water, acetone, and benzene. The studies indicated cross-linking occurs as a consequence of the reaction of the epoxide ring with acrylic acid. Asphaltite adds by means of the short alkyl substituents and guinoid structures. 4 tables. (DP)

  15. High strength nickel-chromium-iron austenitic alloy

    DOEpatents

    Gibson, Robert C.; Korenko, Michael K.

    1980-01-01

    A solid solution strengthened Ni-Cr-Fe alloy capable of retaining its strength at high temperatures and consisting essentially of 42 to 48% nickel, 11 to 13% chromium, 2.6 to 3.4% niobium, 0.2 to 1.2% silicon, 0.5 to 1.5% vanadium, 2.6 to 3.4% molybdenum, 0.1 to 0.3% aluminum, 0.1 to 0.3% titanium, 0.02 to 0.05% carbon, 0.002 to 0.015% boron, up to 0.06 zirconium, and the balance iron. After solution annealing at 1038.degree. C. for one hour, the alloy, when heated to a temperature of 650.degree. C., has a 2% yield strength of 307 MPa, an ultimate tensile strength of 513 MPa and a rupture strength of as high as 400 MPa after 100 hours.

  16. Corrosion fatigue of high strength fastener materials in seawater

    NASA Technical Reports Server (NTRS)

    Tipton, D. G.

    1983-01-01

    Environmental effects which significantly reduce the fatigue life of metals are discussed. Corrosion fatigue is a major concern in the engineering application of high strength fasteners in marine environments. The corrosion fatigue failure of an AISI 41L4O high strength steel blade to hub attachment bolt at the MOD-OA 200 kW wind turbine generator was investigated. The reduction of fatigue strength of AISI 41L4O in marine environments and to obtain similar corrosion fatigue data for candidate replacement materials was studied. The AISI 4140, PH 13-8Mo stainless steel, alloy 718 and alloy MP-35N were tested in axial fatigue at a frequency of 20 Hz in dry air and natural seawater. The fatigue data are fitted by regression equations to allow determination of fatigue strength for a given number of cycles to failure.

  17. Corrosion fatigue of high strength fastener materials in seawater

    NASA Astrophysics Data System (ADS)

    Tipton, D. G.

    1983-12-01

    Environmental effects which significantly reduce the fatigue life of metals are discussed. Corrosion fatigue is a major concern in the engineering application of high strength fasteners in marine environments. The corrosion fatigue failure of an AISI 41L4O high strength steel blade to hub attachment bolt at the MOD-OA 200 kW wind turbine generator was investigated. The reduction of fatigue strength of AISI 41L4O in marine environments and to obtain similar corrosion fatigue data for candidate replacement materials was studied. The AISI 4140, PH 13-8Mo stainless steel, alloy 718 and alloy MP-35N were tested in axial fatigue at a frequency of 20 Hz in dry air and natural seawater. The fatigue data are fitted by regression equations to allow determination of fatigue strength for a given number of cycles to failure.

  18. Spontaneous Radiation Emission from Short, High Field Strength Insertion Devices

    SciTech Connect

    Geoffrey Krafft

    2005-09-15

    Since the earliest papers on undulaters were published, it has been known how to calculate the spontaneous emission spectrum from ''short'' undulaters when the magnetic field strength parameter is small compared to unity, or in ''single'' frequency sinusoidal undulaters where the magnetic field strength parameter is comparable to or larger than unity, but where the magnetic field amplitude is constant throughout the undulater. Fewer general results have been obtained in the case where the insertion device is both short, i.e., the magnetic field strength parameter changes appreciably throughout the insertion device, and the magnetic field strength is high enough that ponderomotive effects, radiation retardation, and harmonic generation are important physical phenomena. In this paper a general method is presented for calculating the radiation spectrum for short, high-field insertion devices. It is used to calculate the emission from some insertion device designs of recent interest.

  19. Role of interfaces i nthe design of ultra-high strength, radiation damage tolerant nanocomposites

    SciTech Connect

    Misra, Amit; Wang, Yongqiang; Nastasi, Michael A; Baldwin, Jon K; Wei, Qiangmin; Li, Nan; Mara, Nathan; Zhang, Xinghang; Fu, Engang; Anderoglu, Osman; Li, Hongqi; Bhattacharyya, Dhriti

    2010-12-09

    The combination of high strength and high radiation damage tolerance in nanolaminate composites can be achieved when the individual layers in these composites are only a few nanometers thick and contain special interfaces that act both as obstacles to slip, as well as sinks for radiation-induced defects. The morphological and phase stabilities and strength and ductility of these nano-composites under ion irradiation are explored as a function of layer thickness, temperature and interface structure. Magnetron sputtered metallic multilayers such as Cu-Nb and V-Ag with a range of individual layer thickness from approximately 2 nm to 50 nm and the corresponding 1000 nm thick single layer films were implanted with helium ions at room temperature. Cross-sectional Transmission Electron Microscopy (TEM) was used to measure the distribution of helium bubbles and correlated with the helium concentration profile measured vis ion beam analysis techniques to obtain the helium concentration at which bubbles are detected in TEM. It was found that in multilayers the minimum helium concentration to form bubbles (approximately I nm in size) that are easily resolved in through-focus TEM imaging was several atomic %, orders of magnitude higher than that in single layer metal films. This observation is consistent with an increased solubility of helium at interfaces that is predicted by atomistic modeling of the atomic structures of fcc-bcc interfaces. At helium concentrations as high as 7 at.%, a uniform distribution of I nm diameter bubbles results in negligible irradiation hardening and loss of deformability in multi layers with layer thicknesses of a few nanometers. The control of atomic structures of interfaces to produce high helium solubility at interfaces is crucial in the design of nano-composite materials that are radiation damage tolerant. Reduced radiation damage also leads to a reduction in the irradiation hardening, particularly at layer thickness of approximately 5 run

  20. High Strength Development at Incompatible Semicrystalline Polymer-Polymer Interfaces

    NASA Astrophysics Data System (ADS)

    Hong, C. H.; Wool, Richard

    2007-03-01

    For incompatible A/B interfaces, the strength G1c is related to the equilibrium width w (normalized to the tube diameter) of the interface by G1c/G* = (w-1), where G* is the virgin strength [R.P. Wool, C.R, Chimie, 9 (2006) 25]. However, the interface strength is quite weak due to very limited interdiffusion. The mechanism of high strength development of a series of thermoplastic polyurethane elastomers (TPU) bonding with ethylene vinyl alcohol copolymers (EVOH) was investigated. During cool down of the A/B interface in the co-extruded melt, there exits a unique process window---the α-β window-which promotes considerable strength development. We used the differences in melting points and the volume contraction during asymmetric crystallization to generate influxes (σ nano-nails/unit area), where an influx occurs by the fluid being pulled into the crystallizing side. TPU samples with higher degree of crystallization typically exhibited higher peel strengths, due to the formation of both inter- and intra- spherulitic influxes of nano-dimension across the interface. The peel energy now behaves as G1c˜ σL^2, where L is the length of the influx and L>>w. Annealing between the α and βt relaxation temperatures of the EVOH generated additional influxes which provided significant connectivity and peel strength.

  1. Mechanical behavior of precipitation hardenable steels exposed to highly corrosive environment

    NASA Technical Reports Server (NTRS)

    Rosa, Ferdinand

    1994-01-01

    Unexpected occurrences of failures, due to stress corrosion cracking (SCC) of structural components, indicate a need for improved characterization of materials and more advanced analytical procedures for reliably predicting structures performance. Accordingly, the purpose of this study was to determine the stress corrosion susceptibility of 15 - 5 PH steel over a wide range of applied strain rates in a highly corrosive environment. The selected environment for this investigation was a 3.5 percent NaCl aqueous solution. The material selected for the study was 15 - 5 PH steel in the H 900 condition. The Slow Strain Rate technique was used to test the metallic specimens.

  2. Extracellular bone matrix exhibits hardening elastoplasticity and more than double cortical strength: Evidence from homogeneous compression of non-tapered single micron-sized pillars welded to a rigid substrate.

    PubMed

    Luczynski, Krzysztof W; Steiger-Thirsfeld, Andreas; Bernardi, Johannes; Eberhardsteiner, Josef; Hellmich, Christian

    2015-12-01

    We here report an improved experimental technique for the determination of Young׳s modulus and uniaxial strength of extracellular bone matrix at the single micrometer scale, giving direct access to the (homogeneous) deformation (or strain) states of the tested samples and to the corresponding mechanically recoverable energy, called potential or elastic energy. Therefore, a new protocol for Focused Ion Beam milling of prismatic non-tapered micropillars, and attaching them to a rigid substrate, was developed. Uniaxial strength turns out as at least twice that measured macroscopically, and respective ultimate stresses are preceded by hardening elastoplastic states, already at very low load levels. The unloading portion of quasi-static load-displacement curves revealed Young׳s modulus of 29GPa in bovine extracellular bone matrix. This value is impressively confirmed by the corresponding prediction of a multiscale mechanics model for bone, which has been comprehensively validated at various other observation scales, across tissues from the entire vertebrate animal kingdom. PMID:25842157

  3. Surface hardening induced by high flux plasma in tungsten revealed by nano-indentation

    NASA Astrophysics Data System (ADS)

    Terentyev, D.; Bakaeva, A.; Pardoen, T.; Favache, A.; Zhurkin, E. E.

    2016-08-01

    Surface hardness of tungsten after high flux deuterium plasma exposure has been characterized by nanoindentation. The effect of plasma exposure was rationalized on the basis of available theoretical models. Resistance to plastic penetration is enhanced within the 100 nm sub-surface region, attributed to the pinning of geometrically necessary dislocations on nanometric deuterium cavities - signature of plasma-induced defects and deuterium retention. Sub-surface extension of thereby registered plasma-induced damage is in excellent agreement with the results of alternative measurements. The study demonstrates suitability of nano-indentation to probe the impact of deposition of plasma-induced defects in tungsten on near surface plasticity under ITER-relevant plasma exposure conditions.

  4. High Strength and Thermally Stable Nanostructured Magnesium Alloys and Nanocomposites

    NASA Astrophysics Data System (ADS)

    Chang, Yuan-Wei

    Magnesium and its alloys are currently in the spotlight of global research because of the need to limit energy consumption and reduce the environmental impact. In particular, their low densities compared to other structural metals make them a very attractive alternative in the automobile and aerospace industries. However, their low strength compared to other structural materials (e.g. Al and steels) has limited their widespread application. This dissertation presents the results of developing and investigation of a high strength nanostructured magnesium-aluminum alloy and composite. The nanostructured magnesium alloy is prepared by cryomilling and consolidated by spark-plasma-sintering. Focused ion beam is used to prepare micropillars with different diameters ranging from 1.5 to 8 mum and micro-compression test is conducted by nanoindenter in order to evaluate the mechanical properties. The yield strength obtained in the present study is around three times higher than conventional magnesium alloys (120 MPa vs. 370 MPa). The yield strength of the nanostructured magnesium alloy is further improved through hot extrusion, resulting in a yield strength of 550 MPa and an ultimate strength of 580 MPa. The nanostructured magnesium alloy exhibits a strong size-dependence, and a significant improvement in strength is observed when the pillar diameter is reduced to below 3.5 mum. The deformation mechanisms of the compressed pillars were characterized using transmission electron microscopy. The size-induced strengthening is attributed to a less number of dislocation sources along with a higher activity of non-basal deformation mechanisms. We have also developed a high strength and thermally stable nanostructured magnesium composite by adding diamantane. A yield strength of 500 MPa is achieved, moreover, excellent thermal stability is demonstrated in the magnesium alloy containing diamantanes. The strength and grain size are thermally stable after annealing at 400°C for 100

  5. A universal fracture criterion for high-strength materials

    PubMed Central

    Qu, Rui Tao; Zhang, Zhe Feng

    2013-01-01

    Recently developed advanced high-strength materials like metallic glasses, nanocrystalline metallic materials, and advanced ceramics usually fracture in a catastrophic brittle manner, which makes it quite essential to find a reasonable fracture criterion to predict their brittle failure behaviors. Based on the analysis of substantial experimental observations of fracture behaviors of metallic glasses and other high-strength materials, here we developed a new fracture criterion and proved it effective in predicting the critical fracture conditions under complex stress states. The new criterion is not only a unified one which unifies the three classical failure criteria, i.e., the maximum normal stress criterion, the Tresca criterion and the Mohr-Coulomb criterion, but also a universal criterion which has the ability to describe the fracture mechanisms of a variety of different high-strength materials under various external loading conditions.

  6. [Hardening of dental instruments].

    PubMed

    Gerasev, G P

    1981-01-01

    The possibility of prolonging the service life of stomatological instruments by the local hardening of their working parts is discussed. Such hardening should be achieved by using hard and wear-resistant materials. The examples of hardening dental elevators and hard-alloy dental drills are given. New trends in the local hardening of instruments are the treatment of their working parts with laser beams, the application of coating on their surface by the gas-detonation method. The results of research work and trials are presented.

  7. Uncertainties in obtaining high reliability from stress-strength models

    NASA Technical Reports Server (NTRS)

    Neal, Donald M.; Matthews, William T.; Vangel, Mark G.

    1992-01-01

    There has been a recent interest in determining high statistical reliability in risk assessment of aircraft components. The potential consequences are identified of incorrectly assuming a particular statistical distribution for stress or strength data used in obtaining the high reliability values. The computation of the reliability is defined as the probability of the strength being greater than the stress over the range of stress values. This method is often referred to as the stress-strength model. A sensitivity analysis was performed involving a comparison of reliability results in order to evaluate the effects of assuming specific statistical distributions. Both known population distributions, and those that differed slightly from the known, were considered. Results showed substantial differences in reliability estimates even for almost nondetectable differences in the assumed distributions. These differences represent a potential problem in using the stress-strength model for high reliability computations, since in practice it is impossible to ever know the exact (population) distribution. An alternative reliability computation procedure is examined involving determination of a lower bound on the reliability values using extreme value distributions. This procedure reduces the possibility of obtaining nonconservative reliability estimates. Results indicated the method can provide conservative bounds when computing high reliability. An alternative reliability computation procedure is examined involving determination of a lower bound on the reliability values using extreme value distributions. This procedure reduces the possibility of obtaining nonconservative reliability estimates. Results indicated the method can provide conservative bounds when computing high reliability.

  8. Effects of Rock High Pressure Strength on Penetration

    NASA Astrophysics Data System (ADS)

    Huang, Hongfa

    2011-06-01

    Perforating of oil/gas well creates communication tunnel between reservoir and wellbore. Shaped charges are widely used as perforators in oilfield industry. The liners of the charges are mostly made of powder metal to prevent solid slug clogging the entrance hole of well casing or locking the hole in perforating gun. High speed jet from the shaped charge pierces through perforating gun, well fluid, well casing, and then penetrates into reservoir formation. Prediction of jet penetration in reservoir rock is critical in modeling of well production. An analytical penetration model developed for solid rod by Tate and Alekseevskii is applied. However, strength of formation rock at high pressure needs to be measured. Lateral stress gauge measurements in plate impact tests are conducted. Piezoelectric pressure gauges are imbedded in samples to measure the longitudinal and transverse stress. The two stresses provide Hugoniot and material compressive strength. Indiana limestone, a typical rock in perforation testing, is selected as target sample material in the plate impact tests. Since target strength effect on penetration is more significant in late stage of penetration when the strength of material becomes significant compared to the impact pressure, all the impact tests are focused on lower impact pressure up to 9 GPa. The measurements show that the strength increases with impact pressure. The results are applied in the penetration calculations. The final penetration matches testing data very well.

  9. The Tensile Behavior of High-Strength Carbon Fibers.

    PubMed

    Langston, Tye

    2016-08-01

    Carbon fibers exhibit exceptional properties such as high stiffness and specific strength, making them excellent reinforcements for composite materials. However, it is difficult to directly measure their tensile properties and estimates are often obtained by tensioning fiber bundles or composites. While these macro scale tests are informative for composite design, their results differ from that of direct testing of individual fibers. Furthermore, carbon filament strength also depends on other variables, including the test length, actual fiber diameter, and material flaw distribution. Single fiber tensile testing was performed on high-strength carbon fibers to determine the load and strain at failure. Scanning electron microscopy was also conducted to evaluate the fiber surface morphology and precisely measure each fiber's diameter. Fiber strength was found to depend on the test gage length and in an effort to better understand the overall expected performance of these fibers at various lengths, statistical weak link scaling was performed. In addition, the true Young's modulus was also determined by taking the system compliance into account. It was found that all properties (tensile strength, strain to failure, and Young's modulus) matched very well with the manufacturers' reported values at 20 mm gage lengths, but deviated significantly at other lengths.

  10. The Tensile Behavior of High-Strength Carbon Fibers.

    PubMed

    Langston, Tye

    2016-08-01

    Carbon fibers exhibit exceptional properties such as high stiffness and specific strength, making them excellent reinforcements for composite materials. However, it is difficult to directly measure their tensile properties and estimates are often obtained by tensioning fiber bundles or composites. While these macro scale tests are informative for composite design, their results differ from that of direct testing of individual fibers. Furthermore, carbon filament strength also depends on other variables, including the test length, actual fiber diameter, and material flaw distribution. Single fiber tensile testing was performed on high-strength carbon fibers to determine the load and strain at failure. Scanning electron microscopy was also conducted to evaluate the fiber surface morphology and precisely measure each fiber's diameter. Fiber strength was found to depend on the test gage length and in an effort to better understand the overall expected performance of these fibers at various lengths, statistical weak link scaling was performed. In addition, the true Young's modulus was also determined by taking the system compliance into account. It was found that all properties (tensile strength, strain to failure, and Young's modulus) matched very well with the manufacturers' reported values at 20 mm gage lengths, but deviated significantly at other lengths. PMID:27278219

  11. AISI/DOE Technology Roadmap Program: Characterization of Fatigue and Crash Performance of New Generation High Strength Steels for Automotive Applications

    SciTech Connect

    Brenda Yan; Dennis Urban

    2003-04-21

    A 2-year project (2001-2002) to generate fatigue and high strain data for a new generation of high strength steels (HSS) has been completed in December 2002. The project tested eleven steel grades, including Dual Phase (DP) steels, Transformation-Induced Plasticity (TRIP) steels, Bake Hardenable (BH) steels, and conventional High Strength Low Alloy (HSLA) steels. All of these steels are of great interest in automotive industry due to the potential benefit in weight reduction, improved fuel economy, enhanced crash energy management and total system cost savings. Fatigue behavior includes strain controlled fatigue data notch sensitivity for high strength steels. High strain rate behavior includes stress-strain data for strain rates from 0.001/s to 1000/s, which are considered the important strain rate ranges for crash event. The steels were tested in two phases, seven were tested in Phase 1 and the remaining steels were tested in Phase. In a addition to the fatigue data and high st rain rate data generated for the steels studied in the project, analyses of the testing results revealed that Advanced High Strength Steels (AHSS) exhibit significantly higher fatigue strength and crash energy absorption capability than conventional HSS. TRIP steels exhibit exceptionally better fatigue strength than steels of similar tensile strength but different microstructure, for conditions both with or without notches present

  12. High-strength porous carbon and its multifunctional applications

    DOEpatents

    Wojtowicz, Marek A; Rubenstein, Eric P; Serio, Michael A; Cosgrove, Joseph E

    2013-12-31

    High-strength porous carbon and a method of its manufacture are described for multifunctional applications, such as ballistic protection, structural components, ultracapacitor electrodes, gas storage, and radiation shielding. The carbon is produced from a polymer precursor via carbonization, and optionally by surface activation and post-treatment.

  13. Fabrication Routes for High Strength High Conductivity Wires

    SciTech Connect

    Han, K.; Embury, J.D.; Sims, J.R.; Pantsyrnyi, V.I.; Shikov, A.; Bochvar, A.A.

    1998-10-01

    The development of suitable wires for magnet windings requires both the attainment of suitable combinations of properties (electrical conductivity and strength), the development of a production route capable of fabricating suitable quantity of wire of required dimension (5.2x7.6mm{sup 2} cross-section and 120 m in length) and a product with acceptable fabricability, joinability and service life. In this survey, the authors consider methods of producing suitable wire products by the codeformation of in-situ composites. This will include details of the quality control of the processing of Cu-Ag and Cu-Nb and the assessment of their detailed mechanical properties.

  14. High strength graphite and method for preparing same

    DOEpatents

    Overholser, Lyle G.; Masters, David R.; Napier, John M.

    1976-01-01

    High strength graphite is manufactured from a mixture of a particulate filler prepared by treating a particulate carbon precursor at a temperature in the range of about 400.degree. to 1000.degree. C., an organic carbonizable binder, and green carbonizable fibers in a concentration of not more than 2 weight per cent of the filler. The use of the relatively small quantity of green fibers provides a substantial increase in the flexural strength of the graphite with only a relatively negligible increase in the modulus of elasticity.

  15. Experimental study of self-compacted concrete in hardened state

    NASA Astrophysics Data System (ADS)

    Parra Costa, Carlos Jose

    The main aim of this work is to investigate the hardened behaviour of Self-Compacting Concrete (SCC). Self compacting Concrete is a special concrete that can flow in its gravity and fill in the formwork alone to its self-weight, passing through the bars and congested sections without the need of any internal or external vibration, while maintaining adequate homogeneity. SCC avoids most of the materials defects due to bleeding or segregation. With regard to its composition, SCC consists of the same components as traditional vibrated concrete (TC), but in different proportions. Thus, the high amount of superplasticizer and high powder content have to taken into account. The high workability of SCC does not allow to use traditional methods for measuring the fresh state properties, so new tests has developed (slump-flow, V-funnel, L-box, and others). The properties of the hardened SCC, which depend on the mix design, should be different from traditional concrete. In order to study the possible modifications of SCC hardened state properties, a review of the bibliography was done. The state of art was focused on the mechanical behaviour (compressive strength, tension strength and elastic modulus), on bond strength of reinforcement steel, and on material durability. The experimental program consisted in the production of two types of concretes: Self-Compacting Concrete and Traditional Concrete. Four different dosages was made with three different water/cement ratio and two strength types of Portland cement, in order to cover the ordinary strength used in construction. Based on this study it can be concluded that compressive strength of SCC and TC are similar (the differences are lesser than 10%), whereas the tensile strength of TC are up to 18% higher. The values of elastic modulus of both concrete are similar. On the other hand, in the ultimate state the bond strength of SCC and TC is similar, although SCC shows higher bond stiffness in the serviceability state (initial

  16. Modifications of the Response of Materials to Shock Loading by Age Hardening

    NASA Astrophysics Data System (ADS)

    Millett, Jeremy C. F.

    2015-10-01

    The shock response of two age-hardened alloys, aluminum 6061 and copper-2 wt pct beryllium (CuBe), has been investigated in terms of their microstructual state; either solution treated or age hardened. While age hardening induces large increases in strength at quasi-static strain rates, age hardening does not produce the same magnitude of strength increase during shock loading. Examination of the shocked microstructures (of 6061) indicates that the presence of a fine distribution of precipitates throughout the microstructure hinders the motion and generation of dislocations and hence reduces the strain-rate sensitivity of the aged material, thus allowing the properties of the solution-treated state to approach those of the aged. It has also been observed that the shear strength of solution-treated CuBe is near identical to that of pure copper. It is suggested that this is the result of two competing processes; large lattice strains as beryllium substitutes onto the copper lattice inducing a high degree of solution strengthening acting against a reduction in shear strength caused by twinning in the alloy.

  17. Microcracking and engineering properties of high-strength concrete

    NASA Astrophysics Data System (ADS)

    Carrasquillo, R. L.

    1980-03-01

    The differences in mechanical properties between high strength and normal strength concretes are established and those differences are explained in terms of differences in observed internal microcracking in concrete at different stages of loading. Concretes made using gravel and crushed limestone coarse aggregates at each of three different strength levels ranging from 4,000 psi to 11,000 psi were studied. The results of the microcracking study and the study of the mechanical properties are presented. A criterion for definition of failure in uniaxial compression for the concretes tested is presented. Failure is considered to occur at the discontinuity point defined as that point when a self propagating microcracking mechanism is developed eventually causing disruptive failure with time. The predicted stress and strain ratios at discontinuity based on the microcracking study are compared to those at which sudden changes occur in the Poisson's ratio and volume change curves.

  18. Age hardening of 6061/alumina-silica fiber composite

    SciTech Connect

    Khangaonkar, P.R.; Shamsul, J.B.; Azmi, R.

    1994-12-31

    Continuous alumina-silica fiber (Altex of Sumitomo) which yields high performance composites with some aluminium alloys was tried for squeeze cast 6061 based composites with volume fractions of 0.5 and 0.32, and the matrix microhardness and resistivity changes during age hardening were studied. The matrix in the composites hardened much more than the unreinforced alloy. Microhardness increases of up to 70 VPN above the solution treated condition at various aging temperatures were observed. The resistivity variation indicated an appreciable state of internal stress which continued to persist even when hardness fell by overaging. Energy dispersive X-ray analysis indicated that the regions close to the fibers had a higher silicon content than the matrix, and amorphous silica in the fiber may have a role in the formation of an enriched layer which may help the bonding and strength in the composite.

  19. Determination of Constant Parameters of Copper as Power-Law Hardening Material at Different Test Conditions

    NASA Astrophysics Data System (ADS)

    Kowser, Md. A.; Mahiuddin, Md.

    2014-11-01

    In this paper a technique has been developed to determine constant parameters of copper as a power-law hardening material by tensile test approach. A work-hardening process is used to describe the increase of the stress level necessary to continue plastic deformation. A computer program is used to show the variation of the stress-strain relation for different values of stress hardening exponent, n and power-law hardening constant, α . Due to its close tolerances, excellent corrosion resistance and high material strength, in this analysis copper (Cu) has been selected as the material. As a power-law hardening material, Cu has been used to compute stress hardening exponent, n and power-law hardening constant, α from tensile test experiment without heat treatment and after heat treatment. A wealth of information about mechanical behavior of a material can be determined by conducting a simple tensile test in which a cylindrical specimen of a uniform cross-section is pulled until it ruptures or fractures into separate pieces. The original cross sectional area and gauge length are measured prior to conducting the test and the applied load and gauge deformation are continuously measured throughout the test. Based on the initial geometry of the sample, the engineering stress-strain behavior (stress-strain curve) can be easily generated from which numerous mechanical properties, such as the yield strength and elastic modulus, can be determined. A universal testing machine is utilized to apply the load in a continuously increasing (ramp) manner according to ASTM specifications. Finally, theoretical results are compared with these obtained from experiments where the nature of curves is found similar to each other. It is observed that there is a significant change of the value of n obtained with and without heat treatment it means the value of n should be determined for the heat treated condition of copper material for their applications in engineering fields.

  20. NEW HIGH STRENGTH AND FASTER DRILLING TSP DIAMOND CUTTERS

    SciTech Connect

    Robert Radtke

    2006-01-31

    The manufacture of thermally stable diamond (TSP) cutters for drill bits used in petroleum drilling requires the brazing of two dissimilar materials--TSP diamond and tungsten carbide. The ENDURUS{trademark} thermally stable diamond cutter developed by Technology International, Inc. exhibits (1) high attachment (shear) strength, exceeding 345 MPa (50,000 psi), (2) TSP diamond impact strength increased by 36%, (3) prevents TSP fracture when drilling hard rock, and (4) maintains a sharp edge when drilling hard and abrasive rock. A novel microwave brazing (MWB) method for joining dissimilar materials has been developed. A conventional braze filler metal is combined with microwave heating which minimizes thermal residual stress between materials with dissimilar coefficients of thermal expansion. The process results in preferential heating of the lower thermal expansion diamond material, thus providing the ability to match the thermal expansion of the dissimilar material pair. Methods for brazing with both conventional and exothermic braze filler metals have been developed. Finite element modeling (FEM) assisted in the fabrication of TSP cutters controllable thermal residual stress and high shear attachment strength. Further, a unique cutter design for absorbing shock, the densification of otherwise porous TSP diamond for increased mechanical strength, and diamond ion implantation for increased diamond fracture resistance resulted in successful drill bit tests.

  1. Hydrogen Embrittlement of Automotive Advanced High-Strength Steels

    NASA Astrophysics Data System (ADS)

    Lovicu, Gianfranco; Bottazzi, Mauro; D'Aiuto, Fabio; De Sanctis, Massimo; Dimatteo, Antonella; Santus, Ciro; Valentini, Renzo

    2012-11-01

    Advanced high-strength steels (AHSS) have a better combination between strength and ductility than conventional HSS, and higher crash resistances are obtained in concomitance with weight reduction of car structural components. These steels have been developed in the last few decades, and their use is rapidly increasing. Notwithstanding, some of their important features have to be still understood and studied in order to completely characterize their service behavior. In particular, the high mechanical resistance of AHSS makes hydrogen-related problems a great concern for this steel grade. This article investigates the hydrogen embrittlement (HE) of four AHSS steels. The behavior of one transformation induced plasticity (TRIP), two martensitic with different strength levels, and one hot-stamping steels has been studied using slow strain rate tensile (SSRT) tests on electrochemically hydrogenated notched samples. The embrittlement susceptibility of these AHSS steels has been correlated mainly to their strength level and to their microstructural features. Finally, the hydrogen critical concentrations for HE, established by SSRT tests, have been compared to hydrogen contents absorbed during the painting process of a body in white (BIW) structure, experimentally determined during a real cycle in an industrial plant.

  2. Measurement of Strength at High Pressures Using Oblique Shock Waves

    NASA Astrophysics Data System (ADS)

    Stolyar, Victoria; Ravichandran, Guruswami; Alexander, Scott

    2013-06-01

    At high pressures and high strain rates, the measurement of strength is important to many implications including planetary impact and inertial confinement fusion. Understanding how strength depends on pressure allows for the characterization of materials and validation of constitutive models. Slotted barrel guns have traditionally been used in experiments, such as the pressure-shear plate impact technique, to generate longitudinal and shear waves through an oblique impact. A new methodology for measuring material strength using normal impact (1-2 km/s) is described. In this configuration, a composite target is designed with an angled material of interest embedded into a driver material. This driver material is used to generate an oblique shock wave that is followed by a shear wave, due to the angled nature of the target material. Using shock polar analysis, the rear surface of the target is designed to be parallel to the transmitted shock wave in order to mitigate wave interactions at the rear surface. A window is used on the rear surface of the target to measure the in-situ particle velocities at the target-window interface. Using three VISAR measurements, the tangential and longitudinal particle velocities at the rear surface of the target are found from which the shear stress (strength) is inferred as a function of pressure. Results are presented for 6061-T6 Aluminum as well as Tantalum. Hydrocode simulations are used to predict the experimental results as well as characterize the wave interactions in the oblique wedge experiments.

  3. Mechanical Properties of Heat Affected Zone of High Strength Steels

    NASA Astrophysics Data System (ADS)

    Sefcikova, K.; Brtnik, T.; Dolejs, J.; Keltamaki, K.; Topilla, R.

    2015-11-01

    High Strength Steels became more popular as a construction material during last decade because of their increased availability and affordability. On the other hand, even though general use of Advanced High Strength Steels (AHSS) is expanding, the wide utilization is limited because of insufficient information about their behaviour in structures. The most widely used technique for joining steels is fusion welding. The welding process has an influence not only on the welded connection but on the area near this connection, the so-called heat affected zone, as well. For that reason it is very important to be able to determine the properties in the heat affected zone (HAZ). This area of investigation is being continuously developed in dependence on significant progress in material production, especially regarding new types of steels available. There are currently several types of AHSS on the world market. Two most widely used processes for AHSS production are Thermo-Mechanically Controlled Processing (TMCP) and Quenching in connection with Tempering. In the presented study, TMCP and QC steels grade S960 were investigated. The study is focused on the changes of strength, ductility, hardness and impact strength in heat affected zone based on the used amount of heat input.

  4. Oxidation resistant high creep strength austenitic stainless steel

    DOEpatents

    Brady, Michael P.; Pint, Bruce A.; Liu, Chain-Tsuan; Maziasz, Philip J.; Yamamoto, Yukinori; Lu, Zhao P.

    2010-06-29

    An austenitic stainless steel displaying high temperature oxidation and creep resistance has a composition that includes in weight percent 15 to 21 Ni, 10 to 15 Cr, 2 to 3.5 Al, 0.1 to 1 Nb, and 0.05 to 0.15 C, and that is free of or has very low levels of N, Ti and V. The alloy forms an external continuous alumina protective scale to provide a high oxidation resistance at temperatures of 700 to 800.degree. C. and forms NbC nanocarbides and a stable essentially single phase fcc austenitic matrix microstructure to give high strength and high creep resistance at these temperatures.

  5. Material Selection for an Ultra High Strength Steel Component Based on the Failure Criteria of CrachFEM

    SciTech Connect

    Kessler, L.; Beier, Th.; Werner, H.; Horstkott, D.; Dell, H.; Gese, H.

    2005-08-05

    An increasing use of combining more than one process step is noticed for coupling crash simulations with the results of forming operations -- mostly by inheriting the forming history like plastic strain and material hardening. Introducing a continuous failure model allows a further benefit of these coupling processes; it sometimes can even be the most attractive result of such a work. In this paper the algorithm CrachFEM for fracture prediction has been used to generate more benefit of the successive forming and crash simulations -- especially for ultra high strength steels. The choice and selection of the material grade in combination with the component design can therefore be done far before the prototyping might show an unsuccessful crash result; and in an industrial applicable manner.

  6. A Modified Johnson-Cook Model for Advanced High-Strength Steels Over a Wide Range of Temperatures

    NASA Astrophysics Data System (ADS)

    Qingdong, Zhang; Qiang, Cao; Xiaofeng, Zhang

    2014-12-01

    Advanced high-strength steel (AHSS) is widely used in automotive industry. In order to investigate the mechanical behaviors of AHSS over a wide range of temperatures, quasi-static tensile experiments were conducted at the temperatures from 298 to 1073 K on a Gleeble-3500 thermo-simulation machine. The results show that flow behaviors are affected by testing temperature significantly. In order to describe the flow features of AHSS, the Johnson-Cook (JC) model is employed. By introducing polynomial functions to consider the effects of temperature on hardening behavior, the JC model is modified and used to predict flow behavior of AHSS at different experimental conditions. The accuracy of the modified JC model is verified and the predicted flow stress is in good agreement with experimental results, which confirms that the modified JC model can give an accurate and precise estimate over a wide range of temperatures.

  7. Performance optimization and computational design of ultra-high strength gear steels

    NASA Astrophysics Data System (ADS)

    Tiemens, Benjamin Lee

    Rising power density requirements in transmission gear applications are swiftly outpacing gear redesign alone and will ultimately depend on better materials. Ni-Co secondary hardening steels show great promise for these applications due to their optimized combination of strength and toughness. The commercially available secondary hardening alloys GearMet RTM C61 and C67 have already demonstrated promising contact fatigue resistance, however bending fatigue is anticipated to be the primary failure mode limiting high power density gear applications. Single tooth bending fatigue testing was therefore completed on C61 and C67 spur gears to both assess the optimized performance of these alloys as well as identify defect populations currently limiting further advances. The resultant best-practice C61 spur gears in a shot peened and isotropic superfinished condition outperformed the top-ranking premium gear steel, demonstrating an approximate 15% improvement in bending fatigue endurance limit. Fatigue failures limiting further bending fatigue performance were identified to primarily initiate at three defect classes: shot peening-induced surface damage, subsurface inter-granular cleavage facets and Al2O3 and La2O2S inclusions. C67 spur gears did not show increased performance despite elevated surface hardness levels due to the inability of current shot peening practices to achieve maximum compressive stress in ultra-high hardness materials. In an effort to reduce the material cost of these alloys through minimization/elimination of cobalt alloying additions, BCC Cu precipitation was incorporated to offset ensuing losses in temper resistance by providing additional heterogeneous nucleation sites for the M2C strengthening dispersion. Fifty-pound experimental heats were made of four designed compositions. Peak hardness levels achieved during tempering fell on average 200 VHN short of the 900 VHN designed surface hardness. 3-dimensional local electrode atom probe (LEAP

  8. Grain refinement of high strength steels to improve cryogenic toughness

    NASA Technical Reports Server (NTRS)

    Rush, H. F.

    1985-01-01

    Grain-refining techniques using multistep heat treatments to reduce the grain size of five commercial high-strength steels were investigated. The goal of this investigation was to improve the low-temperature toughness as measured by Charpy V-notch impact test without a significant loss in tensile strength. The grain size of four of five alloys investigated was successfully reduced up to 1/10 of original size or smaller with increases in Charpy impact energy of 50 to 180 percent at -320 F. Tensile properties were reduced from 0 to 25 percent for the various alloys tested. An unexpected but highly beneficial side effect from grain refining was improved machinability.

  9. High ionic strength electrokinetics of melamine-formaldehyde latex.

    PubMed

    Kosmulski, Marek; Dahlsten, Per; Próchniak, Piotr; Rosenholm, Jarl B

    2006-09-15

    The electrokinetic potential of melamine-formaldehyde latex at high ionic strengths was measured by means of two different instruments. The present study confirms that the zeta potentials in 1 M 1-1 electrolyte solutions can be as high as +/-20 mV. The IEP of latex at low ionic strengths was at pH 11. The increase in the electrolyte concentration induced a shift in the IEP to low pH for all studied salts, and this indicates specific adsorption of the anions. The magnitude of the shift depends chiefly on the nature of the anion and increases in the series Cl < NO(3) = Br < I, and the nature of the cation (Li, Na, K, Cs) plays a rather insignificant role.

  10. NDE detectability of fatigue type cracks in high strength alloys

    NASA Technical Reports Server (NTRS)

    Christner, B. K.; Rummel, W. D.

    1983-01-01

    Specimens suitable for investigating the reliability of production nondestructive evaluation (NDE) to detect tightly closed fatigue cracks in high strength alloys representative of those materials used in spacecraft engine/booster construction were produced. Inconel 718 was selected as representative of nickel base alloys and Haynes 188 was selected as representative of cobalt base alloys used in this application. Cleaning procedures were developed to insure the reusability of the test specimens and a flaw detection reliability assessment of the fluorescent penetrant inspection method was performed using the test specimens produced to characterize their use for future reliability assessments and to provide additional NDE flaw detection reliability data for high strength alloys. The statistical analysis of the fluorescent penetrant inspection data was performed to determine the detection reliabilities for each inspection at a 90% probability/95% confidence level.

  11. ULTRA-HIGH STRENGTH IN NANOCRYSTALLINE MATERIALS UNDER SHOCK LOADING

    SciTech Connect

    Bringa, E M; Caro, A; Wang, Y M; Victoria, M; McNaney, J; Remington, B A; Smith, R; Torralva, B; Van Swygenhoven, H

    2005-04-11

    Molecular dynamics simulations of nanocrystalline (nc) copper under shock loading show an unexpected ultra-high strength behind the shock front. The strength at high pressure can be up to twice the value at low pressure, for all grain sizes studied here (5-50 nm grains, with up to {approx}4 10{sup 8} atoms). Partial and perfect dislocations, twinning, and debris from dislocation interactions are found behind the shock front. Results are interpreted in terms of the pressure dependence of both deformation mechanisms active at these grain sizes, namely dislocation plasticity and grain boundary sliding. These simulations, together with new shock experiments on nc nickel, raise the possibility of achieving ultra-hard materials during and after shock loading.

  12. Effect of size, shape, and end condition of test specimen on compressive strength of high-strength concrete

    NASA Astrophysics Data System (ADS)

    Ipatti, A.

    Compressive testing of high-strength concrete is a critical issue on which no consensus has yet been reached. Among the many factors that are under discussion are the size, shape, and end condition of test specimens for high-strength concrete. The experimental program described herein was designed primarily to investigate the effects and the possible interactions of the above-mentioned factors on compressive strength of high-strength concrete. Three levels of specimen sizes, three methods of specimen capping (mould surface, sulphur capping, grinding), and four grades of concrete strengths were selected. A 3 x 3 x 4 factorial experimental design was adopted with two replicates (each an average of three specimens), giving a total of 72 test values (216 specimens). The strictest possible precautions were taken to ensure that all other factors which would conceivably effect the compressive strength were held constant. The statistical methods utilized included analyses of variance, linear regressions, and pairwise comparisons of factor main effects.

  13. Construction procedures using self hardening fly ash

    NASA Astrophysics Data System (ADS)

    Thornton, S. I.; Parker, D. G.

    1980-07-01

    Fly ash produced in Arkansas from burning Wyoming low sulfur coal is self-hardening and can be effective as a soil stabilizing agent for clays and sands. The strength of soil-self hardening fly ash develops rapidly when compacted immediately after mixing. Seven day unconfined compressive strengths up to 1800 psi were obtained from 20% fly ash and 80% sand mixtures. A time delay between mixing the fly ash with the soil and compaction of the mixture reduced the strength. With two hours delay, over a third of the strength was lost and with four hours delay, the loss was over half. Gypsum and some commercial concrete retarders were effective in reducing the detrimental effect of delayed compaction. Adequate mixing of the soil and fly ash and rapid compaction of the mixtures were found to be important parameters in field construction of stabilized bases.

  14. Magnetic and Magnetostrictive Characterization and Modeling of High Strength Steel

    NASA Astrophysics Data System (ADS)

    Burgy, Christopher Donald

    High strength steels exhibit small amounts of magnetostriction, which is a useful property for non-destructive testing amongst other things. This property cannot currently be fully utilized due to a lack of adequate measurements and models. This thesis reports measurements of these material parameters, and derives a model using these parameters to predict magnetization changes due to the application of compressive stresses and magnetic fields. The resulting Preisach model, coupled with COMSOL MultiphysicsRTM finite element modeling, accurately predicts the magnetization change seen in a separate high strength steel sample previously measured by the National Institute of Standards and Technology. Three sets of measurements on low-carbon, low-alloy high strength steel are introduced in this research. The first experiment measured magnetostriction in steel rods under uniaxial compressive stresses and magnetic fields. The second experiment consisted of magnetostriction and magnetization measurements of the same steel rods under the influence of bi-axially applied magnetic fields. The final experiment quantified the small effect that temperature has on magnetization of steels. The experiments demonstrated that the widely used approximation of stress as an "effective field" is inadequate, and that temperatures between -50 and 100 °C cause minimal changes in magnetization. Preisach model parameters for the prediction of the magnetomechanical effect were derived from the experiments. The resulting model accurately predicts experimentally derived major and minor loops for a high strength steel sample, including the bulging and coincident points attributed to compressive stresses. A framework is presented which couples the uniaxial magnetomechanical model with a finite element package, and was used successfully to predict experimentally measured magnetization changes on a complex sample. These results show that a 1-D magnetomechanical model can be applied to predict 3-D

  15. Damage tolerance of a helicopter rotor high-strength steel

    NASA Astrophysics Data System (ADS)

    Henaff, Gilbert; Petit, Jean; Ranganathan, Narayamaswami

    1992-07-01

    The fatique crack growth behavior of a high strength steel is investigated in air and in vacuum under loading representative of helicopter spectra. The near threshold regime is considered with a high baseline level (R = 0.7). Although strong interaction effects are brought out, non concomitant closure is detected due to the high mean level of the different loading blocks. A model of the observed retardation phenomenon, which incorporates crack growth laws previously developed to describe the influence of environment, is proposed. The results are in good agreement with experimental data.

  16. Possible correlation between work-hardening and fatigue-failure

    NASA Technical Reports Server (NTRS)

    Kettunen, P. O.; Kocks, U. F.

    1969-01-01

    Conceptual theory proposes that cyclic hardening due to non-uniform strain and stress amplitudes during testing, especially during the initial application of stress to a specimen, may correlate positively with the ultimate strength of the specimen under test.

  17. New steels and methods for induction hardening of bearing rings and rollers

    SciTech Connect

    Ouchakov, B.K.; Shepeljakovsky, K.Z.

    1998-12-31

    The new method of through-surface hardening (TSH) of bearing rings and rollers was developed and used in Russia and former USSR. The principles of the method include the use of special steels of low or controlled hardenability, through-the-section induction of furnace heating and intense quenching of the parts by water stream in special devices. Due to the low hardenability of applied steels, the bearing rings and rollers have high-strength martensitic surface layer, combined with a core strengthened with a troostite and sorbite structure. High compressive residual stresses are formed in the martensitic surface layers. For a long time TSH has been successfully used for inner rings of bearings for railway car boxes, large rings and rollers of bearings for cement furnaces and rolling mills. Recently TSH was used for hollow rollers of railway bearings. For bearing rings made of SAE 52100 type high-carbon, chromium-alloyed steel a new method of low-deformation hardening was developed. The method is based on self-calibration of the rings during the quenching process and is intended for through hardening by induction heating and quenching by rapidly moved water stream.

  18. Fatigue and fracture behavior of high strength and high conductivity copper alloys for high heat flux applications

    NASA Astrophysics Data System (ADS)

    Li, Meimei

    High strength, high conductivity copper alloys are candidate materials for high heat flux applications in fusion systems. In these applications, copper alloys must withstand exposure in extreme irradiation and thermal conditions. Most studies have concentrated on the influence of temperature, environment, irradiation exposure and microstructure on tensile properties. Relatively few studies have been performed on fatigue and fracture behavior of these alloys. This work aims to characterize and understand fracture, fatigue and creep-fatigue for three copper alloys, dispersion-strengthened CuAl25, and precipitation-hardened CuCrZr and CuNiBe. The role of temperature and environment on the fracture behavior of copper alloys was examined in vacuum between 20 and 300°C. This was accomplished through mechanical tests, microstructural examination and in-situ TEM straining experiments. The results showed that all three copper alloys experienced a loss of fracture resistance at elevated temperatures. Environment is not the single, or even most important, factor contributing to poor toughness at high temperatures. The evaluation of fracture mechanisms revealed that grain boundaries have a significant impact on the fracture behavior of copper alloys. The influence of irradiation on the fatigue behavior of two selected copper alloys, CuAl25 and CuCrZr, was evaluated. The fatigue lives were estimated from tensile properties using the Universal Slopes method. It was found that the influence of irradiation on fatigue performance was not as severe as on tensile properties. The Universal Slopes method provides a reasonable prediction of fatigue response for most unirradiated and irradiated conditions. The fatigue performance of CuAl25 and CuCrZr and OFHC copper was also evaluated under creep-fatigue loading conditions. It was found that creep and stress relaxation have a major impact on fatigue behavior. Fatigue lives were reduced notably with hold time even at room temperature

  19. High Strength Discontinuously Reinforced Aluminum For Rocket Applications

    NASA Technical Reports Server (NTRS)

    Pandey, A. B.; Shah, S. R.; Shadoan, M.

    2003-01-01

    This study presents results on the development of a new aluminum alloy with very high strength and ductility. Five compositions of Al-Mg-Sc-Gd-Zr alloy were selected for this purpose. These alloys were also reinforced with 15 volume percent silicon-carbide and boron-carbide particles to produce Discontinuously Reinforced Aluminum (DRA) materials. Matrix alloys and DRA were processed using a powder metallurgy process. The helium gas atomization produced very fine powder with cellular-dentritic microstructure. The microstructure of matrix alloys showed fine Al3Sc based precipitate which provides significant strengthening in these alloys. DRA showed uniform distribution of reinforcement in aluminum matrix. DRA materials were tested at -320 F, 75 F in air and 7S F in gaseous hydrogen environments and matrix alloys were tested at 75 F in air. DRA showed high strengths in the range of 89-111 ksi (614-697 MPa) depending on alloy compositions and test environments. Matrix alloys had a good combination of strength, 84-89 ksi (579-621 MPa) and ductility, 4.5-6.5%. The properties of these materials can further be improved by proper control of processing parameters.

  20. New high-strength neodymium phosphate laser glass

    SciTech Connect

    Galagan, B I; Glushchenko, I N; Denker, B I; Kalachev, Yu L; Mikhailov, Viktor A; Sverchkov, S E; Shcherbakov, Ivan A; Kuleshov, N V

    2009-12-31

    A high-strength neodymium laser glass (SNLG) based on an alumoborophosphate composition is developed and synthesised; its physicochemical, spectral, luminescent, and lasing characteristics are studied. It is found that the chemical stability and thermal resistance of the new glass are considerably higher than the corresponding characteristics of known neodymium-doped phosphate laser glasses. Investigations of lasing upon longitudinal diode pumping showed that, due to the higher thermal resistance, the new glass allows one to obtain output powers twice as high as those of industrial GLS22 glass. (active media)

  1. Design of an Eta-Phase Precipitation-Hardenable Nickel-Based Alloy with the Potential for Improved Creep Strength Above 1023 K (750 °C)

    NASA Astrophysics Data System (ADS)

    Wong, Matthew J.; Sanders, Paul G.; Shingledecker, John P.; White, Calvin L.

    2015-07-01

    In a number of nickel-based superalloy systems strengthened by gamma prime ( γ'), eta-phase (Ni3Ti, η) forms during prolonged high-temperature exposure, but its effect on mechanical properties is not well characterized. Using thermodynamic modeling and design-of-experiments techniques, three modifications of the nickel-based superalloy Nimonic (Nimonic® is a trademark of Special Metals Corporation group of companies.) 263 were identified that yield increased volume fractions of the eta-phase (Ni3Ti, η) at temperatures above 1023 K (750 °C). Volume fractions of η-phase were evaluated for each alloy and heat-treatment condition using optical microscopy, scanning electron microscopy, energy dispersive spectroscopy, and X-ray diffraction. Compared to Nimonic 263, small additions of V and Ta were found to increase the volume fraction of η-phase above 1023 K (750 °C) from approximately 5 pct to above 15 pct, thus providing a route for future mechanical behavior experimental studies, which was not in the scope of this work.

  2. 'Fire hardening' spear wood does slightly harden it, but makes it much weaker and more brittle.

    PubMed

    Ennos, Antony Roland; Chan, Tak Lok

    2016-05-01

    It is usually assumed that 'fire hardening' the tips of spears, as practised by hunter-gatherers and early Homo spp., makes them harder and better suited for hunting. This suggestion was tested by subjecting coppiced poles of hazel to a fire-hardening process and comparing their mechanical properties to those of naturally seasoned poles. A Shore D hardness test showed that fire treatment slightly increased the hardness of the wood, but flexural and impact tests showed that it reduced the strength and work of fracture by 30% and 36%, respectively. These results suggest that though potentially slightly sharper and more durable, fire-hardened tips would actually be more likely to break off when used, as may have been the case with the earliest known wooden tool, the Clacton spear. Fire might first have been used to help sharpen the tips of spears, and fire-hardening would have been a mostly negative side effect, not its primary purpose.

  3. 'Fire hardening' spear wood does slightly harden it, but makes it much weaker and more brittle.

    PubMed

    Ennos, Antony Roland; Chan, Tak Lok

    2016-05-01

    It is usually assumed that 'fire hardening' the tips of spears, as practised by hunter-gatherers and early Homo spp., makes them harder and better suited for hunting. This suggestion was tested by subjecting coppiced poles of hazel to a fire-hardening process and comparing their mechanical properties to those of naturally seasoned poles. A Shore D hardness test showed that fire treatment slightly increased the hardness of the wood, but flexural and impact tests showed that it reduced the strength and work of fracture by 30% and 36%, respectively. These results suggest that though potentially slightly sharper and more durable, fire-hardened tips would actually be more likely to break off when used, as may have been the case with the earliest known wooden tool, the Clacton spear. Fire might first have been used to help sharpen the tips of spears, and fire-hardening would have been a mostly negative side effect, not its primary purpose. PMID:27194289

  4. Hardening of the arteries

    MedlinePlus

    Atherosclerosis; Arteriosclerosis; Plaque buildup - arteries; Hyperlipidemia - atherosclerosis; Cholesterol - atherosclerosis ... Hardening of the arteries often occurs with aging. As you grow older, ... narrows your arteries and makes them stiffer. These changes ...

  5. High Breakdown Strength, Multilayer Ceramics for Compact Pulsed Power Applications

    SciTech Connect

    Gilmore, B.; Huebner, W.; Krogh, M.L.; Lundstrom, J.M.; Pate, R.C.; Rinehart, L.F.; Schultz, B.C.; Zhang, S.C.

    1999-07-20

    Advanced ceramics are being developed for use in large area, high voltage devices in order to achieve high specific energy densities (>10 6 J/m 3 ) and physical size reduction. Initial materials based on slip cast TiO2 exhibited a high bulk breakdown strength (BDS >300 kV/cm) and high permittivity with low dispersion (e�100). However, strong area and thickness dependencies were noted. To increase the BDS, multilayer dielectric compositions are being developed based on glass/TiO2 composites. The addition of glass increases the density (�99.8% theoretical), forms a continuous grain boundary phase, and also allows the use of high temperature processes to change the physical shape of the dielectric. The permittivity can also be manipulated since the volume fraction and connectivity of the glassy phase can be readily shifted. Results from this study on bulk breakdown of TiO2 multilayer structures with an area of 2cm 2 and 0.1cm thickness have measured 650 kV/cm. Furthermore, a strong dependence of breakdown strength and permittivity has been observed and correlated with microstructure and the glass composition. This paper presents the interactive effects of manipulation of these variables.

  6. Radiation and chemical crosslinking promote strain hardening behavior and molecular alignment in ultra high molecular weight polyethylene during multi-axial loading conditions.

    PubMed

    Kurtz, S M; Pruitt, L A; Jewett, C W; Foulds, J R; Edidin, A A

    1999-08-01

    The mechanical behavior and evolution of crystalline morphology during large deformation of eight types of virgin and crosslinked ultra high molecular weight polyethylene (UHMWPE) were studied using the small punch test and transmission electron microscopy (TEM). We investigated the hypothesis that both radiation and chemical crosslinking hinder molecular mobility at large deformations, and hence promote strain hardening and molecular alignment during the multiaxial loading of the small punch test. Chemical crosslinking of UHMWPE was performed using 0.25% dicumyl peroxide (GHR 8110, GUR 1020 and 1050), and radiation crosslinking was performed using 150 kGy of electron beam radiation (GUR 1150). Crosslinking increased the ultimate load at failure and decreased the ultimate displacement of the polyethylenes during the small punch test. Crosslinking also increased the near-ultimate hardening behavior of the polyethylenes. Transmission electron microscopy was used to characterize the crystalline morphology of the bulk material, undeformed regions of the small punch test specimens, and deformed regions of the specimens oriented perpendicular and parallel to the punch direction. In contrast with the virgin polyethylenes, which showed only subtle evidence of lamellar alignment, the crosslinked polyethylenes exhibited enhanced crystalline lamellae orientation after the small punch test, predominantly in the direction parallel to the punch direction or deformation axis. Thus, the results of this study support the hypothesis that crosslinking promotes strain hardening during multiaxial loading because of increased resistance to molecular mobility at large deformations effected by molecular alignment. The data also illustrate the sensitivity of large deformation mechanical behavior and crystalline morphology to the method of crosslinking and resin of polyethylene. PMID:10458558

  7. Cold Hardening in Citrus Stems

    PubMed Central

    Yelenosky, George

    1975-01-01

    Stem cold hardening developed to different levels in citrus types tested in controlled environments. Exotherms indicated ice spread was more uniform and rapid in unhardened than in cold-hardened stems. All attempts to inhibit the functioning of citrus leaves resulted in less cold hardening in the stems. Citrus leaves contribute a major portion of cold hardening in the wood. PMID:16659340

  8. Manufacturing of high-strength Ni-free Co-Cr-Mo alloy rods via cold swaging.

    PubMed

    Yamanaka, Kenta; Mori, Manami; Yoshida, Kazuo; Kuramoto, Koji; Chiba, Akihiko

    2016-07-01

    The strengthening of biomedical metallic materials is crucial to increasing component durability in biomedical applications. In this study, we employ cold swaging as a strengthening method for Ni-free Co-Cr-Mo alloy rods and examine its effect on the resultant microstructures and mechanical properties. N is added to the alloy to improve the cold deformability, and a maximum reduction in area (r) of 42.6% is successfully obtained via cold swaging. The rod strength and ductility increase and decrease, respectively, with increasing cold-swaging reduction r. Further, the 0.2% proof stress at r=42.6% eventually reaches 1900MPa, which is superior to that obtained for the other strengthening methods proposed to date. Such significant strengthening resulting from the cold-swaging process may be derived from extremely large work hardening due to a strain-induced γ (fcc)→ε (hcp) martensitic transformation, with the resultant intersecting ε-martensite plates causing local strain accumulation at the interfaces. The lattice defects (dislocations/stacking faults) inside the ε phase also likely contribute to the overall strength. However, excessive application of strain during the cold-swaging process results in a severe loss in ductility. The feasibility of cold swaging for the manufacture of high-strength Co-Cr-Mo alloy rods is discussed.

  9. High-strength silk protein scaffolds for bone repair

    PubMed Central

    Mandal, Biman B.; Grinberg, Ariela; Seok Gil, Eun; Panilaitis, Bruce; Kaplan, David L.

    2012-01-01

    Biomaterials for bone tissue regeneration represent a major focus of orthopedic research. However, only a handful of polymeric biomaterials are utilized today because of their failure to address critical issues like compressive strength for load-bearing bone grafts. In this study development of a high compressive strength (~13 MPa hydrated state) polymeric bone composite materials is reported, based on silk protein-protein interfacial bonding. Micron-sized silk fibers (10–600 µm) obtained utilizing alkali hydrolysis were used as reinforcement in a compact fiber composite with tunable compressive strength, surface roughness, and porosity based on the fiber length included. A combination of surface roughness, porosity, and scaffold stiffness favored human bone marrow-derived mesenchymal stem cell differentiation toward bone-like tissue in vitro based on biochemical and gene expression for bone markers. Further, minimal in vivo immunomodulatory responses suggested compatibility of the fabricated silk-fiber-reinforced composite matrices for bone engineering applications. PMID:22552231

  10. Scratch-resistant, highly conductive, and high-strength carbon nanotube-based composite yarns.

    PubMed

    Liu, Kai; Sun, Yinghui; Lin, Xiaoyang; Zhou, Ruifeng; Wang, Jiaping; Fan, Shoushan; Jiang, Kaili

    2010-10-26

    High-strength and conductive carbon nanotube (CNT) yarns are very attractive in many potential applications. However, there is a difficulty when simultaneously enhancing the strength and conductivity of CNT yarns. Adding some polymers into CNT yarns to enhance their strength will decrease their conductivity, while treating them in acid or coating them with metal nanoparticles to enhance their conductivity will reduce their strength. To overcome this difficulty, here we report a method to make high-strength and highly conductive CNT-based composite yarns by using a continuous superaligned CNT (SACNT) yarn as a conductive framework and then inserting polyvinyl alcohol (PVA) into the intertube spaces of the framework through PVA/dimethyl sulphoxide solution to enhance the strength of yarns. The as-produced CNT/PVA composite yarns possess very high tensile strengths up to 2.0 GPa and Young's moduli more than 120 GPa, much higher than those of the CNT/PVA yarns reported. The electric conductivity of as-produced composite yarns is as high as 9.2 × 10(4) S/m, comparable to HNO(3)-treated or Au nanoparticle-coated CNT yarns. These composite yarns are flexible, lightweight, scratch-resistant, very stable in the lab environment, and resistant to extremely humid ambient and as a result can be woven into high-strength and heatable fabrics, showing potential applications in flexible heaters, bullet-proof vests, radiation protection suits, and spacesuits.

  11. Effect of surface modification, microstructure, and trapping on hydrogen diffusion coefficients in high strength alloys

    NASA Astrophysics Data System (ADS)

    Jebaraj Johnley Muthuraj, Josiah

    Cathodic protection is widely used for corrosion prevention. However, this process generates hydrogen at the protected metal surface, and diffusion of hydrogen through the metal may cause hydrogen embrittlement or hydrogen induced stress corrosion cracking. Thus the choice of a metal for use as fasteners depends upon its hydrogen uptake, permeation, diffusivity and trapping. The diffusivity of hydrogen through four high strength alloys (AISI 4340, alloy 718, alloy 686, and alloy 59) was analyzed by an electrochemical method developed by Devanathan and Stachurski. The effect of plasma nitriding and microstructure on hydrogen permeation through AISI 4340 was studied on six different specimens: as-received (AR) AISI 4340, nitrided samples with and without compound layer, samples quenched and tempered (Q&T) at 320° and 520°C, and nitrided samples Q&T 520°C. Studies on various nitrided specimens demonstrate that both the gamma'-Fe 4N rich compound surface layer and the deeper N diffusion layer that forms during plasma nitriding reduce the effective hydrogen diffusion coefficient, although the gamma'-Fe4N rich compound layer has a larger effect. Multiple permeation transients yield evidence for the presence of only reversible trap sites in as-received, Q&T 320 and 520 AISI 4340 specimens, and the presence of both reversible and irreversible trap sites in nitrided specimens. Moreover, the changes in microstructure during the quenching and tempering process result in a significant decrease in the diffusion coefficient of hydrogen compared to as-received specimens. In addition, density functional theory-based molecular dynamics simulations yield hydrogen diffusion coefficients through gamma'- Fe4N one order of magnitude lower than through α-Fe, which supports the experimental measurements of hydrogen permeation. The effect of microstructure and trapping was also studied in cold rolled, solutionized, and precipitation hardened Inconel 718 foils. The effective hydrogen

  12. Effect of microstructure on the fracture response of advanced high strength steels

    NASA Astrophysics Data System (ADS)

    Taylor, Mark David

    The effect of constituent hardness on formability performance for higher-strength dual phase (DP) steels was evaluated. A commercially-produced DP steel with 1080 MPa ultimate tensile strength (UTS) was processed to create eight additional constituent hardness conditions by tempering and cold-rolling, processes that primarily affected constituent hardness properties. Using nanoindentation, ferrite and martensite hardness values for the nine conditions of the DP steel (as-received, four as-tempered, four temper cold-rolled) provided a range of hardness values to evaluate formability performance. Formability performance for the nine steel conditions was evaluated using tensile and hole expansion testing. A decrease in martensite/ferrite hardness ratio corresponded to an increase in hole expansion ratio (HER), and an increase in yield strength (YS). A lower hardness ratio (increased similarity of ferrite and martensite hardness) was interpreted to increase strain-sharing between ferrite and martensite, which suppressed plastic strain localization to higher stresses for the case of YS, and to higher formability limits for the case of HER. A lower hardness ratio corresponded to a decrease in work-hardening, and was interpreted to be caused by the suppression of strain localization in ferrite. Multiple studies from literature correlated HER to tensile properties, and the nine steel conditions produced consistent trends with the data reported in each study, confirming the experimental HER and tensile properties obtained in the current study are consistent with literature. The microstructural response to plastic deformation was evaluated using two DP steels with equivalent UTS and different hardness ratios. Nanoindentation analyses on tensile specimens deformed to the UTS revealed a greater increase in ferrite hardness for the higher hardness ratio steel, interpreted to be caused by the greater amount of work hardening. EBSD crystallographic orientation maps for the two DP

  13. Study on the limited hardenability steel

    SciTech Connect

    Xu, L.P.; Li, L.; Min, Y.A.; Xu, M.H.; Le, J.P.; Liu, R.H.

    1998-12-31

    A series of measurements were taken in the limited hardenability bearing steel rings which were induction hardened and tempered. Measurements showed several features which strengthened the rings: (1) Compressive residual stress are generated from surface to a depth of 3.2 mm and high residual compressive stress at the location where fatigue fracture initiates. (2) The matrix of the hardened layer was composed mainly of lath martensite with dispersed carbides whose formula was Me{sub 3} according to the X-ray spectrum analysis. The carbon content of martensite was estimated to be lower than 0.58% (by weight). The core was constituted of troostite transformed from spheroidal carbide. (3) The amount of retained austenite in the hardened layer was about 5% (in volume) which ensures the high dimensional stability of bearing.

  14. Control technology for surface treatment of materials using induction hardening

    SciTech Connect

    Kelley, J.B.; Skocypec, R.D.

    1997-04-01

    In the industrial and automotive industries, induction case hardening is widely used to provide enhanced strength, wear resistance, and toughness in components made from medium and high carbon steels. The process uses significantly less energy than competing batch process, is environmentally benign, and is a very flexible in-line manufacturing process. As such, it can directly contribute to improved component reliability, and the manufacture of high-performance lightweight parts. However, induction hardening is not as widely used as it could be. Input material and unexplained process variations produce significant variation in product case depth and quality. This necessitates frequent inspection of product quality by destructive examination, creates higher than desired scrap rates, and causes de-rating of load stress sensitive components. In addition, process and tooling development are experience-based activities, accomplished by trial and error. This inhibits the use of induction hardening for new applications, and the resultant increase in energy efficiency in the industrial sectors. In FY96, a Cooperative Research and Development Agreement under the auspices of the Technology Transfer Initiative and the Partnership for a New Generation of Vehicles was completed. A multidisciplinary team from Sandia National Labs and Delphi Saginaw Steering Systems investigated the induction hardening by conducting research in the areas of process characterization, computational modeling, materials characterization, and high speed data acquisition and controller development. The goal was to demonstrate the feasibility of closed-loop control for a specific material, geometry, and process. Delphi Steering estimated annual savings of $2-3 million per year due to reduced scrap losses, inspection costs, and machine down time if reliable closed-loop control could be achieved. A factor of five improvement in process precision was demonstrated and is now operational on the factory floor.

  15. TOUGHREACT Testing in High Ionic Strength Brine Sandstone Systems

    SciTech Connect

    Xu, Tianfu

    2008-09-01

    Deep saline formations and oil and gas reservoirs often contain concentrated brine solutions of ionic strength greater than 1 (I > 1 M). Geochemical modeling, involving high ionic strength brines, is a challenge. In the original TOUGHREACT code (Xu et al., 2004; Xu et al., 2006), activity coefficients of charged aqueous species are computed using an extended Debye-Huckel (DH) equation and parameters derived by Helgeson et al. (1981). The DH model can deal with ionic strengths from dilute to moderately saline water (up to 6 molal for an NaCl-dominant solution). The equations implemented for the DH model are presented in Appendix A. During the course of the Yucca Mountain project, a Pitzer ion-interaction model was implemented into TOUGHREACT. This allows the application of this simulator to problems involving much more concentrated aqueous solutions, such as those involving geochemical processes in and around high-level nuclear waste repositories where fluid evaporation and/or boiling is expected to occur (Zhang et al., 2007). The Pitzer ion-interaction model, which we refer to as the Pitzer virial approach, and associated ion-interaction parameters have been applied successfully to study non-ideal concentrated aqueous solutions. The formulation of the Pitzer model is presented in Appendix B; detailed information can be founded in Zhang et al. (2007). For CO{sub 2} geological sequestration, the Pitzer ion-interaction model for highly concentrated brines was incorporated into TOUGHREACT/ECO2N, then was tested and compared with a previously implemented extended Debye-Hueckel (DH) ion activity model. The comparison was made through a batch geochemical system using a Gulf Coast sandstone saline formation.

  16. Method for providing a low density high strength polyurethane foam

    SciTech Connect

    Whinnery, Jr., Leroy L.; Goods, Steven H.; Skala, Dawn M.; Henderson, Craig C.; Keifer, Patrick N.

    2013-06-18

    Disclosed is a method for making a polyurethane closed-cell foam material exhibiting a bulk density below 4 lbs/ft.sup.3 and high strength. The present embodiment uses the reaction product of a modified MDI and a sucrose/glycerine based polyether polyol resin wherein a small measured quantity of the polyol resin is "pre-reacted" with a larger quantity of the isocyanate in a defined ratio such that when the necessary remaining quantity of the polyol resin is added to the "pre-reacted" resin together with a tertiary amine catalyst and water as a blowing agent, the polymerization proceeds slowly enough to provide a stable foam body.

  17. High Strength, Large Core Pure Silica Fibers For Laser Surgery

    NASA Astrophysics Data System (ADS)

    Skutnik, B. J.; Hodge, M. H.; Clarkin, J. P.

    1988-06-01

    Recently many researchers, doctors and instrument companies have begun developing fiber optic laser power delivery systems to accomplish less traumatic surgery or localized irradiation treatment(1). With high power levels, particularly in short bursts, large core fibers are needed to keep the power densities from approaching the damage threshold of silica. Among the many advantages of using optical fibers in laser surgery are the following: microsurgery can be employed, trauma is reduced, access to interior through catheter introduction into vascular, gastrointestinal or respiratory tracts, accurate application of laser power through a flexible lightweight medium to provide localized irradiation as well as surgical removal, and the devices are sterilizable and of moderate cost permitting one-time use (disposable) probes. To achieve these wonderful gains in surgical procedures, the optical fibers must satisfy many optical and mechanical requirements. In use the optical fibers are often required to bend around curves or obstructions to reach the desired application area. Large tensile stresses can occur on the outer radius of the bent fiber, especially with large core fibers, thus high strength fibers are needed. Furthermore, since body fluids are primarily water, stress corrosion and fatigue(2-6) will occur. Therefore, the fibers should have excellent fatigue resistance as well as high strength. This paper further describes these requirements and presents details about an optical fiber which meets these requirements and provides additional very useful properties. These fibers with pure silica cores are called Hard Clad Silica, HCS*, fibers because of their hard bonded cladding over silica structure.

  18. The Strengths of High-Achieving Black High School Students in a Racially Diverse Setting

    ERIC Educational Resources Information Center

    Marsh, Kris; Chaney, Cassandra; Jones, Derrick

    2012-01-01

    Robert Hill (1972) identified strengths of Black families: strong kinship bonds, strong work orientation, adaptability of family roles, high achievement orientation, and religious orientation. Some suggest these strengths sustain the physical, emotional, social, and spiritual needs of Blacks. This study used narratives and survey data from a…

  19. Scintillation-Hardened GPS Receiver

    NASA Technical Reports Server (NTRS)

    Stephens, Donald R.

    2015-01-01

    CommLargo, Inc., has developed a scintillation-hardened Global Positioning System (GPS) receiver that improves reliability for low-orbit missions and complies with NASA's Space Telecommunications Radio System (STRS) architecture standards. A software-defined radio (SDR) implementation allows a single hardware element to function as either a conventional radio or as a GPS receiver, providing backup and redundancy for platforms such as the International Space Station (ISS) and high-value remote sensing platforms. The innovation's flexible SDR implementation reduces cost, weight, and power requirements. Scintillation hardening improves mission reliability and variability. In Phase I, CommLargo refactored an open-source GPS software package with Kalman filter-based tracking loops to improve performance during scintillation and also demonstrated improved navigation during a geomagnetic storm. In Phase II, the company generated a new field-programmable gate array (FPGA)-based GPS waveform to demonstrate on NASA's Space Communication and Navigation (SCaN) test bed.

  20. Magnetic Implosion for Novel Strength Measurements at High Strain Rates

    SciTech Connect

    Lee, H.; Preston, D.L.; Bartsch, R.R.; Bowers, R.L.; Holtkamp, D.; Wright, B.L.

    1998-10-19

    Recently Lee and Preston have proposed to use magnetic implosions as a new method for measuring material strength in a regime of large strains and high strain rates inaccessible to previously established techniques. By its shockless nature, this method avoids the intrinsic difficulties associated with an earlier approach using high explosives. The authors illustrate how the stress-strain relation for an imploding liner can be obtained by measuring the velocity and temperature history of its inner surface. They discuss the physical requirements that lead us to a composite liner design applicable to different test materials, and also compare the code-simulated prediction with the measured data for the high strain-rate experiments conducted recently at LANL. Finally, they present a novel diagnostic scheme that will enable us to remove the background in the pyrometric measurement through data reduction.

  1. Cardiac work remains high after strength exercise in elderly.

    PubMed

    Queiroz, A C C; Kanegusuku, H; Chehuen, M R; Costa, L A R; Wallerstein, L F; Dias da Silva, V J; Mello, M T; Ugrinowitsch, C; Forjaz, C L M

    2013-05-01

    Moderate- to high-intensity strength training is recommended for healthy adults. In young subjects, a single session of strength training decreases blood pressure, while heart rate and cardiac work remain elevated afterwards. However, these effects have not been clearly demonstrated in elderly subjects. To investigate this issue, 16 elderly subjects each underwent a Control and an Exercise (3 sets, 8 RM, 9 exercises) session conducted in random order. Haemodynamic variables and heart rate variability were measured before and after the interventions. Systolic blood pressure did not change after the exercise session but did increase after the control session (+8.1±1.6 mm Hg, P≤0.05). Diastolic blood pressure, as well as systemic vascular resistance increased similarly after both sessions. Cardiac output and stroke volume decreased, while heart rate, rate-pressure product and the low- to high-frequency ratio of heart rate variability increased only after the exercise session ( - 0.5±0.1 L/min, - 9.3±2.0 ml,+3.8±1.6 bpm, +579.3±164.1 mmHg.bpm and +0.71±0.34, P≤0.05). Ambulatory blood pressure was similar after both sessions, while heart rate and rate pressure product remained higher after the exercise session for up to 4.5 h. After a single session of strength training, cardiac sympathetic modulation and heart rate remain elevated in elderly subjects, keeping cardiac work elevated for a long period of time.

  2. Mechanisms of Neutron Irradiation Hardening in Impurity-Doped Ferritic Alloys

    NASA Astrophysics Data System (ADS)

    Nishiyama, Y.; Liu, X. Y.; Kameda, J.

    2008-05-01

    Mechanisms of neutron irradiation hardening in phosphorus (P)-doped, sulfur (S)-doped, and copper (Cu)-doped ferritic alloys have been studied by applying a rate theory to the temperature dependence of the yield strength. Hardening behavior induced by neutron irradiation at various temperatures (473 to 711 K) is characterized in terms of the variations in athermal stress and activation energy for plasticity controlled by precipitation or solid solution, and kink-pair formation with the content and type of impurities. In P-doped alloys, neutron irradiation below 563 K brings about a remarkable increase in the athermal stress and activation energy, due to the dispersion of fine (˜1.7-nm) P-rich precipitates that is more extensive than that for the Cu-rich precipitates reported in irradiated steel. During neutron irradiation above 668 K, precipitation hardening occurs to some extent in Cu-doped and S-doped alloys, compared to small or negligible hardening in the P-doped alloys. In alloys with a low to moderate content of various dissolved impurities subjected to high-temperature irradiation, the formation of kink pairs becomes considerably difficult. Differing dynamic interactions of dissolved and precipitated impurities, i.e., P and Cu, with the nucleation and growth of dislocations are discussed, giving rise to irradiation hardening.

  3. Fatigue behavior of high-strength concrete under marine conditions

    SciTech Connect

    Mor, A.

    1987-01-01

    In this study, 24 high-strength reinforced concrete beams were tested in fatigue under simulated marine conditions. Low-cycle, high-magnitude loading was imposed on beams, some of which were exposed to air, and others which were submerged in water. The beams were cycled at 1 Hz, to 80% of their yield capacity in negative and positive flexure. Four concrete mixes were compared. Half of the specimens were made with lightweight aggregate (LWA), and half were made with river gravel (NWA). Half of each group contained silica-fume as partial replacement of cement (13%). By manipulating the water/cement ratio, the 28-day compressive strength of all concretes was 9500 {plus minus} 300 psi. The previously reported phenomenon of water pumping through the cracks was observed, but did not appear to be directly related to the subsequent failure. When silica fume is added to the concrete mix, the adhesion is greatly improved. LWA concrete utilizes this additional adhesion effectively. NWA concrete with silica-fume, on the other hand, is not able to utilize the increased adhesion due to microcracking. Main findings of both the fatigue and pull-out bond tests are listed.

  4. Extraordinary strain hardening by gradient structure.

    PubMed

    Wu, XiaoLei; Jiang, Ping; Chen, Liu; Yuan, Fuping; Zhu, Yuntian T

    2014-05-20

    Gradient structures have evolved over millions of years through natural selection and optimization in many biological systems such as bones and plant stems, where the structures change gradually from the surface to interior. The advantage of gradient structures is their maximization of physical and mechanical performance while minimizing material cost. Here we report that the gradient structure in engineering materials such as metals renders a unique extra strain hardening, which leads to high ductility. The grain-size gradient under uniaxial tension induces a macroscopic strain gradient and converts the applied uniaxial stress to multiaxial stresses due to the evolution of incompatible deformation along the gradient depth. Thereby the accumulation and interaction of dislocations are promoted, resulting in an extra strain hardening and an obvious strain hardening rate up-turn. Such extraordinary strain hardening, which is inherent to gradient structures and does not exist in homogeneous materials, provides a hitherto unknown strategy to develop strong and ductile materials by architecting heterogeneous nanostructures.

  5. Hydration and strength development of binder based on high-calcium oil shale fly ash. Part 2: Influence of curing conditions on long-term stability

    SciTech Connect

    Freidin, C.

    1999-11-01

    The distinguishing feature of high-calcium oil shale fly ash (HCOSFA) used in experiments is the high amount of free CaO and SO{sub 3} in form of lime and anhydrite. Strength development as well as the microstructure and composition of the new formations of fly ash binder (FAB) based on HCOSFA and low-calcium coal fly ash after curing in different conditions and long-term exposure in various environments were studied. It was determined that moist air and water are the most favorable conditions for aging processes of FAB. In atmospheric air three stages in strength change of cured FAB are observed: increase of compressive strength over 1 month; sharp drop after 1 month up to the 3 to months; stabilization or slowdown of loss in strength after 3 to 6 months of exposure. The duration of the second and third stages depends on HCOSFA content and does not depend on curing conditions. One of the hydration products of FAB is ettringite. Its instability in air could be a reason for the decrease in strength of FAB and some disintegration of the hardened system. In the presence of low-calcium coal fly ash, additional amounts of stable calcium silicate hydrates are formed during FAB curing especially during steam curing. This has a positive effect on compressive strength and stability of FAB in atmospheric air.

  6. Experimental investigation of bond strength under high loading rates

    NASA Astrophysics Data System (ADS)

    Michal, Mathias; Keuser, Manfred; Solomos, George; Peroni, Marco; Larcher, Martin; Esteban, Beatriz

    2015-09-01

    The structural behaviour of reinforced concrete is governed significantly by the transmission of forces between steel and concrete. The bond is of special importance for the overlapping joint and anchoring of the reinforcement, where rigid bond is required. It also plays an important role in the rotational capacity of plastic hinges, where a ductile bond behaviour is preferable. Similar to the mechanical properties of concrete and steel also the characteristics of their interaction changes with the velocity of the applied loading. For smooth steel bars with its main bond mechanisms of adhesion and friction, nearly no influence of loading rate is reported in literature. In contrast, a high rate dependence can be found for the nowadays mainly used deformed bars. For mechanical interlock, where ribs of the reinforcing steel are bracing concrete material surrounding the bar, one reason can be assumed to be in direct connection with the increase of concrete compressive strength. For splitting failure of bond, characterized by the concrete tensile strength, an even higher dynamic increase is observed. For the design of Structures exposed to blast or impact loading the knowledge of a rate dependent bond stress-slip relationship is required to consider safety and economical aspects at the same time. The bond behaviour of reinforced concrete has been investigated with different experimental methods at the University of the Bundeswehr Munich (UniBw) and the Joint Research Centre (JRC) in Ispra. Both static and dynamic tests have been carried out, where innovative experimental apparatuses have been used. The bond stress-slip relationship and maximum pull-out-forces for varying diameter of the bar, concrete compressive strength and loading rates have been obtained. It is expected that these experimental results will contribute to a better understanding of the rate dependent bond behaviour and will serve for calibration of numerical models.

  7. Prediction of Microstructure in High-Strength Ductile Forging Parts

    SciTech Connect

    Urban, M.; Back, A.; Hirt, G.; Keul, C.; Bleck, W.

    2010-06-15

    Governmental, environmental and economic demands call for lighter, stiffer and at the same time cheaper products in the vehicle industry. Especially safety relevant parts have to be stiff and at the same time ductile. The strategy of this project was to improve the mechanical properties of forging steel alloys by employing a high-strength and ductile bainitic microstructure in the parts while maintaining cost effective process chains to reach these goals for high stressed forged parts. Therefore, a new steel alloy combined with an optimized process chain has been developed. To optimize the process chain with a minimum of expensive experiments, a numerical approach was developed to predict the microstructure of the steel alloy after the process chain based on FEM simulations of the forging and cooling combined with deformation-time-temperature-transformation-diagrams.

  8. Mechanical Properties of High Strength Al-Mg Alloy Sheet

    NASA Astrophysics Data System (ADS)

    Choi, Bong-Jae; Hong, Kyung-Eui; Kim, Young-Jig

    The aim of this research is to develop the high strength Al alloy sheet for the automotive body. For the fabrication Al-Mg alloy sheet, the composition of alloying elements was designed by the properties database and CALPHAD (Calculation Phase Diagram) approach which can predict the phases during solidification using thermodynamic database. Al-Mg alloys were designed using CALPHAD approach according to the high content of Mg with minor alloying elements. After phase predictions by CALPHAD, designed Al-Mg alloys were manufactured. Addition of Mg in Al melts were protected by dry air/Sulphur hexafluoride (SF6) mixture gas which can control the severe Mg ignition and oxidation. After rolling procedure of manufactured Al-Mg alloys, mechanical properties were examined with the variation of the heat treatment conditions.

  9. Guidelines for Stretch Flanging Advanced High Strength Steels

    NASA Astrophysics Data System (ADS)

    Sriram, S.; Chintamani, J.

    2005-08-01

    Advanced High Strength Steels (AHSS) are currently being considered for use in closure and structural panels in the automotive industry because of their high potential for affordable weight reduction and improved performance. AHSS such as dual phase steels are currently being used in some vehicle platforms. From a manufacturing perspective, stretch flanging during stamping is an important deformation mode requiring careful consideration of geometry and the die process. This paper presents some geometric and process guidelines for stretch flanging AHSS. Hole expansion experiments were conducted to determine the failure limit for a sheared edge condition. Effects of punching clearance, prestrain and prior strain path on hole expansion were explored in these experiments. In addition, dynamic explicit FE calculations using LS-DYNA were also conducted for a typical stretch flange by varying some key geometric parameters. The experimental and FEA results were then analyzed to yield process and geometric guidelines to enable successful stretch flanging of AHSS.

  10. Development of microstructure and irradiation hardening of Zircaloy during low dose neutron irradiation at nominally 358 C

    SciTech Connect

    Cockeram, Brian V; Smith, Richard W; Leonard, Keith J; Byun, Thak Sang; Snead, Lance Lewis

    2011-01-01

    Wrought Zircaloy-2 and Zircaloy-4 were neutron irradiated at nominally 358 C in the high flux isotope reactor (HFIR) at relatively low neutron fluences between 5.8 1022 and 2.9 1025 n/m2 (E > 1 MeV). The irradiation hardening and change in microstructure were characterized following irradiation using tensile testing and examinations of microstructure using Analytical Electron Microscopy (AEM). Small increments of dose (0.0058, 0.11, 0.55, 1.08, and 2.93 1025 n/m2) were used in the range where the saturation of irradiation hardening is typically observed so that the role of microstructure evolution and hai loop formation on irradiation hardening could be correlated. An incubation dose between 5.8 1023 and 1.1 1024 n/m2 was needed for loop nucleation to occur that resulted in irradiation hardening. Increases in yield strength were consistent with previous results in this temperature regime, and as expected less irradiation hardening and lower hai loop number density values than those generally reported in literature for irradiations at 260 326 C were observed. Unlike previous lower temperature data, there is evidence in this study that the irradiation hardening can decrease with dose over certain ranges of fluence. Irradiation induced voids were observed in very low numbers in the Zircaloy-2 materials at the highest fluence.

  11. Accelerated Creep Testing of High Strength Aramid Webbing

    NASA Technical Reports Server (NTRS)

    Jones, Thomas C.; Doggett, William R.; Stnfield, Clarence E.; Valverde, Omar

    2012-01-01

    A series of preliminary accelerated creep tests were performed on four variants of 12K and 24K lbf rated Vectran webbing to help develop an accelerated creep test methodology and analysis capability for high strength aramid webbings. The variants included pristine, aged, folded and stitched samples. This class of webbings is used in the restraint layer of habitable, inflatable space structures, for which the lifetime properties are currently not well characterized. The Stepped Isothermal Method was used to accelerate the creep life of the webbings and a novel stereo photogrammetry system was used to measure the full-field strains. A custom MATLAB code is described, and used to reduce the strain data to produce master creep curves for the test samples. Initial results show good correlation between replicates; however, it is clear that a larger number of samples are needed to build confidence in the consistency of the results. It is noted that local fiber breaks affect the creep response in a similar manner to increasing the load, thus raising the creep rate and reducing the time to creep failure. The stitched webbings produced the highest variance between replicates, due to the combination of higher local stresses and thread-on-fiber damage. Large variability in the strength of the webbings is also shown to have an impact on the range of predicted creep life.

  12. Structural influences on the work hardening behavior of aluminum

    SciTech Connect

    Chu, D.

    1994-12-01

    Effects of various grain and subgrain morphologies on low temperature work hardening of pure Al is studied using tensile tests. Plotting the work hardening rate as a function of true stress, the work hardening is separable into two distinct regimes. Both regimes are approximated by a line {Theta} = {Theta}{sub 0} {minus} K{sub 2}{sigma}, where {Theta}{sub 0} is theoretical work hardening rate at zero stress and K{sub 2} is related to dynamic recovery rate. The first or early deformation regime exhibits greater values of {Theta}{sub 0} and K{sub 2} and can extend up to the first 10% strain of tensile deformation. This early deformation regime is contingent on the existence of a pre-existent dislocation substructure from previous straining. The {Theta}{sub 0} and K{sub 2} associated with the early deformation regime are dependent on the strength and orientation of the pre-existent dislocation substructure relative to the new strain path. At high enough temperatures, this pre-existent dislocation substructure is annealed out, resulting in the near elimination of the early deformation regime. In comparison, the latter regime is dominated by the initial grain and/or subgrain morphology and exhibit lower values of {Theta}{sub 0} and K{sub 2}. The actual value of K{sub 2} in the latter regime is strongly dependent on the existence of a subgrain morphology. Recrystallized or well-annealed microstructures exhibit greater values of K{sub 2} than microstructures that remain partially or fully unrecrystallized. The higher K{sub 2} value is indicative of a more rapid dynamic recovery rate and a greater degree of strain relaxation. The ability to achieve a more relaxed state produces a low-energy cellular dislocation substructure upon deformation. The introduction of subgrains hinders the evolution of a low-energy dislocation cell network, giving way to a more random distribution of the dislocation density.

  13. High-strength carbon nanotube fibre-like ribbon with high ductility and high electrical conductivity.

    PubMed

    Wang, J N; Luo, X G; Wu, T; Chen, Y

    2014-01-01

    Macroscopic fibres made up of carbon nanotubes exhibit properties far below theoretical predictions and even much lower than those for conventional carbon fibres. Here we report improvements of mechanical and electrical properties by more than one order of magnitude by pressurized rolling. Our carbon nanotubes self-assemble to a hollow macroscopic cylinder in a tube reactor operated at high temperature and then condense in water or ethanol to form a fibre, which is continually spooled in an open-air environment. This initial fibre is densified by rolling under pressure, leading to a combination of high tensile strength (3.76-5.53 GPa), high tensile ductility (8-13%) and high electrical conductivity ((1.82-2.24) × 10(4) S cm(-1)). Our study therefore demonstrates strategies for future performance maximization and the very considerable potential of carbon nanotube assemblies for high-end uses.

  14. 42. INTERIOR VIEW OF THE NAIL HARDENER USED TO HARDEN ...

    Library of Congress Historic Buildings Survey, Historic Engineering Record, Historic Landscapes Survey

    42. INTERIOR VIEW OF THE NAIL HARDENER USED TO HARDEN AND TEMPER THE NAILS; WEST TUBES IN FOREGRPUND AND DRAWBACK TUBE IN THE CENTER - LaBelle Iron Works, Thirtieth & Wood Streets, Wheeling, Ohio County, WV

  15. Contribution of β' and β precipitates to hardening in as-solutionized Ag-20Pd-12Au-14.5Cu alloys for dental prosthesis applications.

    PubMed

    Kim, Yonghwan; Niinomi, Mitsuo; Hieda, Junko; Nakai, Masaaki; Cho, Ken; Fukui, Hisao

    2014-04-01

    Dental Ag-20Pd-12Au-14.5Cu alloys exhibit a unique hardening behavior, which the mechanical strengths enhance significantly which enhances the mechanical strength significantly after high-temperature (1123K) solution treatment without aging treatment. The mechanism of the unique hardening is not clear. The contribution of two precipitates (β' and β phases) to the unique hardening behavior in the as-solutionized Ag-20Pd-12Au-14.5Cu alloys was investigated. In addition, the chemical composition of the β' phase was investigated. The fine β' phase densely precipitates in a matrix. The β' phase (semi-coherent precipitate), which causes lattice strain, contributes greatly to the unique hardening behavior. On the other hand, the coarse β phase sparsely precipitates in the matrix. The contribution of the β phase (incoherent precipitate), which does not cause lattice strain, is small. The chemical composition of the β' phase was determined. This study reveals that the fine β' phase precipitated by high-temperature solution treatment leads to the unique hardening behavior in dental Ag-20Pd-12Au-14.5Cu alloys in the viewpoints of the lattice strain contrast and interface coherency. It is expected to make the heat treatment process more practical for hardening. The determined chemical composition of β' phase would be helpful to study an unknown formation process of β' phase.

  16. Laser Surface Hardening of AISI 1045 Steel

    NASA Astrophysics Data System (ADS)

    Li, Ruifeng; Jin, Yajuan; Li, Zhuguo; Qi, Kai

    2014-09-01

    The study investigates laser surface hardening in the AISI 1045 steel using two different types of industrial laser: a high-power diode laser (HPDL) and a CO2 laser, respectively. The effect of process parameters such as beam power, travel speed on structure, case depth, and microhardness was examined. In most cases, a heat-affected zone (HAZ) formed below the surface; a substantial increase in surface hardness was achieved. In addition, big differences were found between the hardened specimens after HPDL surface hardening and CO2 laser surface hardening. For HPDL, depths of the HAZ were almost equal in total HAZ o, without surface melting. For CO2 laser, the depths changed a lot in the HAZ, with surface melting in the center. To better understand the difference of laser hardening results when use these two types of laser, numerical (ANSYS) analysis of the heat conduction involved in the process was also studied. For HPDL method, a rectangular beam spot and uniform energy distribution across the spot were assumed, while for CO2 laser, a circular beam spot and Gaussian energy distribution were assumed. The results showed that the energy distribution variety altered the thermal cycles of the HAZ dramatically. The rectangular HPDL laser beam spot with uniform energy distribution is much more feasible for laser surface hardening.

  17. Method of making high strength, tough alloy steel

    DOEpatents

    Thomas, Gareth; Rao, Bangaru V. N.

    1979-01-01

    A high strength, tough alloy steel, particularly suitable for the mining industry, is formed by heating the steel to a temperature in the austenite range (1000.degree.-1100.degree. C.) to form a homogeneous austenite phase and then cooling the steel to form a microstructure of uniformly dispersed dislocated martensite separated by continuous thin boundary films of stabilized retained austenite. The steel includes 0.2-0.35 weight % carbon, at least 1% and preferably 3-4.5% chromium, and at least one other subsitutional alloying element, preferably manganese or nickel. The austenite film is stable to subsequent heat treatment as by tempering (below 300.degree. C.) and reforms to a stable film after austenite grain refinement.

  18. Strength and flexibility of bulk high-{Tc} superconductors

    SciTech Connect

    Goretta, K.C.; Jiang, M.; Kupperman, D.S.; Lanagan, M.T.; Singh, J.P.; Vasanthamohan, N.; Hinks, D.G.; Mitchell, J.F.; Richardson, J.W. Jr.

    1996-08-01

    Strength, fracture toughness, and elastic modulus data have been gathered for bulk high-temperature superconductors, commercial 99.9% Ag, and a 1.2 at.% Mg/Ag alloy. These data have been used to calculate fracture strains for bulk conductors. The calculations indicate that the superconducting cores of clad tapes should begin to fracture at strains below 0.2%. In addition, residual strains in Ag-clad (Bi,Pb){sub 2}Sr{sub 2}Ca{sub 2}Cu{sub 3}O{sub x} tapes have been measured by neutron diffraction. An explanation is offered for why many tapes appear to be able to tolerate large strains before exhibiting a reduction in current transport.

  19. Thermal Transport in High-Strength Polymethacrylimide (PMI) Foam Insulations

    NASA Astrophysics Data System (ADS)

    Qiu, L.; Zheng, X. H.; Zhu, J.; Tang, D. W.; Yang, S. Y.; Hu, A. J.; Wang, L. L.; Li, S. S.

    2015-11-01

    Thermal transport in high-strength polymethacrylimide (PMI) foam insulations is described, with special emphasis on the density and temperature effects on the thermal transport performance. Measurements of the effective thermal conductivity are performed by a freestanding sensor-based 3ω method. A linear relationship between the density and the effective thermal conductivity is observed. Based on the analysis of the foam insulation morphological structures and the corresponding geometrical cell model, the quantitative contribution of the solid conductivity and the gas conductivity as well as the radiative conductivity to the total effective thermal conductivity as a function of the density and temperature is calculated. The agreement between the curves of the results from the developed model and experimental data indicate the model can be used for PMI foam insulating performance optimization.

  20. Advanced Gear Alloys for Ultra High Strength Applications

    NASA Technical Reports Server (NTRS)

    Shen, Tony; Krantz, Timothy; Sebastian, Jason

    2011-01-01

    Single tooth bending fatigue (STBF) test data of UHS Ferrium C61 and C64 alloys are presented in comparison with historical test data of conventional gear steels (9310 and Pyrowear 53) with comparable statistical analysis methods. Pitting and scoring tests of C61 and C64 are works in progress. Boeing statistical analysis of STBF test data for the four gear steels (C61, C64, 9310 and Pyrowear 53) indicates that the UHS grades exhibit increases in fatigue strength in the low cycle fatigue (LCF) regime. In the high cycle fatigue (HCF) regime, the UHS steels exhibit better mean fatigue strength endurance limit behavior (particularly as compared to Pyrowear 53). However, due to considerable scatter in the UHS test data, the anticipated overall benefits of the UHS grades in bending fatigue have not been fully demonstrated. Based on all the test data and on Boeing s analysis, C61 has been selected by Boeing as the gear steel for the final ERDS demonstrator test gearboxes. In terms of potential follow-up work, detailed physics-based, micromechanical analysis and modeling of the fatigue data would allow for a better understanding of the causes of the experimental scatter, and of the transition from high-stress LCF (surface-dominated) to low-stress HCF (subsurface-dominated) fatigue failure. Additional STBF test data and failure analysis work, particularly in the HCF regime and around the endurance limit stress, could allow for better statistical confidence and could reduce the observed effects of experimental test scatter. Finally, the need for further optimization of the residual compressive stress profiles of the UHS steels (resulting from carburization and peening) is noted, particularly for the case of the higher hardness C64 material.

  1. High-strength, thermally-stable nanostructured materials

    NASA Astrophysics Data System (ADS)

    Shankar, Ravi

    The properties of two technologically important precipitation-treatable alloys - Al 6061 and Inconel 718, that are deformed to large plastic strains at room temperature by machining, are presented. The strong effect of prior density of precipitates on the consequent microstructure refinement during chip formation was determined by deforming Al 6061 of different tempers to varying levels of strain, by varying the tool rake angle. Chips cut from peak-aged 6061, consisting of a fine dispersion of precipitates, produced the finest microstructure and are composed of sub-100 nm grains. On the other hand, coarser precipitate distributions in over-aged 6061 and an absence of precipitates in solution-treated 6061 resulted in much coarser microstructures. Thermal stability of such nanostructured chips with different levels of strain and precipitate distributions is analyzed by studying evolution of Vickers micro-hardness and microstructure after different heat treatments. Chips produced from the peak-aged temper and over-aged temper soften following heat treatment while those from the solution-treated state first, gain strength before softening. The results are rationalized based on prior studies of the characteristics and kinetics of precipitation and coarsening in Al-Mg-Si systems. It is then demonstrated that precipitate-stabilized nanostructured materials synthesized from a prototypical alloy system - Inconel 718, are extremely stable even after prolonged heat treatment for 240 hours at temperatures as high as one-half of the melting point. This extraordinary thermal stability is traced to the retention of a fine dispersion of precipitates in a nanostructured matrix even after extended heat treatment. It is anticipated that general design principles garnered from understanding of the causal phenomena determining strengthening and thermal stability, can lead to the development of alloy systems for the manufacture of high-strength, thermally-stable nanostructured materials.

  2. Corrosion and embrittlement of high-strength steel bridge wires

    NASA Astrophysics Data System (ADS)

    Vermaas, Garry Wayne

    Suspension bridge cable inspections have revealed severely corroded and broken wires in some main cables. Accelerated cyclic corrosion studies were conducted to assess the relative effect of corrosion on high-strength steel bridge wire. Galvanized and ungalvanized wire samples were corroded under various levels of sustained loads in a cabinet that cyclically applied an acidic salt spray, dry conditions, and 100% relative humidity at elevated temperature. Mass loss, hydrogen concentration, ultimate load, and elongation at failure were measured for corroded and uncorroded samples. Elongation measurements indicated a significant embrittlement of the wires that could not be explained only by the presence of absorbed hydrogen (hydrogen embrittlement). The main cause of reduction of wire elongation was found to be the surface irregularities induced by the corrosion process. The corrosion process in a high-strength steel wire was modeled and analyzed using finite element methods. Forty-one separate FEM tests were run and this data was compared to the experimental data. In addition, for the purpose of comparison, a previously developed hydrogen embrittlement model was analyzed and its validity was discussed in detail. SEM photographs of the fracture surfaces were taken and possible causes and mechanisms of fracture were suggested by observations of the fracture morphology. It was shown through this experimental and numerical research work that the geometry of the wire, determined by the amount of corrosion, pitting, and surface irregularities, controls the ultimate elongation of the wire sample, as also confirmed by the SEM analysis of the fracture surfaces. It was also shown that, using a generally accepted hydrogen embrittlement model, there is no evidence that hydrogen embrittlement is occurring, or at least that hydrogen evolution is not the controlling factor in the loss of wire's ductility.

  3. Fracture strength of glass chips for high-pressure microfluidics

    NASA Astrophysics Data System (ADS)

    Andersson, Martin; Hjort, Klas; Klintberg, Lena

    2016-09-01

    High-pressure microfluidics exposes new areas in chemistry. In this paper, the reliability of transparent borosilicate glass chips is investigated. Two designs of circular cavities are used for fracture strength tests, either 1.6 mm wide with rounded corners to the fluid inlets, or 2.0 mm wide with sharp inlet corners. Two kinds of tests are done, either short-term, e.g. pressurization to fracture at room temperature, or long-term, with fracture at constant pressurization for up to one week, in the temperature region 11-125 °C. The speed of crack fronts is measured using a high-speed camera. Results show fracture stresses in the range of 129 and 254 MPa for short-term measurements. Long-term measurements conclude the presences of a temperature and stress dependent delayed fracture. For a reliability of one week at 11-38 °C, a pressure limit is found at the lower end of the short-term measurements, or 15% lower than the average. At 80 °C, this pressure limit is 45% lower. Crack speeds are measured to be 10-5 m s-1 during short-term fracture. These measurements are comparable with estimations based on slow crack growth and show that the growth affects the reliability of glass chips. This effect is strongly affected by high temperatures, thus lowers the operating window of high-pressure glass microfluidic devices.

  4. Fracture strength of glass chips for high-pressure microfluidics

    NASA Astrophysics Data System (ADS)

    Andersson, Martin; Hjort, Klas; Klintberg, Lena

    2016-09-01

    High-pressure microfluidics exposes new areas in chemistry. In this paper, the reliability of transparent borosilicate glass chips is investigated. Two designs of circular cavities are used for fracture strength tests, either 1.6 mm wide with rounded corners to the fluid inlets, or 2.0 mm wide with sharp inlet corners. Two kinds of tests are done, either short-term, e.g. pressurization to fracture at room temperature, or long-term, with fracture at constant pressurization for up to one week, in the temperature region 11–125 °C. The speed of crack fronts is measured using a high-speed camera. Results show fracture stresses in the range of 129 and 254 MPa for short-term measurements. Long-term measurements conclude the presences of a temperature and stress dependent delayed fracture. For a reliability of one week at 11–38 °C, a pressure limit is found at the lower end of the short-term measurements, or 15% lower than the average. At 80 °C, this pressure limit is 45% lower. Crack speeds are measured to be 10‑5 m s‑1 during short-term fracture. These measurements are comparable with estimations based on slow crack growth and show that the growth affects the reliability of glass chips. This effect is strongly affected by high temperatures, thus lowers the operating window of high-pressure glass microfluidic devices.

  5. Folding and faulting of strain-hardening sedimentary rocks

    USGS Publications Warehouse

    Johnson, A.M.

    1980-01-01

    The question of whether single- or multi-layers of sedimentary rocks will fault or fold when subjected to layer-parallel shortening is investigated by means of the theory of elastic-plastic, strain-hardening materials, which should closely describe the properties of sedimentary rocks at high levels in the Earth's crust. The most attractive feature of the theory is that folding and faulting, intimately related in nature, are different responses of the same idealized material to different conditions. When single-layers of sedimentary rock behave much as strain-hardening materials they are unlikely to fold, rather they tend to fault, because contrasts in elasticity and strength properties of sedimentary rocks are low. Amplifications of folds in such materials are negligible whether contacts between layer and media are bonded or free to slip for single layers of dolomite, limestone, sandstone, or siltstone in media of shale. Multilayers of these same rocks fault rather than fold if contacts are bonded, but they fold readily if contacts between layers are frictionless, or have low yield strengths, for example due to high pore-water pressure. Faults may accompany the folds, occurring where compression is increased in cores of folds. Where there is predominant reverse faulting in sedimentary sequences, there probably were few structural units. ?? 1980.

  6. Effect of high doses of chemical admixtures on the strength development and freeze-thaw durability of portland cement mortar

    NASA Astrophysics Data System (ADS)

    Korhonen, Charles J.

    This thesis examines the low-temperature strength development of portland cement concrete made with high doses of chemical admixtures dissolved in the mixing water and the possible beneficial effect of these admixtures on that concrete's long-term freeze-thaw durability. The literature shows that high doses of chemical admixtures can protect fresh concrete against freezing and that, under certain conditions, these admixtures can enhance the freeze-thaw durability of concrete. The challenge is that there are no acceptance standards in the U.S. that allow chemicals to be used to protect concrete against freezing. Also, the perception is that chemicals might somehow harm the concrete. This perception seems to be based on the fact that deicing salts, when applied to concrete pavement, cause roadways to scale away. This study investigated the effect of high doses of commercially available admixtures on fresh concrete while it gained strength at low temperature and on hardened concrete exposed to repeated cycles of freezing and thawing in a moist environment. The reason for studying off-the-shelf admixtures was that these materials are approved for use in concrete; they were already governed by their own set of standards. Four mortars were examined, each with a different cement and water content, when dosed with five commercial admixtures. This allowed the fresh mortar to gain appreciable strength when it was kept at nearly -10C. The admixtures also enhanced the freeze-thaw durability of the mortar, even when it was not air-entrained. Clearly, as the dosage of admixture increased beyond approximately 22% by weight of water, the mortar appeared to be unaffected by up to 700 cycles of freezing and thawing.

  7. Constitutive modelling of evolving flow anisotropy including distortional hardening

    SciTech Connect

    Pietryga, Michael P.; Vladimirov, Ivaylo N.; Reese, Stefanie

    2011-05-04

    The paper presents a new constitutive model for anisotropic metal plasticity that takes into account the expansion or contraction (isotropic hardening), translation (kinematic hardening) and change of shape (distortional hardening) of the yield surface. The experimentally observed region of high curvature ('nose') on the yield surface in the loading direction and flattened shape in the reverse loading direction are modelled here by means of the concept of directional distortional hardening. The modelling of directional distortional hardening is accomplished by means of an evolving fourth-order tensor. The applicability of the model is illustrated by fitting experimental subsequent yield surfaces at finite plastic deformation. Comparisons with test data for aluminium low and high work hardening alloys display a good agreement between the simulation results and the experimental data.

  8. Anomalous softening of yield strength in tantalum at high pressures

    SciTech Connect

    Jing, Qiumin Wu, Qiang; Xu, Ji-an; Bi, Yan; Liu, Lei; Liu, Shenggang; Zhang, Yi; Geng, Huayun

    2015-02-07

    The pressure dependence of the yield strength of tantalum was investigated experimentally up to 101 GPa at room temperature using a diamond anvil cell. A yield strength softening is observed between 52 and 84 GPa, whereas a normal trend is observed below 52 GPa and above 84 GPa. The onset pressure of the softening is in agreement with previous results obtained by the pressure gradient method and shock wave experiments. This unusual strength softening in tantalum is not related with structural transformation, preferred orientation, or material damage. Our measurements indicate that microscopic deviatoric strain is the major reason for the observed strength softening in tantalum.

  9. Extracting strength from high pressure ramp-release experiments

    SciTech Connect

    Brown, J. L.; Alexander, C. S.; Asay, J. R.; Vogler, T. J.; Ding, J. L.

    2013-12-14

    Unloading from a plastically deformed state has long been recognized as a sensitive measure of a material's deviatoric response. In the case of a ramp compression and unload, time resolved particle velocity measurements of a sample/window interface may be used to gain insight into the sample material's strength. Unfortunately, measurements of this type are often highly perturbed by wave interactions associated with impedance mismatches. Additionally, wave attenuation, the finite pressure range over which the material elastically unloads, and rate effects further complicate the analysis. Here, we present a methodology that overcomes these shortcomings to accurately calculate a mean shear stress near peak compression for experiments of this type. A new interpretation of the self-consistent strength analysis is presented and then validated through the analysis of synthetic data sets on tantalum to 250 GPa. The synthetic analyses suggest that the calculated shear stresses are within 3% of the simulated values obtained using both rate-dependent and rate-independent constitutive models. Window effects are addressed by a new technique referred to as the transfer function approach, where numerical simulations are used to define a mapping to transform the experimental measurements to in situ velocities. The transfer function represents a robust methodology to account for complex wave interactions and a dramatic improvement over the incremental impedance matching methods traditionally used. The technique is validated using experiments performed on both lithium fluoride and tantalum ramp compressed to peak stresses of 10 and 15 GPa, respectively. In each case, various windows of different shock impedance are used to ensure consistency within the transfer function analysis. The data are found to be independent of the window used and in good agreement with previous results.

  10. Microscopic Origin of Strain Hardening in Methane Hydrate.

    PubMed

    Jia, Jihui; Liang, Yunfeng; Tsuji, Takeshi; Murata, Sumihiko; Matsuoka, Toshifumi

    2016-03-24

    It has been reported for a long time that methane hydrate presents strain hardening, whereas the strength of normal ice weakens with increasing strain after an ultimate strength. However, the microscopic origin of these differences is not known. Here, we investigated the mechanical characteristics of methane hydrate and normal ice by compressive deformation test using molecular dynamics simulations. It is shown that methane hydrate exhibits strain hardening only if the hydrate is confined to a certain finite cross-sectional area that is normal to the compression direction. For normal ice, it does not present strain hardening under the same conditions. We show that hydrate guest methane molecules exhibit no long-distance diffusion when confined to a finite-size area. They appear to serve as non-deformable units that prevent hydrate structure failure, and thus are responsible for the strain-hardening phenomenon.

  11. Microscopic Origin of Strain Hardening in Methane Hydrate

    PubMed Central

    Jia, Jihui; Liang, Yunfeng; Tsuji, Takeshi; Murata, Sumihiko; Matsuoka, Toshifumi

    2016-01-01

    It has been reported for a long time that methane hydrate presents strain hardening, whereas the strength of normal ice weakens with increasing strain after an ultimate strength. However, the microscopic origin of these differences is not known. Here, we investigated the mechanical characteristics of methane hydrate and normal ice by compressive deformation test using molecular dynamics simulations. It is shown that methane hydrate exhibits strain hardening only if the hydrate is confined to a certain finite cross-sectional area that is normal to the compression direction. For normal ice, it does not present strain hardening under the same conditions. We show that hydrate guest methane molecules exhibit no long-distance diffusion when confined to a finite-size area. They appear to serve as non-deformable units that prevent hydrate structure failure, and thus are responsible for the strain-hardening phenomenon. PMID:27009239

  12. High strength glass-ceramic to metal seals

    SciTech Connect

    Haws, L D; Kramer, D P; Moddeman, W E; Wooten, G W

    1986-12-01

    In many applications, ceramics are joined to other materials, especially metals. In such cases, interfacial strength is as important as the strength of each constituent material. Examples are presented for tailoring materials and processes to optimize the glass-ceramic-to-metal seal. Means for detecting defects, nondestructively, are also identified.

  13. High strength alumina produced by direct coagulation casting

    SciTech Connect

    Baader, F.H.; Will, J.; Tieche, D.

    1995-09-01

    Direct Coagulation Casting is a new colloidal forming technique. Double layer stabilized, concentrated alumina suspensions are solidified by shifting the suspensions pH from 4 towards the isoelectric point at 9 using the in situ enzyme-catalyzed decomposition of urea. This reaction minimizes the repulsive forces between the suspended particles. The remaining, attractive Van der Waals forces form a stiff particle network. Suspensions with low viscosities (0.3 Pa*s, 59 vol%) were prepared at pH 4. Deagglomeration of the suspensions by ball milling reduced the agglomerate size below 5 pm. The coagulation kinetics could be influenced either by the urease concentration or by the suspension temperature. Process variables were established, providing long idle times, which allowed additional filtration and degassing steps. Coagulation was followed by drying and sintering, whereby densities of more than 3.97 g/cm{sup 3}, a 4-point bending strength of 685 MPa (HIPed) and a high reliablility (m = 40) for high purity alumina were achieved. DCC has the potential to improve the reliability of alumina components of complex shape, as well as to avoid expensive molding.

  14. High-strength and high-ductility nanostructured and amorphous metallic materials.

    PubMed

    Kou, Hongning; Lu, Jian; Li, Ying

    2014-08-20

    The development of materials with dual properties of high strength and high ductility has been a constant challenge since the foundation of the materials science discipline. The rapid progress of nanotechnology in recent decades has further brought this challenge to a new era. This Research News highlights a few newly developed strategies to optimize advanced nanomaterials and metallic glasses with exceptional dual mechanical properties of high strength and high ductility. A general concept of strain non-localization is presented to describe the role of multiscale (i.e., macroscale, microscale, nanoscale, and atomic scale) heterogeneities in the ductility enhancement of materials reputed to be intrinsically brittle, such as nanostructured metallic materials and bulk metallic glasses. These nanomaterials clearly form a new group of materials that display an extraordinary relationship between yield strength and the uniform elongation with the same chemical composition. Several other examples of nanomaterials such as those reinforced by nanoprecipitates will also be described.

  15. Orbital Winch for High-Strength, Space-Survivable Tethers

    NASA Technical Reports Server (NTRS)

    Hoyt, Robert; Barnes, Ian; Slostad, Jeffrey; Frank, Scott

    2010-01-01

    An Orbital Winch mechanism enables high-load, multi-line tethers to be deployed and retracted without rotating the spool on which the tether is wound. To minimize damage to the tether and the wound package during retraction or deployment under load, it can incorporate a Tension Management Module that reduces the infeed tension by a factor of 15 through the use of a powered capstan with guide rollers. This design eliminates the need for rotating high-voltage electrical connections in tether systems that use propellantless electro-dynamic propulsion. It can also eliminate the need for rotating optical connections in applications where the tether contains optical fibers. This winch design was developed to deploy a 15-km-long, 15-kg high-strength Hoytether structure incorporating conductive wires as part of the MXER-1 demonstration mission concept. Two slewing rings that orbit around the tether spool, combined with translation of one of the slewing rings back and forth along the spool axis to traverse the wind point, enables the winch to wind the tether. Variations of the traverse motion of the slewing ring can accomplish level winds and conical pirn winds. By removing the non-traversing slewing ring, and adding an actuated guide arm, the winch can manage rapid, low-drag deployment of a tether off the end of a pirn-wound spool, followed by controlled retraction and rewinding, in a manner very similar to a spin-casting reel. The winch requires at least two motor driver controller units to coordinate the action of two stepper motors to accomplish tether deployment or retraction.

  16. High-strength transparent spinel with fine, unimodal grain size

    NASA Astrophysics Data System (ADS)

    Sweeney, S. M.; Brun, M. K.; Yosenick, T. J.; Kebbede, A.; Manoharan, M.

    2009-05-01

    Spinel (MgAl2O4) is a good candidate material for transparent armor and IR window applications. Traditionally, transparent spinel has suffered from poor strength and difficult polishing owing to its large, bimodal grain structure. Starting from a spinel nanopowder, spinel ceramics with a grain size of less than 2 microns have been made with better than 80% in-line transmittance at 632 nm wavelength for 3/8" thick samples. A ring-on-ring test has been used to measure biaxial flexural strength on samples machined to 0.8 mm thickness. The average strength was found to exceed 480 MPa.

  17. A lightweight, high strength dexterous manipulator for commercial applications

    NASA Technical Reports Server (NTRS)

    Marzwell, Neville I.; Schena, Bruce M.; Cohan, Steve M.

    1991-01-01

    The concept, design, and features are described of a lightweight, high strength, modular robot manipulator being developed for space and commercial applications. The manipulator has seven fully active degrees of freedom and is fully operational in 1 G. Each of the seven joints incorporates a unique drivetrain design which provides zero backlash operation, is insensitive to wear, and is single fault tolerant to motor or servo amplifier failure. Feedback sensors provide position, velocity, torque, and motor winding temperature information at each joint. This sensing system is also designed to be single fault tolerant. The manipulator consists of five modules (not including gripper). These modules join via simple quick-disconnect couplings and self-mating connectors which allow rapid assembly and/or disassembly for reconfiguration, transport, or servicing. The manipulator is a completely enclosed assembly, with no exposed components or wires. Although the initial prototype will not be space qualified, the design is well suited to meeting space requirements. The control system provides dexterous motion by controlling the endpoint location and arm pose simultaneously. Potential applications are discussed.

  18. Thermal Desorption Analysis of Hydrogen in High Strength Martensitic Steels

    NASA Astrophysics Data System (ADS)

    Enomoto, M.; Hirakami, D.; Tarui, T.

    2012-02-01

    Thermal desorption analyses (TDA) were conducted in high strength martensitic steels containing carbon from 0.33 to 1.0 mass pct, which were charged with hydrogen at 1223 K (950 °C) under hydrogen of one atmospheric pressure and quenched to room temperature. In 0.33C steel, which had the highest M s temperature, only one desorption peak was observed around 373 K (100 °C), whereas two peaks, one at a similar temperature and the other around and above 573 K (300 °C), were observed in the other steels, the height of the second peak increasing with carbon content. In 0.82C steel, both peaks disappeared during exposure at room temperature in 1 week, whereas the peak heights decreased gradually over 2 weeks in specimens electrolytically charged with hydrogen and aged for varying times at room temperature. From computer simulation, by means of the McNabb-Foster theory coupled with theories of carbon segregation, these peaks are likely to be due to trapping of hydrogen in the strain fields and cores of dislocations, and presumably to a lesser extent in prior austenite grain boundaries. The results also indicate that carbon atoms prevent and even expel hydrogen from trapping sites during quenching and aging in these steels.

  19. Anomolous Fatigue Crack Growth Phenomena in High-Strength Steel

    NASA Technical Reports Server (NTRS)

    Forth, Scott C.; James, Mark A.; Johnston, William M., Jr.; Newman, James C., Jr.

    2004-01-01

    The growth of a fatigue crack through a material is the result of a complex interaction between the applied loading, component geometry, three-dimensional constraint, load history, environment, material microstructure and several other factors. Previous studies have developed experimental and computational methods to relate the fatigue crack growth rate to many of the above conditions, with the intent of discovering some fundamental material response, i.e. crack growth rate as a function of something. Currently, the technical community uses the stress intensity factor solution as a simplistic means to relate fatigue crack growth rate to loading, geometry and all other variables. The stress intensity factor solution is a very simple linear-elastic representation of the continuum mechanics portion of crack growth. In this paper, the authors present fatigue crack growth rate data for two different high strength steel alloys generated using standard methods. The steels exhibit behaviour that appears unexplainable, compared to an aluminium alloy presented as a baseline for comparison, using the stress intensity factor solution.

  20. Titanium cholla : lightweight, high-strength structures for aerospace applications.

    SciTech Connect

    Atwood, Clinton J.; Voth, Thomas Eugene; Taggart, David G.; Gill, David Dennis; Robbins, Joshua H.; Dewhurst, Peter

    2007-10-01

    Aerospace designers seek lightweight, high-strength structures to lower launch weight while creating structures that are capable of withstanding launch loadings. Most 'light-weighting' is done through an expensive, time-consuming, iterative method requiring experience and a repeated design/test/redesign sequence until an adequate solution is obtained. Little successful work has been done in the application of generalized 3D optimization due to the difficulty of analytical solutions, the large computational requirements of computerized solutions, and the inability to manufacture many optimized structures with conventional machining processes. The Titanium Cholla LDRD team set out to create generalized 3D optimization routines, a set of analytically optimized 3D structures for testing the solutions, and a method of manufacturing these complex optimized structures. The team developed two new computer optimization solutions: Advanced Topological Optimization (ATO) and FlexFEM, an optimization package utilizing the eXtended Finite Element Method (XFEM) software for stress analysis. The team also developed several new analytically defined classes of optimized structures. Finally, the team developed a 3D capability for the Laser Engineered Net Shaping{trademark} (LENS{reg_sign}) additive manufacturing process including process planning for 3D optimized structures. This report gives individual examples as well as one generalized example showing the optimized solutions and an optimized metal part.

  1. High strength bioactive glass-ceramic scaffolds for bone regeneration.

    PubMed

    Vitale-Brovarone, Chiara; Baino, Francesco; Verné, Enrica

    2009-02-01

    This research work is focused on the preparation of macroporous glass-ceramic scaffolds with high mechanical strength, equivalent with cancellous bone. The scaffolds were prepared using an open-cells polyurethane sponge as a template and glass powders belonging to the system SiO(2)-P(2)O(5)-CaO-MgO-Na(2)O-K(2)O. The glass, named as CEL2, was synthesized by a conventional melting-quenching route, ground and sieved to obtain powders of specific size. A slurry of CEL2 powders, polyvinyl alcohol (PVA) as a binder and water was prepared in order to coat, by a process of impregnation, the polymeric template. A thermal treatment was then used to remove the sponge and to sinter the glass powders, in order to obtain a replica of the template structure. The scaffolds were characterized by means of X-ray diffraction analysis, morphological observations, density measurements, volumetric shrinkage, image analysis, capillarity tests, mechanical tests and in vitro bioactivity evaluation.

  2. Cleavage fracture in high strength low alloy weld metal

    SciTech Connect

    Bose, W.W.; Bowen, P.; Strangwood, M.

    1996-12-31

    The present investigation gives an evaluation of the effect of microstructure on the cleavage fracture process of High Strength Low Alloy (HSLA) multipass weld metals. With additions of alloying elements, such as Ti, Ni, Mo and Cr, the microstructure of C-Mn weld metal changes from the classical composition, i.e., allotriomorphic ferrite with acicular ferrite and Widmanstaetten ferrite, to bainite and low carbon martensite. Although the physical metallurgy of some HSLA weld metals has been studied before, more work is necessary to correlate the effect of the microstructure on the fracture behavior of such weld metals. In this work detailed microstructural analysis was carried out using optical and electron (SEM and TEM) microscopy. Single edge notched (SEN) bend testpieces were used to assess the cleavage fracture stress, {sigma}{sub F}. Inclusions beneath the notch surface were identified as the crack initiators of unstable cleavage fracture. From the size of such inclusions and the value of tensile stress predicted at the initiation site, the effective surface energy for cleavage was calculated using a modified Griffth energy balance for a penny shape crack. The results suggest that even though inclusions initiate cleavage fracture, the local microstructure may play an important role in the fracture process of these weld metals. The implications of these observations for a quantitative theory of the cleavage fracture of ferritic steels is discussed.

  3. Polyimide films from vapor deposition: toward high strength, NIF capsules

    SciTech Connect

    Cook, R C; Hsieh, E J; Letts, S A; Roberts, C C; Saculla, M

    1998-10-16

    The focus of recent efforts at LLNL has been to demonstrate that vapor deposition processing is a suitable technique to form polyimide fnms with sufficient strength for current national ignition facility target specifications. Production of polyimide films with controlled stoichiometry was acccomplished by: 1) depositing a novel co-functional monomer and 2) matching the vapor pressure of each monomer in PMDA/ODA co-depositions. The sublimation and deposition rate for the monomers was determined over a range of temperatures. Polyimide films with thicknesses up to 30 p.m were fabricated. Composition, structure and strength were assessed using FTIR, SEM and biaxial burst testing. The best films had a tensile strength of approximately 100 MPa. A qualitative relationship between the stoichiometry and tensile strength of the film was demonstrated. Thin films ({approximately}3.5 {micro}m) were typically smooth with an rms of 1.5 nm.

  4. Precipitation hardening austenitic superalloys

    DOEpatents

    Korenko, Michael K.

    1985-01-01

    Precipitation hardening, austenitic type superalloys are described. These alloys contain 0.5 to 1.5 weight percent silicon in combination with about 0.05 to 0.5 weight percent of a post irradiation ductility enhancing agent selected from the group of hafnium, yttrium, lanthanum and scandium, alone or in combination with each other. In addition, when hafnium or yttrium are selected, reductions in irradiation induced swelling have been noted.

  5. Nuclear effects hardened shelters

    NASA Astrophysics Data System (ADS)

    Lindke, Paul

    1990-11-01

    The Houston Fearless 76 Government Projects Group has been actively engaged for more than twenty-five years as a sub-contractor and currently as a prime contractor in the design, manufacture, repair and logistics support of custom mobile ground stations and their equipment accommodations. Other associated products include environmental control units (ECU's), mobilizers for shelters and a variety of mobile power generation units (MPU's). Since 1984, Houston Fearless 76 has designed and manufactured four 8' x 8' x 22' nuclear hardened mobile shelters. These shelters were designed to contain electronic data processing/reduction equipment. One shelter is currently being operated by the Air Force as a Defense Intelligence Agency (DIA) approved and certified Special Corrpartmented Information Facility (SCIF). During the development and manufacturing process of the shelters, we received continual technical assistance and design concept evaluations from Science Applications International Corporation (SAIC) Operations Analysis and Logistics Engineering Division and the Nondestructive Inspection Lab at McClellan AFB. SAIC was originally employed by the Air Force to design the nuclear hardening specifications applied to these shelters. The specific levels of hardening to which the shelters were designed are classified and will not be mentioned during this presentation.

  6. Highly controllable and green reduction of graphene oxide to flexible graphene film with high strength

    SciTech Connect

    Wan, Wubo; Zhao, Zongbin; Hu, Han; Gogotsi, Yury; Qiu, Jieshan

    2013-11-15

    Graphical abstract: Highly controllable and green reduction of GO to chemical converted graphene (CCG) was achieved with sodium citrate as a facile reductant. Self-assembly of the as-made CCG sheets results in a flexible CCG film, of which the tensile strength strongly depends on the deoxygenation degree of graphene sheets. - Highlights: • Graphene was synthesized by an effective and environmentally friendly approach. • We introduced a facile X-ray diffraction analysis method to investigate the reduction process from graphene oxide to graphene. • Flexible graphene films were prepared by self-assembly of the graphene sheets. • The strength of the graphene films depends on the reduction degree of graphene. - Abstract: Graphene film with high strength was fabricated by the assembly of graphene sheets derived from graphene oxide (GO) in an effective and environmentally friendly approach. Highly controllable reduction of GO to chemical converted graphene (CCG) was achieved with sodium citrate as a facile reductant, in which the reduction process was monitored by XRD analysis and UV–vis absorption spectra. Self-assembly of the as-made CCG sheets results in a flexible CCG film. This method may open an avenue to the easy and scalable preparation of graphene film with high strength which has promising potentials in many fields where strong, flexible and electrically conductive films are highly demanded.

  7. Microstructure Evolution and Hardness of an Ultra-High Strength Cu-Ni-Si Alloy During Thermo-mechanical Processing

    NASA Astrophysics Data System (ADS)

    Lei, Q.; Li, Z.; Hu, W. P.; Liu, Y.; Meng, C. L.; Derby, B.; Zhang, W.

    2016-07-01

    Microstructure evolution and hardness changes of an ultra-high strength Cu-Ni-Si alloy during thermo-mechanical processing have been investigated. For hot-compressive deformation specimens, dynamic recrystallization preferentially appeared on deformation bands. As deformation temperature increased from 750 to 900 °C, elongated grains with the Cubic texture {001} <100> were substituted by recrystallized grains with Copper texture {112} <111>. For the samples having undergone cold rolling followed by annealing, static recrystallization preferentially occurred in the deformation bands, and then complete recrystallization occurred. Goss, Cubic, and Brass textures remained after annealing at 600 and 700 °C for 1 h; R texture {111} <211> and recrystallization texture {001} <100> were formed in samples annealed at 800 and 900 °C for 1 h, respectively. For samples processed under multi-directional forging at cryogenic temperature, the hardness was increased as a result of work hardening and grain refinement strengthening. These were attributed to the formation of equiaxed sub-grain structures and a high dislocation density.

  8. In Situ Nanoindentation Studies on Detwinning and Work Hardening in Nanotwinned Monolithic Metals

    DOE PAGES

    Liu, Y.; Li, N.; Bufford, D.; Lee, J. H.; Wang, J.; Wang, H.; Zhang, X.

    2015-07-14

    Certain nanotwinned (nt) metals have rare combinations of high mechanical strength and ductility. Here, we review recent in situ nanoindentation studies (using transmission electron microscopes) on the deformation mechanisms of nt face-centered cubic metals including Cu, Ni, and Al with a wide range of stacking fault energy (SFE). Moreover, in nt Cu with low-to-intermediate SFE, detwinning (accompanied by rapid twin boundary migration) occurs at ultralow stress. In Ni with relatively high SFE, coherent {111} twin boundaries lead to substantial work hardening. Twinned Al has abundant {112} incoherent twin boundaries, which induce significant work-hardening capability and plasticity in Al. Finally, twinmore » boundaries in Al also migrate but at very high stresses. Furthermore, molecular dynamics simulations reveal the influence of SFE on deformation mechanisms in twinned metals.« less

  9. In Situ Nanoindentation Studies on Detwinning and Work Hardening in Nanotwinned Monolithic Metals

    SciTech Connect

    Liu, Y.; Li, N.; Bufford, D.; Lee, J. H.; Wang, J.; Wang, H.; Zhang, X.

    2015-07-14

    Certain nanotwinned (nt) metals have rare combinations of high mechanical strength and ductility. Here, we review recent in situ nanoindentation studies (using transmission electron microscopes) on the deformation mechanisms of nt face-centered cubic metals including Cu, Ni, and Al with a wide range of stacking fault energy (SFE). Moreover, in nt Cu with low-to-intermediate SFE, detwinning (accompanied by rapid twin boundary migration) occurs at ultralow stress. In Ni with relatively high SFE, coherent {111} twin boundaries lead to substantial work hardening. Twinned Al has abundant {112} incoherent twin boundaries, which induce significant work-hardening capability and plasticity in Al. Finally, twin boundaries in Al also migrate but at very high stresses. Furthermore, molecular dynamics simulations reveal the influence of SFE on deformation mechanisms in twinned metals.

  10. High-strength stainless steels for corrosion mitigation in prestressed concrete: Development and evaluation

    NASA Astrophysics Data System (ADS)

    Moser, Robert D.

    Corrosion of prestressing reinforcement in concrete structures exposed to marine environments and/or deicing chemicals is a problem of critical concern. While many corrosion mitigation technologies are available for reinforced concrete (RC), those available for use in prestressed concrete (PSC) are limited and in many cases cannot provide the 100+ year service life needed in new construction, particularly when exposed to severe marine environments. The use of stainless steel alloys in RC structures has shown great success in mitigating corrosion in even the most severe of exposures. However, the use of high-strength stainless steels (HSSSs) for corrosion mitigation in PSC structures has received limited attention. To address these deficiencies in knowledge, an experimental study was conducted to investigate the feasibility of using HSSSs for corrosion mitigation in PSC. The study examined mechanical behavior, corrosion resistance, and techniques for the production of HSSS prestressing strands. Stainless steel grades 304, 316, 2101, 2205, 2304, and 17-7 were produced as cold drawn wires with diameters of approximately 4 mm (0.16 in). A 1080 prestressing steel was also included to serve as a control. Tensile strengths of 1250 to 1550 MPa (181 to 225 ksi) were achieved in the cold-drawn candidate HSSSs. Non-ductile failure modes with no post-yield strain hardening were observed in all candidate HSSSs. 1000 hr stress relaxation of all candidate HSSSs was predicted to be between 6 and 8 % based on the results of 200 hr tests conducted at 70 % of the ultimate tensile strength. Residual stresses due to the cold drawing had a significant influence on stress vs. strain behavior and stress relaxation. Electrochemical corrosion testing found that in solutions simulating alkaline concrete, all candidate HSSSs showed exceptional corrosion resistance at chloride (Cl-) concentrations from zero to 0.25 M. However, when exposed to solutions simulating carbonated concrete, corrosion

  11. TRP 9904 - Constitutive Behavior of High Strength Multiphase Sheel Steel Under High Strain Rate Deformation

    SciTech Connect

    David Matlock; John Speer

    2005-03-31

    The focus of the research project was to systematically assess the strain rate dependence of strengthening mechanisms in new advanced high strength sheet steels. Data were obtained on specially designed and produced Duel Phase and TRIP steels and compared to the properties of automotive steels currently in use.

  12. High-strength high-conductivity Cu-Nb microcomposite sheet fabricated via multiple roll bonding

    NASA Astrophysics Data System (ADS)

    Jha, S. C.; Delagi, R. G.; Forster, J. A.; Krotz, P. D.

    1993-01-01

    Copper-niobium microcomposites are a new class of high-strength high-conductivity materials that have attractive properties for room- and elevated-temperature applications. Since Nb has little solid solubility in Cu, addition of Nb to Cu does not affect its conductivity. Copper-niobium microcomposites are melted and cast so that the microstructure of cast Cu-Nb ingots consists of 1-to 10 μm Nb dendrites uniformly distributed within the copper matrix. Extensive wire drawing with a true processing strain ( η > 12) of Cu-Nb alloy leads to refinement and elongation of Nb dendrites into 1-to 10 nm-thick filaments. The presence of such fine Nb filaments causes a significant increase in the strength of Cu-Nb wires. The tensile strength of heavily drawn Cu-Nb wires was determined to be significantly higher than the values predicted by the rule of mixtures. This article reports the fabrication of high-strength Cu-Nb micro-composite sheet by multiple roll bonding. It is difficult and impractical to attain high processing strains ( η > 3) by simple cold rolling. In most practical cold-rolling operation, the thickness reduction does not exceed 90 pct ( η ≅ 2). Therefore, innovative processing is required to generate high strength in Cu-Nb microcomposite sheet. Multiple roll bonding of Cu-Nb has been utilized to store high processing strain ( η > 10) in the material and refine the Nb particle size within the copper matrix. This article describes the microstructure, mechanical properties, and thermal stability of roll-bonded Cu-Nb microcomposite sheet.

  13. Grain boundary hardening and triple junction hardening in polycrystalline molybdenum

    SciTech Connect

    Kobayashi, Shigeaki . E-mail: skoba@ashitech.ac.jp; Tsurekawa, Sadahiro; Watanabe, Tadao

    2005-02-01

    The grain boundary and triple junction hardenings in molybdenum with different carbon content were studied in connection with the character and the connectivity of grain boundaries at triple junctions by the micro-indentation test. The triple junction hardening is smaller at the junctions composed of low-angle and {sigma} boundaries than at the junctions composed of random boundaries. This difference in the hardening depending on the grain boundary connectivity becomes more significant with a decrease in carbon content in molybdenum.

  14. Strain Hardening and Size Effect in Five-fold Twinned Ag Nanowires.

    PubMed

    Narayanan, Sankar; Cheng, Guangming; Zeng, Zhi; Zhu, Yong; Zhu, Ting

    2015-06-10

    Metallic nanowires usually exhibit ultrahigh strength but low tensile ductility owing to their limited strain hardening capability. Here we study the unique strain hardening behavior of the five-fold twinned Ag nanowires by nanomechanical testing and atomistic modeling. In situ tensile tests within a scanning electron microscope revealed strong strain hardening behavior of the five-fold twinned Ag nanowires. Molecular dynamics simulations showed that such strain hardening was critically controlled by twin boundaries and pre-existing defects. Strain hardening was size dependent; thinner nanowires achieved more hardening and higher ductility. The size-dependent strain hardening was found to be caused by the obstruction of surface-nucleated dislocations by twin boundaries. Our work provides mechanistic insights into enhancing the tensile ductility of metallic nanostructures by engineering the internal interfaces and defects.

  15. Deformation in metals after low temperature irradiation: Part II - Irradiation hardening, strain hardening, and stress ratios

    SciTech Connect

    Byun, Thak Sang; Li, Meimei

    2008-03-01

    Effects of irradiation at temperatures 200oC on tensile stress parameters are analyzed for dozens of bcc, fcc, and hcp pure metals and alloys, focusing on irradiation hardening, strain hardening, and relationships between the true stress parameters. Similar irradiation-hardening rates are observed for all the metals irrespective of crystal type; typically, the irradiation-hardening rates are large, in the range 100 - 1000 GPa/dpa, at the lowest dose of <0.0001 dpa and decrease with dose to a few tens of MPa/dpa or less at about 10 dpa. However, average irradiation-hardening rates over the dose range of 0 dpa − (the dose to plastic instability at yield) are considerably lower for stainless steels due to their high uniform ductility. It is shown that whereas low temperature irradiation increases the yield stress, it does not significantly change the strain-hardening rate of metallic materials; it decreases the fracture stress only when non-ductile failure occurs. Such dose independence in strain hardening behavior results in strong linear relationships between the true stress parameters. Average ratios of plastic instability stress to unirradiated yield stress are about 1.4, 3.9, and 1.3 for bcc metals (and precipitation hardened IN718 alloy), annealed fcc metals (and pure Zr), and Zr-4 alloy, respectively. Ratios of fracture stress to plastic instability stress are calculated to be 2.2, 1.7, and 2.1, respectively. Comparison of these values confirms that the annealed fcc metals and other soft metals have larger uniform ductility but smaller necking ductility when compared to other materials.

  16. Modeling of Irradiation Hardening of Polycrystalline Materials

    SciTech Connect

    Li, Dongsheng; Zbib, Hussein M.; Garmestani, Hamid; Sun, Xin; Khaleel, Mohammad A.

    2011-09-14

    High energy particle irradiation of structural polycrystalline materials usually produces irradiation hardening and embrittlement. The development of predict capability for the influence of irradiation on mechanical behavior is very important in materials design for next generation reactors. In this work a multiscale approach was implemented to predict irradiation hardening of body centered cubic (bcc) alpha-iron. The effect of defect density, texture and grain boundary was investigated. In the microscale, dislocation dynamics models were used to predict the critical resolved shear stress from the evolution of local dislocation and defects. In the macroscale, a viscoplastic self-consistent model was applied to predict the irradiation hardening in samples with changes in texture and grain boundary. This multiscale modeling can guide performance evaluation of structural materials used in next generation nuclear reactors.

  17. Radiation-Hardened Electronics for the Space Environment

    NASA Technical Reports Server (NTRS)

    Keys, Andrew S.; Watson, Michael D.

    2007-01-01

    RHESE covers a broad range of technology areas and products. - Radiation Hardened Electronics - High Performance Processing - Reconfigurable Computing - Radiation Environmental Effects Modeling - Low Temperature Radiation Hardened Electronics. RHESE has aligned with currently defined customer needs. RHESE is leveraging/advancing SOA space electronics, not duplicating. - Awareness of radiation-related activities through out government and industry allow advancement rather than duplication of capabilities.

  18. Radiation Hardened Electronics for Space Environments (RHESE)

    NASA Technical Reports Server (NTRS)

    Keys, Andrew S.; Adams, James H.; Frazier, Donald O.; Patrick, Marshall C.; Watson, Michael D.; Johnson, Michael A.; Cressler, John D.; Kolawa, Elizabeth A.

    2007-01-01

    Radiation Environmental Modeling is crucial to proper predictive modeling and electronic response to the radiation environment. When compared to on-orbit data, CREME96 has been shown to be inaccurate in predicting the radiation environment. The NEDD bases much of its radiation environment data on CREME96 output. Close coordination and partnership with DoD radiation-hardened efforts will result in leveraged - not duplicated or independently developed - technology capabilities of: a) Radiation-hardened, reconfigurable FPGA-based electronics; and b) High Performance Processors (NOT duplication or independent development).

  19. Growing the Seeds of Strength in High Risk Urban Neighborhoods.

    ERIC Educational Resources Information Center

    Saegert, Susan

    The lives of poor minority city residents demonstrate the diversity, multiple potentials, and vulnerability to external structures. In spite of the stereotypes of failure and the very real problems of the urban poor, there are many strengths among the so-called urban underclass and there are aspects of life that are successful and productive. In…

  20. High-pressure reactions and shear strength of serpentinized dunite.

    PubMed

    Sclar, C B; Carrison, L C; Rooney, T P; Riecker, R E

    1966-09-01

    The recently reported Pronounced decrease in shear strength of serpentine-bearing rocks at 30 to 40 kilobars in the temperature range 300 degrees to 520 degrees C may be attributed to the transformation of serpentine to a Pressure-dependent, 10-angstrom,2: 1 layer silicate plus brucite and periclase. This reaction increases density by about 8.5 percent. PMID:17754251

  1. Weld Metallurgy and Mechanical Properties of High Manganese Ultra-high Strength Steel Dissimilar Welds

    NASA Astrophysics Data System (ADS)

    Dahmen, Martin; Lindner, Stefan; Monfort, Damien; Petring, Dirk

    The increasing demand for ultra-high strength steels in vehicle manufacturing leads to the application of new alloys. This poses a challenge on joining especially by fusion welding. A stainless high manganese steel sheet with excellent strength and deformation properties stands in the centre of the development. Similar and dissimilar welds with a metastable austenitic steel and a hot formed martensitic stainless steel were performed. An investigation of the mixing effects on the local microstructure and the hardness delivers the metallurgical features of the welds. Despite of carbon contents above 0.4 wt.% none of the welds have shown cracks. Mechanical properties drawn from tensile tests deliver high breaking forces enabling a high stiffness of the joints. The results show the potential for the application of laser beam welding for joining in assembly of structural parts.

  2. High strength-high conductivity Cu--Fe composites produced by powder compaction/mechanical reduction

    DOEpatents

    Verhoeven, John D.; Spitzig, William A.; Gibson, Edwin D.; Anderson, Iver E.

    1991-08-27

    A particulate mixture of Cu and Fe is compacted and mechanically reduced to form an "in-situ" Cu-Fe composite having high strength and high conductivity. Compaction and mechanical reduction of the particulate mixture are carried out at a temperature and time at temperature selected to avoid dissolution of Fe into the Cu matrix particulates to a harmful extent that substantially degrades the conductivity of the Cu-Fe composite.

  3. High strength-high conductivity Cu-Fe composites produced by powder compaction/mechanical reduction

    DOEpatents

    Verhoeven, J.D.; Spitzig, W.A.; Gibson, E.D.; Anderson, I.E.

    1991-08-27

    A particulate mixture of Cu and Fe is compacted and mechanically reduced to form an ''in-situ'' Cu-Fe composite having high strength and high conductivity. Compaction and mechanical reduction of the particulate mixture are carried out at a temperature and time at temperature selected to avoid dissolution of Fe into the Cu matrix particulates to a harmful extent that substantially degrades the conductivity of the Cu-Fe composite. 5 figures.

  4. Modelling and simulation of the influence of forming processes on the structural behavior of high strength steels

    NASA Astrophysics Data System (ADS)

    Gelin, J. C.; Thibaud, S.; Boudeau, N.

    2005-08-01

    The paper first describes experiments and modeling concerning the identification of material behavior for high strength steels with phase transformations associated to plastic deformation. The experiments consist of tensile and bulging tests carried out on 316L stainless steels and TRIP 700 steels used in automotive industry. These experiments have permitted to determine the hardening curves of such materials vs. the martensite volume fraction associated to plastic deformation. It has been demonstrated that the stress triaxiality has a major role in the martenstic transformation and a model is proposed to define the flow stress vs. effective strain accounting planar anisotropy and variation of martenstic volume fraction. Then a plasticity model has been proposed in an anisotropic form and the related flow rules have been defined. The resulting model has been implemented in different finite elements software, and applied in numerical simulations of stamping and hydroforming of typical components to prove the effects of forming processes on the resulting properties of the components. Finally, the structural behavior of the resulting components is investigated and the effects of forming processes on the resulting structural behaviour are analyzed. Two cases are presented, one concerns the deep drawing of a cylindrical cup and the other concerns the stamping of a closed U channel used as a structural part for crash frames. Is has been clearly proved that the variation of martensite volume fraction arising during processing has a strong influence on the resulting behaviour of the parts considering springback and crash resistance.

  5. Practical aspects of systems hardening

    SciTech Connect

    Shepherd, W.J.

    1989-01-01

    Applications of hardening technology in a practical system require a balance between the factors governing affordability, producibility, and survivability of the finished design. Without careful consideration of the top-level system operating constraints, a design engineer may find himself with a survivable but overweight, unproductive, expensive design. This paper explores some lessons learned in applying hardening techniques to several laser communications programs and is intended as an introductory guide to novice designers faced with the task of hardening a space system.

  6. High breakdown-strength composites from liquid silicone rubbers

    NASA Astrophysics Data System (ADS)

    Vudayagiri, Sindhu; Zakaria, Shamsul; Yu, Liyun; Sager Hassouneh, Suzan; Benslimane, Mohamed; Ladegaard Skov, Anne

    2014-10-01

    In this paper we investigate the performance of liquid silicone rubbers (LSRs) as dielectric elastomer transducers. Commonly used silicones in this application include room-temperature vulcanisable (RTV) silicone elastomers and composites thereof. Pure LSRs and their composites with commercially available fillers (an anatase TiO2, a core-shell TiO2-SiO2 and a CaCu3Ti4O12 filler) are evaluated with respect to dielectric permittivity, elasticity (Young’s modulus) and electrical breakdown strength. Film formation properties are also evaluated. The best-performing formulations are those with anatase TiO2 nanoparticles, where the highest relative dielectric permittivity of 5.6 is obtained, and with STX801, a core-shell morphology TiO2-SiO2 filler from Evonik, where the highest breakdown strength of 173 V μm-1 is obtained.

  7. Understanding Depth Variation of Deep Seismicity from in situ Measurements of Mineral Strengths at High Pressures

    SciTech Connect

    Chen, J.

    2010-01-01

    Strengths of major minerals of Earth's mantle have been measured using in situ synchrotron X-ray diffraction at high pressures. Analysis of the diffraction peak widths is used to derive the yield strengths. Systematic analysis of the experimental result for olivine, wadsleyite, ringwoodite and perovskite indicates that minerals in the upper mantle, the transition zone and the lower mantle have very distinct strength character. Increasing temperature weakens the upper mantle mineral, olivine, significantly. At high temperature and high pressure, the transition zone minerals, wadsleyite and ringwoodite, have higher strengths than the upper mantle mineral. Among all the minerals studied, the lower mantle mineral, perovskite, has the highest strength. While both the upper mantle and the transition zone minerals show a notable strength drop, the strength of the lower mantle mineral shows just an increase of relaxation rate (no strength drop) when the temperature is increased stepwise by 200 K. The strength characteristics of these major mantle minerals at high pressures and temperatures indicate that yield strength may play a crucial role in defining the profile of deep earthquake occurrence with depth.

  8. The characterization of Vicker`s microhardness indentations and pile-up profiles as a strain-hardening microprobe

    SciTech Connect

    Santos, C. Jr.; Odette, G.R.; Lucas, G.E.; Schroeter, B.; Klinginsmith, D.; Yamamoto, T.

    1998-04-01

    Microhardness measurements have long been used to examine strength properties and changes in strength properties in metals, for example, as induced by irradiation. Microhardness affords a relatively simple test that can be applied to very small volumes of material. Microhardness is nominally related to the flow stress of the material at a fixed level of plastic strain. Further, the geometry of the pile-up of material around the indentation is related to the strain-hardening behavior of a material; steeper pile-ups correspond to smaller strain-hardening rates. In this study the relationship between pile-up profiles and strain hardening is examined using both experimental and analytical methods. Vickers microhardness tests have been performed on a variety of metal alloys including low alloy, high Cr and austenitic stainless steels. The pile-up topology around the indentations has been quantified using confocal microscopy techniques. In addition, the indentation and pile-up geometry has been simulated using finite element method techniques. These results have been used to develop an improved quantification of the relationship between the pile-up geometry and the strain-hardening constitutive behavior of the test material.

  9. Commercialization of NASA's High Strength Cast Aluminum Alloy for High Temperature Applications

    NASA Technical Reports Server (NTRS)

    Lee, Jonathan A.

    2003-01-01

    In this paper, the commercialization of a new high strength cast aluminum alloy, invented by NASA-Marshall Space Flight Center, for high temperature applications will be presented. Originally developed to meet U.S. automotive legislation requiring low- exhaust emission, the novel NASA aluminum alloy offers dramatic improvement in tensile and fatigue strengths at elevated temperatures (450 F-750 F), which can lead to reducing part weight and cost as well as improving performance for automotive engine applications. It is an ideal low cost material for cast components such as pistons, cylinder heads, cylinder liners, connecting rods, turbo chargers, impellers, actuators, brake calipers and rotors. NASA alloy also offers greater wear resistance, dimensional stability, and lower thermal expansion compared to conventional aluminum alloys, and the new alloy can be produced economically from sand, permanent mold and investment casting. Since 2001, this technology was licensed to several companies for automotive and marine internal combustion engines applications.

  10. Advanced nickel base alloys for high strength, corrosion applications

    DOEpatents

    Flinn, John E.

    1998-01-01

    Improved nickel-base alloys of enhanced strength and corrosion resistance, produced by atomization of an alloy melt under an inert gas atmosphere and of composition 0-20Fe, 10-30Cr, 2-12Mo, 6 max. Nb, 0.05-3 V, 0.08 max. Mn, 0.5 max. Si, less than 0.01 each of Al and Ti, less than 0.05 each of P and S, 0.01-0.08C, less than 0.2N, 0.1 max. 0, bal. Ni.

  11. Advanced nickel base alloys for high strength, corrosion applications

    DOEpatents

    Flinn, J.E.

    1998-11-03

    Improved nickel-base alloys of enhanced strength and corrosion resistance, produced by atomization of an alloy melt under an inert gas atmosphere and of composition 0--20Fe, 10--30Cr, 2--12Mo, 6 max. Nb, 0.05--3 V, 0.08 max. Mn, 0.5 max. Si, less than 0.01 each of Al and Ti, less than 0.05 each of P and S, 0.01--0.08C, less than 0.2N, 0.1 max. 0, bal. Ni. 3 figs.

  12. Epoxy adhesive formulations for engineered wood manufacturing: Design of Experiment (DOE) and hardener modification

    NASA Astrophysics Data System (ADS)

    Wangkheeree, W.; Meekum, U.

    2016-03-01

    The effect of IPDA, DDS, BPA and DICY, as main ingredient of TETA based hardener were examined. The 2k design of experiment(DOE) with k=3 were preliminary explored. The designed parameters A(IPDA), B(DDS) and C(BPA) were assigned as low(-) and high(+) levels, respectively. The Design Expert™ was hired as the analyzing tool at α=0.05. The mixed epoxy resin was based on the commercial one. The designed responds including tcure, t50, impact strengths, flexural properties and HDT were measured, respectively. Regarding to ANOVA conclusion, it was found that, there were no significant effects on the assigned parameters on the interested responds, except for the HDT where BPA(C) was negative effect was found. The lower in the crosslink density of cured epoxy, inferior in HDT, the higher in BPA addition was hypothesized. It was found that impact strength of cured epoxy derived from all formula were unacceptable low and tcure and t50, were too short. Thus, the further investigation by adding DICY into hardener was explored. The results showed that no significant change by mechanical means of cured epoxy by resolving 5-30 phr of DICY into the hardener. However, it was observed that the DICY added formula showed the obvious long cure times and behave as prepreg formula. The room temperature cured epoxy was incompletely crosslinked. The degrees of linear chain fragment were evidence, by weight, when higher DICY loading was engaged. Complete crosslink was achieved at 150°C post curing. The hardener comprised of TETA/aliphatic Epoxy(RD108) adduct was studied for enhancing the toughness of epoxy resin. It was observed that longer cure time at 150°C but lower toughness was experienced, on both prepreg and engineered wood made from the resins, at high TETA/RD108 ratio. Incomplete cure was explained for the mechanical inferior at high RD108 loading.

  13. The hardening phenomenon in irritant contact dermatitis: an interpretative update.

    PubMed

    Watkins, Shannon A; Maibach, Howard I

    2009-03-01

    Irritant contact dermatitis (ICD) is common and poses a significant problem in high-risk populations. In most cases, ICD resolves despite continued exposure in a process known as 'hardening', allowing individuals to continue with their work. Those who cannot clear ICD develop chronic ICD, which is a significant source of emotional, physical, and financial distress for affected individuals. While hardening is well known among labourers and clinicians, its mechanism remains to be elucidated. Much can be learned from the study of self-healing processes like the hardening phenomenon. This overview briefly documents the pathogenesis of ICD, focuses on the latest advances pertaining to the hardening phenomenon in ICD, and then highlights potential avenues of productive research. A better understanding of the 'hardening' process in the skin will hopefully lead to advances for the treatment of ICD.

  14. Development of high toughness, high strength aluminide-bonded carbide ceramics

    SciTech Connect

    Becher, P.F.; Plucknett, K.P.; Tiegs, T.N.

    1997-04-01

    Cemented carbides are widely used in applications where resistance to abrasion and wear are important, particularly in combination with high strength and stiffness. In the present case, ductile aluminides have been used as a binder phase to fabricate dense carbide cermets by either sintering of mixed powders or a melt-infiltration sintering process. The choice of an aluminide binder was based on the exceptional high temperature strength and chemical stability exhibited by these alloys. For example, TiC-based composites with a Ni{sub 3}Al binder phase exhibit improved oxidation resistance, Young`s moduli > 375 GPa, high fracture strengths (> 1 GPa) that are retained to {ge} 900{degrees}C, and fracture toughness values of 10 to 15 MPa{radical}m, identical to that measured in commercial cobalt-bonded WC with the same test method. The thermal diffusivity values at 200{degrees}C for these composites are {approximately} 0.070 to 0.075 cm{sup 2}/s while the thermal expansion coefficients rise with Ni3Al content from {approximately} 8 to {approximately}11 x 10{sup {minus}6}/{degrees}C over the range of 8 to 40 vol. % Ni{sub 3}Al. The oxidation and acidic corrosion resistances are quite promising as well. Finally, these materials also exhibit good electrical conductivity allowing them to be sectioned and shaped by electrical discharge machining (EDM) processes.

  15. Characterization of the effect of cryogenic treatment on the tempering behavior of a secondary hardening high Co-Ni steel

    NASA Astrophysics Data System (ADS)

    Gruber, M.; Ressel, G.; Ploberger, S.; Marsoner, S.; Ebner, R.

    2016-03-01

    For high Co-Ni steels sub-zero treatments are conducted to reduce the retained austenite phase fraction for obtaining excellent fracture toughness properties, but in general, cryogenic treatment has a great impact on the microstructural evolution of steels during tempering. Hence, the aim of this work was to analyze the influence of cryogenic treatments on the microstructural evolution of high Co-Ni steels, including carbide precipitation kinetics and austenite phase fraction evolution, during heating to elevated temperatures. In order to study the formation properties of carbides, the heating processes of cryogenically and non- cryogenically treated specimens were analyzed by dilatometer measurements. Furthermore, for determining the evolution of austenite phase fraction and hardness due to tempering, dilatometer investigations were combined with X-ray diffraction analyses and hardness measurements. It is revealed that sub-zero treated samples exhibit much stronger carbide precipitation signals. This was ascribed to the lower phase fraction of retained austenite, as more carbon is available for carbide precipitation.

  16. ETV Program Report: Big Fish Septage and High Strength Waste Water Treatment System

    EPA Science Inventory

    Verification testing of the Big Fish Environmental Septage and High Strength Wastewater Processing System for treatment of high-strength wastewater was conducted at the Big Fish facility in Charlevoix, Michigan. Testing was conducted over a 13-month period to address different c...

  17. Study to determine and analyze the strength of high modulus glass in epoxy-matrix composites

    NASA Technical Reports Server (NTRS)

    Bacon, J. F.

    1974-01-01

    Glass composition research was conducted to produce a high modulus, high strength beryllium-free glass fiber. This program was built on the previous research for developing high modulus, high strength glass fibers which had a 5 weight percent beryllia content. The fibers resulting from the composition program were then used to produce fiber reinforced-epoxy resin composites which were compared with composites reinforced by commercial high modulus glass fibers, Thornel S graphite fiber, and hybrids where the external quarters were reinforced with Thornel S graphite fiber and the interior half with glass fiber as well as the reverse hybrid. The composites were given tensile strength, compressive strength, short-beam shear strength, creep and fatigue tests. Comments are included on the significance of the test data.

  18. Extraordinary strain hardening by gradient structure

    PubMed Central

    Wu, XiaoLei; Jiang, Ping; Chen, Liu; Yuan, Fuping; Zhu, Yuntian T.

    2014-01-01

    Gradient structures have evolved over millions of years through natural selection and optimization in many biological systems such as bones and plant stems, where the structures change gradually from the surface to interior. The advantage of gradient structures is their maximization of physical and mechanical performance while minimizing material cost. Here we report that the gradient structure in engineering materials such as metals renders a unique extra strain hardening, which leads to high ductility. The grain-size gradient under uniaxial tension induces a macroscopic strain gradient and converts the applied uniaxial stress to multiaxial stresses due to the evolution of incompatible deformation along the gradient depth. Thereby the accumulation and interaction of dislocations are promoted, resulting in an extra strain hardening and an obvious strain hardening rate up-turn. Such extraordinary strain hardening, which is inherent to gradient structures and does not exist in homogeneous materials, provides a hitherto unknown strategy to develop strong and ductile materials by architecting heterogeneous nanostructures. PMID:24799688

  19. Laser-Assisted Sheet Metal Working of High Strength Steels in Serial Production

    NASA Astrophysics Data System (ADS)

    Brecher, Christian; Emonts, Michael; Eckert, Markus

    Within the sheet metal working industry the demand for thinner sheet materials with very high strength is growing due to the increasing need to save energy and a responsible use of natural resources. The high strength and the low ductility restricts using state of art technology to sheer, bend, emboss or deep draw parts with the needed complexity and quality. The Fraunhofer IPT developed a combination of laser-assisted preheating and conventional punching to a new hybrid technology which allows to shear, bend, emboss and draw high strength materials with a high quality and complexity in a serial production.

  20. Dynamic bake hardening of interstitial-free steels

    SciTech Connect

    Dehghani, K.; Jonas, J.J.

    2000-05-01

    Two types of dynamic strain aging (DSA) strengthening methods were investigated to determine their potentials for industrial use. They are referred to here as dynamic-static bake hardening (DSBH) and dynamic bake hardening (DBH). For this purpose, a 0.06 pct Ti interstitial-free (IF) steel was reheated to 900 C and cooled at 12 C/s to room temperature. It was then dynamically bake hardened in the temperature range 100 C to 250 C to strains of 2 to 8 pct at a strain rate of 10{sup {minus}3} s{sup {minus}1}. The tensile properties were determined before and after these treatments. It was found that the occurrence of DSA during dynamic baking led to significant increases in work-hardening rate as well as in the final strength. The results indicate that, for a given solute carbon level, the dynamically and then statically aged samples have higher strengths than those that are bake hardened in the conventional way.

  1. Precision continuous high-strength Azimuth track for large telescopes

    NASA Astrophysics Data System (ADS)

    Antebi, Joseph; Kan, Frank W.

    2003-01-01

    A novel track joint was developed for the azimuth track of the 50-m diameter Large Millimeter Telescope (LMT) now under construction in Mexico at an elevation of 4,600 m. The track, which is 430 mm wide by 230 mm deep, must be flat to within +/- 0.3 mm, and the material hardness at least 290 Brinell. This design uses a partial penetration narrow gap groove weld on the top surface of the track and a splice plate welded to the underside of the track. Pre-camber of the joint compensates for weld shrinkage which is small because of the use of the narrow gap groove weld. The residual deviations from flatness are reduced to the required tolerance by adjusting anchor bolts using an optimization procedure. The feasibility of the design with respect to fabrication, strength, fatigue, and alignment was demonstrated by detailed finite element analyses, trial welding and alignment of full scale joints, and testing of the mechanical properties of the joint and adjacent metal.

  2. Fabrication of carbon nanotube high-frequency nanoelectronic biosensor for sensing in high ionic strength solutions.

    PubMed

    Kulkarni, Girish S; Zhong, Zhaohui

    2013-01-01

    The unique electronic properties and high surface-to-volume ratios of single-walled carbon nanotubes (SWNT) and semiconductor nanowires (NW) make them good candidates for high sensitivity biosensors. When a charged molecule binds to such a sensor surface, it alters the carrier density in the sensor, resulting in changes in its DC conductance. However, in an ionic solution a charged surface also attracts counter-ions from the solution, forming an electrical double layer (EDL). This EDL effectively screens off the charge, and in physiologically relevant conditions ~100 millimolar (mM), the characteristic charge screening length (Debye length) is less than a nanometer (nm). Thus, in high ionic strength solutions, charge based (DC) detection is fundamentally impeded. We overcome charge screening effects by detecting molecular dipoles rather than charges at high frequency, by operating carbon nanotube field effect transistors as high frequency mixers. At high frequencies, the AC drive force can no longer overcome the solution drag and the ions in solution do not have sufficient time to form the EDL. Further, frequency mixing technique allows us to operate at frequencies high enough to overcome ionic screening, and yet detect the sensing signals at lower frequencies. Also, the high transconductance of SWNT transistors provides an internal gain for the sensing signal, which obviates the need for external signal amplifier. Here, we describe the protocol to (a) fabricate SWNT transistors, (b) functionalize biomolecules to the nanotube, (c) design and stamp a poly-dimethylsiloxane (PDMS) micro-fluidic chamber onto the device, and (d) carry out high frequency sensing in different ionic strength solutions. PMID:23912795

  3. Fabrication of carbon nanotube high-frequency nanoelectronic biosensor for sensing in high ionic strength solutions.

    PubMed

    Kulkarni, Girish S; Zhong, Zhaohui

    2013-01-01

    The unique electronic properties and high surface-to-volume ratios of single-walled carbon nanotubes (SWNT) and semiconductor nanowires (NW) make them good candidates for high sensitivity biosensors. When a charged molecule binds to such a sensor surface, it alters the carrier density in the sensor, resulting in changes in its DC conductance. However, in an ionic solution a charged surface also attracts counter-ions from the solution, forming an electrical double layer (EDL). This EDL effectively screens off the charge, and in physiologically relevant conditions ~100 millimolar (mM), the characteristic charge screening length (Debye length) is less than a nanometer (nm). Thus, in high ionic strength solutions, charge based (DC) detection is fundamentally impeded. We overcome charge screening effects by detecting molecular dipoles rather than charges at high frequency, by operating carbon nanotube field effect transistors as high frequency mixers. At high frequencies, the AC drive force can no longer overcome the solution drag and the ions in solution do not have sufficient time to form the EDL. Further, frequency mixing technique allows us to operate at frequencies high enough to overcome ionic screening, and yet detect the sensing signals at lower frequencies. Also, the high transconductance of SWNT transistors provides an internal gain for the sensing signal, which obviates the need for external signal amplifier. Here, we describe the protocol to (a) fabricate SWNT transistors, (b) functionalize biomolecules to the nanotube, (c) design and stamp a poly-dimethylsiloxane (PDMS) micro-fluidic chamber onto the device, and (d) carry out high frequency sensing in different ionic strength solutions.

  4. Fabrication of Carbon Nanotube High-Frequency Nanoelectronic Biosensor for Sensing in High Ionic Strength Solutions

    PubMed Central

    Kulkarni, Girish S.; Zhong, Zhaohui

    2013-01-01

    The unique electronic properties and high surface-to-volume ratios of single-walled carbon nanotubes (SWNT) and semiconductor nanowires (NW) 1-4 make them good candidates for high sensitivity biosensors. When a charged molecule binds to such a sensor surface, it alters the carrier density5 in the sensor, resulting in changes in its DC conductance. However, in an ionic solution a charged surface also attracts counter-ions from the solution, forming an electrical double layer (EDL). This EDL effectively screens off the charge, and in physiologically relevant conditions ~100 millimolar (mM), the characteristic charge screening length (Debye length) is less than a nanometer (nm). Thus, in high ionic strength solutions, charge based (DC) detection is fundamentally impeded6-8. We overcome charge screening effects by detecting molecular dipoles rather than charges at high frequency, by operating carbon nanotube field effect transistors as high frequency mixers9-11. At high frequencies, the AC drive force can no longer overcome the solution drag and the ions in solution do not have sufficient time to form the EDL. Further, frequency mixing technique allows us to operate at frequencies high enough to overcome ionic screening, and yet detect the sensing signals at lower frequencies11-12. Also, the high transconductance of SWNT transistors provides an internal gain for the sensing signal, which obviates the need for external signal amplifier. Here, we describe the protocol to (a) fabricate SWNT transistors, (b) functionalize biomolecules to the nanotube13, (c) design and stamp a poly-dimethylsiloxane (PDMS) micro-fluidic chamber14 onto the device, and (d) carry out high frequency sensing in different ionic strength solutions11. PMID:23912795

  5. Bond and fatigue characteristics of high-strength cement-based composites

    SciTech Connect

    Chimamphant, S.D.

    1989-01-01

    The results of a series of tests on a variety of high strength cementitious composites yield a model from which an empirical equation of general normalized pull-out stress vs. pull-out displacement relationship is developed. A new variable named the Brittleness Index and is defined and used in the proposed equation. Additionally, the concept of maximum strain is used to predict the fatigue life of high strength concrete. Three sizes of deformed bars and two types of steel fiber with four different volume fractions were used to observe bond-slip and pull-out characteristics of high strength concrete. The results indicate that the maximum slippage of deformed bars is only about 10% of that observed in normal concrete. Consequently, the required development length may have to be longer for high strength concrete members as compared to normal concrete. For the fatigue characteristics study, standard 3 x 6 in. cylinders were tested at the rates of 6 and 12 Hz. in a closed-loop load-controlled system. The results show that as the compressive strength of the composites increases from 4000 to 11000 psi., the fatigue strength increases by 17 percents. The rate of loading does not significantly affect the S-N relationship, fatigue strength and fatigue limit of the high strength cement-based composites. The S-N curves of high strength concrete shows a faster decay rate than those of normal concrete. The maximum strain at any cycle under cyclic loading is always less than the maximum strain at failure under monotonic loading. Also observed is that the maximum strain-cycle relationship is linear. These results indicate that the design code for flexure of normal concrete cannot be applied to high strength concrete.

  6. Changes in peak torque arm-shoulder strength of high school baseball pitchers during the season.

    PubMed

    Whitley, J D; Terrio, T

    1998-06-01

    Pre- and postseason measurements of peak torque arm strength were made at 180 deg./sec. and 300 deg./sec. on both throwing and nonthrowing arms of five male high school varsity baseball pitchers. The major findings were significant losses in adduction strength in both throwing and nonthrowing shoulders at 180 deg./ sec. and internal rotation strength for both sides at both speeds. The primary implication from these preliminary findings is that significant losses of arm-shoulder strength may be associated with injuries to the pitching arm.

  7. Surrogate Modeling of High-Fidelity Fracture Simulations for Real-Time Residual Strength Predictions

    NASA Technical Reports Server (NTRS)

    Spear, Ashley D.; Priest, Amanda R.; Veilleux, Michael G.; Ingraffea, Anthony R.; Hochhalter, Jacob D.

    2011-01-01

    A surrogate model methodology is described for predicting in real time the residual strength of flight structures with discrete-source damage. Starting with design of experiment, an artificial neural network is developed that takes as input discrete-source damage parameters and outputs a prediction of the structural residual strength. Target residual strength values used to train the artificial neural network are derived from 3D finite element-based fracture simulations. A residual strength test of a metallic, integrally-stiffened panel is simulated to show that crack growth and residual strength are determined more accurately in discrete-source damage cases by using an elastic-plastic fracture framework rather than a linear-elastic fracture mechanics-based method. Improving accuracy of the residual strength training data would, in turn, improve accuracy of the surrogate model. When combined, the surrogate model methodology and high-fidelity fracture simulation framework provide useful tools for adaptive flight technology.

  8. Characterization and hardening of concrete with ultrasonic testing.

    PubMed

    del Río, L M; Jiménez, A; López, F; Rosa, F J; Rufo, M M; Paniagua, J M

    2004-04-01

    In this study, we describe a technique which can be used to characterize some relevant properties of 26 cylindrical samples (15 x 30 cm2) of concrete. The characterization has been performed, according to Spanish regulations in force, by some destructive and ultrasound-based techniques using frequencies of 40 kHz. Samples were manufactured using different water/cement ratios (w/c), ranging from 0.48 to 0.80, in order to simulate different values of compressive strength at each sample. We have correlated the propagation velocity v of ultrasonic waves through the samples to compressive strength R values. As some other authors remark, there exists an exponential relationship between the two above parameters. We have found that a highly linear relationship is present between R and w/c concentration at the samples. Nevertheless, when the same linear model is adopted to describe the relationship between v and w/c, the value of r decreases significantly. Thus, we have performed a multiple regression analysis which takes into account the impact of different concrete constituents (water, cement, sand, etc.) on ultrasound propagation speed. One of the most relevant practical issues addressed in our study is the estimation of the hardening curve of concrete, which can be used to quantify the viability of applying the proposed method in a real scenario. Subsequently, we also show a detailed analysis of the temporal evolution of v and R through 61 days, beginning at the date where the samples were manufactured. After analyzing both parameters separately, a double reciprocal relationship is deduced. Using the above parameters, we develop an NDE-based model which can be used to estimate hardening time of concrete samples.

  9. Conducting High Cycle Fatigue Strength Step Tests on Gamma TiAl

    NASA Technical Reports Server (NTRS)

    Lerch, Brad; Draper, Sue; Pereira, J. Mike

    2002-01-01

    High cycle fatigue strength testing of gamma TiAl by the step test method is investigated. A design of experiments was implemented to determine if the coaxing effect occurred during testing. Since coaxing was not observed, step testing was deemed a suitable method to define the fatigue strength at 106 cycles.

  10. Production of small diameter high-temperature-strength refractory metal wires

    NASA Technical Reports Server (NTRS)

    Petrasek, D. W.; Signorelli, R. A.; King, G. W.

    1973-01-01

    Special thermomechanical techniques (schedules) have been developed to produce small diameter wire from three refractory metal alloys: colombian base alloy, tantalum base alloy, and tungsten base alloy. High strengths of these wires indicate their potential for contributing increased strength to metallic composites.

  11. Propagation Behavior of a Fatigue Crack of High Strength Al Alloy

    NASA Astrophysics Data System (ADS)

    Maeda, Hideki; Kariya, Kohji; Kawagoishi, Norio; Nu, Yan; Goto, Masahiro

    In order to investigate the effect of humidity change on growth behavior of a fatigue crack of an extruded and age-hardened Al alloy 7075-T6, rotating bending fatigue tests were carried out using plain specimens in relative humidity of 25% and 85%. In constant humidity, a crack propagated in a tensile mode macroscopically in low humidity and in a shear mode in high humidity. The crack growth rate was accelerated by high humidity. By changing humidity, the growth rate and the growth mode of a crack were changed to those corresponding to the changed humidity. That is, cumulative fatigue life in humidity change may be estimated by the fatigue life in constant humidity.

  12. Enhanced long-term strength and durability of shotcrete with high-strength C{sub 12}A{sub 7} mineral-based accelerator

    SciTech Connect

    Won, Jong-Pil Hwang, Un-Jong; Lee, Su-Jin

    2015-10-15

    This study evaluated the performance of shotcrete using high strength C{sub 12}A{sub 7} mineral-based accelerator that has been developed to improve the durability and long-term strength. Rebound, compressive strength and flexural strength were tested in the field. Test result showed that existing C{sub 12}A{sub 7} mineral-based accelerator exhibits better early strength than the high-strength C{sub 12}A{sub 7} mineral-based accelerator until the early age, but high-strength C{sub 12}A{sub 7} mineral-based accelerator shows about 29% higher at the long-term age of 28 days. Microstructural analysis such as scanning electron microscope (SEM), X-ray diffraction (XRD) and nitrogen adsorption method was evaluated to analyze long-term strength development mechanism of high strength C{sub 12}A{sub 7} mineral-based accelerator. As analysis result, it had more dense structure due to the reaction product by adding material that used to enhanced strength. It had better resistance performance in chloride ion penetration, freezing–thawing and carbonation than shotcrete that used existing C{sub 12}A{sub 7} mineral-based accelerator.

  13. Microstructures and Mechanical Properties of a New As-Hot-Rolled High-Strength DP Steel Subjected to Different Cooling Schedules

    NASA Astrophysics Data System (ADS)

    Hu, Jun; Du, Lin-Xiu; Wang, Jian-Jun; Gao, Cai-Ru; Yang, Tong-Zi; Wang, An-Yang; Misra, R. D. K.

    2013-11-01

    Controlled rolling followed by accelerated cooling was carried out in-house to study the microstructure and mechanical properties of a low carbon dual-phase steel. The objective of the study described here was to explore the effect of cooling schedule, such as air cooling temperature and coiling temperature, on the final microstructure and mechanical properties of dual-phase steels. Furthermore, the precipitation behavior and yield ratio are discussed. The study demonstrates that it is possible to obtain tensile strength and elongation of 780 MPa and 22 pct, respectively, at the two cooling schedules investigated. The microstructure consists of 90 pct ferrite and 10 pct martensite when subjected to moderate air cooling and low temperature coiling, such that the yield ratio is a low 0.69. The microstructure consists of 75 pct ferrite and 25 pct granular bainite with a high yield ratio of 0.84 when the steel is directly cooled to the coiling temperature. Compared to the conventional dual-phase steels, the high yield strength is attributed to precipitation hardening induced by nanoscale TiC particles and solid solution strengthening by high Si content. The interphase precipitates form at a suitable ledge mobility, and the row spacing changes with the rate of ferrite transformation. There are different orientations of the rows in the same grain because of the different growth directions of the ferrite grain boundaries, and the interface of the two colonies is devoid of precipitates because of the competitive mechanisms of the two orientations.

  14. Cup-Drawing Behavior of High-Strength Steel Sheets Containing Different Volume Fractions of Martensite

    NASA Astrophysics Data System (ADS)

    Choi, Shi-Hoon; Kim, Dae-Wan; Yang, Hoe-Seok; Han, Seong-Ho; Yoon, Jeong Whan

    2010-06-01

    Planar anisotropy and cup-drawing behavior were investigated for high-strength steel sheets containing different volume fractions of martensite. Macrotexture analysis using XRD was conducted to capture the effect of crystallographic orientation on the planar anisotropy of high-strength steel sheets. A phenomenological yield function, Yld96, which accounts for the anisotropy of yield stress and r-values, was implemented into ABAQUS using the user subroutine UMAT. Cup drawing of high-strength steel sheets was simulated using the FEM code. The profiles of earing and thickness strain were compared with the experimentally measured results.

  15. Unravel the key genes potentially related to high strength of cotton fiber by comparative phenotypic and genomic analyses

    Technology Transfer Automated Retrieval System (TEKTRAN)

    The demand of high strength of cotton fibers has been increased dramatically with the advent of modern high speed spinning technology for producing yarn. Bundle fiber strength is affected by fiber-to-fiber interactions in addition to the individual fiber strength. The bundle fiber strength is not al...

  16. Assessment of the Critical Parameters Influencing the Edge Stretchability of Advanced High-Strength Steel Sheet

    NASA Astrophysics Data System (ADS)

    Pathak, N.; Butcher, C.; Worswick, M.

    2016-09-01

    The edge formability of ferritic-martensitic DP (dual-phase) and ferritic-bainitic CP (complex-phase) steels was evaluated using a hole expansion test for different edge conditions. Hole expansion tests involving the standard conical punch as well as a custom flat punch were performed to investigate formability when the hole is expanded out-of-plane (conical punch) and in-plane using the flat punch. A range of edge conditions were considered, in order to isolate the influence of a range of factors thought to influence edge formability. The results demonstrate that work hardening and void damage at the sheared edge govern formability, while the sheared surface quality plays a minor or secondary role. A comparison of the edge stretching limits of DP and CP steels demonstrates the advantages of a ferritic-bainitic microstructure for forming operations with severe local deformation as in a stretch-flanging operation. A comparison of a traditional DP780 steel with a CP steel of similar strength showed that the edge stretching limit of the CP steel was three times larger than that of the DP780.

  17. Development of pulsed gas discharge lasers for shock hardening

    NASA Astrophysics Data System (ADS)

    Hintz, Gerd; Tkotz, R.; Keusch, C.; Negendanck, Matthias; Christiansen, Jens; Hoffmann, D. H. H.

    1996-08-01

    Shock hardening of metals (e.g. Ti, stainless steel) by pulsed lasers offers the possibility of large hardening depth (several millimeters) without serious damage to the surface of the workpiece. Previous investigations for shock hardening have mainly been performed with high power solid state lasers. The adaptation of commercial, high power gas discharge lasers to the shock hardening process could make this process relevant for industrial applications, as high repetition rates may be used. Two different laser systems have been investigated: a TEA carbon-dioxide laser and a XeCl laser. Both systems have pulse energies of some joule, a pulse length of several ten nanoseconds, and pulse repetition rates of up to 10 Hertz. The divergence of the beam was minimized to improve focusing properties. Systematic measurements of the laser induced pressure by means of piezo probes have been performed. An enhancement of the hardness of illuminated Ti(RT15) targets has been found and is reported.

  18. Statistical thermodynamics of strain hardening in polycrystalline solids

    DOE PAGES

    Langer, James S.

    2015-09-18

    This paper starts with a systematic rederivation of the statistical thermodynamic equations of motion for dislocation-mediated plasticity proposed in 2010 by Langer, Bouchbinder, and Lookman. The paper then uses that theory to explain the anomalous rate-hardening behavior reported in 1988 by Follansbee and Kocks and to explore the relation between hardening rate and grain size reported in 1995 by Meyers et al. A central theme is the need for physics-based, nonequilibrium analyses in developing predictive theories of the strength of polycrystalline materials.

  19. Statistical thermodynamics of strain hardening in polycrystalline solids.

    PubMed

    Langer, J S

    2015-09-01

    This paper starts with a systematic rederivation of the statistical thermodynamic equations of motion for dislocation-mediated plasticity proposed in 2010 by Langer, Bouchbinder, and Lookman [Acta Mat. 58, 3718 (2010)ACMAFD1359-645410.1016/j.actamat.2010.03.009]. It then uses that theory to explain the anomalous rate-hardening behavior reported in 1988 by Follansbee and Kocks and to explore the relation between hardening rate and grain size reported in 1995 by Meyers et al. A central theme is the need for physics-based, nonequilibrium analyses in developing predictive theories of the strength of polycrystalline materials.

  20. Statistical thermodynamics of strain hardening in polycrystalline solids

    SciTech Connect

    Langer, James S.

    2015-01-01

    This paper starts with a systematic rederivation of the statistical thermodynamic equations of motion for dislocation-mediated plasticity proposed in 2010 by Langer, Bouchbinder, and Lookman. The paper then uses that theory to explain the anomalous rate-hardening behavior reported in 1988 by Follansbee and Kocks and to explore the relation between hardening rate and grain size reported in 1995 by Meyers et al. A central theme is the need for physics-based, nonequilibrium analyses in developing predictive theories of the strength of polycrystalline materials.

  1. The strain-rate sensitivity of high-strength high-toughness steels.

    SciTech Connect

    Dilmore, M.F.; Crenshaw, Thomas B.; Boyce, Brad Lee

    2006-01-01

    The present study examines the strain-rate sensitivity of four high strength, high-toughness alloys at strain rates ranging from 0.0002 s-1 to 200 s-1: Aermet 100, a modified 4340, modified HP9-4-20, and a recently developed Eglin AFB steel alloy, ES-1c. A refined dynamic servohydraulic method was used to perform tensile tests over this entire range. Each of these alloys exhibit only modest strain-rate sensitivity. Specifically, the strain-rate sensitivity exponent m, is found to be in the range of 0.004-0.007 depending on the alloy. This corresponds to a {approx}10% increase in the yield strength over the 7-orders of magnitude change in strain-rate. Interestingly, while three of the alloys showed a concominant {approx}3-10% drop in their ductility with increasing strain-rate, the ES1-c alloy actually exhibited a 25% increase in ductility with increasing strain-rate. Fractography suggests the possibility that at higher strain-rates ES-1c evolves towards a more ductile dimple fracture mode associated with microvoid coalescence.

  2. Dynamic Strength of 304L stainless steel under impact

    NASA Astrophysics Data System (ADS)

    Werdiger, Meir; Bakshi, Lior; Glam, Benny; Pistinner, Shlomi

    2011-06-01

    We use the Asay self consistent technique to analyze the effects of pressure hardening and strain hardening on SS304L. Previously unloading experiment has been used to infer the strength of this material at high pressure, and recently the Johnson-Cook (JC) model has been calibrated at low strain rate. Release and reshock experiments with impact velocity range of 300-1700 m/s were preformed. We used VISAR to extract the particle velocity of the SS304L- LiF window interface. The velocity profile compared to hydrodynamic simulation using JC model. Our unloading experiments have clearly demonstrate that the material yield but does not fail. Thus infer substantial effect of pressure hardening.

  3. Mechanical properties evaluations of an age hardenable martensitic steel deformed by equal channel angular pressing.

    PubMed

    Nili-Ahmadabadi, M; Shirazi, H; Iranpour Mobarake, M; Poorganji, B; Hossein Nedjad, S; Furuhara, T

    2010-09-01

    Effect of severe plastic deformation by equal channel angular pressing on the mechanical properties of an age hardenable low carbon martensitic steel was investigated. Equal Channel angular pressing was carried out on the solution-annealed steel up to four passes at room temperature through the route Bc. Aging was carried out at 753 K for 2.4 ks. It was found that after four passes deformation, the microstructure is consist of fine grained high angle grain boundaries and lamellar dislocation cell block. The strength of steel is increased considerably while a increasing in elongation is revealed. PMID:21133170

  4. Nanospherical arabinogalactan proteins are a key component of the high-strength adhesive secreted by English ivy.

    PubMed

    Huang, Yujian; Wang, Yongzhong; Tan, Li; Sun, Leming; Petrosino, Jennifer; Cui, Mei-Zhen; Hao, Feng; Zhang, Mingjun

    2016-06-01

    Over 130 y have passed since Charles Darwin first discovered that the adventitious roots of English ivy (Hedera helix) exude a yellowish mucilage that promotes the capacity of this plant to climb vertical surfaces. Unfortunately, little progress has been made in elucidating the adhesion mechanisms underlying this high-strength adhesive. In the previous studies, spherical nanoparticles were observed in the viscous exudate. Here we show that these nanoparticles are predominantly composed of arabinogalactan proteins (AGPs), a superfamily of hydroxyproline-rich glycoproteins present in the extracellular spaces of plant cells. The spheroidal shape of the AGP-rich ivy nanoparticles results in a low viscosity of the ivy adhesive, and thus a favorable wetting behavior on the surface of substrates. Meanwhile, calcium-driven electrostatic interactions among carboxyl groups of the AGPs and the pectic acids give rise to the cross-linking of the exuded adhesive substances, favor subsequent curing (hardening) via formation of an adhesive film, and eventually promote the generation of mechanical interlocking between the adventitious roots of English ivy and the surface of substrates. Inspired by these molecular events, a reconstructed ivy-mimetic adhesive composite was developed by integrating purified AGP-rich ivy nanoparticles with pectic polysaccharides and calcium ions. Information gained from the subsequent tensile tests, in turn, substantiated the proposed adhesion mechanisms underlying the ivy-derived adhesive. Given that AGPs and pectic polysaccharides are also observed in bioadhesives exuded by other climbing plants, the adhesion mechanisms revealed by English ivy may forward the progress toward understanding the general principles underlying diverse botanic adhesives. PMID:27217558

  5. Nanospherical arabinogalactan proteins are a key component of the high-strength adhesive secreted by English ivy

    NASA Astrophysics Data System (ADS)

    Huang, Yujian; Wang, Yongzhong; Tan, Li; Sun, Leming; Petrosino, Jennifer; Cui, Mei-Zhen; Hao, Feng; Zhang, Mingjun

    2016-06-01

    Over 130 y have passed since Charles Darwin first discovered that the adventitious roots of English ivy (Hedera helix) exude a yellowish mucilage that promotes the capacity of this plant to climb vertical surfaces. Unfortunately, little progress has been made in elucidating the adhesion mechanisms underlying this high-strength adhesive. In the previous studies, spherical nanoparticles were observed in the viscous exudate. Here we show that these nanoparticles are predominantly composed of arabinogalactan proteins (AGPs), a superfamily of hydroxyproline-rich glycoproteins present in the extracellular spaces of plant cells. The spheroidal shape of the AGP-rich ivy nanoparticles results in a low viscosity of the ivy adhesive, and thus a favorable wetting behavior on the surface of substrates. Meanwhile, calcium-driven electrostatic interactions among carboxyl groups of the AGPs and the pectic acids give rise to the cross-linking of the exuded adhesive substances, favor subsequent curing (hardening) via formation of an adhesive film, and eventually promote the generation of mechanical interlocking between the adventitious roots of English ivy and the surface of substrates. Inspired by these molecular events, a reconstructed ivy-mimetic adhesive composite was developed by integrating purified AGP-rich ivy nanoparticles with pectic polysaccharides and calcium ions. Information gained from the subsequent tensile tests, in turn, substantiated the proposed adhesion mechanisms underlying the ivy-derived adhesive. Given that AGPs and pectic polysaccharides are also observed in bioadhesives exuded by other climbing plants, the adhesion mechanisms revealed by English ivy may forward the progress toward understanding the general principles underlying diverse botanic adhesives.

  6. Nanospherical arabinogalactan proteins are a key component of the high-strength adhesive secreted by English ivy.

    PubMed

    Huang, Yujian; Wang, Yongzhong; Tan, Li; Sun, Leming; Petrosino, Jennifer; Cui, Mei-Zhen; Hao, Feng; Zhang, Mingjun

    2016-06-01

    Over 130 y have passed since Charles Darwin first discovered that the adventitious roots of English ivy (Hedera helix) exude a yellowish mucilage that promotes the capacity of this plant to climb vertical surfaces. Unfortunately, little progress has been made in elucidating the adhesion mechanisms underlying this high-strength adhesive. In the previous studies, spherical nanoparticles were observed in the viscous exudate. Here we show that these nanoparticles are predominantly composed of arabinogalactan proteins (AGPs), a superfamily of hydroxyproline-rich glycoproteins present in the extracellular spaces of plant cells. The spheroidal shape of the AGP-rich ivy nanoparticles results in a low viscosity of the ivy adhesive, and thus a favorable wetting behavior on the surface of substrates. Meanwhile, calcium-driven electrostatic interactions among carboxyl groups of the AGPs and the pectic acids give rise to the cross-linking of the exuded adhesive substances, favor subsequent curing (hardening) via formation of an adhesive film, and eventually promote the generation of mechanical interlocking between the adventitious roots of English ivy and the surface of substrates. Inspired by these molecular events, a reconstructed ivy-mimetic adhesive composite was developed by integrating purified AGP-rich ivy nanoparticles with pectic polysaccharides and calcium ions. Information gained from the subsequent tensile tests, in turn, substantiated the proposed adhesion mechanisms underlying the ivy-derived adhesive. Given that AGPs and pectic polysaccharides are also observed in bioadhesives exuded by other climbing plants, the adhesion mechanisms revealed by English ivy may forward the progress toward understanding the general principles underlying diverse botanic adhesives.

  7. Application technologies for effective utilization of advanced high strength steel sheets

    NASA Astrophysics Data System (ADS)

    Suehiro, Masayoshi

    2013-12-01

    Recently, application of high strength steel sheets for automobiles has increased in order to meet a demand of light weighting of automobiles to reduce a carbon footprint while satisfying collision safety. The formability of steel sheets generally decreases with the increase in strength. Fracture and wrinkles tend to occur easily during forming. The springback phenomenon is also one of the issues which we should cope with, because it makes it difficult to obtain the desired shape after forming. Advanced high strength steel sheets with high formability have been developed in order to overcome these issues, and at the same time application technologies have been developed for their effective utilization. These sheets are normally used for cold forming. As a different type of forming, hot forming technique has been developed in order to produce parts with ultra high strength. In this report, technologies developed at NSSMC in this field will be introduced.

  8. Treatment of semivolatile compounds in high strength wastes using an anaerobic expanded-bed GAC reactor

    EPA Science Inventory

    The potential of the anaerobic, expanded bed granular activated carbon (GAC) reactor in treating a high strength waste containing RCRA semivolatile organic compounds (VOCs) was studied. Six semivolatiles, orthochlorophenol, nitrobenzene, naphthalene, para-nitrophenol, lindane, a...

  9. TREATMENT OF VOCS IN HIGH STRENGTH WASTES USING AN ANAEROBIC EXPANDED-BED GAS REACTOR

    EPA Science Inventory

    The potential of the expanded-bed granular activated carbon (GAC) anaerobic reactor in treating a high strength waste containing RCRA volatile organic compounds (VOCs) was studied. A total of six VOCs, methylene chloride, chlorobenzene, carbon tetrachloride, chloroform, toluene ...

  10. Application technologies for effective utilization of advanced high strength steel sheets

    SciTech Connect

    Suehiro, Masayoshi

    2013-12-16

    Recently, application of high strength steel sheets for automobiles has increased in order to meet a demand of light weighting of automobiles to reduce a carbon footprint while satisfying collision safety. The formability of steel sheets generally decreases with the increase in strength. Fracture and wrinkles tend to occur easily during forming. The springback phenomenon is also one of the issues which we should cope with, because it makes it difficult to obtain the desired shape after forming. Advanced high strength steel sheets with high formability have been developed in order to overcome these issues, and at the same time application technologies have been developed for their effective utilization. These sheets are normally used for cold forming. As a different type of forming, hot forming technique has been developed in order to produce parts with ultra high strength. In this report, technologies developed at NSSMC in this field will be introduced.

  11. Comparison of high and moderate intensity of strength training on mood and anxiety in older adults.

    PubMed

    Tsutsumi, T; Don, B M; Zaichkowsky, L D; Takenaka, K; Oka, K; Ohno, T

    1998-12-01

    This study was designed to examine the psychological benefits of anaerobic exercise for older adults. Specifically, strength training was employed to examine the effects on mood and anxiety in a group of healthy but sedentary older women. 36 women (mean age = 68.5 yr.) were randomly assigned to groups given high intensity or moderate intensity strength training or to a control group. Strength training was conducted three days a week for 12 weeks. After the training period, both high and moderate strength-training programs produced marked improvements in muscle strength and body composition compared to the control subjects. The average improvements in the high and moderate intensity strength-training groups for muscle strength were 40.5 and 35.5%, respectively, and for percent body fat 1.52 and 2.50%, respectively. As for psychological changes, both training groups significantly improved positive mood (vigor), and the moderate intensity group significantly reduced trait anxiety compared to means of the control group. Also, both training groups showed some decrease in tension and state anxiety after the training period. These findings provide evidence for the effectiveness of anaerobic training to enhance perception of psychological well-being in older women. A moderate intensity rather than high intensity of training regimen may be more beneficial for sedentary older women to improve psychological health.

  12. Development of a Low Loss, High Dielectric Strength Microwave Substrate

    SciTech Connect

    Sanders, D; Sampayan, S; Caporaso, G; Rhodes, M; Watson, J; Slenes, K; Jacquina, J; De La Fuenta, R; Thurmond, L

    2006-06-05

    This work describes a comparison of two candidate materials for pulse forming line fabrication with respect to bulk dielectric breakdown, frequency response of relative permittivity and dielectric loss. One material is a commercially available microwave substrate material that can be procured in sheet form without a high voltage specification while the other is a newly developed material that also comes in sheet form that can also be cast between the electrodes.

  13. Nanostructured Cu-Cr alloy with high strength and electrical conductivity

    SciTech Connect

    Islamgaliev, R. K. Nesterov, K. M.; Bourgon, J.; Champion, Y.; Valiev, R. Z.

    2014-05-21

    The influence of nanostructuring by high pressure torsion (HPT) on strength and electrical conductivity in the Cu-Cr alloy has been investigated. Microstructure of HPT samples was studied by transmission electron microscopy with special attention on precipitation of small chromium particles after various treatments. Effect of dynamic precipitation leading to enhancement of strength and electrical conductivity was observed. It is shown that nanostructuring leads to combination of high ultimate tensile strength of 790–840 MPa, enhanced electrical conductivity of 81%–85% IACS and thermal stability up to 500 °C. The contributions of grain refinement and precipitation to enhanced properties of nanostructured alloy are discussed.

  14. High Strength and Wear Resistant Aluminum Alloy for High Temperature Applications

    NASA Technical Reports Server (NTRS)

    Lee, Jonathan A.; Chen, Po Shou

    2003-01-01

    Originally developed by NASA as high performance piston alloys to meet U.S. automotive legislation requiring low exhaust emission, the novel NASA alloys now offer dramatic increase in tensile strength for many other applications at elevated temperatures from 450 F (232 C) to about 750 F (400 C). It is an ideal low cost material for cast automotive components such as pistons, cylinder heads, cylinder liners, connecting rods, turbo chargers, impellers, actuators, brake calipers and rotors. It can be very economically produced from conventional permanent mold, sand casting or investment casting, with silicon content ranging from 6% to 18%. At high silicon levels, the alloy exhibits excellent thermal growth stability, surface hardness and wear resistant properties.

  15. Analysis of particle size and interface effects on the strength and ductility of advanced high strength steels

    NASA Astrophysics Data System (ADS)

    Ettehad, Mahmood

    This thesis is devoted to the numerical investigation of mechanical behavior of Dual phase (DP) steels. Such grade of advanced high strength steels (AHSS) is favorable to the automotive industry due the unique properties such as high strength and ductility with low finished cost. Many experimental and numerical studies have been done to achieve the optimized behavior of DP steels by controlling their microstructure. Experiments are costly and time consuming so in recent years numerical tools are utilized to help the metallurgist before doing experiments. Most of the numerical studies are based on classical (local) constitutive models where no material length scale parameters are incorporated in the model. Although these models are proved to be very effective in modeling the material behavior in the large scales but they fail to address some critical phenomena which are important for our goals. First, they fail to address the size effect phenomena which materials show at microstructural scale. This means that materials show stronger behavior at small scales compared to large scales. Another issue with classical models is the mesh size dependency in modeling the softening behavior of materials. This means that in the finite element context (FEM) the results will be mesh size dependent and no converged solution exist upon mesh refinement. Thereby by applying the classical (local) models one my loose the accuracy on measuring the strength and ductility of DP steels. Among the non-classical (nonlocal) models, gradient-enhanced plasticity models which consider the effect of neighboring point on the behavior of one specific point are proved to be numerically effective and versatile tools to accomplish the two concerns mentioned above. So in this thesis a gradient-enhanced plasticity model which incorporates both the energetic and dissipative material length scales is derived based on the laws of thermodynamics. This model also has a consistent yield-like function for the

  16. Surrogate Modeling of High-Fidelity Fracture Simulations for Real-Time Residual Strength Predictions

    NASA Technical Reports Server (NTRS)

    Spear, Ashley D.; Priest, Amanda R.; Veilleux, Michael G.; Ingraffea, Anthony R.; Hochhalter, Jacob D.

    2011-01-01

    A surrogate model methodology is described for predicting, during flight, the residual strength of aircraft structures that sustain discrete-source damage. Starting with design of experiment, an artificial neural network is developed that takes as input discrete-source damage parameters and outputs a prediction of the structural residual strength. Target residual strength values used to train the artificial neural network are derived from 3D finite element-based fracture simulations. Two ductile fracture simulations are presented to show that crack growth and residual strength are determined more accurately in discrete-source damage cases by using an elastic-plastic fracture framework rather than a linear-elastic fracture mechanics-based method. Improving accuracy of the residual strength training data does, in turn, improve accuracy of the surrogate model. When combined, the surrogate model methodology and high fidelity fracture simulation framework provide useful tools for adaptive flight technology.

  17. Influence of grain structure and solute composition on the work hardening behavior of aluminium at cryogenic temperatures

    SciTech Connect

    Chu, D.; Morris, J.W. Jr.

    1993-07-01

    An unrecrystallized structure is found to significantly improve the work hardening characteristics by lowering the work hardening rate during early stages of deformation. This is in contrast to a recrystallized structure, which requires a higher work hardening rate to accommodate the greater degree of multiple slip necessary to maintain strain compatibility between the more randomly oriented grains. The stronger texture associated with the unrecrystallized structure allows deformation to occur more efficiently. Addition of magnesium also improves work hardening by increasing overall level of the work hardening rate. The improved characteristics of the work hardening behavior result in a parallel increase in both the strength and ductility at cryogenic temperatures. These findings are positive since they suggest a method by which improvements in the work hardening behavior and subsequent mechanical properties may be obtained through practical modifications of the microstructure and composition.

  18. Exceptional high fatigue strength in Cu-15at.%Al alloy with moderate grain size

    PubMed Central

    Liu, Rui; Tian, Yanzhong; Zhang, Zhenjun; An, Xianghai; Zhang, Peng; Zhang, Zhefeng

    2016-01-01

    It is commonly proposed that the fatigue strength can be enhanced by increasing the tensile strength, but this conclusion needs to be reconsidered according to our study. Here a recrystallized α-Cu-15at.%Al alloy with moderate grain size of 0.62 μm was fabricated by cold rolling and annealing, and this alloy achieved exceptional high fatigue strength of 280 MPa at 107 cycles. This value is much higher than the fatigue strength of 200 MPa for the nano-crystalline counterpart (0.04 μm in grain size) despite its higher tensile strength. The remarkable improvement of fatigue strength should be mainly attributed to the microstructure optimization, which helps achieve the reduction of initial damage and the dispersion of accumulated damage. A new strategy of “damage reduction” was then proposed for fatigue strength improvement, to supplement the former strengthening principle. The methods and strategies summarized in this work offer a general pathway for further improvement of fatigue strength, in order to ensure the long-term safety of structural materials. PMID:27264347

  19. Exceptional high fatigue strength in Cu-15at.%Al alloy with moderate grain size

    NASA Astrophysics Data System (ADS)

    Liu, Rui; Tian, Yanzhong; Zhang, Zhenjun; An, Xianghai; Zhang, Peng; Zhang, Zhefeng

    2016-06-01

    It is commonly proposed that the fatigue strength can be enhanced by increasing the tensile strength, but this conclusion needs to be reconsidered according to our study. Here a recrystallized α-Cu-15at.%Al alloy with moderate grain size of 0.62 μm was fabricated by cold rolling and annealing, and this alloy achieved exceptional high fatigue strength of 280 MPa at 107 cycles. This value is much higher than the fatigue strength of 200 MPa for the nano-crystalline counterpart (0.04 μm in grain size) despite its higher tensile strength. The remarkable improvement of fatigue strength should be mainly attributed to the microstructure optimization, which helps achieve the reduction of initial damage and the dispersion of accumulated damage. A new strategy of “damage reduction” was then proposed for fatigue strength improvement, to supplement the former strengthening principle. The methods and strategies summarized in this work offer a general pathway for further improvement of fatigue strength, in order to ensure the long-term safety of structural materials.

  20. Exceptional high fatigue strength in Cu-15at.%Al alloy with moderate grain size.

    PubMed

    Liu, Rui; Tian, Yanzhong; Zhang, Zhenjun; An, Xianghai; Zhang, Peng; Zhang, Zhefeng

    2016-01-01

    It is commonly proposed that the fatigue strength can be enhanced by increasing the tensile strength, but this conclusion needs to be reconsidered according to our study. Here a recrystallized α-Cu-15at.%Al alloy with moderate grain size of 0.62 μm was fabricated by cold rolling and annealing, and this alloy achieved exceptional high fatigue strength of 280 MPa at 10(7) cycles. This value is much higher than the fatigue strength of 200 MPa for the nano-crystalline counterpart (0.04 μm in grain size) despite its higher tensile strength. The remarkable improvement of fatigue strength should be mainly attributed to the microstructure optimization, which helps achieve the reduction of initial damage and the dispersion of accumulated damage. A new strategy of "damage reduction" was then proposed for fatigue strength improvement, to supplement the former strengthening principle. The methods and strategies summarized in this work offer a general pathway for further improvement of fatigue strength, in order to ensure the long-term safety of structural materials. PMID:27264347

  1. Grain-refining heat treatments to improve cryogenic toughness of high-strength steels

    NASA Technical Reports Server (NTRS)

    Rush, H. F.

    1984-01-01

    The development of two high Reynolds number wind tunnels at NASA Langley Research Center which operate at cryogenic temperatures with high dynamic pressures has imposed severe requirements on materials for model construction. Existing commercial high strength steels lack sufficient toughness to permit their safe use at temperatures approaching that of liquid nitrogen (-320 F). Therefore, a program to improve the cryogenic toughness of commercial high strength steels was conducted. Significant improvement in the cryogenic toughness of commercial high strength martensitic and maraging steels was demonstrated through the use of grain refining heat treatments. Charpy impact strength at -320 F was increased by 50 to 180 percent for the various alloys without significant loss in tensile strength. The grain sizes of the 9 percent Ni-Co alloys and 200 grade maraging steels were reduced to 1/10 of the original size or smaller, with the added benefit of improved machinability. This grain refining technique should permit these alloys with ultimate strengths of 220 to 270 ksi to receive consideration for cryogenic service.

  2. Development of high-strength and high-conductivity conductor materials for pulsed high-field magnets at Dresden

    NASA Astrophysics Data System (ADS)

    Grünberger, W.; Heilmaier, M.; Schultz, L.

    2001-01-01

    The work at the IFW Dresden is focused on the development of microcomposite Cu-Ag alloys and steel-copper macrocomposites with high-nitrogen steel and pearlitic steel jackets, respectively. In Cu-Ag alloys the investigation of continuously cast rods with different starting diameters suggests that the cooling rate during solidification determining the dendrite arm spacing has a minor influence on the development of the strength compared to the cooling velocity after solidification which determines the extent of the Ag-supersaturation in the Cu solid solution. Maximum strength at minimum drawing strain demands (i) a sufficient volume fraction of eutectic in order to suppress discontinuous precipitation (absence of grain boundaries) and (ii) a sufficiently rapid cooling after solidification in order to prevent pre-precipitation. With a continuously cast starting rod of 12 mm diameter a maximum tensile strength of 1.3 GPa was obtained after a drawing strain of only η=4.3. Steel-copper macrocomposites were fabricated by the ‘rod-in-tube’ technology. The experiments with austenitic high-nitrogen steels were performed with two alloys. With the commercial alloy Nicrofer 3033 a strength level of 1.2 GPa has been achieved with a 52 vol% Cu composite at a drawing strain of η=2.3. A composite with pearlitic C60-steel (0.6 wt% C) and 56 vol% Cu showed a tensile strength of 1.53 GPa after a final patenting at a diameter of 14.7 mm and a drawing strain of η=4.

  3. Development of high-strength, high-corrosion resistant austenitic stainless steel for sour gas service

    SciTech Connect

    Nakayama, T.; Fujiwara, K.; Torii, Y.; Inoue, T.

    1988-01-01

    An austenitic stainless steel for sour gas service has been developed. The new steel has been shown to offer high strength, i.e., 0.2% PS exceeding 42kgf/mm/sup 2/ (414MPa) under solution-annealed conditions, along with excellent resistance to sulphide stress corrosion cracking, pitting corrosion, and crevice corrosion, in comparison with conventional martensitic stainless steel such as CA-6NM, duplex stainless steel such as ASTM A790 UNS S31803, and austenitic stainless steels such as Type 316. Its higher resistance to corrosion cracking, etc., then Type 316 was thought to be attributable to the higher contents of Cr, Mo, and N, which help to form more stable passive film in a shorter time.

  4. Garnet Yield Strength at High Pressures and Implications for Upper Mantle and Transition Zone Rheology

    SciTech Connect

    Kavner,A.

    2008-01-01

    Garnet helps control the mechanical behavior of the Earth's crust, mantle, and transition zone. Here, measurements are presented suggesting that garnet, long considered to be a high-viscosity phase, is actually weaker than the other dominant components in the transition zone. The mechanical behavior of garnet at high pressures was examined using radial diffraction techniques in the diamond anvil cell. The yield strength of grossular garnet was inferred from synchrotron X-ray measurements of differential lattice strains. The differential stress was found to increase from 1.3 ({+-}0.6) GPa at a hydrostatic pressure 5.8 ({+-}1.1) GPa to 4.1 ({+-}0.4) GPa at 15.7 ({+-}1.0) GPa, where it was level to 19 GPa. The strength results are consistent with inferred strength values for majorite garnet from measurements in the diamond cell normal geometry, bolstering the idea that garnet-structured materials may all have similar strengths. In this low-temperature, high differential stress regime, garnet is shown to be significantly weaker than anhydrous ringwoodite and to have a strength similar to hydrous ringwoodite. This result suggests that the presence of water in the transition zone may not be required to explain a weak rheology, and therefore models of transition zone behavior built assuming that garnet is the high-strength phase may need to be revised.

  5. Study of X80 grade high strength line pipe for sour service

    SciTech Connect

    Kushida, T.; Okaguchi, S.; Hamada, M.; Yamamoto, A.; Ohnishi, K.; Fujino, J.

    1997-08-01

    X80 grade high strength large diameter line pipe (UOE Pipe) for sour service have been studied. Increasing Mn content to provide strength of X80 increases HIC susceptibility due to center segregation of Mn in continuously cast slabs. The Mn content should be controlled less than 1.4% to maintain HIC resistance in the NACE TM0177 solution. The required strength can be obtained by addition of 0.5% Cr and accelerated controlled cooling after rolling. It has been clarified that Cr is very useful in providing high strength X70 without accelerating the center segregation of Mn. SSC resistance can be improved by controlling maximum hardness of weld metal lower than 230 Hv. Sour service X80 UOE pipes of two sizes were manufactured on large scales based on these experimental results. These pipes showed good low temperature toughness and HIC resistance in the NACE TM0177 solution.

  6. Process study of polycyanate resin for wet-filament wound high-strength composites

    SciTech Connect

    Frame, B.J.

    1997-12-31

    Polycyanate (or cyanate ester) resins offer advantages as composite matrices because of their high thermal stability, low outgassing, low water absorption and radiation resistance. This report describes the results of a processing study to develop high-strength hoop-wound composite by the wet-filament winding method using Toray T1000G carbon fiber and YLA RS-14 polycyanate resin as the constituent materials. T1000G/RS-14 composite cylinders were wet-wound and cured using different process schedules and then evaluated for hoop tensile strength and modulus, transverse flexural strength and short beam shear strength. The results of material characterization tests performed on the T1000G carbon fiber and RS-14 resin constituents used in this study are also presented.

  7. The resistance of selected high strength alloys to embrittlement by a hydrogen environment

    NASA Technical Reports Server (NTRS)

    Benson, R. B., Jr.

    1974-01-01

    Selected high strength iron base and cobalt base alloys with yield strengths in the range from 1233 to 2129 MN per sq m (179 to 309 KSI) were resistant to degradation of mechanical properties in a one atmosphere hydrogen environment at ambient temperature. These alloys were strengthened initially by cold working which produced strain induced epsilon prime-hcp martensite and fcc mechanical twins in an fcc matrix. Heat treatment of the cobalt base alloy after cold working produced carbide precipitates with retention of an hcp epsilon phase which increased the yield strength level to a maximum of 2129 MN per sq m (309 KSI). High-strength alloys can be produced which have some resistance to degradation of mechanical properties by a hydrogen environment under certain conditions.

  8. Dose dependence of strength after low-temperature irradiation in metallic materials

    SciTech Connect

    Byun, Thak Sang; Li, Meimei; Farrell, Kenneth

    2013-01-01

    This study intends to review and characterize the low-temperature (< 200 oC) irradiation hardening behaviors in metallic materials and to propose new interpretations on the dose dependence of strength, particularly in the pre-hardening and saturation regimes. The analysis results of yield stress-dose curves indicate that four dose-dependence regimes exist: the pre-hardening, main hardening, saturation, and embrittlement regimes. The semi-log plots of yield stress versus dose data revealed that the pre-hardening regime displaying zero-hardening or softening was common at least for the alloys with low dose data available. It was observed that the dose range of the pre-hardening regime increased with the strength of material, which indicates that slower initiation in irradiation hardening is expected when strength is higher. For the majority of the metallic materials analyzed, it was reconfirmed that the exponent of the power-law hardening function was evaluated to be about 0.5 in the main hardening regime and about 0.1 in the saturation regime. In these positive hardening regimes the low strength pure metals such as Fe, Ta, Cu, and Zr displayed lower hardening exponents. The minimum dose to the saturation of irradiation hardening was in the range of 0.003 0.08 dpa, depending on the category of materials. It was also reaffirmed that there exists a strong relationship between the saturation in irradiation hardening and the occurrence of plastic instability at yield.

  9. Pulsed laser surface hardening of ferrous alloys.

    SciTech Connect

    Xu, Z.; Reed, C. B.; Leong, K. H.; Hunter, B. V.

    1999-09-30

    A high power pulsed Nd:YAG laser and special optics were used to produce surface hardening on 1045 steel and gray cast iron by varying the process parameters. Unlike CO{sub 2} lasers, where absorptive coatings are required, the higher absorptivity of ferrous alloys at the Nd:YAG laser wavelength eliminates the necessity of applying a coating before processing. Metallurgical analysis of the treated tracks showed that very fine and hard martensitic microstructure (1045 steel) or inhomogeneous martensite (gray cast iron) were obtained without surface melting, giving maximum hardness of HRC 61 and HRC 40 for 1045 steel and gray cast iron respectively. The corresponding maximum case depths for both alloys at the above hardness are 0.6 mm. Gray cast iron was more difficult to harden without surface melting because of its lower melting temperature and a significantly longer time-at-temperature required to diffuse carbon atoms from the graphite flakes into the austenite matrix during laser heating. The thermal distortion was characterized in term of flatness changes after surface hardening.

  10. New Powder Metallurgical Approach to Achieve High Fatigue Strength in Ti-6Al-4V Alloy

    NASA Astrophysics Data System (ADS)

    Cao, Fei; Ravi Chandran, K. S.; Kumar, Pankaj; Sun, Pei; Zak Fang, Z.; Koopman, Mark

    2016-05-01

    Recently, manufacturing of titanium by sintering and dehydrogenation of hydride powders has generated a great deal of interest. An overarching concern regarding powder metallurgy (PM) titanium is that critical mechanical properties, especially the high-cycle fatigue strength, are lower than those of wrought titanium alloys. It is demonstrated here that PM Ti-6Al-4V alloy with mechanical properties comparable (in fatigue strength) and exceeding (in tensile properties) those of wrought Ti-6Al-4V can be produced from titanium hydride powder, through the hydrogen sintering and phase transformation process. Tensile and fatigue behavior, as well as fatigue fracture mechanisms, have been investigated under three processing conditions. It is shown that a reduction in the size of extreme-sized pores by changing the hydride particle size distribution can lead to improved fatigue strength. Further densification by pneumatic isostatic forging leads to a fatigue strength of ~550 MPa, comparable to the best of PM Ti-6Al-4V alloys prepared by other methods and approaching the fatigue strengths of wrought Ti-6Al-4V alloys. The microstructural factors that limit fatigue strength in PM titanium have been investigated, and pathways to achieve greater fatigue strengths in PM Ti-6Al-4V alloys have been identified.

  11. Evaluation of the stress corrosion cracking resistance of several high strength low alloy steels

    NASA Technical Reports Server (NTRS)

    Humphries, T. S.; Nelson, E. E.

    1980-01-01

    The stress corrosion cracking resistance was studied for high strength alloy steels 4130, 4340, for H-11 at selected strength levels, and for D6AC and HY140 at a single strength. Round tensile and C-ring type specimens were stressed up to 100 percent of their yield strengths and exposed to alternate immersion in salt water, salt spray, the atmosphere at Marshall Space Flight Center, and the seacoast at Kennedy Space Center. Under the test conditions, 4130 and 4340 steels heat treated to a tensile strength of 1240 MPa (180 ksi), H-11 and D6AC heat treated to a tensile strength of 1450 MPa (210 ksi), and HY140 (1020 MPa, 148 ksi) are resistant to stress corrosion cracking because failures were not encountered at stress levels up to 75 percent of their yield strengths. A maximum exposure period of one month for alternate immersion in salt water or salt spray and three months for seacoast is indicated for alloy steel to avoid false indications of stress corrosion cracking because of failure resulting from severe pitting.

  12. Elastic Properties in Tension and Shear of High Strength Nonferrous Metals and Stainless Steel - Effect of Previous Deformation and Heat Treatment

    NASA Technical Reports Server (NTRS)

    Mebs, R W; Mcadam, D J

    1947-01-01

    A resume is given of an investigation of the influence of plastic deformation and of annealing temperature on the tensile and shear elastic properties of high strength nonferrous metals and stainless steels in the form of rods and tubes. The data were obtained from earlier technical reports and notes, and from unpublished work in this investigation. There are also included data obtained from published and unpublished work performed on an independent investigation. The rod materials, namely, nickel, monel, inconel, copper, 13:2 Cr-Ni steel, and 18:8 Cr-Ni steel, were tested in tension; 18:8 Cr-Ni steel tubes were tested in shear, and nickel, monel, aluminum-monel, and Inconel tubes were tested in both tension and shear. There are first described experiments on the relationship between hysteresis and creep, as obtained with repeated cyclic stressing of annealed stainless steel specimens over a constant load range. These tests, which preceded the measurements of elastic properties, assisted in devising the loading time schedule used in such measurements. From corrected stress-set curves are derived the five proof stresses used as indices of elastic or yield strength. From corrected stress-strain curves are derived the secant modulus and its variation with stress. The relationship between the forms of the stress-set and stress-strain curves and the values of the properties derived is discussed. Curves of variation of proof stress and modulus with prior extension, as obtained with single rod specimens, consist in wavelike basic curves with superposed oscillations due to differences of rest interval and extension spacing; the effects of these differences are studied. Oscillations of proof stress and modulus are generally opposite in manner. The use of a series of tubular specimens corresponding to different amounts of prior extension of cold reduction gave curves almost devoid of oscillation since the effects of variation of rest interval and extension spacing were

  13. Hardened Client Platforms for Secure Internet Banking

    NASA Astrophysics Data System (ADS)

    Ronchi, C.; Zakhidov, S.

    We review the security of e-banking platforms with particular attention to the exploitable attack vectors of three main attack categories: Man-in-the-Middle, Man-in-the-PC and Man-in-the-Browser. It will be shown that the most serious threats come from combination attacks capable of hacking any transaction without the need to control the authentication process. Using this approach, the security of any authentication system can be bypassed, including those using SecureID Tokens, OTP Tokens, Biometric Sensors and Smart Cards. We will describe and compare two recently proposed e-banking platforms, the ZTIC and the USPD, both of which are based on the use of dedicated client devices, but with diverging approaches with respect to the need of hardening the Web client application. It will be shown that the use of a Hardened Browser (or H-Browser) component is critical to force attackers to employ complex and expensive techniques and to reduce the strength and variety of social engineering attacks down to physiological fraud levels.

  14. Strain rate hardening: a hidden but critical mechanism for biological composites?

    PubMed

    Chintapalli, Ravi Kiran; Breton, Stephanie; Dastjerdi, Ahmad Khayer; Barthelat, Francois

    2014-12-01

    Natural materials such as nacre, bone, collagen and spider silk boast unusual combinations of stiffness, strength and toughness. Behind this performance is a staggered microstructure, which consists of stiff and elongated inclusions embedded in a softer and more deformable matrix. The micromechanics of deformation and failure associated with this microstructure are now well understood at the "unit cell" level, the smallest representative volume for this type of material. However, these mechanisms only translate to high performance if they propagate throughout large volumes, an important condition which is often overlooked. Here we present, for the first time, a model which captures the conditions for either spreading of deformations or localization, which determines whether a staggered composite is brittle or deformable at the macroscale. The macroscopic failure strain for the material was calculated as function of the viscoplastic properties of the interfaces and the severity of the defect. As expected, larger strains at failure can be achieved when smaller defects are present within the material, or with more strain hardening at the interface. The model also shows that strain rate hardening is a powerful source of large deformations for the material as well, a result we confirmed and validated with tensile experiments on glass-polydimethylsiloxane (PDMS) nacre-like staggered composites. An important implication is that natural materials, largely made of rate-dependent materials, could rely on strain rate hardening to tolerate initial defects and damage to maintain their functionality. Strain rate hardening could also be harnessed and optimized in bio-inspired composites in order to maximize their overall performance. PMID:25174668

  15. Strain rate hardening: a hidden but critical mechanism for biological composites?

    PubMed

    Chintapalli, Ravi Kiran; Breton, Stephanie; Dastjerdi, Ahmad Khayer; Barthelat, Francois

    2014-12-01

    Natural materials such as nacre, bone, collagen and spider silk boast unusual combinations of stiffness, strength and toughness. Behind this performance is a staggered microstructure, which consists of stiff and elongated inclusions embedded in a softer and more deformable matrix. The micromechanics of deformation and failure associated with this microstructure are now well understood at the "unit cell" level, the smallest representative volume for this type of material. However, these mechanisms only translate to high performance if they propagate throughout large volumes, an important condition which is often overlooked. Here we present, for the first time, a model which captures the conditions for either spreading of deformations or localization, which determines whether a staggered composite is brittle or deformable at the macroscale. The macroscopic failure strain for the material was calculated as function of the viscoplastic properties of the interfaces and the severity of the defect. As expected, larger strains at failure can be achieved when smaller defects are present within the material, or with more strain hardening at the interface. The model also shows that strain rate hardening is a powerful source of large deformations for the material as well, a result we confirmed and validated with tensile experiments on glass-polydimethylsiloxane (PDMS) nacre-like staggered composites. An important implication is that natural materials, largely made of rate-dependent materials, could rely on strain rate hardening to tolerate initial defects and damage to maintain their functionality. Strain rate hardening could also be harnessed and optimized in bio-inspired composites in order to maximize their overall performance.

  16. A low-cost hierarchical nanostructured beta-titanium alloy with high strength

    NASA Astrophysics Data System (ADS)

    Devaraj, Arun; Joshi, Vineet V.; Srivastava, Ankit; Manandhar, Sandeep; Moxson, Vladimir; Duz, Volodymyr A.; Lavender, Curt

    2016-04-01

    Lightweighting of automobiles by use of novel low-cost, high strength-to-weight ratio structural materials can reduce the consumption of fossil fuels and in turn CO2 emission. Working towards this goal we achieved high strength in a low cost β-titanium alloy, Ti-1Al-8V-5Fe (Ti185), by hierarchical nanostructure consisting of homogenous distribution of micron-scale and nanoscale α-phase precipitates within the β-phase matrix. The sequence of phase transformation leading to this hierarchical nanostructure is explored using electron microscopy and atom probe tomography. Our results suggest that the high number density of nanoscale α-phase precipitates in the β-phase matrix is due to ω assisted nucleation of α resulting in high tensile strength, greater than any current commercial titanium alloy. Thus hierarchical nanostructured Ti185 serves as an excellent candidate for replacing costlier titanium alloys and other structural alloys for cost-effective lightweighting applications.

  17. EXPERIMENTAL TESTS OF VANADIUM STRENGTH MODELS AT HIGH PRESSURES AND STRAIN RATES

    SciTech Connect

    Park, H; Barton, N R; Becker, R C; Bernier, J V; Cavallo, R M; Lorenz, K T; Pollaine, S M; Remington, B A; Rudd, R E

    2010-03-02

    Experimental results showing significant reductions from classical in the Rayleigh-Taylor (RT) instability growth rate due to high pressure material strength or effective lattice viscosity in metal foils are presented. On the Omega Laser in the Laboratory for Laser Energetics, University of Rochester, target samples of polycrystalline vanadium are compressed and accelerated quasi-isentropically at {approx}1 Mbar pressures, while maintaining the samples in the solid-state. Comparison of the results with constitutive models for solid state strength under these conditions show that the measured RT growth is substantially lower than predictions using existing models that work well at low pressures and long time scales. High pressure, high strain rate data can be explained by the enhanced strength due to a phonon drag mechanism, creating a high effective lattice viscosity.

  18. High-strength bioresorbable Fe–Ag nanocomposite scaffolds: Processing and properties

    SciTech Connect

    Sharipova, Aliya; Psakhie, Sergey G.; Swain, Sanjaya K.; Gutmanas, Elazar Y. Gotman, Irena

    2015-10-27

    High strength ductile iron-silver nanocomposite scaffolds were fabricated employing high energy attrition milling of micron-submicron powders, followed by cold sintering/high pressure consolidation. Particulate leaching method with soluble Na{sub 2}SO{sub 4} and K{sub 2}CO{sub 3} salts as porogens was used to create scaffolds with 50, 55, 60 and 73% volume fraction of pores. Part of specimens was annealed at 600, 800 and 900°C. Specimens were characterized employing X-ray diffraction, scanning electron microscopy (SEM) with electron probe microanalysis (EDS) and high resolution SEM. Mechanical properties were measured in compression and permeability was measured in permeameter based on Darcy’s law. Scaffolds with 50% and 55% porosity exhibited high compressive strength (18–22 MPa), compressive strength of 8–12 MPa was observed for scaffolds with 73% porosity. Treatments at 800 and 900°C result in increase of strength and ductility with some coarsening of microstructure. Best combination of compressive strength (15 MPa) and permeability (0.6{sup −6} cm{sup 2}) is close to the range of trabecular bone.

  19. High Salt Diets, Bone Strength and Mineral Content of Mature Femur After Skeletal Unloading

    NASA Technical Reports Server (NTRS)

    Liang, Michael T. C.

    1998-01-01

    It is known that high salt diets increase urinary calcium (Ca) loss, but it is not known whether this effect weakens bone during space flight. The Bone Hormone Lab has studied the effect of high salt diets on Ca balance and whole body Ca in a space flight model (2,8). Neither the strength nor mineral content of the femurs from these studies has been evaluated. The purpose of this study was to determine the effect of high salt diets (HiNa) and skeletal unloading on femoral bone strength and bone mineral content (BMC) in mature rats.

  20. STRENGTH PROPERTIES OF POLED PZT SUBJECTED TO BIAXIAL FLEXURAL LOADING IN HIGH ELECTRIC FIELD

    SciTech Connect

    Wang, Hong; Lin, Hua-Tay; Wereszczak, Andrew A

    2010-01-01

    Failure of poled PZT has been experimentally studied using ball-on-ring (BoR) biaxial flexure strength tests with an electric field concurrently applied. The as-received and aged PZTs were tested in high electric fields of -3 to 4 times the coercive field. Both the sign and the magnitude of electric field had a significant effect on the strength of poled PZT. A surface flaw type with a depth of around 18 m was identified as the strength limiter and responsible for the failure of the tested PZT. With a value of 0.76 MPa m1/2 in the open circle condition, the fracture toughness of the poled PZT was affected by an applied electric field just as the strength was affected. These results and observations have the potential to serve probabilistic reliability analysis and design optimization of multilayer PZT piezo actuators.

  1. High efficient preparation of carbon nanotube-grafted carbon fibers with the improved tensile strength

    NASA Astrophysics Data System (ADS)

    Fan, Wenxin; Wang, Yanxiang; Wang, Chengguo; Chen, Jiqiang; Wang, Qifen; Yuan, Yan; Niu, Fangxu

    2016-02-01

    An innovative technique has been developed to obtain the uniform catalyst coating on continuously moving carbon fibers. Carbon nanotube (CNT)-grafted carbon fibers with significantly improved tensile strength have been succeeded to produce by using chemical vapor deposition (CVD) when compared to the tensile strength of untreated carbon fibers. The critical requirements for preparation of CNT-grafted carbon fibers with high tensile strength have been found, mainly including (i) the obtainment of uniform coating of catalyst particles with small particle size, (ii) the low catalyst-induced and mechano-chemical degradation of carbon fibers, and (iii) the high catalyst activity which could facilitate the healing and strengthening of carbon fibers during the growth of CNTs. The optimum growth temperature was found to be about 500 °C, and the optimum catalyst is Ni due to its highest activity, there is a pronounced increase of 10% in tensile strength of carbon fibers after CNT growth at 500 °C by using Ni catalyst. Based on the observation from HRTEM images, a healing and crosslink model of neighboring carbon crystals by CNTs has been formulated to reveal the main reason that causes an increase in tensile strength of carbon fibers after the growth of CNTs. Such results have provided the theoretical and experimental foundation for the large-scale preparation of CNT-grafted carbon fibers with the improved tensile strength, significantly promoting the development of CNT-grafted carbon fiber reinforced polymer composites.

  2. High-capacity, high-strength trailer designs for the GA-4/GA-9 Casks

    SciTech Connect

    Kissinger, J.A.; Rickard, N.D.; Taylor, C.; Zimmer, A.

    1991-01-01

    General Atomics (GA) is developing final designs for two dedicated legal-weight trailers to transport the GA-4 and GA-9 Spent-Fuel Casks. The basic designs for these high-capacity, high-strength trailers are essentially identical except for small modifications to account for the differences in cask geometry. We are designing both trailers to carry a 55,000 lb (24,900 kg) payload and to withstand a 2.5 g vertical design load. The GA-4 and GA-9 trailers are designed for significantly higher loads than are typical commercial semitrailers, which are designed to loads in the range of 1.7 to 2.0 g. To meet the federal gross vehicle weight limit for legal-weight trucks, GA has set a target design weight for the trailers of 9000 lb (4080 kg). This weight includes the personnel barrier, cask tiedowns, and impact limiter removal and storage system. Based on the preliminary trailer designs, the final design weight is expected to be very close to this target weight. 3 refs., 3 figs.

  3. Observations on the Nonlinear Unloading Behavior of Advanced High Strength Steels

    NASA Astrophysics Data System (ADS)

    Pavlina, Erik J.; Lee, Myoung-Gyu; Barlat, Frédéric

    2015-01-01

    The unloading behavior was compared for three different steel grades: a dual-phase steel, a transformation-induced plasticity steel, and a twinning-induced plasticity steel. Steels that harden by phase transformation or deformation twinning exhibited a smaller component of microplastic strain during unloading and a smaller reduction in the chord modulus compared to the conventional hardening steel. As a result, unloading is closer to pure elastic unloading when the TRIP effect or TWIP effect is active.

  4. Strength-Based Factors for Successful Adaptation to an Early College High School Environment

    ERIC Educational Resources Information Center

    Abernethy, Catherine

    2010-01-01

    In an early college high school setting, students are subject to varying academic, social and contextual demands of a higher educational environment. In a strength-based study of 136 diverse early college high school students, this research explored the relationship of internal and external developmental assets to adaptive functioning of…

  5. Strength-toughness requirements for thick-walled high pressure vessels

    NASA Astrophysics Data System (ADS)

    Kapp, Joseph A.

    1992-05-01

    The strength and toughness requirements of materials used in high pressure vessels has been the subject of some discussion in the meetings of the Materials Task Group of the Special Working Group - High Pressure Vessels. A fracture mechanics analysis has been performed to theoretically establish the required toughness for a high pressure vessel. The analysis is based on the validity requirement for plane-strain fracture of fracture toughness test specimens. This means that at fracture, the crack length, uncracked ligament, and vessel length must each be greater than fifty times the crack tip plastic zone since for brittle fracture to occur. For high pressure piping applications, the limiting physical dimension is the uncracked ligament, since it can be assumed that the other dimensions are always greater than fifty times the crack tip plastic zone. To perform the fracture mechanics analysis, several parameters must be known, including vessel dimensions, material strength, degree of autofrettage, and design pressure. Remarkably, the results of the analysis show that the effects of radius ratio, pressure, and degree of autofrettage can be ignored when establishing strength and toughness requirements for design code purposes. The only parameters that enter into the calculation are yield strength, toughness and vessel thickness. The final results can easily be represented as a graph of yield strength against toughness on which several curves, one for each vessel thickness, are plotted.

  6. Fabrication and processing of high-strength densely packed carbon nanotube yarns without solution processes.

    PubMed

    Liu, Kai; Zhu, Feng; Liu, Liang; Sun, Yinghui; Fan, Shoushan; Jiang, Kaili

    2012-06-01

    Defects of carbon nanotubes, weak tube-tube interactions, and weak carbon nanotube joints are bottlenecks for obtaining high-strength carbon nanotube yarns. Some solution processes are usually required to overcome these drawbacks. Here we fabricate ultra-long and densely packed pure carbon nanotube yarns by a two-rotator twisting setup with the aid of some tensioning rods. The densely packed structure enhances the tube-tube interactions, thus making high tensile strengths of carbon nanotube yarns up to 1.6 GPa. We further use a sweeping laser to thermally treat as-produced yarns for recovering defects of carbon nanotubes and possibly welding carbon nanotube joints, which improves their Young's modulus by up to ∼70%. The spinning and laser sweeping processes are solution-free and capable of being assembled together to produce high-strength yarns continuously as desired. PMID:22538869

  7. Fabrication and processing of high-strength densely packed carbon nanotube yarns without solution processes

    NASA Astrophysics Data System (ADS)

    Liu, Kai; Zhu, Feng; Liu, Liang; Sun, Yinghui; Fan, Shoushan; Jiang, Kaili

    2012-05-01

    Defects of carbon nanotubes, weak tube-tube interactions, and weak carbon nanotube joints are bottlenecks for obtaining high-strength carbon nanotube yarns. Some solution processes are usually required to overcome these drawbacks. Here we fabricate ultra-long and densely packed pure carbon nanotube yarns by a two-rotator twisting setup with the aid of some tensioning rods. The densely packed structure enhances the tube-tube interactions, thus making high tensile strengths of carbon nanotube yarns up to 1.6 GPa. We further use a sweeping laser to thermally treat as-produced yarns for recovering defects of carbon nanotubes and possibly welding carbon nanotube joints, which improves their Young's modulus by up to ~70%. The spinning and laser sweeping processes are solution-free and capable of being assembled together to produce high-strength yarns continuously as desired.

  8. Improvement of formability of high strength steel sheets in shrink flanging

    NASA Astrophysics Data System (ADS)

    Hamedon, Z.; Abe, Y.; Mori, K.

    2016-02-01

    In the shrinkage flanging, the wrinkling tends to occur due to compressive stress. The wrinkling will cause a difficulty in assembling parts, and severe wrinkling may leads to rupture of parts. The shrinkage flange of the ultra-high strength steel sheets not only defects the product by the occurrence of the wrinkling but also causes seizure and wear of the dies and shortens the life of dies. In the present study, a shape of a punch having gradual contact was optimized in order to prevent the wrinkling in shrinkage flanging of ultra-high strength steel sheets. The sheet was gradually bent from the corner of the sheet to reduce the compressive stress. The wrinkling in the shrink flanging of the ultra-high strength steel sheets was prevented by the punch having gradual contact. It was found that the punch having gradual contact is effective in preventing the occurrence of wrinkling in the shrinkage flanging.

  9. Hardening and yielding in colloidal gels

    NASA Astrophysics Data System (ADS)

    Del Gado, Emanuela; Colombo, Jader; Bouzid, Mehdi

    Attractive colloidal gel networks are disordered elastic solids that can form even in extremely dilute particle suspensions. With interaction strengths comparable to the thermal energy, their stress-bearing network can locally restructure via breaking and reforming inter-particle bonds. We use molecular dynamics simulations of a model system to investigate the strain hardening and the yielding process. During shear start up protocol, the system exhibits strong localization of tensile stresses that may be released through the breaking and formation of new bonds. In this regime, the small amplitude oscillatory shear analysis shows that the storage and the loss modulus follow a power law behavior that are closely reminiscent of experimental observations. At large accumulated strains, the strain-induced reorganization of the gel may trigger flow heterogeneities and eventually lead to the yielding of the gel via a quasi brittle damage of its structure.

  10. Simplified identification of material parameters for Yoshida-Uemori kinematic hardening model

    NASA Astrophysics Data System (ADS)

    Phongsai, T.; Uthaisangsuk, V.; Chongthairungruang, B.; Suranuntchai, S.; Jirathearanat, S.

    2014-06-01

    In sheet metal forming process of Advanced High Strength (AHS) steels, springback effect is one of the most critical problems for manufacturer. The springback of a formed part occurs due to residual stress released after deformation. FE simulations were often used to describe both forming and springback behavior of steel sheets. Recently, the Yoshida- Uemori (Y-U) kinematic hardening model has been successfully applied for the springback simulation. The model is capable of reproducing the transient Bauschinger effect, permanent softening and work hardening stagnation during a large deformation. In this work, method for determining materials parameter of the Y-U model was briefly presented. Initially, cyclic tests were performed under both tension and compression loads for the high strength steel grade JSC780Y and JSC980Y. FE simulations of 1-element model were carried in order to investigate predicted cyclic stress strain curves. Both Y-U model and a mixed isotropic-kinematic Barlat2000 model were used in the simulations. Stamping tests of hat shape sample were carried out for verifying the experimental and numerical results. It was found that the Y-U model provided more accurate springback results than the other model.

  11. Application of Quenching and Partitioning (Q&P) Processing to Press Hardening Steel

    NASA Astrophysics Data System (ADS)

    Seo, Eun Jung; Cho, Lawrence; De Cooman, Bruno Charles

    2014-08-01

    Press hardening steel (PHS) has been increasingly used for the manufacture of structural automotive parts in recent years. One of the most critical characteristics of PHS is a low residual ductility related to a martensitic microstructure. The present work proposes the application of quenching and partitioning (Q&P) processing to improve the ductility of PHS. Q&P processing was applied to a Si- and Cr-added Q&P-compatible PHS, leading to a press hardened microstructure consisting of a tempered martensite matrix containing carbide-free bainite and retained austenite. The simultaneous addition of Si and Cr was used to increase the retained austenite fraction in the Q&P-compatible PHS. The Q&P processing of the PHS resulted in a high volume fraction of C-enriched retained austenite, and excellent mechanical properties. After a quench at 543 K (270 °C) and a partition treatment at 673 K (400 °C), the PHS microstructure contained a high volume fraction of retained austenite and a total elongation (TE) of 17 pct was achieved. The yield strength (YS) and the tensile strength were 1098 and 1320 MPa, respectively. The considerable improvement of the ductility of the Q&P-compatible PHS should lead to an improved in-service ductility beneficial to the passive safety of vehicle passengers.

  12. Life cycle CO{sub 2} evaluation on reinforced concrete structures with high-strength concrete

    SciTech Connect

    Tae, Sungho; Baek, Cheonghoon Shin, Sungwoo

    2011-04-15

    The purpose of this study is to evaluate the environment performance of high-strength concrete used in super tall buildings as material of environmental load reduction. To this end, this study proposed a plan for the evaluation of energy consumption and CO{sub 2} emission throughout the life cycle of the building, and calculated the energy consumption and CO{sub 2} emission throughout the life cycle of tall apartment building that was actually constructed using this plan. Then, we evaluated the energy consumption and CO{sub 2} emission reduction performance for the life cycle of the building by the decrease of concrete and reinforced rebar quantities and the increase of building lifespan obtained through conversion of existing building's concrete compressive strength to 40 MPa high-strength concrete. As a result, the life cycle energy consumption in case 3, a high-strength concrete building, decreased 15.53% and 2.95% respectively compared with cases 1 and 2. The evaluation of the general strength concrete buildings and the life cycle CO{sub 2} emission also decreased 16.70% and 3.37% respectively, compared with cases 1 and 2.

  13. Coseismic landslides reveal near-surface rock strength in a high-relief tectonically active setting

    USGS Publications Warehouse

    Gallen, Sean F; Clark, Marin K; Godt, Jonathan W.

    2014-01-01

    We present quantitative estimates of near-surface rock strength relevant to landscape evolution and landslide hazard assessment for 15 geologic map units of the Longmen Shan, China. Strength estimates are derived from a novel method that inverts earthquake peak ground acceleration models and coseismic landslide inventories to obtain material proper- ties and landslide thickness. Aggregate rock strength is determined by prescribing a friction angle of 30° and solving for effective cohesion. Effective cohesion ranges are from 70 kPa to 107 kPa for 15 geologic map units, and are approximately an order of magnitude less than typical laboratory measurements, probably because laboratory tests on hand-sized specimens do not incorporate the effects of heterogeneity and fracturing that likely control near-surface strength at the hillslope scale. We find that strength among the geologic map units studied varies by less than a factor of two. However, increased weakening of units with proximity to the range front, where precipitation and active fault density are the greatest, suggests that cli- matic and tectonic factors overwhelm lithologic differences in rock strength in this high-relief tectonically active setting.

  14. High strength, low carbon, dual phase steel rods and wires and process for making same

    DOEpatents

    Thomas, Gareth; Nakagawa, Alvin H.

    1986-01-01

    A high strength, high ductility, low carbon, dual phase steel wire, bar or rod and process for making the same is provided. The steel wire, bar or rod is produced by cold drawing to the desired diameter in a single multipass operation a low carbon steel composition characterized by a duplex microstructure consisting essentially of a strong second phase dispersed in a soft ferrite matrix with a microstructure and morphology having sufficient cold formability to allow reductions in cross-sectional area of up to about 99.9%. Tensile strengths of at least 120 ksi to over 400 ksi may be obtained.

  15. ZERODUR glass ceramics: strength data for the design of structures with high mechanical stresses

    NASA Astrophysics Data System (ADS)

    Hartmann, Peter; Nattermann, Kurt; Döhring, Thorsten; Kuhr, Markus; Thomas, Peter; Kling, Guenther; Gath, Peter; Lucarelli, Stefano

    2008-07-01

    With an increasing number of applications mirrors and support structures made of the zero expansion glass ceramic material ZERODUR® has to endure high mechanical loads, e.g. rocket launches or controlled deformations for optical image correction. Like for other glassy materials, the strength of glass ceramics is dominated by its surface condition. Test specimens have been ground with fine grain tools (e.g. D64 diamond grains) and / or subsequently etched. The strength data basis for the design of highly stressed structures has been extended and new information has been derived for the extrapolation to low failure probabilities.

  16. Empirical beam hardening correction (EBHC) for CT

    SciTech Connect

    Kyriakou, Yiannis; Meyer, Esther; Prell, Daniel; Kachelriess, Marc

    2010-10-15

    C-arm CT scanner (Axiom Artis dTA, Siemens Healthcare, Forchheim, Germany). A large variety of phantom, small animal, and patient data were used to demonstrate the data and system independence of EBHC. Results: Although no physics apart from the initial segmentation procedure enter the correction process, beam hardening artifacts were significantly reduced by EBHC. The image quality for clinical CT, micro-CT, and C-arm CT was highly improved. Only in the case of C-arm CT, where high scatter levels and calibration errors occur, the relative improvement was smaller. Conclusions: The empirical beam hardening correction is an interesting alternative to conventional iterative higher order beam hardening correction algorithms. It does not tend to over- or undercorrect the data. Apart from the segmentation step, EBHC does not require assumptions on the spectra or on the type of material involved. Potentially, it can therefore be applied to any CT image.

  17. Life on the Hardened Border

    ERIC Educational Resources Information Center

    Miller, Bruce Granville

    2012-01-01

    The many Coast Salish groups distributed on both sides of the United States-Canada border on the Pacific coast today face significant obstacles to cross the international border, and in some cases are denied passage or intimidated into not attempting to cross. The current situation regarding travel by Aboriginal people reflects the "hardening" of…

  18. Effect of preseason concurrent muscular strength and high-intensity interval training in professional soccer players.

    PubMed

    Wong, Pui-lam; Chaouachi, Anis; Chamari, Karim; Dellal, Alexandre; Wisloff, Ulrik

    2010-03-01

    This study examined the effect of concurrent muscular strength and high-intensity running interval training on professional soccer players' explosive performances and aerobic endurance. Thirty-nine players participated in the study, where both the experimental group (EG, n = 20) and control group (CG, n = 19) participated in 8 weeks of regular soccer training, with the EG receiving additional muscular strength and high-intensity interval training twice per week throughout. Muscular strength training consisted of 4 sets of 6RM (repetition maximum) of high-pull, jump squat, bench press, back half squat, and chin-up exercises. The high-intensity interval training consisted of 16 intervals each of 15-second sprints at 120% of individual maximal aerobic speed interspersed with 15 seconds of rest. EG significantly increased (p < or = 0.05) 1RM back half squat and bench press but showed no changes in body mass. Within-subject improvement was significantly higher (p < or = 0.01) in the EG compared with the CG for vertical jump height, 10-m and 30-m sprint times, distances covered in the Yo-Yo Intermittent Recovery Test and maximal aerobic speed test, and maximal aerobic speed. High-intensity interval running can be concurrently performed with high load muscular strength training to enhance soccer players' explosive performances and aerobic endurance.

  19. Neck strength: a protective factor reducing risk for concussion in high school sports.

    PubMed

    Collins, Christy L; Fletcher, Erica N; Fields, Sarah K; Kluchurosky, Lisa; Rohrkemper, Mary Kay; Comstock, R Dawn; Cantu, Robert C

    2014-10-01

    As the number of high school students participating in athletics continues to increase, so will the number of sports-related concussions unless effective concussion prevention programs are developed. We sought to develop and validate a cost-effective tool to measure neck strength in a high school setting, conduct a feasibility study to determine if the developed tool could be reliably applied by certified athletic trainers (ATs) in a high school setting, and conduct a pilot study to determine if anthropometric measurements captured by ATs can predict concussion risk. In the study's first phase, 16 adult subjects underwent repeated neck strength testing by a group of five ATs to validate the developed hand-held tension scale, a cost effective alternative to a hand-held dynamometer. In the second phase, during the 2010 and 2011 academic years, ATs from 51 high schools in 25 states captured pre-season anthropometric measurements for 6,704 high school athletes in boys' and girls' soccer, basketball, and lacrosse, as well as reported concussion incidence and athletic exposure data. We found high correlations between neck strength measurements taken with the developed tool and a hand-held dynamometer and the measurements taken by five ATs. Smaller mean neck circumference, smaller mean neck to head circumference ratio, and weaker mean overall neck strength were significantly associated with concussion. Overall neck strength (p < 0.001), gender (p < 0.001), and sport (p = 0.007) were significant predictors of concussions in unadjusted models. After adjusting for gender and sport, overall neck strength remained a significant predictor of concussion (p = 0.004). For every one pound increase in neck strength, odds of concussion decreased by 5 % (OR = 0.95, 95 % CI 0.92-0.98). We conclude that identifying differences in overall neck strength may be useful in developing a screening tool to determine which high school athletes are at higher risk of concussion. Once identified

  20. Neck strength: a protective factor reducing risk for concussion in high school sports.

    PubMed

    Collins, Christy L; Fletcher, Erica N; Fields, Sarah K; Kluchurosky, Lisa; Rohrkemper, Mary Kay; Comstock, R Dawn; Cantu, Robert C

    2014-10-01

    As the number of high school students participating in athletics continues to increase, so will the number of sports-related concussions unless effective concussion prevention programs are developed. We sought to develop and validate a cost-effective tool to measure neck strength in a high school setting, conduct a feasibility study to determine if the developed tool could be reliably applied by certified athletic trainers (ATs) in a high school setting, and conduct a pilot study to determine if anthropometric measurements captured by ATs can predict concussion risk. In the study's first phase, 16 adult subjects underwent repeated neck strength testing by a group of five ATs to validate the developed hand-held tension scale, a cost effective alternative to a hand-held dynamometer. In the second phase, during the 2010 and 2011 academic years, ATs from 51 high schools in 25 states captured pre-season anthropometric measurements for 6,704 high school athletes in boys' and girls' soccer, basketball, and lacrosse, as well as reported concussion incidence and athletic exposure data. We found high correlations between neck strength measurements taken with the developed tool and a hand-held dynamometer and the measurements taken by five ATs. Smaller mean neck circumference, smaller mean neck to head circumference ratio, and weaker mean overall neck strength were significantly associated with concussion. Overall neck strength (p < 0.001), gender (p < 0.001), and sport (p = 0.007) were significant predictors of concussions in unadjusted models. After adjusting for gender and sport, overall neck strength remained a significant predictor of concussion (p = 0.004). For every one pound increase in neck strength, odds of concussion decreased by 5 % (OR = 0.95, 95 % CI 0.92-0.98). We conclude that identifying differences in overall neck strength may be useful in developing a screening tool to determine which high school athletes are at higher risk of concussion. Once identified

  1. Single cell mechanics: stress stiffening and kinematic hardening.

    PubMed

    Fernández, Pablo; Ott, Albrecht

    2008-06-13

    Cell mechanical properties are fundamental to the organism but remain poorly understood. We report a comprehensive phenomenological framework for the complex rheology of single fibroblast cells: a superposition of elastic stiffening and viscoplastic kinematic hardening. Despite the complexity of the living cell, its mechanical properties can be cast into simple, well-defined rules. Our results reveal the key role of crosslink slippage in determining mechanical cell strength and robustness. PMID:18643547

  2. Elastic constant versus temperature behavior of three hardened maraging steels

    NASA Technical Reports Server (NTRS)

    Ledbetter, H. M.; Austin, M. W.

    1985-01-01

    Elastic constants of three maraging steels were determined by measuring ultrasonic velocities. Annealed steels show slightly lower bulk moduli and considerably lower shear moduli than hardened steels. All the elastic constants (Young's modulus, shear modulus, bulk modulus and Poisson's ratio) show regular temperature behavior between 76 and 400 K. Young's modulus and the shear modulus increase with increasing yield strength, but the bulk modulus and Poisson's ratio are relatively unchanged. Elastic anisotropy is quite small.

  3. Status of High-Strength Nanotube Composites at Johnson Space Center

    NASA Technical Reports Server (NTRS)

    Files, Bradley S.; Mayeaux, Brian; Proft, William; Nikolaev, Pavel; Nicholson, Leonard S. (Technical Monitor)

    2000-01-01

    Single-wall carbon nanotubes offer extraordinary mechanical properties that could start a revolution in materials science. The combination of very high strength and modulus with high strain to failure makes nanotubes an ideal fiber for strengthening in composites. Because of the scale of these fibers, new challenges exist for processing of composite materials and materials characterization. Our project includes aspects of nanotube materials from production and characterization to purification and incorporation into composites for mechanical testing. Early results show that some new techniques will be necessary for the strength of single wall nanotubes to be fully utilized. Current research at JSC focuses on structural polymeric materials to attempt to lower the weight of spacecraft necessary for interplanetary missions. Studies show good nanotube dispersion and wetting by the epoxy materials. Results of tensile strength tests will also be reported. This presentation will focus on current research into polymer nanotube composites and the next steps toward this revolution in aerospace materials.

  4. Effects of creep damage, shot peening, and case hardening on magnetic Barkhausen noise analysis

    SciTech Connect

    Sipahi, L.B. Iowa State Univ., Ames, IA . Inst. for Physical Research and Technology)

    1994-11-01

    The micromagnetic emissions, commonly known as Barkhausen noise, are very sensitive to variations in the microstructure and sub-surface stress states of magnetic materials. Steel pipelines at power plants often have creep damage due to microstructural changes in their service life. Early detection of this damage will prevent costly failures. There is also an increasing demand to characterize the sub-surface stress states in structural materials such as high strength materials used in landing gear components in the aerospace industry. Shot peening is used to improve the fatigue strength of these components by the introduction of residual compressive stresses to the surface. Because the magnitude of Barkhausen noise varies with the magnitude of compressive stress, these noise measurements can be used for in-situ evaluation of the effectiveness of the shot peening process. Furthermore, surface modification such as case hardened magnetic samples can be easily observed using micromagnetic Barkhausen noise (MBE) to determine further modification needs.

  5. Radiation hardening of diagnostics

    SciTech Connect

    Siemon, R.E.

    1991-01-01

    The world fusion program has advanced to the stage where it is appropriate to construct a number of devices for the purpose of burning DT fuel. In these next-generation experiments, the expected flux and fluence of 14 MeV neutrons and associated gamma rays will pose a significant challenge to the operation and diagnostics of the fusion device. Radiation effects include structural damage to materials such as vacuum windows and seals, modifications to electrical properties such as electrical conductivity and dielectric strength and impaired optical properties such as reduced transparency and luminescence of windows and fiber optics during irradiation. In preparation for construction and operation of these new facilities, the fusion diagnostics community needs to work with materials scientists to develop a better understanding of radiation effects, and to undertake a testing program aimed at developing workable solutions for this multi-faceted problem. A unique facility to help in this regard is the Los Alamos Spallation Radiation Effects Facility, a neutron source located at the beam stop of the world's most powerful accelerator, the Los Alamos Meson Physics Facility (LAMPF). The LAMPF proton beam generates 10{sup 16} neutrons per second because of spallation'' reactions when the protons collide with the copper nuclei in the beam stop.

  6. CSCS certification and school enrollment impacts upon high school strength facilities, equipment, and safety.

    PubMed

    Judge, Lawrence W; Petersen, Jeffrey C; Bellar, David M; Craig, Bruce W; Gilreath, Erin L

    2013-09-01

    The rapid growth and expanding use of high school strength and conditioning facilities (SCFs) creates a need to research and better understand these vital facilities. This study was designed to examine SCFs at the high school level including facility size, equipment, leadership/staffing, and safety. A 70-item online survey instrument, developed with expert input from certified strength professionals, was used to collect data regarding the SCFs in high schools throughout a midwestern state, and was distributed via email to a total of 390 high school athletic directors. Survey respondents (n = 108) all reported the presence of SCFs with 95.4% indicating a dedicated SCF space. A strong positive correlation (r = 0.610, p ≤ 0.001) was determined between the variables of SCF size in square feet and school size measured by total enrollment. Analysis of variance and χ² analyses revealed significant differences in equipment, facility size, and safety factors based on the categorical variables of school size and the presence of certified strength and conditioning specialist (CSCS) leadership. It appears the CSCS's application of their scientific knowledge goes beyond training athletes for the goal of improving athletic performance to actually influence the SCF itself. Athletic administrators at the high school level need to recognize the impact CSCS program leadership can have on the overall quality of the strength and conditioning program and facility.

  7. A Study on Forming Characteristics of Roll Forming Process with High Strength Steel

    NASA Astrophysics Data System (ADS)

    Joo, ByeongDon; Lee, HyunJong; Kim, DongKyu; Moon, YoungHoon

    2011-08-01

    Roll forming is a kind of sheet metal forming process used to manufacture long sheet metal products with constant cross section. Recently, roll forming technology draws attentions of automotive industries due to its various advantages, such as high production speed, reduced tooling cost and improved quality. In automotive industries, roll formed automotive parts used as structural components in vehicle body frame or sub frame and high strength steel becomes more common to improve safety and fuel efficiency. However, when roll forming process is performed with high strength steel, rolling forming defects, such as spring back, buckling and scratch should be considered more carefully. In this study, efforts to avoid roll forming defects and to optimize forming parameters were performed. FE analysis was performed with high strength steels using commercially available simulation software, COPRA-RF™ and SHAPE-RF™. Forming characteristics were analyzed and roll flower model and proper roll-pass sequences were suggested by analyzing longitudinal strain and deformation behavior. This study provided considerable experience about roll forming process design that using high strength steel.

  8. Effects of high pressure strength of rock material on penetration by shaped charge jet

    NASA Astrophysics Data System (ADS)

    Huang, Hongfa

    2012-03-01

    Perforating of oil/gas well creates communication tunnel between reservoir and wellbore. Shaped charges are widely used as perforators in oilfield industry. The liners of the charges are mostly made of powder metal to prevent solid slug clogging the entrance hole of well casing or locking the hole in perforating gun. High speed jet from the shaped charge pierces through perforating gun, well fluid, well casing, and then penetrates into reservoir formation. Prediction of jet penetration in reservoir rock is critical in modeling of well production. An analytical penetration model developed for solid rod by Tate and Alekseevskii is applied in this work. For better results, strength of formation rock at high pressure needs to be measured. Lateral stress gauge measurements in plate impact tests are conducted. Piezoelectric pressure gauges are imbedded in samples to measure the longitudinal and transverse stress simultaneously. The two stresses provide Hugoniot and material compressive strength. Indiana limestone, a typical rock in perforation testing, is selected as target sample material in the plate impact tests. Since target strength effect on penetration is more important in late stage of penetration when the strength of material becomes significant compared to the impact pressure, all the impact tests are focused on lower impact pressure up to 9 GPa. The measurements show that the strength increases with impact pressure. The results are applied in the penetration calculations. The final penetration matches testing data very well.

  9. Heterogeneous lamella structure unites ultrafine-grain strength with coarse-grain ductility.

    PubMed

    Wu, Xiaolei; Yang, Muxin; Yuan, Fuping; Wu, Guilin; Wei, Yujie; Huang, Xiaoxu; Zhu, Yuntian

    2015-11-24

    Grain refinement can make conventional metals several times stronger, but this comes at dramatic loss of ductility. Here we report a heterogeneous lamella structure in Ti produced by asymmetric rolling and partial recrystallization that can produce an unprecedented property combination: as strong as ultrafine-grained metal and at the same time as ductile as conventional coarse-grained metal. It also has higher strain hardening than coarse-grained Ti, which was hitherto believed impossible. The heterogeneous lamella structure is characterized with soft micrograined lamellae embedded in hard ultrafine-grained lamella matrix. The unusual high strength is obtained with the assistance of high back stress developed from heterogeneous yielding, whereas the high ductility is attributed to back-stress hardening and dislocation hardening. The process discovered here is amenable to large-scale industrial production at low cost, and might be applicable to other metal systems. PMID:26554017

  10. Heterogeneous lamella structure unites ultrafine-grain strength with coarse-grain ductility

    PubMed Central

    Wu, Xiaolei; Yang, Muxin; Yuan, Fuping; Wu, Guilin; Wei, Yujie; Huang, Xiaoxu; Zhu, Yuntian

    2015-01-01

    Grain refinement can make conventional metals several times stronger, but this comes at dramatic loss of ductility. Here we report a heterogeneous lamella structure in Ti produced by asymmetric rolling and partial recrystallization that can produce an unprecedented property combination: as strong as ultrafine-grained metal and at the same time as ductile as conventional coarse-grained metal. It also has higher strain hardening than coarse-grained Ti, which was hitherto believed impossible. The heterogeneous lamella structure is characterized with soft micrograined lamellae embedded in hard ultrafine-grained lamella matrix. The unusual high strength is obtained with the assistance of high back stress developed from heterogeneous yielding, whereas the high ductility is attributed to back-stress hardening and dislocation hardening. The process discovered here is amenable to large-scale industrial production at low cost, and might be applicable to other metal systems. PMID:26554017

  11. Influence of Precipitation Hardening in Mg-Y-Nd on Mechanical and Corrosion Properties

    NASA Astrophysics Data System (ADS)

    Maier, P.; Peters, R.; Mendis, C. L.; Müller, S.; Hort, N.

    2016-04-01

    Precipitation hardening is an effective strengthening mechanism to achieve high strength at moderate ductility in Mg-RE alloys. However, improved mechanical properties by precipitates that strengthen the alloy can affect corrosion rates as the finely dispersed particles are often more noble than the matrix. Biodegradable implant material should show a certain corrosion rate, but should be free of pitting, because wide and deep pits are notches that can cause higher stress concentration. WE43 has generally shown an acceptable biological response. In this study, a Mg-Y-Nd-Gd-Dy (WE32) alloy in extruded, solution and precipitation heat-treated conditions has been investigated. Solution heat treatment causes grain growth and strength loss. A rather short ageing response to peak hardness was observed, where peak hardening causes hardness values to exceed that of the initial extruded condition. Grain growth during ageing is not significant. Corrosion was evaluated with potentiodynamic polarization in Ringer Acetate solution. The highest corrosion rate was observed in the T4 condition. The peak aged alloy showed the most homogenous form of corrosion.

  12. Characterizing Hardening on Annealing of Cold-Rolled Aluminum AA3103 Strips

    NASA Astrophysics Data System (ADS)

    Govindaraj, Nagaraj Vinayagam; Bjørge, Ruben; Holmedal, Bjørn

    2013-10-01

    AA3103 aluminum strips were cold rolled to various von Mises strains up to 4.7. In addition, two severely deformed conditions were obtained by one and four cycles of cold accumulated roll bonding subsequent to cold rolling to a strain of 4.2. For cases of subsequent annealing at 498 K (225 °C) for 10 minutes, an increase in the ultimate tensile strength was observed at the rolling strains of 1.7 and higher. Similar hardening is observed for a wide range of temperature-time combinations for temperatures greater than 423 K (150 °C). The yield stress is also increased by a few per cent during further cold rolling. The magnitude of the increase in strength on annealing increased with the increasing strain. Electron backscattered diffraction and transmission electron microscopy studies showed no significant changes in the high- or low-angle grain boundary spacings by this annealing. A systematic investigation on the roles played by Si and Mn was made with different homogenization treatments of AA3103 and of an AlSi alloy. Based on tensile tests, and differential scanning calorimetry and electrical conductivity measurements, it is concluded that Mn plays a major role. The exact mechanisms causing hardening on annealing are not identified, but through elimination of other explanations, it is suggested that some sort of clustering or precipitation mechanism is involved.

  13. High dose weekly oral prednisone improves strength in boys with Duchenne muscular dystrophy.

    PubMed

    Connolly, Anne M; Schierbecker, Jeanine; Renna, Renee; Florence, Julaine

    2002-12-01

    Daily prednisone improves strength in boys with Duchenne muscular dystrophy, but side effects are almost universal. We used a different dosing regimen of prednisone to determine if benefit to boys with Duchenne muscular dystrophy might be maintained with fewer side effects. Twice weekly oral prednisone was given each Friday and Saturday (5mg/kg/dose). This total dose is twice as high as the daily low dosage prednisone regimen (0.75 mg/kg/day). Twenty boys (8.0+/-1.2 years) were treated. Historical control groups included 18 untreated boys (6.1+/-1.6 years) and four boys (7.3+/-0.6 years) treated with daily prednisone. Strength (using a hand-held manometer and grip meter) and timed functional testing were measured. There was an improvement in upper extremity strength for 95% of boys (n=20) at 6 months using quantitative strength testing. Improvement in lower extremity strength occurred in all boys with antigravity quadriceps strength (17/17). The improvement (P=0.001 for proximal upper extremities; P=0.002 for grip; and P<0.0001 for proximal lower extremities) was significant compared to untreated boys. Sixteen boys were treated continuously for more than 12 months (22+/-1.5 months). Of these, 15 remained significantly stronger than prior to treatment and 8/16 showed additional gains in strength after six months of treatment. Six boys were on the weekly prednisolone 2 years or longer without interruption. All six had upper and lower extremity strength at follow-up that was as good or better than at baseline. Functional testing improved in boys less than 8 years without contractures. Three boys without antigravity quadriceps strength at the start of treatment lost the ability to walk unassisted within 6 months. Eight other boys lost the ability to ambulate unassisted between 12 and 24 months of treatment. In each, progressive contractures developed. Linear growth was maintained in all boys on weekly treatment. Obesity rates did not differ from untreated boys. Twice

  14. Span-to-depth ratio effect on shear strength of steel fiber-reinforced high-strength concrete deep beams using ANN model

    NASA Astrophysics Data System (ADS)

    Naik, Uday; Kute, Sunil

    2013-12-01

    The paper predicts the shear strength of high-strength steel fiber-reinforced concrete deep beams. It studies the effect of clear span-to-overall depth ratio on shear capacity of steel fiber high-strength deep beams using artificial neural network (ANN8). The three-layered model has eight input nodes which represent width, effective depth, volume fraction, fiber aspect ratio and shear span-to-depth ratio, longitudinal steel, compressive strength of concrete, and clear span-to-overall depth ratio. The model predicts the shear strength of high-strength steel fiber deep beams to be reasonably good when compared with the results of proposed equations by researchers as well as the results obtained by neural network (ANN7) which is developed for seven inputs excluding span-to-depth ratio. The developed neural network ANN8 proves the versatility of artificial neural networks to establish the relations between various parameters affecting complex behavior of steel fiber-reinforced concrete deep beams and costly experimental processes.

  15. Formability Analysis of Diode-Laser-Welded Tailored Blanks of Advanced High-Strength Steel Sheets

    NASA Astrophysics Data System (ADS)

    Panda, S. K.; Baltazar Hernandez, V. H.; Kuntz, M. L.; Zhou, Y.

    2009-08-01

    Currently, advances due to tailored blanking can be enhanced by the development of new grades of advanced high-strength steels (HSSs), for the further weight reduction and structural improvement of automotive components. In the present work, diode laser welds of three different grades of advanced high-strength dual-phase (DP) steel sheets (with tensile strengths of 980, 800, and 450 MPa) to high-strength low-alloy (HSLA) material were fabricated by applying the proper welding parameters. Formability in terms of Hecker’s limiting dome height (LDH), the strain distribution on the hemispherical dome surface, the weld line movement during deformation, and the load-bearing capacity during the stretch forming of these different laser-welded blanks were compared. Finite element (FE) analysis of the LDH tests of both the parent metals and laser-welded blanks was done using the commercially available software package LS-DYNA (Livermore Software Technology Corporation, Livermore, CA); the results compared well with the experimental data. It was also found that the LDH was not affected by the soft zone or weld zone properties; it decreased, however, with an increase in a nondimensional parameter, the “strength ratio” (SR). The weld line movement during stretch forming is an indication of nonuniform deformation resulting in a decrease in the LDH. In all the dissimilar weldments, fracture took place on the HSLA side, but the fracture location shifted to near the weld line (at the pole) in tailor-welded blanks (TWBs) of a higher strength ratio.

  16. Design of Hierarchically Cut Hinges for Highly Stretchable and Reconfigurable Metamaterials with Enhanced Strength.

    PubMed

    Tang, Yichao; Lin, Gaojian; Han, Lin; Qiu, Songgang; Yang, Shu; Yin, Jie

    2015-11-25

    Applying hierarchical cuts to thin sheets of elastomer generates super-stretchable and reconfigurable metamaterials, exhibiting highly nonlinear stress-strain behaviors and tunable phononic bandgaps. The cut concept fails on brittle thin sheets due to severe stress concentration in the rotating hinges. By engineering the local hinge shapes and global hierarchical structure, cut-based reconfigurable metamaterials with largely enhanced strength are realized.

  17. Hydration and muscular performance: does fluid balance affect strength, power and high-intensity endurance?

    PubMed

    Judelson, Daniel A; Maresh, Carl M; Anderson, Jeffrey M; Armstrong, Lawrence E; Casa, Douglas J; Kraemer, William J; Volek, Jeff S

    2007-01-01

    Significant scientific evidence documents the deleterious effects of hypohydration (reduced total body water) on endurance exercise performance; however, the influence of hypohydration on muscular strength, power and high-intensity endurance (maximal activities lasting >30 seconds but <2 minutes) is poorly understood due to the inconsistent results produced by previous investigations. Several subtle methodological choices that exacerbate or attenuate the apparent effects of hypohydration explain much of this variability. After accounting for these factors, hypohydration appears to consistently attenuate strength (by approximately 2%), power (by approximately 3%) and high-intensity endurance (by approximately 10%), suggesting alterations in total body water affect some aspect of force generation. Unfortunately, the relationships between performance decrement and crucial variables such as mode, degree and rate of water loss remain unclear due to a lack of suitably uninfluenced data. The physiological demands of strength, power and high-intensity endurance couple with a lack of scientific support to argue against previous hypotheses that suggest alterations in cardiovascular, metabolic and/or buffering function represent the performance-reducing mechanism of hypohydration. On the other hand, hypohydration might directly affect some component of the neuromuscular system, but this possibility awaits thorough evaluation. A critical review of the available literature suggests hypohydration limits strength, power and high-intensity endurance and, therefore, is an important factor to consider when attempting to maximise muscular performance in athletic, military and industrial settings.

  18. Preparation of high-strength nanometer scale twinned coating and foil

    DOEpatents

    Zhang, Xinghang; Misra, Amit; Nastasi, Michael A.; Hoagland, Richard G.

    2006-07-18

    Very high strength single phase stainless steel coating has been prepared by magnetron sputtering onto a substrate. The coating has a unique microstructure of nanometer spaced twins that are parallel to each other and to the substrate surface. For cases where the coating and substrate do not bind strongly, the coating can be peeled off to provide foil.

  19. High strength, light weight Ti-Y composites and method of making same

    DOEpatents

    Verhoeven, J.D.; Ellis, T.W.; Russell, A.M.; Jones, L.L.

    1993-04-06

    A high strength, light weight in-situ'' Ti-Y composite is produced by deformation processing a cast body having Ti and Y phase components distributed therein. The composite comprises elongated, ribbon-shaped Ti and Y phase components aligned along an axis of the deformed body.

  20. High strength, light weight Ti-Y composites and method of making same

    DOEpatents

    Verhoeven, John D.; Ellis, Timothy W.; Russell, Alan M.; Jones, Lawrence L.

    1993-04-06

    A high strength, light weight "in-situ" Ti-Y composite is produced by deformation processing a cast body having Ti and Y phase components distributed therein. The composite comprises elongated, ribbon-shaped Ti and Y phase components aligned along an axis of the deformed body.

  1. An investigation of the plastic fracture of high strength steels. Ph.D. Thesis

    NASA Technical Reports Server (NTRS)

    Cox, T. B.; Low, J. R., Jr.

    1973-01-01

    Three generally recognized stages of plastic fracture in high strength steels are considered in detail. These stages consist of void initiation, void growth, and void coalescence. A brief review of the existing literature on plastic fracture is included along with an outline of the experimental approach used in the investigation.

  2. Relationship of Muscular Strength on Work Performance in High School Students with Mental Retardation

    ERIC Educational Resources Information Center

    Smail, Karen M.; Horvat, Michael

    2006-01-01

    The relationship of muscular strength on work performance measures in high school students with mild mental retardation was investigated. Ten students from a self contained Special Education class were matched according to age, gender, height, and weight then randomly assigned to either the treatment group or control group. The treatment group…

  3. Kic size effect study on two high-strength steels using notched bend specimens

    NASA Technical Reports Server (NTRS)

    Stonesifer, F. R.

    1974-01-01

    Five methods are used to calculate plane strain fracture toughness (K sub Q) values for bend-specimens of various sizes from two high-strength steels. None of the methods appeared to satisfactorily predict valid stress intensity factor (K sub IC) values from specimens of sizes well below that required by E399 standard tests.

  4. Marketing research for EE G Mound Applied Technologies' heat treatment process of high strength materials

    SciTech Connect

    Shackson, R.H.

    1991-10-09

    This report summarizes research conducted by ITI to evaluate the commercialization potential of EG G Mound Applied Technologies' heat treatment process of high strength materials. The remainder of the report describes the nature of demand for maraging steel, extent of demand, competitors, environmental trends, technology life cycle, industry structure, and conclusion. (JL)

  5. Neptunium(V) Adsorption to Bacteria at Low and High Ionic Strength

    NASA Astrophysics Data System (ADS)

    Ams, D.; Swanson, J. S.; Reed, D. T.

    2010-12-01

    Np(V) is expected to be the predominant oxidation state of neptunium in aerobic natural waters. Np(V), as the NpO2+ aquo and associated complexed species, is readily soluble, interacts weakly with geologic media, and has a high redox stability under a relatively wide range of subsurface conditions. These chemical properties, along with a long half-life make it a primary element of concern regarding long-term nuclear waste storage and subsurface containment. The fate and transport of neptunium in the environment may be influenced by adsorption onto bacterial surfaces. The adsorption of neptunium to bacterial surfaces ties the mobility of the contaminant to the mobility of the bacterium. In this study, the adsorption of the neptunyl (NpO2+) ion was evaluated at low ionic strength on a common soil bacterium and at high ionic strength on a halophilic bacterium isolated from a briny groundwater near the Waste Isolation Pilot Plant (WIPP) in southeast New Mexico. Adsorption experiments were performed in batch reactors as a function of pH, ionic strength, and bacteria/Np mass ratio. Np(V) adsorption was modeled using a surface complexation approach with the mathematical program FITEQL to determine functional group specific binding constants. The data from acid and base titrations of the bacteria used were also modeled to estimate the concentrations and deprotonation constants of discrete bacterial surface functional groups. Bacterial functional group characteristics and Np(V) adsorption behavior between the soil bacterium and the halophilic bacterium were compared. These results highlight key similarities and differences in actinide adsorption behavior in environments of significantly different ionic strength. The observed adsorption behavior may be linked to similarities and differences in the characteristics of the moieties between the cell walls of common gram-negative soil and halophilic bacteria. Moreover, differences in adsorption behavior may also reflect ionic

  6. Neptunium(V) adsorption to bacteria at low and high ionic strength

    SciTech Connect

    Ams, David A; Swanson, Juliet S; Reed, Donald T; Fein, Jeremy B

    2010-12-08

    Np(V) is expected to be the predominant oxidation state of neptunium in aerobic natural waters. Np(V), as the NpO{sub 2}{sup +} aquo and associated complexed species, is readily soluble, weakly interacting with geologic media, and has a high redox stability under a relatively wide range of subsurface conditions. These chemical properties, along with a long half-life make it a primary element of concern regarding long-term nuclear waste storage and subsurface contaminant. The fate and transport of neptunium in the environment may be influenced by adsorption onto bacterial surfaces. The adsorption of neptunium to bacterial surfaces ties the mobility of the contaminant to the mobility of the bacterium. In this study, the adsorption of the neptunyl (NpO{sub 2}{sup +}) ion was evaluated at low ionic strength on a common soil bacterium and at high ionic strength on a halophilic bacterium isolated from a briny groundwater near the Waste Isolation Pilot Plant (WIPP) in southeast New Mexico. Adsorption experiments were performed in batch reactors as a function of pH, ionic strength, and bacterialNp mass ratio. Np(V) adsorption was modeled using a surface complexation approach with the mathematical program FITEQL to determine functional group specific binding constants. The data from acid and base titrations of the bacteria were also modeled to estimate the concentrations and deprotonation constants of discrete bacterial surface functional groups. Bacterial functional group characteristics and Np(V) adsorption behavior between the soil bacterium and the halophilic bacterium were compared. These results highlight the key similarities and differences in actinide adsorption behavior in environments of significantly different ionic strength. Similarities in adsorption behavior may be linked to similarities in the characteristics of the moieties between all bacterial cell walls. Differences in adsorption behavior may reflect differences in ionic strength effects, rather than

  7. Properties of Galvanized and Galvannealed Advanced High Strength Hot Rolled Steels

    SciTech Connect

    V.Y. Guertsman; E. Essadiqi; S. Dionne; O. Dremmailova; R. Bouchard; B. Voyzelle; J. McDermid; R. Fourmentin

    2008-04-01

    The objectives of the project were (i) to develop the coating process information to achieve good quality coatings on 3 advanced high strength hot rolled steels while retaining target mechanical properties, (ii) to obtain precise knowledge of the behavior of these steels in the various forming operations and (iii) to establish accurate user property data in the coated conditions. Three steel substrates (HSLA, DP, TRIP) with compositions providing yield strengths in the range of 400-620 MPa were selected. Only HSLA steel was found to be suitable for galnaizing and galvannealing in the hot rolled condition.

  8. Low-noise, high-strength, spiral-bevel gears for helicopter transmissions

    NASA Astrophysics Data System (ADS)

    Lewicki, David G.; Handschuh, Robert F.; Henry, Zachary S.; Litvin, Faydor L.

    1994-05-01

    Advanced-design spiral-bevel gears were tested in an OH-58D helicopter transmission using the NASA 500-hp Helicopter Transmission Test Stand. Three different gear designs tested included: the current design of the OH-58D transmission; a higher-strength design the same as the current but with a full fillet radius to reduce gear tooth bending stress (and thus, weight); and a lower-noise design the same as the high-strength but with modified tooth geometry to reduce transmission error and noise. Noise, vibration, and tooth strain tests were performed and significant gear stress and noise reductions were achieved.

  9. A promising structure for fabricating high strength and high electrical conductivity copper alloys

    PubMed Central

    Li, Rengeng; Kang, Huijun; Chen, Zongning; Fan, Guohua; Zou, Cunlei; Wang, Wei; Zhang, Shaojian; Lu, Yiping; Jie, Jinchuan; Cao, Zhiqiang; Li, Tingju; Wang, Tongmin

    2016-01-01

    To address the trade-off between strength and electrical conductivity, we propose a strategy: introducing precipitated particles into a structure composed of deformation twins. A Cu-0.3%Zr alloy was designed to verify our strategy. Zirconium was dissolved into a copper matrix by solution treatment prior to cryorolling and precipitated in the form of Cu5Zr from copper matrix via a subsequent aging treatment. The microstructure evolutions of the processed samples were investigated by transmission electron microscopy and X-ray diffraction analysis, and the mechanical and physical behaviours were evaluated through tensile and electrical conductivity tests. The results demonstrated that superior tensile strength (602.04 MPa) and electrical conductivity (81.4% IACS) was achieved. This strategy provides a new route for balancing the strength and electrical conductivity of copper alloys, which can be developed for large-scale industrial application. PMID:26856764

  10. A promising structure for fabricating high strength and high electrical conductivity copper alloys.

    PubMed

    Li, Rengeng; Kang, Huijun; Chen, Zongning; Fan, Guohua; Zou, Cunlei; Wang, Wei; Zhang, Shaojian; Lu, Yiping; Jie, Jinchuan; Cao, Zhiqiang; Li, Tingju; Wang, Tongmin

    2016-02-09

    To address the trade-off between strength and electrical conductivity, we propose a strategy: introducing precipitated particles into a structure composed of deformation twins. A Cu-0.3%Zr alloy was designed to verify our strategy. Zirconium was dissolved into a copper matrix by solution treatment prior to cryorolling and precipitated in the form of Cu5Zr from copper matrix via a subsequent aging treatment. The microstructure evolutions of the processed samples were investigated by transmission electron microscopy and X-ray diffraction analysis, and the mechanical and physical behaviours were evaluated through tensile and electrical conductivity tests. The results demonstrated that superior tensile strength (602.04 MPa) and electrical conductivity (81.4% IACS) was achieved. This strategy provides a new route for balancing the strength and electrical conductivity of copper alloys, which can be developed for large-scale industrial application.

  11. A promising structure for fabricating high strength and high electrical conductivity copper alloys.

    PubMed

    Li, Rengeng; Kang, Huijun; Chen, Zongning; Fan, Guohua; Zou, Cunlei; Wang, Wei; Zhang, Shaojian; Lu, Yiping; Jie, Jinchuan; Cao, Zhiqiang; Li, Tingju; Wang, Tongmin

    2016-01-01

    To address the trade-off between strength and electrical conductivity, we propose a strategy: introducing precipitated particles into a structure composed of deformation twins. A Cu-0.3%Zr alloy was designed to verify our strategy. Zirconium was dissolved into a copper matrix by solution treatment prior to cryorolling and precipitated in the form of Cu5Zr from copper matrix via a subsequent aging treatment. The microstructure evolutions of the processed samples were investigated by transmission electron microscopy and X-ray diffraction analysis, and the mechanical and physical behaviours were evaluated through tensile and electrical conductivity tests. The results demonstrated that superior tensile strength (602.04 MPa) and electrical conductivity (81.4% IACS) was achieved. This strategy provides a new route for balancing the strength and electrical conductivity of copper alloys, which can be developed for large-scale industrial application. PMID:26856764

  12. Effects of atamp-charging coke making on strength and high temperature thermal properties of coke.

    PubMed

    Zhang, Yaru; Bai, Jinfeng; Xu, Jun; Zhong, Xiangyun; Zhao, Zhenning; Liu, Hongchun

    2013-12-01

    The stamp-charging coke making process has some advantages of improving the operation environment, decreasing fugitive emission, higher gas collection efficiency as well as less environmental pollution. This article describes the different structure strength and high temperature thermal properties of 4 different types of coke manufactured using a conventional coking process and the stamp-charging coke making process. The 4 kinds of cokes were prepared from the mixture of five feed coals blended by the petrography blending method. The results showed that the structure strength indices of coke prepared using the stamp-charging coke method increase sharply. In contrast with conventional coking process, the stamp-charging process improved the coke strength after reaction but had little impact on the coke reactivity index.

  13. Carbon nanotube yarns with high tensile strength made by a twisting and shrinking method.

    PubMed

    Liu, Kai; Sun, Yinghui; Zhou, Ruifeng; Zhu, Hanyu; Wang, Jiaping; Liu, Liang; Fan, Shoushan; Jiang, Kaili

    2010-01-29

    We report a simple and continuous spinning method that combines twisting and shrinking processes to produce carbon nanotube yarns. In this method, a yarn freshly spun from a super-aligned carbon nanotube array is first twisted and then passes through a volatile solvent for shrinking. The as-produced yarn consists of densely packed carbon nanotubes, and thus has a tensile strength up to about 1 GPa. The tensile strength depends on the diameter and the twisting angle of the yarn. Different kinds of solvents, such as water, ethanol, and acetone, are used to shrink the twisted yarns, and acetone shows the best shrinking effect. The origin of the solvent shrinking effect is investigated. Our method is favorable for continuous mass production of high strength carbon nanotube yarns with a wide range of diameters, especially ultra-thin yarns. PMID:20009208

  14. High Tensile Strength Amalgams for In-Space Fabrication and Repair

    NASA Technical Reports Server (NTRS)

    Grugel, Richard N.

    2006-01-01

    Amalgams are well known for their use in dental practice as a tooth filling material. They have a number of useful attributes that include room temperature fabrication, corrosion resistance, dimensional stability, and very good compressive strength. These properties well serve dental needs but, unfortunately, amalgams have extremely poor tensile strength, a feature that severely limits other potential applications. Improved material properties (strength and temperature) of amalgams may have application to the freeform fabrication of repairs or parts that might be necessary during an extended space mission. Advantages would include, but are not limited to: the ability to produce complex parts, a minimum number of processing steps, minimum crew interaction, high yield - minimum wasted material, reduced gravity compatibility, minimum final finishing, safety, and minimum power consumption. The work presented here shows how the properties of amalgams can be improved by changing particle geometries in conjunction with novel engineering metals.

  15. High Tensile Strength Amalgams for In-Space Repair and Fabrication

    NASA Technical Reports Server (NTRS)

    Grugel, R. N.

    2005-01-01

    Amalgams are defined as an alloy of mercury with one or more other metals. These, along with those based on gallium (also liquid at near room temperature), are widely used in dental practice as a tooth filling material. Amalgams have a number of useful attributes that indude room temperature compounding. corrosion resistance, dimensional stability, and good compressive strength. These properties well serve dental needs but, unfortunately, amalgams have extremely poor tensile strength, a feature that severely limits their applications. The work presented here demonstrates how, by modifying particle geometry, the tensile strength of amalgams can be increased and thus extending the range of potential applications. This is relevant to, for example, the freeform fabrication of replacement parts that might be necessary during an extended space mission. Advantages, i.e. Figures-of-Merit. include the ability to produce complex parts, minimum crew interaction, high yield - minimum wasted material, reduced gravity compatibility, minimum final finishing, safety, and minimum power consumption.

  16. Structural optimization of 3D-printed synthetic spider webs for high strength

    NASA Astrophysics Data System (ADS)

    Qin, Zhao; Compton, Brett G.; Lewis, Jennifer A.; Buehler, Markus J.

    2015-05-01

    Spiders spin intricate webs that serve as sophisticated prey-trapping architectures that simultaneously exhibit high strength, elasticity and graceful failure. To determine how web mechanics are controlled by their topological design and material distribution, here we create spider-web mimics composed of elastomeric filaments. Specifically, computational modelling and microscale 3D printing are combined to investigate the mechanical response of elastomeric webs under multiple loading conditions. We find the existence of an asymptotic prey size that leads to a saturated web strength. We identify pathways to design elastomeric material structures with maximum strength, low density and adaptability. We show that the loading type dictates the optimal material distribution, that is, a homogeneous distribution is better for localized loading, while stronger radial threads with weaker spiral threads is better for distributed loading. Our observations reveal that the material distribution within spider webs is dictated by the loading condition, shedding light on their observed architectural variations.

  17. Structural optimization of 3D-printed synthetic spider webs for high strength.

    PubMed

    Qin, Zhao; Compton, Brett G; Lewis, Jennifer A; Buehler, Markus J

    2015-01-01

    Spiders spin intricate webs that serve as sophisticated prey-trapping architectures that simultaneously exhibit high strength, elasticity and graceful failure. To determine how web mechanics are controlled by their topological design and material distribution, here we create spider-web mimics composed of elastomeric filaments. Specifically, computational modelling and microscale 3D printing are combined to investigate the mechanical response of elastomeric webs under multiple loading conditions. We find the existence of an asymptotic prey size that leads to a saturated web strength. We identify pathways to design elastomeric material structures with maximum strength, low density and adaptability. We show that the loading type dictates the optimal material distribution, that is, a homogeneous distribution is better for localized loading, while stronger radial threads with weaker spiral threads is better for distributed loading. Our observations reveal that the material distribution within spider webs is dictated by the loading condition, shedding light on their observed architectural variations. PMID:25975372

  18. Nonlinear finite element analysis of high-strength concrete columns and experimental verification

    NASA Astrophysics Data System (ADS)

    Lu, Xilin; Chen, Shaolin

    2008-03-01

    This paper describes a nonlinear finite element (FE) analysis of high strength concrete (HSC) columns, and verifies the results through laboratory experiments. First, a cyclically lateral loading test on nine cantilever column specimens of HSC is described and a numerical simulation is presented to verify the adopted FE models. Next, based on the FE model for specimen No.6, numerical simulations for 70 cases, in which different concrete strengths, stirrup ratios and axial load ratios are considered, are presented to explore the effect of these parameters on the behavior of the HSC columns, and to check the rationality of requirements for these columns specified in the China Code for Seismic Design of Buildings ( GB 50011-2001). In addition, three cases with different stirrup strengths are analyzed to investigate their effect on the behavior of HSC columns. Finally, based on the numerical results some conclusions are presented.

  19. Structural optimization of 3D-printed synthetic spider webs for high strength

    PubMed Central

    Qin, Zhao; Compton, Brett G.; Lewis, Jennifer A.; Buehler, Markus J.

    2015-01-01

    Spiders spin intricate webs that serve as sophisticated prey-trapping architectures that simultaneously exhibit high strength, elasticity and graceful failure. To determine how web mechanics are controlled by their topological design and material distribution, here we create spider-web mimics composed of elastomeric filaments. Specifically, computational modelling and microscale 3D printing are combined to investigate the mechanical response of elastomeric webs under multiple loading conditions. We find the existence of an asymptotic prey size that leads to a saturated web strength. We identify pathways to design elastomeric material structures with maximum strength, low density and adaptability. We show that the loading type dictates the optimal material distribution, that is, a homogeneous distribution is better for localized loading, while stronger radial threads with weaker spiral threads is better for distributed loading. Our observations reveal that the material distribution within spider webs is dictated by the loading condition, shedding light on their observed architectural variations. PMID:25975372

  20. Sliding wear, toughness and microstructural relationships in high strength Fe/Cr/C experimental steels

    SciTech Connect

    Salesky, W.J.

    1980-06-01

    Hardness has been believed to be the major parameter influencing wear resistance of materials. Recently, it was suggested that combinations of high strength and toughness may lead to optimum wear resistance. It is known that the martensite transformation can be exploited to provide a variety of strength-toughness combinations. Small additions of Mn or Ni to the Fe/4Cr/.3C martensitic alloys have been shown to increase toughness while maintaining strength via increasing the volume fraction of retained austenite. An investigation of the relationships between microstructure, toughness, and sliding wear resistance for these experimental alloys is reported. Comparative studies were performed on several industrial alloys to provide a practical basis for comparison of these medium carbon experimental steels.

  1. High-Strength Composite Fabric Tested at Structural Benchmark Test Facility

    NASA Technical Reports Server (NTRS)

    Krause, David L.

    2002-01-01

    Large sheets of ultrahigh strength fabric were put to the test at NASA Glenn Research Center's Structural Benchmark Test Facility. The material was stretched like a snare drum head until the last ounce of strength was reached, when it burst with a cacophonous release of tension. Along the way, the 3-ft square samples were also pulled, warped, tweaked, pinched, and yanked to predict the material's physical reactions to the many loads that it will experience during its proposed use. The material tested was a unique multi-ply composite fabric, reinforced with fibers that had a tensile strength eight times that of common carbon steel. The fiber plies were oriented at 0 and 90 to provide great membrane stiffness, as well as oriented at 45 to provide an unusually high resistance to shear distortion. The fabric's heritage is in astronaut space suits and other NASA programs.

  2. Metallurgical and mechanical properties of laser welded high strength low alloy steel.

    PubMed

    Oyyaravelu, Ramachandran; Kuppan, Palaniyandi; Arivazhagan, Natarajan

    2016-05-01

    The study aimed at investigating the microstructure and mechanical properties of Neodymium-Doped Yttrium Aluminum Garnet (Nd:YAG) laser welded high strength low alloy (HSLA) SA516 grade 70 boiler steel. The weld joint for a 4 mm thick plate was successfully produced using minimum laser power of 2 kW by employing a single pass without any weld preheat treatment. The micrographs revealed the presence of martensite phase in the weld fusion zone which could be due to faster cooling rate of the laser weldment. A good correlation was found between the microstructural features of the weld joints and their mechanical properties. The highest hardness was found to be in the fusion zone of cap region due to formation of martensite and also enrichment of carbon. The hardness results also showed a narrow soft zone at the heat affected zone (HAZ) adjacent to the weld interface, which has no effect on the weld tensile strength. The yield strength and ultimate tensile strength of the welded joints were 338 MPa and 549 MPa, respectively, which were higher than the candidate metal. These tensile results suggested that the laser welding process had improved the weld strength even without any weld preheat treatment and also the fractography of the tensile fractured samples showed the ductile mode of failure. PMID:27222751

  3. A study on high strength concrete prepared with large volumes of low calcium fly ash

    SciTech Connect

    Poon, C.S.; Lam, L.; Wong, Y.L.

    2000-03-01

    This paper presents the results of a laboratory study on high strength concrete prepared with large volumes of low calcium fly ash. The parameters studied included compressive strength, heat of hydration, chloride diffusivity, degree of hydration, and pore structures of fly ash/cement concrete and corresponding pastes. The experimental results showed that concrete with a 28-day compressive strength of 80 MPA could be obtained with a water-to-binder (w/b) ratio of 0.24, with a fly ash content of 45%. Such concrete has lower heat of hydration and chloride diffusivity than the equivalent plain cement concrete or concrete prepared with lower fly ash contents. The test results showed that at lower w/b ratios, the contribution to strength by the fly ash was higher than in the mixes prepared with higher w/b ratios. The study also quantified the reaction rates of cement and fly ash in the cementitious materials. The results demonstrated the dual effects of fly ash in concrete: (1) act as a micro-aggregate and (2) being a pozzolana. It was also noted that the strength contribution of fly ash in concrete was better than in the equivalent cement/fly ash pastes suggesting the fly ash had improved the interfacial bond between the past and the aggregates in the concrete. Such an improvement was also reflected in the results of the mercury intrusion porosimetry (MIP) test.

  4. Metallurgical and mechanical properties of laser welded high strength low alloy steel

    PubMed Central

    Oyyaravelu, Ramachandran; Kuppan, Palaniyandi; Arivazhagan, Natarajan

    2016-01-01

    The study aimed at investigating the microstructure and mechanical properties of Neodymium-Doped Yttrium Aluminum Garnet (Nd:YAG) laser welded high strength low alloy (HSLA) SA516 grade 70 boiler steel. The weld joint for a 4 mm thick plate was successfully produced using minimum laser power of 2 kW by employing a single pass without any weld preheat treatment. The micrographs revealed the presence of martensite phase in the weld fusion zone which could be due to faster cooling rate of the laser weldment. A good correlation was found between the microstructural features of the weld joints and their mechanical properties. The highest hardness was found to be in the fusion zone of cap region due to formation of martensite and also enrichment of carbon. The hardness results also showed a narrow soft zone at the heat affected zone (HAZ) adjacent to the weld interface, which has no effect on the weld tensile strength. The yield strength and ultimate tensile strength of the welded joints were 338 MPa and 549 MPa, respectively, which were higher than the candidate metal. These tensile results suggested that the laser welding process had improved the weld strength even without any weld preheat treatment and also the fractography of the tensile fractured samples showed the ductile mode of failure. PMID:27222751

  5. Metallurgical and mechanical properties of laser welded high strength low alloy steel.

    PubMed

    Oyyaravelu, Ramachandran; Kuppan, Palaniyandi; Arivazhagan, Natarajan

    2016-05-01

    The study aimed at investigating the microstructure and mechanical properties of Neodymium-Doped Yttrium Aluminum Garnet (Nd:YAG) laser welded high strength low alloy (HSLA) SA516 grade 70 boiler steel. The weld joint for a 4 mm thick plate was successfully produced using minimum laser power of 2 kW by employing a single pass without any weld preheat treatment. The micrographs revealed the presence of martensite phase in the weld fusion zone which could be due to faster cooling rate of the laser weldment. A good correlation was found between the microstructural features of the weld joints and their mechanical properties. The highest hardness was found to be in the fusion zone of cap region due to formation of martensite and also enrichment of carbon. The hardness results also showed a narrow soft zone at the heat affected zone (HAZ) adjacent to the weld interface, which has no effect on the weld tensile strength. The yield strength and ultimate tensile strength of the welded joints were 338 MPa and 549 MPa, respectively, which were higher than the candidate metal. These tensile results suggested that the laser welding process had improved the weld strength even without any weld preheat treatment and also the fractography of the tensile fractured samples showed the ductile mode of failure.

  6. High-Strength Low-Alloy (HSLA) Mg-Zn-Ca Alloys with Excellent Biodegradation Performance

    NASA Astrophysics Data System (ADS)

    Hofstetter, J.; Becker, M.; Martinelli, E.; Weinberg, A. M.; Mingler, B.; Kilian, H.; Pogatscher, S.; Uggowitzer, P. J.; Löffler, J. F.

    2014-04-01

    This article deals with the development of fine-grained high-strength low-alloy (HSLA) magnesium alloys intended for use as biodegradable implant material. The alloys contain solely low amounts of Zn and Ca as alloying elements. We illustrate the development path starting from the high-Zn-containing ZX50 (MgZn5Ca0.25) alloy with conventional purity, to an ultrahigh-purity ZX50 modification, and further to the ultrahigh-purity Zn-lean alloy ZX10 (MgZn1Ca0.3). It is shown that alloys with high Zn-content are prone to biocorrosion in various environments, most probably because of the presence of the intermetallic phase Mg6Zn3Ca2. A reduction of the Zn content results in (Mg,Zn)2Ca phase formation. This phase is less noble than the Mg-matrix and therefore, in contrast to Mg6Zn3Ca2, does not act as cathodic site. A fine-grained microstructure is achieved by the controlled formation of fine and homogeneously distributed (Mg,Zn)2Ca precipitates, which influence dynamic recrystallization and grain growth during hot forming. Such design scheme is comparable to that of HSLA steels, where low amounts of alloying elements are intended to produce a very fine dispersion of particles to increase the material's strength by refining the grain size. Consequently our new, ultrapure ZX10 alloy exhibits high strength (yield strength R p = 240 MPa, ultimate tensile strength R m = 255 MPa) and simultaneously high ductility (elongation to fracture A = 27%), as well as low mechanical anisotropy. Because of the anodic nature of the (Mg,Zn)2Ca particles used in the HSLA concept, the in vivo degradation in a rat femur implantation study is very slow and homogeneous without clinically observable hydrogen evolution, making the ZX10 alloy a promising material for biodegradable implants.

  7. Springback analysis for the stamping of an automotive part with high strength steel sheet

    NASA Astrophysics Data System (ADS)

    Hung, Tzu-Hao; Tsai, Heng-Kuang; Chang, Chih-Kai; Hsu, Yu-Hung; Chen, Fuh-Kuo; Chung, Kuo-Hsin

    2013-05-01

    The study of springback analysis of 440MPa high strength steel is investigated in this paper. Because of the springback phenomenon is related to the material properties and the deformation mechanism during the forming process, the material properties of 440MPa high strength steel are studied at first. The material properties of 440MPa high strength steel are obtained by conducting cyclic uniaxial tension-compression tests with different strain ranges. In order to apply the material properties obtained from the experiments to the finite element analysis, the material constants required in the Yoshida-Uemori model (Y-U model) with the Bauschinger effect considered are established. For realizing the springback characteristics of 440MPa high strength steel, the U-hat draw-bending and V-shape bending are examined by the finite element analysis. From the simulation results, it finds that the side wall curl phenomenon occurs in the U-hat drawbending and the springback phenomenon appears in the V-shape bending. Moreover, it also shows that the side wall curl phenomenon and springback phenomenon are more obvious in the finite element simulations with the Bauschinger effect considered. Finally, the validation of springback prediction is performed by stamping an engine hood reinforcement with 440MPa high strength steel sheet. From the stamping results, it shows that the simulation results of springback prediction are in a well agreement to the production part data. It also finds that the springback predictions are more accurate by the finite element simulations with the use of the Y-U model. It is also found that for a stamping part which is subjected to a reversed tension-compression deformation in the forming process, the occurrence of the Bauschinger effect is obvious. It is also concluded that the accuracy of springback prediction can be much improved by the use of material model with the Bauschinger effect considered.

  8. Kinematic hardening in creep of Zircaloy

    NASA Astrophysics Data System (ADS)

    Sedláček, Radan; Deuble, Dietmar

    2016-10-01

    Results of biaxial creep tests with stress changes on Zircaloy-2 tube samples are presented. A Hollomon-type viscoplastic strain hardening model is extended by the Armstrong-Frederic nonlinear kinematic hardening law, resulting in a mixed (i.e. isotropic and kinematic) strain hardening model. The creep tests with stress changes and similar tests published in the literature are simulated by the models. It is shown that introduction of the kinematic strain hardening in the viscoplastic strain hardening model is sufficient to describe the creep transients following stress drops, stress reversals and stress removals.

  9. Anisotropic hardening model based on non-associated flow rule and combined nonlinear kinematic hardening for sheet materials

    NASA Astrophysics Data System (ADS)

    Taherizadeh, Aboozar; Green, Daniel E.; Yoon, Jeong W.

    2013-12-01

    A material model for more effective analysis of plastic deformation of sheet materials is presented in this paper. The model is capable of considering the following aspects of plastic deformation behavior of sheet materials: the anisotropy in yielding stresses in different directions by using a quadratic yield function (based on Hill's 1948 model and stress ratios), the anisotropy in work hardening by introducing non-constant flow stress hardening in different directions, the anisotropy in plastic strains in different directions by using a quadratic plastic potential function and non-associated flow rule (based on Hill's 1948 model and plastic strain ratios, r-values), and finally some of the cyclic hardening phenomena such as Bauschinger's effect and transient behavior for reverse loading by using a coupled nonlinear kinematic hardening (so-called Armstrong-Frederick-Chaboche model). Basic fundamentals of the plasticity of the model are presented in a general framework. Then, the model adjustment procedure is derived for the plasticity formulations. Also, a generic numerical stress integration procedure is developed based on backward-Euler method (so-called multi-stage return mapping algorithm). Different aspects of the model are verified for DP600 steel sheet. Results show that the new model is able to predict the sheet material behavior in both anisotropic hardening and cyclic hardening regimes more accurately. By featuring the above-mentioned facts in the presented constitutive model, it is expected that more accurate results can be obtained by implementing this model in computational simulations of sheet material forming processes. For instance, more precise results of springback prediction of the parts formed from highly anisotropic hardened materials or that of determining the forming limit diagrams is highly expected by using the developed material model.

  10. Burst Strength of Tubing and Casing Based on Twin Shear Unified Strength Theory

    PubMed Central

    Lin, Yuanhua; Deng, Kuanhai; Sun, Yongxing; Zeng, Dezhi; Liu, Wanying; Kong, Xiangwei; Singh, Ambrish

    2014-01-01

    The internal pressure strength of tubing and casing often cannot satisfy the design requirements in high pressure, high temperature and high H2S gas wells. Also, the practical safety coefficient of some wells is lower than the design standard according to the current API 5C3 standard, which brings some perplexity to the design. The ISO 10400: 2007 provides the model which can calculate the burst strength of tubing and casing better than API 5C3 standard, but the calculation accuracy is not desirable because about 50 percent predictive values are remarkably higher than real burst values. So, for the sake of improving strength design of tubing and casing, this paper deduces the plastic limit pressure of tubing and casing under internal pressure by applying the twin shear unified strength theory. According to the research of the influence rule of yield-to-tensile strength ratio and mechanical properties on the burst strength of tubing and casing, the more precise calculation model of tubing-casing's burst strength has been established with material hardening and intermediate principal stress. Numerical and experimental comparisons show that the new burst strength model is much closer to the real burst values than that of other models. The research results provide an important reference to optimize the tubing and casing design of deep and ultra-deep wells. PMID:25397886

  11. Notch fatigue behavior: Metallic glass versus ultra-high strength steel

    PubMed Central

    Wang, X. D.; Qu, R. T.; Wu, S. J.; Duan, Q. Q.; Liu, Z. Q.; Zhu, Z. W.; Zhang, H. F.; Zhang, Z. F.

    2016-01-01

    Studying the effect of notch on the fatigue behavior of structural materials is of significance for the reliability and safety designing of engineering structural components. In this work, we conducted notch fatigue experiments of two high-strength materials, i.e. a Ti32.8Zr30.2Ni5.3Cu9Be22.7 metallic glass (MG) and a 00Ni18Co15Mo8Ti ultra-high strength steel (CM400 UHSS), and compared their notch fatigue behavior. Experimental results showed that although both the strength and plasticity of the MG were much lower than those of the UHSS, the fatigue endurance limit of the notched MG approached to that of the notched UHSS, and the fatigue ratio of the notched MG was even higher. This interesting finding can be attributed to the unique shear banding mechanism of MG. It was found that during fatigue process abundant shear bands formed ahead of the notch root and in the vicinity of the crack in the notched MG, while limited plastic deformation was observed in the notched UHSS. The present results may improve the understanding on the fatigue mechanisms of high-strength materials and offer new strategies for structural design and engineering application of MG components with geometrical discontinuities. PMID:27752136

  12. Nano DCPA-whisker composites with high strength and Ca and PO(4) release.

    PubMed

    Xu, H H K; Sun, L; Weir, M D; Antonucci, J M; Takagi, S; Chow, L C; Peltz, M

    2006-08-01

    The main challenges facing composite restorations are secondary caries and bulk fracture. The objective of this study was to develop nano DCPA (dicalcium phosphate anhydrous)-whisker composites with high strength and Ca and PO(4) ion release to combat caries. Flexural strength for the nano DCPA-whisker composites at a nano DCPA:whisker mass ratio of 1:2 ranged from (148 +/- 9) MPa to (167 +/- 23) MPa, significantly higher than the (103 +/- 32) MPa of an inlay/onlay commercial control composite without Ca-PO(4) release. The nano DCPA-whisker composite released PO(4) to a concentration of (1.95 +/- 0.13) mmol/L and Ca of (0.68 +/- 0.05) mmol/L. Compared with previous conventional Ca- and PO(4)-releasing composites, the nano DCPA-whisker composites had strengths two-fold higher, and released comparable or higher levels of Ca and PO(4). In conclusion, combining nano-DCPA with whiskers yielded novel composites that released high levels of Ca and PO(4) requisite for remineralization. These high-strength composites may provide a unique combination of stress-bearing and caries-inhibiting capabilities.

  13. Nano DCPA-Whisker Composites with High Strength and Ca and PO4 Release

    PubMed Central

    Xu, H.H.K.; Sun, L.; Weir, M.D.; Antonucci, J.M.; Takagi, S.; Chow, L.C.; Peltz, M.

    2008-01-01

    The main challenges facing composite restorations are secondary caries and bulk fracture. The objective of this study was to develop nano DCPA (dicalcium phosphate anhydrous)-whisker composites with high strength and Ca and PO4 ion release to combat caries. Flexural strength for the nano DCPA-whisker composites at a nano DCPA:whisker mass ratio of 1:2 ranged from (148 ± 9) MPa to (167 ± 23) MPa, significantly higher than the (103 ± 32) MPa of an inlay/onlay commercial control composite without Ca-PO4 release. The nano DCPA-whisker composite released PO4 to a concentration of (1.95 ± 0.13) mmol/L and Ca of (0.68 ± 0.05) mmol/L. Compared with previous conventional Ca- and PO4-releasing composites, the nano DCPA-whisker composites had strengths two-fold higher, and released comparable or higher levels of Ca and PO4. In conclusion, combining nano-DCPA with whiskers yielded novel composites that released high levels of Ca and PO4 requisite for remineralization. These high-strength composites may provide a unique combination of stress-bearing and caries-inhibiting capabilities. PMID:16861289

  14. Microstructural effects on the springback of advanced high-strength steel

    NASA Astrophysics Data System (ADS)

    Gan, Wei; Babu, S. S.; Kapustka, Nick; Wagoner, Robert H.

    2006-11-01

    The application of advanced high-strength steels (AHSS) has been growing rapidly in the automotive industry. Because of their high-strength, thinner sheet metals can be used for body components to achieve both weight savings and increased safety. However, this will lead to greater springback deviation from design after the forming operation. Fundamental understanding and prediction of springback are required for springback compensation and tooling design. While various types of continuum mechanics based models have been proposed to simulate the mechanical behavior of advanced high-strength steels, few of them consider microstructural effects such as material heterogeneity. In this study, through sheet thickness strength variation has been observed in DP 780 and TRIP 780 steels. Finite-element simulation indicates that the through thickness effect (TTE) can have a significant impact on the springback behavior of these sheet metals. This is verified through our experimental work using draw-bend testing. The results suggest that microstructural effects should be considered to accurately simulate springback of AHSS. Based on these results, implications of different microstructural designs will be discussed.

  15. High-velocity frictional strength across the Tohoku-Oki megathrust determined from surface drilling torque

    NASA Astrophysics Data System (ADS)

    Ujiie, Kohtaro; Inoue, Tomoya; Ishiwata, Junya

    2016-03-01

    High-velocity frictional strength is one of the primary factors controlling earthquake faulting. The Japan Trench Fast Drilling Project drilled through the shallow plate boundary fault, where displacement was ~50 m during the 2011 Tohoku-Oki earthquake. To determine downhole frictional strength, we analyzed the surface drilling torque data acquired at rotation rates equivalent to seismic slip rates (0.8-1.3 m/s). The results show a clear contrast in high-velocity frictional strength across the plate boundary fault: the apparent friction coefficient of frontal prism sediments (hemipelagic mudstones) in the hanging wall is 0.1-0.3, while that of the underthrust sediments (mudstone, laminar pelagic claystone, and chert) in the footwall increases to 0.2-0.4. The apparent friction coefficient of the smectite-rich pelagic clay in the plate boundary fault is 0.08-0.19, which is consistent with that determined from high-velocity (1.1-1.3 m/s) friction experiments. This suggests that surface drilling torque is useful in obtaining downhole frictional strength.

  16. High Temperature Strength of YSZ Joints Brazed with Palladium Silver Copper Oxide Filler Metals

    SciTech Connect

    Darsell, Jens T.; Weil, K. Scott

    2010-06-09

    The Ag-CuOx system is being investigated as potential filler metals for use in air brazing high-temperature electrochemical devices such as solid oxide fuel cells and gas concentrators. The current study examines the effects of palladium addition on the high temperature joint strength of specimens prepared from yttria stabilized zirconia (YSZ) bars brazed with the binary Ag-CuOx, and 15Pd-Ag-CuO. It was found that while the binary Ag-CuOx system exhibits stronger room temperature strength than the 15Pd system the strength is reduced to values equivalent of the 15Pd system at 800°C. The 15Pd system exhibits a lower ambient temperature strength that is retained at 800°C. In both systems the failure mechanism at high temperature appears to be peeling of the noble metal component from the oxide phases and tearing through the noble metal phase whereas sufficient adhesion is retained at lower temperatures to cause fracture of the YSZ substrate.

  17. [The effect of daily exposure to low hardening temperature on plant vital activity].

    PubMed

    Markovskaia, E F; Sysoeva, M I; Sherudilo, E G

    2008-01-01

    Phenomenological responses of plants to daily short-term exposure to low hardening temperature was studied under chamber and field conditions. Experiments were carried out on cucumber (Cucumis sativus L.), barley (Hordeum vulgare L.), marigolds (Tagetes L.), and petunia (Petunia x hybrida) plants. The obtained data demonstrated a similar pattern of response in all studied plant species to different variants of exposure to low hardening temperature. The main features of plant response to daily short-term exposure to low hardening temperature include: a higher rate of increase in cold tolerance (cf. two- or threefold increase relative to constant low hardening temperature) that peaked on day 5 (cf. day 2 at constant low hardening temperature) and was maintained for 2 weeks (cf. 3-4 days at constant low hardening temperature); a simultaneous increase in heat tolerance (cf. twofold relative to constant low hardening temperature) maintained over a long period (cf. only in the beginning of the exposure to constant low hardening temperature); a sharp drop in the subsequent cold tolerance after plant incubation in the dark (cf. a very low decrease in cold tolerance following the exposure to constant low hardening temperature); a combination of high cold tolerance and high photochemical activity of the photosynthetic apparatus (cf. a low non-photochemical quenching at constant low hardening temperature); and the capacity to rapidly increase cold tolerance in response to repeated short-term exposures to low hardening temperature in plants grown outdoors (cf. a gradual increase after repeated exposure to constant low hardening temperature). Possible methods underlying the plant response to daily short-term exposure to low temperature are proposed.

  18. Energetic-particle synthesis of high-strength Al(O) alloys

    SciTech Connect

    Follstaedt, D.M.; Knapp, J.A.; Barbour, J.C.; Myers, S.M.; Dugger, M.T.

    1995-09-28

    High-strength Al(O) alloys, initially discovered by ion implantation, have now been produced with electron-cyclotron resonance plasma deposition and pulsed-laser deposition. The mechanical properties of these deposited alloy layers were examined with nanoindentation, and finite element modeling of the indented layer on Si substrates was used to determine yield stresses for the alloys of {approximately} 1--5 GPa. The key to these high strengths is the high density of nanometer-size {gamma}-Al{sub 2}O{sub 3} precipitates formed when high concentrations (5--30 at.%) of oxygen are introduced into aluminum as individual atoms or molecules. The strongest alloys have precipitates as small as 1 nm, implying that such small precipitates block dislocation motion. Based upon previous studies with oxygen-implanted aluminum, improved tribological properties are expected for layers made by the two new deposition methods.

  19. Biodegradability oriented treatability studies on high strength segregated wastewater of a woolen textile dyeing plant.

    PubMed

    Baban, Ahmet; Yediler, Ayfer; Ciliz, NilgunKiran; Kettrup, Antonius

    2004-11-01

    Textile dyeing and finishing industry involves considerable amount of water usage as well as polluted and highly colored wastewater discharges. Biological treatability by means of mineralization, nitrification and denitrification of high strength woolen textile dye bathes, first- and second-rinses is presented. COD fractionation study was carried out and kinetic parameters were determined. Biodegradability of organic compounds in highly loaded composite wastewater after segregation and the effluent of applied biological treatment of high strength composite wastewater were measured by determining oxygen consumption rates. The results were used in terms of assessing an alternative method for inert COD fractionation. The study implied that about 80% soluble COD, 50% color and 75% toxicity reduction were possible by single sludge biological processes. Sixteen per cent of total COD was found to be initially inert. Inert fraction was increased to 22% by production of soluble and particulate microbial products through biological treatment. PMID:15488936

  20. Temperature Dependence of Sound Velocity in High-Strength Fiber-Reinforced Plastics

    NASA Astrophysics Data System (ADS)

    Nomura, Ryuji; Yoneyama, Keiichi; Ogasawara, Futoshi; Ueno, Masashi; Okuda, Yuichi; Yamanaka, Atsuhiko

    2003-08-01

    Longitudinal sound velocity in unidirectional hybrid composites or high-strength fiber-reinforced plastics (FRPs) was measured along the fiber axis over a wide temperature range (from 77 K to 420 K). We investigated two kinds of high-strength crystalline polymer fibers, polyethylene (Dyneema) and polybenzobisoxazole (Zylon), which are known to have negative thermal expansion coefficients and high thermal conductivities along the fiber axis. Both FRPs had very high sound velocities of about 9000 m/s at low temperatures and their temperature dependences were very strong. Sound velocity monotonically decreased with increasing temperature. The temperature dependence of sound velocity was much stronger in Dyneema-FRP than in Zylon-FRP.

  1. High-strength and thermally stable bulk nanolayered composites due to twin-induced interfaces.

    PubMed

    Zheng, Shijian; Beyerlein, Irene J; Carpenter, John S; Kang, Keonwook; Wang, Jian; Han, Weizhong; Mara, Nathan A

    2013-01-01

    Bulk nanostructured metals can attribute both exceptional strength and poor thermal stability to high interfacial content, making it a challenge to utilize them in high-temperature environments. Here we report that a bulk two-phase bimetal nanocomposite synthesised via severe plastic deformation uniquely possesses simultaneous high-strength and high thermal stability. For a bimetal spacing of 10 nm, this composite achieves an order of magnitude increase in hardness of 4.13 GPa over its constituents and maintains it (4.07 GPa), even after annealing at 500 °C for 1 h. It owes this extraordinary property to an atomically well-ordered bimaterial interface that results from twin-induced crystal reorientation, persists after extreme strains and prevails over the entire bulk. This discovery proves that interfaces can be designed within bulk nanostructured composites to radically outperform previously prepared bulk nanocrystalline materials, with respect to both mechanical and thermal stability. PMID:23591863

  2. Rayleigh-Taylor stabilization by material strength at Mbar pressures

    SciTech Connect

    Park, H; Lorenz, K T; Cavallo, R M; Pollaine, S M; Prisbrey, S T; Remington, B A; Rudd, R E; Becker, R C; Bernier, J V

    2009-05-27

    Studies of solid-state material dynamics at high pressures ({approx}1 Mbar) and ultrahigh strain rates (>10{sup 6} s{sup -1}) are performed using a unique laser based, quasi-isentropic high-pressure acceleration platform. Vanadium foils with pre-imposed sinusoidal ripples are accelerated in the solid state with this ramped high pressure drive. This causes Rayleigh-Taylor (RT) instability growth at the interface, where the rate of growth is sensitive to the solid-state material properties. The RT growth history is measured by face-on radiography using synchronized laser-driven x-ray backlighters at the Omega Laser. The experimental results are compared with 2D hydrodynamics simulations utilizing constitutive models of high pressure material strength. We find that the vanadium strength increases by a factor of 3.5-4 at peak pressure, compared to its ambient (undriven) strength. Both pressure hardening and strain rate hardening are the suggested cause for this increase in strength. An analysis treating strength as an effective lattice viscosity finds that a viscosity of {approx}400 poise is required to reproduce our RT data.

  3. Consequences of heat hardening on a field fitness component in Drosophila depend on environmental temperature.

    PubMed

    Loeschcke, Volker; Hoffmann, Ary A

    2007-02-01

    Heat hardening increases thermal resistance to more extreme temperatures in the laboratory. However, heat hardening also has negative consequences, and the net benefit of hardening has not been evaluated in the field. We tested short-term heat hardening effects on the likelihood of Drosophila melanogaster to be caught at different temperatures at baits in field sites without natural resources. We predicted that hardened flies should be more frequently caught at the baits at high but not low temperatures. Under cool conditions, flies hardened at 36 degrees C, and to a lesser extent at 34 degrees C, were less frequently caught at baits than nonhardened flies a few hours after release, indicating a negative effect of hardening. In later captures, negative effects tended to disappear, particularly in males. Under warm conditions, there was an overall balance of negative and positive effects, though with a different temporal resolution. Under very hot conditions, when capture rates were low, there was a large benefit of hardening at 36 degrees C and 34 degrees C but not 33 degrees C. Finally, based on climatic records, the overall benefit of hardening in D. melanogaster is discussed as an evolved response to high temperatures occasionally experienced by organisms at some locations.

  4. Stress corrosion cracking evaluation of martensitic precipitation hardening stainless steels

    NASA Technical Reports Server (NTRS)

    Humphries, T. S.; Nelson, E. E.

    1980-01-01

    The resistance of the martensitic precipitation hardening stainless steels PH13-8Mo, 15-5PH, and 17-4PH to stress corrosion cracking was investigated. Round tensile and c-ring type specimens taken from several heats of the three alloys were stressed up to 100 percent of their yield strengths and exposed to alternate immersion in salt water, to salt spray, and to a seacoast environment. The results indicate that 15-5PH is highly resistant to stress corrosion cracking in conditions H1000 and H1050 and is moderately resistant in condition H900. The stress corrosion cracking resistance of PH13-8Mo and 17-4PH stainless steels in conditions H1000 and H1050 was sensitive to mill heats and ranged from low to high among the several heats included in the tests. Based on a comparison with data from seacoast environmental tests, it is apparent that alternate immersion in 3.5 percent salt water is not a suitable medium for accelerated stress corrosion testing of these pH stainless steels.

  5. Stress corrosion cracking of several high strength ferrous and nickel alloys

    NASA Technical Reports Server (NTRS)

    Nelson, E. E.

    1971-01-01

    The stress corrosion cracking resistance of several high strength ferrous and nickel base alloys has been determined in a sodium chloride solution. Results indicate that under these test conditions Multiphase MP35N, Unitemp L605, Inconel 718, Carpenter 20Cb and 20Cb-3 are highly resistant to stress corrosion cracking. AISI 410 and 431 stainless steels, 18 Ni maraging steel (250 grade) and AISI 4130 steel are susceptible to stress corrosion cracking under some conditions.

  6. Improving UV Resistance of High Strength Fibers Used In Large Scientific Balloons

    NASA Technical Reports Server (NTRS)

    Said, M.; Gupta, A.; Seyam, A.; Mock, G.; Theyson, T.

    2004-01-01

    For the last three decades, NASA has been involved in the development of giant balloons that are capable of lifting heavy payloads of equipment (such as large telescopes and scientific instruments) to the upper atmosphere. While the use of such balloons has led to scientific discoveries, the demand for competitive science payloads and observational programs continues to rise. The NASA Balloon Program Office has entered a new phase of research to develop an Ultra Long Duration Balloon (ULDB) that will lift payloads of up to 3,600 kg to altitudes of up to 40 km. The flight duration is targeted to ranges between 30 to 100 days. Attaining these target durations requires the development of a super-pressure balloon design. The use of textile structures have already been established in these missions in the form of high strength tendons essential for the super pressure pumpkin design. Unfortunately, high strength fibers lose significant strength upon exposure to Ultra Violet (UV) radiation. Such UV degradation poses a serious challenge for the development of the ULDB. To improve the mission performance of the ULDB, new methods for protecting the tendons from the environmental effects need to be developed. NASA and NC State University College of Textiles are undertaking a research program to address these issues. Four tracks have been identified to prepare finishes that are believed to enhance the resistance of high strength fibers to UV. These tracks are: (a) self-polymerizing, (b) diffusion application, (c) polymer-filled with 30-40% UV absorber, and (d) combination of dyeing plus surface application. Four high performance fibers have been selected for this research investigation. These are Vectran (trademark), Spectra (trademark), Kevlar (trademark) and, PBO (Zylon (trademark)). This work will address the current progress of evaluating the performance of the UV finishes. This will be accomplished by comparing the tensile properties (strength, breaking elongation

  7. Radiation Hardening of Computers

    NASA Technical Reports Server (NTRS)

    Nichols, D. K.; Smith, L. S.; Zoutendyk, J. A.; Giddings, A. E.; Hewlett, F. W.; Treece, R. K.

    1986-01-01

    Single-event upsets reduced by use of oversize transistors. Computers made less susceptible to ionizing radiation by replacing bipolar integrated circuits with properly designed, complementary metaloxide-semiconductor (CMOS) circuits. CMOS circuit chips made highly resistant to single-event upset (SEU), especially when certain feedback resistors are incorporated. Redesigned chips also consume less power than original chips.

  8. Hydration and strength development of binder based on high-calcium oil shale fly ash

    SciTech Connect

    Freidin, C.

    1998-06-01

    The properties of high-calcium oil shale fly ash and low-calcium coal fly ash, which are produced in Israeli power stations, were investigated. High-calcium oil shale fly ash was found to contain a great amount of CaO{sub free} and SO{sub 3} in the form of lime and anhydrite. Mixtures of high-calcium oil shale fly ash and low-calcium coal fly ash, termed fly ash binder, were shown to cure and have improved strength. The influence of the composition and curing conditions on the compressive strength of fly ash binders was examined. The microstructure and the composition of fly ash binder after curing and long-term exposure in moist air, water and open air conditions were studied. It was determined that ettringite is the main variable in the strength and durability of cured systems. The positive effect of calcium silicate hydrates, CSH, which are formed by interaction of high-calcium oil shale fly ash and low-calcium coal fly ash components, on the carbonation and dehydration resistance of fly ash binder in open air is pronounced. It was concluded that high-calcium oil shale fly ash with high CaO{sub free} and SO{sub 3} content can be used as a binder for building products.

  9. [Anaerobic membrane bioreactors for treating agricultural and food processing wastewater at high strength].

    PubMed

    Wei, Yuan-Song; Yu, Da-Wei; Cao, Lei

    2014-04-01

    As the second largest amounts of COD discharged in 41 kinds of industrial wastewater, it is of great urgency for the agricultural and food processing industry to control water pollution and reduce pollutants. Generally the agricultural and food processing industrial wastewater with high strength COD of 8 000-30 000 mg x L(-1), is mainly treated with anaerobic and aerobic processes in series, but which exists some issues of long process, difficult maintenance and high operational costs. Through coupling anaerobic digestion and membrane separation together, anaerobic membrane bioreactor (AnMBR) has typical advantages of high COD removal efficiency (92%-99%), high COD organic loading rate [2.3-19.8 kg x (m3 x d)(-1)], little sludge discharged (SRT > 40 d) and low cost (HRT of 8-12 h). According to COD composition of high strength industrial wastewater, rate-limiting step of methanation could be either hydrolysis and acidification or methanogenesis. Compared with aerobic membrane bioreactor (MBR), membrane fouling of AnMBR is more complicated in characterization and more difficult in control. Measures for membrane fouling control of AnMBR are almost the same as those of MBR, including cross flow, air sparging and membrane relaxation. For meeting discharging standard of food processing wastewater with high strength, AnMBR is a promising technology with very short process, by enhancing COD removal efficiency, controlling membrane fouling and improving energy recovery.

  10. In situ nanoindentation study on plasticity and work hardening in aluminium with incoherent twin boundaries.

    PubMed

    Bufford, D; Liu, Y; Wang, J; Wang, H; Zhang, X

    2014-01-01

    Nanotwinned metals have been the focus of intense research recently, as twin boundaries may greatly enhance mechanical strength, while maintaining good ductility, electrical conductivity and thermal stability. Most prior studies have focused on low stacking-fault energy nanotwinned metals with coherent twin boundaries. In contrast, the plasticity of twinned high stacking-fault energy metals, such as aluminium with incoherent twin boundaries, has not been investigated. Here we report high work hardening capacity and plasticity in highly twinned aluminium containing abundant Σ3{112} incoherent twin boundaries based on in situ nanoindentation studies in a transmission electron microscope and corresponding molecular dynamics simulations. The simulations also reveal drastic differences in deformation mechanisms between nanotwinned copper and twinned aluminium ascribed to stacking-fault energy controlled dislocation-incoherent twin boundary interactions. This study provides new insight into incoherent twin boundary-dominated plasticity in high stacking-fault energy twinned metals. PMID:25204688

  11. Time-Dependent Behavior of High-Strength Kevlar and Vectran Webbing

    NASA Technical Reports Server (NTRS)

    Jones, Thomas C.; Doggett, William R.

    2014-01-01

    High-strength Kevlar and Vectran webbings are currently being used by both NASA and industry as the primary load-bearing structure in inflatable space habitation modules. The time-dependent behavior of high-strength webbing architectures is a vital area of research that is providing critical material data to guide a more robust design process for this class of structures. This paper details the results of a series of time-dependent tests on 1-inch wide webbing including an initial set of comparative tests between specimens that underwent realtime and accelerated creep at 65 and 70% of their ultimate tensile strength. Variability in the ultimate tensile strength of the webbings is investigated and compared with variability in the creep life response. Additional testing studied the effects of load and displacement rate, specimen length and the time-dependent effects of preconditioning the webbings. The creep test facilities, instrumentation and test procedures are also detailed. The accelerated creep tests display consistently longer times to failure than their real-time counterparts; however, several factors were identified that may contribute to the observed disparity. Test setup and instrumentation, grip type, loading scheme, thermal environment and accelerated test postprocessing along with material variability are among these factors. Their effects are discussed and future work is detailed for the exploration and elimination of some of these factors in order to achieve a higher fidelity comparison.

  12. High Strength and Compatible Aluminum Alloy for Hydrogen-Peroxide Fuel Tanks

    NASA Technical Reports Server (NTRS)

    Lee, Jonathan A.

    2004-01-01

    This paper describes the development of a new high strength and Hydrogen Peroxide (HP) propellant compatible aluminum alloy for NASA Hyper-X vehicle's fuel tanks and structures. The tensile strength of the new alloy is more than 3 times stronger than the conventional 5254 alloy while it still maintains HP compatibility similar to 5254 (Class 1 category). The alloy development strategy consists of selecting certain rare earth and transition metals, with unique electrochemical properties, that will not act as catalysts to decompose liquid HP at the atomic level. Such elements will added to the aluminum alloy and the mixture will be cast and rolled into thin sheet metals. Test coupons are machined from sheet metals for HP long-term exposure testing and mechanical properties testing. In addition, the ability to weld the new alloy using Friction Stir Welding has also been explored. Currently, aluminum alloy 5254 is the state-of-the-art material for HP storage, but its yield strength is very low (420 ksi) and may not be suitable for the development of light-weight fuel tanks for Hyper-X vehicles. The new high strength and HP compatible alloy could represent an enabling material technology for NASA's Hyper-X vehicles, where flight weight reduction is a critical requirement. These X-planes are currently under studied as air-breathing hypersonic research vehicles featuring a lifting body configuration with a Rocket Based Combined Cycle (RBCC) engine system.

  13. Improved Tensile Adhesion Specimens for High Strength Epoxy Systems in Aerospace Applications

    NASA Technical Reports Server (NTRS)

    Haddock, M. Reed; McLennan, Michael L.

    2000-01-01

    An improved tensile adhesion button has been designed and tested that results in higher measured tensile adhesion strength while providing increased capability for testing high strength epoxy adhesive systems. The best attributes of two well-established tensile button designs were combined and refined into an optimized tensile button. The most significant design change to the tensile button was to improve alignment of the bonded tensile button specimens during tensile testing by changing the interface between the tensile button and the tensile test machine. The established or old button design uses a test fixture that pulls from a grooved annulus or anvil head while the new button design pulls from a threaded hole in the centerline of the button. Finite element (FE) analysis showed that asymmetric loading of the established anvil head tensile button significantly increases the stress concentration in the adhesive, causing failure at lower tensile test loads. The new tensile button was designed to eliminate asymmetric loading and eliminate misalignment sensitivity. Enhanced alignment resulted in improved tensile adhesion strength measurement up to 13.8 MPa (2000psi) over the established button design. Another design change increased the capability of the button by increasing the threaded hole diameter allowing it to test high strength epoxy systems up to 85 MPa(less than 12,000 psi). The improved tensile button can be used in button- to-button or button-to-panel configurations.

  14. Study on technology of high-frequency pulsed magnetic field strength measurement.

    PubMed

    Chen, Yi-Mei; Liu, Zhi-Peng; Yin, Tao

    2012-01-01

    High-frequency transient weak magnetic field is always involved in researches about biomedical engineering field while common magnetic-field sensors cannot work properly at frequencies as high as MHz. To measure the value of MHz-level weak pulsed magnetic-field strength accurately, this paper designs a measurement and calibration method for pulsed magnetic-field. In this paper, a device made of Nonferromagnetic material was independently designed and applied to pulsed magnetic field measurement. It held an accurately relative position between the magnetic field generating coil and the detecting coil. By applying a sinusoidal pulse to the generator, collecting the induced electromotive force of the detector, the final magnetic field strength was worked out through algorithms written in Matlab according to Faraday's Law. Experiments were carried out for measurement and calibration. Experiments showed that, under good stability and consistency, accurate measurement of magnetic-field strength of a sinepulse magnetic-field can be achieved, with frequency at 0.5, 1, 1.5 MHz and strength level at micro-Tesla. Calibration results carried out a measuring relative error about 2.5%.

  15. Hugoniot-measurements of room- and high-temperature metals for study of EOS and strength

    NASA Astrophysics Data System (ADS)

    Mashimo, Tsutomu; Gomoto, Yuya; Takashima, Hideyuki; Murai, Mitsuru; Yoshiasa, Akira

    2011-06-01

    Pressure calibration in static high-pressure experiments has been undertaken on the basis of the EOS derived from the Hugoniot compression curves of metals (Au, Pt, Cu, W, etc.), MgO, etc. To obtain the strict EOS at room- and high-temperatures, we need to precisely measure the Hugoniot data, and access the strength and Grüneisen parameter under shock compression. If the Hugoniot data of elevated temperature samples are measured, the high-temperature EOS can be accurately derived, and the Grüneisen parameter can be directly discussed. The strength might decrease at high temperature. The Hugoniot-measurement experiments have been performed on single crystal Au, oxygen-free Cu, forged Ta and W by a streak photographic system equipped with a powder gun and two-stage light gas gun in the pressure range up to >200 GPa. In addition, the Hugoniot-measurement experiment of the elevated temperature samples was started using high-frequency heating on W, Au, etc. Some of the results will be presented, and the EOS and strength are discussed.

  16. Effects of high NH(+) 4 on K(+) uptake, culm mechanical strength and grain filling in wheat.

    PubMed

    Kong, Lingan; Sun, Mingze; Wang, Fahong; Liu, Jia; Feng, Bo; Si, Jisheng; Zhang, Bin; Li, Shengdong; Li, Huawei

    2014-01-01

    It is well established that a high external NH(+) 4 concentration depresses many processes in plant development, but the underlying mechanisms are still not well understood. To determine whether the negative effects of high levels of NH(+) 4 are related to competitive cation uptake, wheat was grown in a field with moderate (18 g N m(-2)) and high (30 g N m(-2)) supplies of NH(+) 4 in the presence or absence of additional K(+) (6 g K2O m(-2)) to examine culm mechanical strength, the main components of the vascular bundle, nitrogen (N) remobilization and the grain-filling rate. The results indicated that an excessive supply of NH(+) 4 significantly decreased culm mechanical strength, the cellulose and lignin contents of vascular bundles, the N remobilization efficiency (NRE) and the grain-filling rate compared with a moderate level of NH(+) 4. The additional provision of K(+) considerably alleviated these negative effects of high NH(+) 4, resulting in a 19.41-26.95% increase in culm mechanical strength during grain filling and a 34.59% increase in the NRE. An assay using the scanning ion-selective electrode technique (SIET) showed that the net rate of transmembrane K(+) influx decreased by 84.62%, and measurements using flame photometry demonstrated that the K(+) content decreased by 36.13% in wheat plants subjected to high NH(+) 4. This study indicates that the effects of high NH(+) 4 on culm mechanical strength, cellulose and lignin contents, the NRE and the grain-filling rate are probably associated with inhibition of K(+) uptake in wheat. PMID:25566278

  17. Effects of high NH+4 on K+ uptake, culm mechanical strength and grain filling in wheat

    PubMed Central

    Kong, Lingan; Sun, Mingze; Wang, Fahong; Liu, Jia; Feng, Bo; Si, Jisheng; Zhang, Bin; Li, Shengdong; Li, Huawei

    2014-01-01

    It is well established that a high external NH+4 concentration depresses many processes in plant development, but the underlying mechanisms are still not well understood. To determine whether the negative effects of high levels of NH+4 are related to competitive cation uptake, wheat was grown in a field with moderate (18 g N m−2) and high (30 g N m−2) supplies of NH+4 in the presence or absence of additional K+ (6 g K2O m−2) to examine culm mechanical strength, the main components of the vascular bundle, nitrogen (N) remobilization and the grain-filling rate. The results indicated that an excessive supply of NH+4 significantly decreased culm mechanical strength, the cellulose and lignin contents of vascular bundles, the N remobilization efficiency (NRE) and the grain-filling rate compared with a moderate level of NH+4. The additional provision of K+ considerably alleviated these negative effects of high NH+4, resulting in a 19.41–26.95% increase in culm mechanical strength during grain filling and a 34.59% increase in the NRE. An assay using the scanning ion-selective electrode technique (SIET) showed that the net rate of transmembrane K+ influx decreased by 84.62%, and measurements using flame photometry demonstrated that the K+ content decreased by 36.13% in wheat plants subjected to high NH+4. This study indicates that the effects of high NH+4 on culm mechanical strength, cellulose and lignin contents, the NRE and the grain-filling rate are probably associated with inhibition of K+ uptake in wheat. PMID:25566278

  18. Mechanism of work hardening in Hadfield manganese steel

    NASA Astrophysics Data System (ADS)

    Dastur, Y. N.; Leslie, W. C.

    1981-05-01

    When Hadfield manganese steel in the single-phase austenitic condition was strained in tension, in the temperature range - 25 to 300 °C, it exhibited jerky (serrated) flow, a negative (inverse) strain-rate dependence of flow stress and high work hardening, characteristic of dynamic strain aging. The strain rate-temperature regime of jerky flow was determined and the apparent activation energies for the appearance and disappearance of serrations were found to be 104 kJ/mol and 146 kJ/mol, respectively. The high work hardening cannot be a result of mechanical twinning because at -50 °C numerous twins were produced, but the work hardening was low and no twins were formed above 225 °C even though work hardening was high. The work hardening decreased above 300 °C because of the cessation of dynamic strain aging and increased again above 400 °C because of precipitation of carbides. An apparent activation energy of 138 kJ/mol was measured for static strain aging between 300 and 400 °C, corresponding closely to the activation energies for the disapperance of serrations and for the volume diffusion of carbon in Hadfield steel. Evidence from the present study, together with the known effect of manganese on the activity of carbon in austenite and previous internal friction studies of high-manganese steels, lead to the conclusion that dynamic strain aging, brought about by the reorientation of carbon members of C-Mn couples in the cores of dislocations, is the principal cause of rapid work hardening in Hadfield steel.

  19. Process for making a high toughness-high strength iron alloy

    NASA Technical Reports Server (NTRS)

    Stephens, J. R.; Witzke, W. R. (Inventor)

    1979-01-01

    A steel alloy is produced by a process which includes using cold rolling at room temperature and subsequent heat treatment at temperatures ranging from 500 C to 650 C. The resulting alloys exhibits excellent strength and toughness characteristics at cryogenic temperatures. This alloy consists essentially of about 10 to 16 percent by weight nickel, to about 1.0 percent by weight aluminum, and 0 to about 3 percent by weight of at least one of the following additional elements: copper, lanthanum, niobium, tantalum, titanium, vanadium, yttrium, zirconium and the rare earth metals, with the balance being essentially iron. The improved alloy possesses a fracture toughness ranging from 200 to 230 ksi sq in. and yield strengths up to 230 ksi.

  20. Temperature and strain rate effects in high strength high conductivity copper alloys tested in air

    SciTech Connect

    Edwards, D.J.

    1998-03-01

    The tensile properties of the three candidate alloys GlidCop{trademark} Al25, CuCrZr, and CuNiBe are known to be sensitive to the testing conditions such as strain rate and test temperature. This study was conducted on GlidCop Al25 (2 conditions) and Hycon 3HP (3 conditions) to ascertain the effect of test temperature and strain rate when tested in open air. The results show that the yield strength and elongation of the GlidCop Al25 alloys exhibit a strain rate dependence that increases with temperature. Both the GlidCop and the Hycon 3 HP exhibited an increase in strength as the strain rate increased, but the GlidCop alloys proved to be the most strain rate sensitive. The GlidCop failed in a ductile manner irrespective of the test conditions, however, their strength and uniform elongation decreased with increasing test temperature and the uniform elongation also decreased dramatically at the lower strain rates. The Hycon 3 HP alloys proved to be extremely sensitive to test temperature, rapidly losing their strength and ductility when the temperature increased above 250 C. As the test temperature increased and the strain rate decreased the fracture mode shifted from a ductile transgranular failure to a ductile intergranular failure with very localized ductility. This latter observation is based on the presence of dimples on the grain facets, indicating that some ductile deformation occurred near the grain boundaries. The material failed without any reduction in area at 450 C and 3.9 {times} 10{sup {minus}4} s{sup {minus}1}, and in several cases failed prematurely.

  1. Sleep monitoring of a six-day microcycle in strength and high-intensity training.

    PubMed

    Kölling, Sarah; Wiewelhove, Thimo; Raeder, Christian; Endler, Stefan; Ferrauti, Alexander; Meyer, Tim; Kellmann, Michael

    2016-08-01

    This study examined the effect of microcycles in eccentric strength and high-intensity interval training (HIT) on sleep parameters and subjective ratings. Forty-two well-trained athletes (mean age 23.2 ± 2.4 years) were either assigned to the strength (n = 21; mean age 23.6 ± 2.1 years) or HIT (n = 21; mean age 22.8 ± 2.6 years) protocol. Sleep monitoring was conducted with multi-sensor actigraphy (SenseWear Armband™, Bodymedia, Pittsburg, PA, USA) and sleep log for 14 days. After a five-day baseline phase, participants completed either eccentric accented strength or high-intensity interval training for six days, with two training sessions per day. This training phase was divided into two halves (part 1 and 2) for statistical analyses. A three-day post phase concluded the monitoring. The Recovery-Stress Questionnaire for Athletes was applied at baseline, end of part 2, and at the last post-day. Mood ratings were decreased during training, but returned to baseline values afterwards in both groups. Sleep parameters in the strength group remained constant over the entire process. The HIT group showed trends of unfavourable sleep during the training phase (e.g., objective sleep efficiency at part 2: mean = 83.6 ± 7.8%, F3,60 = 2.57, P = 0.06, [Formula: see text] = 0.114) and subjective improvements during the post phase for awakenings (F3,60 = 2.96, P = 0.04, [Formula: see text] = 0.129) and restfulness of sleep (F3,60 = 9.21, P < 0.001, [Formula: see text] = 0.315). Thus, the HIT protocol seems to increase higher recovery demands than strength training, and sufficient sleep time should be emphasised and monitored.

  2. Dentin bond strength after ablation using a CO2 laser operating at high pulse repetition rates

    NASA Astrophysics Data System (ADS)

    Hedayatollahnajafi, Saba; Staninec, Michal; Watanabe, Larry; Lee, Chulsung; Fried, Daniel

    2009-02-01

    Pulsed CO2 lasers show great promise for the rapid and efficient ablation of dental hard tissues. Our objective was to demonstrate that CO2 lasers operated at high repetition rates can be used for the rapid removal of dentin without excessive thermal damage and without compromising adhesion to restorative materials. Human dentin samples (3x3mm2) were rapidly ablated with a pulsed CO2 laser operating at a wavelength of 9.3-µm, pulse repetition rate of 300-Hz and an irradiation intensity of 18-J/cm2. The bond strength to composite was determined by the modified single plane shear test. There were 8 test groups each containing 10 blocks: negative control (non-irradiated non-etched), positive control (non-irradiated acid-etched), and six laser treated groups (three etched and three non-etched sets). The first and second etched and non-etched sets were ablated at a speed of 25 mm/sec and 50 mm/sec with water, respectively. The third set was also ablated at 50 mm/sec without application of water during laser irradiation. Minimal thermal damage was observed on the dentin surfaces for which water cooling was applied. Bond strengths exceeded 20 MPa for laser treated surfaces that were acid-etched after ablation (25-mm/sec: 29.9-MPa, 50-mm/sec: 21.3-MPa). The water-cooled etched laser groups all produced significantly stronger bonds than the negative control (p<0.001) and a lower bond strength than the positive control (p<0.05). These measurements demonstrate that dentin surfaces can be rapidly ablated by a CO2 lasers with minimal peripheral thermal damage. Additional studies are needed to determine if a lower bond strength than the acid-etched control samples is clinically significant where durability of these bonded restoration supersedes high bond strength.

  3. High-velocity frictional strength across the Tohoku-Oki megathrust determined from surface drilling torque

    NASA Astrophysics Data System (ADS)

    Ujiie, K.; Inoue, T.; Ishiwata, J.

    2015-12-01

    Frictional strength at seismic slip rates is a key to evaluate fault weakening and rupture propagation during earthquakes. The Japan Trench First Drilling Project (JFAST) drilled through the shallow plate-boundary thrust, where huge displacements of ~50 m occurred during the 2011 Tohoku-Oki earthquake. To determine the downhole frictional strength at drilled site (Site C0019), we analyzed surface drilling data. The equivalent slip rate estimated from the rotation rate and inner and outer radiuses of the drill bit ranges from 0.8 to 1.3 m/s. The measured torque includes the frictional torque between the drilling string and borehole wall, the viscous torque between the drilling string and seawater/drilling fluid, and the drilling torque between the drill bit and sediments. We subtracted the former two from the measured torque using the torque data during bottom-up rotating operations at several depths. Then, the shear stress was calculated from the drilling torque taking the configuration of the drill bit into consideration. The normal stress was estimated from the weight on bit data and the projected area of the drill bit. Assuming negligible cohesion, the frictional strength was obtained by dividing shear stress by normal stress. The results show a clear contrast in high-velocity frictional strength across the plate-boundary thrust: the friction coefficient of frontal prism sediments (hemipelagic mudstones) in hanging wall is 0.1-0.2, while that in subducting sediments (hemipelagic to pelagic mudstones and chert) in footwall increases to 0.2-0.4. The friction coefficient of smectite-rich pelagic clay in the plate-boundary thrust is ~0.1, which is consistent with that obtained from high-velocity (1.3 m/s) friction experiments and temperature measurements. We conclude that surface drilling torque provides useful data to obtain a continuous downhole frictional strength.

  4. A low-cost hierarchical nanostructured beta-titanium alloy with high strength

    DOE PAGES

    Devaraj, Arun; Joshi, Vineet V.; Srivastava, Ankit; Manandhar, Sandeep; Moxson, Vladimir; Duz, Volodymyr A.; Lavender, Curt

    2016-04-01

    Lightweighting of automobiles by use of novel low-cost, high strength-to-weight ratio structural materials can reduce the consumption of fossil fuels and in turn CO2 emission. Working towards this goal we achieved high strength in a low cost β-titanium alloy, Ti-1Al-8V-5Fe (Ti185), by hierarchical nanostructure consisting of homogenous distribution of micron-scale and nanoscale α-phase precipitates within the β-phase matrix. The sequence of phase transformation leading to this hierarchical nanostructure is explored using electron microscopy and atom probe tomography. Our results suggest that the high number density of nanoscale α-phase precipitates in the β-phase matrix is due to ω assisted nucleation ofmore » α resulting in high tensile strength, greater than any current commercial titanium alloy. Furthermore hierarchical nanostructured Ti185 serves as an excellent candidate for replacing costlier titanium alloys and other structural alloys for cost-effective lightweighting applications.« less

  5. Perspectives and limitations of parallel MR imaging at high field strengths.

    PubMed

    Heidemann, Robin M; Seiberlich, Nicole; Griswold, Mark A; Wohlfarth, Katrin; Krueger, Gunnar; Jakob, Peter M

    2006-05-01

    In medical magnetic resonance imaging (MRI) imaging, it is standard practice to use MR scanners with a field strength of 1.5 Tesla. Recently, an ongoing trend towards higher field strengths can be observed, with a new potential clinical standard of 3.0 Tesla. High-field MR imaging, with its intrinsic higher signal-to-noise ratio (SNR), can enable new applications for MRI in medical diagnosis, or can serve to improve existing methods. The use of high field MRI is not without its limitations, however. Besides SNR, other unwanted effects increase with a higher field strength. Without correction, these high field problems can cause a serious loss in image quality. An elegant way to address these problems is the use of parallel imaging. In many clinical applications, parallel MRI (pMRI) is part of the standard protocol, as pMRI can enhance virtually every MRI application without necessarily affecting the contrast behavior of the underlying imaging sequence. In addition to the speed advantages offered by pMRI, the capability of parallel imaging to reduce significant high field-specific problems, thereby improving image quality, will be of major importance.

  6. Analysis of local warm forming of high strength steel using near infrared ray energy

    NASA Astrophysics Data System (ADS)

    Yang, W. H.; Lee, K.; Lee, E. H.; Yang, D. Y.

    2013-12-01

    The automotive industry has been pressed to satisfy more rigorous fuel efficiency requirements to promote energy conservation, safety features and cost containment. To satisfy this need, high strength steel has been developed and used for many different vehicle parts. The use of high strength steels, however, requires careful analysis and creativity in order to accommodate its relatively high springback behavior. An innovative method, called local warm forming with near infrared ray, has been developed to help promote the use of high strength steels in sheet metal forming. For this method, local regions of the work piece are heated using infrared ray energy, thereby promoting the reduction of springback behavior. In this research, a V-bend test is conducted with DP980. After springback, the bend angles for specimens without local heating are compared to those with local heating. Numerical analysis has been performed using the commercial program, DEFORM-2D. This analysis is carried out with the purpose of understanding how changes to the local stress distribution will affect the springback during the unloading process. The results between experimental and computational approaches are evaluated to assure the accuracy of the simulation. Subsequent numerical simulation studies are performed to explore best practices with respect to thermal boundary conditions, timing, and applicability to the production environment.

  7. Analysis of local warm forming of high strength steel using near infrared ray energy

    SciTech Connect

    Yang, W. H.; Lee, K.; Lee, E. H. E-mail: dyyang@kaist.ac.kr; Yang, D. Y. E-mail: dyyang@kaist.ac.kr

    2013-12-16

    The automotive industry has been pressed to satisfy more rigorous fuel efficiency requirements to promote energy conservation, safety features and cost containment. To satisfy this need, high strength steel has been developed and used for many different vehicle parts. The use of high strength steels, however, requires careful analysis and creativity in order to accommodate its relatively high springback behavior. An innovative method, called local warm forming with near infrared ray, has been developed to help promote the use of high strength steels in sheet metal forming. For this method, local regions of the work piece are heated using infrared ray energy, thereby promoting the reduction of springback behavior. In this research, a V-bend test is conducted with DP980. After springback, the bend angles for specimens without local heating are compared to those with local heating. Numerical analysis has been performed using the commercial program, DEFORM-2D. This analysis is carried out with the purpose of understanding how changes to the local stress distribution will affect the springback during the unloading process. The results between experimental and computational approaches are evaluated to assure the accuracy of the simulation. Subsequent numerical simulation studies are performed to explore best practices with respect to thermal boundary conditions, timing, and applicability to the production environment.

  8. A low-cost hierarchical nanostructured beta-titanium alloy with high strength.

    PubMed

    Devaraj, Arun; Joshi, Vineet V; Srivastava, Ankit; Manandhar, Sandeep; Moxson, Vladimir; Duz, Volodymyr A; Lavender, Curt

    2016-01-01

    Lightweighting of automobiles by use of novel low-cost, high strength-to-weight ratio structural materials can reduce the consumption of fossil fuels and in turn CO2 emission. Working towards this goal we achieved high strength in a low cost β-titanium alloy, Ti-1Al-8V-5Fe (Ti185), by hierarchical nanostructure consisting of homogenous distribution of micron-scale and nanoscale α-phase precipitates within the β-phase matrix. The sequence of phase transformation leading to this hierarchical nanostructure is explored using electron microscopy and atom probe tomography. Our results suggest that the high number density of nanoscale α-phase precipitates in the β-phase matrix is due to ω assisted nucleation of α resulting in high tensile strength, greater than any current commercial titanium alloy. Thus hierarchical nanostructured Ti185 serves as an excellent candidate for replacing costlier titanium alloys and other structural alloys for cost-effective lightweighting applications. PMID:27034109

  9. A low-cost hierarchical nanostructured beta-titanium alloy with high strength

    PubMed Central

    Devaraj, Arun; Joshi, Vineet V.; Srivastava, Ankit; Manandhar, Sandeep; Moxson, Vladimir; Duz, Volodymyr A.; Lavender, Curt

    2016-01-01

    Lightweighting of automobiles by use of novel low-cost, high strength-to-weight ratio structural materials can reduce the consumption of fossil fuels and in turn CO2 emission. Working towards this goal we achieved high strength in a low cost β-titanium alloy, Ti–1Al–8V–5Fe (Ti185), by hierarchical nanostructure consisting of homogenous distribution of micron-scale and nanoscale α-phase precipitates within the β-phase matrix. The sequence of phase transformation leading to this hierarchical nanostructure is explored using electron microscopy and atom probe tomography. Our results suggest that the high number density of nanoscale α-phase precipitates in the β-phase matrix is due to ω assisted nucleation of α resulting in high tensile strength, greater than any current commercial titanium alloy. Thus hierarchical nanostructured Ti185 serves as an excellent candidate for replacing costlier titanium alloys and other structural alloys for cost-effective lightweighting applications. PMID:27034109

  10. Continuous Hardening During Isothermal Aging at 723 K (450 °C) of a Precipitation Hardening Stainless Steel

    NASA Astrophysics Data System (ADS)

    Celada-Casero, Carola; Chao, Jesús; Urones-Garrote, Esteban; San Martin, David

    2016-11-01

    The isothermal aging behavior of a cold-rolled precipitation hardening stainless steel has been studied at 723 K (450 °C) for holding times up to 72 hours. The precipitation hardening has been investigated using microhardness Vickers (Hv), thermoelectric power (TEP) measurements, and tensile testing. Microhardness compared to TEP measurements is more sensitive to detect the initial stages of aging. Two precipitation regimes have been observed: the first one related to the formation of Cu-clusters for aging times below 1 hour and a second one associated with formation of Ni-rich precipitates. The results show that the material exhibits an outstanding continuous age strengthening response over the aging time investigated, reaching a hardness of 710 ± 4 HV1 and an ultimate tensile strength ( σ UTS) of 2.65 ± 0.02 GPa after 72 hours. Engineering stress-plastic strain curves reveal that the strength increases and the ductility decreases as the aging time increases. However, after prolonged holding times (24-72 hours) and, although small, a rise in both the strength and the total elongation is observed. The precipitation kinetics can be well predicted over the entire range of aging times by the Johnson-Mehl-Avrami-Kolmogorov (JMAK) equation. Finally, a reliable linear hardness-yield strength correlation has been found, which enables a rapid evaluation of the strength from bulk hardness measurements.

  11. Continuous Hardening During Isothermal Aging at 723 K (450 °C) of a Precipitation Hardening Stainless Steel

    NASA Astrophysics Data System (ADS)

    Celada-Casero, Carola; Chao, Jesús; Urones-Garrote, Esteban; San Martin, David

    2016-06-01

    The isothermal aging behavior of a cold-rolled precipitation hardening stainless steel has been studied at 723 K (450 °C) for holding times up to 72 hours. The precipitation hardening has been investigated using microhardness Vickers (Hv), thermoelectric power (TEP) measurements, and tensile testing. Microhardness compared to TEP measurements is more sensitive to detect the initial stages of aging. Two precipitation regimes have been observed: the first one related to the formation of Cu-clusters for aging times below 1 hour and a second one associated with formation of Ni-rich precipitates. The results show that the material exhibits an outstanding continuous age strengthening response over the aging time investigated, reaching a hardness of 710 ± 4 HV1 and an ultimate tensile strength (σ UTS) of 2.65 ± 0.02 GPa after 72 hours. Engineering stress-plastic strain curves reveal that the strength increases and the ductility decreases as the aging time increases. However, after prolonged holding times (24-72 hours) and, although small, a rise in both the strength and the total elongation is observed. The precipitation kinetics can be well predicted over the entire range of aging times by the Johnson-Mehl-Avrami-Kolmogorov (JMAK) equation. Finally, a reliable linear hardness-yield strength correlation has been found, which enables a rapid evaluation of the strength from bulk hardness measurements.

  12. Hardening by bubbles in He-implanted Ni

    SciTech Connect

    Knapp, J. A.; Follstaedt, D. M.; Myers, S. M.

    2008-01-01

    Detailed finite-element modeling of nanoindentation data is used to obtain the mechanical properties of Ni implanted with 1-10 at. % He. The mechanical properties of this material elucidate the fundamental materials science of dislocation pinning by nanometer-size gas bubbles and also have implications for radiation damage of materials. Cross-section transmission electron microscopy showed that implantation of 1-5 at. % He at room temperature or at 200 deg. C produced a highly damaged layer extending to a depth of 700-800 nm and containing a fine dispersion of He bubbles with diameters of 1.1{+-}0.2 nm. Implantation at 500 deg. C enlarged the bubble sizes. By fitting the nanoindentation data with a finite-element model that includes the responses of both the implanted layer and the unimplanted substrate in the deformation, the Ni(He) layers are shown to have hardnesses as much as approximately seven times that of untreated Ni, up to 8.3{+-}0.6 GPa. Examination of the dependence of yield strength on He concentration, bubble size, and bubble density reveals that an Orowan hardening mechanism is likely to be in operation, indicating that the bubbles pin dislocation motion as strongly as hard second-phase precipitates do. This strong pinning of dislocations by bubbles is also supported by our numerical simulations, which show that substantial applied shear stress is required to move a dislocation through an empty cavity.

  13. lsokinetic Shoulder Strength of High School and College-Aged Pitchers*.

    PubMed

    Alderink, G J; Kuck, D J

    1986-01-01

    The purpose of this study was to determine the isokinetic strength of the shoulders of high school and college-aged baseball pitchers. Twenty-four athletes ranging from 14 to 21 years of age volunteered for this study. The Cybex(R) II and U.B.X. T. were utilized to test the strength of the shoulder abductors/adductors, flexors/extensors, horizontal abductors/adductors, and external/internal rotators at 90, 120, 2 10, and 300 degrees /sec. There were no consistent differences between dominant and nondominant arm strength, except for the shoulder adductors and shoulder extensors. The shoulder abductors and flexors were approximately 50% as strong as the adductors and extensors, respectively. There was a 1:1 ratio between the horizontal abductors/ adductors. The external rotators were approximately two-thirds as strong as the internal rotators. A positive correlation was found between total body weight and shoulder strength. This information is relatively new to the literature and should provide clinicians with some training and rehabilitation guidelines. J Orthop Sports Phys Ther 1986;7(4):163-172.

  14. Progress in press forming computer aided analysis for high strength steel sheet applications

    NASA Astrophysics Data System (ADS)

    Hiramoto, Jiro; Urabe, Masaki; Ishiwatari, Akinobu; Urabe, Toshiaki

    2013-12-01

    The development of press-forming analysis technologies is important to expand the application of high strength steel sheets to automotive body structures. In general, there are various problems in the forming process of high strength steel sheets. In this study the improvements in the prediction accuracy of stretch-flange-fracture and springback were especially focused. In terms of the prediction accuracy of stretch-flange-fracture, a new stretch-flange-fracture prediction technology was developed based on a maximum principal strain gradient. It enables the accurate prediction of stretch- flange-fracture in press-forming of practical parts. On the other hand, springback prediction technologies were developed to solve springback problems. It is very important to clarify the root cause of springback in order to control. Therefore, a new method of springback factor analysis was developed, which can extract the areas and residual stresses which have major impacts on springback at press-forming.

  15. High-strength clad current collector for silicon-based negative electrode in lithium ion battery

    NASA Astrophysics Data System (ADS)

    Kataoka, Riki; Oda, Yoshimitsu; Inoue, Ryouji; Kitta, Mitsunori; Kiyobayashi, Tetsu

    2016-01-01

    We develop a clad foil current collector with a high tensile strength that endures a large volume change in the active material during the charge and discharge, such as the Si-based materials. The nano-Si negative electrode with the clad current collector retains 76% of the initial capacity after 40 cycles, while the capacity of the nano-Si electrode with a conventional Cu foil drops to less than 70% only after 10 cycles. A full cell with the SiO negative electrode and the LiFePO4 positive electrode retains more than 90% of its capacity at the 10th cycle after 800 cycles. The conventional rolled Cu foil wrinkles during the cycling test. The high-strength clad current foil hardly deforms during the test regardless of the electrode size.

  16. Boron enhances strength and alters mineral composition of bone in rabbits fed a high energy diet.

    PubMed

    Hakki, Sema S; Dundar, Niyazi; Kayis, Seyit Ali; Hakki, Erdogan E; Hamurcu, Mehmet; Kerimoglu, Ulku; Baspinar, Nuri; Basoglu, Abdullah; Nielsen, Forrest H

    2013-04-01

    An experiment was performed to determine whether boron had a beneficial effect on bone strength and composition in rabbits with apparent adiposity induced by a high energy diet. Sixty female New Zealand rabbits, aged 8 months, were randomly divided into five groups with the following treatments for seven months: control 1, fed alfalfa hay only (5.91 MJ/kg); control 2, high energy diet (11.76 MJ and 3.88 mg boron/kg); B10, high energy diet+10 mg/kg body weight boron gavage/96 h; B30, high energy diet+30 mg/kg body weight boron gavage/96 h; B50, high energy diet+50mg/kg body weight boron gavage/96 h. Bone boron concentrations were lowest in rabbits fed the high energy diet without boron supplementation, which suggested an inferior boron status. Femur maximum breaking force was highest in the B50 rabbits. Tibia compression strength was highest in B30 and B50 rabbits. All boron treatments significantly increased calcium and magnesium concentrations, and the B30 and B50 treatments increased the phosphorus concentration in tibia of rabbits fed the high energy diet. The B30 treatment significantly increased calcium, phosphorus and magnesium concentrations in femur of rabbits fed the high energy diet. Principal component analysis of the tibia minerals showed that the three boron treatments formed a separate cluster from controls. Discriminant analysis suggested that the concentrations of the minerals in femur could predict boron treatment. The findings indicate boron has beneficial effects on bone strength and mineral composition in rabbits fed a high energy diet.

  17. Physically Based Model of the Yield Strength for an Al-Mg-Si-Cu-Zn Alloy

    NASA Astrophysics Data System (ADS)

    Hosseini-Benhangi, Pooya; Mazinani, Mohammad; Haddad-Sabzevar, Mohsen

    2015-11-01

    The aim of this work is to implement recently developed modeling approaches to predict the mechanical behavior of a precipitation-hardened Al-Mg-Si-Cu-Zn alloy. Assuming that precipitates act as weak or strong obstacles to dislocation motion, a yield strength model, originally introduced for AA6111 alloy, is used to derive the precipitate strengthening formulations. The application of the model provides accurate predictions for the evolution of yield strength of the alloy during artificial aging. The transition point, at which shearable precipitates become non-shearable ones, has been identified directly from the result of tensile tests of AA6011(m) samples at different stages of artificial aging using work-hardening rate model. The linear/non-linear behavior of work-hardening rate of AA6011(m) samples at different stages of artificial aging is also studied. It is explained that high dynamic recovery rate in presence of non-shearable precipitates causes the non-linear work-hardening behavior of massively overaged sample. The modeling results for underaged samples show better agreement with measured values of yield strength when the weak obstacle model has been implemented, while strong obstacle model shows relatively good agreement between the experimental and calculated results for the peak-aged and overaged samples.

  18. Stress relaxation of high strength A-286 bolts in simulated storage at room temperature

    NASA Technical Reports Server (NTRS)

    Sampson, R. C.

    1972-01-01

    It was concluded that thermally activated relaxation of the type customarily encountered at high temperatures was not expected to occur at the low temperatures where long time NERVA storage conditions will prevail. Instances where relaxation occurred by a different mechanism at such moderate temperatures were also reported. Twelve simulated bolted flange test specimens were prepared. Parameters that were varied among the twelve specimens were the flange material, the bolt shank diameter, and the bolt loading in terms of percent of yield strength.

  19. Improving uv resistance of high strength fibers used in large scientific balloons

    NASA Astrophysics Data System (ADS)

    Said, M.; Gupta, A.; Seyam, A.; Mock, G.; Theyson, T.

    For the last three decades, NASA has been involved in the development of giant balloons that are capable of lifting heavy payloads of equipment (such as large telescopes and scientific instruments) to the upper atmosphere. While the use of such balloons has led to scientific discoveries, the demand for competitive science payloads and observational programs continues to rise. The NASA Balloon Program Office has entered a new phase of research to develop an Ultra Long Duration Balloon (ULDB) that will lift payloads of up to 3,600 kg to altitudes of up to 40 km. The flight duration is targeted to ranges between 30 to 100 days. Attaining these target durations requires the development of a super-pressure balloon design. The use of textile structures have already been established in these missions in the form of high strength tendons essential for the super pressure pumpkin design. Unfortunately, high strength fibers lose significant strength upon exposure to Ultra Violet (UV) radiation. Such UV degradation poses a serious challenge for the development of the ULDB. To improve the mission performance of the ULDB, new methods for protecting the tendons from the environmental effects need to be developed. NASA and NC State University College of Textiles are undertaking a research program to address these issues. Four tracks have been identified to prepare finishes that are believed to enhance the resistance of high strength fibers to UV. These tracks are: (a) self-polymerizing, (b) diffusion application, (c) polymer-filled with 30-40% UV absorber, and (d) combination of dyeing plus surface application. Four high performance fibers have been selected for this research investigation. These are Vectran, Spectra, Kevlar and, PBO (Zylon). This work will address the current progress of evaluating the performance of the UV finishes. This will be accomplished by comparing the tensile properties (strenthg, breaking elongation, modulus, etc) of untreated, unexposed to UV fibers

  20. A Novel Method for Electroplating Ultra-High-Strength Glassy Metals

    NASA Technical Reports Server (NTRS)

    Ramsey, Brian; Engelhaupt, Darell; Six, N. Frank (Technical Monitor)

    2002-01-01

    A novel method for electroplating ultra-high-strength glassy metals, nickel-phosphorous and nickel-cobalt-phosphorous, has been developed at NASA Marshall Space Flight Center, cooperatively with the University of Alabama in Huntsville. Traditionally, thin coatings of these metals are achieved via electroless deposition. Benefits of the new electrolytic process include thick, low-stress deposits, free standing shapes, lower plating temperature, low maintenance, and safer operation with substantially lower cost.

  1. Sound velocity of high-strength polymer with negative thermal expansion coefficient

    NASA Astrophysics Data System (ADS)

    Nomura, R.; Ueno, M.; Okuda, Y.; Burmistrov, S.; Yamanaka, A.

    2003-05-01

    Sound velocities of fiber reinforced plastics (FRPs) were measured along the fiber axis at temperatures between 360 and 77 K. We used two kinds of the high-strength crystalline polymer fibers, polyethylene (Dyneema) and polybenzobisoxazole (Zylon), which have negative thermal expansion coefficients. They also have high thermal conductivities and high resistances for flash over voltage, and are expected as new materials for coil bobbins or spacers at cryogenic temperatures. They have very large sound velocities of about 9000 (m/s) at 77 K, which are 4.5 times larger than that of the ordinary polyethylene fiber.

  2. Rapidly sintering of interconnected porous Ti-HA biocomposite with high strength and enhanced bioactivity.

    PubMed

    Zhang, L; He, Z Y; Zhang, Y Q; Jiang, Y H; Zhou, R

    2016-10-01

    In this work, interconnected porous Ti-HA biocomposites with enhanced bioactivity, high porosity and compressive strength were prepared by spark plasma sintering (SPS) and space holder method. Pore characteristics, mechanical properties, corrosion behaviors and in vitro bioactivity of the porous Ti-HA were investigated. Results showed that porous Ti-HA with 5-30wt% HA contents possessed not only low elastic modulus of 8.2-15.8GPa (close to that of human bone) but also high compressive strength (86-388MPa). Although the HA partially decomposed and formed secondary phases, the sintered porous Ti-HA can still be good bioactivity. The homogeneity and the thickness of apatite layer increased significantly with the increase of HA. But with the thickness of apatite layer increased, micro-cracks appeared on the surface of porous Ti-30%HA. A model was built to discuss the current distribution and sintering mechanism of HA on Ti matrix during SPS process. It indicated that the excessive addition of HA would deteriorate the sintering quality, thus decreasing the mechanical properties and corrosion resistance. However, the combination of interconnected pore characteristics, low elastic modulus, high compressive strength and enhanced bioactivity might make porous Ti-HA biocomposites prepared by SPS a promising candidate for hard tissue implants. PMID:27287104

  3. Nitrate removal from high strength nitrate-bearing wastes in granular sludge sequencing batch reactors.

    PubMed

    Krishna Mohan, Tulasi Venkata; Renu, Kadali; Nancharaiah, Yarlagadda Venkata; Satya Sai, Pedapati Murali; Venugopalan, Vayalam Purath

    2016-02-01

    A 6-L sequencing batch reactor (SBR) was operated for development of granular sludge capable of denitrification of high strength nitrates. Complete and stable denitrification of up to 5420 mg L(-1) nitrate-N (2710 mg L(-1) nitrate-N in reactor) was achieved by feeding simulated nitrate waste at a C/N ratio of 3. Compact and dense denitrifying granular sludge with relatively stable microbial community was developed during reactor operation. Accumulation of large amounts of nitrite due to incomplete denitrification occurred when the SBR was fed with 5420 mg L(-1) NO3-N at a C/N ratio of 2. Complete denitrification could not be achieved at this C/N ratio, even after one week of reactor operation as the nitrite levels continued to accumulate. In order to improve denitrification performance, the reactor was fed with nitrate concentrations of 1354 mg L(-1), while keeping C/N ratio at 2. Subsequently, nitrate concentration in the feed was increased in a step-wise manner to establish complete denitrification of 5420 mg L(-1) NO3-N at a C/N ratio of 2. The results show that substrate concentration plays an important role in denitrification of high strength nitrate by influencing nitrite accumulation. Complete denitrification of high strength nitrates can be achieved at lower substrate concentrations, by an appropriate acclimatization strategy.

  4. Hollow-fiber membrane bioreactor for the treatment of high-strength landfill leachate.

    PubMed

    Rizkallah, Marwan; El-Fadel, Mutasem; Saikaly, Pascal E; Ayoub, George M; Darwiche, Nadine; Hashisho, Jihan

    2013-10-01

    Performance assessment of membrane bioreactor (MBR) technology for the treatability of high-strength landfill leachate is relatively limited or lacking. This study examines the feasibility of treating high-strength landfill leachate using a hollow-fiber MBR. For this purpose, a laboratory-scale MBR was constructed and operated to treat leachate with a chemical oxygen demand (COD) of 9000-11,000 mg/l, a 5-day biochemical oxygen demand (BOD5) of 4000-6,000 mg/l, volatile suspended solids (VSS) of 300-500 mg/l, total nitrogen (TN) of 2000-6000 mg/l, and an ammonia-nitrogen (NH3-N) of 1800-4000 mg/l. VSS was used with the BOD and COD data to simulate the biological activity in the activated sludge. Removal efficiencies > 95-99% for BOD5, VSS, TN and NH3-N were attained. The coupled experimental and simulation results contribute in filling a gap in managing high-strength landfill leachate and providing guidelines for corresponding MBR application. PMID:23856789

  5. Mechanical Behavior of Two High Strength Alloy Steels Under Conditions of Cyclic Tension

    NASA Astrophysics Data System (ADS)

    Srivatsan, T. S.; Manigandan, K.; Sastry, S.; Quick, T.; Schmidt, M. L.

    2014-01-01

    The results of a recent study aimed at understanding the conjoint influence of load ratio and microstructure on the high cycle fatigue properties and resultant fracture behavior of two high strength alloy steels is presented and discussed. Both the chosen alloy steels, i.e., 300M and Tenax™ 310 have much better strength and ductility properties to offer in comparison with the other competing high strength steels having near similar chemical composition. Test specimens were precision machined from the as-provided stock of each steel. The machined specimens were deformed in both uniaxial tension and cyclic fatigue under conditions of stress control. The test specimens of each alloy steel were cyclically deformed over a range of maximum stress at two different load ratios and the number of cycles to failure recorded. The specific influence of load ratio on cyclic fatigue life is presented and discussed keeping in mind the maximum stress used during cyclic deformation. The fatigue fracture surfaces were examined in a scanning electron microscope to establish the macroscopic mode and to concurrently characterize the intrinsic features on the fracture surface. The conjoint influence of nature of loading, maximum stress, and microstructure on cyclic fatigue life is discussed.

  6. Stress and Distortion Evolution During Induction Case Hardening of Tube

    NASA Astrophysics Data System (ADS)

    Nemkov, Valentin; Goldstein, Robert; Jackowski, John; Ferguson, Lynn; Li, Zhichao

    2013-07-01

    Simulation of stresses during heat treatment relates usually to furnace heating. Induction heating provides a very different evolution of temperature in the part and therefore different stresses. This may be positive for service properties or negative, reducing component strength or even causing cracks. A method of coupled simulation between electromagnetic, thermal, structural, stress, and deformation phenomena during induction tube hardening is described. Commercial software package ELTA is used to calculate the power density distribution in the load resulting from the induction heating process. The program DANTE is used to predict temperature distribution, phase transformations, stress state, and deformation during heating and quenching. Analyses of stress and deformation evolution were made on a simple case of induction hardening of external (1st case) and internal (2nd case) surfaces of a thick-walled tubular body.

  7. Effect of MX type particles on creep strength of ferritic steel

    NASA Astrophysics Data System (ADS)

    Tamura, M.; Sakasegawa, H.; Kohyama, A.; Esaka, H.; Shinozuka, K.

    2003-09-01

    Creep rupture strength at 650 °C and microstructures of the plain ferritic steels with fine particles of the NaCl type (MX) were studied. Precipitation hardening by the fine MX type particles is more effective than solid solution hardening by tungsten. Excess precipitation of MX type particles relatively weakens the grain boundaries as compared with the matrix and, as a consequence, lowers the rupture strength. The equivalent obstacle spacing for mobile dislocations is calculated from the rupture data and is comparable to the interparticle distance observed by transmission electron microscopy. By controlling the interparticle distance of MX type particles with some adjustments of the chemical composition to meet the engineering requirements, it is feasible to develop a new alloy with high rupture strength at 650 °C which is superior to the conventional ferritic steels.

  8. Thermal Processing Effects on the Adhesive Strength of PS304 High Temperature Solid Lubricant Coatings

    NASA Technical Reports Server (NTRS)

    DellaCorte, Christopher; Edmonds, Brian J.; Benoy, Patricia A.

    2001-01-01

    In this paper the effects of post deposition heat treatments on the cohesive and adhesive strength properties of PS304, a plasma sprayed nickel-chrome based, high temperature solid lubricant coating deposited on stainless steel, are studied. Plasma spray deposited coating samples were exposed in air at temperatures from 432 to 650 C for up to 500 hr to promote residual stress relief, enhance particle to particle bonding and increase coating to substrate bond strength. Coating pull-off strength was measured using a commercial adhesion tester that utilizes 13 mm diameter aluminum pull studs attached to the coating surface with epoxy. Pull off force was automatically recorded and converted to coating pull off strength. As deposited coating samples were also tested as a baseline. The as-deposited (untreated) samples either delaminated at the coating-substrate interface or failed internally (cohesive failure) at about 17 MPa. Samples heat treated at temperatures above 540 C for 100 hr or at 600 C or above for more than 24 hr exhibited strengths above 31 MPa, nearly a two fold increase. Coating failure occurred inside the body of the coating (cohesive failure) for nearly all of the heat-treated samples and only occasionally at the coating substrate interface (adhesive failure). Metallographic analyses of heat-treated coatings indicate that the Nickel-Chromium binder in the PS304 appears to have segregated into two phases, a high nickel matrix phase and a high chromium precipitated phase. Analysis of the precipitates indicates the presence of silicon, a constituent of a flow enhancing additive in the commercial NiCr powder. The exact nature and structure of the precipitate phase is not known. This microstructural change is believed to be partially responsible for the coating strength increase. Diffusion bonding between particles may also be playing a role. Increasing the heat treatment temperature, exposure time or both accelerate the heat treatment process. Preliminary

  9. High-Intensity Intermittent Exercise and its Effects on Heart Rate Variability and Subsequent Strength Performance

    PubMed Central

    Panissa, Valéria L. G.; Cal Abad, Cesar C.; Julio, Ursula F.; Andreato, Leonardo V.; Franchini, Emerson

    2016-01-01

    Prupose: To investigate the effects of a 5-km high-intensity interval exercise (HIIE) on heart rate variability (HRV) and subsequent strength performance. Methods: Nine trained males performed a control session composed of a half-squat strength exercise (4 × 80% of one repetition maximum—1 RM) in isolation and 30-min, 1-, 4-, 8-, and 24-h after an HIIE (1-min at the velocity peak:1-min passive recovery). All experimental sessions were performed on different days. The maximum number of repetitions (MNR) and total weight lifted (TWL) during the strength exercise were registered in all conditions; in addition, prior to each session, HRV were assessed [beat-to-beat intervals (RR) and log-transformed of root means square of successive differences in the normal-to-normal intervals (lnRMSSD)]. Results: Performance in the strength exercise dropped at 30-min (31%) and 1-h (19%) post-HIIE concomitantly with lower values of RR (781 ± 79 ms; 799 ± 134 ms, respectively) in the same recovery intervals compared to the control (1015 ± 197 ms). Inferential analysis did not detect any effect of condition on lnRMSSD, however, values were lower after 30-min (3.5 ± 0.4 ms) and 1-h (3.3 ± 0.5 ms) with moderate and large effect sizes (0.9 and 1.2, respectively) compared with the control condition (3.9 ± 0.4 ms). Conclusion: Both RR and lnRMSSD seem to be associated with deleterious effects on strength performance, although further studies should be conducted to clarify this association. PMID:26973543

  10. Neptunium (V) Adsorption to a Halophilic Bacterium Under High Ionic Strength Conditions: A Surface Complexation Modeling Approach

    SciTech Connect

    Ams, David A

    2012-06-11

    Rationale for experimental design: Np(V) -- important as analog for Pu(V) and for HLW scenarios; High ionic strength -- relevant to salt-based repositories such as the WIPP; Halophilic microorganisms -- representative of high ionic strength environments. For the first time showed: Significant adsorbant to halophilic microorganisms over entire pH range under high ionic strength conditions; Strong influence of ionic strength with increasing adsorption with increasing ionic strength (in contrast to trends of previous low ionic strength studies); Effect of aqueous Np(V) and bacterial surface site speciation on adsorption; and Developed thermodynamic models that can be incorporated into geochemical speciation models to aid in the prediction of the fate and transport of Np(V) in more complex systems.

  11. Photothermal characterization of grind-hardened steel

    NASA Astrophysics Data System (ADS)

    Prekel, H.; Ament, Ch.; Goch, G.

    2003-01-01

    Grind hardening is a promising production process which combines grinding and hardening within one step. Due to the fact that many material and process parameters partially influence the properties of the workpieces in a nonlinear way, it is difficult to predict for instance the surface hardness and hardness penetration depth. In this study, photothermal radiometry is used as an approach to determine the hardness penetration depth. Photothermal phase signals have been measured as a function of frequency. First measurements showed a strong influence of surface roughness, causing phase signal maxima at unexpected high frequencies (f>60 Hz). After finishing of the surfaces, the maxima of phase signals shifted toward lower frequencies (f<10 Hz). In an attempt to extract a preliminary calibration curve, the measured phase values of each sample were added and correlated to the hardness penetration depth. The resulting curve reveals a good correlation between phase sum and the hardness penetration depth. Further research is necessary to collect more experimental data and to support the current results by theoretical models.

  12. Effect of test temperature and strain rate on the tensile properties of high-strength, high-conductivity copper alloys

    SciTech Connect

    Zinkle, S.J.; Eatherly, W.S.

    1997-04-01

    The unirradiated tensile properties of wrought GlidCop AL25 (ITER grade zero, IGO) solutionized and aged CuCrZr, and cold-worked and aged and solutionized and aged Hycon 3HP{trademark} CuNiBe have been measured over the temperature range of 20-500{degrees}C at strain rates between 4 x 10{sup {minus}4} s{sup {minus}1} and 0.06 s{sup {minus}1}. The measured room temperature electrical conductivity ranged from 64 to 90% IACS for the different alloys. All of the alloys were relatively insensitive to strain rate at room temperature, but the strain rate sensitivity of GlidCop Al25 increased significantly with increasing temperature. The CuNiBe alloys exhibited the best combination of high strength and high conductivity at room temperature. The strength of CuNiBe decreased slowly with increasing temperature. However, the ductility of CuNiBe decreased rapidly with increasing temperature due to localized deformation near grain boundaries, making these alloy heats unsuitable for typical structural applications above 300{degrees}C. The strength and uniform elongation of GlidCop Al25 decreased significantly with increasing temperature at a strain rate of 1 x 10{sup {minus}3} s{sup {minus}1}, whereas the total elongation was independent of test temperature. The strength and ductility of CuCrZr decreased slowly with increasing temperature.

  13. Enzymatic surface erosion of high tensile strength polycarbonates based on natural phenols.

    PubMed

    Sommerfeld, Sven D; Zhang, Zheng; Costache, Marius C; Vega, Sebastián L; Kohn, Joachim

    2014-03-10

    Surface erosion has been recognized as a valuable design tool for resorbable biomaterials within the context of drug delivery devices, surface coatings, and when precise control of strength retention is critical. Here we report on high tensile strength, aromatic-aliphatic polycarbonates based on natural phenols, tyrosol (Ty) and homovanillyl alcohol (Hva), that exhibit enzymatic surface erosion by lipase. The Young's moduli of the polymers for dry and fully hydrated samples are 1.0 to 1.2 GPa and 0.8 to 1.2 GPa, respectively. Typical characteristics of enzymatic surface erosion were confirmed for poly(tyrosol carbonate) films with concomitant mass-loss and thickness-loss at linear rates of 0.14 ± 0.01 mg cm(-2) d(-1) and 3.0 ± 0.8 μm d(-1), respectively. The molecular weight and the mechanical properties of the residual films remained constant. Changing the ratio of Ty and Hva provided control over the glass transition temperature (T(g)) and the enzymatic surface erosion: increasing the Hva content in the polymers resulted in higher T(g) and lower enzymatic erosion rate. Polymers with more than 50 mol % Hva were stable at 37 °C in enzyme solution. Analysis on thin films using quartz crystal microbalance with dissipation (QCM-D) demonstrated that the onset temperature of the enzymatic erosion was approximately 20 °C lower than the wet T(g) for all tested polymers. This new finding demonstrates that relatively high tensile strength polycarbonates can undergo enzymatic surface erosion. Moreover, it also sheds light on the connection between T(g) and enzymatic degradation and explains why few of the high strength polymers follow an enzyme-meditated degradation pathway.

  14. Enzymatic Surface Erosion of High Tensile Strength Polycarbonates Based on Natural Phenols

    PubMed Central

    2015-01-01

    Surface erosion has been recognized as a valuable design tool for resorbable biomaterials within the context of drug delivery devices, surface coatings, and when precise control of strength retention is critical. Here we report on high tensile strength, aromatic–aliphatic polycarbonates based on natural phenols, tyrosol (Ty) and homovanillyl alcohol (Hva), that exhibit enzymatic surface erosion by lipase. The Young’s moduli of the polymers for dry and fully hydrated samples are 1.0 to 1.2 GPa and 0.8 to 1.2 GPa, respectively. Typical characteristics of enzymatic surface erosion were confirmed for poly(tyrosol carbonate) films with concomitant mass-loss and thickness-loss at linear rates of 0.14 ± 0.01 mg cm–2 d–1 and 3.0 ± 0.8 μm d–1, respectively. The molecular weight and the mechanical properties of the residual films remained constant. Changing the ratio of Ty and Hva provided control over the glass transition temperature (Tg) and the enzymatic surface erosion: increasing the Hva content in the polymers resulted in higher Tg and lower enzymatic erosion rate. Polymers with more than 50 mol % Hva were stable at 37 °C in enzyme solution. Analysis on thin films using quartz crystal microbalance with dissipation (QCM-D) demonstrated that the onset temperature of the enzymatic erosion was approximately 20 °C lower than the wet Tg for all tested polymers. This new finding demonstrates that relatively high tensile strength polycarbonates can undergo enzymatic surface erosion. Moreover, it also sheds light on the connection between Tg and enzymatic degradation and explains why few of the high strength polymers follow an enzyme-meditated degradation pathway. PMID:24432806

  15. Microwave drying of high strength dental stone: effects on dimensional accuracy.

    PubMed

    Yap, Adrian U J; Yap, S H; Teo, Jason C K; Tay, C M; Ng, K L; Thean, Hilary P Y

    2003-01-01

    High-strength dental stone is widely used to produce dies for the fabrication of restorations with the lost-wax technique. It is normal to wait at least 24 hours for casts to dry and gain sufficient strength prior to initiating laboratory procedures. This waiting time may be greatly reduced by using microwave drying. This study determined the optimum microwave energy density for preserving working die accuracy of a Type IV high-strength dental stone (Silky Rock; Whipmix). Cylindrical die specimens were fabricated according to manufacturer's instructions and allowed to set for one hour. The specimens were subsequently treated as follows: Group I (Control group)--air dried; Group II--microwaved at 700W for 40 seconds; Group III--microwaved at 490W for 60 seconds. The percentage weight loss of cylindrical specimens (n = 6) and the percentage dimensional change (n = 7) of die specimens in three axes (x, y and z) were determined at 30 minutes, 1 hour and 24 hours after air drying/microwaving. Weight loss was measured using an electronic digital balance, while dimensional changes were assessed using image analysis software. Data was subject to ANOVA/Scheffe's tests at significance level 0.05. No significant difference in percentage weight loss was observed between air drying for 24 hours and microwaved specimens at all time intervals. Although no significant difference in percentage dimensional changes was observed between specimens microwaved at 490W for 60 seconds and specimens air dried for 24 hours, significant changes in x, y and z dimensions were observed after microwaving at 700W for 40 seconds at various time intervals. Microwave radiation at 490W for 60 seconds is recommended for drying Type IV high-strength dental stone. Further investigations are required to determine changes in physical properties associated with the aforementioned microwave power density. PMID:12670076

  16. Nitriding of high speed steel by bipolar PBII for improvement in adhesion strength of DLC films

    NASA Astrophysics Data System (ADS)

    Choi, Junho; Soejima, Koji; Kato, Takahisa; Kawaguchi, Masahiro; Lee, Wonsik

    2012-02-01

    In the present study, bipolar plasma based ion implantation and deposition (bipolar PBII) was used for plasma nitriding of high speed steel (SKH2), and the effects of the treatment parameters (positive pulse voltage, negative pulse voltage, treatment pressure, treatment time, and precursor gases) on the nitriding process were investigated. The hardness, roughness, and depth of nitride layer were also measured. The adhesion strength of diamond-like carbon (DLC) films coated on the nitride substrate was evaluated by carrying out Rockwell indentation and microscratch tests. Nitriding by bipolar PBII was achieved in the combining of two effects: nitrogen ion implantation by applying a high negative pulse voltage and thermal diffusion of nitrogen atoms under the application of a high positive pulse voltage. However, a very high voltage negative pulse caused surface roughening of the nitride layer. Application of a high positive pulse voltage during nitriding was found to be effective in promoting the thermal diffusion of the implanted nitrogen atoms. Effective nitriding could be achieved under the following conditions: high positive pulse voltage, low negative pulse voltage, high nitrogen gas pressure, and addition of hydrogen to the precursor gas. The adhesion strength of the DLC films on the SKH2 substrate was well improved after nitriding.

  17. A Profile of Glenohumeral Internal and External Rotation Motion in the Uninjured High School Baseball Pitcher, Part II: Strength

    PubMed Central

    Hurd, Wendy J.; Kaplan, Kevin M.; ElAttrache, Neal S.; Jobe, Frank W.; Morrey, Bernard F.; Kaufman, Kenton R.

    2011-01-01

    Context: A database describing the range of normal rotator cuff strength values in uninjured high school pitchers has not been established. Chronologic factors that contribute to adaptations in strength also have not been established. Objectives: To establish a normative profile of rotator cuff strength in uninjured high school baseball pitchers and to determine whether bilateral differences in rotator cuff strength are normal findings in this age group. Design: Cohort study. Setting: Baseball playing field. Patients or Other Participants: A total of 165 uninjured male high school baseball pitchers (age = 16 ± 1 years, height = 1.8 ± 0.1 m, mass = 76.8 ± 10.1 kg, pitching experience = 7 ± 2 years). Main Outcome Measure(s): Isometric rotator cuff strength was measured bilaterally with a handheld dynamometer. We calculated side-to-side differences in strength (external rotation [ER], internal rotation [IR], and the ratio of ER:IR at 90° of abduction), differences in strength by age, and the influence of chronologic factors (participant age, years of pitching experience) on limb strength. Results: Side-to-side differences in strength were found for ER, IR, and ER:IR ratio at 90° of abduction. Age at the time of testing was a significant but weak predictor of both ER strength (R2 = 0.032, P = .02) and the ER:IR ratio (R2 = 0.051, P = .004) at 90° of abduction. Conclusions: We established a normative profile of rotator cuff strength for the uninjured high school baseball pitcher that might be used to assist clinicians and researchers in the interpretation of muscle strength performance in this population. These data further suggested that dominant-limb adaptations in rotator cuff strength are a normal finding in this age group and did not demonstrate that these adaptations were a consequence of the age at the time of testing or the number of years of pitching experience. PMID:21669099

  18. Interrelation of Steel Composition, Hardening Route, and Tempering Response of Medium Carbon Low-Alloy Steels

    NASA Astrophysics Data System (ADS)

    Hussein, Abdel-Hamid A.; Abdu, Mahmoud T.; El-Banna, El-Sayed M.; Soliman, Saied E.; Tash, Mahmoud M.

    2016-04-01

    Four medium carbon and low-alloy steels were hardened through oil and forced air cooling. Tempering was then performed in the temperature range 250-600 °C. The martensite content increased with an increased hardenability and/or the rate of cooling. Tempering at T > M s caused a gradual decline in both hardness and strength and an improvement in the Charpy V-notch impact toughness. The low-alloy steels underwent tempered martensite embrittlement (as a result of the formation of carbides at the martensite interlaths and prior austenite grain boundaries) and enhancement of phosphorus segregation (particularly in the presence of Ni). Higher hardenability steels were found to be better hardened via the more recent forced air quenching rather than the conventional oil quenching. In this work, a modest, novel attempt is presented to empirically correlate the impact toughness with the hardness measurements to enable future prediction of impact toughness from hardness measurements.

  19. Plasma methods of obtainment of multifunctional composite materials, dispersion-hardened by nanoparticles

    NASA Astrophysics Data System (ADS)

    Sizonenko, O. N.; Grigoryev, E. G.; Zaichenko, A. D.; Pristash, N. S.; Torpakov, A. S.; Lipyan, Ye V.; Tregub, V. A.; Zholnin, A. G.; Yudin, A. V.; Kovalenko, A. A.

    2016-04-01

    The new approach in developed plasma methods consists in that dispersionhardening additives (TiC, TiB2 in particular) are not mechanically added to powder mixture as additional component, as in conventional methods, but are instead synthesized during high voltage electric discharges (HVED) in disperse system “hydrocarbon liquid - powder” preservation of ultrafine structure is ensured due to use of spark plasma sintering (SPS) as a consolidation method. HVED in disperse system “hydrocarbon liquid - powder” due to impact of plasma discharge channel, electromagnetic fields, shock waves mechanical impact, hydro flows and volume microcavitation leads to synthesis of nanocarbon, metal powders dispersion and synthesis of micro- (from 10-6 to 10-7 m) and nanosized (from 10-7 to 10-9 m) composite powders of hardening phases. SPS is the passage of pulsed current (superposition of direct and alternating current) through powder with the simultaneous mechanical compressing. The formation of plasma is initiated in gaseous phase that fills gaps between particles. SPS allows targeted control of grain growth rate and thus allows obtainment of multifunctional composite materials dispersion hardened by nanoparticles. Processes of HVED synthesis of micro- and nanosized powders of new compositions from elemental metal powders and their mixtures with the subsequent application of high-speed SPS of obtained powders create conditions for increase of strength (by 10 - 20%), hardness and wear-resistance (by 30 - 60%) of obtained materials.

  20. Graded High-Strength Spring-Steels by a Special Inductive Heat T reatment

    NASA Astrophysics Data System (ADS)

    Tump, A.; Brandt, R.

    2016-03-01

    A method for effective lightweight design is the use of materials with high specific strength. As materials e.g. titanium are very expensive, steel is still the most important material for manufacturing automotive components. Steel is cost efficient, easy to recycle and its tensile strength easily exceeds 2,000 MPa by means of modern QT-technology (Quenched and Tempered). Therefore, lightweight design is still feasible in spite of the high density of steel. However, a further increase of tensile strength is limited, especially due to an increasing notch sensitivity and exposure to a corrosive environment. One solution is a special QT-process for steel, which creates a hardness gradient from the surface to the core of the material. This type of tailored material possesses a softer layer, which improves material properties such as fracture toughness and notch sensitivity. This leads to a better resistance to stress corrosion cracking and corrosion fatigue. Due to this optimization, a weight reduction is feasible without the use of expensive alloying elements. To understand the damage mechanism a comprehensive testing procedure was performed on homogeneous and gradient steels. Some results regarding the fracture mechanic behavior of such steels will be discussed.