Analysis of a Temperature-Controlled Exhaust Thermoelectric Generator During a Driving Cycle

NASA Astrophysics Data System (ADS)

Brito, F. P.; Alves, A.; Pires, J. M.; Martins, L. B.; Martins, J.; Oliveira, J.; Teixeira, J.; Goncalves, L. M.; Hall, M. J.

2016-03-01

Thermoelectric generators can be used in automotive exhaust energy recovery. As car engines operate under wide variable loads, it is a challenge to design a system for operating efficiently under these variable conditions. This means being able to avoid excessive thermal dilution under low engine loads and being able to operate under high load, high temperature events without the need to deflect the exhaust gases with bypass systems. The authors have previously proposed a thermoelectric generator (TEG) concept with temperature control based on the operating principle of the variable conductance heat pipe/thermosiphon. This strategy allows the TEG modules’ hot face to work under constant, optimized temperature. The variable engine load will only affect the number of modules exposed to the heat source, not the heat transfer temperature. This prevents module overheating under high engine loads and avoids thermal dilution under low engine loads. The present work assesses the merit of the aforementioned approach by analysing the generator output during driving cycles simulated with an energy model of a light vehicle. For the baseline evaporator and condenser configuration, the driving cycle averaged electrical power outputs were approximately 320 W and 550 W for the type-approval Worldwide harmonized light vehicles test procedure Class 3 driving cycle and for a real-world highway driving cycle, respectively.

High-temperature properties of joint interface of VPS-tungsten coated CFC

NASA Astrophysics Data System (ADS)

Tamura, S.; Liu, X.; Tokunaga, K.; Tsunekawa, Y.; Okumiya, M.; Noda, N.; Yoshida, N.

2004-08-01

Tungsten coated carbon fiber composite (CFC) is a candidate material for the high heat flux components in fusion reactors. In order to investigate the high-temperature properties at the joint interface of coating, heat load experiments by using electron beam were performed on VPS-tungsten coated CX-2002U samples. After the heat load test for 3.6 ks at 1400 °C, tungsten-rhenium multilayer (diffusion barrier for carbon) at the joint interface of coating was observed clearly. But, at the temperatures above 1600 °C, the multilayer was disappeared and a tungsten carbide layer was formed in the VPS-tungsten coating. At the temperatures below 1800 °C, the thickness of this layer logarithmically increased with increasing its loading time. At 2000 °C, the growth of the tungsten carbide layer was proportional to the square root of loading time. These results indicate that the diffusion barrier for carbon is not expected to suppress the carbide formation at the joint interface of the VPS-tungsten coating above 1600 °C.

Fundamental aspects of and failure modes in high-temperature composites

NASA Technical Reports Server (NTRS)

Chamis, Christos C.; Ginty, Carol A.

1990-01-01

Fundamental aspects of and attendant failure mechanisms for high temperature composites are summarized. These include: (1) in-situ matrix behavior; (2) load transfer; (3) limits on matrix ductility to survive a given number of cyclic loadings; (4) fundamental parameters which govern thermal stresses; (5) vibration stresses; and (6) impact resistance. The resulting guidelines are presented in terms of simple equations which are suitable for the preliminary assessment of the merits of a particular high temperature composite in a specific application.

Multi-range force sensors utilizing shape memory alloys

DOEpatents

Varma, Venugopal K.

2003-04-15

The present invention provides a multi-range force sensor comprising a load cell made of a shape memory alloy, a strain sensing system, a temperature modulating system, and a temperature monitoring system. The ability of the force sensor to measure contact forces in multiple ranges is effected by the change in temperature of the shape memory alloy. The heating and cooling system functions to place the shape memory alloy of the load cell in either a low temperature, low strength phase for measuring small contact forces, or a high temperature, high strength phase for measuring large contact forces. Once the load cell is in the desired phase, the strain sensing system is utilized to obtain the applied contact force. The temperature monitoring system is utilized to ensure that the shape memory alloy is in one phase or the other.

An Improved Metal-Packaged Strain Sensor Based on A Regenerated Fiber Bragg Grating in Hydrogen-Loaded Boron–Germanium Co-Doped Photosensitive Fiber for High-Temperature Applications

PubMed Central

Tu, Yun; Ye, Lin; Zhou, Shao-Ping; Tu, Shan-Tung

2017-01-01

Local strain measurements are considered as an effective method for structural health monitoring of high-temperature components, which require accurate, reliable and durable sensors. To develop strain sensors that can be used in higher temperature environments, an improved metal-packaged strain sensor based on a regenerated fiber Bragg grating (RFBG) fabricated in hydrogen (H2)-loaded boron–germanium (B–Ge) co-doped photosensitive fiber is developed using the process of combining magnetron sputtering and electroplating, addressing the limitation of mechanical strength degradation of silica optical fibers after annealing at a high temperature for regeneration. The regeneration characteristics of the RFBGs and the strain characteristics of the sensor are evaluated. Numerical simulation of the sensor is conducted using a three-dimensional finite element model. Anomalous decay behavior of two regeneration regimes is observed for the FBGs written in H2-loaded B–Ge co-doped fiber. The strain sensor exhibits good linearity, stability and repeatability when exposed to constant high temperatures of up to 540 °C. A satisfactory agreement is obtained between the experimental and numerical results in strain sensitivity. The results demonstrate that the improved metal-packaged strain sensors based on RFBGs in H2-loaded B–Ge co-doped fiber provide great potential for high-temperature applications by addressing the issues of mechanical integrity and packaging. PMID:28241465

An Improved Metal-Packaged Strain Sensor Based on A Regenerated Fiber Bragg Grating in Hydrogen-Loaded Boron-Germanium Co-Doped Photosensitive Fiber for High-Temperature Applications.

PubMed

Tu, Yun; Ye, Lin; Zhou, Shao-Ping; Tu, Shan-Tung

2017-02-23

Local strain measurements are considered as an effective method for structural health monitoring of high-temperature components, which require accurate, reliable and durable sensors. To develop strain sensors that can be used in higher temperature environments, an improved metal-packaged strain sensor based on a regenerated fiber Bragg grating (RFBG) fabricated in hydrogen (H₂)-loaded boron-germanium (B-Ge) co-doped photosensitive fiber is developed using the process of combining magnetron sputtering and electroplating, addressing the limitation of mechanical strength degradation of silica optical fibers after annealing at a high temperature for regeneration. The regeneration characteristics of the RFBGs and the strain characteristics of the sensor are evaluated. Numerical simulation of the sensor is conducted using a three-dimensional finite element model. Anomalous decay behavior of two regeneration regimes is observed for the FBGs written in H₂-loaded B-Ge co-doped fiber. The strain sensor exhibits good linearity, stability and repeatability when exposed to constant high temperatures of up to 540 °C. A satisfactory agreement is obtained between the experimental and numerical results in strain sensitivity. The results demonstrate that the improved metal-packaged strain sensors based on RFBGs in H₂-loaded B-Ge co-doped fiber provide great potential for high-temperature applications by addressing the issues of mechanical integrity and packaging.

Brillouin distributed temperature sensing system for monitoring of submarine export cables of off-shore wind farms

NASA Astrophysics Data System (ADS)

Marx, Benjamin; Rath, Alexander; Kolm, Frederick; Schröder, Andreas; Buntebarth, Christian; Dreß, Albrecht; Hill, Wieland

2016-05-01

For high-voltage cables, the maximum temperature of the insulation must never be exceeded at any location and at any load condition. The local temperatures depend not only on the cable design and load history, but also on the local thermal environment of the cable. Therefore, distributed temperature monitoring of high-voltage cables is essential to ensure the integrity of the cable at high load. Especially, the load of the export cables of wind farms varies strongly in dependence on weather conditions. In this field study, we demonstrate the measurement performance of a new, robust Brillouin distributed temperature sensing system (Brillouin-DTS). The system is based on spontaneous Brillouin scattering and does not require a fibre loop. This is essential for long submarine high-voltage cables, where normally no loop can be formed in the seabed. It is completely passively cooled and does not contain any moving or wearing parts. The instrument is dedicated for use in industrial and other rough environments. With a measuring time below 10 min, the temperature resolution is better than 1 °C for distances up to 50 km. In the field study, the submarine export cable of an off-shore wind farm has been monitored. The temperature profile of the export cable shows several hot spots, mostly located at cable joints, and also several cold spots.

Effects of microbial loading and sporulation temperature on atmospheric plasma inactivation of Bacillus subtilis spores

NASA Astrophysics Data System (ADS)

Deng, X. T.; Shi, J. J.; Shama, G.; Kong, M. G.

2005-10-01

Current inactivation studies of Bacillus subtilis spores using atmospheric-pressure glow discharges (APGD) do not consider two important factors, namely microbial loading at the surface of a substrate and sporulation temperature. Yet these are known to affect significantly microbial resistance to heat and hydrogen peroxide. This letter investigates effects of microbial loading and sporulation temperature on spore resistance to APGD. It is shown that microbial loading can lead to a stacking structure as a protective shield against APGD treatment and that high sporulation temperature increases spore resistance by altering core water content and cross-linked muramic acid content of B. subtilis spores.

Strain Measurement System Developed for Biaxially Loaded Cruciform Specimens

NASA Technical Reports Server (NTRS)

Krause, David L.

2000-01-01

A new extensometer system developed at the NASA Glenn Research Center at Lewis Field measures test area strains along two orthogonal axes in flat cruciform specimens. This system incorporates standard axial contact extensometers to provide a cost-effective high-precision instrument. The device was validated for use by extensive testing of a stainless steel specimen, with specimen temperatures ranging from room temperature to 1100 F. In-plane loading conditions included several static biaxial load ratios, plus cyclic loadings of various waveform shapes, frequencies, magnitudes, and durations. The extensometer system measurements were compared with strain gauge data at room temperature and with calculated strain values for elevated-temperature measurements. All testing was performed in house in Glenn's Benchmark Test Facility in-plane biaxial load frame.

Fast loading ester fluorescent Ca2+ and pH indicators into pollen of Pyrus pyrifolia.

PubMed

Qu, Haiyong; Jiang, Xueting; Shi, Zebin; Liu, Lianmei; Zhang, Shaoling

2012-01-01

Loading of Ca(2+)-sensitive fluorescent probes into plant cells is an essential step to measure activities of free Ca(2+) ions in cytoplasm with a fluorescent imaging technique. Fluo-3 is one of the most suitable Ca(2+) indicators for CLSM. We loaded pollen with fluo-3/AM at three different temperatures. Fluo-3/AM was successfully loaded into pollen at both low (4°C) and high (37°C) temperatures. However, high loading temperature was best suited for pollen, because germination rate of pollen and growth of pollen tubes were relatively little impaired and loading time was shortened. Moreover, Ca(2+) distribution increased in the three apertures of pollen after hydration and showed a Ca(2+) gradient, similar to the tip of growing pollen tubes. The same protocol can be used with the AM-forms of other fluorescent dyes for effective labeling. When loading BCECF-AM into pollen at high temperature, the pollen did not show a pH gradient after hydration. Ca(2+) activities and fluxes had the same periodicity as pollen germination, but pH did not show the same phase and mostly lagged behind. However, the clear zone was alkaline when pollen tube growth was slowed or stopped and turned acidic when growth recovered. It is likely that apical pH(i) regulated pollen tube growth.

In situ fatigue loading stage inside scanning electron microscope

NASA Technical Reports Server (NTRS)

Telesman, Jack; Kantzos, Peter; Brewer, David

1988-01-01

A fatigue loading stage inside a scanning electron microscopy (SEM) was developed. The stage allows dynamic and static high-magnification and high-resolution viewing of the fatigue crack initiation and crack propagation processes. The loading stage is controlled by a closed-loop servohydraulic system. Maximum load is 1000 lb (4450 N) with test frequencies ranging up to 30 Hz. The stage accommodates specimens up to 2 inches (50 mm) in length and tolerates substantial specimen translation to view the propagating crack. At room temperature, acceptable working resolution is obtainable for magnifications ranging up to 10,000X. The system is equipped with a high-temperature setup designed for temperatures up to 2000 F (1100 C). The signal can be videotaped for further analysis of the pertinent fatigue damage mechanisms. The design allows for quick and easy interchange and conversion of the SEM from a loading stage configuration to its normal operational configuration and vice versa. Tests are performed entirely in the in-situ mode. In contrast to other designs, the NASA design has greatly extended the life of the loading stage by not exposing the bellows to cyclic loading. The loading stage was used to investigate the fatigue crack growth mechanisms in the (100)-oriented PWA 1480 single-crystal, nickel-based supperalloy. The high-magnification observations revealed the details of the crack growth processes.

Friction and oxidative wear of 440C ball bearing steels under high load and extreme bulk temperatures

NASA Technical Reports Server (NTRS)

Chaudhuri, Dilip K.; Slifka, Andrew J.; Siegwarth, James D.

1993-01-01

Unlubricated sliding friction and wear of 440C steels in an oxygen environment have been studied under a variety of load, speed, and temperature ranging from approximately -185 to 675 deg C. A specially designed test apparatus with a ball-on-flat geometry has been used for this purpose. The observed dependencies of the initial coefficient of friction, the average dynamic coefficient of friction, and the wear rate on load, speed, and test temperatures have been examined from the standpoint of existing theories of friction and wear. High contact temperatures are generated during the sliding friction, causing rapid oxidation and localized surface melting. A combination of fatigue, delamination, and loss of hardness due to tempering of the martensitic structure is responsible for the high wear rate observed and the coefficient of friction.

In vitro assessment of temperature change in the pulp chamber during cavity preparation.

PubMed

Oztürk, Bora; Uşümez, Aslihan; Oztürk, A Nilgun; Ozer, Füsun

2004-05-01

Tooth preparation with a high-speed handpiece may cause thermal harm to the dental pulp. This in vitro study evaluated the temperature changes in the pulp chamber during 4 different tooth preparation techniques and the effects of 3 different levels of water cooling. The tip of a thermocouple was positioned in the center of the pulp chamber of 120 extracted Shuman premolar teeth. Four different tooth preparation techniques were compared: (1) Low air pressure plus low load (LA/LL), (2) low air pressure plus high load (LA/HL), (3) high air pressure plus low load (HA/LL), and (4) high air pressure plus high load (HA/HL) in combination with 3 different water cooling rates. Control specimens were not water cooled; low water cooling consisted of 15 mL/min, and high water cooling consisted of 40 mL/min. Twelve different groups were established (n=10). An increase of 5.5 degrees C was regarded as critical value for pulpal health. The results were analyzed with a 3-factor ANOVA and Bonferroni adjusted Mann Whitney U test (alpha=.004). For all techniques without water cooling (LA/LL/0, LA/HL/0, HA/LL/0, and HA/HL/0), the average temperature rise within the pulpal chamber exceeded 5.5 degrees C during cavity preparation (7.1 degrees C; 8.9 degrees C; 11.4 degrees C, and 19.7 degrees C, respectively). When low water cooling was used with high air pressure and high load technique (HA/HL/15), the average temperature rise exceeded 5.5 degrees C limit (5.9 degrees C). However, when high water cooling (LA/LL/40, LA/HL/40, HA/LL/40, and HA/HL/40) was utilized, the critical 5.5 degrees C value was not reached with any air pressure or load (3.1 degrees C, 2.8 degrees C, 2.2 degrees C, and -1.8 degrees C, respectively). Within the limitations of this in vitro study, the results indicate that reducing the amount of water cooling or increasing air pressure and load during cavity preparation increased the temperature of the pulp chamber in extracted teeth.

Report on FY15 Two-Bar Thermal Ratcheting Test Results

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Yanli; Jetter, Robert I; Baird, Seth T

2015-06-22

Alloy 617 is a reference structural material for very high temperature components of advanced-gas cooled reactors with outlet temperatures in the range of . In order for designers to be able to use Alloy 617 for these high temperature components, Alloy 617 has to be approved for use in Section III (the nuclear section) of the American Society of Mechanical Engineers (ASME) Boiler and Pressure Vessel Code. A plan has been developed to submit a draft code for Alloy 617 to ASME Section III by 2015. However, the current rules in Subsection NH* for the evaluation of strain limits andmore » creep-fatigue damage using simplified methods based on elastic analysis have been deemed inappropriate for Alloy 617 at temperatures above . The rationale for this exclusion is that at higher temperatures it is not feasible to decouple plasticity and creep deformation, which is the basis for the current simplified rules. This temperature, , is well below the temperature range of interest for this material in High Temperature Gas Cooled Reactor (HTGR) applications. The only current alternative is, thus, a full inelastic analysis which requires sophisticated material models which have been formulated but not yet verified. To address this issue, proposed code rules have been developed which are based on the use of elastic-perfectly plastic (EPP) analysis methods and which are expected to be applicable to very high temperatures. These newly proposed rules also address a long-term objective to provide an option for more simple, comprehensive and easily applied rules than the current so called simplified rules These two-bar tests discussed herein are part of an ongoing series of tests with cyclic loading at high temperatures using specimens representing key features of potential component designs. The initial focus of the two-bar ratcheting test program, to verify the procedure for evaluation of strain limits for Alloy 617 at very high temperatures, has been expanded to respond to guidance from ASME Code committees that the proposed EPP methodology should also apply to other Subsection NH materials throughout their allowed temperature range. To support these objectives, two suites of tests have been accomplished during this reporting period. One suite addresses the issue of the response of Alloy 617 at a lower temperature with tests in range of 500 800oC and a few at 350 650°C. The other suite addresses the response of SS316H up to its current maximum allowed temperature of 1500°F (815°C) In the two-bar test methodology, the two bars can be viewed as specimens taken out of a tubular component across the wall thickness representing the inner wall element and the outer wall element respectively. The two bars are alternately heated and cooled under sustained axial loading to generate ratcheting. A sustained hold time is introduced at the hot extreme of the cycle to capture the accelerated ratcheting and strain accumulation due to creep. Since the boundary conditions are a combination of strain control and load control it is necessary to use two coupled servo-controlled testing machines to achieve the key features of the two-bar representation of actual component behavior. Two-bar thermal ratcheting test results with combinations of applied mean stresses, transient temperature difference and heating and cooling rates were recorded. Tests performed at heating and cooling rates of 30°C/min are comparable to a strain rate of 10 ⁻⁵/sec. At high mean stresses in tension the direction of ratcheting was in-phase with the load, e.g. tensile strain ratcheting under high tensile loading; however, at lower loads, strain ratcheting in compression was observed under net tensile mean stresses. The strain accumulation was proportional to the applied thermal load. However, there was a narrow range of applied load in which the high applied thermal loading did not result in significant strain accumulation. Unfortunately, when the proposed EPP strain limit evaluation rules were applied to the loading history for the two-bar configuration, the predicted narrow range of low strain accumulation did not coincide with the experimental data. However, by the use of inelastic analysis in conjunction with an analytic experiment it was possible to show that the EPP strain limit code case rules could be applied to high temperature structures where the stress and temperature is not uniform throughout which is the general case. Interestingly, the suite of tests on Alloy 617 at the lower temperature range of 500°C to 800oC showed good agreement with the proposed EPP strain limit rules with a much wider band of applied load that exhibited minimal ratcheting. The four tests conducted at the lower temperature range of 350°C to 650°C showed no ratcheting. The suite of tests on SS316H at a temperature range of 515°C to 815°C resembled the results from the tests on Alloy 617 at 650°C to 950°C. Both exhibited a narrow band of applied load wher...« less

Compliant Foil Journal Bearing Performance at Alternate Pressures and Temperatures

NASA Technical Reports Server (NTRS)

Bruckner, Robert J.; Puleo, Bernadette J.

2008-01-01

An experimental test program has been conducted to determine the highly loaded performance of current generation gas foil bearings at alternate pressures and temperatures. Typically foil bearing performance has been reported at temperatures relevant to turbomachinery applications but only at an ambient pressure of one atmosphere. This dearth of data at alternate pressures has motivated the current test program. Two facilities were used in the test program, the ambient pressure rig and the high pressure rig. The test program utilized a 35 mm diameter by 27 mm long foil journal bearing having an uncoated Inconel X-750 top foil running against a shaft with a PS304 coated journal. Load capacity tests were conducted at 3, 6, 9, 12, 15, 18, and 21 krpm at temperatures from 25 to 500 C and at pressures from 0.1 to 2.5 atmospheres. Results show an increase in load capacity with increased ambient pressure and a reduction in load capacity with increased ambient temperature. Below one-half atmosphere of ambient pressure a dramatic loss of load capacity is experienced. Additional lightly loaded foil bearing performance in nitrogen at 25 C and up to 48 atmospheres of ambient pressure has also been reported. In the lightly loaded region of operation the power loss increases for increasing pressure at a fixed load. Knowledge of foil bearing performance at operating conditions found within potential machine applications will reduce program development risk of future foil bearing supported turbomachines.

Cardiorespiratory parameters in draught horses before and after short term draught work pulling loads.

PubMed

Pérez, R; Recabarren, S E; Mora, G; Jara, C; Quijada, G; Hetz, E

1992-04-01

In order to establish the relationship between draught force and cardiorespiratory responses to exercise heart rate (HR), respiratory rate (RR), arterial and venous blood gases, pH, hemoglobin concentration and temperature were measured in five draught horses during rest, immediately after exercise and 30 min post-exercise under field conditions. A wagon equipped with an odometer and a hydraulic dynamometer was used for measuring distance and draught force. The wagon was loaded with 946 kg for the low load, 1,979 kg for the medium load and 2,994 kg for the high load, and drawn for a distance of 1,500 m. Draught force and load weight were linearly related. The response of the draught horse to low and medium load exercise was characterized by a moderate increase in HR, RR and temperature with no significant changes in arterial blood gases and pH. An increase in HR, RR and temperature was observed, whereas no changes in arterial PO2 and increases in venous PO2 were noticed after high load exercise. Slight increase in venous lactic acid concentration as a result of high load exercise was observed, suggesting that some anaerobic work was performed. However this was insufficient to produce changes in blood pH. The increase in metabolic requirements during the three levels of draught exercise was associated with increases in arterial hemoglobin concentration and oxygen content of blood.

A numerical and experimental study of temperature effects on deformation behavior of carbon steels at high strain rates

NASA Astrophysics Data System (ADS)

Pouya, M.; Winter, S.; Fritsch, S.; F-X Wagner, M.

2017-03-01

Both in research and in the light of industrial applications, there is a growing interest in methods to characterize the mechanical behavior of materials at high strain rates. This is particularly true for steels (the most important structural materials), where often the strain rate-dependent material behavior also needs to be characterized in a wide temperature range. In this study, we use the Finite Element Method (FEM), first, to model the compressive deformation behavior of carbon steels under quasi-static loading conditions. The results are then compared to experimental data (for a simple C75 steel) at room temperature, and up to testing temperatures of 1000 °C. Second, an explicit FEM model that captures wave propagation phenomena during dynamic loading is developed to closely reflect the complex loading conditions in a Split-Hopkinson Pressure Bar (SHPB) - an experimental setup that allows loading of compression samples with strain rates up to 104 s-1 The dynamic simulations provide a useful basis for an accurate analysis of dynamically measured experimental data, which considers reflected elastic waves. By combining numerical and experimental investigations, we derive material parameters that capture the strain rate- and temperature-dependent behavior of the C75 steel from room temperature to 1000 °C, and from quasi-static to dynamic loading.

Advances In High Temperature (Viscoelastoplastic) Material Modeling for Thermal Structural Analysis

NASA Technical Reports Server (NTRS)

Arnold, Steven M.; Saleeb, Atef F.

2005-01-01

Typical High Temperature Applications High Temperature Applications Demand High Performance Materials: 1) Complex Thermomechanical Loading; 2) Complex Material response requires Time-Dependent/Hereditary Models: Viscoelastic/Viscoplastic; and 3) Comprehensive Characterization (Tensile, Creep, Relaxation) for a variety of material systems.

An Indentation Technique for Nanoscale Dynamic Viscoelastic Measurements at Elevated Temperature

NASA Astrophysics Data System (ADS)

Ye, Jiping

2012-08-01

Determination of nano/micro-scale viscoelasticity is very important to understand the local rheological behavior and degradation phenomena of multifunctional polymer blend materials. This article reviews research results concerning the development of indentation techniques for making nanoscale dynamic viscoelastic measurements at elevated temperature. In the last decade, we have achieved breakthroughs in noise floor reduction in air and thermal load drift/noise reduction at high temperature before taking on the challenge of nanoscale viscoelastic measurements. A high-temperature indentation technique has been developed that facilitates viscoelastic measurements up to 200 °C in air and 500 °C in a vacuum. During the last year, two viscoelastic measurement methods have been developed by making a breakthrough in suppressing the contact area change at high temperature. One is a sharp-pointed time-dependent nanoindentation technique for microscale application and the other is a spherical time-dependent nanoindentation technique for nanoscale application. In the near future, we expect to lower the thermal load drift and load noise floor even more substantially.

Long-duration heat load measurement approach by novel apparatus design and highly efficient algorithm

NASA Astrophysics Data System (ADS)

Zhu, Yanwei; Yi, Fajun; Meng, Songhe; Zhuo, Lijun; Pan, Weizhen

2017-11-01

Improving the surface heat load measurement technique for vehicles in aerodynamic heating environments is imperative, regarding aspects of both the apparatus design and identification efficiency. A simple novel apparatus is designed for heat load identification, taking into account the lessons learned from several aerodynamic heating measurement devices. An inverse finite difference scheme (invFDM) for the apparatus is studied to identify its surface heat flux from the interior temperature measurements with high efficiency. A weighted piecewise regression filter is also proposed for temperature measurement prefiltering. Preliminary verification of the invFDM scheme and the filter is accomplished via numerical simulation experiments. Three specific pieces of apparatus have been concretely designed and fabricated using different sensing materials. The aerodynamic heating process is simulated by an inductively coupled plasma wind tunnel facility. The identification of surface temperature and heat flux from the temperature measurements is performed by invFDM. The results validate the high efficiency, reliability and feasibility of heat load measurements with different heat flux levels utilizing the designed apparatus and proposed method.

Effect of production microclimate on female thermal state with increased temperature and air humidity

NASA Technical Reports Server (NTRS)

Machablishvili, O. G.

1980-01-01

The thermal state of women during the effect of high air temperature and relative humidity with a varying degree of physical loads was studied. Parameters for air temperature, relative humidity, and air movement were established. It was established that in women the thermo-regulatory stress occurs at lower air temperatures and with lower physical loads than in men. The accumulation of heat in women was revealed with lower air temperature than in men. It is concluded that to preserve the normal physiological state of the female organism it is necessary to create more favorable microclimate conditions and decrease the physical loads.

Seal Technology for Hypersonic Vehicle and Propulsion: An Overview

NASA Technical Reports Server (NTRS)

Steinetz, Bruce M.

2008-01-01

Hypersonic vehicles and propulsion systems pose an extraordinary challenge for structures and materials. Airframes and engines require lightweight, high-temperature materials and structural configurations that can withstand the extreme environment of hypersonic flight. Some of the challenges posed include very high temperatures, heating of the whole vehicle, steady-state and transient localized heating from shock waves, high aerodynamic loads, high fluctuating pressure loads, potential for severe flutter, vibration, and acoustic loads and erosion. Correspondingly high temperature seals are required to meet these aggressive requirements. This presentation reviews relevant seal technology for both heritage (e.g. Space Shuttle, X-15, and X-38) vehicles and presents several seal case studies aimed at providing lessons learned for future hypersonic vehicle seal development. This presentation also reviews seal technology developed for the National Aerospace Plane propulsion systems and presents several seal case studies aimed at providing lessons learned for future hypersonic propulsion seal development.

Self-heating forecasting for thick laminate specimens in fatigue

NASA Astrophysics Data System (ADS)

Lahuerta, F.; Westphal, T.; Nijssen, R. P. L.

2014-12-01

Thick laminate sections can be found from the tip to the root in most common wind turbine blade designs. Obtaining accurate and reliable design data for thick laminates is subject of investigations, which include experiments on thick laminate coupons. Due to the poor thermal conductivity properties of composites and the material self-heating that occurs during the fatigue loading, high temperature gradients may appear through the laminate thickness. In the case of thick laminates in high load regimes, the core temperature might influence the mechanical properties, leading to premature failures. In the present work a method to forecast the self-heating of thick laminates in fatigue loading is presented. The mechanical loading is related with the laminate self-heating, via the cyclic strain energy and the energy loss ratio. Based on this internal volumetric heat load a thermal model is built and solved to obtain the temperature distribution in the transient state. Based on experimental measurements of the energy loss factor for 10mm thick coupons, the method is described and the resulting predictions are compared with experimental surface temperature measurements on 10 and 30mm UD thick laminate specimens.

A furnace with rotating load frame for in situ high temperature deformation and creep experiments in a neutron diffraction beam line

DOE Office of Scientific and Technical Information (OSTI.GOV)

Reiche, H. M.; New Mexico State University, Las Cruces, New Mexico 88003; Vogel, S. C.

2012-05-15

A resistive furnace combined with a load frame was built that allows for in situ neutron diffraction studies of high temperature deformation, in particular, creep. A maximum force of 2700 N can be applied at temperatures up to 1000 deg. C. A load control mode permits studies of, e.g., creep or phase transformations under applied uni-axial stress. In position control, a range of high temperature deformation experiments can be achieved. The examined specimen can be rotated up to 80 deg. around the vertical compression axis allowing texture measurements in the neutron time-of-flight diffractometer HIPPO (High Pressure - Preferred Orientation). Wemore » present results from the successful commissioning, deforming a Zr-2.5 wt.% Nb cylinder at 975 deg. C. The device is now available for the user program of the HIPPO diffractometer at the LANSCE (Los Alamos Neutron Science Center) user facility.« less

An experimental system for high temperature X-ray diffraction studies with in situ mechanical loading

PubMed Central

Oswald, Benjamin B.; Schuren, Jay C.; Pagan, Darren C.; Miller, Matthew P.

2013-01-01

An experimental system with in situ thermomechanical loading has been developed to enable high energy synchrotron x-ray diffraction studies of crystalline materials. The system applies and maintains loads of up to 2250 N in uniaxial tension or compression at a frequency of up to 100 Hz. The furnace heats the specimen uniformly up to a maximum temperature of 1200 °C in a variety of atmospheres (oxidizing, inert, reducing) that, combined with in situ mechanical loading, can be used to mimic processing and operating conditions of engineering components. The loaded specimen is reoriented with respect to the incident beam of x-rays using two rotational axes to increase the number of crystal orientations interrogated. The system was used at the Cornell High Energy Synchrotron Source to conduct experiments on single crystal silicon and polycrystalline Low Solvus High Refractory nickel-based superalloy. The data from these experiments provide new insights into how stresses evolve at the crystal scale during thermomechanical loading and complement the development of high-fidelity material models. PMID:23556825

High temperature lubricating process

DOEpatents

Taylor, R.W.; Shell, T.E.

1979-10-04

It has been difficult to provide adequate lubrication for load bearing, engine components when such engines are operating in excess of about 475/sup 0/C. The present invention is a process for providing a solid lubricant on a load bearing, solid surface, such as in an engine being operated at temperatures in excess of about 475/sup 0/C. The process comprises contacting and maintaining the following steps: a gas phase is provided which includes at least one component reactable in a temperature dependent reaction to form a solid lubricant; the gas phase is contacted with the load bearing surface; the load bearing surface is maintained at a temperature which causes reaction of the gas phase component and the formation of the solid lubricant; and the solid lubricant is formed directly on the load bearing surface. The method is particularly suitable for use with ceramic engines.

High temperature lubricating process

DOEpatents

Taylor, Robert W.; Shell, Thomas E.

1982-01-01

It has been difficult to provide adaquate lubrication for load bearing, engine components when such engines are operating in excess of about 475.degree. C. The present invention is a process for providing a solid lubricant on a load bearing, solid surface (14), such as in an engine (10) being operated at temperatures in excess of about 475.degree. C. The process comprises contacting and maintaining steps. A gas phase (42) is provided which includes at least one component reactable in a temperature dependent reaction to form a solid lubricant. The gas phase is contacted with the load bearing surface. The load bearing surface is maintained at a temperature which causes reaction of the gas phase component and the formation of the solid lubricant. The solid lubricant is formed directly on the load bearing surface. The method is particularly suitable for use with ceramic engines.

Adaptive Beam Loading Compensation in Room Temperature Bunching Cavities

DOE Office of Scientific and Technical Information (OSTI.GOV)

Edelen, J. P.; Chase, B. E.; Cullerton, E.

In this paper we present the design, simulation, and proof of principle results of an optimization based adaptive feedforward algorithm for beam-loading compensation in a high impedance room temperature cavity. We begin with an overview of prior developments in beam loading compensation. Then we discuss different techniques for adaptive beam loading compensation and why the use of Newton?s Method is of interest for this application. This is followed by simulation and initial experimental results of this method.

High density load bearing insulation peg

DOEpatents

Nowobilski, Jeffert J.; Owens, William J.

1985-01-01

A high density peg which can support a large load and exhibits excellent thermal resistance produced by a method wherein the peg is made in compliance with specified conditions of time, temperature and pressure.

Effect of the Conditions of the Nanostructuring Frictional Treatment Process on the Structural and Phase States and the Strengthening of Metastable Austenitic Steel

NASA Astrophysics Data System (ADS)

Makarov, A. V.; Skorynina, P. A.; Yurovskikh, A. S.; Osintseva, A. L.

2017-12-01

The effect of the multiplicity of frictional loading with a sliding synthetic diamond indenter at room temperature in an argon medium and the temperature of loading in the range of -196 to +250°C on the phase composition, fine structure, and micromechanical properties of the surface layer of metastable austenitic chromium-nickel steel has been studied. It has been established that the completeness of the strain-induced martensitic γ → α' transformation in the surface layer of steel is determined by the loading multiplicity and temperature, as well as the level of strengthening grows with an increase in the frictional loading multiplicity, but weakly depends on the frictional treatment temperature. According to the microindentation data, the characteristics of the surface layer strength and resistance to elastic and plastic deformation are improved with an increase in the frictional loading multiplicity. Frictional treatment by scanning with a synthetic diamond indenter at room and negative temperatures provides high quality for the treated surface with a low roughness parameter ( Ra = 80.115 nm), and an increase in the frictional loading temperature to 150-250°C leads to the development of a seizure and growth in Ra to 195-255 nm. Using transmission electron microscopy (TEM), it has been shown that frictional treatment results in the formation of nanocrystalline and fragmented submicrocrystalline structures of strain-induced α'-martensite (at a loading temperature of -196°C) and austenite (at a loading temperature of +250°C) in the surface layer of steel alongside with two-phase martensitic-austenitic structures (at a loading temperature of +20°C).

Effects of Potassium loading and thermal aging on K/Pt/Al2O3 high-temperature lean NOx trap catalysts

DOE Office of Scientific and Technical Information (OSTI.GOV)

Luo, Jinyong; Gao, Feng; Kim, Do Heui

2014-03-31

The effects of K loading and thermal aging on the structural properties and high temperature performance of Pt/K/Al2O3 lean NOx trap (LNT) catalysts were investigated using in situ X-ray diffraction (XRD), temperature-programmed decomposition/desorption of NOx (NOx-TPD), transmission electron microscopy (TEM), NO oxidation and NOx storage tests. In situ XRD results demonstrate that KNO3 becomes extremely mobile on the Al2O3 surface, and experiences complex transformations between orthorhombic and rhombohedral structures, accompanied by sintering, melting and thermal decomposition upon heating. NOx storage results show an optimum K loading around 10% for the best performance at high temperatures. At lower K loadings wheremore » the majority of KNO3 stays as a surface layer, the strong interaction between KNO3 and Al2O3 promotes KNO3 decomposition and deteriorates high-temperature performance. At K loadings higher than 10%, the performance drop is not caused by NOx diffusion limitations as for the case of barium-based LNTs, but rather from the blocking of Pt sites by K species, which adversely affects NO oxidation. Thermal aging at 800 ºC severely deactivates the Pt/K/Al2O3 catalysts due to Pt sintering. However, in the presence of potassium, some Pt remains in a dispersed and oxidized form. These Pt species interact strongly with K and, therefore, do not sinter. After a reduction treatment, these Pt species remain finely dispersed, contributing to a partial recovery of NOx storage performance.« less

Buckling of Thermoviscoelastic Structures Under Temporal and Spatial Temperature Variations

NASA Technical Reports Server (NTRS)

Tsuyuki, Richard; Knauss, Wolfgang G.

1992-01-01

The problem of lateral instability of a viscoelastic in-plane loaded structure is considered in terms of thermorheolgically simple materials. As an example of a generally in-plane loaded structure, we examine the simple column under axial load: Both cyclic loading is considered (with constant or in-phase variable temperature excursions) as well as the case of constant load in the presence of thermal gradients through the thickness of the structure. The latter case involves a continuous movement of the neutral axis from the center to the colder side and then back to the center. In both cases, temperature has a very strong effect on the instability evolution, and under in-phase thermal cycling the critical loads are reduced compared to those at constant temperatures. The primary effect of thermal gradients beyond that of thermally-induced rate accelerations is occasioned by the generation of an "initial imperfection" or "structural bowing." Because the coefficient of thermal expansion tends to be large for many polymeric materials, it it may be necessary to take special care in lay-up design of composite structures intended for use under compressive loads in high-temperature applications. Finally, the implications for the temperature sensitivities of composites to micro-instability (fiber crimping) are also apparent from the results delineated here.

Characterization and prediction of rate-dependent flexibility in lumbar spine biomechanics at room and body temperature.

PubMed

Stolworthy, Dean K; Zirbel, Shannon A; Howell, Larry L; Samuels, Marina; Bowden, Anton E

2014-05-01

The soft tissues of the spine exhibit sensitivity to strain-rate and temperature, yet current knowledge of spine biomechanics is derived from cadaveric testing conducted at room temperature at very slow, quasi-static rates. The primary objective of this study was to characterize the change in segmental flexibility of cadaveric lumbar spine segments with respect to multiple loading rates within the range of physiologic motion by using specimens at body or room temperature. The secondary objective was to develop a predictive model of spine flexibility across the voluntary range of loading rates. This in vitro study examines rate- and temperature-dependent viscoelasticity of the human lumbar cadaveric spine. Repeated flexibility tests were performed on 21 lumbar function spinal units (FSUs) in flexion-extension with the use of 11 distinct voluntary loading rates at body or room temperature. Furthermore, six lumbar FSUs were loaded in axial rotation, flexion-extension, and lateral bending at both body and room temperature via a stepwise, quasi-static loading protocol. All FSUs were also loaded using a control loading test with a continuous-speed loading-rate of 1-deg/sec. The viscoelastic torque-rotation response for each spinal segment was recorded. A predictive model was developed to accurately estimate spine segment flexibility at any voluntary loading rate based on measured flexibility at a single loading rate. Stepwise loading exhibited the greatest segmental range of motion (ROM) in all loading directions. As loading rate increased, segmental ROM decreased, whereas segmental stiffness and hysteresis both increased; however, the neutral zone remained constant. Continuous-speed tests showed that segmental stiffness and hysteresis are dependent variables to ROM at voluntary loading rates in flexion-extension. To predict the torque-rotation response at different loading rates, the model requires knowledge of the segmental flexibility at a single rate and specified temperature, and a scaling parameter. A Bland-Altman analysis showed high coefficients of determination for the predictive model. The present work demonstrates significant changes in spine segment flexibility as a result of loading rate and testing temperature. Loading rate effects can be accounted for using the predictive model, which accurately estimated ROM, neutral zone, stiffness, and hysteresis within the range of voluntary motion. Copyright © 2014 Elsevier Inc. All rights reserved.

The stress relaxation of cement clinkers under high temperature

NASA Astrophysics Data System (ADS)

Wang, Xiufang; Bao, Yiwang; Liu, Xiaogen; Qiu, Yan

2015-12-01

The energy consumption of crushing is directly affected by the mechanical properties of cement materials. This research provides a theoretical proof for the mechanism of the stress relaxation of cement clinkers under high temperature. Compression stress relaxation under various high temperatures is discussed using a specially developed load cell, which can measure stress and displacement under high temperatures inside an autoclave. The cell shows that stress relaxation dramatically increases and that the remaining stress rapidly decreases with an increase in temperature. Mechanical experiments are conducted under various temperatures during the cooling process to study the changes in the grinding resistance of the cement clinker with temperature. The effects of high temperature on the load-displacement curve, compressive strength, and elastic modulus of cement clinkers are systematically studied. Results show that the hardening phenomenon of the clinker becomes apparent with a decrease in temperature and that post-peak behaviors manifest characteristics of the transformation from plasticity to brittleness. The elastic modulus and compressive strength of cement clinkers increase with a decrease in temperature. The elastic modulus increases greatly when the temperature is lower than 1000 °C. The compressive strength of clinkers increases by 73.4% when the temperature drops from 1100 to 800 °C.

Fluid mass and thermal loading effects on the modal characteristics of space shuttle main engine liquid oxygen inlet splitter vanes

NASA Technical Reports Server (NTRS)

Panossian, H. V.; Boehnlein, J. J.

1987-01-01

An analysis and evaluation of experimental modal survey test data on the variations of modal characteristics induced by pressure and thermal loading events are presented. Extensive modal survey tests were carried out on a Space Shuttle Main Engine (SSME) test article using liquid nitrogen under cryogenic temperatures and high pressures. The results suggest that an increase of pressure under constant cryogenic temperature or a decrease of temperature under high pressure induces an upward shift of frequencies of various modes of the structures.

Arrays of Regenerated Fiber Bragg Gratings in Non-Hydrogen-Loaded Photosensitive Fibers for High-Temperature Sensor Networks

PubMed Central

Lindner, Eric; Chojetztki, Christoph; Brueckner, Sven; Becker, Martin; Rothhardt, Manfred; Vlekken, Johan; Bartelt, Hartmut

2009-01-01

We report about the possibility of using regenerated fiber Bragg gratings generated in photosensitive fibers without applying hydrogen loading for high temperature sensor networks. We use a thermally induced regenerative process which leads to a secondary increase in grating reflectivity. This refractive index modification has shown to become more stable after the regeneration up to temperatures of 600 °C. With the use of an interferometric writing technique, it is possible also to generate arrays of regenerated fiber Bragg gratings for sensor networks. PMID:22408510

High density load bearing insulation peg

DOEpatents

Nowobilski, J.J.; Owens, W.J.

1985-01-29

A high density peg is disclosed which can support a large load and exhibits excellent thermal resistance produced by a method wherein the peg is made in compliance with specified conditions of time, temperature and pressure. 4 figs.

A Study of the Efficiency of High-strength, Steel, Cellular-core Sandwich Plates in Compression

NASA Technical Reports Server (NTRS)

Johnson, Aldie E , Jr; Semonian, Joseph W

1956-01-01

Structural efficiency curves are presented for high-strength, stainless-steel, cellular-core sandwich plates of various proportions subjected to compressive end loads for temperatures of 80 F and 600 F. Optimum proportions of sandwich plates for any value of the compressive loading intensity can be determined from the curves. The efficiency of steel sandwich plates of optimum proportions is compared with the efficiency of solid plates of high-strength steel and aluminum and titanium alloys at the two temperatures.

Thermal activation in Au-based bulk metallic glass characterized by high-temperature nanoindentation

NASA Astrophysics Data System (ADS)

Yang, Bing; Wadsworth, Jeffrey; Nieh, Tai-Gang

2007-02-01

High-temperature nanoindentation experiments have been conducted on a Au49Ag5.5Pd2.3Cu26.9Si16.3 bulk metallic glass from 30to140°C, utilizing loading rates ranging from 0.1to100mN/s. Generally, the hardness decreased with increasing temperature. An inhomogeneous-to-homogeneous flow transition was clearly observed when the test temperature approached the glass transition temperature. Analyses of the pop-in pattern and hardness variation showed that the inhomogeneous-to-homogeneous transition temperature was loading-rate dependent. Using a free-volume model, the authors deduced the size of the basic flow units and the activation energy for the homogeneous flow. In addition, the strain rate dependency of the transition temperature was predicted.

Effects of stress ratio on the temperature-dependent high-cycle fatigue properties of alloy steels

NASA Astrophysics Data System (ADS)

Lü, Zhi-yang; Wan, Ao-shuang; Xiong, Jun-jiang; Li, Kuang; Liu, Jian-zhong

2016-12-01

This paper addresses the effects of stress ratio on the temperature-dependent high-cycle fatigue (HCF) properties of alloy steels 2CrMo and 9CrCo, which suffer from substantial vibrational loading at small stress amplitude, high stress ratio, and high frequency in the high-temperature environments in which they function as blade and rotor spindle materials in advanced gas or steam turbine engines. Fatigue tests were performed on alloy steels 2CrMo and 9CrCo subjected to constant-amplitude loading at four stress ratios and at four and three temperatures, respectively, to determine their temperature-dependent HCF properties. The interaction mechanisms between high temperature and stress ratio were deduced and compared with each other on the basis of the results of fractographic analysis. A phenomenological model was developed to evaluate the effects of stress ratio on the temperature-dependent HCF properties of alloy steels 2CrMo and 9CrCo. Good correlation was achieved between the predictions and actual experiments, demonstrating the practical and effective use of the proposed method.

Fracture Mechanisms of Zirconium Diboride Ultra-High Temperature Ceramics under Pulse Loading

NASA Astrophysics Data System (ADS)

Skripnyak, Vladimir V.; Bragov, Anatolii M.; Skripnyak, Vladimir A.; Lomunov, Andrei K.; Skripnyak, Evgeniya G.; Vaganova, Irina K.

2015-06-01

Mechanisms of failure in ultra-high temperature ceramics (UHTC) based on zirconium diboride under pulse loading were studied experimentally by the method of SHPB and theoretically using the multiscale simulation method. The obtained experimental and numerical data are evidence of the quasi-brittle fracture character of nanostructured zirconium diboride ceramics under compression and tension at high strain rates and the room temperatures. Damage of nanostructured porous zirconium diboride -based UHTC can be formed under stress pulse amplitude below the Hugoniot elastic limit. Fracture of nanostructured ultra-high temperature ceramics under pulse and shock-wave loadings is provided by fast processes of intercrystalline brittle fracture and relatively slow processes of quasi-brittle failure via growth and coalescence of microcracks. A decrease of the shear strength can be caused by nano-voids clusters in vicinity of triple junctions between ceramic matrix grains and ultrafine-grained ceramics. This research was supported by grants from ``The Tomsk State University Academic D.I. Mendeleev Fund Program'' and also N. I. Lobachevski State University of Nizhny Novgorod (Grant of post graduate mobility).

In-Plane Shear Testing of Medium and High Modulus Woven Graphite Fiber Reinforced/Polyimide Composites

NASA Technical Reports Server (NTRS)

Gentz, M.; Armentrout, D.; Rupnowski, P.; Kumosa, L.; Shin, E.; Sutter, J. K.; Kumosa, M.

2004-01-01

Iosipescu shear tests were performed at room temperature and at 316 C (600 F) o woven composites with either M40J or M60J graphite fibers and PMR-II-50 polyimide resin matrix. The composites were tested as supplied and after thermo-cycling, with the thermo-cycled composites being tested under dry and wet conditions. Acoustic emission (AE) was monitored during the room and high temperature Iosipescu experiments. The shear stresses at the maximum loads and the shear stresses at the significant onset of AE were determined for the composites as function of temperature and conditioning. The combined effects of thermo-cycling and moisture on the strength and stiffness properties of the composites were evaluated. It was determined that the room and high temperature shear stresses at the maximum loads were unaffected by conditioning. However, at room temperature the significant onset of AE was affected by conditioning; the thermal conditioned wet specimens showed the highest shear stress at the onset of AE followed by thermal-conditioned and then as received specimens. Also, at igh temperature the significant onset of AE occurred in some specimens after the maximum load due to the viscoelastoplastic nature of the matrix material.

Properties of a Ni(sub 19.5)Pd(sub 30)Ti(sub 50.5) high-temperature shape memory alloy in tension and compression

NASA Technical Reports Server (NTRS)

Noebe, Ronald; Padula, Santo, II; Bigelow, Glen; Rios, Orlando; Garg, Anita; Lerch, Brad

2006-01-01

Potential applications involving high-temperature shape memory alloys have been growing in recent years. Even in those cases where promising new alloys have been identified, the knowledge base for such materials contains gaps crucial to their maturation and implementation in actuator and other applications. We begin to address this issue by characterizing the mechanical behavior of a Ni19.5Pd30Ti50.5 high-temperature shape memory alloy in both uniaxial tension and compression at various temperatures. Differences in the isothermal uniaxial deformation behavior were most notable at test temperatures below the martensite finish temperature. The elastic modulus of the material was very dependent on strain level; therefore, dynamic Young#s Modulus was determined as a function of temperature by an impulse excitation technique. More importantly, the performance of a thermally activated actuator material is dependent on the work output of the alloy. Consequently, the strain-temperature response of the Ni19.5Pd30Ti50.5 alloy under various loads was determined in both tension and compression and the specific work output calculated and compared in both loading conditions. It was found that the transformation strain and thus, the specific work output were similar regardless of the loading condition. Also, in both tension and compression, the strain-temperature loops determined under constant load conditions did not close due to the fact that the transformation strain during cooling was always larger than the transformation strain during heating. This was apparently the result of permanent plastic deformation of the martensite phase with each cycle. Consequently, before this alloy can be used under cyclic actuation conditions, modification of the microstructure or composition would be required to increase the resistance of the alloy to plastic deformation by slip.

Temperature Dependences of Torque Generation and Membrane Voltage in the Bacterial Flagellar Motor

PubMed Central

Inoue, Yuichi; Baker, Matthew A.B.; Fukuoka, Hajime; Takahashi, Hiroto; Berry, Richard M.; Ishijima, Akihiko

2013-01-01

In their natural habitats bacteria are frequently exposed to sudden changes in temperature that have been shown to affect their swimming. With our believed to be new methods of rapid temperature control for single-molecule microscopy, we measured here the thermal response of the Na+-driven chimeric motor expressed in Escherichia coli cells. Motor torque at low load (0.35 μm bead) increased linearly with temperature, twofold between 15°C and 40°C, and torque at high load (1.0 μm bead) was independent of temperature, as reported for the H+-driven motor. Single cell membrane voltages were measured by fluorescence imaging and these were almost constant (∼120 mV) over the same temperature range. When the motor was heated above 40°C for 1–2 min the torque at high load dropped reversibly, recovering upon cooling below 40°C. This response was repeatable over as many as 10 heating cycles. Both increases and decreases in torque showed stepwise torque changes with unitary size ∼150 pN nm, close to the torque of a single stator at room temperature (∼180 pN nm), indicating that dynamic stator dissociation occurs at high temperature, with rebinding upon cooling. Our results suggest that the temperature-dependent assembly of stators is a general feature of flagellar motors. PMID:24359752

Waiting time effect of a GM type orifice pulse tube refrigerator

NASA Astrophysics Data System (ADS)

Zhu, Shaowei; Kakimi, Yasuhiro; Matsubara, Yoichi

In a general GM type orifice pulse tube refrigerator, there are two short periods during which both the high pressure valve and the low pressure valve are closed in one cycle. We call the short period `waiting time'. The pressure differences across the high pressure valve and the low pressure valve are decreased by using long waiting time. The pressure difference loss is decreased. Thus, the cooling capacity and the efficiency are increased, and the no-load temperature is decreased. The mechanism of the waiting time is discussed with numerical analysis and verified by experiments. Experiments show that there is an optimum waiting time for the no-load temperature, the cooling capacity and the efficiency, respectively. The no-load temperature of 40.3 K was achieved with a 90° waiting time. The cooling capacity of 58 W at 80 K was achieved with a 60° waiting time. The no-load temperature of 45.1 K and the cooling capacity of 45 W at 80 K were achieved with a 1° waiting time.

Damage accumulation in titanium matrix composites under generic hypersonic vehicle flight simulation and sustained loads

DOE Office of Scientific and Technical Information (OSTI.GOV)

Johnson, W.S.; Mirdamadi, M.; Bakuckas, J.G. Jr.

1996-12-31

Titanium matrix composites (TMC), such as Ti-15V-3Cr-3Al-3Sn (Ti-15-3) reinforced with continuous silicon-carbide fibers (SCS-6), are being evaluated for use in hypersonic vehicles and advanced gas turbine engines where high strength-to-weight and high stiffness-to-weight ratios at elevated temperatures are critical. Such applications expose the composite to mechanical fatigue loading as well as thermally induced cycles. The damage accumulation behavior of a [0/90]2s laminate made of Ti-15V-3Cr-3Al-3Sn (Ti-15-3) reinforced with continuous silicon-carbide fibers (SCS-6) subjected to a simulated generic hypersonic flight profile, portions of the flight profile, and sustained loads was evaluated experimentally. Portions of the flight profile were used separately tomore » isolate combinations of load and time at temperature that influenced the fatigue behavior of the composite. Sustained load tests were also conducted and the results were compared with the fatigue results under the flight profile and its portions. The test results indicated that the fatigue strength of this materials system is considerably reduced by a combination of load and time at temperature.« less

Special considerations for qualifying thin films for super pressure pumpkin ultra long duration balloon missions

NASA Astrophysics Data System (ADS)

Said, Magdi A.

2004-01-01

The assessment of creep and dynamic response behaviors on materials intended for ultra long duration balloon (ULDB) applications is essential. The first provides needed information for design and fabrication. The second ensures that the film is sufficiently tough to survive the dynamic events during launch and ascent. Characterization and assessment of these two important parameters are discussed in this paper. Visco-elastic behavior of materials in a loaded structure, such as the ULDB film change their geometry significantly over time under load causing possible changes in the load path and the stress distribution. These changes must be held in check to satisfy the functional requirements of the structure over its service life. Typically, the balloon experiences during its service life various environmental conditions each with a different creep response. These are characterized by a simplified load temperature history for the purpose of lifetime response assessment. At mid-latitudes a significant portion of the service life is spent at night, i.e., at low temperature and low load; for the ULDB film this night-time contribution to creep is negligible. By contrast, flight exposure in an Antarctic summer is at an almost constant high temperature and corresponding high pressure. This paper presents the creep behavior of the ULDB film as a function of load, temperature, and time along with an overview of its implementation in the design. In addition, it presents a quantitative assessment on the toughness of the material under dynamic "Snatch" loading.

Nitrogen removal via nitrite from seawater contained sewage.

PubMed

Peng, Yongzhen; Yu, De-Shuang; Liang, Dawei; Zhu, Guibing

2004-01-01

Under the control of both pH and the concentration of free ammonia (FA), the nitrification-denitrification via nitrite pathway was accomplished in SBR to achieve enhanced biological nitrogen removal from seawater contained wastewater, which is used to flush toilet, under relatively high salinity. Several parameters including salinity, temperature, pH, and NH4+-N loading rate were studied to evaluate their effects. The results indicate that at different salinity the nitrogen removal efficiency is relative to ammonia-nitrogen loading rate. The nitrogen removal efficiency reaches above 90% when the NH4+-N loading does not exceed 0.15 kg NH4+-N/kg MLSS d. With the salinity increasing, the ammonia-nitrogen loading rate should be lowered to obtain high removal efficiency. The evaluation of temperature effect shows that nitrogen removal efficiency is promoted twice when reaction temperature is elevated from 20 to 30 degrees C. Moderately high pH in the range of 7.5-8.5 has advantage to achieve effective nitrification-denitrification via nitrite, the process of which is caused by the selective inhibition of free ammonia (FA).

Effects of High and Low Temperature on the Tensile Strength of Glass Fiber Reinforced Polymer Composites

NASA Astrophysics Data System (ADS)

Kumarasamy, S.; Shukur Zainol Abidin, M.; Abu Bakar, M. N.; Nazida, M. S.; Mustafa, Z.; Anjang, A.

2018-05-01

In this paper, the tensile performance of glass fiber reinforced polymer (GFRP) composites at high and low temperature was experimentally evaluated. GFRP laminates were manufactured using the wet hand lay-up assisted by vacuum bag, which has resulted in average fibre volume fraction of 0.45. Using simultaneous heating/cooling and loading, glass fiber epoxy and polyester laminates were evaluated for their mechanical performance in static tensile loading. In the elevated temperature environment test, the tension mechanical properties; stress and modulus were reduced with increasing temperature from 25°C to 80°C. Results of low temperature environment from room temperature to a minimum temperature of -20°C, indicated that there is no considerable effect on the tensile strength, however a slight decrease of tensile modulus were observed on the GFRP laminates. The results obtained from the research highlight the structural survivability on tensile properties at low and high temperature of the GFRP laminates.

Air temperature gradient in large industrial hall

NASA Astrophysics Data System (ADS)

Karpuk, Michał; Pełech, Aleksander; Przydróżny, Edward; Walaszczyk, Juliusz; Szczęśniak, Sylwia

2017-11-01

In the rooms with dominant sensible heat load, volume airflow depends on many factors incl. pre-established temperature difference between exhaust and supply airflow. As the temperature difference is getting higher, airflow volume drops down, consequently, the cost of AHU is reduced. In high industrial halls with air exhaust grids located under the ceiling additional temperature gradient above working zone should be taken into consideration. In this regard, experimental research of the vertical air temperature gradient in high industrial halls were carried out for the case of mixing ventilation system The paper presents the results of air temperature distribution measurements in high technological hall (mechanically ventilated) under significant sensible heat load conditions. The supply airflow was delivered to the hall with the help of the swirl diffusers while exhaust grids were located under the hall ceiling. Basing on the air temperature distribution measurements performed on the seven pre-established levels, air temperature gradient in the area between 2.0 and 7.0 m above the floor was calculated and analysed.

Pressure and temperature effects on fuels with varying octane sensitivity at high load in SI engines

DOE PAGES

Szybist, James P.; Splitter, Derek A.

2017-01-06

The octane sensitivity (S), defined as the difference between the Research Octane Number (RON) and the Motor Octane Number (MON), is of increasing interest in spark ignition (SI) engines because of its relevance to knock resistance at boosted high load conditions. In this study, three fuels with nearly constant RON (99.2-100) and varying S (S = 0, 6.5, and 12) are operated at the knock limited spark advance (KLSA) at nominal engine loads of 10, 15, and 20 bar IMEP in a single cylinder SI engine with side-mount direct injection fueling, at λ =1 stoichiometry. At each load condition, themore » intake manifold temperature is swept from 35 °C to 95 °C to alter the temperature and pressure history of the charge. Results show that at the 10 bar IMEP condition, knock resistance is inversely proportional to fuel S where the S=0 fuel is the most knock resist, but as load increases the trend reverses and knock resistance becomes proportional to fuel S, and the S=12 fuel is the most knock resistant. The reversal of knock resistance as a function of S with load it is attributed to changing fuel ignition delay, as bulk gas intermediate temperature heat release (ITHR) is observed for the S = 0 several crank angles prior to the spark command and ITHR magnitude is a function of increasing intake temperature. As intake temperature continued to increase, the S=0 fuel transitioned from ITHR to low-temperature heat release (LTHR) prior to the spark event. At the highest load and intake temperature, 95 C, the S=0 fuel exhibits distinct LTHR and negative temperature coefficient (NTC), and the intermediate S value fuel (S=6.5) exhibited distinct ITHR behavior several crank angles prior to the spark command. However, for the tested conditions, the S=12 fuel exhibits neither ITHR nor LTHR. To understand the measured trends, chemical kinetic modeling is used to elucidate the fuel specific dependencies on in-cylinder temperature and pressure history. Lastly, the bulk gas composition change that occurs for fuels and conditions exhibiting ITHR and LTHR is analyzed in the modeling, including their implications on flame speed and combustion stability at late phasing. Furthermore, the combined findings illustrate the commonality and utility of fuel S, ITHR, LTHR, and NTC across a wide range of conditions, and the associated implications of fuel S in highly boosted modern GDI SI engines relative to the RON and MON tests.« less

Peg supported thermal insulation panel

DOEpatents

Nowobilski, Jeffert J.; Owens, William J.

1985-01-01

A thermal insulation panel which is lightweight, load bearing, accommodates thermal stress, and has excellent high temperature insulation capability comprising high performance insulation between thin metal walls supported by high density, high strength glass pegs made in compliance with specified conditions of time, temperature and pressure.

Prediction of Fretting Crack Location and Orientation in a Single Crystal Nickel Alloy

NASA Technical Reports Server (NTRS)

Matlik, J. F.; Farris, T. N.; Haynes, J.; Swanson, G. R.; Ham-Battista, G.

2005-01-01

Fretting is a structural damage mechanism arising between two nominally clamped surfaces subjected to an oscillatory loading. A critical location for fretting induced damage has been identified at the blade/disk and blade/damper interfaces of gas turbine engine turbomachinery and space propulsion components. The high- temperature, high-frequency loading environment seen by these components lead to severe stress gradients at the edge-of-contact that could potentially foster crack growth leading to component failure. These contact stresses drive crack nucleation in fretting and are very sensitive to the geometry of the contacting bodies, the contact loads, materials, temperature, and contact surface tribology (friction). Recently, a high-frequency, high-temperature load frame has been designed for experimentally investigating fretting damage of single crystal nickel materials employed in aircraft and spacecraft turbomachinery. A modeling method for characterizing the fretting stresses of the spherical fretting contact stress behavior in this experiment is developed and described. The calculated fretting stresses for a series of experiments are then correlated to the observed fretting damage. Results show that knowledge of the normal stresses and resolved shear stresses on each crystal plane can aid in predicting crack locations and orientations.

Physics Features of TRU-Fueled VHTRs

DOE PAGES

Lewis, Tom G.; Tsvetkov, Pavel V.

2009-01-01

The current waste management strategy for spent nuclear fuel (SNF) mandated by the US Congress is the disposal of high-level waste (HLW) in a geological repository at Yucca Mountain. Ongoing efforts on closed-fuel cycle options and difficulties in opening and safeguarding such a repository have led to investigations of alternative waste management strategies. One potential strategy for the US fuel cycle would be to make use of fuel loadings containing high concentrations of transuranic (TRU) nuclides in the next-generation reactors. The use of such fuels would not only increase fuel supply but could also potentially facilitate prolonged operation modes (viamore » fertile additives) on a single fuel loading. The idea is to approach autonomous operation on a single fuel loading that would allow marketing power units as nuclear batteries for worldwide deployment. Studies have already shown that high-temperature gas-cooled reactors (HTGRs) and their Generation IV (GEN IV) extensions, very-high-temperature reactors (VHTRs), have encouraging performance characteristics. This paper is focused on possible physics features of TRU-fueled VHTRs. One of the objectives of a 3-year U.S. DOE NERI project was to show that TRU-fueled VHTRs have the possibility of prolonged operation on a single fuel loading. A 3D temperature distribution was developed based on conceivable operation conditions of the 600 MWth VHTR design. Results of extensive criticality and depletion calculations with varying fuel loadings showed that VHTRs are capable for autonomous operation and HLW waste reduction when loaded with TRU fuel.« less

The deformation and acoustic emission of aluminum-magnesium alloy under non-isothermal thermo-mechanical loading

DOE Office of Scientific and Technical Information (OSTI.GOV)

Makarov, S. V.; Plotnikov, V. A., E-mail: plotnikov@phys.asu.ru; Lysikov, M. V.

2015-10-27

The following study investigates the deformation behavior and acoustic emission in aluminum-magnesium alloy under conditions of non-isothermal thermo-mechanical loading. The accumulation of deformation in the alloy, in conditions of change from room temperature to 500°C, occurs in two temperature intervals (I, II), characterized by different rates of deformation. The rate of deformation accumulation is correlated with acoustic emission. With load increasing in cycles from 40 to 200 MPa, the value of the boundary temperature (T{sub b}) between intervals I and II changes non-monotonically. In cycles with load up to 90 MPa, the T{sub b} value increases, while an increase up to 200 MPamore » makes T{sub b} shift toward lower temperatures. This suggests that the shift of boundaries in the region of low temperatures and the appearance of high-amplitude pulses of acoustic emission characterize the decrease of the magnitude of thermal fluctuations with increasing mechanical load, leading to the rupture of interatomic bonds in an elementary deformation act.« less

Thermal management of batteries

NASA Astrophysics Data System (ADS)

Gibbard, H. F.; Chen, C.-C.

Control of the internal temperature during high rate discharge or charge can be a major design problem for large, high energy density battery systems. A systematic approach to the thermal management of such systems is described for different load profiles based on: thermodynamic calculations of internal heat generation; calorimetric measurements of heat flux; analytical and finite difference calculations of the internal temperature distribution; appropriate system designs for heat removal and temperature control. Examples are presented of thermal studies on large lead-acid batteries for electrical utility load levelling and nickel-zinc and lithium-iron sulphide batteries for electric vehicle propulsion.

Development of ultra-high temperature material characterization capabilities using digital image correlation analysis

NASA Astrophysics Data System (ADS)

Cline, Julia Elaine

2011-12-01

Ultra-high temperature deformation measurements are required to characterize the thermo-mechanical response of material systems for thermal protection systems for aerospace applications. The use of conventional surface-contacting strain measurement techniques is not practical in elevated temperature conditions. Technological advancements in digital imaging provide impetus to measure full-field displacement and determine strain fields with sub-pixel accuracy by image processing. In this work, an Instron electromechanical axial testing machine with a custom-designed high temperature gripping mechanism is used to apply quasi-static tensile loads to graphite specimens heated to 2000°F (1093°C). Specimen heating via Joule effect is achieved and maintained with a custom-designed temperature control system. Images are captured at monotonically increasing load levels throughout the test duration using an 18 megapixel Canon EOS Rebel T2i digital camera with a modified Schneider Kreutznach telecentric lens and a combination of blue light illumination and narrow band-pass filter system. Images are processed using an open-source Matlab-based digital image correlation (DIC) code. Validation of source code is performed using Mathematica generated images with specified known displacement fields in order to gain confidence in accurate software tracking capabilities. Room temperature results are compared with extensometer readings. Ultra-high temperature strain measurements for graphite are obtained at low load levels, demonstrating the potential for non-contacting digital image correlation techniques to accurately determine full-field strain measurements at ultra-high temperature. Recommendations are given to improve the experimental set-up to achieve displacement field measurements accurate to 1/10 pixel and strain field accuracy of less than 2%.

Off-Axis Ratcheting Behavior of Unidirectional Carbon/Epoxy Laminate under Asymmetric Cyclic Loading at High Temperature

DTIC Science & Technology

2011-11-01

ply unidirectional carbon/epoxy laminates [0]12 were fabricated from the prepreg tape of P3252-20 (TORAY). They were laid up by hand and cured in...Off-Axis Ratcheting Behavior of Unidirectional Carbon/Epoxy Laminate under Asymmetric Cyclic Loading at High Temperature Takafumi Suzuki 1 and...Development of an engineering model for predicting the off-axis ratcheting behavior of a unidirectional CFRP laminate has been attempted. For this purpose

Peg supported thermal insulation panel

DOEpatents

Nowobilski, J.J.; Owens, W.J.

1985-04-30

A thermal insulation panel which is lightweight, load bearing, accommodates thermal stress, and has excellent high temperature insulation capability comprises high performance insulation between thin metal walls supported by high density, high strength glass pegs made in compliance with specified conditions of time, temperature and pressure. 2 figs.

Correlation between Mechanical Behavior and Actuator-type Performance of Ni-Ti-Pd High-temperature Shape Memory Alloys

NASA Technical Reports Server (NTRS)

Bigelow, Glen S.; Padula, Santo A., II; Garg, Anita; Noebe, Ronald D.

2007-01-01

High-temperature shape memory alloys in the NiTiPd system are being investigated as lower cost alternatives to NiTiPt alloys for use in compact solid-state actuators for the aerospace, automotive, and power generation industries. A range of ternary NiTiPd alloys containing 15 to 46 at.% Pd has been processed and actuator mimicking tests (thermal cycling under load) were used to measure transformation temperatures, work behavior, and dimensional stability. With increasing Pd content, the work output of the material decreased, while the amount of permanent strain resulting from each load-biased thermal cycle increased. Monotonic isothermal tension testing of the high-temperature austenite and low temperature martensite phases was used to partially explain these behaviors, where a mismatch in yield strength between the austenite and martensite phases was observed at high Pd levels. Moreover, to further understand the source of the permanent strain at lower Pd levels, strain recovery tests were conducted to determine the onset of plastic deformation in the martensite phase. Consequently, the work behavior and dimensional stability during thermal cycling under load of the various NiTiPd alloys is discussed in relation to the deformation behavior of the materials as revealed by the strain recovery and monotonic tension tests.

Correlation between mechanical behavior and actuator-type performance of Ni-Ti-Pd high-temperature shape memory alloys

NASA Astrophysics Data System (ADS)

Bigelow, Glen S.; Padula, Santo A., II; Garg, Anita; Noebe, Ronald D.

2007-04-01

High-temperature shape memory alloys in the NiTiPd system are being investigated as lower cost alternatives to NiTiPt alloys for use in compact solid-state actuators for the aerospace, automotive, and power generation industries. A range of ternary NiTiPd alloys containing 15 to 46 at.% Pd has been processed and actuator mimicking tests (thermal cycling under load) were used to measure transformation temperatures, work behavior, and dimensional stability. With increasing Pd content, the work output of the material decreased, while the amount of permanent strain resulting from each load-biased thermal cycle increased. Monotonic isothermal tension testing of the high-temperature austenite and low temperature martensite phases was used to partially explain these behaviors, where a mismatch in yield strength between the austenite and martensite phases was observed at high Pd levels. Moreover, to further understand the source of the permanent strain at lower Pd levels, strain recovery tests were conducted to determine the onset of plastic deformation in the martensite phase. Consequently, the work behavior and dimensional stability during thermal cycling under load of the various NiTiPd alloys is discussed in relation to the deformation behavior of the materials as revealed by the strain recovery and monotonic tension tests.

Determining the tensile response of materials at high temperature using DIC and the Virtual Fields Method

NASA Astrophysics Data System (ADS)

Valeri, Guillermo; Koohbor, Behrad; Kidane, Addis; Sutton, Michael A.

2017-04-01

An experimental approach based on Digital Image Correlation (DIC) is successfully applied to predict the uniaxial stress-strain response of 304 stainless steel specimens subjected to nominally uniform temperatures ranging from room temperature to 900 °C. A portable induction heating device equipped with custom made water-cooled copper coils is used to heat the specimen. The induction heater is used in conjunction with a conventional tensile frame to enable high temperature tension experiments. A stereovision camera system equipped with appropriate band pass filters is employed to facilitate the study of full-field deformation response of the material at elevated temperatures. Using the temperature and load histories along with the full-field strain data, a Virtual Fields Method (VFM) based approach is implemented to identify constitutive parameters governing the plastic deformation of the material at high temperature conditions. Results from these experiments confirm that the proposed method can be used to measure the full field deformation of materials subjected to thermo-mechanical loading.

Model A: High-Temperature Tribometer

DTIC Science & Technology

1992-02-01

spring loaded collet which grips the pin. In previous machines Inconel 625 collets and sleeves with 450 contact angles were used without collet...Triboeter, high temperature, friction, wear 11 1 08__ 19 ABSTRACT (Continue on revere if necewry and identify by blck number) A high temperature...tribometer has been specifically designed and fabricated to accurately measure, in real time, friction and wear characteristics of materials at temperatures

[Optimization on trehalose loading technique as protective conditioning for lyophilization of human platelets].

PubMed

Liu, Jing-Han; Zhou, Jun; Ouyang, Xi-Lin; Li, Xi-Jin; Lu, Fa-Qiang

2005-08-01

This study was aimed to further optimize trehalose loading technique including loading temperature, loading time, loading solution and loading concentration of trehalose, based on the established parameters. Loading efficiency in plasma was compared with that in buffer at 37 degrees C; the curves of intracellular trehalose concentration versus loading time at 37 degrees C and 16 degrees C were measured; curves of mean platelet volume (MPV) versus loading time and loading concentration were investigated and compared. According to results obtained, the loaing time, loading temperature, loading solution and trehalose concentration were ascertained for high loading efficiency of trehalose into human platelet. The results showed that the loading efficiency in plasma was markedly higher than that in buffer at 37 degrees C, the loading efficiency in plasma at 37 degrees C was significantly higher than that at 16 degrees C and reached 19.51% after loading for 4 hours, but 6.16% at 16 degrees C. MPV at 16 degrees C was increased by 43.2% than that at 37 degrees C, but had no distinct changes with loading time and loading concentration. In loading at 37 degrees C, MPV increased with loading time and loading concentration positively. Loading time and loading concentration displayed synergetic effect on MPV. MPV increased with loading time and concentration while trehalose loading concentration was above 50 mmol/L. It is concluded that the optimization parameters of trehalose loading technique are 37 degrees C (temperature), 4 hours (leading time), plasma (loading solution), 50 mmol/L (feasible trehalose concentration). The trehalose concentration can be adjusted to meet the requirement of lyophilization.

Development of a 1 kW, 200 C Mapham Inventor

NASA Technical Reports Server (NTRS)

Hammoud, Ahmad; Gerber, Scott; Bauman, Eric; Overton, Eric; Myers, Ira; Bercaw, Robert

1995-01-01

Electronic systems and components are often exposed to high temperature environment in space-based applications, nuclear power facilities, and geothermal energy extraction fields. A key requirement for these systems is, therefore, to withstand the high temperature exposure while maintaining efficient and reliable operation. Efforts were taken to design and develop a high temperature power inverter capable of 200 C operation. A 1 kW, 20 kHz Mapham inverter was designed and evaluated as a function of temperature at different load levels. The inverter system, excluding its input, control, and logic circuits, was characterized at temperatures from ambient to 200 C at 0%, 50%, and 100% resistive loading. With an applied input voltage of 75 VDC, the inverter produced an output of 250 VAC. The results obtained, which indicate good operational characteristics of the inverter up to 200 C, are presented and discussed.

Accelerated testing of composites

NASA Technical Reports Server (NTRS)

Papazian, H. A.

1983-01-01

It is shown that the Zhurkov method for testing the strength of solids can be applied to dynamic tension and to cyclic loading and provides a viable approach to accelerated testing of composites. Data from the literature are used to demonstrate a straightforward application of the method to dynamic tension of glass fiber and cyclic loading for glass/polymer, metal matrix, and graphite/epoxy composites. Zhurkov's equation can be used at relatively high loads to obtain failure times at any temperature of interest. By taking a few data points at one or two other temperatures the spectrum of failure times can be expanded to temperatures not easily accessible.

Wear Behavior and Mechanism of a Cr-Mo-V Cast Hot-Working Die Steel

NASA Astrophysics Data System (ADS)

Wei, M. X.; Wang, S. Q.; Zhao, Y. T.; Chen, K. M.; Cui, X. H.

2011-06-01

The wear behavior and mechanisms of a Cr-Mo-V cast hot-working die steel with three microstructures (tempered martensite, troostite, and sorbite) were studied systematically through the dry-sliding wear tests within a normal load range of 50 to 300 N and an ambient temperature range of 298 K to 673 K (25 °C to 400 °C) by a pin-on-disk high-temperature wear machine. Five different mechanisms were observed in the experiments, namely adhesive, abrasive, mild oxidative, oxidative, and extrusive wear; one or more of those mechanisms would be dominant within particular ranges of load and temperature. The transition of wear mechanisms depended on the formation of tribo-oxides, which was related closely to load and temperature, and their delamination, which was mainly influenced by the matrix. By increasing the load and ambient temperature, the protective effect of tribo-oxides first strengthened, then decreased, and in some cases disappeared. Under a load ranging 50 to 300 N at 298 K (25 °C) and a load of 50 N at 473 K (200 °C), adhesive wear was the dominant wear mechanism, and abrasive wear appeared simultaneously. The wear was of mild oxidative type under a load ranging 100 to 300 N at 473 K (200 °C) and a load ranging 50 to 150 N at 673 K (400 °C) for tempered martensite and tempered troostite as well as under a load of 100 N at 473 K (200 °C) and a load ranging 50 to 100 N at 673 K (400 °C) for tempered sorbite. At the load of 200 N or greater, or the temperatures above 673 K (400 °C), oxidative wear (beyond mild oxidative wear) prevailed. When the highest load of 300 N at 673 K (400 °C) was applied, extrusive wear started to dominate for the tempered sorbite.

Triple effect absorption chiller utilizing two refrigeration circuits

DOEpatents

DeVault, Robert C.

1988-01-01

A triple effect absorption method and apparatus having a high coefficient of performance. Two single effect absorption circuits are combined with heat exchange occurring between a condenser and absorber of a high temperature circuit, and a generator of a low temperature circuit. The evaporators of both the high and low temperature circuits provide cooling to an external heat load.

Fermentative high-titer ethanol production from Douglas-fir forest residue without detoxification using SPORL: high SO2 loading at low temperature

Treesearch

Feng Gu; William Gilles; Roland Gleisner; J.Y. Zhu

2016-01-01

This study evaluated high sulfur dioxide (SO2) loading in applying Sulfite Pretreatment to Overcome the Recalcitrance of Lignocelluloses (SPORL) to Douglas-fir forest residue (FS-10) for ethanol production through yeast fermentation. Three pretreatments were conducted at 140

Microwave-assisted regeneration of activated carbons loaded with pharmaceuticals.

PubMed

Ania, C O; Parra, J B; Menéndez, J A; Pis, J J

2007-08-01

The purpose of this work was to explore the application of microwaves for the regeneration of activated carbons spent with salicylic acid, a metabolite of a common analgesic frequently found in wastewater from the pharmaceutical industry. The exhausted carbon was treated in a quartz reactor by microwave irradiation at 2450 MHz at different temperatures and atmospheres, the regeneration efficiency being highly dependent on the operating conditions. Quantitative desorption of the pollutant was achieved at high temperature and oxidizing atmosphere, with regeneration efficiencies as high as 99% after six cycles. The stripping efficiency was superior to 95% at high temperatures and decreased at 450 degrees C. The incomplete desorption of the adsorbate at low temperature was further confirmed by the changes in the porosity observed by N2 and CO2 adsorption isotherms. Hence, micropores remain blocked which results in a reduction in loading capacities in successive cycles.

Au/Cr Sputter Coating for the Protection of Alumina During Sliding at High Temperatures

NASA Technical Reports Server (NTRS)

Benoy, Patricia A.; Dellacorte, Christopher

1995-01-01

A sputter deposited bilayer coating of gold and chromium was investigated as a potential solid lubricant to protect alumina substrates in applications involving sliding at high temperature. The proposed lubricant was tested in a pin-on-disk tribometer with coated alumina disks sliding against uncoated alumina pins. Three test parameters; temperature, load, and sliding velocity were varied over a wide range in order to determine the performance envelope on the gold/chromium (Au/Cr) solid lubricant film. The tribo-tests were run in an air atmosphere at temperatures of 25 to 1000 C, under loads of 4.9 to 49.0 N and at sliding velocities from 1 to 15 m/sec. Post test analyses included surface profilometry, wear factor determination and scanning electron microscopy/energy dispersive spectroscopy (SEM/EDS) examination of worn surfaces. Compared to unlubricated Al2O3 sliding, the use of the Au/Cr film reduced friction by 30 to 50 percent and wear by one to two orders of magnitude. Increases in test temperature resulted in lower friction and the Au/Cr film continued to provide low friction, about 0.3, even at 1000 C. Pin wear factors and friction were largely unaffected by increasing loads up to 29.4 N. Sliding velocity had essentially no effect on friction, however, increased velocity reduced coating life (total sliding distance). Based upon these research results, the Au/Cr film is a promising lubricant for moderately loaded, low speed applications operating at temperatures as high as 1000 C.

MS212--A Homogeneous Sputtered Solid Lubricant Coating for Use to 800 C

NASA Technical Reports Server (NTRS)

Sliney, Harold E.; Waters, William J.; Soltis, Richard

1997-01-01

Composite coatings containing chromium carbide, stable fluorides and silver were prepared by magnetron sputtering. The microstructure of the coatings is very homogeneous compared to that of plasma sprayed and sintered versions of the same chemical composition. Friction and wear of MS212-coated and baseline uncoated aluminum and Inconel X-750 are compared. At room temperature, the friction and wear of coated aluminum is dramatically better compared to the baseline. The acceptable load is limited by deformation of the soft aluminum substrate. In the case of the nickel alloy, lower friction is observed for the coated alloy at all temperatures up to the maximum test temperature of 800 C. Pin wear factors for sliding against the coated alloy are lower than the baseline at room temperature and 350 C, and comparable to baseline wear at higher test temperatures. Low baseline wear at high temperatures is due to the lubricious nature of the natural oxides formed on nickel-chromium alloys in a hot, oxidizing atmosphere. No load limit was found for coated Inconel X-750 at loads up to five times the load limit for coated aluminum.

Thermo-elastic-plastic analysis for elastic component under high temperature fatigue crack growth rate

NASA Astrophysics Data System (ADS)

Ali, Mohammed Ali Nasser

The research project presents a fundamental understanding of the fatigue crack growth mechanisms of AISI 420 martensitic stainless steel, based on the comparison analysis between the theoretical and numerical modelling, incorporating research findings under isothermal fatigue loading for solid cylindrical specimen and the theoretical modelling with the numerical simulation for tubular specimen when subjected to cyclic mechanical loading superimposed by cyclic thermal shock.The experimental part of this research programme studied the fatigue stress-life data for three types of surface conditions specimen and the isothermal stress-controlled fatigue testing at 300 °C - 600 °C temperature range. It is observed that the highest strength is obtained for the polished specimen, while the machined specimen shows lower strength, and the lowest strength is the notched specimen due to the high effect of the stress concentration. The material behaviour at room and high temperatures shows an initial hardening, followed by slow extension until fully plastic saturation then followed by crack initiation and growth eventually reaching the failure of the specimen, resulting from the dynamic strain ageing occurred from the transformation of austenitic microstructure to martensite and also, the nucleation of precipitation at grain boundaries and the incremental temperature increase the fatigue crack growth rate with stress intensity factor however, the crack growth rate at 600 °C test temperature is less than 500 °C because of the creep-fatigue taking place.The theoretical modelling presents the crack growth analysis and stress and strain intensity factor approaches analysed in two case studies based on the addition of thermo-elastic-plastic stresses to the experimental fatigue applied loading. Case study one estimates the thermal stresses superimposed sinusoidal cyclic mechanical stress results in solid cylinder under isothermal fatigue simulation. Case study two estimates the transient thermal stresses superimposed on cyclic mechanical loading results in hollow cylinder under thermal shock in heating case and down shock cooling case. The combination of stress and strain intensity factor theoretical calculations with the experimental output recorded data shows a similar behaviour with increasing temperature, and there is a fair correlation between the profiles at the beginning and then divergence with increasing the crack length. The transient influence of high temperature in case two, giving a very high thermal shock stress as a heating or cooling effects, shifting up the combined stress, when applied a cyclic mechanical load in fraction of seconds, and the reputations of these shocks, causing a fast failure under high thermal shock stress superimposed with mechanical loading.Finally, the numerical modelling analyses three cases studied were solved due to the types of loading and types of specimen geometry by using finite element models constructed through the ANSYS Workbench version 13.0. The first case is a low cyclic fatigue case for a solid cylinder specimen simulated by applying a cyclic mechanical loading. The second is an isothermal fatigue case for solid cylinder specimen simulated by supplying different constant temperatures on the outer surface with cyclic mechanical loading, where the two cases are similar to the experimental tests and the third case, is a thermo-mechanical fatigue for a hollow cylinder model by simulating a thermal up-shock generated due to transient heating on the outer surface of the model or down shock cooling on the inner surface with the cyclic mechanical loading. The results show a good agreement with the experimental data in terms of alternative stress and life in the first case. In case two results show the strain intensity factor is increases with increasing temperature similar to the theoretical solution due to the influence of the modulus of elasticity and the difference in life estimation with the experimental output record is related to the input data made of theoretical physical properties and the experimental stress-life data.

Field investigation of low-temperature cracking and stiffness moduli on selected roads with conventional and high modulus asphalt concrete

NASA Astrophysics Data System (ADS)

Judycki, Józef; Jaczewski, Mariusz; Ryś, Dawid; Pszczoła, Marek; Jaskuła, Piotr; Glinicki, Adam

2017-09-01

High Modulus Asphalt Concrete (HMAC) was introduced in Poland as a one of the solutions to the problem of rutting, type of deterioration common in the 1990s. After first encouraging trials in 2002 HMAC was widely used for heavily loaded national roads and motorways. However some concerns were raised about low-temperature cracking of HMAC. This was the main reason of the studies presented in this article were started. The article presents the comparison of performance of pavements constructed in typical contract conditions with the road bases made of HMAC and conventional asphalt concrete (AC). The field investigation was focused on the number of low-temperature cracks, bearing capacity (based on FWD test) of road sections localized in coldest region of Poland. Also load transfer efficiency of selected low-temperature cracks was assessed. FWD test confirmed lower deflections of pavements with HMAC and two times higher stiffness modulus of asphalt courses in comparison to pavements constructed with conventional AC mixtures. Relation of stiffness of asphalt layers and amount of low-temperature cracks showed that the higher stiffness modulus of asphalt layers could lead to increase of the number of low-temperature cracks. FWD test results showed that the load transfer efficiency of low-temperature cracks on pavements with HMAC presents very low values, very close to lack of load transfer. It was surprising as section with HMAC road base were aged from 2 to 5 years and presented very good bearing capacity.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bouchard, P.J.

A forthcoming revision to the R6 Leak-before-Break Assessment Procedure is briefly described. Practical application of the LbB concepts to safety-critical nuclear plant is illustrated by examples covering both low temperature and high temperature (>450{degrees}C) operating regimes. The examples highlight a number of issues which can make the development of a satisfactory LbB case problematic: for example, coping with highly loaded components, methodology assumptions and the definition of margins, the effect of crack closure owing to weld residual stresses, complex thermal stress fields or primary bending fields, the treatment of locally high stresses at crack intersections with free surfaces, the choicemore » of local limit load solution when predicting ligament breakthrough, and the scope of calculations required to support even a simplified LbB case for high temperature steam pipe-work systems.« less

Turbo-Brayton cryocooler technology for low-temperature space applications

NASA Astrophysics Data System (ADS)

Zagarola, Mark V.; Breedlove, Jeffrey F.; McCormick, John A.; Swift, Walter L.

2003-03-01

High performance, low temperature cryocoolers are being developed for future space-borne telescopes and instruments. To meet mission objectives, these coolers must be compact, lightweight, have low input power, operate reliably for 5-10 years, and produce no disturbances that would affect the pointing accuracy of the instruments. This paper describes progress in the development of turbo-Brayton cryocoolers addressing cooling in the 5 K to 20 K temperature range for loads of up to 300 mW. The key components for these cryocoolers are the miniature, high-speed turbomachines and the high performance recuperative heat exchangers. The turbomachines use gas-bearings to support the low mass, high speed rotors, resulting in negligible vibration and long life. Precision fabrication techniques are used to produce the necessary micro-scale geometric features that provide for high cycle efficiencies at these reduced sizes. Turbo-Brayton cryocoolers for higher temperatures and loads have been successfully developed for space applications. For efficient operation at low temperatures and capacities, advances in the core technologies have been pursued. Performance test results of a new, low poer compressor will be presented, and early cryogenic test results on a low temperature expansion turbine will be discussed. Projections for several low temperature cooler configurations are summarized.

High Temperature Multilayer Environmental Barrier Coatings Deposited Via Plasma Spray-Physical Vapor Deposition

NASA Technical Reports Server (NTRS)

Harder, Bryan James; Zhu, Dongming; Schmitt, Michael P.; Wolfe, Douglas E.

2014-01-01

Si-based ceramic matrix composites (CMCs) require environmental barrier coatings (EBCs) in combustion environments to avoid rapid material loss. Candidate EBC materials have use temperatures only marginally above current technology, but the addition of a columnar oxide topcoat can substantially increase the durability. Plasma Spray-Physical Vapor Deposition (PS-PVD) allows application of these multilayer EBCs in a single process. The PS-PVD technique is a unique method that combines conventional thermal spray and vapor phase methods, allowing for tailoring of thin, dense layers or columnar microstructures by varying deposition conditions. Multilayer coatings were deposited on CMC specimens and assessed for durability under high heat flux and load. Coated samples with surface temperatures ranging from 2400-2700F and 10 ksi loads using the high heat flux laser rigs at NASA Glenn. Coating morphology was characterized in the as-sprayed condition and after thermomechanical loading using electron microscopy and the phase structure was tracked using X-ray diffraction.

Acoustic Levitator Maintains Resonance

NASA Technical Reports Server (NTRS)

Barmatz, M. B.; Gaspar, M. S.

1986-01-01

Transducer loading characteristics allow resonance tracked at high temperature. Acoustic-levitation chamber length automatically adjusted to maintain resonance at constant acoustic frequency as temperature changes. Developed for containerless processing of materials at high temperatures, system does not rely on microphones as resonance sensors, since microphones are difficult to fabricate for use at temperatures above 500 degrees C. Instead, system uses acoustic transducer itself as sensor.

High Temperature Metallic Seal Development For Aero Propulsion and Gas Turbine Applications

NASA Technical Reports Server (NTRS)

More, Greg; Datta, Amit

2006-01-01

A viewgraph presentation on metallic high temperature static seal development at NASA for gas turbine applications is shown. The topics include: 1) High Temperature Static Seal Development; 2) Program Review; 3) Phase IV Innovative Seal with Blade Alloy Spring; 4) Spring Design; 5) Phase IV: Innovative Seal with Blade Alloy Spring; 6) PHase IV: Testing Results; 7) Seal Seating Load; 8) Spring Seal Manufacturing; and 9) Other Applications for HIgh Temperature Spring Design

Dynamic and thermal analysis of high speed tapered roller bearings under combined loading

NASA Technical Reports Server (NTRS)

Crecelius, W. J.; Milke, D. R.

1973-01-01

The development of a computer program capable of predicting the thermal and kinetic performance of high-speed tapered roller bearings operating with fluid lubrication under applied axial, radial and moment loading (five degrees of freedom) is detailed. Various methods of applying lubrication can be considered as well as changes in bearing internal geometry which occur as the bearing is brought to operating speeds, loads and temperatures.

Special Considerations for Qualifying Thin Films for Supper Pressure Pumpkin Ultra Long Duration Balloon (ULDB) Missions

NASA Astrophysics Data System (ADS)

Said, M.

Pumpkin type super pressure balloons require much less stringent mechanical requirements on the envelope film material when compared to spherical super pressure type balloons. However, since suitable thin films are typically viscoelastic in nature, their creep characteristics must be fully characterized and must not exceed specific and predetermined design limits. Proper assessment of materials limits to meet these design limits requires creep-load-temperature data that characterizes the performance of the material over a time that exceeds the duration of the design service life by some specified margin. Contrary to the behavior of materials with purely elastic response, visco-elastic materials such as these considered for the ULDB design, change their geometry under sustained loading over time. This change is usually reflected by exhibiting a significant visco-elastic component over the service life of the mission. For that regime of large visco-elastic response, where the material is highly nonlinear, a certain load-temperature threshold can be reached where the creep is limited by an asymptote that depends on both the temperature and load level. Such creep is recoverable, although the recovery period may be much longer than the 100 day design service life of the ULDB structure plus the factor of safety required for the design. For a typical flight, the most significant creep occurs at the highest temperature, which also produces the highest internal pressure. At mid- latitudes a significant portion of the service life is spent at night, i.e. at low temperature and low load; for the ULDB film, this nighttime contribution to creep is insignificant in comparison to any daytime contribution. By contrast, flight exposure in an Antarctic summer is at an almost constant high temperature and corresponding high pressure. This response behavior must be sufficiently characterized to serve the needs of the structural design and performance predictions of the vehicle in service. In this work, a special emphasis will be given to the creep and dynamic characteristics of selected coextruded films and their dependence on the loading level and temperature. Preliminary testing has suggested t at the creep behavior of theh coextruded linear low density resin films is highly dependent on temperature and that the dynamic response depends on the make up of the composite film. In addition, the paper will, in general, highlight the process of qualify ing thin films for the pumpkin class of super pressure balloons.

Apparatus for material tests using an internal loading system in high-pressure gas at room temperature.

PubMed

Imade, M; Fukuyama, S; Yokogawa, K

2008-07-01

A new type of apparatus for material tests using an internal loading system in high-pressure gas up to 100 MPa at room temperature without conventional material testing equipment was developed. The apparatus consists of a high-pressure control system and a pressure vessel, in which a piston is installed in the cylinder of the pressure vessel. The load caused by the pressure difference between spaces separated by the piston in the vessel cylinder is applied on the specimen connected to the piston in the vessel cylinder. The actual load on the specimen is directly measured by an external load cell and the displacement of the specimen is also measured by an external extensometer. As an example of the application of the apparatus, a tensile test on SUS316 stainless steel the Japanese Industrial Standard (JIS) G4303, which is comparable to the type 316 stainless steel ASTM A276, was conducted in 90 MPa hydrogen and argon. Hydrogen showed a marked effect on the tensile property of the material. The hydrogen gas embrittlement of the material was briefly discussed.

Apparatus for material tests using an internal loading system in high-pressure gas at room temperature

NASA Astrophysics Data System (ADS)

Imade, M.; Fukuyama, S.; Yokogawa, K.

2008-07-01

A new type of apparatus for material tests using an internal loading system in high-pressure gas up to 100MPa at room temperature without conventional material testing equipment was developed. The apparatus consists of a high-pressure control system and a pressure vessel, in which a piston is installed in the cylinder of the pressure vessel. The load caused by the pressure difference between spaces separated by the piston in the vessel cylinder is applied on the specimen connected to the piston in the vessel cylinder. The actual load on the specimen is directly measured by an external load cell and the displacement of the specimen is also measured by an external extensometer. As an example of the application of the apparatus, a tensile test on SUS316 stainless steel the Japanese Industrial Standard (JIS) G4303, which is comparable to the type 316 stainless steel ASTM A276, was conducted in 90MPa hydrogen and argon. Hydrogen showed a marked effect on the tensile property of the material. The hydrogen gas embrittlement of the material was briefly discussed.

Analysis and Design of the NASA Langley Cryogenic Pressure Box

NASA Technical Reports Server (NTRS)

Glass, David E.; Stevens, Jonathan C.; Vause, R. Frank; Winn, Peter M.; Maguire, James F.; Driscoll, Glenn C.; Blackburn, Charles L.; Mason, Brian H.

1999-01-01

A cryogenic pressure box was designed and fabricated for use at NASA Langley Research Center (LaRC) to subject 72 in. x 60 in. curved panels to cryogenic temperatures and biaxial tensile loads. The cryogenic pressure box is capable of testing curved panels down to -423 F (20K) with 54 psig maximum pressure on the concave side, and elevated temperatures and atmospheric pressure on the convex surface. The internal surface of the panel is cooled by high pressure helium as that is cooled to -423 F by liquid helium heat exchangers. An array of twelve independently controlled fans circulate the high pressure gaseous helium to provide uniform cooling on the panel surface. The load introduction structure, consisting of four stainless steel load plates and numerous fingers attaching the load plates to the test panel, is designed to introduce loads into the test panel that represent stresses that will he observed in the actual tank structure. The load plates are trace cooled with liquid nitrogen to reduce thermal gradients that may result in bending the load plates, and thus additional stresses in the test panel. The design of the cryogenic systems, load introduction structure, and control system are discussed in this report.

Advantages of MgAlOx over gamma-Al2O3 as a support material for potassium-based high temperature lean NOx traps

DOE Office of Scientific and Technical Information (OSTI.GOV)

Luo, Jinyong; Gao, Feng; Karim, Ayman M.

MgAlOx mixed oxides were employed as supports for potassium-based lean NOx traps (LNTs) targeted for high temperature applications. Effects of support compositions, K/Pt loadings, thermal aging and catalyst regeneration on NOx storage capacity were systematically investigated. The catalysts were characterized by XRD, NOx-TPD, TEM, STEM-HAADF and in-situ XAFS. The results indicate that MgAlOx mixed oxides have significant advantages over conventional gamma-Al2O3-supports for LNT catalysts, in terms of high temperature NOx trapping capacity and thermal stability. First, as a basic support, MgAlOx stabilizes stored nitrates (in the form of KNO3) to much higher temperatures than mildly acidic gamma-Al2O3. Second, MgAlOx minimizesmore » Pt sintering during thermal aging, which is not possible for gamma-Al2O3 supports. Notably, combined XRD, in-situ XAFS and STEM-HAADF results indicate that Pt species in the thermally aged Pt/MgAlOx samples are finely dispersed in the oxide matrix as isolated atoms. This strong metal-support interaction stabilizes Pt and minimizes the extent of sintering. However, such strong interactions result in Pt oxidation via coordination with the support so that NO oxidation activity can be adversely affected after aging which, in turn, decreases NOx trapping ability for these catalysts. Interestingly, a high-temperature reduction treatment regenerates essentially full NOx trapping performance. In fact, regenerated Pt/K/MgAlOx catalyst exhibits much better NOx trapping performance than fresh Pt/K/Al2O3 LNTs over the entire temperature range investigated here. In addition to thermal aging, Pt/K loading effects were systemically studied over the fresh samples. The results indicate that NOx trapping is kinetically limited at low temperatures, while thermodynamically limited at high temperatures. A simple conceptual model was developed to explain the Pt and K loading effects on NOx storage. An optimized K loading, which allows balancing between the stability of nitrates and exposed Pt surface, gives the best NOx trapping capability.« less

High-temperature, high-frequency fretting fatigue of a single crystal nickel alloy

NASA Astrophysics Data System (ADS)

Matlik, John Frederick

Fretting is a structural damage mechanism arising from a combination of wear, corrosion, and fatigue between two nominally clamped surfaces subjected to an oscillatory loading. A critical location for fretting induced damage has been identified at the blade/disk and blade/damper interfaces of gas turbine engine turbomachinery and space propulsion components. The high-temperature, high-frequency loading environment seen by these components lead to severe stress gradients at the edge-of-contact that could potentially foster crack growth leading to component failure. These contact stresses drive crack nucleation in fretting and are very sensitive to the geometry of the contacting bodies, the contact loads, materials, temperature, and contact surface tribology (friction). To diagnose the threat that small and relatively undetectable fretting fatigue cracks pose to damage tolerance and the ensuing structural integrity of aerospace components, a strong motivation exists to develop a quantitative mechanics based understanding of fretting crack nucleation in advanced aerospace alloys. In response to this need, the objective of this work is to characterize the fretting behavior exhibited by a polycrystalline/single crystal nickel contact subjected to elevated frequency and temperature. The effort to meet this objective is two fold: (1) to develop a well-characterized experimental fretting rig to investigate fretting behavior of advanced aerospace alloys at high frequency and high temperature, and (2) to develop the associated contact modeling tools for calculating contact stresses given in-situ experimentally measured remote contact loads. By coupling the experimental results and stress analysis, this effort aims to correlate the fretting crack nucleation behavior with the local contact stresses calculated from the devised three dimensional, anisotropic, dissimilar material contact model. The experimental effort is first motivated by a survey of recent fretting issues and investigations of aerospace components. A detailed description of the high-frequency, high-temperature fretting rig to be used in this investigation follows. Finally, development of a numerical submodeling technique for calculating the experimental contact traction and near-surface stresses is presented and correlated to the experimental fretting crack nucleation observations.

Investigation into the Cyclic Strength of the Bodies of Steam Shutoff Valves from 10Kh9MFB-Sh Steel

NASA Astrophysics Data System (ADS)

Skorobogatykh, V. N.; Kunavin, S. A.; Prudnikov, D. A.; Shchenkova, I. A.; Bazhenov, A. M.; Zadoinyi, V. A.; Starkovskii, G. L.

2018-02-01

Steam shutoff valves are operated under complex loading conditions at thermal and nuclear power stations. In addition to exposure to high temperature and stresses resulting in fatigue, these valves are subjected to cyclic loads in heating-up-cooling down, opening-closing, etc. cycles. The number of these cycles to be specified in designing the valves should not exceed the maximum allowable value. Hence, the problem of cyclic failure rate of steam shutoff valve bodies is critical. This paper continues the previous publications about properties of the construction material for steam shutoff valve bodies (grade 10Kh9MFB-Sh steel) produced by electroslag melting and gives the results of investigation into the cyclic strength of this material. Fatigue curves for the steal used for manufacturing steam shutoff valve bodies are presented. The experimental data are compared with the calculated fatigue curves plotted using the procedures outlined in PNAE G-002-986 and RD 10-249-98. It is confirmed that these procedures may be used in designing valve bodies from 10Kh9MFB-Sh steel. The effect of the cyclic damage after preliminary cyclic loading of the specimens according to the prescribed load conditions on the high-temperature strength of the steel is examined. The influence of cyclic failure rate on the long-term strength was investigated using cylindrical specimens with a smooth working section in the as-made conditions and after two regimes of preliminary cyclic loading (training) at a working temperature of 570°C and the number of load cycles exceeding the design value, which was 2 × 103 cycles. The experiments corroborated that the material (10Kh9MFB-Sh steel) of the body manufactured by the method of electroslag melting had high resistance to cyclic failure rate. No effect of cyclic damages in the metal of the investigated specimens on the high-temperature strength has been found.

Experimental investigations on thermo mechanical behaviour of aluminium alloys subjected to tensile loading and laser irradiation

NASA Astrophysics Data System (ADS)

Jelani, Mohsan; Li, Zewen; Shen, Zhonghua; Sardar, Maryam; Tabassum, Aasma

2017-05-01

The present work reports the investigation of the thermal and mechanical behaviour of aluminium alloys under the combined action of tensile loading and laser irradiations. The two types of aluminium alloys (Al-1060 and Al-6061) are used for the experiments. The continuous wave Ytterbium fibre laser (wavelength 1080 nm) was employed as irradiation source, while tensile loading was provided by tensile testing machine. The effects of various pre-loading and laser power densities on the failure time, temperature distribution and on deformation behaviour of aluminium alloys are analysed. The experimental results represents the significant reduction in failure time and temperature for higher laser powers and for high load values, which implies that preloading may contribute a significant role in the failure of the material at elevated temperature. The reason and characterization of material failure by tensile and laser loading are explored in detail. A comparative behaviour of under tested materials is also investigated. This work suggests that, studies considering only combined loading are not enough to fully understand the mechanical behaviour of under tested materials. For complete characterization, one must consider the effect of heating as well as loading rate.

High-Temperature, Lightweight, Self-Healing Ceramic Composites for Aircraft Engine Applications

NASA Technical Reports Server (NTRS)

Raj, Sai V.; Bhatt, Ramkrishna

2013-01-01

The use of reliable, high-temperature, lightweight materials in the manufacture of aircraft engines is expected to result in lower fossil and biofuel consumption, thereby leading to cost savings and lower carbon emissions due to air travel. Although nickel-based superalloy blades and vanes have been successfully used in aircraft engines for several decades, there has been an increased effort to develop high-temperature, lightweight, creep-resistant substitute materials under various NASA programs over the last two decades. As a result, there has been a great deal of interest in developing SiC/SiC ceramic matrix composites (CMCs) due to their higher damage tolerance compared to monolithic ceramics. Current-generation SiC/SiC ceramic matrix composites rely almost entirely on the SiC fibers to carry the load, owing to the premature cracking of the matrix during loading. Thus, the high-temperature usefulness of these CMCs falls well below their theoretical capabilities. The objective of this work is to develop a new class of high-temperature, lightweight, self-healing, SiC fiber-reinforced, engineered matrix ceramic composites.

Investigation of Tokamak Solid Divertor Target Options.

DTIC Science & Technology

1981-05-26

but materials are not known which could operate at the high resulting wall temperatures . Mist- steam flows would also demand a relatively high ...flux P = coolant density = bulk coolant viscosity w = coolant viscosity at average wall temperature = units conversion At high heat loads and moderate...therefore, the inner wall temperature will be over 300 OF, posing a high temp- erature materials challenge. E. Swirl and Mixed Flow Schemes Extensive work

Dynamic High-Temperature Tensile Characterization of an Iridium Alloy with Kolsky Tension Bar Techniques

DOE PAGES

Song, Bo; Nelson, Kevin; Lipinski, Ronald; ...

2015-05-29

In this study, conventional Kolsky tension bar techniques were modified to characterize an iridium alloy in tension at elevated strain rates and temperatures. The specimen was heated to elevated temperatures with an induction coil heater before dynamic loading; whereas, a cooling system was applied to keep the bars at room temperature during heating. A preload system was developed to generate a small pretension load in the bar system during heating in order to compensate for the effect of thermal expansion generated in the high-temperature tensile specimen. A laser system was applied to directly measure the displacements at both ends ofmore » the tensile specimen in order to calculate the strain in the specimen. A pair of high-sensitivity semiconductor strain gages was used to measure the weak transmitted force due to the low flow stress in the thin specimen at elevated temperatures. The dynamic high-temperature tensile stress–strain curves of a DOP-26 iridium alloy were experimentally obtained at two different strain rates (~1000 and 3000 s -1) and temperatures (~750 and 1030°C). The effects of strain rate and temperature on the tensile stress–strain response of the iridium alloy were determined. Finally, the iridium alloy exhibited high ductility in stress–strain response that strongly depended on strain-rate and temperature.« less

DOE Office of Scientific and Technical Information (OSTI.GOV)

Song, Bo; Nelson, Kevin; Lipinski, Ronald

In this study, conventional Kolsky tension bar techniques were modified to characterize an iridium alloy in tension at elevated strain rates and temperatures. The specimen was heated to elevated temperatures with an induction coil heater before dynamic loading; whereas, a cooling system was applied to keep the bars at room temperature during heating. A preload system was developed to generate a small pretension load in the bar system during heating in order to compensate for the effect of thermal expansion generated in the high-temperature tensile specimen. A laser system was applied to directly measure the displacements at both ends ofmore » the tensile specimen in order to calculate the strain in the specimen. A pair of high-sensitivity semiconductor strain gages was used to measure the weak transmitted force due to the low flow stress in the thin specimen at elevated temperatures. The dynamic high-temperature tensile stress–strain curves of a DOP-26 iridium alloy were experimentally obtained at two different strain rates (~1000 and 3000 s -1) and temperatures (~750 and 1030°C). The effects of strain rate and temperature on the tensile stress–strain response of the iridium alloy were determined. Finally, the iridium alloy exhibited high ductility in stress–strain response that strongly depended on strain-rate and temperature.« less

Improvement of the Measurement Range and Temperature Characteristics of a Load Sensor Using a Quartz Crystal Resonator with All Crystal Layer Components.

PubMed

Murozaki, Yuichi; Sakuma, Shinya; Arai, Fumihito

2017-05-08

Monitoring multiple biosignals, such as heart rate, respiration cycle, and weight transitions, contributes to the health management of individuals. Specifically, it is possible to measure multiple biosignals using load information obtained through contact with the environment, such as a chair and bed, in daily use. A wide-range load sensor is essential since load information contains multiple biosignals with various load ranges. In this study, a load sensor is presented by using a quartz crystal resonator (QCR) with a wide measurement range of 1.5 × 10⁶ (0.4 mN to 600 N), and its temperature characteristic of load is improved to -7 Hz/°C (-18 mN/°C). In order to improve the measurement range of the load, a design method of this sensor is proposed by restraining the buckling of QCR and by using a thinner QCR. The proposed sensor allows a higher allowable load with high sensitivity. The load sensor mainly consists of three layers, namely a QCR layer and two holding layers. As opposed to the conventional holding layer composed of silicon, quartz crystal is utilized for the holding layers to improve the temperature characteristic of the load sensor. In the study, multiple biosignals, such as weight and pulse, are detected by using a fabricated sensor.

Nanotwin Formation in High-Manganese Austenitic Steels Under Explosive Shock Loading

NASA Astrophysics Data System (ADS)

Canadinc, D.; Uzer, B.; Elmadagli, M.; Guner, F.

2018-04-01

The micro-deformation mechanisms active in a high-manganese austenitic steel were investigated upon explosive shock loading. Single system of nanotwins forming within primary twins were shown to govern the deformation despite the elevated temperatures attained during testing. The benefits of nanotwin formation for potential armor materials were demonstrated.

Combined bending and thermal fatigue of high-temperature metal-matrix composites - Computational simulation

NASA Technical Reports Server (NTRS)

Gotsis, Pascal K.; Chamis, Christos C.

1992-01-01

The nonlinear behavior of a high-temperature metal-matrix composite (HT-MMC) was simulated by using the metal matrix composite analyzer (METCAN) computer code. The simulation started with the fabrication process, proceeded to thermomechanical cyclic loading, and ended with the application of a monotonic load. Classical laminate theory and composite micromechanics and macromechanics are used in METCAN, along with a multifactor interaction model for the constituents behavior. The simulation of the stress-strain behavior from the macromechanical and the micromechanical points of view, as well as the initiation and final failure of the constituents and the plies in the composite, were examined in detail. It was shown that, when the fibers and the matrix were perfectly bonded, the fracture started in the matrix and then propagated with increasing load to the fibers. After the fibers fractured, the composite lost its capacity to carry additional load and fractured.

Combined thermal and bending fatigue of high-temperature metal-matrix composites: Computational simulation

NASA Technical Reports Server (NTRS)

Gotsis, Pascal K.

1991-01-01

The nonlinear behavior of a high-temperature metal-matrix composite (HT-MMC) was simulated by using the metal matrix composite analyzer (METCAN) computer code. The simulation started with the fabrication process, proceeded to thermomechanical cyclic loading, and ended with the application of a monotonic load. Classical laminate theory and composite micromechanics and macromechanics are used in METCAN, along with a multifactor interaction model for the constituents behavior. The simulation of the stress-strain behavior from the macromechanical and the micromechanical points of view, as well as the initiation and final failure of the constituents and the plies in the composite, were examined in detail. It was shown that, when the fibers and the matrix were perfectly bonded, the fracture started in the matrix and then propagated with increasing load to the fibers. After the fibers fractured, the composite lost its capacity to carry additional load and fractured.

Testing of a Miniature Loop Heat Pipe with Multiple Evaporators and Multiple Condensers for Space Applications

NASA Technical Reports Server (NTRS)

Nagano, Hosei; Ku, Jentung

2006-01-01

Thermal performance of a miniature loop heat pipe (MLHP) with two evaporators and two condensers is described. A comprehensive test program, including start-up, high power, low power, power cycle, and sink temperature cycle tests, has been executed at NASA Goddard Space Flight Center for potential space applications. Experimental data showed that the loop could start with heat loads as low as 2W. The loop operated stably with even and uneven evaporator heat loads, and even and uneven condenser sink temperatures. Heat load sharing between the two evaporators was also successfully demonstrated. The loop had a heat transport capability of l00W to 120W, and could recover from a dry-out by reducing the heat load to evaporators. Low power test results showed the loop could work stably for heat loads as low as 1 W to each evaporator. Excellent adaptability of the MLHP to rapid changes of evaporator power and sink temperature were also demonstrated.

Optical high temperature sensor based on fiber Bragg grating

NASA Astrophysics Data System (ADS)

Zhang, Bowei

The aim of this thesis is to fabricate a fiber Bragg grating (FBG) temperature sensor that is capable to measure temperatures in excess of 1100°C. For this purpose, two topics have been studied and investigated during this project. One of them is the development of a high temperature resistant molecular-water induced FBGs; and the other is to investigate the effect of microwave-irradiation on the hydrogen-loaded FBG. The molecular-water induced FBGs are different from the other types of FBG. In these devices the refractive index is modulated by the periodic changes of molecular-water concentration within the grating. The device was developed using thermal annealing technology based on hydrogen-load FBG. Thermal stability of these devices was studied by measuring the grating reflectivity from room temperature to 1000°C. The stability of the device was tested by examining the FBG reflectivity for a period of time at certain temperatures. The results show that these devices are extremely stable at temperatures in excess of 1000°C. The hydroxyl concentration in the grating has been also investigated during this thesis. Based on the knowledge of hydroxyl groups inside FBG, a microwave treatment was designed to increase the hydroxyl concentration in the FBG area. The results show that the molecular-water induced grating, which was fabricated using microwave radiated hydrogen-loaded FBI, are stable at temperatures above 1100°C.

Parametric analysis and temperature effect of deployable hinged shells using shape memory polymers

NASA Astrophysics Data System (ADS)

Tao, Ran; Yang, Qing-Sheng; He, Xiao-Qiao; Liew, Kim-Meow

2016-11-01

Shape memory polymers (SMPs) are a class of intelligent materials, which are defined by their capacity to store a temporary shape and recover an original shape. In this work, the shape memory effect of SMP deployable hinged shell is simulated by using compiled user defined material subroutine (UMAT) subroutine of ABAQUS. Variations of bending moment and strain energy of the hinged shells with different temperatures and structural parameters in the loading process are given. The effects of the parameters and temperature on the nonlinear deformation process are emphasized. The entire thermodynamic cycle of SMP deployable hinged shell includes loading at high temperature, load carrying with cooling, unloading at low temperature and recovering the original shape with heating. The results show that the complicated thermo-mechanical deformation and shape memory effect of SMP deployable hinge are influenced by the structural parameters and temperature. The design ability of SMP smart hinged structures in practical application is prospected.

The Effects of Elevated Temperatures on the Response of Resins Under Dynamic and Static Loadings

NASA Technical Reports Server (NTRS)

Gilat, Amos

2005-01-01

The overall objective of the research is to experimentally study the combined effects of temperature and strain rate on the response of two resins that are commonly used for the matrix material in composites. The resins are loaded at various temperatures in shear and in tension over a wide range of strain rates. These two types of loadings provide an opportunity to examine also the effect that temperature might have on the effects of the hydrostatic stress component on the material response. The experimental data provide the information needed for NASA scientists for the development of a nonlinear, strain rate, and temperature dependent deformation and strength models for composites that can subsequently be used in design. This year effort was directed into the development and testing of the epoxy resin at elevated temperatures. Two types of epoxy resins were tested in shear at high strain rates of about 10(exp-4)/s and elevated temperatures of 50 and 8OC. The results show that the temperature significantly affects the response of epoxy.

Plant temperatures and heat flux in a Sonoran Desert ecosystem.

PubMed

Gibbs, Joan G; Patten, D T

1970-09-01

In the extreme desert environment the potential energy load is high, consequently high temperatures might be a limiting factor for plant survival. Field measurements of plant temperatures in a Sonoran Desert ecosystem were made using fine thermocouples. Temperatures of six desert species were measured: Opuntia engelmannii, Opuntia bigelovii, Opuntia acanthocarpa, Echinocereus engelmannii, Larrea tridentata and Franseria deltoidea. Daily temperature profiles were used to compare the different responses of cacti and shrubs to the desert heat load and also to compare spring and summer responses. Leaf temperature of shrubs was at or near air temperature during both the mild, spring season and the hotter dry season. The cacti, on the other hand, absorbed and stored heat, thus temperatures were often above air temperature. The energy absorbed is determined largely by plant orientation and surface area exposed to the sun. Actual energy absorbed by the plants was estimated from energy diagrams.The flat stem pads of Opuntia engelmannii plants are oriented to receive maximum sunlight without long periods of continuous heating. Opuntia bigelovii spines reflect and absorb much of the environmental energy load, thereby protecting the thick, succulent stems from overheating. The smaller stems of Opuntia acanthocarpa dissipate heat more effectively by their large surface area exposed to convective air currents. Leaves on desert shrubs remain nearer to air temperature than do succulent stems of cacti, because their very large surface to volume ratio allows them to dissipate much heat by convection.

Low cycle fatigue

NASA Technical Reports Server (NTRS)

Solomon, H. D. (Editor); Kaisand, L. R. (Editor); Halford, G. R. (Editor); Leis, B. N. (Editor)

1988-01-01

The papers contained in this volume focus on various aspects of low cycle fatigue, including cyclic deformation, crack propagation, high-temperature low cycle fatigue, microstructural defects, multiaxial and variable amplitude loading, and life prediction. Papers are presented on the low cycle fatigue of some aluminum alloys, prediction of crack growth under creep-fatigue loading conditions, high-temperature low cycle fatigue behavior and lifetime prediction of a nickel-base ODS alloy, and an integrated approach to creep-fatigue life prediction. Other topics discussed include thermal fatigue testing of coated monocrystalline superalloys, low cycle fatigue of Al-Mg-Si alloys, and the effect of superimposed stresses at high frequency on low cycle fatigue.

The High Strain Rate Deformation Behavior of High Purity Magnesium and AZ31B Magnesium Alloy

NASA Astrophysics Data System (ADS)

Livescu, Veronica; Cady, Carl M.; Cerreta, Ellen K.; Henrie, Benjamin L.; Gray, George T.

The deformation in compression of pure magnesium and AZ31B magnesium alloy, both with a strong basal pole texture, has been investigated as a function of temperature, strain rate, and specimen orientation. The mechanical response of both metals is highly dependent upon the orientation of loading direction with respect to the basal pole. Specimens compressed along the basal pole direction have a high sensitivity to strain rate and temperature and display a concave down work hardening behavior. Specimens loaded perpendicularly to the basal pole have a yield stress that is relatively insensitive to strain rate and temperature and a work hardening behavior that is parabolic and then linearly upwards. Both specimen orientations display a mechanical response that is sensitive to temperature and strain rate. Post mortem characterization of the pure magnesium was conducted on a subset of specimens to determine the microstructural and textural evolution during deformation and these results are correlated with the observed work hardening behavior and strain rate sensitivities were calculated.

Relationship between white spot syndrome virus (WSSV) loads and characterizations of water quality in Litopenaeus vannamei culture ponds during the tropical storm.

PubMed

Zhang, J S; Li, Z J; Wen, G L; Wang, Y L; Luo, L; Zhang, H J; Dong, H B

2016-01-01

An in-situ experiment was conducted to investigate the effect of tropical storm on the white spot syndrome virus (WSSV) loads in Litopenaeus vannamei rearing ponds. White spot syndrome virus loads, heterotrophic bacteria, Vibrio and water quality (including temperature, dissolved oxygen (DO), salinity, pH, NH 4 -N, and NO 2 -N) were continually monitored through one tropical storm. The WSSV loads decreased when tropical storm made landfall, and substantially increased when typhoon passed. The variation of WSSV loads was correlated with DO, temperature, heterotrophic bacteria count, and ammonia-N concentrations. These results suggested that maintaining high level DO and promoting heterotrophic bacteria growth in the shrimp ponds might prevent the diseases' outbreak after the landfall of tropical storm.

Relationship between white spot syndrome virus (WSSV) loads and characterizations of water quality in Litopenaeus vannamei culture ponds during the tropical storm

PubMed Central

Zhang, J. S.; Li, Z. J.; Wen, G. L.; Wang, Y. L.; Luo, L.; Zhang, H. J.; Dong, H. B.

2016-01-01

An in-situ experiment was conducted to investigate the effect of tropical storm on the white spot syndrome virus (WSSV) loads in Litopenaeus vannamei rearing ponds. White spot syndrome virus loads, heterotrophic bacteria, Vibrio and water quality (including temperature, dissolved oxygen (DO), salinity, pH, NH4-N, and NO2-N) were continually monitored through one tropical storm. The WSSV loads decreased when tropical storm made landfall, and substantially increased when typhoon passed. The variation of WSSV loads was correlated with DO, temperature, heterotrophic bacteria count, and ammonia-N concentrations. These results suggested that maintaining high level DO and promoting heterotrophic bacteria growth in the shrimp ponds might prevent the diseases’ outbreak after the landfall of tropical storm. PMID:27822254

DOE Office of Scientific and Technical Information (OSTI.GOV)

Miao, Yinbin; Mo, Kun; Zhou, Zhangjian

Here the high temperature tensile performance of an oxide dispersion-strengthened (ODS) 310 steel is reported upon. The microstructure of the steel was examined through both transmission electron microscopy (TEM) and synchrotron scattering. In situ synchrotron tensile investigation was performed at a variety of temperatures, from room temperature up to 800°C. Pyrochlore structure yttrium titanate and sodium chloride structure titanium nitride phases were identified in the steel along with an austenite matrix and marginal residual α’-martensite. The inclusion phases strengthen the steel by taking extra load through particle-dislocation interaction during plastic deformation or dislocation creep procedures. As temperature rises, the loadmore » partitioning effect of conventional precipitate phases starts to diminish, whereas those ultra-fine oxygen-enriched nanoparticles continue to bear a considerable amount of extra load. Introduction of oxygen-enriched nanoparticles in austenitic steel proves to improve the high temperature performance, making austenitic ODS steels promising for advanced nuclear applications.« less

An EBSD Evaluation of the Microstructure of Crept Nimonic 101 for the Validation of a Polycrystal-Plasticity Model

NASA Astrophysics Data System (ADS)

Reschka, S.; Munk, L.; Wriggers, P.; Maier, H. J.

2017-12-01

Nimonic 101 is one of the early nickel-based superalloys developed for the use in gas turbines. In such environments, the material is exposed to a combination of both high temperatures and mechanical loads for a long duration. Hence, thermal creep is of the utmost concern as it often limits service life. This study focuses on creep tests, carried out on Nimonic 101 at different temperatures under a constant tensile load of 735 MPa. To characterize the microstructural evolution, electron backscatter diffraction (EBSD) measurements were employed before and after loading. At higher temperatures, a significant change of the microstructure was observed. The grains elongated and aligned their orientation along the load axis. In parallel, a crystal plasticity material model has been set up in the classical large deformation framework. Modeling results are compared to the acquired EBSD data.

Effects of Loading Frequency on Fatigue Behavior, Residual Stress, and Microstructure of Deep-Rolled Stainless Steel AISI 304 at Elevated Temperatures

NASA Astrophysics Data System (ADS)

Nikitin, I.; Juijerm, P.

2018-02-01

The effects of loading frequency on the fatigue behavior of non-deep-rolled (NDR) and deep-rolled (DR) austenitic stainless steel AISI 304 were systematically clarified at elevated temperatures, especially at temperatures exhibiting the dynamic strain aging (DSA) phenomena. Tension-compression fatigue tests were performed isothermally at temperatures of 573 K and 773 K (300 °C and 500 °C) with different loading frequencies of 5, 0.5, 0.05, and 0.005 Hz. For the DR condition, the residual stresses and work-hardening states will be presented. It was found that DSA would be detected at appropriate temperatures and deformation rates. The cyclic deformation curves and the fatigue lives of the investigated austenitic stainless steel AISI 304 are considerably affected by the DSA, especially on the DR condition having high dislocation densities at the surface and in near-surface regions. In the temperature range of the DSA, residual stresses and work-hardening states of the DR condition seem to be stabilized. The microstructural alterations were investigated by transmission electron microscopy (TEM). At an appropriate temperature with low loading frequency, the plastic deformation mechanism shifted from a wavy slip manner to a planar slip manner in the DSA regimes, whereas the dislocation movements were obstructed.

Temperature variations at nano-scale level in phase transformed nanocrystalline NiTi shape memory alloys adjacent to graphene layers.

PubMed

Amini, Abbas; Cheng, Chun; Naebe, Minoo; Church, Jeffrey S; Hameed, Nishar; Asgari, Alireza; Will, Frank

2013-07-21

The detection and control of the temperature variation at the nano-scale level of thermo-mechanical materials during a compression process have been challenging issues. In this paper, an empirical method is proposed to predict the temperature at the nano-scale level during the solid-state phase transition phenomenon in NiTi shape memory alloys. Isothermal data was used as a reference to determine the temperature change at different loading rates. The temperature of the phase transformed zone underneath the tip increased by ∼3 to 40 °C as the loading rate increased. The temperature approached a constant with further increase in indentation depth. A few layers of graphene were used to enhance the cooling process at different loading rates. Due to the presence of graphene layers the temperature beneath the tip decreased by a further ∼3 to 10 °C depending on the loading rate. Compared with highly polished NiTi, deeper indentation depths were also observed during the solid-state phase transition, especially at the rate dependent zones. Larger superelastic deformations confirmed that the latent heat transfer through the deposited graphene layers allowed a larger phase transition volume and, therefore, more stress relaxation and penetration depth.

Biofiltration of high loads of ethyl acetate in the presence of toluene.

PubMed

Deshusses, M; Johnson, C T; Leson, G

1999-08-01

To date, biofilters have been used primarily to control dilute, usually odorous, off-gases with relatively low volatile organic compound (VOC) concentrations (< 1 g m-3) and VOC loads (< 50 g m-3 hr-1). Recently, however, U.S. industry has shown an interest in applying biofilters to higher concentrations of VOCs and hazardous air pollutants (HAPs). In this study, the behavior of biofilters under high loads of binary VOC mixtures was studied. Two bench-scale biofilters were operated using a commercially available medium and a mixture of wood chips and compost. Both were exposed to varying mixtures of ethyl acetate and toluene. Concentration profiles and the corresponding removal efficiencies as a function of VOC loading were determined through frequent grab-sampling and GC analysis. Biofilter response to two frequently encountered operating problems--media dry-out and operating temperatures exceeding 40 degrees C--was also evaluated under controlled conditions. Microbial populations were also monitored to confirm the presence of organisms capable of degrading both major off-gas constituents. The results demonstrated several characteristics of biofilters operating under high VOC load conditions. Maximum elimination capacities for ethyl acetate were typically in the range of 200 g m-3 hr-1. Despite the presence of toluene degraders, the removal of toluene was inhibited by high loads of ethyl acetate. Several byproducts, particularly ethanol, were formed. Short-term dry-out and temperature excursions resulted in reduced performance.

Quantifying impacts of heat waves on power grid operation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ke, Xinda; Wu, Di; Rice, Jennie S.

Climate change is projected to cause an increase in the severity and frequency of extreme weather events such as heat waves and droughts. Such changes present planning and operating challenges and risks to many economic sectors. In the electricity sector, statistics of extreme events in the past have been used to help plan for future peak loads, determine associated infrastructure requirements, and evaluate operational risks, but industry-standard planning tools have yet to be coupled with or informed by temperature models to explore the impacts of the "new normal" on planning studies. For example, high ambient temperatures during heat waves reducemore » the output capacity and efficiency of gas fired combustion turbines just when they are needed most to meet peak demands. This paper describes the development and application of a production cost and unit commitment model coupled to high resolution, hourly temperature data and a temperature dependent load model. The coupled system has the ability to represent the impacts of hourly temperatures on load conditions and available capacity and efficiency of combustion turbines, and therefore capture the potential impacts on system reliability and production cost. Ongoing work expands this capability to address the impacts of water availability and temperature on power grid operation.« less

Application of CCG Sensors to a High-Temperature Structure Subjected to Thermo-Mechanical Load.

PubMed

Xie, Weihua; Meng, Songhe; Jin, Hua; Du, Chong; Wang, Libin; Peng, Tao; Scarpa, Fabrizio; Xu, Chenghai

2016-10-13

This paper presents a simple methodology to perform a high temperature coupled thermo-mechanical test using ultra-high temperature ceramic material specimens (UHTCs), which are equipped with chemical composition gratings sensors (CCGs). The methodology also considers the presence of coupled loading within the response provided by the CCG sensors. The theoretical strain of the UHTCs specimens calculated with this technique shows a maximum relative error of 2.15% between the analytical and experimental data. To further verify the validity of the results from the tests, a Finite Element (FE) model has been developed to simulate the temperature, stress and strain fields within the UHTC structure equipped with the CCG. The results show that the compressive stress exceeds the material strength at the bonding area, and this originates a failure by fracture of the supporting structure in the hot environment. The results related to the strain fields show that the relative error with the experimental data decrease with an increase of temperature. The relative error is less than 15% when the temperature is higher than 200 °C, and only 6.71% at 695 °C.

Review of specimen heating in mechanical tests at cryogenic temperatures

NASA Astrophysics Data System (ADS)

Ogata, T.; Yuri, T.; Ono, Y.

2014-01-01

At cryogenic temperatures near 4 K, a discontinuous deformation produces a large amount of specimen temperature rise that might bring significant changes in mechanical properties. The authors measured the specimen heating in tensile tests, fatigue test, and other tests in liquid helium for stainless steels and other materials. In this paper, we have measured the specimen temperature in high-cycle and low-cycle fatigue tests for stainless steels at various frequencies and stress levels and evaluated the testing conditions to keep the specimen at a specified temperature. We proposed maximum frequency in load-controlled fatigue tests for specified loading variables and a maximum strain rate in strain-controlled fatigue tests.

Fine characterization rock thermal damage by acoustic emission technique

NASA Astrophysics Data System (ADS)

Kong, Biao; Li, Zenghua; Wang, Enyuan

2018-02-01

This paper examines the differences in the thermal mechanical properties and acoustic emission (AE) characteristics during the deformation and fracture of rock under the action of continuous heating and after high-temperature treatment. Using AE 3D positioning technology, the development and evolution of the internal thermal cracks and the time domain of AE signals in rock were analyzed. High-temperature treatment causes thermal damage to rock. Under the action of continuous heating, the phase characteristics of AE time series correspond to the five stages of rock thermal deformation and fracture, respectively: the micro-defect development stage, the threshold interval of rock micro-cracks, the crack initiation stage, the crack propagation stage, and the crack multistage propagation evolution. When the initial crack propagates, the crack initiation of the rock causes the AE signal to produce a sudden mutation change. Mechanical fraction characteristics during rock uniaxial compression after temperature treatment indicated that the decrease rate of the rock compressive strength, wave velocity, and elastic modulus are relatively large during uniaxial compression tests after high-temperature treatment. During the deformation and fracture of rock under loading, there is faster growth of AE counts and AE events, indicating an increase in the speed of rock deformation and fracture under loading. AE counts show obvious changes during the latter loading stages, whereas AE events show obvious changes during the loading process. The results obtained are valuable for rock thermal stability detection and evaluation in actual underground engineering.

Analysis tool and methodology design for electronic vibration stress understanding and prediction

NASA Astrophysics Data System (ADS)

Hsieh, Sheng-Jen; Crane, Robert L.; Sathish, Shamachary

2005-03-01

The objectives of this research were to (1) understand the impact of vibration on electronic components under ultrasound excitation; (2) model the thermal profile presented under vibration stress; and (3) predict stress level given a thermal profile of an electronic component. Research tasks included: (1) retrofit of current ultrasonic/infrared nondestructive testing system with sensory devices for temperature readings; (2) design of software tool to process images acquired from the ultrasonic/infrared system; (3) developing hypotheses and conducting experiments; and (4) modeling and evaluation of electronic vibration stress levels using a neural network model. Results suggest that (1) an ultrasonic/infrared system can be used to mimic short burst high vibration loads for electronics components; (2) temperature readings for electronic components under vibration stress are consistent and repeatable; (3) as stress load and excitation time increase, temperature differences also increase; (4) components that are subjected to a relatively high pre-stress load, followed by a normal operating load, have a higher heating rate and lower cooling rate. These findings are based on grayscale changes in images captured during experimentation. Discriminating variables and a neural network model were designed to predict stress levels given temperature and/or grayscale readings. Preliminary results suggest a 15.3% error when using grayscale change rate and 12.8% error when using average heating rate within the neural network model. Data were obtained from a high stress point (the corner) of the chip.

Combined effects of cadmium, temperature and hypoxia-reoxygenation on mitochondrial function in rainbow trout (Oncorhynchus mykiss).

PubMed

Onukwufor, John O; Stevens, Don; Kamunde, Collins

2017-01-01

Although aquatic organisms face multiple environmental stressors that may interact to alter adverse outcomes, our knowledge of stressor-stressor interaction on cellular function is limited. We investigated the combined effects of cadmium (Cd), hypoxia-reoxygenation (H-R) and temperature on mitochondrial function. Liver mitochondria from juvenile rainbow trout were exposed to Cd (0-20μM) and H-R (0 and 5min) at 5, 13 and 25°C followed by measurements of mitochondrial Cd load, volume, complex І active (A)↔deactive (D) transition, membrane potential, ROS release and ultrastructural changes. At high temperature Cd exacerbated H-R-imposed reduction of maximal complex I (CI) respiration whereas at low temperature 5 and 10μM stimulated maximal CI respiration post H-R. The basal respiration showed a biphasic response at high temperatures with low Cd concentrations reducing the stimulatory effect of H-R and high concentrations enhancing this effect. At low temperature Cd monotonically enhanced H-R-induced stimulation of basal respiration. Cd and H-R reduced both the P/O ratio and the RCR at all 3 temperatures. Temperature rise alone increased mitochondrial Cd load and toxicity, but combined H-R and temperature exposure reduced mitochondrial Cd load but surprisingly exacerbated the mitochondrial dysfunction. Mitochondrial dysfunction induced by H-R was associated with swelling of the organelle and blocking of conversion of CІ D to A form. However, low amounts of Cd protected against H-R induced swelling and prevented the inhibition of H-R-induced CI D to A transition. Both H-R and Cd dissipated mitochondrial membrane potential Δψ m and damaged mitochondrial structure. We observed increased reactive oxygen species (H 2 O 2 ) release that together with the protection afforded by EGTA, vitamin E and N-acetylcysteine against the Δψ m dissipation suggested direct involvement of Cd and oxidative stress. Overall, our findings indicate that mitochondrial sensitivity to Cd toxicity was enhanced by the effects of H-R and temperature, and changes in mitochondrial Cd load did not always explain this effect. Copyright © 2016 Elsevier B.V. All rights reserved.

Abrasion-Resistant Coating for Flexible Insulation

NASA Technical Reports Server (NTRS)

Mui, D.; Headding, R. E.

1986-01-01

Ceramic coating increases durability and heat resistance of flexible high-temperature insulation. Coating compatible with quartz-fabric insulation allowing it to remain flexible during and after repeated exposures to temperatures of 1,800 degree F (982 degree C). Prevents fabric from becoming brittle while increasing resistance to aerodynamic abrasion and loading. Coating consists of penetrating precoat and topcoat. Major ingredients high-purity colloidal silica binder and ground silica filler, which ensure stability and compatibility with fabric at high temperatures. Both precoat and topcoat cured at room temperature.

Changes in leaf epicuticular wax load and its effect on leaf temperature and physiological traits in wheat cultivars (Triticum aestivum L.) exposed to high temperatures during anthesis

USDA-ARS?s Scientific Manuscript database

The physiological functions of epicuticular wax (EW) include reflectance of irradiation and the reduction of water loss. When a plant experiences stressful conditions, most notably, high irradiance and temperature, damage to the photosynthetic apparatus can occur and is signaled by a decrease in the...

Application of High-Temperature Extrinsic Fabry-Perot Interferometer Strain Sensor

NASA Technical Reports Server (NTRS)

Piazza, Anthony

2008-01-01

In this presentation to the NASA Aeronautics Sensor Working Group the application of a strain sensor is outlined. The high-temperature extrinsic Fabry-Perot interferometer (EFPI) strain sensor was developed due to a need for robust strain sensors that operate accurately and reliably beyond 1800 F. Specifically, the new strain sensor would provide data for validating finite element models and thermal-structural analyses. Sensor attachment techniques were also developed to improve methods of handling and protecting the fragile sensors during the harsh installation process. It was determined that thermal sprayed attachments are preferable even though cements are simpler to apply as cements are more prone to bond failure and are often corrosive. Previous thermal/mechanical cantilever beam testing of EFPI yielded very little change to 1200 F, with excellent correlation with SG to 550 F. Current combined thermal/mechanical loading for sensitivity testing is accomplished by a furnace/cantilever beam loading system. Dilatometer testing has can also be used in sensor characterization to evaluate bond integrity, evaluate sensitivity and accuracy and to evaluate sensor-to-sensor scatter, repeatability, hysteresis and drift. Future fiber optic testing will examine single-mode silica EFPIs in a combined thermal/mechanical load fixture on C-C and C-SiC substrates, develop a multi-mode Sapphire strain-sensor, test and evaluate high-temperature fiber Bragg Gratings for use as strain and temperature sensors and attach and evaluate a high-temperature heat flux gauge.

An Ultrahigh CO2-Loaded Silicalite-1 Zeolite: Structural Stability and Physical Properties at High Pressures and Temperatures.

PubMed

Marqueño, Tomas; Santamaria-Perez, David; Ruiz-Fuertes, Javier; Chuliá-Jordán, Raquel; Jordá, Jose L; Rey, Fernando; McGuire, Chris; Kavner, Abby; MacLeod, Simon; Daisenberger, Dominik; Popescu, Catalin; Rodriguez-Hernandez, Placida; Muñoz, Alfonso

2018-06-04

We report the formation of an ultrahigh CO 2 -loaded pure-SiO 2 silicalite-1 structure at high pressure (0.7 GPa) from the interaction of empty zeolite and fluid CO 2 medium. The CO 2 -filled structure was characterized in situ by means of synchrotron powder X-ray diffraction. Rietveld refinements and Fourier recycling allowed the location of 16 guest carbon dioxide molecules per unit cell within the straight and sinusoidal channels of the porous framework to be analyzed. The complete filling of pores by CO 2 molecules favors structural stability under compression, avoiding pressure-induced amorphization below 20 GPa, and significantly reduces the compressibility of the system compared to that of the parental empty one. The structure of CO 2 -loaded silicalite-1 was also monitored at high pressures and temperatures, and its thermal expansivity was estimated.

Bending cyclic load test for crystalline silicon photovoltaic modules

NASA Astrophysics Data System (ADS)

Suzuki, Soh; Doi, Takuya; Masuda, Atsushi; Tanahashi, Tadanori

2018-02-01

The failures induced by thermomechanical fatigue within crystalline silicon photovoltaic modules are a common issue that can occur in any climate. In order to understand these failures, we confirmed the effects of compressive or tensile stresses (which were cyclically loaded on photovoltaic cells and cell interconnect ribbons) at subzero, moderate, and high temperatures. We found that cell cracks were induced predominantly at low temperatures, irrespective of the compression or tension applied to the cells, although the orientation of cell cracks was dependent on the stress applied. The fracture of cell interconnect ribbons was caused by cyclical compressive stress at moderate and high temperatures, and this failure was promoted by the elevation of temperature. On the basis of these results, the causes of these failures are comprehensively discussed in relation to the viscoelasticity of the encapsulant.

Biofiltration of hydrogen sulfide by Sulfolobus metallicus at high temperatures.

PubMed

Morales, M; Silva, J; Morales, P; Gentina, J C; Aroca, G

2012-01-01

Biofiltration of reduced sulfur compounds such as hydrogen sulfide has been mainly applied to emissions at mild temperatures (25 to 35 °C). However, an important number of industrial gaseous emission containing sulfur compounds, from diverse industrial sectors (petroleum refinery, cellulose production, smelting, rendering plants and food industries) are emitted at temperatures over 50 °C. Most of the studies on thermophilic systems report that a higher elimination capacity can be obtained at elevated temperature, allowing the design of smaller equipment for the same loading rate than that required for removing the same load under mesophilic conditions. A biotrickling filter inoculated with Sulfolobus metallicus, which operates at three different residence times, 60, 80 and 120 s, and two different temperatures (45 and 55 °C) for treating H(2)S is reported. The input loads of H(2)S were progressively increased from 0 to 100 gS/m(3). The aim of this study was to determine the capacity and ability of S. metallicus to oxidize H(2)S at high temperatures. The better removal capacity of H(2)S obtained was 37.1 ± 1.7 gS/m(3) h at 55 °C for a residence time of 120 s. The difference of the removal capacity of H(2)S between the two temperatures was 4 g/m(3) h on average of sulfur removal for the different residence times.

Vacuum die attach for integrated circuits

DOEpatents

Schmitt, E.H.; Tuckerman, D.B.

1991-09-10

A thin film eutectic bond for attaching an integrated circuit die to a circuit substrate is formed by coating at least one bonding surface on the die and substrate with an alloying metal, assembling the die and substrate under compression loading, and heating the assembly to an alloying temperature in a vacuum. A very thin bond, 10 microns or less, which is substantially void free, is produced. These bonds have high reliability, good heat and electrical conduction, and high temperature tolerance. The bonds are formed in a vacuum chamber, using a positioning and loading fixture to compression load the die, and an IR lamp or other heat source. For bonding a silicon die to a silicon substrate, a gold silicon alloy bond is used. Multiple dies can be bonded simultaneously. No scrubbing is required. 1 figure.

Vacuum die attach for integrated circuits

DOEpatents

Schmitt, Edward H.; Tuckerman, David B.

1991-01-01

A thin film eutectic bond for attaching an integrated circuit die to a circuit substrate is formed by coating at least one bonding surface on the die and substrate with an alloying metal, assembling the die and substrate under compression loading, and heating the assembly to an alloying temperature in a vacuum. A very thin bond, 10 microns or less, which is substantially void free, is produced. These bonds have high reliability, good heat and electrical conduction, and high temperature tolerance. The bonds are formed in a vacuum chamber, using a positioning and loading fixture to compression load the die, and an IR lamp or other heat source. For bonding a silicon die to a silicon substrate, a gold silicon alloy bond is used. Multiple dies can be bonded simultaneously. No scrubbing is required.

An investigation of preload relaxation behaviour of three zinc- aluminum alloys

NASA Astrophysics Data System (ADS)

Mir, A. A.

2016-08-01

Zinc alloy castings are usually assembled together or mounted by screwed steel fasteners, and are tightened to a predetermined torque to develop the required tensile preload in the fastener. Due to relaxation processes in the castings, creep may cause a partial preload loss at an elevated temperature. The equipment used for load relaxation tests consists of a loadmonitoring device, an oil bath, and a data-acquisition system. A load cell monitoring device is used to monitor the load loss in an ISO-metric M6*1 steel screw set into sand castings made from alloys No. 3, No. 5 and No. 2 and tightened to produce an initial preload of 6 kN. The castings were held at constant temperature in the range 80 - 120°C in an oil bath. The oil bath maintains the desired test temperature throughout the experiment. All tests were conducted for periods of up to 160 h. For all alloys, the initial load loss was high, decreasing gradually with time, but not ceasing. The load loss increased rapidly with test temperature, and almost all of the relaxation curves approximated to a logarithmic decay of load with time. Alloy No. 2 had the best resistance to load loss, with No. 5 next and No. 3 worst at all temperatures. The lower resistance to relaxation of alloy No. 3 was mainly due to the lower relaxation strength of copper-free primary dendrites, whereas in alloys No. 5 and No. 2, the higher copper contents contribute greatly to their relaxation strength in the form of second-phase particles.

The 77 K operation of a multi-resonant power converter

NASA Technical Reports Server (NTRS)

Ray, Biswajit; Gerber, Scott S.; Patterson, Richard L.; Myers, Ira T.

1995-01-01

The liquid-nitrogen temperature (77 K) operation of a 55 W, 200 kHz, 48/28 V zero-voltage switching multi-resonant dc/dc converter designed with commercially available components is reported. Upon dipping the complete converter (power and control circuits) into liquid-nitrogen, the converter performance improved as compared to the room-temperature operation. The switching frequency, resonant frequency, and the characteristic impedance did not change significantly. Accordingly, the zero-voltage switching was maintained from no-load to full-load for the specified line variations. Cryoelectronics can provide high density power converters, especially for high power applications.

Temperature dependent mechanical property of PZT film: an investigation by nanoindentation.

PubMed

Li, Yingwei; Feng, Shangming; Wu, Wenping; Li, Faxin

2015-01-01

Load-depth curves of an unpoled Lead Zirconate Titanate (PZT) film composite as a function of temperature were measured by nanoindentation technique. Its reduce modulus and hardness were calculated by the typical Oliver-Pharr method. Then the true modulus and hardness of the PZT film were assessed by decoupling the influence of substrate using methods proposed by Zhou et al. and Korsunsky et al., respectively. Results show that the indentation depth and modulus increase, but the hardness decreases at elevated temperature. The increasing of indentation depth and the decreasing of hardness are thought to be caused by the decreasing of the critical stress needed to excite dislocation initiation at high temperature. The increasing of true modulus is attributed to the reducing of recoverable indentation depth induced by back-switched domains. The influence of residual stress on the indentation behavior of PZT film composite was also investigated by measuring its load-depth curves with pre-load strains.

Analysis of intelligent hinged shell structures: deployable deformation and shape memory effect

NASA Astrophysics Data System (ADS)

Shi, Guang-Hui; Yang, Qing-Sheng; He, X. Q.

2013-12-01

Shape memory polymers (SMPs) are a class of intelligent materials with the ability to recover their initial shape from a temporarily fixable state when subjected to external stimuli. In this work, the thermo-mechanical behavior of a deployable SMP-based hinged structure is modeled by the finite element method using a 3D constitutive model with shape memory effect. The influences of hinge structure parameters on the nonlinear loading process are investigated. The total shape memory of the processes the hinged structure goes through, including loading at high temperature, decreasing temperature with load carrying, unloading at low temperature and recovering the initial shape with increasing temperature, are illustrated. Numerical results show that the present constitutive theory and the finite element method can effectively predict the complicated thermo-mechanical deformation behavior and shape memory effect of SMP-based hinged shell structures.

In Situ Characterization of Mesoporous Co/CeO 2 Catalysts for the High-Temperature Water-Gas Shift

DOE Office of Scientific and Technical Information (OSTI.GOV)

Vovchok, Dimitriy; Guild, Curtis J.; Dissanayake, Shanka

Here, mesoporous Co/CeO 2 catalysts were found to exhibit significant activity for the high-temperature water-gas shift (WGS) reaction with cobalt loadings as low as 1 wt %. The catalysts feature a uniform dispersion of cobalt within the CeO 2 fluorite type lattice with no evidence of discrete cobalt phase segregation. In situ XANES and ambient pressure XPS experiments were used to elucidate the active state of the catalysts as partially reduced cerium oxide doped with oxidized cobalt atoms. In situ XRD and DRIFTS experiments suggest facile cerium reduction and oxygen vacancy formation, particularly with lower cobalt loadings. In situ DRIFTSmore » analysis also revealed the presence of surface carbonate and bidentate formate species under reaction conditions, which may be associated with additional mechanistic pathways for the WGS reaction. Deactivation behavior was observed with higher cobalt loadings. XANES data suggest the formation of small metallic cobalt clusters at temperatures above 400 °C may be responsible. Notably, this deactivation was not observed for the 1% cobalt loaded catalyst, which exhibited the highest activity per unit of cobalt.« less

In Situ Characterization of Mesoporous Co/CeO 2 Catalysts for the High-Temperature Water-Gas Shift

DOE PAGES

Vovchok, Dimitriy; Guild, Curtis J.; Dissanayake, Shanka; ...

2018-04-04

Here, mesoporous Co/CeO 2 catalysts were found to exhibit significant activity for the high-temperature water-gas shift (WGS) reaction with cobalt loadings as low as 1 wt %. The catalysts feature a uniform dispersion of cobalt within the CeO 2 fluorite type lattice with no evidence of discrete cobalt phase segregation. In situ XANES and ambient pressure XPS experiments were used to elucidate the active state of the catalysts as partially reduced cerium oxide doped with oxidized cobalt atoms. In situ XRD and DRIFTS experiments suggest facile cerium reduction and oxygen vacancy formation, particularly with lower cobalt loadings. In situ DRIFTSmore » analysis also revealed the presence of surface carbonate and bidentate formate species under reaction conditions, which may be associated with additional mechanistic pathways for the WGS reaction. Deactivation behavior was observed with higher cobalt loadings. XANES data suggest the formation of small metallic cobalt clusters at temperatures above 400 °C may be responsible. Notably, this deactivation was not observed for the 1% cobalt loaded catalyst, which exhibited the highest activity per unit of cobalt.« less

Catalytic Decarboxylation of Fatty Acids to Aviation Fuels over Nickel Supported on Activated Carbon

PubMed Central

Wu, Jianghua; Shi, Juanjuan; Fu, Jie; Leidl, Jamie A.; Hou, Zhaoyin; Lu, Xiuyang

2016-01-01

Decarboxylation of fatty acids over non-noble metal catalysts without added hydrogen was studied. Ni/C catalysts were prepared and exhibited excellent activity and maintenance for decarboxylation. Thereafter, the effects of nickel loading, catalyst loading, temperature, and carbon number on the decarboxylation of fatty acids were investigated. The results indicate that the products of cracking increased with high nickel loading or catalyst loading. Temperature significantly impacted the conversion of stearic acid but did not influence the selectivity. The fatty acids with large carbon numbers tend to be cracked in this reaction system. Stearic acid can be completely converted at 370 °C for 5 h, and the selectivity to heptadecane was around 80%. PMID:27292280

Tailored metal matrix composites for high-temperature performance

NASA Technical Reports Server (NTRS)

Morel, M. R.; Saravanos, D. A.; Chamis, C. C.

1992-01-01

A multi-objective tailoring methodology is presented to maximize stiffness and load carrying capacity of a metal matrix cross-ply laminated at elevated temperatures. The fabrication process and fiber volume ratio are used as the design variables. A unique feature is the concurrent effects from fabrication, residual stresses, material nonlinearity, and thermo-mechanical loading on the laminate properties at the post-fabrication phase. For a (0/90)(sub s) graphite/copper laminate, strong coupling was observed between the fabrication process, laminate characteristics, and thermo-mechanical loading. The multi-objective tailoring was found to be more effective than single objective tailoring. Results indicate the potential to increase laminate stiffness and load carrying capacity by controlling the critical parameters of the fabrication process and the laminate.

High-response and low-temperature nitrogen dioxide gas sensor based on gold-loaded mesoporous indium trioxide.

PubMed

Li, Shan; Cheng, Ming; Liu, Guannan; Zhao, Lianjing; Zhang, Bo; Gao, Yuan; Lu, Huiying; Wang, Haiyu; Zhao, Jing; Liu, Fangmeng; Yan, Xu; Zhang, Tong; Lu, Geyu

2018-04-10

Nitrogen dioxide (NO 2 ), as a typical threatening atmospheric pollutant, is hazardous to the environment and human health. Thus, the development of a gas sensor with high response and low detection limit for NO 2 detection is highly important. The highly ordered mesoporous indium trioxide (In 2 O 3 ) prepared by simple nanocasting method using mesoporous silica as template and decorated with Au nanoparticles was investigated for NO 2 detection. The prepared materials were characterized by X-ray diffraction, transmission electron microscopy, and X-ray photoelectron spectroscopy. Characterization results showed that the samples exhibited ordered mesostructure and were successfully decorated with Au. The gas sensing performance of the sensors based on a series of Au-loaded mesoporous In 2 O 3 were systematically investigated. The Au loading level strongly affected the sensing performance toward NO 2 . The optimal sensor, which was based on 0.5 wt% Au-loaded In 2 O 3 , displayed high sensor response and low detection limit of 10 ppb at low operating temperature of 65 °C. The excellent sensing properties were mainly attributed to the ordered mesoporous structure and the catalytic performance of Au. We believe that the Au-loaded mesoporous In 2 O 3 can provide a promising platform for NO 2 gas sensors with excellent performance. Copyright © 2018 Elsevier Inc. All rights reserved.

System Design of a Natural Gas PEM Fuel Cell Power Plant for Buildings

DOE Office of Scientific and Technical Information (OSTI.GOV)

Joe Ferrall, Tim Rehg, Vesna Stanic

2000-09-30

The following conclusions are made based on this analysis effort: (1) High-temperature PEM data are not available; (2) Stack development effort for Phase II is required; (3) System results are by definition preliminary, mostly due to the immaturity of the high-temperature stack; other components of the system are relatively well defined; (4) The Grotthuss conduction mechanism yields the preferred system characteristics; the Grotthuss conduction mechanism is also much less technically mature than the vehicle mechanism; (5) Fuel processor technology is available today and can be procured for Phase II (steam or ATR); (6) The immaturity of high-temperature membrane technology requiresmore » that a robust system design be developed in Phase II that is capable of operating over a wide temperature and pressure range - (a) Unpressurized or Pressurized PEM (Grotthuss mechanism) at 140 C, Highest temperature most favorable, Lowest water requirement most favorable, Pressurized recommended for base loaded operation, Unpressurized may be preferred for load following; (b) Pressurized PEM (vehicle mechanism) at about 100 C, Pressure required for saturation, Fuel cell technology currently available, stack development required. The system analysis and screening evaluation resulted in the identification of the following components for the most promising system: (1) Steam reforming fuel processor; (2) Grotthuss mechanism fuel cell stack operating at 140 C; (3) Means to deliver system waste heat to a cogeneration unit; (4) Pressurized system utilizing a turbocompressor for a base-load power application. If duty cycling is anticipated, the benefits of compression may be offset due to complexity of control. In this case (and even in the base loaded case), the turbocompressor can be replaced with a blower for low-pressure operation.« less

Development of thermosensitive microgel-loaded cotton fabric for controlled drug release

NASA Astrophysics Data System (ADS)

Sun, Xiao-Zhu; Wang, Xiao; Wu, Jun-Zi; Li, Shu-De

2017-05-01

COS-g-PVCL copolymer was synthesized and infiltrated into CaCO3 particles to prepare thermosensitive porous microgels which exhibited phase transition behavior at the temperature that was similar to the lower critical solution temperature(LCST) of copolymer. The incorporation of microgel to cotton was done by pad-dry-cure method from aqueous microparticle dispersion that contained citric acid as a crosslinking agent. In vitro drug release experiments were performed at two different temperatures (25 and 37 °C) in PBS of pH 7.4 to study its drug release behavior with response to temperature. Due to the shrinkage of microgels, drug release profiles obtained were found to have enhanced release for aloin when the temperature was above LCST than other release conditions. Microgel-loaded fabrics proved to be in vivo biocompatible by skin irritation studies and displayed an obviously high water vapor permeability at 40 °C. The MTT assay showed no obvious cytotoxicity of microgel-loaded cotton against mouse fibroblast cells within 5 days. The results obtained demonstrated the potential use of the thermos-responsive microgel-loaded cotton fabrics as a textile-based drug delivery system for treating sunburn or skin care.

Parametric study of the lubrication of thrust loaded 120-mm bore ball bearings to 3 million DN

NASA Technical Reports Server (NTRS)

Signer, H.; Bamberger, E. N.; Zaretsky, E. V.

1973-01-01

A parametric study was performed with 120-mm bore angular-contact ball bearings under varying thrust loads, bearing and lubricant temperatures, and cooling and lubricant flow rates. Contact angles were nominally 20 and 24 deg with bearing speeds to 3 million DN. Endurance tests were run at 3 million DN and a temperature of 492 K (425 F) with 10 bearings having a nominal 24 deg contact angle at a thrust load of 22241 N (5000 lb). Bearing operating temperature, differences in temperatures between the inner and outer races, and bearing power consumption can be tuned to any desirable operating requirement by varying 4 parameters. These parameters are outer-race cooling, inner-race cooling, lubricant flow to the inner race, and oil inlet temperature. Preliminary endurance tests at 3 million DN and 492 K (425 F) indicate that long term bearing operation can be achieved with a high degree of reliability.

Steam-load-forecasting technique for central-heating plants. Final report

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lin, M.C.; Carnahan, J.V.

Because boilers generally are most efficient at full loads, the Army could achieve significant savings by running fewer boilers at high loads rather than more boilers at low loads. A reliable load prediction technique could help ensure that only those boilers required to meet demand are on line. This report presents the results of an investigation into the feasibility of forecasting heat plant steam loads from historical patterns and weather information. Using steam flow data collected at Fort Benjamin Harrison, IN, a Box-Jenkins transfer function model with an acceptably small prediction error was initially identified. Initial investigation of forecast modelmore » development appeared successful. Dynamic regression methods using actual ambient temperatures yielded the best results. Box-Jenkins univariate models' results appeared slightly less accurate. Since temperature information was not needed for model building and forecasting, however, it is recommended that Box-Jenkins models be considered prime candidates for load forecasting due to their simpler mathematics.« less

Oil-Free Rotor Support Technologies for an Optimized Helicopter Propulsion System

NASA Technical Reports Server (NTRS)

DellaCorte, Christopher; Bruckner, Robert J.

2007-01-01

An optimized rotorcraft propulsion system incorporating a foil air bearing supported Oil-Free engine coupled to a high power density gearbox using high viscosity gear oil is explored. Foil air bearings have adequate load capacity and temperature capability for the highspeed gas generator shaft of a rotorcraft engine. Managing the axial loads of the power turbine shaft (low speed spool) will likely require thrust load support from the gearbox through a suitable coupling or other design. Employing specially formulated, high viscosity gear oil for the transmission can yield significant improvements (approx. 2X) in allowable gear loading. Though a completely new propulsion system design is needed to implement such a system, improved performance is possible.

The Reduced Effectiveness of EGR to Mitigate Knock at High Loads in Boosted SI Engines

DOE Office of Scientific and Technical Information (OSTI.GOV)

Szybist, James P.; Wagnon, Scott W.; Splitter, Derek A.

Numerous studies have demonstrated that exhaust gas recirculation (EGR) can attenuate knock propensity in spark ignition (SI) engines at naturally aspirated or lightly boosted conditions. In this paper, we investigate the role of cooled EGR under higher load conditions with multiple fuel compositions, where highly retarded combustion phasing typical of modern SI engines was used. It was found that under these conditions, EGR attenuation of knock is greatly reduced, where EGR doesn’t allow significant combustion phasing advance as it does under lighter load conditions. Detailed combustion analysis shows that when EGR is added, the polytropic coefficient increases causing the compressivemore » pressure and temperature to increase. At sufficiently highly boosted conditions, the increase in polytropic coefficient and additional trapped mass from EGR can sufficiently reduce fuel ignition delay to overcome knock attenuation effects. Kinetic modeling demonstrates that the effectiveness of EGR to mitigate knock is highly dependent on the pressure-temperature condition. Experiments at 2000 rpm have confirmed reduced fuel ignition delay under highly boosted conditions relevant to modern downsized boosted SI engines, where in-cylinder pressure is higher and the temperature is cooler. Finally, at these conditions, charge reactivity increases compared to naturally aspirated conditions, and attenuation of knock by EGR is reduced.« less

The Reduced Effectiveness of EGR to Mitigate Knock at High Loads in Boosted SI Engines

DOE PAGES

Szybist, James P.; Wagnon, Scott W.; Splitter, Derek A.; ...

2017-09-04

Numerous studies have demonstrated that exhaust gas recirculation (EGR) can attenuate knock propensity in spark ignition (SI) engines at naturally aspirated or lightly boosted conditions. In this paper, we investigate the role of cooled EGR under higher load conditions with multiple fuel compositions, where highly retarded combustion phasing typical of modern SI engines was used. It was found that under these conditions, EGR attenuation of knock is greatly reduced, where EGR doesn’t allow significant combustion phasing advance as it does under lighter load conditions. Detailed combustion analysis shows that when EGR is added, the polytropic coefficient increases causing the compressivemore » pressure and temperature to increase. At sufficiently highly boosted conditions, the increase in polytropic coefficient and additional trapped mass from EGR can sufficiently reduce fuel ignition delay to overcome knock attenuation effects. Kinetic modeling demonstrates that the effectiveness of EGR to mitigate knock is highly dependent on the pressure-temperature condition. Experiments at 2000 rpm have confirmed reduced fuel ignition delay under highly boosted conditions relevant to modern downsized boosted SI engines, where in-cylinder pressure is higher and the temperature is cooler. Finally, at these conditions, charge reactivity increases compared to naturally aspirated conditions, and attenuation of knock by EGR is reduced.« less

Study on the effect of temperature rise on grain refining during fabrication of nanocrystalline copper under explosive loading

NASA Astrophysics Data System (ADS)

Wang, Jinxiang; Yang, Rui; Jiang, Li; Wang, Xiaoxu; Zhou, Nan

2013-11-01

Nanocrystalline (NC) copper was fabricated by severe plastic deformation of coarse-grained copper at a high strain rate under explosive loading. The feasibility of grain refinement under different explosive loading and the influence of overall temperature rise on grain refinement under impact compression were studied in this paper. The calculation model for the macroscopic temperature rise was established according to the adiabatic shock compression theory. The calculation model for coarse-grained copper was established by the Voronoi method and the microscopic temperature rise resulted from severe plastic deformation of grains was calculated by ANSYS/ls-dyna finite element software. The results show that it is feasible to fabricate NC copper by explosively dynamic deformation of coarse-grained copper and the average grain size of the NC copper can be controlled between 200˜400 nm. The whole temperature rise would increase with the increasing explosive thickness. Ammonium nitrate fuel oil explosive was adopted and five different thicknesses of the explosive, which are 20 mm, 25 mm, 30 mm, 35 mm, 45 mm, respectively, with the same diameter using 20 mm to the fly plate were adopted. The maximum macro and micro temperature rise is up to 532.4 K, 143.4 K, respectively, which has no great effect on grain refinement due to the whole temperature rise that is lower than grain growth temperature according to the high pressure melting theory.

Investigation of the deformation mechanisms of core-shell rubber-modified epoxy at cryogenic temperatures

NASA Astrophysics Data System (ADS)

Brown, Hayley Rebecca

The industrial demand for high strength-to-weight ratio materials is increasing due to the need for high performance components. Epoxy polymers, although often used in fiber-reinforced polymeric composites, have an inherent low toughness that further decreases with decreasing temperatures. Second-phase additives have been effective in increasing the toughness of epoxies at room temperature; however, the mechanisms at low temperatures are still not understood. In this study, the deformation mechanisms of a DGEBA epoxy modified with MX960 core-shell rubber (CSR) particles were investigated under quasi-static tensile and impact loads at room temperature (RT) and liquid nitrogen (LN 2) temperature. Overall, the CSR had little effect on the tensile properties at RT and LN2 temperature. The impact strength decreased from neat to 3 wt% but increased from neat to 5 wt% at RT and LN2 temperature, with a higher impact strength at RT at all CSR loadings. The CSR particles debonded in front of the crack tip, inducing voids into the matrix. It was found that an increase in shear deformation and void growth likely accounted for the higher impact strength at 5 wt% CSR loading at RT while the thermal stress fields due to the coefficient of thermal expansion mismatch between rubber and epoxy and an increase in secondary cracking is likely responsible for the higher impact strength at 5 wt% tested at LN2 temperature. While a large toughening effect was not seen in this study, the mechanisms analyzed herein will likely be of use for further material investigations at cryogenic temperatures.

Effects of Adiabatic Heating on the High Strain Rate Deformation of Polymer Matrix Composites

NASA Technical Reports Server (NTRS)

Sorini, Chris; Chattopadhyay, Aditi; Goldberg, Robert K.

2017-01-01

Polymer matrix composites (PMCs) are increasingly being used in aerospace structures that are expected to experience complex dynamic loading conditions throughout their lifetime. As such, a detailed understanding of the high strain rate behavior of the constituents, particularly the strain rate, temperature, and pressure dependent polymer matrix, is paramount. In this paper, preliminary efforts in modeling experimentally observed temperature rises due to plastic deformation in PMCs subjected to dynamic loading are presented. To this end, an existing isothermal viscoplastic polymer constitutive formulation is extended to model adiabatic conditions by incorporating temperature dependent elastic properties and modifying the components of the inelastic strain rate tensor to explicitly depend on temperature. It is demonstrated that the modified polymer constitutive model is capable of capturing strain rate and temperature dependent yield as well as thermal softening associated with the conversion of plastic work to heat at high rates of strain. The modified constitutive model is then embedded within a strength of materials based micromechanics framework to investigate the manifestation of matrix thermal softening, due to the conversion of plastic work to heat, on the high strain rate response of a T700Epon 862 (T700E862) unidirectional composite. Adiabatic model predictions for high strain rate composite longitudinal tensile, transverse tensile, and in-plane shear loading are presented. Results show a substantial deviation from isothermal conditions; significant thermal softening is observed for matrix dominated deformation modes (transverse tension and in-plane shear), highlighting the importance of accounting for the conversion of plastic work to heat in the polymer matrix in the high strain rate analysis of PMC structures.

Optimizing the performance of catalytic traps for hydrocarbon abatement during the cold-start of a gasoline engine.

PubMed

Puértolas, B; Navlani-García, M; García, T; Navarro, M V; Lozano-Castelló, D; Cazorla-Amorós, D

2014-08-30

A key target to reduce current hydrocarbon emissions from vehicular exhaust is to improve their abatement under cold-start conditions. Herein, we demonstrate the potential of factorial analysis to design a highly efficient catalytic trap. The impact of the synthesis conditions on the preparation of copper-loaded ZSM-5 is clearly revealed by XRD, N2 sorption, FTIR, NH3-TPD, SEM and TEM. A high concentration of copper nitrate precursor in the synthesis improves the removal of hydrocarbons, providing both strong adsorption sites for hydrocarbon retention at low temperature and copper oxide nanoparticles for full hydrocarbon catalytic combustion at high temperature. The use of copper acetate precursor leads to a more homogeneous dispersion of copper oxide nanoparticles also providing enough catalytic sites for the total oxidation of hydrocarbons released from the adsorption sites, although lower copper loadings are achieved. Thus, synthesis conditions leading to high copper loadings jointly with highly dispersed copper oxide nanoparticles would result in an exceptional catalytic trap able to reach superior hydrocarbon abatement under highly demanding operational conditions. Copyright © 2014 Elsevier B.V. All rights reserved.

Mechanical properties of shape memory polymers for morphing aircraft applications

NASA Astrophysics Data System (ADS)

Keihl, Michelle M.; Bortolin, Robert S.; Sanders, Brian; Joshi, Shiv; Tidwell, Zeb

2005-05-01

This investigation addresses basic characterization of a shape memory polymer (SMP) as a suitable structural material for morphing aircraft applications. Tests were performed for monotonic loading in high shear at constant temperature, well below, or just above the glass transition temperature. The SMP properties were time-and temperature-dependent. Recovery by the SMP to its original shape needed to be unfettered. Based on the testing SMPs appear to be an attractive and promising component in the solution for a skin material of a morphing aircraft. Their multiple state abilities allow them to easily change shape and, once cooled, resist large loads.

Constitutive response of Rene 80 under thermal mechanical loads

NASA Technical Reports Server (NTRS)

Kim, K. S.; Cook, T. S.; Mcknight, R. L.

1988-01-01

The applicability of a classical constitutive model for stress-strain analysis of a nickel base superalloy, Rene' 80, in the gas turbine thermomechanical fatigue (TMF) environment is examined. A variety of tests were conducted to generate basic material data and to investigate the material response under cyclic thermomechanical loading. Isothermal stress-strain data were acquired at a variety of strain rates over the TMF temperature range. Creep curves were examined at 2 temperature ranges, 871 to 982 C and 760 to 871 C. The results provide optimism on the ability of the classical constitutive model for high temperature applications.

Performance and Durability of High Temperature Foil Air Bearings for Oil-Free Turbomachinery

NASA Technical Reports Server (NTRS)

DellaCorte, C.; Lukaszewicz, V.; Valco, M. J.; Radil, K. C.; Heshmat, H.

2000-01-01

The performance and durability of advanced, high temperature foil air bearings are evaluated under a wide range (10-50 kPa) of loads at temperatures from 25 to 650 C. The bearings are made from uncoated nickel based superalloy foils. The foil surface experiences sliding contact with the shaft during initial start/stop operation. To reduce friction and wear, the solid lubricant coating, PS304, is applied to the shaft by plasma spraying. PS304 is a NiCr based Cr2O3 coating with silver and barium fluoride/calcium fluoride solid lubricant additions. The results show that the bearings provide lives well in excess of 30,000 cycles under all of the conditions tested. Several bearings exhibited lives in excess of 100,000 cycles. Wear is a linear function of the bearing load. The excellent performance measured in this study suggests that these bearings and the PS304 coating are well suited for advanced high temperature, oil-free turbomachinery applications.

Thermocryogenic buckling and stress analyses of a partially filled cryogenic tank subjected to cylindrical strip heating

NASA Technical Reports Server (NTRS)

Ko, William L.

1994-01-01

Thermocryogenic buckling and stress analyses were conducted on a horizontally oriented cryogenic tank using the finite element method. The tank is a finite-length circular cylindrical shell with its two ends capped with hemispherical shells. The tank is subjected to cylindrical strip heating in the region above the liquid-cryogen fill level and to cryogenic cooling below the fill level (i.e., under thermocryogenic loading). The effects of cryogen fill level on the buckling temperature and thermocryogenic stress field were investigated in detail. Both the buckling temperature and stress magnitudes were relatively insensitive to the cryogen fill level. The buckling temperature, however, was quite sensitive to the radius-to-thickness ratio. A mechanical stress analysis of the tank also was conducted when the tank was under: (1) cryogen liquid pressure loading; (2) internal pressure loading; and (3) tank-wall inertia loading. Deformed shapes of the cryogenic tanks under different loading conditions were shown, and high-stress domains were mapped on the tank wall for the strain-gage installations. The accuracies of solutions from different finite element models were compared.

An Experimental Investigation Into the Temperature Profile of a Compliant Foil Air Bearing

NASA Technical Reports Server (NTRS)

Radil, Kevin; Zeszotek, Michelle

2004-01-01

A series of tests was performed to determine the internal temperature profile in a compliant bump-type foil journal air bearing operating at room temperature under various speeds and load conditions. The temperature profile was collected by instrumenting a foil bearing with nine, type K thermocouples arranged in the center and along the bearing s edges in order to measure local temperatures and estimate thermal gradients in the axial and circumferential directions. To facilitate the measurement of maximum temperatures from viscous shearing in the air film, the thermocouples were tack welded to the backside of the bumps that were in direct contact with the top foil. The mating journal was coated with a high temperature solid lubricant that, together with the bearing, underwent high temperature start-stop cycles to produce a smooth, steady-state run-in surface. Tests were conducted at speeds from 20 to 50 krpm and loads ranging from 9 to 222 N. The results indicate that, over the conditions tested, both journal rotational speed and radial load are responsible for heat generation with speed playing a more significant role in the magnitude of the temperatures. The temperature distribution was nearly symmetric about the bearing center at 20 and 30 krpm but became slightly skewed toward one side at 40 and 50 krpm. Surprisingly, the maximum temperatures did not occur at the bearing edge where the minimum film thickness is expected but rather in the middle of the bearing where analytical investigations have predicted the air film to be much thicker. Thermal gradients were common during testing and were strongest in the axial direction from the middle of the bearing to its edges, reaching 3.78 8C/mm. The temperature profile indicated the circumferential thermal gradients were negligible.

Apparatus for combinatorial screening of electrochemical materials

DOEpatents

Kepler, Keith Douglas [Belmont, CA; Wang, Yu [Foster City, CA

2009-12-15

A high throughput combinatorial screening method and apparatus for the evaluation of electrochemical materials using a single voltage source (2) is disclosed wherein temperature changes arising from the application of an electrical load to a cell array (1) are used to evaluate the relative electrochemical efficiency of the materials comprising the array. The apparatus may include an array of electrochemical cells (1) that are connected to each other in parallel or in series, an electronic load (2) for applying a voltage or current to the electrochemical cells (1), and a device (3), external to the cells, for monitoring the relative temperature of each cell when the load is applied.

Effects of Brass (Cu3Zn2) as High Thermal Expansion Material on Shrink Disc Performance During High Thermal Loading

NASA Astrophysics Data System (ADS)

Mazlan, MIS; Mohd, SA; Bahar, ND; Aziz, SAA

2018-03-01

This research work is focused on shrink disc operation at high temperature. Geometrical and material design selections have been done by taking into consideration the existing shrink disc operating at high temperature condition. The existing shrink disc confronted slip between shaft and shaft sleeve during thermal loading condition. The assessment has been obtained through virtual experiment by using Finite Element Analysis (FEA) -Thermal Transient Stress for 900 seconds with 300 °C of thermal loading. This investigation consists of the current and improved version of shrink disc, where identical geometries and material properties were utilized. High Thermal Expansion (HTE) material has been introduced to overcome the current design of the shrink disc. Brass (Cu3Zn2) has been selected as the HTE material in the improved shrink disc design due to its high thermal expansion properties. The HTE has shown a significant improvement on the total contact area and contact pressure on the shaft and the shaft sleeve. The improved shrink disc embedded with HTE during thermal loading exhibit a minimum of 1244.1 mm2 of the total area on shaft and shaft sleeve which uninfluenced the total contact area at normal condition which is 1254.3 mm2. Meanwhile, the total pressure of improved shrink disc had an increment of 108.1 MPa while existing shrink disc total pressure has lost 17.2 MPa during thermal loading.

Ternary nucleation as a mechanism for the production of diesel nanoparticles: experimental analysis of the volatile and hygroscopic properties of diesel exhaust using the volatilization and humidification tandem differential mobility analyzer.

PubMed

Meyer, N K; Ristovski, Z D

2007-11-01

The volatile and hygroscopic properties of diesel nanoparticles were simultaneously determined under a range of engine loads using the volatilization and humidification tandem differential mobility analyzer (VH-TDMA). Additionally, the VH-TDMA was used to measure changes in the hygroscopic behavior of the heterogeneously nucleated diesel nanoparticles as one or more semivolatile species were removed via thermal evaporation or decomposition. Particles produced at high loads exhibited high, dual-step volatility, while those particles produced at low loads were less volatile and exhibited continuous volatilization curves. The hygroscopic growth factor of the particles was shown to be load dependent with high-load particles exhibiting growth factors similar to that of ammonium sulfate. At 85% relative humidity, particles produced at moderate loads exhibited growth factors of approximately 1.1 while low-load particles were shown to be hydrophobic. Growth factors and volatilization temperatures measured for high-load particles clearly indicate that ternary nucleation is involved in particle formation.

Prophylactic augmentation of the proximal femur: an investigation of two techniques.

PubMed

Raas, Christoph; Hofmann-Fliri, Ladina; Hörmann, Romed; Schmoelz, Werner

2016-03-01

Osteoporotic hip fractures are an increasing problem in an ageing population. They result in high morbidity, mortality and high socioeconomic costs. For patients with poor bone quality, prophylactic augmentation of the proximal femur might be an option for fracture prevention. In two groups of paired human femora the potential of limited polymethyl-methacrylate (PMMA) augmentation (11-15 ml) in a V-shape pattern and the insertion of a proximal femur nail antirotation (PFNA) blade were investigated. The testing was carried out pair wise simulating the single leg stand. The untreated femur in each pair served as control. An axial load was applied until failure. Load displacement parameters and temperature increase during the augmentation process were recorded. In the PMMA group no significant difference was found between the augmented and non-augmented specimen concerning load to failure (p = 0.35) and energy to failure (p = 0.9). A median temperature increase of 9.5 °C was observed in the augmented specimen. A significant correlation was found between the amount of applied PMMA and the temperature increase (Cor. Coef. = 0.82, p = 0.042). In the PFNA group, a significant decrease of load to failure and a non-significant decrease of energy to failure were observed (p = 0.037 and p = 0.075). Limited V-shaped PMMA augmentation and PFNA blade insertion did not show any improvement in failure load or energy to failure. Volumes of up to 15 ml PMMA did not cause a critical surface temperature increase.

Improving the High Temperature Creep and Rupture Resistance of Oxide- Dispersion-Strengthened Alloys

DTIC Science & Technology

1982-04-30

more ready availability and its es - tablished high temperature data base. When work was formally initiated, an order was placed for a billet of...between the specimen heads and grips. -. The test apparatus used to perform the tensile tests was an Instron- Satec furnace combination, Temperature...12,000 lb. capacity) modified to produce constant stress rather than constant load. The furnaces were of the Satec tube-type, with a maximum temperature

Dynamic Fracture Initiation Toughness at Elevated Temperatures With Application to the New Generation of Titanium Aluminide Alloys. Chapter 8

NASA Technical Reports Server (NTRS)

Shazly, Mostafa; Prakash, Vikas; Draper, Susan; Shukla, Arun (Editor)

2006-01-01

Recently, a new generation of titanium aluminide alloy, named Gamma-Met PX, has been developed with better rolling and post-rolling characteristics. I'revious work on this alloy has shown the material to have higher strengths at room and elevated temperatures when compared with other gamma titanium aluminides. In particular, this new alloy has shown increased ductility at elevated temperatures under both quasi-static and high strain rate uniaxial compressive loading. However, its high strain rate tensile ductility at room and elevated temperatures is limited to approx. 1%. In the present chapter, results of a study to investigate the effects of loading rate and test temperature on the dynamic fracture initiation toughness in Gamma-Met PX are presented. Modified split Hopkinson pressure bar was used along with high-speed photography to determine the crack initiation time. Three-point bend dynamic fracture experiments were conducted at impact speeds of approx. 1 m/s and tests temperatures of up-to 1200 C. The results show that thc dynamic fracture initiation toughness decreases with increasing test temperatures beyond 600 C. Furthermore, thc effect of long time high temperature air exposure on the fracture toughness was investigated. The dynamic fracture initiation toughness was found to decrease with increasing exposure time. The reasons behind this drop are analyzed and discussed.

Bithermal fatigue: A simplified alternative to thermomechanical fatigue

NASA Technical Reports Server (NTRS)

Verrilli, Michael J.

1988-01-01

A bithermal fatigue test technique was proposed as a simplified alternative to the thermomechanical fatigue test. Both the thermomechanical cycle and the bithermal technique can be used to study nonisothermal fatigue behavior. The difference between the two cycles is that in a conventional thermomechanical fatigue cycle the temperature is continuously varied concurrently with the applied mechanical strains, but in the bithermal fatigue cycle the specimen is held at zero load during the temperature excursions and all the loads are applied at the two extreme temperatures of the cycle. Experimentally, the bithermal fatigue test technique offers advantages such as ease in synchronizing the temperature and mechanical strain waveforms, in minimizing temperature gradients in the specimen gauge length, and in reducing and interpreting thermal fatigue such as the influence of alternate high and low temperatures on the cyclic stress-strain response characteristics, the effects of thermal state, and the possibility of introducing high- and low-temperature deformation mechanisms within the same cycle. The bithermal technique was used to study nonisothermal fatigue behavior of alloys such as single-crystal PWA 1480, single-crystal Rene N4, cast B1900+Hf, and wrought Haynes 188.

Preliminary analytical study on the feasibility of using reinforced concrete pile foundations for renewable energy storage by compressed air energy storage technology

NASA Astrophysics Data System (ADS)

Tulebekova, S.; Saliyev, D.; Zhang, D.; Kim, J. R.; Karabay, A.; Turlybek, A.; Kazybayeva, L.

2017-11-01

Compressed air energy storage technology is one of the promising methods that have high reliability, economic feasibility and low environmental impact. Current applications of the technology are mainly limited to energy storage for power plants using large scale underground caverns. This paper explores the possibility of making use of reinforced concrete pile foundations to store renewable energy generated from solar panels or windmills attached to building structures. The energy will be stored inside the pile foundation with hollow sections via compressed air. Given the relatively small volume of storage provided by the foundation, the required storage pressure is expected to be higher than that in the large-scale underground cavern. The high air pressure typically associated with large temperature increase, combined with structural loads, will make the pile foundation in a complicated loading condition, which might cause issues in the structural and geotechnical safety. This paper presents a preliminary analytical study on the performance of the pile foundation subjected to high pressure, large temperature increase and structural loads. Finite element analyses on pile foundation models, which are built from selected prototype structures, have been conducted. The analytical study identifies maximum stresses in the concrete of the pile foundation under combined pressure, temperature change and structural loads. Recommendations have been made for the use of reinforced concrete pile foundations for renewable energy storage.

Molecular dynamics simulation of shock-wave loading of copper and titanium

NASA Astrophysics Data System (ADS)

Bolesta, A. V.; Fomin, V. M.

2017-10-01

At extreme pressures and temperatures common materials form new dense phases with compacted atomic arrangements. By classical molecular dynamics simulation we observe that FCC copper undergo phase transformation to BCC structure. The transition occurs under shock wave loading at the pressures above 80 GPa and corresponding temperatures above 2000 K. We calculate phase diagram, show that at these pressures and low temperature FCC phase of copper is still stable and discuss the thermodynamic reason for phase transformation at high temperature shock wave regime. Titanium forms new hexagonal phase at high pressure as well. We calculate the structure of shock wave in titanium and observe that shock front splits in three parts: elastic, plastic and phase transformation. The possibility of using a phase transition behind a shock wave with further unloading for designing nanocrystalline materials with a reduced grain size is also shown.

Elevated temperature biaxial fatigue

NASA Technical Reports Server (NTRS)

Jordan, E. H.

1984-01-01

A three year experimental program for studying elevated temperature biaxial fatigue of a nickel based alloy Hastelloy-X has been completed. A new high temperature fatigue test facility with unique capabilities has been developed. Effort was directed toward understanding multiaxial fatigue and correlating the experimental data to the existing theories of fatigue failure. The difficult task of predicting fatigue lives for non-proportional loading was used as an ultimate test for various life prediction methods being considered. The primary means of reaching improved undertanding were through several critical non-proportional loading experiments. It was discovered that the cracking mode switched from primarily cracking on the maximum shear planes at room temperature to cracking on the maximum normal strain planes at 649 C.

Hostile environments and high temperature measurements; Proceedings of the Conference, Kansas City, MO, Nov. 6-8, 1989

NASA Astrophysics Data System (ADS)

Topics presented include the identification of stagnant region in a fluidized bed combustor, high sensitivity objective grating speckle, an X-ray beam method for displacement and strain distributions using the moire method, and high-temperature deformation of a Ti-alloy composite under complex loading. Also addressed are a hybrid procedure for dynamic characterization of ceramics at elevated temperature, thermo-structural measurements in a SiC coated carbon-carbon hypersonic glide vehicle, and recent experience with elevated-temperature foil strain gages with application to thin-gage materials.

Enzymatic saccharification of brown seaweed for production of fermentable sugars.

PubMed

Sharma, Sandeep; Horn, Svein Jarle

2016-08-01

This study shows that high drying temperatures negatively affect the enzymatic saccharification yield of the brown seaweed Saccharina latissima. The optimal drying temperature of the seaweed in terms of enzymatic sugar release was found to be 30°C. The enzymatic saccharification process was optimized by investigating factors such as kinetics of sugar release, enzyme dose, solid loading and different blend ratios of cellulases and an alginate lyase. It was found that the seaweed biomass could be efficiently hydrolysed to fermentable sugars using a commercial cellulase cocktail. The inclusion of a mono-component alginate lyase was shown to improve the performance of the enzyme blend, in particular at high solid loadings. At 25% dry matter loading a combined glucose and mannitol concentration of 74g/L was achieved. Copyright © 2016 Elsevier Ltd. All rights reserved.

Sliding Contact Bearings for Service to 700 C

NASA Technical Reports Server (NTRS)

Sliney, Harold E.

1996-01-01

Cylindrical, sliding contact bearings made entirely of a self-lubricating powder metallurgy composite (PM212) or of super alloy shells lined with clad PM212 were tested in an oscillating mode at temperatures from 25 to 700 C. Tests of 100 hr duration or longer were conducted at a bearing unit load of 3.45 Mpa (500 psi). Shorter duration tests at various unit loads up to 24.1 Mpa (3500 psi) were also conducted. In comparison tests, bearings lubricated with PM212 had superior anti-wear characteristics compared to the baseline, unlubricated, super alloy bearings: no galling of PM212-lubricated bearings occurred, while severe surface damage including galling occurred, especially at high loads, during the baseline tests. A heat treatment procedure, which dimensionally stabilizes PM212 and thereby minimizes clearance changes during high temperature bearing operation, is described.

High-Temperature Vibration Damper

NASA Technical Reports Server (NTRS)

Clarke, Alan; Litwin, Joel; Krauss, Harold

1987-01-01

Device for damping vibrations functions at temperatures up to 400 degrees F. Dampens vibrational torque loads as high as 1,000 lb-in. but compact enough to be part of helicopter rotor hub. Rotary damper absorbs energy from vibrating rod, dissipating it in turbulent motion of viscous hydraulic fluid forced by moving vanes through small orifices.

Effect of K loadings on nitrate formation/decomposition and on NOx storage performance of K-based NOx storage-reduction catalysts

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kim, Do Heui; Mudiyanselage, Kumudu K.; Szanyi, Janos

2013-10-25

We have investigated nitrate formation and decomposition processes, and measured NOx storage performance on Pt-K2O/Al2O3 catalysts as a function of potassium loading. After NO2 adsorption at room temperature, ionic and bidentate nitrates were observed by fourier transform infra-red (FTIR) spectroscopy. The ratio of the former to the latter species increased with increasing potassium loading up to 10 wt%, and then stayed almost constant with additional K, demonstrating a clear dependence of loading on the morphology of the K species. Although both K2O(10)/Al2O3 and K2O(20)/Al2O3 samples have similar nitrate species after NO2 adsorption, the latter has more thermally stable nitrate speciesmore » as evidenced by FTIR and NO2 temperature programmed desorption (TPD) results. With regard to NOx storage performance, the temperature of maximum NOx uptake (Tmax) is 573 K up to a potassium loading of 10 wt%. As the potassium loading increases from 10 wt% to 20 wt%, Tmax shifted from 573 K to 723 K. Moreover, the amount of NO uptake (38 cm3 NOx/g catal) at Tmax increased more than three times, indicating that efficiency of K in storing NOx is enhanced significantly at higher temperature, in good agreement with the NO2 TPD and FTIR results. Thus, a combination of characterization and NOx storage performance results demonstrates an unexpected effect of potassium loading on nitrate formation and decomposition processes; results important for developing Pt-K2O/Al2O3 for potential applications as high temperature NOx storage-reduction catalysts.« less

Design and evaluation of thin metal surface insulation for hypersonic flight

NASA Technical Reports Server (NTRS)

Miller, R. C.; Petach, A. M.

1976-01-01

An all-metal insulation was studied as a thermal protection system for hypersonic vehicles. Key program goals included fabricating the insulation in thin packages which are optimized for high temperature insulation of an actively cooled aluminum structure, and the use of state-of-the-art alloys. The insulation was fabricated from 300 series stainless steel in thicknesses of 0.8 to 12 mm. The outer, 0.127 mm thick, skin was textured to accommodate thermal expansion and oxidized to increase emittance. The thin insulating package was achieved using an insulation concept consisting of foil radiation shields spaced within the package, and conical foil supports to carry loads from the skin and maintain package dimensions. Samples of the metal-insulation were tested to evaluate thermal insulation capability, rain and sand erosion resistance, high temperature oxidation resistance, applied load capability, and high temperature emittance.

Design of high precision temperature control system for TO packaged LD

NASA Astrophysics Data System (ADS)

Liang, Enji; Luo, Baoke; Zhuang, Bin; He, Zhengquan

2017-10-01

Temperature is an important factor affecting the performance of TO package LD. In order to ensure the safe and stable operation of LD, a temperature control circuit for LD based on PID technology is designed. The MAX1978 and an external PID circuit are used to form a control circuit that drives the thermoelectric cooler (TEC) to achieve control of temperature and the external load can be changed. The system circuit has low power consumption, high integration and high precision,and the circuit can achieve precise control of the LD temperature. Experiment results show that the circuit can achieve effective and stable control of the laser temperature.

Navy High-Strength Steel Corrosion-Fatigue Modeling Program

DTIC Science & Technology

2006-10-01

interest. In the global analysis, the axial loading and residual stress (via the temperature profile discussed in the previous section) were applied to...developed based on observa- tions from analyses of axial load components with sinusoidally varying surface geometries. These observations indicated that...profile parameters (height and wavelength in each surface direction) and the applied axial loading . Stress Varies Sinusoidally 180° Out of Phase

Application of CCG Sensors to a High-Temperature Structure Subjected to Thermo-Mechanical Load

PubMed Central

Xie, Weihua; Meng, Songhe; Jin, Hua; Du, Chong; Wang, Libin; Peng, Tao; Scarpa, Fabrizio; Xu, Chenghai

2016-01-01

This paper presents a simple methodology to perform a high temperature coupled thermo-mechanical test using ultra-high temperature ceramic material specimens (UHTCs), which are equipped with chemical composition gratings sensors (CCGs). The methodology also considers the presence of coupled loading within the response provided by the CCG sensors. The theoretical strain of the UHTCs specimens calculated with this technique shows a maximum relative error of 2.15% between the analytical and experimental data. To further verify the validity of the results from the tests, a Finite Element (FE) model has been developed to simulate the temperature, stress and strain fields within the UHTC structure equipped with the CCG. The results show that the compressive stress exceeds the material strength at the bonding area, and this originates a failure by fracture of the supporting structure in the hot environment. The results related to the strain fields show that the relative error with the experimental data decrease with an increase of temperature. The relative error is less than 15% when the temperature is higher than 200 °C, and only 6.71% at 695 °C. PMID:27754356

Characteristics of ring type traveling wave ultrasonic motor in vacuum.

PubMed

Qu, Jianjun; Zhou, Ningning; Tian, Xiu; Jin, Long; Xu, Zhike

2009-03-01

The characteristics of ultrasonic motor strongly depend on the properties of stator/rotor contact interface which are affected by ambient environment. With the developed apparatus, load properties of two ring type traveling wave ultrasonic motors in atmosphere, low vacuum and high vacuum were studied, respectively. Wear of friction material, variations of vacuum degree and the temperature of motor during the experiment were also measured. The results show that load properties of motor A in vacuum were poorer than those in atmosphere, when load torque M(f) was less than 0.55 N m. Compared to motor A, load properties of motor B were affected a little by environmental pressure. Wear of friction material in vacuum was more severe than wear in atmosphere. The temperature of motor in vacuum rose more quickly than it in atmosphere and had not reached equilibrium in 2 h experiment. However, the temperature of motor in atmosphere had reached equilibrium in about forth minutes. Furthermore, outgas was also observed during experiment under vacuum conditions.

Effects of repeated bending load at room temperature for composite Nb3Sn wires

NASA Astrophysics Data System (ADS)

Awaji, Satoshi; Watanabe, Kazuo; Katagiri, Kazumune

2003-09-01

In order to realize a react and wind (R&W) method for Nb3Sn wires, the influences of a bending load at room temperature are investigated. Usually, the superconducting wires undergo bending loads at room temperature repeatedly during winding and insulation processes. We define these bending loads as 'pre-bending' treatments. We applied the pre-bending strain of 0 and 0.5% to the highly strengthened CuNb/(Nb, Ti)3Sn wires, and measured the stress/strain properties and critical currents. The improvements of stress dependence of normalized critical current and the increase of the maximum critical current by the pre-bending treatments were found. The model based on the distribution of the local tensile strain as a bending strain describes the experimental results well without the increase of the maximum critical current. When the pre-bending strain was applied, the calculated results indicate that the mechanical properties are improved due to the local work hardening, and hence the stress dependence of Ic increases.

Study of factors influencing the mechanical properties of polyurethane foams under dynamic compression

NASA Astrophysics Data System (ADS)

Linul, E.; Marsavina, L.; Voiconi, T.; Sadowski, T.

2013-07-01

Effect of density, loading rate, material orientation and temperature on dynamic compression behavior of rigid polyurethane foams are investigated in this paper. These parameters have a very important role, taking into account that foams are used as packing materials or dampers which require high energy impact absorption. The experimental study was carried out on closed-cell rigid polyurethane (PUR) foam specimens of different densities (100, 160 respectively 300 kg/m3), having a cubic shape. The specimens were subjected to uniaxial dynamic compression with loading rate in range of 1.37-3.25 m/s, using four different temperatures (20, 60, 90, 110°C) and two loading planes (direction (3) - rise direction and direction (2) - in plane). Experimental results show that Young's modulus, yield stress and plateau stress values increases with increasing density. One of the most significant effects of mechanical properties in dynamic compression of rigid PUR foams is the density, but also the loading speed, material orientation and temperature influences the behavior in compression

Elastoviscoplastic snap-through behavior of shallow arches subjected to thermomechanical loads

NASA Technical Reports Server (NTRS)

Simitses, George J.; Song, Yuzhao; Sheinman, Izhak

1991-01-01

The problem of snap-through buckling of clamped shallow arches under thermomechanical loads is investigated. The analysis is based on nonlinear kinematic relations and nonlinear rate-dependent unified constitutive equations. A finite element approach is employed to predict the, in general, inelastic buckling behavior. The construction material is alloy B1900 + Hf, which is commonly utilized in high-temperature environments. The effect of several parameters is assessed. These parameters include the rise parameter and temperature. Comparison between elastic and elastoviscoplastic responses is also presented.

Past Performance analysis of HPOTP bearings

NASA Technical Reports Server (NTRS)

Bhat, B. N.; Dolan, F. J.

1982-01-01

The past performance analysis conducted on three High Pressure Oxygen Turbopump (HPOTP) bearings from the Space Shuttle Main Engine is presented. Metallurgical analysis of failed bearing balls and races, and wear track and crack configuration analyses were carried out. In addition, one bearing was tested in laboratory at very high axial loads. The results showed that the cracks were surface initiated and propagated into subsurface locations at relatively small angles. Subsurface cracks were much more extensive than was appeared on the surface. The location of major cracks in the races corresponded to high radial loads rather than high axial loads. There was evidence to suggest that the inner races were heated to elevated temperatures. A failure scenario was developed based on the above findings. According to this scenario the HPOTP bearings are heated by a combination of high loads and high coefficient of friction (poor lubrication). Different methods of extending the HPOTP bearing life are also discussed. These include reduction of axial loads, improvements in bearing design, lubrication and cooling, and use of improved bearing materials.

Influence of Crystal Expansion/Contraction on Zeolite Membrane Permeation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sorenson, Stephanie G; Payzant, E Andrew; Noble, Richard D

X-ray diffraction was used to measure the unit cell parameters of B-ZSM-5, SAPO-34, and NaA zeolite powders as a function of adsorbate loading at 303 K, and in one case, at elevated temperatures. Most adsorbates expanded the zeolite crystals below saturation loading at 303 K: n-hexane and SF6 in B-ZSM-5, methanol and CO2 in SAPO-34, and methanol in NaA zeolite. As the loadings increased, the crystals expanded more. Changes in the unit cell volumes of B-ZSM-5 and SAPO-34 zeolite powders correlated with changes in permeation through zeolite membranes defects. When the zeolite crystals expanded or contracted upon adsorption, the defectmore » sizes decreased or increased. In B-ZSM-5 membranes, the fluxes through defects decreased dramatically when n-hexane or SF6 adsorbed. In contrast, i-butane adsorption at 303 K contracted B-ZSM-5 crystals at low loadings and expanded them at higher loadings. Correspondingly, the flux through B-ZSM-5 membrane defects increased at low i-butane loadings and decreased at high loading because the defects increased in size at low loading and decreased at high loadings. At 398 K and 473 K, n-hexane expanded the B-ZSM-5 unit cell more as the temperature increased from 303 to 473 K. The silicalite-1 and B-ZSM-5 unit cell volumes expanded similarly upon n-hexane adsorption at 303 K; boron substitution had little effect on volume expansion.« less

Two-stage high frequency pulse tube refrigerator with base temperature below 10 K

NASA Astrophysics Data System (ADS)

Chen, Liubiao; Wu, Xianlin; Liu, Sixue; Zhu, Xiaoshuang; Pan, Changzhao; Guo, Jia; Zhou, Yuan; Wang, Junjie

2017-12-01

This paper introduces our recent experimental results of pulse tube refrigerator driven by linear compressor. The working frequency is 23-30 Hz, which is much higher than the G-M type cooler (the developed cryocooler will be called high frequency pulse tube refrigerator in this paper). To achieve a temperature below 10 K, two types of two-stage configuration, gas coupled and thermal coupled, have been designed, built and tested. At present, both types can achieve a no-load temperature below 10 K by using only one compressor. As to gas-coupled HPTR, the second stage can achieve a cooling power of 16 mW/10K when the first stage applied a 400 mW heat load at 60 K with a total input power of 400 W. As to thermal-coupled HPTR, the designed cooling power of the first stage is 10W/80K, and then the temperature of the second stage can get a temperature below 10 K with a total input power of 300 W. In the current preliminary experiment, liquid nitrogen is used to replace the first coaxial configuration as the precooling stage, and a no-load temperature 9.6 K can be achieved with a stainless steel mesh regenerator. Using Er3Ni sphere with a diameter about 50-60 micron, the simulation results show it is possible to achieve a temperature below 8 K. The configuration, the phase shifters and the regenerative materials of the developed two types of two-stage high frequency pulse tube refrigerator will be discussed, and some typical experimental results and considerations for achieving a better performance will also be presented in this paper.

Erosion/corrosion of turbine airfoil materials in the high-velocity effluent of a pressurized fluidized coal combustor

NASA Technical Reports Server (NTRS)

Zellars, G. R.; Rowe, A. P.; Lowell, C. E.

1978-01-01

Four candidate turbine airfoil superalloys were exposed to the effluent of a pressurized fluidized bed with a solids loading of 2 to 4 g/scm for up to 100 hours at two gas velocities, 150 and 270 m/sec, and two temperatures, 730 deg and 795 C. Under these conditions, both erosion and corrosion occurred. The damaged specimens were examined by cross-section measurements, scanning electron and light microscopy, and X-ray analysis to evaluate the effects of temperature, velocity, particle loading, and alloy material. Results indicate that for a given solids loading the extent of erosion is primarily dependent on gas velocity. Corrosion occurred only at the higher temperature. There was little difference in the erosion/corrosion damage to the four alloys tested under these severe conditions.

On the Lateral Compressive Behavior of Empty and Ex-Situ Aluminum Foam-Filled Tubes at High Temperature

PubMed Central

Movahedi, Nima; Marsavina, Liviu

2018-01-01

In this research work, the effect of lateral loading (LL) on the crushing performance of empty tubes (ETs) and ex situ aluminum foam-filled tubes (FFTs) was investigated at 300 °C. The cylindrical thin-walled steel tube was filled with the closed-cell aluminum alloy foam that compressed under quasi-static loading conditions. During the compression test, the main mechanical properties of the ETs improved due to the interaction effect between the cellular structure of the foam and the inner wall of the empty tube. In addition, the initial propagated cracks on the steel tubes reduced considerably as a result of such interaction. Furthermore, the obtained results of the LL loading were compared with the axial loading (AL) results for both ETs and FFTs at the same temperature. The findings indicated that the application of loading on the lateral surface of the composite causes the lower mechanical properties of both ETs and FFTs in comparison with the axial loading conditions. PMID:29617300

DOE Office of Scientific and Technical Information (OSTI.GOV)

Szybist, James P.; Splitter, Derek A.

The octane sensitivity (S), defined as the difference between the Research Octane Number (RON) and the Motor Octane Number (MON), is of increasing interest in spark ignition (SI) engines because of its relevance to knock resistance at boosted high load conditions. In this study, three fuels with nearly constant RON (99.2-100) and varying S (S = 0, 6.5, and 12) are operated at the knock limited spark advance (KLSA) at nominal engine loads of 10, 15, and 20 bar IMEP in a single cylinder SI engine with side-mount direct injection fueling, at λ =1 stoichiometry. At each load condition, themore » intake manifold temperature is swept from 35 °C to 95 °C to alter the temperature and pressure history of the charge. Results show that at the 10 bar IMEP condition, knock resistance is inversely proportional to fuel S where the S=0 fuel is the most knock resist, but as load increases the trend reverses and knock resistance becomes proportional to fuel S, and the S=12 fuel is the most knock resistant. The reversal of knock resistance as a function of S with load it is attributed to changing fuel ignition delay, as bulk gas intermediate temperature heat release (ITHR) is observed for the S = 0 several crank angles prior to the spark command and ITHR magnitude is a function of increasing intake temperature. As intake temperature continued to increase, the S=0 fuel transitioned from ITHR to low-temperature heat release (LTHR) prior to the spark event. At the highest load and intake temperature, 95 C, the S=0 fuel exhibits distinct LTHR and negative temperature coefficient (NTC), and the intermediate S value fuel (S=6.5) exhibited distinct ITHR behavior several crank angles prior to the spark command. However, for the tested conditions, the S=12 fuel exhibits neither ITHR nor LTHR. To understand the measured trends, chemical kinetic modeling is used to elucidate the fuel specific dependencies on in-cylinder temperature and pressure history. Lastly, the bulk gas composition change that occurs for fuels and conditions exhibiting ITHR and LTHR is analyzed in the modeling, including their implications on flame speed and combustion stability at late phasing. Furthermore, the combined findings illustrate the commonality and utility of fuel S, ITHR, LTHR, and NTC across a wide range of conditions, and the associated implications of fuel S in highly boosted modern GDI SI engines relative to the RON and MON tests.« less

Zr Extrusion – Direct Input for Models & Validation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cerreta, Ellen Kathleen

As we examine differences in the high strain rate, high strain tensile response of high purity, highly textured Zr as a function of loading direction, temperature and extrusion velocity with primarily post mortem characterization techniques, we have also developed a technique for characterizing the in-situ extrusion process. This particular measurement is useful for partitioning energy of the system during the extrusion process: friction, kinetic energy, and temperature

Experimental investigation into the coupling effects of magnetic field, temperature and pressure on electrical resistivity of non-oriented silicon steel sheet

NASA Astrophysics Data System (ADS)

Xiao, Lijun; Yu, Guodong; Zou, Jibin; Xu, Yongxiang

2018-05-01

In order to analyze the performance of magnetic device which operate at high temperature and high pressure, such as submersible motor, oil well transformer, the electrical resistivity of non-oriented silicon steel sheets is necessary for precise analysis. But the reports of the examination of the measuring method suitable for high temperature up to 180 °C and high pressure up to 140 MPa are few. In this paper, a measurement system based on four-probe method and Archimedes spiral shape measurement specimens is proposed. The measurement system is suitable for measuring the electrical resistivity of unconventional specimens under high temperature and high pressure and can simultaneously consider the influence of the magnetic field on the electrical resistivity. It can be seen that the electrical resistivity of the non-oriented silicon steel sheets will fluctuate instantaneously when the magnetic field perpendicular to the conductive path of the specimens is loaded or removed. The amplitude and direction of the fluctuation are not constant. Without considering the effects of fluctuations, the electrical resistivity of the non-oriented silicon steel sheets is the same when the magnetic field is loaded or removed. And the influence of temperature on the electrical resistivity of the non-oriented silicon steel sheet is still the greatest even though the temperature and the pressure are coupled together. The measurement results also show that the electrical resistivity varies linearly with temperature, so the temperature coefficient of resistivity is given in the paper.

Mechanical and Microstructure Study of Nickel-Based ODS Alloys Processed by Mechano-Chemical Bonding and Ball Milling

NASA Astrophysics Data System (ADS)

Amare, Belachew N.

Due to the need to increase the efficiency of modern power plants, land-based gas turbines are designed to operate at high temperature creating harsh environments for structural materials. The elevated turbine inlet temperature directly affects the materials at the hottest sections, which includes combustion chamber, blades, and vanes. Therefore, the hottest sections should satisfy a number of material requirements such as high creep strength, ductility at low temperature, high temperature oxidation and corrosion resistance. Such requirements are nowadays satisfied by implementing superalloys coated by high temperature thermal barrier coating (TBC) systems to protect from high operating temperature required to obtain an increased efficiency. Oxide dispersive strengthened (ODS) alloys are being considered due to their high temperature creep strength, good oxidation and corrosion resistance for high temperature applications in advanced power plants. These alloys operating at high temperature are subjected to different loading systems such as thermal, mechanical, and thermo-mechanical combined loads at operation. Thus, it is critical to study the high temperature mechanical and microstructure properties of such alloys for their structural integrity. The primary objective of this research work is to investigate the mechanical and microstructure properties of nickel-based ODS alloys produced by combined mechano-chemical bonding (MCB) and ball milling subjected to high temperature oxidation, which are expected to be applied for high temperature turbine coating with micro-channel cooling system. Stiffness response and microstructure evaluation of such alloy systems was studied along with their oxidation mechanism and structural integrity through thermal cyclic exposure. Another objective is to analyze the heat transfer of ODS alloy coatings with micro-channel cooling system using finite element analysis (FEA) to determine their feasibility as a stand-alone structural coating. During this project it was found that stiffness response to increase and remain stable to a certain level and reduce at latter stages of thermal cyclic exposure. The predominant growth and adherent Ni-rich outer oxide scale was found on top of the alumina scale throughout the oxidation cycles. The FEA analysis revealed that ODS alloys could be potential high temperature turbine coating materials if micro-channel cooling system is implemented.

Rudder/Fin Seal Investigations for the X-38 Re-Entry Vehicle

NASA Technical Reports Server (NTRS)

Dunlap, Patrick H., Jr.; Steinetz, Bruce M.; Curry, Donald M.

2000-01-01

NASA is currently developing the X-38 vehicle that will be used to demonstrate the technologies required for a crew return vehicle (CRV) for the International Space Station. The X-38 control surfaces require high temperature seals to limit hot gas ingestion and transfer of heat to underlying low-temperature structures to prevent over-temperature of these structures and possible loss of the vehicle. This paper presents results for thermal analyses and flow and compression tests conducted on as-received and thermally exposed seals for the rudder/fin location of the X-38. A thermal analysis of the rudder/fin dual seal assembly based on representative heating rates on the windward surface of the rudder/fin area predicted a peak seal temperature of 1900 F. The temperature-exposed seals were heated in a compressed state at 1900 F corresponding to the predicted peak temperature. Room temperature compression tests were performed to determine load versus linear compression, preload, contact area, stiffness, and resiliency characteristics for the as-received and temperature-exposed seals. Temperature exposure resulted in permanent set and loss of resiliency in these seals. Unit loads and contact pressures for the seals were below the 5 lb/in. and 10 psi limits set to limit the loads on the Shuttle thermal tiles that the seals seal against in the rudder/fin location. Measured seal flow rates for a double seal were about 4.5 times higher than the preliminary seal flow goal. The seal designs examined in this study are expected to be able to endure the high temperatures that they will be exposed to for a single-use life. Tests performed herein combined with future analyses, arc jet tests, and scrubbing tests will be used to select the final seal design for this application.

Rudder/Fin Seal Investigations for the X-38 Re-Entry Vehicle

NASA Technical Reports Server (NTRS)

Dunlap, Patrick H., Jr.; Steinetz, Bruce M.; Curry, Donald M.

2000-01-01

NASA is currently developing the X-38 vehicle that will be used to demonstrate the technologies required for a crew return vehicle (CRV) for the International Space Station. The X-38 control surfaces require high temperature seals to limit hot gas ingestion and transfer of heat to underlying low-temperature structures to prevent over-temperature of these structures and possible loss of the vehicle. This paper presents results for thermal analyses and flow and compression tests conducted on as-received and thermally exposed seals for the rudder/fin location of the X-38. A thermal analysis of the rudder/fin dual seal assembly based on representative heating rates on the windward surface of the rudder/fin area predicted a peak seal temperature of 1900 F. The temperature-exposed seals were heated in a compressed state at 1900 F corresponding to the predicted peak temperature. Room temperature compression tests were performed to determine load versus linear compression, preload, contact area, stiffness, and resiliency characteristics for the as-received and temperature-exposed seals. Temperature exposure resulted in permanent set and loss of resiliency in these seals. Unit loads and contact pressures for the seals were below the five pounds/inch and ten psi limits set to limit the loads on the Shuttle thermal tiles that the seals seal against in the rudder/fin location. Measured seal flow rates for a double seal were about 4.5 times higher than the preliminary seal flow goal. The seal designs examined in this study are expected to be able to endure the high temperatures that they will be exposed to for a single-use life. Tests performed herein combined with future analyses, arc jet tests, and scrubbing tests will be used to select the final seal design for this application.

The first man-loading high temperature superconducting Maglev test vehicle in the world

NASA Astrophysics Data System (ADS)

Wang, Jiasu; Wang, Suyu; Zeng, Youwen; Huang, Haiyu; Luo, Fang; Xu, Zhipei; Tang, Qixue; Lin, Guobin; Zhang, Cuifang; Ren, Zhongyou; Zhao, Guomin; Zhu, Degui; Wang, Shaohua; Jiang, He; Zhu, Min; Deng, Changyan; Hu, Pengfei; Li, Chaoyong; Liu, Fang; Lian, Jisan; Wang, Xiaorong; Wang, Lianghui; Shen, Xuming; Dong, Xiaogang

2002-10-01

The first man-loading high temperature superconducting Maglev test vehicle in the world is reported. This vehicle was first tested successfully on December 31, 2000 in the Applied Superconductivity Laboratory, Southwest Jiaotong University, China. Heretofore over 17,000 passengers took the vehicle, and it operates very well from beginning to now. The function of suspension is separated from one of propulsion. The high temperature superconducting Maglev provides inherent stable forces both in the levitation and in the guidance direction. The vehicle is 3.5 m long, 1.2 m wide, and 0.8 m high. When five people stand on vehicle and the total weight is 530 kg, the net levitation gap is more than 20 mm. The whole vehicle system includes three parts, vehicle body, guideway and controlling system. The high temperature superconducting Maglev equipment on board is the most important for the system. The onboard superconductors are melt-textured YBaCuO bulks. The superconductors are fixed on the bottom of liquid nitrogen vessels and cooled by liquid nitrogen. The guideway consists of two parallel permanent magnetic tracks, whose surface concentrating magnetic field is up to 1.2 T. The guideway is 15.5 m long.

Delayed elasticity in Zerodur® at room temperature

NASA Astrophysics Data System (ADS)

Pepi, John W.; Golini, Donald

1991-12-01

Much has been written about structural relaxation, viscous flow, delayed elasticity, hysteresis, and other dimensional stability phenomena of glass and ceramics at elevated temperatures. Less has been documented about similar effects at room temperature. The time dependent phenomenon of delayed elasticity exhibited by Zerodur has been studied at room temperature and is presented here. Using a high-performance mechanical profilometer, a delayed strain on the order of 1 percent is realized over a period of a few weeks, under low stress levels. An independent test using optical interferometry validates the results. A comparison of Corning ULE silica glass is also made. The effect is believed to be related to the alkali oxide content of the glass ceramic and rearrangement of the ion groups within the structure during stress. The effect, apparent under externally applied load, is elastic and repeatable, that is, no hysteresis of permanent set, as measured at elevated temperature, is evidenced within measurement capabilities. Nonetheless, it must be accounted for in determining the magnitude of distortion under load (delayed elastic creep) and upon load removal (delayed elastic recovery). This is particularly important for large lightweight optics which might undergo large strain during fabrication and environmental loading, such as experienced in gravity release or in dynamic control of active optics.

Northwest Manufacturing Initiative

DTIC Science & Technology

2013-03-26

Testing of Metallic Materials] specifications. For high temperature tests, a heated water bath was use while for low temperature testing down to...Weld metal and heat affected zones were evaluated using Charpy and E399 fracture toughness methods. The influence of temperature , loading rate, CVN...determine the influence of fracture test methods and welding procedures on toughness. Room temperature E399 tests, (CTS) were carried out under

Thermal Analysis for Ion-Exchange Column System

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lee, Si Y.; King, William D.

2012-12-20

Models have been developed to simulate the thermal characteristics of crystalline silicotitanate ion exchange media fully loaded with radioactive cesium either in a column configuration or distributed within a waste storage tank. This work was conducted to support the design and operation of a waste treatment process focused on treating dissolved, high-sodium salt waste solutions for the removal of specific radionuclides. The ion exchange column will be installed inside a high level waste storage tank at the Savannah River Site. After cesium loading, the ion exchange media may be transferred to the waste tank floor for interim storage. Models weremore » used to predict temperature profiles in these areas of the system where the cesium-loaded media is expected to lead to localized regions of elevated temperature due to radiolytic decay. Normal operating conditions and accident scenarios (including loss of solution flow, inadvertent drainage, and loss of active cooling) were evaluated for the ion exchange column using bounding conditions to establish the design safety basis. The modeling results demonstrate that the baseline design using one central and four outer cooling tubes provides a highly efficient cooling mechanism for reducing the maximum column temperature. In-tank modeling results revealed that an idealized hemispherical mound shape leads to the highest tank floor temperatures. In contrast, even large volumes of CST distributed in a flat layer with a cylindrical shape do not result in significant floor heating.« less

In- Situ Synchrotron Diffraction Studies on Transformation Strain Development in a High-Strength Quenched and Tempered Structural Steel—Part II. Martensitic Transformation

NASA Astrophysics Data System (ADS)

Dutta, R. K.; Huizenga, R. M.; Petrov, R. H.; Amirthalingam, M.; King, A.; Gao, H.; Hermans, M. J. M.; Richardson, I. M.

2014-01-01

In-situ synchrotron diffraction studies on the kinetics of phase transformation and transformation strain development during bainitic transformation were presented in part I of the current article. In the current article, in-situ phase transformation behavior of a high-strength (830 MPa yield stress) quenched and tempered S690QL1 [Fe-0.16C-0.2Si-0.87Mn-0.33Cr-0.21Mo (wt. pct)] structural steel, during continuous cooling and under different mechanical loading conditions to promote martensitic transformation, has been studied. Time-temperature-load resolved 2D synchrotron diffraction patterns were recorded and used to calculate the phase fractions and lattice parameters of the phases during heating and cooling cycles under different loading conditions. In addition to the thermal expansion behavior, the effects of the applied stress on the elastic strains during the martensitic transformation were calculated. The results show that small tensile stresses applied at the transformation temperature do not change the kinetics of the phase transformation. The start temperature for the martensitic transformation increases with the increasing applied tensile stress. The elastic strains are not affected significantly with the increasing tensile stress. The variant selection during martensitic transformation under small applied loads (in the elastic region) is weak.

Gas gun driven dynamic fracture and fragmentation of Ti-6Al-4V cylinders

NASA Astrophysics Data System (ADS)

Jones, D. R.; Chapman, D. J.; Eakins, D. E.

2014-05-01

The dynamic fracture and fragmentation of a material is a complex late stage phenomenon occurring in many shock loading scenarios. Improving our predictive capability depends upon exercising our current failure models against new loading schemes and data. We present axially-symmetric high strain rate (104 s-1) expansion of Ti-6Al-4V cylinders using a single stage light gas gun technique. A steel ogive insert was located inside the target cylinder, into which a polycarbonate rod was launched. Deformation of this rod around the insert drives the cylinder into rapid expansion. This technique we have developed facilitates repeatable loading, independent of the temperature of the sample cylinder, with straightforward adjustment of the radial strain rate. Expansion velocity was measured with multiple channels of photon Doppler velocimetry. High speed imaging was used to track the overall expansion process and record strain to failure and crack growth. Results from a cylinder at a temperature of 150 K are compared with work at room temperature, examining the deformation, failure mechanisms and differences in fragmentation.

Floral preferences and climate influence in nectar and pollen foraging by Melipona rufiventris Lepeletier (Hymenoptera: Meliponini) in Ubatuba, São Paulo state, Brazil.

PubMed

Fidalgo, Adriana de O; Kleinert, Astrid de M P

2010-01-01

We describe the environment effects on the amount and quality of resources collected by Melipona rufiventris Lepeletier in the Atlantic Forest at Ubatuba city, São Paulo state, Brazil (44º48'W, 23º22'S). Bees carrying pollen and/or nectar were captured at nest entrances during 5 min every hour, from sunrise to sunset, once a month. Pollen loads were counted and saved for acetolysis. Nectar was collected, the volume was determined and the total dissolved solids were determined by refractometer. Air temperature, relative humidity and light intensity were also registered. The number of pollen loads reached its maximum value between 70% and 90% of relative humidity and 18ºC and 23ºC; for nectar loads this range was broader, 50-90% and 20-30ºC. The number of pollen loads increased as relative humidity rose (rs = 0.401; P < 0.01) and high temperatures had a strong negative influence on the number of pollen loads collected (rs = -0.228; P < 0.01). The number of nectar loads positively correlated with temperature (rs = 0.244; P < 0.01) and light intensity (rs = 0.414; P < 0.01). The percentage of total dissolved solids (TDS) on nectar loads positively correlated with temperature and light intensity (rs = 0.361; P < 0.01 and rs = 0.245; P < 0.01), negatively correlated with relative humidity (rs = -0.629; P < 0.01), and it increased along the day. Most nectar loads had TDS between 11% and 30%, with an average of 24.7%. The volume measures did not show any pattern. Important pollen sources were Sapindaceae, Anacardiaceae, Rubiaceae, Arecaceae, Solanaceae and Myrtaceae; nectar sources were Sapindaceae, Fabaceae, Rubiaceae, Arecaceae and Solanaceae.

YJ101-YF-17 Aircraft Prototype Development Summary

DTIC Science & Technology

1977-01-01

requirements were selected to evaluate engi of the considerations was the impact of idl operation, while other arenas as altitude f loads , EMI, and JP...designed to be compatible with the air combat fighter installation environment temperatures and "g" loads . 2.2.1 Evaluation Testing Program. An...ratio per stage. It has a cylindrical hub and tapered tip flowpath to provide high loading within reasonable rim speeds. Development

Use of Pd-Pt loaded graphene aerogel on nickel foam in direct ethanol fuel cell

NASA Astrophysics Data System (ADS)

Tsang, Chi Him A.; Leung, D. Y. C.

2018-01-01

A size customized binder-free bimetallic Pd-Pt loaded graphene aerogel deposited on nickel foam plate (Pd-Pt/GA/NFP) was prepared and used as an electrode for an alkaline direct ethanol fuel cell (DEFC) under room temperature. The effect of fuel concentration and metal composition on the output power density of the DEFC was systematically investigated. Under the optimum fuel concentration, the cell could achieve a value of 3.6 mW cm-2 at room temperature for the graphene electrode with Pd/Pt ratio approaching 1:1. Such results demonstrated the possibility of producing a size customized metal loaded GA/NFP electrode for fuel cell with high performance.

Modeling and Measurement of Sustained Loading and Temperature-Dependent Deformation of Carbon Fiber-Reinforced Polymer Bonded to Concrete.

PubMed

Jeong, Yoseok; Lee, Jaeha; Kim, WooSeok

2015-01-29

This paper aims at presenting the effects of short-term sustained load and temperature on time-dependent deformation of carbon fiber-reinforced polymer (CFRP) bonded to concrete and pull-off strength at room temperature after the sustained loading period. The approach involves experimental and numerical analysis. Single-lap shear specimens were used to evaluate temperature and short-term sustained loading effects on time-dependent behavior under sustained loading and debonding behavior under pull-off loading after a sustained loading period. The numerical model was parameterized with experiments on the concrete, FRP, and epoxy. Good correlation was seen between the numerical results and single-lap shear experiments. Sensitivity studies shed light on the influence of temperature, epoxy modulus, and epoxy thickness on the redistribution of interfacial shear stress during sustained loading. This investigation confirms the hypothesis that interfacial stress redistribution can occur due to sustained load and elevated temperature and its effect can be significant.

Modeling and Measurement of Sustained Loading and Temperature-Dependent Deformation of Carbon Fiber-Reinforced Polymer Bonded to Concrete

PubMed Central

Jeong, Yoseok; Lee, Jaeha; Kim, WooSeok

2015-01-01

This paper aims at presenting the effects of short-term sustained load and temperature on time-dependent deformation of carbon fiber-reinforced polymer (CFRP) bonded to concrete and pull-off strength at room temperature after the sustained loading period. The approach involves experimental and numerical analysis. Single-lap shear specimens were used to evaluate temperature and short-term sustained loading effects on time-dependent behavior under sustained loading and debonding behavior under pull-off loading after a sustained loading period. The numerical model was parameterized with experiments on the concrete, FRP, and epoxy. Good correlation was seen between the numerical results and single-lap shear experiments. Sensitivity studies shed light on the influence of temperature, epoxy modulus, and epoxy thickness on the redistribution of interfacial shear stress during sustained loading. This investigation confirms the hypothesis that interfacial stress redistribution can occur due to sustained load and elevated temperature and its effect can be significant. PMID:28787948

Effects of Palladium Content, Quaternary Alloying, and Thermomechanical Processing on the Behavior of Ni-Ti-Pd Shape Memory Alloys for Actuator Applications

NASA Technical Reports Server (NTRS)

Bigelow, Glen

2008-01-01

The need for compact, solid-state actuation systems for use in the aerospace, automotive, and other transportation industries is currently driving research in high-temperature shape memory alloys (HTSMA) having transformation temperatures above 100 C. One of the basic high temperature systems under investigation to fill this need is NiTiPd. Prior work on this alloy system has focused on phase transformations and respective temperatures, no-load shape memory behavior (strain recovery), and tensile behavior for selected alloys. In addition, a few tests have been done to determine the effect of boron additions and thermomechanical treatment on the aforementioned properties. The main properties that affect the performance of a solid state actuator, namely work output, transformation strain, and permanent deformation during thermal cycling under load have mainly been neglected. There is also no consistent data representing the mechanical behavior of this alloy system over a broad range of compositions. For this thesis, ternary NiTiPd alloys containing 15 to 46 at.% palladium were processed and the transformation temperatures, basic tensile properties, and work characteristics determined. However, testing reveals that at higher levels of alloying addition, the benefit of increased transformation temperature begins to be offset by lowered work output and permanent deformation or "walking" of the alloy during thermal cycling under load. In response to this dilemma, NiTiPd alloys have been further alloyed with gold, platinum, and hafnium additions to solid solution strengthen the martensite and parent austenite phases in order to improve the thermomechanical behavior of these materials. The tensile properties, work behavior, and dimensional stability during repeated thermal cycling under load for the ternary and quaternary alloys were compared and discussed. In addition, the benefits of more advanced thermomechanical processing or training on the dimensional stability of these alloys during repeated actuation were investigated. Finally, the effect of quaternary alloying on the thermal stability of NiTiPdX alloys is determined via thermal cycling of the materials to increasing temperatures under load. It was found that solid solution additions of platinum and gold resulted in about a 30 C increase in upper use temperature compared to the baseline NiTiPd alloy, providing an added measure of over-temperature protection.

Effect of drying temperature on warp and downgrade of 2 by 4's from small-diameter ponderosa pine

Treesearch

William T. Simpson

2004-01-01

Kiln drying at high temperature may reduce warp in dimension lumber sawn from small-diameter trees. In this study, we examined the effect on warp of high drying temperatures in conjunction with top loading immediately after drying and after storage in typical conditions that result in further moisture loss. Eight-foot-long 2- by 4-in. (2 by 4) boards sawn from open-...

On the Use of Accelerated Aging Methods for Screening High Temperature Polymeric Composite Materials

NASA Technical Reports Server (NTRS)

Gates, Thomas S.; Grayson, Michael A.

1999-01-01

A rational approach to the problem of accelerated testing of high temperature polymeric composites is discussed. The methods provided are considered tools useful in the screening of new materials systems for long-term application to extreme environments that include elevated temperature, moisture, oxygen, and mechanical load. The need for reproducible mechanisms, indicator properties, and real-time data are outlined as well as the methodologies for specific aging mechanisms.

Temperature Dependent Mechanical Property of PZT Film: An Investigation by Nanoindentation

PubMed Central

Li, Yingwei; Feng, Shangming; Wu, Wenping; Li, Faxin

2015-01-01

Load-depth curves of an unpoled Lead Zirconate Titanate (PZT) film composite as a function of temperature were measured by nanoindentation technique. Its reduce modulus and hardness were calculated by the typical Oliver-Pharr method. Then the true modulus and hardness of the PZT film were assessed by decoupling the influence of substrate using methods proposed by Zhou et al. and Korsunsky et al., respectively. Results show that the indentation depth and modulus increase, but the hardness decreases at elevated temperature. The increasing of indentation depth and the decreasing of hardness are thought to be caused by the decreasing of the critical stress needed to excite dislocation initiation at high temperature. The increasing of true modulus is attributed to the reducing of recoverable indentation depth induced by back-switched domains. The influence of residual stress on the indentation behavior of PZT film composite was also investigated by measuring its load-depth curves with pre-load strains. PMID:25768957

Effects of melamine formaldehyde resin and CaCO3 diffuser-loaded encapsulation on correlated color temperature uniformity of phosphor-converted LEDs.

PubMed

Yang, Liang; Lv, Zhicheng; Jiaojiao, Yuan; Liu, Sheng

2013-08-01

Phosphor-free dispensing is the most widely used LED packaging method, but this method results in poor quality in angular CCT uniformity. This study proposes a diffuser-loaded encapsulation to solve the problem; the effects of melamine formaldehyde (MF) resin and CaCO3 loaded encapsulation on correlated color temperature (CCT) uniformity and luminous efficiency reduction of the phosphor-converted LEDs are investigated. Results reveal that MF resin loaded encapsulation has better light diffusion performance compared to MF resin loaded encapsulation at the same diffuser concentration, but CaCO3 loaded encapsulation has better luminous efficiency maintenance. The improvements in angular color uniformity for the LEDs emitting with MF resin and CaCO3 loaded encapsulation can be explained by the increase in photon scattering. The utility of this low cost and controllable mineral diffuser packaging method provides a practical approach for enhancing the angular color uniformity of LEDs. The diffuser mass ratio of 1% MF resin or 10% CaCO3 is the optimum condition to obtain low angular CCT variance and high luminous efficiency.

Relationship between current load and temperature for quasi-steady state and transient conditions

NASA Astrophysics Data System (ADS)

Lyon, Bernard R., Jr.; Orlove, Gary L.; Peters, Donna L.

2000-03-01

Infrared thermographers involved in predictive maintenance programs often use temperature measurement as a means of quantifying the severity of a problem. Temperature is certainly an important factor in evaluating equipment. However, if you follow guidelines that are based solely on absolute temperature measurement--or on a temperature rise (Delta T)--you run the risk of incorrectly diagnosing your problems. The consequences of such actions can lead to a false sense of security, equipment failure, fire, and even the possibility of personal injury. Understanding the additional factors involved in diagnosis is essential for obtaining productive results. One of these factors is the load or current flowing through conductors. The load can have a drastic effect on the temperature of a component. Changing loads can cause additional concerns because temperature changes lag behind load changes. The purpose of this paper is to illustrate the relationship between load and temperature of a faulty connection. The thermal response of a changing load is also investigated.

High heat flux properties of pure tungsten and plasma sprayed tungsten coatings

NASA Astrophysics Data System (ADS)

Liu, X.; Tamura, S.; Tokunaga, K.; Yoshida, N.; Noda, N.; Yang, L.; Xu, Z.

2004-08-01

High heat flux properties of pure tungsten and plasma sprayed tungsten coatings on carbon substrates have been studied by annealing and cyclic heat loading. The recrystallization temperature and an activation energy QR=126 kJ/mol for grain growth of tungsten coating by vacuum plasma spray (VPS) were estimated, and the microstructural changes of multi-layer tungsten and rhenium interface pre-deposited by physical vapor deposition (PVD) with anneal temperature were investigated. Cyclic load tests indicated that pure tungsten and VPS-tungsten coating could withstand 1000 cycles at 33-35 MW/m 2 heat flux and 3 s pulse duration, and inert gas plasma spray (IPS)-tungsten coating showed local cracks by 300 cycles but did not induce failure by further cycles. However, the failure of pure tungsten and VPS-tungsten coating by fatigue cracking was observed under higher heat load (55-60 MW/m 2) for 420 and 230 cycles, respectively.

Startup analysis for a high temperature gas loaded heat pipe

NASA Technical Reports Server (NTRS)

Sockol, P. M.

1973-01-01

A model for the rapid startup of a high-temperature gas-loaded heat pipe is presented. A two-dimensional diffusion analysis is used to determine the rate of energy transport by the vapor between the hot and cold zones of the pipe. The vapor transport rate is then incorporated in a simple thermal model of the startup of a radiation-cooled heat pipe. Numerical results for an argon-lithium system show that radial diffusion to the cold wall can produce large vapor flow rates during a rapid startup. The results also show that startup is not initiated until the vapor pressure p sub v in the hot zone reaches a precise value proportional to the initial gas pressure p sub i. Through proper choice of p sub i, startup can be delayed until p sub v is large enough to support a heat-transfer rate sufficient to overcome a thermal load on the heat pipe.

Life prediction of materials exposed to monotonic and cyclic loading: Bibliography

NASA Technical Reports Server (NTRS)

Carpenter, J. L., Jr.; Moya, N.; Stuhrke, W. F.

1975-01-01

This bibliography is comprised of approximately 1200 reference citations related to the mechanics of failure in aerospace structures. Most of the references are for information on life prediction for materials exposed to monotonic and cyclic loading in elevated temperature environments such as that in the hot end of a gas turbine engine. Additional citations listed are for documents on the thermal and mechanical effects on solar cells in the cryogenic vacuum environment; radiation effects on high temperature mechanical properties; and high cycle fatigue technology as applicable to gas turbine engine bearings. The bibliography represents a search of the literature published in the period April 1962 through April 1974 and is largely limited to documents published in the United States. It is a companion volume to NASA CR-134750, Life Prediction of Materials Exposed to Monotonic and cyclic Loading - A Technology Survey.

The Liquid Nitrogen System for Chamber A: A Change from Original Forced Flow Design to a Natural Flow (Thermo Siphon) System

NASA Technical Reports Server (NTRS)

Homan, Jonathan; Montz, Michael; Sidi-Yekhlef, Ahmed; Ganni, Venkatarao (Rao); Knudsen, Peter; Garcia, Sam; Linza, Robert; Meagher, Daniel; Lauterbauch, John

2008-01-01

NASA Johnson Space Center (JSC) in Houston is currently supplementing its 20K helium refrigeration system to meet the new requirements for testing the James Web Space Telescope in the environmental control Chamber-A (65 dia x 120 high) in Building 32. The new system is required to meet the various operating modes which include a high 20K heat load, a required temperature stability at the load, rapid (but controlled) cool down and warm up and bake out of the chamber. This paper will present the proposed modifications to the existing helium system(s) to incorporate the new requirements and the integration of the new helium refrigerator with the existing two 3.5KW 20K helium refrigerators. In addition, the floating pressure process control philosophy to achieve high efficiency over the operating range (40% to 100% of the refrigeration system capacity), and the required temperature stability of +/- 0.25 K at the load will be discussed. The refrigeration systems ability to naturally seek the operating conditions under various loads and thus minimizing operator involvement and the over all improvements to the system operability and the reliability will be explained.

Creep Strain and Strain Rate Response of 2219 Al Alloy at High Stress Levels

NASA Technical Reports Server (NTRS)

Taminger, Karen M. B.; Wagner, John A.; Lisagor, W. Barry

1998-01-01

As a result of high localized plastic deformation experienced during proof testing in an International Space Station connecting module, a study was undertaken to determine the deformation response of a 2219-T851 roll forging. After prestraining 2219-T851 Al specimens to simulate strains observed during the proof testing, creep tests were conducted in the temperature range from ambient temperature to 107 C (225 F) at stress levels approaching the ultimate tensile strength of 2219-T851 Al. Strain-time histories and strain rate responses were examined. The strain rate response was extremely high initially, but decayed rapidly, spanning as much as five orders of magnitude during primary creep. Select specimens were subjected to incremental step loading and exhibited initial creep rates of similar magnitude for each load step. Although the creep rates decreased quickly at all loads, the creep rates dropped faster and reached lower strain rate levels for lower applied loads. The initial creep rate and creep rate decay associated with primary creep were similar for specimens with and without prestrain; however, prestraining (strain hardening) the specimens, as in the aforementioned proof test, resulted in significantly longer creep life.

Elevated temperature biaxial fatigue

NASA Technical Reports Server (NTRS)

Jordan, E. H.

1985-01-01

A 3 year experimental program for studying elevated temperature biaxial fatigue of a nickel based alloy Hastelloy-X has been completed. A new high temperature fatigue test facility with unique capabilities has been developed. Effort was directed toward understanding multiaxial fatigue and correlating the experimental data to the existing theories of fatigue failure. The difficult task of predicting fatigue lives for nonproportional loading was used as an ultimate test for various life prediction methods being considered. The primary means of reaching improved understanding were through several critical nonproportional loading experiments. The direction of cracking observed on failed specimens was also recorded and used to guide the development of the theory. Cyclic deformation responses were permanently recorded digitally during each test. It was discovered that the cracking mode switched from primarily cracking on the maximum shear planes at room temperature to cracking on the maximum normal strain planes at 649 C. In contrast to some other metals, loading path in nonproportional loading had little effect on fatigue lives. Strain rate had a small effect on fatigue lives at 649 C. Of the various correlating parameters the modified plastic work and octahedral shear stress were the most successful.

Simulated building energy demand biases resulting from the use of representative weather stations

DOE PAGES

Burleyson, Casey D.; Voisin, Nathalie; Taylor, Z. Todd; ...

2017-11-06

Numerical building models are typically forced with weather data from a limited number of “representative cities” or weather stations representing different climate regions. The use of representative weather stations reduces computational costs, but often fails to capture spatial heterogeneity in weather that may be important for simulations aimed at understanding how building stocks respond to a changing climate. Here, we quantify the potential reduction in temperature and load biases from using an increasing number of weather stations over the western U.S. Our novel approach is based on deriving temperature and load time series using incrementally more weather stations, ranging frommore » 8 to roughly 150, to evaluate the ability to capture weather patterns across different seasons. Using 8 stations across the western U.S., one from each IECC climate zone, results in an average absolute summertime temperature bias of ~4.0 °C with respect to a high-resolution gridded dataset. The mean absolute bias drops to ~1.5 °C using all available weather stations. Temperature biases of this magnitude could translate to absolute summertime mean simulated load biases as high as 13.5%. Increasing the size of the domain over which biases are calculated reduces their magnitude as positive and negative biases may cancel out. Using 8 representative weather stations can lead to a 20–40% bias of peak building loads during both summer and winter, a significant error for capacity expansion planners who may use these types of simulations. Using weather stations close to population centers reduces both mean and peak load biases. Our approach could be used by others designing aggregate building simulations to understand the sensitivity to their choice of weather stations used to drive the models.« less

Simulated building energy demand biases resulting from the use of representative weather stations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Burleyson, Casey D.; Voisin, Nathalie; Taylor, Z. Todd

Numerical building models are typically forced with weather data from a limited number of “representative cities” or weather stations representing different climate regions. The use of representative weather stations reduces computational costs, but often fails to capture spatial heterogeneity in weather that may be important for simulations aimed at understanding how building stocks respond to a changing climate. Here, we quantify the potential reduction in temperature and load biases from using an increasing number of weather stations over the western U.S. Our novel approach is based on deriving temperature and load time series using incrementally more weather stations, ranging frommore » 8 to roughly 150, to evaluate the ability to capture weather patterns across different seasons. Using 8 stations across the western U.S., one from each IECC climate zone, results in an average absolute summertime temperature bias of ~4.0 °C with respect to a high-resolution gridded dataset. The mean absolute bias drops to ~1.5 °C using all available weather stations. Temperature biases of this magnitude could translate to absolute summertime mean simulated load biases as high as 13.5%. Increasing the size of the domain over which biases are calculated reduces their magnitude as positive and negative biases may cancel out. Using 8 representative weather stations can lead to a 20–40% bias of peak building loads during both summer and winter, a significant error for capacity expansion planners who may use these types of simulations. Using weather stations close to population centers reduces both mean and peak load biases. Our approach could be used by others designing aggregate building simulations to understand the sensitivity to their choice of weather stations used to drive the models.« less

Properties and Potential of Two (ni,pt)ti Alloys for Use as High-temperature Actuator Materials

NASA Technical Reports Server (NTRS)

Noebe, Ronald; Gaydosh, Darrell; Padula, Santo, II.; Garg, Anita; Biles, Tiffany; Nathal, Michael

2005-01-01

The microstructure, transformation temperatures, basic tensile properties, shape memory behavior, and work output for two (Ni,Ti)Pt high-temperature shape memory alloys have been characterized. One was a Ni30Pt20Ti50 alloy (referred to as 20Pt) with transformation temperatures above 230 C and the other was a Ni20Pt30Ti50 alloy (30Pt) with transformation temperatures about 530 C. Both materials displayed shape memory behavior and were capable of 100% (no-load) strain recovery for strain levels up to their fracture limit (3-4%) when deformed at room temperature. For the 20Pt alloy, the tensile strength, modulus, and ductility dramatically increased when the material was tested just about the austenite finish (A(sub f)) temperature. For the 30Pt alloy, a similar change in yield behavior at temperatures above the A(sub f) was not observed. In this case the strength of the austentite phase was at best comparable and generally much weaker than the martensite phase. A ductility minimum was also observed just below the A(sub s) temperature in this alloy. As a result of these differences in tensile behavior, the two alloys performed completely different when thermally cycled under constant load. The 20Pt alloy behaved similar to conventional binary NiTi alloys with work output due to the martensite-to-austenite transformation initially increasing with applied stress. The maximum work output measured in the 20Pt alloy was nearly 9 J/cu cm and was limited by the tensile ductility of the material. In contrast, the martensite-to-austenite transformation in the 30Pt alloy was not capable of performing work against any bias load. The reason for this behavior was traced back to its basic mechanical properties, where the yield strength of the austenite phase was similar to or lower than that of the martensite phase, depending on temperature. Hence, the recovery or transformation strain for the 30Pt alloy under load was essentially zero, resulting in zero work output.

Sol-gel preparation of Ag-silica nanocomposite with high electrical conductivity

NASA Astrophysics Data System (ADS)

Ma, Zhijun; Jiang, Yuwei; Xiao, Huisi; Jiang, Bofan; Zhang, Hao; Peng, Mingying; Dong, Guoping; Yu, Xiang; Yang, Jian

2018-04-01

Sol-gel derived noble-metal-silica nanocomposites are very useful in many applications. Due to relatively low price, higher conductivity, and higher chemical stability of silver (Ag) compared with copper (Cu), Ag-silica has gained much more research interest. However, it remains a significant challenge to realize high loading of Ag content in sol-gel Ag-silica composite with high structural controllability and nanoparticles' dispersity. Different from previous works by using multifunctional silicon alkoxide to anchor metal ions, here we report the synthesis of Ag-silica nanocomposite with high loading of Ag nanoparticles by employing acetonitrile bi-functionally as solvent and metal ions stabilizer. The electrical conductivity of the Ag-silica nanocomposite reached higher than 6800 S/cm. In addition, the Ag-silica nanocomposite could simultaneously possess high electrical conductivity and positive conductivity-temperature coefficient by properly controlling the loading content of Ag. Such behavior is potentially advantageous for high-temperature devices (like phosphoric acid fuel cells) and inhibiting the thermal-induced increase of devices' internal resistance. The strategy proposed here is also compatible with block-copolymer directed self-assembly of mesoporous material, spin-coating of film and electrospinning of nanofiber, making it more charming in various practical applications.

A temperature dependent cyclic plasticity model for hot work tool steel including particle coarsening

NASA Astrophysics Data System (ADS)

Jilg, Andreas; Seifert, Thomas

2018-05-01

Hot work tools are subjected to complex thermal and mechanical loads during hot forming processes. Locally, the stresses can exceed the material's yield strength in highly loaded areas as e.g. in small radii in die cavities. To sustain the high loads, the hot forming tools are typically made of martensitic hot work steels. While temperatures for annealing of the tool steels usually lie in the range between 400 and 600 °C, the steels may experience even higher temperatures during hot forming, resulting in softening of the material due to coarsening of strengthening particles. In this paper, a temperature dependent cyclic plasticity model for the martensitic hot work tool steel 1.2367 (X38CrMoV5-3) is presented that includes softening due to particle coarsening and that can be applied in finite-element calculations to assess the effect of softening on the thermomechanical fatigue life of hot work tools. To this end, a kinetic model for the evolution of the mean size of secondary carbides based on Ostwald ripening is coupled with a cyclic plasticity model with kinematic hardening. Mechanism-based relations are developed to describe the dependency of the mechanical properties on carbide size and temperature. The material properties of the mechanical and kinetic model are determined on the basis of tempering hardness curves as well as monotonic and cyclic tests.

A Si/Glass Bulk-Micromachined Cryogenic Heat Exchanger for High Heat Loads: Fabrication, Test, and Application Results.

PubMed

Zhu, Weibin; White, Michael J; Nellis, Gregory F; Klein, Sanford A; Gianchandani, Yogesh B

2010-02-01

This paper reports on a micromachined Si/glass stack recuperative heat exchanger with in situ temperature sensors. Numerous high-conductivity silicon plates with integrated platinum resistance temperature detectors (Pt RTDs) are stacked, alternating with low-conductivity Pyrex spacers. The device has a 1 x 1-cm(2) footprint and a length of up to 3.5 cm. It is intended for use in Joule-Thomson (J-T) coolers and can sustain pressure exceeding 1 MPa. Tests at cold-end inlet temperatures of 237 K-252 K show that the heat exchanger effectiveness is 0.9 with 0.039-g/s helium mass flow rate. The integrated Pt RTDs present a linear response of 0.26%-0.30%/K over an operational range of 205 K-296 K but remain usable at lower temperatures. In self-cooling tests with ethane as the working fluid, a J-T system with the heat exchanger drops 76.1 K below the inlet temperature, achieving 218.7 K for a pressure of 835.8 kPa. The system reaches 200 K in transient state; further cooling is limited by impurities that freeze within the flow stream. In J-T self-cooling tests with an external heat load, the system reaches 239 K while providing 1 W of cooling. In all cases, there is an additional parasitic heat load estimated at 300-500 mW.

Climatic variability and its role in regulating C, N and P retention in the James River Estuary

NASA Astrophysics Data System (ADS)

Bukaveckas, Paul A.; Beck, Michael; Devore, Dana; Lee, William M.

2018-05-01

Transformations and retention of C, N and P inputs to estuaries are subject to external factors such as discharge-driven variation in loading rates, and internal processes regulating biogeochemical cycles. We used an 8-year time series of finely resolved (monthly) mass balances for the tidal freshwater segment of the James River Estuary to assess the influence of discharge and temperature on C, N and P retention. Peak export and retention of organic, likely particulate, fractions occurred in months of highest discharge. With increasing discharge we observed higher mass retention, greater proportional retention (in relation to inputs) and more selective retention (with P retained preferentially over N and C). DIN retention was strongly influenced by water temperature with 10-fold high retention occurring at high (>20 °C) vs. low (<15 °C) water temperature at corresponding discharge. Our findings suggest that rising temperatures will have a greater effect on the retention of N than P because a greater proportion of the total N delivered to estuaries is in dissolved inorganic form, and therefore subject to temperature dependent rates of biological assimilation and denitrification. By contrast, the bulk of the P load was in particulate form, which is retained via sediment trapping, and not appreciably affected by water temperature. The tidal freshwater estuary was an important site for nutrient removal where the accumulation of N- and P- rich materials may delay recovery in response to nutrient load reductions.

Evaluation of two polyimides and of an improved liner retention design for self-lubricating bushings

NASA Technical Reports Server (NTRS)

Sliney, H. E.

1984-01-01

Two different polyimide polymers were studied and the effectiveness of a design feature to improve retention of the self lubricating composite liners under high load was evaluated. The basic bearing design consisted of a molded layer of chopped graphite-fiber-reinforced-polyimide (GFRP) composite bonded to the bore of a steel bushing. The friction, wear, and load carrying ability of the bushings were determined in oscillating tests at 25, 260 and 315 C at radial unit loads up to 260 MPa. Friction coefficients were typically 0.15 to 0.25. Bushings with liners containing a new partially fluorinated polymer were functional, but had a lower load capacity and higher wear rate than those containing a more conventional, high temperature polyimide. The liner retention design feature reduced the tendency of the liners to crack and work out of the contact zone under high oscillating loads.

Validation of the solar heating and cooling high speed performance (HISPER) computer code

NASA Technical Reports Server (NTRS)

Wallace, D. B.

1980-01-01

Developed to give a quick and accurate predictions HISPER, a simplification of the TRNSYS program, achieves its computational speed by not simulating detailed system operations or performing detailed load computations. In order to validate the HISPER computer for air systems the simulation was compared to the actual performance of an operational test site. Solar insolation, ambient temperature, water usage rate, and water main temperatures from the data tapes for an office building in Huntsville, Alabama were used as input. The HISPER program was found to predict the heating loads and solar fraction of the loads with errors of less than ten percent. Good correlation was found on both a seasonal basis and a monthly basis. Several parameters (such as infiltration rate and the outside ambient temperature above which heating is not required) were found to require careful selection for accurate simulation.

Thermal-gradient migration of brine inclusions in salt crystals. [Synthetic single crystals of NaCl and KCl

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yagnik, S.K.

1982-09-01

It has been proposed that high-level nuclear waste be disposed in a geologic repository. Natural-salt deposits, which are being considered for this purpose, contain a small volume fraction of water in the form of brine inclusions distributed throughout the salt. Radioactive-decay heating of the nuclear wastes will impose a temperature gradient on the surrounding salt which mobilizes the brine inclusions. Inclusions filled completely with brine migrate up the temperature gradient and eventually accumulate brine near the buried waste forms. The brine may slowly corrode or degrade the waste forms which is undesirable. In this work, thermal gradient migration of bothmore » all-liquid and gas-liquid inclusions was experimentally studied in synthetic single crystals of NaCl and KCl using a hot-stage attachment to an optical microscope which was capable of imposing temperature gradients and axial compressive loads on the crystals. The migration velocities of the inclusions were found to be dependent on temperature, temperature gradient, and inclusion shape and size. The velocities were also dictated by the interfacial mass transfer resistance at brine/solid interface. This interfacial resistance depends on the dislocation density in the crystal, which in turn, depends on the axial compressive loading of the crystal. At low axial loads, the dependence between the velocity and temperature gradient is non-linear.At high axial loads, however, the interfacial resistance is reduced and the migration velocity depends linearly on the temperature gradient. All-liquid inclusions filled with mixed brines were also studied. For gas-liquid inclusions, three different gas phases (helium, air and argon) were compared. Migration studies were also conducted on single crystallites of natural salt as well as in polycrystalline natural salt samples. The behavior of the inclusions at large angle grain boundaries was observed. 35 figures, 3 tables.« less

On the Henry constant and isosteric heat at zero loading in gas phase adsorption.

PubMed

Do, D D; Nicholson, D; Do, H D

2008-08-01

The Henry constant and the isosteric heat of adsorption at zero loading are commonly used as indicators of the strength of the affinity of an adsorbate for a solid adsorbent. It is assumed that (i) they are observable in practice, (ii) the Van Hoff's plot of the logarithm of the Henry constant versus the inverse of temperature is always linear and the slope is equal to the heat of adsorption, and (iii) the isosteric heat of adsorption at zero loading is either constant or weakly dependent on temperature. We show in this paper that none of these three points is necessarily correct, first because these variables might not be observable since they are outside the range of measurability; second that the linearity of the Van Hoff plot breaks down at very high temperature, and third that the isosteric heat versus loading is a strong function of temperature. We demonstrate these points using Monte Carlo integration and Monte Carlo simulation of adsorption of various gases on a graphite surface. Another issue concerning the Henry constant is related to the way the adsorption excess is defined. The most commonly used equation is the one that assumes that the void volume is the volume extended all the way to a boundary passing through the centres of the outermost solid atoms. With this definition the Henry constant can become negative at high temperatures. Although adsorption at these temperatures may not be practical because of the very low value of the Henry constant, it is more useful to define the Henry constant in such a way that it is always positive at all temperatures. Here we propose the use of the accessible volume; the volume probed by the adsorbate when it is in nonpositive regions of the potential, to calculate the Henry constant.

Experimental evaluation of cooling efficiency of the high performance cooling device

NASA Astrophysics Data System (ADS)

Nemec, Patrik; Malcho, Milan

2016-06-01

This work deal with experimental evaluation of cooling efficiency of cooling device capable transfer high heat fluxes from electric elements to the surrounding. The work contain description of cooling device, working principle of cooling device, construction of cooling device. Experimental part describe the measuring method of device cooling efficiency evaluation. The work results are presented in graphic visualization of temperature dependence of the contact area surface between cooling device evaporator and electronic components on the loaded heat of electronic components in range from 250 to 740 W and temperature dependence of the loop thermosiphon condenser surface on the loaded heat of electronic components in range from 250 to 740 W.

Environmental Effects on Long Term Displacement Data of Woven Fabric Webbings Under Constant Load for Inflatable Structures

NASA Technical Reports Server (NTRS)

Kenner, WInfred S.; Jones, Thomas C.; Doggett, William R.; Duncan, Quinton; Plant, James

2015-01-01

An experimental study of the effects of environmental temperature and humidity conditions on long-term creep displacement data of high strength Kevlar and VectranTM woven fabric webbings under constant load for inflatable structures is presented. The restraint layer of an inflatable structure for long-duration space exploration missions is designed to bear load and consists of an assembly of high strength webbings. Long-term creep displacement data of webbings can be utilized by designers to validate service life parameters of restraint layers of inflatable structures. Five groups of high-strength webbings were researched over a two year period. Each group had a unique webbing length, load rating, applied load, and test period. The five groups consisted of 1.) 6K Vectran webbings loaded to 49% ultimate tensile strength (UTS), 2.) 6K Vectran webbings loaded to 55% UTS, 3.) 12.5K Vectran webbings loaded to 22% UTS, 4.) 6K Kevlar webbings loaded to 40% and 43% UTS, and 5.) 6K Kevlar webbings loaded to 48% UTS. Results show that all webbing groups exhibit the initial two stages of three of a typical creep curve of an elastic material. Results also show that webbings exhibit unique local wave patterns over the duration of the test period. Data indicate that the local pattern is primarily generated by daily variations in relative humidity values within the test facility. Data indicate that after a three to six month period, where webbings reach a steady-state creep condition, an annual sinusoidal displacement pattern is exhibited, primarily due to variations in annual mean temperature values. Data indicates that variations in daily temperature values and annual mean humidity values have limited secondary effects on creep displacement behavior. Results show that webbings in groups 2 and 5 do not exhibit well defined annual displacement patterns because the magnitude of the applied loads cause large deformations, and data indicate that material yielding within a webbing tends to neutralize the annual sinusoidal displacement pattern. Study indicates that applied load, environmental effects, mechanical strength, coefficient of thermal expansion, and hygroscopic properties of webbings are fundamental requirements for quantifying accurate creep displacements and behaviors over multiple year time periods. Results from a study of the environmental effects on long-term creep displacement data of Kevlar and Vectran woven webbings are presented to increase the knowledge base of webbing materials and to enhance designs of inflatable space structures for long-duration space missions.

Recent Loads Calibration Experience With a Delta Wing Airplane

NASA Technical Reports Server (NTRS)

Jenkins, Jerald M.; Kuhl, Albert E.

1977-01-01

Aircraft which are designed for supersonic and hypersonic flight are evolving with delta wing configurations. An integral part of the evolution of all new aircraft is the flight test phase. Included in the flight test phase is an effort to identify and evaluate the loads environment of the aircraft. The most effective way of examining the loads environment is to utilize calibrated strain gages to provide load magnitudes. Using strain gage data to accomplish this has turned out to be anything but a straightforward task. The delta wing configuration has turned out to be a very difficult type of wing structure to calibrate. Elevated structural temperatures result in thermal effects which contaminate strain gage data being used to deduce flight loads. The concept of thermally calibrating a strain gage system is an approach to solving this problem. This paper will address how these problems were approached on a program directed toward measuring loads on the wing of a large, flexible supersonic aircraft. Structural configurations typical of high-speed delta wing aircraft will be examined. The temperature environment will be examined to see how it induces thermal stresses which subsequently cause errors in loads equations used to deduce the flight loads.

Thermoresponsive core-shell magnetic nanoparticles for combined modalities of cancer therapy.

PubMed

Purushotham, S; Chang, P E J; Rumpel, H; Kee, I H C; Ng, R T H; Chow, P K H; Tan, C K; Ramanujan, R V

2009-07-29

Thermoresponsive polymer-coated magnetic nanoparticles loaded with anti-cancer drugs are of considerable interest for novel multi-modal cancer therapies. Such nanoparticles can be used for magnetic drug targeting followed by simultaneous hyperthermia and drug release. Gamma-Fe(2)O(3) iron oxide magnetic nanoparticles (MNP) with average sizes of 14, 19 and 43 nm were synthesized by high temperature decomposition. Composite magnetic nanoparticles (CNP) of 43 nm MNP coated with the thermoresponsive polymer poly-n-isopropylacrylamide (PNIPAM) were prepared by dispersion polymerization of n-isopropylacrylamide monomer in the presence of the MNP. In vitro drug release of doxorubicin-(dox) loaded dehydrated CNP at temperatures below and above the lower critical solution temperature of PNIPAM (34 degrees C) revealed a weak dependence of drug release on swelling behavior. The particles displayed Fickian diffusion release kinetics; the maximum dox release at 42 degrees C after 101 h was 41%. In vitro simultaneous hyperthermia and drug release of therapeutically relevant quantities of dox was achieved, 14.7% of loaded dox was released in 47 min at hyperthermia temperatures. In vivo magnetic targeting of dox-loaded CNP to hepatocellular carcinoma (HCC) in a buffalo rat model was studied by magnetic resonance imaging (MRI) and histology. In summary, the good in vitro and in vivo performance of the doxorubicin-loaded thermoresponsive polymer-coated magnetic nanoparticles suggests considerable promise for applications in multi-modal treatment of cancer.

Specimen loading list for the varying temperature experiment

DOE Office of Scientific and Technical Information (OSTI.GOV)

Qualls, A.L.; Sitterson, R.G.

1998-09-01

The varying temperature experiment HFIR-RB-13J has been assembled and inserted in the reactor. Approximately 5300 specimens were cleaned, inspected, matched, and loaded into four specimen holders. A listing of each specimen loaded into the steady temperature holder, its position in the capsule, and the identification of the corresponding specimen loaded into the varying temperature holder is presented in this report.

Load Transmission Through Artificial Hip Joints due to Stress Wave Loading

NASA Astrophysics Data System (ADS)

Tanabe, Y.; Uchiyama, T.; Yamaoka, H.; Ohashi, H.

Since wear of the polyethylene (Ultra High Molecular Weight Polyethylene or UHMWPE) acetabular cup is considered to be the main cause of loosening of the artificial hip joint, the cross-linked UHMWPE with high durability to wear has been developed. This paper deals with impact load transmission through the complex of an artificial hip joint consisting of a UHMWPE acetabular cup (or liner), a metallic femoral head and stem. Impact compressive tests on the complex were performed using the split-Hopkinson pressure bar apparatus. To investigate the effects of material (conventional or cross-linked UHMWPE), size and setting angle of the liner, and test temperature on force transmission, the impact load transmission ratio (ILTR) was experimentally determined. The ILTR decreased with an increase of the setting angle independent of material and size of the liner, and test temperature. The ILTR values at 37°C were larger than those at 24 °C and 60°C. The ILTR also appeared to be affected by the type of material as well as size of the liner.

Optimum Platinum Loading In Pt/SnO2 CO-Oxidizing Catalysts

NASA Technical Reports Server (NTRS)

Schryer, David R.; Upchurch, Billy T.; Davis, Patricia P.; Brown, Kenneth G.; Schryer, Jacqueline

1991-01-01

Platinum on tin oxide (Pt/SnO2) good catalyst for oxidation of carbon monoxide at or near room temperature. Catalytic activity peaks at about 17 weight percent Pt. Catalysts with platinum loadings as high as 46 percent fabricated by technique developed at Langley Research Center. Work conducted to determine optimum platinum loading for this type of catalyst. Major application is removal of unwanted CO and O2 in CO2 lasers.

Boron carbide coating deposition on tungsten and testing of tungsten layers and coating under intense plasma load

DOE Office of Scientific and Technical Information (OSTI.GOV)

Airapetov, A. A.; Begrambekov, L. B., E-mail: lbb@plasma.mephi.ru; Buzhinskiy, O. I.

2015-12-15

A device intended for boron carbide coating deposition and material testing under high heat loads is presented. A boron carbide coating 5 μm thick was deposited on the tungsten substrate. These samples were subjected to thermocycling loads in the temperature range of 400–1500°C. Tungsten layers deposited on tungsten substrates were tested in similar conditions. Results of the surface analysis are presented.

Simulated Reentry Heating by Torching

NASA Technical Reports Server (NTRS)

Harvey, Gale A.

2008-01-01

The two first order reentry heating parameters are peak heating flux (W/cm2) and peak heat load (kJ/cm2). Peak heating flux (and deceleration, gs) is higher for a ballistic reentry and peak heat load is higher for a lifting reentry. Manned vehicle reentries are generally lifting reentries at nominal 1-5 gs so that personnel will not be crushed by high deceleration force. A few off-nominal manned reentries have experienced 8 or more gs with corresponding high heating flux (but below nominal heat load). The Shuttle Orbiter reentries provide about an order of magnitude difference in peak heating flux at mid-bottom (TPS tiles, approximately 6 W/cm2 or 5 BTU/ft2- sec) and leading edge (RCC, approximately 60 W/cm2 or 50 BTU/ft2- sec). Orion lunar return and Mars sample lander are of the same order of magnitude as orbiter leading edge peak heat loads. Flight temperature measurements are available for some orbiter TPS tile and RCC locations. Return-to-Flight on-orbit tile-repair-candidate-material-heating performance was evaluated by matching propane torch heating of candidate-materials temperatures at several depths to orbiter TPS tile flight-temperatures. Char and ash characteristics, heat expansion, and temperature histories at several depths of the cure-in-place ablator were some of the TPS repair material performance characteristics measured. The final char surface was above the initial surface for the primary candidate (silicone based) material, in contrast to a receded surface for the Apollo-type ablative heat shield material. Candidate TPS materials for Orion CEV (LEO and lunar return), and for Mars sample lander are now being evaluated. Torching of a candidate ablator material, PICA, was performed to match the ablation experienced by the STARDUST PICA heat shield. Torching showed that the carbon fiberform skeleton in a sample of PICA was inhomogeneous in that sample, and allowed measurements (of the clumps and voids) of the inhomogeneity. Additional reentry heating-performance characterizations of high temperature insulation materials were performed.

High and low torque handpieces: cutting dynamics, enamel cracking and tooth temperature.

PubMed

Watson, T F; Flanagan, D; Stone, D G

2000-06-24

The aim of these experiments was to compare the cutting dynamics of high-speed high-torque (speed-increasing) and high-speed low-torque (air-turbine) handpieces and evaluate the effect of handpiece torque and bur type on sub-surface enamel cracking. Temperature changes were also recorded in teeth during cavity preparation with high and low torque handpieces with diamond and tungsten carbide (TC) burs. The null hypothesis of this study was that high torque handpieces cause more damage to tooth structure during cutting and lead to a rise in temperature within the pulp-chamber. Images of the dynamic interactions between burs and enamel were recorded at video rate using a confocal microscope. Central incisors were mounted on a specially made servomotor driven stage for cutting with a type 57 TC bur. The two handpiece types were used with simultaneous recording of cutting load and rate. Sub-surface enamel cracking caused by the use of diamond and TC burs with high and low torque was also examined. Lower third molars were sectioned horizontally to remove the cusp tips and then the two remaining crowns cemented together with cyanoacrylate adhesive, by their flat surfaces. Axial surfaces of the crowns were then prepared with the burs and handpieces. The teeth were then separated and the original sectioned surface examined for any cracks using a confocal microscope. Heat generation was measured using thermocouples placed into the pulp chambers of extracted premolars, with diamond and TC burs/high-low torque handpiece variables, when cutting occlusal and cervical cavities. When lightly loaded the two handpiece types performed similarly. However, marked differences in cutting mechanisms were noted when increased forces were applied to the handpieces with, generally, an increase in cutting rate. The air turbine could not cope with steady heavy loads, tending to stall. 'Rippling' was seen in the interface as this stall developed, coinciding with the bur 'clearing' itself. No differences were noted between different handpieces and burs, in terms of sub-surface enamel cracking. Similarly, no differences were recorded for temperature rise during cavity preparation. Differences in cutting mechanisms were seen between handpieces with high and low torque, especially when the loads and cutting rates were increased. The speed increasing handpiece was better able to cope with increased loading. Nevertheless, there was no evidence of increased tooth cracking or heating with this type handpiece, indicating that these do not have any deleterious effects on the tooth.

Lubrication and Cooling Studies of Cylindrical-Roller Bearings at High Speeds

NASA Technical Reports Server (NTRS)

Macks, E Fred; Nemeth, Zolton N

1952-01-01

The results of an experimental investigation of the effect of oil inlet distribution and oil inlet temperature on the inner and outer-race temperatures of 75-millimeter-bore (size 215) cylindrical-roller inner-race-riding cage-type bearings are reported. A radial-load test rig was used over a range of dn values (product of the bearing bore in mm and the shaft speed in r.p.m) from 0.3 x 10(5) to 1.2 x 10(6) and static radial loads from 7 to 1113 pounds.

Slot Antenna Integrated Re-Entrant Resonator Based Wireless Pressure Sensor for High-Temperature Applications.

PubMed

Su, Shujing; Lu, Fei; Wu, Guozhu; Wu, Dezhi; Tan, Qiulin; Dong, Helei; Xiong, Jijun

2017-08-25

The highly sensitive pressure sensor presented in this paper aims at wireless passive sensing in a high temperature environment by using microwave backscattering technology. The structure of the re-entrant resonator was analyzed and optimized using theoretical calculation, software simulation, and its equivalent lump circuit model was first modified by us. Micro-machining and high-temperature co-fired ceramic (HTCC) process technologies were applied to fabricate the sensor, solving the common problem of cavity sealing during the air pressure loading test. In addition, to prevent the response signal from being immersed in the strong background clutter of the hermetic metal chamber, which makes its detection difficult, we proposed two key techniques to improve the signal to noise ratio: the suppression of strong background clutter and the detection of the weak backscattered signal of the sensor. The pressure sensor demonstrated in this paper works well for gas pressure loading between 40 and 120 kPa in a temperature range of 24 °C to 800 °C. The experimental results show that the sensor resonant frequency lies at 2.1065 GHz, with a maximum pressure sensitivity of 73.125 kHz/kPa.

Analysis of temperature changes on three-phase synchronous generator using infrared: comparison between balanced and unbalanced load

NASA Astrophysics Data System (ADS)

Amien, S.; Yoga, W.; Fahmi, F.

2018-02-01

Synchronous generators are a major tool in an electrical energy generating systems, the load supplied by the generator is unbalanced. This paper discusses the effect of synchronous generator temperature on the condition of balanced load and unbalanced load, which will then be compared with the measurement result of both states of the generator. Unbalanced loads can be caused by various asymmetric disturbances in the power system and the failure of load forecasting studies so that the load distribution in each phase is not the same and causing the excessive heat of the generator. The method used in data collection was by using an infrared thermometer and resistance calculation method. The temperature comparison result between the resistive, inductive and capacitive loads in the highest temperature balance occured when the generator is loaded with a resistive load, where T = 31.9 ° C and t = 65 minutes. While in a state of unbalanced load the highest temperature occured when the generator is loaded with a capacitive load, where T = 40.1 ° C and t = 60 minutes. By understanding this behavior, we can maintain the generator for longer operation life.

Mechanical Properties and Real-Time Damage Evaluations of Environmental Barrier Coated SiC/SiC CMCs Subjected to Tensile Loading Under Thermal Gradients

NASA Technical Reports Server (NTRS)

Appleby, Matthew; Zhu, Dongming; Morscher, Gregory

2015-01-01

SiC/SiC ceramic matrix composites (CMCs) require new state-of-the art environmental barrier coatings (EBCs) to withstand increased temperature requirements and high velocity combustion corrosive combustion gasses. The present work compares the response of coated and uncoated SiC/SiC CMC substrates subjected to simulated engine environments followed by high temperature mechanical testing to asses retained properties and damage mechanisms. Our focus is to explore the capabilities of electrical resistance (ER) measurements as an NDE technique for testing of retained properties under combined high heat-flux and mechanical loading conditions. Furthermore, Acoustic Emission (AE) measurements and Digital Image Correlation (DIC) were performed to determine material damage onset and accumulation.

Thermal analysis of the intact mandibular premolar: a finite element analysis.

PubMed

Oskui, I Z; Ashtiani, M N; Hashemi, A; Jafarzadeh, H

2013-09-01

To obtain temperature distribution data through human teeth focusing on the pulp-dentine junction (PDJ). A three-dimensional tooth model was reconstructed using computer-aided design software from computed tomographic images. Subsequently, temperature distribution was numerically determined through the tooth for three different heat loads. Loading type I was equivalent to a 60° C mouth temperature for 1 s. Loading type II started with a 60° C mouth temperature, decreasing linearly to 37° C over 10 s. Loading type III repeated the pattern of type II in three consecutive cycles, with a 5 s resting time between cycles. The maximum temperatures of the pulp were 37.9° C, 39.0° C and 41.2° C for loading types I, II, and III, respectively. The largest temperature rise occurred with the cyclic loading, that is, type III. For the heat loads considered, the predicted peak temperatures at the PDJ were less than the reported temperature thresholds of irreversible pulpal damage. © 2013 International Endodontic Journal. Published by John Wiley & Sons Ltd.

Anne K. Starace | NREL

Science.gov Websites

, Thermal Systems Group, 2010-2013 Featured Publications "Effects of Torrefaction Temperature on ;Biomass Catalytic Pyrolysis on Ni/ZSM-5: Effects of Nickel Pretreatment and Loading," Energy and inorganic dispersions be high-temperature heat-transfer and thermal energy storage fluids?" Journal of

Calculation methods for steadily loaded, off-set pivot, tilting pad thrust bearings. (Guide to use of computer program A9235.)

NASA Astrophysics Data System (ADS)

1992-12-01

ESDU 92035 provides details of a FORTRAN program that implements the calculation method of ESDU 83004. It allows performance analysis of an existing design, or the design of a bearing dimensions, subject to any space constraint, are recommended. The predicted performance includes the lubricant film thickness under load, its temperature and flow rate, the power loss, and the bearing temperature. Recommendations are also made on surface finish. Warning messages are output in the following cases, for each of which possible remedial actions are suggested: drain or pad temperature too high, churning losses too great, film thickness too small, pad number too high, ratio or inner to outer pad radius too large, flow rate too great, lubricant or pad temperature outside usable range. A lubricant database is provided that may be extended or edited. The program applies to Newtonian lubricants in laminar flow. Worked examples illustrate the use of the program.

Behaviors of Char Gasification Based on Two-stage Gasifier of Biomass

NASA Astrophysics Data System (ADS)

Taniguchi, Miki; Sasauchi, Kenichi; Ahn, Chulju; Ito, Yusuke; Hayashi, Toshiaki; Akamatsu, Fumiteru

In order to develop a small-scale gasifier in which biomass can be converted to energy with high efficiency, we planed a gasification process that consists of two parts: pyrolysis part (rotary kiln) and gasification part (downdraft gasifier). We performed fundamental experiments on gasification part and discussed the apropriate conditions such as air supply location, air ratio, air temperature and hearth load. The following results was found: 1) the air supply into the char bed is more effective than that into the gas phase, 2) we can have the maximum cold gas efficiency of 80% on the following conditions: air supply location: char layer, air temperature: 20°C, air ratio: 0.2. 3) As air temperature is higher, the cold gas efficiency is larger. As for the hearth load, the cold gas efficiency becomes higher and reaches the constant level. It is expected from the results that high temperature in the char layer is effective on the char gasification.

Studies on thermo-elastic heating of horns used in ultrasonic plastic welding.

PubMed

Roopa Rani, M; Prakasan, K; Rudramoorthy, R

2015-01-01

Ultrasonic welding horn is half wavelength section or tool used to focus the ultrasonic vibrations to the components being welded. The horn is designed in such a way that it maximizes the amplitude of the sound wave passing through it. The ends of the horn represent the displacement anti-nodes and the center the 'node' of the wave. As the horns perform 20,000 cycles of expansion and contraction per second, they are highly stressed at the nodes and are heated owing to thermo-elastic effects. Considerable temperature rise may be observed in the horn, at the nodal region when working at high amplitudes indicating high stress levels leading to failure of horns due to cyclic loading. The limits for amplitude must therefore be evaluated for the safe working of the horn. Horns made of different materials have different thermo-elastic behaviors and hence different temperatures at the nodes and antinodes. This temperature field can be used as a control mechanism for setting the amplitude/weld parameters. Safe stress levels can be predicted using modal and harmonic analyses followed by a stress analysis to study the effect of cyclic loads. These are achieved using 'Ansys'. The maximum amplitude level obtained from the stress analysis is used as input for 'Comsol' to predict the temperature field. The actual temperature developed in the horn during operation is measured using infrared camera and compared with the simulated temperature. From experiments, it is observed that horn made of titanium had the lowest temperature rise at the critical region and can be expected to operate at amplitudes up to 77 μm without suffering failure due to cyclic loading. The method of predicting thermo-elastic stresses and temperature may be adopted by the industry for operating the horn within the safe stress limits thereby extending the life of the horn. Copyright © 2014 Elsevier B.V. All rights reserved.

Preparation of carboplatin-Fe@C-loaded chitosan nanoparticles and study on hyperthermia combined with pharmacotherapy for liver cancer.

PubMed

Li, Fu-rong; Yan, Wen-hui; Guo, Yue-hua; Qi, Hui; Zhou, Han-xin

2009-08-01

Magnetic fluid hyperthermia is a kind of technology for treating tumors based on nanotechnology. It is suitable to various types of tumors. The purpose of this study was to prepare carboplatin-Fe@C-loaded chitosan nanoparticles with Fe@C as a magnetic core and to investigate efficacy of hyperthermia combined with chemotherapy for transplanted liver cancer in rats. Fe@C nanopowder was treated with dilute hydrochloric acid to prepare Fe@C nanocage. Carboplatin-Fe@C-loaded chitosan nanoparticles were prepared by reverse microemulsion method with the nanocages as the magnetic cores, chitosan as the matrix. The shape, size, drug-loading rate, and in vitro cumulative release of the nanoparticles were observed and heat product under high frequency alternating electromagnetic field in vitro was explored. Eighty rats with transplanted liver cancer were randomly divided into 4 groups (group A: control group, group B: free carboplatin group, group C: nanoparticles with static magnetic field group, and group D: nanoparticles with static field and alternating magnetic field). Drug was injected into the hepatic artery. The therapeutic effect of hyperthermia combined with chemotherapy for tumor, toxicity and rat survival time were observed. Carboplatin-Fe@C-loaded chitosan nanoparticles were spherical in shape with an average size of (207 +/- 21) nm and high saturation magnetization. The drug-loading rate of the nanoparticles was 11.0 +/- 1.1%. The cumulative release percentage of carboplatin-Fe@C-loaded chitosan nanoparticles in vitro at different point time phase of 24 h, 48 h, 72 h, 96 h and 120 h were 51%, 68%, 80%, 87% and 91%, respectively. With an increase in carboplatin-Fe@C-loaded chitosan nanoparticle concentration and magnetic field strength, the heating rate and constant temperature of carboplatin-Fe@C-loaded chitosan nanoparticles dispersed in physiological saline were increased in an alternating magnetic field. In vivo experiments showed that after particle injection, tumor temperature reached 42.6 degrees +/- 0.2 degrees C within 10 min in the alternating magnetic field; and the temperatures in the right hepatic lobes and the rectum were significantly lower than in the tumor and the constant temperature could last up to 30 min. The inhibition ratio of tumor weight in group D was significantly enhanced, no obviously toxic and side-effect occurred and survival time was prolonged. Carboplatin-Fe@C-loaded chitosan nanoparticles possess good magnetic targeting and heat production properties. They can target liver cancer tissue by static magnetic field, and with the application of alternating magnetic field, effectively raise tumor tissue temperature and facilitate tumor apoptosis. The combination of chemotherapy and magnetic materials into nanoparticles as described herein demonstrates promising efficacy.

Influence of Temperature on Fatigue-Induced Martensitic Phase Transformation in a Metastable CrMnNi-Steel

NASA Astrophysics Data System (ADS)

Biermann, Horst; Glage, Alexander; Droste, Matthias

2016-01-01

Metastable austenitic steels can exhibit a fatigue-induced martensitic phase transformation during cyclic loading. It is generally agreed that a certain strain amplitude and a threshold of the cumulated plastic strain must be exceeded to trigger martensitic phase transformation under cyclic loading. With respect to monotonic loading, the martensitic phase transformation takes place up to a critical temperature—the so-called M d temperature. The goal of the present investigation is to determine an M d,c temperature which would be the highest temperature at which a fatigue-induced martensitic phase transformation can take place. For this purpose, fatigue tests controlled by the total strain were performed at different temperatures. The material investigated was a high-alloy metastable austenitic steel X3CrMnNi16.7.7 (16.3Cr-7.2Mn-6.6Ni-0.03C-0.09N-1.0Si) produced using the hot pressing technique. The temperatures were set in the range of 283 K (10 °C) ≤ T ≤ 473 K (200 °C). Depending on the temperature and strain amplitude, the onset of the martensitic phase transformation shifted to different values of the cumulated plastic strain, or was inhibited completely. Moreover, it is known that metastable austenitic CrMnNi steels with higher nickel contents can exhibit the deformation-induced twinning effect. Thus, at higher temperatures and strain amplitudes, a transition from the deformation-induced martensitic transformation to deformation-induced twinning takes place. The fatigue-induced martensitic phase transformation was monitored during cyclic loading using a ferrite sensor. The microstructure after the fatigue tests was examined using the back-scattered electrons, the electron channeling contrast imaging and the electron backscatter diffraction techniques to study the temperature-dependent dislocation structures and phase transformations.

Porous Chromatographic Materials as Substrates for Preparing Synthetic Nuclear Explosion Debris Particles

DOE Office of Scientific and Technical Information (OSTI.GOV)

Harvey, Scott D.; Liezers, Martin; Antolick, Kathryn C.

2013-06-13

In this study, we investigated several porous chromatographic materials as synthetic substrates for preparing surrogate nuclear explosion debris particles. The resulting synthetic debris materials are of interest for use in developing analytical methods. Eighteen metals, including some of forensic interest, were loaded onto materials by immersing them in metal solutions (556 mg/L of each metal) to fill the pores, applying gentle heat (110°C) to drive off water, and then treating them at high temperatures (up to 800°C) in air to form less soluble metal species. High-boiling-point metals were uniformly loaded on spherical controlled-pore glass to emulate early fallout, whereas low-boiling-pointmore » metals were loaded on core-shell silica to represent coated particles formed later in the nuclear fallout-formation process. Analytical studies were applied to characterize solubility, material balance, and formation of recalcitrant species. Dissolution experiments indicated loading was 1.5 to 3 times higher than expected from the pore volume alone, a result attributed to surface coating. Analysis of load solutions before and after filling the material pores revealed that most metals were passively loaded; that is, solutions filled the pores without active metal discrimination. However, niobium and tin concentrations were lower in solutions after pore filling, and were found in elevated concentrations in the final products, indicating some metals were selectively loaded. High-temperature treatments caused reduced solubility of several metal species, and loss of some metals (rhenium and tellurium) because volatile species were formed. Sample preparation reproducibility was high (the inter-batch relative standard deviation was 7.8%, and the intra-batch relative standard deviation was 0.84%) indicating that this material is suitable for use as a working standard for analytical methods development. We anticipate future standardized radionuclide-loaded materials will find use in radioanalytical methods development and/or serve as a starting material for the synthesis of more complex forms of nuclear explosion debris (e.g., Trinitite).« less

Venus Surface Power and Cooling System Design

NASA Technical Reports Server (NTRS)

Landis, Geoffrey A.; Mellott, Kenneth D.

2004-01-01

A radioisotope power and cooling system is designed to provide electrical power for the a probe operating on the surface of Venus. Most foreseeable electronics devices and sensors simply cannot operate at the 450 C ambient surface temperature of Venus. Because the mission duration is substantially long and the use of thermal mass to maintain an operable temperature range is likely impractical, some type of active refrigeration may be required to keep certain components at a temperature below ambient. The fundamental cooling requirements are comprised of the cold sink temperature, the hot sink temperature, and the amount of heat to be removed. In this instance, it is anticipated that electronics would have a nominal operating temperature of 300 C. Due to the highly thermal convective nature of the high-density atmosphere, the hot sink temperature was assumed to be 50 C, which provided a 500 C temperature of the cooler's heat rejecter to the ambient atmosphere. The majority of the heat load on the cooler is from the high temperature ambient surface environment on Venus. Assuming 5 cm radial thickness of ceramic blanket insulation, the ambient heat load was estimated at approximately 77 watts. With an estimated quantity of 10 watts of heat generation from electronics and sensors, and to accommodate some level of uncertainty, the total heat load requirement was rounded up to an even 100 watts. For the radioisotope Stirling power converter configuration designed, the Sage model predicts a thermodynamic power output capacity of 478.1 watts, which slightly exceeds the required 469.1 watts. The hot sink temperature is 1200 C, and the cold sink temperature is 500 C. The required heat input is 1740 watts. This gives a thermodynamic efficiency of 27.48 %. The maximum theoretically obtainable efficiency is 47.52 %. It is estimated that the mechanical efficiency of the power converter design is on the order of 85 %, based on experimental measurements taken from 500 watt power class, laboratory-tested Stirling engines at GRC. The overall efficiency is calculated to be 23.36 %. The mass of the power converter is estimated at approximately 21.6 kg.

Crack growth induced by thermal-mechanical loading

NASA Astrophysics Data System (ADS)

John, R.; Hartman, G. A.; Gallagher, J. P.

1992-06-01

Advanced aerospace structures are often subjected to combined thermal and mechanical loads. The fracture-mechanics behavior of the structures may be altered by the thermal state existing around the crack. Hence, design of critical structural elements requires the knowledge of stress-intensity factors under both thermal and mechanical loads. This paper describes the development of an experimental technique to verify the thermal-stress-intensity factor generated by a temperature gradient around the crack. Thin plate specimens of a model material (AISI-SAE 1095 steel) were used for the heat transfer and thermal-mechanical fracture tests. Rapid thermal loading was achieved using high-intensity focused infrared spot heaters. These heaters were also used to generate controlled temperature rates for heat-transfer verification tests. The experimental results indicate that thermal loads can generate stress-intensity factors large enough to induce crack growth. The proposed thermal-stress-intensity factors appear to have the same effect as the conventional mechanical-stress-intensity factors with respect to fracture.

FEM Modeling of the Relationship between the High-Temperature Hardness and High-Temperature, Quasi-Static Compression Experiment.

PubMed

Zhang, Tao; Jiang, Feng; Yan, Lan; Xu, Xipeng

2017-12-26

The high-temperature hardness test has a wide range of applications, but lacks test standards. The purpose of this study is to develop a finite element method (FEM) model of the relationship between the high-temperature hardness and high-temperature, quasi-static compression experiment, which is a mature test technology with test standards. A high-temperature, quasi-static compression test and a high-temperature hardness test were carried out. The relationship between the high-temperature, quasi-static compression test results and the high-temperature hardness test results was built by the development of a high-temperature indentation finite element (FE) simulation. The simulated and experimental results of high-temperature hardness have been compared, verifying the accuracy of the high-temperature indentation FE simulation.The simulated results show that the high temperature hardness basically does not change with the change of load when the pile-up of material during indentation is ignored. The simulated and experimental results show that the decrease in hardness and thermal softening are consistent. The strain and stress of indentation were analyzed from the simulated contour. It was found that the strain increases with the increase of the test temperature, and the stress decreases with the increase of the test temperature.

FEM Modeling of the Relationship between the High-Temperature Hardness and High-Temperature, Quasi-Static Compression Experiment

PubMed Central

Zhang, Tao; Jiang, Feng; Yan, Lan; Xu, Xipeng

2017-01-01

The high-temperature hardness test has a wide range of applications, but lacks test standards. The purpose of this study is to develop a finite element method (FEM) model of the relationship between the high-temperature hardness and high-temperature, quasi-static compression experiment, which is a mature test technology with test standards. A high-temperature, quasi-static compression test and a high-temperature hardness test were carried out. The relationship between the high-temperature, quasi-static compression test results and the high-temperature hardness test results was built by the development of a high-temperature indentation finite element (FE) simulation. The simulated and experimental results of high-temperature hardness have been compared, verifying the accuracy of the high-temperature indentation FE simulation.The simulated results show that the high temperature hardness basically does not change with the change of load when the pile-up of material during indentation is ignored. The simulated and experimental results show that the decrease in hardness and thermal softening are consistent. The strain and stress of indentation were analyzed from the simulated contour. It was found that the strain increases with the increase of the test temperature, and the stress decreases with the increase of the test temperature. PMID:29278398

High sensitive FBG load cell for icing of overhead transmission lines

NASA Astrophysics Data System (ADS)

Mao, Naiqiang; Ma, Guoming; Li, Chengrong; Li, Yabo; Shi, Cheng; Du, Yue

2017-04-01

Heavy ice coating of overhead transmission lines created the serious threat on the safe operation of power grid. The measurement of conductor icing had been an effective and reliable methods to prevent potential risks, such as conductor breakage, insulator flashover and tower collapse. Because of the advantages of immunity to electromagnetic interference and no demand for power supply in site, the optical load cell has been widely applied in monitoring the ice coating of overhead transmission lines. In this paper, we have adopted the shearing structure with additional grooves as elastic element of load cell to detect the eccentric load. Then, two welding package fiber Bragg gratings (FBGs) were mounted onto the grooves of elastic element with a direction deviation of 90° to eliminate temperature effects on strain measurement without extra FBG. After that, to avoid the occurrence of load cell breakage in heavy load measurement, the protection part has been proposed and added to the elastic element. The results of tension experiments indicate that the resolution of the load cell is 7.78 N in the conventional measuring range (0-10 kN). And in addition, the load cell proposed in this paper also has a good performance in actual experiment in which the load and temperature change simultaneously.

High-temperature-resistant distributed Bragg reflector fiber laser written in Er/Yb co-doped fiber.

PubMed

Guan, Bai-Ou; Zhang, Yang; Wang, Hong-Jun; Chen, Da; Tam, Hwa-Yaw

2008-03-03

We present a high-temperature-resistant distributed Bragg reflector fiber laser photowritten in Er/Yb codoped phosphosilicate fiber that is capable of long-term operation at 500 degrees C. Highly saturated Bragg gratings are directly inscribed into the Er/Yb fiber without hydrogen loading by using a 193 nm excimer laser and phase mask method. After annealing at elevated temperature, the remained gratings are strong enough for laser oscillation. The laser operates in robust single mode with output power more than 1 dBm and signal-to-noise ratio better than 70 dB over the entire temperature range from room temperature to 500 degrees C.

Intermediate photovoltaic system application experiment operational performance report. Volume 6: Beverly High School, Beverly, Mass.

NASA Astrophysics Data System (ADS)

1982-03-01

Performance data are given for the month of February, 1982 for a photovoltaic power supply at a Massachusetts high school. Data given include: monthly and daily electrical energy yield; monthly and daily insolation; monthly and daily array efficiency; energy production as a function of power level, voltage, cell temperature, and hour of day; insolation as a function of hour of the day; input, output and efficiency for each of two power conditioning units and for the total power conditioning system; energy supplied to the load by the photovoltaic system and by the grid; photovoltaic system efficiency; dollar value of the energy supplied by the photovoltaic system; capacity factor; daily photovoltaic energy to load; daily system availability and hours of daylight; heating and cooling degree days; hourly cell temperature, ambient temperature, wind speed, and insolation; average monthly wind speed; wind direction distribution; and daily data acquisition mode and recording interval plot.

High efficiency 40 K single-stage Stirling-type pulse tube cryocooler

NASA Astrophysics Data System (ADS)

Wu, X. L.; Chen, L. B.; Pan, C. Z.; Cui, C.; Wang, J. J.; Zhou, Y.

2017-12-01

A high efficiency single-stage Stirling-type coaxial pulse tube cryocooler (SPTC) operating at around 40 K has been designed, built and tested. The double-inlet and the inertance tubes together with the gas reservoir were adopted as the phase shifters. Under the conditions of 2.5 MPa charging pressure and 30 Hz operating frequency, the prototype has achieved a no-load temperature of 23.8 K with 330 W of electric input power at a rejection temperature of 279 K. When the input power increases to 400 W, it can achieve a cooling capacity of 4.7 W/40 K while rejecting heat at 279 K yielding an efficiency of 7.02% relative to Carnot. It achieves a cooling capacity of 5 W/40 K with an input power of 450 W. It takes 10 minutes for the SPTC to cool to its no-load temperature of 40 K from 295 K.

Visualizing In Situ Microstructure Dependent Crack Tip Stress Distribution in IN-617 Using Nano-mechanical Raman Spectroscopy

NASA Astrophysics Data System (ADS)

Zhang, Yang; Mohanty, Debapriya P.; Tomar, Vikas

2016-11-01

Inconel 617 (IN-617) is a solid solution alloy, which is widely used in applications that require high-temperature component operation due to its high-temperature stability and strength as well as strong resistance to oxidation and carburization. The current work focuses on in situ measurements of stress distribution under 3-point bending at elevated temperature in IN-617. A nanomechanical Raman spectroscopy measurement platform was designed and built based on a combination of a customized open Raman spectroscopy (NMRS) system incorporating a motorized scanning and imaging system with a nanomechanical loading platform. Based on the scanning of the crack tip notch area using the NMRS notch tip, stress distribution under applied load with micron-scale resolution for analyzed microstructures is predicted. A finite element method-based formulation to predict crack tip stresses is presented and validated using the presented experimental data.

Subcritical water liquefaction of oil palm fruit press fiber in the presence of sodium hydroxide: an optimisation study using response surface methodology.

PubMed

Mazaheri, Hossein; Lee, Keat Teong; Bhatia, Subhash; Mohamed, Abdul Rahman

2010-12-01

Thermal decomposition of oil palm fruit press fiber (FPF) into a liquid product (LP) was achieved using subcritical water treatment in the presence of sodium hydroxide in a high pressure batch reactor. This study uses experimental design and process optimisation tools to maximise the LP yield using response surface methodology (RSM) with central composite rotatable design (CCRD). The independent variables were temperature, residence time, particle size, specimen loading, and additive loading. The mathematical model that was developed fit the experimental results well for all of the response variables that were studied. The optimal conditions were found to be a temperature of 551 K, a residence time of 40 min, a particle size of 710-1000 microm, a specimen loading of 5 g, and a additive loading of 9 wt.% to achieve a LP yield of 76.16%. 2010 Elsevier Ltd. All rights reserved.

Study on Characteristic of Temperature Coefficient of Reactivity for Plutonium Core of Pebbled Bed Reactor

NASA Astrophysics Data System (ADS)

Zuhair; Suwoto; Setiadipura, T.; Bakhri, S.; Sunaryo, G. R.

2018-02-01

As a part of the solution searching for possibility to control the plutonium, a current effort is focused on mechanisms to maximize consumption of plutonium. Plutonium core solution is a unique case in the high temperature reactor which is intended to reduce the accumulation of plutonium. However, the safety performance of the plutonium core which tends to produce a positive temperature coefficient of reactivity should be examined. The pebble bed inherent safety features which are characterized by a negative temperature coefficient of reactivity must be maintained under any circumstances. The purpose of this study is to investigate the characteristic of temperature coefficient of reactivity for plutonium core of pebble bed reactor. A series of calculations with plutonium loading varied from 0.5 g to 1.5 g per fuel pebble were performed by the MCNPX code and ENDF/B-VII library. The calculation results show that the k eff curve of 0.5 g Pu/pebble declines sharply with the increase in fuel burnup while the greater Pu loading per pebble yields k eff curve declines slighter. The fuel with high Pu content per pebble may reach long burnup cycle. From the temperature coefficient point of view, it is concluded that the reactor containing 0.5 g-1.25 g Pu/pebble at high burnup has less favorable safety features if it is operated at high temperature. The use of fuel with Pu content of 1.5 g/pebble at high burnup should be considered carefully from core safety aspect because it could affect transient behavior into a fatal accident situation.

Corrosion in MDEA sour gas treating plants: Correlation between laboratory testing and field experience

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bich, N.N.; Vacha, F.; Schubert, R.

1996-08-01

Corrosion in MDEA sour gas treating systems operating in severely loaded conditions is investigated using both laboratory data and actual gas plant experience. Effects of acid gas loading, flow turbulence, solution quality, temperature, etc. on corrosion are being studied. Preliminary results indicated severe corrosion of several mm/y would occur if acid gas loading, circulation rate and level of suspended solids are all high. A mitigation strategy based on operating envelopes is formulated.

Program for the development of high temperature electrical materials and components

NASA Technical Reports Server (NTRS)

Neff, W. S.; Lowry, L. R.

1972-01-01

Evaluation of high temperature, space-vacuum performance of selected electrical materials and components, high temperature capacitor development, and evaluation, construction, and endurance testing of compression sealed pyrolytic boron nitride slot insulation are described. The first subject above covered the aging evaluation of electrical devices constructed from selected electrical materials. Individual materials performances were also evaluated and reported. The second subject included study of methods of improving electrical performance of pyrolytic boron nitride capacitors. The third portion was conducted to evaluate the thermal and electrical performance of pyrolytic boron nitride as stator slot liner material under varied temperature and compressive loading. Conclusions and recommendations are presented.

High performance aluminum–cerium alloys for high-temperature applications

DOE PAGES

Sims, Zachary C.; Rios, Orlando R.; Weiss, David; ...

2017-08-01

Light-weight high-temperature alloys are important to the transportation industry where weight, cost, and operating temperature are major factors in the design of energy efficient vehicles. Aluminum alloys fill this gap economically but lack high-temperature mechanical performance. Alloying aluminum with cerium creates a highly castable alloy, compatible with traditional aluminum alloy additions, that exhibits dramatically improved high-temperature performance. These compositions display a room temperature ultimate tensile strength of 400 MPa and yield strength of 320 MPa, with 80% mechanical property retention at 240 °C. A mechanism is identified that addresses the mechanical property stability of the Al-alloys to at least 300more » °C and their microstructural stability to above 500 °C which may enable applications without the need for heat treatment. Lastly, neutron diffraction under load provides insight into the unusual mechanisms driving the mechanical strength.« less

Performance Testing of a High Temperature Linear Alternator for Stirling Convertors

NASA Technical Reports Server (NTRS)

Metscher, Jonathan; Geng, Steven

2016-01-01

The NASA Glenn Research Center has conducted performance testing of a high temperature linear alternator (HTLA) in support of Stirling power convertor development for potential future Radioisotope Power Systems (RPS). The high temperature linear alternator is a modified version of that used in Sunpowers Advanced Stirling Convertor (ASC), and is capable of operation at temperatures up to 200 C. Increasing the temperature capability of the linear alternator could expand the mission space of future Stirling RPS designs. High temperature Neodymium-Iron-Boron (Nd-Fe-B) magnets were selected for the HTLA application, and were fully characterized and tested prior to uses. Higher temperature epoxy for alternator assembly was also selected and tested for thermal stability and strength. A characterization test was performed on the HTLA to measure its performance at various amplitudes, loads, and temperatures. HTLA endurance testing at 200 C is currently underway.

Performance Testing of a High Temperature Linear Alternator for Stirling Convertors

NASA Technical Reports Server (NTRS)

Metscher, Jonathan F.; Geng, Steven M.

2016-01-01

The NASA Glenn Research Center has conducted performance testing of a high temperature linear alternator (HTLA) in support of Stirling power convertor development for potential future Radioisotope Power Systems (RPS). The high temperature linear alternator is a modified version of that used in Sunpower's Advanced Stirling Convertor (ASC), and is capable of operation at temperatures up to 200 deg. Increasing the temperature capability of the linear alternator could expand the mission set of future Stirling RPS designs. High temperature Neodymium-Iron-Boron (Nd-Fe-B) magnets were selected for the HTLA application, and were fully characterized and tested prior to use. Higher temperature epoxy for alternator assembly was also selected and tested for thermal stability and strength. A characterization test was performed on the HTLA to measure its performance at various amplitudes, loads, and temperatures. HTLA endurance testing at 200 deg is currently underway.

High-temperature gas/liquid stress relaxometers

NASA Technical Reports Server (NTRS)

Kalfayan, S. H.; Silver, R. H.

1974-01-01

Two relaxometers allow testing of elastomers in various fluids. First relaxometer uses fork-like loading spacer interposed between loading lever and support ring, so that sample is stretched predetermined amount. In second relaxometer, degree of initial elongation is set by means of adjustable collar, which, when locked in place on piston rod, enables sample to be stretched predetermined length.

High pressure solubility of carbon dioxide (CO2) in aqueous solution of piperazine (PZ) activated N-methyldiethanolamine (MDEA) solvent for CO2 capture

NASA Astrophysics Data System (ADS)

Khan, Saleem Nawaz; Hailegiorgis, Sintayehu Mekuria; Man, Zakaria; Shariff, Azmi Mohd

2017-10-01

In this study, the solubility of carbon dioxide (CO2) in the aqueous solution of piperazine (PZ) activated N-methyldiethanolamine (MDEA) was investigated. In the aqueous solution the concentrations of the N-methyldiethanolamine (MDEA) and piperazine (PZ) were kept constant at 30 wt. % and 3 wt. %, respectively. The solubility experiments were carried out between the temperatures ranges of 303.15 to 333.15 K. The pressure range was selected as 2-50 bar for solubility of carbon dioxide in the aqueous solution. The solubility of the CO2 is reported in terms of CO2 loading capacity of the solvent. The loading capacity of the solvent is the ratio between the numbers of moles of CO2 absorbed to the numbers of moles of solvent used. The experimental data showed that the CO2 loading increased with increase in CO2 partial pressure, while it decreased with increase in system's temperature. It was also observed from the experimental data that the higher pressure favors the absorption process while the increased temperature hinders the absorption process of CO2 capture. The loading capacity of the investigated solvent was compared with the loading capacity of the solvents reported in the literature. The investigated solvent showed better solubility in terms of loading capacity.

Temperature and Material Flow Prediction in Friction-Stir Spot Welding of Advanced High-Strength Steel

NASA Astrophysics Data System (ADS)

Miles, M.; Karki, U.; Hovanski, Y.

2014-10-01

Friction-stir spot welding (FSSW) has been shown to be capable of joining advanced high-strength steel, with its flexibility in controlling the heat of welding and the resulting microstructure of the joint. This makes FSSW a potential alternative to resistance spot welding if tool life is sufficiently high, and if machine spindle loads are sufficiently low that the process can be implemented on an industrial robot. Robots for spot welding can typically sustain vertical loads of about 8 kN, but FSSW at tool speeds of less than 3000 rpm cause loads that are too high, in the range of 11-14 kN. Therefore, in the current work, tool speeds of 5000 rpm were employed to generate heat more quickly and to reduce welding loads to acceptable levels. Si3N4 tools were used for the welding experiments on 1.2-mm DP 980 steel. The FSSW process was modeled with a finite element approach using the Forge® software. An updated Lagrangian scheme with explicit time integration was employed to predict the flow of the sheet material, subjected to boundary conditions of a rotating tool and a fixed backing plate. Material flow was calculated from a velocity field that is two-dimensional, but heat generated by friction was computed by a novel approach, where the rotational velocity component imparted to the sheet by the tool surface was included in the thermal boundary conditions. An isotropic, viscoplastic Norton-Hoff law was used to compute the material flow stress as a function of strain, strain rate, and temperature. The model predicted welding temperatures to within 4%, and the position of the joint interface to within 10%, of the experimental results.

Temperature and Material Flow Prediction in Friction-Stir Spot Welding of Advanced High-Strength Steel

DOE Office of Scientific and Technical Information (OSTI.GOV)

Miles, Michael; Karki, U.; Hovanski, Yuri

Friction-stir spot welding (FSSW) has been shown to be capable of joining advanced high-strength steel, with its flexibility in controlling the heat of welding and the resulting microstructure of the joint. This makes FSSW a potential alternative to resistance spot welding if tool life is sufficiently high, and if machine spindle loads are sufficiently low that the process can be implemented on an industrial robot. Robots for spot welding can typically sustain vertical loads of about 8 kN, but FSSW at tool speeds of less than 3000 rpm cause loads that are too high, in the range of 11–14 kN.more » Therefore, in the current work, tool speeds of 5000 rpm were employed to generate heat more quickly and to reduce welding loads to acceptable levels. Si3N4 tools were used for the welding experiments on 1.2-mm DP 980 steel. The FSSW process was modeled with a finite element approach using the Forge* software. An updated Lagrangian scheme with explicit time integration was employed to predict the flow of the sheet material, subjected to boundary conditions of a rotating tool and a fixed backing plate. Material flow was calculated from a velocity field that is two-dimensional, but heat generated by friction was computed by a novel approach, where the rotational velocity component imparted to the sheet by the tool surface was included in the thermal boundary conditions. An isotropic, viscoplastic Norton-Hoff law was used to compute the material flow stress as a function of strain, strain rate, and temperature. The model predicted welding temperatures to within percent, and the position of the joint interface to within 10 percent, of the experimental results.« less

[New methods for determining the relative load due to physical effort of the human body].

PubMed

Szubert, Józef; Szubert, Sławomir; Koszada-Włodarczyk, Wiesława; Bortkiewicz, Alicja

2014-01-01

The relative physical load (% VO2max) is the quotient of oxygen uptake (Vo2) during physical effort and maximum oxygen uptake (VO2max) by the human body. For this purpose the stress test must be performed. The relative load shows a high correlation with minute ventilation, cardiac output, heart rate, stroke volume, increased concentrations of catecholamines in the blood, inner temperature, weight, height and human body surface area. The relative load is a criterion for the maximum workloads admissible for healthy and sick workers. Besides, the classification of effort can be more precise when based on the relative load than on the energy output. Based on our own and international empirical evidence and the laws of heat transfer and fluid mechanics, a model of temperature control system has been developed, involving the elements of human cardiovascular and respiratory systems. Using this model, we have been able to develop our own methods of determining the relative load, applying only the body core temperature (Tw) or heart rate within one minute (HR), body mass (m), height (H), and body surface area (AD) instead of VO,max. The values of the relative physical load (% VO2max) obtained by using our own methods do not differ significantly from those obtained by other methods and by other researchers. The developed methods for determining the relative physical load (% VO2max) do not require the exercise test to be performed, therefore, they may be considered (after verification in an experimental study) a feasible alternative to current methods.

Effects of various calcined ash and sludge waste loadings on the durability of a soda-lime-silica glass

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kramer, D.P.; Lewis, E.L.; Armstrong, K.M.

1982-01-01

A commercially available joule-heated glass furnace system is currently being evaluated at Mound as a means of reducing the volume of low-level radioactive waste similar to that found in light water reactor facilities. The furnace utilizes molten soda-lime-silica to initiate and support combustion of the waste feed and to serve as an immobilization matrix. First, corrosion studies were performed to determine the result that various waste loadings of glass would have on the refractory lining the furnace. Second, the chemical durability of soda-lime-silica under various waste loadings was assessed to determine its resistance to leaching under conditions similar to thosemore » encountered at waste disposal sites. Results proved that, although corrosion was quite significant for pure soda-lime-silica and a 10% waste loading, by the time a waste loading of 40% was achieved, the effects of corrosion were virtually nil. The temperature dependence of the corrosion caused by a 0% waste loading of soda-lime-silica on the refractory was also investigated. With an increase in temperature to 2650/sup 0/F, corrosion more than tripled. As a result, incineration and idle temperature is being maintained at, or below, 2400/sup 0/F. In conclusion, from the fact that the higher waste loading of soda-lime glass produced both increased chemical durability and increased refractory life, waste loadings in excess of 40%, and as high as 80%, may be achieved without adverse effect to the glass furnace system or its effectiveness for immobilizing radioactive waste.« less

X ray attenuation measurements for high-temperature materials characterization and in-situ monitoring of damage accumulation. Ph.D. Thesis - Cleveland State Univ., 1991

NASA Technical Reports Server (NTRS)

Baaklini, George Y.

1992-01-01

The scope of this dissertation is to develop and apply x ray attenuation measurement systems that are capable of: (1) characterizing density variations in high-temperature materials, e.g., monolithic ceramics, ceramic and intermetallic matrix composites, and (2) noninvasively monitoring damage accumulation and failure sequences in ceramic matrix composites under room temperature tensile testing. This dissertation results in the development of: (1) a point scan digital radiography system, and (2) an in-situ x ray material testing system. Radiographic evaluation before, during, and after loading shows the effect of preexisting volume flaws on the fracture behavior of composites. Results show that x ray film radiography can monitor damage accumulation during tensile loading. Matrix cracking, fiber matrix debonding, fiber bridging, and fiber pullout are imaged throughout the tensile loading of the specimens. Further in-situ radiography is found to be a practical technique for estimating interfacial shear strength between the silicon carbide fibers and the reaction bonded silicon nitride matrix. It is concluded that pretest, in-situ, and post test x ray imaging can provide for greater understanding of ceramic matrix composite mechanical behavior.

Correlation of Electrical Resistance to CMC Stress-Strain and Fracture Behavior Under High Heat-Flux Thermal and Stress Gradients

NASA Technical Reports Server (NTRS)

Appleby, Matthew; Morscher, Gregory; Zhu, Dongming

2015-01-01

Because SiCSiC ceramic matrix composites (CMCs) are under consideration for use as turbine engine hot-section components in extreme environments, it becomes necessary to investigate their performance and damage morphologies under complex loading and environmental conditions. Monitoring of electrical resistance (ER) has been shown as an effective tool for detecting damage accumulation of woven melt-infiltrated SiCSiC CMCs. However, ER change under complicated thermo-mechanical loading is not well understood. In this study a systematic approach is taken to determine the capabilities of ER as a relevant non-destructive evaluation technique for high heat-flux testing, including thermal gradients and localized stress concentrations. Room temperature and high temperature, laser-based tensile tests were conducted in which stress-dependent damage locations were determined using modal acoustic emission (AE) monitoring and compared to full-field strain mapping using digital image correlation (DIC). This information is then compared with the results of in-situ ER monitoring, post-test ER inspection and fractography in order to correlate ER response to convoluted loading conditions and damage evolution.

BMI Sandwich Wing Box Analysis and Test

NASA Technical Reports Server (NTRS)

Palm, Tod; Mahler, Mary; Shah, Chandu; Rouse, Marshall; Bush, Harold; Wu, Chauncey; Small, William J.

2000-01-01

A composite sandwich single bay wing box test article was developed by Northrop Grumman and tested recently at NASA Langley Research Center. The objectives for the wing box development effort were to provide a demonstration article for manufacturing scale up of structural concepts related to a high speed transport wing, and to validate the structural performance of the design. The box concept consisted of highly loaded composite sandwich wing skins, with moderately loaded composite sandwich spars. The dimensions of the box were chosen to represent a single bay of the main wing box, with a spar spacing of 30 inches, height of 20 inches constant depth, and length of 64 inches. The bismaleimide facesheet laminates and titanium honeycomb core chosen for this task are high temperature materials able to sustain a 300F service temperature. The completed test article is shown in Figure 1. The tests at NASA Langley demonstrated the structures ability to sustain axial tension and compression loads in excess of 20,000 lb/in, and to maintain integrity in the thermal environment. Test procedures, analysis failure predictions, and test results are presented.

Fixed target matrix for femtosecond time-resolved and in situ serial micro-crystallography

PubMed Central

Mueller, C.; Marx, A.; Epp, S. W.; Zhong, Y.; Kuo, A.; Balo, A. R.; Soman, J.; Schotte, F.; Lemke, H. T.; Owen, R. L.; Pai, E. F.; Pearson, A. R.; Olson, J. S.; Anfinrud, P. A.; Ernst, O. P.; Dwayne Miller, R. J.

2015-01-01

We present a crystallography chip enabling in situ room temperature crystallography at microfocus synchrotron beamlines and X-ray free-electron laser (X-FEL) sources. Compared to other in situ approaches, we observe extremely low background and high diffraction data quality. The chip design is robust and allows fast and efficient loading of thousands of small crystals. The ability to load a large number of protein crystals, at room temperature and with high efficiency, into prescribed positions enables high throughput automated serial crystallography with microfocus synchrotron beamlines. In addition, we demonstrate the application of this chip for femtosecond time-resolved serial crystallography at the Linac Coherent Light Source (LCLS, Menlo Park, California, USA). The chip concept enables multiple images to be acquired from each crystal, allowing differential detection of changes in diffraction intensities in order to obtain high signal-to-noise and fully exploit the time resolution capabilities of XFELs. PMID:26798825

Fixed target matrix for femtosecond time-resolved and in situ serial micro-crystallography.

PubMed

Mueller, C; Marx, A; Epp, S W; Zhong, Y; Kuo, A; Balo, A R; Soman, J; Schotte, F; Lemke, H T; Owen, R L; Pai, E F; Pearson, A R; Olson, J S; Anfinrud, P A; Ernst, O P; Dwayne Miller, R J

2015-09-01

We present a crystallography chip enabling in situ room temperature crystallography at microfocus synchrotron beamlines and X-ray free-electron laser (X-FEL) sources. Compared to other in situ approaches, we observe extremely low background and high diffraction data quality. The chip design is robust and allows fast and efficient loading of thousands of small crystals. The ability to load a large number of protein crystals, at room temperature and with high efficiency, into prescribed positions enables high throughput automated serial crystallography with microfocus synchrotron beamlines. In addition, we demonstrate the application of this chip for femtosecond time-resolved serial crystallography at the Linac Coherent Light Source (LCLS, Menlo Park, California, USA). The chip concept enables multiple images to be acquired from each crystal, allowing differential detection of changes in diffraction intensities in order to obtain high signal-to-noise and fully exploit the time resolution capabilities of XFELs.

Interpretation of dynamic tensile behavior by austenite stability in ferrite-austenite duplex lightweight steels.

PubMed

Park, Jaeyeong; Jo, Min Cheol; Jeong, Hyeok Jae; Sohn, Seok Su; Kwak, Jai-Hyun; Kim, Hyoung Seop; Lee, Sunghak

2017-11-16

Phenomena occurring in duplex lightweight steels under dynamic loading are hardly investigated, although its understanding is essentially needed in applications of automotive steels. In this study, quasi-static and dynamic tensile properties of duplex lightweight steels were investigated by focusing on how TRIP and TWIP mechanisms were varied under the quasi-static and dynamic loading conditions. As the annealing temperature increased, the grain size and volume fraction of austenite increased, thereby gradually decreasing austenite stability. The strain-hardening rate curves displayed a multiple-stage strain-hardening behavior, which was closely related with deformation mechanisms. Under the dynamic loading, the temperature rise due to adiabatic heating raised the austenite stability, which resulted in the reduction in the TRIP amount. Though the 950 °C-annealed specimen having the lowest austenite stability showed the very low ductility and strength under the quasi-static loading, it exhibited the tensile elongation up to 54% as well as high strain-hardening rate and tensile strength (1038 MPa) due to appropriate austenite stability under dynamic loading. Since dynamic properties of the present duplex lightweight steels show the excellent strength-ductility combination as well as continuously high strain hardening, they can be sufficiently applied to automotive steel sheets demanded for stronger vehicle bodies and safety enhancement.

Effects of Heat of Vaporization and Octane Sensitivity on Knock-Limited Spark Ignition Engine Performance

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ratcliff, Matthew A; Burton, Jonathan L; Sindler, Petr

Knock-limited loads for a set of surrogate gasolines all having nominal 100 research octane number (RON), approximately 11 octane sensitivity (S), and a heat of vaporization (HOV) range of 390 to 595 kJ/kg at 25 degrees C were investigated. A single-cylinder spark-ignition engine derived from a General Motors Ecotec direct injection (DI) engine was used to perform load sweeps at a fixed intake air temperature (IAT) of 50 degrees C, as well as knock-limited load measurements across a range of IATs up to 90 degrees C. Both DI and pre-vaporized fuel (supplied by a fuel injector mounted far upstream ofmore » the intake valves and heated intake runner walls) experiments were performed to separate the chemical and thermal effects of the fuels' knock resistance. The DI load sweeps at 50 degrees C intake air temperature showed no effect of HOV on the knock-limited performance. The data suggest that HOV acts as a thermal contributor to S under the conditions studied. Measurement of knock-limited loads from the IAT sweeps for DI at late combustion phasing showed that a 40 vol% ethanol (E40) blend provided additional knock resistance at the highest temperatures, compared to a 20 vol% ethanol blend and hydrocarbon fuel with similar RON and S. Using the pre-vaporized fuel system, all the high S fuels produced nearly identical knock-limited loads at each temperature across the range of IATs studied. For these fuels RON ranged from 99.2 to 101.1 and S ranged from 9.4 to 12.2, with E40 having the lowest RON and highest S. The higher knock-limited loads for E40 at the highest IATs examined were consistent with the slightly higher S for this fuel, and the lower engine operating condition K values arising from use of this fuel. The study highlights how fuel HOV can affect the temperature at intake valve closing, and consequently the pressure-temperature history of the end gas leading to more negative values of K, thereby enhancing the effect of S on knock resistance.« less

High performance diesel oxidation catalysts using ultra-low Pt loading on titania nanowire array integrated cordierite honeycombs

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hoang, Son; Lu, Xingxu; Tang, Wenxiang

High performance of an ultra-low Pt loading diesel oxidation catalyst can be achieved by using a combination of novel nano-array structured support, precise control of ultrafine active Pt particles, and an addition of H 2 as a promoter into the exhausts. Highly stable mesoporous rutile TiO 2 nano-array was uniformly grown on three-dimensional (3-D) cordierite honeycomb monoliths using a solvothermal synthesis. Atomic layer deposition was employed for precise dispersion of ultrafine Pt particles (0.95 ± 0.24 nm) on TiO 2 nano-array with a Pt loading of 1.1 g/ft 3. Despite low Pt loading, the Pt/TiO 2 nano-array catalyst shows impressivemore » low-temperature oxidation reactivity, with the conversion of CO and total hydrocarbon (THC) reaching 50% at 224 and 285 °C, respectively, in the clean diesel combustion (CDC) simulated exhaust conditions. The excellent activity is attributed to the unique nano-array structure that promotes gas-solid interaction and ultra-small Pt particle dispersion that increase surface Pt atoms. We also demonstrate that addition of more H 2 into the exhaust can lower light-off temperature for CO and THC by up to ~60 °C and ~30 °C, respectively.« less

High performance diesel oxidation catalysts using ultra-low Pt loading on titania nanowire array integrated cordierite honeycombs

DOE PAGES

Hoang, Son; Lu, Xingxu; Tang, Wenxiang; ...

2017-11-15

High performance of an ultra-low Pt loading diesel oxidation catalyst can be achieved by using a combination of novel nano-array structured support, precise control of ultrafine active Pt particles, and an addition of H 2 as a promoter into the exhausts. Highly stable mesoporous rutile TiO 2 nano-array was uniformly grown on three-dimensional (3-D) cordierite honeycomb monoliths using a solvothermal synthesis. Atomic layer deposition was employed for precise dispersion of ultrafine Pt particles (0.95 ± 0.24 nm) on TiO 2 nano-array with a Pt loading of 1.1 g/ft 3. Despite low Pt loading, the Pt/TiO 2 nano-array catalyst shows impressivemore » low-temperature oxidation reactivity, with the conversion of CO and total hydrocarbon (THC) reaching 50% at 224 and 285 °C, respectively, in the clean diesel combustion (CDC) simulated exhaust conditions. The excellent activity is attributed to the unique nano-array structure that promotes gas-solid interaction and ultra-small Pt particle dispersion that increase surface Pt atoms. We also demonstrate that addition of more H 2 into the exhaust can lower light-off temperature for CO and THC by up to ~60 °C and ~30 °C, respectively.« less

Advanced gearbox technology

NASA Technical Reports Server (NTRS)

Anderson, N. E.; Cedoz, R. W.; Salama, E. E.; Wagner, D. A.

1987-01-01

An advanced 13,000 HP, counterrotating (CR) gearbox was designed and successfully tested to provide a technology base for future designs of geared propfan propulsion systems for both commercial and military aircraft. The advanced technology CR gearbox was designed for high efficiency, low weight, long life, and improved maintainability. The differential planetary CR gearbox features double helical gears, double row cylindrical roller bearings integral with planet gears, tapered roller prop support bearings, and a flexible ring gear and diaphragm to provide load sharing. A new Allison propfan back-to-back gearbox test facility was constructed. Extensive rotating and stationary instrumentation was used to measure temperature, strain, vibration, deflection and efficiency under representative flight operating conditions. The tests verified smooth, efficient gearbox operation. The highly-instrumented advanced CR gearbox was successfully tested to design speed and power (13,000 HP), and to a 115 percent overspeed condition. Measured CR gearbox efficiency was 99.3 percent at the design point based on heat loss to the oil. Tests demonstrated low vibration characteristics of double helical gearing, proper gear tooth load sharing, low stress levels, and the high load capacity of the prop tapered roller bearings. Applied external prop loads did not significantly affect gearbox temperature, vibration, or stress levels. Gearbox hardware was in excellent condition after the tests with no indication of distress.

Control of the low-load region in partially premixed combustion

NASA Astrophysics Data System (ADS)

Ingesson, Gabriel; Yin, Lianhao; Johansson, Rolf; Tunestal, Per

2016-09-01

Partially premixed combustion (PPC) is a low temperature, direct-injection combustion concept that has shown to give promising emission levels and efficiencies over a wide operating range. In this concept, high EGR ratios, high octane-number fuels and early injection timings are used to slow down the auto-ignition reactions and to enhance the fuel and are mixing before the start of combustion. A drawback with this concept is the combustion stability in the low-load region where a high octane-number fuel might cause misfire and low combustion efficiency. This paper investigates the problem of low-load PPC controller design for increased engine efficiency. First, low-load PPC data, obtained from a multi-cylinder heavy- duty engine is presented. The data shows that combustion efficiency could be increased by using a pilot injection and that there is a non-linearity in the relation between injection and combustion timing. Furthermore, intake conditions should be set in order to avoid operating points with unfavourable global equivalence ratio and in-cylinder temperature combinations. Model predictive control simulations were used together with a calibrated engine model to find a gas-system controller that fulfilled this task. The findings are then summarized in a suggested engine controller design. Finally, an experimental performance evaluation of the suggested controller is presented.

Nonlinear Constitutive Relations for High Temperature Applications

NASA Technical Reports Server (NTRS)

1983-01-01

The topics of discussion addressed were material behavior, design analysis, deformation kinetics, metallurgical characterization, mechanical subelement models, stress analysis, fracture mechanics, viscoplasticity, and thermal loading.

Power Generation from a Radiative Thermal Source Using a Large-Area Infrared Rectenna

NASA Astrophysics Data System (ADS)

Shank, Joshua; Kadlec, Emil A.; Jarecki, Robert L.; Starbuck, Andrew; Howell, Stephen; Peters, David W.; Davids, Paul S.

2018-05-01

Electrical power generation from a moderate-temperature thermal source by means of direct conversion of infrared radiation is important and highly desirable for energy harvesting from waste heat and micropower applications. Here, we demonstrate direct rectified power generation from an unbiased large-area nanoantenna-coupled tunnel diode rectifier called a rectenna. Using a vacuum radiometric measurement technique with irradiation from a temperature-stabilized thermal source, a generated power density of 8 nW /cm2 is observed at a source temperature of 450 °C for the unbiased rectenna across an optimized load resistance. The optimized load resistance for the peak power generation for each temperature coincides with the tunnel diode resistance at zero bias and corresponds to the impedance matching condition for a rectifying antenna. Current-voltage measurements of a thermally illuminated large-area rectenna show current zero crossing shifts into the second quadrant indicating rectification. Photon-assisted tunneling in the unbiased rectenna is modeled as the mechanism for the large short-circuit photocurrents observed where the photon energy serves as an effective bias across the tunnel junction. The measured current and voltage across the load resistor as a function of the thermal source temperature represents direct current electrical power generation.

Unusual plasticity and strength of metals at ultra-short load durations

NASA Astrophysics Data System (ADS)

Kanel, G. I.; Zaretsky, E. B.; Razorenov, S. V.; Ashitkov, S. I.; Fortov, V. E.

2017-08-01

This paper briefly reviews recent experimental results on the temperature-rate dependences of flow and fracture stresses in metals under high strain rate conditions for pulsed shock-wave loads with durations from tens of picoseconds up to microseconds. In the experiments, ultimate (‘ideal’) values of the shear and tensile strengths have been approached and anomalous growth of the yield stress with temperature at high strain rates has been confirmed for some metals. New evidence is obtained for the intense dislocation multiplication immediately originating in the elastic precursor of a compression shock wave. It is found that under these conditions inclusions and other strengthening factors may have a softening effect. Novel and unexpected features are observed in the evolution of elastoplastic compression shock waves.

An atomic beam source for fast loading of a magneto-optical trap under high vacuum

DOE Office of Scientific and Technical Information (OSTI.GOV)

McDowall, Peter D.; Gruenzweig, Tzahi; Hilliard, Andrew

2012-05-15

We report on a directional atomic beam created using an alkali metal dispenser and a nozzle. By applying a high current (15 A) pulse to the dispenser at room temperature we can rapidly heat it to a temperature at which it starts dispensing, avoiding the need for preheating. The atomic beam produced is capable of loading 90% of a magneto-optical trap (MOT) in less than 7 s while maintaining a low vacuum pressure of <10{sup -11} Torr. The transverse velocity components of the atomic beam are measured to be within typical capture velocities of a rubidium MOT. Finally, we showmore » that the atomic beam can be turned off within 1.8 s.« less

National Aerospace Plane Integrated Fuselage/Cryotank Risk Reduction program

NASA Astrophysics Data System (ADS)

Dayton, K. E.

1993-06-01

The principal objectives and results of the National Aerospace Plane (NASP) Integrated Risk Reduction program are briefly reviewed. The program demonstrated the feasibility of manufacturing lightweight advanced composite materials for single-stage-to-orbit hypersonic flight vehicle applications. A series of combined load simulation tests (thermal, mechanical, and cryogenic) demonstrated proof of concept performance for an all unlined composite cryogenic fuel tank with flat end bulkheads and a high-temperature thin-shell advanced composite fuselage. Temperatures of the fuselage were as high as 1300 F, with 100 percent bending and shear loads applied to the tank while filled with 850 gallons of cryogenic fluid hydrogen (-425 F). Leak rates measured on and around the cryotank shell and bulkheads were well below acceptable levels.

Blast and Penetration Resistant Tactical Shelters

DTIC Science & Technology

1979-07-01

2. Hardened Wall Material Properties 32 3. S-280 Shelter Panal Properties 33 4. Results Zor Dynamic Response of Complete S-280 Shelters 32 £-". In...insulation from a -6501 low to a 120 0F high plus a solar heating load 7. Corrosion resistance including salt fog 8. Blackout capability 9. Fungus...65 0 F), high temperature (120 0 F) plus a solar heating (BTU) load. g. Corrosion resistance (salt fog). 19 h. Blackout capability. i. Fungus

On the formation of adiabatic shear bands in titanium alloy Ti17 under severe loading conditions

NASA Astrophysics Data System (ADS)

Boubaker, H. Ben; Ayed, Y.; Mareau, C.; Germain, G.

2018-05-01

For metallic materials, fabrication processes (e.g. machining and forging) may involve important strain rates and high temperatures. For such severe loading conditions, the development of damage is often associated with the formation of Adiabatic Shear Bands (ASB). In this work, the impact of loading conditions (strain rate, temperature) on the formation of ASB in a beta rich titanium alloy (Ti17) is investigated. In this perspective, uniaxial compression tests have been conducted on cylindrical samples with a Gleeble-3500 thermo-mechanical simulator at temperatures ranging from 25°C to 800°C and strain rates ranging from 0.1 to 50 s-1 with axial strains of approximately 50 %. According to the experimental results, the flow curves exhibit hardening from 25°C to 550°C and softening from 600°C to 800°C. When looking at the evolution of flow stress, the strain rate sensitivity is found to increase significantly with increasing temperatures. Also, adiabatic shear bands are preferably observed for high strain rates and low temperatures. The formation of ASB thus seems to be quite dependent on the evolution of the strain rate sensitivity of Ti17. Finally, metallographic observations have been carried out to better understand the process leading to the formation of ASB. Such observations demonstrate that the average width of ASB increases with increasing temperatures and decreasing strain rates. However, such observations do not allow for identifying whether some specific microstructural transformations (e.g recrystallization or phase transformation) could explain the formation of ASB or not.

A Si/Glass Bulk-Micromachined Cryogenic Heat Exchanger for High Heat Loads: Fabrication, Test, and Application Results

PubMed Central

Zhu, Weibin; White, Michael J.; Nellis, Gregory F.; Klein, Sanford A.; Gianchandani, Yogesh B.

2010-01-01

This paper reports on a micromachined Si/glass stack recuperative heat exchanger with in situ temperature sensors. Numerous high-conductivity silicon plates with integrated platinum resistance temperature detectors (Pt RTDs) are stacked, alternating with low-conductivity Pyrex spacers. The device has a 1 × 1-cm2 footprint and a length of up to 3.5 cm. It is intended for use in Joule–Thomson (J–T) coolers and can sustain pressure exceeding 1 MPa. Tests at cold-end inlet temperatures of 237 K–252 K show that the heat exchanger effectiveness is 0.9 with 0.039-g/s helium mass flow rate. The integrated Pt RTDs present a linear response of 0.26%–0.30%/K over an operational range of 205 K–296 K but remain usable at lower temperatures. In self-cooling tests with ethane as the working fluid, a J–T system with the heat exchanger drops 76.1 K below the inlet temperature, achieving 218.7 K for a pressure of 835.8 kPa. The system reaches 200 K in transient state; further cooling is limited by impurities that freeze within the flow stream. In J–T self-cooling tests with an external heat load, the system reaches 239 K while providing 1 W of cooling. In all cases, there is an additional parasitic heat load estimated at 300–500 mW. PMID:20490284

Measurements of the apparent thermal conductivity of multi-layer insulation between 20 K and 90 K

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hurd, Joseph A.; Van Sciver, Steven W.

NASA has the need to efficiently store cryogenic propellants in space for long periods of time. One method to improve storage efficiency is to use multi-layer insulation (MLI), a technique that minimizes the boiling rate due to radiation heat transfer. Typically, the thermal performance of MLI is determined by measuring the rate of evaporation of liquid nitrogen from a calibrated cryostat. The main limitation with this method is that testing conditions are restricted by the boiling temperature of the LN{sub 2}, which may not match the requirements of the application. The Multi-Layer Insulation Thermal Conductivity Experiment (MIKE) at the Nationalmore » High Magnetic Field Laboratory is capable of measuring the effective thermal conductivity of MLI at variable boundary temperatures. MIKE uses cryo-refrigerators to control boundary temperatures in the calorimeter and a calibrated thermal link to measure the heat load. To make the measurements requested by NASA, MIKE needed to be recalibrated for the 20 K to 90 K range. Also, due to the expectation of a lower heat transfer rate, the heat load support rod material was changed to one with a lower thermal conductivity to ensure the temperature difference seen on the cold rod could be measurable at the estimated heat load. Presented are the alterations to MIKE including calibration data and heat load measurements on new load-bearing MLI supplied by NASA.« less

Low-temperature operation of a Buck DC/DC converter

NASA Technical Reports Server (NTRS)

Ray, Biswajit; Gerber, Scott S.; Patterson, Richard L.; Myers, Ira T.

1995-01-01

Low-temperature (77 K) operation of a 42/28 V, 175 W, 50 kHz PWM Buck DC/DC converter designed with commercially available components is reported. Overall, the converter losses decreased at 77 K compared to room temperature operation. A full-load efficiency of 97 percent was recorded at liquid-nitrogen temperature, compared to 95.8 percent at room temperature. Power MOSFET operation improved significantly where as the output rectifier operation deteriorated at low-temperature. The performance of the output filter inductor and capacitor did not change significantly at 77 K compared to room temperature performance. It is possible to achieve high-density and high efficiency power conversion at low-temperatures due to improved electronic, electrical and thermal properties of materials.

Activation energy of the low-load NaCl transition from nanoindentation loading curves.

PubMed

Kaupp, Gerd

2014-01-01

Access to activation energies E(a) of phase transitions is opened by unprecedented analyses of temperature dependent nanoindentation loading curves. It is based on kinks in linearized loading curves, with additional support by coincidence of kink and electrical conductivity of silicon loading curves. Physical properties of B1, B2, NaCl and further phases are discussed. The normalized low-load transition energy of NaCl (Wtrans/µN) increases with temperature and slightly decreases with load. Its semi-logarithmic plot versus T obtains activation energy E(a)/µN for calculation of the transition work for all interesting temperatures and pressures. Arrhenius-type activation energy (kJ/mol) is unavailable for indentation phase transitions. The E(a) per load normalization proves insensitive to creep-on-load, which excludes normalization to depth or volume for large temperature ranges. Such phase transition E(a)/µN is unprecedented material's property and will be of practical importance for the compatibility of composite materials under impact and further shearing interactions at elevated temperatures. © 2014 Wiley Periodicals, Inc.

Scaling of X pinches from 1 MA to 6 MA.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bland, Simon Nicholas; McBride, Ryan D.; Wenger, David Franklin

This final report for Project 117863 summarizes progress made toward understanding how X-pinch load designs scale to high currents. The X-pinch load geometry was conceived in 1982 as a method to study the formation and properties of bright x-ray spots in z-pinch plasmas. X-pinch plasmas driven by 0.2 MA currents were found to have source sizes of 1 micron, temperatures >1 keV, lifetimes of 10-100 ps, and densities >0.1 times solid density. These conditions are believed to result from the direct magnetic compression of matter. Physical models that capture the behavior of 0.2 MA X pinches predict more extreme parametersmore » at currents >1 MA. This project developed load designs for up to 6 MA on the SATURN facility and attempted to measure the resulting plasma parameters. Source sizes of 5-8 microns were observed in some cases along with evidence for high temperatures (several keV) and short time durations (<500 ps).« less

Effect of structural factors on mechanical properties of the magnesium alloy Ma2-1 under quasi-static and high strain rate deformation conditions

NASA Astrophysics Data System (ADS)

Garkushin, G. V.; Razorenov, S. V.; Krasnoveikin, V. A.; Kozulin, A. A.; Skripnyak, V. A.

2015-02-01

The elastic limit and tensile strength of deformed magnesium alloys Ma2-1 with different structures and textures were measured with the aim of finding a correlation between the spectrum of defects in the material and the resistance to deformation and fracture under quasi-static and dynamic loading conditions. The studies were performed using specimens in the as-received state after high-temperature annealing and specimens subjected to equal-channel angular pressing at a temperature of 250°C. The anisotropy of strength characteristics of the material after shock compression with respect to the direction of rolling of the original alloy was investigated. It was shown that, in contrast to the quasi-static loading conditions, under the shock wave loading conditions, the elastic limit and tensile strength of the magnesium alloy Ma2-1 after equal-channel angular pressing decrease as compared to the specimens in the as-received state.

Influence of engineered interfaces on residual stresses and mechanical response in metal matrix composites

NASA Technical Reports Server (NTRS)

Arnold, Steven M.; Wilt, Thomas E.

1992-01-01

Because of the inherent coefficient of thermal expansion (CTE) mismatch between fiber and matrix within metal and intermetallic matrix composite systems, high residual stresses can develop under various thermal loading conditions. These conditions include cooling from processing temperature to room temperature as well as subsequent thermal cycling. As a result of these stresses, within certain composite systems, radial, circumferential, and/or longitudinal cracks have been observed to form at the fiber matrix interface region. A number of potential solutions for reducing this thermally induced residual stress field have been proposed recently. Examples of some potential solutions are high CTE fibers, fiber preheating, thermal anneal treatments, and an engineered interface. Here the focus is on designing an interface (by using a compensating/compliant layer concept) to reduce or eliminate the thermal residual stress field and, therefore, the initiation and propagation of cracks developed during thermal loading. Furthermore, the impact of the engineered interface on the composite's mechanical response when subjected to isothermal mechanical load histories is examined.

Design Considerations for Ceramic Matrix Composite Vanes for High Pressure Turbine Applications

NASA Technical Reports Server (NTRS)

Boyle, Robert J.; Parikh, Ankur H.; Nagpal, Vinod K.; Halbig, Michael C.

2013-01-01

Issues associated with replacing conventional metallic vanes with Ceramic Matrix Composite (CMC) vanes in the first stage of the High Pressure Turbine (HPT) are explored. CMC materials have higher temperature capability than conventional HPT vanes, and less vane cooling is required. The benefits of less vane coolant are less NOx production and improved vane efficiency. Comparisons between CMC and metal vanes are made at current rotor inlet temperatures and at an vane inlet pressure of 50 atm.. CMC materials have directionally dependent strength characteristics, and vane designs must accommodate these characteristics. The benefits of reduced NOx and improved cycle efficiency obtainable from using CMC vanes. are quantified Results are given for vane shapes made of a two dimensional CMC weave. Stress components due to thermal and pressure loads are shown for all configurations. The effects on stresses of: (1) a rib connecting vane pressure and suction surfaces; (2) variation in wall thickness; and (3) trailing edge region cooling options are discussed. The approach used to obtain vane temperature distributions is discussed. Film cooling and trailing edge ejection were required to avoid excessive vane material temperature gradients. Stresses due to temperature gradients are sometimes compressive in regions where pressure loads result in high tensile stresses.

Rate constants for chemical reactions in high-temperature nonequilibrium air

NASA Technical Reports Server (NTRS)

Jaffe, R. L.

1986-01-01

In the nonequilibrium atmospheric chemistry regime that will be encountered by the proposed Aeroassisted Orbital Transfer Vehicle in the upper atmosphere, where air density is too low for thermal and chemical equilibrium to be maintained, the detailed high temperature air chemistry plays a critical role in defining radiative and convective heating loads. Although vibrational and electronic temperatures remain low (less than 15,000 K), rotational and translational temperatures may reach 50,000 K. Attention is presently given to the effects of multiple temperatures on the magnitudes of various chemical reaction rate constants, for the cases of both bimolecular exchange reactions and collisional excitation and dissociation reactions.

Experimental characterization of nonlinear, rate-dependent behavior in advanced polymer matrix composites

NASA Technical Reports Server (NTRS)

Gates, Thomas S.

1992-01-01

In order to support materials selection for the next-generation supersonic civilian-passenger transport aircraft, a study has been undertaken to evaluate the material stress/strain relationships needed to describe advanced polymer matrix composites under conditions of high load and elevated temperature. As part of this effort, this paper describes the materials testing which was performed to investigate the viscoplastic behavior of graphite/thermoplastic and graphite/bismaleimide composites. Test procedures, results and data-reduction schemes which were developed for generating material constants for tension and compression loading, over a range of useful temperatures, are explained.

Low-Flow Liquid Desiccant Air-Conditioning: Demonstrated Performance and Cost Implications

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kozubal, E.; Herrmann, L.; Deru, M.

2014-09-01

Cooling loads must be dramatically reduced when designing net-zero energy buildings or other highly efficient facilities. Advances in this area have focused primarily on reducing a building's sensible cooling loads by improving the envelope, integrating properly sized daylighting systems, adding exterior solar shading devices, and reducing internal heat gains. As sensible loads decrease, however, latent loads remain relatively constant, and thus become a greater fraction of the overall cooling requirement in highly efficient building designs, particularly in humid climates. This shift toward latent cooling is a challenge for heating, ventilation, and air-conditioning (HVAC) systems. Traditional systems typically dehumidify by firstmore » overcooling air below the dew-point temperature and then reheating it to an appropriate supply temperature, which requires an excessive amount of energy. Another dehumidification strategy incorporates solid desiccant rotors that remove water from air more efficiently; however, these systems are large and increase fan energy consumption due to the increased airside pressure drop of solid desiccant rotors. A third dehumidification strategy involves high flow liquid desiccant systems. These systems require a high maintenance separator to protect the air distribution system from corrosive desiccant droplet carryover and so are more commonly used in industrial applications and rarely in commercial buildings. Both solid desiccant systems and most high-flow liquid desiccant systems (if not internally cooled) add sensible energy which must later be removed to the air stream during dehumidification, through the release of sensible heat during the sorption process.« less

Control of Thermal Deflection, Panel Flutter and Acoustic Fatigue at Elevated Temperatures Using Shape Memory Alloys

NASA Technical Reports Server (NTRS)

Mei, Chuh; Huang, Jen-Kuang

1996-01-01

The High Speed Civil Transport (HSCT) will have to be designed to withstand high aerodynamic load at supersonic speeds (panel flutter) and high acoustic load (acoustic or sonic fatigue) due to fluctuating boundary layer or jet engine acoustic pressure. The thermal deflection of the skin panels will also alter the vehicle's configuration, thus it may affect the aerodynamic characteristics of the vehicle and lead to poor performance. Shape memory alloys (SMA) have an unique ability to recover large strains completely when the alloy is heated above the characteristic transformation (austenite finish T(sub f)) temperature. The recovery stress and elastic modulus are both temperature dependent, and the recovery stress also depends on the initial strain. An innovative concept is to utilize the recovery stress by embedding the initially strained SMA wire in a graphite/epoxy composite laminated panel. The SMA wires are thus restrained and large inplane forces are induced in the panel at elevated temeperatures. By embedding SMA in composite panel, the panel becomes much stiffer at elevated temperatures. That is because the large tensile inplane forces induced in the panel from the SMA recovery stress. A stiffer panel would certainly yield smaller dynamic responses.

Properties of immobile hydrogen confined in microporous carbon

DOE PAGES

Bahadur, Jitendra; Bhabha Atomic Research Centre; Contescu, Cristian I.; ...

2017-03-06

The mobility of H2 confined in microporous carbon was studied as a function of temperature and pressure using inelastic neutron scattering, and the translational and rotational motion of H2 molecules has been probed. At low loading, rotation of H2 molecules adsorbed in the smallest carbon pores (~6 ) is severely hindered, suggesting that the interaction between H2 and the host matrix is anisotropic. At higher loading, H2 molecules behave as nearly free rotor, implying lower anisotropic interactions with adsorption sites. At supercritical temperatures where bulk H2 is a gas, the inelastic spectrum of confined H2 provides evidence of a significantmore » fraction of immobile, solid-like hydrogen. The onset temperature for molecular mobility depends strongly on the loaded amount. The fraction of immobile molecules increases with pressure and attains a plateau at high pressures. Surprisingly, immobile H2 is present even at temperatures as high as ~110 K. This research at ORNL s Spallation Neutron Source was sponsored by the Scientific User Facilities Division, Office of Basic Energy Sciences, U. S. Department of Energy. This research was supported in part by the ORNL Postdoctoral Research Associates Program, administered jointly by the ORNL and the Oak Ridge Institute for Science and Education. CIC and NCG acknowledge support from the Materials Science and Engineering Division, Office of Basic Energy Sciences, U.S. Department of Energy.« less

Behaviour of Epoxy Silica Nanocomposites Under Static and Creep Loading

NASA Astrophysics Data System (ADS)

Constantinescu, Dan Mihai; Picu, Radu Catalin; Sandu, Marin; Apostol, Dragos Alexandru; Sandu, Adriana; Baciu, Florin

2017-12-01

Specific manufacturing technologies were applied for the fabrication of epoxy-based nanocomposites with silica nanoparticles. For dispersing the fillers in the epoxy resin special equipment such as a shear mixer and a high energy sonicator with temperature control were used. Both functionalized and unfunctionalized silica nanoparticles were added in three epoxy resins. The considered filling fraction was in most cases 0.1, 0.3 and 0.5 wt%.. The obtained nanocomposites were subjected to monotonic uniaxial and creep loading at room temperature. The static mechanical properties were not significantly improved regardless the filler percentage and type of epoxy resin. Under creep loading, by increasing the stress level, the nanocomposite with 0.1 wt% silica creeps less than all other materials. Also the creep rate is reduced by adding silica nanofillers.

A High-Sensitivity Hydraulic Load Cell for Small Kitchen Appliances

PubMed Central

Pačnik, Roman; Novak, Franc

2010-01-01

In this paper we present a hydraulic load cell made from hydroformed metallic bellows. The load cell was designed for a small kitchen appliance with the weighing function integrated into the composite control and protection of the appliance. It is a simple, low-cost solution with small dimensions and represents an alternative to the existing hydraulic load cells in industrial use. A good non-linearity and a small hysteresis were achieved. The influence of temperature leads to an error of 7.5%, which can be compensated for by software to meet the requirements of the target application. PMID:22163665

A high-sensitivity hydraulic load cell for small kitchen appliances.

PubMed

Pačnik, Roman; Novak, Franc

2010-01-01

In this paper we present a hydraulic load cell made from hydroformed metallic bellows. The load cell was designed for a small kitchen appliance with the weighing function integrated into the composite control and protection of the appliance. It is a simple, low-cost solution with small dimensions and represents an alternative to the existing hydraulic load cells in industrial use. A good non-linearity and a small hysteresis were achieved. The influence of temperature leads to an error of 7.5%, which can be compensated for by software to meet the requirements of the target application.

Evaluation of the microclimate in poultry transport module drawers during the marketing process of end-of-lay hens from farm to slaughter.

PubMed

Richards, G J; Wilkins, L J; Weeks, C A; Knowles, T G; Brown, S N

2012-11-10

Changes in module drawer temperature and relative humidity were monitored for 24 commercial loads of hens. Mathematical models revealed significant differences in predicted drawer temperature depending on their location and the outside environmental temperature. Higher predicted temperatures were found in uppermost drawers of the top modules at the front of the lorry, and lower temperatures in drawers on the outer sides of modules and in those drawers in modules next to the back of the lorry in both the upper and lower modules during transport. In the lairage, drawer temperature generally decreased, except in drawers at the top of modules where temperatures increased. Temperature increases were most often recorded in modules which had been located at the rear of the lorry, which were generally cooler during transport. End-of-lay hens would appear to be exposed to a greater risk of cold stress rather than heat stress in the UK. Inspection of birds during transport, or upon arrival, should be directed to the bottom and side drawers of a load when looking for cold stress, and the top row of drawers (centre) of the top modules when looking for heat stress. The frequency of inspections should increase at times of high ambient temperature while the birds are being held in lairages. Adjusting the numbers of birds loaded per drawer according to bird condition and weather appears to be an effective mitigation strategy which is already in use commercially.

Influence of gaseous hydrogen on metals

NASA Technical Reports Server (NTRS)

Walter, R. J.; Chandler, W. T.

1973-01-01

Tensile, fracture toughness, threshold stress intensity for sustained-load crack growth, and cyclic and sustained load crack growth rate measurements were performed on a number of alloys in high-pressure hydrogen and helium environments. The results of tensile tests performed in 34.5 MN/m2 (5000 psi) hydrogen indicated that Inconel 625 was considerable embrittled at ambient temperature but was not embrittled at 144 K (-200 F). The tensile properties of AISI 321 stainless steel were slightly reduced at ambient temperature and 144 K (-200 F). The tensile properties of Ti-5Al-2.5 Sn ELI were essentially unaffected by hydrogen at 144 K (-200 F). OFHC copper was not embrittled by hydrogen at ambient temperature or at 144 K (-200 F).

Ultrasound Velocity Measurements in High-Chromium Steel Under Plastic Deformation

NASA Astrophysics Data System (ADS)

Lunev, Aleksey; Bochkareva, Anna; Barannikova, Svetlana; Zuev, Lev

2016-04-01

In the present study, the variation of the propagation velocity of ultrasound in the plastic deformation of corrosion-resistant high-chromium steel 40X13 with ferrite-carbide (delivery status), martensitic (quenched) and sorbitol (after high-temperature tempering) structures have beem studied/ It is found that each state shows its view of the loading curve. In the delivery state diagram loading is substantially parabolic throughout, while in the martensitic state contains only linear strain hardening step and in the sorbitol state the plastic flow curve is three-step. The velocity of ultrasonic surface waves (Rayleigh waves) was measured simultaneously with the registration of the loading curve in the investigated steel in tension. It is shown that the dependence of the velocity of ultrasound in active loading is determined by the law of plastic flow, that is, the staging of the corresponding diagram of loading. Structural state of the investigated steel is not only changing the type of the deformation curve under uniaxial tension, but also changes the nature of ultrasound speed of deformation.

An Evaluation of High Temperature Airframe Seals for Advanced Hypersonic Vehicles

NASA Technical Reports Server (NTRS)

DeMange, Jeffrey J.; Dunlap, Patrick H.; Steinetz, Bruce M.; Drlik, Gary J.

2007-01-01

High temperature seals are required for advanced hypersonic airframe applications. In this study, both spring tube thermal barriers and innovative wafer seal systems were evaluated under relevant hypersonic test conditions (temperatures, pressures, etc.) via high temperature compression testing and room temperature flow assessments. Thermal barriers composed of a Rene 41 spring tube filled with Saffil insulation and overbraided with a Nextel 312 sheath showed acceptable performance at 1500 F in both short term and longer term compression testing. Nextel 440 thermal barriers with Rene 41 spring tubes and Saffil insulation demonstrated good compression performance up to 1750 F. A silicon nitride wafer seal/compression spring system displayed excellent load performance at temperatures as high as 2200 F and exhibited room temperature leakage values that were only 1/3 those for the spring tube rope seals. For all seal candidates evaluated, no significant degradation in leakage resistance was noted after high temperature compression testing. In addition to these tests, a superalloy seal suitable for dynamic seal applications was optimized through finite element techniques.

Improved Polyurethane Storage Tank Performance

DTIC Science & Technology

2010-12-15

determined through testing that the initial weld adhesion and weld adhesion after high temperature fuel (HTF) immersion have a linear relationship ...Unfortunately, the relationship between HTF weld adhesion and HTF dead- load performance is not as predictive. From 30 to approximately 45 lbsf/inch...consequently, will handle a higher ( theoretically double) shear load. This weld joint is currently being used to fabricate collapsible fuel tanks

The effect of temperature and loading frequency on the converse piezoelectric response of soft PZT ceramics

NASA Astrophysics Data System (ADS)

Dapeng, Zhu; Qinghui, Jiang; Yingwei, Li

2017-12-01

The converse piezoelectric coefficient d 33 of soft PZT ceramics was measured from 20 °C to 150 °C under different loading frequency. Results showed that in the tested temperature range, the evolution of d 33 obeys the Rayleigh-law behavior. The influence of temperature on d 33 is a little complicated. For instance, the maximum d 33 was observed at 150 °C when the applied electric field E was at 0.1 kV mm-1. When E increased to 0.3 kV mm-1 and 0.4 kV mm-1, the maximum d 33 was observed at 120 °C and 100 °C, respectively. Such behaviors are rationalized by the evolution of the Rayleigh parameters d init and α. For d init, it increases as temperature increases. While for α, it first increases and then decreases with the increase of temperature due to the evolution of the spontaneous strain and the volume of the switched domains. In the tested loading frequency, d 33 decreased linearly with the logarithm of the frequency of electric field. With the increase of temperature, the influence of frequency on d 33 gradually weakened, implying that at high temperature, the motion of domain walls became active and the pinning effect of defects nearly disappeared.

Pyrolysis of polyethylene terephthalate containing real waste plastics using Ni loaded zeolite catalysts

NASA Astrophysics Data System (ADS)

Al-asadi, M.; Miskolczi, N.

2018-05-01

In this work the pyrolysis of polyethylene terephthalate (PET) containing real waste plastic was investigated using different Ni loaded catalysts: Ni/ZSM-5, Ni/y-zeolite, Ni/β-zeolite and Ni/natural zeolite (clinoptilolite). Raw materials were pyrolyzed in a horizontal tubular reactor between 600 and 900°C using 10% of catalysts. It was found, that both temperature increasing and catalysts presence can increase the gas yields, however owing to gasification reactions, the pyrolysis oil yield decreased with increasing temperature. Ni/y-zeolite catalyst had the most benefit in gas yield increasing at low temperature; however Ni/ZSM-5 showed advanced property in gas yield increasing at high temperature. Gases contained hydrogen, carbon oxides and hydrocarbons, which composition was significantly affected by catalysts. Ni loaded zeolites favoured to the formation of hydrogen and branched hydrocarbons; furthermore the concentrations of both CO and CO2 were also increased as function of elevated temperature. That phenomenon was attributed to the further decomposition of PET, especially to the side chain scission reactions. Owing to the Boudouard reaction, the ratio of CO2/CO can increased with temperature. Pyrolysis oils were the mixtures of n-saturated, n-unsaturated, branched, oxygen free aromatics and oxygenated hydrocarbons. Temperature increasing has a significant effect to the aromatization and isomerization reactions, while the catalysts can efficiently decreased the concentration of oxygen containing compounds.

Advanced Software for Analysis of High-Speed Rolling-Element Bearings

NASA Technical Reports Server (NTRS)

Poplawski, J. V.; Rumbarger, J. H.; Peters, S. M.; Galatis, H.; Flower, R.

2003-01-01

COBRA-AHS is a package of advanced software for analysis of rigid or flexible shaft systems supported by rolling-element bearings operating at high speeds under complex mechanical and thermal loads. These loads can include centrifugal and thermal loads generated by motions of bearing components. COBRA-AHS offers several improvements over prior commercial bearing-analysis programs: It includes innovative probabilistic fatigue-life-estimating software that provides for computation of three-dimensional stress fields and incorporates stress-based (in contradistinction to prior load-based) mathematical models of fatigue life. It interacts automatically with the ANSYS finite-element code to generate finite-element models for estimating distributions of temperature and temperature-induced changes in dimensions in iterative thermal/dimensional analyses: thus, for example, it can be used to predict changes in clearances and thermal lockup. COBRA-AHS provides an improved graphical user interface that facilitates the iterative cycle of analysis and design by providing analysis results quickly in graphical form, enabling the user to control interactive runs without leaving the program environment, and facilitating transfer of plots and printed results for inclusion in design reports. Additional features include roller-edge stress prediction and influence of shaft and housing distortion on bearing performance.

Advanced thermal energy management: A thermal test bed and heat pipe simulation

NASA Technical Reports Server (NTRS)

Barile, Ronald G.

1986-01-01

Work initiated on a common-module thermal test simulation was continued, and a second project on heat pipe simulation was begun. The test bed, constructed from surplus Skylab equipment, was modeled and solved for various thermal load and flow conditions. Low thermal load caused the radiator fluid, Coolanol 25, to thicken due to its temperature avoided by using a regenerator-heat-exchanger. Other possible solutions modeled include a radiator heater and shunting heat from the central thermal bus to the radiator. Also, module air temperature can become excessive with high avionics load. A second preoject concerning advanced heat pipe concepts was initiated. A program was written which calculates fluid physical properties, liquid and vapor pressure in the evaporator and condenser, fluid flow rates, and thermal flux. The program is directed to evaluating newer heat pipe wicks and geometries, especially water in an artery surrounded by six vapor channels. Effects of temperature, groove and slot dimensions, and wick properties are reported.

Performance comparison of single-stage mixed-refrigerant Joule-Thomson cycle and reverse Brayton cycle for cooling 80 to 120 K temperature-distributed heat loads

NASA Astrophysics Data System (ADS)

Wang, H. C.; Chen, G. F.; Gong, M. Q.; Li, X.

2017-12-01

Thermodynamic performance comparison of single-stage mixed-refrigerant Joule-Thomson cycle (MJTR) and pure refrigerant reverse Brayton cycle (RBC) for cooling 80 to 120 K temperature-distributed heat loads was conducted in this paper. Nitrogen under various liquefaction pressures was employed as the heat load. The research was conducted under nonideal conditions by exergy analysis methods. Exergy efficiency and volumetric cooling capacity are two main evaluation parameters. Exergy loss distribution in each process of refrigeration cycle was also investigated. The exergy efficiency and volumetric cooling capacity of MJTR were obviously superior to RBC in 90 to 120 K temperature zone, but still inferior to RBC at 80 K. The performance degradation of MJTR was caused by two main reasons: The high fraction of neon resulted in large entropy generation and exergy loss in throttling process. Larger duty and WLMTD lead to larger exergy losses in recuperator.

Friction Stir Welding of Al-Cu Bilayer Sheet by Tapered Threaded Pin: Microstructure, Material Flow, and Fracture Behavior

NASA Astrophysics Data System (ADS)

Beygi, R.; Kazeminezhad, M.; Kokabi, A. H.; Loureiro, A.

2015-06-01

The fracture behavior and intermetallic formation are investigated after friction stir welding of Al-Cu bilayer sheets performed by tapered threaded pin. To do so, temperature, axial load, and torque measurements during welding, and also SEM and XRD analyses and tensile tests on the welds are carried out. These observations show that during welding from Cu side, higher axial load and temperature lead to formation of different kinds of Al-Cu intermetallics such as Al2Cu, AlCu, and Al4Cu9. Also, existence of Al(Cu)-Al2Cu eutectic structures, demonstrates liquation during welding. The presence of these intermetallics leads to highly brittle fracture and low strength of the joints. In samples welded from Al side, lower axial load and temperature are developed during welding and no intermetallic compound is observed which results in higher strength and ductility of the joints in comparison with those welded from Cu side.

Temperature Dependent Modal Test/Analysis Correlation of X-34 Fastrac Composite Rocket Nozzle

NASA Technical Reports Server (NTRS)

Brown, Andrew M.; Brunty, Joseph A. (Technical Monitor)

2001-01-01

A unique high temperature modal test and model correlation/update program has been performed on the composite nozzle of the FASTRAC engine for the NASA X-34 Reusable Launch Vehicle. The program was required to provide an accurate high temperature model of the nozzle for incorporation into the engine system structural dynamics model for loads calculation; this model is significantly different from the ambient case due to the large decrease in composite stiffness properties due to heating. The high-temperature modal test was performed during a hot-fire test of the nozzle. Previously, a series of high fidelity modal tests and finite element model correlation of the nozzle in a free-free configuration had been performed. This model was then attached to a modal-test verified model of the engine hot-fire test stand and the ambient system mode shapes were identified. A reduced set of accelerometers was then attached to the nozzle, the engine fired full-duration, and the frequency peaks corresponding to the ambient nozzle modes individually isolated and tracked as they decreased during the test. To update the finite-element model of the nozzle to these frequency curves, the percentage differences of the anisotropic composite moduli due to temperature variation from ambient, which had been used in the initial modeling and which were obtained by small sample coupon testing, were multiplied by an iteratively determined constant factor. These new properties were used to create high-temperature nozzle models corresponding to 10 second engine operation increments and tied into the engine system model for loads determination.

Design and Operating Characteristics of High-Speed, Small-Bore, Angular-Contact Ball Bearings

NASA Technical Reports Server (NTRS)

Pinel, Stanley I.; Signer, Hans R.; Zaretsky, Erwin V.

1998-01-01

The computer program SHABERTH was used to analyze 35-mm-bore, angular-contact ball bearings designed and manufactured for high-speed turbomachinery applications. Parametric tests of the bearings were conducted on a high-speed, high-temperature bearing tester and were compared with the computer predictions. Four bearing and cage designs were studied. The bearings were lubricated either by jet lubrication or through the split inner ring with and without outer-ring cooling. The predicted bearing life decreased with increasing speed because of increased operating contact stresses caused by changes in contact angle and centrifugal load. For thrust loads only, the difference in calculated life for the 24 deg. and 30 deg. contact-angle bearings was insignificant. However, for combined loading, the 24 deg. contact-angle bearing gave longer life. For split-inner-ring bearings, optimal operating conditions were obtained with a 24 deg. contact angle and an inner-ring, land-guided cage, using outer-ring cooling in conjunction with low lubricant flow rates. Lower temperature and power losses were obtained with a single-outer-ring, land-guided cage for the 24 deg. contact-angle bearing having a relieved inner ring and partially relieved outer ring. Inner-ring temperatures were independent of lubrication mode and cage design. In comparison with measured values, reasonably good engineering correlation was obtained using the computer program SHABERTH for predicted bearing power loss and for inner- and outer-ring temperatures. The Parker formula for XCAV (used in SHABERTH, a measure of oil volume in the bearing cavity) may need to be refined to reflect bearing lubrication mode, cage design, and location of cage-controlling land.

Methods for structural design at elevated temperatures

NASA Technical Reports Server (NTRS)

Ellison, A. M.; Jones, W. E., Jr.; Leimbach, K. R.

1973-01-01

A procedure which can be used to design elevated temperature structures is discussed. The desired goal is to have the same confidence in the structural integrity at elevated temperature as the factor of safety gives on mechanical loads at room temperature. Methods of design and analysis for creep, creep rupture, and creep buckling are presented. Example problems are included to illustrate the analytical methods. Creep data for some common structural materials are presented. Appendix B is description, user's manual, and listing for the creep analysis program. The program predicts time to a given creep or to creep rupture for a material subjected to a specified stress-temperature-time spectrum. Fatigue at elevated temperature is discussed. Methods of analysis for high stress-low cycle fatigue, fatigue below the creep range, and fatigue in the creep range are included. The interaction of thermal fatigue and mechanical loads is considered, and a detailed approach to fatigue analysis is given for structures operating below the creep range.

The effect of dryer load on freeze drying process design.

PubMed

Patel, Sajal M; Jameel, Feroz; Pikal, Michael J

2010-10-01

Freeze-drying using a partial load is a common occurrence during the early manufacturing stages when insufficient amounts of active pharmaceutical ingredient (API) are available. In such cases, the immediate production needs are met by performing lyophilization with less than a full freeze dryer load. However, it is not obvious at what fractional load significant deviations from full load behavior begin. The objective of this research was to systematically study the effects of variation in product load on freeze drying behavior in laboratory, pilot and clinical scale freeze-dryers. Experiments were conducted with 5% mannitol (high heat and mass flux) and 5% sucrose (low heat and mass flux) at different product loads (100%, 50%, 10%, and 2%). Product temperature was measured in edge as well as center vials with thermocouples. Specific surface area (SSA) was measured by BET gas adsorption analysis and residual moisture was measured by Karl Fischer. In the lab scale freeze-dryer, the molar flux of inert gas was determined by direct flow measurement using a flowmeter and the molar flux of water vapor was determined by manometric temperature measurement (MTM) and tunable diode laser absorption spectroscopy (TDLAS) techniques. Comparative pressure measurement (capacitance manometer vs. Pirani) was used to determine primary drying time. For both 5% mannitol and 5% sucrose, primary drying time decreases and product temperature increases as the load on the shelves decreases. No systematic variation was observed in residual moisture and vapor composition as load decreased. Further, SSA data suggests that there are no significant freezing differences under different load conditions. Independent of dryer scale, among all the effects, variation in radiation heat transfer from the chamber walls to the product seems to be the dominant effect resulting in shorter primary drying time as the load on the shelf decreases (i.e., the fraction of edge vials increases).

Management of Local Stressors Can Improve the Resilience of Marine Canopy Algae to Global Stressors

PubMed Central

Strain, Elisabeth M. A.; van Belzen, Jim; van Dalen, Jeroen; Bouma, Tjeerd J.; Airoldi, Laura

2015-01-01

Coastal systems are increasingly threatened by multiple local anthropogenic and global climatic stressors. With the difficulties in remediating global stressors, management requires alternative approaches that focus on local scales. We used manipulative experiments to test whether reducing local stressors (sediment load and nutrient concentrations) can improve the resilience of foundation species (canopy algae along temperate rocky coastlines) to future projected global climate stressors (high wave exposure, increasing sea surface temperature), which are less amenable to management actions. We focused on Fucoids (Cystoseira barbata) along the north-western Adriatic coast in the Mediterranean Sea because of their ecological relevance, sensitivity to a variety of human impacts, and declared conservation priority. At current levels of sediment and nutrients, C. barbata showed negative responses to the simulated future scenarios of high wave exposure and increased sea surface temperature. However, reducing the sediment load increased the survival of C. barbata recruits by 90.24% at high wave exposure while reducing nutrient concentrations resulted in a 20.14% increase in the survival and enhanced the growth of recruited juveniles at high temperature. We conclude that improving water quality by reducing nutrient concentrations, and particularly the sediment load, would significantly increase the resilience of C. barbata populations to projected increases in climate stressors. Developing and applying appropriate targets for specific local anthropogenic stressors could be an effective management action to halt the severe and ongoing loss of key marine habitats. PMID:25807516

Advanced Electrical Materials and Components Being Developed

NASA Technical Reports Server (NTRS)

Schwarze, Gene E.

2004-01-01

All aerospace systems require power management and distribution (PMAD) between the energy and power source and the loads. The PMAD subsystem can be broadly described as the conditioning and control of unregulated power from the energy source and its transmission to a power bus for distribution to the intended loads. All power and control circuits for PMAD require electrical components for switching, energy storage, voltage-to-current transformation, filtering, regulation, protection, and isolation. Advanced electrical materials and component development technology is a key technology to increasing the power density, efficiency, reliability, and operating temperature of the PMAD. The primary means to develop advanced electrical components is to develop new and/or significantly improved electronic materials for capacitors, magnetic components, and semiconductor switches and diodes. The next important step is to develop the processing techniques to fabricate electrical and electronic components that exceed the specifications of presently available state-of-the-art components. The NASA Glenn Research Center's advanced electrical materials and component development technology task is focused on the following three areas: 1) New and/or improved dielectric materials for the development of power capacitors with increased capacitance volumetric efficiency, energy density, and operating temperature; 2) New and/or improved high-frequency, high-temperature soft magnetic materials for the development of transformers and inductors with increased power density, energy density, electrical efficiency, and operating temperature; 3) Packaged high-temperature, high-power density, high-voltage, and low-loss SiC diodes and switches.

Numerical Stress Analysis during Cooldown and Compressive Loading in an Imperfect Nb 3Sn Wire

DOE Office of Scientific and Technical Information (OSTI.GOV)

d’Hauthuille, Luc; Zhai, Yuhu

In this paper, high field superconductors are critical to the success of next step magnetic fusion confinement devices such as ITER and DEMO. The low-temperature superconducting material that is currently favored for these applications, Nb 3Sn, is susceptible to performance due to its brittleness and high strain-sensitivity. Under extreme loads, an irreversible degradation in the maximum critical current density has been shown to occur and believed to be strongly influenced by two factors: plasticity and cracked filaments. Cracks in filaments are induced when sufficiently high stress concentrations occur in the wire. In this paper, we explore using finite element analysismore » the impact that voids have on the stress distributions and peak stresses under two loading conditions: transverse compressive loading in a 2D model, and a full cool down phase in a 3D model.« less

Numerical Stress Analysis during Cooldown and Compressive Loading in an Imperfect Nb 3Sn Wire

DOE PAGES

d’Hauthuille, Luc; Zhai, Yuhu

2017-07-11

In this paper, high field superconductors are critical to the success of next step magnetic fusion confinement devices such as ITER and DEMO. The low-temperature superconducting material that is currently favored for these applications, Nb 3Sn, is susceptible to performance due to its brittleness and high strain-sensitivity. Under extreme loads, an irreversible degradation in the maximum critical current density has been shown to occur and believed to be strongly influenced by two factors: plasticity and cracked filaments. Cracks in filaments are induced when sufficiently high stress concentrations occur in the wire. In this paper, we explore using finite element analysismore » the impact that voids have on the stress distributions and peak stresses under two loading conditions: transverse compressive loading in a 2D model, and a full cool down phase in a 3D model.« less

Gas loading apparatus for the Paris-Edinburgh press

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bocian, A.; Kamenev, K. V.; Bull, C. L.

2010-09-15

We describe the design and operation of an apparatus for loading gases into the sample volume of the Paris-Edinburgh press at room temperature and high pressure. The system can be used for studies of samples loaded as pure or mixed gases as well as for loading gases as pressure-transmitting media in neutron-scattering experiments. The apparatus consists of a high-pressure vessel and an anvil holder with a clamp mechanism. The vessel, designed to operate at gas pressures of up to 150 MPa, is used for applying the load onto the anvils located inside the clamp. This initial load is sufficient formore » sealing the pressurized gas inside the sample containing gasket. The clamp containing the anvils and the sample is then transferred into the Paris-Edinburgh press by which further load can be applied to the sample. The clamp has apertures for scattered neutron beams and remains in the press for the duration of the experiment. The performance of the gas loading system is illustrated with the results of neutron-diffraction experiments on compressed nitrogen.« less

Pilot-scale studies on biological treatment of hypersaline wastewater at low temperature.

PubMed

Peng, Y Z; Zhu, G B; Wang, S Y; Yu, D S; Cui, Y W; Meng, X S

2005-01-01

In order to investigate the feasibility of biological treatment of hypersaline wastewater produced from toilet flushing with seawater at low temperature, pilot-scale studies were established with plug-flow activated sludge process at low temperature (5-9 degrees C) based on bench-scale experiments. The critical salinity concentration of 30 g/L, which resulted from the cooperation results of the non-halophilic bacteria and the halophilic bacteria, was drawn in bench-scale experiments. Pilot-scale studies showed that high COD removal efficiency, higher than 80%, was obtained at low temperature when 30 percent seawater was introduced. The salinity improved the settleability of activated sludge, and average sludge value dropped down from 38% to 22.5% after adding seawater. Seawater salinity had a strong negative effect on notronomonas and nitrobacter growth, but much more on the nitrobacter. The nitrification action was mainly accomplished by nitrosomonas. Bench-scale experiments using two SBRs were carried out for further investigation under different conditions of salinities, ammonia loadings and temperatures. Biological nitrogen removal via nitrite pathway from wastewater containing 30 percent seawater was achieved, but the ammonia removal efficiency was strongly related not only to the influent ammonia loading at different salinities but also to temperature. When the ratio of seawater to wastewater was 30 percent, and the ammonia loading was below the critical value of 0.15 kgNH4+-N/(kgMLSS.d), the ammonia removal efficiency via nitrite pathway was above 90%. The critical level of ammonia loading was 0.15, 0.08 and 0.03 kgNH4+-N/(kgMLSS.d) respectively at the different temperature 30 degrees C, 25 degrees C and 20 degrees C when the influent ammonia concentration was 60-80 mg/L and pH was 7.5-8.0.

T4 bacteriophage conjugated magnetic particles for E. coli capturing: Influence of bacteriophage loading, temperature and tryptone.

PubMed

Liana, Ayu Ekajayanthi; Marquis, Christopher P; Gunawan, Cindy; Gooding, J Justin; Amal, Rose

2017-03-01

This work demonstrates the use of bacteriophage conjugated magnetic particles (Fe 3 O 4 ) for the rapid capturing and isolation of Escherichia coli. The investigation of T4 bacteriophage adsorption to silane functionalised Fe 3 O 4 with amine (NH 2 ), carboxylic (COOH) and methyl (CH 3 ) surface functional groups reveals the domination of net electrostatic and hydrophobic interactions in governing bacteriophage adsorption. The bare Fe 3 O 4 and Fe 3 O 4 -NH 2 with high T4 loading captured 3-fold more E. coli (∼70% capturing efficiency) compared to the low loading T4 on Fe 3 O 4 -COOH, suggesting the significance of T4 loading in E. coli capturing efficiency. Importantly, it is further revealed that E. coli capture is highly dependent on the incubation temperature and the presence of tryptone in the media. Effective E. coli capturing only occurs at 37°C in tryptone-containing media with the absence of either conditions resulted in poor bacteria capture. The incubation temperature dictates the capturing ability of Fe 3 O 4 /T4, whereby T4 and E. coli need to establish an irreversible binding that occurred at 37°C. The presence of tryptophan-rich tryptone in the suspending media was also critical, as shown by a 3-fold increase in E. coli capture efficiency of Fe 3 O 4 /T4 in tryptone-containing media compared to that in tryptone-free media. This highlights for the first time that successful bacteria capturing requires not only an optimum tailoring of the particle's surface physicochemical properties for favourable bacteriophage loading, but also an in-depth understanding of how factors, such as temperature and solution chemistry influence the subsequent bacteriophage-bacteria interactions. Copyright © 2016 Elsevier B.V. All rights reserved.

A high-speed, eight-wavelength visible light-infrared pyrometer for shock physics experiments

NASA Astrophysics Data System (ADS)

Wang, Rongbo; Li, Shengfu; Zhou, Weijun; Luo, Zhen-Xiong; Meng, Jianhua; Tian, Jianhua; He, Lihua; Cheng, Xianchao

2017-09-01

An eight-channel, high speed pyrometer for precise temperature measurement is designed and realized in this work. The addition of longer-wavelength channels sensitive at lower temperatures highly expands the measured temperature range, which covers the temperature of interest in shock physics from 1500K-10000K. The working wavelength range is 400-1700nm from visible light to near-infrared (NIR). Semiconductor detectors of Si and InGaAs are used as photoelectric devices, whose bandwidths are 50MHz and 150MHz respectively. Benefitting from the high responsivity and high speed of detectors, the time resolution of the pyrometer can be smaller than 10ns. By combining the high-transmittance beam-splitters and narrow-bandwidth filters, the peak spectrum transmissivity of each channel can be higher than 60%. The gray-body temperatures of NaI crystal under shock-loading are successfully measured by this pyrometer.

Pressure-induced critical influences on workpiece-tool thermal interaction in high speed dry machining of titanium

NASA Astrophysics Data System (ADS)

Abdel-Aal, H. A.; Mansori, M. El

2012-12-01

Cutting tools are subject to extreme thermal and mechanical loads during operation. The state of loading is intensified in dry cutting environment especially when cutting the so called hard-to-cut-materials. Although, the effect of mechanical loads on tool failure have been extensively studied, detailed studies on the effect of thermal dissipation on the deterioration of the cutting tool are rather scarce. In this paper we study failure of coated carbide tools due to thermal loading. The study emphasizes the role assumed by the thermo-physical properties of the tool material in enhancing or preventing mass attrition of the cutting elements within the tool. It is shown that within a comprehensive view of the nature of conduction in the tool zone, thermal conduction is not solely affected by temperature. Rather it is a function of the so called thermodynamic forces. These are the stress, the strain, strain rate, rate of temperature rise, and the temperature gradient. Although that within such consideration description of thermal conduction is non-linear, it is beneficial to employ such a form because it facilitates a full mechanistic understanding of thermal activation of tool wear.

Evaluating Moisture Control of Variable-Capacity Heat Pumps in Mechanically Ventilated, Low-Load Homes in Climate Zone 2A

DOE Office of Scientific and Technical Information (OSTI.GOV)

Martin, Eric; Withers, Chuck; McIlvaine, Janet

The well-sealed, highly insulated building enclosures constructed by today's home building industry coupled with efficient lighting and appliances are achieving significantly reduced heating and cooling loads. These low-load homes can present a challenge when selecting appropriate space-conditioning equipment. Conventional, fixed-capacity heating and cooling equipment is often oversized for small homes, causing increased first costs and operating costs. Even if fixed-capacity equipment can be properly specified for peak loads, it remains oversized for use during much of the year. During these part-load cooling hours, oversized equipment meets the target dry-bulb temperatures very quickly, often without sufficient opportunity for moisture control. Themore » problem becomes more acute for high-performance houses in humid climates when meeting ASHRAE Standard 62.2 recommendations for wholehouse mechanical ventilation.« less

High Efficiency, High Performance Clothes Dryer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Peter Pescatore; Phil Carbone

This program covered the development of two separate products; an electric heat pump clothes dryer and a modulating gas dryer. These development efforts were independent of one another and are presented in this report in two separate volumes. Volume 1 details the Heat Pump Dryer Development while Volume 2 details the Modulating Gas Dryer Development. In both product development efforts, the intent was to develop high efficiency, high performance designs that would be attractive to US consumers. Working with Whirlpool Corporation as our commercial partner, TIAX applied this approach of satisfying consumer needs throughout the Product Development Process for bothmore » dryer designs. Heat pump clothes dryers have been in existence for years, especially in Europe, but have not been able to penetrate the market. This has been especially true in the US market where no volume production heat pump dryers are available. The issue has typically been around two key areas: cost and performance. Cost is a given in that a heat pump clothes dryer has numerous additional components associated with it. While heat pump dryers have been able to achieve significant energy savings compared to standard electric resistance dryers (over 50% in some cases), designs to date have been hampered by excessively long dry times, a major market driver in the US. The development work done on the heat pump dryer over the course of this program led to a demonstration dryer that delivered the following performance characteristics: (1) 40-50% energy savings on large loads with 35 F lower fabric temperatures and similar dry times; (2) 10-30 F reduction in fabric temperature for delicate loads with up to 50% energy savings and 30-40% time savings; (3) Improved fabric temperature uniformity; and (4) Robust performance across a range of vent restrictions. For the gas dryer development, the concept developed was one of modulating the gas flow to the dryer throughout the dry cycle. Through heat modulation in a gas dryer, significant time and energy savings, combined with dramatically reduced fabric temperatures, was achieved in a cost-effective manner. The key design factor lay in developing a system that matches the heat input to the dryer with the fabrics ability to absorb it. The development work done on the modulating gas dryer over the course of this program led to a demonstration dryer that delivered the following performance characteristics: (1) Up to 25% reduction in energy consumption for small and medium loads; (2) Up to 35% time savings for large loads with 10-15% energy reduction and no adverse effect on cloth temperatures; (3) Reduced fabric temperatures, dry times and 18% energy reduction for delicate loads; and, (4) Robust performance across a range of vent restrictions.« less

Design and Development of a Series Switch for High Voltage in RF Heating

NASA Astrophysics Data System (ADS)

Patel, Himanshu K.; Shah, Deep; Thacker, Mauli; Shah, Atman

2013-02-01

Plasma is the fourth state of matter. To sustain plasma in its ionic form very high temperature is essential. RF heating systems are used to provide the required temperature. Arching phenomenon in these systems can cause enormous damage to the RF tube. Heavy current flows across the anode-cathode junction, which need to be suppressed in minimal time for its protection. Fast-switching circuit breakers are used to cut-off the load from the supply in cases of arching. The crowbar interrupts the connection between the high voltage power supply (HVPS) and the RF tube for a temporary period between which the series switch has to open. The crowbar shunts the current across the load but in the process leads to short circuiting the HVPS. Thus, to protect the load as well as the HVPS a series switch is necessary. This paper presents the design and development of high voltage Series Switch for the high power switching applications. Fiber optic based Optimum triggering scheme is designed and tested to restrict the time delay well within the stipulated limits. The design is well supported with the experimental results for the whole set-up along with the series switch at various voltage level before its approval for operation at 5.2 kV.

A Review of Fatigue Crack Growth of Pressure Vessel and Piping Steels in High-Temperature, Pressurized Reactor-Grade Water.

DTIC Science & Technology

1980-09-19

ratio, irradiation, materials Germany Kraftwerk Union Materials, temperature, Erlangen, Germany load ratio, frequency, electro- chemical potential Italy...H. Munster, "Frequenzeinfluss auf das Risswachstumsverhalten des Stahles 22NiMoCr37", KWU/R 413/8/80, Kraftwerk Union, Erlangen (1980). 76. D. F

An experimental and modeling study investigating the ignition delay in a military diesel engine running hexadecane (cetane) fuel

DOE PAGES

Cowart, Jim S.; Fischer, Warren P.; Hamilton, Leonard J.; ...

2013-02-01

In an effort aimed at predicting the combustion behavior of a new fuel in a conventional diesel engine, cetane (n-hexadecane) fuel was used in a military engine across the entire speed–load operating range. The ignition delay was characterized for this fuel at each operating condition. A chemical ignition delay was also predicted across the speed–load range using a detailed chemical kinetic mechanism with a constant pressure reactor model. At each operating condition, the measured in-cylinder pressure and predicted temperature at the start of injection were applied to the detailed n-hexadecane kinetic mechanism, and the chemical ignition delay was predicted withoutmore » any kinetic mechanism calibration. The modeling results show that fuel–air parcels developed from the diesel spray with an equivalence ratio of 4 are the first to ignite. The chemical ignition delay results also showed decreasing igntion delays with increasing engine load and speed, just as the experimental data revealed. At lower engine speeds and loads, the kinetic modeling results show the characteristic two-stage negative temperature coefficient behavior of hydrocarbon fuels. However, at high engine speeds and loads, the reactions do not display negative temperature coefficient behavior, as the reactions proceed directly into high-temperature pathways due to higher temperatures and pressure at injection. A moderate difference between the total and chemical ignition delays was then characterized as a phyical delay period that scales inversely with engine speed. This physical delay time is representative of the diesel spray development time and is seen to become a minority fraction of the total igntion delay at higher engine speeds. In addition, the approach used in this study suggests that the ignition delay and thus start of combustion may be predicted with reasonable accuracy using kinetic modeling to determine the chemical igntion delay. Then, in conjunction with the physical delay time (experimental or modeling based), a new fuel’s acceptability in a conventional engine could be assessed by determining that the total ignition delay is not too short or too long.« less

Fatigue behavior and life prediction of a SiC/Ti-24Al-11Nb composite under isothermal conditions. Ph.D. Thesis

NASA Technical Reports Server (NTRS)

Bartolotta, Paul A.

1991-01-01

Metal Matrix Composites (MMC) and Intermetallic Matrix Composites (IMC) were identified as potential material candidates for advanced aerospace applications. They are especially attractive for high temperature applications which require a low density material that maintains its structural integrity at elevated temperatures. High temperature fatigue resistance plays an important role in determining the structural integrity of the material. This study attempts to examine the relevance of test techniques, failure criterion, and life prediction as they pertain to an IMC material, specifically, unidirectional SiC fiber reinforced titanium aluminide. A series of strain and load controlled fatigue tests were conducted on unidirectional SiC/Ti-24Al-11Nb composite at 425 and 815 C. Several damage mechanism regimes were identified by using a strain-based representation of the data, Talreja's fatigue life diagram concept. Results of these tests were then used to address issues of test control modes, definition of failure, and testing techniques. Finally, a strain-based life prediction method was proposed for an IMC under tensile cyclic loadings at elevated temperatures.

Characterization of Ternary NiTiPd High-Temperature Shape-Memory Alloys under Load-Biased Thermal Cycling

NASA Technical Reports Server (NTRS)

Bigelow, Glen S.; Padula, Santo A.; Noebe, Ronald D.; Garg, Anita; Gaydosh, Darrell

2010-01-01

While NiTiPd alloys have been extensively studied for proposed use in high-temperature shape-memory applications, little is known about the shape-memory response of these materials under stress. Consequently, the isobaric thermal cyclic responses of five (Ni,Pd)49.5Ti50.5 alloys with constant stoichiometry and Pd contents ranging from 15 to 46 at. pct were investigated. From these tests, transformation temperatures, transformation strain (which is proportional to work output), and unrecovered strain per cycle (a measure of dimensional instability) were determined as a function of stress for each alloy. It was found that increasing the Pd content over this range resulted in a linear increase in transformation temperature, as expected. At a given stress level, work output decreased while the amount of unrecovered strain produced during each load-biased thermal cycle increased with increasing Pd content, during the initial thermal cycles. However, continued thermal cycling at constant stress resulted in a saturation of the work output and nearly eliminated further unrecovered strain under certain conditions, resulting in stable behavior amenable to many actuator applications.

Development of a Numerical Model for High-Temperature Shape Memory Alloys

NASA Technical Reports Server (NTRS)

DeCastro, Jonathan A.; Melcher, Kevin J.; Noebe, Ronald D.; Gaydosh, Darrell J.

2006-01-01

A thermomechanical hysteresis model for a high-temperature shape memory alloy (HTSMA) actuator material is presented. The model is capable of predicting strain output of a tensile-loaded HTSMA when excited by arbitrary temperature-stress inputs for the purpose of actuator and controls design. Common quasi-static generalized Preisach hysteresis models available in the literature require large sets of experimental data for model identification at a particular operating point, and substantially more data for multiple operating points. The novel algorithm introduced here proposes an alternate approach to Preisach methods that is better suited for research-stage alloys, such as recently-developed HTSMAs, for which a complete database is not yet available. A detailed description of the minor loop hysteresis model is presented in this paper, as well as a methodology for determination of model parameters. The model is then qualitatively evaluated with respect to well-established Preisach properties and against a set of low-temperature cycled loading data using a modified form of the one-dimensional Brinson constitutive equation. The computationally efficient algorithm demonstrates adherence to Preisach properties and excellent agreement to the validation data set.

PRELIMINARY RESULTS OF THE AGC-4 IRRADIATION IN THE ADVANCED TEST REACTOR AND DESIGN OF AGC-5 (HTR16-18469)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Davenport, Michael; Petti, D. A.

The United States Department of Energy’s Advanced Reactor Technologies (ART) Program will irradiate up to six nuclear graphite creep experiments in the Advanced Test Reactor (ATR) located at the Idaho National Laboratory (INL). The graphite experiments are being irradiated over an approximate eight year period to support development of a graphite irradiation performance data base on the new nuclear grade graphites now available for use in high temperature gas reactors. The goals of the irradiation experiments are to obtain irradiation performance data, including irradiation creep, at different temperatures and loading conditions to support design of the Very High Temperature Gasmore » Reactor (VHTR), as well as other future gas reactors. The experiments each consist of a single capsule that contain six stacks of graphite specimens, with half of the graphite specimens in each stack under a compressive load, while the other half of the specimens are not be subjected to a compressive load during irradiation. The six stacks have differing compressive loads applied to the top half of diametrically opposite pairs of specimen stacks. A seventh specimen stack in the center of the capsule does not have a compressive load. The specimens are being irradiated in an inert sweep gas atmosphere with on-line temperature and compressive load monitoring and control. There are also samples taken of the sweep gas effluent to measure any oxidation or off-gassing of the specimens that may occur during initial start-up of the experiment. The first experiment, AGC-1, started its irradiation in September 2009, and the irradiation was completed in January 2011. The second experiment, AGC-2, started its irradiation in April 2011 and completed its irradiation in May 2012. The third experiment, AGC-3, started its irradiation in late November 2012 and completed in the April of 2014. AGC-4 is currently being irradiated in the ATR. This paper will briefly discuss the preliminary irradiation results of the AGC-4 experiment, as well as the design of AGC-5.« less

Deformation mechanisms in a precipitation-strengthened ferritic superalloy revealed by in situ neutron diffraction studies at elevated temperatures

DOE PAGES

Huang, Shenyan; Gao, Yanfei; An, Ke; ...

2014-10-22

In this study, the ferritic superalloy Fe–10Ni–6.5Al–10Cr–3.4Mo strengthened by ordered (Ni,Fe)Al B2-type precipitates is a candidate material for ultra-supercritical steam turbine applications above 923 K. Despite earlier success in improving its room-temperature ductility, the creep resistance of this material at high temperatures needs to be further improved, which requires a fundamental understanding of the high-temperature deformation mechanisms at the scales of individual phases and grains. In situ neutron diffraction has been utilized to investigate the lattice strain evolution and the microscopic load-sharing mechanisms during tensile deformation of this ferritic superalloy at elevated temperatures. Finite-element simulations based on the crystal plasticitymore » theory are employed and compared with the experimental results, both qualitatively and quantitatively. Based on these interphase and intergranular load-partitioning studies, it is found that the deformation mechanisms change from dislocation slip to those related to dislocation climb, diffusional flow and possibly grain boundary sliding, below and above 873 K, respectively. Insights into microstructural design for enhancing creep resistance are also discussed.« less

Characterization of centrifugally-loaded flame migration for ultra-compact combustors

NASA Astrophysics Data System (ADS)

LeBay, Kenneth D.

The Air Force Research Laboratory (AFRL) has designed a centrifugally-loaded Ultra-Compact Combustor (UCC) showing viable merit for reducing gas turbine combustor length by as much as 66%. The overarching goal of this research was to characterize the migration of centrifugally-loaded flames in a sectional model of the UCC to enable scaling of the design from 15 cm to the 50--75 cm diameter of most engines. Two-line Planar Laser-Induced Fluorescence thermometry (PLIF) of OH, time-resolved Particle Image Velocimetry (PIV), and high-speed video data were collected. Using a sectional UCC model, the flame migration angle was determined to be a function of the UCC/core velocity ratio (VR) while both the VR and the centrifugal or "g-load" affected the migration quantity. Higher g-loads and lower VRs yielding higher migration but lower VRs had lower core flow temperatures due to higher core air mass flow. A comparison of the straight and curved UCC sections showed the centrifugal load increased the flame migration but increased unsteadiness. The flame migration into the core was estimated using pressure and temperature measurements upstream, and PIV measurements downstream of the core flow interface with constant density and velocity profile assumptions. The flame migration quantity was used to estimate the core flow temperature which was in relatively good agreement with the measured PLIF values. The migration quantity scaled relatively linearly with the UCC tangential velocity, which corresponds to the g-load value, with the slope determined by the VR. A simple analytical model resulted for the dependence of the migration quantity on the tangential velocity and VR. The quantitative relationships determined in this research provided a detailed description of the migration of centrifugally-loaded flames in a sectional UCC.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Panwar, Ranvir Singh, E-mail: ranvir.panwar@thapar.edu; Pandey, O.P., E-mail: oppandey@thapar.edu

Particulate reinforced aluminum metal matrix composite is in high demand in automobile industry where the operational conditions vary from low to high temperature. In order to understand the wear mode at elevated temperature, this study was planned. For this purpose we developed a metal matrix composite containing aluminum alloy (LM13) as matrix and zircon sand as particulate reinforcement by stir casting process. Different amounts of zircon sand (5, 10, 15 and 20 wt.%) were incorporated in the matrix to study the effect of reinforcement on the wear resistance. Dispersion of zircon sand particles in the matrix was confirmed by usingmore » optical microscopy. Sliding wear tests were done to study the durability of the composite with respect to the base alloy. The effects of load and temperature on wear behavior from room temperature to 300 Degree-Sign C were studied to understand the wear mechanism deeply. Surface morphology of the worn surfaces after the wear tests as well as wear debris was observed under scanning electron microscope. Mild to severe wear transition was noticed in tests at high temperature and high load. However, there is interesting change in wear behavior of the composite near the critical temperature of the composite. All the observed behavior has been explained with reference to the observed microstructure of the wear track and debris. - Highlights: Black-Right-Pointing-Pointer Good interfacial bonding between zircon sand particles and Al matrix was observed. Black-Right-Pointing-Pointer The effect of temperature on the wear behavior of LM13/Zr composites was studied. Black-Right-Pointing-Pointer Wear resistance of the composite was improved with addition of zircon sand. Black-Right-Pointing-Pointer Transition temperature from mild to severe wear also improved in composite. Black-Right-Pointing-Pointer SEM analysis of the tracks and debris was done to establish wear mechanism.« less

Investigation of tension-compression fatigue behavior of a cross-ply metal matrix composite at room and elevated temperatures. Master's thesis

DOE Office of Scientific and Technical Information (OSTI.GOV)

Boyum, E.A.

1993-12-01

This research, the first load-controlled tension-compression fatigue testing to be performed on a MMC, extends the existing knowledge of MMC fatigue damage mechanisms to include the tension compression loading condition. To accomplish this, a (0/90)2, SCS-6/Ti-15-3 laminate was subjected to tension-tension fatigue at room temperature, and tension-compression fatigue at both room temperature and 427 deg C. Stress and strain data was taken to evaluate the macro-mechanic behavior of the material. Microscopy and fractography were performed to characterize the damage on a micro-mechanic level. On a maximum applied stress basis, the room temperature tension-tension specimens had longer fatigue lives than themore » room temperature tension-compression specimens. The room and high temperature tension-compression fatigue lives were nearly identical in the fiber-dominated high stress region of the SN curve. However, the increased ductility and diffused plasticity of the titanium matrix at 427 deg C delayed the onset and severity of matrix cracking, and thus increased the elevated temperature fatigue lives in the matrix dominated region of the SN curve. In all cases, matrix damage initiated at reaction zone cracks which nucleated both matrix plasticity and matrix cracking. Metal matrix composite, Elevated temperature, Fatigue testing, Compression, Fully-reversed, Titanium, Silicon carbide.« less

Hydrophilic thermoplastic polyurethanes for the manufacturing of highly dosed oral sustained release matrices via hot melt extrusion and injection molding.

PubMed

Verstraete, G; Van Renterghem, J; Van Bockstal, P J; Kasmi, S; De Geest, B G; De Beer, T; Remon, J P; Vervaet, C

2016-06-15

Hydrophilic aliphatic thermoplastic polyurethane (Tecophilic™ grades) matrices for high drug loaded oral sustained release dosage forms were formulated via hot melt extrusion/injection molding (HME/IM). Drugs with different aqueous solubility (diprophylline, theophylline and acetaminophen) were processed and their influence on the release kinetics was investigated. Moreover, the effect of Tecophilic™ grade, HME/IM process temperature, extrusion speed, drug load, injection pressure and post-injection pressure on in vitro release kinetics was evaluated for all model drugs. (1)H NMR spectroscopy indicated that all grades have different soft segment/hard segment ratios, allowing different water uptake capacities and thus different release kinetics. Processing temperature of the different Tecophilic™ grades was successfully predicted by using SEC and rheology. Tecophilic™ grades SP60D60, SP93A100 and TG2000 had a lower processing temperature than other grades and were further evaluated for the production of IM tablets. During HME/IM drug loads up to 70% (w/w) were achieved. In addition, Raman mapping and (M)DSC results confirmed the homogenous distribution of mainly crystalline API in all polymer matrices. Besides, hydrophilic TPU based formulations allowed complete and sustained release kinetics without using release modifiers. As release kinetics were mainly affected by drug load and the length of the PEO soft segment, this polymer platform offers a versatile formulation strategy to adjust the release rate of drugs with different aqueous solubility. Copyright © 2016 Elsevier B.V. All rights reserved.

Constitution of pseudobinary hypoeutectic beta-NiAl + alpha-V alloys

NASA Technical Reports Server (NTRS)

Cotton, J. D.; Kaufman, M. J.; Noebe, R. D.

1991-01-01

The formation of pseudobinary eutectics between NiAl (beta) and V (alpha) at high temperatures was investigated as a possible way of improving the ductility and toughness of the alloy. It is found that a pseudobinary eutectic, characterized by a large beta+alpha field, is formed in the Ni-Al-V ternary system below about 1370 C. The high-temperature solubility of V in beta is about 14 percent, decreasing markedly with decreasing temperature and increasing Al content above 50 at. pct Al. The pseudobinary hypoeutectic exibits crack resistance under indentation loading.

Dynamic Heat Generation Modeling and Thermal Management of Electromechanical Actuators

DTIC Science & Technology

2012-07-01

PCM Module In situations where the heat load is high and the convection heat transfer is ineffective (such as in an aircraft bay with near stagnant...excess thermal energy in the PCM , we should choose a PCM with a melting temperature range below 150oC and a high latent heat of fusion. In this...chapter, we select Erythritol as the PCM [21]. This PCM has a high latent heat (340 kJ/kg) and suitable phase change temperature range (~120oC). The

Loading rate and test temperature effects on fracture of In Situ niobium silicide-niobium composites

NASA Astrophysics Data System (ADS)

Rigney, Joseph D.; Lewandowski, John J.

1996-10-01

Arc cast, extruded, and heat-treated in situ composites of niobium suicide (Nb5Si3) intermetallic with niobium phases (primary—Nbp and secondary—Nbs) exhibited high fracture resistance in comparison to monolithic Nb5Si3. In toughness tests conducted at 298 K and slow applied loading rates, the fracture process proceeded by the microcracking of the Nb5Si3 and plastic deformation of the Nbp and Nbs phases, producing resistance-curve behavior and toughnesses of 28 MPa√m with damage zone lengths less than 500 μm. The effects of changes in the Nbp yield strength and fracture behavior on the measured toughnesses were investigated by varying the loading rates during fracture tests at both 77 and 298 K. Quantitative fractography was utilized to completely characterize each fracture surface created at 298 K in order to determine the type of fracture mode ( i.e., dimpled, cleavage) exhibited by the Nbp. Specimens tested at either higher loading rates or lower test temperatures consistently exhibited a greater amount of cleavage fracture in the Nbp, while the Nbs, always remained ductile. However, the fracture toughness values determined from experiments spanning six orders of magnitude in loading rate at 298 and 77 K exhibited little variation, even under conditions when the majority of Nbp phases failed by cleavage at 77 K. The changes in fracture mode with increasing loading rate and/or decreasing test temperature and their effects on fracture toughness are rationalized by comparison to existing theoretical models.

Control of hydrocarbon emissions from gasoline loading by refrigeration systems. Final report Dec 80-Apr 81

DOE Office of Scientific and Technical Information (OSTI.GOV)

Battye, W.; Brown, P.; Misenheimer, D.

1981-07-01

The report gives results of a study of the capabilities of refrigeration systems, operated at three temperatures, to control volatile organic compound (VOC) emissions from truck loading at bulk gasoline terminals. Achievable VOC emission rates were calculated for refrigeration systems cooling various gasoline/air mixtures to -62 C, -73 C, and -84 C by estimating vapor/liquid equilibrium compositions for VOC/air mixtures. Emission rates were calculated for inlet streams containing vapors from low- and high-volatility gasolines at concentrations of 15, 30, and 50% by volume (22.5, 45, and 75% measured as propane). Predicted VOC emission rates for systems cooling various inlet streamsmore » to -62 C ranged from 48 to 59 mg VOC/liter of gasoline loaded. Predicted VOC were 21 to 28 mg/l loaded for systems operating at -73 C and 8.7 to 12 mg/l loaded for systems operating at -84 C. Compressor electrical requirements and relative capital costs for systems operating at the above temperatures were estimated for model systems using the results of a computer simulation. Compressor electrical requirements ranged from 0.11 to 0.45 Whr/l loaded, depending on the inlet VOC concentration and the outlet temperature. The capital cost to build a system designed to cool vapors to -84 C is estimated to be about 9% higher than for a system designed to operate at -73 C.« less

High-temperature, high-pressure bonding of nested tubular metallic components

DOEpatents

Quinby, T.C.

A tool is described for effecting high-temperature, high-compression bonding between the confronting faces of nested, tubular, metallic components. In a typical application, the tool is used to produce tubular target assemblies for irradiation in nuclear reactors or particle accelerators. The target assembly comprising a uranum foil and an aluninum-alloy substrate. The tool is composed of graphite. It comprises a tubular restraining member in which a mechanically expandable tubular core is mounted to form an annulus. The components to be bonded are mounted in nested relation in the annulus. The expandable core is formed of individually movable, axially elongated segments whose outer faces cooperatively define a cylindrical pressing surface and whose inner faces cooperatively define two opposed, inwardly tapered, axial bores. Tapered rams extend into the bores. The loaded tool is mounted in a conventional hot-press provided with evacuation means, heaters for maintaining its interior at bonding temperature, and hydraulic cylinders for maintaining a selected inwardly directed pressure on the tapered rams. With the hot-press evacuated and the loaded tool at the desired temperature, the cylinders are actuated to apply the selected pressure to the rams. The rams in turn expand the segmented core to maintain the nested components in compression against the restraining member. These conditions are maintained until the confronting faces of the nested components are joined in a continuous, uniform bond characterized by high thermal conductivity.

Sodium effects on mechanical performance and consideration in high temperature structural design for advanced reactors

NASA Astrophysics Data System (ADS)

Natesan, K.; Li, Meimei; Chopra, O. K.; Majumdar, S.

2009-07-01

Sodium environmental effects are key limiting factors in the high temperature structural design of advanced sodium-cooled reactors. A guideline is needed to incorporate environmental effects in the ASME design rules to improve the performance reliability over long operating times. This paper summarizes the influence of sodium exposure on mechanical performance of selected austenitic stainless and ferritic/martensitic steels. Focus is on Type 316SS and mod.9Cr-1Mo. The sodium effects were evaluated by comparing the mechanical properties data in air and sodium. Carburization and decarburization were found to be the key factors that determine the tensile and creep properties of the steels. A beneficial effect of sodium exposure on fatigue life was observed under fully reversed cyclic loading in both austenitic stainless steels and ferritic/martensitic steels. However, when hold time was applied during cyclic loading, the fatigue life was significantly reduced. Based on the mechanical performance of the steels in sodium, consideration of sodium effects in high temperature structural design of advanced fast reactors is discussed.

High Performance Pulse Tube Cryocoolers

NASA Astrophysics Data System (ADS)

Olson, J. R.; Roth, E.; Champagne, P.; Evtimov, B.; Nast, T. C.

2008-03-01

Lockheed Martin's Advanced Technology Center has been developing pulse tube cryocoolers for more than ten years. Recent innovations include successful testing of four-stage coldheads, no-load temperature below 4 K, and the recent development of a high-efficiency compressor. This paper discusses the predicted performance of single and multiple stage pulse tube coldheads driven by our new 6 kg "M5Midi" compressor, which is capable of 90% efficiency with 200 W input power, and a maximum input power of 1000 W. This compressor retains the simplicity of earlier LM-ATC compressors: it has a moving magnet and an external electrical coil, minimizing organics in the working gas and requiring no electrical penetrations through the pressure wall. Motor losses were minimized during design, resulting in a simple, easily-manufactured compressor with state-of-the-art motor efficiency. The predicted cryocooler performance is presented as simple formulae, allowing an engineer to include the impact of a highly-optimized cryocooler into a full system analysis. Performance is given as a function of the heat rejection temperature and the cold tip temperatures and cooling loads.

Phase transformation and long-term service of high-temperature martensitic chromium steels

NASA Astrophysics Data System (ADS)

Kalashnikov, I. S.; Tarasenko, L.; Acselrad, O.; Pereira, L. C.; Shalkevich, A.; Soboleva, G.

2000-02-01

Martensitic high Cr (10 - 16%) steels alloyed with Ni (Co), Mo, W, V, and N are widely used in constructions subjected to cyclic loads at temperatures up to 600 degrees Celsius, in general after quenching from 1100 - 1150 degrees Celsius followed by tempering at 650 - 690 degrees Celsius. Due to long term service exposure at high temperatures, different microstructural changes take place, such as second-phases precipitation, formation of low-angle grain boundaries, as well as internal damage caused by cyclic loads and creep. Specific phase diagrams are presented that can be used to define time periods for reliable operation of parts with given composition, based on the time required for the appearance of second phase particles known to be detrimental to mechanical strength and performance. Restoring thermal treatments to be applied after long time exposure at service conditions, aiming at increasing service life, are also presented and discussed. The combined use of the diagrams and the restoring treatment ensures prediction of a reliable service-life period for components made of these steels.

Phase transformation and long-term service of high-temperature martensitic chromium steels

NASA Astrophysics Data System (ADS)

Kalashnikov, I. S.; Tarasenko, L.; Acselrad, O.; Pereira, L. C.; Shalkevich, A.; Soboleva, G.

2001-02-01

Martensitic high Cr (10 - 16%) steels alloyed with Ni (Co), Mo, W, V, and N are widely used in constructions subjected to cyclic loads at temperatures up to 600 degrees Celsius, in general after quenching from 1100 - 1150 degrees Celsius followed by tempering at 650 - 690 degrees Celsius. Due to long term service exposure at high temperatures, different microstructural changes take place, such as second-phases precipitation, formation of low-angle grain boundaries, as well as internal damage caused by cyclic loads and creep. Specific phase diagrams are presented that can be used to define time periods for reliable operation of parts with given composition, based on the time required for the appearance of second phase particles known to be detrimental to mechanical strength and performance. Restoring thermal treatments to be applied after long time exposure at service conditions, aiming at increasing service life, are also presented and discussed. The combined use of the diagrams and the restoring treatment ensures prediction of a reliable service-life period for components made of these steels.

Apparatus and methods for supplying auxiliary steam in a combined cycle system

DOEpatents

Gorman, William G.; Carberg, William George; Jones, Charles Michael

2002-01-01

To provide auxiliary steam, a low pressure valve is opened in a combined cycle system to divert low pressure steam from the heat recovery steam generator to a header for supplying steam to a second combined cycle's steam turbine seals, sparging devices and cooling steam for the steam turbine if the steam turbine and gas turbine lie on a common shaft with the generator. Cooling steam is supplied the gas turbine in the combined cycle system from the high pressure steam turbine. Spent gas turbine cooling steam may augment the low pressure steam supplied to the header by opening a high pressure valve whereby high and low pressure steam flows are combined. An attemperator is used to reduce the temperature of the combined steam in response to auxiliary steam flows above a predetermined flow and a steam header temperature above a predetermined temperature. The auxiliary steam may be used to start additional combined cycle units or to provide a host unit with steam turbine cooling and sealing steam during full-speed no-load operation after a load rejection.

Characterization of the temperature evolution during high-cycle fatigue of the ULTIMET superalloy: Experiment and theoretical modeling

NASA Astrophysics Data System (ADS)

Jiang, L.; Wang, H.; Liaw, P. K.; Brooks, C. R.; Klarstrom, D. L.

2001-09-01

High-speed, high-resolution infrared thermography, as a noncontact, full-field, and nondestructive technique, was used to study the temperature variations of a cobalt-based ULTIMET alloy subjected to high-cycle fatigue. During each fatigue cycle, the temperature oscillations, which were due to the thermal-elastic-plastic effects, were observed and related to stress-strain analyses. A constitutive model was developed for predicting the thermal and mechanical responses of the ULTIMET alloy subjected to cyclic deformation. The model was constructed in light of internal-state variables, which were developed to characterize the inelastic strain of the material during cyclic loading. The predicted stress-strain and temperature responses were found to be in good agreement with the experimental results. In addition, the change of temperature during fatigue was employed to reveal the accumulation of fatigue damage, and the measured temperature was utilized as an index for fatigue-life prediction.

Design and implementation of a multiaxial loading capability during heating on an engineering neutron diffractometer.

PubMed

Benafan, O; Padula, S A; Skorpenske, H D; An, K; Vaidyanathan, R

2014-10-01

A gripping capability was designed, implemented, and tested for in situ neutron diffraction measurements during multiaxial loading and heating on the VULCAN engineering materials diffractometer at the spallation neutron source at Oak Ridge National Laboratory. The proposed capability allowed for the acquisition of neutron spectra during tension, compression, torsion, and/or complex loading paths at elevated temperatures. The design consisted of age-hardened, Inconel(®) 718 grips with direct attachment to the existing MTS load frame having axial and torsional capacities of 100 kN and 400 N·m, respectively. Internal cooling passages were incorporated into the gripping system for fast cooling rates during high temperature experiments up to ∼1000 K. The specimen mounting couplers combined a threaded and hexed end-connection for ease of sample installation/removal without introducing any unwanted loads. Instrumentation of this capability is documented in this work along with various performance parameters. The gripping system was utilized to investigate deformation in NiTi shape memory alloys under various loading/control modes (e.g., isothermal, isobaric, and cyclic), and preliminary results are presented. The measurements facilitated the quantification of the texture, internal strain, and phase fraction evolution in NiTi shape memory alloys under various loading/control modes.

Design and implementation of a multiaxial loading capability during heating on an engineering neutron diffractometer

NASA Astrophysics Data System (ADS)

Benafan, O.; Padula, S. A.; Skorpenske, H. D.; An, K.; Vaidyanathan, R.

2014-10-01

A gripping capability was designed, implemented, and tested for in situ neutron diffraction measurements during multiaxial loading and heating on the VULCAN engineering materials diffractometer at the spallation neutron source at Oak Ridge National Laboratory. The proposed capability allowed for the acquisition of neutron spectra during tension, compression, torsion, and/or complex loading paths at elevated temperatures. The design consisted of age-hardened, Inconel® 718 grips with direct attachment to the existing MTS load frame having axial and torsional capacities of 100 kN and 400 N.m, respectively. Internal cooling passages were incorporated into the gripping system for fast cooling rates during high temperature experiments up to ˜1000 K. The specimen mounting couplers combined a threaded and hexed end-connection for ease of sample installation/removal without introducing any unwanted loads. Instrumentation of this capability is documented in this work along with various performance parameters. The gripping system was utilized to investigate deformation in NiTi shape memory alloys under various loading/control modes (e.g., isothermal, isobaric, and cyclic), and preliminary results are presented. The measurements facilitated the quantification of the texture, internal strain, and phase fraction evolution in NiTi shape memory alloys under various loading/control modes.

Cellulose-Hemicellulose Interactions at Elevated Temperatures Increase Cellulose Recalcitrance to Biological Conversion

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mittal, Ashutosh; Himmel, Michael E; Kumar, Rajeev

It has been previously shown that cellulose-lignin droplets' strong interactions, resulting from lignin coalescence and redisposition on cellulose surface during thermochemical pretreatments, increase cellulose recalcitrance to biological conversion, especially at commercially viable low enzyme loadings. However, information on the impact of cellulose-hemicellulose interactions on cellulose recalcitrance following relevant pretreatment conditions are scarce. Here, to investigate the effects of plausible hemicellulose precipitation and re-association with cellulose on cellulose conversion, different pretreatments were applied to pure Avicel(R) PH101 cellulose alone and Avicel mixed with model hemicellulose compounds followed by enzymatic hydrolysis of resulting solids at both low and high enzyme loadings. Solidsmore » produced by pretreatment of Avicel mixed with hemicelluloses (AMH) were found to contain about 2 to 14.6% of exogenous, precipitated hemicelluloses and showed a remarkably much lower digestibility (up to 60%) than their respective controls. However, the exogenous hemicellulosic residues that associated with Avicel following high temperature pretreatments resulted in greater losses in cellulose conversion than those formed at low temperatures, suggesting that temperature plays a strong role in the strength of cellulose-hemicellulose association. Molecular dynamics simulations of hemicellulosic xylan and cellulose were found to further support this temperature effect as the xylan-cellulose interactions were found to substantially increase at elevated temperatures. Furthermore, exogenous, precipitated hemicelluloses in pretreated AMH solids resulted in a larger drop in cellulose conversion than the delignified lignocellulosic biomass containing comparably much higher natural hemicellulose amounts. Increased cellulase loadings or supplementation of cellulase with xylanases enhanced cellulose conversion for most pretreated AMH solids; however, this approach was less effective for solids containing mannan polysaccharides, suggesting stronger association of cellulose with (hetero) mannans or lack of enzymes in the mixture required to hydrolyze such polysaccharides.« less

40 CFR 63.6675 - What definitions apply to this subpart?

Code of Federal Regulations, 2012 CFR

2012-07-01

... for use during periods of high demand that are not emergencies. Percent load means the fractional... stationary RICE in which a high boiling point liquid fuel injected into the combustion chamber ignites when the air charge has been compressed to a temperature sufficiently high for auto-ignition. This process...

A Novel Thermal Management Approach for Radial Foil Air Bearings

DTIC Science & Technology

2010-07-01

injection air. The tests were conducted at room temperature with the bearing operating at speeds from 20 to 50 krpm while supporting 222N. Two different...14  List of Tables Table 1. Bearing temperature results for the two injection air flows at three different operating...no further than the research stage (3, 4). However, during the last 15 years, more advanced, higher load capacity bearings and high temperature

Co-production of hydrogen and carbon nanotubes on nickel foam via methane catalytic decomposition

NASA Astrophysics Data System (ADS)

Ping, Dan; Wang, Chaoxian; Dong, Xinfa; Dong, Yingchao

2016-04-01

The co-production of COx-free hydrogen and carbon nanotubes (CNTs) was achieved on 3-dimensional (3D) macroporous nickel foam (NF) via methane catalytic decomposition (MCD) over nano-Ni catalysts using chemical vapor deposition (CVD) technique. By a simple coating of a NiO-Al2O3 binary mixture sol followed by a drying-calcination-reduction treatment, NF supported composite catalysts (denoted as NiyAlOx/NF) with Al2O3 transition-layer incorporated with well-dispersed nano-Ni catalysts were successfully prepared. The effects of Ni loading, calcination temperature and reaction temperature on the performance for simultaneous production of COx-free hydrogen and CNTs were investigated in detail. Catalysts before and after MCD were characterized by XRD, TPR, SEM, TEM, TG and Raman spectroscopy technology. Results show that increasing Ni loading, lowering calcination temperature and optimizing MCD reaction temperature resulted in high production efficiency of COx-free H2 and carbon, but broader diameter distribution of CNTs. Through detailed parameter optimization, the catalyst with a Ni/Al molar ratio of 0.1, calcination temperature of 550 °C and MCD temperature of 650 °C was favorable to simultaneously produce COx-free hydrogen with a growth rate as high as 10.3% and CNTs with uniform size on NF.

Fatigue Behavior of Glass Fiber-Reinforced Polymer Bars after Elevated Temperatures Exposure.

PubMed

Li, Guanghui; Zhao, Jun; Wang, Zike

2018-06-16

Fiber-reinforced polymer (FRP) bars have been widely applied in civil engineering. This paper presents the results of an experimental study to investigate the tensile fatigue mechanical properties of glass fiber-reinforced polymer (GFRP) bars after elevated temperatures exposure. For this purpose, a total of 105 GFRP bars were conducted for testing. The specimens were exposed to heating regimes of 100, 150, 200, 250, 300 and 350 °C for a period of 0, 1 or 2 h. The GFRP bars were tested with different times of cyclic load after elevated temperatures exposure. The results show that the tensile strength and elastic modulus of GFRP bars decrease with the increase of elevated temperature and holding time, and the tensile strength of GFRP bars decreases obviously by 19.5% when the temperature reaches 250 °C. Within the test temperature range, the tensile strength of GFRP bars decreases at most by 28.0%. The cyclic load accelerates the degradation of GFRP bars after elevated temperature exposure. The coupling of elevated temperature and holding time enhance the degradation effect of cyclic load on GFRP bars. The tensile strength of GFRP bars after elevated temperatures exposure at 350 °C under cyclic load is reduced by 50.5% compared with that at room temperature and by 36.3% compared with that after exposing at 350 °C without cyclic load. In addition, the elastic modulus of GFRP bars after elevated temperatures exposure at 350 °C under cyclic load is reduced by 17.6% compared with that at room temperature and by 6.0% compared with that after exposing at 350 °C without cyclic load.

Thermal conductivity of a graphite bipolar plate (BPP) and its thermal contact resistance with fuel cell gas diffusion layers: Effect of compression, PTFE, micro porous layer (MPL), BPP out-of-flatness and cyclic load

NASA Astrophysics Data System (ADS)

Sadeghifar, Hamidreza; Djilali, Ned; Bahrami, Majid

2015-01-01

This paper reports on measurements of thermal conductivity of a graphite bipolar plate (BPP) as a function of temperature and its thermal contact resistance (TCR) with treated and untreated gas diffusion layers (GDLs). The thermal conductivity of the BPP decreases with temperature and its thermal contact resistance with GDLs, which has been overlooked in the literature, is found to be dominant over a relatively wide range of compression. The effects of PTFE loading, micro porous layer (MPL), compression, and BPP out-of-flatness are also investigated experimentally. It is found that high PTFE loadings, MPL and even small BPP out-of-flatness increase the BPP-GDL thermal contact resistance dramatically. The paper also presents the effect of cyclic load on the total resistance of a GDL-BPP assembly, which sheds light on the behavior of these materials under operating conditions in polymer electrolyte membrane fuel cells.

Mechanics of Failure of High Temperature Metal Matrix Composites

DTIC Science & Technology

1993-12-22

by two inhomogeneities that sustain an eigenstrain loading, proportional to the difference of fiber/matrx thermal expansion coefficients. Utilizing the...appropriate eigenstrain field. sustained by the fiber cross sections. Our primary interest is to determine how the fiber interaction relates to the local...inhomogeneities (fiber cross sections). with a central distance c. undergo an eigenstrain loading. Utilizing the di. -Sacement potentials approach. an

The effect of mass loading on the temperature of a flowing plasma. [in vicinity of Io

NASA Technical Reports Server (NTRS)

Linker, Jon A.; Kivelson, Margaret G.; Walker, Raymond J.

1989-01-01

How the addition of ions at rest (mass loading) affects the temperature of a flowing plasma in a MHD approximation is investigated, using analytic theory and time dependent, three-dimensional MHD simulations of plasma flow past Io. The MHD equations show that the temperature can increase or decrease relative to the background, depending on the local sonic Mach number M(S), of the flow. For flows with M(S) of greater than sq rt 9/5 (when gamma = 5/3), mass loading increases the plasma temperature. However, the simulations show a nonlinear response to the addition of mass. If the mass loading rate is large enough, the temperature increase may be smaller than expected, or the temperature may actually decrease, because a large mass loading rate slows the flow and decreases the thermal energy of the newly created plasma.

Modeling spot markets for electricity and pricing electricity derivatives

NASA Astrophysics Data System (ADS)

Ning, Yumei

Spot prices for electricity have been very volatile with dramatic price spikes occurring in restructured market. The task of forecasting electricity prices and managing price risk presents a new challenge for market players. The objectives of this dissertation are: (1) to develop a stochastic model of price behavior and predict price spikes; (2) to examine the effect of weather forecasts on forecasted prices; (3) to price electricity options and value generation capacity. The volatile behavior of prices can be represented by a stochastic regime-switching model. In the model, the means of the high-price and low-price regimes and the probabilities of switching from one regime to the other are specified as functions of daily peak load. The probability of switching to the high-price regime is positively related to load, but is still not high enough at the highest loads to predict price spikes accurately. An application of this model shows how the structure of the Pennsylvania-New Jersey-Maryland market changed when market-based offers were allowed, resulting in higher price spikes. An ARIMA model including temperature, seasonal, and weekly effects is estimated to forecast daily peak load. Forecasts of load under different assumptions about weather patterns are used to predict changes of price behavior given the regime-switching model of prices. Results show that the range of temperature forecasts from a normal summer to an extremely warm summer cause relatively small increases in temperature (+1.5%) and load (+3.0%). In contrast, the increases in prices are large (+20%). The conclusion is that the seasonal outlook forecasts provided by NOAA are potentially valuable for predicting prices in electricity markets. The traditional option models, based on Geometric Brownian Motion are not appropriate for electricity prices. An option model using the regime-switching framework is developed to value a European call option. The model includes volatility risk and allows changes in prices and volatility to be correlated. The results show that the value of a power plant is much higher using the financial option model than using traditional discounted cash flow.

Performance of large-bore tapered-roller bearings under combined radial and thrust load at shaft speeds to 15,000 rpm

NASA Technical Reports Server (NTRS)

Parker, R. J.; Signer, H. R.

1977-01-01

The performance of 120.65-mm bore tapered roller bearings was investigated at shaft speeds up to 15,000 rpm. Temperature distribution and bearing heat generation were determined as a function of shaft speed, radial and thrust loads, lubricant flow rate, and lubricant inlet temperature. Lubricant was supplied by either jets or by a combination of holes through the cone directly to the cone-rib contact and jets at the roller small-end side. Cone-rib lubrication significantly improved high-speed tapered-roller bearing performance, yielding lower cone-face temperatures and lower power loss and allowing lower lubricant flow rates for a given speed condition. Bearing temperatures increased with increased shaft speed and decreased with increased lubricant flow rate. Bearing power loss increased with increased shaft speed and increased lubricant flow rate.

On nonlinear thermo-electro-elasticity.

PubMed

Mehnert, Markus; Hossain, Mokarram; Steinmann, Paul

2016-06-01

Electro-active polymers (EAPs) for large actuations are nowadays well-known and promising candidates for producing sensors, actuators and generators. In general, polymeric materials are sensitive to differential temperature histories. During experimental characterizations of EAPs under electro-mechanically coupled loads, it is difficult to maintain constant temperature not only because of an external differential temperature history but also because of the changes in internal temperature caused by the application of high electric loads. In this contribution, a thermo-electro-mechanically coupled constitutive framework is proposed based on the total energy approach. Departing from relevant laws of thermodynamics, thermodynamically consistent constitutive equations are formulated. To demonstrate the performance of the proposed thermo-electro-mechanically coupled framework, a frequently used non-homogeneous boundary-value problem, i.e. the extension and inflation of a cylindrical tube, is solved analytically. The results illustrate the influence of various thermo-electro-mechanical couplings.

On nonlinear thermo-electro-elasticity

PubMed Central

Mehnert, Markus; Hossain, Mokarram

2016-01-01

Electro-active polymers (EAPs) for large actuations are nowadays well-known and promising candidates for producing sensors, actuators and generators. In general, polymeric materials are sensitive to differential temperature histories. During experimental characterizations of EAPs under electro-mechanically coupled loads, it is difficult to maintain constant temperature not only because of an external differential temperature history but also because of the changes in internal temperature caused by the application of high electric loads. In this contribution, a thermo-electro-mechanically coupled constitutive framework is proposed based on the total energy approach. Departing from relevant laws of thermodynamics, thermodynamically consistent constitutive equations are formulated. To demonstrate the performance of the proposed thermo-electro-mechanically coupled framework, a frequently used non-homogeneous boundary-value problem, i.e. the extension and inflation of a cylindrical tube, is solved analytically. The results illustrate the influence of various thermo-electro-mechanical couplings. PMID:27436985

High temperature ceramic interface study

NASA Technical Reports Server (NTRS)

Lindberg, L. J.

1984-01-01

Monolithic SiC and Si3N4 are susceptible to contact stress damage at static and sliding interfaces. Transformation-toughened zirconia (TTZ) was evaluated under sliding contact conditions to determine if the higher material fracture toughness would reduce the susceptibility to contact stress damage. Contact stress tests were conducted on four commercially available TTZ materials at normal loads ranging from 0.455 to 22.7 kg (1 to 50 pounds) at temperatures ranging from room temperature to 1204C (2200 F). Static and dynamic friction were measured as a function of temperature. Flexural strength measurements after these tests determined that the contact stress exposure did not reduce the strength of TTZ at contact loads of 0.455, 4.55, and 11.3 kg (1, 10, and 25 pounds). Prior testing with the lower toughness SiC and Si3N4 materials resulted in a substantial strength reduction at loads of only 4.55 and 11.3 kg (10 and 25 pounds). An increase in material toughness appears to improve ceramic material resistance to contact stress damage. Baseline material flexure strength was established and the stress rupture capability of TTZ was evaluated. Stress rupture tests determined that TTZ materials are susceptible to deformation due to creep and that aging of TTZ materials at elevated temperatures results in a reduction of material strength.

Comparison of simulated and experimental results of temperature distribution in a closed two-phase thermosyphon cooling system

NASA Astrophysics Data System (ADS)

Shaanika, E.; Yamaguchi, K.; Miki, M.; Ida, T.; Izumi, M.; Murase, Y.; Oryu, T.; Yanamoto, T.

2017-12-01

Superconducting generators offer numerous advantages over conventional generators of the same rating. They are lighter, smaller and more efficient. Amongst a host of methods for cooling HTS machinery, thermosyphon-based cooling systems have been employed due to their high heat transfer rate and near-isothermal operating characteristics associated with them. To use them optimally, it is essential to study thermal characteristics of these cryogenic thermosyphons. To this end, a stand-alone neon thermosyphon cooling system with a topology resembling an HTS rotating machine was studied. Heat load tests were conducted on the neon thermosyphon cooling system by applying a series of heat loads to the evaporator at different filling ratios. The temperature at selected points of evaporator, adiabatic tube and condenser as well as total heat leak were measured. A further study involving a computer thermal model was conducted to gain further insight into the estimated temperature distribution of thermosyphon components and heat leak of the cooling system. The model employed boundary conditions from data of heat load tests. This work presents a comparison between estimated (by model) and experimental (measured) temperature distribution in a two-phase cryogenic thermosyphon cooling system. The simulation results of temperature distribution and heat leak compared generally well with experimental data.

Evaluation of hybrid processes for nitrification by comparing MBBR/AS and IFAS configurations.

PubMed

Germain, E; Bancroft, L; Dawson, A; Hinrichs, C; Fricker, L; Pearce, P

2007-01-01

An integrated fixed-film activated sludge (IFAS) pilot plant and a moving bed biofilm reactor coupled with an activated sludge process (MBBR/AS) were operated under different temperatures, carbon loadings and solids retention times (SRTs). These two types of hybrid systems were compared, focusing on the nitrification capacity and the nitrifiers population of the media and suspended biomass alongside other process performances such as carbonaceous and total nitrogen (TN) removal rates. At high temperatures and loadings rates, both processes were fully nitrifying and achieved similarly high carbonaceous removal rates. However, under these conditions, the IFAS configuration performed better in terms of TN removal. Lower temperatures and carbon loadings led to lower carbonaceous removal rates for the MBBR/AS configuration, whereas the IFAS configuration was not affected. However, the nitrification capacity of the IFAS process decreased significantly under these conditions and the MBBR/AS process was more robust in terms of nitrification. Ammonia oxidising bacteria (AOB) and nitrite oxidising bacteria (NOB) population counts accurately reflected the changes in nitrification capacity. However, significantly less NOBs than AOBs were observed, without noticeable nitrite accumulation, suggesting that the characterisation method used was not as sensitive for NOBs and/or that the NOBs had a higher activity than the AOBs.

Characteristics of DO, organic matter, and ammonium profile for practical-scale DHS reactor under various organic load and temperature conditions.

PubMed

Nomoto, Naoki; Ali, Muntjeer; Jayaswal, Komal; Iguchi, Akinori; Hatamoto, Masashi; Okubo, Tsutomu; Takahashi, Masanobu; Kubota, Kengo; Tagawa, Tadashi; Uemura, Shigeki; Yamaguchi, Takashi; Harada, Hideki

2018-04-01

Profile analysis of the down-flow hanging sponge (DHS) reactor was conducted under various temperature and organic load conditions to understand the organic removal and nitrification process for sewage treatment. Under high organic load conditions (3.21-7.89 kg-COD m -3  day -1 ), dissolved oxygen (DO) on the upper layer of the reactor was affected by organic matter concentration and water temperature, and sometimes reaches around zero. Almost half of the COD Cr was removed by the first layer, which could be attributed to the adsorption of organic matter on sponge media. After the first layer, organic removal proceeded along the first-order reaction equation from the second to the fourth layers. The ammoniacal nitrogen removal ratio decreased under high organic matter concentration (above 100 mg L -1 ) and low DO (less than 1 mg L -1 ) condition. Ammoniacal nitrogen removal proceeded via a zero-order reaction equation along the reactor height. In addition, the profile results of DO, COD Cr , and NH 3 -N were different in the horizontal direction. Thus, it is thought the concentration of these items and microbial activities were not in a uniform state even in the same sponge layer of the DHS reactor.

Testing of a single graded groove variable conductance heat pipe

NASA Astrophysics Data System (ADS)

Kapolnek, Michael R.; Holmes, H. R.; Hager, Brian

1992-07-01

Variable conductance heat pipes (VCHPs) with transport capacities in the 50,000 to 100,000 Watt-inch range will be required to transport the large heat loads anticipated for advanced spacecraft. A high-reliability, nonarterial constant conductance heat pipe with this capacity, the Single Graded Groove (SGG) heat pipe, was developed for NASA's Space Station Freedom. The design and testing of a variable conductance SGG heat pipe are described. Response of the pipe to startup and heat load changes was excellent. After correcting for condenser temperature changes, the evaporator temperature varied by only +/- 4 F for large evaporator heat load changes. The surface tension difference between ends of the gas blocked region was found to measurably affect the performance of the pipe. Performance was negligibly affected by Marangoni flow in the gas blocked region.

Space Shuttle Projects

NASA Image and Video Library

1987-07-01

A forward segment is being lowered into the Transient Pressure Test Article (TPTA) test stand at the Marshall Space Flight Center (MSFC) east test area. The TPTA test stand, 14-feet wide, 27-feet long, and 33-feet high, was built in 1987 to provide data to verify the sealing capability of the redesign solid rocket motor (SRM) field and nozzle joints. The test facility applies pressure, temperature, and external loads to a short stack of solid rocket motor hardware. The simulated SRM ignition pressure and temperature transients are achieved by firing a small amount of specially configured solid propellant. The pressure transient is synchronized with external programmable dynamic loads that simulate lift off loads at the external tank attach points. Approximately one million pounds of dead weight on top of the test article simulates the weight of the other Shuttle elements.

Space Shuttle Projects

NASA Image and Video Library

1987-07-01

A forward segment is being lowered into the Transient Pressure Test Article (TPTA) test stand at thw Marshall Space Flight Center (MSFC) east test area. The TPTA test stand, 14-feet wide, 27-feet long, and 33-feet high, was built in 1987 to provide data to verify the sealing capability of the redesign solid rocket motor (SRM) field and nozzle joints. The test facility applies pressure, temperature, and external loads to a short stack of solid rocket motor hardware. The simulated SRM ignition pressure and temperature transients are achieved by firing a small amount of specially configured solid propellant. The pressure transient is synchronized with external programmable dynamic loads that simulate lift off loads at the external tank attach points. Approximately one million pounds of dead weight on top of the test article simulates the weight of the other Shuttle elements.

Thin film system with integrated load and temperature sensors for the technical application in deep drawing process

NASA Astrophysics Data System (ADS)

Biehl, Saskia; Paetsch, Nancy; Meyer-Kornblum, Eike

2017-05-01

In these days industry 4.0 resounded throughout the land and means the fourth industrial revolution. The industry has to tackle the task of a flexible and customer-oriented production. Therefor the need of sensor systems for the measurement of temperature and load, the two most important categories in production, is rising. For getting the real specification during the production process the integration of sensor elements in high load regions of machinery is very important. Thus wear resistant thin film sensor systems directly applied onto the surface of plant components are in development. These multilayer systems combine excellent wear resistance with sensory behaviour. The sensor data will lead to a deeper process understanding, to optimization of simulation tools, to reduction of rejects and to an improvement of flexibility in production.

Estimates of crystalline LiF thermal conductivity at high temperature and pressure by a Green-Kubo method

DOE PAGES

Jones, R. E.; Ward, D. K.

2016-07-18

Here, given the unique optical properties of LiF, it is often used as an observation window in high-temperature and -pressure experiments; hence, estimates of its transmission properties are necessary to interpret observations. Since direct measurements of the thermal conductivity of LiF at the appropriate conditions are difficult, we resort to molecular simulation methods. Using an empirical potential validated against ab initio phonon density of states, we estimate the thermal conductivity of LiF at high temperatures (1000–4000 K) and pressures (100–400 GPa) with the Green-Kubo method. We also compare these estimates to those derived directly from ab initio data. To ascertainmore » the correct phase of LiF at these extreme conditions, we calculate the (relative) phase stability of the B1 and B2 structures using a quasiharmonic ab initio model of the free energy. We also estimate the thermal conductivity of LiF in an uniaxial loading state that emulates initial stages of compression in high-stress ramp loading experiments and show the degree of anisotropy induced in the conductivity due to deformation.« less

On rate-dependent polycrystal deformation: the temperature sensitivity of cold dwell fatigue

PubMed Central

Zhang, Zhen; Cuddihy, M. A.; Dunne, F. P. E.

2015-01-01

A temperature and rate-dependent crystal plasticity framework has been used to examine the temperature sensitivity of stress relaxation, creep and load shedding in model Ti-6Al polycrystal behaviour under dwell fatigue conditions. A temperature close to 120°C is found to lead to the strongest stress redistribution and load shedding, resulting from the coupling between crystallographic slip rate and slip system dislocation hardening. For temperatures in excess of about 230°C, grain-level load shedding from soft to hard grains diminishes because of the more rapid stress relaxation, leading ultimately to the diminution of the load shedding and hence, it is argued, the elimination of the dwell debit. Under conditions of cyclic stress dwell, at temperatures between 20°C and 230°C for which load shedding occurs, the rate-dependent accumulation of local slip by ratcheting is shown to lead to the progressive cycle-by-cycle redistribution of stress from soft to hard grains. This phenomenon is termed cyclic load shedding since it also depends on the material's creep response, but develops over and above the well-known dwell load shedding, thus providing an additional rationale for the incubation of facet nucleation. PMID:26528078

Computational fluid dynamics modeling of bun baking process under different oven load conditions.

PubMed

Tank, A; Chhanwal, N; Indrani, D; Anandharamakrishnan, C

2014-09-01

A computational fluid dynamics (CFD) model was developed to study the temperature profile of the bun during baking process. Evaporation-condensation mechanism and effect of the latent heat during phase change of water was incorporated in this model to represent actual bun baking process. Simulation results were validated with experimental measurements of bun temperature at two different positions. Baking process is completed within 20 min, after the temperature of crumb become stable at 98 °C. Further, this study was extended to investigate the effect of partially (two baking trays) loaded and fully loaded (eight baking trays) oven on temperature profile of bun. Velocity and temperature profile differs in partially loaded and fully loaded oven. Bun placed in top rack showed rapid baking while bun placed in bottom rack showed slower baking due to uneven temperature distribution in the oven. Hence, placement of bun inside the oven affects temperature of bun and consequently, the quality of the product.

Effects of moisture, elevated temperature, and fatigue loading on the behavior of graphite/epoxy buffer strip panels with center cracks

NASA Technical Reports Server (NTRS)

Bigelow, C. A.

1988-01-01

The effects of fatigue loading combined with moisture and heat on the behavior of graphite epoxy panels with either Kevlar-49 or S-glass buffer strips were studied. Buffer strip panels, that had a slit in the center to represent damage, were moisture conditioned or heated, fatigue loaded, and then tested in tension to measure their residual strength. The buffer strips were parallel to the loading direction and were made by replacing narrow strips of the 0 deg graphite plies with Kevlar-49 epoxy or S-glass epoxy on a 1-for-1 basis. The panels were subjected to a fatigue loading spectrum. One group of panels was preconditioned by soaking in 60 C water to produce a 1 percent weight gain then tested at room temperature. One group was heated to 82 C during the fatigue loading. Another group was moisture conditioned and then tested at 82 C. The residual strengths of the buffer panels were not highly affected by the fatigue loading, the number of repetitions of the loading spectrum, or the maximum strain level. The moisture conditioning reduced the residual strengths of the S-glass buffer strip panel by 10 to 15 percent below the ambient results. The moisture conditioning did not have a large effect on the Kevlar-49 panels.

Effect of the load size on the efficiency of microwave heating under stop flow and continuous flow conditions.

PubMed

Patil, Narendra G; Rebrov, Evgeny V; Eränen, Kari; Benaskar, Faysal; Meuldijk, Jan; Mikkola, Jyri-Pekka; Hessel, Volker; Hulshof, Lumbertus A; Murzin, Dmitry Yu; Schouten, Jaap C

2012-01-01

A novel heating efficiency analysis of the microwave heated stop-flow (i.e. stagnant liquid) and continuous-flow reactors has been presented. The thermal losses to the surrounding air by natural convection have been taken into account for heating efficiency calculation of the microwave heating process. The effect of the load diameter in the range of 4-29 mm on the heating efficiency of ethylene glycol was studied in a single mode microwave cavity under continuous flow and stop-flow conditions. The variation of the microwave absorbing properties of the load with temperature was estimated. Under stop-flow conditions, the heating efficiency depends on the load diameter. The highest heating efficiency has been observed at the load diameter close to the half wavelength of the electromagnetic field in the corresponding medium. Under continuous-flow conditions, the heating efficiency increased linearly. However, microwave leakage above the propagation diameter restricted further experimentation at higher load diameters. Contrary to the stop-flow conditions, the load temperature did not raise monotonously from the inlet to outlet under continuous-flow conditions. This was due to the combined effect of lagging convective heat fluxes in comparison to volumetric heating. This severely disturbs the uniformity of the electromagnetic field in the axial direction and creates areas of high and low field intensity along the load Length decreasing the heating efficiency as compared to stop-flow conditions.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nemec, Patrik, E-mail: patrik.nemec@fstroj.uniza.sk; Malcho, Milan, E-mail: milan.malcho@fstroj.uniza.sk

This work deal with experimental evaluation of cooling efficiency of cooling device capable transfer high heat fluxes from electric elements to the surrounding. The work contain description of cooling device, working principle of cooling device, construction of cooling device. Experimental part describe the measuring method of device cooling efficiency evaluation. The work results are presented in graphic visualization of temperature dependence of the contact area surface between cooling device evaporator and electronic components on the loaded heat of electronic components in range from 250 to 740 W and temperature dependence of the loop thermosiphon condenser surface on the loaded heatmore » of electronic components in range from 250 to 740 W.« less

Large-Strain Transparent Magnetoactive Polymer Nanocomposites

NASA Technical Reports Server (NTRS)

Meador, Michael A.

2012-01-01

A document discusses polymer nano - composite superparamagnetic actuators that were prepared by the addition of organically modified superparamagnetic nanoparticles to the polymer matrix. The nanocomposite films exhibited large deformations under a magnetostatic field with a low loading level of 0.1 wt% in a thermoplastic polyurethane elastomer (TPU) matrix. The maximum actuation deformation of the nanocomposite films increased exponentially with increasing nanoparticle concentration. The cyclic deformation actuation of a high-loading magnetic nanocomposite film was examined in a low magnetic field, and it exhibited excellent reproducibility and controllability. Low-loading TPU nanocomposite films (0.1-2 wt%) were transparent to semitransparent in the visible wavelength range, owing to good dispersion of the magnetic nanoparticles. Magnetoactuation phenomena were also demonstrated in a high-modulus, high-temperature polyimide resin with less mechanical deformation.

High pressure and high temperature apparatus

DOEpatents

Voronov, Oleg A.

2005-09-13

A design for high pressure/high temperature apparatus and reaction cell to achieve .about.30 GPa pressure in .about.1 cm volume and .about.100 GPa pressure in .about.1 mm volumes and 20-5000.degree. C. temperatures in a static regime. The device includes profiled anvils (28) action on a reaction cell (14, 16) containing the material (26) to be processed. The reaction cell includes a heater (18) surrounded by insulating layers and screens. Surrounding the anvils are cylindrical inserts and supporting rings (30-48) whose hardness increases towards the reaction cell. These volumes may be increased considerably if applications require it, making use of presses that have larger loading force capability, larger frames and using larger anvils.

Electrical contact structures for solid oxide electrolyte fuel cell

DOEpatents

Isenberg, Arnold O.

1984-01-01

An improved electrical output connection means is provided for a high temperature solid oxide electrolyte type fuel cell generator. The electrical connection of the fuel cell electrodes to the electrical output bus, which is brought through the generator housing to be connected to an electrical load line maintains a highly uniform temperature distribution. The electrical connection means includes an electrode bus which is spaced parallel to the output bus with a plurality of symmetrically spaced transversely extending conductors extending between the electrode bus and the output bus, with thermal insulation means provided about the transverse conductors between the spaced apart buses. Single or plural stages of the insulated transversely extending conductors can be provided within the high temperatures regions of the fuel cell generator to provide highly homogeneous temperature distribution over the contacting surfaces.

Novel chitosan derivative for temperature and ultrasound dual-sensitive liposomal microbubble gel.

PubMed

Chen, Daquan; Yu, Hongyun; Mu, Hongjie; Wei, Junhua; Song, Zhenkun; Shi, Hong; Liang, Rongcai; Sun, Kaoxiang; Liu, Wanhui

2013-04-15

In this study, a novel liposome-loaded microbubble gel based on N-cholesteryl hemisuccinate-O-sulfate chitosan (NCHOSC) was designed. The structure of the NCHOSC was characterized by FTIR and (1)H NMR. The liposomal microbubble gel based on NCHOSC with a high encapsulation efficiency of curcumin was formed and improved the solubility of curcumin. The diameter of most liposomal microbubble was about 950 nm. The temperature-sensitive CS/GP gel could be formulated at room temperature and would form a gel at body temperature. Simultaneously, the ultrasound-sensitive induced release of curcumin was 85% applying ultrasound. The results of cytotoxicity assay indicated that encapsulated curcumin in Cur-LM or Cur-LM-G was less toxic. The anti-tumor efficacy in vivo suggested that Cur-LM-G by ultrasound suppressed tumor growth most efficiently. These findings have shed some light on the potential NCHOSC material used to liposome-loaded microbubble gel for temperature and ultrasound dual-sensitive drug delivery. Copyright © 2013 Elsevier Ltd. All rights reserved.

Probing structural transition and guest dynamics of hydroquinone clathrates by temperature-dependent terahertz time-domain spectroscopy.

PubMed

Lee, Eui Su; Han, Kyu Won; Yoon, Ji-Ho; Jeon, Tae-In

2011-01-13

The structural transition from hydroquinone clathrates to crystalline α-form hydroquinone was observed up to the range of 3 THz frequency as a function of temperatures. We found that all three hydroquinone clathrates, CO(2)-, CH(4)-, and CO(2)/CH(4)-loaded hydroquinone clathrates, transform into the α-form hydroquinone at around 102 ± 7 °C. The resonance peak of the CO(2)-loaded hydroquinone clathrate at 2.15 THz decreases with increasing temperature, indicating that CO(2) guest molecules are readily released from the host framework prior to the structural transformation. This reveals that the hydroquinone clathrates may transform into the stable α-form hydroquinone via the metastable form of guest-free clathrate, which depends on guest molecules enclathrated in the cages of the host frameworks. A strong resonance of the α-form hydroquinone at 1.18 THz gradually shifts to the low frequency with increasing temperature and shifts back to the high frequency with decreasing temperature.

Mechanical behaviour of TWIP steel under shear loading

NASA Astrophysics Data System (ADS)

Vincze, G.; Butuc, M. C.; Barlat, F.

2016-08-01

Twinning induced plasticity steels (TWIP) are very good candidate for automotive industry applications because they potentially offer large energy absorption before failure due to their exceptional strain hardening capability and high strength. However, their behaviour is drastically influenced by the loading conditions. In this work, the mechanical behaviour of a TWIP steel sheet sample was investigated at room temperature under monotonic and reverse simple shear loading. It was shown that all the expected features of load reversal such as Bauschinger effect, transient strain hardening with high rate and permanent softening, depend on the prestrain level. This is in agreement with the fact that these effects, which occur during reloading, are related to the rearrangement of the dislocation structure induced during the predeformation. The homogeneous anisotropic hardening (HAH) approach proposed by Barlat et al. (2011) [1] was successfully employed to predict the experimental results.

Mechanistic basis of temperature-dependent dwell fatigue in titanium alloys

NASA Astrophysics Data System (ADS)

Zheng, Zebang; Balint, Daniel S.; Dunne, Fionn P. E.

2017-10-01

The temperature-dependent dwell sensitivity of Ti-6242 and Ti-6246 alloys has been assessed over a temperature range from - 50∘ C to 390 °C using discrete dislocation plasticity which incorporates both thermal activation of dislocation escape from obstacles and slip transfer across grain boundaries. The worst-case load shedding in Ti-6242 alloy is found to be at or close to 120 °C under dwell fatigue loading, which diminishes and vanishes at temperatures lower than - 50∘ C or higher than 230 °C. Load shedding behaviour is predicted to occur in alloy Ti-6246 also but over a range of higher temperatures which are outside those relevant to in-service conditions. The key controlling dislocation mechanism with respect to load shedding in titanium alloys, and its temperature sensitivity, is shown to be the time constant associated with the thermal activation of dislocation escape from obstacles, with respect to the stress dwell time. The mechanistic basis of load shedding and dwell sensitivity in dwell fatigue loading is presented and discussed in the context of experimental observations.

Effects of Stoichiometry on Transformation Temperatures and Actuator-Type Performance of NiTiPd and NiTiPdX High-Temperature Shape Memory Alloys

NASA Technical Reports Server (NTRS)

Bigelow, Glen S.; Gaydosh, Darrell; Garg, Anita; Padula, Santo A., II; Noebe, Ronald D.

2007-01-01

High-temperature shape memory NiTiPd and NiTiPdX (X=Au, Pt, Hf) alloys were produced with titanium equivalent (Ti+Hf) compositions of 50.5, 50.0, 49.5, and 49.0 at.%. Thermo-mechanical testing in compression was used to evaluate the transformation temperatures, transformation strain, work output, and permanent deformation behavior of each alloy to study the effects of quaternary alloying and stoichiometry on high-temperature shape memory alloy behavior. Microstructural evaluation showed the presence of second phases for all alloy compositions. No load transformation temperatures in the stoichiometric alloys were relatively unchanged by Au and Pt substitutions, while the substitution of Hf for Ti causes a drop in transformation temperatures. The NiTiPd, NiTiPdAu and NiTiPdHf alloys exhibited transformation temperatures that were highest in the Ti-rich compositions, slightly lower at stoichiometry, and significantly reduced when the Ti equivalent composition was less than 50 at.%. For the NiTiPdPt alloy, transformation temperatures were highest for the Ti-rich compositions, lowest at stoichiometry, and slightly higher in the Ni-rich composition. When thermally cycled under constant stresses of up to 300 MPa, all of the alloys had transformation strains, and therefore work outputs, which increased with increasing stress. In each series of alloys, the transformation strain and thus work output was highest for stoichiometric or Ti-rich compositions while permanent strain associated with the constant-load thermal cycling was lowest for alloys with Ni-equivalent-rich compositions. Based on these results, basic rules for optimizing the composition of NiTiPd alloys for actuator performance will be discussed.

Mechanical properties of ZrB2- and HfB2-based ultra-high temperature ceramics fabricated by spark plasma sintering

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zapata-Solvas, E.; Jayaseelan, D.; Lin, Hua-Tay

2013-01-01

Flexural strengths at room temperature, at 1400 C in air and at room temperature after 1 h oxidation at 1400 C were determined for ZrB2- and HfB2-based ultra-high temperature ceramics (UHTCs). Defects caused by electrical discharge machining (EDM) lowered measured strengths significantly and were used to calculate fracture toughness via a fracture mechanics approach. ZrB2 with 20 vol.% SiC had room temperature strength of 700 90 MPa, fracture toughness of 6.4 0.6 MPa, Vickers hardness at 9.8 N load of 21.1 0.6 GPa, 1400 C strength of 400 30 MPa and room temperature strength after 1 h oxidation at 1400more » C of 678 15 MPa with an oxide layer thickness of 45 5 m. HfB2 with 20 vol.% SiC showed room temperature strength of 620 50 MPa, fracture toughness of 5.0 0.4 MPa, Vickers hardness at 9.8 N load of 27.0 0.6 GPa, 1400 C strength of 590 150 MPa and room temperature strength after 1 h oxidation at 1400 C of 660 25 MPa with an oxide layer thickness of 12 1 m. 2 wt.% La2O3 addition to UHTCs slightly reduced mechanical performance while increasing tolerance to property degradation after oxidation and effectively aided internal stress relaxation during spark plasma sintering (SPS) cooling, as quantified by X-ray diffraction (XRD). Slow crack growth was suggested as the failure mechanism at high temperatures as a consequence of sharp cracks formation during oxidation.« less

PS300 Tribomaterials Evaluated at 6500C by Bushing Test Rig

NASA Technical Reports Server (NTRS)

Striebing, Donald R.; DellaCorte, Christopher

2004-01-01

A new facility has been developed to test the tribological behavior (friction and wear) of PS300 solid lubricant bushings at high temperatures. PS300 is a commercially available solid lubricant invented at the NASA Glenn Research Center. It can be prepared as a plasma spray coating or as a free-standing powder metallurgy component, designated PM300. PS300 and PM300 composites are designed to lubricate sliding components at temperatures above the capability of today's best oils, greases, and solid lubricants. One of the primary applications being pursued for PM300 is the development of bushings for use in high-temperature machinery. Examples include inlet guide vane bushings for gas turbines and conveyors, and bearings for industrial furnaces and ovens. Encouraging preliminary field trials indicate that PS300 and PM300 lubricant materials have been commercialized successfully in several industrial applications. However, the lack of laboratory performance data has hindered further commercialization especially for new applications that differ significantly from the established experience base. The purpose of the newly developed bushing test rig will be to determine the performance characteristics of PM300, and other materials, under conditions closely matching intended applications. The data will be used to determine engineering friction and wear rates and to estimate the life expectancy of bushings for new applications. In the new rig, the bushing is loaded against a rotating shaft inside a furnace enclosure (see the preceding photograph). Loads can vary from 5 to 200 N, speeds from 1 to 400 rpm, and temperatures from 25 to 800 C. Furnace temperature, bushing temperature, shaft speed, and torque are monitored during the test, and wear of both the bushing and the shaft is measured after testing is completed. Initially, PM300 bushings will be evaluated and compared with lower temperature, traditional bushing materials like graphite and porous bronze. The baseline PM304 composition is 60 wt% NiCr (a binder), 20 wt% Cr2O3 (a hardener), 10 wt% BaF2/CaF2 (a high-temperature lubricant), and 10 wt% Ag (a low-temperature lubricant). Future research efforts will include determining the effects of load, sliding speed, and temperature on tribological performance and, possibly, tailoring composition for specific applications. We expect that the availability of measured performance data will enhance the market penetration of PM300 technology.

Fixed target matrix for femtosecond time-resolved and in situ serial micro-crystallography

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mueller, C.; Marx, A.; Epp, S. W.

We present a crystallography chip enabling in situ room temperature crystallography at microfocus synchrotron beamlines and X-ray free-electron laser (X-FEL) sources. Compared to other in situ approaches, we observe extremely low background and high diffraction data quality. The chip design is robust and allows fast and efficient loading of thousands of small crystals. The ability to load a large number of protein crystals, at room temperature and with high efficiency, into prescribed positions enables high throughput automated serial crystallography with microfocus synchrotron beamlines. In addition, we demonstrate the application of this chip for femtosecond time-resolved serial crystallography at the Linacmore » Coherent Light Source (LCLS, Menlo Park, California, USA). As a result, the chip concept enables multiple images to be acquired from each crystal, allowing differential detection of changes in diffraction intensities in order to obtain high signal-to-noise and fully exploit the time resolution capabilities of XFELs.« less

Fixed target matrix for femtosecond time-resolved and in situ serial micro-crystallography

DOE PAGES

Mueller, C.; Marx, A.; Epp, S. W.; ...

2015-08-18

We present a crystallography chip enabling in situ room temperature crystallography at microfocus synchrotron beamlines and X-ray free-electron laser (X-FEL) sources. Compared to other in situ approaches, we observe extremely low background and high diffraction data quality. The chip design is robust and allows fast and efficient loading of thousands of small crystals. The ability to load a large number of protein crystals, at room temperature and with high efficiency, into prescribed positions enables high throughput automated serial crystallography with microfocus synchrotron beamlines. In addition, we demonstrate the application of this chip for femtosecond time-resolved serial crystallography at the Linacmore » Coherent Light Source (LCLS, Menlo Park, California, USA). As a result, the chip concept enables multiple images to be acquired from each crystal, allowing differential detection of changes in diffraction intensities in order to obtain high signal-to-noise and fully exploit the time resolution capabilities of XFELs.« less

Outstanding compressive creep strength in Cr/Ir-codoped (Mo0.85Nb0.15)Si2 crystals with the unique cross-lamellar microstructure.

PubMed

Hagihara, Koji; Ikenishi, Takaaki; Araki, Haruka; Nakano, Takayoshi

2017-06-21

A (Mo 0.85 Nb 0.15 )Si 2 crystal with an oriented, lamellar, C40/C11 b two-phase microstructure is a promising ultrahigh-temperature (UHT) structural material, but its low room-temperature fracture toughness and low high-temperature strength prevent its practical application. As a possibility to overcome these problems, we first found a development of unique "cross-lamellar microstructure", by the cooping of Cr and Ir. The cross-lamellar microstructure consists of a rod-like C11 b -phase grains that extend along a direction perpendicular to the lamellar interface in addition to the C40/C11 b fine lamellae. In this study, the effectiveness of the cross-lamellar microstructure for improving the high-temperature creep deformation property, being the most essential for UHT materials, was examined by using the oriented crystals. The creep rate significantly reduced along a loading orientation parallel to the lamellar interface. Furthermore, the degradation in creep strength for other loading orientation that is not parallel to the lamellar interface, which has been a serious problem up to now, was also suppressed. The results demonstrated that the simultaneous improvement of high-temperature creep strength and room temperature fracture toughness can be first accomplished by the development of unique cross-lamellar microstructure, which opens a potential avenue for the development of novel UHT materials as alternatives to existing Ni-based superalloys.

A Compact, Continuous Adiabatic Demagnetization Refrigerator with High Heat Sink Temperature

NASA Technical Reports Server (NTRS)

Shirron, P. J.; Canavan, E. R.; DiPirro, M. J.; Jackson, M.; Tuttle, J. G.

2003-01-01

In the continuous adiabatic demagnetization refrigerator (ADR), the existence of a constant temperature stage attached to the load breaks the link between the requirements of the load (usually a detector array) and the operation of the ADR. This allows the ADR to be cycled much faster, which yields more than an order of magnitude improvement in cooling power density over single-shot ADRs. Recent effort has focused on developing compact, efficient higher temperature stages. An important part of this work has been the development of passive gas-gap heat switches that transition (from conductive to insulating) at temperatures around 1 K and 4 K without the use of an actively heated getter. We have found that by carefully adjusting available surface area and the number of He-3 monolayers, gas-gap switches can be made to operate passively. Passive operation greatly reduces switching time and eliminates an important parasitic heat load. The current four stage ADR provides 6 micro W of cooling at 50 mK (21 micro W at 100 mK) and weighs less than 8 kg. It operates from a 4.2 K heat sink, which can be provided by an unpumped He bath or many commercially available mechanical cryocoolers. Reduction in critical current with temperature in our fourth stage NbTi magnet presently limits the maximum temperature of our system to approx. 5 K. We are developing compact, low-current Nb3Sn magnets that will raise the maximum heat sink temperature to over 10 K.

Durability and Damage Development in Woven Ceramic Matrix Composites

NASA Technical Reports Server (NTRS)

Haque, A.; Rahman, M.; Tyson, O. Z.; Jeelani, S.; Verrilli, Michael J. (Technical Monitor)

2001-01-01

Damage development in woven SiC/SiNC ceramic matrix composites (CMC's) under tensile and cyclic loading both at room and elevated temperatures have been investigated for the exhaust nozzle of high-efficient turbine engines. The ultimate strength, failure strain, proportional limit and modulus data at a temperature range of 23 to 1250 C are generated. The tensile strength of SiC/SiNC woven composites have been observed to increase with increased temperatures up to 1000 C. The stress/strain plot shows a pseudo-yield point at 25 percent of the failure strain (epsilon(sub r)) which indicates damage initiation in the form of matrix cracking. The evolution of damage beyond 0.25 epsilon(sub f), both at room and elevated temperature comprises multiple matrix cracking, interfacial debonding, and fiber pullout. Although the nature of the stress/strain plot shows damage-tolerant behavior under static loading both at room and elevated temperature, the life expectancy of SiC/SiNC composites degrades significantly under cyclic loading at elevated temperature. This is mostly due to the interactions of fatigue damage caused by the mechanically induced plastic strain and the damage developed by the creep strain. The in situ damage evolutions are monitored by acoustic event parameters, ultrasonic C-scan and stiffness degradation. Rate equations for modulus degradation and fatigue life prediction of ceramic matrix composites both at room and elevated temperatures are developed. These rate equations are observed to show reasonable agreement with experimental results.

Improved Regression Analysis of Temperature-Dependent Strain-Gage Balance Calibration Data

NASA Technical Reports Server (NTRS)

Ulbrich, N.

2015-01-01

An improved approach is discussed that may be used to directly include first and second order temperature effects in the load prediction algorithm of a wind tunnel strain-gage balance. The improved approach was designed for the Iterative Method that fits strain-gage outputs as a function of calibration loads and uses a load iteration scheme during the wind tunnel test to predict loads from measured gage outputs. The improved approach assumes that the strain-gage balance is at a constant uniform temperature when it is calibrated and used. First, the method introduces a new independent variable for the regression analysis of the balance calibration data. The new variable is designed as the difference between the uniform temperature of the balance and a global reference temperature. This reference temperature should be the primary calibration temperature of the balance so that, if needed, a tare load iteration can be performed. Then, two temperature{dependent terms are included in the regression models of the gage outputs. They are the temperature difference itself and the square of the temperature difference. Simulated temperature{dependent data obtained from Triumph Aerospace's 2013 calibration of NASA's ARC-30K five component semi{span balance is used to illustrate the application of the improved approach.

Strain measurements in a rotary engine housing

NASA Technical Reports Server (NTRS)

Lee, C. M.; Bond, T. H.; Addy, H. E.; Chun, K. S.; Lu, C. Y.

1989-01-01

The development of structural design tools for Rotary Combustion Engines (RCE) using Finite Element Modeling (FEM) requires knowledge about the response of engine materials to various service conditions. This paper describes experimental work that studied housing deformation as a result of thermal, pressure and mechanical loads. The measurement of thermal loads, clamping pressure, and deformation was accomplished by use of high-temperature strain gauges, thermocouples, and a high speed data acquisition system. FEM models for heat transfer stress analysis of the rotor housing will be verified and refined based on these experimental results.

Steady-state temperature determination on the base of hysteresis loop energy for CuZn37 brass

NASA Astrophysics Data System (ADS)

Lipski, Adam; Skibicki, Dariusz; Pejkowski, Łukasz

2017-03-01

This paper presents the verification of the relationship between the temperature and the hysteresis loop energy for the CuZn37 brass under multiaxial fatigue loading. Fatigue tests were performed on the hollow specimens subjected to fully reversed tension-compression, torsion, proportional loading, 90° out-of-phase non-proportional loading and two another non-proportional loadings with frequency differences. All test were strain-controlled. Calculations of a plastic strain energy were based on midlife strain hysteresis loops data. The calculated specimen temperatures were compared with temperatures observed by thermographic camera.

Seasonal variation in coat characteristics, tick loads, cortisol levels, some physiological parameters and temperature humidity index on Nguni cows raised in low- and high-input farms

NASA Astrophysics Data System (ADS)

Katiyatiya, C. L. F.; Muchenje, V.; Mushunje, A.

2015-06-01

Seasonal variations in hair length, tick loads, cortisol levels, haematological parameters (HP) and temperature humidity index (THI) in Nguni cows of different colours raised in two low-input farms, and a commercial stud was determined. The sites were chosen based on their production systems, climatic characteristics and geographical locations. Zazulwana and Komga are low-input, humid-coastal areas, while Honeydale is a high-input, dry-inland Nguni stud farm. A total of 103 cows, grouped according to parity, location and coat colour, were used in the study. The effects of location, coat colour, hair length and season were used to determine tick loads on different body parts, cortisol levels and HP in blood from Nguni cows. Highest tick loads were recorded under the tail and the lowest on the head of each of the animals ( P < 0.05). Zazulwana cows recorded the highest tick loads under the tails of all the cows used in the study from the three farms ( P < 0.05). High tick loads were recorded for cows with long hairs. Hair lengths were longest during the winter season in the coastal areas of Zazulwana and Honeydale ( P < 0.05). White and brown-white patched cows had significantly longer ( P < 0.05) hair strands than those having a combination of red, black and white colour. Cortisol and THI were significantly lower ( P < 0.05) in summer season. Red blood cells, haematoglobin, haematocrit, mean cell volumes, white blood cells, neutrophils, lymphocytes, eosinophils and basophils were significantly different ( P < 0.05) as some associated with age across all seasons and correlated to THI. It was concluded that the location, coat colour and season had effects on hair length, cortisol levels, THI, HP and tick loads on different body parts and heat stress in Nguni cows.

Operating experience with the southwire 30-meter high-temperature superconducting power cable

NASA Astrophysics Data System (ADS)

Stovall, J. P.; Lue, J. W.; Demko, J. A.; Fisher, P. W.; Gouge, M. J.; Hawsey, R. A.; Armstrong, J. W.; Hughey, R. L.; Lindsay, D. T.; Roden, M. L.; Sinha, U. K.; Tolbert, J. C.

2002-05-01

Southwire Company is operating a high-temperature superconducting (HTS) cable system at its corporate headquarters. The 30-m long, 3-phase cable system is powering three Southwire manufacturing plants and is rated at 12.4-kV, 1250-A, 60-Hz. Cooling is provided by a pressurized liquid nitrogen system operating at 70-80 K. The cables were energized on January 5, 2000 for on-line testing and operation and in April 2000 were placed into extended service. As of June 1, 2001, the HTS cables have provided 100% of the customer load for 8000 hours. The cryogenic system has been in continuous operation since November 1999. The HTS cable system has not been the cause of any power outages to the average 20 MW industrial load served by the cable. The cable has been exposed to short-circuit currents caused by load-side faults without damage. Based upon field measurements described herein, the cable critical current-a key performance parameter-remains the same and has not been affected by the hours of real-world operation, further proving the viability of this promising technology.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Winter, Lea R.; Gomez, Elaine; Yan, Binhang

CO 2 hydrogenation over Fe-modified Ni/CeO 2 catalysts was investigated in a batch reactor using time-resolved in situ FTIR spectroscopy. Low loading of Ni/CeO 2 was associated with high selectivity to CO over CH 4, while higher Ni loading improved CO 2 hydrogenation activity with a reduced CO selectivity. X-ray absorption near-edge structure (XANES) analysis revealed Ni to be metallic for all catalysts including the CO-selective low loading 0.5% Ni catalyst, suggesting that the selectivity trend is due to structural rather than oxidation state effects. The loading amount of 1.5% Ni was selected for co-impregnation with Fe, based on themore » significant shift in product selectivity towards CH 4 for that loading amount, in order to shift the selectivity towards CO while maintaining high activity. Temperature programmed reduction (TPR) results indicated bimetallic interactions between Ni and Fe, and XANES analysis showed that about 70% of Fe in the bimetallic catalysts was oxidized. The Ni-Fe catalysts demonstrated improved selectivity towards CO without significantly compromising activity, coupling the high activity of Ni catalysts and the high CO selectivity of Fe. The general trends in Ni loading and bimetallic modification should guide efforts to develop non-precious metal catalysts for the selective production of CO by CO 2 hydrogenation.« less

77 FR 64249 - Track Safety Standards; Improving Rail Integrity

Federal Register 2010, 2011, 2012, 2013, 2014

2012-10-19

... specific problems. This is a result of high traffic volumes that load the rail and accelerate defect growth... influenced by tonnage. Rapid growth rates can also be associated with rail where high-tensile residual stresses are present in the railhead and in CWR in lower temperature ranges where the rail is in high...

Rugged switch responds to minute pressure differentials

NASA Technical Reports Server (NTRS)

Friend, L. C.; Shaub, K. D.

1967-01-01

Pressure responsive switching device exhibits high sensitivity but is extremely rugged and resistant to large amplitude shock and velocity loading. This snap-action, single pole-double throw switch operates over a wide temperature range.

Structural efficiencies of various aluminum, titanium, and steel alloys at elevated temperatures

NASA Technical Reports Server (NTRS)

Heimerl, George J; Hughes, Philip J

1953-01-01

Efficient temperature ranges are indicated for two high-strength aluminum alloys, two titanium alloys, and three steels for some short-time compression-loading applications at elevated temperatures. Only the effects of constant temperatures and short exposure to temperature are considered, and creep is assumed not to be a factor. The structural efficiency analysis is based upon preliminary results of short-time elevated-temperature compressive stress-strain tests of the materials. The analysis covers strength under uniaxial compression, elastic stiffness, column buckling, and the buckling of long plates in compression or in shear.

Thermal performance of phase change wallboard for residential cooling application

DOE Office of Scientific and Technical Information (OSTI.GOV)

Feustel, H.E.; Stetiu, C.

1997-04-01

Cooling of residential California buildings contributes significantly to electrical consumption and peak power demand mainly due to very poor load factors in milder climates. Thermal mass can be utilized to reduce the peak-power demand, downsize the cooling systems, and/or switch to low-energy cooling sources. Large thermal storage devices have been used in the past to overcome the shortcomings of alternative cooling sources, or to avoid high demand charges. The manufacturing of phase change material (PCM) implemented in gypsum board, plaster or other wall-covering material, would permit the thermal storage to become part of the building structure. PCMs have two importantmore » advantages as storage media: they can offer an order-of-magnitude increase in thermal storage capacity, and their discharge is almost isothermal. This allows the storage of high amounts of energy without significantly changing the temperature of the room envelope. As heat storage takes place inside the building, where the loads occur, rather than externally, additional transport energy is not required. RADCOOL, a thermal building simulation program based on the finite difference approach, was used to numerically evaluate the latent storage performance of treated wallboard. Extended storage capacity obtained by using double PCM-wallboard is able to keep the room temperatures close to the upper comfort limits without using mechanical cooling. Simulation results for a living room with high internal loads and weather data for Sunnyvale, California, show significant reduction of room air temperature when heat can be stored in PCM-treated wallboards.« less

Combined Space and Water Heating: Next Steps to Improved Performance

DOE Office of Scientific and Technical Information (OSTI.GOV)

B. Schoenbauer; Bohac, D.; Huelman, P.

2016-07-13

A combined space- and water-heating (combi) system uses a high-efficiency direct-vent burner that eliminates safety issues associated with natural draft appliances. Past research with these systems shows that using condensing water heaters or boilers with hydronic air handling units can provide both space and water heating with efficiencies of 90% or higher. Improved controls have the potential to reduce complexity and improve upon the measured performance. This project demonstrates that controls can significantly benefit these first-generation systems. Laboratory tests and daily load/performance models showed that the set point temperature reset control produced a 2.1%–4.3% (20–40 therms/year) savings for storage andmore » hybrid water heater combi systems operated in moderate-load homes. The full modulation control showed additional savings over set point control (in high-load homes almost doubling the savings: 4%–5% over the no-control case). At the time of installation the reset control can be implemented for $200–$400, which would provide paybacks of 6–25 years for low-load houses and 3–15 years for high-load houses. Full modulation implementation costs would be similar to the outdoor reset and would provide paybacks of 5-½–20 years for low-load houses and 2-½–10 years for high-load houses.« less

Geoengineering as an optimization problem

NASA Astrophysics Data System (ADS)

Ban-Weiss, George A.; Caldeira, Ken

2010-07-01

There is increasing evidence that Earth's climate is currently warming, primarily due to emissions of greenhouse gases from human activities, and Earth has been projected to continue warming throughout this century. Scientists have begun to investigate the potential for geoengineering options for reducing surface temperatures and whether such options could possibly contribute to environmental risk reduction. One proposed method involves deliberately increasing aerosol loading in the stratosphere to scatter additional sunlight to space. Previous modeling studies have attempted to predict the climate consequences of hypothetical aerosol additions to the stratosphere. These studies have shown that this method could potentially reduce surface temperatures, but could not recreate a low-CO2 climate in a high-CO2 world. In this study, we attempt to determine the latitudinal distribution of stratospheric aerosols that would most closely achieve a low-CO2 climate despite high CO2 levels. Using the NCAR CAM3.1 general circulation model, we find that having a stratospheric aerosol loading in polar regions higher than that in tropical regions leads to a temperature distribution that is more similar to the low-CO2 climate than that yielded by a globally uniform loading. However, such polar weighting of stratospheric sulfate tends to degrade the degree to which the hydrological cycle is restored, and thus does not markedly contribute to improved recovery of a low-CO2 climate. In the model, the optimal latitudinally varying aerosol distributions diminished the rms zonal mean land temperature change from a doubling of CO2 by 94% and the rms zonal mean land precipitation minus evaporation change by 74%. It is important to note that this idealized study represents a first attempt at optimizing the engineering of climate using a general circulation model; uncertainties are high and not all processes that are important in reality are modeled.

A Method for Studying the Temperature Dependence of Dynamic Fracture and Fragmentation.

PubMed

Jones, David R; Chapman, David J; Eakins, Daniel E

2015-06-28

The dynamic fracture of a body is a late-stage phenomenon typically studied under simplified conditions, in which a sample is deformed under uniform stress and strain rate. This can be produced by evenly loading the inner surface of a cylinder. Due to the axial symmetry, as the cylinder expands the wall is placed into a tensile hoop stress that is uniform around the circumference. While there are various techniques to generate this expansion such as explosives, electromagnetic drive, and existing gas gun techniques they are all limited in the fact that the sample cylinder must be at room temperature. We present a new method using a gas gun that facilitates experiments on cylinders from 150 K to 800 K with a consistent, repeatable loading. These highly diagnosed experiments are used to examine the effect of temperature on the fracture mechanisms responsible for failure, and their resulting influence on fragmentation statistics. The experimental geometry employs a steel ogive located inside the target cylinder, with the tip located about halfway in. A single stage light gas gun is then used to launch a polycarbonate projectile into the cylinder at 1,000 m/sec(-1). The projectile impacts and flows around the rigid ogive, driving the sample cylinder from the inside. The use of a non-deforming ogive insert allows us to install temperature control hardware inside the rear of the cylinder. Liquid nitrogen (LN₂) is used for cooling and a resistive high current load for heating. Multiple channels of upshifted photon Doppler velocimetry (PDV) track the expansion velocity along the cylinder enabling direct comparison to computer simulations, while High speed imaging is used to measure the strain to failure. The recovered cylinder fragments are also subject to optical and electron microscopy to ascertain the failure mechanism.

A Method for Studying the Temperature Dependence of Dynamic Fracture and Fragmentation

PubMed Central

Jones, David R.; Chapman, David J.; Eakins, Daniel E.

2015-01-01

The dynamic fracture of a body is a late-stage phenomenon typically studied under simplified conditions, in which a sample is deformed under uniform stress and strain rate. This can be produced by evenly loading the inner surface of a cylinder. Due to the axial symmetry, as the cylinder expands the wall is placed into a tensile hoop stress that is uniform around the circumference. While there are various techniques to generate this expansion such as explosives, electromagnetic drive, and existing gas gun techniques they are all limited in the fact that the sample cylinder must be at room temperature. We present a new method using a gas gun that facilitates experiments on cylinders from 150 K to 800 K with a consistent, repeatable loading. These highly diagnosed experiments are used to examine the effect of temperature on the fracture mechanisms responsible for failure, and their resulting influence on fragmentation statistics. The experimental geometry employs a steel ogive located inside the target cylinder, with the tip located about halfway in. A single stage light gas gun is then used to launch a polycarbonate projectile into the cylinder at 1,000 m/sec-1. The projectile impacts and flows around the rigid ogive, driving the sample cylinder from the inside. The use of a non-deforming ogive insert allows us to install temperature control hardware inside the rear of the cylinder. Liquid nitrogen (LN2) is used for cooling and a resistive high current load for heating. Multiple channels of upshifted photon Doppler velocimetry (PDV) track the expansion velocity along the cylinder enabling direct comparison to computer simulations, while High speed imaging is used to measure the strain to failure. The recovered cylinder fragments are also subject to optical and electron microscopy to ascertain the failure mechanism. PMID:26168019

Root cause analysis of oxide scale forming and shedding in high temperature reheater of a 200MW super high pressure boiler

NASA Astrophysics Data System (ADS)

Bo, Jiang; Hao, Weidong; Hu, Zhihong; Liu, Fuguo

2015-12-01

In order to solve the problem of over temperature tube-burst caused by oxide scale shedding and blocking tubes of high temperature reheater of a 200MW super high pressure power plant boiler, this paper expounds the mechanism of scale forming and shedding, and analyzes the probable causes of the tube-burst failure. The results show that the root cause of scale forming is that greater steam extraction flow after reforming of the second extraction leads to less steam flow into reheater, which causes over temperature to some of the heated tubes; and the root cause of scale shedding is that long term operation in AGC-R mode brings about great fluctuations of unit load, steam temperature and pressure, accelerating scale shedding. In conclusion, preventive measures are drawn up considering the operation mode of the unit.

UO{sub 2} and PuO{sub 2} utilization in high temperature engineering test reactor with helium coolant

DOE Office of Scientific and Technical Information (OSTI.GOV)

Waris, Abdul, E-mail: awaris@fi.itb.ac.id; Novitrian,; Pramuditya, Syeilendra

High temperature engineering test reactor (HTTR) is one of high temperature gas cooled reactor (HTGR) types which has been developed by Japanese Atomic Energy Research Institute (JAERI). The HTTR is a graphite moderator, helium gas coolant, 30 MW thermal output and 950 °C outlet coolant temperature for high temperature test operation. Original HTTR uses UO{sub 2} fuel. In this study, we have evaluated the use of UO{sub 2} and PuO{sub 2} in form of mixed oxide (MOX) fuel in HTTR. The reactor cell calculation was performed by using SRAC 2002 code, with nuclear data library was derived from JENDL3.2. Themore » result shows that HTTR can obtain its criticality condition if the enrichment of {sup 235}U in loaded fuel is 18.0% or above.« less

The effect of temperature, gradient, and load carriage on oxygen consumption, posture, and gait characteristics.

PubMed

Hinde, Katrina; Lloyd, Ray; Low, Chris; Cooke, Carlton

2017-03-01

The purpose of this experiment was to evaluate the effect of load carriage in a range of temperatures to establish the interaction between cold exposure, the magnitude of change from unloaded to loaded walking and gradient. Eleven participants (19-27 years) provided written informed consent before performing six randomly ordered walking trials in six temperatures (20, 10, 5, 0, -5, and -10 °C). Trials involved two unloaded walking bouts before and after loaded walking (18.2 kg) at 4 km · h -1 , on 0 and 10% gradients in 4 min bouts. The change in absolute oxygen consumption (V̇O 2 ) from the first unloaded bout to loaded walking was similar across all six temperatures. When repeating the second unloaded bout, V̇O 2 at both -5 and -10 °C was greater compared to the first. At -10 °C, V̇O 2 was increased from 1.60 ± 0.30 to 1.89 ± 0.51 L · min -1 . Regardless of temperature, gradient had a greater effect on V̇O 2 and heart rate (HR) than backpack load. HR was unaffected by temperature. Stride length (SL) decreased with decreasing temperature, but trunk forward lean was greater during cold exposure. Decreased ambient temperature did not influence the magnitude of change in V̇O 2 from unloaded to loaded walking. However, in cold temperatures, V̇O 2 was significantly higher than in warm conditions. The increased V̇O 2 in colder temperatures at the same exercise intensity is predicted to ultimately lead to earlier onset of fatigue and cessation of exercise. These results highlight the need to consider both appropriate clothing and fitness during cold exposure.

Investigation of instability, dynamic forces, and effect of dynamic loading on strength of cages for the bearings in the high pressure oxygen turbopumps for the space shuttle main engine

NASA Technical Reports Server (NTRS)

Dufrane, K. F.; Kannel, J. W.; Merriman, T. L.; Rosenfield, A. R.

1985-01-01

Experiments were performed to determine the effect of cyclic loading on bearing cage strength. A long term working tensile load of approximately 1300 N (300 lbs) was found to be the likely maximum. Higher loads caused a decrease in cage tensile strength after the 125,000 cycle testing period. Poisson's ratio in compression was found to be highly dependent upon the direction of the fiberglass plies. At room temperature the value was 0.15 with the plies and 0.68 across the plies. At -196 C (-321 F), the value with the plies was 0.20. The results of the analyses conducted have again demonstrated the critical need for improved lubrication in the high pressure oxygen turbopump bearings. Lubricant films with low shear strength and low friction coefficients promote cage stability and decrease ball/cage forces during marginal operating conditions. The analysis of the effect of combined bearing loads on ball/cage loads has identified a radial load of 3600 N (800 lbs) as the maximum for the current clearance of the balls and cage pockets. Liquid oxygen impinging on the cage in the direction of rotation was found to enhance cage stability.

Thermo-Mechanical Characterization of Silicon Carbide-Silicon Carbide Composites at Elevated Temperatures Using a Unique Combustion Facility

DTIC Science & Technology

2009-09-10

Calibration Tool(s) Surface Temperature ~1250oC Furnace, R-type TC & IR Gas Temperature < 1800oC R-type TC Gas Velocity ~ Mach 0.5 XS -4 High Speed...Camera Equivalence Ratio ~ 0.9 HVOFTM Flow Controller Gas Composition H 2 O, O 2 ,CO 2 , CO, NOx Testo XL 350 Gas Analyzer Mechanical Loading Fatigue...unavailability, however, gas velocity was measured using the X-StreamTM XS -4 High Speed Camera. The range of our interest was the velocity in the upstream of a

Thermal Vacuum Testing of a Proto-flight Miniature Loop Heat Pipe with Two Evaporators and Two Condensers

NASA Technical Reports Server (NTRS)

Ku, Jentung; Ottenstein, Laura

2011-01-01

This paper describes thermal vacuum testing of a proto-flight miniature loop heat pipe (MLHP) with two evaporators and two condensers designed for future small systems applications requiring low mass, low power and compactness. Each evaporator contains a wick with an outer diameter of 6.35 mm, and each has its own integral compensation chamber (CC). Miniaturization of the loop components reduces the volume and mass of the thermal system. Multiple evaporators provide flexibility for placement of instruments that need to be maintained at the same temperature, and facilitate heat load sharing among instruments, reducing the auxiliary heater power requirement. A flow regulator is used to regulate heat dissipations between the two condensers, allowing flexible placement of radiators on the spacecraft. A thermoelectric converter (TEC) is attached to each CC for control of the operating temperature and enhancement of start-up success. Tests performed include start-up, power cycle, sink temperature cycle, high power and low power operation, heat load sharing, and operating temperature control. The proto-flight MLHP demonstrated excellent performance in the thermal vacuum test. The loop started successfully and operated stably under various evaporator heat loads and condenser sink temperatures. The TECs were able to maintain the loop operating temperature within b1K of the desired set point temperature at all power levels and all sink temperatures. The un-powered evaporator would automatically share heat from the other powered evaporator. The flow regulator was able to regulate the heat dissipation among the radiators and prevent vapor from flowing into the liquid line.

Effect of daily environmental temperature on farrowing rate and total born in dam line sows.

PubMed

Bloemhof, S; Mathur, P K; Knol, E F; van der Waaij, E H

2013-06-01

Heat stress is known to adversely affect reproductive performance of sows. However, it is important to know on which days or periods during the reproduction cycle heat stress has the greatest effects for designing appropriate genetic or management strategies. Therefore, this study was conducted to identify days and periods that have greatest effects on farrowing rate and total born of sows using 5 different measures of heat stress. The data consisted of 22,750 records on 5024 Dutch Yorkshire dam line sows from 16 farms in Spain and Portugal. Heat stress on a given day was measured in terms of maximum temperature, diurnal temperature range and heat load. The heat load was estimated using 3 definitions considering different upper critical temperatures. Identification of days during the reproduction cycle that had maximum effect was based on the Pearson correlation between the heat stress variable and the reproduction trait, estimated for each day during the reproduction cycle. Polynomial functions were fitted to describe the trends of these correlations and the days with greatest negative correlation were considered as days with maximum effect. Correlations were greatest for maximum temperature, followed by those for heat load and diurnal temperature range. Correlations for both farrowing rate and total born were stronger in gilts than in sows. This implies that heat stress has a stronger effect on reproductive performance of gilts than of sows. Heat stress during the third week (21 to 14 d) before first insemination had largest effect on farrowing rate. Heat stress during the period between 7 d before successful insemination until 12 d after that had largest effect on total born. Correlations between temperatures on consecutive days during these periods were extremely high ( > 0.9). Therefore, for farrowing rate the maximum temperature on 21 d before first insemination and for total born the maximum temperature at day of successful insemination can be used as predictive measures of heat stress in commercial sow farms. Additionally, differences between daughter groups of sires were identified in response to high temperatures. This might indicate possibilities for genetic selection on heat tolerance.

How is the River Water Quality Response to Climate Change Impacts?

NASA Astrophysics Data System (ADS)

Nguyen, T. T.; Willems, P.

2015-12-01

Water quality and its response to climate change have been become one of the most important issues of our society, which catches the attention of many scientists, environmental activists and policy makers. Climate change influences the river water quality directly and indirectly via rainfall and air temperature. For example, low flow decreases the volume of water for dilution and increases the residence time of the pollutants. By contrast, high flow leads to increases in the amount of pollutants and sediment loads from catchments to rivers. The changes in hydraulic characteristics, i.e. water depth and velocity, affect the transportation and biochemical transformation of pollutants in the river water body. The high air temperature leads to increasing water temperature, shorter growing periods of different crops and water demands from domestic households and industries, which eventually effects the level of river pollution. This study demonstrates the quantification of the variation of the water temperature and pollutant concentrations along the Molse Neet river in the North East of Belgium as a result of the changes in the catchment rainfall-runoff, air temperature and nutrient loads. Firstly, four climate change scenarios were generated based on a large ensemble of available global and regional climate models and statistical downscaling based on a quantile perturbation method. Secondly, the climatic changes to rainfall and temperature were transformed to changes in the evapotranspiration and runoff flow through the conceptual hydrological model PDM. Thirdly, the adjustment in nutrient loads from agriculture due to rainfall and growing periods of crops were calculated by means of the semi-empirical SENTWA model. Water temperature was estimated from air temperature by a stochastic model separating the temperature into long-term annual and short-term residual components. Next, hydrodynamic and water quality models of the river, implemented in InfoWorks RS, were simulated for both historical (2000-2010) and projected future periods (2050-2060). The advection movement and physico-biochemical processes were considered for simulation of the following water quality variables: water temperature, dissolved oxygen, biological oxygen demand, ammonium, nitrate, nitrite and organic nitrogen.

Understanding the effect of annealing temperature on crystalline structure, morphology, and photocatalytic activity of silver-loaded TiO2 nanotubes

NASA Astrophysics Data System (ADS)

Viet, Pham Van; Phuong Trang, Duong Dao; Phat, Bui Dai; Hieu, Le Van; Thi, Cao Minh

2018-05-01

In this study, we classified the effect of the annealing temperature on silver-loaded TiO2 nanotubes (Ag/TNTs). X-ray diffraction results demonstrate that TNTs have a tendency of phase transformation owing to silver nanoparticles (Ag NPs). The Brunauer-Emmett-Teller method indicates that Ag/TNTs is a mesopore material and the surface area of Ag/TNTs decreases when the annealing temperature increases. This research concluded that the TNT structure begins to break at high annealing temperatures (>400 °C) and is completely broken at 500 °C. The average diameter of the Ag NPs in Ag/TNTs increases linearly with the annealing temperature. In addition, this study clearly explained the oxidation state transformation of Ag in Ag/TNTs under the impact of the annealing temperature, therein, the Ag0 state is transferred completely to Ag+ at 400 °C, and some Ag+ is oxidized to form Ag2+. The Ag/TNTs and Ag/TNTs annealed at 300 °C provided the good methylene blue photodegradation ability for 150 min under sunlight condition.

Feasibility study of solid oxide fuel cell engines integrated with sprinter gas turbines: Modeling, design and control

NASA Astrophysics Data System (ADS)

Jia, Zhenzhong; Sun, Jing; Dobbs, Herb; King, Joel

2015-02-01

Conventional recuperating solid oxide fuel cell (SOFC)/gas turbine (GT) system suffers from its poor dynamic capability and load following performance. To meet the fast, safe and efficient load following requirements for mobile applications, a sprinter SOFC/GT system concept is proposed in this paper. In the proposed system, an SOFC stack operating at fairly constant temperature provides the baseline power with high efficiency while the fast dynamic capability of the GT-generator is fully explored for fast dynamic load following. System design and control studies have been conducted by using an SOFC/GT system model consisting of experimentally-verified component models. In particular, through analysis of the steady-state simulation results, an SOFC operation strategy is proposed to maintain fairly constant SOFC power (less than 2% power variation) and temperature (less than 2 K temperature variation) over the entire load range. A system design procedure well-suited to the proposed system has also been developed to help determining component sizes and the reference steady-state operation line. In addition, control analysis has been studied for both steady-state and transient operations. Simulation results suggest that the proposed system holds the promise to achieve fast and safe transient operations by taking full advantage of the fast dynamics of the GT-generator.

Effects of temperature and organic loading rate on the performance and microbial community of anaerobic co-digestion of waste activated sludge and food waste.

PubMed

Gou, Chengliu; Yang, Zhaohui; Huang, Jing; Wang, Huiling; Xu, Haiyin; Wang, Like

2014-06-01

Anaerobic co-digestion of waste activated sludge and food waste was investigated semi-continuously using continuously stirred tank reactors. Results showed that the performance of co-digestion system was distinctly influenced by temperature and organic loading rate (OLR) in terms of gas production rate (GPR), methane yield, volatile solids (VS) removal efficiency and the system stability. The highest GPR at 55 °C was 1.6 and 1.3 times higher than that at 35 and 45 °C with the OLR of 1 g VSL(-1)d(-1), and the corresponding average CH₄ yields were 0.40, 0.26 and 0.30 L CH₄ g(-1)VSadded, respectively. The thermophilic system exhibited the best load bearing capacity at extremely high OLR of 7 g VSL(-1)d(-1), while the mesophilic system showed the best process stability at low OLRs (< 5 g VSL(-1)d(-1)). Temperature had a more remarkable effect on the richness and diversity of microbial populations than the OLR. Copyright © 2014 Elsevier Ltd. All rights reserved.

Study on power grid characteristics in summer based on Linear regression analysis

NASA Astrophysics Data System (ADS)

Tang, Jin-hui; Liu, You-fei; Liu, Juan; Liu, Qiang; Liu, Zhuan; Xu, Xi

2018-05-01

The correlation analysis of power load and temperature is the precondition and foundation for accurate load prediction, and a great deal of research has been made. This paper constructed the linear correlation model between temperature and power load, then the correlation of fault maintenance work orders with the power load is researched. Data details of Jiangxi province in 2017 summer such as temperature, power load, fault maintenance work orders were adopted in this paper to develop data analysis and mining. Linear regression models established in this paper will promote electricity load growth forecast, fault repair work order review, distribution network operation weakness analysis and other work to further deepen the refinement.

Load sensing system

DOEpatents

Sohns, Carl W.; Nodine, Robert N.; Wallace, Steven Allen

1999-01-01

A load sensing system inexpensively monitors the weight and temperature of stored nuclear material for long periods of time in widely variable environments. The system can include an electrostatic load cell that encodes weight and temperature into a digital signal which is sent to a remote monitor via a coaxial cable. The same cable is used to supply the load cell with power. When multiple load cells are used, vast

Optimization Research on Ampacity of Underground High Voltage Cable Based on Interior Point Method

NASA Astrophysics Data System (ADS)

Huang, Feng; Li, Jing

2017-12-01

The conservative operation method which takes unified current-carrying capacity as maximum load current can’t make full use of the overall power transmission capacity of the cable. It’s not the optimal operation state for the cable cluster. In order to improve the transmission capacity of underground cables in cluster, this paper regards the maximum overall load current as the objective function and the temperature of any cables lower than maximum permissible temperature as constraint condition. The interior point method which is very effective for nonlinear problem is put forward to solve the extreme value of the problem and determine the optimal operating current of each loop. The results show that the optimal solutions obtained with the purposed method is able to increase the total load current about 5%. It greatly improves the economic performance of the cable cluster.

Energy-based fatigue model for shape memory alloys including thermomechanical coupling

NASA Astrophysics Data System (ADS)

Zhang, Yahui; Zhu, Jihong; Moumni, Ziad; Van Herpen, Alain; Zhang, Weihong

2016-03-01

This paper is aimed at developing a low cycle fatigue criterion for pseudoelastic shape memory alloys to take into account thermomechanical coupling. To this end, fatigue tests are carried out at different loading rates under strain control at room temperature using NiTi wires. Temperature distribution on the specimen is measured using a high speed thermal camera. Specimens are tested to failure and fatigue lifetimes of specimens are measured. Test results show that the fatigue lifetime is greatly influenced by the loading rate: as the strain rate increases, the fatigue lifetime decreases. Furthermore, it is shown that the fatigue cracks initiate when the stored energy inside the material reaches a critical value. An energy-based fatigue criterion is thus proposed as a function of the irreversible hysteresis energy of the stabilized cycle and the loading rate. Fatigue life is calculated using the proposed model. The experimental and computational results compare well.

Intermediate photovoltaic system application experiment operational performance report: Volume 5, for Beverly High School, Beverly, Mass.

NASA Astrophysics Data System (ADS)

1982-02-01

Performance data for the month of January, 1982 for a grid connected photovoltaic power supply in Massachusetts are presented. Data include: monthly and daily electrical energy produced; monthly and daily solar energy incident on the array; monthly and daily array efficiency; plots of energy produced as a function of power level, voltage, cell temperature and time of day; power conditioner input, output and efficiency for each of two individual units and for the total power conditioning system; photovoltaic system efficiency; capacity factor; PV system to load and grid to load energies and corresponding dollar values; daily energy supplies to the load by the PV system; daily PV system availability; monthly and hourly insolation; monthly and hourly temperature average; monthly and hourly wind speed; wind direction distribution; average heating and cooling degree days; number of freeze/thaw cycles; and the data acquisition mode and recording interval plot.

Thermal effects on the enhanced ductility in non-monotonic uniaxial tension of DP780 steel sheet

NASA Astrophysics Data System (ADS)

Majidi, Omid; Barlat, Frederic; Korkolis, Yannis P.; Fu, Jiawei; Lee, Myoung-Gyu

2016-11-01

To understand the material behavior during non-monotonic loading, uniaxial tension tests were conducted in three modes, namely, the monotonic loading, loading with periodic relaxation and periodic loading-unloadingreloading, at different strain rates (0.001/s to 0.01/s). In this study, the temperature gradient developing during each test and its contribution to increasing the apparent ductility of DP780 steel sheets were considered. In order to assess the influence of temperature, isothermal uniaxial tension tests were also performed at three temperatures (298 K, 313 K and 328 K (25 °C, 40 °C and 55 °C)). A digital image correlation system coupled with an infrared thermography was used in the experiments. The results show that the non-monotonic loading modes increased the apparent ductility of the specimens. It was observed that compared with the monotonic loading, the temperature gradient became more uniform when a non-monotonic loading was applied.

Variable primary producer responses to nutrient and ...

EPA Pesticide Factsheets

Mesocosm experiments have been used to evaluate the impacts of nutrient loading on estuarine plant communities in order to develop nutrient response relationships. Mesocosm eutrophication studies tend to focus on long residence time systems. In the Pacific Northwest, many estuaries have high nutrient loads, short water residence times, seasonal macroalgal blooms, while intertidal seagrass meadows persist under what appear to be largely naturally-derived eutrophic conditions. Using experimental mesocosms, we examined how primary producer communities in rapidly flushed systems respond to a range of temperature (10 and 20 °C) and nutrient loads (ambient, 1.5, 3 and 6 x ambient). Thermal and nutrient loading regimes were maintained for three sets of 3 week-duration experiments during the summer of 2013. Statistical analysis was performed using an information criterion approach to evaluate the best fit model. Green macroalgal (GMA) growth and tissue N increased in response to nutrient loading. Irrespective of nutrient load, GMA at 10 °C remained intercalated among seagrass shoots, but at 20 °C formed floating mats that overtopped seagrass. Outgassing of O2 in combination with photosynthetic O2 production likely induced floating mat formation. No phytoplankton blooms were observed. Zostera japonica leaf biomass and C:N responded to temperature while other metrics exhibited no statistically significant difference. Z. marina growth, wasting disease, and morphological

High-temperature, high-pressure bonding of nested tubular metallic components

DOEpatents

Quinby, Thomas C.

1980-01-01

This invention is a tool for effecting high-temperature, high-compression bonding between the confronting faces of nested, tubular, metallic components. In a typical application, the tool is used to produce tubular target assemblies for irradiation in nuclear reactors or particle accelerators, the target assembly comprising a uranium foil and an aluminum-alloy substrate. The tool preferably is composed throughout of graphite. It comprises a tubular restraining member in which a mechanically expandable tubular core is mounted to form an annulus with the member. The components to be bonded are mounted in nested relation in the annulus. The expandable core is formed of individually movable, axially elongated segments whose outer faces cooperatively define a cylindrical pressing surface and whose inner faces cooperatively define two opposed, inwardly tapered, axial bores. Tapered rams extend respectively into the bores. The loaded tool is mounted in a conventional hot-press provided with evacuation means, heaters for maintaining its interior at bonding temperature, and hydraulic cylinders for maintaining a selected inwardly directed pressure on the tapered rams. With the hot-press evacuated and the loaded tool at the desired temperature, the cylinders are actuated to apply the selected pressure to the rams. The rams in turn expand the segmented core to maintain the nested components in compression against the restraining member. These conditions are maintained until the confronting faces of the nested components are joined in a continuous, uniform bond characterized by high thermal conductivity.

Observational Constraints on Lithospheric Rheology and Their Implications for Lithospheric Dynamics and Plate Tectonics

NASA Astrophysics Data System (ADS)

Zhong, S.; Watts, A. B.

2014-12-01

Lithospheric rheology and strength are important for understanding crust and lithosphere dynamics, and the conditions for plate tectonics. Laboratory studies suggest that lithospheric rheology is controlled by frictional sliding, semi-brittle, low-temperature plasticity, and high-temperature creep deformation mechanisms as pressure and temperature increase from shallow to large depths. Although rheological equations for these deformation mechanisms have been determined in laboratory settings, it is necessary to validate them using field observations. Here we present an overview of lithospheric rheology constrained by observations of seismic structure and load-induced flexure. Together with mantle dynamic modeling, rheological equations for high-temperature creep derived from laboratory studies (Hirth and Kohlstedt, 2003; Karato and Jung, 2003) satisfactorily explain the seismic structure of the Pacific upper mantle (Hunen et al., 2005) and Hawaiian swell topography (Asaadi et al., 2011). In a recent study that compared modeled surface flexure and stress induced by volcano loads in the Hawaiian Islands region with the observed flexure and seismicity, Zhong and Watts (2013) showed that the coefficient of friction is between 0.25 and 0.7, and is consistent with laboratory studies and also in-situ borehole measurements. However, this study indicated that the rheological equation for the low-temperature plasticity from laboratory studies (e.g., Mei et al., 2010) significantly over-predicts lithospheric strength and viscosity. Zhong and Watts (2013) also showed that the maximum lithospheric stress beneath Hawaiian volcano loads is about 100-200 MPa, which may be viewed as the largest lithospheric stress in the Earth's lithosphere. We show that the relatively weak lithospheric strength in the low-temperature plasticity regime is consistent with seismic observation of reactivated mantle lithosphere in the western US and the eastern North China. We discuss here the causes of this weakening in the context of the potential effects on laboratory studies of reduced grain size and Peierls stress on the low-temperature deformation regime.

Airborne particulate in Varanasi over middle Indo-Gangetic Plain: variation in particulate types and meteorological influences.

PubMed

Murari, Vishnu; Kumar, Manish; Mhawish, Alaa; Barman, S C; Banerjee, Tirthankar

2017-04-01

The variation in particulate mass and particulate types (PM 2.5 and PM 10 ) with respect to local/regional meteorology was analyzed from January to December 2014 (n = 104) for an urban location over the middle Indo-Gangetic Plain (IGP). Both coarser (mean ± SD; PM 10 161.3 ± 110.4 μg m -3 , n = 104) and finer particulates (PM 2.5 81.78 ± 66.4 μg m -3 ) revealed enormous mass loading with distinct seasonal effects (range: PM 10 12-535 μg m -3 ; PM 2.5 8-362 μg m -3 ). Further, 56% (for PM 2.5 ) to 81% (for PM 10 ) of monitoring events revealed non-attainment national air quality standard especially during winter months. Particulate types (in terms of PM 2.5 /PM 10 0.49 ± 0.19) also exhibited temporal variations with high PM 2.5 loading particularly during winter (0.62) compared to summer months (0.38). Local meteorology has clear distinguishing trends in terms of dry summer (March to June), wet winter (December to February), and monsoon (July to September). Among all the meteorological variables (average temperature, rainfall, relative humidity (RH), wind speed (WS)), temperature was found to be inversely related with particulate loading (r PM10 -0.79; r PM2.5 -0.87) while RH only resulted a significant association with PM 2.5 during summer (r PM10 0.07; r PM2.5 0.55) and with PM 10 during winter (r PM10 0.53; r PM2.5 0.24). Temperature, atmospheric boundary layer (ABL), and RH were cumulatively recognized as the dominant factors regulating particulate concentration as days with high particulate loading (PM 2.5 >150 μg m -3 ; PM 10 >260 μg m -3 ) appeared to have lower ABL (mean 660 m), minimum temperature (<22.6 °C), and high RH (∼79%). The diurnal variations of particulate ratio were mostly insignificant except minor increases during night having a high wintertime ratio (0.58 ± 0.07) over monsoon (0.34 ± 0.05) and summer (0.30 ± 0.07). Across the region, atmospheric visibility appeared to be inversely associated with particulate (r PM2.5 -0.84; r PM10 -0.79) for all humid conditions, while at RH ≥80%, RH appeared as the most dominant factor in regulating visibility compared to particulate loading. The Lagrangian particle dispersion model was further used to identify possible regions contributing particulate loading through regional/transboundary movement.

Friction Durability of Extremely Thin Diamond-Like Carbon Films at High Temperature

PubMed Central

Miyake, Shojiro; Suzuki, Shota; Miyake, Masatoshi

2017-01-01

To clarify the friction durability, both during and after the high-temperature heating of nanometer-thick diamond-like carbon (DLC) films, deposited using filtered cathodic vacuum arc (FCVA) and plasma chemical vapor deposition (P-CVD) methods, the dependence of the friction coefficient on the load and sliding cycles of the DLC films, were evaluated. Cluster-I consisted of a low friction area in which the DLC film was effective, while cluster-II consisted of a high friction area in which the lubricating effect of the DLC film was lost. The friction durability of the films was evaluated by statistical cluster analysis. Extremely thin FCVA-DLC films exhibited an excellent wear resistance at room temperature, but their friction durability was decreased at high temperatures. In contrast, the durability of the P-CVD-DLC films was increased at high temperatures when compared with that observed at room temperature. This inverse dependence on temperature corresponded to the nano-friction results obtained by atomic force microscopy. The decrease in the friction durability of the FCVA-DLC films at high temperatures, was caused by a complex effect of temperature and friction. The tribochemical reaction produced by the P-CVD-DLC films reduced their friction coefficient, increasing their durability at high temperatures. PMID:28772520

Friction Durability of Extremely Thin Diamond-Like Carbon Films at High Temperature.

PubMed

Miyake, Shojiro; Suzuki, Shota; Miyake, Masatoshi

2017-02-10

To clarify the friction durability, both during and after the high-temperature heating of nanometer-thick diamond-like carbon (DLC) films, deposited using filtered cathodic vacuum arc (FCVA) and plasma chemical vapor deposition (P-CVD) methods, the dependence of the friction coefficient on the load and sliding cycles of the DLC films, were evaluated. Cluster-I consisted of a low friction area in which the DLC film was effective, while cluster-II consisted of a high friction area in which the lubricating effect of the DLC film was lost. The friction durability of the films was evaluated by statistical cluster analysis. Extremely thin FCVA-DLC films exhibited an excellent wear resistance at room temperature, but their friction durability was decreased at high temperatures. In contrast, the durability of the P-CVD-DLC films was increased at high temperatures when compared with that observed at room temperature. This inverse dependence on temperature corresponded to the nano-friction results obtained by atomic force microscopy. The decrease in the friction durability of the FCVA-DLC films at high temperatures, was caused by a complex effect of temperature and friction. The tribochemical reaction produced by the P-CVD-DLC films reduced their friction coefficient, increasing their durability at high temperatures.

Initial Mechanical Testing of Superalloy Lattice Block Structures Conducted

NASA Technical Reports Server (NTRS)

Krause, David L.; Whittenberger, J. Daniel

2002-01-01

The first mechanical tests of superalloy lattice block structures produced promising results for this exciting new lightweight material system. The testing was performed in-house at NASA Glenn Research Center's Structural Benchmark Test Facility, where small subelement-sized compression and beam specimens were loaded to observe elastic and plastic behavior, component strength levels, and fatigue resistance for hundreds of thousands of load cycles. Current lattice block construction produces a flat panel composed of thin ligaments arranged in a three-dimensional triangulated trusslike structure. Investment casting of lattice block panels has been developed and greatly expands opportunities for using this unique architecture in today's high-performance structures. In addition, advances made in NASA's Ultra-Efficient Engine Technology Program have extended the lattice block concept to superalloy materials. After a series of casting iterations, the nickel-based superalloy Inconel 718 (IN 718, Inco Alloys International, Inc., Huntington, WV) was successfully cast into lattice block panels; this combination offers light weight combined with high strength, high stiffness, and elevated-temperature durability. For tests to evaluate casting quality and configuration merit, small structural compression and bend test specimens were machined from the 5- by 12- by 0.5-in. panels. Linear elastic finite element analyses were completed for several specimen layouts to predict material stresses and deflections under proposed test conditions. The structural specimens were then subjected to room-temperature static and cyclic loads in Glenn's Life Prediction Branch's material test machine. Surprisingly, the test results exceeded analytical predictions: plastic strains greater than 5 percent were obtained, and fatigue lives did not depreciate relative to the base material. These assets were due to the formation of plastic hinges and the redundancies inherent in lattice block construction, which were not considered in the simplified computer models. The fatigue testing proved the value of redundancies since specimen strength was maintained even after the fracture of one or two ligaments. This ongoing test program is planned to continue through high-temperature testing. Also scheduled for testing are IN 718 lattice block panels with integral face sheets, as well as specimens cast from a higher temperature alloy. The initial testing suggests the value of this technology for large panels under low and moderate pressure loadings and for high-risk, damage-tolerant structures. Potential aeropropulsion uses for lattice blocks include turbine-engine actuated panels, exhaust nozzle flaps, and side panel structures.

Impact of High Temperature Creep on the Buckling of Axially Compressed Steel Members

NASA Astrophysics Data System (ADS)

Włóka, Agata; Pawłowski, Kamil; Świerzko, Robert

2017-10-01

The paper presents results of the laboratory tests of the impact of creep on the buckling of axially compressed steel members at elevated temperatures. Tests were conducted on samples prepared of normal strength steel (S235JR) and high strength steel (S355J2). Samples were made in the form of a prismatic bar of a rectangular cross section 12 x 30 mm and a length of 500 mm. Support type of the specimens during tests was hinged on both ends. The tests were done at 600, 700 and 800°C. Experiments were carried out at static loads corresponding to values 0,8Ncr,T, 0,9Ncr,T, 1,0Ngr,T, where Ncr,T was theoretical value of Euler’s critical load at given temperature. Short-term creep analyses were performed in the universal testing machine Instron/Satec KN 600 equipped with a furnace for high-temperature testing type SF-16 2230, that enables testing at temperatures up to 1200°C. Temperature of the sample placed inside the furnace was verified and recorded with use of the compactRIO cRIO-9076 controller, equipped with a module for the connection of NI 9211 and K-type thermocouples. The system for the measurement and recording of the temperature of the analysed samples operated in the LabVIEW software environment. To measure lateral and longitudinal displacements LVTD Solatron ACR 100 displacement transducer was used. During the tests, the samples were heated to the given temperature (600, 700 or 800°C) and then subjected to a constant compressive load. During each test, for each sample following data was registered: the temperature on the surface of samples, longitudinal and lateral displacements in the middle of the sample. Basing on the conducted tests it was noted, for both analysed steel types, at the temperature of 800°C, growth of lateral displacements due to creep was very rapid, and tested elements were losing bearing capacity over the period of tens to hundreds of seconds, depending on stress level and the grade of the steel. At a temperature of 700°C growth of lateral displacements was much slower and the total loss of the bearing capacity of tested samples has occurred after 2 to 5 hours. At the temperature of 600°C samples did not show significant increments of lateral displacements at the test duration more than 6 hours, while maintaining throughout the test rectilinear form.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hallerman, G.; Gray, R.J.

The design and testing procedures of two elevatedtemperature hardness testers are described. One device uses a Rockwell tester with a large vertical capacity and a load range of 15 to 150 kg. The tester is equipped with a 900 deg C heating chamber which maintains an argon atmosphere over the specimen and can be laterally displaced by a cross-feed mechanism to allow repeated hardness readings to be made on the same specimen. The second instrument is a microindentation hardness tester for hardness determinations to a maximum temperature of 1000 deg C in vacuum of 10/sup -4/ to 10/sup -5/ torr.more » A deadweight loading system with a 136-deg diamond pyramid (Vickers) indenter, capable of delivering static loads between 0.150 and 3 kg, is contained within the vacuum chamber to avoid calibration problems that arise when loads are applied from outside the vacuum system. The microindentation hardness tester allows up to 100 determinations to be made on a single specimen without opening the test chamber. The applicability of the testers is illustrated by elevatedtemperature hardness measurements on several commercial alloys, a group of niobium-vanadium alloys, and by the changes in hardness occurring at the transformation temperatures of iron and steel. Hardness values of Haynes alloy No. 25 were determined at the temperatures of aging and are shown to be different from those obtained with the customary method of investigating age hardening. The testing is currently being used to aid and accelerate the development of alloys with desirable high-temperature properties. (auth)« less

Using Dynamic Simulation to Evaluate Attemperator Operation in a Natural Gas Combined Cycle With Duct Burners in the Heat Recovery Steam Generator

DOE Office of Scientific and Technical Information (OSTI.GOV)

Liese, Eric; Zitney, Stephen E.

A generic training simulator of a natural gas combined cycle was modified to match operations at a real plant. The objective was to use the simulator to analyze cycling operations of the plant. Initial operation of the simulator revealed the potential for saturation conditions in the final high pressure superheater as the attemperator tried to control temperature at the superheater outlet during gas turbine loading and unloading. Subsequent plant operational data confirmed simulation results. Multiple simulations were performed during loading and unloading of the gas turbine to determine operational strategies that prevented saturation and increased the approach to saturation temperature.more » The solutions included changes to the attemperator temperature control setpoints and strategic control of the steam turbine inlet pressure control valve.« less

Room Temperature Tensile Behavior and Damage Accumulation of Hi-Nicalon Reinforced SiC Matrix Composites

NASA Technical Reports Server (NTRS)

Morscher, G. N.; Gyekenyesi, J. Z.

1998-01-01

Composites consisting of woven Hi-Nicalon fibers, BN interphases, and different SiC matrices were studied in tension at room temperature. Composites with SiC matrices processed by CVI and melt infiltration were compared. Monotonic and load/unload/reload tensile hysteresis experiments were performed. A modal acoustic emission (AE) analyzer was used to monitor damage accumulation during the tensile test. Post test polishing of the tensile gage sections was performed to determine the extent of cracking. The occurrence and location of cracking could easily be determined using modal AE. The loss of modulus could also effectively be determined from the change in the velocity of sound across the sample. Finally, the stresses where cracks appear to intersect the load-bearing fibers correspond with high temperature low cycle fatigue run out stresses for these materials.

PREDICTED IMPACTS OF ELEVATED TEMPERATURE ON THE MAGNATUDE OF THE WINTER-SPRING PHYTOPLANKTON BLOOM IN TEMPERATE COASTAL WATERS: A MESOCOSM STUDY

EPA Science Inventory

An experiment was conducted with six 13-m3 land-based mesocosms (5 m deep) in December 1996/February 1997 to address the impact of increased temperature on the trophic structure of nutrient-rich coastal systems. All mesocosms were exposed to a high nutrient loading rate (2.31 mmo...

Electrical Properties of Low Temperature Sintering Step-Down Multilayer Piezoelectric Transformer

NASA Astrophysics Data System (ADS)

Yoo, Juhyun; Kim, Kookjin; Jeong, Yeongho

2007-06-01

The multilayer structured ceramic transformers were sintered at the low temperature of 940 °C and manufactured with the size of 27 × 27 × 2.2 mm3, respectively, using 0.07Pb(Mn1/3Nb2/3)O3-0.06Pb(Zn1/3Nb2/3)O3-0.87Pb(Zr0.48Ti0.52)O3 (A-type) and 0.07Pb(Mn1/3Nb2/3)O3-0.10Pb(Ni1/3Nb2/3)O3-0.83Pb(Zr0.48Ti0.52)O3 (B-type) composition ceramics. And then, their electrical properties were investigated according to the variations of frequency and load resistance. The voltage step-up ratio of the transformers showed the maximum values at the vicinity of 69 kHz. At the load resistance of 100 Ω, A-type and B-type piezoelectric transformers showed the temperature rises of about 21 °C at the output power of 15 and 18 W, respectively. At B-type transformer with high effective electromechanical coupling factor (keff) and high piezoelectric constant (d33), lower temperature increase was relatively appeared.

Effect of Warm Asphalt Additive on the Creep and Recovery Behaviour of Aged Binder Containing Waste Engine Oil

NASA Astrophysics Data System (ADS)

Hassan, Norhidayah Abdul; Kamaruddin, Nurul Hidayah Mohd; Rosli Hainin, Mohd; Ezree Abdullah, Mohd

2017-08-01

The use of waste engine oil as an additive in asphalt mixture has been reported to be able to offset the stiffening effect caused by the recycled asphalt mixture. Additionally, the fumes and odor of the waste engine oil has caused an uncomfortable condition for the workers during road construction particularly at higher production temperature. Therefore, this problem was addressed by integrating chemical warm asphalt additive into the mixture which functions to reduce the mixing and compaction temperature. This study was initiated by blending the additive in the asphalt binder of bitumen penetration grade 80/100 prior to the addition of pavement mixture. The effect of chemical warm asphalt additive, Rediset WMX was investigated by modifying the aged binder containing waste engine oil with 0%, 1%, 2% and 3% by weight of the binder. The samples were then tested for determining the rutting behaviour under different loading stress levels of 3Pa (low), 10Pa (medium) and 50Pa (high) using Dynamic Shear Rheometer (DSR). A reference temperature of 60 °C was fixed to reflect the maximum temperature of the pavement. The results found that the addition of Rediset did not affect the creep and recovery behavior of the modified binder under different loading. On the other hand, 2% Rediset resulted a slight decrease in its rutting resistance as shown by the reduction of non-recoverable compliance under high load stress. However, overall, the inclusion of chemical warm asphalt additive to the modified binder did not adversely affect the rutting resistance which could be beneficial in lowering the temperature of asphalt production and simultaneously not compromising the binder properties.

Experimental and theoretical investigation of temperature-dependent electrical fatigue studies on 1-3 type piezocomposites

NASA Astrophysics Data System (ADS)

Mohan, Y.; Arockiarajan, A.

2016-03-01

1-3 type piezocomposites are very attractive materials for transducers and biomedical application, due to its high electromechanical coupling effects. Reliability study on 1-3 piezocomposites subjected to cyclic loading condition in transducer application is one of the primary concern. Hence, this study focuses on 1-3 piezocomposites for various PZT5A1 fiber volume fraction subjected to electrical fatigue loading up-to 106 cycles and at various elevated temperature. Initially experiments are performed on 1-3 piezocomposites, in order to understand the degradation phenomena due to various range in amplitude of electric fields (unipolar & bipolar), frequency of applied electric field and for various ambient temperature. Performing experiments for high cycle fatigue and for different fiber volume fraction of PZT5A1 is a time consuming process. Hence, a simplified macroscopic uni-axial model based on physical mechanisms of domain switching and continuum damage mechanics has been developed to predict the non-linear fatigue behaviour of 1-3 piezocomposites for temperature dependent electrical fatigue loading conditions. In this model, damage effects namely domain pinning, frozen domains and micro cracks, are considered as a damage variable (ω). Remnant variables and material properties are considered as a function of internal damage variable and the growth of the damage is derived empirically based on the experimental observation to predict the macroscopic changes in the properties. The measured material properties and dielectric hysteresis (electric displacement vs. electric field) as well as butterfly curves (longitudinal strain vs. electric field) are compared with the simulated results. It is observed that variation in amplitude of bipolar electric field and temperature has a strong influence on the response of 1-3 piezocomposites.

SSME turbopump bearing analytical study

NASA Technical Reports Server (NTRS)

Kannel, J. W.; Merriman, T.

1980-01-01

Three shuttle pump bearings operating under severe overspeed and shut-down conditions are evaluated. The specific parameters investigated include outer race stresses, cage stresses, cage-race drag, bearing heating, and crush loading. A quasi-dynamic version of the BASDAP computer code was utilized which involved the calculation of ball-race forces (inner and outer), contact pressures, contact dimensions, and contact angles as a function of (1) axial load, (2) radial load, and (3) centrifugal load on the bearing. Generally, radial loads on the order of 13,300 N (3000 pounds) per bearing or 26,700 N (6000 pounds) per bearing pair, could be expected to cause severe problems to any of the bearings with a 17,800 N (4000 pounds) axial load. Further, when possible temperature excursions are considered, even a load of 8900 N (2000 pounds) may be excessive. However, high momentary radial loads with a 3800 N (850 pounds) axial load would not be anticipated to cause catastrophic failure of the fuel pump bearing.

Testing of active heat sink for advanced high-power laser diodes

NASA Astrophysics Data System (ADS)

Vetrovec, John; Copeland, Drew A.; Feeler, Ryan; Junghans, Jeremy

2011-03-01

We report on the development of a novel active heat sink for high-power laser diodes offering unparalleled capacity in high-heat flux handling and temperature control. The heat sink employs convective heat transfer by a liquid metal flowing at high speed inside a miniature sealed flow loop. Liquid metal flow in the loop is maintained electromagnetically without any moving parts. Thermal conductance of the heat sink is electronically adjustable, allowing for precise control of diode temperature and the laser light wavelength. This paper presents the principles and challenges of liquid metal cooling, and data from testing at high heat flux and high heat loads.

Hydrothermal deformation of granular quartz sand

NASA Astrophysics Data System (ADS)

Karner, Stephen L.; Kronenberg, Andreas K.; Chester, Frederick M.; Chester, Judith S.; Hajash, Andrew

2008-05-01

Isotropic and triaxial compression experiments were performed on porous aggregates of St Peter quartz sand to explore the influence of temperature (to 225°C). During isotropic stressing, samples loaded at elevated temperature exhibit the same sigmoidal stress-strain curves and non-linear acoustic emission rates as have previously been observed from room temperature studies on sands, sandstones, and soils. However, results from our hydrothermal experiments show that the critical effective pressure (P*) associated with the onset of significant pore collapse and pervasive cataclastic flow is lower at increased temperature. Samples subjected to triaxial loading at elevated temperature show yield behavior resembling that observed from room temperature studies on granular rocks and soils. When considered in terms of distortional and mean stresses, the yield strength data for a given temperature define an elliptical envelope consistent with critical state and CAP models from soil mechanics. For the conditions we tested, triaxial yield data at low effective pressure are essentially temperature-insensitive whereas yield levels at high effective pressure are lowered as a function of elevated temperature. We interpret our yield data in a manner consistent with Arrhenius behavior expected for thermally assisted subcritical crack growth. Taken together, our results indicate that increased stresses and temperatures associated with subsurface burial will significantly alter the yield strength of deforming granular media in systematic and predictable ways.

Combined Loads Test Fixture for Thermal-Structural Testing Aerospace Vehicle Panel Concepts

NASA Technical Reports Server (NTRS)

Fields, Roger A.; Richards, W. Lance; DeAngelis, Michael V.

2004-01-01

A structural test requirement of the National Aero-Space Plane (NASP) program has resulted in the design, fabrication, and implementation of a combined loads test fixture. Principal requirements for the fixture are testing a 4- by 4-ft hat-stiffened panel with combined axial (either tension or compression) and shear load at temperatures ranging from room temperature to 915 F, keeping the test panel stresses caused by the mechanical loads uniform, and thermal stresses caused by non-uniform panel temperatures minimized. The panel represents the side fuselage skin of an experimental aerospace vehicle, and was produced for the NASP program. A comprehensive mechanical loads test program using the new test fixture has been conducted on this panel from room temperature to 500 F. Measured data have been compared with finite-element analyses predictions, verifying that uniform load distributions were achieved by the fixture. The overall correlation of test data with analysis is excellent. The panel stress distributions and temperature distributions are very uniform and fulfill program requirements. This report provides details of an analytical and experimental validation of the combined loads test fixture. Because of its simple design, this unique test fixture can accommodate panels from a variety of aerospace vehicle designs.

Shock-activated reaction synthesis and high pressure response of titanium-based ternary carbide and nitride ceramics

NASA Astrophysics Data System (ADS)

Jordan, Jennifer Lynn

The objectives of this study were to (a) investigate the effect of shock activation of precursor powders for solid-state reaction synthesis of Ti-based ternary ceramics and (b) to determine the high pressure phase stability and Hugoniot properties of Ti3SiC2. Dynamically densified compacts of Ti, SiC, and graphite precursor powders and Ti and AlN precursor powders were used to study the shock-activated formation of Ti 3SiC2 and Ti2AlN ternary compounds, respectively, which are considered to be novel ceramics having high stiffness but low hardness. Gas gun and explosive loading techniques were used to obtain a range of loading conditions resulting in densification and activation. Measurements of fraction reacted as a function of time and temperature and activation energies obtained from DTA experiments were used to determine the degree of activation caused by shock compression and its subsequent effect on the reaction mechanisms and kinetics. In both systems, shock activation led to an accelerated rate of reaction at temperatures less than 1600°C and, above that temperature, it promoted the formation of almost 100% of the ternary compound. A kinetics-based mathematical model based on mass and thermal transport was developed to predict the effect of shock activation and reaction synthesis conditions that ensure formation of the ternary compounds. Model predictions revealed a transition temperature above which the reaction is taken over by the "run-away" combustion-type mode. The high pressure phase stability of pre-alloyed Ti 3SiC2 compound was investigated by performing Hugoniot shock and particle velocity measurements using the facilities at the National Institute for Materials Science (Tsukuba, Japan). Experiments performed at pressures of 95--120 GPa showed that the compressibility of Ti3SiC 2 at these pressures deviates from the previously reported compressibility of the material under static high pressure loading. The deviation in compressibility behavior is indicative of the transformation of the Ti3 SiC2 ceramic to a high pressure, high density phase.

Fretting Fatigue Analysis of Additively Manufactured Blade Root Made of Intermetallic Ti-48Al-2Cr-2Nb Alloy at High Temperature.

PubMed

Lavella, Mario; Botto, Daniele

2018-06-21

Slots in the disk of aircraft turbines restrain the centrifugal load of blades. Contact surfaces between the blade root and the disk slot undergo high contact pressure and relative displacement that is the typical condition in which fretting occurs. The load level ranges from zero to the maximum during take-off. This cycle is repeated for each mission. In this paper, a fretting fatigue analysis of additively manufactured blades is presented. Blades are made of an intermetallic alloy γTiAl. Fretting fatigue experiments were performed at a frequency of 0.5 Hz and at a temperature of 640 °C to match the operating condition of real blades. The minimum load was fixed at 0.5 KN and three maximum loads were applied, namely 16, 18 and 20 kN. Both an analytical and a two-dimensional finite element model were used to evaluate the state of stress at the contact interfaces. The results of the analytical model showed good agreement with the numerical model. Experiments showed that cracks nucleate where the analytical model predicts the maximum contact pressure and the numerical model predicts the maximum equivalent stress. A parametric analysis performed with the analytical model indicates that there exists an optimum geometry to minimize the contact pressure. Tests showed that the component life changed dramatically with the maximum load variation. Optical topography and scanning electron microscopy (SEM) analysis reveals information about the damage mechanism.

Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stoupin, Stanislav; Antipov, Sergey; Butler, James E.

Fabrication and results of high-resolution X-ray topography characterization of diamond single-crystal plates with large surface area (10 mm × 10 mm) and (111) crystal surface orientation for applications in high-heat-load X-ray crystal optics are reported. The plates were fabricated by laser-cutting of the (111) facets of diamond crystals grown using high-pressure high-temperature methods. The intrinsic crystal quality of a selected 3 mm × 7 mm crystal region of one of the studied samples was found to be suitable for applications in wavefront-preserving high-heat-load crystal optics. Wavefront characterization was performed using sequential X-ray diffraction topography in the pseudo plane wave configurationmore » and data analysis using rocking-curve topography. In conclusion, the variations of the rocking-curve width and peak position measured with a spatial resolution of 13 µm × 13 µm over the selected region were found to be less than 1 µrad.« less

Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics.

PubMed

Stoupin, Stanislav; Antipov, Sergey; Butler, James E; Kolyadin, Alexander V; Katrusha, Andrey

2016-09-01

Fabrication and results of high-resolution X-ray topography characterization of diamond single-crystal plates with large surface area (10 mm × 10 mm) and (111) crystal surface orientation for applications in high-heat-load X-ray crystal optics are reported. The plates were fabricated by laser-cutting of the (111) facets of diamond crystals grown using high-pressure high-temperature methods. The intrinsic crystal quality of a selected 3 mm × 7 mm crystal region of one of the studied samples was found to be suitable for applications in wavefront-preserving high-heat-load crystal optics. Wavefront characterization was performed using sequential X-ray diffraction topography in the pseudo plane wave configuration and data analysis using rocking-curve topography. The variations of the rocking-curve width and peak position measured with a spatial resolution of 13 µm × 13 µm over the selected region were found to be less than 1 µrad.

Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics

DOE PAGES

Stoupin, Stanislav; Antipov, Sergey; Butler, James E.; ...

2016-08-10

Fabrication and results of high-resolution X-ray topography characterization of diamond single-crystal plates with large surface area (10 mm × 10 mm) and (111) crystal surface orientation for applications in high-heat-load X-ray crystal optics are reported. The plates were fabricated by laser-cutting of the (111) facets of diamond crystals grown using high-pressure high-temperature methods. The intrinsic crystal quality of a selected 3 mm × 7 mm crystal region of one of the studied samples was found to be suitable for applications in wavefront-preserving high-heat-load crystal optics. Wavefront characterization was performed using sequential X-ray diffraction topography in the pseudo plane wave configurationmore » and data analysis using rocking-curve topography. In conclusion, the variations of the rocking-curve width and peak position measured with a spatial resolution of 13 µm × 13 µm over the selected region were found to be less than 1 µrad.« less

Loading and unloading of freeze-dryers: airborne contamination risks for aseptically manufactured sterile drug products.

PubMed

Ljungqvist, Bengt; Reinmüller, Berit

2007-01-01

In pharmaceutical manufacturing, freeze-drying processes can be adversely affected by temperature differences relative to the surrounding air. Loading and unloading of freeze-dryers are performed either without or with temperature differences between the cleanroom and the chamber of the freeze-dryer. This operation can cause a flow of room air through the opening, creating a contamination risk, especially when manual handling of material is performed in this area. To minimize this risk, a high-efficiency particulate air (HEPA) filter unit should be installed above the opening to provide clean air and protect the opening. Here the theoretical relationships are discussed and design criteria are presented.

High-power closed-cycle 4He cryostat with top-loading sample exchange

NASA Astrophysics Data System (ADS)

Piegsa, F. M.; van den Brandt, B.; Kirch, K.

2017-10-01

We report on the development of a versatile cryogen-free laboratory cryostat based upon a commercial pulse tube cryocooler. It provides enough cooling power for continuous recondensation of circulating 4He gas at a condensation pressure of approximately 250 mbar. Moreover, the cryostat allows for exchange of different cryostat-inserts as well as fast and easy ;wet; top-loading of samples directly into the 1 K pot with a turn-over time of less than 75 min. Starting from room temperature and using a 4He cryostat-insert, a base temperature of 1.0 K is reached within approximately seven hours and a cooling power of 250 mW is established at 1.24 K.

Thermal analysis and optimization of the EAST ICRH antenna

NASA Astrophysics Data System (ADS)

Qingxi, YANG; Wei, SONG; Qunshan, DU; Yuntao, SONG; Chengming, QIN; Xinjun, ZHANG; Yanping, ZHAO

2018-02-01

The ion cyclotron resonance of frequency heating (ICRH) plays an important role in plasma heating. Two ICRH antennas were designed and applied on the EAST tokamak. In order to meet the requirement imposed by high-power and long-pulse operation of EAST in the future, an active cooling system is mandatory to be designed to remove the heat load deposited on the components. Thermal analyses for high heat-load components have been carried out, which presented clear temperature distribution on each component and provided the reference data to do the optimization. Meanwhile, heat pipes were designed to satisfy the high requirement imposed by a Faraday shield and lateral limiter.

Fiber-Reinforced Superalloys For Rocket Engines

NASA Technical Reports Server (NTRS)

Lewis, Jack R.; Yuen, Jim L.; Petrasek, Donald W.; Stephens, Joseph R.

1990-01-01

Report discusses experimental studies of fiber-reinforced superalloy (FRS) composite materials for use in turbine blades in rocket engines. Intended to withstand extreme conditions of high temperature, thermal shock, atmospheres containing hydrogen, high cycle fatigue loading, and thermal fatigue, which tax capabilities of even most-advanced current blade material - directionally-solidified, hafnium-modified MAR M-246 {MAR M-246 (Hf) (DS)}. FRS composites attractive combination of properties for use in turbopump blades of advanced rocket engines at temperatures from 870 to 1,100 degrees C.

Effect of matrix material on the fracture behavior and toughness of high temperature polymer composites

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chenock, T.A.Jr.; Heshmet, A.

1990-07-01

The effect of matrix material on the strength, toughness, and fracture behavior of two high temperature polyimide/carbon fiber composites has been studied and compared. The polyimide matrix resins under investigation are PMR-II-20, PMR-15. Each system was reinforced with epoxy sized Celion G30-500 carbon fabric (8HSW, 3K tow). Un-notched and notched specimens were tested under 4-point bend loading in both translaminar and crosslaminar directions.

Cooperative implementation of a high temperature acoustic sensor

NASA Technical Reports Server (NTRS)

Baldini, S. E.; Nowakowski, Edward; Smith, Herbert G.; Friebele, E. J.; Putnam, Martin A.; Rogowski, Robert; Melvin, Leland D.; Claus, Richard O.; Tran, Tuan; Holben, Milford S., Jr.

1991-01-01

The current status and results of a cooperative program aimed at the implementation of a high-temperature acoustic/strain sensor onto metallic structures are reported. The sensor systems that are to be implemented under this program will measure thermal expansion, maneuver loads, aircraft buffet, sonic fatigue, and acoustic emissions in environments that approach 1800 F. The discussion covers fiber development, fabrication of an extrinsic Fabry-Perot interferometer acoustic sensor, sensor mounting/integration, and results of an evaluation of the sensor capabilities.

Unified constitutive models for high-temperature structural applications

NASA Technical Reports Server (NTRS)

Lindholm, U. S.; Chan, K. S.; Bodner, S. R.; Weber, R. M.; Walker, K. P.

1988-01-01

Unified constitutive models are characterized by the use of a single inelastic strain rate term for treating all aspects of inelastic deformation, including plasticity, creep, and stress relaxation under monotonic or cyclic loading. The structure of this class of constitutive theory pertinent for high temperature structural applications is first outlined and discussed. The effectiveness of the unified approach for representing high temperature deformation of Ni-base alloys is then evaluated by extensive comparison of experimental data and predictions of the Bodner-Partom and the Walker models. The use of the unified approach for hot section structural component analyses is demonstrated by applying the Walker model in finite element analyses of a benchmark notch problem and a turbine blade problem.

Synchrotron X-ray micro-tomography at the Advanced Light Source: Developments in high-temperature in-situ mechanical testing

NASA Astrophysics Data System (ADS)

Barnard, Harold S.; MacDowell, A. A.; Parkinson, D. Y.; Mandal, P.; Czabaj, M.; Gao, Y.; Maillet, E.; Blank, B.; Larson, N. M.; Ritchie, R. O.; Gludovatz, B.; Acevedo, C.; Liu, D.

2017-06-01

At the Advanced Light Source (ALS), Beamline 8.3.2 performs hard X-ray micro-tomography under conditions of high temperature, pressure, mechanical loading, and other realistic conditions using environmental test cells. With scan times of 10s-100s of seconds, the microstructural evolution of materials can be directly observed over multiple time steps spanning prescribed changes in the sample environment. This capability enables in-situ quasi-static mechanical testing of materials. We present an overview of our in-situ mechanical testing capabilities and recent hardware developments that enable flexural testing at high temperature and in combination with acoustic emission analysis.

Power Ultrasound to Process Dairy Products

NASA Astrophysics Data System (ADS)

Bermúdez-Aguirre, Daniela; Barbosa-Cánovas, Gustavo V.

Conventional methods of pasteurizing milk involve the use of heat regardless of treatment (batch, high temperature short time - HTST or ultra high temperature - UHT sterilization), and the quality of the milk is affected because of the use of high temperatures. Consequences of thermal treatment are a decrease in nutritional properties through the destruction of vitamins or denaturation of proteins, and sometimes the flavor of milk is undesirably changed. These changes are produced at the same time that the goal of the pasteurization process is achieved, which is to have a microbiological safe product, free of pathogenic bacteria, and to reduce the load of deteriorative microorganisms and enzymes, resulting in a product with a longer storage life.

High-temperature friction and wear studies of Fe-Cu-Sn alloy with graphite as solid lubricant under dry sliding conditions

NASA Astrophysics Data System (ADS)

Mushtaq, Shuhaib; Wani, M. F.

2018-02-01

Solid lubricants are particularly used in the advanced mechanical motion systems with extreme conditions such as (high temperature, vacuum, radiation, extreme contact pressure, etc). The main focus of this paper is to study the dry sliding friction and wear behavior of Fe-Cu-Sn alloy with varying wt% of graphite at high temperature up to 423 K. The influence of temperature, sliding distance and load on friction and wear behavior of Fe-Cu-Sn alloy against EN8 steel was studied using ball (EN8) on disc (Fe-Cu-Sn alloy). Lower wear and lower friction of Fe-Cu-Sn alloy were observed at high temperature, as compared to room temperature. Surface morphological and surface analytical studies of fresh and worn surfaces were carried out using optical microscopy, 3D profilometer, scanning electron microscope, energy dispersive x-ray spectroscopy, XRD, and Raman spectroscopy to understand the friction and wear behavior.

Fiber-optic temperature profiling for thermal protection system heat shields

NASA Astrophysics Data System (ADS)

Black, Richard J.; Costa, Joannes M.; Zarnescu, Livia; Hackney, Drew A.; Moslehi, Behzad; Peters, Kara J.

2016-11-01

To achieve better designs for spacecraft heat shields for missions requiring atmospheric aero-capture or entry/reentry, reliable thermal protection system (TPS) sensors are needed. Such sensors will provide both risk reduction and heat-shield mass minimization, which will facilitate more missions and enable increased payloads and returns. This paper discusses TPS thermal measurements provided by a temperature monitoring system involving lightweight, electromagnetic interference-immune, high-temperature resistant fiber Bragg grating (FBG) sensors with a thermal mass near that of TPS materials together with fast FBG sensor interrogation. Such fiber-optic sensing technology is highly sensitive and accurate, as well as suitable for high-volume production. Multiple sensing FBGs can be fabricated as arrays on a single fiber for simplified design and reduced cost. Experimental results are provided to demonstrate the temperature monitoring system using multisensor FBG arrays embedded in a small-size super-light ablator (SLA) coupon which was thermally loaded to temperatures in the vicinity of the SLA charring temperature. In addition, a high-temperature FBG array was fabricated and tested for 1000°C operation, and the temperature dependence considered over the full range (cryogenic to high temperature) for which silica fiber FBGs have been subjected.

Advances in Non-Contact Measurement of Creep Properties

NASA Technical Reports Server (NTRS)

Hyers, Robert; Canepari, Stacy; White, Erica Bischoff; Cretegny, Laurent; Rogers, jan

2009-01-01

As the required service temperatures for superalloys increases, so do the demands on testing for development of these alloys. Non-contact measurement of creep of refractory metals using electrostatic levitation has been demonstrated at temperatures up to 2300 C using samples of only 20-40 mg. These measurements load the spherical specimen by inertial forces due to rapid rotation. However, the first measurements relied on photon pressure to accelerate the samples to the high rotational rates of thousands of rotations per second, limiting the applicability to low stresses and high temperatures. Recent advances in this area extend this measurement to higher stresses and lower-temperatures through the use of an induction motor to drive the sample to such high rotational speeds. Preliminary results on new measurements on new materials will be presented.

Elevated Temperature Crack Growth Behavior in HSCT Structural Materials

NASA Technical Reports Server (NTRS)

Saxena, Ashok

1998-01-01

Structures in super-sonic aircraft are subjected to conditions of high temperature and cyclic and sustained loading for extended periods of time. The durability of structures fabricated from aluminum and certain titanium alloys in such demanding conditions is of primary concern to the designers and manufacturers of futuristic transport aircraft. Accordingly, the major goal of this project was to evaluate the performance and durability of high temperature aluminum and titanium alloys for use in high speed civil transport (HSCT) structures. Additional goals were to develop time-dependent fracture mechanics methodology and test methods for characterizing and predicting elevated temperature crack growth behavior in creep-brittle materials such as ones being considered for use in HSCT structures and to explore accelerated methods of simulating microstructural degradation during service and measuring degraded properties in these materials.

Unified high-temperature behavior of thin-gauge superalloys

NASA Astrophysics Data System (ADS)

England, Raymond Oliver

This research proposes a methodology for accelerated testing in the area of high-temperature creep and oxidation resistance for thin-gauge superalloy materials. Traditional long-term creep (stress-relaxation) and oxidation tests are completed to establish a baseline. The temperature range used in this study is between 1200 and 1700°F. The alloys investigated are Incoloy MA 956, Waspaloy, Haynes 214, Haynes 242, Haynes 230, and Incoloy 718. The traditional creep test involves loading the specimens to a constant test mandrel radius of curvature, and measuring the retained radius of curvature as a function of time. The accelerated creep test uses a servohydraulic test machine to conduct single specimen, variable strain-rate load relaxation experiments. Standard metallographic evaluations are used to determine extent and morphology of attack in the traditional oxidation tests, while the accelerated oxidation test utilizes thermogravimetric analysis to obtain oxidation rate data. The traditional long-term creep testing indicates that the mechanically-alloyed material Incoloy MA 956 and Haynes alloy 214 may be suitable for long-term, high-temperature (above 1400°F) structural applications. The accelerated creep test produced a continuous linear function of log stress versus strain rate which can be used to calculate creep rate. The long-term and traditional oxidation tests indicate that Al2O3 scale formers such as Incoloy MA 956 and Haynes 214 are much more resistant to high-temperature oxidation than Cr2O3 scale formers such as Waspaloy. Both accelerated tests can be completed within roughly one day, and can evaluate multiple test temperatures using standardized single specimens. These simple experiments can be correlated with traditional long-term tests which require years to complete.

Mechanical Properties of Ceramics for High Temperature Applications

DTIC Science & Technology

1976-12-01

difficult so far. Also torsion creep tests have been performed /2 /, not considered in this figure. The data show a relatively consistent picture...mittent creep test. Corrosion effects are claimed to be operative during fatigue : The lifetime of a fa- tigue specimen, being controlled by the slow...of plot at extremely low rates of loading. The static fatigue limit on this type of plot is the strength below which there is no effect of loading

A microwave exciter for Cs frequency standards based on a sapphire-loaded cavity oscillator.

PubMed

Koga, Y; McNeilage, C; Searls, J H; Ohshima, S

2001-01-01

A low noise and highly stable microwave exciter system has been built for Cs atomic frequency standards using a tunable sapphire-loaded cavity oscillator (SLCO), which works at room temperature. This paper discusses the successful implementation of a control system for locking the SLCO to a long-term reference signal and reports an upper limit of the achieved frequency tracking error 6 x 10(-15) at tau = 1 s.

Demonstration Program for Low-Cost, High-Energy-Saving Dynamic Windows

DTIC Science & Technology

2014-09-01

Design The scope of this project was to demonstrate the impact of dynamic windows via energy savings and HVAC peak-load reduction; to validate the...temperature and glare. While the installed dynamic window system does not directly control the HVAC or lighting of the facility, those systems are designed ...optimize energy efficiency and HVAC load management. The conversion to inoperable windows caused an unforeseen reluctance to accept the design and

Experimental Study of the Influence of Speed and Load on Thermal Behavior of High-Speed Helical Gear Trains

NASA Technical Reports Server (NTRS)

Handschuh, R.; Kilmain, C.

2005-01-01

An experimental effort has been conducted on an aerospace-quality helical gear train to investigate the thermal behavior of the gear system as speed, load, and lubricant flow rate were varied. Temperature test data from a helical gear train at varying speeds and loads (to 5000 hp and 15000 rpm) was collected using thermocouple rakes and axial arrays. The instrumentation was able to capture the radial and axial expelled lubricant-air environment (fling-off lubricant) that is expelled during the gear meshing process. Effects of operational characteristics are presented.

FRACTURE BEHAVIOR OF ALLOY 600, ALLOY 690, EN82H WELDS AND EN52 WELDS IN WATER

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mills, W.J., Brown, C.M. and Burke, M.G.

2000-01-11

The cracking resistance of Alloy 600, Alloy 690 and their welds, EN82H and EN52, was characterized by conducting J{sub IC} rising load tests in air and hydrogenated water and cooldown testing in water under constant-displacement conditions. All test materials displayed excellent toughness in air and high temperature water, but Alloy 690 and the two welds were severely embrittled in low temperature water. In 54 C water with 150 cc H{sub 2}/kg H{sub 2}O, J{sub IC} values were reduced by 70% to 95%, relative to their air counterpart. The toughness degradation was associated with a fracture mechanism transition from microvoid coalescencemore » to intergranular fracture. Comparison of the cracking response in water with that for hydrogen-precharged specimens tested in air demonstrated that susceptibility to low temperature crack propagation (LTCP) is due to hydrogen embrittlement of grain boundaries. The effects of water temperature, hydrogen content and loading rate on LTCP were studied. In addition, testing of specimens containing natural weld defects and as-machined notches was performed to determine if low temperature cracking can initiate at these features. Unlike the other materials, Alloy 600 is not susceptible to LTCP as the toughness in 54 C water remained high and a microvoid coalescence mechanism was operative in both air and water. Cooldown testing of EN82H welds under constant-displacement conditions was performed to determine if LTCP data from rising load J{sub IC}/K{sub Pmax} tests predict the onset of LTCP for other load paths. In these tests, bolt-loaded CT specimens were subjected to 288 C water for up to 1 week, cooled to 54 C and held in 54 C hydrogenated water for 1 week. This cycle was repeated up to 6 times. For two of the three welds tested, critical K{sub I} levels for LTCP under constant-displacement conditions were much higher than rising load K{sub Pmax} values. Bolt-loaded specimens from a third weld were found to exhibit LTCP at K{sub I} levels comparable to K{sub Pmax} values. Although work to date indicates that rising load tests either accurately or conservatively predict the critical conditions for LTCP under constant displacement conditions, the potential for LTCP at K{sub I} levels less than K{sub Pmax} has not been fully evaluated. Annealing at 1093 C reduces or eliminates LTCP susceptibility. The microstructure and mechanical properties for susceptible and nonsusceptible EN82H welds were characterized to identify the key material parameters responsible for LTCP in the as-welded condition. The key microstructural feature associated with LTCP appears to be fine Nb- and Ti-rich carbonitrides decorating grain boundaries. In addition, the higher yield strength for the as-fabricated weld also promotes LTCP because it increases stresses and local hydrogen concentrations ahead of a crack.« less

Farmland-atmosphere feedbacks amplify decreases in diffuse nitrogen pollution in a freeze-thaw agricultural area under climate warming conditions.

PubMed

Gao, Xiang; Ouyang, Wei; Hao, Zengchao; Shi, Yandan; Wei, Peng; Hao, Fanghua

2017-02-01

Although climate warming and agricultural land use changes are two of the primary instigators of increased diffuse pollution, they are usually considered separately or additively. This likely lead to poor decisions regarding climate adaptation. Climate warming and farmland responses have synergistic consequences for diffuse nitrogen pollution, which are hypothesized to present different spatio-temporal patterns. In this study, we propose a modeling framework to simulate the synergistic impacts of climate warming and warming-induced farmland shifts on diffuse pollution. Active accumulated temperature response for latitudinal and altitudinal directions was predicted based on a simple agro-climate model under different temperature increments (△T 0 is from 0.8°C to 1.4°C at an interval of 0.2°C). Spatial distributions of dryland shift to paddy land were determined by considering accumulated temperature. Different temperature increments and crop distributions were inserted into Soil and Water Assessment Tool model, which quantified the spatio-temporal changes of nitrogen. Warming led to a decrease of the annual total nitrogen loading (2.6%-14.2%) in the low latitudes compared with baseline, which was larger than the decrease (0.8%-6.2%) in the high latitudes. The synergistic impacts amplified the decrease of the loading in the low and high latitudes at the sub-basin scale. Warming led to a decrease of the loading at a rate of 0.35kg/ha/°C, which was lower than the synergistic impacts (3.67kg/ha/°C) at the watershed level. However, warming led to the slight increase of the annual averaged NO3 (LAT) (0.16kg/ha/°C), which was amplified by the synergistic impacts (0.22kg/ha/°C). Expansion of paddy fields led to a decrease in the monthly total nitrogen loading throughout the year, but amplified an increase in the loading in August and September. The decreased response in spatio-temporal nitrogen patterns is substantially amplified by farmland-atmosphere feedbacks associated with farmland shifts in response to warming. Copyright © 2016 Elsevier B.V. All rights reserved.

Parametric analysis of parameters for electrical-load forecasting using artificial neural networks

NASA Astrophysics Data System (ADS)

Gerber, William J.; Gonzalez, Avelino J.; Georgiopoulos, Michael

1997-04-01

Accurate total system electrical load forecasting is a necessary part of resource management for power generation companies. The better the hourly load forecast, the more closely the power generation assets of the company can be configured to minimize the cost. Automating this process is a profitable goal and neural networks should provide an excellent means of doing the automation. However, prior to developing such a system, the optimal set of input parameters must be determined. The approach of this research was to determine what those inputs should be through a parametric study of potentially good inputs. Input parameters tested were ambient temperature, total electrical load, the day of the week, humidity, dew point temperature, daylight savings time, length of daylight, season, forecast light index and forecast wind velocity. For testing, a limited number of temperatures and total electrical loads were used as a basic reference input parameter set. Most parameters showed some forecasting improvement when added individually to the basic parameter set. Significantly, major improvements were exhibited with the day of the week, dew point temperatures, additional temperatures and loads, forecast light index and forecast wind velocity.

Development of high precision and cryogenic lens holders

NASA Astrophysics Data System (ADS)

Reutlinger, A.; Boesz, Anton; Mottaghibonab, A.; Eckert, P.; Dubowy, M.; Gebler, H.; Grupp, F.; Geis, N.; Bode, A.; Katterloher, R.; Bender, R.

2017-11-01

The optical system of the Near Infrared Spectrometer and Photometer (NISP) of the EUCLID mission consists mainly of a filter and grism wheel and 4 aspherical lenses with large diameters up to 170 mm. The single lenses require a high precision positioning at the operational temperature of 150 K. An additional design driver represents the CaF2 material of a lens, which is very sensitive wrt brittleness. The technical maturity of the combination of single features such as CaF2, large diameter (and mass), high precision and cryogenic conditions is considered as low. Therefore, a dedicated pre-development program has been launched to design and develop a first prototype of lens holder and to demonstrate the functional performance at representative operational conditions. The 4 lenses are divided into 3x lenses for the Camera Lens Assembly (CaLA) and 1x lens for the Corrector Lens Assembly (CoLA). Each lens is glue mounted onto solid state springs, part of an adaption ring. The adaption ring shall provide protection against vibration loads, high accuracy positioning, as well as quasi load free mounting of the lens under operational conditions. To reduce thermomechanical loads on the lens, the CTE of the adaption ring is adapted to that of the lens. The glue between lens and solid state spring has to withstand high tension loads during vibration. At the operational temperature the deviating CTE between glue and lens/adaption ring introduces shear loads into the glue interface, which are critical, in particular for the fragile CaF2 lens material. For the case of NISP the shear loads are controlled with the glue pad diameter and the glue thickness. In the context of the development activity many technology aspects such as various solid state spring designs, glue selection and glue handling have been investigated. A parametric structural model was developed to derive the specific design feature of each ring, such as spring force, number of springs, eigenfrequency, etc. This paper presents the design of the adaption ring in conjunction with test results from functional verification. These results are presented on behalf of the EUCLID consortium.

Characterization of a New Phase and Its Effect on the Work Characteristics of a Near-Stoichiometric Ni30Pt20Ti50 High-Temperature Shape Memory Alloy (HTSMA)

NASA Technical Reports Server (NTRS)

Garg, A.; Gaydosh, D.; Noebe, R.D.; Padula II, Santo; Bigelow, G.S.; Kaufman, M.; Kovarik, L.; Mills, M.J.; Diercks, D.; McMurray, S.

2008-01-01

A new phase observed in a nominal Ni30Pt20Ti50 (at.%) high temperature shape memory alloy has been characterized using transmission electron microscopy and 3-D atom probe tomography. This phase forms homogeneously in the B2 austenite matrix by a nucleation and growth mechanism and results in a concomitant increase in the martensitic transformation temperature of the base alloy. Although the structure of this phase typically contains a high density of faults making characterization difficult, it appears to be trigonal (-3m point group) with a(sub o) approx. 1.28 nm and c(sub o) approx. 1.4 nm. Precipitation of this phase increases the microhardness of the alloy substantially over that of the solution treated and quenched single-phase material. The effect of precipitation strengthening on the work characteristics of the alloy has been explored through load-biased strain-temperature testing in the solution-treated condition and after aging at 500 C for times ranging from 1 to 256 hours. Work output was found to increase in the aged alloy as a result of an increase in transformation strain, but was not very sensitive to aging time. The amount of permanent deformation that occurred during thermal cycling under load was small but increased with increasing aging time and stress. Nevertheless, the dimensional stability of the alloy at short aging times (1-4 hours) was still very good making it a potentially useful material for high-temperature actuator applications.

An active homopolar magnetic bearing with high temperature superconductor (HTS) coils and ferromagnetic cores

NASA Technical Reports Server (NTRS)

Brown, G. V.; Dirusso, E.; Provenza, A. J.

1995-01-01

A proof-of-feasibility demonstration showed that high temperature superconductor (HTS) coils can be used in a high-load, active magnetic bearing in liquid nitrogen. A homopolar radial bearing with commercially wound HTS (Bi 2223) bias and control coils produced over 200 lb (890 N) radial load capacity (measured non-rotating) and supported a shaft to 14000 rpm. The goal was to show that HTS coils can operate stably with ferromagnetic cores in a feedback controlled system at a current density similar to that in Cu in liquid nitrogen. Design compromises permitted use of circular coils with rectangular cross section. Conductor improvements will eventually permit coil shape optimization, higher current density and higher bearing load capacity. The bias coil, wound with non-twisted, multifilament HTS conductor, required negligible power to carry its direct current. The control coils were wound with monofilament HTS sheathed in Ag. These dissipated negligible power for direct current (i.e. for steady radial load components). When an alternating current (AC) was added, the AC component dissipated power which increased rapidly with frequency and quadratically with AC amplitude. In fact at frequencies above about 2 hz, the effective resistance of the control coil conductor actually exceeds that of the silver which is in electrical parallel with the oxide superconductor. This is at least qualitatively understandable in the context of a Bean-type model of flux and current penetration into a Type II superconductor. Fortunately the dynamic currents required for bearing stability are of small amplitude. These results show that while twisted multifilament conductor is not needed for stable levitation, twisted multifilaments will be required to reduce control power for sizable dynamic loads, such as those due to unbalance.

Mitigation of divertor heat loads by strike point sweeping in high power JET discharges

NASA Astrophysics Data System (ADS)

Silburn, S. A.; Matthews, G. F.; Challis, C. D.; Frigione, D.; Graves, J. P.; Mantsinen, M. J.; Belonohy, E.; Hobirk, J.; Iglesias, D.; Keeling, D. L.; King, D.; Kirov, K.; Lennholm, M.; Lomas, P. J.; Moradi, S.; Sips, A. C. C.; Tsalas, M.; Contributors, JET

2017-12-01

Deliberate periodic movement (sweeping) of the high heat flux divertor strike lines in tokamak plasmas can be used to manage the heat fluxes experienced by exhaust handling plasma facing components, by spreading the heat loads over a larger surface area. Sweeping has recently been adopted as a routine part of the main high performance plasma configurations used on JET, and has enabled pulses with 30 MW plasma heating power and 10 MW radiation to run for 5 s without overheating the divertor tiles. We present analysis of the effectiveness of sweeping for divertor temperature control on JET, using infrared camera data and comparison with a simple 2D heat diffusion model. Around 50% reduction in tile temperature rise is obtained with 5.4 cm sweeping compared to the un-swept case, and the temperature reduction is found to scale slower than linearly with sweeping amplitude in both experiments and modelling. Compatibility of sweeping with high fusion performance is demonstrated, and effects of sweeping on the edge-localised mode behaviour of the plasma are reported and discussed. The prospects of using sweeping in future JET experiments with up to 40 MW heating power are investigated using a model validated against existing experimental data.

A historical perspective of the YF-12A thermal loads and structures program

NASA Technical Reports Server (NTRS)

Jenkins, Jerald M.; Quinn, Robert D.

1996-01-01

Around 1970, the Y-F-12A loads and structures efforts focused on numerous technological issues that needed defining with regard to aircraft that incorporate hot structures in the design. Laboratory structural heating test technology with infrared systems was largely created during this program. The program demonstrated the ability to duplicate the complex flight temperatures of an advanced supersonic airplane in a ground-based laboratory. The ability to heat and load an advanced operational aircraft in a laboratory at high temperatures and return it to flight status without adverse effects was demonstrated. The technology associated with measuring loads with strain gages on a hot structure was demonstrated with a thermal calibration concept. The results demonstrated that the thermal stresses were significant although the airplane was designed to reduce thermal stresses. Considerable modeling detail was required to predict the heat transfer and the corresponding structural characteristics. The overall YF-12A research effort was particularly productive, and a great deal of flight, laboratory, test and computational data were produced and cross-correlated.

Solubility of carbon dioxide in aqueous mixtures of alkanolamines

DOE Office of Scientific and Technical Information (OSTI.GOV)

Dawodu, O.F.; Meisen, A.

1994-07-01

The solubility of CO[sub 2] in water + N-methyldiethanolamine + monoethanolamine (MDEA + MEA) and water + N-methyldiethanolamine + diethanolamine (MDEA + DEA) are reported at two compositions of 3.4 M MDEA + 0.8 M MEA or DEA and 2.1 M MDEA + 2.1 M MEA or DEA at temperatures from 70 to 180 C and CO[sub 2] partial pressures from 100 to 3,850 kPa. The solubility of CO[sub 2] in the blends decreased with an increase in temperature but increased with an increase in CO[sub 2] partial pressure. At low partial pressures of CO[sub 2] and the same totalmore » amine concentration, the equilibrium CO[sub 2] loadings were in the order MDEA + MEA > MDEA + DEA > MDEA. However, at high CO[sub 2] partial pressures, the equilibrium CO[sub 2] loadings in the MDEA solutions were higher than those of the MDEA + MEA and MDEA + DEA blends of equal molar strengths due to the stoichiometric loading limitations of MEA and DEA. The nonadditivity of the equilibrium loadings for single amine systems highlights the need for independent measurements on amine blends.« less

Electroluminescence of hot electrons in AlGaN/GaN high-electron-mobility transistors under radio frequency operation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Brazzini, Tommaso, E-mail: tommaso.brazzini@bristol.ac.uk; Sun, Huarui; Uren, Michael J.

2015-05-25

Hot electrons in AlGaN/GaN high electron mobility transistors are studied during radio frequency (RF) and DC operation by means of electroluminescence (EL) microscopy and spectroscopy. The measured EL intensity is decreased under RF operation compared to DC at the same average current, indicating a lower hot electron density. This is explained by averaging the DC EL intensity over the measured load line used in RF measurements, giving reasonable agreement. In addition, the hot electron temperature is lower by up to 15% under RF compared to DC, again at least partially explainable by the weighted averaging along the specific load line.more » However, peak electron temperature under RF occurs at high V{sub DS} and low I{sub DS} where EL is insignificant suggesting that any wear-out differences between RF and DC stress of the devices will depend on the balance between hot-carrier and field driven degradation mechanisms.« less

Analytical and experimental studies of heat pipe radiation cooling of hypersonic propulsion systems

NASA Technical Reports Server (NTRS)

Martin, R. A.; Merrigan, M. A.; Elder, M. G.; Sena, J. T.; Keddy, E. S.; Silverstein, C. C.

1992-01-01

Analytical and experimental studies were completed to assess the feasibility of using high-temperature heat pipes to cool hypersonic engine components. This new approach involves using heat pipes to transport heat away from the combustor, nozzle, or inlet regions, and to reject it to the environment by thermal radiation from an external heat pipe nacelle. For propulsion systems using heat pipe radiation cooling (HPRC), it is possible to continue to use hydrocarbon fuels into the Mach 4 to Mach 6 speed range, thereby enhancing the economic attractiveness of commercial or military hypersonic flight. In the second-phase feasibility program recently completed, it is found that heat loads produced by considering both convection and radiation heat transfer from the combustion gas can be handled with HPRC design modifications. The application of thermal insulation to ramburner and nozzle walls was also found to reduce the heat load by about one-half and to reduce peak HPRC system temperatures to below 2700 F. In addition, the operation of HPRC at cruise conditions of around Mach 4.5 and at an altitude of 90,000 ft lowers the peak hot-section temperatures to around 2800 F. An HPRC heat pipe was successfully fabricated and tested at Mach 5 conditions of heat flux, heat load, and temperature.

Time-Temperature Dependent Response of Filament Wound Composites for Flywheel Rotors

NASA Technical Reports Server (NTRS)

Thesken, John C.; Bowman, Cheryl L.; Arnold, Steven M.; Thompson, Richard C.

2004-01-01

Flywheel energy storage offers an attractive alternative to battery systems used in space applications such as the International Space Station. Rotor designs capable of high specific energies benefit from the load carrying capacity of hoop wound carbon fibers but their long-term durability may be limited by time-temperature dependent radial deformations. This was investigated for the carbon/epoxy rotor material, IM7/8552. Coupon specimens were sectioned from filament wound panels. These were tested in compression and tension at room temperature (RT), 95 and 135 C for strain rates from 5x10(exp -6) per second to 5x10(exp -3) per second. Time, temperature and load sign dependent effects were significant transverse to the fiber. At -0.5 percent strain for 72 hr, compressive stresses relaxed 16.4 percent at 135 C and 13 percent at 95 C. Tensile stresses relaxed only 7 percent in 72 hr at 135 C for 0.5 percent strain. Using linear hereditary material response and Boltzmann s principle of superposition to describe this behavior is problematic if not intractable. Micromechanics analysis including the effects of processing residual stresses is needed to resolve the paradoxes. Uniaxial compressive stress relaxation data may be used to bound the loss of radial pre-load stresses in flywheel rotors.

Solid Polymer Electrolyte (SPE) fuel cell technology program

NASA Technical Reports Server (NTRS)

1978-01-01

Many previously demonstrated improved fuel cell features were consolidated to (1) obtain a better understanding of the observed characteristics of the operating laboratory-sized cells; (2) evaluate appropriate improved fuel cell features in 0.7 sq ft cell hardware; and (3) study the resultant fuel cell capability and determine its impact on various potential fuel cell space missions. The observed performance characteristics of the fuel cell at high temperatures and high current densities were matched with a theoretical model based on the change in Gibbs free energy voltage with respect to temperature and internal resistance change with current density. Excellent agreement between the observed and model performance was obtained. The observed performance decay with operational time on cells with very low noble metal loadings (0.05 mg/sq cm) were shown to be related to loss in surface area. Cells with the baseline amount of noble catalyst electrode loading demonstrated over 40,000 hours of stable performance.

Analyzing Axial Stress and Deformation of Tubular for Steam Injection Process in Deviated Wells Based on the Varied (T, P) Fields

PubMed Central

Liu, Yunqiang; Xu, Jiuping; Wang, Shize; Qi, Bin

2013-01-01

The axial stress and deformation of high temperature high pressure deviated gas wells are studied. A new model is multiple nonlinear equation systems by comprehensive consideration of axial load of tubular string, internal and external fluid pressure, normal pressure between the tubular and well wall, and friction and viscous friction of fluid flowing. The varied temperature and pressure fields were researched by the coupled differential equations concerning mass, momentum, and energy equations instead of traditional methods. The axial load, the normal pressure, the friction, and four deformation lengths of tubular string are got ten by means of the dimensionless iterative interpolation algorithm. The basic data of the X Well, 1300 meters deep, are used for case history calculations. The results and some useful conclusions can provide technical reliability in the process of designing well testing in oil or gas wells. PMID:24163623

Elevated temperature biaxial fatigue

NASA Technical Reports Server (NTRS)

Jordan, E. H.

1983-01-01

Biaxial fatigue is often encountered in the complex thermo-mechanical loadings present in gas turbine engines. Engine strain histories can involve non-constant temperature, mean stress, creep, environmental effects, both isotropic and anisotropic materials and non-proportional loading. Life prediction for the general case involving all the above factors is not a practicable research project. The current research program is limited to isothermal fatigue at room temperature and 1200 F of Hastalloy-X for both proportional and non-proportional loading. An improved method for predicting the fatigue life and deformation response under biaxial cycle loading is sought.

Strong Electron Self-Cooling in the Cold-Electron Bolometers Designed for CMB Measurements

NASA Astrophysics Data System (ADS)

Kuzmin, L. S.; Pankratov, A. L.; Gordeeva, A. V.; Zbrozhek, V. O.; Revin, L. S.; Shamporov, V. A.; Masi, S.; de Bernardis, P.

2018-03-01

We have realized cold-electron bolometers (CEB) with direct electron self-cooling of the nanoabsorber by SIN (Superconductor-Insulator-Normal metal) tunnel junctions. This electron self-cooling acts as a strong negative electrothermal feedback, improving noise and dynamic properties. Due to this cooling the photon-noise-limited operation of CEBs was realized in array of bolometers developed for the 345 GHz channel of the OLIMPO Balloon Telescope in the power range from 10 pW to 20 pW at phonon temperature Tph =310 mK. The negative electrothermal feedback in CEB is analogous to TES but instead of artificial heating we use cooling of the absorber. The high efficiency of the electron self-cooling to Te =100 mK without power load and to Te=160 mK under power load is achieved by: - a very small volume of the nanoabsorber (0.02 μm3) and a large area of the SIN tunnel junctions, - effective removal of hot quasiparticles by arranging double stock at both sides of the junctions and close position of the normal metal traps, - self-protection of the 2D array of CEBs against interferences by dividing them between N series CEBs (for voltage interferences) and M parallel CEBs (for current interferences), - suppression of Andreev reflection by a thin layer of Fe in the AlFe absorber. As a result even under high power load the CEBs are working at electron temperature Te less than Tph . To our knowledge, there is no analogue in the bolometers technology in the world for bolometers working at electron temperature colder than phonon temperature.

Development and qualification of a bulk tungsten divertor row for JET

NASA Astrophysics Data System (ADS)

Mertens, Ph.; Altmann, H.; Hirai, T.; Philipps, V.; Pintsuk, G.; Rapp, J.; Riccardo, V.; Schweer, B.; Uytdenhouwen, I.; Samm, U.

2009-06-01

A bulk tungsten divertor row has been developed in the frame of the ITER-like Wall project at JET. It consists of 96 tiles grouped in 48 modules around the torus. The outer strike point is located on those tiles for most of the ITER-relevant, high triangularity plasmas. High power loads (locally up to 10-20 MW/m 2) and erosion rates are expected, even a risk of melting, especially with the transients or ELM loads. These are demanding conditions for an inertially cooled design as prescribed. A lamella design has been selected for the tungsten, arranged to control the eddy and halo current flows. The lamellae must also withstand high temperature gradients (2200 to 220 °C over 40 mm height), without overheating the supporting carrier (600-700 °C maximum). As a consequence of the tungsten emissivity, the radiative cooling drops appreciably in comparison with the current CFC tiles, calling for interleaved plasma scenarios in terms of performance. The compromise between shadowing and power handling is discussed, as well as the consequences for operation. Prototypes have been exposed in TEXTOR and in an electron beam facility (JUDITH-2) to the nominal power density of 7 MW/m 2 for 10 s and, in addition, to higher loads leading to surface temperatures above 2000 °C.

Creep-Fatigue Damage Investigation and Modeling of Alloy 617 at High Temperatures

NASA Astrophysics Data System (ADS)

Tahir, Fraaz

The Very High Temperature Reactor (VHTR) is one of six conceptual designs proposed for Generation IV nuclear reactors. Alloy 617, a solid solution strengthened Ni-base superalloy, is currently the primary candidate material for the tubing of the Intermediate Heat Exchanger (IHX) in the VHTR design. Steady-state operation of the nuclear power plant at elevated temperatures leads to creep deformation, whereas loading transients including startup and shutdown generate fatigue. A detailed understanding of the creep-fatigue interaction in Alloy 617 is necessary before it can be considered as a material for nuclear construction in ASME Boiler and Pressure Vessel Code. Current design codes for components undergoing creep-fatigue interaction at elevated temperatures require creep-fatigue testing data covering the entire range from fatigue-dominant to creep-dominant loading. Classical strain-controlled tests, which produce stress relaxation during the hold period, show a saturation in cycle life with increasing hold periods due to the rapid stress-relaxation of Alloy 617 at high temperatures. Therefore, applying longer hold time in these tests cannot generate creep-dominated failure. In this study, uniaxial isothermal creep-fatigue tests with non-traditional loading waveforms were designed and performed at 850 and 950°C, with an objective of generating test data in the creep-dominant regime. The new loading waveforms are hybrid strain-controlled and force-controlled testing which avoid stress relaxation during the creep hold. The experimental data showed varying proportions of creep and fatigue damage, and provided evidence for the inadequacy of the widely-used time fraction rule for estimating creep damage under creep-fatigue conditions. Micro-scale damage features in failed test specimens, such as fatigue cracks and creep voids, were quantified using a Scanning Electron Microscope (SEM) to find a correlation between creep and fatigue damage. Quantitative statistical imaging analysis showed that the microstructural damage features (cracks and voids) are correlated with a new mechanical driving force parameter. The results from this image-based damage analysis were used to develop a phenomenological life-prediction methodology called the effective time fraction approach. Finally, the constitutive creep-fatigue response of the material at 950°C was modeled using a unified viscoplastic model coupled with a damage accumulation model. The simulation results were used to validate an energy-based constitutive life-prediction model, as a mechanistic model for potential component and structure level creep-fatigue analysis.

Further Investigations of Control Surface Seals for the X-38 Re-Entry Vehicle

NASA Technical Reports Server (NTRS)

Dunlap, Patrick H., Jr.; Steinetz, Bruce M.; Curry, Donald M.; Newquist, Charles W.; Verzemnieks, Juris

2001-01-01

NASA is currently developing the X-38 vehicle that will be used to demonstrate the technologies required for a potential crew return vehicle (CRV) for the International Space Station. This vehicle would serve both as an ambulance for medical emergencies and as an evacuation vehicle for the Space Station. Control surfaces on the X-38 (body flaps and rudder/fin assemblies) require high temperature seals to limit hot gas ingestion and transfer of heat to underlying low-temperature structures to prevent over-temperature of these structures and possible loss of the vehicle. NASAs Johnson Space Center (JSC) and Glenn Research Center (GRC) are working together to develop and evaluate seals for these control surfaces. This paper presents results for compression. flow, scrub, and arc jet tests conducted on the baseline X-38 rudder/fin seal design. Room temperature seal compression tests were performed at low compression levels to determine load versus linear compression, preload. contact area, stiffness. and resiliency characteristics under low load conditions. For all compression levels that were tested, unit loads and contact pressures for the seals were below the 5 lb/in. and 10 psi limits required to limit the loads on the adjoining Shuttle thermal tiles that the seals will contact. Flow rates through an unloaded (i.e. 0% compression) double arrangement were twice those of a double seal compressed to the 20% design compression level. The seals survived an ambient temperature 1000 cycle scrub test over relatively rough Shuttle tile surfaces. The seals were able to disengage and re-engage the edges of the rub surface tiles while being scrubbed over them. Arc jet tests were performed to experimentally determine anticipated seal temperatures for representative flow boundary conditions (pressures and temperatures) under simulated vehicle re-entry conditions. Installation of a single seat in the gap of the test fixture caused a large temperature drop (1710 F) across the seal location as compared to an open gap condition (140 F) confirming the need for seals in the rudder/fin gap location. The seal acted as an effective thermal barrier limiting heat convection through the seal gap and minimizing temperature increases downstream of the seal during maximum heating conditions.

Multifunctional Properties of Cyanate Ester Composites with SiO2 Coated Fe3O4 Fillers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sun, Weixing; Sun, Wuzhu; Kessler, Michael R

2013-02-22

SiO2 coated Fe3O4 submicrometer spherical particles (a conducting core/insulating shell configuration) are fabricated using a hydrothermal method and are loaded at 10 and 20 vol % into a bisphenol E cyanate ester matrix for synthesis of multifunctional composites. The dielectric constant of the resulting composites is found to be enhanced over a wide frequency and temperature range while the low dielectric loss tangent of the neat cyanate ester polymer is largely preserved up to 160 ?C due to the insulating SiO2 coating on individual conductive Fe3O4 submicrometer spheres. These composites also demonstrate high dielectric breakdown strengths at room temperature. Dynamicmore » mechanical analysis indicates that the storage modulus of the composite with a 20 vol % filler loading is twice as high as that of neat resin, but the glass transition temperature considerably decreases with increasing filler content. Magnetic measurements reveal a large saturation magnetization and negligibly low coercivity and remanent magnetization in these composites.« less