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Sample records for high wear applications

  1. Elastomer Compound Developed for High Wear Applications

    NASA Technical Reports Server (NTRS)

    Crawford, D.; Feuer, H.; Flanagan, D.; Rodriguez, G.; Teets, A.; Touchet, P.

    1993-01-01

    The U.S. Army is currently spending 300 million dollars per year replacing rubber track pads. An experimental rubber compound has been developed which exhibits 2 to 3 times greater service life than standard production pad compounds. To improve the service life of the tank track pads various aspects of rubber chemistry were explored including polymer, curing and reinforcing systems. Compounds that exhibited superior physical properties based on laboratory data were then fabricated into tank pads and field tested. This paper will discuss the compounding studies, laboratory data and field testing that led to the high wear elastomer compound.

  2. High Temperature Solid Lubricant Coating for High Temperature Wear Applications

    NASA Technical Reports Server (NTRS)

    DellaCorte, Christopher (Inventor); Edmonds, Brian J (Inventor)

    2014-01-01

    A self-lubricating, friction and wear reducing composite useful over a wide temperature range is described herein. The composite includes metal bonded chromium oxide dispersed in a metal binder having a substantial amount of nickel. The composite contains a fluoride of at least one Group I, Group II, or rare earth metal, and optionally a low temperature lubricant metal.

  3. High Strength and Wear Resistant Aluminum Alloy for High Temperature Applications

    NASA Technical Reports Server (NTRS)

    Lee, Jonathan A.; Munafo, Paul M. (Technical Monitor)

    2002-01-01

    In this paper, a new high strength and wear resistant aluminum cast alloy invented by NASA-MSFC for high temperature applications will be presented. Developed to meet U.S. automotive legislation requiring low-exhaust emission, the novel NASA 398 aluminum-silicon alloy offers dramatic improvement in tensile and fatigue strengths at elevated temperatures (500 F-800 F), enabling new pistons to utilize less material, which can lead to reducing part weight and cost as well as improving performance. NASA 398 alloy also offers greater wear resistance, surface hardness, dimensional stability, and lower thermal expansion compared to conventional aluminum alloys for several commercial and automotive applications. The new alloy can be produced economically using permanent steel molds from conventional gravity casting or sand casting. The technology was developed to stimulate the development of commercial aluminum casting products from NASA-developed technology by offering companies the opportunity to license this technology.

  4. Nano Structured Plasma Spray Coating for Wear and High Temperature Corrosion Resistance Applications

    NASA Astrophysics Data System (ADS)

    Ghosh, D.; Shukla, A. K.; Roy, H.

    2014-04-01

    The nano structured coating is a major challenge today to improve the different mechanical properties, wear and high temperature corrosion resistance behaviour of different industrial alloys. This paper is a review on synthesis of nano powder, plasma spraying methods, techniques of nano structured coating by plasma spray method, mechanical properties, tribological properties and high temperature corrosion behaviour of nano structured coating. Nano structured coatings of ceramic powders/composites are being developed for wide variety of applications like boiler, turbine and aerospace industries, which requires the resistance against wear, corrosion, erosion etc. The nano sized powders are subjected to agglomeration by spray drying, after which nano structured coating can be successfully applied over the substrate. Nano structured coating shows improved mechanical wear resistance and high temperature corrosion resistance. The significant improvement of wear and corrosion resistance is mainly attributed to formation of semi molten nano zones in case of nano structured coatings. The future scope of application of nano structured coating has also been highlighted in this paper.

  5. High Strength and Wear Resistant Aluminum Alloy for High Temperature Applications

    NASA Technical Reports Server (NTRS)

    Lee, Jonathan A.; Chen, Po Shou

    2003-01-01

    Originally developed by NASA as high performance piston alloys to meet U.S. automotive legislation requiring low exhaust emission, the novel NASA alloys now offer dramatic increase in tensile strength for many other applications at elevated temperatures from 450 F (232 C) to about 750 F (400 C). It is an ideal low cost material for cast automotive components such as pistons, cylinder heads, cylinder liners, connecting rods, turbo chargers, impellers, actuators, brake calipers and rotors. It can be very economically produced from conventional permanent mold, sand casting or investment casting, with silicon content ranging from 6% to 18%. At high silicon levels, the alloy exhibits excellent thermal growth stability, surface hardness and wear resistant properties.

  6. Characterization of thermally sprayed coatings for high-temperature wear-protection applications

    SciTech Connect

    Li, C.C.

    1980-03-01

    Under normal high-temperature gas-cooled reactor (HTGR) operating conditions, faying surfaces of metallic components under high contact pressure are prone to friction, wear, and self-welding damage. Component design calls for coatings for the protection of the mating surfaces. Anticipated operating temperatures up to 850 to 950/sup 0/C (1562 to 1742/sup 0/F) and a 40-y design life require coatings with excellent thermal stability and adequate wear and spallation resistance, and they must be compatible with the HTGR coolant helium environment. Plasma and detonation-gun (D-gun) deposited chromium carbide-base and stabilized zirconia coatings are under consideration for wear protection of reactor components such as the thermal barrier, heat exchangers, control rods, and turbomachinery. Programs are under way to address the structural integrity, helium compatibility, and tribological behavior of relevant sprayed coatings. In this paper, the need for protection of critical metallic components and the criteria for selection of coatings are discussed. The technical background to coating development and the experience with the steam cycle HTGR (HTGR-SC) are commented upon. Coating characterization techniques employed at General Atomic Company (GA) are presented, and the progress of the experimental programs is briefly reviewed. In characterizing the coatings for HTGR applications, it is concluded that a systems approach to establish correlation between coating process parameters and coating microstructural and tribological properties for design consideration is required.

  7. Development and Application of High Performance Quenched and Tempered Wear Resistant Steels in Material Handling and Construction Machinery

    NASA Astrophysics Data System (ADS)

    Su, Fenwei; Sidiras, Evangelos

    The demand for more sustainable development promotes the need for components and steel structures with a longer useful life and better performance. Upgrade of wear steel plate used in key industry segments such as mining, recycling and road building results in the stable growth of global market with high quality grade Q&T wear plates (Hardness HBW≥400, and Yield strength ≥690 Mpa). SSAB has now expanded its wear steel product range by both thicker and thinner Q&T plate to meet the needs of the market, and can offer wear plates from 0.7 mm to 160 mm. The continuous research and development is being done to offer even thicker plates. This article introduces the performance and advantages of high quality grade Q&T wear resistant steel products (plate, strip, tube and round bars) produced in SSAB, and also describes typical applications in some industrial segments such as material handling and construction machinery.

  8. NASA PS400: A New Temperature Solid Lubricant Coating for High Temperature Wear Applications

    NASA Technical Reports Server (NTRS)

    DellaCorte, C.; Edmonds, B. J.

    2009-01-01

    A new solid lubricant coating, NASA PS400, has been developed for high temperature tribological applications. This plasma sprayed coating is a variant of the patented PS304 coating and has been formulated to provide higher density, smoother surface finish and better dimensional stability than PS304. PS400 is comprised of a nickel-molybdenum binder that provides strength, creep resistance and extreme oxidative and dimensional stability. Chromium oxide, silver and barium-calcium fluoride eutectic are added to the binder to form PS400.Tribological properties were evaluated with a pin-on-disk test rig in sliding contact to 650 C. Coating material samples were exposed to air, argon and vacuum at 760 C followed by cross section microscopic analysis to assess microstructure stability. Oil-Free microturbine engine hot section foil bearing tests were undertaken to assess PS400 s suitability for hot foil gas bearing applications. The preliminary results indicate that PS400 exhibits tribological characteristics comparable to the PS304 coating but with enhanced creep resistance and dimensional stability suitable for demanding, dynamic applications.

  9. Wear of highly crosslinked polyethylene acetabular components

    PubMed Central

    Callary, Stuart A; Solomon, Lucian B; Holubowycz, Oksana T; Campbell, David G; Munn, Zachary; Howie, Donald W

    2015-01-01

    Background and purpose Wear rates of highly crosslinked polyethylene (XLPE) acetabular components have varied considerably between different published studies. This variation is in part due to the different techniques used to measure wear and to the errors inherent in measuring the relatively low amounts of wear in XLPE bearings. We undertook a scoping review of studies that have examined the in vivo wear of XLPE acetabular components using the most sensitive method available, radiostereometric analysis (RSA). Methods A systematic search of the PubMed, Scopus, and Cochrane databases was performed to identify published studies in which RSA was used to measure wear of XLPE components in primary total hip arthroplasty (THA). Results 18 publications examined 12 primary THA cohorts, comprising only 260 THAs at 2–10 years of follow-up. The mean or median proximal wear rate reported ranged from 0.00 to 0.06 mm/year. However, differences in the manner in which wear was determined made it difficult to compare some studies. Furthermore, differences in RSA methodology between studies, such as the use of supine or standing radiographs and the use of beaded or unbeaded reference segments, may limit future meta-analyses examining the effect of patient and implant variables on wear rates. Interpretation This scoping review confirmed the low wear rates of XLPE in THA, as measured by RSA. We make recommendations to enhance the standardization of reporting of RSA wear results, which will facilitate early identification of poorly performing implants and enable a better understanding of the effects of surgical and patient factors on wear. PMID:25301435

  10. P/M Materials for Wear Applications

    SciTech Connect

    Hawk, Jeffrey A.

    2000-10-01

    Wear resistant materials usually consist of either very hard homogeneous single phase materials (e.g., ceramics like Al2O3, SiC, etc.) or heterogenous materials (e.g., white cast irons, composites or cermets, or composite-type materials), typically with a hard reinforcing phase dispersed in a softer matrix. In both instances, the result is the same, less penetration of the abrasive into the surface of the material being worn. Composite type materials can be produced using either a melting/solidification scheme or through powder metallurgy (P/M) techniques. In either case the result is the same, a microstructure that consists of a high volume fraction of hard, usually brittle, second phase particles in a softer matrix. However, P/M can be used to create a wider range of these materials than can melting/solidification, because in P/M processing, the desired phase does not have to be precipitated during solidification. Thus, more materials can be produced with higher volume fractions of reinforcing phases. Obviously, other factors like reinforcement size, matrix-particle interfacial strength, plastic accommodation of the matrix, etc. become important in the wear behavior of these materials. Various categories of P/M wear resistant materials will be discussed, and their wear behavior will be compared against traditional wear resistant cast materials like white cast iron and tool steels.

  11. High Temperature Wear of Advanced Ceramics

    NASA Technical Reports Server (NTRS)

    DellaCorte, C.

    2005-01-01

    It was initially hypothesized that advanced ceramics would exhibit favorable high te- friction and wear properties because of their high hot hardness and low achievable surface roughness welding observed in metals does not occur in ceramics. More recent tribological studies of many nitride, carbide, oxide and composite ceramics, however, have revealed that ceramics often exhibit high friction and wear in non-lubricated, high temperature sliding contacts. A summary is given to measure friction and wear factor coefficients for a variety of ceramics from self mated ceramic pin-on-disk tests at temperatures from 25 to up to 1200 C. Observed steady state friction coefficients range from about 0.5 to 1.0 or above. Wear factor coefficients are also very high and range from about to 10(exp -5) to 10(exp -2) cubic millimeters per N-m. By comparison, oil lubricated steel sliding results in friction coefficients of 0.1 or less and wear factors less than 10(exp -9) cubic millimeters per N-m.

  12. Consideration of wear rates at high velocity

    NASA Astrophysics Data System (ADS)

    Hale, Chad S.

    The development of the research presented here is one in which high velocity relative sliding motion between two bodies in contact has been considered. Overall, the wear environment is truly three-dimensional. The attempt to characterize three-dimensional wear was not economically feasible because it must be analyzed at the micro-mechanical level to get results. Thus, an engineering approximation was carried out. This approximation was based on a metallographic study identifying the need to include viscoplasticity constitutive material models, coefficient of friction, relationships between the normal load and velocity, and the need to understand wave propagation. A sled test run at the Holloman High Speed Test Track (HHSTT) was considered for the determination of high velocity wear rates. In order to adequately characterize high velocity wear, it was necessary to formulate a numerical model that contained all of the physical events present. The experimental results of a VascoMax 300 maraging steel slipper sliding on an AISI 1080 steel rail during a January 2008 sled test mission were analyzed. During this rocket sled test, the slipper traveled 5,816 meters in 8.14 seconds and reached a maximum velocity of 1,530 m/s. This type of environment was never considered previously in terms of wear evaluation. Each of the features of the metallography were obtained through micro-mechanical experimental techniques. The byproduct of this analysis is that it is now possible to formulate a model that contains viscoplasticity, asperity collisions, temperature and frictional features. Based on the observations of the metallographic analysis, these necessary features have been included in the numerical model, which makes use of a time-dynamic program which follows the movement of a slipper during its experimental test run. The resulting velocity and pressure functions of time have been implemented in the explicit finite element code, ABAQUS. Two-dimensional, plane strain models

  13. Sensitivity of Dielectric Properties to Wear Process on Carbon Nanofiber/High-Density Polyethylene Composites

    NASA Astrophysics Data System (ADS)

    Liu, Tian; Wood, Weston; Zhong, Wei-Hong

    2011-12-01

    We examined the correlation of wear effects with dielectric properties of carbon nanofibers (CNFs; untreated and organosilane-treated)-reinforced high-density polyethylene (HDPE) composites. Wear testing for the nanocomposites over up to 120 h was carried out, and then, dielectric permittivity and dielectric loss factor of the polymer composites with the increased wear time were studied. Scanning electron microscope and optical microscope observations were made to analyze the microstructure features of the nanocomposites. The results reveal that there exist approximate linear relationships of permittivity with wear coefficient for the nanocomposites. Composites containing silanized CNFs with the sufficiently thick coating exhibited high wear resistance. The change in permittivity was more sensitive to the increased wear coefficient for the nanocomposites with lower wear resistance. This work provides potential for further research on the application of dielectric signals to detect the effects of wear process on lifetime of polymeric materials.

  14. Sensitivity of Dielectric Properties to Wear Process on Carbon Nanofiber/High-Density Polyethylene Composites.

    PubMed

    Liu, Tian; Wood, Weston; Zhong, Wei-Hong

    2011-12-01

    We examined the correlation of wear effects with dielectric properties of carbon nanofibers (CNFs; untreated and organosilane-treated)-reinforced high-density polyethylene (HDPE) composites. Wear testing for the nanocomposites over up to 120 h was carried out, and then, dielectric permittivity and dielectric loss factor of the polymer composites with the increased wear time were studied. Scanning electron microscope and optical microscope observations were made to analyze the microstructure features of the nanocomposites. The results reveal that there exist approximate linear relationships of permittivity with wear coefficient for the nanocomposites. Composites containing silanized CNFs with the sufficiently thick coating exhibited high wear resistance. The change in permittivity was more sensitive to the increased wear coefficient for the nanocomposites with lower wear resistance. This work provides potential for further research on the application of dielectric signals to detect the effects of wear process on lifetime of polymeric materials.

  15. Sensitivity of Dielectric Properties to Wear Process on Carbon Nanofiber/High-Density Polyethylene Composites

    PubMed Central

    2011-01-01

    We examined the correlation of wear effects with dielectric properties of carbon nanofibers (CNFs; untreated and organosilane-treated)-reinforced high-density polyethylene (HDPE) composites. Wear testing for the nanocomposites over up to 120 h was carried out, and then, dielectric permittivity and dielectric loss factor of the polymer composites with the increased wear time were studied. Scanning electron microscope and optical microscope observations were made to analyze the microstructure features of the nanocomposites. The results reveal that there exist approximate linear relationships of permittivity with wear coefficient for the nanocomposites. Composites containing silanized CNFs with the sufficiently thick coating exhibited high wear resistance. The change in permittivity was more sensitive to the increased wear coefficient for the nanocomposites with lower wear resistance. This work provides potential for further research on the application of dielectric signals to detect the effects of wear process on lifetime of polymeric materials. PMID:27502631

  16. Friction, wear, transfer and wear surface morphology of ultra-high-molecular-weight polyethylene

    NASA Technical Reports Server (NTRS)

    Fusaro, R. L.

    1983-01-01

    Tribological studies at 25 C in a 50-percent-relative-humidity air atmosphere were conducted using hemispherically tipped 440 C HT (high temperature) stainless steel pins sliding against ultra-high-molecular-weight polyethylene (UHMWPE) disks. The results indicate that sliding speed, sliding distance, contact stress and specimen geometry can markedly affect friction, UHMWPE wear, UHMWPE transfer and the type of wear mechanisms that occur. Adhesion appears to be the predominant wear mechanism; but after long sliding distances at slow speeds, heavy ridges of transfer result which can induce fatigue-like wear on the UHMWPE disk wear track. In one instance, abrasive wear to the metallic pin was observed. This was caused by a hard particle embedded in the UHMWPE disk wear track.

  17. High-speed wear testing of selected ceramics in abrasive slurry

    NASA Astrophysics Data System (ADS)

    Ismailov, Arnold; Levänen, Erkki

    2013-12-01

    Due to increased production speeds in modern process environments, the loading conditions in sliding contact applications have become more challenging. Therefore it is important to have good understanding of wear mechanisms in high-speed sliding conditions. A wear testing device was manufactured for the purpose of cost-efficient simulation of water-containing high-speed sliding conditions. Sliding speeds up to 40 meters per second can be achieved while abrasive-containing slurry is fed into the contact interface of material samples and a rubber coated drum. High-speed wear tests were run with three ceramic materials: silicon nitride, silicon carbide and partially stabilized zirconia. Wear behavior of these ceramics was analyzed as a function of sliding speed and slurry composition. Results indicate that in mild wear region increase in sliding speed reduced overall wear, whereas in severe wear conditions increasing speed accelerated wear. A transition from mild to severe wear was observed for silicon carbide when tested in alumina-containing slurry. For the materials that had high enough hardness, wear rates were dictated by the respective order of fracture toughness. Visual inspection of the worn samples supported the interpretation of wear mode transition.

  18. Abrasive wear of ceramic wear protection at ambient and high temperatures

    NASA Astrophysics Data System (ADS)

    Varga, M.; Adam, K.; Tumma, M.; Alessio, K. O.

    2017-05-01

    Ceramic wear protection is often applied in abrasive conditions due to their excellent wear resistance. This is especially necessary in heavy industries conveying large amounts of raw materials, e.g. in steel industry. Some plants also require material transport at high temperatures and velocities, making the need of temperature stable and abrasion resistant wear protection necessary. Various types and wear behaviour of ceramic protection are known. Hence, the goal of this study is to identify the best suitable ceramic materials for abrasive conditions in harsh environments at temperatures up to 950°C and severe thermal gradients. Chamottes, known for their excellent thermal shock resistance are compared to high abrasion resistant ceramic wear tiles and a cost efficient cement-bounded hard compound. Testing was done under high-stress three-body abrasion regime with a modified ASTM G65 apparatus enabling for investigations up to ~950°C. Thereto heated abrasive is introduced into the wear track and also preheated ceramic samples were used and compared to ambient temperature experiments. Results indicate a significant temperature influence on chamottes and the hard compound. While the chamottes benefit from temperature increase, the cement-bounded hard compound showed its limitation at abrasive temperatures of 950°C. The high abrasion resistant wear tiles represented the materials with the best wear resistance and less temperature influence in the investigated range.

  19. Wear performance of garnet aluminium composites at high contact pressure

    NASA Astrophysics Data System (ADS)

    Sharma, Anju; Arora, Rama; Kumar, Suresh; Singh, Gurmel; Pandey, O. P.

    2016-05-01

    To satisfy the needs of the engineering sector, researchers and material scientists in this area adopted the development of composites with tailor made properties to enhance efficiency and cost savings in the manufacturing sector. The technology of the mineral industry is shaping the supply and demand of minerals derived materials. The composites are best classified as high performance materials have high strength-to-weight ratios, and require controlled manufacturing environments for optimum performance. Natural mineral garnet was used as the reinforcement of composite because of satisfactory mechanical properties as well as an attractive ecological alternative to others ceramics. For this purpose, samples have been prepared with different sizesof the garnet reinforcement using the mechanical stirring method to achieve the homogeneously dispersed strengthening phase. A systematic study of the effect of high contact pressure on the sliding wear behaviour of garnet reinforced LM13 alloy composites is presented in this paper. The SEM analysis of the worn samples and debris reveals the clues about the wear mechanism. The drastic improvement in the wear resistance of the composites at high contact pressure shows the high potential of the material to be used in engineering applications.

  20. A review on nozzle wear in abrasive water jet machining application

    NASA Astrophysics Data System (ADS)

    Syazwani, H.; Mebrahitom, G.; Azmir, A.

    2016-02-01

    This paper discusses a review on nozzle wear in abrasive water jet machining application. Wear of the nozzle becomes a major problem since it may affect the water jet machining performance. Design, materials, and life of the nozzle give significance effect to the nozzle wear. There are various parameters that may influence the wear rate of the nozzle such as nozzle length, nozzle inlet angle, nozzle diameter, orifice diameter, abrasive flow rate and water pressure. The wear rate of the nozzle can be minimized by controlling these parameters. The mechanism of wear in the nozzle is similar to other traditional machining processes which uses a cutting tool. The high pressure of the water and hard abrasive particles may erode the nozzle wall. A new nozzle using a tungsten carbide-based material has been developed to reduce the wear rate and improve the nozzle life. Apart from that, prevention of the nozzle wear has been achieved using porous lubricated nozzle. This paper presents a comprehensive review about the wear of abrasive water jet nozzle.

  1. Wear Testing of Moving Components in Ultra-High Vacuum

    NASA Astrophysics Data System (ADS)

    Short, Arnelia; McAlister, T.; Ellis, R.; Mosleh, M.

    2010-11-01

    Wear and friction in moving parts in an Ultra-High Vacuum (UHV) environment is a fundamental challenge in the design of mechanical assemblies in fusion experiments. In a reactor-scale experiment, constraints have been placed on the material choices and mechanical motions within the system due to their vacuum environment. Wear and friction only serve to complicate these constraints. Textured surfaces, bonded lubricants, and vacuum compatible greases have shown promise as possible means of reducing friction and wear. We have designed a machine for testing wear in a UHV environment, at room temperature, and elevated temperatures. This poster describes the design of the wear test machine and its operating parameters. We have presented an outline of the material test program along with a discussion of the pros and cons of anti-friction and anti-wear treatments.

  2. Consideration of Wear Rates at High Velocity

    DTIC Science & Technology

    2010-03-01

    37 α ferrite or alpha phase iron . . . . . . . . . . . . . . . . . . 37 ux horizontal displacement degree of freedom . . . . . . . . . 85 uy vertical...steel, constantan, zinc , aluminum and nickel. The disk, made of gun steel, was 60.96 cm in diameter. Wear was determined by measuring the weight loss of... ferrite , or alpha phase iron. When held at equilibrium at temperatures of 590◦C (1100◦F) and above under equilibrium conditions, the structure will

  3. Evaluation of the wear properties of high interstitial stainless steels

    SciTech Connect

    Tylczak, J.H.; Rawers, J.C.; Alman, D.E.

    2007-04-01

    Adding carbon to high nitrogen steels increases interstitial concentrations over what can be obtained with nitrogen addition alone. This can results in an increase in hardness, strength, and wear resistance. The alloys produced for this study were all based on commercially available high-nitrogen Fe-18Cr-18Mn stainless steel. This study is the first significant wear study of these new high interstitial nitrogen-carbon stainless steel alloys. Wear tests included: scratch, pin-on-disk abrasion, dry sand/rubber wheel abrasion, impeller impact, and jet erosion. Increasing interstitial concentration increased strength and hardness and improved wear resistance under all test conditions. The results are discussed in terms of overall interstitial alloy concentration.

  4. Experiment on wear behavior of high pressure gas seal faces

    NASA Astrophysics Data System (ADS)

    Xu, Jing; Peng, Xudong; Bai, Shaoxian; Meng, Xiangkai; Li, Jiyun

    2014-11-01

    Current researches show that mechanical deformation of seal ring face makes fluid film clearance decrease at high pressure side, thus a divergent clearance is formed and face wear occurs more seriously at the high pressure side than that on the low pressure side. However, there is still lack of published experimental works enough to prove the theoretical results. In this paper, a spiral groove dry gas seal at high pressures is experimentally investigated so as to prove the face wear happened at the high pressure side of seal faces due to the face mechanical deformation, and the wear behavior affected by seal ring structure is also studied. The experimental results show that face wear would occur at the high pressure side of seal faces due to the deformation, thus the leakage and face temperature increase, which all satisfies the theoretical predictions. When sealed pressure is not less than 5 MPa, the pressure can provide enough opening force to separate the seal faces. The seal ring sizes have obvious influence on face wear. Face wear, leakage and face temperature of a dry gas seal with the smaller cross sectional area of seal ring are less than that of a dry gas seal with bigger one, and the difference of leakage rate between these two sizes of seal face width is in the range of 24%-25%. Compared with the effect of seal ring sizes, the effect of secondary O-ring seal position on face deformation and face wear is less. The differences between these two types of dry gas seals with different secondary O-ring seal positions are less than 5.9% when the rotational speed varies from 0 to 600 r/min. By linking face wear and sealing performance changes to the shift in mechanical deformation of seal ring, this research presents an important experimental method to study face deformation of a dry gas seal at high pressures.

  5. An Evaluation of High Velocity Wear

    DTIC Science & Technology

    2007-03-01

    x10F~ -4 [18:18-19]. Authors such as Hutchings and Rabinowicz however, do not explicitly limit equation (12) to plastic wear. They suggest that...2:0; K=11604.5; %Constant for converting from Kelvin to eV for CTH N=size(y,1); T0=T(1); Tf=T(N); [C,I]=max(T); %Find the Maximum...package rail * normal level rail height material 2 numsub 100 temperature = 2.55935e-2 * eV = 74.93F = 297 K xvel 0.0 yvel 0.0

  6. Sliding friction and wear behavior of high entropy alloys at room and elevated temperatures

    NASA Astrophysics Data System (ADS)

    Kadhim, Dheyaa

    Structure-tribological property relations have been studied for five high entropy alloys (HEAs). Microhardness, room and elevated (100°C and 300°C) temperature sliding friction coefficients and wear rates were determined for five HEAs: Co0.5 Cr Cu0.5 Fe Ni1.5 Al Ti0.4; Co Cr Fe Ni Al0.25 Ti0.75; Ti V Nb Cr Al; Al0.3CoCrFeNi; and Al0.3CuCrFeNi2. Wear surfaces were characterized with scanning electron microscopy and micro-Raman spectroscopy to determine the wear mechanisms and tribochemical phases, respectively. It was determined that the two HEAs Co0.5 Cr Cu0.5 Fe Ni1.5 Al Ti0.4 and Ti V Nb Cr Al exhibit an excellent balance of high hardness, low friction coefficients and wear rates compared to 440C stainless steel, a currently used bearing steel. This was attributed to their more ductile body centered cubic (BCC) solid solution phase along with the formation of tribochemical Cr oxide and Nb oxide phases, respectively, in the wear surfaces. This study provides guidelines for fabricating novel, low-friction, and wear-resistant HEAs for potential use at room and elevated temperatures, which will help reduce energy and material losses in friction and wear applications.

  7. Surface texture measurement for dental wear applications

    NASA Astrophysics Data System (ADS)

    Austin, R. S.; Mullen, F.; Bartlett, D. W.

    2015-06-01

    The application of surface topography measurement and characterization within dental materials science is highly active and rapidly developing, in line with many modern industries. Surface measurement and structuring is used extensively within oral and dental science to optimize the optical, tribological and biological performance of natural and biomimetic dental materials. Although there has historically been little standardization in the use and reporting of surface metrology instrumentation and software, the dental industry is beginning to adopt modern areal measurement and characterization techniques, especially as the dental industry is increasingly adopting digital impressioning techniques in order to leverage CAD/CAM technologies for the design and construction of dental restorations. As dental treatment becomes increasingly digitized and reliant on advanced technologies such as dental implants, wider adoption of standardized surface topography and characterization techniques will become evermore essential. The dental research community welcomes the advances that are being made in surface topography measurement science towards realizing this ultimate goal.

  8. WEAR BEHAVIOR OF CARBON NANOTUBE/HIGH DENSITY POLYETHYLENE COMPOSITES

    PubMed Central

    Johnson, Brian B.; Novotny, John E.; Advani, Suresh G.

    2009-01-01

    Carbon Nanotube/High Density Polyethylene (CNT/HDPE) composites were manufactured and tested to determine their wear behavior. The nanocomposites were made from untreated multi-walled carbon nanotubes and HDPE pellets. Thin films of the precursor materials were created with varying weight percentages of nanotubes (1%, 3%, and 5%), through a process of mixing and extruding. The precursor composites were then molded and machined to create test specimens for mechanical and wear tests. These included small punch testing to compare stiffness, maximum load and work-to-failure and block-on-ring testing to determine wear behavior. Each of the tests was conducted for the different weight percentages of composite as well as pure HDPE as the baseline. The measured mechanical properties and wear resistance of the composite materials increased with increasing nanotube content in the range studied. PMID:20161101

  9. New Oxide Ceramic Developed for Superior High-Temperature Wear Resistance

    NASA Technical Reports Server (NTRS)

    Sayir, Ali; Miyoshi, Kazuhisa; Farmer, Serene C.

    2003-01-01

    Ceramics, for the most part, do not have inherently good tribological properties. For example friction coefficients in excess of 0.7 have been reported for silicon nitride sliding on silicon nitride or on bearing steel (ref. 1). High friction is always accompanied by considerable wear. Despite their inherently poor tribological properties, the high strength and high toughness of silicon nitride (Si3N4) ceramics has led to their successful use in tribological applications (refs. 1 to 4). The upper temperature limit for the application of Si3N4 as wear-resistant material is limited by reaction with the tribological environment (ref. 3). Silicon nitride is known to produce a thin silicon dioxide film with easy shear capability that results in low friction and low wear in a moist environment (ref. 5). At elevated temperatures, the removal of the reaction product that acts as lubricant causes the friction coefficient to increase and, consequently, the wear performance to become poor. New materials are sought that will have wear resistance superior to that of Si3N4 at elevated temperatures and in harsh environments. A new class of oxide ceramic materials has been developed with potential for excellent high-temperature wear resistance. The new material consists of a multicomponent oxide with a two-phase microstructure, in which the wear resistance of the mixed oxide is significantly higher than that of the individual constituents. This is attributed to the strong constraining effects provided by the interlocking microstructures at different length scales, to the large aspect ratio of the phases, to the strong interphase bonding, and to the residual stresses. Fretting wear tests were conducted by rubbing the new ceramic material against boron carbide (B4C). The new ceramic material produced a wear track groove on B4C, suggesting significantly higher wear resistance for the oxide ceramic. The new material did not suffer from any microstructural degradation after the wear

  10. High Strength and Wear Resistance of Tantalum by Ultrasonic Nanocrystalline Surface Modification Technique at High Temperatures

    NASA Astrophysics Data System (ADS)

    Amanov, A.; Pyun, Y. S.; Vasudevan, V. K.

    2017-05-01

    Enhancing the strength of materials is of great concern in that the failures such as wear, corrosion and fatigue occur on the surface. A tantalum (Ta), which is a refractory metal, was subjected to severe plastic deformation induced by ultrasonic nanocrystalline surface modification (UNSM) technique at room- and high-temperatures of 200°C and 800°C. The mechanical properties and wear resistance of Ta before and after UNSM treatment were characterized by X-ray diffraction (XRD), hardness tester, and ball-on-disk tribometer, respectively. The UNSM treatment at 800°C led to the intensity reduction and broadening, and the diffraction peaks were shifted to lower angles, which means the presence of compressive residual stress and grain size refinement. The hardness of the UNSM-treated sample at room temperature was higher than that of the untreated one, and it was further increased with increasing the UNSM treatment temperature. In addition, the effect of UNSM treatment at high-temperature on wear resistance was significant than that of the UNSM treatment at room-temperature. We demonstrate the possibility of further increasing the mechanical properties and wear resistance of Ta by UNSM treatment at high-temperatures in comparison with the untreated and UNSM-treatment at room temperature, which would be beneficial for applications of Ta.

  11. Carbon-Based Wear Coatings: Properties and Applications

    NASA Technical Reports Server (NTRS)

    Miyoshi, Kazuhisa

    2003-01-01

    The technical function of numerous engineering systems - such as vehicles, machines, and instruments - depends on the processes of motion and on the surface systems. Many processes in nature and technology depend on the motion and dynamic behavior of solids, liquids, and gases. Smart surface systems are essential because of the recent technological push toward higher speeds, loads, and operating temperatures; longer life; lighter weight and smaller size (including nanotechnology); and harsh environments in mechanical, mechatronic, and biomechanical systems. If proper attention is not given to surface systems, then vehicles, machines, instruments, and other technical systems could have short lives, consume excessive energy, experience breakdowns, result in liabilities, and fail to accomplish their missions. Surface systems strongly affect our national economy and our lifestyles. At the NASA Glenn Research Center, we believe that proper attention to surface systems, especially in education, research, and application, could lead to economic savings of between 1.3 and 1.6 percent of the gross domestic product. Wear coatings and surface systems continue to experience rapid growth as new coating and surface engineering technologies are discovered, more cost-effective coating and surface engineering solutions are developed, and marketers aggressively pursue, uncover, and exploit new applications for engineered surface systems in cutting tools and wear components. Wear coatings and smart surface systems have been used widely in industrial, consumer, automotive, aerospace, and biomedical applications. This presentation expresses the author's views of and insights into smart surface systems in wear coatings. A revolution is taking place in carbon science and technology. Diamond, an allotrope of carbon, joins graphite, fullerenes, and nanotubes as its major pure carbon structures. It has a unique combination of extreme properties: hardness and abrasion resistance; adhesion

  12. Carbon-Based Wear Coatings: Properties and Applications

    NASA Technical Reports Server (NTRS)

    Miyoshi, Kazuhisa

    2003-01-01

    The technical function of numerous engineering systems - such as vehicles, machines, and instruments - depends on the processes of motion and on the surface systems. Many processes in nature and technology depend on the motion and dynamic behavior of solids, liquids, and gases. Smart surface systems are essential because of the recent technological push toward higher speeds, loads, and operating temperatures; longer life; lighter weight and smaller size (including nanotechnology); and harsh environments in mechanical, mechatronic, and biomechanical systems. If proper attention is not given to surface systems, then vehicles, machines, instruments, and other technical systems could have short lives, consume excessive energy, experience breakdowns, result in liabilities, and fail to accomplish their missions. Surface systems strongly affect our national economy and our lifestyles. At the NASA Glenn Research Center, we believe that proper attention to surface systems, especially in education, research, and application, could lead to economic savings of between 1.3 and 1.6 percent of the gross domestic product. Wear coatings and surface systems continue to experience rapid growth as new coating and surface engineering technologies are discovered, more cost-effective coating and surface engineering solutions are developed, and marketers aggressively pursue, uncover, and exploit new applications for engineered surface systems in cutting tools and wear components. Wear coatings and smart surface systems have been used widely in industrial, consumer, automotive, aerospace, and biomedical applications. This presentation expresses the author's views of and insights into smart surface systems in wear coatings. A revolution is taking place in carbon science and technology. Diamond, an allotrope of carbon, joins graphite, fullerenes, and nanotubes as its major pure carbon structures. It has a unique combination of extreme properties: hardness and abrasion resistance; adhesion

  13. Tribology: Wear test selection for design and application

    SciTech Connect

    Ruff, A.W.; Bayer, R.G.

    1993-01-01

    One important area of concern that has not been covered in previous symposia by the ASTM's Committee on Wear and Erosion is the connection between laboratory testing and actual operating performance of systems or components. This connection between laboratory testing, test results, and final design and performance is a crucial one in the practical application of tribology science and engineering. One of the aims of this symposium was to show by example how successful simulative testing has been accomplished. Specific examples are presented from a number of applications involving different forms of wear, including some from such specialized areas as computer peripherals, engines, and prosthetic devices. An important consideration in all the presentations was the identification of critical use conditions. Nine of the papers have been processed separately for inclusion on the data base.

  14. Wear Characteristics of Oleophobic Coatings in Aerospace Applications

    NASA Astrophysics Data System (ADS)

    Shams, Hamza; Basit, Kanza

    2016-05-01

    This paper investigates the wear characteristics of oleophobic coatings when applied over Inconel 718, which has widespread applications in the aerospace industry. Coatings once applied were selectively exposed to controlled uni-and then multi-directional stand storm conditions. Size and speed of sand particles colliding with the work surface were carefully moderated to simulate sand storm conditions. Study of friction was performed using Lateral Force Microscopy (LFM) coupled with standard optical microscopy. The analysis has been used to devise a coefficient of friction value and in turn suggest wear behavior of the coated surface including the time associated with exposure of the base substrate. The analysis after validation aims to suggest methods for safe usage of these coatings for aerospace applications.

  15. Wear Characteristics of Oleophobic Coatings in Aerospace Applications

    NASA Astrophysics Data System (ADS)

    Shams, Hamza; Siddiqui, Bilal A.; Saleem, Sajid

    This paper investigates the wear characteristics of oleophobic coatings when applied over Inconel 718, which has widespread applications in the aerospace industry. Coatings once applied were selectively exposed to controlled uni-and then multi-directional stand storm conditions. Size and speed of sand particles colliding with the work surface were carefully moderated to simulate sand storm conditions. Study of friction was performed using Lateral Force Microscopy (LFM) coupled with standard optical microscopy. The analysis has been used to devise a coefficient of friction value and in turn suggest wear behavior of the coated surface including the time associated with exposure of the base substrate. The analysis after validation aims to suggest methods for safe usage of these coatings for aerospace applications.

  16. Wear-resistant ball bearings for space applications

    NASA Technical Reports Server (NTRS)

    Boving, H.; Hintermann, H. E.; Hanni, W.; Bondivenne, E.; Boeto, M.; Conde, E.

    1977-01-01

    Ball bearings consisting of steel parts of which the rings are coated with hard, wear resistant, chemical vapor deposited TiC are described. Experiments conducted in ultrahigh vacuum, using cages of various materials with self-lubricating properties, show that such bearings are suitable for space applications. The results of laboratory tests on the ESA Meteosat Radiometer Focalizing mechanism, which contains six coated bearings, are summarized.

  17. Wear measurement of highly cross-linked UHMWPE using a 7Be tracer implantation technique.

    PubMed

    Wimmer, Markus A; Laurent, Michel P; Dwiwedi, Yasha; Gallardo, Luis A; Chipps, Kelly A; Blackmon, Jeffery C; Kozub, Raymond L; Bardayan, Daniel W; Gross, Carl J; Stracener, Daniel W; Smith, Michael S; Nesaraja, Caroline D; Erikson, Luke; Patel, Nidhi; Rehm, Karl E; Ahmad, Irshad; Greene, John P; Greife, Uwe

    2013-04-01

    The very low wear rates achieved with the current highly cross-linked ultrahigh molecular weight polyethylenes (UHMWPE) used in joint prostheses have proven to be difficult to measure accurately by gravimetry. Tracer methods are therefore being explored. The purpose of this study was to perform a proof-of-concept experiment on the use of the radioactive tracer beryllium-7 ((7)Be) for the determination of in vitro wear in a highly cross-linked orthopedic UHMWPE. Three cross-linked and four conventional UHMWPE pins made from compression-molded GUR 1050, were activated with 10(9) to 10(10) (7)Be nuclei using a new implantation setup that produced a homogenous distribution of implanted nuclei up to 8.5 μm below the surface. The pins were tested for wear in a six-station pin-on-flat apparatus for up to 7.1 million cycles (178 km). A Germanium gamma detector was employed to determine activity loss of the UHMWPE pins at preset intervals during the wear test. The wear of the cross-linked UHMWPE pins was readily detected and estimated to be 17 ± 3 μg per million cycles. The conventional-to-cross-linked ratio of the wear rates was 13.1 ± 0.8, in the expected range for these materials. Oxidative degradation damage from implantation was negligible; however, a weak dependence of wear on implantation dose was observed limiting the number of radioactive tracer atoms that can be introduced. Future applications of this tracer technology may include the analysis of location-specific wear, such as loss of material in the post or backside of a tibial insert.

  18. Friction and wear of hydroxyapatite reinforced high density polyethylene against the stainless steel counterface.

    PubMed

    Wang, M; Chandrasekaran, M; Bonfield, W

    2002-06-01

    Hydroxyapatite (HA) reinforced high density polyethylene (HDPE) was invented as a biomaterial for skeletal applications. In this investigation, tribological properties (e.g. wear rate and coefficient of friction) of unfilled HDPE and HA/HDPE composites were evaluated against the duplex stainless steel in dry and lubricated conditions, with distilled water or aqueous solutions of proteins (egg albumen or glucose) being lubricants. Wear tests were conducted in a custom-built test rig for HDPE and HA/HDPE containing up to 40 vol % of HA. It was found that HA/HDPE composites had lower coefficients of friction than unfilled HDPE under certain conditions. HA/HDPE also exhibited less severe fatigue failure marks than HDPE. The degradation and fatigue failure of HDPE due to the presence of proteins were severe for low speed wear testing (100 rpm) as compared to high speed wear testing (200 rpm). This was due possibly to the high shear rate at the contact which could remove any degraded film instantaneously at high sliding speed, while with a low sliding speed the build-up of a degraded layer of protein could occur. The degraded protein layer would stay at the contact for a longer time and mechanical activation would induce adverse reactions, weakening the surface layer of HDPE. Both egg albumen and glucose were found to be corrosive to steel and adversely reactive for HDPE and HA/HDPE composites. The wear modes observed were similar to that of ultra-high molecular weight polyethylene. Specimens tested with egg albumen also displayed higher wear rates, which was again attributed to corrosion accelerated wear.

  19. Erosive wear of selected materials for fossil energy applications

    SciTech Connect

    Adler, Thomas A.; Rawers, James C.; Tylczak, Joseph H.; Hawk, Jeffrey A.

    2001-01-01

    A number of materials have been evaluated to determine their erosion resistance for fossil energy applications. This is part of a larger program to study wear and corrosion at Albany Research Center. This paper will present the results for some of these materials, including FeAl, FeAl cermets, WC-Co cemented carbides, Si3N4-MoSi2, Si3N4, Stellite 6B, white cast irons and 440C steel. Trends in erosion rates due to material properties and erosive conditions will be presented. FeAl cermets performed well compared to the WC-Co cemented carbides. The interparticle spacing of the WC-Co cemented carbides correlated with the erosion rate. The erosion rate of the WC-Co cemented carbides decreased as the interparticle spacing decreased. It is important to realize that erosion resistance is not an intrinsic material property, but is a system response. A change in the wear environment can significantly alter the relative rankings of materials with respect to their wear rate. For example, at relatively low velocities, the carbides in the white cast irons are more erosion resistant than the matrix, while at higher velocities the matrix is more erosion resistant.

  20. Development of an extremely wear-resistant ultra high molecular weight polyethylene for total hip replacements.

    PubMed

    McKellop, H; Shen, F W; Lu, B; Campbell, P; Salovey, R

    1999-03-01

    Osteolysis induced by ultra high molecular weight polyethylene wear debris is one of the primary factors limiting the lifespan of total hip replacements. Crosslinking polyethylene is known to improve its wear resistance in certain industrial applications, and crosslinked polyethylene acetabular cups have shown improved wear resistance in two clinical studies. In the present study, crosslinked polyethylene cups were produced by two methods. Chemically crosslinked cups were produced by mixing a peroxide with ultra high molecular weight polyethylene powder and then molding the cups directly to shape. Radiation-crosslinked cups were produced by exposing conventional extruded ultra high molecular weight polyethylene bar stock to gamma radiation at various doses from 3.3 to 100 Mrad (1 Mrad = 10 kGy), remelting the bars to extinguish residual free radicals (i.e., to minimize long-term oxidation), and then machining the cups by conventional techniques. In hip-joint simulator tests lasting as long as 5 million cycles, both types of cross-linked cups exhibited dramatically improved resistance to wear. Artificial aging of the cups by heating for 30 days in air at 80 degrees C induced oxidation of the chemically crosslinked cups. However, a chemically crosslinked cup that was aged 2.7 years at room temperature had very little oxidation. Thus, whether substantial oxidation of chemically crosslinked polyethylene would occur at body temperature remains unclear. The radiation-crosslinked remelted cups exhibited excellent resistance to oxidation. Because crosslinking can reduce the ultimate tensile strength, fatigue strength, and elongation to failure of ultra high molecular weight polyethylene, the optimal crosslinking dose provides a balance between these physical properties and the wear resistance of the implant and might substantially reduce the incidence of wear-induced osteolysis with total hip replacements.

  1. The research on tool wear of high speed milling titanium alloy TC4

    NASA Astrophysics Data System (ADS)

    Shi, Hongliang; Wang, Zhichao; Ren, Huanhuan; Yuan, Haoteng

    2017-01-01

    In this paper, carbide cutting tools with physical vapor deposition (PVD) coating was used to high speed milling α+β phase TC4 titanium alloy. The PVD tool was used to study the process of milling TC4 titanium alloy tool wear patterns and wear mechanisms. The results showed that the PVD coating surface wear was small after cutter blade. The cutting life was long, it was suitable for processing of titanium alloy TC4, the wear of rake face was mainly adhesion wear and oxidation wear, the flank face was mainly boundary wear. That was because the adhesion wear of the rake face and the boundary wear of the flank face had a weakening effect on the cutting edge , which made the micro crack blade of the main cutting edge.

  2. Improvement in high stress abrasive wear property of steel by hardfacing

    SciTech Connect

    Kumar, S.; Mondal, D.P.; Khaira, H.K.; Jha, A.K.

    1999-12-01

    High stress abrasive wear behavior of mild steel, medium carbon steel, and hardfacing alloy has been studied to ascertain the extent of improvement in the wear properties after hardfacing of steel. High stress abrasive wear tests were carried out by sliding the specimen against the abrasive media consisting of silicon carbide particles, rigidly bonded on paper base and mounted on disk. Maximum wear was found in the case of mild steel followed by a medium carbon alloy steel and a hardfacing alloy. Different compositions of steels and constituent phases present led to different wear rates of the specimen. The extent of improvement in wear performance of steel due to hardfacing is quite appreciable (twice compared to mild steel). Microstructural examination of the wear surface has been carried out to understand the wear mechanism.

  3. Controlled tip wear on high roughness surfaces yields gradual broadening and rounding of cantilever tips

    PubMed Central

    Vorselen, Daan; Kooreman, Ernst S.; Wuite, Gijs J. L.; Roos, Wouter H.

    2016-01-01

    Tip size in atomic force microscopy (AFM) has a major impact on the resolution of images and on the results of nanoindentation experiments. Tip wear is therefore a key limitation in the application of AFM. Here we show, however, how wear can be turned into an advantage as it allows for directed tip shaping. We studied tip wear on high roughness polycrystalline titanium and diamond surfaces and show that tip wear on these surfaces leads to an increased tip size with a rounded shape of the apex. Next, we fitted single peaks from AFM images in order to track the changes in tip radius over time. This method is in excellent agreement with the conventional blind tip reconstruction method with the additional advantage that we could use it to demonstrate that the increase in tip size is gradual. Moreover, with our approach we can shape and control the tip size, while retaining identical chemical and cantilever properties. This significantly expands the reproducibility of AFM force spectroscopy data and is therefore expected to find a wide applicability. PMID:27833143

  4. Controlled tip wear on high roughness surfaces yields gradual broadening and rounding of cantilever tips

    NASA Astrophysics Data System (ADS)

    Vorselen, Daan; Kooreman, Ernst S.; Wuite, Gijs J. L.; Roos, Wouter H.

    2016-11-01

    Tip size in atomic force microscopy (AFM) has a major impact on the resolution of images and on the results of nanoindentation experiments. Tip wear is therefore a key limitation in the application of AFM. Here we show, however, how wear can be turned into an advantage as it allows for directed tip shaping. We studied tip wear on high roughness polycrystalline titanium and diamond surfaces and show that tip wear on these surfaces leads to an increased tip size with a rounded shape of the apex. Next, we fitted single peaks from AFM images in order to track the changes in tip radius over time. This method is in excellent agreement with the conventional blind tip reconstruction method with the additional advantage that we could use it to demonstrate that the increase in tip size is gradual. Moreover, with our approach we can shape and control the tip size, while retaining identical chemical and cantilever properties. This significantly expands the reproducibility of AFM force spectroscopy data and is therefore expected to find a wide applicability.

  5. Application of ion implantation to wear protection of materials

    NASA Astrophysics Data System (ADS)

    Hubler, O. K.; Smidt, F. A.

    1985-03-01

    Key results from the literature for the wear behavior of N- and Ti-implanted steels are reviewed. A qualitative model which rationalizes the mechanisms producing improvements in the sliding wear resistance of steels is presented. In the limited regime of low sliding velocities the model provides guidelines for choosing the experimental conditions of applied load, composition, hardness and heat treatment of the steel under which implantation will improve wear resistance.

  6. Unified wear model for highly crosslinked ultra-high molecular weight polyethylenes (UHMWPE).

    PubMed

    Muratoglu, O K; Bragdon, C R; O'Connor, D O; Jasty, M; Harris, W H; Gul, R; McGarry, F

    1999-08-01

    Crosslinking has been shown to improve the wear resistance of ultra-high molecular weight polyethylene in both in vitro and clinical in vivo studies. The molecular mechanisms and material properties that are responsible for this marked improvement in wear resistance are still not well understood. In fact, following crosslinking a number of mechanical properties of UHMWPE are decreased including toughness, modulus, ultimate tensile strength, yield strength, and hardness. In general, these changes would be expected to constitute a precursor for lower wear resistance, presenting a paradox in that wear resistance increases with crosslinking. In order to understand better and to analyze this paradoxical behaviour of crosslinked UHMWPE, we investigated the wear behavior of (i) radiation-crosslinked GUR 1050 resin, (ii) peroxide-crosslinked GUR 1050 resin and (iii) peroxide-crosslinked Himont 1900 resin using a bi-directional pin-on-disk (POD) machine. Wear behavior was analyzed as a function of crystallinity, ultimate tensile strength (UTS), yield strength (YS), and molecular weight between crosslinks (Mc). The crosslink density increased with increasing radiation dose level and initial peroxide content. The UTS, YS, and crystallinity decreased with increasing crosslink density. While these variations followed the same trend, the absolute changes as a function of crosslink density were different for the three types of crosslinked UHMWPE studied. There was no unified correlation for the wear behavior of the three types of crosslinked UHMWPE with the crystallinity, UTS and YS. However, the POD wear rate showed the identical linear dependence on Mc with all three types of crosslinked UHMWPEs studied. Therefore, we have strong evidence to propose that Mc or crosslink density is a fundamental material property that governs the lubricated adhesive and abrasive wear mechanisms of crosslinked UHMWPEs, overriding the possible effects of other material properties such as UTS, YS

  7. A new application of dental wear analyses: estimation of duration of hominid occupations in archaeological localities.

    PubMed

    Rivals, Florent; Schulz, Ellen; Kaiser, Thomas M

    2009-04-01

    Characterization of settlement patterns is one of the core concepts in archeological research. The duration of an occupation is usually estimated through zooarchaeology (e.g., density of remains, cementochronology) and is limited by taphonomic processes and sample size. We propose a new application of dental wear methods for estimating the relative duration of hominid settlements in Paleolithic sites. Dental microwear is known to be sensitive to seasonal changes in diet. In this new application we use microwear scratch counts to estimate the variation in the dietary signal of various ungulate species. We propose that this variation is correlated to the duration of site occupation. Each season presents a limited and different set of food resources available in the environment. If animals are sampled only during a specific season (i.e., during a short term occupation) then they would be expected to have a dental wear signal with little variation. On the other hand, a greater diversity of food is available across different seasons. Therefore, if game animals are hunted through various seasons during long occupation periods, then they would be expected to have more variable dental wear. The application of this technique to the Middle Paleolithic site of Arago Cave (France), where various types of occupations occurred, supports this hypothesis. When combined with multidisciplinary studies of archaeological localities (seasonality in particular), this new application of dental wear analysis presents valuable information about hominid settlements and behavior. We contextualize our data with results from lithic and zooarchaeological analyses from Arago. These results reveal the presence of both high and low mobility groups of Homo heidelbergensis throughout the sequence of the Arago Cave.

  8. Application of an X-ray Fluorescence Instrument to Helicopter Wear Debris Analysis

    DTIC Science & Technology

    2008-04-01

    Application of an X-ray Fluorescence Instrument to Helicopter Wear Debris Analysis Andrew Becker Air Vehicles Division...instrument to determine the composition of wear debris collected from helicopter magnetic chip detectors and oil filters. The Twin-X XRF (assessed in this...report) is a commercially produced bench-top XRF and has not previously been applied to wear debris analysis of Australian Defence Force aircraft

  9. Development of wear resistant nanostructured duplex coatings by high velocity oxy-fuel process for use in oil sands industry.

    PubMed

    Saha, Gobinda C; Khan, Tahir I; Glenesk, Larry B

    2009-07-01

    Oil sands deposits in Northern Alberta, Canada represent a wealth of resources attracting huge capital investment and significant research focus in recent years. As of 2005, crude oil production from the current oil sands operators accounted for 50% of Canada's domestic production. Alberta's oil sands deposits contain approximately 1.7 trillion barrels of bitumen, of which over 175 billion are recoverable with current technology, and 315 billion barrels are ultimately recoverable with technological advances. A major problem of operating machinery and equipment in the oil sands is the unpredictable failure from operating in this highly aggressive environment. One of the significant causes of that problem is premature material wear. An approach to minimize this wear is the use of protective coatings and, in particular, a cermet thin coating. A high level of coating homogeneity is critical for components such as bucketwheels, draglines, conveyors, shovels, heavyhauler trucks etc. that are subjected to severe degradation through abrasive wear. The identification, development and application of optimum wear solutions for these components pose an ongoing challenge. Nanostructured cermet coatings have shown the best results of achieving the degree of homogeneity required for these applications. In this study, WC-17Co cermet powder with nanocrystalline WC core encapsulated with 'duplex' Co layer was used to obtain a nanostructured coating. To apply this coating, high velocity oxy-fuel (HVOF) thermal spraying technique was used, as it is known for producing wear-resistant coatings superior to those obtained from plasma-based techniques. Mechanical, sliding wear and microstructural behavior of the coating was compared with those of the microstructured coating obtained from spraying WC-10Co-4Cr cermet powder by HVOF technique. Results from the nanostructured coating, among others, showed an average of 25% increase in microhardness, 30% increase in sliding wear resistance and

  10. Laboratory evaluation of low cobalt wear materials for nuclear applications

    SciTech Connect

    Shiels, S.A.; Wilson, W.L.; Rosengarth, K.W.; Wire, G.L.

    1994-09-01

    Laboratory wear and corrosion screening tests were conducted on several commercially available, low-cobalt and cobalt-free hardsurfacing alloys to evaluate their relative wear and corrosion performance under simulated Pressurized Water Reactor (PWR) primary heat transport circuit conditions. Wear tests were performed under reciprocating, sliding contact. Corrosion performance was evaluated in both steady state and off-normal chemistry conditions. The wear behavior of the candidate hardsurfacing alloys was generally comparable to or better than that of Stellite 6, a material of proven wear performance under PWR operating conditions. With the exception of Tristelle 5183, the iron base alloys exhibited unacceptable corrosion behavior under wet layup conditions. The Tristelle 5183 experienced minor corrosion attack in primary coolant having elevated oxygen levels. The twelve percent cobalt alloy, Tristelle TS-2, performed well but exhibited some attack after a simulated decontamination treatment.

  11. Online Wear Detection Using High-Speed Imaging.

    PubMed

    Soleimani, Seyfollah; Sukumaran, Jacob; Douterloigne, Koen; De Baets, Patrick; Philips, Wilfried

    2016-08-01

    In this paper, the change detection of a fast turning specimen is studied at micro-level, whereas the images are acquired without stopping the rotation. In the beginning of the experiment, the imaging system is focused on the surface of the specimen. By starting the rotation of the specimen, the diameter of the specimen changes due to wear, which results in de-focusing of the imaging system. So the amount of blur in the images can be used as evidence of the wear phenomenon. Due to the properties of the microscope, the corners of the frames were dark and had to be cropped. So, each micrograph reflects only a small area of the surface. Nevertheless, techniques like stitching of multiple images can provide a significant surface area for micro-level investigation which increases the effectiveness of analyzing the material modification. Based on the results computer vision could detect a change of about 1.2 µm in the diameter of the specimen. More important is that we could follow the same locations of the surface in the microscopic images despite blurring, uneven illumination, change on the surface, and relatively a high-speed rotation.

  12. Wear of PEEK-OPTIMA® and PEEK-OPTIMA®-Wear Performance articulating against highly cross-linked polyethylene.

    PubMed

    East, Rebecca H; Briscoe, Adam; Unsworth, Anthony

    2015-03-01

    The idea of all polymer artificial joints, particularly for the knee and finger, has been raised several times in the past 20 years. This is partly because of weight but also to reduce stress shielding in the bone when stiffer materials such as metals or ceramics are used. With this in mind, pin-on-plate studies of various polyetheretherketone preparations against highly cross-linked polyethylene were conducted to investigate the possibility of using such a combination in the design of a new generation of artificial joints. PEEK-OPTIMA(®) (no fibre) against highly cross-linked polyethylene gave very low wear factors of 0.0384 × 10(-6) mm(3)/N m for the polyetheretherketone pins and -0.025 × 10(-6) mm(3)/N m for the highly cross-linked polyethylene plates. The carbon-fibre-reinforced polyetheretherketone (PEEK-OPTIMA(®)-Wear Performance) also produced very low wear rates in the polyetheretherketone pins but produced very high wear in the highly cross-linked polyethylene, as might have been predicted since the carbon fibres are quite abrasive. When the fibres were predominantly tangential to the sliding plane, the mean wear factor was 0.052 × 10(-6) mm(3)/N m for the pins and 49.3 × 10(-6) mm(3)/N m for the highly cross-linked polyethylene plates; a half of that when the fibres ran axially in the pins (0.138 × 10(-6) mm(3)/N m for the pins and 97.5 × 10(-6) mm/ N m for the cross-linked polyethylene plates). PEEK-OPTIMA(®) against highly cross-linked polyethylene merits further investigation.

  13. Assessment of thermal spray coatings for wear and abrasion resistance applications

    NASA Astrophysics Data System (ADS)

    Karode, Ishaan Nitin

    Thermal spray cermet and metallic coatings are extensively used for wear, abrasion and corrosion control in a variety of industries. The first part of the thesis focuses mainly on testing of sand erosion resistance of thermal spray coatings on carbon composites used in the manufacture of helicopter rotor blades. The test set-up employed is a sand blasting machine and is an effort to duplicate the in-flight conditions especially those encountered in hot arid conditions. The technique adopted follows the Department of Defence test method standard. Carbon Composites have excellent stiffness, strength and low weight/density. The strength to weight ratio is high. Hence, these are used in aerospace applications to a large extent. However, the biggest problem encountered with carbon composites is its low abrasion resistance as its surface is very weak. Hence, thermal spray coatings are used to improve the surface properties of CFRP. Zinc bond coats and WC-Co coatings were tested. However, high amount of thermal stresses were developed between the substrate and the coating due to large differences in the CTE's of the both, leading to high mass losses within two minutes and just 130 grams of sand sprayed on to the coatings with the sand blasting machine built; and hence the coatings with CC as a substrate could not qualify for the application. The second part of the thesis focuses on the assessment of different thermal spray coatings used for manufacture of mechanical seals in pumps and analyze the best coating material for the wear resistance application through detail quantification of material loss by block-on-ring test set-up. A machine based on Block-on-ring test set-up following ASTM G77 (Measurement of Adhesive wear resistance of thermal spray coatings) standards was built to duplicate the pump conditions. Thermally sprayed coated materials were tested in different conditions (Load, time, abrasive). WC-Co had the highest wear resistance (lower volume losses) and

  14. Wear resistance properties of austempered ductile iron

    NASA Astrophysics Data System (ADS)

    Lerner, Y. S.; Kingsbury, G. R.

    1998-02-01

    A detailed review of wear resistance properties of austempered ductile iron (ADI) was undertaken to examine the potential applications of this material for wear parts, as an alternative to steels, alloyed and white irons, bronzes, and other competitive materials. Two modes of wear were studied: adhesive (frictional) dry sliding and abrasive wear. In the rotating dry sliding tests, wear behavior of the base material (a stationary block) was considered in relationship to countersurface (steel shaft) wear. In this wear mode, the wear rate of ADI was only one-fourth that of pearlitic ductile iron (DI) grade 100-70-03; the wear rates of aluminum bronze and leaded-tin bronze, respectively, were 3.7 and 3.3 times greater than that of ADI. Only quenched DI with a fully martensitic matrix slightly outperformed ADI. No significant difference was observed in the wear of steel shafts running against ADI and quenched DI. The excellent wear performance of ADI and its countersurface, combined with their relatively low friction coefficient, indicate potential for dry sliding wear applications. In the abrasive wear mode, the wear rate of ADI was comparable to that of alloyed hardened AISI 4340 steel, and approximately one-half that of hardened medium-carbon AISI 1050 steel and of white and alloyed cast irons. The excellent wear resistance of ADI may be attributed to the strain-affected transformation of high-carbon austenite to martensite that takes place in the surface layer during the wear tests.

  15. High stress abrasive wear behavior of some hardfaced surfaces produced by thermal spraying

    NASA Astrophysics Data System (ADS)

    Jha, A. K.; Gachake, Arati; Prasad, B. K.; Dasgupta, Rupa; Singh, M.; Yegneswaran, A. H.

    2002-02-01

    Steel surfaces were thermally sprayed with nickel chromium boron (NCB) powder (with and without tungsten carbide) using an oxy-acetylene torch. The sprayed (hard) surfaces and substrate were characterized for abrasive wear properties. Test parameters such as load and sliding distance were varied. A significant improvement in the abrasive wear resistance (inverse of wear rate) was noted for the thermally sprayed surfaces as compared to that of the substrate. Wear surfaces, subsurface regions, and debris were examined in order to ascertain the operating wear mechanisms. Substrate (mild steel), because of its low hardness, suffered severe wear through the cutting, ploughing, and wedging action of the hard abrasive (silicon carbide). Deep cuts on the worn surface, a bulky transfer layer, subsurface cracks, and large-size debris were observed. However, wear was reduced due to high hardness of the layer of NCB powder on the substrate, which resisted the penetration of abrasive into the surface. Presence of tungsten carbide in the layer of NCB powder further reduced the wear of the corresponding specimen because of very high hardness of the tungsten carbide. Shallow wear grooves and finer debris were observed for the NCB coating with and without tungsten carbide. Cutting was the predominating wear mechanism in the case of coatings.

  16. Wear Measurement of Highly Cross-linked UHMWPE using a 7Be Tracer Implantation Technique

    SciTech Connect

    Wimmer, Markus A.; Laurent, Michael P.; Dwivedi, Yasha; Gallardo, Luis A.; Chipps, K.; Blackmon, Jeffery C; Kozub, R. L.; Bardayan, Daniel W; Gross, Carl J; Stracener, Daniel W; Smith, Michael Scott; Nesaraja, Caroline D; Erikson, Luke; Patel, Nidhi; Rehm, Karl E.; Ahmad, Irshad; Greene, John P.; Greife, Uwe

    2013-01-01

    The very low wear rates achieved with the current highly cross-linked ultrahigh molecular weight polyethylenes (UHMWPE) used in joint prostheses have proven to be difficult to measure accurately by gravimetry. Tracer methods are there- fore being explored. The purpose of this study was to perform a proof-of-concept experiment on the use of the radioactive tracer beryllium-7 (7Be) for the determination of in vitro wear in a highly cross-linked orthopedic UHMWPE. Three cross-linked and four conventional UHMWPE pins made from compression- molded GUR 1050, were activated with 109 to 1010 7Be nuclei using a new implantation setup that produced a homogenous distribution of implanted nuclei up to 8.5 lm below the surface. The pins were tested for wear in a six-station pin-on-flat appara- tus for up to 7.1 million cycles (178 km). A Germanium gamma detector was employed to determine activity loss of the UHMWPE pins at preset intervals during the wear test. The wear of the cross-linked UHMWPE pins was readily detected and esti- mated to be 17 6 3 lg per million cycles. The conventional-to- cross-linked ratio of the wear rates was 13.1 6 0.8, in the expected range for these materials. Oxidative degradation dam- age from implantation was negligible; however, a weak depend- ence of wear on implantation dose was observed limiting the number of radioactive tracer atoms that can be introduced. Future applications of this tracer technology may include the analysis of location-specific wear, such as loss of material in the post or backside of a tibial insert.

  17. High-Power Diode Laser Surface Treated HVOF Coating to Combat High Energy Particle Impact Wear

    NASA Astrophysics Data System (ADS)

    Mann, B. S.; Arya, Vivek; Pant, B. K.

    2013-07-01

    High-velocity oxy-fuel (HVOF)-sprayed coatings have performed exceptionally well in low-energy particle impact wear and are accepted worldwide. However, their application for high-energy particle impact wear (HEPIW) requires a different approach and more efforts. HVOF-coating systems typically use WC-Co, WC-Co-Cr, WC-Ni-Cr, and FeCrAlY-Cr3C2 powders. WC-Co-Cr powders are preferred when there is a high demand for corrosion resistance. WC-10Co-4Cr coating powder has been selected in the current study. To improve coating properties such as microhardness, fracture toughness, and HEPIW resistance, a new approach of surface treatment with robotically controlled high-power diode laser (HPDL) is attempted. The robotically controlled HVOF-coating deposition and laser surface treatment were monitored using real-time diagnostic control. The HPDL-treated coating has been compared with "as-sprayed" HVOF coating for HEPIW resistance, fracture toughness, microhardness and microstructure. The coating characteristics and properties after laser surface treatment have improved many times compared with "as-sprayed" HVOF coating. This is due to the elimination of pores in the coating and formation of a metallurgical bond between coating and substrate. This new development opens up a possibility of using such laser treatments in specialized areas where HEPIW damages are acute. The fracture toughness and HEPIW resistance along with optical micrographs of HPDL-treated and untreated HVOF coatings are discussed and reported in this article. HEPIW resistance is observed to be proportional to the product of fracture toughness and microhardness of the HVOF coating.

  18. High Density Infrared (HDI) Transient Liquid Coatings for Improved Wear and Corrosion Resistance

    SciTech Connect

    Ronald W. Smith

    2007-07-05

    This report documents a collaborative effort between Oak Ridge National Laboratory (ORNL), Materials Resources International and an industry team of participants to develop, evaluate and understand how high density infrared heating technology could be used to improve infiltrated carbide wear coatings and/or to densify sprayed coatings. The research included HDI fusion evaluations of infiltrated carbide suspensions such (BrazeCoat® S), composite suspensions with tool steel powders, thermally sprayed Ni-Cr- B-Si (self fluxing alloy) and nickel powder layers. The applied work developed practical HDI / transient liquid coating (TLC) procedures on test plates that demonstrated the ability to fuse carbide coatings for industrial applications such as agricultural blades, construction and mining vehicles. Fundamental studies helped create process models that led to improved process understanding and control. The coating of agricultural blades was demonstrated and showed the HDI process to have the ability to fuse industrial scale components. Sliding and brasive wear tests showed that high degree of wear resistance could be achieved with the addition of tool steel powders to carbide particulate composites.

  19. Increasing the wear resistance of ultra-high molecular weight polyethylene by adding solid lubricating fillers

    SciTech Connect

    Panin, S. V.; Kornienko, L. A.; Poltaranin, M. A.; Ivanova, L. R.; Suan, T. Nguen

    2014-11-14

    In order to compare effectiveness of adding solid lubricating fillers for polymeric composites based on ultra-high molecular weight polyethylene (UHMWPE) with graphite, molybdenum disulfide and polytetrafluoroethylene, their tribotechnical characteristics under dry friction, boundary lubrication and abrasive wearing were investigated. The optimal weight fractions of fillers in terms of improving wear resistance have been determined. The supramolecular structure and topography of wear track surfaces of UHMWPE-based composites with different content of fillers have been studied.

  20. Wear resistance of experimental titanium alloys for dental applications.

    PubMed

    Faria, Adriana Cláudia Lapria; Rodrigues, Renata Cristina Silveira; Claro, Ana Paula Rosifini Alves; da Gloria Chiarello de Mattos, Maria; Ribeiro, Ricardo Faria

    2011-11-01

    The present study evaluated microstructure, microhardness and wear resistance of experimental titanium alloys containing zirconium and tantalum. Alloys were melted in arc melting furnace according to the following compositions: Ti-5Zr, Ti-5Ta and Ti-5Ta-5Zr (%wt). Hemispheres and disks were obtained from wax patterns that were invested and cast by plasma. Microstructures were evaluated using optical microscopy and X-ray diffraction (XRD) analysis and also Vickers microhardness was measured. Hemispherical samples and disks were used for 2-body wear tests, performed by repeated grinding of the samples. Wear resistance was assessed as height loss after 40,000 cycles. The data were compared using ANOVA and post-hoc Tukey test. Ti-5Zr presented a Widmanstätten structure and the identified phases were α and α' while Ti-5Ta and Ti-5Ta-5Zr presented α, β, α' and α" phases, but the former presented a lamellar structure, and the other, acicular. The microhardness of Ti-5Zr was significantly greater than other materials and cp Ti presented wear resistance significantly lower than experimental alloys. It was concluded that wear resistance was improved when adding Ta and Zr to titanium and Zr increased microhardness of Ti-5Zr alloy. Copyright © 2011 Elsevier Ltd. All rights reserved.

  1. Application of surface analysis to solve problems of wear

    NASA Technical Reports Server (NTRS)

    Buckley, D. H.

    1981-01-01

    Results are presented for the use of surface analytical tools including field ion microscopy, Auger emission spectroscopy analysis (AES), cylindrical mirror Auger analysis and X-ray photoelectron spectroscopy (XPS). Data from the field ion microscope reveal adhesive transfer (wear) at the atomic level with the formation of surface compounds not found in the bulk, and AES reveals that this transfer will occur even in the presence of surface oxides. Both AES and XPS reveal that in abrasive wear with silicon carbide and diamond contacting the transition metals, the surface and the abrasive undergo a chemical or structural change which effects wear. With silicon carbide, silicon volatilizes leaving behind a pseudo-graphitic surface and the surface of diamond is observed to graphitize.

  2. Wear Consideration in Gear Design for Space Applications

    DTIC Science & Technology

    1989-01-01

    profile. The Archard 1/2 wear equation ( Rabinowicz , 1965) will be used to calcu- late depth wear (h) as follows b " ’ (5) h= (2) 3pAa where where =rltv aiso...This can be calculated from: e5 =h5/Rb where h5 KWNPy EV . 0.005671 e h I ( 3PF I rad e5 . 0.005671/1.1746 - 0.0048 rad, or 0.280 3 also the top...Subtract 0.0018 in. for initial backlash plus Handbook, ASME, New York. tooth-to-tooth composite error (when new) to get Rabinowicz , E., 1965, Friction and

  3. Ultrananocrystalline diamond film as a wear resistant and protective coating for mechanical seal applications.

    SciTech Connect

    Sumant, A. V.; Krauss, A. R.; Gruen, D. M.; Auciello, O.; Erdemir, A.; Williams, M.; Artiles, A. F.; Adams, W.; Western Michigan Univ.; Flowserve Corp.

    2005-01-01

    Mechanical shaft seals used in pumps are critically important to the safe operation of the paper, pulp, and chemical process industry, as well as petroleum and nuclear power plants. Specifically, these seals prevent the leakage of toxic gases and hazardous chemicals to the environment and final products from the rotating equipment used in manufacturing processes. Diamond coatings have the potential to provide negligible wear, ultralow friction, and high corrosion resistance for the sliding surfaces of mechanical seals, because diamond exhibits outstanding tribological, physical, and chemical properties. However, diamond coatings produced by conventional chemical vapor deposition (CVD) exhibit high surface roughness (R{sub a} {>=} 1 {mu}m), which results in high wear of the seal counterface, leading to premature seal failure. To avoid this problem, we have developed an ultrananocrystalline diamond (UNCD) film formed by a unique CH{sub 4}/Ar microwave plasma CVD method. This method yields extremely smooth diamond coatings with surface roughness R{sub a} = 20-30 nm and an average grain size of 2-5 nm. We report the results of a systematic test program involving uncoated and UNCD-coated SiC shaft seals. Results confirmed that the UNCD-coated seals exhibited neither measurable wear nor any leakage during long-duration tests that took 21 days to complete. In addition, the UNCD coatings reduced the frictional torque for seal rotation by five to six times compared with the uncoated seals. This work promises to lead to rotating shaft seals with much improved service life, reduced maintenance cost, reduced leakage of environmentally hazardous materials, and increased energy savings. This technology may also have many other tribological applications involving rolling or sliding contacts.

  4. Short-term wear of Japanese highly cross-linked polyethylene in cementless THA.

    PubMed

    Miyanishi, Keita; Hara, Toshihiko; Kaminomachi, Shigekazu; Maekawa, Masayuki; Iwamoto, Mikio; Torisu, Takehiko

    2008-09-01

    Production of polyethylene wear from acetabular liners is thought, in part, to mediate the periprosthetic osteolysis. This study examined the in vivo wear performance of Japanese highly cross-linked polyethylene (Aeonian) in cementless total hip arthroplasty. Ninety-five hips received a highly cross-linked polyethylene liner, while 20 hips were implanted with conventional polyethylene. Two-dimensional linear wear was measured on radiographs and volumetric wear was then calculated. Both linear and volumetric wear rates were examined for the 1-year postoperative period as well as for the time frame beginning after 1 year ending with the final follow-up. The amount of linear wear was significantly lower in the cross-linked group at 3 and 5 years postoperatively (P < 0.01 and < 0.001, respectively). Linear and volumetric wear rates after 1 year postoperatively for hips with the cross-linked polyethylene were significantly reduced by 57 and 59%, respectively, when compared to rates for those who received conventional polyethylene (P < 0.01). A multiple logistic regression analysis revealed that cross-linking was a significant factor influencing linear wear rate after 1 year postoperatively with an odds ratio, exp(ss) = 10.033 (P < 0.001). These results suggest that the highly cross-linked polyethylene reduces penetration of the femoral head and may be an optimal bearing surface for patients receiving total hip arthroplasty.

  5. Wear Resistance of H13 and a New Hot-Work Die Steel at High temperature

    NASA Astrophysics Data System (ADS)

    Li, Shuang; Wu, Xiaochun; Chen, Shihao; Li, Junwan

    2016-07-01

    The friction and wear behaviors of a new hot-work die steel, SDCM-SS, were studied at high temperature under dry air conditions. The wear mechanism and microstructural characteristics of the SDCM-SS steel were also investigated. The results showed that the SDCM-SS steel had greater wear resistance compared with H13 steel; this was owed to its high oxidizability and temper stability. These features facilitate the generation, growth, and maintenance of a tribo-oxide layer at high temperature under relatively stable conditions. The high oxidizability and thermal stability of the SDCM-SS steel originate from its particular alloy design. No chromium is added to the steel; this ensures that the material has high oxidizability, and facilitates the generation of tribo-oxides during the sliding process. Molybdenum, tungsten, and vanadium additions promote the high temper resistance and stability of the steel. Many fine Mo2C and VC carbides precipitate during the tempering of SDCM-SS steel. During sliding, these carbides can delay the recovery process and postpone martensitic softening. The high temper stability postpones the transition from mild to severe wear and ensures that conditions of mild oxidative wear are maintained. Mild oxidative wear is the dominant wear mechanism for SDCM-SS steel between 400 and 700 °C.

  6. Wear Analysis of Second-generation Highly Cross-Linked Polyethylene in Primary Total Hip Arthroplasty.

    PubMed

    Samujh, Christopher; Bhimani, Samrath; Smith, Langan; Malkani, Arthur L

    2016-11-01

    A major limiting factor in the longevity of total hip replacement is the wear rate of the hip bearing. As manufacturing technology has improved during the past several decades, much attention has been focused on developing newer generations of polyethylene that have lower rates of wear while minimizing free radical formation and subsequent osteolysis. The turning point for the manufacture of polyethylene was moving from gamma irradiation in air to irradiation in a low oxygen environment, which reduced free radical formation while increasing the wear resistance. New polyethylene manufacturing methods, including multiple cycles of irradiation and annealing, have resulted in greater wear resistance. Wear analysis studies are essential to determine if these new liners actually show a benefit from prior generations of polyethylene and, more importantly, if they are safe to use. This study involved a single center retrospective review of 60 patients with a mean follow-up of 5.5 years who underwent primary total hip arthroplasty with a second-generation highly cross-linked polyethylene manufactured by 3 cycles of sequential irradiation and annealing. Linear and volumetric wear rates were determined from digitized radiographs using contemporary wear analysis software. The mean linear wear rate for the entire group was 0.025 millimeters per year (mm/y). This value represents a linear wear rate 2.7 times less than that of a first-generation highly cross-linked polyethylene and 4.2 times less than that of a conventional polyethylene. At an average of 5 years, compared with a first-generation highly cross-linked polyethylene, a second-generation highly cross-linked polyethylene appears to show significant improvement regarding wear. [Orthopedics. 2016; 39(6):e1178-e1182.].

  7. Load application for the contact mechanics analysis and wear prediction of total knee replacement.

    PubMed

    Zhang, Jing; Chen, Zhenxian; Wang, Ling; Li, Dichen; Jin, Zhongmin

    2017-05-01

    Tibiofemoral contact forces in total knee replacement have been measured at the medial and lateral sites respectively using an instrumented prosthesis, and predicted from musculoskeletal multibody dynamics models with a reasonable accuracy. However, it is uncommon that the medial and lateral forces are applied separately to replace a total axial load according to the ISO standard in the majority of current finite element analyses. In this study, we quantified the different effects of applying the medial and lateral loads separately versus the traditional total axial load application on contact mechanics and wear prediction of a patient-specific knee prosthesis. The load application position played an important role under the medial-lateral load application. The loading set which produced the closest load distribution to the multibody dynamics model was used to predict the contact mechanics and wear for the prosthesis and compared with the total axial load application. The medial-lateral load distribution using the present method was found to be closer to the multibody dynamics prediction than the traditional total axial load application, and the maximum contact pressure and contact area were consistent with the corresponding load variation. The predicted total volumetric wear rate and area were similar between the two load applications. However, the split of the predicted wear volumes on the medial and the lateral sides was different. The lateral volumetric wear rate was 31.46% smaller than the medial from the traditional load application prediction, while from the medial-lateral load application, the lateral side was only 11.8% smaller than the medial. The medial-lateral load application could provide a new and more accurate method of load application for patient-specific preclinical contact mechanics and wear prediction of knee implants.

  8. Wear and creep of highly crosslinked polyethylene against cobalt chrome and ceramic femoral heads.

    PubMed

    Galvin, A L; Jennings, L M; Tipper, J L; Ingham, E; Fisher, J

    2010-10-01

    The wear and creep characteristics of highly crosslinked ultrahigh-molecular-weight polyethylene (UHMWPE) articulating against large-diameter (36mm) ceramic and cobalt chrome femoral heads have been investigated in a physiological anatomical hip joint simulator for 10 million cycles. The crosslinked UHMWPE/ceramic combination showed higher volume deformation due to creep plus wear during the first 2 million cycles, and a steady-state wear rate 40 per cent lower than that of the crosslinked UHMWPE/cobalt chrome combination. Wear particles were isolated and characterized from the hip simulator lubricants. The wear particles were similar in size and morphology for both head materials. The particle isolation methodology used could not detect a statistically significant difference between the particles produced by the cobalt chrome and alumina ceramic femoral heads.

  9. Friction and wear of carbon-graphite materials for high energy brakes

    NASA Technical Reports Server (NTRS)

    Bill, R. C.

    1975-01-01

    Caliper-type brakes simulation experiments were conducted on seven different carbon-graphite material formulations against a steel disk material and against a carbon-graphite disk material. The effects of binder level, boron carbide (B4C) additions, graphite fiber additions, and graphite cloth reinforcement on friction and wear behavior were investigated. Reductions in binder level and additions of B4C each resulted in increased wear. The wear rate was not affected by the addition of graphite fibers. Transition to severe wear and high friction was observed in the case of graphite-cloth-reinforced carbon sliding against a disk of similar composition. This transition was related to the disruption of a continuous graphite shear film that must form on the sliding surfaces if low wear is to occur. The exposure of the fiber structure of the cloth constituent is believed to play a role in the shear film disruption.

  10. Friction and wear of carbon-graphite materials for high-energy brakes

    NASA Technical Reports Server (NTRS)

    Bill, R. C.

    1978-01-01

    Caliper type brake simulation experiments were conducted on seven different carbon graphite materials formulations against a steel disk material and against a carbon graphite disk material. The effects of binder level, boron carbide (B4C) additions, SiC additions, graphite fiber additions, and graphite cloth reinforcement on friction and wear behavior were investigated. Reductions in binder level, additions of B4C, and additions of SiC each resulted in increased wear. The wear rate was not affected by the addition of graphite fibers. Transition to severe wear and high friction was observed in the case of graphite-cloth-reinforced carbon sliding against a disk of similar composition. The transition was related to the disruption of a continuous graphite shear film that must form on the sliding surfaces if low wear is to occur.

  11. High vitamin E content, impact resistant UHMWPE blend without loss of wear resistance.

    PubMed

    Oral, Ebru; Neils, Andrew; Muratoglu, Orhun K

    2015-05-01

    Antioxidant stabilization of radiation cross-linked ultrahigh molecular weight polyethylene (UHMWPE) has been introduced to improve the oxidative stability of total joint implant bearing surfaces. Blending of antioxidants (most commonly vitamin E) with UHMWPE resin powder followed by consolidation and uniform radiation cross-linking is currently available for use in both total hips and total knees. It was previously shown that the fatigue resistance of vitamin E-blended and irradiated UHMWPEs could be further improved by spatially manipulating the vitamin E concentration throughout the implant and limiting cross-linking to the surface of the implant where it is necessary for wear resistance. This was possible by designing a low concentration of vitamin E on the surface and higher concentration in the bulk of the implant because cross-linking is hindered in UHMWPE as a function of increasing vitamin E concentration. In this study, we hypothesized that such a surface cross-linked UHMWPE with low wear rate and high fatigue strength could be obtained by limiting the penetration of radiation into UHMWPE with uniform vitamin E concentration. Our hypothesis tested positive; we were able to obtain control of the surface cross-linked region by manipulating the energy of the irradiation, resulting in extremely low wear, and high impact strength. In addition, we discussed alternatives of improving the oxidation resistance of such a material by using additional vitamin E reservoirs. These results are significant because this material may allow increased use of antioxidant-stabilized, cross-linked UHMWPEs in high stress applications and in more active patients.

  12. Volatility and Wear Characteristics of a Variety of Liquid Lubricants for Space Applications

    NASA Technical Reports Server (NTRS)

    Nguyen, QuynhGiao N.; Jones, William R., Jr.

    2001-01-01

    The vapor pressures and wear characteristics are critical properties for liquid lubricants to assure long-term reliability and performance in space applications. Vapor pressures, obtained using a Knudsen cell technique, and wear properties, obtained using a vacuum four-ball apparatus, were measured for a series of unformulated liquid lubricants. These included two multiply alkylated cyclopentanes (MACs) (X-1000 and X2000), two linear perfluoropolyalkylethers (PFPAEs) (Z-25 and 815Z), and four silahydrocarbons (a tri, a tetra, and two pentas). Vapor pressures were measured at three elevated temperatures (423, 448, and 498 K) and extrapolated to room temperature 298 K. The lowest 298 K vapor pressure of 5.7 x 10(exp -14) Pa was obtained with the PFPAE fluid (815Z) and the highest value with the low molecular weight MAC (X-1000) at 3.6 x 10(exp -7) Pa. In addition, vacuum wear rates were determined for some of the lubricants. The lowest wear rates (approximately 3 x 10(exp -11) cubic mm/mm) were observed for three of the silahydrocarbons while the highest wear rates (approximately 2 x 10(exp -9) cubic mm/mm) were observed with the two PFPAE fluids (Z-25 and 815Z). The MAC (X-2000) yielded a wear rate of about 10(exp -10) cubic mm/mm. The results indicated that the silahydrocarbon class of liquid lubricants offers the better potential for space applications.

  13. Wear resistance improvement of a commercially pure titanium by high current pulsed electron beam treatment

    NASA Astrophysics Data System (ADS)

    Zhang, Xiangdong; Wang, Xiaoying; Li, Fangfang; Xiao, Hong

    2017-03-01

    A commercially pure titanium was selected as target material and treated by high current pulsed electron beam. The phase and structure changes occurring in the modified surface layers were observed with optical microscopy, scanning electron microscope, and transmission electron microscope. The increase in the wear resistance was observed for the pure titanium samples after pulsed electron beam surface melting. The mechanism for wear resistance modification was discussed. The results indicated that the presence of ultrafine martensite and defects in the treated surface layer were key factors for the improvement of the wear properties of pure titanium treated by high current pulsed beam treatment.

  14. Extended-wear of high oxygen-permeable quantum contact lenses.

    PubMed

    Kok, J H; Hilbrink, H J; Rosenbrand, R M; Visser, R

    1992-03-01

    This study was performed to investigate the effects of extended-wear of rigid aspherical high gas-permeable contact lenses on the cornea. In the study 32 subjects (62 eyes) were followed over a period of 3 to 24 months. A high gas-permeable contact lens (Dk 92), made of fluoro-silicone-acrylate copolymer, was used. Vision remained constant during the studied period. The corneal thickness decreased significantly (p less than 0.05) during the first six months. Significant changes (p less than 0.05) were found after three months in the corneal curvature, especially in the vertical meridian. No further topographical changes were noted in the period between three and six months of extended-wear. Complications, like acute red eye syndrome and bacterial infections, which may be encountered in soft lens extended-wear, were not noticed. At the end of the study 20 subjects (38 eyes, 61%) were still on extended-wear, 9 subjects (18 eyes, 29%) changed to daily wear and 3 subjects (six eyes, 10%) became unavailable for follow-up. Extended-wear of rigid aspherical high gas-permeable contact lenses may be considered as an acceptable alternative for soft lens extended-wear.

  15. Comparative wear tests of ultra-high molecular weight polyethylene and cross-linked polyethylene.

    PubMed

    Harsha, A P; Joyce, Tom J

    2013-05-01

    Wear particle-induced osteolysis is a major concern in hip implant failure. Therefore, recent research work has focussed on wear-resistant materials, one of the most important of which is cross-linked polyethylene. In view of this, the objective of this study was to compare the in vitro wear performance of cross-linked polyethylene to traditional ultra-high molecular weight polyethylene. In order to mimic appropriate in vivo conditions, a novel high-capacity wear tester called a circularly translating pin-on-disc was used. The results of this in vitro study demonstrated that the wear rate for cross-linked polyethylene was about 80% lower than that of conventional ultra-high molecular weight polyethylene. This difference closely matches in vivo results reported in the literature for total hip replacements that use the two biopolymers. The in vitro results were also verified against ASTM F732-00 (standard test method for wear testing of polymeric materials for use in total joint prostheses). The 50-station circularly translating pin-on-disc proved to be a reliable device for in vitro wear studies of orthopaedic biopolymers.

  16. High-temperature wear and deformation processes in metal matrix composites

    NASA Astrophysics Data System (ADS)

    Singh, J.; Alpas, A. T.

    1996-10-01

    Dry-sliding wear behaviors of a particulate-reinforced aluminum matrix composite 6061 Al-20 pet A12O3 and an unreinforced 6061 Al alloy were investigated in the temperature range 25 °C to 500 °C against a SAE 52100 bearing steel counterface. Experiments were carried out at a constant sliding speed of 0.2 m·s- at different test loads. The deformation behavior of the materials was studied by performing uniaxial compression tests in the same temperature range as the wear tests. Both alloys showed a mild-to-severe wear transition above a certain test temperature. In the mild wear regime, the wear rate and the coefficient of friction of the unreinforced 6061 Al decreased slightly with temperature, but the temperature had almost no effect on the wear rate and the coefficient of friction of the 6061 Al-20 pet Al2O3 in the same regime. Particulate reinforcement led to an increase in the transition temperature and a 50 to 70 pet improvement in the wear resistance in the severe wear regime. This was attributed to the formation of tribological layers consisting of comminuted A12O3 particles at the contact surface. High-temperature compression tests showed that the flow strength of 6061 Al-20 pet A12O3 and 6061 Al decreased monotonically with temperature and both alloys exhibited a work-softening behavior at temperatures higher than the inflection point on the flow stress vs temperature curves. The logarithmic maximum stress vs reciprocal temperature relationship was not linear, indicating that the deformation processes were too complicated to be characterized by a single activation energy over the whole temperature range. For the range of 250 °C to 450 °C, the activation energy for deformation was estimated to be 311 kJ·mol-1; for both the matrix alloy and the composite. Severe wear proceeded by thermally activated deformation processes involving dynamic recrystallization along a subsurface strain gradient. A power-Arrhenius type relationship was found to describe well

  17. A high sensitivity wear debris sensor using ferrite cores for online oil condition monitoring

    NASA Astrophysics Data System (ADS)

    Zhu, Xiaoliang; Zhong, Chong; Zhe, Jiang

    2017-07-01

    Detecting wear debris and measuring the increasing number of wear debris in lubrication oil can indicate abnormal machine wear well ahead of machine failure, and thus are indispensable for online machine health monitoring. A portable wear debris sensor with ferrite cores for online monitoring is presented. The sensor detects wear debris by measuring the inductance change of two planar coils wound around a pair of ferrite cores that make the magnetic flux denser and more uniform in the sensing channel, thereby improving the sensitivity of the sensor. Static testing results showed this wear debris sensor is capable of detecting 11 µm and 50 µm ferrous debris in 1 mm and 7 mm diameter fluidic pipes, respectively; such a high sensitivity has not been achieved before. Furthermore, a synchronized sampling method was also applied to reduce the data size and realize real-time data processing. Dynamic testing results demonstrated that the sensor is capable of detecting wear debris in real time with a high throughput of 750 ml min-1 the measured debris concentration is in good agreement with the actual concentration.

  18. The High performance of nanocrystalline CVD diamond coated hip joints in wear simulator test.

    PubMed

    Maru, M M; Amaral, M; Rodrigues, S P; Santos, R; Gouvea, C P; Archanjo, B S; Trommer, R M; Oliveira, F J; Silva, R F; Achete, C A

    2015-09-01

    The superior biotribological performance of nanocrystalline diamond (NCD) coatings grown by a chemical vapor deposition (CVD) method was already shown to demonstrate high wear resistance in ball on plate experiments under physiological liquid lubrication. However, tests with a close-to-real approach were missing and this constitutes the aim of the present work. Hip joint wear simulator tests were performed with cups and heads made of silicon nitride coated with NCD of ~10 μm in thickness. Five million testing cycles (Mc) were run, which represent nearly five years of hip joint implant activity in a patient. For the wear analysis, gravimetry, profilometry, scanning electron microscopy and Raman spectroscopy techniques were used. After 0.5 Mc of wear test, truncation of the protruded regions of the NCD film happened as a result of a fine-scale abrasive wear mechanism, evolving to extensive plateau regions and highly polished surface condition (Ra<10nm). Such surface modification took place without any catastrophic features as cracking, grain pullouts or delamination of the coatings. A steady state volumetric wear rate of 0.02 mm(3)/Mc, equivalent to a linear wear of 0.27 μm/Mc favorably compares with the best performance reported in the literature for the fourth generation alumina ceramic (0.05 mm(3)/Mc). Also, squeaking, quite common phenomenon in hard-on-hard systems, was absent in the present all-NCD system.

  19. Friction and wear evaluation of high-strength gel

    NASA Astrophysics Data System (ADS)

    Kameyama, Toshiki; Wada, Masato; Makino, Masato; Kawakami, Masaru; Furukawa, Hidemitsu

    2016-04-01

    In the last decade, several innovative polymer gel materials with enhanced mechanical proper ties have been invented by Japanese researches. In 2003, a most effective but simple way was proposed to synthesize double network gels, with compression fracture stress of about 30MPa, compared to several tens of kPa for common gels. In this study, we evaluate the wear of a double network gel, both with and without water lubrication. In the un-lubricated experiment, the gel surface is worn with a stainless steel ball. In the other experiment with water lubrication, the gel surface is worn by different counter surfaces because the stainless steel ball was too smooth to wear. It was found that frictional vibration of wear gel is transitioning to steady sliding in lubricated. As conventional reduction method of the friction by the contact between general solids, there are surface processing such as the texturing, attachment of lubrication materials. In the case of gel, the minute processing to the surface such as the texturing is difficult, because the gel is soft in comparison with the hard materials such as the metal. By proceeding with this study, the surface processing of low-frictional gels will be enabled.

  20. Do tissues from THA revision of highly crosslinked UHMWPE liners contain wear debris and associated inflammation?

    PubMed

    Baxter, Ryan M; Freeman, Theresa A; Kurtz, Steven M; Steinbeck, Marla J

    2011-08-01

    Polyethylene wear debris is a major contributor to inflammation and the development of implant loosening, a leading cause of THA revisions. To reduce wear debris, highly crosslinked ultrahigh-molecular-weight polyethylene (UHMWPE) was introduced to improve wear properties of bearing surfaces. As highly crosslinked UHMWPE revision tissues are only now becoming available, it is possible to examine the presence and association of wear debris with inflammation in early implant loosening. We asked: (1) Does the presence of UHMWPE wear debris in THA revision tissues correlate with innate and/or adaptive immune cell numbers? (2) Does the immune cell response differ between conventional and highly crosslinked UHMWPE cohorts? We collected tissue samples from revision surgery of nine conventional and nine highly crosslinked UHMWPE liners. Polarized light microscopy was used to determine 0.5- to 2-μm UHMWPE particle number/mm2, and immunohistochemistry was performed to determine macrophage, T cell, and neutrophil number/mm2. For the conventional cohort, correlations were observed between wear debris and the magnitude of individual patient macrophage (ρ=0.70) and T cell responses (ρ=0.71) and between numbers of macrophages and T cells (ρ=0.77) in periprosthetic tissues. In comparison, the highly crosslinked UHMWPE cohort showed a correlation between wear debris and the magnitude of macrophage responses (ρ=0.57) and between macrophage and T cell numbers (ρ=0.68). Although macrophages and T cells were present in both cohorts, the highly crosslinked UHMWPE cohort had lower numbers, which may be associated with shorter implantation times. The presence of wear debris and inflammation in highly crosslinked UHMWPE revision tissues may contribute to early implant loosening.

  1. Impact of high myopia and duration of hard contact lens wear on the progression of ptosis.

    PubMed

    Watanabe, Akihide; Imai, Kojiro; Kinoshita, Shigeru

    2013-03-01

    To investigate the impact of myopia and duration of hard contact lens (HCL) wear on the progression of ptosis. This study involved 194 eyes of 98 patients with either bilateral or unilateral ptosis with long-term HCL wear. The ptosis of each eyelid was classified into 1 of 4 grades (no ptosis, mild, moderate and severe), and the average spherical equivalent refractive error (SERE), patient age and the duration of HCL wear were then examined. The average SERE (in diopters) in 99 severe eyes was -8.34, in 47 moderate eyes, -6.28, in 37 mild eyes -5.57 and in 11 no ptosis eyes, -4.80, while the average duration of HCL wear (in years) were 34, 30, 29, and 31, respectively. The average SERE was significantly higher in the severe than in the moderate, mild and no ptosis eyelids, and the average duration of HCL wear was significantly longer in the severe than in the moderate and mild ptosis eyelids. Path analysis showed that the severity of ptosis is significantly influenced by SERE, as well as by patient age and the duration of HCL wear. High myopia, patient age and long-term HCL wear are risk factors associated with the progression of ptosis.

  2. Characteristics of highly cross-linked polyethylene wear debris in vivo.

    PubMed

    Baxter, Ryan M; MacDonald, Daniel W; Kurtz, Steven M; Steinbeck, Marla J

    2013-04-01

    Despite the widespread implementation of highly cross-linked polyethylene (HXLPE) liners to reduce the clinical incidence of osteolysis, it is not known if the improved wear resistance will outweigh the inflammatory potential of HXLPE wear debris generated in vivo. Thus, we asked: What are the differences in size, shape, number, and biological activity of polyethylene wear particles obtained from primary total hip arthroplasty revision surgery of conventional polyethylene (CPE) versus remelted or annealed HXLPE liners? Pseudocapsular tissue samples were collected from revision surgery of CPE and HXLPE (annealed and remelted) liners, and digested using nitric acid. The isolated polyethylene wear particles were evaluated using scanning electron microscopy. Tissues from both HXLPE cohorts contained an increased percentage of submicron particles compared to the CPE cohort. However, the total number of particles was lower for both HXLPE cohorts, as a result there was no significant difference in the volume fraction distribution and specific biological activity (SBA; the relative biological activity per unit volume) between cohorts. In contrast, based on the decreased size and number of HXLPE wear debris there was a significant decrease in total particle volume (mm(3)/g of tissue). Accordingly, when the SBA was normalized by total particle volume (mm(3)/gm tissue) or by component wear volume rate (mm(3)/year), functional biological activity of the HXLPE wear debris was significantly decreased compared to the CPE cohort. Indications for this study are that the osteolytic potential of wear debris generated by HXLPE liners in vivo is significantly reduced by improvements in polyethylene wear resistance. Copyright © 2013 Wiley Periodicals, Inc.

  3. Characteristics of highly cross-linked polyethylene wear debris in vivo

    PubMed Central

    Baxter, Ryan M.; MacDonald, Daniel W.; Kurtz, Steven M.; Steinbeck, Marla J.

    2014-01-01

    Despite the widespread implementation of highly cross-linked polyethylene (HXLPE) liners to reduce the clinical incidence of osteolysis, it is not known if the improved wear resistance will outweigh the inflammatory potential of HXLPE wear debris generated in vivo. Thus, we asked: What are the differences in size, shape, number, and biological activity of polyethylene wear particles obtained from primary total hip arthroplasty revision surgery of conventional polyethylene (CPE) versus remelted or annealed HXLPE liners? Pseudocapsular tissue samples were collected from revision surgery of CPE and HXLPE (annealed and remelted) liners, and digested using nitric acid. The isolated polyethylene wear particles were evaluated using scanning electron microscopy. Tissues from both HXLPE cohorts contained an increased percentage of submicron particles compared to the CPE cohort. However, the total number of particles was lower for both HXLPE cohorts, as a result there was no significant difference in the volume fraction distribution and specific biological activity (SBA; the relative biological activity per unit volume) between cohorts. In contrast, based on the decreased size and number of HXLPE wear debris there was a significant decrease in total particle volume (mm3/g of tissue). Accordingly, when the SBA was normalized by total particle volume (mm3/gm tissue) or by component wear volume rate (mm3/year), functional biological activity of the HXLPE wear debris was significantly decreased compared to the CPE cohort. Indications for this study are that the osteolytic potential of wear debris generated by HXLPE liners in vivo is significantly reduced by improvements in polyethylene wear resistance. PMID:23436587

  4. Investigation of Wear and Corrosion of a High-Carbon Stellite Alloy for Hip Implants

    NASA Astrophysics Data System (ADS)

    Hu, P. S.; Liu, R.; Liu, J.; McRae, G.

    2014-04-01

    Low-carbon Stellite 21 has been used as hip implant material for a number of decades; however, its limited metal-on-metal bearing has resulted in loosening between the femoral head and the acetabular cup of hip implants. In order to improve the metal-on-metal bearing, it is proposed that a high-carbon alloy, Stellite 720, surface coating be applied on Stellite 21 hip implants to improve mechanical and tribological performance. For this coating to be practical, it must also meet the requirements of corrosion resistance for orthopedic implant materials. In this research, Stellite 720 is investigated with pin-on-disk wear tests, and electrochemical and immersion corrosion tests in simulated human body fluid (Hank's solution; pH 7.4 at temperature of 37°C). The experimental results demonstrate that Stellite 720 exhibits much better wear resistance than Stellite 21, and has the potential for better corrosion resistance as well. The applicability of coating Stellite 21 hip implants with Stellite 720 is discussed.

  5. A thermal, thermoelastic, and wear analysis of high-energy disk brakes

    NASA Technical Reports Server (NTRS)

    Kennedy, F. E., Jr.; Wu, J. J.; Ling, F. F.

    1974-01-01

    A thermomechanical investigation of the sliding contact problem encountered in high-energy disk brakes is described. The analysis includes a modelling, using the finite element method of the thermoelastic instabilities that cause transient changes in contact area to occur on the friction surface. In order to include the effect of wear at the contact surface, a wear criterion is proposed that results in the prediction of wear rates for disk brakes that are quite close to experimentally determined wear rates. The thermal analysis shows that the transient temperature distribution in a disk brake assembly can be determined more accurately by use of this thermomechanical analysis than by a more conventional analysis that assumes constant contact conditions. It also shows that lower, more desirable, temperatures in disk brakes can be attained by increasing the volume, the thermal conductivity, and, especially, the heat capacity of the brake components.

  6. Wear-resistant ball bearings for space applications. [coated with titanium carbide

    NASA Technical Reports Server (NTRS)

    Boving, H.; Hintermann, H. E.; Haenni, W.; Bondivenne, E.; Boeto, M.; Conde, M.

    1977-01-01

    Ball bearings for hostile environments were developed. They consist of normal ball bearing steel parts of which the rings are coated with hard, wear-resistant, chemical vapor deposited (C.V.D) TiC. Experiments in ultrahigh vacuum, using cages of various materials with self-lubricating properties, have shown that such bearings are suitable for space applications.

  7. Novel Ti-Nb alloys with improved wear resistance for biomedical implant application.

    PubMed

    Chapala, Praveen; Acharyya, Swati Ghosh; Shariff, S M; Naik, Ganesh

    2016-08-01

    The present study involved fabrication of titanium niobium based alloys having elastic modulus close to that of human bone and subsequently determining the wear resistance of these alloys for biomedical application. In the present study three beta stabilized titanium niobium alloys having composition Ti-24Nb-4Zr-8Sn, Ti-35Nb-4Sn and Ti-29Nb-13Ta-7Zr were made by vacuum arc melting. The alloys were then aged at 1000 C for 6 hours in an argon atmosphere. Detailed microstructural characterization and phase identification was carried out using scanning electron microscopy and x-ray diffraction respectively. The hardness of the samples were measured by micro hardness measurements. The wear resistance and the friction coefficient of the samples were measured by testing in Ringer's solution (simulated body fluid). The results showed improved wear resistance of the fabricated alloys.

  8. Enhanced wear resistivity of a Zr-based bulk metallic glass processed by high-pressure torsion under reciprocating dry conditions

    NASA Astrophysics Data System (ADS)

    Joo, Soo-Hyun; Pi, Dong-Hai; Guo, Jing; Kato, Hidemi; Lee, Sunghak; Kim, Hyoung Seop

    2016-05-01

    Wear properties of bulk metallic glasses (BMGs) are important for industrial applications as much as strength and ductility. Free volume of BMGs is a significant factor which decides wear mechanism and resistance. Increased free volume of a Zr55Al10Ni5Cu30 BMG processed by high-pressure torsion (HPT) affected wear resistance under dry reciprocating conditions. Two- and three-body abrasive wear as well as the delamination of oxide layers simultaneously operated during the wear tests of both as-cast and HPT-processed BMG (HPT-BMG). However, the HPT- BMG had a larger area of the oxide layers on a worn surface compared to the as-cast BMG at the early stage of the wear tests. The increased free volume by the HPT process resulted in ductile plastic deformation, prohibited crack propagation, and delayed delamination of the oxide layers. Therefore, the HPT-BMG had thicker oxide layers, which acted as an adequate protection and increased wear properties of the Zr-based BMG.

  9. Abrasive wear of high velocity oxygen fuel (HVOF) superalloy coatings under vibration load

    NASA Astrophysics Data System (ADS)

    Kandeva, M.; Ivanova, B.; Karastoyanov, D.; Grozdanova, T.; Assenova, E.

    2017-02-01

    The present paper considers wear of coatings deposited by HVOF (High velocity oxy-fuel) technology, under conditions of dry friction against abrasive surface accompanied with the action of vibrations perpendicular to the sliding axis. Results are obtained with four type coatings: two types with Ni matrix of composition 602P – without preliminary heating of the basic surface (the substrate) and after substrate heating up to 650°C in a chamber; coating WC-12Co with tungsten matrix and coating obtained by 1:1 proportion powder mixture of both compositions 602P and WC-12Co. Results about the thickness, hardness and coating’ morphology are presented, as well as dependences of the wear and the relative wear resistance on vibration speeds in the interval 3.03 to 21.08 mm/s. New results are obtained about the nonlinear relationship between abrasive wear and vibration speed showing minimal wear for all specimens by 6.04 mm/s. It is found that lowest wear shows WC-12Co coating in the entire interval of vibration speed variation: 3.03 to 21.08 mm/s. The obtained results are new in the literature; they are not presented and published by the authors.

  10. Lightweight materials for automotive applications/topic 2: Wear resistant aluminum alloy

    SciTech Connect

    Viswanathan, S.

    1997-01-31

    The replacement of cast iron by aluminum alloys in automotive engine blocks and heads represents a significant weight reduction in automobiles. The primary hurdle to the widespread use of aluminum alloy engine blocks in the North American automobile industry was high cost. The lack of wear resistance in most aluminum alloys added to manufacturing cost, since expensive procedures such as the incorporation of cast iron liners or special coatings were needed to achieve the required wear properties. The project targeted the development of a wear resistant aluminum alloy, as well as tools and the knowledge-base required to design the casting process, to allow it to be cast economically into engine blocks without the use of a cast iron liner or special coating, thereby providing benefits to both the material and manufacturing aspects of the process. The project combined the alloy development, wear and microstructural characterization, and casting modeling capabilities of the laboratory with the partners extensive alloy and casting process development and manufacturing experience to develop a suitable wear resistant aluminum alloy and casting process.

  11. A study of energy-size relationship and wear rate in a lab-scale high pressure grinding rolls unit

    NASA Astrophysics Data System (ADS)

    Rashidi Dashtbayaz, Samira

    This study is focused on two independent topics of energy-size relationship and wear-rate measurements on a lab-scale high pressure grinding rolls (HPGR). The first part of this study has been aimed to investigate the influence of the operating parameters and the feed characteristics on the particle-bed breakage using four different ore samples in a 200 mm x 100 mm lab-scale HPGR. Additionally, multistage grinding, scale-up from a lab-scale HPGR, and prediction of the particle size distributions have been studied in detail. The results obtained from energy-size relationship studies help with better understanding of the factors contributing to more energy-efficient grinding. It will be shown that the energy efficiency of the two configurations of locked-cycle and open multipass is completely dependent on the ore properties. A test procedure to produce the scale-up data is presented. The comparison of the scale-up factors between the data obtained on the University of Utah lab-scale HPGR and the industrial machine at the Newmont Boddington plant confirmed the applicability of lab-scale machines for trade-off studies. The population balance model for the simulation of product size distributions has shown to work well with the breakage function estimated through tests performed on the HPGR at high rotational speed. Selection function has been estimated by back calculation of population balance model with the help of the experimental data. This is considered to be a major step towards advancing current research on the simulation of particle size distribution by using the HPGR machine for determining the breakage function. Developing a technique/setup to measure the wear rate of the HPGR rolls' surface is the objective of the second topic of this dissertation. A mockup was initially designed to assess the application of the linear displacement sensors for measuring the rolls' weight loss. Upon the analysis of that technique and considering the corresponding sources of

  12. Wear testing of a canine hip resurfacing implant using highly cross-linked polyethylene.

    PubMed

    Warburton, Kevin J; Everingham, John B; Helms, Jillian L; Kazanovicz, Andrew J; Hollar, Katherine A; Brourman, Jeff D; Fox, Steven M; Lujan, Trevor J

    2017-09-23

    Hip resurfacing offers advantages for young active patients afflicted with hip osteoarthritis, and may also be a beneficial treatment for adult canines. Conventional hip resurfacing uses metal-on-metal bearings to preserve bone stock, but it may be feasible to use metal-on-polyethylene bearings to reduce metal wear debris, while still preserving bone. This study characterized the short-term wear behavior of a novel hip resurfacing implant for canines that uses a 1.5 mm thick liner of highly cross-linked polyethylene in the acetabular component. This implant was tested in an orbital bearing machine that simulated canine gait for 1.1 million cycles. Wear of the liner was evaluated using gravimetric analysis and by measuring wear depth with an optical scanner. The liners had a steady-state mass wear rate of 0.99 ± 0.17 mg per million cycles, and an average wear depth in the central liner region of 0.028 mm. No liners, shells, or femoral heads had any catastrophic failure due to yielding or fracture. These results suggest that the thin liners will not prematurely crack after implantation in canines. This is the first hip resurfacing device developed for canines, and this study is the first to characterize the in vitro wear of highly cross-linked polyethylene liners in a hip resurfacing implant. The canine implant developed in this study may be an attractive treatment option for canines afflicted with hip osteoarthritis, and can serve as a valuable animal model to support the development of metal-on-polyethylene hip resurfacing technology for human patients. This article is protected by copyright. All rights reserved. This article is protected by copyright. All rights reserved.

  13. Study on critical-sized ultra-high molecular weight polyethylene wear particles loaded with alendronate sodium: in vitro release and cell response.

    PubMed

    Liu, Yumei; Shi, Feng; Gong, Kemeng; Liu, Yang; Zhi, Wei; Weng, Jie; Qu, Shuxin

    2017-04-01

    The aim of this study was to investigate the in vitro release and the effect of RAW 264.7 macrophages of critical-sized wear particles of ultra-high molecular weight polyethylene (UHMWPE) loaded with alendronate sodium (ALN), one of the most effective drugs to treat osteoporosis in clinic. The critical-sized UHMWPE-ALN 0.5 wt.% wear particles were prepared by vacuum gradient filtration combined with Pluronic F-68. In vitro release of ALN from critical-sized UHMWPE-ALN wear particles was investigated in phosphate buffered saline (PBS) at 37 °C with a shaker. Cell morphology, proliferation, lactate dehydrogenase (LDH) leakage and secretions of cytokines were evaluated after co-cultured with critical-sized UHMWPE-ALN wear particles in vitro. Results showed that ALN released from critical-sized UHMWPE-ALN wear particles included burst release and slow release in vitro. Macrophages would be chemotaxis and aggregated around the critical-sized UHMWPE-ALN or UHMWPE wear particle, which was phagocytosed with time. The proliferation of macrophages co-cultured with critical-sized UHMWPE-ALN wear particles was significantly decreased compared with that of critical-sized UHMWPE group. Meanwhile, the critical-sized UHMWPE-ALN wear particles significantly induced the LDH leakage of macrophages, which indicated the cell death. The death of macrophages induced by ALN was one of pathways to inhibit their proliferation. The secretions of cytokines (interleukin-6 and tumor necrosis factor-alpha) in critical-sized UHMWPE-ALN group were significantly lower than those in critical-sized UHMWPE group due to the released ALN. The present results suggested that UHMWPE-ALN had the potential application in clinic to treat osteolysis induced by wear particles.

  14. Cold atmospheric pressure gas plasma enhances the wear performance of ultra-high molecular weight polyethylene.

    PubMed

    Perni, Stefano; Kong, Michael G; Prokopovich, Polina

    2012-03-01

    Ultra-high molecular weight polyethylene (UHMWPE) is frequently employed in joint replacements because of its high biocompatibility; however, this material does not exhibit particularly strong wear performance, thus potentially reducing the longevity of such devices. Numerous techniques have been investigated to increase the resistance to wear of UHMWPE, but they are all based on expensive machinery and require a high level of safety precautions. Cold atmospheric pressure gas plasma treatment is an inexpensive process that has been used as a surface modification method and as a sterilization technique. We demonstrate for the first time that a helium/oxygen cold atmospheric pressure gas plasma can be used to enhance the wear performance of UHMWPE without affecting the cytocompatibility of the material. The exposure to a cold atmospheric pressure gas plasma results in a greater level of crosslinking of the polyethylene chains. As a consequence of the higher crosslinking, the material stiffness of the treated surface is increased.

  15. Comprehensive study of the abrasive wear and slurry erosion behavior of an expanded system of high chromium cast iron and microstructural modification for enhanced wear resistance

    NASA Astrophysics Data System (ADS)

    Chung, Reinaldo Javier

    High chromium cast irons (HCCIs) have been demonstrated to be an effective material for a wide range of applications in aggressive environments, where resistances to abrasion, erosion and erosion-corrosion are required. For instance, machinery and facilities used in mining and extraction in Alberta's oil sands suffer from erosion and erosion-corrosion caused by silica-containing slurries, which create challenges for the reliability and maintenance of slurry pumping systems as well as other processing and handling equipment. Considerable efforts have been made to determine and understand the relationship between microstructural features of the HCCIs and their wear performance, in order to guide the material selection and development for specific service conditions with optimal performance. The focus was previously put on a narrow group of compositions dictated by ASTM A532. However, with recent advances in casting technology, the HCCI compositional range can be significantly expanded, which potentially brings new alloys that can be superior to those which are currently employed. This work consists of three main aspects of study. The first one is the investigation of an expanded system of white irons with their composition ranging from 1 to 6 wt.% C and 5 to 45 wt.% Cr, covering 53 alloys. This work has generated wear and corrosion maps and established correlation between the performance and microstructural features for the alloys. The work was conducted in collaboration with the Materials Development Center of Weir Minerals in Australia, and the results have been collected in a database that is used by the company to guide materials selection for slurry pump components in Alberta oil sands and in other mining operations throughout the world. The second part consists of three case studies on effects of high chromium and high carbon, respectively, on the performance of the HCCIs. The third aspect is the development of an approach to enhance the wear resistance of

  16. Development of the High Temperature Fretting Wear Simulator for Steam Generator

    NASA Astrophysics Data System (ADS)

    Lee, Choon Yeol; Kim, Joong Ho; Bae, Joon Woo; Chai, Young Suck

    In nuclear power plant, fretting wear due to a combination of impact and sliding motions of the U-tubes against the supports and/or foreign objects caused by flow induced vibration, can make a serious problem in steam generator. A test rig, fretting wear simulator, is developed to elucidate fretting wear mechanism qualitatively and quantitatively. The realistic condition of steam generator of high temperature up to 320°C, high pressure up to 15 MPa, and water environment could be achieved by a test rig. The fretting wear simulator consists of main frame, water loop system, and control unit. Actual contact region under a realistic condition of steam generator was isolated using autoclave. Effects of various parameters such as the amounts of impact and sliding motions, applied loads and initial gaps and so forth are considered in this research. After the experiment, wear damage was measured by a three-dimensional profiler and the surface was also studied by SEM microscopically. Initial results were also presented.

  17. Suspension High Velocity Oxy-Fuel (SHVOF)-Sprayed Alumina Coatings: Microstructure, Nanoindentation and Wear

    NASA Astrophysics Data System (ADS)

    Murray, J. W.; Ang, A. S. M.; Pala, Z.; Shaw, E. C.; Hussain, T.

    2016-12-01

    Suspension high velocity oxy-fuel spraying can be used to produce thermally sprayed coatings from powdered feedstocks too small to be processed by mechanical feeders, allowing formation of nanostructured coatings with improved density and mechanical properties. Here, alumina coatings were produced from submicron-sized feedstock in aqueous suspension, using two flame combustion parameters yielding contrasting microstructures. Both coatings were tested in dry sliding wear conditions with an alumina counterbody. The coating processed with high combustion power of 101 kW contained 74 wt.% amorphous phase and 26 wt.% crystalline phase (95 wt.% gamma and 3 wt.% alpha alumina), while the 72-kW coating contained lower 58 wt.% amorphous phase and 42 wt.% crystalline phases (73 wt.% was alpha and 26 wt.% gamma). The 101-kW coating had a dry sliding specific wear rate between 4 and 4.5 × 10-5 mm3/Nm, 2 orders of magnitude higher than the 72-kW coating wear rate of 2-4.2 × 10-7 mm3/Nm. A severe wear regime dominated by brittle fracture and grain pullout of the coating was responsible for the wear of the 101-kW coating, explained by mean fracture toughness three times lower than the 72-kW coating, owing to the almost complete absence of alpha alumina.

  18. Composition, microstructure, hardness, and wear properties of high-speed steel rolls

    SciTech Connect

    Park, J.W.; Lee, H.C.; Lee, S.

    1999-02-01

    The effects of alloying elements on the microstructural factors, hardness, and wear properties of four high-speed steel (HSS) rolls fabricated by centrifugal casting were investigated. A hot-rolling simulation test was carried out using a high-temperature wear tester capable of controlling speed, load, and temperature. The test results revealed that the HSS roll containing a larger amount of vanadium showed the best wear resistance because it contained a number of hard MC-type carbides. However, it showed a very rough roll surface because of cracking along cell boundaries, the preferential removal of the matrix, and the sticking of the rolled material onto the roll surface during the wear process, thereby leading to an increase in the friction coefficient and rolling force. In order to improve wear resistance with consideration to surface roughness, it is suggested that a reduction in the vanadium content, an increase in solid-solution hardening by adding alloying elements, an increase in secondary hardening by precipitation of fine carbides in the matrix, and formation of refined prior austenite grains by preaustenitization treatment be employed to strengthen the matrix, which can hold hard carbides in it.

  19. Flank wear analysing of high speed end milling for hardened steel D2 using Taguchi Method

    NASA Astrophysics Data System (ADS)

    Hazza Faizi Al-Hazza, Muataz; Ibrahim, Nur Asmawiyah bt; Adesta, Erry T. Y.; Khan, Ahsan Ali; Abdullah Sidek, Atiah Bt.

    2017-03-01

    One of the main challenges for any manufacturer is how to decrease the machining cost without affecting the final quality of the product. One of the new advanced machining processes in industry is the high speed hard end milling process that merges three advanced machining processes: high speed milling, hard milling and dry milling. However, one of the most important challenges in this process is to control the flank wear rate. Therefore a analyzing the flank wear rate during machining should be investigated in order to determine the best cutting levels that will not affect the final quality of the product. In this research Taguchi method has been used to investigate the effect of cutting speed, feed rate and depth of cut and determine the best level s to minimize the flank wear rate up to total length of 0.3mm based on the ISO standard to maintain the finishing requirements.

  20. Wear and friction properties of experimental Ti-Si-Zr alloys for biomedical applications.

    PubMed

    Tkachenko, Serhii; Datskevich, Oleg; Kulak, Leonid; Jacobson, Staffan; Engqvist, Håkan; Persson, Cecilia

    2014-11-01

    Titanium alloys are widely used in biomedical applications due to their higher biocompatibility in comparison to other metallic biomaterials. However, they commonly contain aluminum and vanadium, whose ions may be detrimental to the nervous system. Furthermore, they suffer from poor wear resistance, which limits their applications. The aim of this study was to evaluate the tribological performance of experimental Ti-1.25Si-5Zr, Ti-2.5Si-5Zr, Ti-6Si-5Zr and Ti-2.5Si-5Zr-0.2Pd alloys as compared to that of control Ti-6Al-4V, CoCr F75 and CoCr F799 alloys. Friction and wear tests were performed using a standard ball-on-disc rig in serum solution at ambient temperature with Si3N4-balls as counterparts. The alloys microstructure and hardness were investigated using optical microscopy, XRD, scanning electron microscopy (SEM) and Vickers indentation. The coefficients of friction of the experimental Ti-Si-Zr alloys were generally lower than the commercial ones with Ti-6Si-5Zr presenting the lowest value (approx. 0.1). Their wear rates were found to be 2-7 times lower than that of the commercial Ti-6Al-4V alloy, but still higher than those of the CoCr alloys. SEM analysis of worn surfaces showed that abrasion was the predominant wear mechanism for all studied materials. Wear and friction were influenced by the formation and stability of transfer layers, and while commercial Ti-6Al-4V as well as the experimental Ti-Si-Zr alloys demonstrated extensive material transfer to the ceramic counterparts, the CoCr alloys did not show such material transfer.

  1. "Severe" wear challenge to 36 mm mechanically enhanced highly crosslinked polyethylene hip liners.

    PubMed

    Bowsher, J G; Williams, P A; Clarke, I C; Green, D D; Donaldson, T K

    2008-07-01

    Our purpose was to compare the wear performance of mechanically enhanced 5Mrad highly crosslinked polyethylene (MEP, ArComXL) hip liners to (control) 3Mrad UHMWPE liners (ArCom) in 36 mm head size. As a more severe synergy of clinically relevant test models, we contrasted wear with custom roughened Co-Cr surfaces (Ra 500 nm) to the standard pristine Co-Cr heads (Ra < 20 nm) using a severe microseparation test mode in our hip simulator. We adopted a previously published model to estimate potential biological activity. On new Co-Cr heads, the MEP liners showed a 47% reduction in volumetric wear a 13% reduction in wear particle size and a 27% reduction in Functional Biological Activity (FBA) compared to our control. On rough Co-Cr heads, the MEP liners showed little advantage in terms of volumetric wear compared with the control. However, the MEP liners overall showed a 38% reduction in FBA compared to the control owing to a larger volume fraction of larger particles. Thus overall the MEP liners appeared to offer advantages in terms of reduced FBA indices.

  2. Reduction of total knee replacement wear with vitamin E blended highly cross-linked ultra-high molecular weight polyethylene.

    PubMed

    Vaidya, C; Alvarez, E; Vinciguerra, J; Bruce, D A; DesJardins, J D

    2011-01-01

    Ultra-high molecular weight polyethylene (UHMWPE) is a common bearing component in total knee replacement (TKR) implants, and its susceptibility to wear continues to be the long-term limiting factor in the life of these implants. This study hypothesized that in TKR systems, a highly cross-linked (HXL) UHMWPE blended with vitamin E will result in reduced wear as compared to a direct compression-moulded (DCM) UHMWPE. A wear simulation study was conducted using an asymmetric lateral pivoting '3D Knee' design to compare the two inserts. The highly cross-linked UHMWPE was aged prior to the testing and force-controlled wear testing was carried out for 5 million cycles using a load-controlled ISO-14243 standard at a frequency of 1 Hz on both groups. Gravimetric measurements of DCM UHMWPE (4.4 +/- 3.0 mg/million cycles) and HXL UHMWPE with vitamin E (1.9 +/- 1.9 mg/million cycles) showed significant statistical differences (p < 0.01) between the wear rates. Wear modes and surface roughness for both groups revealed no significant dissimilarities.

  3. Microstructure and wear behaviors of laser clad NiCr/Cr3C2-WS2 high temperature self-lubricating wear-resistant composite coating

    NASA Astrophysics Data System (ADS)

    Yang, Mao-Sheng; Liu, Xiu-Bo; Fan, Ji-Wei; He, Xiang-Ming; Shi, Shi-Hong; Fu, Ge-Yan; Wang, Ming-Di; Chen, Shu-Fa

    2012-02-01

    The high temperature self-lubricating wear-resistant NiCr/Cr3C2-30%WS2 coating and wear-resistant NiCr/Cr3C2 coating were fabricated on 0Cr18Ni9 austenitic stainless steel by laser cladding. Phase constitutions and microstructures were investigated, and the tribological properties were evaluated using a ball-on-disc wear tester under dry sliding condition at room-temperature (17 °C), 300 °C and 600 °C, respectively. Results indicated that the laser clad NiCr/Cr3C2 coating consisted of Cr7C3 primary phase and γ-(Fe,Ni)/Cr7C3 eutectic colony, while the coating added with WS2 was mainly composed of Cr7C3 and (Cr,W)C carbides, with the lubricating WS2 and CrS sulfides as the minor phases. The wear tests showed that the friction coefficients of two coatings both decrease with the increasing temperature, while the both wear rates increase. The friction coefficient of laser clad NiCr/Cr3C2-30%WS2 is lower than the coating without WS2 whatever at room-temperature, 300 °C, 600 °C, but its wear rate is only lower at 300 °C. It is considered that the laser clad NiCr/Cr3C2-30%WS2 composite coating has good combination of anti-wear and friction-reducing capabilities at room-temperature up to 300 °C.

  4. The application of counter immunoelectrophoresis (CIE) in ocular protein studies Part II: Kinin activity in the lens wearing eye.

    PubMed

    Mann, Aisling M; Tighe, Brian J

    2002-06-01

    The kinin family are a group of bioactive peptides that are closely involved in the modulation of vascular inflammation and local injury. We have demonstrated here, for the first time, a link between kinin activity and contact lens wear. Protein extracts from daily and extended wear etafilcon A, Group IV, Acuvue lenses (Vistakon), were analysed by counter immunoelectrophoresis. In this way, kinin activity associated with contact lens wear was detected. High molecular weight kininogen was used as the marker protein. In contrast, no kinin activity was detected in the non-lens wearing normal eye.

  5. Ultra-high wear resistance of ultra-nanocrystalline diamond film: Correlation with microstructure and morphology

    SciTech Connect

    Rani, R.; Kumar, N.; Lin, I-Nan

    2016-05-23

    Nanostructured diamond films are having numerous unique properties including superior tribological behavior which is promising for enhancing energy efficiency and life time of the sliding devices. High wear resistance is the principal criterion for the smooth functioning of any sliding device. Such properties are achievable by tailoring the grain size and grain boundary volume fraction in nanodiamond film. Ultra-nanocrystalline diamond (UNCD) film was attainable using optimized gas plasma condition in a microwave plasma enhanced chemical vapor deposition (MPECVD) system. Crystalline phase of ultra-nanodiamond grains with matrix phase of amorphous carbon and short range ordered graphite are encapsulated in nanowire shaped morphology. Film showed ultra-high wear resistance and frictional stability in micro-tribological contact conditions. The negligible wear of film at the beginning of the tribological contact was later transformed into the wearless regime for prolonged sliding cycles. Both surface roughness and high contact stress were the main reasons of wear at the beginning of sliding cycles. However, the interface gets smoothened due to continuous sliding, finally leaded to the wearless regime.

  6. Volatility and Wear Characteristics of a Variety of Liquid Lubricants for Space Applications

    NASA Technical Reports Server (NTRS)

    Nguyen, Quynhgiao N.; Jones, William R., Jr.

    2001-01-01

    The vapor pressures and near characteristics are critical properties for liquid lubricants to assure long-term reliability and performance in space applications. Vapor pressures, obtained using a Knudsen cell technique, and near properties, obtained using a vacuum four-ball apparatus, were measured for a series of unformulated liquid lubricants. These include: two multiple alkylated cyclopentanes (MACs) (X-1000 and X-2000), two linear perfluoropolyalkylethers (PFPAEs) (Z-25 and 815Z), and four silahydrocarbons (a tri-, a tetra-, and two pentas). Vapor pressures were measured at three elevated temperatures (423, 448, and 498 K) and extrapolated to room temperature 298 K. The lowest 298 K vapor pressure of 5.7 x 10(exp -14) Pa, was obtained with the PFPAE fluid (815Z) and the highest value with the low molecular weight MAC (X-1000) at 3.6 x 10(exp -7) Pa. In addition, vacuum near rates were determined for some of the lubricants. The lowest wear rates (approximately 3 x 10(exp -11) cubic mm/mm) were observed for three of the silahydrocarbons while the highest wear rate (approximately 2 x 10(exp-9) cubic mm/mm) were observed with the two PFPAE fluids (Z-25 and 815Z). The MAC (X-2000) yielded a wear rate of about 10(exp -10) cubic mm/mm. The results indicated that the silahydrocarbon class of liquid lubricants offers the better potential for space applications.

  7. Extended release of high molecular weight hydroxypropyl methylcellulose from molecularly imprinted, extended wear silicone hydrogel contact lenses.

    PubMed

    White, Charles J; McBride, Matthew K; Pate, Kayla M; Tieppo, Arianna; Byrne, Mark E

    2011-08-01

    Symptoms of contact lenses induced dry eye (CLIDE) are typically treated through application of macromolecular re-wetting agents via eye drops. Therapeutic soft contact lenses can be formulated to alleviate CLIDE symptoms by slowly releasing comfort agent from the lens. In this paper, we present an extended wear silicone hydrogel contact lens with extended, controllable release of 120 kDa hydroxypropyl methylcellulose (HPMC) using a molecular imprinting strategy. A commercial silicone hydrogel lens was tailored to release approximately 1000 μg of HPMC over a period of up to 60 days in a constant manner at a rate of 16 μg/day under physiological flowrates, releasing over the entire range of continuous wear. Release rates could be significantly varied by the imprinting effect and functional monomer to template ratio (M/T) with M/T values 0, 0.2, 2.8, 3.4 corresponding to HPMC release durations of 10, 13, 23, and 53 days, respectively. Lenses had high optical quality and adequate mechanical properties for contact lens use. This work highlights the potential of imprinting in the design and engineering of silicone hydrogel lenses to release macromolecules for the duration of wear, which may lead to decreased CLIDE symptoms and more comfortable contact lenses.

  8. Dry Sliding Wear Behaviours of Valve Seat Inserts Produced from High Chromium White Iron

    NASA Astrophysics Data System (ADS)

    Kalyon, Ali; Özyürek, Dursun; Günay, Mustafa; Aztekin, Hasan

    2015-11-01

    In this present study, wear behaviours of high chromium white iron valve seat inserts and tappets used in the automotive sector were investigated. Wear behaviours of three different rates of high chromium white cast irons (containing 10, 12 and 14% chromium) were examined under heavy service conditions. For that purpose, the produced valve seat inserts were characterized through Scanning Electron Microscopy (SEM), Energy Dispersive Spectroscopy (EDS), X-ray diffraction (XRD) and hardness measurements. They were tested at a sliding speed of 1 ms-1, under 120 N load and for six different sliding distances (500, 1000, 1500, 2000, 2500, 3000 m) by using a standard wear apparatus (pin-on-disk type). The result showed that as the amount of Cr increased in the alloys, their hardness decreased. The decrease in the hardness were considered to be as the result of transformation of M7C3 carbides into M23C6 carbides in the structure. This decrease in hardness with increasing chromium content also increased the weight loss. Thus, it was determined that the white iron with 14% Cr (which had a greater amount of M23C6 carbides) was subjected to the highest wear.

  9. Microstructure and properties of laser-clad high-temperature wear-resistant alloys

    NASA Astrophysics Data System (ADS)

    Yang, Yongqiang

    1999-02-01

    A 2-kW CO 2 laser with a powder feeder was used to produce alloy coatings with high temperature-wear resistance on the surface of steel substrates. To analyze the microstructure and microchemical composition of the laser-clad layers, a scanning electron microscope (SEM) equipped with an energy dispersive X-ray microanalysis system was employed. X-ray diffraction techniques were applied to characterize the phases formed during the cladding process. The results show that the microstructure of the cladding alloy consists mainly of many dispersed particles (W 2C, (W,Ti)C 1- x, WC), a lamellar eutectic carbide M 12C, and an (f.c.c) matrix. Hardness tested at room and high temperature showed that the laser-clad zone has a moderate room temperature hardness and relatively higher elevated temperature hardness. The application of the laser-clad layer to a hot tool was very successful, and its operational life span was prolonged 1 to 4 times.

  10. Cyclostationarity approach for monitoring chatter and tool wear in high speed milling

    NASA Astrophysics Data System (ADS)

    Lamraoui, M.; Thomas, M.; El Badaoui, M.

    2014-02-01

    Detection of chatter and tool wear is crucial in the machining process and their monitoring is a key issue, for: (1) insuring better surface quality, (2) increasing productivity and (3) protecting both machines and safe workpiece. This paper presents an investigation of chatter and tool wear using the cyclostationary method to process the vibrations signals acquired from high speed milling. Experimental cutting tests were achieved on slot milling operation of aluminum alloy. The experimental set-up is designed for acquisition of accelerometer signals and encoding information picked up from an encoder. The encoder signal is used for re-sampling accelerometers signals in angular domain using a specific algorithm that was developed in LASPI laboratory. The use of cyclostationary on accelerometer signals has been applied for monitoring chatter and tool wear in high speed milling. The cyclostationarity appears on average properties (first order) of signals, on the energetic properties (second order) and it generates spectral lines at cyclic frequencies in spectral correlation. Angular power and kurtosis are used to analyze chatter phenomena. The formation of chatter is characterized by unstable, chaotic motion of the tool and strong anomalous fluctuations of cutting forces. Results show that stable machining generates only very few cyclostationary components of second order while chatter is strongly correlated to cyclostationary components of second order. By machining in the unstable region, chatter results in flat angular kurtosis and flat angular power, such as a pseudo (white) random signal with flat spectrum. Results reveal that spectral correlation and Wigner Ville spectrum or integrated Wigner Ville issued from second-order cyclostationary are an efficient parameter for the early diagnosis of faults in high speed machining, such as chatter, tool wear and bearings, compared to traditional stationary methods. Wigner Ville representation of the residual signal shows

  11. Wear of materials - 1987

    SciTech Connect

    Ludema, K.C.

    1987-01-01

    This book presents the papers given at a conference on materials testing to determine wear resistance. Topics considered at the conference included the wear of metals in a magnetic field, ceramics in advanced heat engine applications, wear tests of silicon carbides, microstructure, hardfacing alloys, sliding friction, coated systems, abrasion, erosion, test methods, tribology, stacking fault energy, and adhesion.

  12. High pressure slurry pump. Sand slurry test loop design and results. Wear parts lifetime analysis

    SciTech Connect

    Fongaro, S.; Severini, P.; Vinciguerra, G.

    2000-07-01

    This paper shows the experimental phase, following previous work presented at the Sixth International Conference on ``Multiphase Flow in Industrial Plants'', Milan, September 98. A Sand Water Slurry Test Loop has been tested using different sand percentages for a total power of 680 HP with a flow-rate of 35,000 [gpm] and pressure of 2300 [psig]. Its design considered, carefully, the particles build-up effect respecting flow velocity and dead space along the loop and into the hydraulics. The test pump is a TRIPLEX SINGLE ACTING that is one third of the COAL SLURRY SEPTUPLEX PUMP designed for a CHINA PROJECT. Wear rate on the main parts of an high pressure slurry pump have been analyzed running at 145 rpm (piston mean speed of 3.3 [ft/s]) with a net flow of 33,290 [gpm] and pressures between 1216 and 1575 [psig]. Tests gave indications of a damaging process on valves, piston seals and the relative weight on the overall damages. Design changes of piston-seal and its material have been done, results being a longer parts lifetime. The authors compared the results with literature on coal slurry and other sand tests. The pump speed, i.e., valve cycle, isn't the main wear factor, while the fluid speed under the valve is. Their goals are to improve the wear parts lifetime and define functions to relate the wear to operating parameters, design choice, and materials used.

  13. Wear resistance of highly cross-linked and remelted polyethylenes after ion implantation and accelerated ageing.

    PubMed

    Medel, F J; Puértolas, J A

    2008-08-01

    Ion implantation may provide medical polyethylenes with excellent mechanical and tribological properties, helping to lower the risk of long-term osteolysis. Highly crosslinked and remelted polyethylenes, materials currently used as soft components in artificial joints, were implanted with N+ and He+ ions at different ion fluences. The mechanical and tribological properties under distilled water lubrication at body temperature were assessed after ion implantation by means of microhardness and pin-on-disc tests respectively. Thus, the influences of the ionic species and implantation dose on surface hardness, friction coefficient, and wear factor were fully characterized. Furthermore, the tribological behaviour was evaluated after an accelerated ageing protocol (120 degrees C for 36h). Ion implantation increased the surface hardness, as well as friction coefficients, and decreased the wear factors especially at the highest doses. Also, even though all artificially aged materials showed a worse wear behaviour, polyethylenes implanted with either N+ or He+ at the highest doses maintained a relatively good wear factor in comparison with the aged non-implanted material. The origins of these modifications are discussed according to the effects of ion implantation on the microstructure of the polymer.

  14. Retrieved highly crosslinked UHMWPE acetabular liners have similar wear damage as conventional UHMWPE.

    PubMed

    Schroder, David T; Kelly, Natalie H; Wright, Timothy M; Parks, Michael L

    2011-02-01

    Highly crosslinked UHMWPE is associated with increased wear resistance in hip simulator and clinical studies. Laboratory and case studies, however, have described rim fracture in crosslinked acetabular liners. Controversy exists, therefore, on the relative merits of crosslinked liners over conventional liners in terms of wear performance versus resistance to fatigue cracking. We asked whether crosslinked liners would show less surface damage than conventional liners but would be more susceptible to fatigue damage. We examined 36 conventional UHMWPE and 39 crosslinked UHMWPE retrieved implants with similar patient demographics and identical design for evidence of wear damage, including articular surface damage, impingement, screw-hole creep, and rim cracks. We observed no difference in wear damage scores for the two liners. Conventional liners more frequently impinged but were more often elevated with smaller head sizes. We observed creep in approximately 70% of both types of liners. Incipient rim cracks were found in five crosslinked liners, and one liner had a rim fracture. Only one conventional liner had an incipient rim crack. Contrary to our expectation, damage was similar between crosslinked and conventional UHMWPE liners. Moreover, the 15% occurrence (six of 39) of incipient or complete fractures in crosslinked liners as compared with a 3% occurrence (one of 36) in conventional liners may have implications for the long-term performance of crosslinked liners. Longer-term studies will be necessary to establish the fate of rim cracks and thus the overall clinical fatigue performance of crosslinked liners.

  15. Does cyclic stress and accelerated ageing influence the wear behavior of highly crosslinked polyethylene?

    PubMed

    Affatato, Saverio; De Mattia, Jonathan Salvatore; Bracco, Pierangiola; Pavoni, Eleonora; Taddei, Paola

    2016-06-01

    First-generation (irradiated and remelted or annealed) and second-generation (irradiated and vitamin E blended or doped) highly crosslinked polyethylenes were introduced in the last decade to solve the problems of wear and osteolysis. In this study, the influence of the Vitamin-E addition on crosslinked polyethylene (XLPE_VE) was evaluated by comparing the in vitro wear behavior of crosslinked polyethylene (XLPE) versus Vitamin-E blended polyethylene XLPE and conventional ultra-high molecular weight polyethylene (STD_PE) acetabular cups, after accelerated ageing according to ASTM F2003-02 (70.0±0.1°C, pure oxygen at 5bar for 14 days). The test was performed using a hip joint simulator run for two millions cycles, under bovine calf serum as lubricant. Mass loss was found to decrease along the series XLPE_VE>STD_PE>XLPE, although no statistically significant differences were found between the mass losses of the three sets of cups. Micro-Raman spectroscopy was used to investigate at a molecular level the morphology changes induced by wear. The spectroscopic analyses showed that the accelerated ageing determined different wear mechanisms and molecular rearrangements during testing with regards to the changes in both the chain orientation and the distribution of the all-trans sequences within the orthorhombic, amorphous and third phases. The results of the present study showed that the addition of vitamin E was not effective to improve the gravimetric wear of PE after accelerated ageing. However, from a molecular point of view, the XLPE_VE acetabular cups tested after accelerated ageing appeared definitely less damaged than the STD_PE ones and comparable to XLPE samples.

  16. Wear transition of solid-solution-strengthened Ti-29Nb-13Ta-4.6Zr alloys by interstitial oxygen for biomedical applications.

    PubMed

    Lee, Yoon-Seok; Niinomi, Mitsuo; Nakai, Masaaki; Narita, Kengo; Cho, Ken; Liu, Huihong

    2015-11-01

    In previous studies, it has been concluded that volume losses (V loss) of the Ti-29Nb-13Ta-4.6Zr (TNTZ) discs and balls are larger than those of the respective Ti-6Al-4V extra-low interstitial (Ti64) discs and balls, both in air and Ringer's solution. These results are related to severe subsurface deformation of TNTZ, which is caused by the lower resistance to plastic shearing of TNTZ than that of Ti64. Therefore, it is necessary to further increase the wear resistance of TNTZ to satisfy the requirements as a biomedical implant. From this viewpoint, interstitial oxygen was added to TNTZ to improve the plastic shear resistance via solid-solution strengthening. Thus, the wear behaviors of combinations comprised of a new titanium alloy, TNTZ with high oxygen content of 0.89 mass% (89O) and a conventional titanium alloy, Ti64 were investigated in air and Ringer's solution for biomedical implant applications. The worn surfaces, wear debris, and subsurface damage were analyzed using a scanning electron microscopy and an electron probe microanalysis. V loss of the 89O discs and balls are smaller than those of the respective TNTZ discs and balls in both air and Ringer's solution. It can be concluded that the solid-solution strengthening by oxygen effectively improves the wear resistance for TNTZ materials. However, the 89O disc/ball combination still exhibits higher V loss than the Ti64 disc/ball combination in both air and Ringer's solution. Moreover, V loss of the disc for the 89O disc/Ti64 ball combination significantly decreases in Ringer's solution compared to that in air. This decrease for the 89O disc/Ti64 ball combination in Ringer's solution can be explained by the transition in the wear mechanism from severe delamination wear to abrasive wear. Copyright © 2015 Elsevier Ltd. All rights reserved.

  17. Friction and Wear Sciences for a Highly Durable Railgun Weapon

    DTIC Science & Technology

    2007-10-01

    required in order to produce a robust method of predicting the life of a railgun barrel given its design and mission. Specific tasks were: 1...life of a railgun barrel given its design and mission. Specific tasks were: 1) investigate the physical and chemical interactions and processes that...lead to a highly disturbed magnetic field near the crack, resulting in an unevenly distributed Lorentz force. Evaluation of the coupling electro

  18. Microstructure of laser-clad high-temperature self-lubricating wear-resistant composite coatings

    NASA Astrophysics Data System (ADS)

    Liu, X. B.; Wang, C. M.; Yu, L. G.; Wang, Hua Ming

    1999-09-01

    In this paper, a 5 kW cw CO2 laser was used to fabricate a new high-temperature self-lubricating wear-resistant composite coating on austenite stainless steel 1Cr18Ni9Ti. Microstructure of the coatings was characterized by OM, SEM, XRD and EDS as functions of laser processing parameters. The hybrid composite coating consists of rapidly solidified wear-resistant primary Cr7C3 and eutectic Cr23C6 carbides, high-temperature self-lubricating CaAgF4 or CaF2 particles and the oxidation-resistant austenitic Ni-Cr matrix. Microstructure and hardness within the whole laser clad composite coating is homogeneous and the bonding to the substrate is purely metallurgical. Microhardness of the composite coating is 700 approximately 1000 HV on average. The hybrid composite coatings fabricated by laser cladding are expected to have good high-temperature tribological properties.

  19. Optical Emission Characterization of High-Power Hall Thruster Wear

    NASA Technical Reports Server (NTRS)

    WIlliams, George J.; Kamhawi, Hani

    2013-01-01

    Optical emission spectroscopy is employed to correlate BN insulator erosion with high-power operation of the NASA 300M Hall-effect thruster. Actinometry leveraging excited xenon states is used to normalize the emission spectra of ground state boron as a function of thruster operating condition. Trends in the strength of the boron signal are correlated with thruster power, discharge voltage, discharge current and magnetic field strength. The boron signals are shown to trend with discharge current and show weak dependence on discharge voltage. The trends are consistent with data previously collected on the NASA 300M and NASA 457M thrusters but are different from conventional wisdom.

  20. Wear Performance of Laser Processed Tantalum Coatings

    PubMed Central

    Dittrick, Stanley; Balla, Vamsi Krishna; Bose, Susmita; Bandyopadhyay, Amit

    2011-01-01

    This first generation investigation evaluates the in vitro tribological performance of laser-processed Ta coatings on Ti for load-bearing implant applications. Linear reciprocating wear tests in simulated body fluid showed one order of magnitude less wear rate, of the order of 10−4mm3(N.m)−1, for Ta coatings compared to Ti. Our results demonstrate that Ta coatings can potentially minimize the early-stage bone-implant interface micro-motion induced wear debris generation due to their excellent bioactivity comparable to that of hydroxyapatite (HA), high wear resistance and toughness compared to popular HA coatings. PMID:22058608

  1. Short term wear of high Dk soft contact lenses does not alter corneal epithelial cell size or viability

    PubMed Central

    Stapleton, F.; Kasses, S.; Bolis, S.; Keay, L.

    2001-01-01

    BACKGROUND/AIMS—Current contact lenses (CLs) when worn on an extended wear basis cause corneal epithelial alterations. The aim of this study was to evaluate changes in corneal epithelial cell morphology and physiology following short term (3 months) wear of highly oxygen permeable CLs and to compare this with disposable CLs.
METHODS—Subjects were wearers of highly oxygen permeable CLs (n=11, wearing CLs on a 30 night schedule), disposable CL users (n=6, wearing CLs on a 6 night schedule), and non-CL wearers (n=20). Mean CL wear experience was 3 months. Epithelial cells were harvested using corneal cytology and were stained using acridine orange and ethidium bromide. Epithelial cell size and viability were determined.
RESULTS—The majority of epithelial cells recovered were non-viable (71%), and the mean longest cell diameter was 38 (SD 8) µm. Disposable CLs caused an increase in cell size (42 (7) µm) compared with both non-wear (39 (7) µm, p=0.01) and wear of highly oxygen permeable CLs (37 (10) µm, p=0.0049). There was no difference in cell viability between groups.
CONCLUSIONS—Extended wear of disposable CLs caused an 8% increase in cell diameter in harvested corneal epithelial cells following 3 months of CL wear. Cells harvested following 3 months' wear of highly oxygen permeable CLs were indistinguishable from those recovered from non-CL wearers.

 PMID:11159475

  2. Wear characteristics of bonded solid film lubricant under high load condition

    NASA Technical Reports Server (NTRS)

    Hiraoka, Naofumi; Sasaki, Akira; Kawashima, Noritsugu; Honda, Toshio

    1991-01-01

    Wear properties of phenolic resin bonded molybdenum disulfide film lubricant were studied. In-vacuo journal bearing tests were performed to evaluate the wear-life of this film lubricant. The wear-life depends on substrate materials and on sliding velocity. Pretreated substrate surfaces were examined to reveal the reasons for these results. Additionally, investigations on film wear mechanisms were made.

  3. Simple colorimetric methods for determination of sub-milligram amounts of ultra-high molecular weight polyethylene wear particles.

    PubMed

    Vesely, F; Zolotarevova, E; Spundova, M; Kaftan, F; Slouf, M; Entlicher, G

    2012-05-01

    New colorimetric methods are described for determination of sub-milligram amounts of ultra-high molecular weight polyethylene (UHMWPE) wear particles. These methods are based on the irreversible binding of the fluorescein-conjugated bovine serum albumin or the hydrophobic dye Oil Red O to wear particles. UHMWPE particles bind both substances from their solutions and thus decrease the absorbance of these solutions. The decrease is linearly dependent on the amount of added wear particles in the sub-milligram range suitable for practical use. The newly developed method offers improved accuracy and precision compared to Fourier transformed infrared spectroscopy (Slouf M, et al. Quantification of UHMWPE wear in periprosthetic tissues of hip arthoplasty: description of a new method based on IR and comparison with radiographic appearance. Wear 2008;265:674-684.).

  4. Study on mild and severe wear of 7075 aluminum alloys by high-speed wire electrical discharge machining

    NASA Astrophysics Data System (ADS)

    Xu, Jinkai; Qiu, Rongxian; Xia, Kui; Wang, Zhichao; Xu, Lining; Yu, Huadong

    2017-01-01

    The recast and the carbon layers were fabricated on 7075Al alloys surface by the high-speed wire electrical discharge machining (HS-WEDM) technologyunder various working parameters. The mechanical properties and friction behaviors of the layers were investigated by UMT. 7075 Al alloys were used to do dry sliding wear tests on a pin-ondisk wear tester at room temperature under various contact pressures. 7075 Al alloys had almost the same wear regularity as a function of sliding velocity and rated frequency. The hardness of recast layer was improved. And this method can enhance durability of 7075 Al alloy effectively.The transition to severe wear occurred at a higher load (12N) for asmachined samples, compared with 7075 matrix (9N), the as-machined samples exhibited lower wear rates within the tested loading range.

  5. Nanoscale wear and kinetic friction between atomically smooth surfaces sliding at high speeds

    NASA Astrophysics Data System (ADS)

    Rajauria, Sukumar; Canchi, Sripathi V.; Schreck, Erhard; Marchon, Bruno

    2015-02-01

    The kinetic friction and wear at high sliding speeds is investigated using the head-disk interface of hard disk drives, wherein the head and the disk are less than 10 nm apart and move at sliding speeds of 5-10 m/s relative to each other. While the spacing between the sliding surfaces is of the same order of magnitude as various AFM based fundamental studies on friction, the sliding speed is nearly six orders of magnitude larger, allowing a unique set-up for a systematic study of nanoscale wear at high sliding speeds. In a hard disk drive, the physical contact between the head and the disk leads to friction, wear, and degradation of the head overcoat material (typically diamond like carbon). In this work, strain gauge based friction measurements are performed; the friction coefficient as well as the adhering shear strength at the head-disk interface is extracted; and an experimental set-up for studying friction between high speed sliding surfaces is exemplified.

  6. Nanoscale wear and kinetic friction between atomically smooth surfaces sliding at high speeds

    SciTech Connect

    Rajauria, Sukumar Canchi, Sripathi V. Schreck, Erhard; Marchon, Bruno

    2015-02-23

    The kinetic friction and wear at high sliding speeds is investigated using the head-disk interface of hard disk drives, wherein the head and the disk are less than 10 nm apart and move at sliding speeds of 5–10 m/s relative to each other. While the spacing between the sliding surfaces is of the same order of magnitude as various AFM based fundamental studies on friction, the sliding speed is nearly six orders of magnitude larger, allowing a unique set-up for a systematic study of nanoscale wear at high sliding speeds. In a hard disk drive, the physical contact between the head and the disk leads to friction, wear, and degradation of the head overcoat material (typically diamond like carbon). In this work, strain gauge based friction measurements are performed; the friction coefficient as well as the adhering shear strength at the head-disk interface is extracted; and an experimental set-up for studying friction between high speed sliding surfaces is exemplified.

  7. Wear of ultra-high molecular weight polyethylene against damaged and undamaged stainless steel and diamond-like carbon-coated counterfaces.

    PubMed

    Firkins, P; Hailey, J L; Fisher, J; Lettington, A H; Butter, R

    1998-10-01

    The wear of ultra-high molecular weight polyethylene (UHMWPE) in artificial joints and the resulting wear debris-induced osteolysis remains a major clinical concern in the orthopaedic sector. Third-body damage of metallic femoral heads is often cited as a cause of accelerated polyethylene wear, and the use of ceramic femoral heads in the hip is gaining increasing favour. In the knee prostheses and for smaller diameter femoral heads, the application of hard surface coatings, such as diamond-like carbon, is receiving considerable attention. However, to date, there has been little or no investigation of the tribology of these coatings in simulated biological environments. In this study, diamond-like carbon (DLC) has been compared to stainless steel in its undamaged form and following simulated third-body damage. The wear of UHMWPE was found to be similar when sliding against undamaged DLC and stainless steel counterfaces. DLC was found to be much more damage resistant than DLC. Under test conditions that simulate third-body damage to the femoral head, the wear of UHMWPE was seven times lower against DLC than against stainless steel (P < 0.05). The study shows DLC has considerable potential as a femoral bearing surface in artificial joints.

  8. Understanding Friction and Wear Mechanisms of High-Purity Titanium against Steel in Liquid Nitrogen Temperature

    NASA Astrophysics Data System (ADS)

    Basu, Bikramjit; Sarkar, J.; Mishra, Ravi

    2009-02-01

    Although the friction and wear properties of several metallic alloys in unlubricated conditions are widely investigated, such understanding for high-purity metals in cryogenic environment is rather limited. This article reports the tribological properties of high-purity α-titanium ( α-Ti), prepared by cold rolling and recrystallization annealing, under liquid nitrogen (LN2) and room temperature (RT) environments against steel (bearing grade: SAE 52100) at varying loads (up to 15 N) and sliding speeds (0.6 to 4.19 m/s). It has been found that the steady-state coefficient of friction (COF) of titanium under LN2 environment (˜0.27 to 0.33) is lower than that at RT COF (˜0.33 to 0.58) irrespective of sliding speed. For cryogenic sliding conditions, the COF decreased steadily with sliding speed to a mean value of about 0.28 and no appreciable variation in COF is noticed for sliding speed of more than 1.5 m/s. The wear rate under both environment conditions was of the order of 10-3 mm3 N-1 m-1 irrespective of variation in operating parameters, but the RT wear rate was found to be higher compared to the LN2 case. Overall, the experimental results demonstrate improved tribological properties of high-purity titanium at LN2 temperature compared to the RT. Flow localization at tribological interfaces because of the large strain rate and subsequent damage accumulation at the titanium test piece are some of the attributes of the wear of Ti at LN2 temperature. In addition, the galling of titanium was also observed to occur under large contact stress and sliding speed conditions.

  9. Friction and wear properties of high-velocity oxygen fuel sprayed WC-17Co coating under rotational fretting conditions

    NASA Astrophysics Data System (ADS)

    Luo, Jun; Cai, Zhenbing; Mo, Jiliang; Peng, Jinfang; Zhu, Minhao

    2016-05-01

    Rotational fretting which exist in many engineering applications has incurred enormous economic loss. Thus, accessible methods are urgently needed to alleviate or eliminate damage by rotational fretting. Surface engineering is an effective approach that is successfully adopted to enhance the ability of components to resist the fretting damage. In this paper, using a high-velocity oxygen fuel sprayed (HVOF) technique WC-17Co coating is deposited on an LZ50 steel surface to study its properties through Vickers hardness testing, scanning electric microscope (SEM), energy dispersive X-ray spectroscopy (EDX), and X-ray diffractrometry (XRD). Rotational fretting wear tests are conducted under normal load varied from 10 N to 50 N, and angular displacement amplitudes vary from 0.125° to 1°. Wear scars are examined using SEM, EDX, optical microscopy (OM), and surface topography. The experimental results reveal that the WC-17Co coating adjusted the boundary between the partial slip regime (PSR) and the slip regime (SR) to the direction of smaller amplitude displacement. As a result, the coefficients of friction are consistently lower than the substrate's coefficients of friction both in the PSR and SR. The damage to the coating in the PSR is very slight. In the SR, the coating exhibits higher debris removal efficiency and load-carrying capacity. The bulge is not found for the coating due to the coating's higher hardness to restrain plastic flow. This research could provide experimental bases for promoting industrial application of WC-17Co coating in prevention of rotational fretting wear.

  10. Measurements of elastohydrodynamic film thickness, wear and tempering behavior of high pressure oxygen turbopump bearings

    NASA Technical Reports Server (NTRS)

    Dufrane, K. F.; Merriman, T. L.; Kannel, J. W.; Stockwell, R. D.; Hauser, D.; Vanecho, J. A.

    1984-01-01

    The reusable design of the Space Shuttle requires a target life of 7.5 hours for the turbopumps of the Space Shuttle main engine (SSME). This large increase from the few hundred seconds required in single-use rockets has caused various problems with the bearings of the turbopumps. The berings of the high pressure oxygen turbopump (HPOTP) were of particular concern because of wear, spalling, and cage failures at service time well below the required 7.5 hours. Lubrication and wear data were developed for the bearings. Since the HPOTP bearings operate in liquid oxygen, conventional liquid lubricants cannot be applied. Therefore, solid lubricant coatings and lubricant transfer from the polytetrafluorethylene (FTFE) cage were the primary lubrication approaches for the bearings. Measurements were made using liquid nitrogen in a rolling disk machine to determine whether usable elastohydrodynamic films could be generated to assist in the bearing lubrication.

  11. Ultra-high molecular weight polyethylene wear particle effects on bioactivity

    NASA Astrophysics Data System (ADS)

    Fang, Hsu-Wei

    Ultra-high molecular weight polyethylene (UHMWPE) wear particles have been recognized as one of the major causes of aseptic loosening in total joint replacements. Macrophage phagocytosis of wear particles induces human biological/physiological responses which eventually lead to bone resorption and osteolysis. However, the dependence of these reactions on the size and shape of the particles has not been elucidated and is not understood. The goal of this study is to develop a technique for producing UHMWPE particles with specified sizes and shapes so as to be able to study the effects of different UHMWPE particles on bioactivity. We applied surface texturing techniques to generate UHMWPE particles and air pouch animal tests to study the biological responses induced by UHMWPE particles. The thesis describes a procedure for generating narrowly distributed UHMWPE particles with controlled size and shape through surface texturing by microfabrication. The textured surface is used to rub against the polymer pins to produce wear particles in water. The surface texture produces narrowly distributed elongated particles or equiaxed particles by design. Experimental results show that the cutting-edge length of the surface features is proportional to the particle length. A larger penetration depth, larger normal load, and smaller sliding speed lead to a smaller aspect ratio of the particle. With this technique, we have been able to generate UHMWPE wear particles with different size and shape within phagocytosable and non-phagocytosable ranges for biological response studies. A mathematical model to predict the dimensions of generated UHMWPE particles has been developed. A correlation model based on the empirical results is also presented. The models can be used to design the dimensions of the surface textures and the operating conditions of the wear tests for generation of the particle population with specified size and shape. Murine air pouch animal tests have been used to test

  12. Practical experience with a high Dk lotrafilcon A fluorosilicone hydrogel extended wear contact lens in Spain.

    PubMed

    Montero Iruzubieta, J; Nebot Ripoll, J R; Chiva, J; Fernández, O E; Rubio Alvarez, J J; Delgado, F; Villa, C; Traverso, L M

    2001-01-01

    Several research studies on high Dk soft contact lens materials have been published, but little has been reported from practical clinical experience with these new materials. This study reports in-practice clinical experience with the lotrafilcon A fluorosilicone hydrogel material from a 6-month study in Spain. Eighty-five patients were dispensed lotrafilcon A lenses (Focuse NIGHT & DAY [CIBA Vision Corporation]) for monthly replacement by 13 investigators from eight practices. The recommended wear schedule was daily wear for the first week and then up to 6-night extended wear through the first month and up to 30-night extended wear through 6 months. Follow-up visits were at 1 week, 1 month, 3 months, and 6 months. Clinical and patient subjective data were collected at each visit. Among patients who continued in the study at each visit, Snellen visual acuity (VA) of 20/25 or better was achieved by at least 96% of all eyes at all visits; lens surfaces assessments for front surface deposits, front surface wetting, and back surface debris averaged less than grade 1 (0-4 scale) for all lenses at all visits; biomicroscopy grades averaged well below grade 1 (0-4 scale) for all eyes at all visits; acceptable or optimal fit was assessed for 97% or more of all lenses at all visits. These patients rated the average overall comfort, vision, and handling above 9 (0-10 scale) at 6 months and 98% reported satisfaction with the lenses at 6 months. Eighty-two percent of patients dispensed completed the study. Seven patients were discontinued because of fit, and seven were discontinued because of positive biomicroscopy signs. The lotrafilcon A lens performed well clinically and it was accepted well by patients, with most practitioners recommending and most patients wearing it for up to 30 nights extended wear. Practitioners should be attentive to fit and discomfort complaints at dispensing and follow-up and may want to recommend lubricating or rewetting drops for those patients

  13. Sliding friction and wear up to 600 C of high speed steels and silicon nitrides for gas turbine bearings

    NASA Astrophysics Data System (ADS)

    Childs, T. H. C.; Mimaroglu, A.

    1993-04-01

    The sliding friction coefficients and specific wear rates of a variety of differently processed high speed steels and silicon nitrides were measured in both dry and boundary lubricated conditions at temperatures from 20 to 600 C or 200 C, respectively. It is concluded that, in dry sliding, the friction and wear of the silicone nitride and high speed steel combinations was dominated by the formation of compacted debris films in the contact areas at all temperatures between room temperature and 600 C. The specific wear rates were remarkably similar up to 400 C, although the friction coefficient of the silicon nitride on silicon nitride was higher than that of the high speed steel on high speed steel. In the temperature range of 400-600 C materials exhibited certain differences. The silicon nitride films on the high speed steel discs were a good sliding combination because protective layers from the disc inhibited the wear of the pin at temperatures above 300 C.

  14. Microstructure and Abrasive-wear Behavior Under High Temperature of Laser Clad Ni-based WC Ceramic Coating

    NASA Astrophysics Data System (ADS)

    Wang, X. H.; Liu, A. M.

    The laser cladding is used on the surface of 4Cr14Ni14NW2Mo heat-resisting steel, Ni-based WC coating can be formed. Observing and analying the microstructure, measuring the hardness of the cladding layer cross section, checking the abrsrssive- wear under high temperature in different temperature. The results showed that the microstructure of Ni21+20%Wc+0.5%CeO2 cladding layer is small and it presents the best abrasive-wear behavior under high temperature in these investigated coatings. Wear mechanism of the laser cladding layer changes with temperature changes.

  15. Structural ceramics for high temperature applications

    SciTech Connect

    Dapkunas, S.J.

    1995-12-31

    Structural ceramics, primarily silicon nitride and silicon carbide, are recognized as offering significant performance benefits in heat engine and other high temperature applications. These benefits accrue from superior high temperature mechanical properties, corrosion and wear resistance and lower density. Improved processing and understanding of the phenomena determining properties and performance have made these materials viable replacements for metallic components in some applications. Cost barriers hinder more widespread use.

  16. Cryogenic Treatment of Production Components in High-Wear Rate Wells

    SciTech Connect

    Milliken, M.

    2002-04-29

    Deep Cryogenic Tempering (DCT) is a specialized process whereby the molecular structure of a material is ''re-trained'' through cooling to -300 F and then heating to +175-1100 F. Cryocon, Inc. (hereafter referred to as Cryocon) and RMOTC entered an agreement to test the process on oilfield production components, including rod pumps, rods, couplings, and tubing. Three Shannon Formation wells were selected (TD about 500 ft) based on their proclivity for high component wear rates. Phase 1 of the test involved operation for a nominal 120 calendar day period with standard, non-treated components. In Phase 2, treated components were installed and operated for another nominal 120 calendar day period. Different cryogenic treatment profiles were used for components in each well. Rod pumps (two treated and one untreated) were not changed between test phases. One well was operated in pumped-off condition, resulting in abnormal wear and disqualification from the test. Testing shows that cryogenic treatment reduced wear of rods, couplers, and pump barrels. Testing of production tubing produced mixed results.

  17. Superomniphobic Surfaces for Military Applications: Nano- and Micro-Fabrication Methods. Chapter 2: Investigation of Wear for Superhydrophobic Surfaces and Development of New Coatings

    DTIC Science & Technology

    2011-01-01

    Canada Superomniphobic Surfaces for Military Applications: Nano - and Micro -Fabrication Methods Chapter 2: Investigation of Wear for...Military Applications: Nano - and Micro -Fabrication Methods Chapter 2: Investigation of Wear for Superhydrophobic Surfaces and Development of New...blank. DRDC Atlantic CR 2010-315 iii Executive summary Superomniphobic Surfaces for Military Applications: Nano - and Micro

  18. Brush Seals for Cryogenic Applications: Performance, Stage Effects, and Preliminary Wear Results in LN2 and LH2

    NASA Technical Reports Server (NTRS)

    Proctor, Margaret P.; Walker, James F.; Perkins, H. Douglas; Hoopes, Joan F.; Williamson, G. Scott

    1996-01-01

    Brush seals are compliant contacting seals and have significantly lower leakage than labyrinth seals in gas turbine applications. Their long life and low leakage make them candidates for use in rocket engine turbopumps. Brush seals, 50.8 mm (2 in.) in diameter with a nominal 127-micron (0.005-in.) radial interference, were tested in liquid nitrogen (LN2) and liquid hydrogen (LH2) at shaft speeds up to 35,000 and 65,000 rpm, respectively, and at pressure drops up to 1.21 MPa (175 psid) per brush. A labyrinth seal was also tested in liquid nitrogen to provide a baseline. The LN2 leakage rate of a single brush seal with an initial radial shaft interference of 127 micron (0.005 in.) measured one-half to one-third the leakage rate of a 12-tooth labyrinth seal with a radial clearance of 127 micron (0.005 in.). Two brushes spaced 7.21 micron (0.248 in.) apart leaked about one-half as much as a single brush, and two brushes tightly packed together leaked about three-fourths as much as a single brush. The maximum measured groove depth on the Inconel 718 rotor with a surface finish of 0.81 micron (32 microinch) was 25 micron (0.0010 in.) after 4.3 hr of shaft rotation in liquid nitrogen. The Haynes-25 bristles wore approximately 25 to 76 micron (0.001 to 0.003 in.) under the same conditions. Wear results in liquid hydrogen were significantly different. In liquid hydrogen the rotor did not wear, but the bristle material transferred onto the rotor and the initial 127 micron (0.005 in.) radial interference was consumed. Relatively high leakage rates were measured in liquid hydrogen. More testing is required to verify the leakage performance, to validate and calibrate analysis techniques, and to determine the wear mechanisms. Performance, staging effects, and preliminary wear results are presented.

  19. A rolling-gliding wear simulator for the investigation of tribological material pairings for application in total knee arthroplasty.

    PubMed

    Richter, Berna I; Ostermeier, Sven; Turger, Anke; Denkena, Berend; Hurschler, Christof

    2010-06-15

    Material wear testing is an important technique in the development and evaluation of materials for use in implant for total knee arthroplasty. Since a knee joint induces a complex rolling-gliding movement, standardised material wear testing devices such as Pin-on-Disc or Ring-on-Disc testers are suitable to only a limited extent because they generate pure gliding motion only. A rolling-gliding wear simulator was thus designed, constructed and implemented, which simulates and reproduces the rolling-gliding movement and loading of the knee joint on specimens of simplified geometry. The technical concept was to run a base-plate, representing the tibia plateau, against a pivoted cylindrical counter-body, representing one femur condyle under an axial load. A rolling movement occurs as a result of the friction and pure gliding is induced by limiting the rotation of the cylindrical counter-body. The set up also enables simplified specimens handling and removal for gravimetrical wear measurements. Long-term wear tests and gravimetrical wear measurements were carried out on the well known material pairings: cobalt chrome-polyethylene, ceramic-polyethylene and ceramic-ceramic, over three million motion cycles to allow material comparisons to be made. The observed differences in wear rates between cobalt-chrome on polyethylene and ceramic on polyethylene pairings were similar to the differences of published data for existing material-pairings. Test results on ceramic-ceramic pairings of different frontal-plane geometry and surface roughness displayed low wear rates and no fracture failures. The presented set up is able to simulate the rolling-gliding movement of the knee joint, is easy to use, and requires a minimum of user intervention or monitoring. It is suitable for long-term testing, and therefore a useful tool for the investigation of new and promising materials which are of interest for application in knee joint replacement implants.

  20. A rolling-gliding wear simulator for the investigation of tribological material pairings for application in total knee arthroplasty

    PubMed Central

    2010-01-01

    Background Material wear testing is an important technique in the development and evaluation of materials for use in implant for total knee arthroplasty. Since a knee joint induces a complex rolling-gliding movement, standardised material wear testing devices such as Pin-on-Disc or Ring-on-Disc testers are suitable to only a limited extent because they generate pure gliding motion only. Methods A rolling-gliding wear simulator was thus designed, constructed and implemented, which simulates and reproduces the rolling-gliding movement and loading of the knee joint on specimens of simplified geometry. The technical concept was to run a base-plate, representing the tibia plateau, against a pivoted cylindrical counter-body, representing one femur condyle under an axial load. A rolling movement occurs as a result of the friction and pure gliding is induced by limiting the rotation of the cylindrical counter-body. The set up also enables simplified specimens handling and removal for gravimetrical wear measurements. Long-term wear tests and gravimetrical wear measurements were carried out on the well known material pairings: cobalt chrome-polyethylene, ceramic-polyethylene and ceramic-ceramic, over three million motion cycles to allow material comparisons to be made. Results The observed differences in wear rates between cobalt-chrome on polyethylene and ceramic on polyethylene pairings were similar to the differences of published data for existing material-pairings. Test results on ceramic-ceramic pairings of different frontal-plane geometry and surface roughness displayed low wear rates and no fracture failures. Conclusions The presented set up is able to simulate the rolling-gliding movement of the knee joint, is easy to use, and requires a minimum of user intervention or monitoring. It is suitable for long-term testing, and therefore a useful tool for the investigation of new and promising materials which are of interest for application in knee joint replacement

  1. Perspectives from the Wearable Electronics and Applications Research (WEAR) Lab, NASA Johnson Space Center

    NASA Technical Reports Server (NTRS)

    Moses, Haifa R.

    2017-01-01

    As NASA moves beyond exploring low earth orbit and into deep space exploration, increased communication delays between astronauts and earth drive a need for crew to become more autonomous (earth-independent). Currently crew on board the International Space Station (ISS) have limited insight into specific vehicle system performance because of the dependency on monitoring and real-time communication with Mission Control. Wearable technology provides a method to bridge the gap between the human (astronaut) and the system (spacecraft) by providing mutual monitoring between the two. For example, vehicle or environmental information can be delivered to astronauts through on-body devices and in return wearables provide data to the spacecraft regarding crew health, location, etc. The Wearable Electronics and Applications Research (WEAR) Lab at the NASA Johnson Space Center utilizes a collaborative approach between engineering and human factors to investigate the use of wearables for spaceflight. Zero and partial gravity environments present unique challenges to wearables that require collaborative, user-centered, and iterative approaches to the problems. Examples of the WEAR Lab's recent wearable projects for spaceflight will be discussed.

  2. A hybrid floating brush seal (HFBS) for improved sealing and wear performance in turbomachinery applications

    NASA Astrophysics Data System (ADS)

    Lattime, Scott Byran

    A conceptually new type of seal has been developed for gas turbine applications which dramatically reduces wear and leakage associated with current labyrinth and brush seal technologies. The Hybrid Floating Brush Seal (HFBS) combines brush seal and film riding face seal technologies to create a hybrid seal that allows both axial and radial excursions of the sealed shaft, while simultaneously eliminating interface surface speeds (friction and heat) between the rotor and the brush material that characterize standard brush seal technology. A simple test rig was designed to evaluate feasibility of the HFBS under relatively low pressures and rotational speeds (50psig, 5krpm). A second test stand was created to study the effects of centrifugal force on bristle deflection. A third test facility was constructed for prototype development and extensive room temperature testing at moderate pressures and fairly high rotational speeds (100psig, 40krpm). This test rig also allowed the evaluation of the HFBS during axial movement of a rotating shaft. An analytical model to predict the effects of centrifugal force on the bristles of a rotating brush seal was developed. Room temperature analysis of the HFBS proved successful for relatively high operating rotational velocities at moderate pressures with very acceptable leakage rates for gas turbine engines. Brush seals were able to track rotor speeds up to 24krpm while maintaining sealing integrity. The HFBS's ability to function under axial shaft displacement and synchronous dynamic radial loading was also proven successful. Hydrodynamic performance of the face seal was proven to provide adequate stiffness and load carrying capacity to keep the brush seal from contacting the face seal at pressure drops across the brush of up to 100psi. Leakage performance over standard brush seal and labyrinth technology was quite dramatic. The HFBS showed its sealing advantage using much higher radial interference between the rotor and the bristle

  3. Voltage assisted asymmetric nanoscale wear on ultra-smooth diamond like carbon thin films at high sliding speeds.

    PubMed

    Rajauria, Sukumar; Schreck, Erhard; Marchon, Bruno

    2016-05-06

    The understanding of tribo- and electro-chemical phenomenons on the molecular level at a sliding interface is a field of growing interest. Fundamental chemical and physical insights of sliding surfaces are crucial for understanding wear at an interface, particularly for nano or micro scale devices operating at high sliding speeds. A complete investigation of the electrochemical effects on high sliding speed interfaces requires a precise monitoring of both the associated wear and surface chemical reactions at the interface. Here, we demonstrate that head-disk interface inside a commercial magnetic storage hard disk drive provides a unique system for such studies. The results obtained shows that the voltage assisted electrochemical wear lead to asymmetric wear on either side of sliding interface.

  4. Voltage assisted asymmetric nanoscale wear on ultra-smooth diamond like carbon thin films at high sliding speeds

    NASA Astrophysics Data System (ADS)

    Rajauria, Sukumar; Schreck, Erhard; Marchon, Bruno

    2016-05-01

    The understanding of tribo- and electro-chemical phenomenons on the molecular level at a sliding interface is a field of growing interest. Fundamental chemical and physical insights of sliding surfaces are crucial for understanding wear at an interface, particularly for nano or micro scale devices operating at high sliding speeds. A complete investigation of the electrochemical effects on high sliding speed interfaces requires a precise monitoring of both the associated wear and surface chemical reactions at the interface. Here, we demonstrate that head-disk interface inside a commercial magnetic storage hard disk drive provides a unique system for such studies. The results obtained shows that the voltage assisted electrochemical wear lead to asymmetric wear on either side of sliding interface.

  5. Voltage assisted asymmetric nanoscale wear on ultra-smooth diamond like carbon thin films at high sliding speeds

    PubMed Central

    Rajauria, Sukumar; Schreck, Erhard; Marchon, Bruno

    2016-01-01

    The understanding of tribo- and electro-chemical phenomenons on the molecular level at a sliding interface is a field of growing interest. Fundamental chemical and physical insights of sliding surfaces are crucial for understanding wear at an interface, particularly for nano or micro scale devices operating at high sliding speeds. A complete investigation of the electrochemical effects on high sliding speed interfaces requires a precise monitoring of both the associated wear and surface chemical reactions at the interface. Here, we demonstrate that head-disk interface inside a commercial magnetic storage hard disk drive provides a unique system for such studies. The results obtained shows that the voltage assisted electrochemical wear lead to asymmetric wear on either side of sliding interface. PMID:27150446

  6. Friction and oxidative wear of 440C ball bearing steels under high load and extreme bulk temperatures

    NASA Technical Reports Server (NTRS)

    Chaudhuri, Dilip K.; Slifka, Andrew J.; Siegwarth, James D.

    1993-01-01

    Unlubricated sliding friction and wear of 440C steels in an oxygen environment have been studied under a variety of load, speed, and temperature ranging from approximately -185 to 675 deg C. A specially designed test apparatus with a ball-on-flat geometry has been used for this purpose. The observed dependencies of the initial coefficient of friction, the average dynamic coefficient of friction, and the wear rate on load, speed, and test temperatures have been examined from the standpoint of existing theories of friction and wear. High contact temperatures are generated during the sliding friction, causing rapid oxidation and localized surface melting. A combination of fatigue, delamination, and loss of hardness due to tempering of the martensitic structure is responsible for the high wear rate observed and the coefficient of friction.

  7. Friction and oxidative wear of 440C ball bearing steels under high load and extreme bulk temperatures

    NASA Technical Reports Server (NTRS)

    Chaudhuri, Dilip K.; Slifka, Andrew J.; Siegwarth, James D.

    1993-01-01

    Unlubricated sliding friction and wear of 440C steels in an oxygen environment have been studied under a variety of load, speed, and temperature ranging from approximately -185 to 675 deg C. A specially designed test apparatus with a ball-on-flat geometry has been used for this purpose. The observed dependencies of the initial coefficient of friction, the average dynamic coefficient of friction, and the wear rate on load, speed, and test temperatures have been examined from the standpoint of existing theories of friction and wear. High contact temperatures are generated during the sliding friction, causing rapid oxidation and localized surface melting. A combination of fatigue, delamination, and loss of hardness due to tempering of the martensitic structure is responsible for the high wear rate observed and the coefficient of friction.

  8. Microstructure and its effect on toughness and wear resistance of laser surface melted and post heat treated high speed steel

    NASA Astrophysics Data System (ADS)

    Åhman, Leif

    1984-10-01

    High speed steel hacksaw blade blanks were laser surface melted and rapidly solidified along one edge. The laser melting resulted in complete carbide dissolution. By subsequent machining and heat treatments saw teeth were manufactured with a refined internal structure of the edges and corners. The structure was fully martensitic with a uniform and dense dispersion of small primary carbides. Sawing tests in quenched and tempered steel showed that blade life was somewhat improved, as compared to conventionally heat treated blades. The increased wear resistance is believed to be due to improved toughness along with high hardness caused by the refined carbide structure. Sawing tests in austenitic stainless steel did not give any significant improvement in performance. The effect of the altered microstructure on performance is likely to be more or less pronounced depending on application, tool and work material.

  9. The effect of plasma nitriding and post oxidation on fretting wear behaviour of a high strength alloy steel

    NASA Astrophysics Data System (ADS)

    Prakash, N. Arun; Bennett, C. J.

    2017-05-01

    The fretting wear performance of the non-nitrided, nitrided and nitrided-post oxidized high strength alloy steel, W460 were investigated in the gross slip regime at ambient condition. Fretting wear tests were performed with an applied normal load of 250 and 650 N at a displacement amplitude of 100 μm using a cylinder-on-flat configuration. X-ray analysis (XRD) revealed the formation of the iron-nitrided Fe3N and Fe4N during plasma nitriding and iron oxide phases of hematite (Fe2O3) and magnetite (Fe3O4) during post-oxidation of the cylindrical steel samples. The steady state tangential force coefficient decreases when the nitrided and post-oxidized samples were fretted against the non-nitrided steel material when compared to the non-nitrided steel contact pair. The steady state tangential force coefficient decreased with an increase in applied normal load across all of the fretting conditions. The total dissipated energy and the total wear volume increased with an increase in applied normal load with total wear volume of the non-nitrided vs nitrided and non-nitrided vs nitrided post-oxidized sample pairs, showing a reduction in the wear volume of approximately 50% compared to the non-nitrided vs non-nitrided combination under the fretting conditions examined. The worn surface morphology of the fretted samples examined using a scanning electron microscope showed the presence of loose wear debris in the wear track, fragmented wear debris, delamination cracks, delamination with large discontinuities, plate-like wear debris, oxide patches and formation of large cavities.

  10. Y-TZP zirconia run against highly crosslinked UHMWPE tibial inserts: knee simulator wear and phase-transformation studies.

    PubMed

    Tsukamoto, Riichiro; Williams, Paul A; Clarke, Ian C; Pezzotti, Giuseppe; Shoji, Hiromu; Akagi, Masao; Yamamoto, Kengo

    2008-07-01

    Zirconia (ZrO(2)) ceramics combined with highly cross-linked polyethylene appears to be a promising approach to minimize wear in artificial knee joints. The wear performance of yttria-stabilized zirconia (YZr) femoral condyles on 7-Mrad tibial inserts was compared in a knee simulator to CoCr bearing on 3.5-Mrad inserts. The knee design was the Bi-Surface type with a 9-year clinical history in Japan (JMM, Japan). A displacement-controlled knee simulator was used with kinematics that included 20 degrees flexion, +/-5 degrees rotation, and 6 mm anterior/posterior translation. Lubricant was alpha-calf serum, test duration was 10 million cycles (10 Mc), and wear was measured by weight-loss techniques. The wear zones were studied by laser interferometry, scanning electron microscopy, and Raman microprobe spectroscopy. At 10 Mc the wear rates of the CoCr controls averaged 4.5 mm(3)/Mc. This was within 7% of the prior estimate at 5-Mc duration and comparable to Bi-Surface wear data from another laboratory. The CoCr condyles increased in roughness (R(a)) from <50 nm to average R(a) = 250 nm due to linear scratching. The ceramic condyles remained pristine throughout the wear study (R(a) <7 nm). With the YZr/7-Mrad combination, the weight change had a positive slope over at 10 Mc, which meant that the actual polyethylene wear was unmeasurable. Microscopic examinations at 10 Mc showed that the zirconia surfaces were intact and there was no detectable change from tetragonal to monoclinic phase. Our laboratory knee wear simulation appeared very supportive of the 9-year YZr/PE clinical results with Bi-Surface total knee replacements in Japan. 2007 Wiley Periodicals, Inc.

  11. Polymer wear and its control

    SciTech Connect

    Lee, L.H.

    1985-01-01

    Recent advances in polymer (P) tribology are discussed in reviews and reports based on contributions to a symposium held by the Division of Polymeric Materials Science and Engineering of the Americal Chemical Society in St. Louis in spring 1984. Topics examined are mechanisms of P wear, controls of P wear, the tribological behavior of Ps, wear of biomaterials and P composites, characterization and measurements of P wear, and degradation and wear of polymeric films and filaments. Consideration is given to the fracture and surface energetics of P wear, fatigue-abrasive mechanisms of P wear, plasma modification of P surfaces, the wear characteristics of articular cartilage, the role of fillers in the wear of high-density polyethylene, the tribology of fiber-reinforced polyimides sliding against steel and Si3N4, laboratory and in-service wear tests of Ps, and the effect of degree of crystallinity on wear of poly(ethylene terephthalate).

  12. Wear of Spur Gears Having a Dithering Motion and Lubricated with a Perfluorinated Polyether Grease

    NASA Technical Reports Server (NTRS)

    Krantz, Timothy; Oswald, Fred; Handschuh, Robert

    2007-01-01

    Gear contact surface wear is one of the important failure modes for gear systems. Dedicated experiments are required to enable precise evaluations of gear wear for a particular application. The application of interest for this study required evaluation of wear of gears lubricated with a grade 2 perfluorinated polyether grease and having a dithering (rotation reversal) motion. Experiments were conducted using spur gears made from AISI 9310 steel. Wear was measured using a profilometer at test intervals encompassing 10,000 to 80,000 cycles of dithering motion. The test load level was 1.1 GPa maximum Hertz contact stress at the pitch-line. The trend of total wear as a function of test cycles was linear, and the wear depth rate was approximately 1.2 nm maximum wear depth per gear dithering cycle. The observed wear rate was about 600 times greater than the wear rate for the same gears operated at high speed and lubricated with oil.

  13. Effects of Alloying Elements on Microstructure, Hardness, Wear Resistance, and Surface Roughness of Centrifugally Cast High-Speed Steel Rolls

    NASA Astrophysics Data System (ADS)

    Ha, Dae Jin; Sung, Hyo Kyung; Park, Joon Wook; Lee, Sunghak

    2009-11-01

    A study was made of the effects of carbon, tungsten, molybdenum, and vanadium on the wear resistance and surface roughness of five high-speed steel (HSS) rolls manufactured by the centrifugal casting method. High-temperature wear tests were conducted on these rolls to experimentally simulate the wear process during hot rolling. The HSS rolls contained a large amount (up to 25 vol pct) of carbides, such as MC, M2C, and M7C3 carbides formed in the tempered martensite matrix. The matrix consisted mainly of tempered lath martensite when the carbon content in the matrix was small, and contained a considerable amount of tempered plate martensite when the carbon content increased. The high-temperature wear test results indicated that the wear resistance and surface roughness of the rolls were enhanced when the amount of hard MC carbides formed inside solidification cells increased and their distribution was homogeneous. The best wear resistance and surface roughness were obtained from a roll in which a large amount of MC carbides were homogeneously distributed in the tempered lath martensite matrix. The appropriate contents of the carbon equivalent, tungsten equivalent, and vanadium were 2.0 to 2.3, 9 to 10, and 5 to 6 pct, respectively.

  14. Microstructure and Wear Behavior of High-Cr WCI Matrix Surface Composite Reinforced with Cemented Carbide Rods

    NASA Astrophysics Data System (ADS)

    Hou, Shuzeng; Bao, Chonggao; Zhang, Zhiyun; Bai, Yaping

    2013-07-01

    The present article reports a new superior wear resistance surface composite prepared by a vacuum evaporative pattern casting-in process. This surface composite was constructed with reinforcing cemented carbide rod (CCR) array within high-Cr white cast iron (WCI) matrix. Three reaction zones that formed around the CCRs were characterized and established the good metallurgical bonding between CCRs and matrix. In addition, some compound carbide containing Fe, Cr, W, and Co elements were formed in the reaction zones, owing to the partial dissolution of the CCRs and the resulting interdiffusion of elements such as W, Co, C, Fe, and Cr. The wear behavior of the composite was evaluated and compared with unreinforced high-Cr WCI by means of a three-body abrasive wear tester. The results showed that the wear resistance of the composite was significantly higher than that of the unreinforced high-Cr WCI. The exciting wear resistance can be ascribed to protective effect introduced by the CCRs during wear process and the good metallurgical bonding between CCRs and matrix.

  15. Characterization of the resistance of pyrolytic carbon to abrasive wear.

    PubMed

    Vitale, E; Giusti, P

    1995-12-01

    Si-alloyed pyrolitic carbon (PyC) is currently employed in many biomedical devices, due to its fairly good biological compatibility and non biodegradeability. For prosthetic heart valve applications, required to operate safely for many years, the resistance to abrasive wear is one of the limiting factors which must be accurately evaluated. The present study reports on abrasive wear testing of Ti/PyC and PyC/PyC sliding couples. For both couples it was found that the wear behaviour can be shifted from a low wear regime, characterised by very small wear rates and reduced scatter, to a high wear regime, characterised by high wear rates and high scatter, due to the presence of particle contamination coming from the environment and/or from the specimen polishing process. Actual biomedical devices, particularly heart valves, should not experience the high wear regime, due to the absence of any hard particle contamination source. The wear observed in these items is in fact minimal and may depend on mechanisms other than abrasive wear. In these conditions the experimental evaluation of the wear behaviour should definetely be performed by tests on actual devices.

  16. Wear behaviour of epoxy resin filled with hard powders

    NASA Astrophysics Data System (ADS)

    Formisano, A.; Boccarusso, L.; Minutolo, F. Capece; Carrino, L.; Durante, M.; Langella, A.

    2016-10-01

    The development of high performance materials based on epoxy resin finds a growing number of applications in which high wear resistance is required. One major drawback in many of these applications is the relatively poor wear resistance of the epoxy resin. Therefore, in order to investigate on the possibility of increasing wear resistance of thermoset polymers filled with hard powders, sliding tests are carried out by means of a pin on disc apparatus. In particular, composite resins, constituted by an epoxy resin filled with different contents and sizes of Silicon Carbide powder, are analyzed; the wear resistance, in terms of volume loss, is measured for different abrasive counterfaces and loads.

  17. Predominant factor determining wear properties of β-type and (α+β)-type titanium alloys in metal-to-metal contact for biomedical applications.

    PubMed

    Lee, Yoon-Seok; Niinomi, Mitsuo; Nakai, Masaaki; Narita, Kengo; Cho, Ken

    2015-01-01

    The predominant factor determining the wear properties of a new titanium alloy, Ti-29Nb-13Ta-4.6Zr (TNTZ) and a conventional titanium alloy, Ti-6Al-4V extra-low interstitial (Ti64) was investigated for TNTZ and Ti64 combinations in metal-to-metal contacting bio-implant applications. The worn surfaces, wear debris, and subsurface damages were analyzed using a scanning electron microscopy combined with energy-dispersive spectroscopy and electron-back scattered diffraction analysis. The volume loss of TNTZ is found to be larger than that of Ti64, regardless of the mating material. The wear track of TNTZ exhibits the galled regions and severe plastic deformation with large flake-like debris, indicative of delamination wear, which strongly suggests the occurrence of adhesive wear. Whereas, the wear track of Ti64 have a large number of regular grooves and microcuttings with cutting chip-like wear debris and microfragmentation of fine oxide debris, indicative of abrasive wear combined with oxidative wear. This difference in the wear type is caused by severe and mild subsurface deformations of TNTZ and Ti64, respectively. The lower resistance to plastic shearing for TNTZ compared to that of Ti64 induces delamination, resulting in a higher wear rate.

  18. Wear in conventional and highly cross-linked polyethylene cups: a 5-year follow-up study.

    PubMed

    Olyslaegers, Christophe; Defoort, Koen; Simon, Jean-Pierre; Vandenberghe, Luc

    2008-06-01

    Highly cross-linked polyethylene (XLPE) has been introduced in total hip arthroplasty in an effort to reduce polyethylene wear and the associated periprosthetic osteolysis. Our aim was to demonstrate these reduced wear rates in a 2-dimensional head penetration model and to perform a clinical comparison of both groups using the Harris Hip Score (and SF-36 questionnaire). Sixty hips with a Trilogy XLPE liner (Zimmer) were matched and compared to a control group of 20 conventional Trilogy PE liners (Zimmer). No differences in clinical outcome were seen, but a statistically significant reduction in linear wear was observed in the XLPEgroup, after 5 years. It is clear that, because of the reduction and stabilization of free radicals in polyethylene, a reduction in annual wear can be achieved.

  19. Evaluation of anti-wear performance of PFPE-soluble additives under sliding contact in high vacuum

    SciTech Connect

    Masuko, M.; Takeshita, N.; Okabe, H.

    1995-07-01

    The anti-wear performances of perfluoropolyether (PEPE)-soluble additives were evaluated under vacuum using a vacuum four-ball tribometer with 440C stainless steel balls as test specimens. PEPE derivatives having the hydroxyl, carboxyl and phosphate groups at the end of the Type D-PEPE molecules were studied. The addition of either PEPE-soluble carboxylic acid or PEPE-soluble phosphates to the PEPE base oil remarkably reduced steady wear rates in a vacuum environment, whereas the addition of PEPE-soluble alcohol did not. Contrary to the performance in vacuum, an appreciable increase in wear rate was observed in the air atmosphere with all the types of additives used. The effect of moisture is studied in explaining the high wear rates obtained with the additives in the air environment. The mechanism of boundary lubrication with PEPE-soluble additives is discussed.

  20. Friction and wear behavior of ultra-high molecular weight polyethylene as a function of polymer crystallinity.

    PubMed

    Kanaga Karuppiah, K S; Bruck, Angela L; Sundararajan, Sriram; Wang, Jun; Lin, Zhiqun; Xu, Zhi-Hui; Li, Xiaodong

    2008-09-01

    In this study the friction, wear and surface mechanical behavior of medical-grade ultra-high molecular weight polyethylene (UHMWPE) (GUR 1050 resin) were evaluated as a function of polymer crystallinity. Crystallinity was controlled by heating UHMWPE to a temperature above its melting point and varying the hold time and cooling rates. The degree of crystallinity of the samples was evaluated using differential scanning calorimetry (DSC). A higher degree of crystallinity in the UHMWPE resulted in lower friction force and an increase in scratch resistance at the micro- and nanoscales. On the nanoscale, the lamellar structure appeared to affect the observed wear resistance. Reciprocating-wear tests performed using a microtribometer showed that an increase in crystallinity also resulted in lower wear depth and width. Nanoindentation experiments also showed an increase in hardness values with an increase in sample crystallinity.

  1. Solid Lubrication Fundamentals and Applications. Properties of Clean Surfaces: Adhesion, Friction, and Wear

    NASA Technical Reports Server (NTRS)

    Miyoshi, Kazuhisa

    1998-01-01

    This chapter presents the adhesion, friction, and wear behaviors of smooth, atomically clean surfaces of solid-solid couples, such as metal-ceramic couples, in a clean environment. Surface and bulk properties, which determine the adhesion, friction, and wear behaviors of solid-solid couples, are described. The primary emphasis is on the nature and character of the metal, especially its surface energy and ductility. Also, the mechanisms of friction and wear for clean, smooth surfaces are stated.

  2. High Wear Resistance of White Cast Iron Treated by Novel Process: Principle and Mechanism

    NASA Astrophysics Data System (ADS)

    Jia, Xiaoshuai; Zuo, Xunwei; Liu, Yu; Chen, Nailu; Rong, Yonghua

    2015-12-01

    Based on microstructure desired, a novel process is proposed to treat Fe-2.4C-12.0Cr (mass pct) white cast iron balls, that is, destabilizing heat treatment following multicycle quenching and sub-critical treatment (De-MQ-Sct) process, and such a complex process is simply performed by alternate water quenching and air cooling. For comparison, the white cast iron balls also were treated by conventional normalization (NOR) process and Oil-quenching process, respectively. The partitioning of carbon from martensite to retained austenite during De-MQ-Sct process promotes the interaction between carbide precipitation and martensitic transformation, while this interaction is a unique effect only produced by multicycle quenching linking destabilizing and sub-critical treatments, which leads to more and finer secondary carbides and more carbon-enriched austenite in De-MQ-Sct sample than those in NOR or Oil-quenching sample. The average hardness of 60 HRC and impact toughness of 12.6 J/cm2 are obtained in De-MQ-Sct white cast iron balls, which are much higher than those in NOR and Oil-quenching ones. The wear behaviours measured by pin-on-disk wear tests indicate that the weight loss of De-MQ-Sct sample is only about one third of the NOR sample and one half of the Oil-quenching sample. Microstructural characterization reveals that high wear resistance related to hardness and toughness of the De-MQ-Sct balls are mainly attributed to the considerable fine secondary carbides and stable carbon-enriched retained austenite.

  3. The creep and wear of highly cross-linked polyethylene: a three-year randomised, controlled trial using radiostereometric analysis.

    PubMed

    Glyn-Jones, S; McLardy-Smith, P; Gill, H S; Murray, D W

    2008-05-01

    The creep and wear behaviour of highly cross-linked polyethylene and standard polyethylene liners were examined in a prospective, double-blind randomised, controlled trial using radiostereometric analysis. We randomised 54 patients to receive hip replacements with either highly cross-linked polyethylene or standard liners and determined the three-dimensional penetration of the liners over three years. After three years the mean total penetration was 0.35 mm (SD 0.14) for the highly cross-linked polyethylene group and 0.45 mm (SD 0.19) for the standard group. The difference was statistically significant (p = 0.0184). From the pattern of penetration it was possible to discriminate creep from wear. Most (95%) of the creep occurred within six months of implantation and nearly all within the first year. There was no difference in the mean degree of creep between the two types of polyethylene (highly cross-linked polyethylene 0.26 mm, SD 0.17; standard 0.27 mm, SD 0.2; p = 0.83). There was, however, a significant difference (p = 0.012) in the mean wear rate (highly cross-linked polyethylene 0.03 mm/yr, SD 0.06; standard 0.07 mm/yr, SD 0.05). Creep and wear occurred in significantly different directions (p = 0.01); creep was predominantly proximal whereas wear was anterior, proximal and medial. We conclude that penetration in the first six months is creep-dominated, but after one year virtually all penetration is due to wear. Highly cross-linked polyethylene has a 60% lower rate of wear than standard polyethylene and therefore will probably perform better in the long term.

  4. Damage tolerant functionally graded materials for advanced wear and friction applications

    NASA Astrophysics Data System (ADS)

    Prchlik, Lubos

    The research work presented in this dissertation focused on processing effects, microstructure development, characterization and performance evaluation of composite and graded coatings used for friction and wear control. The following issues were addressed. (1) Definition of prerequisites for a successful composite and graded coating formation by means of thermal spraying. (2) Improvement of characterization methods available for homogenous thermally sprayed coating and their extension to composite and graded materials. (3) Development of novel characterization methods specifically for FGMs, with a focus on through thickness property measurement by indentation and in-situ curvature techniques. (4) Design of composite materials with improved properties compared to homogenous coatings. (5) Fabrication and performance assessment of FGM with improved wear and impact damage properties. Materials. The materials studied included several material systems relevant to low friction and contact damage tolerant applications: MO-Mo2C, WC-Co cermets as materials commonly used sliding components of industrial machinery and NiCrAlY/8%-Yttria Partially Stabilized Zirconia composites as a potential solution for abradable sections of gas turbines and aircraft engines. In addition, uniform coatings such as molybdenum and Ni5%Al alloy were evaluated as model system to assess the influence of microstructure variation onto the mechanical property and wear response. Methods. The contact response of the materials was investigated through several techniques. These included methods evaluating the relevant intrinsic coating properties such as elastic modulus, residual stress, fracture toughness, scratch resistance and tests measuring the abrasion and friction-sliding behavior. Dry-sand and wet two-body abrasion testing was performed in addition to traditional ball on disc sliding tests. Among all characterization techniques the spherical indentation deserved most attention and enabled to

  5. Erosive Wear Behavior of High-Alloy Cast Iron and Duplex Stainless Steel under Mining Conditions

    NASA Astrophysics Data System (ADS)

    Yoganandh, J.; Natarajan, S.; Kumaresh Babu, S. P.

    2015-09-01

    Centrifugal pumps used in the lignite mines encounter erosive wear problems, leading to a disastrous failure of the pump casings. This paper attempts to evaluate the erosive wear resistance of Ni-Hard 4, high-chromium iron, and Cast CD4MCu duplex stainless steel (DSS), for mining conditions. The prepared test coupons were subjected to an erosion test by varying the impingement velocity and the angle of impingement, under two different pH conditions of 3 and 7, which pertained to the mining conditions. XRD analysis was carried out to confirm the phases present in the alloy. The eroded surface was subjected to SEM analysis to identify the erosion mechanisms. The surface degradation of Ni-Hard 4 and high-chromium iron came from a low-angle abrasion with a grooving and plowing mechanism at a low angle of impingement. At normal impingement, deep indentations resulted in lips and crater formations, leading to degradation of the surface in a brittle manner. A combined extrusion-forging mechanism is observed in the CD4MCu DSS surface at all the impingement angles.

  6. Antibacterial activity, corrosion resistance and wear behavior of spark plasma sintered Ta-5Cu alloy for biomedical applications.

    PubMed

    Cui, Jing; Zhao, Liang; Zhu, Weiwei; Wang, Bi; Zhao, Cancan; Fang, Liming; Ren, Fuzeng

    2017-10-01

    Tantalum has been widely used in orthopedic and dental implants. However, the major barrier to the extended use of such medical devices is the possibility of bacterial adhesion to the implant surface which will cause implant-associated infections. To solve this problem, bulk Ta-5Cu alloy has been fabricated by a combination of mechanical alloying and spark plasma sintering. The effect of the addition of Cu on the hardness, antibacterial activity, cytocompatibility, corrosion resistance and wear performance was systematically investigated. The sintered Ta-5Cu alloy shows enhanced antibacterial activity against E. Coli due to the sustained release of Cu ions. However, the addition of Cu would produce slight cytotoxicity and decrease corrosion resistance of Ta. Furthermore, pin-on-disk wear tests show that Ta-5Cu alloy has a much lower coefficient of friction but a higher wear rate and shows a distinct wear mode from that of Ta upon sliding against stainless steel 440C. Wear-induced plastic deformation leads to elongation of Ta and Cu grains along the sliding direction and nanolayered structures were observed upon approaching the sliding surface. The presence of hard oxides also shows a profound effect on the plastic flow of the base material and results in localized vortex patterns. The obtained results are expected to provide deep insights into the development of novel Ta-Cu alloy for biomedical applications. Copyright © 2017 Elsevier Ltd. All rights reserved.

  7. Impact of previous extended and daily wear schedules on signs and symptoms with high Dk lotrafilcon A lenses.

    PubMed

    Chalmers, Robin L; Dillehay, Sally; Long, Bill; Barr, Joseph T; Bergenske, Peter; Donshik, Peter; Secor, Glenda; Yoakum, John

    2005-06-01

    This study measured the impact of previous contact lens wearing schedule on the resolution of signs and contact lens-related symptoms among wearers of lotrafilcon A lenses. One hundred forty adapted low Dk daily wear (DW) and 140 adapted low Dk extended wear (EW) subjects were enrolled and examined for 1 year (overall study length is 3 years). All subjects wore lotrafilcon A lenses on a wearing schedule of up to 30 nights continuous wear with monthly replacement of lenses. Examinations were conducted at 1 week, 1, 6, and 12 months. The former EW wearers presented at baseline with significantly higher conjunctival staining and epithelial microcysts (p < 0.05) and lower ocular surface symptoms of end of day dryness than the former DW wearers. There were no significant differences in other ocular signs at baseline for the former DW and EW wearers. After use of lotrafilcon A, clinical signs of limbal, conjunctival redness, and neovascularization were significantly better by the 1-week visit for both groups of wearers. Regardless of former wearing schedule, symptoms of dryness (during and at the end of the day) and photophobia were significantly better after 1 week of lotrafilcon A use. The frequency and severity of symptoms of dryness during the day improved significantly among former low Dk DW and EW wearers within 1 week as did severity of dryness during the day for the former DW wearers, in part as a result of their higher prevalence at baseline in the DW group. Subjects reported redness improved significantly by the 1-month visit. Continuous wear of high Dk silicone hydrogel lenses resulted in an improvement in ocular redness and neovascularization and dryness symptoms among subjects in this trial, regardless of their previous low Dk lens-wearing schedule. All improvements in signs and symptoms were sustained through 12 months.

  8. Microstructures and friction-wear behaviors of cathodic arc ion plated CrC coating at high temperatures

    NASA Astrophysics Data System (ADS)

    Dejun, Kong; Shouyu, Zhu

    2016-11-01

    A CrC coating was deposited on YT14 cemented carbide cutting tools by a CAIP (cathodic arc ion plating). The surface and interface morphologies, chemical composition, and phases of the obtained coating were analyzed with a field emission scanning electronic microscope (FESEM), energy dispersive spectroscope (EDS), and x-ray diffraction (XRD), respectively. The COFs (coefficient of frictions) and worn morphologies of the CrC coating at 300 °C, 400 °C, and 500 °C were investigated by using a high temperature tribometer, the effects of wear temperatures on the friction-wear properties of the CrC coating were discussed. The results show that the CrC coating exhibits fine dense structure, and the lattice constants of CrC coatings are dependent on processing parameters. The C and Cr elements in the coating are mutually diffused with the W, Co, and Ti in the substrate. The average COF of the coating at 300 °C, 400 °C, and 500 °C is 0.64, 0.63, and 0.40, respectively. The Cr2O3 layer formed on the CrC coating at 500 °C has excellent oxidation resistance, which improves lubrication and wear performance, the wear mechanism is abrasive wear and oxidation wear.

  9. Role of hard second phases in the mild oxidational wear mechanism of high-speed steel-based materials

    NASA Astrophysics Data System (ADS)

    Vardavoulias, M.

    1994-04-01

    In the case of dry unlubricated wear of metals, an oxidational wear mechanism can be established under certain conditions, with oxide films being developed on the sliding surface which markedly influence the friction and wear behaviour. For high-speed steel-based materials containing various hard second phases, an a-Fe2O3 film is formed during pin-on-disc testing (under mild conditions of load and sliding speed), which reaches a critical thickness of 1-2 microns before breaking up in loose wear debris. The role of the second phases in the oxidational wear mechanism was studied in this investigation. The size of the hard second phase particles appears to be the most important parameter determining the possibility for the particles to provide protection against oxidational wear of the matrix. Particles of a size less than or equal to the critical thickness are carried away when the oxide breaks up, while particles larger than the critical oxide thickness remain in place. In this case, their ability to protect the metallic matrix from the loads imposed by the counterbody depends on their mechanical resistance to these loads, as well as the strength of their cohesion with the metallic matrix.

  10. The comparison of manual lymph drainage and ultrasound therapy on the leg swelling caused by wearing high heels.

    PubMed

    Lee, Dong-Yeop; Han, Ji-Su; Jang, Eun-Ji; Seo, Dong-Kwon; Hong, Ji-Heon; Lee, Sang-Sook; Lee, Dong-Geol; Yu Lee, Jae-Ho

    2014-01-01

    One of the major symptoms when women are wearing high heels for a long time is leg swelling. The purpose of this study was to compare the effect of manual lymph drainage with ultrasound therapy. The forty-five healthy women of twenties were participated in this study and divided randomly into three groups; manual lymph drainage group (n=15), ultrasound therapy group (n=15) and control group (n=15). Swelling was measured before wearing the high heels (10 cm-height), after one-hour of wearing the high heels, wearing the high heels of one-hour after the intervention of 15 minutes. Also swelling was calculated by using a tape measure, volumeter and body composition analyzer. Statistical analysis of the comparison between the three groups was performed by one-way ANOVA. Also comparison to the mean value in swelling according to the time was performed by repeated measure ANOVA. As the result of this study, a significant changes have emerged within each of manual lymph drainage, ultrasound therapy and control group (p< 0.05). However, there were no significant differences between each group (p> 0.05). But the mean value of manual lymph drainage group showed the tendency of fast recovering before causing swelling. Therefore, we consider that the clinical treatment of manual lymph drainage and ongoing studies will be made since manual lymph drainage is very effective in releasing the leg swelling caused by wearing high heels and standing for a long time at work.

  11. Development of a gear vibration indicator and its application in gear wear monitoring

    NASA Astrophysics Data System (ADS)

    Hu, Chongqing; Smith, Wade A.; Randall, Robert B.; Peng, Zhongxiao

    2016-08-01

    Gear tooth wear is an inevitable phenomenon and has a significant influence on gear dynamic features. Although vibration analysis has been widely used to diagnose localised gear tooth faults, its techniques for gear wear monitoring have not been well-established. This paper aims at developing a vibration indicator to evaluate the effects of wear on gear performance. For this purpose, a gear state vector is extracted from time synchronous averaged gear signals to describe the gear state. This gear state vector consists of the sideband ratios obtained from a number of tooth meshing harmonics and their sidebands. Then, two averaged logarithmic ratios, ALR and mALR, are defined with fixed and moving references, respectively, to provide complementary information for gear wear monitoring. Since a fixed reference is utilised in the definition of ALR, it reflects the cumulated wear effects on the gear state. An increase in the ALR value indicates that the gear state deviates further from its reference condition. With the use of a moving reference, the indicator mALR shows changes in the gear state within short time intervals, making it suitable for wear process monitoring. The efficiency of these vibration indicators is demonstrated using experimental results from two sets of tests, in which the gears experienced different wear processes. In addition to gear wear monitoring, the proposed indicators can be used as general parameters to detect the occurrence of other faults, such as a tooth crack or shaft misalignment, because these faults would also change the gear vibrations.

  12. Effect of high-intensity ultrasonic treatment on microstructure, hardness and wear behaviour of the hypereutectic Mg-5Si alloy

    NASA Astrophysics Data System (ADS)

    Moussa, M. E.; Waly, M. A.; El-Sheikh, A. M.

    2016-07-01

    The effect of high-intensity ultrasonic treatment (HIUST) on microstructure, hardness and wear behavior in Mg-5wt.%Si hypereutectic alloy has been investigated. The results showed clearly that without HIUST, most of primary Mg2Si appeared as coarse dendritic morphology with average size of about 200 µm. With HIUST, the average size of primary Mg2Si decreased significantly to about 33 µm and their morphologies changed to polyhedral shape. The modification mechanism is mainly attributed conjugation of two mechanisms: cavitation-enhanced heterogeneous nucleation and cavitation-induced dendrite fragmentation. The alloy treated with HIUST has higher hardness and wear resistance than that untreated with HIUST. The wear mechanism of investigated alloys at low applied load (10 N) and low sliding speed (0.3 m/s) is a mild abrasive oxidative wear with little adhesion. However, the wear mechanism due to the applied high loads (30, 50 N) at low sliding speed (0.3 m/s) and/or to the applied high sliding speeds (0.6, 0.9 m/s) under low load (10 N), could be described as delamination mechanism. The microstructures of the specimens were analyzed by optical microscope (OM) (model OPTIKA M-790, Italy). Energy dispersion spectrum (EDS) affiliated to field emission scanning electron microscopy (FESEM) (model Quanta FEG, The Netherlands) were performed to reveal the concentration of alloying elements in selected areas of the microstructure.

  13. Safety and efficacy of a high-adhesion whitening strip under extended wear regimen.

    PubMed

    Oliveira, Gustavo M; Miguez, Patricia A; Oliveira, Greice B; Swift, Edward J; Farrell, Svetlana; Anastasia, Mary Kay; Conde, Erinn; Walter, Ricardo

    2013-08-01

    This randomized, parallel group, single centre clinical trial was conducted to evaluate the safety and compare the whitening efficacy for an extended wear of an experimental 9.5% H₂O₂ high-adhesion whitening strip, relative to a marketed 10% H₂O₂ control strip. Twenty-nine eligible adult volunteers were randomly assigned to either a treatment series with an experimental 9.5% H₂O₂ high-adhesion whitening strip at home for 2h, once a day, for 8 days; or a marketed 10% H₂O₂ whitening strip for 30 min, on a similar daily regimen. Tooth color/whitening progression was recorded under standardized lighting conditions at baseline, day 3, day 5, and day 9, via digital imaging. Outcomes were reported using the CIELAB system. Usage safety was also assessed at each follow-up visit. Whitening efficacy for each group was investigated using a paired-difference t-test. The treatment groups were compared among each other using the analysis of covariance, with the baseline value and age as the covariates. Both treatment groups demonstrated statistically significant mean color improvement from baseline for b* (yellow ness) and L* (lightness) at each post-baseline visit. In addition, the 2-h high-adhesion strips demonstrated significantly greater improvement in b* and L* relative to the 30-min strip group at each follow-up visit. The 2-h regimen for the 9.5% H₂O₂ high-adhesion whitening strip was more efficient for tooth whitening than the 30-min regimen of 10% H₂O₂ whitening strip. Both treatments were well tolerated and the use of the test products during the study time frame was considered safe. Extending the daily wear time of whitening strips can improve the efficacy of the treatment and ultimately shorten the length of the treatment without any significant adverse effects. Copyright © 2012 Elsevier Ltd. All rights reserved.

  14. Fabrication of wear-resistant silicon microprobe tips for high-speed surface roughness scanning devices

    NASA Astrophysics Data System (ADS)

    Wasisto, Hutomo Suryo; Yu, Feng; Doering, Lutz; Völlmeke, Stefan; Brand, Uwe; Bakin, Andrey; Waag, Andreas; Peiner, Erwin

    2015-05-01

    Silicon microprobe tips are fabricated and integrated with piezoresistive cantilever sensors for high-speed surface roughness scanning systems. The fabrication steps of the high-aspect-ratio silicon microprobe tips were started with photolithography and wet etching of potassium hydroxide (KOH) resulting in crystal-dependent micropyramids. Subsequently, thin conformal wear-resistant layer coating of aluminum oxide (Al2O3) was demonstrated on the backside of the piezoresistive cantilever free end using atomic layer deposition (ALD) method in a binary reaction sequence with a low thermal process and precursors of trimethyl aluminum and water. The deposited Al2O3 layer had a thickness of 14 nm. The captured atomic force microscopy (AFM) image exhibits a root mean square deviation of 0.65 nm confirming the deposited Al2O3 surface quality. Furthermore, vacuum-evaporated 30-nm/200-nm-thick Au/Cr layers were patterned by lift-off and served as an etch mask for Al2O3 wet etching and in ICP cryogenic dry etching. By using SF6/O2 plasma during inductively coupled plasma (ICP) cryogenic dry etching, micropillar tips were obtained. From the preliminary friction and wear data, the developed silicon cantilever sensor has been successfully used in 100 fast measurements of 5- mm-long standard artifact surface with a speed of 15 mm/s and forces of 60-100 μN. Moreover, the results yielded by the fabricated silicon cantilever sensor are in very good agreement with those of calibrated profilometer. These tactile sensors are targeted for use in high-aspect-ratio microform metrology.

  15. Does ultra-mild wear play any role for dry friction applications, such as automotive braking?

    PubMed

    Osterle, Werner; Dmitriev, A I; Kloss, H

    2012-01-01

    Nanostructured third body films and/or storage of wear debris at the surfaces of the first bodies are deemed as prerequisites of sliding under ultra-mild wear conditions. Since such features have been observed experimentally on brake pads and discs, attempts were undertaken to study their sliding behaviour by modelling on the nanoscopic scale with an approach based on Movable Cellular Automata (MCA). The model rendered the possibility to study the influence of different nanostructures systematically and to assess the impact of different brake pad ingredients on the sliding behaviour, velocity accommodation and friction force stabilization at a sliding contact. Besides providing a review on previously published modelling results, some additional new graphs enabling better visualization of dynamic processes are presented. Although ultra-mild wear conditions were considered to be essential for achieving the desired tribological properties, transitions to mesoscopic and macroscopic wear mechanisms were studied as well. The final conclusion is that ultra-mild wear and corresponding smooth sliding behaviour play an important role during automotive braking, even though temporarily and locally events of severe wear may cause friction instabilities, surface damage and release of coarse wear particles.

  16. Wear Testing of Moderate Activities of Daily Living Using In Vivo Measured Knee Joint Loading

    PubMed Central

    Reinders, Jörn; Sonntag, Robert; Vot, Leo; Gibney, Christian; Nowack, Moritz; Kretzer, Jan Philippe

    2015-01-01

    Resumption of daily living activities is a basic expectation for patients provided with total knee replacements. However, there is a lack of knowledge regarding the impact of different activities on the wear performance. In this study the wear performance under application of different daily activities has been analyzed. In vivo load data for walking, walking downstairs/upstairs, sitting down/standing up, and cycling (50 W & 120 W) has been standardized for wear testing. Wear testing of each activity was carried out on a knee wear simulator. Additionally, ISO walking was tested for reasons of comparison. Wear was assessed gravimetrically and wear particles were analyzed. In vivo walking produced the highest overall wear rates, which were determined to be three times higher than ISO walking. Moderate wear rates were determined for walking upstairs and downstairs. Low wear rates were determined for standing up/sitting down and cycling at power levels of 50 W and 120 W. The largest wear particles were observed for cycling. Walking based on in vivo data has been shown to be the most wear-relevant activity. Highly demanding activities (stair climbing) produced considerably less wear. Taking into account the expected number of loads, low-impact activities like cycling may have a greater impact on articular wear than highly demanding activities. PMID:25811996

  17. The Effects of Austenitizing Conditions on the Microstructure and Wear Resistance of a Centrifugally Cast High-Speed Steel Roll

    NASA Astrophysics Data System (ADS)

    Kang, Minwoo; Lee, Young-Kook

    2016-07-01

    The influences of austenitizing conditions on the microstructure and wear resistance of a centrifugally cast high-speed steel roll were investigated through thermodynamic calculation, microstructural analysis, and high-temperature wear tests. When the austenitizing temperature was between 1323 K and 1423 K (1050 °C and 1150 °C), coarse eutectic M2C plates were decomposed into a mixture of MC and M6C particles. However, at 1473 K (1200 °C), the M2C plates were first replaced by both new austenite grains and MC particles without M6C particles, and then remaining M2C particles were dissolved during the growth of MC particles. The wear resistance of the HSS roll was improved with increasing austenitizing temperature up to 1473 K (1200 °C) because the coarse eutectic M2C plates, which are vulnerable to crack propagation, changed to disconnected hard M6C and MC particles.

  18. The influence of scratches to metallic counterfaces on the wear of ultra-high molecular weight polyethylene.

    PubMed

    Fisher, J; Firkins, P; Reeves, E A; Hailey, J L; Isaac, G H

    1995-01-01

    A number of studies of explanted metallic femoral heads have shown scratches or damage caused by bone cement, bone or metallic particles. This damage has been cited as a cause of increased wear of ultra-high molecular weight polyethylene (UHMWPE) acetabular cups. In this laboratory study, small scratches 2 mu m deep were made on smooth stainless steel surfaces at a spacing of 10 mm. These individual scratches were found to increase the wear rate of UHMWPE by a factor of 30 in unidirectional sliding and a factor of 70 in reciprocating motion. It is of particular concern that a single small scratch, which is not detected by the average surface roughness measurement Ra can cause such a dramatic increase in the wear of ultra-high molecular weight polyethylene.

  19. Poly(2-methacryloyloxyethyl phosphorylcholine) grafting and vitamin E blending for high wear resistance and oxidative stability of orthopedic bearings.

    PubMed

    Kyomoto, Masayuki; Moro, Toru; Yamane, Shihori; Watanabe, Kenichi; Hashimoto, Masami; Takatori, Yoshio; Tanaka, Sakae; Ishihara, Kazuhiko

    2014-08-01

    The ultimate goal in manipulating the surface and substrate of a cross-linked polyethylene (CLPE) liner is to obtain not only high wear resistance but also high oxidative stability and high-mechanical properties for life-long orthopedic bearings. We have demonstrated the fabrication of highly hydrophilic and lubricious poly(2-methacryloyloxyethyl phosphorylcholine) (PMPC) grafting layer onto the antioxidant vitamin E-blended CLPE (HD-CLPE(VE)) surface. The PMPC grafting layer with a thickness of 100 nm was successfully fabricated on the vitamin E-blended CLPE surface by using photoinduced-radical graft polymerization. Since PMPC has a highly hydrophilic nature, the water wettability and lubricity of the PMPC-grafted CLPE and HD-CLPE(VE) surfaces were greater than that of the untreated CLPE surface. The PMPC grafting contributed significantly to wear reduction in a hip-joint simulator wear test. Despite high-dose gamma-ray irradiation for cross-linking and further UV irradiation for PMPC grafting, the substrate modified by vitamin E blending maintained high-oxidative stability because vitamin E is an extremely efficient radical scavenger. Furthermore, the mechanical properties of the substrate remained almost unchanged even after PMPC grafting or vitamin E blending, or both PMPC grafting and vitamin E blending. In conclusion, the PMPC-grafted HD-CLPE(VE) provided simultaneously high-wear resistance, oxidative stability, and mechanical properties.

  20. Generation of a large volume of clinically relevant nanometre-sized ultra-high-molecular-weight polyethylene wear particles for cell culture studies.

    PubMed

    Liu, Aiqin; Ingham, Eileen; Fisher, John; Tipper, Joanne L

    2014-04-01

    It has recently been shown that the wear of ultra-high-molecular-weight polyethylene in hip and knee prostheses leads to the generation of nanometre-sized particles, in addition to micron-sized particles. The biological activity of nanometre-sized ultra-high-molecular-weight polyethylene wear particles has not, however, previously been studied due to difficulties in generating sufficient volumes of nanometre-sized ultra-high-molecular-weight polyethylene wear particles suitable for cell culture studies. In this study, wear simulation methods were investigated to generate a large volume of endotoxin-free clinically relevant nanometre-sized ultra-high-molecular-weight polyethylene wear particles. Both single-station and six-station multidirectional pin-on-plate wear simulators were used to generate ultra-high-molecular-weight polyethylene wear particles under sterile and non-sterile conditions. Microbial contamination and endotoxin levels in the lubricants were determined. The results indicated that microbial contamination was absent and endotoxin levels were low and within acceptable limits for the pharmaceutical industry, when a six-station pin-on-plate wear simulator was used to generate ultra-high-molecular-weight polyethylene wear particles in a non-sterile environment. Different pore-sized polycarbonate filters were investigated to isolate nanometre-sized ultra-high-molecular-weight polyethylene wear particles from the wear test lubricants. The use of the filter sequence of 10, 1, 0.1, 0.1 and 0.015 µm pore sizes allowed successful isolation of ultra-high-molecular-weight polyethylene wear particles with a size range of < 100 nm, which was suitable for cell culture studies.

  1. Generation of a large volume of clinically relevant nanometre-sized ultra-high-molecular-weight polyethylene wear particles for cell culture studies

    PubMed Central

    Ingham, Eileen; Fisher, John; Tipper, Joanne L

    2014-01-01

    It has recently been shown that the wear of ultra-high-molecular-weight polyethylene in hip and knee prostheses leads to the generation of nanometre-sized particles, in addition to micron-sized particles. The biological activity of nanometre-sized ultra-high-molecular-weight polyethylene wear particles has not, however, previously been studied due to difficulties in generating sufficient volumes of nanometre-sized ultra-high-molecular-weight polyethylene wear particles suitable for cell culture studies. In this study, wear simulation methods were investigated to generate a large volume of endotoxin-free clinically relevant nanometre-sized ultra-high-molecular-weight polyethylene wear particles. Both single-station and six-station multidirectional pin-on-plate wear simulators were used to generate ultra-high-molecular-weight polyethylene wear particles under sterile and non-sterile conditions. Microbial contamination and endotoxin levels in the lubricants were determined. The results indicated that microbial contamination was absent and endotoxin levels were low and within acceptable limits for the pharmaceutical industry, when a six-station pin-on-plate wear simulator was used to generate ultra-high-molecular-weight polyethylene wear particles in a non-sterile environment. Different pore-sized polycarbonate filters were investigated to isolate nanometre-sized ultra-high-molecular-weight polyethylene wear particles from the wear test lubricants. The use of the filter sequence of 10, 1, 0.1, 0.1 and 0.015 µm pore sizes allowed successful isolation of ultra-high-molecular-weight polyethylene wear particles with a size range of < 100 nm, which was suitable for cell culture studies. PMID:24658586

  2. Effect of slide track shape on the wear of ultra-high molecular weight polyethylene in a pin-on-disk wear simulation of total hip prosthesis.

    PubMed

    Saikko, Vesa; Calonius, Olof; Keränen, Jaakko

    2004-05-15

    Prosthetic joints appear to show a strong relationship between the type of relative motion and wear, requiring careful consideration in the design of wear simulators. This relationship was studied with a 12-station pin-on-disk device, specifically adapted for the wear simulation of prosthetic hip joints. Each station had a unique motion, characterized by the so-called slide track, the track of the pin on the disk. The slide track shapes included 10 ellipses, their aspect ratio (AR) varying from 1.1 to 11.0, and a circle and a straight line as extreme cases. Hence for the first time in hip wear simulation, the motion was systematically varied over a wide range. Conventional UHMWPE pins were tested against polished CoCr disks in diluted calf serum three times for 3 million cycles. Below the AR value of 5.5, the polyethylene wear factor and wear mechanisms agreed with clinical observations. Above this value, the wear factor decreased to unrealistically low values, and the wear surface topography differed from that of retrieved acetabular cups. The wear particles, however, were similar to those isolated from periprosthetic tissues, irrespective of the AR value. In conclusion, it is recommended that the AR value be kept well below the critical point of 5.5.

  3. Design of High-speed Wear Lifetime Tester of the Instrument Ball Bearings

    NASA Astrophysics Data System (ADS)

    Liu, C. H.; Gu, J. M.; Sun, Y.; Chen, X. Y.

    2006-10-01

    The instrument ball bearings are the key components of movable components for various kinds of measuring and control instruments; they often operate in the environmental condition of high-speed and light preload. In general, the non metal, disposable oilimpregnated retainer material has been used for these kinds of high precision miniature bearing. The engineering practice shows that the common failure mode of them is the wear which appears under the condition of insufficient lubrication condition. As the results, the vibration and noise will be enlarged, so does the frictional torque, which makes the ball bearings to lose its original working accuracy. It is the lifetime test of bearings that can enable the designers and manufacturers to chose the material of the bearing properly, optimize the product structure, mend the manufacturing technique process, and to enhance the technical level of the bearing products significantly. In this paper, the wear lifetime tester has been designed according to the requirements of the life test for the instrument ball bearings, which consists of the main body of tester, electric system, drive unit and computer measure and control system, etc. The motor spindle has been selected to drive the device which is supported by the aerostatic bearing; frequency conversion speed adjustment mode, its scope of rotating speed is between 0 and 10,000 rpm. A pair of bearings can be tested under the pure axial preload condition, the maximum load is up to 50N, the control accuracy is ±2% the scope of temperature control is up to 200°C. The variation of frictional torque on the bearing couple will be measured by an online torque transducer. The variation of power dissipation can be monitored under arbitrary speed by use of an on-line high-precision power meter. The wear and quality situation of the contact surface of the bearings will be reflected on these two parameters. Meanwhile, the values of temperature and vibration will also be monitored

  4. Wear Characteristics of Metallic Biomaterials: A Review

    PubMed Central

    Hussein, Mohamed A.; Mohammed, Abdul Samad; Al-Aqeeli, Naser

    2015-01-01

    Metals are extensively used in a variety of applications in the medical field for internal support and biological tissue replacements, such as joint replacements, dental roots, orthopedic fixation, and stents. The metals and alloys that are primarily used in biomedical applications are stainless steels, Co alloys, and Ti alloys. The service period of a metallic biomaterial is determined by its abrasion and wear resistance. A reduction in the wear resistance of the implant results in the release of incompatible metal ions into the body that loosen the implant. In addition, several reactions may occur because of the deposition of wear debris in tissue. Therefore, developing biomaterials with high wear resistance is critical to ensuring a long life for the biomaterial. The aim of this work is to review the current state of knowledge of the wear of metallic biomaterials and how wear is affected by the material properties and conditions in terms of the type of alloys developed and fabrication processes. We also present a brief evaluation of various experimental test techniques and wear characterization techniques that are used to determine the tribological performance of metallic biomaterials.

  5. High friction and low wear properties of laser-textured ceramic surface under dry friction

    NASA Astrophysics Data System (ADS)

    Xing, Youqiang; Deng, Jianxin; Wu, Ze; Wu, Fengfang

    2017-08-01

    Two kinds of grooved textures with different spacing were fabricated on Al2O3/TiC ceramic surface by an Nd:YAG laser. The dry tribological properties of the textured samples were investigated by carrying out unidirectional rotary sliding friction and wear tests using a ball-on-disk tribometer. Results show that the laser textured samples exhibit higher friction coefficient and excellent wear resistance compared with the smooth sample under dry friction conditions. Furthermore, the texture morphology and spacing have a significant influence on the tribological properties. The sample with small texture spacing may be beneficial to increasing the friction coefficient, and the wavy-grooved sample exhibits the highest friction coefficient and shallowest wear depth. The increasing friction coefficient and anti-wear properties are attributed to the combined effects of the increased surface roughness, reduced real contact area, micro-cutting effect by the texture edges and entrapment of wear debris.

  6. Sliding wear behaviors of steam generator tube materials in high temperature water environment

    NASA Astrophysics Data System (ADS)

    Park, Gi Sung; Kim, Gyung Guk; Kim, Seon Jin

    2006-06-01

    Wear damage of steam generator tubes for nuclear power plants can cause the leakage of radioactive substances. Therefore, the evaluation of the tube integrity is very important in the view point of nuclear safety. In the present study, to investigate the effects of the applied normal load and sliding distance on wear volume in 575 K water environment, sliding wear tests were performed with Inconel 600 and 690 steam generator tube materials mated with 409 stainless steel commonly used as support plate. Based on the accumulated data, the newly modified Archard equation was proposed and then the wear coefficients of tube materials were estimated with both Archard equation and the modified Archard equation. The reliabilities, which are parameters to assess how well a model fits a set of data, for prediction of wear behaviors of Inconel 600 and 690 improved from 20.5% to 65.5% and from 38.5 to 65.3%, respectively.

  7. Wear resistance of the biocompatible phospholipid polymer-grafted highly cross-linked polyethylene liner against larger femoral head.

    PubMed

    Moro, Toru; Takatori, Yoshio; Kyomoto, Masayuki; Ishihara, Kazuhiko; Kawaguchi, Hiroshi; Hashimoto, Masami; Tanaka, Takeyuki; Oshima, Hirofumi; Tanaka, Sakae

    2015-07-01

    The use of larger femoral heads to prevent the dislocation of artificial hip joints has recently become more common. However, concerns about the subsequent use of thinner polyethylene liners and their effects on wear rate have arisen. Previously, we prepared and evaluated the biological and mechanical effects of a novel highly cross-linked polyethylene (CLPE) liner with a nanometer-scaled graft layer of poly(2-methacryloyloxyethyl phosphorylcholine) (PMPC). Our findings showed that the PMPC-grafted particles were biologically inert and caused no subsequent bone resorptive responses and that the PMPC-grafting markedly decreased wear in a hip joint simulator. However, the metal or ceramic femoral heads used in this previous study had a diameter of 26 mm. Here, we investigated the wear-resistance of the PMPC-grafted CLPE liner with a 40-mm femoral head during 10 × 10(6) cycles of loading in the hip joint simulator. The results provide preliminary evidence that the grafting markedly decreased gravimetric wear rate and the volume of wear particles, even when coupled with larger femoral heads. Thus, we believe the PMPC-grafting will prolong artificial hip joint longevity both by preventing aseptic loosening and by improving the stability of articular surface.

  8. Wear behaviour and microstructural characterization of worn surfaces and wear debris of a high purity aluminum and an aluminum-silicon alloy and an aluminum-silicon/silicon carbide composite sliding against an M2 steel

    NASA Astrophysics Data System (ADS)

    Li, Xianyao

    1999-11-01

    The present dissertation discusses wear behavior and microstructural characterization of the wear surface and wear debris of an Al-Si alloy (A356) and an Al-Si (A356) based composite reinforced with 20 vol.% SiC particulate as well as a high purity (99.99%) Al sliding against an M2 steel under unlubricated conditions using a block-on-ring sliding wear tester. It was observed that the wear resistance of the Al-Si/SiCp composite material was superior to that of the Al-Si alloy by one order of magnitude at a low sliding load. It was also observed that the wear resistance of the Al-Si/SiC composite could slightly be increased by approximately 10% due to the T6 beat treatment of the composite. The increase in the wear resistance, however, was not significant when compared to the increase in the hardness of the matrix due to the beat treatment. This can be partially attributed to the fact that in-situ precipitation occurred in the subsurface during the sliding wear of the as-cast Al composites. Microstructural characterization of the worn surfaces and weer debris was carried out by using Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM) equipped with Energy Dispersive Spectroscopy (EDS), X-ray mapping and X-ray Diffraction (XRD). In particular, longitudinal cross-section TEM analyses of the worn surfaces and wear debris were successfully conducted in the present work. The results showed that the deformed structures in the worn surfaces of the Al-Si alloy and the composite contained a large number of cells and elongated subgrains with an aspect ratio of 5 to 10. It was also observed that mechanically mixed layers (MMLs) were formed during the sliding wear of the Al-Si/SiC composite and Al-Si alloy as well as the high purity (BP) Al against the steel. Characterization of the wear debris by means of the above mentioned techniques and Mossbauer spectroscopy revealed that the wear debris had features similar to those of the MMLs in the worn surfaces

  9. Improving Tribological Properties of Cast Al-Si Alloys through Application of Wear-Resistant Thermal Spray Coatings

    NASA Astrophysics Data System (ADS)

    Culliton, David; Betts, Anthony; Carvalho, Sandra; Kennedy, David

    2013-04-01

    Flame Spray Thermal Spray coatings are low-cost, high-wear surface-treatment technologies. However, little has been reported on their potential effects on cast automotive aluminum alloys. The aim of this research was to investigate the tribological properties of as-sprayed NiCrBSi and WC/12Co Flame Spray coatings applied to two cast aluminum alloys: high-copper LM24 (AlSi8Cu3Fe), and low-copper LM25 (AlSi7Mg). Potential interactions between the mechanical properties of the substrate and the deposited coatings were deemed to be significant. Microstructural, microhardness, friction, and wear (pin-on-disk, microabrasion, Taber abrasion, etc.) results are reported, and the performance differences between coatings on the different substrates were noted. The coefficient of friction was reduced from 0.69-0.72 to 0.12-0.35. Wear (pin-on-disk) was reduced by a factor of 103-104, which was related to the high surface roughness of the coatings. Microabrasion wear was dependent on coating hardness and applied load. Taber abrasion results showed a strong dependency on the substrate, coating morphology, and homogeneity.

  10. Applications of Electrostatic Sensor for Wear Debris Detecting in the Lubricating Oil

    NASA Astrophysics Data System (ADS)

    Wen, Z.; Yin, X.; Jiang, Z.

    2013-10-01

    In this study, an advanced monitoring technology has been presented based on the electrostatic induction principle to monitor timely wear fault on-line. The paper begins with the principle of the electrostatic monitoring technology, then we focus on the electrostatic sensor, the most important component in the electrostatic monitoring system, establish a measurement model for an electrostatic sensor with the given structure parameters. Based on the measurement model, we use the finite element method to analyze the characteristics of an electrostatic sensor for wear debris detecting in lubricating oil. Lastly we build an experiment platform to validate the feasibility of the electrostatic monitoring method. The experiment results show, to some extent, that the electrostatic signal can reflect the relative density of wear debris, and the sensor proposed can satisfy the primary demand of wear debris on-line monitoring.

  11. Abrasive wear of cemented carbides

    SciTech Connect

    Hawk, Jeffrey A.; Wilson, Rick D.

    2003-10-01

    Cemented carbides are used for a wide variety of applications where wear is a problem. Usually the wear of the cemented carbides is a combination of metal-to-metal and abrasion. Wear can occur at room or elevated temperatures. This research summarizes initial research to understand the abrasive wear of various cemented carbides (various grain sizes, carbide types, carbide grain sizes and binder compositions) in terms of absolute material removal rates and material removal mechanisms.

  12. Wear simulation of ultra-high molecular weight polyethylene hip implants by incorporating the effects of cross-shear and contact pressure.

    PubMed

    Kang, L; Galvin, A L; Brown, T D; Fisher, J; Jin, Z-M

    2008-10-01

    The effect of multi-directional cross-shear (CS) motion and contact pressure on ultra-high molecular weight polyethylene (UHMWPE) wear was investigated in this study, based on an integrated experimental and computational approach. The wear factor as a function of CS was determined experimentally from a multi-directional pin-on-plate wear tester under a nominal contact pressure of 1 MPa. A computational wear model was developed which included the effects of CS as well as the load and sliding distance imposed on the hip joint employing a UHMWPE cup against a metallic femoral head under both gait and Leeds ProSim hip joint simulator conditions. The CS ratios were quantified over the articular surface of the UHMWPE cup and the CS-dependent wear factors derived from multi-directional pin-on-plate studies were applied in the computational wear model. Outputs from the computational wear model were validated independently against an experimental hip simulator study. Comparisons of linear and volumetric wear were made between the computational wear model and the hip simulator testing for a nominal conventional (0 MRad) UHMWPE cup of 28mm diameter and a highly cross-linked (10 MRad) UHMWPE cup. The difference between the computed and experimental volumetric wear was approximately 30 per cent for the 0 MRad UHMWPE, although the worn areas between the prediction and the measurement were similar. For the 10 MRad UHMWPE, the discrepancy was reduced to 16 per cent. In both cases, the computational model predicted a lower wear rate than the experimental simulator testing. The effect of using alternative wear factors under a different nominal contact pressure of 3MPa was also considered. The input wear factor to the computational model, derived from a constant loaded pin-on-plate test configuration, may underestimate the dynamic effect due to the variation in the load in the hip joint simulator.

  13. Surface modification of Monel K-500 as a means of reducing friction and wear in high-pressure oxygen

    NASA Technical Reports Server (NTRS)

    Gunaji, Mohan; Stoltzfus, Joel M.; Schoenman, Leonard; Kazaroff, John

    1989-01-01

    A study is conducted of the tribological characteristics of Monel K-500 during rubbing in a high pressure oxygen atmosphere, upon surface treatment by ion-implanted oxygen, chromium, lead, and silver, as well as electrolyzed chromium and an electroless nickel/SiC composite. The electrolyzed chromium dramatically increased total sample wear, while other surface treatments affected sample wear only moderately. Although the ion-implant treatments reduced the average coefficient of friction at low contact pressure, higher contact pressures eliminated this improvement.

  14. Surface modification of Monel K-500 as a means of reducing friction and wear in high-pressure oxygen

    NASA Technical Reports Server (NTRS)

    Gunaji, Mohan; Stoltzfus, Joel M.; Schoenman, Leonard; Kazaroff, John

    1989-01-01

    A study is conducted of the tribological characteristics of Monel K-500 during rubbing in a high pressure oxygen atmosphere, upon surface treatment by ion-implanted oxygen, chromium, lead, and silver, as well as electrolyzed chromium and an electroless nickel/SiC composite. The electrolyzed chromium dramatically increased total sample wear, while other surface treatments affected sample wear only moderately. Although the ion-implant treatments reduced the average coefficient of friction at low contact pressure, higher contact pressures eliminated this improvement.

  15. Wear Measurement System

    NASA Technical Reports Server (NTRS)

    1995-01-01

    Lewis Research Center developed a tribometer for in-house wear tests. Implant Sciences Corporation (ISC), working on a NASA contract to develop coatings to enhance the wear capabilities of materials, adapted the tribometer for its own use and developed a commercial line of user-friendly systems. The ISC-200 is a pin-on-disk type of tribometer, functioning like a record player and creating a wear groove on the disk, with variables of speed and load. The system can measure the coefficient of friction, the wear behavior between materials, and the integrity of thin films or coatings. Applications include measuring wear on contact lenses and engine parts and testing disk drives.

  16. Clinical safety and wear resistance of the phospholipid polymer-grafted highly cross-linked polyethylene liner.

    PubMed

    Moro, Toru; Takatori, Yoshio; Tanaka, Sakae; Ishihara, Kazuhiko; Oda, Hiromi; Kim, Yoon Taek; Umeyama, Takashige; Fukatani, Eisei; Ito, Hideya; Kyomoto, Masayuki; Oshima, Hirofumi; Tanaka, Takeyuki; Kawaguchi, Hiroshi; Nakamura, Kozo

    2016-11-03

    To reduce the production of wear particles and subsequent aseptic loosening, we created a human articular cartilage-mimicked surface for a highly cross-linked polyethylene liner, whose surface grafted layer consisted of a biocompatible phospholipid polymer, poly(2-methacryloyloxyethyl phosphorylcholine). Although our previous in vitro findings showed that poly(2-methacryloyloxyethyl phosphorylcholine)-grafted particles were biologically inert and caused no subsequent bone resorptive responses, and poly(2-methacryloyloxyethyl phosphorylcholine) grafting markedly decreased wear in hip joint simulator tests, the clinical safety, and in vivo wear resistance of poly(2-methacryloyloxyethyl phosphorylcholine)-grafted highly cross-linked polyethylene liners remained open to question. Therefore, in the present study, we evaluated clinical and radiographic outcomes of poly(2-methacryloyloxyethyl phosphorylcholine)-grafted highly cross-linked polyethylene liners 5 years subsequent to total hip replacement in 68 consecutive patients. No reoperation was required for any reason, and no adverse events were associated with the implanted liners. The average Harris Hip Score increased from 38.6 preoperatively to 96.5 5 years postoperatively, and health-related quality of life, as indicated by the Short Form 36 Health Survey, improved. Radiographic analyses showed no periprosthetic osteolysis or implant migration. Between 1 and 5 years postoperatively, the mean steady-state wear rate was 0.002 mm/year, which represented a marked reduction relative to other highly cross-linked polyethylene liners, and appeared to be unaffected by patient-related or surgical factors. Although longer follow up is required, poly(2-methacryloyloxyethyl phosphorylcholine)-grafted highly cross-linked polyethylene liners improved mid-term clinical outcomes. The clinical safety and wear-resistance results are encouraging with respect to the improvement of long-term clinical outcomes with poly(2

  17. Effects of high heeled shoes wearing experience and heel height on human standing balance and functional mobility.

    PubMed

    Hapsari, Vaniessa Dewi; Xiong, Shuping

    2016-01-01

    This study aimed to examine the effects of high heeled shoes (HHS) wearing experience and heel height on human standing balance and functional mobility. Thirty young and healthy females (ten experienced and twenty inexperienced HHS wearers) participated in a series of balance tests when they wore shoes of four different heel heights: 1 cm (flat), 4 cm (low), 7 cm (medium) and 10 cm (high). Experimental results show that regardless of the wearing experience, the heel elevation induces more effort from lower limb muscles (particularly calf muscles) and results in worse functional mobility starting at 7 cm heel height. While the heel height increased to 10 cm, the standing balance also becomes worse. Experienced HHS wearers do not show significantly better overall performance on standing balance and functional mobility than inexperienced controls, even though they have better directional control (76.8% vs. 74.4%) and larger maximum excursion (93.3% vs. 89.7%). To maintain standing balance, experienced wearers exert less effort on tibialis anterior, vastus lateralis and erector spinae muscles at the cost of more intensive effort from gastrocnemius medialis muscle. Many women wear high heeled shoes (HHS) to increase female attractiveness. This study shows that HHS induce more muscular effort and worse human standing balance and functional mobility, especially when heel height reaches 10 cm. HHS wearing experience only provides certain advantages to wearers on limits of stability in terms of larger maximum excursion and better directional control.

  18. Fret wear mediation of NIRCam filter wheel assembly

    NASA Astrophysics Data System (ADS)

    Privári, Béla I.

    2011-10-01

    We will discuss a fret wear solution developed for the James Webb Space Telescope NIRCam filter wheel assembly by implementation of a hard coating. With mechanisms and structures designed for space flight application, titanium is often selected as the choice material of construction. Titanium offers a low-density high strength material that is good for use with many optical instruments due to its' favorable thermal properties. An important factor to consider with titanium mechanisms and structures are component fits and the vibration environment that must be survived during launch. In many instances, small (slip) fits between titanium components can cause fret wear during launch induced vibration. Titanium is particularly susceptible to fret wear, although other materials also demonstrate the fret wear. Fretting is adhesive failure of a material that experiences impact and micro-slip with an adjacent part. The mechanism of fret wear involves small particles that are pulled from the surface of parts that turn into hard oxides that further accelerate the wear between the parts. To mitigate fret wear, the mechanism or structure can be designed to eliminate all slip fits altogether, lubricants may be added to the wear surfaces or hard coatings can be applied to the wear surfaces when the other approaches are not feasible. For the NIRCam filter wheel assembly, which must operate at 35K and remain optically clean, only hard coatings are feasible. A discussion of several coating alternatives and associated wear testing will be presented along with the selection of an optimal solution.

  19. Enamel wear of modified porcelains.

    PubMed

    Imai, Y; Suzuki, S; Fukushima, S

    2000-12-01

    To evaluate the wear of three different modified ceramics along with a conventional porcelain and the wear of opposing enamel at initial wear cycle on a two-body and a three-body wear simulation. Modified ceramics used in this study included a low fusing/low crystal porcelain (Finesse), a high fusing/low crystal porcelain (Softspar), and a heat-pressable ceramic (IPS Empress). A conventional porcelain (Ceramco II) was used as the control material. Hemispherical shaped ceramic styli (1/8 inch in diameter) made of respective materials were fabricated according to the manufacturers' directions. Proximal surfaces of non-carious human molars were ground flat within the enamel with a silicon carbide paper to 600 grit with copious irrigation. They were perpendicularly opposed to each other with or without intermediate material as a food bolus and subjected to in vitro wear test by a UAB wear simulator. A 75.6 N load was applied vertically onto the surface at 1.2 Hz. The surface was duplicated after respective wear cycles. Seven specimens were tested for each group of both simulations. The enamel wear loss when opposing the modified ceramics was less than the Ceramco II control which exhibited the greatest values. The IPS Empress material showed the least amount of wear among them. Statistically significant differences were seen between the IPS Empress and the Ceramco II for every cycle interval evaluated (ANOVA, P < 0.05). Although the enamel wear loss when opposing the IPS Empress was significantly less (ANOVA, P < 0.05) than the others until 20,000 wear cycles, no significant differences were found among the modified ceramics at the end of 50,000 wear cycles. The concentric wear patterns were already prominent at 5,000 wear cycles on two-body wear, however, the wear facet of the three-body wear was smaller (the wear depth of 0-5 microm) than the two-body wear test, as it was quite similar to the one of the two-body wear test at 100 wear cycles. On the other hand

  20. Epidural application of spinal instrumentation particulate wear debris: a comprehensive evaluation of neurotoxicity using an in vivo animal model.

    PubMed

    Cunningham, Bryan W; Hallab, Nadim J; Hu, Nianbin; McAfee, Paul C

    2013-09-01

    The introduction and utilization of motion-preserving implant systems for spinal reconstruction served as the impetus for this basic scientific investigation. The effect of unintended wear particulate debris resulting from micromotion at spinal implant interconnections and bearing surfaces remains a clinical concern. Using an in vivo rabbit model, the current study quantified the neural and systemic histopathological responses following epidural application of 11 different types of medical-grade particulate wear debris produced from spinal instrumentation. A total of 120 New Zealand White rabbits were equally randomized into 12 groups based on implant treatment: 1) sham (control), 2) stainless steel, 3) titanium alloy, 4) cobalt chromium alloy, 5) ultra-high molecular weight polyethylene (UHMWPe), 6) ceramic, 7) polytetrafluoroethylene, 8) polycarbonate urethane, 9) silicone, 10) polyethylene terephthalate, 11) polyester, and 12) polyetheretherketone. The surgical procedure consisted of a midline posterior approach followed by resection of the L-6 spinous process and L5-6 ligamentum flavum, permitting interlaminar exposure of the dural sac. Four milligrams of the appropriate treatment material (Groups 2-12) was then implanted onto the dura in a dry, sterile format. All particles (average size range 0.1-50 μm in diameter) were verified to be endotoxin free prior to implantation. Five animals from each treatment group were sacrificed at 3 months and 5 were sacrificed at 6 months postoperatively. Postmortem analysis included epidural cultures and histopathological assessment of local and systemic tissue samples. Immunocytochemical analysis of the spinal cord and overlying epidural fibrosis quantified the extent of proinflammatory cytokines (tumor necrosis factor-α, tumor necrosis factor-β, interleukin [IL]-1α, IL-1β, and IL-6) and activated macrophages. Epidural cultures were negative for nearly all cases, and there was no evidence of particulate debris or

  1. Extremely high wear resistance and ultra-low friction behaviour of oxygen-plasma-treated nanocrystalline diamond films

    NASA Astrophysics Data System (ADS)

    Radhika, R.; Kumar, N.; Sankaran, K. J.; Dumpala, Ravikumar; Dash, S.; Ramachandra Rao, M. S.; Arivuoli, D.; Tyagi, A. K.; Tai, N. H.; Lin, I.-Nan

    2013-10-01

    The diamond nanowire (DNW) film was deposited by N2-enriched microwave plasma-enhanced chemical vapour deposition (MPECVD) process. As-deposited DNW film was treated in O2 plasma which resulted in chemical and microstructural modification. Sheath of the DNW film is chemically constituted by amorphous carbon (a-C)- and graphite (sp2C=C)-like bonding. However, nanowires transformed into ultra-small spherical grains after the O2-plasma treatments. In this condition, a-C and sp2C=C bonding significantly reduced due to plasma etching caused by oxygen atoms. After the O2-plasma treatment, formation of functional groups such as C=O, C-O-C, O-H, O-CH3 and H2O was observed on the surface and inside the wear track as evident from the micro FTIR analysis. H2O is hydrogen bonded to oxygen-containing groups such as -OH and -H. The O2-plasma-exposed DNW film exhibits surface charging and causes formation of dangling bonds and electron trapping centres. This results in significant decrease in contact angle, hence superhydrophilic behaviour. The friction coefficient of O2-plasma-treated film showed super low value ˜0.002 with high wear resistance 2 × 10-12 mm3 N-1 m-1. In the reciprocating ball-on-disc tribology test, only ˜80 nm wear loss was observed after the 1 km of sliding distance at 10 N loads. Such an advance in tribological properties is explained by passivation of covalent carbon bonding and transformation of sliding surfaces by weak van der Waals and hydrogen bondings. High surface energy and the consequent superhydrophilic behaviour of film is attributed to the formation of the above-mentioned functional groups on the surface. This protects against deformation of the wear track leading to extremely high wear resistance.

  2. Ti6Al4V Blade Wear Behavior During High-Speed Rubbing with NiAl-hBN Abradable Seal Coating

    NASA Astrophysics Data System (ADS)

    Xue, Weihai; Gao, Siyang; Duan, Deli; Zhang, Jiaping; Liu, Yang; Li, Shu

    2016-12-01

    The high-speed rubbing wear behavior between a Ti6Al4V blade and a NiAl-hBN seal coating was studied with a high-speed rub test rig. Blade wear behavior, which had not received enough attentions, was the key concern of this study. The rub tests conducted at different linear speeds and single-pass depths indicated that although wear distance was constant and rub forces decreased at high linear speed, blade wear increased with the increment of linear speed when single-pass depth was invariable. According to scanning electron microscopy, x-ray diffraction, electron probe microanalysis and microhardness analyses of the wear scars, different blade and coating wear mechanisms were observed when rubbed at different linear speeds. Remarkably, when rubbing was done at high linear speed, there was severe blade oxidation with the generation of oxidation layer full of cracks and high-hardness transfer layer in the coating wear scar, and these were identified as reasons of aggravated blade wear.

  3. Ti6Al4V Blade Wear Behavior During High-Speed Rubbing with NiAl-hBN Abradable Seal Coating

    NASA Astrophysics Data System (ADS)

    Xue, Weihai; Gao, Siyang; Duan, Deli; Zhang, Jiaping; Liu, Yang; Li, Shu

    2017-02-01

    The high-speed rubbing wear behavior between a Ti6Al4V blade and a NiAl-hBN seal coating was studied with a high-speed rub test rig. Blade wear behavior, which had not received enough attentions, was the key concern of this study. The rub tests conducted at different linear speeds and single-pass depths indicated that although wear distance was constant and rub forces decreased at high linear speed, blade wear increased with the increment of linear speed when single-pass depth was invariable. According to scanning electron microscopy, x-ray diffraction, electron probe microanalysis and microhardness analyses of the wear scars, different blade and coating wear mechanisms were observed when rubbed at different linear speeds. Remarkably, when rubbing was done at high linear speed, there was severe blade oxidation with the generation of oxidation layer full of cracks and high-hardness transfer layer in the coating wear scar, and these were identified as reasons of aggravated blade wear.

  4. High Kinetic Energy Penetrator Shielding and High Wear Resistance Materials Fabricated with Boron Nitride Nanotubes (BNNTS) and BNNT Polymer Composites

    NASA Technical Reports Server (NTRS)

    Kang, Jin Ho (Inventor); Park, Cheol (Inventor); Sauti, Godfrey (Inventor); Smith, Michael W. (Inventor); Jordan, Kevin C. (Inventor); Lowther, Sharon E. (Inventor); Bryant, Robert George (Inventor)

    2015-01-01

    Boron nitride nanotubes (BNNTs), boron nitride nanoparticles (BNNPs), carbon nanotubes (CNTs), graphites, or combinations, are incorporated into matrices of polymer, ceramic or metals. Fibers, yarns, and woven or nonwoven mats of BNNTs are used as toughening layers in penetration resistant materials to maximize energy absorption and/or high hardness layers to rebound or deform penetrators. They can be also used as reinforcing inclusions combining with other polymer matrices to create composite layers like typical reinforcing fibers such as Kevlar.RTM., Spectra.RTM., ceramics and metals. Enhanced wear resistance and usage time are achieved by adding boron nitride nanomaterials, increasing hardness and toughness. Such materials can be used in high temperature environments since the oxidation temperature of BNNTs exceeds 800.degree. C. in air. Boron nitride based composites are useful as strong structural materials for anti-micrometeorite layers for spacecraft and space suits, ultra strong tethers, protective gear, vehicles, helmets, shields and safety suits/helmets for industry.

  5. Deflectometric analysis of high volume injection molds for production of occupational eye wear.

    PubMed

    Speck, Alexis; Zelzer, Benedikt; Speich, Marco; Börret, Rainer; Langenbucher, Achim; Eppig, Timo

    2013-12-01

    Most of the protective eye wear devices currently on the market are manufactured on simple polycarbonate shields, produced by injection molding techniques. Despite high importance of optical quality, injection molds are rarely inspected for surface quality before or during the manufacturing process. Quality degradation is mainly monitored by optical testing of the molded parts. The purpose of this work was to validate a non-contact deflectometric measurement technique for surface and shape analysis of injection molds to facilitate deterministic surface quality control and to monitor minor conformity of the injection mold with the design data. The system is based on phase-measuring deflectometry with a operating measurement field of 80×80 mm(2) (±18° slope), a lateral resolution of 60μm and a local sensitivity of some nanometers. The calibration was tested with a calibration normal and a reference sphere. The results were crosschecked against a measurement of the same object with a tactile coordinate measuring machine. Eight injection molds for production of safety goggles with radii of +58mm (convex) and -60mm (concave) were measured in this study. The molds were separated into two groups (cavity 1 and 2 of the tool with different polishing techniques) and measured to test whether the measurement tool could extract differences. The analysis was performed on difference height between the measured surface and the spherical model. The device could derive the surface change due to polishing and discriminate between both polishing techniques, on the basis of the measured data. The concave nozzle sides of the first group (cavity 1) showed good shape conformity. In comparison, the nozzle sides of the second group (cavity 2) showed local deviations from design data up to 14.4μm. Local form variations of about 5μm occurred in the field of view. All convex ejector sides of both groups (cavity 1 and 2) showed rotational symmetric errors and the molds were measured in

  6. Effects of duration of wearing high-heeled shoes on plantar pressure.

    PubMed

    Yin, Chun-Ming; Pan, Xiao-Hua; Sun, Yu-Xin; Chen, Zhi-Bin

    2016-10-01

    In the present study we investigated the effects of different durations of using high-heeled shoes on plantar pressure and gait. A questionnaire survey and dynamic plantar pressure measurements were performed in 20 control females and 117 females who had worn high-heeled shoes for a long time. According to the duration of using high-heeled shoes (as specified in the questionnaire), subjects were divided into a control group and five groups with different durations of use (i.e. <2years, 2-5years, 6-10years, 11-20years and >20years). Parameters, including peak pressure, impulse and pressure duration, in different plantar regions were measured with the Footscan pressure plate. The 2-5years group had smaller midfoot contact areas for both feet and higher subtalar joint mobility, while the 6-10years group had larger midfoot contact areas for both feet and prolonged foot flat phase during gait. The peak pressure and impulse under the second and fourth metatarsus were increased with the prolonged wearing of high-heeled shoes, and the pressure and impulse under the midfoot were substantially reduced in the 2-5years group. The findings suggest that long-term use of high-heeled shoes can induce changes in arch morphology: the longitudinal arch tends to be elevated within 2-5years; the longitudinal arch tends to be flattened within 6-10years; and the forefoot latitudinal arch tends to collapse in more than 20years. Copyright © 2016. Published by Elsevier B.V.

  7. Effect of high-pressure torsion on the microstructure and wear behavior of NiTi alloy

    NASA Astrophysics Data System (ADS)

    Farvizi, Mohammad; Akbarpour, Mohammad Reza; Yoon, Eun Yoo; Kim, Hyoung Seop

    2015-09-01

    The wear property of NiTi is one of the most important properties of this alloy. In the current study, the effect of high-pressure torsion (HPT) process on the wear properties of an austenitic NiTi shape memory alloy is investigated. Full density NiTi samples with a composition of Ti-56 wt% Ni are fabricated using hot isostatic pressing (HIP), followed by the HPT process at room temperature, with an applied pressure of 6 GPa for 10 turns. The microstructural analysis reveals that the HIP-processed samples with a B2-NiTi phase evolve into significant grain refinement after HPT process and an interwoven B2-B19' nanocrystalline/amorphous structure formed, leading to increased hardness in these samples. The results of the wear tests using a ball-on-disc configuration at room temperature demonstrate that the wear performance of the samples is improved after the HPT process. This is due to greater hardness and better pseudo-elasticity in the HPT-processed samples.

  8. Effect of niobium interlayer on high-temperature sliding friction and wear of silver films on alumina

    SciTech Connect

    Erdemir, A.; Erck, R.A.

    1994-03-01

    We investigated the effect of a thin Nb bond layer (15--20 mn thick) on the high-temperature sliding friction and wear of silver films ({approx}1.5 {mu}m thick) produced on {alpha}-alumina (Al{sub 2}O{sub 3}) substrates by ion-beam assisted deposition. The friction coefficients of test pairs without an Ag film fluctuated between 0.8 to 1.1, whereas the friction coefficients of pairs with an Ag film were 0.32 to 0.5. The wear of uncoated Al{sub 2}O{sub 3} balls sliding against the Ag-coated flats was reduced by factors of 25 to {approx}2000, depending on test temperature and the presence or absence of an Nb bond layer. The wear of silver-coated flats was virtually unmeasurable after tests at temperatures up to 400C. At much higher temperatures (e.g., 600C), Ag films without an Nb bond layer delaminated from the sliding surfaces and lost their effectiveness; however, Ag films with an Nb bond layer remained intact on the sliding surfaces of the Al{sub 2}O{sub 3} substrates even at 600C and continued to impart low friction and low wear.

  9. Effects of high-temperature hydrogenation treatment on sliding friction and wear behavior of carbide-derived carbon films.

    SciTech Connect

    Erdemir, A.; Kovalchenko, A.; McNallan, M. J.; Welz, S.; Lee, A.; Gogotsi, Y.; Carroll, B.; Energy Technology; Univ. of Illinois; Drexel Univ.

    2004-01-01

    In this study, we investigated the effects of a high-temperature hydrogenation treatment on the sliding friction and wear behavior of nanostructured carbide-derived carbon (CDC) films in dry nitrogen and humid air environments. These films are produced on the surfaces of silicon carbide substrates by reacting the carbide phase with chlorine or chlorine-hydrogen gas mixtures at 1000 to 1100 C in a sealed tube furnace. The typical friction coefficients of CDC films in open air are in the range of 0.2 to 0.25, but in dry nitrogen, the friction coefficients are 0.15. In an effort to achieve lower friction on CDC films, we developed and used a special hydrogenation process that was proven to be very effective in lowering friction of CDC films produced on SiC substrates. Specifically, the films that were post-hydrogen-treated exhibited friction coefficients as low as 0.03 in dry nitrogen, while the friction coefficients in humid air were 0.2. The wear of Si{sub 3}N{sub 4} counterface balls was hard to measure after the tests, while shallow wear tracks had formed on CDC films on SiC disks. Detailed mechanical and structural characterizations of the CDC films and sliding contact surfaces were done using a series of analytical techniques and these findings were correlated with the friction and wear behaviors of as-produced and hydrogen-treated CDC films.

  10. The influence of irradiation dose on mechanical properties and wear resistance of molded and extruded ultra high molecular weight polyethylene.

    PubMed

    Xiong, Lei; Xiong, Dangsheng

    2012-05-01

    Ultra high molecular weight polyethylene (UHMWPE) is a type of biomedical material used in total joint replacement. In this study, molded and extruded UHMWPE was used to investigate the influence of irradiation dose on its mechanical properties and wear resistance. The results of tensile and compressive tests showed that tensile properties decreased as the irradiation dose increased. Compressive properties decreased significantly after irradiation, but then increased as the irradiation dose increased. Microhardness also had a similar variety tendency as compressive properties. It could be corresponding to the variety of crystallinity for UHMWPE. The fracture surfaces of tensile samples indicated that molded and extruded UHMWPE had a similar fracture mechanism, although the tensile properties were significantly different. The wear tests of knee joint moving simulator showed that the wear rate of molded and extruded UHMWPE decreased as the irradiation dose increased, and a significant reduction of wear rate was exhibited till the irradiation dose of 100 kGy under saline lubrication, and 150 kGy under calf serum lubrication. The IR results indicated that packaging and remelting in vacuum was an effective method to remove oxygen in UHMWPE blocks.

  11. Improved resistance to wear and fatigue fracture in high pressure crystallized vitamin E-containing ultra-high molecular weight polyethylene

    PubMed Central

    Oral, Ebru; Beckos, Christine A. Godleski; Lozynsky, Andrew J.; Malhi, Arnaz S.; Muratoglu, Orhun K.

    2013-01-01

    Higher crystallinity and extended chain morphology are induced in ultra-high molecular weight polyethylene (UHMWPE) in the hexagonal phase at temperatures and pressures above the triple point, resulting in improved mechanical properties. In this study, we report the effects of the presence of a plasticizing agent, namely vitamin E (α-tocopherol), in UHMWPE during high pressure crystallization. We found that this new vitamin E-blended and high pressure crystallized UHMWPE (VEHPE) has improved fatigue strength and wear resistance compared to virgin high pressure crystallized (HP) UHMWPE. This suggested different mechanisms of wear reduction and fatigue crack propagation resistance in UHMWPE. PMID:19135247

  12. Improved resistance to wear and fatigue fracture in high pressure crystallized vitamin E-containing ultra-high molecular weight polyethylene.

    PubMed

    Oral, Ebru; Godleski Beckos, Christine A; Lozynsky, Andrew J; Malhi, Arnaz S; Muratoglu, Orhun K

    2009-04-01

    Higher crystallinity and extended chain morphology are induced in ultra-high molecular weight polyethylene (UHMWPE) in the hexagonal phase at temperatures and pressures above the triple point, resulting in improved mechanical properties. In this study, we report the effects of the presence of a plasticizing agent, namely vitamin E (alpha-tocopherol), in UHMWPE during high pressure crystallization. We found that this new vitamin E-blended and high pressure crystallized UHMWPE (VEHPE) has improved fatigue strength and wear resistance compared to virgin high pressure crystallized (HP) UHMWPE. This suggested different mechanisms of wear reduction and fatigue crack propagation resistance in UHMWPE.

  13. Effect of experimental parameters on the high-stress abrasive wear behavior of steels and a software package for its prediction

    SciTech Connect

    Dasgupta, R.; Roy, A.; Prasad, B.K.; Yegneswaran, A.H.

    1999-06-01

    The effect of different experimental factors on the high-stress abrasive wear properties of steels has been studied. A correlation among the factors has been established by linear regression analysis. A computer software in Microsoft Basic language utilizing linear regression analysis has been developed with the capability of predicting the wear response of steels from the experimental factors.

  14. Facile and scalable preparation of highly wear-resistance superhydrophobic surface on wood substrates using silica nanoparticles modified by VTES

    NASA Astrophysics Data System (ADS)

    Jia, Shanshan; Liu, Ming; Wu, Yiqiang; Luo, Sha; Qing, Yan; Chen, Haibo

    2016-11-01

    In this study, an efficient, facile method has been developed for fabricating superhydrophobic surfaces on wood substrates using silica nanoparticles modified by VTES. The as-prepared superhydrophobic wood surface had a water contact angle of 154° and water slide angle close to 0°. Simultaneously, this superhydrophobic wood showed highly durable and robust wear resistance when having undergone a long period of sandpaper abrasion or being scratched by a knife. Even under extreme conditions of boiling water, the superhydrophobicity of the as-prepared wood composite was preserved. Characterizations by scanning electron microscopy, energy-dispersive X-ray spectroscopy, and Fourier transform infrared spectroscopy showed that a typical and tough hierarchical micro/nanostructure was created on the wood substrate and vinyltriethoxysilane contributed to preventing the agglomeration of silica nanoparticles and serving as low-surface-free-energy substances. This superhydrophobic wood was easy to fabricate, mechanically resistant and exhibited long-term stability. Therefore, it is considered to be of significant importance in the industrial production of functional wood, especially for outdoor applications.

  15. A comparison of the wear and physical properties of silane cross-linked polyethylene and ultra-high molecular weight polyethylene.

    PubMed

    Sakoda, H; Voice, A M; McEwen, H M; Isaac, G H; Hardaker, C; Wroblewski, B M; Fisher, J

    2001-12-01

    Cross-linked polyethylenes are being introduced widely in acetabular cups in hip prostheses as a strategy to reduce the incidence of wear debris-induced osteolysis. It will be many years before substantial clinical data can be collected on the wear of these new materials. Silane cross-linked polyethylene (XLPE) was introduced into clinical practice in a limited series of acetabular cups in 1986 articulating against 22.225-mm alumina ceramic femoral heads and showed reduced wear rates compared with conventionally sterilized (gamma irradiation in air) ultra-high molecular weight polyethylene (UHMWPE). We compared the wear of XLPE manufactured in 1986 with the wear of UHMWPE manufactured in 1986 in nonirradiated and irradiated forms. In the nonirradiated forms, the wear of XLPE was 3 times less than UHWMPE when articulating against smooth counterfaces. The nonirradiated materials did not show signs of oxidation. In the irradiated forms, only UHMWPE showed high levels of oxidation, and this caused a substantial increase in wear. Antioxidants added to XLPE during processing gave resistance to oxidative degradation. When sliding against scratched counterfaces, the wear of UHMWPE increased by a factor of 2 to 3 times. Against the same scratched counterfaces, the wear of XLPE increased dramatically by 30 to 200 times. This difference may be attributed to the reduction in toughness of XLPE. Clinically, XLPE has been articulated against damage-resistant ceramic heads, and this probably has been an important factor in contributing to reduced wear. New cross-linked polyethylenes differ considerably from XLPE. This study indicates that it is prudent to examine the wear of new polyethylenes under a range of conditions that may occur in vivo.

  16. Effect of cryogenic treatment on wear resistance of Ti-6Al-4V alloy for biomedical applications.

    PubMed

    Gu, Kaixuan; Wang, Junjie; Zhou, Yuan

    2014-02-01

    The effect of cryogenic treatment on wear resistance of Ti-6Al-4V alloy for biomedical applications was experimentally investigated in this paper. Cryogenic treatments with the same soaking time of 24h at different temperatures of -80°C, -140°C and -196°C were conducted and the treatments at the same temperature of -196°C were then further given different soaking time of 3h, 48h and 72h to be investigated. After cryogenic treatment, the Vickers hardness of specimens was measured. Wear resistance of Ti-6Al-4V alloy was measured by pin-on-disk wear test under dry sliding condition. The results demonstrated that the Vickers hardness increased slightly with the reduction of temperature while it increased obviously with the elongation of soaking time at -196°C. The friction coefficients of specimens cryo-treated at -196°C were lower than those of untreated and of cryo-treated at -80°C and -140°C. And the longer the soaking time is during the cryogenic treatment, the higher the friction coefficient reduction can be achieved. The obvious reduction of mass loss can be obtained at -196°C with 72h soaking. The X-ray diffraction (XRD) and scanning electron microscopy (SEM) were used to detect the microstructure and worn surface of specimens. By cryogenic treatment, the plowing in the worn surface was smoothed and shallowed, and the degree of plastic deformation in the subsurface was decreased. There was no obvious phase transformation which can be detected in the microstructure after cryogenic treatment. However, the tendency of refinement in grain size can be detected by XRD which improved the wear resistance of Ti-6Al-4V alloy. © 2013 Published by Elsevier Ltd.

  17. Wearing gloves in the hospital

    MedlinePlus

    Infection control - wearing gloves; Patient safety - wearing gloves; Personal protective equipment - wearing gloves; PPE - wearing gloves; Nosocomial infection - wearing gloves; Hospital acquired infection - wearing gloves

  18. Ceramic-on-metal for total hip replacement: mixing and matching can lead to high wear.

    PubMed

    Affatato, Saverio; Spinelli, Michele; Zavalloni, Mara; Traina, Francesco; Carmignato, Simone; Toni, Aldo

    2010-04-01

    Ceramic-on-ceramic and metal-on-metal bearing surfaces are often employed for total hip replacement because of their resistance to wear. However, they have some limits: brittleness is a major concern for ceramic, and ion release is a drawback for metal. To reduce the effect of these limitations, a hybrid coupling of ceramic-on-metal has been proposed. The theoretical advantage of this new coupling might lead orthopedic surgeons to use it indiscriminately. We asked whether the wear rate of this innovative solution was comparable with that of ceramic-on-ceramic, which is considered to be the gold standard for wear resistance. In a hip simulator study, we tested the wear pattern of a hybrid ceramic-on-metal coupling supplied by the same distributor; in particular, three different configurations were tested for 5 million cycles: 36-mm ceramic-on-ceramic, 32-mm and 36-mm ceramic-on-metal. These combinations were gravimetrically and geometrically evaluated. After 5 million cycles, the volumetric loss for the metal acetabular cups (Phi 36-mm) was 20-fold greater than that of the ceramic cups of the same size (Phi 36-mm); a volumetric loss of 4.35 mm(3) and 0.26 mm(3) was observed, respectively, for ceramic-on-metal and ceramic-on-ceramic combinations. Significant statistical differences were observed between all 36-mm different combinations (P < 0.0001). The increased diameter of the 36-mm ceramic-on-metal configuration resulted in a lower volumetric loss compared with that of the 32-mm ceramic-on-metal configuration. Our findings showed an increase in wear for the proposed hybrid specimens with respect to that of the ceramic-on-ceramic ones. This confirms that even in the case of ceramic-on-metal bearings, mixing and matching could not prove effective wear behavior, not even comparable with that of the ceramic-on-ceramic gold standard.

  19. Low wear partially fluorinated polyimides

    NASA Technical Reports Server (NTRS)

    Fusaro, R. L.; Hady, W. F.

    1984-01-01

    Tribological studies were conducted on five different polyimide solid bodies formulated from the diamine 2,2-bis 4-(4-aminophenoxy)phenyl hexafluoropropane (4-BDAF) and the dianhydrides pyromellitic acid (PMDS) and benzophenonetetracarboxylic acid (BTDA). The following polyimides were evaluated 4-BDAF/PMDA, 4-BDAF/BTDA, 4-BDAF/80 mole percent PMDA, 20 mole percent BTDA, 4-BDAF/60 mole percent BTDA. Friction coefficients, polyimide wear rates, polyimide surface morphology and transfer films were evaluated at sliding speeds of 0.31 to 11.6 m/s and at temperatures of 25 C to 300 C. The results indicate that the tribological properties are highly dependent on the composition of the polyimide and on the experimental conditions. Two polyimides were found which produced very low wear rates but very high friction coefficients (greater than 0.85) under ambient conditions. They offer considerable potential for high traction types of application such as brakes.

  20. Low wear partially fluorinated polyimides

    SciTech Connect

    Fusaro, R.L.; Hady, W.F.

    1984-01-01

    Tribological studies were conducted on five different polyimide solid bodies formulated from the diamine 2,2-bis 4-(4-aminophenoxy)phenyl hexafluoropropane (4-BDAF) and the dianhydrides pyromellitic acid (PMDS) and benzophenonetetracarboxylic acid (BTDA). The following polyimides were evaluated 4-BDAF/PMDA, 4-BDAF/BTDA, 4-BDAF/80 mole percent PMDA, 20 mole percent BTDA, 4-BDAF/60 mole percent BTDA. Friction coefficients, polyimide wear rates, polyimide surface morphology and transfer films were evaluated at sliding speeds of 0.31 to 11.6 m/s and at temperatures of 25 C to 300 C. The results indicate that the tribological properties are highly dependent on the composition of the polyimide and on the experimental conditions. Two polyimides were found which produced very low wear rates but very high friction coefficients (greater than 0.85) under ambient conditions. They offer considerable potential for high traction types of application such as brakes.

  1. Ultra-High Molecular Weight Polyethylene: Influence of the Chemical, Physical and Mechanical Properties on the Wear Behavior. A Review

    PubMed Central

    Bellare, Anuj; Bistolfi, Alessandro

    2017-01-01

    Ultra-high molecular weight polyethylene (UHMWPE) is the most common bearing material in total joint arthroplasty due to its unique combination of superior mechanical properties and wear resistance over other polymers. A great deal of research in recent decades has focused on further improving its performances, in order to provide durable implants in young and active patients. From “historical”, gamma-air sterilized polyethylenes, to the so-called first and second generation of highly crosslinked materials, a variety of different formulations have progressively appeared in the market. This paper reviews the structure–properties relationship of these materials, with a particular emphasis on the in vitro and in vivo wear performances, through an analysis of the existing literature. PMID:28773153

  2. Definition and evaluation of testing scenarios for knee wear simulation under conditions of highly demanding daily activities.

    PubMed

    Schwiesau, Jens; Schilling, Carolin; Kaddick, Christian; Utzschneider, Sandra; Jansson, Volkmar; Fritz, Bernhard; Blömer, Wilhelm; Grupp, Thomas M

    2013-05-01

    The objective of our study was the definition of testing scenarios for knee wear simulation under various highly demanding daily activities of patients after total knee arthroplasty. This was mainly based on a review of published data on knee kinematics and kinetics followed by the evaluation of the accuracy and precision of a new experimental setup. We combined tibio-femoral load and kinematic data reported in the literature to develop deep squatting loading profiles for simulator input. A servo-hydraulic knee wear simulator was customised with a capability of a maximum flexion of 120°, a tibio-femoral load of 5000N, an anterior-posterior (AP) shear force of ±1000N and an internal-external (IE) rotational torque of ±50Nm to simulate highly demanding patient activities. During the evaluation of the newly configurated simulator the ability of the test machine to apply the required load and torque profiles and the flexion kinematics in a precise manner was examined by nominal-actual profile comparisons monitored periodically during subsequent knee wear simulation. For the flexion kinematics under displacement control a delayed actuator response of approximately 0.05s was inevitable due to the inertia of masses in movement of the coupled knee wear stations 1-3 during all applied activities. The axial load and IE torque is applied in an effective manner without substantial deviations between nominal and actual load and torque profiles. During the first third of the motion cycle a marked deviation between nominal and actual AP shear load profiles has to be noticed but without any expected measurable effect on the latter wear simulation due to the fact that the load values are well within the peak magnitude of the nominal load amplitude. In conclusion the described testing method will be an important tool to have more realistic knee wear simulations based on load conditions of the knee joint during activities of daily living. Copyright © 2012 IPEM. Published by

  3. Quality of life in high myopia: implantable Collamer lens implantation versus contact lens wear.

    PubMed

    Ieong, Alvin; Rubin, Gary S; Allan, Bruce D S

    2009-02-01

    To compare vision-related quality of life in implantable Collamer lens (ICL) recipients and successful contact lens (CL) wearers not seeking refractive surgery. A comparative cross-sectional study of consecutive cases. Forty-one consecutive cases of bilateral ICL implantation in Moorfields Eye Hospital, London, and a control group of 41 CL wearers with a similar starting level of myopia attending consecutively at 1 of 2 community optometric practices in the London area. Quality of Life Impact of Refractive Correction questionnaire administration in a semistructured interview. Quality of Life Impact of Refractive Correction score. Quality of Life Impact of Refractive Correction scores were significantly higher (P<0.001) in ICL recipients (53.67+/-4.50) than in CL wearers (44.42+/-5.07). Age (mean+/-standard deviation [SD], 37.7+/-7 vs. 37.5+/-7.3), gender distribution (% female, 90% vs. 74%; P = 0.295), and preoperative (ICL recipients) or uncorrected (CL wearers) refractive error (mean refractive spherical equivalent+/-SD, 11.0+/-2.7 vs. 11.3+/-3.5) were similar in ICL recipients and CL wearers, respectively. Postoperative uncorrected visual acuities in ICL recipients (0.04 [20/20]+/-0.18) and CL-corrected visual acuities in control patients (0.01 [20/20]+/-0.14) measured in the better eye in each group also were similar (P = 0.53). Implantable Collamer lens implantation may offer significant quality-of-life advantages over CL wear for patients with high myopia. The author(s) have no proprietary or commercial interest in any materials discussed in this article.

  4. Prediction of plastic strains in ultra-high molecular weight polyethylene due to microscopic asperity interactions during sliding wear.

    PubMed

    McNie, C; Barton, D C; Stone, M H; Fisher, J

    1998-01-01

    Studies of explanted femoral heads have shown that scratches caused by bone cement, bone or metallic particles are present on the rubbing surface. This damage has been cited as a cause of increased wear of ultra-high molecular weight polyethylene (UHMWPE) acetabular cups and it is known that the particulate wear debris produced leads to osteolysis. A series of explanted Charnley femoral heads have been surface characterized using a Talysurf 6 profilometer and found to have scratches with lip heights in the size range 0.1-3.25 microns with an average height of 1 micron giving an average aspect ratio (defined as height/half-width) of 0.1. These geometries were incorporated into a finite element model of a stainless steel asperity sliding over UHMWPE under conditions similar to those in an artificial hip system. It was found that as the aspect ratio of the asperity lip increased, the plastic strains both on and below the surface of the UHMWPE increased non-linearly, but that the magnitude of the strain was independent of the asperity height. The asperity aspect ratio was also found to affect the position of the maximum sub-surface strain, as the asperity aspect ratio was increased the maximum strain rose to the surface. The high plastic strains predicted offer an explanation for the highly elevated wear rates in scratched counterface tests and the aspect ratio of scratch lips is therefore a critical determinant of plastic strain.

  5. Wear resistant performance of highly cross-linked and annealed ultra-high molecular weight polyethylene against ceramic heads in total hip arthroplasty.

    PubMed

    Sato, Taishi; Nakashima, Yasuharu; Akiyama, Mio; Yamamoto, Takuaki; Mawatari, Taro; Itokawa, Takashi; Ohishi, Masanobu; Motomura, Goro; Hirata, Masanobu; Iwamoto, Yukihide

    2012-12-01

    The purpose of this study was to examine the effects of ceramic femoral head material, size, and implantation periods on the wear of annealed, cross-linked ultra-high molecular weight polyethylene (UHMWPE) (XLPE) in total hip arthroplasty compared to non-cross-linked conventional UHMWPE (CPE). XLPE was fabricated by cross-linking with 60 kGy irradiation and annealing. Femoral heads made from zirconia and alumina ceramics and cobalt-chrome (CoCr) of 22 or 26 mm diameter were used. In this retrospective cohort study, the femoral head penetration into the cup was measured digitally on radiographs of 367 hips with XLPE and 64 hips with CPE. The average follow-up periods were 6.3 and 11.9 years, respectively. Both XLPE creep and wear rates were significantly lower than those of CPE (0.19 mm vs. 0.44 mm, 0.0001 mm/year vs. 0.09 mm/year, respectively). Zirconia displayed increased wear rates compared to alumina in CPE; however, there was no difference among head materials in XLPE (0.0008, 0.00007, and -0.009 mm/year for zirconia, alumina, and CoCr, respectively). Neither head size or implantation period impacted XLPE wear. In contrast to CPE, XLPE displayed low wear rates surpassing the effects of varying femoral head material, size, implantation period, and patient demographics. Further follow-up is required to determine the long-term clinical performance of the annealed XLPE.

  6. Developing acceptance limits for measured bearing wear of the Space Shuttle Main Engine high pressure oxidizer turbopump

    NASA Technical Reports Server (NTRS)

    Genge, Gary G.

    1991-01-01

    The probabilistic design approach currently receiving attention for structural failure modes has been adapted for obtaining measured bearing wear limits in the Space Shuttle Main Engine high-pressure oxidizer turbopump. With the development of the shaft microtravel measurements to determine bearing health, an acceptance limit was neeed that protects against all known faiure modes yet is not overly conservative. This acceptance criteria limit has been successfully determined using probabilistic descriptions of preflight hardware geometry, empirical bearing wear data, mission requirements, and measurement tool precision as an input for a Monte Carlo simulation. The result of the simulation is a frequency distribution of failures as a function of preflight acceptance limits. When the distribution is converted into a reliability curve, a conscious risk management decision is made concerning the acceptance limit.

  7. Processing, Characterization and Fretting Wear of Zinc Oxide and Silver Nanoparticles Reinforced Ultra High Molecular Weight Polyethylene Biopolymer Nanocomposite

    NASA Astrophysics Data System (ADS)

    Alam, Fahad; Kumar, Anil; Patel, Anup Kumar; Sharma, Rajeev K.; Balani, Kantesh

    2015-04-01

    Ultra-high molecular weight polyethylene (UHMWPE) is the most widely used biopolymer for articulating surfaces, such as an acetabular cup liner interfacing with a metal/ceramic femoral head. However, the formation of wear debris leads to the aseptic loosening of implants. Thus, in order to improve the life span via enhancing the fretting wear resistance, UHMWPE is reinforced with ZnO/Ag nanoparticles. It is envisaged that the ZnO/Ag addition will also exhibit antibacterial properties. In the current study, the synergetic effect of the reinforcement of ZnO/Ag nanoparticles (0-3 wt.% combinations) on the fretting wear behavior of a UHMWPE matrix is assessed. The phase characterization of compression- molded UHMWPE-Ag-ZnO biopolymer nanocomposites has elicited the retention of starting phases. All samples were processed at >98% density using compression molding. Silver and ZnO reinforcement showed enhanced hardness ~20.4% for U3A and 42.0% for U3Z. Fretting wear performance was evaluated at varying loads (5-15 N), keeping in mind the weight at different joints, with constant frequency (5 Hz) as well as amplitude of oscillation (100 µm). Laser surface profilometry showed change of wear volume from 8.6 × 10-5 mm3 for neat polymer to 5.8 × 10-5 mm3 with 1 wt.% Ag + 1 wt.% ZnO reinforcement (at 15 N load). Consequently, the mechanics of resistance offered by Ag and ZnO is delineated in the UHMWPE matrix. Further, S. aureus viability reduction is ~28.7% in cases with 1 wt.% Ag addition, ~42.5% with 1 wt.% ZnO addition, but synergistically increase to ~58.6% and 47.1% when each of Ag and ZnO is added with 1 wt.% and 3 wt.%, respectively (when compared to that of the UHMWPE control sample). Increased wear resistance and superior bioactivity and enhanced anti-bacterial properties of 1 wt.% Ag + 1 wt.% ZnO and 3 wt.% Ag + 3 wt.% ZnO shows the potential use of ZnO-Ag-UHMWPE biopolymer composites as an articulating surface.

  8. The Wear Behavior of HVOF Sprayed Near-Nanostructured WC-17%Ni(80/20)Cr Coatings in Dry and Slurry Wear Conditions

    NASA Astrophysics Data System (ADS)

    Ben Mahmud, Tarek A.; Atieh, Anas M.; Khan, Tahir I.

    2017-07-01

    The ability to deposit nanostructured feedstock by using high-velocity oxygen-fuel (HVOF) spray offers potential improvements in coating hardness, wear resistance and toughness for applications in the oil sands industry. In this study, the wear behavior of a near-nanostructured coating was compared under dry and slurry abrasive wear test using an uncoated AISI-1018 low-carbon steel substrate as a reference. The coating microstructures were analyzed in the as-sprayed, dry and slurry test conditions using scanning electron microscopy, x-ray diffraction and microhardness measurements. Wear behavior of the steel and coating surfaces were assessed using a pin-on-plate wear test under various loads. The results showed that a coating could be successfully deposited using the HVOF spraying technique and with retention of the near-nanosized WC dispersion within the coating structure. The wear rate under dry test conditions was greater for the steel and coating compared to tests performed under slurry conditions. Examination of the wear tracks revealed that the wear mechanism was different for the two test conditions. Wear in the dry test condition resulted from 2-body abrasion, while 3-body abrasion dominated wear in slurry conditions. The latter showed lower wear rates due to a lubricating effect of the oil.

  9. Fabrication and Wear Behavior Analysis on AlCrFeNi High Entropy Alloy Coating Under Dry Sliding and Oil Lubrication Test Conditions

    NASA Astrophysics Data System (ADS)

    Tang, Yipin; Wang, Shouren; Sun, Bin; Wang, Yan; Qiao, Yang

    2016-03-01

    In this paper, AlCrFeNi high entropy alloy coating was fabricated on the surface of Q235 steel using hot pressing sintering process. The coating has the controlled thickness size and excellent mechanical properties. Scanning electron microscopy (SEM), XRD and hardness testing method were used to study the morphology, phase structure and hardness of high entropy alloys coating. The lattice distortion plays a significant role in increasing the hardness. Coating formation mechanism caused by the element diffusion under the hot pressing effect is also discussed in the paper. Simultaneously, the dry sliding and oil lubrication wear tests, wear morphology observation and wear mechanism discussion were completed. As the result shows, AlCrFeNi high entropy alloys coating exhibits superior wear resistance either at dry sliding or oil lubrication tests owing to its hard high entropy solid solution structure.

  10. Influence of microscopic surface asperities on the wear of ultra-high molecular weight polyethylene in a knee prosthesis.

    PubMed

    Cho, C-H; Murakami, T; Sawae, Y

    2010-01-01

    The wear of ultra-high molecular weight polyethylene (UHMWPE) in knee and hip prostheses is one of the major factors restricting the longevity of these implants. A number of microscopic scratches caused by various factors were observed on the metallic femoral components of the retrieved knee prostheses with an anatomical design. It appears that microscopic surface asperities caused by this surface damage contribute to increasing and/or accelerating the wear of the UHMWPE tibial insert. In this study, in the first step, microscopic observations and surface roughness measurements of several retrieved metallic femoral components were performed in order to produce simplified two-dimensional (2D) finite-element method (FEM) models of a microscopic surface asperity using roughness parameters. Next, a three-dimensional (3D) microscopic surface profile measurement of the damaged surface of a retrieved metallic femoral component and the reproduction of the femoral component surface were performed in order to produce 3D FEM models of a microscopic surface asperity based on actual measurement data. 2D and 3D elastoplastic contact analyses between a metallic microscopic surface asperity and UHMWPE were also performed in order to investigate the mechanical state and microscopic wear of UHMWPE caused by a metallic microscopic surface asperity. The analytical findings of this study suggest that the aspect ratio, shape ratio, and indentation depth of the microscopic surface asperity have significant influence on increasing and/or accelerating the wear of UHMWPE. Higher aspect ratios, shape ratios, and indentation depths cause higher contact stresses and plastic strains in UHMWPE.

  11. The gigapixel image concept for graphic SEM documentation. Applications in archeological use-wear studies.

    PubMed

    Vergès, Josep M; Morales, Juan I

    2014-10-01

    In this paper, we propose a specific procedure to create gigapixel-like images from SEM (scanning electron microscope) micrographs. This methodology allows intensive SEM observations to be made for those disciplines that require of large surfaces to be analyzed at different scales once the SEM sessions have been completed (e.g., stone tools use-wear studies). This is also a very useful resource for academic purposes or as a support for collaborative studies, thus reducing the number of live observation sessions and the associated expense. Copyright © 2014 Elsevier Ltd. All rights reserved.

  12. Unveiling Ultra-High Temperature Wear and Indentation Damage Mechanisms of Thermal Barrier Coatings

    NASA Astrophysics Data System (ADS)

    Bumgardner, Clifton; Li, Xiaodong

    2015-12-01

    Thermal barrier coatings are necessary to protect turbine blades within jet engines from extreme environments that the substrate material may not be capable of withstanding. Therefore, failure of the coating due to wear during its operational lifecycle is a critical event. In order to understand the failure mechanisms of the coating layers, a zirconia-based coating on a nickel alloy substrate was subjected to wear testing to simulate pressure and temperature conditions within a jet engine. Using a Hertzian contact model, the maximum shear and its depth were determined and analyzed in conjunction with the coating material properties and scanning electron microscopy and energy dispersive x-ray spectrometry images. The coupled imaging and contact model analyses made possible the identification of the location and time of delamination and its underlying causes. Our findings provide key insights for the development of more resilient thermal barrier coatings.

  13. Wear Resistant Amorphous and Nanocomposite Coatings

    SciTech Connect

    Racek, O

    2008-03-26

    Glass forming materials (critical cooling rate <10{sup 4}K.s{sup -1}) are promising for their high corrosion and wear resistance. During rapid cooling, the materials form an amorphous structure that transforms to nanocrystalline during a process of devitrification. High hardness (HV 1690) can be achieved through a controlled crystallization. Thermal spray process has been used to apply coatings, which preserves the amorphous/nanocomposite structure due to a high cooling rate of the feedstock particles during the impact on a substrate. Wear properties have been studied with respect to process conditions and feedstock material properties. Application specific properties such as sliding wear resistance have been correlated with laboratory tests based on instrumented indentation and scratch tests.

  14. WEAR RESISTANCE AND MECHANICAL PROPERTIES OF HIGHLY CROSSLINKED UHMWPE DOPED WITH VITAMIN-E

    PubMed Central

    Oral, Ebru; Christensen, Steven D.; Malhi, Arnaz S.; Wannomae, Keith K.; Muratoglu, Orhun K.

    2008-01-01

    Our hypothesis was that cross-linked UHMWPE stabilized with vitamin-E would be wear and fatigue resistant. Acetabular liners were radiation cross-linked, doped with vitamin E and γ-sterilized. Hip simulator wear rate of vitamin E-stabilized UHMWPE was approximately 1 and 6 mg/million-cycles in clean serum and in serum with third-body bone cement particles, respectively; a four to ten-fold decrease from that of conventional UHMWPE. The ultimate strength, yield strength, elongation-at-break and fatigue resistance of vitamin E-stabilized UHMWPE were significantly higher than that of 100-kGy irradiated and melted UHMWPE and were unaffected by accelerated aging. Rim impingement testing with 3.7 mm-thick acetabular liners up to 2 million-cycles showed no significant damage of the cross-linked liners compared to conventional, gamma-sterilized in inert UHMWPE vitamin-E stabilized liners. The data indicate good wear properties and improved mechanical and fatigue properties for vitamin-E stabilized cross-linked UHMWPE. PMID:16781413

  15. Comparison of Periprosthetic Tissue Digestion Methods for Ultra-High Molecular Weight Polyethylene Wear Debris Extraction

    PubMed Central

    Baxter, R.M.; Steinbeck, M.J.; Tipper, J.L.; Parvizi, J.; Marcolongo, M.; Kurtz, S.M.

    2009-01-01

    There is considerable interest in characterization of wear debris from polyethylene (UHMWPE) bearing components used in total joint replacement. To isolate UHMWPE wear debris, tissue samples must be excised from regions adjacent to revised UHMWPE implant components, followed by exposure to one of many available tissue digestion methods. Numerous studies demonstrate successful digestion, but the relative efficiency of each method is not clear. The purpose of this study was to evaluate a variety of conditions for tissue digestion to provide a quantitative comparison of methods. Porcine and human hip tissues were exposed for 24 hr to basic, acidic or enzymatic agents, filtered and digestion efficiency calculated based on the percentage of initial to final tissue weight. Of the conditions tested, 5M NaOH, 5M KOH, 15M KOH or 15.8M HNO3 yielded the most complete porcine hip tissue digestion (<1% residual tissue weight; p<0.05). Proteinase K and Liberase Blendzyme 3 did not effectively digest tissue in a 24 hour period. Similar to results from the porcine dataset, human tissues digestion was most efficient using 5M NaOH, 5M KOH or 15.8M HNO3 (<1% residual tissue weight; p<0.05). To verify that particle surface modifications did not occur after prolonged reagent exposure, GUR415 and Ceridust 3715 particles were immersed in each solution for 24 hours. Overall, this study provides a framework for thorough and efficient digestive methods for UHMWPE wear debris extraction. PMID:19507139

  16. Refractory lining system for high wear area of high temperature reaction vessel

    DOEpatents

    Hubble, D.H.; Ulrich, K.H.

    1998-09-22

    A refractory-lined high temperature reaction vessel comprises a refractory ring lining constructed of refractory brick, a cooler, and a heat transfer medium disposed between the refractory ring lining and the cooler. The refractory brick comprises magnesia (MgO) and graphite. The heat transfer medium contacts the refractory brick and a cooling surface of the cooler, and is composed of a material that accommodates relative movement between the refractory brick and the cooler. The brick is manufactured such that the graphite has an orientation providing a high thermal conductivity in the lengthwise direction through the brick that is higher than the thermal conductivity in directions perpendicular to the lengthwise direction. The graphite preferably is flake graphite, in the range of about 10 to 20 wt %, and has a size distribution selected to provide maximum brick density. The reaction vessel may be used for performing a reaction process including the steps of forming a layer of slag on a melt in the vessel, the slag having a softening point temperature range, and forming a protective frozen layer of slag on the interior-facing surface of the refractory lining in at least a portion of a zone where the surface contacts the layer of slag, the protective frozen layer being maintained at or about the softening point of the slag. 10 figs.

  17. Refractory lining system for high wear area of high temperature reaction vessel

    DOEpatents

    Hubble, D.H.; Ulrich, K.H.

    1998-04-21

    A refractory-lined high temperature reaction vessel comprises a refractory ring lining constructed of refractory brick, a cooler, and a heat transfer medium disposed between the refractory ring lining and the cooler. The refractory brick comprises magnesia (MgO) and graphite. The heat transfer medium contacts the refractory brick and a cooling surface of the cooler, and is composed of a material that accommodates relative movement between the refractory brick and the cooler. The brick is manufactured such that the graphite has an orientation providing a high thermal conductivity in the lengthwise direction through the brick that is higher than the thermal conductivity in directions perpendicular to the lengthwise direction. The graphite preferably is flake graphite, in the range of about 10 to 20 wt %, and has a size distribution selected to provide maximum brick density. The reaction vessel may be used for performing a reaction process including the steps of forming a layer of slag on a melt in the vessel, the slag having a softening point temperature range, and forming a protective frozen layer of slag on the interior-facing surface of the refractory lining in at least a portion of a zone where the surface contacts the layer of slag, the protective frozen layer being maintained at or about the softening point of the slag. 10 figs.

  18. Refractory lining system for high wear area of high temperature reaction vessel

    DOEpatents

    Hubble, David H.; Ulrich, Klaus H.

    1998-01-01

    A refractory-lined high temperature reaction vessel comprises a refractory ring lining constructed of refractory brick, a cooler, and a heat transfer medium disposed between the refractory ring lining and the cooler. The refractory brick comprises magnesia (MgO) and graphite. The heat transfer medium contacts the refractory brick and a cooling surface of the cooler, and is composed of a material that accommodates relative movement between the refractory brick and the cooler. The brick is manufactured such that the graphite has an orientation providing a high thermal conductivity in the lengthwise direction through the brick that is higher than the thermal conductivity in directions perpendicular to the lengthwise direction. The graphite preferably is flake graphite, in the range of about 10 to 20 wt %, and has a size distribution selected to provide maximum brick density. The reaction vessel may be used for performing a reaction process including the steps of forming a layer of slag on a melt in the vessel, the slag having a softening point temperature range, and forming a protective frozen layer of slag on the interior-facing surface of the refractory lining in at least a portion of a zone where the surface contacts the layer of slag, the protective frozen layer being maintained at or about the softening point of the slag.

  19. Refractory lining system for high wear area of high temperature reaction vessel

    DOEpatents

    Hubble, David H.; Ulrich, Klaus H.

    1998-01-01

    A refractory-lined high temperature reaction vessel comprises a refractory ring lining constructed of refractory brick, a cooler, and a heat transfer medium disposed between the refractory ring lining and the cooler. The refractory brick comprises magnesia (MgO) and graphite. The heat transfer medium contacts the refractory brick and a cooling surface of the cooler, and is composed of a material that accommodates relative movement between the refractory brick and the cooler. The brick is manufactured such that the graphite has an orientation providing a high thermal conductivity in the lengthwise direction through the brick that is higher than the thermal conductivity in directions perpendicular to the lengthwise direction. The graphite preferably is flake graphite, in the range of about 10 to 20 wt %, and has a size distribution selected to provide maximum brick density. The reaction vessel may be used for performing a reaction process including the steps of forming a layer of slag on a melt in the vessel, the slag having a softening point temperature range, and forming a protective frozen layer of slag on the interior-facing surface of the refractory lining in at least a portion of a zone where the surface contacts the layer of slag, the protective frozen layer being maintained at or about the softening point of the slag.

  20. Ultralow wear of gallium nitride

    NASA Astrophysics Data System (ADS)

    Zeng, Guosong; Tan, Chee-Keong; Tansu, Nelson; Krick, Brandon A.

    2016-08-01

    Here, we reveal a remarkable (and surprising) physical property of GaN: it is extremely wear resistant. In fact, we measured the wear rate of GaN is approaching wear rates reported for diamond. Not only does GaN have an ultralow wear rate but also there are quite a few experimental factors that control the magnitude of its wear rate, further contributing to the rich and complex physics of wear of GaN. Here, we discovered several primary controlling factors that will affect the wear rate of III-Nitride materials: crystallographic orientation, sliding environment, and coating composition (GaN, InN and InGaN). Sliding in the ⟨ 1 2 ¯ 10 ⟩ is significantly lower wear than ⟨ 1 1 ¯ 00 ⟩ . Wear increases by 2 orders of magnitude with increasing humidity (from ˜0% to 50% RH). III-Nitride coatings are promising as multifunctional material systems for device design and sliding wear applications.

  1. Oxide Ceramic Films Grown on 55Ni-45Ti for NASA and Department of Defense Applications: Unidirectional Sliding Friction and Wear Evaluation

    NASA Technical Reports Server (NTRS)

    Miyoshi, Kazuhisa; Lukco, Dorothy; Cytron, Sheldon J.

    2004-01-01

    An investigation was conducted to examine the friction and wear behavior of the two types of oxide ceramic films furnished by the U.S. Army Research Laboratory, Development and Engineering Center (ARDEC) under Space Act Agreement SAA3 567. These two types of oxide ceramics were grown on 55Ni-45Ti (60 wt% Ni and 40 wt% Ti) substrates: one was a TiO2 with no other species (designated the B film) and the other was a TiO2 with additional species (designated the G film). Unidirectional ball-on-disk sliding friction experiments were conducted with the oxide films in contact with sapphire at 296 K (23 C) in approx. 50-percent relative humidity laboratory air in this investigation. All material characterization and sliding friction experiments were conducted at the NASA Glenn Research Center. The results indicate that both films greatly improve the surface characteristics of 55Ni-45Ti, enhancing its tribological characteristics. Both films decreased the coefficient of friction by a factor of 4 and increased wear resistance by a two-figure factor, though the B film was superior to the G film in wear resistance and endurance life. The levels of coefficient of friction and wear resistance of both films in sliding contact with sapphire were acceptable for NASA and Department of Defense tribological applications. The decrease in friction and increase in wear resistance will contribute to longer wear life for parts, lower energy consumption, reduced related breakdowns, decreased maintenance costs, and increased reliability.

  2. High frequency circular translation pin-on-disk method for accelerated wear testing of ultrahigh molecular weight polyethylene as a bearing material in total hip arthroplasty.

    PubMed

    Saikko, Vesa

    2015-01-21

    The temporal change of the direction of sliding relative to the ultrahigh molecular weight polyethylene (UHMWPE) component of prosthetic joints is known to be of crucial importance with respect to wear. One complete revolution of the resultant friction vector is commonly called a wear cycle. It was hypothesized that in order to accelerate the wear test, the cycle frequency may be substantially increased if the circumference of the slide track is reduced in proportion, and still the wear mechanisms remain realistic and no overheating takes place. This requires an additional slow motion mechanism with which the lubrication of the contact is maintained and wear particles are conveyed away from the contact. A three-station, dual motion high frequency circular translation pin-on-disk (HF-CTPOD) device with a relative cycle frequency of 25.3 Hz and an average sliding velocity of 27.4 mm/s was designed. The pins circularly translated at high frequency (1.0 mm per cycle, 24.8 Hz, clockwise), and the disks at low frequency (31.4mm per cycle, 0.5 Hz, counter-clockwise). In a 22 million cycle (10 day) test, the wear rate of conventional gamma-sterilized UHMWPE pins against polished CoCr disks in diluted serum was 1.8 mg per 24 h, which was six times higher than that in the established 1 Hz CTPOD device. The wear mechanisms were similar. Burnishing of the pin was the predominant feature. No overheating took place. With the dual motion HF-CTPOD method, the wear testing of UHMWPE as a bearing material in total hip arthroplasty can be substantially accelerated without concerns of the validity of the wear simulation.

  3. Body regional influences of L-menthol application on the alleviation of heat strain while wearing firefighter's protective clothing.

    PubMed

    Lee, Joo-Young; Nakao, Kouhei; Bakri, Ilham; Tochihara, Yutaka

    2012-06-01

    The purpose of this study was to investigate the influences of menthol application according to the amount of surface area on physiological and psychological heat strains, along with body regional influences. Male students underwent two stages of experiments: [Experiment 1] Cutaneous thermal threshold test at rest on eight body regions with/without a 0.8% menthol application at T (a) 28°C and 50% RH; [Experiment 2] Six exercise tests with/without a 0.8% menthol spray at T (a) 28°C and 40% RH, while wearing firefighter's protective clothing (No menthol, PC(NO); Face and neck menthol, PC(FN); Upper body menthol, PC(UP); Whole body menthol application, PC(WB)) or wearing normal clothing (No menthol, NC(NO); Upper body menthol, NC(UP)). Experiment 1 showed that menthol caused no significant influence on cutaneous warm thresholds, while menthol applications evoked earlier detection of cool sensations, especially on the chest (P = 0.043). Experiment 2 revealed that NC(UP), PC(UP) and PC(WB) caused lower mean skin temperature, especially with higher peripheral vasoconstrictions on the extremities at rest. During exercise, NC(UP), PC(UP) and PC(WB) induced greater and earlier increases in rectal temperatures (T (re)) and a delayed sweat response, but lessened psychological burdens (P < 0.05). Both physiological and psychological effects of PC(FN) were insignificant. For a composite analysis, individual Menthol Sensitivity Index at cooling in Experiment 1 had significant relationships with the threshold for T (re) increase and changes in heart rate in NC(UP) of Experiment 2 (P < 0.05). Our results indicate that menthol's topical influence is body region-dependent, as well as depending on the exposed body surface area.

  4. Microstructure and Wear Behavior of Atmospheric Plasma-Sprayed AlCoCrFeNiTi High-Entropy Alloy Coating

    NASA Astrophysics Data System (ADS)

    Tian, Li-Hui; Xiong, Wei; Liu, Chuan; Lu, Sheng; Fu, Ming

    2016-12-01

    Due to the advantages such as high strength, high hardness and good wear resistance, high-entropy alloys (HEAs) attracted more and more attentions in recent decades. However, most reports on HEAs were limited to bulk materials. Although a few of studies on atmospheric plasma-sprayed (APS) HEA coatings were carried out, the wear behavior, especially the high-temperature wear behavior of those coatings has not been investigated till now. Therefore, in this study, APS was employed to deposit AlCoCrFeNiTi high-entropy alloy coating using mechanically alloyed AlCoCrFeNiTi powder as the feedstock. The phase structure of the initial powder, the feedstock powder and the as-sprayed coating was examined by an x-ray diffractometer. The surface morphology of the feedstock powder and the microstructure of the as-sprayed coating were analyzed by field emission scanning electron microscopy and energy-dispersive spectroscopy. The bonding strength and the microhardness of the as-sprayed coating were tested. The wear behavior of the coating at 25, 500, 700 and 900 °C was investigated by analysis of the wear surface morphology and measurements of the volume wear rate and the coefficient of friction.

  5. In vivo wear performance of highly cross-linked polyethylene vs. yttria stabilized zirconia and alumina stabilized zirconia at a mean seven-year follow-up

    PubMed Central

    2013-01-01

    Background Zirconia was introduced as an alternative to alumina for use in the femoral head. The yttria stabilized zirconia material was improved by adding alumina. We evaluated highly cross-linked polyethylene wear performance of zirconia in total hip arthroplasty. The hypothesis was that alumina stabilized zirconia could decrease highly cross-linked polyethylene wear. Methods Highly cross-linked polyethylene wear was measured with a computerized method (PolyWare) in 91 hips. The steady-state wear rates were measured based on the radiographs from the first year postoperatively to the final follow-up and were compared between hips with yttria stabilized zirconia and alumina stabilized zirconia. Results The steady-state wear rate of highly cross-linked polyethylene against zirconia was 0.02 mm/year at a mean follow-up of 7 years. No significant difference was observed between groups with yttria stabilized zirconia and alumina stabilized zirconia. Conclusions Addition of alumina to the zirconia material failed to show further reduction of highly cross-linked polyethylene wear and our hypothesis was not verified. PMID:23634809

  6. Fractal characterization of wear-erosion surfaces

    SciTech Connect

    Rawers, J.; Tylczak, J.

    1999-12-01

    Wear erosion is a complex phenomenon resulting in highly distorted and deformed surface morphologies. Most wear surface features have been described only qualitatively. In this study wear surfaces features were quantified using fractal analysis. The ability to assign numerical values to wear-erosion surfaces makes possible mathematical expressions that will enable wear mechanisms to be predicted and understood. Surface characterization came from wear-erosion experiments that included varying the erosive materials, the impact velocity, and the impact angle. Seven fractal analytical techniques were applied to micrograph images of wear-erosion surfaces. Fourier analysis was the most promising. Fractal values obtained were consistent with visual observations and provided a unique wear-erosion parameter unrelated to wear rate. In this study stainless steel was evaluated as a function of wear erosion conditions.

  7. Low wear rates seen in THAs with highly crosslinked polyethylene at 9 to 14 years in patients younger than age 50 years.

    PubMed

    Garvin, Kevin L; White, Tyler C; Dusad, Anand; Hartman, Curtis W; Martell, John

    2015-12-01

    Patients 50 years or younger are at high risk for wear-related complications of their total hip arthroplasty (THA) because of their generally higher levels of activity. Highly crosslinked polyethylene (HXLPE) is believed to be more durable for this population than conventional polyethylene because of its improved wear; however, limited information is available on the wear of HXLPE in this population, particularly the wear of HXLPE when it articulates with alternative bearings like Oxinium (Smith & Nephew, Memphis, TN, USA). The purpose of this study was to evaluate two questions relative to this population of patients undergoing THA. First, what was the linear and volumetric wear rate of HXLPE in patients 50 years or younger at a minimum followup of 9 years and was osteolysis observed in any of these hips? Given the potential for damage to the Oxinium femoral head surface, was the wear of HXLPE in the patients with this material similar to the other bearings or was there accelerated or runaway wear that was visible in any of the patients? From November 1999 to April 2005, 105 THAs were performed in 95 patients 50 years of age or younger (mean, 42 years; range, 20-50 years). The mean body mass index was 30 kg/m(2) (range, 17-51 kg/m(2)).The mean followup was 12 years (range, 9-14 years). Two patients died, five patients (one bilateral) were lost to followup, and one hip was revised elsewhere for pain. The patients' information was not included in the study, which left 87 patients with 96 hips for analysis. Highly crosslinked polyethylene was the acetabular bearing for all of the hips. We analyzed the linear and volumetric wear of all of the hips using the Martell method. Eighty hips had the same diameter head (28 mm) allowing us to more accurately compare the different bearing materials. The type of femoral head used was related to our sequential use of materials beginning with cobalt chrome (14), ceramic (23) followed by Oxinium (43) in the hips with 28-mm heads

  8. Establishing a role for vancomycin powder application for prosthetic joint infection prevention-results of a wear simulation study.

    PubMed

    Qadir, Rabah; Ochsner, J Lockwood; Chimento, George F; Meyer, Mark S; Waddell, Bradford; Zavatsky, Joseph M

    2014-07-01

    Topical vancomycin powder (VP) has shown efficacy and safety in decreasing post-operative spine infections. VP use in arthroplasty has not been established. Concerns remain for third-body wear with the addition of crystalline substrate at the implant interface. The study's purpose was to compare wear behavior of CoCr on UHMWPE to identical wear couples with VP. A six-station wear simulator was utilized and cyclic articulations were run for 10 million cycles (Mc). UHMWPE wear was measured using photography, stereomicroscopy, and gravimetric measurement. There were no differences in wear mark length (P = 0.43), width (P = 0.49), or gravimetric wear at 10 Mc (P = 0.98). VP and control groups lost 0.32 and 0.33 mg, respectively. VP may have a role in PJI prevention. A well-designed clinical study is needed.

  9. Wear of ultra-high molecular weight polyethylene (UHMWPE) in total knee prostheses: a review of key influences.

    PubMed

    McGloughlin, T M; Kavanagh, A G

    2000-01-01

    The formation and development of wear is now widely accepted as one of the major concerns in the long-term survivorship of contemporary knee prostheses in vivo. This review examines the role of surface topography, third-body debris, load, contact mechanics and material quality in the wear process. Some of the kinematic and physiological issues that need to be modelled in the development of wear testing regimes for evaluation of material combinations and geometrical combinations in total knee implant designs are considered. Wear testing procedures and some of the results from wear tests are discussed and the need to consider the impact of rolling and sliding in the study of wear in total knee components is highlighted. The dominant wear mechanisms that occur in vivo are identified and the role of these mechanisms is currently being examined experimentally at the University of Limerick wear testing machine.

  10. The wear of ultra-high molecular weight polyethylene sliding on metallic and ceramic counterfaces representative of current femoral surfaces in joint replacement.

    PubMed

    Lancaster, J G; Dowson, D; Isaac, G H; Fisher, J

    1997-01-01

    A number of studies have investigated the influence of surface roughness on the wear of ultra-high molecular weight polyethylene (UHMWPE) in total joint replacement. The results of these studies have shown that the wear factor is proportional to the counterface roughness raised to a power greater than one. In this laboratory study, the effect of surface finish of several biomaterials on the wear of UHMWPE was studied. The study was conducted using reciprocating pin-on-plate wear tests with bovine serum as a lubricant. The biomaterials investigated as the counterface material included stainless steel, cast cobalt chrome (CoCr), CoCr (ASTM F799), alumina ceramic and zirconia ceramic. The counterface topographies of the wear plates were produced using techniques representative of current manufacturing methods. The surface roughness of the wear plates was varied in the range Ra = 0.005-0.04 micron; this was representative of femoral heads and femoral knee components currently used clinically. Metals and ceramics with a similar surface roughness produced a similar wear rate of UHMWPE. For the limited range of smooth counterfaces used in this study only a moderate correlation was found between the surface roughness and the wear factors. For a change in counterface roughness Ra of 0.005 to 0.04 micron, the wear factor increased from 7.4 +/- 1.6 to 16.5 +/- 2.4 x 10(-9) mm3/N m (mean +/- standard error). This variation in counterface roughness had much less effect in wear than previously reported for rougher counterfaces. For an extended range of counterface roughness, a stronger correlation was found using an exponential function for the regression fit. The exponential function shows the benefits of decreased wear with decreased surface roughness. Although the wear rate decreased less rapidly with decreased counterface roughness for Ra values below 0.05 micron, there were significant advantages to be gained from improved femoral head roughness to below 0.01 micron Ra.

  11. Wear comparison between conventional and highly cross-linked polyethylene against a zirconia head: a concise follow-up, at an average 10 years, of a previous report.

    PubMed

    Fukui, Kiyokazu; Kaneuji, Ayumi; Sugimori, Tanzo; Ichiseki, Toru; Matsumoto, Tadami

    2013-10-01

    We previously reported the results of wear comparison at a minimum of 5 years between highly cross-linked polyethylene (HXLPE) and conventional polyethylene (PE) against a zirconia femoral head. We now report the mean wear at 10 years for 52 patients (56 hips) of the original cohort of 61 patients (65 hips) who had undergone primary total hip arthroplasty at our hospital between November 1999 and August 2000. The mean steady-state linear wear rate of HXLPE was 0.045 mm/y, compared with 0.080 mm/y for conventional PE (P=.0003). The incidence of osteolysis was 25% in the conventional PE group compared with 0% in the HXLPE group. Our study demonstrated that the steady-state wear rate for HXLPE remains significantly lower than that for conventional PE against a zirconia femoral head at a mean of 10 years after implantation. Copyright © 2013 Elsevier Inc. All rights reserved.

  12. Hardface coating systems and methods for metal alloys and other materials for wear and corrosion resistant applications

    DOEpatents

    Seals, Roland D.

    2015-08-18

    The present disclosure relates generally to hardface coating systems and methods for metal alloys and other materials for wear and corrosion resistant applications. More specifically, the present disclosure relates to hardface coatings that include a network of titanium monoboride (TiB) needles or whiskers in a matrix, which are formed from titanium (Ti) and titanium diboride (TiB.sub.2) precursors by reactions enabled by the inherent energy provided by the process heat associated with coating deposition and, optionally, coating post-heat treatment. These hardface coatings are pyrophoric, thereby generating further reaction energy internally, and may be applied in a functionally graded manner. The hardface coatings may be deposited in the presence of a number of fluxing agents, beta stabilizers, densification aids, diffusional aids, and multimode particle size distributions to further enhance their performance characteristics.

  13. Low-temperature growth of low friction wear-resistant amorphous carbon nitride thin films by mid-frequency, high power impulse, and direct current magnetron sputtering

    SciTech Connect

    Bakoglidis, Konstantinos D. Schmidt, Susann; Garbrecht, Magnus; Ivanov, Ivan G.; Jensen, Jens; Greczynski, Grzegorz; Hultman, Lars

    2015-09-15

    GPa. Nanoindentation showed a significant increase in film hardness and reduced elastic modulus with increasing V{sub s} for all techniques. The harder films were produced by MFMS with hardness as high as 25 GPa. Low friction coefficients, between 0.05 and 0.06, were recorded for all films. Furthermore, CN{sub x} films produced by MFMS and DCMS at V{sub s} = 100 and 120 V presented a high wear resistance with wear coefficients of k ≤ 2.3 × 10{sup −5} mm{sup 3}/Nm. While all CN{sub x} films exhibit low friction, wear depends strongly on the structural and mechanical characteristics of the films. The MFMS mode is best suited for the production of hard CN{sub x} films, although high compressive stresses challenge the application on steel substrates. Films grown in HiPIMS mode provide adequate adhesion due to low residual stress values, at the expense of lower film hardness. Thus, a relatively wide mechanical property envelope is presented for CN{sub x} films, which is relevant for the optimization of CN{sub x} film properties intended to be applied as low friction and wear resistant coatings.

  14. Plasma deposition of elastic wear resistant Si-C coatings on nickel-titanium for biomedical applications

    NASA Astrophysics Data System (ADS)

    Schauer, Janine-Christina; Winter, Jörg

    2008-06-01

    A bilayer system consisting of carbon and silicon has been developed to coat metals such as copper, stainless steel, nickel, and especially NiTi with an elastic, wear, and corrosion resistant film. The plasma deposited film system exhibits excellent adhesion on all metals under investigation. This adhesion is promoted by silicide formation. Additionally, the film system shows good performance under extremely high load induced via cavitation admission. Tensile tests reveal high elasticity of the film system, in that it can be elongated up to 5% before occurrence of damage of the film. The intrinsic stress inside this film system is reduced compared to pure diamondlike carbon films. Both good chemical bonding and reduced stress lead to good adhesion of the film systems on metals.

  15. Investigation of the mechanical properties of FeNiCrMnSi high entropy alloy wear resistant

    NASA Astrophysics Data System (ADS)

    Buluc, G.; Florea, I.; Chelariu, R.; Popescu, G.; Carcea, I.

    2016-06-01

    In this paper we investigated microstructure, hardness and wear resistance for FeNiCrMnAl, high entropy alloy. The FeNiCrMnSi, high entropy alloy was elaborated in a medium induction furnace, by choosing the silicon, as an alliance element within the equi- atomic high entropy alloy, we managed to obtain a dendritic structure, the formation of intermetallic compounds or separated silicon. The medium hardness value of the investigated alloy was 948.33 HV and the medium value of the friction coefficient was 0.6655 in the first 20 seconds and 0.5425 for 1667 seconds. The volume loss of the high entropy alloy FeNiCrMnSi was 0.0557 mm3.

  16. Wear resistance of hydrophobic surfaces

    NASA Astrophysics Data System (ADS)

    Martinez, MA; Abenojar, J.; Pantoja, M.; López de Armentia, S.

    2017-05-01

    Nature has been an inspiration source to develop artificial hydrophobic surfaces. During the latest years the development of hydrophobic surfaces has been widely researched due to their numerous ranges of industrial applications. Industrially the use of hydrophobic surfaces is being highly demanded. This is why many companies develop hydrophobic products to repel water, in order to be used as coatings. Moreover, these coating should have the appropriated mechanical properties and wear resistance. In this work wear study of a hydrophobic coating on glass is carried out. Hydrophobic product used was Sika Crystal Dry by Sika S.A.U. (Alcobendas, Spain). This product is currently used on car windshield. To calculate wear resistance, pin-on-disk tests were carried out in dry and water conditions. The test parameters were rate, load and sliding distance, which were fixed to 60 rpm, 5 N and 1000 m respectively. A chamois was used as pin. It allows to simulate a real use. The friction coefficient and loss weight were compared to determinate coating resistance

  17. Effects of heat treatment on wear resistance and fracture toughness of duo-cast materials composed of high-chromium white cast iron and low-chromium steel

    NASA Astrophysics Data System (ADS)

    Kim, Chang Kyu; Lee, Sunghak; Jung, Jae-Young

    2006-03-01

    The objective of this study is to investigate effects of heat treatment on wear resistance and fracture toughness in duo-cast materials composed of a high-chromium white cast iron and a low-chromium steel as a wear-resistant part and a ductile part, respectively. Different size, volume fraction, and distribution of M7C3 carbides were employed in the wear-resistant part by changing the amount of chromium, and the volume fraction of martensite in the austenitic matrix was varied by the heat treatment. In the alloys containing a small amount of chromium, an interdendritic structure of eutectic M7C3 carbides was formed, and led to the improvement of wear resistance and fracture toughness. After the heat treatment, the selective wear of the matrix and the cracking or spalled-off carbides were considerably reduced since the hardness difference between carbides and matrix decreased by the increase in the matrix hardness, thereby leading to the improvement of the wear resistance. However, the fracture toughness of the heat-treated alloys was lower than that of the as-cast alloys because the matrix containing a considerable amount of martensite did not effectively prevent the crack propagation.

  18. Fractal characterization of wear-erosion surfaces

    SciTech Connect

    Rawers, James C.; Tylczak, Joseph H.

    1999-12-01

    Wear erosion is a complex phenomenon resulting in highly distorted and deformed surface morphologies. Most wear surface features have been described only qualitatively. In this study wear surfaces features were quantified using fractal analysis. The ability to assign numerical values to wear-erosion surfaces makes possible mathematical expressions that will enable wear mechanisms to be predicted and understood. Surface characterization came from wear-erosion experiments that included varying the erosive materials, the impact velocity, and the impact angle. Seven fractal analytical techniques were applied to micrograph images of wear-erosion surfaces. Fourier analysis was the most promising. Fractal values obtained were consistent with visual observations and provided a unique wear-erosion parameter unrelated to wear rate.

  19. Effect of load on the friction-wear behavior of magnetron sputtered DLC film at high temperature

    NASA Astrophysics Data System (ADS)

    Ze, Sun; Dejun, Kong

    2017-01-01

    A DLC (diamond-like carbon) film was deposited on a YT14 cemented carbide cutting tool by using magnetron sputtering. The surface-interfacial morphologies, chemical composition, and phases of the obtained DLC film were analyzed by using scanning electron microscopy, energy dispersive spectroscopy, and x-ray diffraction, respectively. The friction and wear characteristics of the DLC film were investigated under different loads, the distribution of the chemical elements on the worn tracks were analyzed by using a plane scan analysis, and the wear mechanism of the DLC film was also examined. The results showed that the DLC particles were uniformly covered on the substrate with a thickness of about 600 nm, and the diamond peaks at the crystal face of (1 1 1), and (2 2 0) appear at diffraction angles of 44.40, and 75.52°, respectively. The average coefficients of friction of the DLC film under loads of 2, 4, and 6 N were 0.65, 0.65, and 0.49, respectively, and the corresponding wear rates were 0.33  ×  10‑9, 0.26  ×  10‑9, and 0.25  ×  10‑9 mm3 N‑1 s‑1, respectively. Therefore, the film represents outstanding reducing friction and wear resistance. With the increasing wear loads, the atomic fraction of C decreased, while that of O increased; the oxidation reaction occurred in the wear test. The wear mechanisms under a load of 2 N were abrasive wear, adhesive wear and oxidation wear, while that under a load of 4 N were adhesive wear and oxidation wear, and that under the load of 6 N were only oxidation wear.

  20. Optimization of the EMS process parameters in compocasting of high-wear-resistant Al-nano-TiC composites

    NASA Astrophysics Data System (ADS)

    Shamsipour, Majid; Pahlevani, Zahra; Shabani, Mohsen Ostad; Mazahery, Ali

    2016-04-01

    Understanding of the electromagnetic stirrer (EMS) process parameters-wear relation in nanocomposite is required for further creation of tailored modifications of process in accordance with the demands for various applications. This study depicts the performance of hybrid algorithm for optimization of the parameters in EMS compocasting of nano-TiC-reinforced Al-Si alloys. Adaptive neuro-fuzzy inference system (ANFIS) coupled with particle swarm optimization (PSO) was applied to find the optimum combination of the inputs including mold temperature, mix time, impeller speed, powder temperature, cast temperature and average particle size. The optimized condition was obtained in minimization of objective function. The objective function is calculated by ANFIS and then minimized by PSO. The optimized parameters were used to produce semisolid cast aluminum matrix composites reinforced with nano-TiC particles. The optimized nanocomposites were then studied for their tribological properties.

  1. Friction and wear behaviour of self lubricating bearing liners

    NASA Astrophysics Data System (ADS)

    Gay, Russell

    The thesis describes a numerical model for evaluating the variation of friction and wear of a self lubricating bearing liner over its useful wear life. Self-lubricating bearings have been in widespread use since the mid-1950s, particularly in the aerospace industry where they have the advantage of being low maintenance components. They are commonly used in relatively low speed, reciprocating applications such as control surface actuators, and usually consist of a spherical bearing with the inner and outer elements separated by a composite textile resin-bonded liner. A finite element model has been developed to predict the local stiffness of a particular liner at different states of wear. Results obtained using the model were used to predict the overall friction coefficient as it evolves due to wear, which is a novel approach. Experimental testing was performed on a bespoke flat-on-flat wear test rig with a reciprocating motion to validate the results of the friction model.. These tests were carried out on a commercially-available bearing liner, predominantly at a high contact pressure and an average sliding speed of 0.2 ms-1. Good agreement between predicted and experimentally measured wear was obtained when appropriate coefficients of friction were used in the friction model, and when the reciprocating sliding distance was above a critical value. A numerical wear model was also developed to predict the trend of backlash development in real bearing geometries using a novel approach. Results from the wear model were validated against full-scale bearing tests carried out elsewhere by the sponsoring company. Good agreement was obtained between the model predictions and the experimental results for the first 80% of the bearing wear life, and explanations for the discrepancy during the last 20% of the wear life have been proposed..

  2. A model for predicting wear rates in tooth enamel.

    PubMed

    Borrero-Lopez, Oscar; Pajares, Antonia; Constantino, Paul J; Lawn, Brian R

    2014-09-01

    It is hypothesized that wear of enamel is sensitive to the presence of sharp particulates in oral fluids and masticated foods. To this end, a generic model for predicting wear rates in brittle materials is developed, with specific application to tooth enamel. Wear is assumed to result from an accumulation of elastic-plastic micro-asperity events. Integration over all such events leads to a wear rate relation analogous to Archard׳s law, but with allowance for variation in asperity angle and compliance. The coefficient K in this relation quantifies the wear severity, with an arbitrary distinction between 'mild' wear (low K) and 'severe' wear (high K). Data from the literature and in-house wear-test experiments on enamel specimens in lubricant media (water, oil) with and without sharp third-body particulates (silica, diamond) are used to validate the model. Measured wear rates can vary over several orders of magnitude, depending on contact asperity conditions, accounting for the occurrence of severe enamel removal in some human patients (bruxing). Expressions for the depth removal rate and number of cycles to wear down occlusal enamel in the low-crowned tooth forms of some mammals are derived, with tooth size and enamel thickness as key variables. The role of 'hard' versus 'soft' food diets in determining evolutionary paths in different hominin species is briefly considered. A feature of the model is that it does not require recourse to specific material removal mechanisms, although processes involving microplastic extrusion and microcrack coalescence are indicated. Published by Elsevier Ltd.

  3. Application of high-rate cutting tools

    NASA Astrophysics Data System (ADS)

    Moriarty, John L., Jr.

    1989-03-01

    Widespread application of the newest high-rate cutting tools to the most appropriate jobs is slowed by the sheer magnitude of developments in tool types, materials, workpiece applications, and by the rapid pace of change. Therefore, a study of finishing and roughing sizes of coated carbide inserts having a variety of geometries for single point turning was completed. The cutting tools were tested for tool life, chip quality, and workpiece surface finish at various cutting conditions with medium alloy steel. An empirical wear-life data base was established, and a computer program was developed to facilitate technology transfer, assist selection of carbide insert grades, and provide machine operating parameters. A follow-on test program was implemented suitable for next generation coated carbides, rotary cutting tools, cutting fluids, and ceramic tool materials.

  4. Rolling Contact Fatigue and Wear Behavior of High-Performance Railway Wheel Steels Under Various Rolling-Sliding Contact Conditions

    NASA Astrophysics Data System (ADS)

    Faccoli, Michela; Petrogalli, Candida; Lancini, Matteo; Ghidini, Andrea; Mazzù, Angelo

    2017-07-01

    An experimental investigation was carried out to study and compare the response to cyclic loading of the high-performance railway wheel steels ER8 EN13262 and SUPERLOS®. Rolling contact tests were performed with the same contact pressure, rolling speed and sliding/rolling ratio, varying the lubrication regime to simulate different climatic conditions. The samples, machined out of wheel rims at two depths within the reprofiling layer, were coupled with UIC 900A rail steel samples. The wear rates, friction coefficients and hardness were correlated with the deformation beneath the contact surface. The crack morphology was studied, and the damage mechanisms were identified. The distribution of crack length and depth at the end of the dry tests was analyzed to quantify the damage. The main difference between the steels lies in the response of the external samples to dry contact: SUPERLOS® is subjected to a higher wear and lower friction coefficient than ER8, and this reduces the density of surface cracks that can propagate under wet contact conditions. The analysis of feedback data from in-service wheels confirmed the experimental results.

  5. Ultra-high molecular weight polyethylene wear debris generated in vivo and in laboratory tests; the influence of counterface roughness.

    PubMed

    Hailey, J L; Ingham, E; Stone, M; Wroblewski, B M; Fisher, J

    1996-01-01

    The objective of this study was to investigate the effect of counterface roughness and lubricant on the morphology of ultra-high molecular weight polyethylene (UHMWPE) wear debris generated in laboratory wear tests, and to compare this with debris isolated from explanted tissue. Laboratory tests used UHMWPE pins sliding against stainless steel counterfaces. Both water and serum lubricants were used in conjunction with rough and smooth counterfaces. The lubricants and tissue from revision hip surgery were processed to digest the proteins and permit filtration. This involved denaturing the proteins with potassium hydroxide (KOH), sedimentation of any remaining proteins, and further digestion of these proteins with chromic acid. All fractions were then passed through a 0.2 micron membrane, and the debris examined using scanning electron microscopy. The laboratory studies showed that the major variable influencing debris morphology was counterface roughness. The rougher counterfaces produced larger numbers of smaller particles, with a size range extending below 1 micron. For smooth counterfaces there were fewer of these small particles, and evidence of larger platelets, greater than 10 microns in diameter. Analysis of the debris from explanted tissues showed a wide variation in the particle size distribution, ranging from below 1 micron up to several millimetres in size. Of major clinical significance in relation to osteolysis and loosening is roughening of the femoral components, which may lead to greater numbers of the sub-micron-sized particles.

  6. Tribo-Mechanical Properties of HVOF Deposited Fe3Al Coatings Reinforced with TiB2 Particles for Wear-Resistant Applications

    PubMed Central

    Amiriyan, Mahdi; Blais, Carl; Savoie, Sylvio; Schulz, Robert; Gariépy, Mario; Alamdari, Houshang

    2016-01-01

    This study reveals the effect of TiB2 particles on the mechanical and tribological properties of Fe3Al-TiB2 composite coatings against an alumina counterpart. The feedstock was produced by milling Fe3Al and TiB2 powders in a high energy ball mill. The high-velocity oxy-fuel (HVOF) technique was used to deposit the feedstock powder on a steel substrate. The effect of TiB2 addition on mechanical properties and dry sliding wear rates of the coatings at sliding speeds ranging from 0.04 to 0.8 m·s−1 and loads of 3, 5 and 7 N was studied. Coatings made from unreinforced Fe3Al exhibited a relatively high wear rate. The Vickers hardness, elastic modulus and wear resistance of the coatings increased with increasing TiB2 content in the Fe3Al matrix. The wear mechanisms strongly depended on the sliding speed and the presence of TiB2 particles but were less dependent on the applied load. This study reveals the effect of TiB2 particles on the mechanical and tribological properties of Fe3Al-TiB2 composite coatings against an alumina counterpart. The feedstock was produced by milling Fe3Al and TiB2 powders in a high energy ball mill. The high-velocity oxy-fuel (HVOF) technique was used to deposit the feedstock powder on a steel substrate. The effect of TiB2 addition on mechanical properties and dry sliding wear rates of the coatings at sliding speeds ranging from 0.04 to 0.8 m·s−1 and loads of 3, 5 and 7 N was studied. Coatings made from unreinforced Fe3Al exhibited a relatively high wear rate. The Vickers hardness, elastic modulus and wear resistance of the coatings increased with increasing TiB2 content in the Fe3Al matrix. The wear mechanisms strongly depended on the sliding speed and the presence of TiB2 particles but were less dependent on the applied load. This study reveals the effect of TiB2 particles on the mechanical and tribological properties of Fe3Al-TiB2 composite coatings against an alumina counterpart. The feedstock was produced by milling Fe3Al and TiB2

  7. The Friction and Wear of Copper in High-Load, Low-Speed, Small-Amplitude Reciprocating Sliding

    DTIC Science & Technology

    1982-08-01

    MUMMER(@) Sidney A. Karpe 9. PERFORMING ORGANIZATION NAME AND ADDRESS 𔃺. PROGRAM ELEME’NTr, PROJECT TASK AREA & WORK UNIT NUMIERS David Taylor Naval Ship...REPORT DATE David Taylor Naval Ship R&D Center (Code 2832) August 1982 Annapolis, MD 21402 I3. NUMBER OF PAGES 96 14. MONITORING AGENCY NAME...carbon, medium chromium and nickel steel Inconel 718 Nickel-chromium based alloy k Wear constant, commonly called Archard wear coefficient n Wear

  8. Superhydrophobic, Biomimetic Surfaces with High and Low Adhesion, Optical Transmittance, and Nanoscale Mechanical Wear Resistance

    NASA Astrophysics Data System (ADS)

    Ebert, Daniel R.

    Superhydrophobic surfaces (defined as surfaces having water contact angle greater than 150°) show great promise for use in a rapidly growing number of engineering applications, ranging from biomedical devices to fluid drag reduction in pipelines. In nature, the surfaces of many organisms, such as certain plant leaves, are known to exhibit superhydrophobicity. In some cases, droplet adhesion is very low (droplet rolls away easily), while in other cases adhesion is high (droplet remains adhered when surface is inverted). The recent advent and development of microscopes with resolution down to a few nanometers (such as atomic force microscopes and scanning electron microscopes) has allowed for in-depth understanding of the micro- and nanoscale mechanisms employed by these plant leaves and other natural surfaces to achieve their particular wetting properties. Biomimetics (or "mimicking nature") is therefore a very promising approach for the development of engineering surfaces with desired wetting characteristics. However, research in creating biomimetic surfaces is still in its early stages, and many of the surfaces created thus far are not mechanically robust, which is required for many potential real-world applications. In addition, for applications such as self-cleaning windows and solar panels, optical transparency is required. In this thesis, a set of original studies are presented in which superhydrophobic surfaces were designed based on biomimetics and fabricated using a wide of variety of techniques. The surfaces were characterized with regard to wetting characteristics such as water contact angle and contact angle hysteresis, micro- and nanoscale mechanical durability, and in some cases optical transmittance. Theoretical wetting models served as guides both in the design and in the understanding of experimental results, especially in regard to different wetting regime and regime transition. This work provides important conclusions and valuable insight for

  9. The rates of wear of X3 highly cross-linked polyethylene at five years when coupled with a 36 mm diameter ceramic femoral head in young patients.

    PubMed

    Selvarajah, E; Hooper, G; Grabowski, K; Frampton, C; Woodfield, T B F; Inglis, G

    2015-11-01

    Polyethylene wear debris can cause osteolysis and the failure of total hip arthroplasty. We present the five-year wear rates of a highly cross-linked polyethylene (X3) bearing surface when used in conjunction with a 36 mm ceramic femoral head. This was a prospective study of a cohort of 100 THAs in 93 patients. Pain and activity scores were measured pre- and post-operatively. Femoral head penetration was measured at two months, one year, two years and at five years using validated edge-detecting software (PolyWare Auto). At a mean of 5.08 years (3.93 to 6.01), 85 hips in 78 patients were available for study. The mean age of these patients was 59.08 years (42 to 73, the mean age of males (n = 34) was 59.15 years, and females (n = 44) was 59.02 years). All patients had significant improvement in their functional scores (p < 0.001). The steady state two-dimensional linear wear rate was 0.109 mm/year. The steady state volumetric wear rate was 29.61 mm(3)/year. No significant correlation was found between rate of wear and age (p = 0.34), acetabular component size (p = 0.12) or clinical score (p = 0.74). Our study shows low steady state wear rates at five years in X3 highly cross-linked polyethylene in conjunction with a 36 mm ceramic femoral head. The linear wear rate was almost identical to the osteolysis threshold of 0.1 mm/year recommended in the literature.

  10. The influence of malalignment and ageing following sterilisation by gamma irradiation in an inert atmosphere on the wear of ultra-high-molecular-weight polyethylene in patellofemoral replacements.

    PubMed

    Maiti, Raman; Cowie, Raelene M; Fisher, John; Jennings, Louise M

    2017-07-01

    Complications of patellofemoral arthroplasty often occur soon after implantation and, as well as other factors, can be due to the design of the implant or its surgical positioning. A number of studies have previously considered the wear of ultra-high-molecular-weight polyethylene patellae following suboptimal implantation; however, studies have primarily been carried out under a limited number of degrees of freedom. The aim of this study was to develop a protocol to assess the wear of patellae under a malaligned condition in a six-axis patellofemoral joint simulator. The malalignment protocol hindered the tracking of the patella centrally in the trochlear groove and imparted a constant 5° external rotation (tilt) on the patella button. Following 3 million cycles of wear simulation, this condition had no influence on the wear of ultra-high-molecular-weight polyethylene patellae aged for 4 years compared to well-positioned non-aged implants (p > 0.05). However, under the malaligned condition, ultra-high-molecular-weight polyethylene patellae aged 8-10 years after unpacking (following sterilisation by gamma irradiation in an inert atmosphere) and worn ultra-high-molecular-weight polyethylene components also aged 4 years after unpacking (following the same sterilisation process) exhibited a high rate of wear. Fatigue failure due to elevated contact stress led to delamination of the ultra-high-molecular-weight polyethylene and in some cases complete failure of the patellae. The results suggest that suboptimal tracking of the patella in the trochlear groove and tilt of the patella button could have a significant effect on the wear of ultra-high-molecular-weight polyethylene and could lead to implant failure.

  11. The influence of malalignment and ageing following sterilisation by gamma irradiation in an inert atmosphere on the wear of ultra-high-molecular-weight polyethylene in patellofemoral replacements

    PubMed Central

    Maiti, Raman; Cowie, Raelene M; Fisher, John; Jennings, Louise M

    2017-01-01

    Complications of patellofemoral arthroplasty often occur soon after implantation and, as well as other factors, can be due to the design of the implant or its surgical positioning. A number of studies have previously considered the wear of ultra-high-molecular-weight polyethylene patellae following suboptimal implantation; however, studies have primarily been carried out under a limited number of degrees of freedom. The aim of this study was to develop a protocol to assess the wear of patellae under a malaligned condition in a six-axis patellofemoral joint simulator. The malalignment protocol hindered the tracking of the patella centrally in the trochlear groove and imparted a constant 5° external rotation (tilt) on the patella button. Following 3 million cycles of wear simulation, this condition had no influence on the wear of ultra-high-molecular-weight polyethylene patellae aged for 4 years compared to well-positioned non-aged implants (p > 0.05). However, under the malaligned condition, ultra-high-molecular-weight polyethylene patellae aged 8–10 years after unpacking (following sterilisation by gamma irradiation in an inert atmosphere) and worn ultra-high-molecular-weight polyethylene components also aged 4 years after unpacking (following the same sterilisation process) exhibited a high rate of wear. Fatigue failure due to elevated contact stress led to delamination of the ultra-high-molecular-weight polyethylene and in some cases complete failure of the patellae. The results suggest that suboptimal tracking of the patella in the trochlear groove and tilt of the patella button could have a significant effect on the wear of ultra-high-molecular-weight polyethylene and could lead to implant failure. PMID:28661229

  12. Cast Aluminum Alloy for High Temperature Applications

    NASA Technical Reports Server (NTRS)

    Lee, Jonathan A.

    2003-01-01

    Originally developed by NASA as high performance piston alloys to meet U.S. automotive legislation requiring low exhaust emission, the novel NASA alloys now offer dramatic increase in tensile strength for many other applications at elevated temperatures from 450 F (232 C) to about 750 F (400 C). It is an ideal low cost material for cast automotive components such as pistons, cylinder heads, cylinder liners, connecting rods, turbo chargers, impellers, actuators, brake calipers and rotors. It can be very economically produced from conventional permanent mold, sand casting or investment casting, with silicon content ranging from 6% to 18%. At high silicon levels, the alloy exhibits excellent dimensional stability, surface hardness and wear resistant properties.

  13. Does being a "SunSmart School" influence hat-wearing compliance? An ecological study of hat-wearing rates at Australian primary schools in a region of high sun exposure.

    PubMed

    Turner, Denise; Harrison, Simone L; Buettner, Petra; Nowak, Madeleine

    2014-03-01

    Childhood sun exposure is an important risk factor for skin cancer. Anecdotal evidence suggests that hats are under-utilized by Australian primary school students. The proportion of students and adult role-models wearing hats was observed at 36 primary schools (63.9% SunSmart schools [SSS]) in Townsville (latitude 19.3°S; high to extreme maximum daily UV-index year round), Queensland, Australia, from 2009 to 2011. Overall, 52.2% of 28,775 students and 47.9% of 2954 adults were observed wearing a hat. Hat use (all styles) among SSS and non-SunSmart school (NSSS) students was similar before (24.2% vs 20.5%; p=0.701), after (25.4% vs 21.7%; p=0.775) and during school-hours (93.0% vs 89.2%; p=0.649) except SSS students wore gold-standard (broad-brim/bucket/legionnaire) hats during school play-breaks more often in the warmer months (October-March) than NSSS students (54.7% vs 37.4%; p=0.02). Although the proportion of adults who wore hats (all styles) was similar at SSS and NSSS (48.2% vs 46.8%; p=0.974), fewer adults at SSS wore them before school (3.7% vs 10.2%; p=0.035). SunSmart status is not consistently associated with better hat-wearing behavior. The protective nature of hats and the proportion of school students and adult role-models wearing them could be improved, possibly by offering incentives to schools that promote sun-safety. Copyright © 2013 Elsevier Inc. All rights reserved.

  14. The influence of bone and bone cement debris on counterface roughness in sliding wear tests of ultra-high molecular weight polyethylene on stainless steel.

    PubMed

    Caravia, L; Dowson, D; Fisher, J; Jobbins, B

    1990-01-01

    Studies of explanted hip prostheses have shown high wear rates of ultra-high molecular weight polyethylene (UHMWPE) acetabular cups and roughening of the surface of the metallic femoral head. Bone and bone cement particles have also been found in the articulating surfaces of some joints. It has been proposed that bone or bone cement particles may cause scratching and deterioration in the surface finish of metallic femoral heads, thus producing increased wear rates and excessive amounts of wear debris. Sliding wear tests of UHMWPE pins on stainless steel have been performed with particles of different types of bone and bone cement added. Damage to the stainless steel counterface and the motion of particles through the interface have been studied. Particles of bone cement with zirconium and barium sulphate additives and particles of cortical bone scratched the stainless steel counterface. The cement particles with zirconium additive produced significantly greater surface damage. The number of particles entering the contact and embedding in the UHMWPE pin was dependent on particle size and geometry, surface roughness and contact stress. Particles are likely to cause surface roughening and increased wear rates in artificial joints.

  15. Quantification of the effect of cross-shear and applied nominal contact pressure on the wear of moderately cross-linked polyethylene.

    PubMed

    Abdelgaied, Abdellatif; Brockett, Claire L; Liu, Feng; Jennings, Louise M; Fisher, John; Jin, Zhongmin

    2013-01-01

    Polyethylene wear is a great concern in total joint replacement. It is now considered a major limiting factor to the long life of such prostheses. Cross-linking has been introduced to reduce the wear of ultra-high-molecular-weight polyethylene (UHMWPE). Computational models have been used extensively for wear prediction and optimization of artificial knee designs. However, in order to be independent and have general applicability and predictability, computational wear models should be based on inputs from independent experimentally determined wear parameters (wear factors or wear coefficients). The objective of this study was to investigate moderately cross-linked UHMWPE, using a multidirectional pin-on-plate wear test machine, under a wide range of applied nominal contact pressure (from 1 to 11 MPa) and under five different kinematic inputs, varying from a purely linear track to a maximum rotation of +/- 55 degrees. A computational model, based on a direct simulation of the multidirectional pin-on-plate wear tester, was developed to quantify the degree of cross-shear (CS) of the polyethylene pins articulating against the metallic plates. The moderately cross-linked UHMWPE showed wear factors less than half of that reported in the literature for, the conventional UHMWPE, under the same loading and kinematic inputs. In addition, under high applied nominal contact stress, the moderately crosslinked UHMWPE wear showed lower dependence on the degree of CS compared to that under low applied nominal contact stress. The calculated wear coefficients were found to be independent of the applied nominal contact stress, in contrast to the wear factors that were shown to be highly pressure dependent. This study provided independent wear data for inputs into computational models for moderately cross-linked polyethylene and supported the application of wear coefficient-based computational wear models.

  16. Patients presenting with miliaria while wearing flame resistant clothing in high ambient temperatures: a case series

    PubMed Central

    2011-01-01

    Introduction Clothing can be a cause of occupational dermatitis. Frequent causes of clothing-related dermatological problems can be the fabric itself and/or chemical additives used in the laundering process, friction from certain fabrics excessively rubbing the skin, or heat retention from perspiration-soaked clothing in hot working environments. To the best of our knowledge, these are the first reported cases of miliaria rubra associated with prolonged use of flame resistant clothing in the medical literature. Case presentation We report 18 cases (14 men and 4 women, with an age range of 19 to 37 years) of moderate to severe skin irritation associated with wearing flame resistant clothing in hot arid environments (temperature range: 39 to 50°C, 5% to 25% relative humidity). We describe the medical history in detail of a 23-year-old Caucasian woman and a 31-year-old African-American man. A summary of the other 16 patients is also provided. Conclusions These cases illustrate the potential serious nature of miliaria with superimposed Staphylococcus infections. All 18 patients fully recovered with topical skin treatment and modifications to their dress ensemble. Clothing, in particular blend fabrics, must be thoroughly laundered to adequately remove detergent residue. While in hot environments, individuals with sensitive skin should take the necessary precautions such as regular changing of clothing and good personal hygiene to ensure that their skin remains as dry and clean as possible. It is also important that they report to their health care provider as soon as skin irritation or rash appears to initiate any necessary medical procedures. Miliaria rubra can take a week or longer to clear, so removal of exposure to certain fabric types may be necessary. PMID:21939537

  17. Wear particle analysis from grease lubricated bearings

    SciTech Connect

    Rosenlieb, W.; Maciejewski, A.S.

    1980-11-01

    Ferrographic analysis has been shown to be useful in evaluating the wear/state condition of grease lubricated components. The major achievement was the successful application of dissolving the grease utilizing a solvent mixture and making ferrograms of equal quality as to that found in oil analysis. The types of wear particles found in used grease samples are comparative to those found in oil lubricated systems. Work is presently being performed on grease lubricated taper roller bearings, similar to the test conditions utilized in this study. The analysis of the grease samples was qualitative vs quantitative. Due to the uneven distribution of wear particulate in the grease and the relatively small amount of grease used in making the ferrograms. The primary emphasis was placed upon size distribution, morphology and elemental composition. The results of the ferrogram analysis showed a good correlation to those of the SKF personnel in terms of monitoring the wear state/condition of the bearings throughout their life. However, the on-condition monitoring of grease lubricated components in the field, is complicated by the physical location of the components and inaccessibility by maintenance personnel to remove grease samples. Where accessibility is no problem, this technique is highly recommended. As it appears presently, this analysis technique seems best suited to the examination of grease obtained from dismantled grease lubricated components or in design applications.

  18. Adverse events in allergy sufferers wearing contact lenses

    PubMed Central

    Urgacz, Agnieszka; Mrukwa, Ewa

    2015-01-01

    Allergy is the fifth leading chronic condition in industrialized countries among all ages, and the third most common chronic disease among children under 18 years old. Many of allergic patients also have problems with vision and want to improve their quality of life by wearing contact lenses. They are most frequently young and active individuals, for whom contact lenses provide greater convenience and more satisfying vision correction than spectacles. However, application of high quality and immunologically neutral products do not protect from allergic side reactions. Nowadays, eye-related allergy and contact lens wear concern larger and larger populations worldwide. The purpose of this review is to summarize the studies on ocular complications associated with wearing contact lenses. The article presents indications for allergic patients especially on the care system and wear schedule. PMID:26161062

  19. Effect of composition and physical properties of silicon nitride on rolling wear and fatigue performance

    NASA Astrophysics Data System (ADS)

    Allen, Deborah L.

    1994-04-01

    The improved performance of silicon nitride components over all-steel bearings in several applications has been demonstrated. However, the effects of grain size, intergranular phase composition, fracture toughness, and hardness on rolling wear and fatigue performance are not completely understood. Three commercial bearing materials were tested under standard conditions and their physical properties were obtained. Wear and fatigue properties were compared to physical properties and material composition. It was found that a high fracture toughness is not required for high fatigue life and wear resistance. Total wear and fatigue life of the assembly must be considered, in addition to performance of the ceramic material alone, for specific applications. Grain boundary composition did not appear to affect the wear mechanism of these hot-isostatically-pressed materials.

  20. High-temperature frictional wear behavior of MCrAlY-based coatings deposited by atmosphere plasma spraying

    NASA Astrophysics Data System (ADS)

    Tao, Chong; Wang, Lei; Song, Xiu

    2017-02-01

    Al2O3-Cr2O3/NiCoCrAlYTa coatings were prepared via atmosphere plasma spraying (APS). The microstructure and phase composition of the coatings were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), laser confocal scanning microscopy (LSCM), and transmission electron microscopy (TEM). The dry frictional wear behavior of the coatings at 500°C in static air was investigated and compared with that of 0Cr25Ni20 steel. The results show that the coatings comprise the slatted layers of oxide phases, unmelted particles, and pores. The hot abrasive resistance of the coatings is enhanced compared to that of 0Cr25Ni20, and their mass loss is approximately one-fifteenth that of 0Cr25Ni20 steel. The main wear failure mechanisms of the coatings are abrasive wear, fatigue wear, and adhesive wear.

  1. The effects of peroxide content on the wear behavior, microstructure and mechanical properties of peroxide crosslinked ultra-high molecular weight polyethylene used in total hip replacement.

    PubMed

    Gul, Rizwan M

    2008-06-01

    The wear of the ultra-high molecular weight polyethylene (UHMWPE) acetabular components and wear debris induced osteolysis are the major causes of failure in total hip replacements. Crosslinking has been shown to improve the wear resistance of UHMWPE by producing a network structure, resisting the plastic deformation of the surface layer. In this study organic peroxides were used to crosslink two different types of UHMWPE resins, using hot isostatic pressing as the processing method. The effects of peroxide content on the different properties were investigated, along with the effect of the crosslink density on the wear behavior. An increase in peroxide content decreases the melting point and the degree of crystallinity, which results in a decrease in the yield strength. The ultimate tensile strength remains essentially unchanged. The molecular weight between crosslinks decreases with an increase in the peroxide content and reaches a saturation limit at around 0.3-0.5 weight percent peroxide, its value at the saturation limit is a function of the virgin resin used for processing. The wear rate decreases linearly with the increase in crosslink density.

  2. Comparison of 10-year clinical wear of annealed and remelted highly cross-linked polyethylene: A propensity-matched cohort study.

    PubMed

    Hamai, Satoshi; Nakashima, Yasuharu; Mashima, Naohiko; Yamamoto, Takuaki; Kamada, Tomomi; Motomura, Goro; Imai, Hiroshi; Fukushi, Jun-Ichi; Miura, Hiromasa; Iwamoto, Yukihide

    2016-06-01

    No previous studies comparing the clinical wear rates of the two different kinds of cross-linked ultra-high-molecular-weight polyethylene (XLPE), annealed and remelted, are available. We compared the creep and steady wear rates of 36 matched pairs (72 hips in total) adjusting for baseline characteristics with propensity score matching techniques. Zirconia femoral heads with 26-mm diameter were used in all cases. The femoral-head cup penetration was measured digitally on radiographs. Significantly greater creep (p=0.006) was detected in the remelted (0.234mm) than annealed (0.159mm) XLPE. However, no significant difference (p=0.19) was found between the steady wear rates (0.003 and 0.008mm/year, respectively) of the annealed and remelted XLPE. Multiple regression analyses showed that remelted XLPE is significant independent variable (p<0.001) that is positively associated with creep. However, the patient age and body weight, cup size, the liner thickness, cup inclination, follow-up periods, and postoperative Merle d'Aubigné hip score had no significant effects (p>0.05) on the steady wear rates. No patients exhibited above the osteolysis threshold of 0.1mm/year, progressive radiolucencies, osteolysis, or polyethylene fracture. This propensity-matched cohort study document no significant difference in wear resistant performances of annealed and remelted XLPE over an average period of 10 years.

  3. Wear and Corrosion Resistance of Thick Ti-6Al-4V Coating Deposited on Ti-6Al-4V Substrate via High-Pressure Cold Spray

    NASA Astrophysics Data System (ADS)

    Khun, N. W.; Tan, A. W. Y.; Sun, W.; Liu, E.

    2017-08-01

    Ti-6Al-4V (Ti64) coating with a thickness of about 9 mm was deposited on commercial Ti64 substrate via a high-pressure cold spray process. The microstructure, hardness, and wear and corrosion resistance of the Ti64 coating were systematically investigated. The hardness of the Ti64 coating was higher than that of the Ti64 substrate due to the cold-worked microstructure of the coating. The tribological results showed that there was no significant difference in the surface wear rates of the Ti64 coating measured on its different layers while the surface wear resistance of the Ti64 coating was lower than its cross-sectional wear resistance. The corrosion results showed that the Ti64 coating did not effectively prevent its underlying Ti64 substrate from corrosion due to the occurrence of pores in the coating microstructure. It could be concluded that the hardness and wear resistance of the Ti64 coating were comparable to those of the commercial Ti64 substrate.

  4. Synthesis of High-Temperature Self-lubricating Wear Resistant Composite Coating on Ti6Al4V Alloy by Laser Deposition

    NASA Astrophysics Data System (ADS)

    Luo, Jian; Liu, Xiu-Bo; Xiang, Zhan-Feng; Shi, Shi-Hong; Chen, Yao; Shi, Gao-Lian; Wu, Shao-Hua; Wu, Yu-Nan

    2015-05-01

    Laser deposition was adopted to prepare novel Ni-based solid solution (γ-NiCrAlTi)/ TiC/α-Ti/CaF2 high-temperature self-lubricating wear resistant composite coating on Ti6Al4V alloy. Microstructure, micro-hardness, wear behavior, and counter-body effect of the coating were investigated systematically. It can be seen that the coating mainly consists of γ-NiCrAlTi, TiC, α-Ti, and small fine CaF2 particles. Average micro-hardness of the coating is 1023 HV0.3, which is about three-factor higher than that of Ti6Al4V substrate (380 HV0.3). The friction coefficient and wear rate of the coating decrease at all test temperatures to different extents with respect to the substrate. The improvement in wear resistance is believed to be the combined effects of the γ-NiCrAlTi solid solution, the dominating anti-wear capabilities of the reinforced TiC carbides, and the self-lubricating property of CaF2.

  5. Wear Mechanism of Chemical Vapor Deposition (CVD) Carbide Insert in Orthogonal Cutting Ti-6Al-4V ELI at High Cutting Speed

    SciTech Connect

    Gusri, A. I.; Che Hassan, C. H.; Jaharah, A. G.

    2011-01-17

    The performance of Chemical Vapor Deposition (CVD) carbide insert with ISO designation of CCMT 12 04 04 LF, when turning titanium alloys was investigated. There were four layers of coating materials for this insert i.e.TiN-Al2O3-TiCN-TiN. The insert performance was evaluated based on the insert's edge resistant towards the machining parameters used at high cutting speed range of machining Ti-6Al-4V ELI. Detailed study on the wear mechanism at the cutting edge of CVD carbide tools was carried out at cutting speed of 55-95 m/min, feed rate of 0.15-0.35 mm/rev and depth of cut of 0.10-0.20 mm. Wear mechanisms such as abrasive and adhesive were observed on the flank face. Crater wear due to diffusion was also observed on the rake race. The abrasive wear occurred more at nose radius and the fracture on tool were found at the feed rate of 0.35 mm/rev and the depth of cut of 0.20 mm. The adhesion wear takes place after the removal of the coating or coating delaminating. Therefore, adhesion or welding of titanium alloy onto the flank and rake faces demonstrates a strong bond at the workpiece-tool interface.

  6. Effect of Boron Doping on the Wear Behavior of the Growth and Nucleation Surfaces of Micro- and Nanocrystalline Diamond Films.

    PubMed

    Buijnsters, Josephus G; Tsigkourakos, Menelaos; Hantschel, Thomas; Gomes, Francis O V; Nuytten, Thomas; Favia, Paola; Bender, Hugo; Arstila, Kai; Celis, Jean-Pierre; Vandervorst, Wilfried

    2016-10-05

    B-doped diamond has become the ultimate material for applications in the field of microelectromechanical systems (MEMS), which require both highly wear resistant and electrically conductive diamond films and microstructures. Despite the extensive research of the tribological properties of undoped diamond, to date there is very limited knowledge of the wear properties of highly B-doped diamond. Therefore, in this work a comprehensive investigation of the wear behavior of highly B-doped diamond is presented. Reciprocating sliding tests are performed on micro- and nanocrystalline diamond (MCD, NCD) films with varying B-doping levels and thicknesses. We demonstrate a linear dependency of the wear rate of the different diamond films with the B-doping level. Specifically, the wear rate increases by a factor of 3 between NCD films with 0.6 and 2.8 at. % B-doping levels. This increase in the wear rate can be linked to a 50% decrease in both hardness and elastic modulus of the highly B-doped NCD films, as determined by nanoindentation measurements. Moreover, we show that fine-grained diamond films are more prone to wear. Particularly, NCD films with a 3× smaller grain size but similar B-doping levels exhibit a double wear rate, indicating the crucial role of the grain size on the diamond film wear behavior. On the other hand, MCD films are the most wear-resistant films due to their larger grains and lower B-doping levels. We propose a graphical scheme of the wear behavior which involves planarization and mechanochemically driven amorphization of the surface to describe the wear mechanism of B-doped diamond films. Finally, the wear behavior of the nucleation surface of NCD films is investigated for the first time. In particular, the nucleation surface is shown to be susceptible to higher wear compared to the growth surface due to its higher grain boundary line density.

  7. Active wear and failure mechanisms of TiN-coated high speed steel and TiN-coated cemented carbide tools when machining powder metallurgically made stainless steels

    SciTech Connect

    Jiang, L.; Haenninen, H.; Paro, J.; Kauppinen, V.

    1996-09-01

    In this study, active wear and failure mechanisms of both TiN-coated high speed steel and TiN-coated cemented carbide tools when machining stainless steels made by powder metallurgy in low and high cutting speed ranges, respectively, have been investigated. Abrasive wear mechanisms, fatigue-induced failure, and adhesive and diffusion wear mechanisms mainly affected the tool life of TiN-coated high speed steel tools at cutting speeds below 35 m/min, between 35 and 45 m/min, and over 45 m/min, respectively. Additionally, fatigue-induced failure was active at cutting speeds over 45 m/min in the low cutting speed range when machining powder metallurgically made duplex stainless steel 2205 and austenitic stainless steel 316L. In the high cutting speed range, from 100 to 250 m/min, fatigue-induced failure together with diffusion wear mechanism, affected the tool life of TiN-coated cemented carbide tools when machining both 316L and 2205 stainless steels. It was noticed that the tool life of TiN-coated high speed steel tools used in the low cutting speed range when machining 2205 steel was longer than that when machining 316L steel, whereas the tool life of TiN-coated cemented carbide tools used in the high cutting speed range when machining 316L steel was longer than that when machining 2205 steel.

  8. Active wear and failure mechanisms of TiN-Coated high speed steel and tin-coated cemented carbide tools when machining powder metallurgically made stainless steels

    NASA Astrophysics Data System (ADS)

    Jiang, Laizhu; Hänninen, Hannu; Paro, Jukka; Kauppinen, Veijo

    1996-09-01

    In this study, active wear and failure mechanisms of both TiN-coated high speed steel and TiN-coated cemented carbide tools when machining stainless steels made by powder metallurgy in low and high cutting speed ranges, respectively, have been investigated. Abrasive wear mechanisms, fatigue-induced failure, and adhesive and diffusion wear mechanisms mainly affected the tool life of TiN-coated high speed steel tools at cutting speeds below 35 m/min, between 35 and 45 m/min, and over 45 m/min, respectively. Additionally, fatigue-induced failure was active at cutting speeds over 45 m/min in the low cutting speed range when machining powder metallurgically made duplex stainless steel 2205 and austenitic stainless steel 316L. In the high cutting speed range, from 100 to 250 m/min, fatigue-induced failure together with diffusion wear mechanism, affected the tool life of TiN-coated cemented carbide tools when machining both 316L and 2205 stainless steels. It was noticed that the tool life of TiN-coated high speed steel tools used in the low cutting speed range when machining 2205 steel was longer than that when machining 316L steel, whereas the tool life of TiN-coated cemented carbide tools used in the high cutting speed range when machining 316L steel was longer than that when machining 2205 steel.

  9. Needs and challenges in precision wear measurement

    SciTech Connect

    Blau, P.J.

    1996-01-10

    Accurate, precise wear measurements are a key element in solving both current wear problems and in basic wear research. Applications range from assessing durability of micro-scale components to accurate screening of surface treatments and thin solid films. Need to distinguish small differences in wear tate presents formidable problems to those who are developing new materials and surface treatments. Methods for measuring wear in ASTM standard test methods are discussed. Errors in using alterate methods of wear measurement on the same test specimen are also described. Human judgemental factors are a concern in common methods for wear measurement, and an experiment involving measurement of a wear scar by ten different people is described. Precision in wear measurement is limited both by the capabilities of the measuring instruments and by the nonuniformity of the wear process. A method of measuring wear using nano-scale indentations is discussed. Current and future prospects for incorporating advanced, higher-precision wear measurement methods into standards are considered.

  10. Is the wear factor in total joint replacements dependent on the nominal contact stress in ultra-high molecular weight polyethylene contacts?

    PubMed

    Vassiliou, K; Unsworth, A

    2004-01-01

    The exact dependence of wear factor on contact stress, load and apparent contact area is much disputed in the literature. This study attempts to solve this dispute. Pin-on-plate studies of ultra high molecular weight polyethylene against stainless steel were conducted under different combinations of load (33-250 N), nominal stress (0.56-12.73 MPa) and face diameter, as well as two tests where both stress and load were kept constant, while the diameter was changed. For these tests the centre of the pin face was bored out to create four different average pin diameters with similar face areas. Diameter and load were found to have no significant effect on the wear factor, while the wear factor decreased with increasing contact stress according to the relation K = 2 x 10(-6) sigma(-0.84).

  11. Laser cladding for high-temperature self-lubricating wear-resistant composite coatings on γ-TiAl intermetallic alloy Ti-48Al-2Cr-2Nb

    NASA Astrophysics Data System (ADS)

    Liu, X. B.; Wang, C. M.; Yu, L. G.; Wang, Hua Ming

    2000-02-01

    High-temperature self-lubricating wear-resistant metal matrix composite coatings are fabricated on substrate of a (gamma) - TiAl intermetallic alloy Ti-48Al-2Cr-2Nb by laser cladding. The hybrid (gamma) -NiCr metal matrix composite coating is mainly reinforced by rapidly solidified wear-resistant phase of hyper-eutectic M7C3 and self-lubricating particles of Ag and CaF2 or CaAgF4. Microstructure and hardness within the whole laser clad composite coating is homogeneous and the bonding to the substrate is purely metallurgical. Both hardness and dry sliding wear resistance of the (gamma) -TiAl intermetallic alloy are significantly enhanced after laser cladding treatment.

  12. Comparison between PEEK and Ti6Al4V concerning micro-scale abrasion wear on dental applications.

    PubMed

    Sampaio, M; Buciumeanu, M; Henriques, B; Silva, F S; Souza, J C M; Gomes, J R

    2016-07-01

    In the oral cavity, abrasive wear is predictable at exposed tooth or restorative surfaces, during mastication and tooth brushing. Also, wear can occur at contacting surfaces between the Ti-based prosthetic structures and implants in presence of abrasive compounds from food or toothpaste. Thus, the aim of this work was to compare the abrasive wear resistance of PEEK and Ti6Al4V on three-body abrasion related to different hydrated silica content and loads. Surfaces of Ti6Al4V or PEEK cylinders (8mm diameter and 4mm height) were wet ground on SiC papers and then polished with 1µm diamond paste. After that, surfaces were ultrasonically cleaned in propyl alcohol for 15min and then in distilled water for 10min. Micro-scale abrasion tests were performed at 60rpm and on different normal loads (0.4, 0.8 or 1.2N) after 600 ball revolutions using suspensions with different weight contents of hydrated silica. After abrasive tests, wear scars on flat samples were measured to quantify the wear volume and characterized by scanning electron microscope (SEM) to identify the dominant wear mechanisms. Results showed a higher volume loss rate on PEEK than that recorded on Ti6Al4V,, when subjected to three-body abrasion tests involving hydrated silica suspensions. An increase in volume loss was noted on both tested materials when the abrasive content or load was increased. PEEK was characterized by less wear resistance than that on Ti6Al4V after micro-scale abrasion wear in contact with hydrated silica particles, as commonly found in toothpastes. Copyright © 2016 Elsevier Ltd. All rights reserved.

  13. Examining concussion rates and return to play in high school football players wearing newer helmet technology: a three-year prospective cohort study.

    PubMed

    Collins, Micky; Lovell, Mark R; Iverson, Grant L; Ide, Thad; Maroon, Joseph

    2006-02-01

    The purpose of this study was to compare concussion rates and recovery times for athletes wearing newer helmet technology compared to traditional helmet design. This was a three-year, prospective, naturalistic, cohort study. Participants were 2,141 high school athletes from Western Pennsylvania. Approximately half of the sample wore the Revolution helmet manufactured by Riddell, Inc. (n = 1,173) and the remainder of the sample used standard helmets (n = 968). Athletes underwent computerized neurocognitive testing through the use of ImPACT at the beginning of the study. Following a concussion, players were reevaluated at various time intervals until recovery was complete. In the total sample, the concussion rate in athletes wearing the Revolution was 5.3% and in athletes wearing standard helmets was 7.6% [chi (1, 2, 141) = 4.96, P < 0.027]. The relative risk estimate was 0.69 (95% confidence interval = 0.499- 0.958). Wearing the Revolution helmet was associated with approximately a 31% decreased relative risk and 2.3% decreased absolute risk for sustaining a concussion in this cohort study. The athletes wearing the Revolution did not differ from athletes wearing standard helmets on the mechanism of injury (e.g., head-to-head strike), on-field concussion markers (e.g., amnesia or loss of consciousness), or on-field presentation of symptoms (e.g., headaches, dizziness, or balance problems). Recent sophisticated laboratory research has better elucidated injury biomechanics associated with concussion in professional football players. This data has led to changes in helmet design and new helmet technology, which appears to have beneficial effects in reducing the incidence of cerebral concussion in high school football players.

  14. The Changes of COP and Foot Pressure after One Hour's Walking Wearing High-heeled and Flat Shoes

    PubMed Central

    Ko, Dong Yeol; Lee, Han Suk

    2013-01-01

    [Purpose] This study aimed to determine the most appropriate height for shoe heels by measuring the displacement of the COP (center of pressure) and changes in the distribution of foot pressure after walking in flat (0.5 cm), middle-heeled (4 cm), and high-heeled (9 cm) shoes for 1 hour. [Methods] A single-subject design was used, with 15 healthy women wearing shoes with heels of each height in a random order. The foot pressure and displacement of COP before and after walking in an ordinary environment for 1 hour were measured using an FDM-S (zebris Medical GmbH, Germany). [Results] The distribution of foot pressure did not change significantly after walking in middle-heeled (4 cm) shoes but did change significantly after walking in either flat (0.5 cm) or high-heeled (9 cm) shoes. Similarly, the COP was not significantly displaced after walking in middle-heeled (4 cm) shoes but was significantly displaced after walking in either flat (0.5 cm) or high-heeled (9 cm) shoes. [Conclusion] Both flat and high-heeled shoes had adverse effects on the body. Middle-heeled (4 cm) shoes are preferable to both flat (0.5 cm) and high-heeled (9 cm) shoes for the health and comfort of the feet. PMID:24259782

  15. The Changes of COP and Foot Pressure after One Hour's Walking Wearing High-heeled and Flat Shoes.

    PubMed

    Ko, Dong Yeol; Lee, Han Suk

    2013-10-01

    [Purpose] This study aimed to determine the most appropriate height for shoe heels by measuring the displacement of the COP (center of pressure) and changes in the distribution of foot pressure after walking in flat (0.5 cm), middle-heeled (4 cm), and high-heeled (9 cm) shoes for 1 hour. [Methods] A single-subject design was used, with 15 healthy women wearing shoes with heels of each height in a random order. The foot pressure and displacement of COP before and after walking in an ordinary environment for 1 hour were measured using an FDM-S (zebris Medical GmbH, Germany). [Results] The distribution of foot pressure did not change significantly after walking in middle-heeled (4 cm) shoes but did change significantly after walking in either flat (0.5 cm) or high-heeled (9 cm) shoes. Similarly, the COP was not significantly displaced after walking in middle-heeled (4 cm) shoes but was significantly displaced after walking in either flat (0.5 cm) or high-heeled (9 cm) shoes. [Conclusion] Both flat and high-heeled shoes had adverse effects on the body. Middle-heeled (4 cm) shoes are preferable to both flat (0.5 cm) and high-heeled (9 cm) shoes for the health and comfort of the feet.

  16. Wear performance of neat and vitamin E blended highly cross-linked PE under severe conditions: The combined effect of accelerated ageing and third body particles during wear test.

    PubMed

    Affatato, Saverio; De Mattia, Jonathan Salvatore; Bracco, Pierangiola; Pavoni, Eleonora; Taddei, Paola

    2016-12-01

    The objective of this study is to evaluate the effects of third-body particles on the in vitro wear behaviour of three different sets of polyethylene acetabular cups after prolonged testing in a hip simulator and accelerated ageing. Vitamin E-blended, cross-linked polyethylene (XLPE_VE), cross-linked polyethylene (XLPE) and conventional polyethylene (STD_PE) acetabular cups were simulator tested for two million cycles under severe conditions (i.e. by adding third-body particles to the bovine calf serum lubricant). Micro-Fourier Transform Infrared and micro-Raman spectroscopic analyses, differential scanning calorimetry, and crosslink density measurements were used to characterize the samples at a molecular level. The STD_PE cups had twice mass loss than the XLPE_VE components and four times than the XLPE samples; statistically significant differences were found between the mass losses of the three sets of cups. The observed wear trend was justified on the basis of the differences in cross-link density among the samples (XLPE>XLPE_VE>STD_PE). FTIR crystallinity profiles, bulk DSC crystallinity and surface micro-Raman crystallinity seemed to have a similar behaviour upon testing: all of them (as well as the all-trans and ortho-trans contents) revealed the most significant changes in XLPE and XLPE_VE samples. The more severe third-body wear testing conditions determined more noticeable changes in all spectroscopic markers with respect to previous tests. Unexpectedly, traces of bulk oxidation were found in both STD_PE (unirradiated) and XLPE (remelting-stabilized), which were expected to be stable to oxidation; on the contrary, XLPE_VE demonstrated a high oxidative stability in the present, highly demanding conditions.

  17. Wear Resistant Carbide-based Thermal Sprayed Coatings: Process, Properties, Mechanical Degradation and Wear

    NASA Astrophysics Data System (ADS)

    Ghabchi, Arash

    Thermally sprayed ceramic-metallic composite (CerMet) materials consist of ceramic particles mainly in form of carbides reinforced by metallic binder exhibit unique microstructural and mechanical characteristics. Such structure brings in a novel combination of hardness and toughness enabling application of this class of material in wear resistant surfaces. Final deposit microstructure that defines the mechanical properties and wear performance of material depends on process parameters and starting material characteristics. Complex interaction of in-flight particles with supersonic flame, formation of complex defective deposit structure comprising of pores, cracks and splat boundaries make comprehending of interrelation of process, microstructure, properties and performance a difficult task. Additional challenge is development of systematic understanding on mechanical degradation, damage and wear mechanisms of cermet coatings due to their complex structure. This dissertation attempts to address these issues first by taking a systematic step by step approach, process map, to establish a correlation between process, particle state, microstructure and properties. Different strategies were proposed and examined to control the high velocity thermal spray process. This strategy assessment enabled a better control over in-flight particles state in high velocity thermal spray process and provided better understanding on interaction of in-flight particles with the flame. Further, possible advantages of reducing the carbide particle size from micron to nano in terms of mechanical properties and different wear performance were explored. It was suggested that poor wear performance of nano-structured coating is due to presence of brittle phases and less available binder promotes the excessive stress detrimental to load carrying capability of material. Material damage and wear mechanisms of coating under different tribological conditions were examined. The results suggest a

  18. Low-wear partially fluorinated polyimides

    NASA Technical Reports Server (NTRS)

    Fusaro, R. L.; Hady, W. F.

    1985-01-01

    Tribological studies were conducted on five different polyimide solid bodies formulated from the diamine 2,2-bis 4-(4-aminophenoxy)pgenyl hexafluoropropane (4-BDAF) and the dianhydrides pyromellitic acid (PMDS) and benzophenonetetracarboxylic acid (BTDA). The following polyimides were evaluated 4-BDAF/PMDA, 4-BDAF/BTDA, 4-BDAF/80 mole percent PMDA, 20 mole percent BTDA, 4-BDAF/60 mole percent BTDA. Friction coefficients, polyimide wear rates, polyimide surface morphology and transfer films were evaluated at sliding speeds of 0.31 to 11.6 m/s and at temperatures of 25 C to 300 C. The results indicate that the tribological properties are highly dependent on the composition of the polyimide and on the experimental conditions. Two polyimides were found which produced very low wear rates but very high friction coefficients (greater than 0.85) under ambient conditions. They offer considerable potential for high traction types of application such as brakes.

  19. Low-wear partially fluorinated polyimides

    SciTech Connect

    Fusaro, R.L.; Hady, W.F.

    1985-10-01

    Tribological studies were conducted on five different polyimide solid bodies formulated from the diamine 2,2-bis 4-(4-aminophenoxy)pgenyl hexafluoropropane (4-BDAF) and the dianhydrides pyromellitic acid (PMDS) and benzophenonetetracarboxylic acid(BTDA). The following polyimides were evaluated 4-BDAF/PMDA, 4-BDAF/BTDA, 4-BDAF/80 mole percent PMDA, 20 mole percent BTDA, 4-BDAF/60 mole percent BTDA. Friction coefficients, polyimide wear rates, polyimide surface morphology and transfer films were evaluated at sliding speeds of 0.31 to 11.6 m/s and at temperatures of 25 C to 300 C. The results indicate that the tribological properties are highly dependent on the composition of the polyimide and on the experimental conditions. Two polyimides were found which produced very low wear rates but very high friction coefficients (greater than 0.85) under ambient conditions. They offer considerable potential for high traction types of application such as brakes. 28 references.

  20. Abrasive wear of structural ceramics

    SciTech Connect

    Olsson, M.; Kahlman, L.; Nyberg, B.

    1995-02-01

    The three-body abrasive wear characteristics of four different ceramic materials were investigated. The work focused on the influence of the type of abrasive particles (alumina and silicon carbide) on the wear rate and the dominating wear mechanisms. A solid-state-sintered silicon carbide (SiC), a silicon carbide reinforced with titanium diboride particles (SiC-TiB{sub 2}) and two hot-pressed silicon carbide-whisker-reinforced alumina materials (WRA I and WRAII) were studied. Of the materials investigated, an alumina reinforced with 25 wt% silicon carbide whiskers showed the highest abrasive resistance. This was probably caused by a unique combination of high hardness and high fracture toughness with a dense and homogeneous microstructure. Depending on the test conditions, plastic deformation, intercrystalline and transcrystalline cracking, and fracture were the dominating wear mechanisms of the materials. The silicon carbide abrasive resulted in 5--10 times higher wear rate than the alumina abrasive. This was mainly caused by the higher hardness of silicon carbide (3015 HV) as compared to alumina (2130 HV). The mechanical properties--i.e., hardness and fracture toughness--cannot be used alone to predict the abrasive wear behavior of engineering ceramics. Instead, the microstructural features, of the surface and the near-surface material--including homogeneity, surface porosity, secondary phases, and defect-rich regions--are important in controlling wear.

  1. The inhibitory effect of alendronate-hydroxyapatite composite coating on wear debris-induced peri-implant high bone turnover.

    PubMed

    Niu, Shun; Cao, Xiaorui; Zhang, Yan; Zhu, Qingsheng; Zhu, Jinyu

    2013-01-01

    Bisphosphonate (BP) has been confirmed as the most potent drug for enhancing implant stability. There have been few studies focused on BP-hydroxyapatite (HA) composite coatings, and the mechanisms through which BPs inhibit wear debris-induced high bone turnover have not been comprehensively discussed. Thirty rabbits were divided into three groups. HA-coated implants were inserted into the proximal region of the medullary cavity of the left tibia. In groups II and III, particles were injected around the implant and into the knee joint during implantation. Low-dose alendronate (ALN) was combined with the HA coating in group III. The efficacy of the composite coating was evaluated using several parameters, including the intra-articular pressure, histology of the synovial membranes and bone-implant interfaces, bone histomorphometry and mineralization, implant stability, osteolysis-related cytokine levels, and the duration of ALN release in vitro. The results indicate that the ALN-HA composite coating reduces peri-implant high bone turnover; improves bone-implant integration, bone quality, and implant stability; and inhibits particle migration. In vitro results suggest that the ALN-HA composite coating can afford long release duration. This study may help us further realize the mechanisms through which BPs enhance bone-implant integration in a state of peri-implant high bone turnover. BP-HA composite coatings are promising materials, particularly in revision surgeries. Copyright © 2013 Elsevier Inc. All rights reserved.

  2. Nanoscale friction and wear maps.

    PubMed

    Tambe, Nikhil S; Bhushan, Bharat

    2008-04-28

    Friction and wear are part and parcel of all walks of life, and for interfaces that are in close or near contact, tribology and mechanics are supremely important. They can critically influence the efficient functioning of devices and components. Nanoscale friction force follows a complex nonlinear dependence on multiple, often interdependent, interfacial and material properties. Various studies indicate that nanoscale devices may behave in ways that cannot be predicted from their larger counterparts. Nanoscale friction and wear mapping can help identify some 'sweet spots' that would give ultralow friction and near-zero wear. Mapping nanoscale friction and wear as a function of operating conditions and interface properties is a valuable tool and has the potential to impact the very way in which we design and select materials for nanotechnology applications.

  3. High temperature wear performance of HVOF-sprayed Cr3C2-WC-NiCoCrMo and Cr3C2-NiCr hardmetal coatings

    NASA Astrophysics Data System (ADS)

    Zhou, Wuxi; Zhou, Kesong; Li, Yuxi; Deng, Chunming; Zeng, Keli

    2017-09-01

    A novel Cr3C2-WC-NiCoCrMo and commercial Cr3C2-NiCr thermal spray-grade powders with particle size of -45 + 15 μm were prepared by an agglomeration and sintering process. Cr3C2-WC-NiCoCrMo and Cr3C2-NiCr coatings were deposited by high velocity oxygen fuel (HVOF) spraying. The fundamental properties of both coatings were evaluated and friction wear test against Al2O3 counterbodies of both coatings at high temperatures (450 °C, 550 °C, 650 °C) were carried out ball-on-disk high temperature tribometer. All specimens were characterized by optical microscopy, X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), scanning electron microscopy with energy dispersive spectroscopy (SEM/EDS) and 3D non-contact surface mapping profiler. The results have shown that the Cr3C2-WC-NiCoCrMo coating exhibited lower porosity, higher micro-hardness compared to the Cr3C2-NiCr coating. The Cr3C2-WC-NiCoCrMo coating also exhibited better wear resistance and higher friction coefficient compared to the Cr3C2-NiCr coating when sliding against the Al2O3 counterpart. Wear rates of both coatings increased with raising temperature. Both coatings experienced abrasive wear; hard phase particles (WC and Cr3C2) with different sizes, distributed in the matrix phase, will effectively improve the resistance against wear at high temperatures.

  4. Thirteen-year wear rate comparison of highly crosslinked and conventional polyethylene in total hip arthroplasty: long-term follow-up of a prospective randomized controlled trial.

    PubMed

    Teeter, Matthew G; Yuan, Xunhua; Somerville, Lyndsay E; MacDonald, Steven J; McCalden, Richard W; Naudie, Douglas D

    2017-06-01

    The purpose of this study was to report the radiographic wear rates from a previous randomized controlled trial of first-generation highly crosslinked versus conventional polyethylene in total hip arthroplasty (THA) at a minimum of 13 years' follow-up. Patients returned for radiographic imaging and radiostereometric analysis (RSA). Radiographs were reviewed for the presence of osteolysis or component loosening. Femoral head penetration (which includes both wear and creep) was measured using RSA. We compared Western Ontario and McMaster Universities Osteoarthritis Index (WOMAC), 12-Item Short Form Health Survey (SF-12) and Harris Hip Scores (HHS) with preoperative values. There was 1 revision in each group. There was no difference in WOMAC, SF-12, or HHS outcome scores between the highly crosslinked and conventional polyethylene groups (all p ≥ 0.13). Wear rate was lower with crosslinked polyethylene than conventional polyethylene (0.04 ± 0.02 mm/year v. 0.08 ± 0.03 mm/year, p = 0.007). First-generation crosslinked polyethylene demonstrates greater wear resistance than conventional polyethylene after 13 years of implantation. Crosslinked polyethylene continues to outperform conventional polyethylene into the second decade of implantation.

  5. Friction and Wear

    NASA Technical Reports Server (NTRS)

    Pomey, Jacques

    1952-01-01

    From the practical point of view, this analysis shows that each problem of friction or wear requires its particular solution. There is no universal solution; one or other of the factors predominates and defines the choice of the solution. In certain cases, copper alloys of great thermal conductivity are preferred; in others, plastics abundantly supplied with water. Sometimes, soft antifriction metals are desirable to distribute the load; at other times, hard metals with high resistance to abrasion or heat.

  6. Polymer Wear Modes.

    DTIC Science & Technology

    1977-10-01

    first was the rubbing of Nylon 6—6, Nylon 11, Delrin 500, Delrin AF, and ultra—high molecular weight polyethylene ( UHMWPE ) against 440C stainless steel...strength at* T T Measured Time to Temperature ofPolymer . room temp. _~~ _i ~2!~ U severe wear counterface substrate UHMWP E 24.1 MPa 140°C 400°C -1.47 rn/s

  7. New Mechanisms of rock-bit wear in geothermal wells

    SciTech Connect

    Macini, Paolo

    1996-01-24

    This paper presents recent results of an investigation on failure mode and wear of rock-bits used to drill geothermal wells located in the area of Larderello (Italy). A new wear mechanism, conceived from drilling records and dull bit evaluation analysis, has been identified and a particular configuration of rock-bit has been developed and tested in order to reduce drilling costs. The role of high Bottom Hole Temperature (BHT) on rock-bit performances seems not yet very well understood: so far, only drillability and formation abrasiveness are generally considered to account for poor drilling performances. In this paper, the detrimental effects of high BHT on sealing and reservoir system of Friction Bearing Rock-bits (FBR) have been investigated, and a new bearing wear pattern for FBR's run in high BHT holes has been identified and further verified via laboratory inspections on dull bits. A novel interpretation of flat worn cutting structure has been derived from the above wear pattern, suggesting the design of a particular bit configuration. Test bits, designed in the light of the above criteria, have been prepared and field tested successfully. The paper reports the results of these tests, which yielded a new rock-bit application, today considered as a standad practice in Italian geothermal fields. This application suggests that the correct evaluation of rock-bit wear can help to improve the overall drilling performances and to minimize drilling problems through a better interpretation of the relationships amongst rock-bits, formation properties and downhole temperature.

  8. Graphitic polymer nanocomposites: Wear performance and wear debris analysis

    NASA Astrophysics Data System (ADS)

    Liu, Tian

    With the addition of appropriate nanofillers, nanocomposites have been shown to be an effective avenue to achieve a multitude of enhanced properties, even extending to multi-functionalities not normally considered possible for conventional polymer materials. However, the structure and properties of polymeric nanocomposites can be influenced by some environmental factors in practical use, such as wear and temperature, due to the nature of viscoelasticity of polymer matrix. The large interfacial areas exist between matrix and nanofillers are also susceptible to the wear/temperature-related changes. In this work, I was devoted to developing high wear and/or thermal performance graphitic nanofiller reinforced high density polyethylene (HDPE) composites. Two critical issues, including appropriate filler-matrix interactions and proper dispersion of the nano-reinforcement, were addressed through the effective nanofiller surface modification. Wear, thermal and mechanical properties of the resultant nanocomposites were systematically investigated. Meanwhile, the wear debris generated on the sliding surface of composite materials was analyzed morphologically and quantitatively. In particular, the research regarding the possibility of determining the effects of wear and thermal processes on the nanocomposites by detecting dielectric signals over the lifetime of polymeric materials was conducted. Correlations that exist between effects of wear or thermal processes and dielectric properties of the nanocomposites were then explored. Based on the studies of HDPE nanocomposites, high quality ultrahigh molecular weight polyethylene (UHMWPE) nanocomposite reinforced by graphitic nanofillers was finally extended in this thesis. UHMWPE is an extremely viscous polymer and thus cannot be processed conventionally, typically resulting in dispersion issues far worse than that of other composite systems. The research presented aims at solving the issue by using ultrasonication-assisted melt

  9. Tribological characteristics of polyethylene glycol (PEG) as a lubricant for wear resistance of ultra-high-molecular-weight polyethylene (UHMWPE ) in artificial knee join.

    PubMed

    Kobayashi, Masanori; Koide, Takayuki; Hyon, Suong-Hyu

    2014-10-01

    For the longevity of total knee joint prostheses, we have developed an artificial lubricant using polyethylene glycol (PEG) for the prevention of wear of ultra-high-molecular-weight polyethylene (UHMWPE). In the present study, the lubricative function of this PEG lubricant was evaluated by a wear test using Co-Cr alloy and UHMWPE counter surface samples. As a result, human synovial fluid including the PEG lubricant showed good result regarding the wear volume and a worn surface of UHMWPE. Considering its lubrication mechanism, it is suspected that interaction between the PEG molecules and the proteins in synovial fluid was involved. Since PE molecules are also organic compounds having a hydroxyl group at one or both ends, the albumin and PEG molecule complex would have bound more strongly to the metal oxide surface and UHMWPE surfaces might enhance and stabilize the lubricating film between the contact surfaces under the boundary lubrication. This study suggests that PEG lubricant as an intra-articular viscous supplement has the potential to prevent wear of UHMWPE by mixing with synovial fluid and to contribute to the longevity of knee joint prostheses. Copyright © 2014 Elsevier Ltd. All rights reserved.

  10. Microstructure and high-temperature wear properties of in situ TiC composite coatings by plasma transferred arc surface alloying on gray cast iron

    NASA Astrophysics Data System (ADS)

    Zhao, Hang; Li, Jian-jun; Zheng, Zhi-zhen; Wang, Ai-hua; Huang, Qi-wen; Zeng, Da-wen

    2015-12-01

    In this work, an in situ synthesized TiC-reinforced metal matrix composite (MMC) coating of approximately 350-400 µm thickness was fabricated on a gray cast iron (GCI) substrate by plasma transferred arc (PTA) surface alloying of Ti-Fe alloy powder. Microhardness tests showed that the surface hardness increased approximately four-fold after the alloying treatment. The microstructure of the MMC coating was mainly composed of residual austenite, acicular martensite, and eutectic ledeburite. Scanning electron microscopy (SEM) and X-ray diffraction analyzes revealed that the in situ TiC particles, which were formed by direct reaction of Ti with carbon originally contained in the GCI, was uniformly distributed at the boundary of residual austenite in the alloying zone. Pin-on-disc high-temperature wear tests were performed on samples both with and without the MMC coating at room temperature and at elevated temperatures (473 K and 623 K), and the wear behavior and mechanism were investigated. The results showed that, after the PTA alloying treatment, the wear resistance of the samples improved significantly. On the basis of our analysis of the composite coatings by optical microscopy, SEM with energy-dispersive X-ray spectroscopy, and microhardness measurements, we attributed this improvement of wear resistance to the transformation of the microstructure and to the presence of TiC particles.

  11. Surface Design and Engineering Toward Wear-Resistant, Self-Lubricating Diamond Films and Coatings

    NASA Technical Reports Server (NTRS)

    Miyoshi, Kazuhisa

    1999-01-01

    The tribological properties of chemical-vapor-deposited (CVD) diamond films vary with the environment, possessing a Jekyll-and-Hyde character. CVD diamond has low coefficient of friction and high wear resistance in air but high coefficient of friction and low wear resistance in vacuum. Improving the tribological functionality of materials (such as achieving low friction and good wear resistance) was an aim of this investigation. Three studies on the surface design, surface engineering, and tribology of CVD diamond have shown that its friction and wear are significantly reduced in ultrahigh vacuum. The main criteria for judging whether diamond films are an effective wear-resistant, self-lubricating material were coefficient of friction and wear rate, which must be less than 0.1 and on the order of 10(exp 6) cu mm/N(dot)m, respectively. In the first study the presence of a thin film (less than 1 micron thick) of amorphous, nondiamond carbon (hydrogenated carbon, also called diamondlike carbon or DLC) on CVD diamond greatly decreased the coefficient of friction and the wear rate. Therefore, a thin DLC film on CVD diamond can be an effective wear-resistant, lubricating coating in ultrahigh vacuum. In the second study the presence of an amorphous, nondiamond carbon surface layer formed on CVD diamond by ion implantation significantly reduced the coefficient of friction and the wear rate in ultrahigh vacuum. Therefore, such surface layers are acceptable for effective self-lubricating, wear-resistant applications of CVD diamond. In the third study CVD diamond in contact with cubic boron nitride exhibited low coefficient of friction in ultra high vacuum. Therefore, this materials combination can provide an effective self-lubricating, wear-resistant couple in ultrahigh vacuum.

  12. Microscale and nanoscale surface strain mapping of single asperity wear in ultra high molecular weight polyethylene: Effects of materials, load, and asperity geometry.

    PubMed

    Wernlé, James D; Gilbert, Jeremy L

    2010-06-15

    Wear of ultra high molecular weight polyethylene (UHMWPE) is a limiting factor in longevity of joint replacements. Therefore, there is a desire to create new materials and enhance processing conditions associated with current materials to reduce wear. This requires understanding the effects of processing on performance of implants and of micron-scale wear mechanisms ongoing. Our goal is to generate detailed understanding of the micron-scale deformation-structure-properties relationships associated with UHMWPE subject to asperity wear processes and ultimately to be predictive of material success, in vivo. In this work, a surface strain analysis technique is developed and used to measure permanent strain from asperity deformations on the nano and micro scales. Deformation was applied to four material types (GUR 1050, GUR 1020, Hylamer, and Marathon) varying in molecular weight, crystallinity, and crosslinking. Surface strains were determined by mapping surface deformation fields and were compared across loading conditions and spatial scale, with variations in tip geometry and size, contact load, and material. Surface strains increased with asperity load for a fixed tip and were dependent on UHMWPE material, with a highly crystalline form exhibiting the most plastic strain and a crosslinked form exhibiting the least. Different asperity geometry [spherical microindenters with radius of 20 and 1500 mum, and a nanoindenter (Berkovich-type)] resulted in different surface strains (e.g., Berkovich vs. spherical were not similar) even when the nominal contact stress was similar. Finally, the extent of deformation during asperity wear correlates to the level of viscoelastic recovery of the materials observed after indentation testing. (c) 2009 Wiley Periodicals, Inc.

  13. Effects of Wearing a Compression Garment During Night Sleep on Recovery From High-Intensity Eccentric-Concentric Quadriceps Muscle Fatigue.

    PubMed

    Shimokochi, Yohei; Kuwano, Satoshi; Yamaguchi, Taichi; Abutani, Hiroyuki; Shima, Norihiro

    2017-10-01

    Shimokochi, Y, Kuwano, S, Yamaguchi, T, Abutani, H, and Shima, N. Effects of wearing a compression garment during night sleep on recovery from high-intensity eccentric-concentric quadriceps muscle fatigue. J Strength Cond Res 31(10): 2816-2824, 2017-This study aimed to investigate the effects of wearing a compression garment (CG) during night sleep on muscle fatigue recovery after high-intensity eccentric and concentric knee extensor exercises. Seventeen male college students participated in 2 experimental sessions under CG and non-CG (NCG) wearing conditions. Before night sleep under CG or NCG wearing conditions, the subjects performed a fatiguing protocol consisting of 10 sets of 10 repetitions of maximal isokinetic eccentric and concentric knee extensor contractions, with 30-second rest intervals between the sets. Immediately before and after and 24 hours after the fatiguing protocol, maximum voluntary isometric contraction (MVIC) force for knee extensor muscles was measured; surface electromyographic data from the vastus medialis and rectus femoris were also measured. A 2-way repeated-measure analysis of variance followed by Bonferroni pairwise comparisons were used to analyze the differences in each variable. Paired-sample t-tests were used to analyze the mean differences between the conditions at the same time points for each variable. The MVIC 24 hours after the fatiguing protocol was approximately 10% greater in the CG than in the NCG condition (p = 0.033). Changes in the electromyographic variables over time did not significantly differ between the conditions. Thus, it was concluded that wearing a CG during night sleep may promote localized muscle fatigue recovery but does not influence neurological factors after the fatiguing exercise.

  14. Scanning Electron Microscopy and Energy-Dispersive X-Ray Spectroscopy as a Valuable Tool to Investigate the Ultra-High-Molecular-Weight Polyethylene Wear Mechanisms and Debris in Hip Implants.

    PubMed

    Schappo, Henrique; Gindri, Izabelle M; Cubillos, Patrícia O; Maru, Marcia M; Salmoria, Gean V; Roesler, Carlos R M

    2017-08-01

    The use of scanning electron microscopy (SEM) and energy-dispersive spectrometry (EDS) was investigated to understand the wear mechanisms from a metal-on-polyethylene bearing couple. Morphological features of femoral head acetabular liner, and isolated particles resulting from hip wear testing were evaluated. EDS was proposed to investigate the polymeric nature of the particles isolated from the wear testing. In this work, 28-mm conventional ultra-high-molecular-weight polyethylene acetabular liners paired with metallic heads were tested in a hip wear simulator over 2 million cycles. SEM-EDS was employed to investigate wear mechanisms on hip implant components and associated wear debris. SEM showed worn surfaces for both hip components, and a significant volume of ultra-high-molecular-weight polyethylene wear particles resulting from hip wear testing. Particles were classified into 3 groups, which were then correlated to wear mechanisms. Group I had particles with smooth surfaces, group II consisted of particles with rough surfaces, and group III comprised aggregate-like particles. Group I EDS revealed that particles from groups I and II had a high C/O ratio raising a concern about the particle source. On the other hand, particles from group III had a low C/O ratio, supporting the hypothesis that they resulted from the wear of acetabular liner. Most of particles identified in group III were in the biologically active size range (0.3 to 20 μm). The use of optical and electron microscopy enabled the morphological characterization of worn surfaces and wear debris, while EDS was essential to elucidate the chemical composition of isolated debris. Copyright © 2017 Elsevier Inc. All rights reserved.

  15. The wear of cross-linked polyethylene against itself.

    PubMed

    Joyce, T J; Ash, H E; Unsworth, A

    1996-01-01

    Cross-linked polyethylene (XLPE) may have an application as a material for an all-plastic surface replacement finger joint. It is inexpensive, biocompatible and can be injection-moulded into the complex shapes that are found on the ends of the finger bones. Further, the cross-linking of polyethylene has significantly improved its mechanical properties. Therefore, the opportunity exists for an all-XLPE joint, and so the wear characteristics of XLPE sliding against itself have been investigated. Wear tests were carried out on both reciprocating pin-on-plate machines and a finger function simulator. The reciprocating pin-on-plate machines had pins loaded at 10 N and 40 N. All pin-on-plate tests show wear factors from the plates very much greater than those of the pins. After 349 km of sliding, a mean wear factor of 0.46 x 10(-6) mm3/N m was found for the plates compared with 0.021 x 10(-6) mm3/N m for the pins. A fatigue mechanism may be causing this phenomenon of greater plate wear. Tests using the finger function simulator give an average wear rate of 0.22 x 10(-6) mm3/N m after 368 km. This sliding distance is equivalent to 12.5 years of use in vivo. The wear factors found were comparable with those of ultra-high molecular weight polyethylene (UHMWPE) against a metallic counterface and, therefore, as the loads across the finger joint are much less than those across the knee or the hip, it is probable that an all-XLPE finger joint will be viable from a wear point of view.

  16. Wear of engineering materials

    SciTech Connect

    Hawk, J.A.

    1998-12-31

    Nearly 60 papers discuss fundamental and applied research in the areas of wear, erosion and wear-corrosion of materials. Focus is on ceramics, ceramic and polymer-matrix composites, and coatings; the effect of sliding wear and wear-corrosion of materials in manufacturing processes, automobiles and bearings; and wear and erosion of materials used in fossil-fuel power plants, minerals processing and heavy manufacturing.

  17. Drilling High Precision Holes in Ti6Al4V Using Rotary Ultrasonic Machining and Uncertainties Underlying Cutting Force, Tool Wear, and Production Inaccuracies.

    PubMed

    Chowdhury, M A K; Sharif Ullah, A M M; Anwar, Saqib

    2017-09-12

    Ti6Al4V alloys are difficult-to-cut materials that have extensive applications in the automotive and aerospace industry. A great deal of effort has been made to develop and improve the machining operations of Ti6Al4V alloys. This paper presents an experimental study that systematically analyzes the effects of the machining conditions (ultrasonic power, feed rate, spindle speed, and tool diameter) on the performance parameters (cutting force, tool wear, overcut error, and cylindricity error), while drilling high precision holes on the workpiece made of Ti6Al4V alloys using rotary ultrasonic machining (RUM). Numerical results were obtained by conducting experiments following the design of an experiment procedure. The effects of the machining conditions on each performance parameter have been determined by constructing a set of possibility distributions (i.e., trapezoidal fuzzy numbers) from the experimental data. A possibility distribution is a probability-distribution-neural representation of uncertainty, and is effective in quantifying the uncertainty underlying physical quantities when there is a limited number of data points which is the case here. Lastly, the optimal machining conditions have been identified using these possibility distributions.

  18. Drilling High Precision Holes in Ti6Al4V Using Rotary Ultrasonic Machining and Uncertainties Underlying Cutting Force, Tool Wear, and Production Inaccuracies

    PubMed Central

    Chowdhury, M. A. K.

    2017-01-01

    Ti6Al4V alloys are difficult-to-cut materials that have extensive applications in the automotive and aerospace industry. A great deal of effort has been made to develop and improve the machining operations of Ti6Al4V alloys. This paper presents an experimental study that systematically analyzes the effects of the machining conditions (ultrasonic power, feed rate, spindle speed, and tool diameter) on the performance parameters (cutting force, tool wear, overcut error, and cylindricity error), while drilling high precision holes on the workpiece made of Ti6Al4V alloys using rotary ultrasonic machining (RUM). Numerical results were obtained by conducting experiments following the design of an experiment procedure. The effects of the machining conditions on each performance parameter have been determined by constructing a set of possibility distributions (i.e., trapezoidal fuzzy numbers) from the experimental data. A possibility distribution is a probability-distribution-neural representation of uncertainty, and is effective in quantifying the uncertainty underlying physical quantities when there is a limited number of data points which is the case here. Lastly, the optimal machining conditions have been identified using these possibility distributions. PMID:28895876

  19. Wear Behavior of Plasma-Sprayed Carbon Nanotube-Reinforced Aluminum Oxide Coating in Marine and High-Temperature Environments

    NASA Astrophysics Data System (ADS)

    Keshri, Anup Kumar; Agarwal, Arvind

    2011-12-01

    Wear behavior of plasma-sprayed carbon nanotube (CNT)-reinforced aluminum oxide (Al2O3) composite coatings are investigated at room temperature (298 K), elevated temperature (873 K), and in sea water. Lowest wear volume loss was observed in the sea water as compared to dry sliding at 298 and 873 K. Relative improvement in the wear resistance of Al2O3-8 wt.% CNT coating compared to Al2O3 was 72% at 298 K, 76% at 873 K, and 66% in sea water. The improvement in the wear resistance of Al2O3-CNT coatings is attributed to (i) larger area coverage by protective film on the wear surface at room temperature and in sea water, (ii) higher fracture toughness of Al2O3-CNT coatings due to CNT bridging between splats, and (iii) anti-friction effect of sea water. The average coefficient of friction (COF) was the lowest (0.55) in sea water and the highest (0.83) at 873 K for Al2O3-8 wt.% CNT coating.

  20. 10-year follow-up wear analysis of first-generation highly crosslinked polyethylene in primary total hip arthroplasty.

    PubMed

    Snir, Nimrod; Kaye, Ian D; Klifto, Christopher S; Hamula, Mathew J; Wolfson, Theodore S; Schwarzkopf, Ran; Jaffe, Fredrick F

    2014-03-01

    Our goal was to report a 10-year follow up of linear penetration rates for HCLPE, and to determine whether a difference exists between penetrations measured on pelvis or hip anterior-posterior radiographs. We reviewed 48 total hip arthroplasties where a first-generation HCLPE liner was used. Femoral head penetration was measured on both AP pelvis and hip radiographs. Total wear and wear rate at 10 years were 1.26 mm and 0.122 mm/y, respectively. The rate decreased significantly after the first 2-3 years, plateauing at a wear rate of 0.05 mm/y for the last 5 years. The AP hip total wear and wear rate were 1.38 mm and 0.133 mm/y respectively, while rates were 1.13 mm and 0.109 mm/y respectively for the pelvis radiographs (P<.05). We found a significant difference in measurements of linear penetration when comparing AP pelvis vs. hip radiographs with lower rates recorded using an AP pelvis. © 2014.

  1. Morphological characteristics of total joint arthroplasty-derived ultra-high molecular weight polyethylene (UHMWPE) wear debris that provoke inflammation in a murine model of inflammation.

    PubMed

    Sieving, Allison; Wu, Bin; Mayton, Lois; Nasser, Sam; Wooley, Paul H

    2003-03-01

    It is recognized that the chronic inflammation in peri-prosthetic tissue that contributes to implant failure frequently is provoked by the presence of wear debris. Some wear debris is inevitable because of the nature of the prosthesis, but not all patients develop severe inflammatory responses. The precise factors that mediate the severity of tissue inflammation to wear debris has yet to be fully defined. Because wear debris retrieved from peri-prosthetic tissue consists of a heterogeneous mixture of materials with various sizes and shapes, this study evaluated the influence of two major physical aspects of ultra-high molecular weight polyethylene (UHMWPE) wear debris (shape and surface texture) using a model of tissue inflammation. UHMWPE debris particulates recovered from 50 peri-prosthetic tissue samples were examined by scanning electron microscopy and categorized into four groups based upon aspect ratio and surface texture of the material. The four groups were defined as: 1) smooth and globular, 2) smooth and fibular, 3) rough and globular, and 4) rough and fibular. Histological analysis and ELISA assays were conducted to evaluate variations in cellular responses and cytokine production between the groups. The strongest expression of tumor necrosis factor alpha and interleukin-1 beta was found in tissues exposed to UHMWPE debris with both a rough surface texture and fibular shape, and this response was significantly elevated over debris particles with a smooth surface texture and globular shape. The data suggest that both shape and texture influence the severity of specific inflammatory responses and that rough debris surface texture exerts a marked effect on adverse tissue responses when combined with particles that have a sharp, elongated shape.

  2. Intelligent Detection of Drill Wear

    NASA Astrophysics Data System (ADS)

    Liu, T. I.; Chen, W. Y.; Anatharaman, K. S.

    1998-11-01

    Backpropagation neural networks (BPNs) were used for on-line detection of drill wear. The neural network consisted of three layers: input, hidden, and output. The input vector comprised drill size, feed rate, spindle speed, and eight features obtained by processing the thrust and torque signals. The output was the drill wear state which either usable or failure. Drilling experiments with various drill sizes, feed rates and spindle speeds were carried out. The learning process was performed effectively by utilising backpropagation with smoothing and an activation function slope. The on-line detection of drill wear states using BPNs achieved 100% reliability even when the drill size, feed rate and spindle speed were changed. In other words, the developed on-line drill wear detection systems have very high robustness and hence can be used in very complex production environments, such as flexible manufacturing systems.

  3. Optical Diagnostic Characterization of High-Power Hall Thruster Wear and Operation

    NASA Technical Reports Server (NTRS)

    Williams, George J., Jr.; Soulas, George C.; Kamhawi, Hani

    2012-01-01

    Optical emission spectroscopy is employed to correlate BN insulator erosion with high-power Hall thruster operation. Specifically, actinometry leveraging excited xenon states is used to normalize the emission spectra of ground state boron as a function of thruster operating condition. Trends in the strength of the boron signal are correlated with thruster power, discharge voltage, and discharge current. In addition, the technique is demonstrated on metallic coupons embedded in the walls of the HiVHAc EM thruster. The OES technique captured the overall trend in the erosion of the coupons which boosts credibility in the method since there are no data to which to calibrate the erosion rates of high-power Hall thrusters. The boron signals are shown to trend linearly with discharge voltage for a fixed discharge current as expected. However, the boron signals of the higher-power NASA 300M and NASA 457Mv2 trend with discharge current and show an unexpectedly weak to inverse dependence on discharge voltage. Electron temperatures measured optically in the near-field plume of the thruster agree well with Langmuir probe data. However, the optical technique used to determine Te showed unacceptable sensitivity to the emission intensities. Near-field, single-frequency imaging of the xenon neutrals is also presented as a function of operating condition for the NASA 457 Mv2.

  4. Real-time measurement of camshaft wear in an automotive engine-a radiometric method

    SciTech Connect

    Schneider, E.W.; Blossfeld, D.H.

    1990-01-01

    A radiometric method has been developed for the determination of camshaft wear during engine operation. After a radioactive tracer is induced at the tips of one or more cam lobes by the technique of surface layer activation, calibration procedures are performed to determine the amount of radioactive material remaining versus the depth worn. The decrease in {gamma}-ray intensity measured external to the engine is then directly related to cam lobe wear. By incorporating a high-resolution detector and an internal radioactive standard, measurement accuracy better than {plus}{equals}0.2 {mu}m at 95% confidence has been achieved. Without the requirement of engine disassembly, this method has provided unique measurements of break-in wear and wear as a function of operating conditions. Because this approach requires only low levels of radiation, it has significant potential applications in wear control.

  5. Erosive wear of ductile metals by a particle-laden high velocity liquid jet

    SciTech Connect

    Ka-Keung Li, Simon; Humphrey, Joseph A. C.; Levy, Alan V.

    1981-11-30

    In this paper, a liquid-solid particle jet impingement flow apparatus is described and experimental measurements are reported for the accelerated erosion of copper, aluminum and mild steel sheet metal by coal suspensions in kerosene and Al2O3 and SiC suspensions in water. Slurry velocities of up to 130 ft s-1 (40 m s-1) and impingement angles of 15°–90° were investigated. The maximum particle concentration used was 40 wt.%. For high velocity the results of this work show two erosion maxima; these are found at impingement angles of 90° and 40°. However, in corresponding gas-solid particle investigations maximum erosion occurs at approximately 20°. In this work both particle concentration and composition were varied. Finally, a polynomial regression technique was used to calculate empirical and semitheoretical correlation constants.

  6. Wear of Vitamin E-Infused Highly Cross-Linked Polyethylene at Five Years.

    PubMed

    Shareghi, Bita; Johanson, Per-Erik; Kärrholm, Johan

    2017-09-06

    In an earlier study with a 2-year follow-up of uncemented cups, we had reported low femoral-head penetration of vitamin E-infused highly cross-linked polyethylene liners (E1) compared with highly cross-linked liners without vitamin E (ArComXL). We studied the penetration rate of E1 compared with that of ArComXL, with a focus on changes occurring between 2 and 5 years after total hip arthroplasty. In this randomized controlled study, we performed radiostereometric analysis of the penetration rate up to 5 years in 63 hips. During the total period of observation, the median proximal penetration for E1, 0.13 mm (mean, 0.11 mm [95% confidence interval (CI), 0.08 to 0.14 mm]), was lower than that for ArComXL, 0.20 mm (mean, 0.22 mm [95% CI, 0.17 to 0.26 mm]). The median proximal penetration rate between 2 and 5 years was 0.02 mm/yr (mean, 0.01 mm/yr [95% CI, 0.01 to 0.02 mm/yr]) for E1 and 0.04 mm/yr (mean, 0.04 mm/yr [95% CI, 0.03 to 0.05 mm/yr) for ArComXL. The corresponding median total (i.e., 3-dimensional resultant) penetration rates were 0.04 mm/yr (mean, 0.04 mm/yr [95% CI, 0.03 to 0.05 mm/yr]) for E1 and 0.07 mm/yr (mean, 0.08 mm/yr [95% CI, 0.06 to 0.10 mm/yr]) for ArComXL. From years 2 to 5, we observed increased penetration in both groups. The penetration rate was higher for ArComXL, resulting in more proximal and total penetration at 5 years than for E1. Therapeutic Level I. See Instructions for Authors for a complete description of levels of evidence.

  7. Features of erosion-corrosion wear in low-pressure evaporators of combined-cycle plant heat-recovery boilers at high void factor values

    NASA Astrophysics Data System (ADS)

    Galetsky, N. S.; Schwarz, A. L.

    2013-12-01

    The features of erosion-corrosion wear (ECW) in a low-pressure evaporator (LPE) combinedcycle plant (CCP) at high void factor values in the heat carrier are considered. It is shown that if the medium pressure in the evaporator is less than 1 MPa and steam quality x ≈ 0.5, the void fraction β is close to 1, at the outlet of the evaporator almost dry saturated steam moves, and the formation of liquid films is excluded. Under these conditions, the wear of the evaporator coil sections has an erosive nature, caused by high velocity steam, carrying the dense particles of corrosion products and large drops of water, previously plucked from the surface of the liquid films.

  8. Prevalence of dental wear among 12-year-old Brazilian adolescents using a modification of the tooth wear index.

    PubMed

    de Carvalho Sales-Peres, S H; Goya, S; de Araújo, J J; Sales-Peres, A; Lauris, J R P; Buzalaf, M A R

    2008-09-01

    This study investigated the prevalence of dental wear in 12-year-old adolescents using a modification of the tooth wear index (TWI). The modifications were proposed in order to fit with the World Health Organization standard, thus allowing application of the index in broad epidemiological surveys. An epidemiological cross-sectional survey was performed by trained, calibrated examiners, using a modified version of the TWI. Urban elementary schools were chosen because they provide a fair representation of the city's population in terms of socio-economic status. The sample included 295 adolescents, selected randomly and systematically. Dental wear was assessed by calibrated examiners (kappa>0.85), using a modified version of the TWI. This modified version includes a code for teeth restored due to wear, and another code for teeth that cannot be assessed. In addition, it does not differentiate the depth of dentine involvement. Proportions and confidence intervals were used to describe the prevalence of dental wear. Mann-Whitney test was used to detect differences in the degree of dental wear between males and females. The level of statistical significance was set at 5%. In total, 24,780 dental surfaces were evaluated. Among these surfaces, 73.10% did not present dental wear, 24.10% had incipient lesions, 2.46% had moderate lesions and 0.34% had been restored. No severe lesions were detected. Tooth wear was mainly seen on the occlusal/incisal surfaces (26.55%), involving enamel or enamel-dentine, but not the secondary dentine or pulp. The prevalence of dental wear was 26.90%. Considering the different teeth, wear was present in 53.22% of incisors, 50.51% of canines, 10.17% of premolars and 10.85% of molars. The prevalence of the different degrees of dental wear was similar in males and females (P>0.05). The modified TWI seems to be an effective tool for use in broad epidemiological surveys, due to easier calibration and high reproducibility rates.

  9. Abrasive wear properties of Cr-Cr3Si composites

    SciTech Connect

    Newkirk, J.W.; Hawk, Jeffrey A.

    2001-10-01

    A series of composites based on the Cr?Cr3Si system, and containing between 50 and 100%Cr3Si, were fabricated by hot pressing. These composites have high stiffness, good thermal conductivity, excellent chemical resistance, and high temperature creep and oxidation resistance, making them potential candidates for hard-facing applications and cutting tools in harsh environments. In this study, the Cr?Cr3Si composites were abrasion tested at ambient temperatures in order to evaluate their wear properties. Single scratch tests were performed to give insight into material removal mechanisms. Although like most metal silicides, these materials behave in a brittle manner, the results of this study indicate that the addition of a ductile second phase (Cr) can enhance both their fracture toughness and abrasive wear resistance. The addition of 10% of the rare earth oxide Er2O3 improves the density of the composite, but has no apparent influence on the wear resistance.

  10. Bench Wear and Single-Cylinder Engine Evaluations of High-Temperature Lubricants for U.S. Army Ground Vehicles

    DTIC Science & Technology

    1994-09-01

    because of viscosity increase, leakage from the rear crankshaft seal, and blowby increase. The blowby increase was caused by the alignment of the...additive concentration (as the oil evaporates), additive depletion, vaporization, and polymerization of the base stock. Extrinsic factors such as build...prohibitively difficult task. As previously stated, lubricant polymerization , additive depletion, oxidation resistance, lubricant vaporization, wear

  11. Effects of simulated oxidation on the in vitro wear and mechanical properties of irradiated and melted highly crosslinked UHMWPE.

    PubMed

    Oral, Ebru; Neils, Andrew L; Doshi, Brinda N; Fu, Jun; Muratoglu, Orhun K

    2016-02-01

    Radiation crosslinked ultrahigh molecular weight polyethylene (UHMWPE) have reduced the wear rate of the bearing surface in total joint arthroplasty and the incidence of peri-prosthetic bone loss due to wear particles. The oxidation potential afforded to the material by the trapped residual free radicals after irradiation was addressed in first generation crosslinked UHMWPEs by using thermal treatments such as annealing or melting after irradiation. Postirradiation melted crosslinked UHMWPE did not contain detectable free radicals at the time of implantation and was expected to be resistant against oxidation for the lifetime of the implants. Recent analyses of long-term retrievals showed it was possible for irradiated and melted UHMWPEs to oxidize in vivo but studies on the effects of oxidation on these materials have been limited. In this study, we determined the effects of in vitro aging on the wear and mechanical properties of irradiated and melted UHMWPE as a function of radiation dose and found that even small amount of oxidation (oxidation index of 0.1) can have detrimental effects on its mechanical properties. There was a gradual increase in the wear rate below an oxidation index of 1 and a drastic increase thereafter. Therefore, it was shown in a simulated environment that oxidation can have detrimental effects to the clinically relevant properties of irradiated and melted UHMWPEs.

  12. Effect of Continuous and Isothermal Hardening on the Wear Resistance of Tools Produced from High-Speed Steels

    NASA Astrophysics Data System (ADS)

    Murav'ev, V. I.; Chernobai, S. P.

    2003-05-01

    The effect of isothermal hardening on the red-hardness (heat resistance) of steel R18 is studied. A complex dependence of the red hardness on the temperature of isothermal hardening and the hold time is shown. Tools from steel R18 are shown to have maximum heat resistance and wear resistance after bainitic hardening in the "pre-transformation" range.

  13. Multifunctional Silicon Aluminum Oxynitride (SiAlON) Ceramic Coatings for High Temperature Applications

    DTIC Science & Technology

    2005-05-30

    Multifunctional Silicon Aluminum Oxynitride (SiAlON) Ceramic Coatings for High Temperature Applications 5b. GRANT NUMBER F49620-02-1-0323 5c. PROGRAM...Joan Fuller Multifunctional Silicon Aluminum Oxynitride (SiAION) Ceramic Coatings for High Temperature Applications Project Period: June 1, 2002 to May...Diagram and Structure of SiAION Ceramics 3.2. XPS Analysis of Chemical Bonding Effects 3.3. Auger Parameter Analysis 3.4. Wear Behavior versus Stoichiometry

  14. Wear tests of polymer composite compressor seal materials in hydrogen environments

    SciTech Connect

    Yu, K.; Bayliss, R.; Hillman, B.

    1999-07-01

    A high-speed reciprocating wear test rig with moisture control facilities has been further developed for undertaking wear tests in hydrogen environments with moisture content of 1--1,OOO ppmV to evaluate the wear performance of four commercial compressor seal materials. The test results are presented and compared to those obtained in nitrogen environment, where available. It was found that the wear rate and the friction coefficient of sample A increased significantly as moisture content decreased below {approximately}150 ppmV, whilst the other three samples showed much less or no dependence of the wear rates and the friction coefficients upon moisture content. Moreover, at moisture content below {approximately}150 ppmV, significant differences in the wear rate as well as friction coefficients were observed for Sample B in hydrogen and in nitrogen. The tests showed that, for a material for compressor applications, it is vitally important to undertake wear tests in the gas to be compressed and at the appropriate moisture levels to obtain a realistic evaluation of wear performance of the material.

  15. Influence of third-body particles originating from bone void fillers on the wear of ultra-high-molecular-weight polyethylene.

    PubMed

    Cowie, Raelene M; Carbone, Silvia; Aiken, Sean; Cooper, John J; Jennings, Louise M

    2016-08-01

    Calcium sulfate bone void fillers are increasingly being used for dead space management in infected arthroplasty revision surgery. The presence of these materials as loose beads close to the bearing surfaces of joint replacements gives the potential for them to enter the joint becoming trapped between the articulating surfaces; the resulting damage to cobalt chrome counterfaces and the subsequent wear of ultra-high-molecular-weight polyethylene is unknown. In this study, third-body damage to cobalt chrome counterfaces was simulated using particles of the calcium sulfate bone void fillers Stimulan(®) (Biocomposites Ltd., Keele, UK) and Osteoset(®) (Wright Medical Technology, TN, USA) using a bespoke rig. Scratches on the cobalt chrome plates were quantified in terms of their density and mean lip height, and the damage caused by the bone void fillers was compared to that caused by particles of SmartSet GMV PMMA bone cement (DePuy Synthes, IN, USA). The surface damage from Stimulan(®) was below the resolution of the analysis technique used; SmartSet GMV caused 0.19 scratches/mm with a mean lip height of 0.03 µm; Osteoset(®) led to a significantly higher number (1.62 scratches/mm) of scratches with a higher mean lip height (0.04 µm). Wear tests of ultra-high-molecular-weight polyethylene were carried out in a six-station multi-axial pin on plate reciprocating rig against the damaged plates and compared to negative (highly polished) and positive control plates damaged with a diamond stylus (2 µm lip height). The wear of ultra-high-molecular-weight polyethylene was shown to be similar against the negative control plates and those damaged with third-body particles; there was a significantly higher (p < 0.001) rate of ultra-high-molecular-weight polyethylene wear against the positive control plates. This study showed that bone void fillers of similar composition can cause varying damage to cobalt chrome counterfaces. However, the lip heights of the

  16. Influence of third-body particles originating from bone void fillers on the wear of ultra-high-molecular-weight polyethylene

    PubMed Central

    Cowie, Raelene M; Carbone, Silvia; Aiken, Sean; Cooper, John J; Jennings, Louise M

    2016-01-01

    Calcium sulfate bone void fillers are increasingly being used for dead space management in infected arthroplasty revision surgery. The presence of these materials as loose beads close to the bearing surfaces of joint replacements gives the potential for them to enter the joint becoming trapped between the articulating surfaces; the resulting damage to cobalt chrome counterfaces and the subsequent wear of ultra-high-molecular-weight polyethylene is unknown. In this study, third-body damage to cobalt chrome counterfaces was simulated using particles of the calcium sulfate bone void fillers Stimulan® (Biocomposites Ltd., Keele, UK) and Osteoset® (Wright Medical Technology, TN, USA) using a bespoke rig. Scratches on the cobalt chrome plates were quantified in terms of their density and mean lip height, and the damage caused by the bone void fillers was compared to that caused by particles of SmartSet GMV PMMA bone cement (DePuy Synthes, IN, USA). The surface damage from Stimulan® was below the resolution of the analysis technique used; SmartSet GMV caused 0.19 scratches/mm with a mean lip height of 0.03 µm; Osteoset® led to a significantly higher number (1.62 scratches/mm) of scratches with a higher mean lip height (0.04 µm). Wear tests of ultra-high-molecular-weight polyethylene were carried out in a six-station multi-axial pin on plate reciprocating rig against the damaged plates and compared to negative (highly polished) and positive control plates damaged with a diamond stylus (2 µm lip height). The wear of ultra-high-molecular-weight polyethylene was shown to be similar against the negative control plates and those damaged with third-body particles; there was a significantly higher (p < 0.001) rate of ultra-high-molecular-weight polyethylene wear against the positive control plates. This study showed that bone void fillers of similar composition can cause varying damage to cobalt chrome counterfaces. However, the lip heights of the scratches

  17. Investigations of mechanical and wear properties of alumina/titania/fire-clay reinforced epoxy composites

    NASA Astrophysics Data System (ADS)

    Patel, Vinay Kumar; Chauhan, Shivani; Sharma, Aarushi

    2016-05-01

    In this work, the effect of various particulates (alumina, titania, fire clay) reinforcements on mechanical and wear properties of epoxy composites have been studied with a prime motive of replacing the costly alumina and titania by much economical fire clay for high mechanical strength and/or wear resistant materials. Fire clay based epoxy composites delivered better mechanical (both tensile and impact) properties than the alumina filled or neat epoxy composites and slightly lower than titania reinforced composites, which qualified the fire clay a very suitable cost effective alternatives of both alumina and titania for high mechanical strength based applications. However, the poor wear behavior of fire clay reinforced composites revealed its poor candidacy for wear and tear applications.

  18. Friction, wear, transfer, and wear surface morphology of ultrahigh-molecular-weight polyethylene

    NASA Technical Reports Server (NTRS)

    Fusaro, R. L.

    1985-01-01

    Tribological studies at 25 C in a 50-percent-relative-humidity air atmosphere were conducted using hemispherically tipped 440 C HT (high temperature) stainless steel pins sliding against ultra-high-molecular-weight polyethylene (UHMWPE) disks. The results indicate that sliding speed, sliding distance, contact stress and specimen geometry can markedly affect friction, UHMWPE wear, UHMWPE transfer and the type of wear mechanisms that occur. Adhesion appears to be the predominant wear mechanism; but after long sliding distances at slow speeds, heavy ridges of transfer result which can induce fatigue-like wear on the UHMWPE disk wear track. In one instance, abrasive wear to the metallic pin was observed. This was caused by a hard particle embedded in the UHMWPE disk wear track.

  19. Microstructural Characterization and Wear Behavior of Nano-Boride Dispersed Coating on AISI 304 Stainless Steel by Hybrid High Velocity Oxy-Fuel Spraying Laser Surface Melting

    NASA Astrophysics Data System (ADS)

    Sharma, Prashant; Majumdar, Jyotsna Dutta

    2015-07-01

    The current study concerns the detailed microstructural characterization and investigation of wear behavior of nano-boride dispersed coating developed on AISI 304 stainless steel by high velocity oxy-fuel spray deposition of nickel-based alloy and subsequent laser melting. There is a significant refinement and homogenization of microstructure with improvement in microhardness due to laser surface melting (1200 VHN as compared to 945 VHN of as-sprayed and 250 VHN of as-received substrate). The high temperature phase stability of the as-coated and laser melted surface has been studied by differential scanning calorimeter followed by detailed phase analysis at room and elevated temperature. There is a significant improvement in wear resistance of laser melted surface as compared to as-sprayed and the as-received one due to increased hardness and reduced coefficient of friction. The mechanism of wear has been investigated in details. Corrosion resistance of the coating in a 3.56 wt pct NaCl solution is significantly improved (4.43 E-2 mm/year as compared to 5 E-1 mm/year of as-sprayed and 1.66 mm/year of as-received substrate) due to laser surface melting as compared to as-sprayed surface.

  20. Conjoint corrosion and wear in titanium alloys.

    PubMed

    Khan, M A; Williams, R L; Williams, D F

    1999-04-01

    When considering titanium alloys for orthopaedic applications it is important to examine the conjoint action of corrosion and wear. In this study we investigate the corrosion and wear behaviour of Ti-6Al-4V, Ti-6Al-7Nb and Ti-13Nb-13Zr in phosphate buffered saline (PBS), bovine albumin solutions in PBS and 10% foetal calf serum solutions in PBS. The tests were performed under four different conditions to evaluate the influence of wear on the corrosion and corrosion on the wear behaviour as follows: corrosion without wear, wear-accelerated corrosion, wear in a non-corrosive environment and wear in a corrosive environment. The corrosion behaviour was investigated using cyclic polarisation studies to measure the ability of the surface to repassivate following breakdown of the passive layer. The properties of the repassivated layer were evaluated by measuring changes in the surface hardness of the alloys. The amount of wear that had occurred was assessed from weight changes and measurement of the depth of the wear scar. It was found that in the presence of wear without corrosion the wear behaviour of Ti-13Nb-13Zr was greater than that of Ti-6Al-7Nb or Ti-6Al-4V and that in the presence of proteins the wear of all three alloys is reduced. In the presence of corrosion without wear Ti-13Nb-13Zr was more corrosion resistant than Ti-6Al-7Nb which was more corrosion resistant than Ti-6Al-4V without proteins whereas in the presence of protein the corrosion resistance of Ti-13Nb-13Zr and Ti-6Al-7Nb was reduced and that of Ti-6Al-4V increased. In the presence of corrosion and wear the corrosion resistance of Ti-13Nb-13Zr is higher than that of Ti-6Al-7Nb or Ti-6Al-4V in PBS but in the presence of proteins the corrosion resistance of Ti-13Nb-13Zr and Ti-6Al-7Nb are very similar but higher than that of Ti-6Al-4V. The wear of Ti-13Nb-13Zr is lower than that of Ti-6Al-7Nb and Ti-6Al-4V with or without the presence of proteins in a corrosive environment. Therefore the overall

  1. Wear Resistant Coatings for Titanium.

    DTIC Science & Technology

    1980-10-01

    resistant, chromium-molybdenum, electroplating, pulse- plating , surface treatment, heat treatment, dry-film lubricants. 20. Abstract (Continue on...to acknowledge the contributions provided by the following individuals. Messrs. S. Tefft and B. Zelazek conducted the plating and performed wear...Chromium-Molybdenum Application Procedure for Steels 28 APPENDIX C - Suggested Military Specification - Chromium-Molybdenum Plating (Electrodeposited

  2. Wear mechanism and wear prevention in coal-fueled diesel engines. Task 3, Traditional approaches to wear prevention

    SciTech Connect

    Schwalb, J.A.

    1991-06-01

    Contamination of the lube-oil with hard abrasive particles leads to a three-body abrasive wear mechanism that highly accelerates piston ring/cylinder liner wear in coal-fueled diesel engines. One approach to reducing that wear is to modify the size and orientation of surface asperities on the cylinder to enhance the formation of a hydrodynamic film, and to provide avenues of escape for particles that would otherwise be trapped in the wear zone. Another approach is to introduce additives into the contaminated lube-oil that further enhance hydrodynamic film formation, form chemical films on the wearing surfaces, or form films on the contaminant particles. This work focuses on defining the effects of cylinder liner surface finish, various configurations of slots in the cylinder liner surface, and various additives in the contaminated lube-oil on the wear process. Wear tests were initiated in a bench apparatus using coal-ash contaminated lube-oil to test the various wear configurations. The results of these tests indicate that the formation of a hydrodynamic film between the ring and cylinder specimens is enhanced by increasing surface roughness, and by orienting the surface asperities normal to the direction of ring travel but modifications to the cylinder liner surface did not greatly reduce the wear rate. Additives to the lubricant seemed to have a much more significant effect on wear, with a dispersant additive highly accelerating the wear, while a detergent additive was able to reduce the wear almost to the rate achieved where there was no contaminant.

  3. Friction and Wear Behavior of Silicon Under Conditions of Sliding.

    NASA Astrophysics Data System (ADS)

    Nadimpalli, Chandrasekhar Venkata

    Silicon is gaining importance as a material in micromechanical applications such as micromotors and microactuators. Friction and wear can affect the performance of these devices and hence it is important to study the friction and wear behavior of silicon. The deformation behavior of n-type silicon is fundamentally different from p-type. On deformation, n -type silicon may convert to p-type, but p-type silicon does not convert to n-type on deformation. This is related to the effect of dislocations interacting with the electrical charge carriers. Friction and wear behavior of n and p-type silicon was studied under conditions of sliding wear. Sliding was selected because the stress system associated with sliding introduces large plastic strains at the surface. The friction and wear behavior of n and p-type silicon is expected to be different due to the differences in their deformation behavior. Also, the n to p transition may show up in the friction and wear behavior. The samples were tested in air and in vacuum. Diamond was used as the slider. The wear tracks showed evidence of plastic flow. The morphology of this material was similar to that seen in more ductile materials. The coefficient of friction was also high. Other researchers have reported that DC Silicon transforms to a more ductile phase when sufficient pressure is applied. When shear stresses are present, as in sliding wear, the pressure for phase transformation has been reported to be about 8 GPa. The maximum pressure under the slider in the present set of experiments was estimated to be 8.2 GPa. Therefore, it is possible that transformed material extruded during sliding to produce the flow-like features observed at the wear track. The work involved in this phase transformation, as well as the work in deforming DC Silicon and/or the ductile product phase would contribute to the frictional energy. The debris from the air tests was DC silicon (as determined by XRD and TEM). No significant differences were

  4. Wear of materials 1985

    SciTech Connect

    Ludema, K.C.

    1985-01-01

    This book presents the papers given at a conference on wear resistance. Topics considered at the conference included erosion in aluminium oxides, abrasive wear tests, x-ray diffraction, transmission electron microscopy, wear tests of low-cobalt alloys for hardfacing nuclear components, microstructure, the elevated temperature erosion of steels, and steels under cyclic operation in corrosive liquids.

  5. Wear-mechanism modelling

    SciTech Connect

    Ashby, M.F. . Dept. of Engineering)

    1993-03-01

    Goals of the program are to calculate the surface temperatures in dry sliding, develop a soft wear tester for ceramics, survey the wear mechanisms in brittle solids, and couple the temperature calculations with models to give wear maps for brittle solids. (DLC)

  6. Comparison of joint angles and electromyographic activity of the lower extremities during standing with wearing standard and revised high-heeled shoes: A pilot study.

    PubMed

    Bae, Young-Hyeon; Ko, Mansoo; Lee, Suk Min

    2016-04-29

    Revised high-heeled shoes (HHSs) were designed to improve the shortcomings of standard HHSs. This study was conducted to compare revised and standard HHSs with regard to joint angles and electromyographic (EMG) activity of the lower extremities during standing. The participants were five healthy young women. Data regarding joint angles and EMG activity of the lower extremities were obtained under three conditions: barefoot, when wearing revised HHSs, and when wearing standard HHSs. Lower extremity joint angles in the three dimensional plane were confirmed using a VICON motion capture system. EMG activity of the lower extremities was measured using active bipolar surface EMG. Kruskal-Wallis one-way analysis of variance by rank applied to analyze differences during three standing conditions. Compared with the barefoot condition, the standard HHSs condition was more different than the revised HHSs condition with regard to lower extremity joint angles during standing. EMG activity of the lower extremities was different for the revised HHSs condition, but the differences among the three conditions were not significant. Wearing revised HHSs may positively impact joint angles and EMG activity of the lower extremities by improving body alignment while standing.

  7. Kinematics and kinetics of the lower extremities of young and elder women during stairs ascent while wearing low and high-heeled shoes.

    PubMed

    Hsue, Bih-Jen; Su, Fong-Chin

    2009-12-01

    The effect of the heel height on the temporal, kinematic and kinetic parameters was investigated in 16 young and 11 elderly females. Kinematic and kinetic data were collected when the subjects ascended stairs with their preferred speed in two conditions: wearing low-heeled shoes (LHS), and high-heeled shoes (HHS). The younger adults showed more adjustments in forces and moments at the knee and hip in frontal and transverse planes. Besides a few significantly changes in joint forces and moments, the elder group demonstrated longer cycle duration and double stance phase, larger trunk sideflexion and hip internal rotation, less hip adduction while wearing HHS. Most differences in joint motions between two groups were found at the hip and knee either in LHS or HHS condition. Instead, the differences in moment occurred at the hip joint and only in HHS. The interaction of the heel height and age showed the influences of heel height on trunk rotation, hip abduction/adduction, and knee and hip force and moment at the frontal plane depended on age. These phenomena suggest that younger and elderly women adapt their gait and postural control differently during stair ascent (SA) while wearing HHS.

  8. Erosive Wear Behavior of Nickel-Based High Alloy White Cast Iron Under Mining Conditions Using Orthogonal Array

    NASA Astrophysics Data System (ADS)

    Yoganandh, J.; Natarajan, S.; Babu, S. P. Kumaresh

    2013-09-01

    Nihard Grade-4, a nickel-bearing cast iron widely used in slurry pumps and hydrodynamic components, is evaluated for its erosive wear response under mining conditions using a statistical approach. Experiments were conducted by varying the factors namely velocity, slurry concentration, angle of impingement, and pH in three levels, using L9 orthogonal array. Analysis of variance was used to rank the factors influencing erosive wear. The results indicate that velocity is the most influencing factor followed by the angle of impingement, slurry concentration, and pH. Interaction effects of velocity, slurry concentration, angle of impingement, and pH on erosion rate have been discussed. Wear morphology was also studied using SEM characterization technique. At lower angle (30°) of impingement, the erosion of material is by micro fracture and shallow ploughing with the plastic deformation of the ductile austenitic matrix. At the normal angle (90°) of impingement, the material loss from the surface is found because of deep indentation, forming protruded lips which are removed by means of repeated impact of the erodent.

  9. Wear resistance of ductile irons

    NASA Astrophysics Data System (ADS)

    Lerner, Y. S.

    1994-06-01

    This study was undertaken to evaluate the wear resistance of different grades of ductile iron as alterna-tives to high- tensile- strength alloyed and inoculated gray irons and bronzes for machine- tool and high-pressure hydraulic components. Special test methods were employed to simulate typical conditions of reciprocating sliding wear with and without abrasive- contaminated lubricant for machine and press guideways. Quantitative relationships were established among wear rate, microstructure and micro-hardness of structural constituents, and nodule size of ductile iron. The frictional wear resistance of duc-tile iron as a bearing material was tested with hardened steel shafts using standard test techniques under continuous rotating movement with lubricant. Lubricated sliding wear tests on specimens and compo-nents for hydraulic equipment and apparatus were carried out on a special rig with reciprocating motion, simulating the working conditions in a piston/cylinder unit in a pressure range from 5 to 32 MPa. Rig and field tests on machine- tool components and units and on hydraulic parts have confirmed the test data.

  10. Rolling-contact and wear resistance of hard coatings on bearing-steel substrates

    SciTech Connect

    Erdemir, A.

    1992-02-01

    Ever-increasing needs for high-performance ball- and roller-bearing components that can endure extreme applications have led to a growing interest in hard coatings for improved fatigue life and wear resistance. In particular, hard TiN and TiC coatings and, quite recently, diamond like carbon films have attracted much attention from manufacturers that produce bearing systems for both rolling- and sliding-contact applications. This paper presents an overview that highlights recent incremental progress in achieving improved fatigue and wear resistance in bearing steels through the use of hard coatings. Effects of coating adhesion, thickness, and morphology on fatigue and wear resistance of hard coatings are discussed in detail. Specific references are made to a few mechanistic models that correlate coating thickness and adhesion to improved fatigue life and wear resistance.

  11. IMPROVEMENT OF WEAR COMPONENT'S PERFORMANCE BY UTILIZING ADVANCED MATERIALS AND NEW MANUFACTURING TECHNOLOGIES: CASTCON PROCESS FOR MINING APPLICATIONS

    SciTech Connect

    Xiaodi Huang; Richard Gertsch

    2003-02-27

    The project was highlighted by continued fabrication of drill bit inserts and testing them: (1) The inserts were subjected to hammer tests to determine brittleness. Selected inserts experienced multiple blows from a 16 pound sledge hammer. The resulting damage was minimal. (2) Three inserts were placed on three different 16.5 inch diameter rotary drill bits, and the bits drilled taconite rock until the entire bit failed. (3) The inserts had somewhat less wear resistance than current art, and exhibited no brittle failures. (4) More work is needed to produce the inserts at near net shape. The test inserts required too much machining. The project next turned to manufacturing 6.5 inch diameter disc cutters. The cutters will feature a core of tungsten carbide (TC) in a disc body composed of H13 tool steel. The TC inserts are in manufacture and the dies for the disc are being designed. The plan for next quarter: (1) Investigate materials and manufacturing changes for the fibrous monolith drill bit inserts that will increase their wear life. (2) Begin manufacturing disc cutters.

  12. Third-body abrasive wear challenge of 32 mm conventional and 44 mm highly crosslinked polyethylene liners in a hip simulator model.

    PubMed

    Sorimachi, T; Clarke, I C; Williams, P A; Gustafson, A; Yamamoto, K

    2009-07-01

    Hip simulator studies have shown that wear in the polyethylene liners used for total hip replacements increased with the larger-diameter femoral balls and could also be exacerbated by third-body abrasion. However, they also indicated that the more highly cross-linked polyethylene (HXPE) bearings were more wear resistant than conventional polyethylene (CXPE) bearings. Unfortunately the HXPE bearings appeared to be particularly sensitive to adverse wear conditions. One simulator study in particular indicated that poly(methyl methacrylate) (PMMA) debris increased wear sixfold by means of two-body abrasive interactions rather than the supposed third-body abrasion or roughening effects of the Co-Cr surfaces. There has been no confirmation of such novel theories. Therefore the goal of this study was to investigate the sensitivity of large-diameter HXPE bearings to the third-body PMMA wear challenge in a hip simulator model. An orbital hip simulator was used in standard test mode with a physiological load profile. The 32 mm control liners were machined from moulded GUR1050 and gamma irradiated to 35 kGy under nitrogen (CXPE). The 44 mm liners were also from moulded blanks, gamma irradiated to 75 kGy, machined to shape, given a proprietary heat treatment, and sterilized by gas plasma (HXPE). As in the published simulator model, the study was conducted in three phases. In phase 1, all cups were run in standard ('clean') lubricant for 1.5 x 10(6) cycles duration. In phase 2, three CXPE cups and six HXPE cups were run for 2 x 10(6) cycles with a slurry of PMMA particles added to the lubricant. In phase 3, the implants were again run in 'clean' lubricant for 2 x 10(6) cycles duration. In addition, three HXPE cups were run as wear controls for 5.5 x 10(6) cycles duration in clean lubricant. In phase-1, the HXPE liners demonstrated twelvefold reduced wear compared with the CXPE controls. The 32 mm and 44 mm Co-Cr balls were judged of comparable roughnesses. However, the surface

  13. The hardness, adhesion, and wear resistance of coatings developed for cobalt-base alloys

    SciTech Connect

    Cockeram, B.V.; Wilson, W.L.

    2000-05-01

    One potential approach for reducing the level of nuclear plant radiation exposure that results from activated cobalt wear debris is the use of a wear resistant coating. However, large differences in stiffness between a coating/substrate can result in high interfacial stresses that produce coating de-adhesion when a coated substrate is subjected to high stress wear contact. Scratch adhesion and indentation tests have been used to identify four promising coating processes [1,2]: (1) the use of a thin Cr-nitride coating with a hard and less-stiff interlayer, (2) the use of a thick, multilayered Cr-nitride coating with graded layers, (3) use of the duplex approach, or nitriding to harden the material subsurface followed by application of a multilayered Cr-nitride coating, and (4) application of nitriding alone. The processing, characterization, and adhesion of these coating systems are discussed. The wear resistance and performance has been evaluated using laboratory pin-on-disc, 4-ball, and high stress rolling contact tests. Based on the results of these tests, the best coating candidate from the high-stress rolling contact wear test was the thin duplex coating, which consists of ion nitriding followed deposition of a thin Cr-nitride coating, while the thin Cr-nitride coating exhibited the best results in the 4-ball wear test.

  14. Development of Modified Pag (Polyalkylene Glycol) High VI High Fuel Efficient Lubricant for LDV Applications

    SciTech Connect

    Gangopadhyay, Arup; McWatt, D. G.; Zdrodowski, R. J.; Liu, Zak; Elie, Larry; Simko, S. J.; Erdemir, Ali; Ramirez, Giovanni; Cuthbert, J.; Hock, E. D.

    2015-09-30

    Engine oils play a critical role in friction reduction. Improvements in engine oil technology steadily improved fuel economy as the industry moved through ILSAC GF-1 to GF-5 specifications. These improvements were influenced by changes in base oil chemistry, development of new friction modifiers and their treat levels, and the total additive package consisting of various other components. However, the improvements are incremental and further fuel consumption reduction opportunities are becoming more challenging. Polyalkylene glycol (PAG) based engine oils are being explored as a step forward for significant fuel consumption reduction. Although PAG fluids are used in many industrial applications, its application as an engine oil has been explored in a limited way. The objective of this project is to deep dive in exploring the applicability of PAG technology in engine oil, understanding the benefits, and limitations, elucidating the mechanism(s) for friction benefits, if any, and finally recommending how to address any limitations. The project was designed in four steps, starting with selection of lubricant technology, followed by friction and wear evaluations in laboratory bench tests which are relatively simple and inexpensive and also served as a screener for further evaluation. Selected formulations were chosen for more complex engine component level tests i.e., motored valvetrain friction and wear, piston ring friction using a motored single cylinder, and motored engine tests. A couple of formulations were further selected based on component level tests for engine dyno tests i.e., Sequence VID (ASTM D6709) for fuel economy, Sequence IVA (ASTM D6891) for valvetrain wear, and Sequence VG (ASTM D6593) for sludge and varnish protection. These are some of the industry standard tests required for qualifying engine oils. Out of these tests, a single PAG oil was selected for chassis roll dynamometer tests for fuel economy and emission measurements using FTP (Federal

  15. Wear Behavior Characterization for the Screening of Magnesium-based Alloys

    NASA Astrophysics Data System (ADS)

    McGhee, Paul R.

    This research is focused on the development of a systematic approach to evaluate the selection of materials for Mg-based alloys under wear conditions for biomedical applications. A pilot study was carried out in order to establish an accurate and reliable wear testing technique for magnesium and its alloys. This pilot study was conducted on aluminum (Al) and pure Mg, and showed that aluminum has a lower wear rate compared to Mg. The technique displayed good repeatability and high precision. For the main study, an ERC Mg-based alloy was to be compared with pure Mg. The same technique, when applied to pure Mg from a different vendor, produced up to 90% scatter in the data. Microstructure was studied to see if it had any correlation with the scatter. It was discovered that Mg ingot from the second vendor had outsized grains that contributed to the disproportional scatter in the wear data. Increasing the stroke length during wear testing was required so that the wear data would be averaged over multiple grains and reduces the variation in computed wear rates. In the main study, wear behavior and friction properties were analyzed using microtribometery, mechanical stylus profilometry, and microindentation. Surface morphology and microstructure were characterized using optical microscopy, scanning electron microscopy, and optical profilometry. For the main study, pure Mg and the ERC alloy as-cast and extruded conditions were compared. Pure Mg and MZCR alloys were extruded at 350°C and 400°C, respectively. Mg and MZCR alloy were cast at 350°C and heat treated at 510°C. The extruded specimens were divided into two sections, cross-section and longitudinal section. Wear tests were carried out under the applied normal load 0.5 N - 2.5 N in 0.5 N increments sliding at a rate of 0.2 Hz for 240 passes. The results show that the alloying and extrusion processes increase the hardness of the MZCR alloy significantly up to 80%. The as-cast MZCR has a lower resistance to wear

  16. Sliding wear of oxide ceramics at elevated temperatures

    SciTech Connect

    Senda, Tetsuya; Drennan, J.; McPherson, R.

    1995-11-01

    Sliding wear tests of sintered alumina and mullite consistently showed that the wear loss significantly decreased at 800 C and above by an order of magnitude. Microscopy of the room-temperature wear surfaces revealed a feature suggesting material removal by brittle fracture. Microscopy of the wear surface at 1,000 C revealed that the immediate vicinity of the wear surface consisted of a very fine grain size polycrystalline structure. The zone below this consisted of heavily deformed grains containing dense dislocation networks forming a cellular structure. The results suggest that, at high temperatures, dynamic recrystallization at the wear surface forms the fine grain size structure which suppresses further material removal.

  17. Wear mechanism and wear prevention in coal-fueled diesel engines

    SciTech Connect

    Schwalb, J.A.; Ryan, T.W.

    1991-10-01

    Coal fueled diesel engines present unique wear problems in the piston ring/cylinder liner area because of their tendency to contaminate the lube-oil with high concentrations of highly abrasive particles. This program involved a series of bench-scale wear tests and engine tests designed to investigate various aspects of the ring/liner wear problem and to make specific recommendations to engine manufacturers as to how to alleviate these problems. The program was organized into tasks, designed to accomplish the following objectives: (1) define the predominant wear mechanisms causing accelerated wear in the ring/liner area; (2) investigate the effectiveness of traditional approaches to wear prevention to prevent wear in coal-fueled engines; (3) further refine information on the most promising approaches to wear prevention; (4) present detailed information and recommendations to engine manufacturers on the most promising approach to wear prevention; (5) present a final report covering the entire program; (6)complete engine tests with a coal-derived liquid fuel, and investigate the effects of the fuel on engine wear and emissions.

  18. Wear mechanism and wear prevention in coal-fueled diesel engines. Final report

    SciTech Connect

    Schwalb, J.A.; Ryan, T.W.

    1991-10-01

    Coal fueled diesel engines present unique wear problems in the piston ring/cylinder liner area because of their tendency to contaminate the lube-oil with high concentrations of highly abrasive particles. This program involved a series of bench-scale wear tests and engine tests designed to investigate various aspects of the ring/liner wear problem and to make specific recommendations to engine manufacturers as to how to alleviate these problems. The program was organized into tasks, designed to accomplish the following objectives: (1) define the predominant wear mechanisms causing accelerated wear in the ring/liner area; (2) investigate the effectiveness of traditional approaches to wear prevention to prevent wear in coal-fueled engines; (3) further refine information on the most promising approaches to wear prevention; (4) present detailed information and recommendations to engine manufacturers on the most promising approach to wear prevention; (5) present a final report covering the entire program; (6)complete engine tests with a coal-derived liquid fuel, and investigate the effects of the fuel on engine wear and emissions.

  19. Gasification Slag and the Mechanisms by Which Phosphorous Additions Reduce Slag Wear and Corrosion in High Cr2O3 Refractories

    NASA Astrophysics Data System (ADS)

    Bennett, James; Nakano, Anna; Nakano, Jinichiro; Thomas, Hugh

    Gasification is a high-temperature/high-pressure process that converts carbonaceous materials such as coal and/or petcoke into CO and H2, feedstock materials used in power generation and chemical production. Gasification is considered an important technology because of its high process efficiency and the ability to capture environmental pollutants such as CO2, SO3 and Hg. Ash impurities in the carbon feedstock materials melt and coalesce during gasification (1325-1575 °C), becoming slag that attaches to and flows down the gasifier sidewall, corroding and eroding the high Cr2O3 refractory liner used to protect the gasification chamber. Phosphate additions to high Cr2O3 refractory have been found to alter slag/refractory interactions and dramatically reduce refractory wear by the following mechanisms: a) spinel formation, b) slag chemistry changes, c) two phase liquid formation, and d) oxidation state changes. The mechanisms and how they work together to impact material wear/corrosion will be discussed.

  20. The Effect of Long-Time Austenization on the Wear Resistance and Thermal Fatigue Properties of a High-Speed Steel Roll

    NASA Astrophysics Data System (ADS)

    Zhang, Xiaodan; Liu, Wei; Godfrey, Andrew; Liu, Qing

    2009-09-01

    The effects of a long-time austenization treatment on a high-speed steel (HSS) roll have been investigated. Several interesting phenomena were observed, including the decomposition of the primary bulky M3C carbides on grain boundaries and the precipitation of a large number of MC carbides of size comparable to the primary MC carbides in the grains. As a consequence of these changes, the overall carbide size decreased and the homogeneity of the carbide distribution increased. The wear resistance and thermal fatigue properties of the HSS roll were also investigated, and it was found that the long-time austenization treatment resulted in improvements to both properties.

  1. Commercialization of NASA's High Strength Cast Aluminum Alloy for High Temperature Applications

    NASA Technical Reports Server (NTRS)

    Lee, Jonathan A.

    2003-01-01

    In this paper, the commercialization of a new high strength cast aluminum alloy, invented by NASA-Marshall Space Flight Center, for high temperature applications will be presented. Originally developed to meet U.S. automotive legislation requiring low- exhaust emission, the novel NASA aluminum alloy offers dramatic improvement in tensile and fatigue strengths at elevated temperatures (450 F-750 F), which can lead to reducing part weight and cost as well as improving performance for automotive engine applications. It is an ideal low cost material for cast components such as pistons, cylinder heads, cylinder liners, connecting rods, turbo chargers, impellers, actuators, brake calipers and rotors. NASA alloy also offers greater wear resistance, dimensional stability, and lower thermal expansion compared to conventional aluminum alloys, and the new alloy can be produced economically from sand, permanent mold and investment casting. Since 2001, this technology was licensed to several companies for automotive and marine internal combustion engines applications.

  2. In-vivo degradation of middle-term highly cross-linked and remelted polyethylene cups: Modification induced by creep, wear and oxidation.

    PubMed

    Miura, Yoshihiro; Hasegawa, Masahiro; Sudo, Akihiro; Pezzotti, Giuseppe; Puppulin, Leonardo

    2015-11-01

    In this study Raman (RS) and Fourier Transform Infrared (FT-IR) spectroscopic techniques were exploited to study 11 retrieved liners made of remelted highly cross-linked polyethylene (HXLPE), with the intent to elucidate their in-vivo mechanical and chemical degradation. The retrievals had different follow-ups, ranging from a few months to 7 years of implantation time and belong to the first generation of highly cross-linked and remelted polyethylene clinically introduced in 1999, but still currently implanted. Raman assessments enabled to discriminate contributes of wear and creep on the total reduction of thickness in different locations of the cup. According to our results, although the most of the viscoelastic deformation occurred during the first year (bedding-in period), it progressed during the steady wear state up to 7 years with much lower but not negligible rate. Overall, the wear rate of this remelted HXLPE liner was low. Preliminary analysis on microtomed sections of the liners after in-vivo and in-vitro accelerated aging (ASTM F2003-02) enabled to obtain a phenomenological correlation between the oxidation index (OI) and the amount of orthorhombic phase fraction (αc), which can be easily non-destructively measured by RS. Profiles of αc obtained from different locations of the cups were used to judge the oxidative degradation of the 11 retrievals, considering also the ex-vivo time elapsed from the revision surgery to the spectroscopic experiments. Low but measurable level of oxidation was detected in all the short-term retrievals, while in the middle-term samples peaks of OI were observed in the subsurface (up to OI=4.5), presumably induced by the combined effect of mechanical stress, lipid absorption and prolonged ex-vivo shelf-aging in air. Copyright © 2015 Elsevier Ltd. All rights reserved.

  3. The Impact of Weather on Women’s Tendency to Wear Red or Pink when at High Risk for Conception

    PubMed Central

    Tracy, Jessica L.; Beall, Alec T.

    2014-01-01

    Women are particularly motivated to enhance their sexual attractiveness during their most fertile period, and men perceive shades of red, when associated with women, as sexually attractive. Building on this research, we recently found that women are more likely to wear reddish clothing when at peak fertility (Beall & Tracy, 2013), presumably as a way of increasing their attractiveness. Here, we first report results from a methodological replication, conducted during warmer weather, which produced a null effect. Investigating this discrepancy, we considered the impact of a potentially relevant contextual difference between previous research and the replication: current weather. If the red-dress effect is driven by a desire to increase one’s sexual appeal, then it should emerge most reliably when peak-fertility women have few alternative options for accomplishing this goal (e.g., wearing minimal clothing). Results from re-analyses of our previously collected data and a new experiment support this account, by demonstrating that the link between fertility and red/pink dress emerges robustly in cold, but not warm, weather. Together, these findings suggest that the previously documented red-dress effect is moderated by current climate concerns, and provide further evidence that under certain circumstances red/pink dress is reliably associated with female fertility. PMID:24586414

  4. The impact of weather on women's tendency to wear red or pink when at high risk for conception.

    PubMed

    Tracy, Jessica L; Beall, Alec T

    2014-01-01

    Women are particularly motivated to enhance their sexual attractiveness during their most fertile period, and men perceive shades of red, when associated with women, as sexually attractive. Building on this research, we recently found that women are more likely to wear reddish clothing when at peak fertility (Beall & Tracy, 2013), presumably as a way of increasing their attractiveness. Here, we first report results from a methodological replication, conducted during warmer weather, which produced a null effect. Investigating this discrepancy, we considered the impact of a potentially relevant contextual difference between previous research and the replication: current weather. If the red-dress effect is driven by a desire to increase one's sexual appeal, then it should emerge most reliably when peak-fertility women have few alternative options for accomplishing this goal (e.g., wearing minimal clothing). Results from re-analyses of our previously collected data and a new experiment support this account, by demonstrating that the link between fertility and red/pink dress emerges robustly in cold, but not warm, weather. Together, these findings suggest that the previously documented red-dress effect is moderated by current climate concerns, and provide further evidence that under certain circumstances red/pink dress is reliably associated with female fertility.

  5. Advanced Wear-resistant Nanocomposites for Increased Energy Efficiency

    SciTech Connect

    Cook, B. A.; Harringa, J. L.; Russel, A. M.

    2012-12-01

    This report summarizes the work performed by an Ames-led project team under a 4-year DOE-ITP sponsored project titled, 'Advanced Wear-resistant Nanocomposites for Increased Energy Efficiency.' The Report serves as the project deliverable for the CPS agreement number 15015. The purpose of this project was to develop and commercialize a family of lightweight, bulk composite materials that are highly resistant to degradation by erosive and abrasive wear. These materials, based on AlMgB{sub 14}, are projected to save over 30 TBtu of energy per year when fully implemented in industrial applications, with the associated environmental benefits of eliminating the burning of 1.5 M tons/yr of coal and averting the release of 4.2 M tons/yr of CO{sub 2} into the air. This program targeted applications in the mining, drilling, machining, and dry erosion applications as key platforms for initial commercialization, which includes some of the most severe wear conditions in industry. Production-scale manufacturing of this technology has begun through a start-up company, NewTech Ceramics (NTC). This project included providing technical support to NTC in order to facilitate cost-effective mass production of the wear-resistant boride components. Resolution of issues related to processing scale-up, reduction in energy intensity during processing, and improving the quality and performance of the composites, without adding to the cost of processing were among the primary technical focus areas of this program. Compositional refinements were also investigated in order to achieve the maximum wear resistance. In addition, synthesis of large-scale, single-phase AlMgB{sub 14} powder was conducted for use as PVD sputtering targets for nanocoating applications.

  6. Analysis of the application of the generalized monod kinetics model to describe the human corneal oxygen-consumption rate during soft contact lens wear.

    PubMed

    Compañ, V; Aguilella-Arzo, M; Del Castillo, L F; Hernández, S I; Gonzalez-Meijome, J M

    2017-11-01

    This work is an analysis of the application of the generalized Monod kinetics model describing human corneal oxygen consumption during soft contact lens wear to models previously used by Chhabra et al. (J Biomed Mater Res B Appl Biomater, 2009a;90:202-209, Optom Vis Sci 2009b;86:454-466) and Larrea and Büchler (Invest Ophthalmol Vis Sci 2009;50:1076-1080). We use oxygen tension from in vivo estimations provided by Bonanno [Bonanno et al., Invest Ophthalmol Vis Sci 2002;43:371-376, and Bonanno et al 2009]. We consider four hydrogel and six silicone hydrogel lenses. The cornea is considered a single homogeneous layer, with constant oxygen permeability regardless of the type of lens worn. Our calculations yield different values for the maximum oxygen consumption rate Qc,max , whith differents oxygen tensions (high and low pc ) at the cornea-tears interface. Surprisingly, for both models, we observe an increase in oxygen consumption near an oxygen tension of 105 mmHg until a maximum is reached, then decreasing for higher levels of oxygen pressure. That is, when lowering the pressure of oxygen, the parameter Qc,max initially increases depending on the intensity of the change in pressure. Which, it could be related with the variation of the pH. Furthermore, it is also noted that to greater reductions in pressure, this parameter decreases, possibly due to changes in the concentration of glucose related to the anaerobic respiration. The averaged in vivo human corneal oxygen consumption rate of 1.47 × 10(-4) cm(3) of O2 /cm(3) tissue s, with Monod kinetics model, considering all the lenses studied, is smaller than the average oxygen consumption rate value obtained using the Larrea and Büchler model. The impact that these calculations have on the oxygen partial pressure available at different depths in the corneal tissue is presented and discussed, taking into consideration previous models used in this study. © 2016 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl

  7. Tooth Wear Inclination in Great Ape Molars.

    PubMed

    Knight-Sadler, Jordan; Fiorenza, Luca

    2017-01-01

    Primate dietary diversity is reflected in their dental morphology, with differences in size and shape of teeth. In particular, the tooth wear angle can provide insight into a species' ability to break down certain foods. To examine dietary and masticatory information, digitized polygon models of dental casts provide a basis for quantitative analysis of wear associated with tooth attrition. In this study, we analyze and compare the wear patterns of Pongo pygmaeus, Gorilla gorillagorilla and Pan troglodytes schweinfurthii lower molars, focusing on the degree of inclination of specific wear facets. The variation in wear angles appears to be indicative of jaw movements and the specific stresses imposed on food during mastication, reflecting thus the ecology of these species. Orangutans exhibit flatter wear angles, more typical of a diet consisting of hard and brittle foods, while gorillas show a wear pattern with a high degree of inclination, reflecting thus their more leafy diet. Chimpanzees, on the other hand, show intermediate inclinations, a pattern that could be related to their highly variable diet. This method is demonstrated to be a powerful tool for better understanding the relationship between food, mastication and tooth wear processes in living primates, and can be potentially used to reconstruct the diet of fossil species. © 2017 S. Karger AG, Basel.

  8. Plasma enhanced chemical vapor deposition of wear resistant gradual a-Si1-x:Cx:H coatings on nickel-titanium for biomedical applications

    NASA Astrophysics Data System (ADS)

    Niermann, Benedikt; Böke, Marc; Schauer, Janine-Christina; Winter, Jörg

    2010-03-01

    Plasma enhanced chemical vapor deposition has been used to deposit thin films with gradual transitions from silicon to carbon on Cu, Ni, stainless steel, and NiTi. Thus show low stress, elasticity, and wear resistance with excellent adhesion on all metals under investigation. Already at low Si concentrations of 10 at. % the intrinsic stress is considerably reduced compared to pure diamondlike carbon (DLC) films. The deposition process is controlled by optical emission spectroscopy. This technique has been applied to monitor the growth precursors and to correlate them with the film composition. The compositions of the films were determined by Rutherford backscattering spectroscopy and XPS measurements. Due to the elastic properties of the gradual transition and the excellent biocompatibility of DLC, the described film systems present a useful coating for biomedical applications.

  9. Effect of size and dimensional tolerance of reverse total shoulder arthroplasty on wear: An in-silico study.

    PubMed

    Mattei, Lorenza; Di Puccio, Francesca; Joyce, Thomas J; Ciulli, Enrico

    2016-08-01

    Although huge research efforts have been devoted to wear analysis of ultra-high molecular weight polyethylene (UHMWPE) in hip and knee implants, shoulder prostheses have been studied only marginally. Recently, the authors presented a numerical wear model of reverse total shoulder arthroplasties (RTSAs), and its application for estimating the wear coefficient k from experimental data according to different wear laws. In this study, such model and k expressions are exploited to investigate the sensitivity of UHMWPE wear to implant size and dimensional tolerance. A set of 10 different geometries was analysed, considering nominal diameters in the range 36-42mm, available on the market, and a cup dimensional tolerance of +0.2, -0.0mm (resulting in a diametrical clearance ranging between 0.04-0.24mm), estimated from measurements on RTSAs. Since the most reliable wear law and wear coefficient k for UHMWPE are still controversial in the literature, both the Archard law (AR) and the wear law of UHMWPE (PE), as well as four different k expressions were considered, carrying out a total of 40 simulations. Results showed that the wear volume increases with the implant size and decreases with the dimensional tolerance for both the wear laws. Interestingly, different trends were obtained for the maximum wear depth vs. clearance: the best performing implants should have a high conformity according to the AR law but low conformity for the PE law. However, according to both laws, wear is highly affected by both implant size and dimensional tolerance, although it is much more sensitive to the latter, with up to a twofold variation of wear predicted. Indeed, dimensional tolerance directly alters the clearance, and therefore the lubrication and contact pressure distribution in the implant. Rather surprisingly the role of dimensional tolerance has been completely disregarded in the literature, as well as in the standards. Furthermore, this study notes some important issues for future

  10. Velocity Dependence of Nanoscale Friction, Adhesion and Wear

    NASA Astrophysics Data System (ADS)

    Tambe, Nikhil; Bhushan, Bharat

    The advent of micro/nanostructures and the subsequent miniaturization of moving components for various nanotechnology applications, such as micro/nanoelectromechanical systems (MEMS/NEMS), have ascribed paramount importance to tribology and mechanics on the nanoscale. Most of these micro/nanodevices and components operate at very high sliding velocities (of the order of tens of mm/s to few m/s). Atomic force microscopy (AFM) studies into potential materials, coatings and lubricants for these devices have been rendered inadequate due to the inherent limitations on the highest sliding velocities achievable with commercial AFMs (<250 μm/s). The development of a new AFM-based technique has allowed nanotribological investigations to be performed over a wide range of velocities (up to 10 mm/s). Research conducted on various materials, coatings and lubricants reveals a strong velocity dependence of friction, adhesion and wear on the nanoscale. Based on the experimental evidence, theoretical formulations have been realized for nanoscale friction behavior in order to design a comprehensive analytical model that explains the velocity dependence. The model takes into consideration the contributions of adhesion at the tip-sample interface, high impact velocity related deformations at the contacting asperities, and atomic-scale stick-slip. Dominant friction mechanisms are identified and critical operating parameters for their transitions are defined. Wear studies are conducted at high sliding velocities to elucidate the primary failure mechanisms. A novel AFM-based nanowear mapping technique to map wear on the nanoscale is developed, and the interdependence of normal load and sliding velocity on sample surface wear is studied. This technique helps identify and classify wear mechanisms and determine the critical parameters responsible for their transitions. The interdependence of mechanical and tribological properties for various materials is explored and tribologically ideal

  11. Fundamental deformation processes controlling nanoscale friction and wear

    NASA Astrophysics Data System (ADS)

    Gotsmann, Bernd

    2010-03-01

    Thermally activated processes are often responsible for the kinetics of deformation and can control tribological performance. In this contribution two such processes are discussed in combination with nanoscale tribology experiments using atomic force microscopy (AFM). The first process describes single asperity wear as an atom-by-atom loss process driven by frictional shear stresses an interface. The wear rate is described by a thermally activated bond breaking process in which the energy barrier is reduced by the frictional shear stress. This leads to dramatic deviations from Archard's wear law which is commonly used to described macroscopic wear. Experimental confirmation of an atom-by-atom wear process is given by AFM wear experiments using different material combinations of tips sliding on surfaces [1]. The second process relates fundamental rearranging processes in polymers to friction. As an example, data of sliding friction between a silicon tip and a highly cross-linked polyaryletherketone film using friction force microscopy are presented. Energy dissipation into so-called molecular relaxations (alpha and beta relaxations) is identified as distinctive maxima of the friction force as a function of temperature between 150 and 500 K. A strong shift of such peak temperatures as a function of applied load is observed. Again, a model with an Arrhenius activation modulated by the applied shear stress describes experimental results quantitatively. The effect of the stress-shifted relaxation on friction-versus-load experiments is discussed [2]. Both processes will be discussed in the context of technological applications. [4pt] [1] B. Gotsmann and M. A. Lantz, Phys. Rev. Lett. 101, 125501 (2008) [0pt] [2] L. Jansen et al. Phys. Rev. Lett. 102, 236101 (2009)

  12. Biologically Based Restorative Management of Tooth Wear

    PubMed Central

    Kelleher, Martin G. D.; Bomfim, Deborah I.; Austin, Rupert S.

    2012-01-01

    The prevalence and severity of tooth wear is increasing in industrialised nations. Yet, there is no high-level evidence to support or refute any therapeutic intervention. In the absence of such evidence, many currently prevailing management strategies for tooth wear may be failing in their duty of care to first and foremost improve the oral health of patients with this disease. This paper promotes biologically sound approaches to the management of tooth wear on the basis of current best evidence of the aetiology and clinical features of this disease. The relative risks and benefits of the varying approaches to managing tooth wear are discussed with reference to long-term follow-up studies. Using reference to ethical standards such as “The Daughter Test”, this paper presents case reports of patients with moderate-to-severe levels of tooth wear managed in line with these biologically sound principles. PMID:22315608

  13. Optical wear assessment system for grinding tools

    NASA Astrophysics Data System (ADS)

    Heger, Thomas; Pandit, Madhukar C.

    2003-04-01

    The inspection and monitoring of the wear of grinding tools is essential in order to ensure the quality of the grinding tool and the finished product. Present methods rely on dismounting the grinding tool for examination of the grinding tool surface. Often, the state of the grinding tool surface is checked indirectly by evaluating the quality of the workpiece. The application of image processing which offers an effective means for in situ inspection and monitoring is described in the paper. By using multi-directional illumination and image fusion, an image with a high degree of relevant information is generated that is then segmented using the wavelet transform (MSA) and classified to distinguish grains and cavities. Results of the application of the algorithms for a high performance grinding wheel with CBN grains embedded in a resin base are presented.

  14. Wear mechanism and wear prevention in coal-fueled diesel engines

    SciTech Connect

    Schwalb, J.A.

    1991-06-01

    Contamination of the lube-oil with hard abrasive particles leads to a three-body abrasive wear mechanism that highly accelerates piston ring/cylinder liner wear in coal-fueled diesel engines. One approach to reducing that wear is to modify the size and orientation of surface asperities on the cylinder to enhance the formation of a hydrodynamic film, and to provide avenues of escape for particles that would otherwise be trapped in the wear zone. Another approach is to introduce additives into the contaminated lube-oil that further enhance hydrodynamic film formation, form chemical films on the wearing surfaces, or form films on the contaminant particles. This work focuses on defining the effects of cylinder liner surface finish, various configurations of slots in the cylinder liner surface, and various additives in the contaminated lube-oil on the wear process. Wear tests were initiated in a bench apparatus using coal-ash contaminated lube-oil to test the various wear configurations. The results of these tests indicate that the formation of a hydrodynamic film between the ring and cylinder specimens is enhanced by increasing surface roughness, and by orienting the surface asperities normal to the direction of ring travel but modifications to the cylinder liner surface did not greatly reduce the wear rate. Additives to the lubricant seemed to have a much more significant effect on wear, with a dispersant additive highly accelerating the wear, while a detergent additive was able to reduce the wear almost to the rate achieved where there was no contaminant.

  15. The application of high-speed camera for analysis of chip creation process during the steel turning

    NASA Astrophysics Data System (ADS)

    Struzikiewicz, Grzegorz

    2016-09-01

    The paper presents the results of application of the high-speed camera Phantom v5.2 and Tracker program for the analysis of chip forming in the case of the AMS6265 steel turning. The experimental research was carried for two cutting speeds and different wear of cutting inserts.

  16. Wear resistance of polypropylene-SiC composite

    NASA Astrophysics Data System (ADS)

    Abenojar, J.; Enciso, B.; Martínez, MA; Velasco, F.

    2017-05-01

    In this work, the wear resistance of thermoplastic composites with a high amount of ceramic is evaluated. Composites made of polypropylene (PP) and silicon carbide (SiC) powder at 50 wt% were used with the final objective of manufacturing ablative materials. This is the first part of a project studying the wear resistance and the mechanical properties of those composites, to be used in applications like habitat industry. In theory, the exposure to high temperature of ablative materials involves the elimination of thermal energy by the sacrifice of surface polymer. In our case, PP will act as a heat sink, up to the reaction temperature (melting or sublimation), where endothermic chemical decomposition into charred material and gaseous products occurs. As the surface is eroded, it is formed a SiC like-foam with improved insulation performance. Composites were produced by extrusion and hot compression. The wear characterization was performed by pin-on-disk test. Wear test was carried out under standard ASTM G99. The parameters were 120 rpm speed, 15 N load, a alumina ball with 6 mm as pin and 1000 m sliding distance. The tracks were also observed by opto-digital microscope.

  17. Tribopolymerization as an anti-wear mechanism. Quarterly progress report

    SciTech Connect

    Furey, M.J.

    1996-04-01

    The primary objective of this activity is to obtain the necessary data which would enhance, promote, and encourage the introduction of advanced lubrication technology into the marketplace. This includes (a) defining specific but different applications, (b) establishing the limits or ranges of applied loads, speeds, and temperatures over which the concept of tribopolymerization would work in reducing wear and/or friction, (c) continuing in efforts to understand the film-forming process (this rates to (b) above), using this knowledge to develop new and even more effective additives, and (d) exploring possible connections with private and investment companies for the licensing and marketing of products which will reduce friction and wear in a variety of applications. Progress was made in several different but connected areas. These included (a) establishing of load/velocity limits of selected monomers for ceramic lubrication, (b) the discovery of new and effective monomers designed for higher temperature anti-wear applications, (c) improvements and modifications of the high load/high speed pin-on-disk machine, (d) the initiation of related or spin-off projects designed to get their advanced technology into the marketplace, (e) the filing of three new patent applications, and (f) collaborative research with Dr. Kajdas--the co-inventor with Dr. Furey--on tribopolymerization as a novel and effective approach to the boundary lubrication of ceramics and steel. These and other elements of progress made during the first Quarter of 1996 are discussed briefly.

  18. Wear studies on the likely performance of CFR-PEEK/CoCrMo for use as artificial joint bearing materials.

    PubMed

    Scholes, S C; Unsworth, A

    2009-01-01

    It is well known that a reduction in the volume of wear produced by articulating surfaces in artificial joints is likely to result in a lower incidence of failure due to wear particle induced osteolysis. Therefore, new materials have been introduced in an effort to produce bearing surfaces with lower, more biologically acceptable wear. Polyetheretherketone (PEEK-OPTIMA) has been successfully used in a number of implant applications due to its combination of mechanical strength and biocompatibility. Pin-on-plate wear tests were performed on various combinations of PEEK-OPTIMA and carbon fibre reinforced PEEK-OPTIMA (CFR-PEEK) against various CoCrMo alloys to assess the potential of this material combination for use in orthopaedic implants. The PEEK/low carbon CoCrMo produced the highest wear. CFR-PEEK against high carbon or low carbon CoCrMo provided low wear factors. Pin-on-plate tests performed on ultra-high molecular weight polyethylene (UHMWPE) against CoCrMo (using comparable test conditions) have shown similar or higher wear than that found for CFR-PEEK/CoCrMo. This study gives confidence in the likelihood of this material combination performing well in orthopaedic applications.

  19. Wear of ultra-high molecular weight polyethylene acetabular cups in a physiological hip joint simulator in the anatomical position using bovine serum as a lubricant.

    PubMed

    Bigsby, R J; Hardaker, C S; Fisher, J

    1997-01-01

    The Leeds physiological anatomical (PA) hip joint simulator was developed to apply three axes of loading and a complex three-dimensional motion so that the forces and motions can reproduce exactly the walking cycles defined by Paul. This paper presents the results of a study using the Leeds PA hip joint simulator to determine the wear of 32 mm ultra-high molecular weight polyethylene (UHMWPE) acetabular cups against stainless steel and zirconia ceramic heads, using bovine serum as lubricant. These results have been compared with the results of a previous study that used water as the lubricant, which led to UHMWPE transfer film being formed on the stainless steel head. Comparisons are also made with clinical results and results from other simulators. The study indicates that it is preferable to use bovine serum in simulator studies. In addition, the results indicate that if the surface roughness of the metallic and femoral heads are similar, and they remain undamaged during the tests, the wear rates of the UHMWPE cups are likely to be similar.

  20. Wear of moderately cross-linked polyethylene in fixed-bearing total knee replacements.

    PubMed

    Brockett, Claire L; Jennings, Louise M; Hardaker, Catherine; Fisher, John

    2012-07-01

    Cross-linked polyethylene has been introduced into total joint replacement to improve wear resistance. Although the performance of highly cross-linked polyethylene is well documented clinically and experimentally for total hip replacements, the reduction in mechanical properties with increasing irradiation is of concern for application to total knee replacement. The aim of this study was to investigate the wear performance of a moderately cross-linked polyethylene material in a fixed-bearing total knee replacement. The study was conducted using two femoral geometries, a conventional cruciate-retaining femoral and a high-flexion femoral geometry. The femoral geometry appeared to have no effect on the wear of the knee replacement under standard gait conditions. A significant reduction in wear volume was measured with the moderately cross-linked polyethylene compared with the conventional polyethylene over a six-million-cycle wear study. This study indicates the use of a moderately cross-linked polyethylene in a fixed-bearing total knee replacement may provide a low wearing option for total knee replacement.

  1. Study of Wear-Preventive Properties of Macrocyclic Compounds for High Temperature Application

    DTIC Science & Technology

    1990-01-01

    RESEARCH INSTITUTE K . [. J. Vesely, Jr. . . Manager Senior Engineer f Li Chemistry Re ch Section ..... M. K. S. Rajan, Ph.D. ... Res I cirector Principal...4 1.1.1.2 Graphite Fluoride .............................. 4 1.1.1.3 Non-Lamilnar Lubricants.......................... 5 1.1.1.4 Organic Solids as...erty as compared to that in the absence of water. IR.H. Savage; J. Appl. Phys. 19, (1948); ibid 27, 136 (󈧼)]. 1.1.1.2 Graphite Fluoride Graphite

  2. Aluminum nanocomposites having wear resistance better than stainless steel

    SciTech Connect

    An, Linan; Qu, Jun; Luo, Jinsong; Fan, Yi; Zhang, Ligong; Liu, Jinling; Xu, Chengying; Blau, Peter Julian

    2011-01-01

    Tribological behavior of alumina-particle-reinforced aluminum composites made by powder metallurgy process has been investigated. The nanocomposite containing 15 vol% of Al2O3 nanoparticles exhibits excellent wear resistance by showing significantly low wear rate and abrasive wear mode. The wear rate of the nanocomposite is even lower than stainless steel. We have also demonstrated that such excellent wear resistance only occurred in the composite reinforced with the high volume fraction of nanosized reinforcing particles. The results were discussed in terms of the microstructure of the nanocomposite.

  3. Research on the effect of wear-ring clearances to the axial and radial force of a centrifugal pump

    NASA Astrophysics Data System (ADS)

    Zhao, W. G.; Y He, M.; Qi, C. X.; Li, Y. B.

    2013-12-01

    Varying of the wear-ring clearance not only has a distinct effect on the volumetric loss of the centrifugal pump, but also on the performance of the centrifugal pump including the axial and radial forces. Comparing with the experimental studies, numerical simulation methods have some special advantages, such as the low cost, fast and high efficiency, and convenient to get the detailed structure of the internal flow characteristics, so it has been widely used in the fluid machinery study in recent years. In order to study the effect of wear-ring clearance on the force performance of the centrifugal pump, based on the Reynolds Time-Averaged N-S equations and RNG k-ε turbulence model, a centrifugal pump with three variable styles of the wear-rings was simulated: Only the clearance of the front wear-ring was changed, only the clearance of the back wear-ring was changed and both were changed. Comparing with the experiment, numerical results show a good agreement. In the three changing styles of the clearance, the variable of the clearance of front wear-ring has the most influence on the axial force of the centrifugal pump, while has tiny effect on the radial force for all the conditions.

  4. Characterization of Wear Mechanisms in Distorted Conical Picks After Coal Cutting

    NASA Astrophysics Data System (ADS)

    Dewangan, Saurabh; Chattopadhyaya, Somnath

    2016-01-01

    The interest in understanding the wear mechanisms of cemented carbide (CC) is not a new development. For a long time, there have been studies on different wear mechanisms under different coal/rock cutting conditions. These studies have helped improving the quality of CC, thereby preventing such wearing of tools. Due to highly unpredictable character of coal/rock, the wearing phenomena cannot be attributed to one single domain of conditions. However, one conclusion that can be drawn in this context is that, under similar working conditions, similar types of CC undergo similar nature of wearing process. An optimum combination of high wear resistance, strength and hardness has facilitated widespread application of CC in the field of mining engineering. The abrasive parts of the mining tools are made of CC materials. The current study is focussed on a detailed characterization of the wear mechanisms of conical picks, which are used for coal mining. Conical picks consist of a steel body with an inserted cone-shaped CC tip. After being used for a certain period of time, both, the CC tip and the steel body get distorted. In this study, selection of appropriate samples was followed by critical observation of them through field emission scanning electron microscopy (FESEM) and energy dispersive X-ray spectroscopy (EDS). In the previous study, we explained the distortion process of both, the tip as well as the body, using the SEM images. For the present study, two samples were taken from our previous investigation for further analysis. Three other samples were also included in the present study. Seven different types of wear mechanisms, such as, cracking and crushing, cavity formation, coal intermixing, chemical degradation along with abrasion, long and deep cracks, heating effect and body deformation were observed in the five tool samples.

  5. Nanoscale thermomechanics of wear-resilient polymeric bilayer systems.

    PubMed

    Kaule, Tassilo; Zhang, Yi; Emmerling, Sebastian; Pihan, Sascha; Foerch, Renate; Gutmann, Jochen; Butt, Hans-Jürgen; Berger, Rüdiger; Duerig, Urs; Knoll, Armin W

    2013-01-22

    We explore the effect of an ultrathin elastic coating to optimize the mechanical stability of an underlying polymer film for nanoscale applications. The coating consists of a several nanometer thin plasma-polymerized norbornene layer. Scanning probes are used to characterize the system in terms of shear-force-induced wear and thermally assisted indentation. The layer transforms a weakly performing polystyrene film into a highly wear-resistive system, ideal for high-density and low-power data storage applications. The result can be understood from the indentation characteristics with a hot and sharp indenter tip. The latter gives rise to a deformation mode in the fully plastic regime, enabling a simple interpretation of the results. The softening transition and the yield stress of the system on a microsecond time scale and a nanometer size scale were obtained. We show that the plastic deformation is governed by yielding in the polystyrene sublayer, which renders the overall system soft for plastic deformation. The ultrathin protection layer contributes as an elastic skin, which shields part of the temperature and pressure and enables the high wear resistance against lateral forces. Moreover, the method of probing polymers at microsecond and nanometer size scales opens up new opportunities for studying polymer physics in a largely unexplored regime. Thus, we find softening temperatures of more than 100 °C above the polystyrene glass transition, which implies that for the short interaction time scales the glassy state of the polymer is preserved up to this temperature.

  6. Effect of radiation cross-linking on the abrasive wear behaviour of polyethylenes

    NASA Astrophysics Data System (ADS)

    Gul, Rizwan M.; Khan, Tahir I.

    2014-06-01

    This study explores the differences in the dry abrasive wear behavior of different polyethylenes, and compares the effect of radiation cross-linking on the wear behavior. Four different types of polyethylenes: LDPE, LLDPE, HDPE and UHMWPE were studied. Cross-linking was carried out by high energy electron beam with radiation dose of 200 kGy. The results show that in unirradiated state UHMWPE has excellent wear resistance, with HDPE showing comparable wear properties; both LDPE and LLDPE exhibit high wear rate. Cross-linking improves wear rate of LDPE and UHMWPE, however, the wear rate of HDPE and LLDPE increases with cross-linking.

  7. Long-wearing TFE/metal bearings

    NASA Technical Reports Server (NTRS)

    Brass, R. A.; Gillon, W. A., Jr.

    1980-01-01

    Method for making metal/polytetrafluoroethylene (TFE) bearing surfaces embeds long-wearing layer of TFE in microscopic pits in metal. Technique has potential applications in automotive gears, ball joints, and roller chain components. Other applications are in use of unlubricated bearings in chemical, pharmaceutical, and food-processing equipment.

  8. Long-wearing TFE/metal bearings

    NASA Technical Reports Server (NTRS)

    Brass, R. A.; Gillon, W. A., Jr.

    1980-01-01

    Method for making metal/polytetrafluoroethylene (TFE) bearing surfaces embeds long-wearing layer of TFE in microscopic pits in metal. Technique has potential applications in automotive gears, ball joints, and roller chain components. Other applications are in use of unlubricated bearings in chemical, pharmaceutical, and food-processing equipment.

  9. Wear Resistant Amorphous and Nanocomposite Steel Coatings

    SciTech Connect

    Branagan, Daniel James; Swank, William David; Haggard, Delon C; Fincke, James Russell; Sordelet, D.

    2001-10-01

    In this article, amorphous and nanocomposite thermally deposited steel coatings have been formed by using both plasma and high-velocity oxy-fuel (HVOF) spraying techniques. This was accomplished by developing a specialized iron-based composition with a low critical cooling rate (?104 K/s) for metallic glass formation, processing the alloy by inert gas atomization to form micron-sized amorphous spherical powders, and then spraying the classified powder to form coatings. A primarily amorphous structure was formed in the as-sprayed coatings, independent of coating thickness. After a heat treatment above the crystallization temperature (568°C), the structure of the coatings self-assembled (i.e., devitrified) into a multiphase nanocomposite microstructure with 75 to 125 nm grains containing a distribution of 20 nm second-phase grain-boundary precipitates. Vickers microhardness testing revealed that the amorphous coatings were very hard (10.2 to 10.7 GPa), with further increases in hardness after devitrification (11.4 to 12.8 GPa). The wear characteristics of the amorphous and nanocomposite coatings were determined using both two-body pin-on-disk and three-body rubber wheel wet-slurry sand tests. The results indicate that the amorphous and nanocomposite steel coatings are candidates for a wide variety of wear-resistant applications.

  10. 7-Be Implantation in Plastics for Prosthesis Wear Studies

    NASA Astrophysics Data System (ADS)

    Greife, Uwe; Erikson, L.; Patel, N.; Wimmer, M.; Dwiwedi, Y.; Laurent, M.; Chipps, K.; Blackmon, J.; Kozub, R.; Bardayan, D.; Gross, C.; Stracener, D.; Smith, M.; Nesaraya, C.; Rehm, E.; Ahmed, I.; Greene, J.

    2010-11-01

    The current generation of highly cross linked ultrahigh molecular weight polyethylenes (PE) for hip and knee joint replacement have achieved such low in vitro wear rates that efforts have been underway to develop more sensitive methods to measure polyethylene wear. The most widely used technique, the gravimetric method, suffers from the notable disadvantage that mass gain by fluid absorption can considerably exceed mass loss by wear, making the wear measurement inaccurate, sometimes even leading to negative ``wear'' values. The purpose of this experiment was to investigate the use of a radioactive tracer, beryllium-7 (7-Be), to circumvent the problem of fluid absorption and thereby achieve a much more sensitive and accurate wear measurement. This proof of principle study demonstrated the general feasibility of 7-Be implantation (performed at the Holifield Radioactive Ion Beam Facility of Oak Ridge National Laboratory) for PE wear analysis.

  11. Structures and Properties of Polymers Important to Their Wear Behavior

    NASA Technical Reports Server (NTRS)

    Tanaka, K.

    1984-01-01

    The wear and transfer of various semicrystalline polymers sliding against smooth steel or glass surfaces were examined. The effects of structures, and properties of polymers on their wear behavior are discussed. It is found that the high wear characteristics of PTFE is due to the easy destruction of the banded structure of PTFE. The size of spherulites and the molecular profile are closely related to the magnitude of wear rates of typical semicrystalline polymers. The effects of these factors on the wear rate on the basis of the destruction or melting of spherulites at the frictional surface are discussed. Although the fatigue theory of wear indicates that some mechanical properties are important to wear behavior, it is shown that the theory does not always explain the experimental result obtained on a smooth surface.

  12. Submicron sized ultra-high molecular weight polyethylene wear particle analysis from revised SB Charité III total disc replacements.

    PubMed

    Punt, Ilona; Baxter, Ryan; van Ooij, André; Willems, Paul; van Rhijn, Lodewijk; Kurtz, Steven; Steinbeck, Marla

    2011-09-01

    Submicron sized particles are frequently observed in retrieved total hip and knee periprosthetic tissues and appear to be critical in the activation of the phagocytic inflammatory response. In this paper the concentration, size and shape of ultra-high molecular weight polyethylene (UHMWPE) wear particles between 0.05 and 2.00μm were determined after isolation from periprosthetic tissues from retrieved lumbar SB Charité III total disc replacements (TDR) using scanning electron microscopy (SEM). For comparison, UHMWPE wear particles were isolated from γ-radiation-air sterilized total hip arthroplasty (THA) revision tissues. The mean concentration of UHMWPE particles in TDR tissues was 1.6×10(9)g(-1)tissue (range 1.3-2.0), which was significantly lower than the concentration of 2.3×10(9)g(-1) THA revision tissue (range 1.8-3.2) (P=0.03). The mean particle size (equivalent circular diameter: TDR, 0.46μm; THA 0.53μm, P=0.60) and mean shape were comparable between TDR and THA (aspect ratio: TDR, 1.89; THA, 1.99, P=0.35; roundness: TDR, 0.58; THA, 0.56, P=0.35). However, the TDR particles tended to be smaller and more round. Although no correlations were found between visible damage to the UHMWPE core and the concentration or shape of the UHMWPE particles, a positive correlation was found between increasing particle size and increasing rim penetration of the TDR core (P=0.04). The presence of UHMWPE particles of similar size and shape in TDR tissue, albeit lower in concentration, might explain why, unlike THA, pain rather than osteolysis is the major reason for revision surgery. Copyright © 2011 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

  13. A hip joint simulator study using simplified loading and motion cycles generating physiological wear paths and rates.

    PubMed

    Barbour, P S; Stone, M H; Fisher, J

    1999-01-01

    In some designs of hip joint simulator the cost of building a highly complex machine has been offset with the requirement for a large number of test stations. The application of the wear results generated by these machines depends on their ability to reproduce physiological wear rates and processes. In this study a hip joint simulator has been shown to reproduce physiological wear using only one load vector and two degrees of motion with simplified input cycles. The actual path of points on the femoral head relative to the acetabular cup were calculated and compared for physiological and simplified input cycles. The in vitro wear rates were found to be highly dependent on the shape of these paths and similarities could be drawn between the shape of the physiological paths and the simplified elliptical paths.

  14. Anti-oxidation treatment of ultra high molecular weight polyethylene components to decrease periprosthetic osteolysis: evaluation of osteolytic and osteogenic properties of wear debris particles in a murine calvaria model.

    PubMed

    Green, Justin M; Hallab, Nadim J; Liao, Yen-Shuo; Narayan, Venkat; Schwarz, Edward M; Xie, Chao

    2013-05-01

    Wear debris-induced osteolysis remains the greatest limitation of long-term success for total joint replacements with ultra-high molecular weight polyethylene (UHMWPE) bearings. To address oxidative degradation post-gamma irradiation, manufacturers are investigating the incorporation of antioxidants into PE resins. Similarly, larger molecular weight monomers have been developed to increase crosslinking and decrease wear debris, and ultimately osteolysis. However, the effects of modifying monomer size, crosslink density, and antioxidant incorporation on UHMWPE particle-induced osteoclastic bone resorption and coupled osteoblastic bone formation have never been tested. Here, we review the field of antioxidant-containing UHMWPE, and present an illustrative pilot study evaluating the osteolytic and osteogenic potential of wear debris generated from three chemically distinct particles (MARATHON®, XLK, and AOX™) as determined by a novel 3D micro-CT algorithm designed for the murine calvaria model. The results demonstrate an approach by which the potential osteoprotective effects of antioxidants in UHMWPE can be evaluated.

  15. Nuclear fuel assembly wear sleeve

    SciTech Connect

    Cadwell, D.J.; Kmonk, S.

    1983-03-08

    An improved control rod guide tube for use in a fuel assembly in a nuclear reactor. The guide tube extends the complete length of the fuel assembly and has its upper end fastened in a cylindrical housing by swaging the guide tube material into grooves formed in the housing walls. To eliminate wear on the guide tube inner walls caused by hydraulic induced vibratory forces on a control rod adapted to move therein, a thin-walled chrome plated sleeve is threaded into the top end of the guide thimble and extends downwardly a distance sufficient to be engaged by the control rod during reactor operation. The sleeve serves as a highly resistant wear surface between the control rod and walls on the guide tube in the fuel assembly.

  16. Microstructure-Wear Resistance Correlation and Wear Mechanisms of Spark Plasma Sintered Cu-Pb Nanocomposites

    NASA Astrophysics Data System (ADS)

    Sharma, Amit Siddharth; Biswas, Krishanu; Basu, Bikramjit

    2014-01-01

    The dispersion of a softer phase in a metallic matrix reduces the coefficient of friction (COF), often at the expense of an increased wear rate at the tribological contact. To address this issue, unlubricated fretting wear tests were performed on spark plasma sintered Cu-Pb nanocomposites against bearing steel. The sintering temperature and the Pb content as well as the fretting parameters were judiciously selected and varied to investigate the role of microstructure (grain size, second-phase content) on the wear resistance properties of Cu-Pb nanocomposites. A combination of the lowest wear rate (~1.5 × 10-6 mm3/Nm) and a modest COF (~0.4) was achieved for Cu-15 wt pct Pb nanocomposites. The lower wear rate of Cu-Pb nanocomposites with respect to unreinforced Cu is attributed to high hardness (~2 to 3.5 GPa) of the matrix, Cu2O/Fe2O3-rich oxide layer formation at tribological interface, and exuding of softer Pb particles. The wear properties are discussed in reference to the characteristics of transfer layer on worn surface as well as subsurface damage probed using focused ion beam microscopy. Interestingly, the flash temperature has been found to have insignificant effect on the observed oxidative wear, and alternative mechanisms are proposed. Importantly, the wear resistance properties of the nanocomposites reveal a weak Hall-Petch-like relationship with grain size of nanocrystalline Cu.

  17. Internal corrosion in dental composite wear.

    PubMed

    Sarkar, N K

    2000-01-01

    The internal corrosion of dental resin composites is associated with water-sorption and leads to (1) interfacial debonding, (2) filler dissolution, (3) matrix cracking, and (4) subsurface damage. The last factor creates a condition for "corrosive-wear" in which the damaged layer is worn with ease exposing a new surface and perpetuating the cycle of corrosion and wear. Central to the simulation of in vivo corrosive-wear is the recreation of the subsurface damage layer. To produce this layer in water, artificial saliva, and in media of low pH is time-consuming, because the degradation process in these environments is extremely slow. In laboratory wear tests using aqueous environments, the contact time of resin composites with water is too short to cause significant internal degradation. Thus, data obtained from such tests represent abrasive and not corrosive-wear, and do not correlate well with in vivo wear data. In considering this limitation of the above media for accelerated wear tests, an alkaline medium has been used in this study to simulate corrosive-wear of eleven commercial composites. The procedure consists of exposing each material to 0.1 N NaOH at 60 degrees C for 2 weeks followed by abrasion in a tooth brushing machine. The medium choice is based on the rationale that in vivo degradation arises from reaction with the OH(-), and this reaction can be enhanced by raising the pH and the temperature of the medium. The warm NaOH solution satisfies both these conditions. Parameters examined to evaluate the resistance of each composite to corrosion and wear were (1) mass loss, (2) Si-loss, (3) degradation depth, and (4) wear depth, respectively. A highly significant correlation has been observed among various corrosion and wear parameters. SEM examination indicated degradation to be associated with interfacial separation, filler dissolution, matrix cracking, and subsurface damage. These features are characteristics of in vivo worn composite restorations. Time is

  18. What Not to Wear and Other Stories: Addressing Religious Diversity in Schools

    ERIC Educational Resources Information Center

    Blair, Ann; Aps, Will

    2005-01-01

    This article considers the position of religion in schools in England and Wales in light of the recent decision in "The Queen on the application of SB v Headteacher and Governors of Denbigh High School". This held that the refusal to allow a pupil to wear the jilbab was a breach of her rights under the European Convention for the…

  19. What Not to Wear and Other Stories: Addressing Religious Diversity in Schools

    ERIC Educational Resources Information Center

    Blair, Ann; Aps, Will

    2005-01-01

    This article considers the position of religion in schools in England and Wales in light of the recent decision in "The Queen on the application of SB v Headteacher and Governors of Denbigh High School". This held that the refusal to allow a pupil to wear the jilbab was a breach of her rights under the European Convention for the…

  20. Corneal epithelial permeability during extended wear of disposable contact lenses versus daily wear of soft contact lenses.

    PubMed Central

    Schurmans, L R; Boets, E P; van Best, J A

    1995-01-01

    AIMS--The corneal epithelial permeability during extended wear of disposable contact lenses was compared with that during daily wear of soft contact lenses. The study was performed to verify whether the extended wear of disposable contact lenses would result in a higher permeability value than the daily wear of soft contact lenses. A higher permeability makes the cornea more vulnerable for bacterial infections and thus could explain the higher incidence of bacterial keratitis found in extended wear of disposable contact lenses in comparison with the daily wear of soft contact lenses. METHOD--The corneal epithelial permeability was determined by fluorophotometry in 33 healthy volunteers after the wear of soft, daily wear contact lenses for at least 6 months. Thereafter the determination was repeated in each volunteer after extended wear of disposable contact lenses for 1 month. The permeability in 34 healthy non-contact lens wearing volunteers was determined as a control. The permeability value was calculated from the amount of fluorescein that passed into the cornea after application by means of an eyebath. RESULTS--The mean permeability values after daily and extended wear were 0.032 nm/s and 0.031 nm/s, respectively. The values were not significantly different (Wilcoxon paired test p > 0.5). The mean permeability for the non-contact lens wearing controls was 0.042 nm/s. CONCLUSION--The results do not sustain the explanation that a difference in permeability value is the main cause of the increased incidence of keratitis during extended wear of disposable contact lenses in comparison with daily wear. PMID:7742282

  1. Study on the applicability of a precise, accurate method for rapid evaluation of engine and lubricant performance. [determination of wear metal in used lubricating oils

    NASA Technical Reports Server (NTRS)

    Kinard, J. T.

    1975-01-01

    The development of a procedure for obtaining data related to wear metal determinations in used lubricants is discussed. The procedure makes it possible to obtain rapid, simultaneous determinations of a number of wear metals at levels of parts per thousand to low parts per billion using a small amount of sample. The electrode assembly and instrumentation used in the process are described. Samples of data obtained from tests conducted under controlled conditions are tabulated.

  2. Tempering-Induced Microstructural Changes in the Weld Heat-Affected Zone of 9 to 12 Pct Cr Steels and Their Influence on Sliding Wear

    NASA Astrophysics Data System (ADS)

    Velkavrh, Igor; Kafexhiu, Fevzi; Klien, Stefan; Diem, Alexander; Podgornik, Bojan

    2017-01-01

    Increasing amount of tribological applications is working under alternating high/low temperature conditions where the material is subjected to temperature fatigue mechanisms such as creep, softening due to annealing, and at the same time must withstand mechanical wear due to sliding contact with pairing bodies. Steam turbine valves, gate valves, valve heads, stems, seats and bushings, and contacting surfaces of the carrier elements are some examples of such applications. The purpose of the present study is to evaluate the potential of X20 and P91 steels as materials for applications operating under combined effect of mechanical wear and alternating high/low temperature conditions. It was focused on how the microstructural changes occurring in the weld zone affect the wear properties of the selected materials. Generally, with longer tempering time and higher tempering temperature, the number of carbide precipitates decreased, while their relative spacing increased. Before tempering, the morphology of the steel matrix (grain size, microstructure homogeneity) governed the wear resistance of both steels, while after tempering wear response was determined by the combination of the number and the size of carbide particles. After tempering, in X20 steel larger number of stable M23C6 carbides was observed as compared with P91 steel, resulting in lower wear rates. It was observed that for both steels, a similar combination of number density and size distribution of carbide particles provided the highest wear resistance.

  3. Are there biological markers of wear?

    PubMed

    Bauer, Thomas W; Shanbhag, Arun S

    2008-01-01

    Potential systemic markers of implant wear include products of the wear process (particles and ions) and mediators of the inflammatory reaction that can be induced by wear. Ions from polymers used in arthroplasty are not specific, but high metal ion levels may help identify patients with unexpectedly high wear of metal-on-metal implants. The kinetics of ion production, transport, and excretion are complex, however, so it is currently difficult to interpret the significance of mild elevations in metal ions. Indices of bone turnover (eg, collagen fragments) and mediators involved in the inflammatory reaction to particles (eg, osteoprotegerin, RANKL, interleukins) may be associated with osteolysis, but systemic disorders (eg, osteoarthritis) and the use of medications that influence bone remodeling limit the predictive value of these analytes with respect to the consequences of implant wear. Using genomic and proteomic methods to measure multiple analytes offers promise, but the challenge is to identify markers specifically associated with wear that are not elevated by other conditions that often coexist in this patient population.

  4. Hardfacing of high temperature alloys for ethylene pyrolysis applications

    SciTech Connect

    Agosta, P.; Levesque, C.; Kurlekar, A.

    1994-12-31

    Materials of construction in an ethylene pyrolysis furnace must withstand severe conditions including high temperatures, alternating oxidizing and carburizing atmospheres, impinging coke particles, and thermal cycling. The creep, high temperature corrosion, and erosion which are experienced by furnace components can be resisted by proper materials selection. Positioned directly in the process stream, thermowells are used to monitor process temperatures. Thermowell materials of construction must be selected with the extreme process conditions in mind. As always, safety is an underlying factor. Given the highly flammable ethylene stream, thermowell failures must be prevented at any cost. No single material was found to resist both creep and erosion under existing operating conditions. However, the combination of a creep resistant base material with a wear resistant coating was found to not only prevent failures, but also greatly extend thermowell life, reducing downtime and maintenance costs. Laboratory research and actual operations data have shown a nickel based superalloy with a ceramic hardfacing to be highly cost effective in thermowell applications in resisting the combination of creep and erosion found in ethylene pyrolysis applications.

  5. Ceramic-like wear behaviour of human dental enamel.

    PubMed

    Arsecularatne, J A; Hoffman, M

    2012-04-01

    This paper reports a transmission electron microscopy (TEM) analysis of subsurfaces of enamel specimens following in vitro reciprocating wear tests with an enamel cusp sliding on a flat enamel specimen under hydrated conditions. The obtained results show that crack formation occurred in the wear scar subsurface. The path followed by these cracks seems to be dictated either by the histological structure of enamel or by the contact stress field. Moreover, the analysis of a set of enamel wear results obtained from the literature and application of fracture-based models, originally developed for ceramics, correlate well, confirming the similar wear processes taking place in these materials. This analysis also reveals a marked influence of coefficient of friction on the enamel wear rate: for a higher coefficient of friction value, enamel wear can be severe even under forces generated during normal operation of teeth.

  6. IMPROVEMENT OF WEAR COMPONENT'S PERFORMANCE BY UTILIZING ADVANCED MATERIALS AND NEW MANUFACTURING TECHNOLOGIES: CASTCON PROCESS FOR MINING APPLICATIONS

    SciTech Connect

    Xiaodi Huang; Richard Gertsch

    2001-10-30

    The fibrous monolith material was successfully consolidated in both the hot press and the hot isostatic press. Initial evaluations indicate the material will have a very high fracture toughness and be very hard. Tungsten carbide was successfully consolidated in an H13 tool steel with the incorporation of a Co-Cr layer between the WC and the steel.

  7. Dynamic surface microstructural changes during tribological contact that determine the wear behaviour of hip prostheses: metals and ceramics.

    PubMed

    Rainforth, W Mark; Zeng, Peng; Ma, Le; Valdez, Akemi Nogiwa; Stewart, Todd

    2012-01-01

    It is often the dynamic microstructural changes induced by tribological contact that determine whether or not a material exhibits good wear resistance. It is well known that the mechanical properties of a surface are significantly different from the bulk, an effect amplified by wear induced plastic deformation and electrochemical effects. Despite the importance of these dynamic microstructural changes, there remains little quantitative understanding of how the surface microstructure changes during tribo-contact, and how this modifies the surface mechanical properties and chemical activity. This contribution will focus on key total hip arthroplasty materials, specifically CoCrMo alloys, third and fourth generation alumina/zirconia toughened alumina. High resolution techniques have been used to characterise the wear induced microstructural changes for both in vivo and in vitro samples, which has provided new insight into the wear mechanisms. The results are discussed in detail, in particular, how they inform future materials development for this important application.

  8. Development of Advanced Surface Enhancement Technology for Decreasing Wear and Corrosion of Equipment Used for Mineral Processing

    SciTech Connect

    Daniel Tao; Craig A. Blue

    2004-08-01

    Equipment wear is a major concern in the mineral processing industry, which dramatically increases the maintenance cost and adversely affects plant operation efficiency. In this research, wear problems of mineral processing equipment including screens, sieve bends, heavy media vessel, dewatering centrifuge, etc., were identified. A novel surface treatment technology, high density infrared (HDI) surface coating process was proposed for the surface enhancement of selected mineral processing equipment. Microstructural and mechanical properties of the coated samples were characterized. Laboratory-simulated wear tests were conducted to evaluate the tribological performance of the coated components. Test results indicate that the wear resistance of AISI 4140 and ASTM A36 steels can be increased 3 and 5 folds, respectively by the application of HDI coatings.

  9. Morphology of powders of tungsten carbide used in wear-resistant coatings and deposition on the PDC drill bits

    NASA Astrophysics Data System (ADS)

    Zakharova, E. S.; Markova, I. Yu; Maslov, A. L.; Polushin, N. I.; Laptev, A. I.

    2017-05-01

    Modern drill bits have high abrasive wear in the area of contact with the rock and removed sludge. Currently, these bits have a protective layer on the bit body, which consists of a metal matrix with inclusions of carbide particles. The research matrix of this coating and the wear-resistant particles is a prerequisite in the design and production of drill bits. In this work, complex investigation was made for various carbide powders of the grades Relit (tungsten carbide produced by Ltd “ROSNAMIS”) which are used as wear-resistant particles in the coating of the drill bit body. The morphology and phase composition of the chosen powders as well as the influence of a particle shape on prospects of their application in wear-resistance coating presented in this work.

  10. Wear Behaviour of Pressible Lithium Disilicate Glass Ceramic

    PubMed Central

    Peng, Zhongxiao; Rahman, Muhammad Izzat Abdul; Zhang, Yu; Yin, Ling

    2015-01-01

    This paper reports effects of surface preparation and contact loads on abrasive wear properties of highly aesthetic and high-strength pressible lithium disilicate glass-ceramics (LDGC). Abrasive wear testing was performed using a pin-on-disk device in which LDGC disks prepared with different surface finishes were against alumina pins at different contact loads. Coefficients of friction and wear volumes were measured as functions of initial surface finishes and contact loads. Wear-induced surface morphology changes in both LDGC disks and alumina pins were characterized using 3D laser scanning microscopy, scanning electron microscopy and energy dispersive x-ray spectroscopy. The results show that initial surface finishes of LDGC specimens and contact loads significantly affected the friction coefficients, wear volumes and wear-induced surface roughness changes of the material. Both wear volumes and friction coefficients of LDGC increased as the load increased while surface roughness effects were complicated. For rough LDGC surfaces, three-body wear was dominant while for fine LDGC surfaces, two-body abrasive wear played a key role. Delamination, plastic deformation and brittle fracture were observed on worn LDGC surfaces. The adhesion of LDGC matrix materials to alumina pins was also discovered. This research has advanced our understanding of the abrasive wear behaviour of LDGC and will provide guidelines for better utilisation and preparation of the material for long-term success in dental restorations. PMID:25980530

  11. Wear behavior of pressable lithium disilicate glass ceramic.

    PubMed

    Peng, Zhongxiao; Izzat Abdul Rahman, Muhammad; Zhang, Yu; Yin, Ling

    2016-07-01

    This article reports effects of surface preparation and contact loads on abrasive wear properties of highly aesthetic and high-strength pressable lithium disilicate glass-ceramics (LDGC). Abrasive wear testing was performed using a pin-on-disk device in which LDGC disks prepared with different surface finishes were against alumina pins at different contact loads. Coefficients of friction and wear volumes were measured as functions of initial surface finishes and contact loads. Wear-induced surface morphology changes in both LDGC disks and alumina pins were characterized using three-dimensional laser scanning microscopy, scanning electron microscopy, and energy dispersive X-ray spectroscopy. The results show that initial surface finishes of LDGC specimens and contact loads significantly affected the friction coefficients, wear volumes and wear-induced surface roughness changes of the material. Both wear volumes and friction coefficients of LDGC increased as the load increased while surface roughness effects were complicated. For rough LDGC surfaces, three-body wear was dominant while for fine LDGC surfaces, two-body abrasive wear played a key role. Delamination, plastic deformation, and brittle fracture were observed on worn LDGC surfaces. The adhesion of LDGC matrix materials to alumina pins was also discovered. This research has advanced our understanding of the abrasive wear behavior of LDGC and will provide guidelines for better utilization and preparation of the material for long-term success in dental restorations. © 2015 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 104B: 968-978, 2016.

  12. Identification of Tool Wear when Machining of Austenitic Steels and Titatium by Miniature Machining

    NASA Astrophysics Data System (ADS)

    Pilc, Jozef; Kameník, Roman; Varga, Daniel; Martinček, Juraj; Sadilek, Marek

    2016-12-01

    Application of miniature machining is currently rapidly increasing mainly in biomedical industry and machining of hard-to-machine materials. Machinability of materials with increased level of toughness depends on factors that are important in the final state of surface integrity. Because of this, it is necessary to achieve high precision (varying in microns) in miniature machining. If we want to guarantee machining high precision, it is necessary to analyse tool wear intensity in direct interaction with given machined materials. During long-term cutting process, different cutting wedge deformations occur, leading in most cases to a rapid wear and destruction of the cutting wedge. This article deal with experimental monitoring of tool wear intensity during miniature machining.

  13. Gender Differences in Wear Rates for 28 versus 32 millimeter Ceramic Femoral Heads on Modern Highly Cross-linked Polyethylene at Midterm Follow-up in Young Patients Undergoing Total Hip Arthroplasty

    PubMed Central

    Stambough, Jeffrey B.; Pashos, Gail; Wu, Ningying; Haynes, Jacob A; Martell, John M.; Clohisy, John C.

    2016-01-01

    Background We report on the midterm linear and volumetric wear of highly cross-linked polyethylene (HXLPE) and survivorship of two prospective young THA cohorts that differed by the size of ceramic femoral head used: 28 vs. 32 millimeters. Methods We prospectively analyzed 220 consecutive primary THAs in patients ≤50 years who received a cementless THA with a ceramic femoral head on HXLPE liner (C-HXLPE). There were 101 patients (46%) with 28mm heads and 119 patients (54%) who received 32mm heads at a mean follow-up of 5.5 years (range 60–109 months). Wear was calculated using Martell Software. Results The 28mm C-HXLPE cohort demonstrated average linear and volumetric wear of 0.020 mm/year (SD 0.074, 95% CI [0.003, 0.037]) and 18.775 mm3/yr (SD 21.743, 95% CI [13.773, 23.778]) compared to 0.032 mm/yr (SD 0.087, 95% CI [0.013, 0.050]) and 29.847 mm3/yr (SD 35.441, 95% CI [22.294, 37.401]) in the 32mm C-HXLPE group. Subgroup analysis by gender and head size discovered significantly greater wear in females with 32mm compared to 28mm heads in both linear (0.01, 95% CI [−0.014, 0.033] vs. 0.048, 95% CI [0.022, 0.074] mm/y, p=0.004) and volumetric wear (14.11, 95% CI [8.957, 19.271] vs. 29.71, 95% CI [17.584, 41.840] mm3/yr, p=0.009). We found a 96% (95% CI [92.30%, 97.94%]) survivorship by Kaplan-Meier analysis at minimum 5-years with no failures due to osteolysis. Conclusions Ceramic-on-HXLPE demonstrates extremely low wear properties in young patients at midterm follow-up. We identified a gender-dependent difference in wear based on head size, with 32mm heads being associated with increased wear in females. PMID:26631286

  14. Optical wear monitoring

    SciTech Connect

    Kidane, Getnet S; Desilva, Upul P.; He, Chengli; Ulerich, Nancy H.

    2016-07-26

    A gas turbine includes first and second parts having outer surfaces located adjacent to each other to create an interface where wear occurs. A wear probe is provided for monitoring wear of the outer surface of the first part, and includes an optical guide having first and second ends, wherein the first end is configured to be located flush with the outer surface of the first part. A fiber bundle includes first and second ends, the first end being located proximate to the second end of the optical guide. The fiber bundle includes a transmit fiber bundle comprising a first plurality of optical fibers coupled to a light source, and a receive fiber bundle coupled to a light detector and configured to detect reflected light. A processor is configured to determine a length of the optical guide based on the detected reflected light.

  15. Wear behavior of austenite containing plate steels

    NASA Astrophysics Data System (ADS)

    Hensley, Christina E.

    As a follow up to Wolfram's Master of Science thesis, samples from the prior work were further investigated. Samples from four steel alloys were selected for investigation, namely AR400F, 9260, Hadfield, and 301 Stainless steels. AR400F is martensitic while the Hadfield and 301 stainless steels are austenitic. The 9260 exhibited a variety of hardness levels and retained austenite contents, achieved by heat treatments, including quench and tempering (Q&T) and quench and partitioning (Q&P). Samples worn by three wear tests, namely Dry Sand/Rubber Wheel (DSRW), impeller tumbler impact abrasion, and Bond abrasion, were examined by optical profilometry. The wear behaviors observed in topography maps were compared to the same in scanning electron microscopy micrographs and both were used to characterize the wear surfaces. Optical profilometry showed that the scratching abrasion present on the wear surface transitioned to gouging abrasion as impact conditions increased (i.e. from DSRW to impeller to Bond abrasion). Optical profilometry roughness measurements were also compared to sample hardness as well as normalized volume loss (NVL) results for each of the three wear tests. The steels displayed a relationship between roughness measurements and observed wear rates for all three categories of wear testing. Nanoindentation was used to investigate local hardness changes adjacent to the wear surface. DSRW samples generally did not exhibit significant work hardening. The austenitic materials exhibited significant hardening under the high impact conditions of the Bond abrasion wear test. Hardening in the Q&P materials was less pronounced. The Q&T microstructures also demonstrated some hardening. Scratch testing was performed on samples at three different loads, as a more systematic approach to determining the scratching abrasion behavior. Wear rates and scratch hardness were calculated from scratch testing results. Certain similarities between wear behavior in scratch testing

  16. IMPROVEMENT OF WEAR COMPONENT'S PERFORMANCE BY UTILIZING ADVANCED MATERIALS AND NEW MANUFACTURING TECHNOLOGIES: CASTCON PROCESS FOR MINING APPLICATIONS

    SciTech Connect

    Xiaodi Huang; Richard Gertsch

    2004-03-22

    During this reporting period, the debinding and off-gassing furnace was switched from a vacuum furnace to a conventional kiln to solve the HIP can expansion problem during high temperature off-gassing, which caused disc distortion. Two 6.5 inch discs were produced. Both looked acceptable and one was machined. It was found that the disc hub section was little bit thin and micro cracks were seen along the disc radial directions.

  17. Casing wear caused by tooljoint hardfacing

    SciTech Connect

    Best, B.

    1986-02-01

    Casing wear caused by new tooljoint hardfacings, such as fine-mesh tungsten-carbide hardfacing and a hardfacing covered with a layer of relatively soft material, has been investigated in the laboratory. The tests were performed on a full-scale test facility with field conditions-forces, motions, and fluids-simulated as closely as possible. It was found that the major mechanisms responsible for casing wear by tooljoints are adhesive wear, abrasive wear, and ploughing. Wear mechanisms can be classified as mild, normal, and severe. A thorough understanding of these mechanisms could lead to measures for lessening casing wear. This can be achieved with (1) tooljoints that have a sufficiently large, smooth, round, and uniform surface and (2) an appropriate mud that has a sufficiently high content of soft solid particles, such as barites, to form a layer in the tooljoint/casing contact area so that metal-to-metal contact is avoided and small, hard mud particles are embedded.

  18. Drill wear monitoring in cortical bone drilling.

    PubMed

    Staroveski, Tomislav; Brezak, Danko; Udiljak, Toma

    2015-06-01

    Medical drills are subject to intensive wear due to mechanical factors which occur during the bone drilling process, and potential thermal and chemical factors related to the sterilisation process. Intensive wear increases friction between the drill and the surrounding bone tissue, resulting in higher drilling temperatures and cutting forces. Therefore, the goal of this experimental research was to develop a drill wear classification model based on multi-sensor approach and artificial neural network algorithm. A required set of tool wear features were extracted from the following three types of signals: cutting forces, servomotor drive currents and acoustic emission. Their capacity to classify precisely one of three predefined drill wear levels has been established using a pattern recognition type of the Radial Basis Function Neural Network algorithm. Experiments were performed on a custom-made test bed system using fresh bovine bones and standard medical drills. Results have shown high classification success rate, together with the model robustness and insensitivity to variations of bone mechanical properties. Features extracted from acoustic emission and servomotor drive signals achieved the highest precision in drill wear level classification (92.8%), thus indicating their potential in the design of a new type of medical drilling machine with process monitoring capabilities. Copyright © 2015 IPEM. Published by Elsevier Ltd. All rights reserved.

  19. Nanotribological investigations of materials, coatings and lubricants for nanotechnology applications at high sliding velocities

    NASA Astrophysics Data System (ADS)

    Tambe, Nikhil S.

    The advent of micro/nanostructures and the subsequent miniaturization of moving components for various nanotechnology applications, such as micro/nanoelectromechanical systems (MEMS/NEMS), have ascribed paramount importance to the tribology and mechanics on the nanoscale. Most of these micro/nanodevices and components operate at very high sliding velocities (of the order of tens of mm/s to few m/s). Atomic force microscopy (AFM) studies to investigate potential materials, coatings and lubricants for these devices have been rendered inadequate due to the inherent limitations on the highest sliding velocities achievable with commercial AFMs (<250 mum/s). The development of a new AFM based technique, done as part of this research work, has allowed nanotribological investigations over a wide range of velocities (up to 10 mm/s). The impacts of this research on the design and development of nanotechnology applications are profound. Research conducted on various materials, coatings and lubricants reveals a strong velocity dependence of friction, adhesion and wear on the nanoscale. Based on the experimental evidence, theoretical formulations have been conducted for nanoscale friction behavior to design a comprehensive analytical model that explains the velocity dependence. The model takes into consideration the contributions of adhesion at the tip-sample interface, high impact velocity related deformations at the contacting asperities and atomic scale stick-slip. Dominant friction mechanisms are identified and the critical operating parameters corresponding to their transitions are defined. Wear studies are conducted at high sliding velocities for materials, coatings and lubricants to understand the primary failure mechanisms. A novel AFM based nanowear mapping technique is developed to map wear on the nanoscale and the interdependence of normal load and sliding velocity on sample surface wear is studied. This technique helps identify and classify wear mechanisms and

  20. Low Temperature Unbalanced Magnetron Deposition of Hard, Wear-Resistant Coatings for Liquid-Film Bearing Applications

    NASA Technical Reports Server (NTRS)

    Sproul, William D.

    1996-01-01

    The original program for evaluating the tribological properties several different hard coatings for liquid film bearing applications was curtailed when the time for the program was reduced from 3 years to 1. Of the several different coatings originally planned for evaluation, we decided to concentrate on one coating, carbon nitride. At BIRL, we have been instrumental in the development of reactively sputtered carbon nitride coatings, and we have found that it is a very interesting new material with very good tribological properties. In this program, we found that the reactively sputtered carbon nitride does not bond well directly to hardened 440C stainless steel; but if an interlayer of titanium nitride is added between the carbon nitride and the 440C, the adhesion of the dual coating combination is very good. Statistically designed experiments were run with the dual layer combination, and 3 variables were chosen for the Box-Benken design, which were the titanium nitride interlayer thickness, the nitrogen partial pressure during the reactive sputtering of the carbon nitride, and the carbon nitride substrate bias voltage. Two responses were studied from these three variables; the adhesion of the dual coating combination to the 440C substrate and the friction coefficient of the carbon nitride in dry sliding contact with 52100 steel in air. The best adhesion came with the thickness interlayer thickness studied, which was 4 micrometers, and the lowest coefficient of friction was 0.1, which was achieved when the bias voltage was in the range of -80 to - 120 V and the nitrogen partial pressure was 3 mTorr.

  1. A novel optical apparatus for the study of rolling contact wear/fatigue based on a high-speed camera and multiple-source laser illumination.

    PubMed

    Bodini, I; Sansoni, G; Lancini, M; Pasinetti, S; Docchio, F

    2016-08-01

    Rolling contact wear/fatigue tests on wheel/rail specimens are important to produce wheels and rails of new materials for improved lifetime and performance, which are able to operate in harsh environments and at high rolling speeds. This paper presents a novel non-invasive, all-optical system, based on a high-speed video camera and multiple laser illumination sources, which is able to continuously monitor the dynamics of the specimens used to test wheel and rail materials, in a laboratory test bench. 3D macro-topography and angular position of the specimen are simultaneously performed, together with the acquisition of surface micro-topography, at speeds up to 500 rpm, making use of a fast camera and image processing algorithms. Synthetic indexes for surface micro-topography classification are defined, the 3D macro-topography is measured with a standard uncertainty down to 0.019 mm, and the angular position is measured on a purposely developed analog encoder with a standard uncertainty of 2.9°. The very small camera exposure time enables to obtain blur-free images with excellent definition. The system will be described with the aid of end-cycle specimens, as well as of in-test specimens.

  2. A novel optical apparatus for the study of rolling contact wear/fatigue based on a high-speed camera and multiple-source laser illumination

    NASA Astrophysics Data System (ADS)

    Bodini, I.; Sansoni, G.; Lancini, M.; Pasinetti, S.; Docchio, F.

    2016-08-01

    Rolling contact wear/fatigue tests on wheel/rail specimens are important to produce wheels and rails of new materials for improved lifetime and performance, which are able to operate in harsh environments and at high rolling speeds. This paper presents a novel non-invasive, all-optical system, based on a high-speed video camera and multiple laser illumination sources, which is able to continuously monitor the dynamics of the specimens used to test wheel and rail materials, in a laboratory test bench. 3D macro-topography and angular position of the specimen are simultaneously performed, together with the acquisition of surface micro-topography, at speeds up to 500 rpm, making use of a fast camera and image processing algorithms. Synthetic indexes for surface micro-topography classification are defined, the 3D macro-topography is measured with a standard uncertainty down to 0.019 mm, and the angular position is measured on a purposely developed analog encoder with a standard uncertainty of 2.9°. The very small camera exposure time enables to obtain blur-free images with excellent definition. The system will be described with the aid of end-cycle specimens, as well as of in-test specimens.

  3. Wear and migration of highly cross-linked and conventional cemented polyethylene cups with cobalt chrome or Oxinium femoral heads: a randomized radiostereometric study of 150 patients.

    PubMed

    Kadar, Thomas; Hallan, Geir; Aamodt, Arild; Indrekvam, Kari; Badawy, Mona; Skredderstuen, Arne; Havelin, Leif Ivar; Stokke, Terje; Haugan, Kristin; Espehaug, Birgitte; Furnes, Ove

    2011-08-01

    This randomized study was performed to compare wear and migration of five different cemented total hip joint articulations in 150 patients. The patients received either a Charnley femoral stem with a 22.2 mm head or a Spectron EF femoral stem with a 28 mm head. The Charnley articulated with a γ-sterilized Charnley Ogee acetabular cup. The Spectron EF was used with either EtO-sterilized non-cross-linked polyethylene (Reflection All-Poly) or highly cross-linked (Reflection All-Poly XLPE) cups, combined with either cobalt chrome (CoCr) or Oxinium femoral heads. The patients were followed with repeated RSA measurements for 2 years. After 2 years, the EtO-sterilized non-cross-linked Reflection All-Poly cups had more than four times higher proximal penetration than its highly cross-linked counterpart. Use of Oxinium femoral heads did not affect penetration at 2 years compared to heads made of CoCr. Further follow-up is needed to evaluate the benefits, if any, of Oxinium femoral heads in the clinical setting. The Charnley Ogee was not outperformed by the more recently introduced implants in our study. We conclude that this prostheses still represents a standard against which new implants can be measured. Copyright © 2011 Orthopaedic Research Society.

  4. 3D finite element modeling of sliding wear

    NASA Astrophysics Data System (ADS)

    Buentello Hernandez, Rodolfo G.

    Wear is defined as "the removal of material volume through some mechanical process between two surfaces". There are many mechanical situations that can induce wear and each can involve many wear mechanisms. This research focuses on the mechanical wear due to dry sliding between two surfaces. Currently there is a need to identify and compare materials that would endure sliding wear under severe conditions such as high velocities. The high costs associated with the field experimentation of systems subject to high-speed sliding, has prevented the collection of the necessary data required to fully characterize this phenomena. Simulating wear through Finite Elements (FE) would enable its prediction under different scenarios and would reduce experimentation costs. In the aerospace, automotive and weapon industries such a model can aid in material selection, design and/or testing of systems subjected to wear in bearings, gears, brakes, gun barrels, slippers, locomotive wheels, or even rocket test tracks. The 3D wear model presented in this dissertation allows one to reasonably predict high-speed sliding mechanical wear between two materials. The model predictions are reasonable, when compared against those measured on a sled slipper traveling over the Holloman High Speed Tests Track. This slipper traveled a distance of 5,816 meters in 8.14 seconds and reached a maximum velocity of 1,530 m/s.

  5. Using a surrogate contact pair to evaluate polyethylene wear in prosthetic knee joints.

    PubMed

    Sanders, Anthony P; Lockard, Carly A; Weisenburger, Joel N; Haider, Hani; Raeymaekers, Bart

    2016-01-01

    With recent improvements to the properties of ultra-high molecular weight polyethylene (UHMWPE) used in joint replacements, prosthetic knee and hip longevity may extend beyond two decades. However, it is difficult and costly to replicate such a long in vivo lifetime using clinically relevant in vitro wear testing approaches such as walking gait joint simulators. We advance a wear test intermediate in complexity between pin-on-disk and knee joint simulator tests. The test uses a surrogate contact pair, consisting of a surrogate femoral and tibial specimen that replicate the contact mechanics of any full-scale knee condyle contact pair. The method is implemented in a standard multi-directional pin-on-disk wear test machine, and we demonstrate its application via a two-million-cycle wear test of three different UHMWPE formulations. Further, we demonstrate the use of digital photography and image processing to accurately quantify fatigue damage based on the reduced transmission of light through a damage area in a UHMWPE specimen. The surrogate contact pairs replicate the knee condyle contact areas within -3% to +12%. The gravimetric wear test results reflect the dose of crosslinking radiation applied to the UHMWPE: 35 kGy yielded a wear rate of 7.4 mg/Mcycles, 55 kGy yielded 1.0 mg/Mcycles, and 75 kGy (applied to a 0.1% vitamin E stabilized UHMWPE) yielded 1.5 mg/Mcycles. A precursor to spalling fatigue is observed and precisely measured in the radiation-sterilized (35 kGy) and aged UHMWPE specimen. The presented techniques can be used to evaluate the high-cycle fatigue performance of arbitrary knee condyle contact pairs under design-specific contact stresses, using existing wear test machines. This makes the techniques more economical and well-suited to standardized comparative testing.

  6. Effect of Polyethylene Crosslinking and Bearing Design on Wear of Unicompartmental Arthroplasty.

    PubMed

    Netter, Jonathan; Hermida, Juan C; D'Alessio, Jerry; Kester, Mark; D'Lima, Darryl D

    2015-08-01

    Wear and polyethylene damage continue to be important factors affecting outcomes of unicompartmental knee arthroplasty. We compared two design rationales for unicompartmental arthroplasty: fully congruent mobile bearings; or moderately conforming fixed bearings using experimental and computational wear simulation. Experimental wear rates were 3.89 (±0.12) mg/million cycles for the highly crosslinked Triathlon PKR fixed bearing compared to 18.35 (±0.19) mg/million cycles for the low crosslinked Oxford mobile bearing. Finite element analysis was used to calculate the effect of crosslinking and backside wear. Increase in polyethylene crosslinking reduced wear by 68% while backside wear comprised 46% of the total wear in the mobile bearing. Increasing conformity may not be the sole predictor of wear performance and highly crosslinked fixed-bearing polyethylene insert can also provide high wear performance. Copyright © 2015 Elsevier Inc. All rights reserved.

  7. Thermal Oxidation of Ti6Al4V Alloy with Enhanced Wear and Corrosion Resistance for Oil and Gas Application: Effect of Temperature

    NASA Astrophysics Data System (ADS)

    Lin, Naiming; Zhou, Peng; Wang, Yating; Zou, Jiaojuan; Ma, Yong; Wang, Zhenxia; Tian, Wei; Yao, Xiaofei; Tang, Bin

    2015-03-01

    Thermal oxidation (TO) treatments were performed at 873 K, 898 K, 923 K, 948 K, 973 K, 998 K and 1023 K for 10 h in air to improve the wear and corrosion resistance of Ti6Al4V alloy. The effect of TO temperature on microstructural characterizations and surface properties of the obtained TO layers were investigated. The results showed that TO layers with various thickness values were formed on Ti6Al4V alloy under different temperatures. The thickness of the TO layers increased with the increasing of TO temperature. TO layer that was obtained at 973 K suggested the highest surface hardness and the best wear resistance. TO layer that was realized at 948 K exhibited superior corrosion resistance to other TO layers. TO treatment could be considered as an effective method for preventing wear and corrosion of Ti6Al4V alloy.

  8. Wear behavior of the plasma and thermal oxidized Ti-15Mo and Ti-6Al-4V alloys

    NASA Astrophysics Data System (ADS)

    Hacisalioglu, I.; Yildiz, F.; Alsaran, A.; Purcek, G.

    2017-02-01

    Titanium and its alloys widely used in load bearing applications. Titanium alloys are capable of providing lower elastic modulus and better corrosion resistance with alloying processes. In spite of the modified mechanical properties, the surface degradation is still the main critical defect. Ti-15Mo alloy is one of the alpa+beta titanium alloys with acceptable mechanical and chemical superiority. Recent researches in literature show that the wear performance of base Ti-15Mo is relatively low as compared to Ti-6Al-4V, using in high performance applications. Plasma oxidized surfaces increase the tribological and chemical performance of titanium alloys. In this study the Ti-15Mo alloy and Ti-6Al-4V alloys were compared in terms of wear performance. To obtain alloys with similar microstructure they were solution treated at 800°C 1H and then air-cooled. The plasma and thermal oxidations were applied at 650°C for 1 hour. Wear performance of oxidized surfaces investigated in dry conditions. Oxidized surface characterized with XRD, SEM, 3D profilometer and hardness measurements. Wear volume calculated with 3D profilometer. Results show that oxidizing increased the surface roughness and improved the wear performance of Ti15Mo alloy. The plasma and thermal oxidized Ti-15Mo showed a remarkable increase in wear resistance.

  9. Measurement of friction and wear

    NASA Technical Reports Server (NTRS)

    Buckley, D. H.

    1978-01-01

    Report reviews various techniques and surface tools available for study of wear of materials. Atomic nature of solid surfaces plays important role in wear behavior for materials in solid-state contact.

  10. Employees Wearing Religious Attire

    ERIC Educational Resources Information Center

    Zirkel, Perry

    2004-01-01

    While adherents to many religions can be identified by distinctive clothing or accessories, the wearing of such garb by teachers is not necessarily related to evangelism in the classroom. The following case and the accompanying question-and-answer discussion illustrate the problem of the principal caught between the rock of First Amendment…

  11. Wear resistant valve

    NASA Technical Reports Server (NTRS)

    Perkins, Gerald S. (Inventor)

    1980-01-01

    A valve which is resistant to wear caused by particles trapped between the valve seat and the valve member or poppet when the valve closes, including an outlet for directing washing fluid at the valve seat and/or sealing face of the poppet and means for supplying pressured fluid to the outlet at the time when the valve is closing.

  12. Employees Wearing Religious Attire

    ERIC Educational Resources Information Center

    Zirkel, Perry

    2004-01-01

    While adherents to many religions can be identified by distinctive clothing or accessories, the wearing of such garb by teachers is not necessarily related to evangelism in the classroom. The following case and the accompanying question-and-answer discussion illustrate the problem of the principal caught between the rock of First Amendment…

  13. The Corrosion and Wear Performance of Microcrystalline WC-10Co-4Cr and Near-Nanocrystalline WC-17Co High Velocity Oxy-Fuel Sprayed Coatings on Steel Substrate

    NASA Astrophysics Data System (ADS)

    Saha, Gobinda C.; Khan, Tahir I.

    2010-11-01

    The study of near-nanocrystalline cermet composite coating was performed by depositing near-nanocrystalline WC-17Co powder using the high velocity oxy-fuel spraying technique. The WC-17Co powder consists of a core with an engineered near-nano-scale WC dispersion with a mean grain size 427 nm. The powder particle contains 6 wt pct of the ductile phase Co matrix mixed into the core to ensure that the reinforcing ceramic phase WC material is discontinuous to limit debridement during wear, while the remainder of the binding phase (11 wt pct) is applied as a coating on the powder particle to improve the ductility. The tribological properties of the coating, in terms of corrosion resistance, microhardness, and sliding abrasive wear, were studied and compared with those of an industrially standard microcrystalline WC-10Co-4Cr coating with a WC mean grain size 3 μm. Results indicated that the WC-17Co coating had superior wear and corrosion resistance compared to the WC-10Co-4Cr coating. The engineered WC-17Co powder with a duplex Co layer had prevented significant decarburization of the WC dispersion in the coating, thereby reducing the intersplat microporosity necessary for initiating microgalvanic cells. The improved wear resistance was attributed to the higher hardness value of the near-nanocrystalline WC-17Co coating.

  14. Measuring Bearing Wear Via Weight Loss

    NASA Technical Reports Server (NTRS)

    Keba, John E.; Moore, Richard S.

    1989-01-01

    Wear in critical parts of bearings measured via amounts of weight lost during use. Technique applicable in general to bearings made of nonporous materials. Weight-loss measurements easier, faster, more precise, and less likely to damage measured parts. Weight-loss measurements performed in clean rooms and under constraint of extreme cleanliness for compatability with liquid oxygen.

  15. Wear analysis of disc cutters of full face rock tunnel boring machine

    NASA Astrophysics Data System (ADS)

    Zhang, Zhaohuang; Meng, Liang; Sun, Fei

    2014-11-01

    Wear is a major factor of disc cutters' failure. No current theory offers a standard for the prediction of disc cutter wear yet. In the field the wear prediction method commonly used is based on the excavation length of tunnel boring machine(TBM) to predict the disc cutter wear and its wear law, considering the location number of each disc cutter on the cutterhead(radius for installation); in theory, there is a prediction method of using arc wear coefficient. However, the preceding two methods have their own errors, with their accuracy being 40% or so and largely relying on the technicians' experience. Therefore, radial wear coefficient, axial wear coefficient and trajectory wear coefficient are defined on the basis of the operating characteristics of TBM. With reference to the installation and characteristics of disc cutters, those coefficients are modified according to penetration, which gives rise to the presentation of comprehensive axial wear coefficient, comprehensive radial wear coefficient and comprehensive trajectory wear coefficient. Calculation and determination of wear coefficients are made with consideration of data from a segment of TBM project(excavation length 173 m). The resulting wear coefficient values, after modification, are adopted to predict the disc cutter wear in the follow-up segment of the TBM project(excavation length of 5621 m). The prediction results show that the disc cutter wear predicted with comprehensive radial wear coefficient and comprehensive trajectory wear coefficient are not only accurate(accuracy 16.12%) but also highly congruous, whereas there is a larger deviation in the prediction with comprehensive axial wear coefficient(accuracy 41%, which is in agreement with the prediction of disc cutters' life in the field). This paper puts forth a new method concerning prediction of life span and wear of TBM disc cutters as well as timing for replacing disc cutters.

  16. Magnetic Fluid Friction and Wear Behavior

    NASA Technical Reports Server (NTRS)

    Keith, Theo G., Jr.

    1998-01-01

    The friction and wear properties of two groups of magnetic fluids, one developed at NASA Lewis Research Center and a commercial fluid, were evaluated for boundary lubrication. Friction and wear measurements were made using a pin-on-disk apparatus. Three different ball materials were evaluated, (1) 440C, (2) Al2O3, and (3) Si3N4 against 440C disks. The first class of magnetic fluids have a low vapor pressure hydrocarbon base oil and are suitable for space application. Four variations of this fluid were evaluated: (1) the base oil, (2) base oil with anti-wear additives, (3) a 100 Gauss strength magnetic fluid, and (4) a 400 gauss magnetic fluid. The commercial fluid base oil and four different magnetic particle concentration levels have been evaluated. A space qualified fluorinated lubricant was tested for base line comparison. Hardness, optical microscopy, surface profilometry, and surface analysis were used to characterize the test specimens. Friction was unaffected by the concentration of magnetic particles. Wear rates for magnetic fluids were slightly higher than the base oil. The low vapor pressure magnetic fluid has better wear characteristics than the space qualified fluorinated lubricant.

  17. Wear performance of ceramic-on-metal hip bearings.

    PubMed

    Reinders, Jörn; Sonntag, Robert; Heisel, Christian; Reiner, Tobias; Vot, Leo; Kretzer, Jan Philippe

    2013-01-01

    Ceramic-on-metal (CoM) bearings are considered to be a promising alternative to polyethylene-based bearings or hard-on-hard bearings (Ceramic-on-Ceramic (CoC) and Metal-on-Metal (MoM)). Although, CoM shows lower wear rates than MoM, in-vitro wear testing of CoM shows widely varying results. This may be related to limitations of wear-measuring methods. Therefore, the aim of this study was to improve the gravimetric measurement technique and to test wear behaviour of CoM bearings compared to CoC bearings. Level walking according to ISO-14242 was simulated for four CoM and four CoC bearings. Prior to simulation, errors in measurement of gravimetric wear were detected and improvements in measurement technique incorporated. The results showed no differences in mean wear rates between CoM and CoC bearings. However, the CoM bearings showed wear results over a wide range of wear performance. High reliability of wear results was recorded for the CoC bearings. Material transfer was observed on the ceramic heads of the CoM bearings. Therefore, for level walking a partial mixed or boundary lubrication has to be assumed for this type of bearing. CoM is a highly sensitive wear-couple. The reasons for the observed behaviour cannot be clarified from this study. Simulator studies have to be considered as an ideal loading condition. Therefore, high variations in wear rates as seen in this study, even at low levels, may have an adverse effect on the in-vivo wear behavior. Careful clinical use may be advisable until the reasons for the variation are fully clarified and understood.

  18. Wear Performance of Ceramic-On-Metal Hip Bearings

    PubMed Central

    Reinders, Jörn; Sonntag, Robert; Heisel, Christian; Reiner, Tobias; Vot, Leo; Kretzer, Jan Philippe

    2013-01-01

    Ceramic-on-metal (CoM) bearings are considered to be a promising alternative to polyethylene-based bearings or hard-on-hard bearings (Ceramic-on-Ceramic (CoC) and Metal-on-Metal (MoM)). Although, CoM shows lower wear rates than MoM, in-vitro wear testing of CoM shows widely varying results. This may be related to limitations of wear-measuring methods. Therefore, the aim of this study was to improve the gravimetric measurement technique and to test wear behaviour of CoM bearings compared to CoC bearings. Level walking according to ISO-14242 was simulated for four CoM and four CoC bearings. Prior to simulation, errors in measurement of gravimetric wear were detected and improvements in measurement technique incorporated. The results showed no differences in mean wear rates between CoM and CoC bearings. However, the CoM bearings showed wear results over a wide range of wear performance. High reliability of wear results was recorded for the CoC bearings. Material transfer was observed on the ceramic heads of the CoM bearings. Therefore, for level walking a partial mixed or boundary lubrication has to be assumed for this type of bearing. CoM is a highly sensitive wear-couple. The reasons for the observed behaviour cannot be clarified from this study. Simulator studies have to be considered as an ideal loading condition. Therefore, high variations in wear rates as seen in this study, even at low levels, may have an adverse effect on the in-vivo wear behavior. Careful clinical use may be advisable until the reasons for the variation are fully clarified and understood. PMID:24009743

  19. Hardfacing and wear plates battle abrasion

    SciTech Connect

    Miller, R.F.

    1983-06-01

    This article examines abrasion-resistant steels and hardfacing as two effective weapons at the disposal of material handlers. It points out that abrasion is probably the single most destructive form of wear in the mixing and processing of coal. Particulate matter such as quartz sand and other minerals including coal curtail in-service life of dragline buckets, chute, crusher rolls, gates and valves, exhauster fan blades, target plates, truck beds, hoppers, vibrating pans, grinding mills, piping elbows, etc. The advantages of abrasion-resistant steels and hardfacing can be obtained in the form of a composite wear plate-hardfacing on a carbon steel backup plate. It concludes that the composite wear plate represents a major innovation since its advantages include ease of handling, low cost and easy installation, minimum on-site welding time and versatility. Its use is limited only to the consumer's creativity in application.

  20. In vivo corneal oxygen uptake during soft-contact-lens wear.

    PubMed

    Takatori, Sho C; Lazon de la Jara, Percy; Holden, Brien; Ehrmann, Klaus; Ho, Arthur; Radke, Clayton J

    2013-05-17

    We develop a new method to compute in situ corneal oxygen uptake during soft-contact-lens (SCL) wear using a micro-polarographic Clark electrode. After steady SCL wear and subsequent removal, a membrane-covered polarographic microelectrode is immediately placed onto the cornea. The resulting polarographic signal is related to the steady-state corneal oxygen uptake rate during soft-contact-lens wear. We devise a new analysis to quantify oxygen uptake into the cornea during lens wear. The proposed procedure is applied to new polarographic data for 10 human subjects with 12 different commercial lenses during open eye. We compare our results with recent theory. Average corneal oxygen uptake rates at open eye during SCL wear for 10 subjects wearing 12 different commercial lenses vary from 2 to 10 μL(STP)/cm(2)/h. High oxygen permeability lenses have uptake rates of -10 μL(STP)/cm(2)/h, in close agreement with our previously obtained no-lens human uptake rates of 9 to 13 μL(STP)/cm(2)/h at open eye.(40) Application of the classical data-interpretation procedure to our experimental data gives corneal-uptake results that are approximately three to five times smaller than those obtained with our new interpretation scheme. We provide a simple and reliable tool to quantify corneal-oxygen-uptake rates during in vivo soft-contact-lens wear. Comparison of our newly measured in vivo oxygen uptakes to model prediction for SCLs of varying oxygen transmissibility is in good agreement with available theory.

  1. Wear characteristics of severely deformed aluminum sheets by accumulative roll bonding (ARB) process

    SciTech Connect

    Talachi, A. Kazemi; Eizadjou, M. Manesh, H. Danesh; Janghorban, K.

    2011-01-15

    Wear behavior of severely deformed aluminum sheets by accumulative roll bonding (ARB) process was characterized using a pin on disc wear machine at different conditions. The sheets were processed up to eight ARB cycles in order to induce a high strain ({approx} 6.4) to the samples. EBSD results showed that after eight cycles of ARB, sheets were found to contain ultrafine grains with high fraction of high angle grain boundaries. Wear experiments were conducted under different loading and operating conditions, including dry and immersion lubrication, and rotation speeds. Wear was continuously monitored by measuring the wear rates and morphologies of worn surfaces by scanning electron microscope (SEM). Contrary to expectation, the wear resistance of the ARBed Al sheets was less than the non-processed sheets. Wear rates of the ARBed Al sheets increased by increasing wear load and rotation speed, while, immersion lubrication decreased the wear rate significantly. Based on the observation and results, a model for the wear of the ARBed Al was proposed. - Research Highlights: {yields}The wear rate of the ARBed Al was higher than that of the non-processed alloy. {yields}This unexpected behavior was related to the low strain hardening capability and evolution of the ARB subsurface microstructure during the wear process. {yields}Sliding wear of the ARBed Al proceeded by surface deformation, and progressed by delamination of the deformed surface layer. {yields}The wear rate of ARBed Al increased by increasing applied load and sliding speed.

  2. Effect of processing, sterilization and crosslinking on UHMWPE fatigue fracture and fatigue wear mechanisms in joint arthroplasty.

    PubMed

    Ansari, Farzana; Ries, Michael D; Pruitt, Lisa

    2016-01-01

    Ultra high molecular weight polyethylene (UHMWPE) has been used as a bearing surface in total joint replacements (TJR) for nearly five decades. This semi-crystalline polymer has extraordinary energetic toughness owing to its high molecular weight and entanglement density. However, it is challenged by a need to offer a combined resistance to fatigue, wear and oxidation in vivo. The processing, sterilization treatment, and microstructural tailoring of UHMWPE has evolved considerably in the past 50 years but an optimized microstructure remains elusive. This review seeks to provide an overview of this processing history to address two primary questions: First, how does microstructure affect fatigue fracture and fatigue wear mechanisms in UHMWPE? And second, can microstructure be optimized to provide resistance to fatigue, oxidation and wear in vivo? Previous literature demonstrates that while crosslinking improves resistance to adhesive/abrasive wear, it also reduces resistance to fatigue crack propagation and fatigue wear by restricting molecular mobility and rendering the polymer more brittle. Crystallinity improves fatigue resistance but generally increases elastic modulus and concomitant contact stresses in vivo. The presence of fusion defects or oxidation reduces further fatigue resistance and enhances fatigue wear. Thus, UHMWPE microstructural evolution comes with trade-offs. Currently there is no singular formulation of UHMWPE that is ideal for all TJR applications.

  3. Tribology of Si/SiO2 in humid air: transition from severe chemical wear to wearless behavior at nanoscale.

    PubMed

    Chen, Lei; He, Hongtu; Wang, Xiaodong; Kim, Seong H; Qian, Linmao

    2015-01-13

    Wear at sliding interfaces of silicon is a main cause for material loss in nanomanufacturing and device failure in microelectromechanical system (MEMS) applications. However, a comprehensive understanding of the nanoscale wear mechanisms of silicon in ambient conditions is still lacking. Here, we report the chemical wear of single crystalline silicon, a material used for micro/nanoscale devices, in humid air under the contact pressure lower than the material hardness. A transmission electron microscopy (TEM) analysis of the wear track confirmed that the wear of silicon in humid conditions originates from surface reactions without significant subsurface damages such as plastic deformation or fracture. When rubbed with a SiO2 ball, the single crystalline silicon surface exhibited transitions from severe wear in intermediate humidity to nearly wearless states at two opposite extremes: (a) low humidity and high sliding speed conditions and (b) high humidity and low speed conditions. These transitions suggested that at the sliding interfaces of Si/SiO2 at least two different tribochemical reactions play important roles. One would be the formation of a strong "hydrogen bonding bridge" between hydroxyl groups of two sliding interfaces and the other the removal of hydroxyl groups from the SiO2 surface. The experimental data indicated that the dominance of each reaction varies with the ambient humidity and sliding speed.

  4. Continued force wear and part correction experiments

    SciTech Connect

    Hannah, P.R.; Day, R.D.; Hatch, D.J.

    1995-12-31

    This abstract reports the near completion of the first phase of this program. It is the aim of this program to provide the operator of a N/C diamond turning machine or N/C grinding machine (jig grinder) with the wear characteristics necessary to achieve uniform material removal. The second phase of this program addresses a different problem, although solving this problem is highly dependent on the results of the first phase. Diamond turned, or any lathe turned surface, exhibits regular tool marks due to the tool passing over the surface being cut. Changes in depth of cut, feed rate and work rpm will change the character of these groves, but will not eliminate them. Optical surfaces produced by this process exhibit increased scattering as the light wavelength decreases limiting their use; at least for optical purposes, to IR and some visible applications. Utilizing wear information gathered in the first part of this program we will attempt to reduce these residual tool marks by polishing. The polishing of diamond turned surfaces is not new. Diamond turned metal surfaces, especially in electroless nickel and high phosphorus nickel electroplate have been polished to improve their scatter characteristics. What we believe is unique is the use of a spherical wheel, rotating on axis and being moved over the part in a prescribed manner by numerical control. Over the past year we have made some major changes in our polishing methods and procedures. We have listed below these changes, as a refresher for the reader as to our previous procedures.

  5. Effect of Different Forefoot and Heel Support Surfaces on the Activities of the RF and HAM Muscles during the Sit-to-stand Task while Wearing High-heel Shoes.

    PubMed

    Yoo, Won-Gyu

    2014-10-01

    [Purpose] The purpose of this study was to show the effect of different forefoot and heel support surfaces on the activities of the rectus femoris and medial hamstring muscles during the sit-to-stand task while wearing high-heel shoes. [Subjects] Fifteen female subjects were recruited. [Methods] The muscle activities of the rectus femoris and hamstring muscles were recorded using an MP150 system during the sit-to-stand task while wearing various high-heeled shoes. [Results] The activities of the rectus femoris and medial hamstring muscles significantly decreased when subjects wore condition 1 shoes compared with when they wore condition 2, 3 or 4 high-heeled shoes. The activities of the rectus femoris and medial hamstring muscles significantly decreased when subjects wore condition 2 high-heeled shoes compared with condition 3 or 4 high-heeled shoes. [Conclusion] The results can be interpreted as indicating that the size of the forefoot supporting surface can influence the lower extremity muscles of women wearing high-heeled shoes more than the size of the heel supporting surface.

  6. Wear testing of materials and surfaces for total knee replacement.

    PubMed

    Walker, P S; Blunn, G W; Lilley, P A

    1996-01-01

    A simple wear test was investigated for evaluating the wear and damage of material pairs when used in total knee replacement. The test consisted of an axially loaded metallic femoral indentor and a reciprocating ultrahigh molecular weight polyethylene (UHMWPE) flat disk that represented the tibial component. A number of variables were studied including the effect of conformity by varying the radii of the femoral surface, distilled water or serum as a lubricant, different femoral materials, and different types of UHMWPE. In general, the different morphologies of the surface wear of the UHMWPE were similar to those seen on retrieved total knee replacements. Increased conformity with a cylindrical indentor gave a reduced wear rate initially, compared with that of the lower conformity spherical indentor. However, the wear rates were similar subsequent to this initial wearing in phase. Transfer films of UHMWPE were observed on the cobalt-chrome indentors for both serum and distilled water lubrication, although this film was more extensive for distilled water. The lowest wear rate was observed when oxidized zirconium was used on the femoral side, which was attributed to greater wettability, surface hardness, and immunity to oxidative wear. Tests using cobalt-chrome femoral cylinders and different grades of UHMWPE showed different wear rates. Of these PEs, GUR 415 showed less wear than both RCH 1000 and UHMWPE containing numerous fusion defects. For the latter, wear was attributed to a fatigue mechanism, although in most cases it was associated with surface phenomena rather than subsurface cracking. However, in some specimens of UHMWPE subsurface crack propagations occurred with defects. The test method is discussed in relation to its applicability to the evaluation and comparison of bearing materials and surfaces, with particular application to total knee replacements.

  7. Electrochemical Wear of Carbon Cathodes in Electrowinning of Aluminum

    NASA Astrophysics Data System (ADS)

    Tschöpe, Kati; Støre, Anne; Solheim, Asbjørn; Skybakmoen, Egil; Grande, Tor; Ratvik, Arne Petter

    2013-11-01

    Cathode wear is the main factor limiting the lifetime of high-amperage aluminum electrolysis cells with graphitized cathodes. The current article deals with an investigation of cathode wear in a laboratory cell, where the cathode is directly exposed to the electrolyte during electrolysis. The wear was shown to be electrochemical in nature and dependent on the current density, the rotation speed, and the depth of prefabricated slots in the cylindrical cathodes. The wear mechanism is discussed with respect to kinetics influencing the electrochemistry as well as the solubility of aluminum carbide in the electrolyte.

  8. Friction and wear of TPS fibers: A study of the adhesion and friction of high modulus fibers

    NASA Technical Reports Server (NTRS)

    Bascom, Willard D.; Lee, Ilzoo

    1990-01-01

    The adhesional and frictional forces between filaments in a woven fabric or felt, strongly influenced the processability of the fiber and the mechanical durability of the final product. Even though the contact loads between fibers are low, the area of contact is extremely small giving rise to very high stresses; principally shear stresses. One consequence of these strong adhesional and frictional forces is the resistance of fibers to slide past each other during weaving or when processed into nonwoven mats or felts. Furthermore, the interfiber frictional forces may cause surface damage and thereby reduce the fiber strength. Once formed into fabrics, flexural handling and manipulation of the material again causes individual filaments to rub against each other resulting in modulus, brittle fibers such as those used in thermal protection systems (TPS). The adhesion and friction of organic fibers, notably polyethylene terephthalate (PET) fibers, have been extensively studied, but there has been very little work reported on high modulus inorganic fibers. An extensive study was made of the adhesion and friction of flame drawn silica fibers in order to develop experimental techniques and a scientific basis for data interpretation. Subsequently, these methods were applied to fibers of interest in TPS materials.

  9. Wear mechanism and tribological characteristics of porous NiTi shape memory alloy for bone scaffold.

    PubMed

    Wu, Shuilin; Liu, Xiangmei; Wu, Guosong; Yeung, Kelvin W K; Zheng, Dong; Chung, C Y; Xu, Z S; Chu, Paul K

    2013-09-01

    The abraded debris might cause osteocytic osteolysis on the interface between implants and bone tissues, thus inducing the subsequent mobilization of implants gradually and finally resulting in the failure of bone implants, which imposes restrictions on the applications of porous NiTi shape memory alloys (SMAs) scaffolds for bone tissue engineering. In this work, the effects of the annealing temperature, applied load, and porosity on the tribological behavior and wear resistance of three-dimensional porous NiTi SMA are investigated systematically. The porous structure and phase transformation during the exothermic process affect the tribological properties and wear mechanism significantly. In general, a larger porosity leads to better tribological resistance but sometimes, SMAs with small porosity possess better wear resistance than ones with higher porosity during the initial sliding stage. It can be ascribed to the better superelasticity of the former at the test temperature. The porous NiTi phase during the exothermic reaction also plays an important role in the wear resistance. Generally, porous NiTi has smaller friction coefficients under high loads due to stress-induced superelasticity. The wear mechanism is discussed based on plastic deformation and microcrack propagation.

  10. Wear and Life Characteristics of Microwave-Sintered Copper-Graphite Composite

    NASA Astrophysics Data System (ADS)

    Rajkumar, K.; Aravindan, S.; Kulkarni, M. S.

    2012-11-01

    Copper-graphite composite is an important tribological material used in electrical sliding contact applications like electrical brushes in motors and generators. The electrical sliding contact experiences multiple stresses such as mechanical pressure and temperature. Traditional life tests under normal operating condition would be a time-consuming process due to the longer expected life of the composite. Accelerated wear testing was carried out to evaluate the life characteristics of the composite. This work focuses on evaluation of tribological performance of microwave-sintered copper-graphite composite using accelerated wear testing methodology using high temperature pin-on-disc tribometer. Microstructural studies of worn out surfaces were carried out using SEM with EDAX. Reliability and analysis on life characteristics were performed on the time-to-failure data using temperature-nonthermal-accelerated life-stress model. The obtained times-to-failure data from the accelerated wear testing was extrapolated to normal usage condition. Temperature and pressure are significantly affecting the wear performance. Self-lubricating action of graphite and improvement in wear resistance is helpful in extending the life of copper graphite composite. The life of the composite obtained through testing at mean and 99% reliability are 18,725 and 16,950 h, respectively.

  11. Wear Resistance and Wear Mechanism of a Hot Dip Aluminized Steel in Sliding Wear Test

    NASA Astrophysics Data System (ADS)

    Xue, Zhiyong; Hao, Xiaoyang; Huang, Yao; Gu, Lingyun; Ren, Yu; Zheng, Ruipeng

    2016-12-01

    Sliding wear experiments were conducted on a hot dip aluminized steel to investigate its wear resistance and wear mechanism. The wear tests were also carried out on a hot dip galvanized steel and the base material (steel Q345) as a comparison. Results show that the wear resistance and hardness of the hot dip aluminized steel are significantly higher than that of the hot dip galvanized steel and the steel Q345 at room temperature. The better wear resistance of the hot dip aluminized steel attributes mainly to the formation of a transition layer containing abundant Fe-Al intermetallic compounds and the transformation of wear-resisting oxides during the friction process. The main phase in the transition layer is Fe2Al5. The thickness of the transition layer is about 90-120 μm. When the wear load increases from 3 N to 19 N, the wear type of the aluminized layer transform from adhesive wear (3 N) into abrasive wear (7 N) and finally into slight wear mixed with oxidation (higher than 11 N).

  12. Dependence of the diffusion wear of the hard alloy surface on its fractal dimension

    NASA Astrophysics Data System (ADS)

    Nesterenko, V. P.; Kondratyuk, A. A.; Belousova, E. B.; Shulepov, I. A.

    2017-02-01

    The paper presents the research results in the synergies between the wear resistance of carbide cutting tools of P-group applicability and fractal dimension of the wear surface occurring on the rake face of the tool when processing the material, which causes intensive diffusion wear. It was found that the resistance of carbide cutting tools increases as the fractal dimension of their wear surface reduces.

  13. Reciprocating seals: Lubrication and wear resistance. (Latest citations from Fluidex (Fluid Engineering Abstracts) database). Published Search

    SciTech Connect

    Not Available

    1993-10-01

    The bibliography contains citations concerning theoretical and practical analyses of reciprocating seal wear and lubrication. Topics include behavior, friction coefficient, cylinder wear, lubrication film thickness, friction forces, design innovations, lubricating oil viscosity, and wear modeling relative to reciprocating seal frictional wear and lifetime optimization. Applications in piston ring lubrication, internal combustion engines, and vehicle suspension systems are considered. (Contains 250 citations and includes a subject term index and title list.)

  14. In Situ Wear Test on Thermal Spray Coatings in a Large Chamber Scanning Electron Microscope

    NASA Astrophysics Data System (ADS)

    Luo, Weifeng; Tillmann, Wolfgang; Selvadurai, Ursula

    2015-01-01

    Currently, the determination of the mass loss is usually used for a quantitative evaluation of wear tests, while the analysis of wear tracks is utilized for a qualitative evaluation of wear. Both evaluation methods can only be used after the wear testing process and their results only present the final outcome of the wear test. However, the changes during the wear test and the time-dependent wear mechanisms are of great interest as well. A running wear test in a large chamber scanning electron microscope (SEM) offers the first opportunity to observe the wear process in situ. Different wear mechanisms, such as the adhesive, abrasive wear, surface fatigue and tribochemical reaction, can be recorded with high magnification. Within this research, a special pin-on-disk testing device is designed for a vacuum environment. Using this device, arc-sprayed NiCrBSi coatings and high-velocity-oxygen-fuel-sprayed WC-12Co coatings were tested in a large chamber SEM with Al2O3 ceramic balls as wear counterparts. During the wear testing, different wear mechanisms were determined and the processes were recorded in short video streams.

  15. Wear Modalities and Mechanisms of the Mining Non-asbestos Composite Brake Material

    NASA Astrophysics Data System (ADS)

    Bao, Jiusheng; Yin, Yan; Zhu, Zhencai; Tong, Minming; Lu, Yuhao; Peng, Yuxing

    2013-08-01

    The mining brake material is generally made of composite materials and its wear has important influences on the braking performance of disc brakes. In order to improve the braking reliability of mine hoisters, this paper did some tribological investigations on the mining brake material to reveal its wear modalities and mechanisms. The mining non-asbestos brake shoe and 16Mn steel were selected as braking pairs and tested on a pad-on-disc friction tester. And a SEM was used to observe the worn surface of the brake shoe. It is shown that the non-asbestos brake material has mainly five wear modalities: adhesive wear, abrasive wear, cutting wear, fatigue wear and high heat wear. At the front period of a single braking the wear modality is mainly composed of some light mechanical wear such as abrasive, cutting and point adhesive. With the temperature rising at the back period it transforms to some heavy mechanical wear such as piece adhesive and fatigue. While in several repeated brakings once the surface temperature rises beyond the thermal-decomposition point of the bonding material, the strong destructive high heat wear takes leading roles on the surface. And a phenomenon called friction catastrophe (FC) occurs easily, which as a result causes a braking failure. It is considered that the friction heat has important influences on the wear modalities of the brake material. And the reduction of friction heat must be an effective technical method for decreasing wear and avoiding braking failures.

  16. Self-Lubricating, Wear-Resistant Diamond Films Developed for Use in Vacuum Environment

    NASA Technical Reports Server (NTRS)

    1996-01-01

    Diamond's outstanding properties--extreme hardness, chemical and thermal inertness, and high strength and rigidity--make it an ideal material for many tribological applications, such as the bearings, valves, and engine parts in the harsh environment found in internal-combustion engines, jet engines, and space propulsion systems. It has been demonstrated that chemical-vapor-deposited diamond films have low coefficients of friction (on the order of 0.01) and low wear rates (less than 10(sup -7) mm (sup 3/N-m)) both in humid air and dry nitrogen but that they have both high coefficients of friction (greater than 0.4) and high wear rates (on the order of 1(sup -4) mm sup 3/N-m)) in vacuum. It is clear that surface modifications that provide acceptable levels of friction and wear properties will be necessary before diamond films can be used for tribological applications in a space-like, vacuum environment. Previously, it was found that coatings of amorphous, non-diamond carbon can provide low friction in vacuum. Therefore, to reduce the friction and wear of diamond film in vacuum, carbon ions were implanted in an attempt to form a surface layer of amorphous carbon phases on the diamond films.

  17. A lightweight, high strength dexterous manipulator for commercial applications

    NASA Technical Reports Server (NTRS)

    Marzwell, Neville I.; Schena, Bruce M.; Cohan, Steve M.

    1991-01-01

    The concept, design, and features are described of a lightweight, high strength, modular robot manipulator being developed for space and commercial applications. The manipulator has seven fully active degrees of freedom and is fully operational in 1 G. Each of the seven joints incorporates a unique drivetrain design which provides zero backlash operation, is insensitive to wear, and is single fault tolerant to motor or servo amplifier failure. Feedback sensors provide position, velocity, torque, and motor winding temperature information at each joint. This sensing system is also designed to be single fault tolerant. The manipulator consists of five modules (not including gripper). These modules join via simple quick-disconnect couplings and self-mating connectors which allow rapid assembly and/or disassembly for reconfiguration, transport, or servicing. The manipulator is a completely enclosed assembly, with no exposed components or wires. Although the initial prototype will not be space qualified, the design is well suited to meeting space requirements. The control system provides dexterous motion by controlling the endpoint location and arm pose simultaneously. Potential applications are discussed.

  18. CrN-based wear resistant hard coatings for machining and forming tools

    NASA Astrophysics Data System (ADS)

    Yang, S.; Cooke, K. E.; Li, X.; McIntosh, F.; Teer, D. G.

    2009-05-01

    Highly wear resistant multicomponent or multilayer hard coatings, based on CrN but incorporating other metals, have been developed using closed field unbalanced magnetron sputter ion plating technology. They are exploited in coated machining and forming tools cutting and forming of a wide range of materials in various application environments. These coatings are characterized by desirable properties including good adhesion, high hardness, high toughness, high wear resistance, high thermal stability and high machining capability for steel. The coatings appear to show almost universal working characteristics under operating conditions of low and high temperature, low and high machining speed, machining of ordinary materials and difficult to machine materials, and machining under lubricated and under minimum lubricant quantity or even dry conditions. These coatings can be used for cutting and for forming tools, for conventional (macro-) machining tools as well as for micromachining tools, either as a single coating or in combination with an advanced, self-lubricating topcoat.

  19. High-temperature wear and oxidation behaviors of TiNi/Ti2Ni matrix composite coatings with TaC addition prepared on Ti6Al4V by laser cladding

    NASA Astrophysics Data System (ADS)

    Lv, Y. H.; Li, J.; Tao, Y. F.; Hu, L. F.

    2017-04-01

    TiNi/Ti2Ni matrix composite coatings were produced on Ti6Al4V surfaces by laser cladding the mixed powders of Ni-based alloy and different contents of TaC (0, 5, 10, 15, 20, 30 and 40 wt.%). Microstructures of the coatings were investigated. High-temperature wear tests of the substrate and the coatings were carried out at 600 °C in air for 30 min. High-temperature oxidation tests of the substrate and the coatings were performed at 1000 °C in air for 50 h. Wear and oxidation mechanisms were revealed in detail. The results showed that TiNi/Ti2Ni as the matrix and TiC/TiB2/TiB as the reinforcements are the main phases of the coatings. The friction coefficients of the substrate and the coatings with different contents of TaC were 0.431 (the substrate), 0.554 (0 wt.%), 0.486 (5 wt.%), 0.457 (10 wt.%), 0.458 (15 wt.%), 0.507 (20 wt.%), 0.462 (30 wt.%) and 0.488 (40 wt.%). The wear rates of the coatings were decreased by almost 83%-98% than that of the substrate and presented a decreasing tendency with increasing TaC content. The wear mechanism of the substrate was a combination of serious oxidation, micro-cutting and brittle debonding. For the coatings, oxidation and slight scratching were predominant during wear, accompanied by slight brittle debonding in partial zones. With the increase in content of TaC, the oxidation film better shielded the coatings from destruction due to the effective friction-reducing role of Ta2O5. The oxidation rates of the substrate and the coatings with different contents of TaC at 1000 °C were 12.170 (the substrate), 5.886 (0 wt.%), 4.937 (5 wt.%), 4.517 (10 wt.%), 4.394 (15 wt.%), 3.951 (20 wt.%), 4.239 (30 wt.%) and 3.530 (40 wt.%) mg2 cm-4 h-1, respectively. The oxidation film formed outside the coating without adding TaC was composed of TiO2, NiO, Cr2O3, Al2O3 and SiO2. When TaC was added, Ta2O5 and TaC were also detected, which effectively improved the oxidation resistance of the coatings. The addition of TaC contributed to the

  20. Wear performance of monolithic dental ceramics with different surface treatments.

    PubMed

    Preis, Verena; Weiser, Felix; Handel, Gerhard; Rosentritt, Martin

    2013-05-01

    To investigate the two-body wear performance of monolithic dental ceramics with different surface treatments. Standardized specimens (n = 8/ series) were fabricated from three monolithic dental ceramics (experimental translucent zirconia, experimental shaded zirconia, lithium disilicate). Four groups of each material were defined according to clinically relevant surface treatments: polished, polishedground, polished-ground-repolished, glazed. Two-body wear tests with steatite antagonists were performed in a chewing simulator. Surface roughness (R(a)) was controlled, and wear depths of specimens and antagonistic wear areas were calculated in relation to human enamel as reference. Statistical analysis of wear data was carried out using one-way ANOVA and Bonferroni multiple comparison test for post hoc analysis (α = .05). Scanning electron microscopy was applied for evaluating wear performance of ceramics and antagonists. Polished, ground, and repolished zirconia showed no wear, while glaze was abraded. Irrespective of the surface treatment, wear depth of lithium disilicate was significantly (P high as for the enamel reference (274.14 µm). Mean relative wear areas of steatite antagonists (enamel reference: 1.25 mm2) ranged between 0.86 and 1.57 for zirconia, and between 1.79 and 2.28 for lithium disilicate, with the highest values found after grinding and glazing. Steatite surfaces were smooth when opposed to polished/ground/repolished zirconia, and ploughed when opposed to glaze and lithium disilicate. Translucent and shaded experimental zirconia yielded superior wear behavior and lower antagonistic wear compared to lithium disilicate. A trend to higher ceramic and antagonistic wear was shown after grinding and glazing.

  1. Corrosive wear principles

    SciTech Connect

    Schumacher, W.J.

    1993-12-31

    The dual effects of corrosion and wear operate together in such industries as paper and pulp, coal handling, mining, and sugar beet extraction. There is a synergistic effect that causes far greater wastage to carbon steels, alloy steels, and even much more abrasion resistant cast irons. Several laboratory and in situ studies have been conducted to better understand the contributions of corrosion and wear to the wastage process. The environmental conditions are usually set by the process. However, there are a few instances where inhibitors as sodium nitrite, sodium chromate, and sodium metasilicate have been successfully used to reduce metal wastage of carbon steels. Hardness has been found to be an unreliable guide to performance under wet sliding conditions. Heat treated alloy steels and cast irons are inferior to stainless steels. Even distilled water is too severe a corrodent for steels. While the austenitic stainlesses perform the best, cold rolling to increase hardness does not further improve their performance. The surface roughness of stainless steels gets smoother during corrosive wear testing while it gets rougher for the alloy steels. This observation substantiated the reputation of improved slideability for stainless alloys over alloy steels.

  2. Development of ball bearings with solid film for high-vacuum, high-temperature, high-speed application

    NASA Astrophysics Data System (ADS)

    Ogawa, Takashi; Konishi, Kazuaki; Aihara, Satoru; Sawamoto, Takeshi

    1993-04-01

    This paper describes the experimental results of long-life solid lubricated ball bearings tested under high-vacuum of 10 exp -4 Pa, high-temperature of 300 C, and high-speed (9000 rpm) conditions. For full ball-type bearings, the thin soft metals, either Ag or Pb, which were coated on the races and balls, appeared to have good torque properties. However, the durability of such bearings was less than 300 hours. The transfer films from the lamellar solid MoS2 and metal composite retainers improved the torque and wear properties. For ceramic, i.e., silicon nitride, balls used with steel rings, wear occurred on the inner rings. All ceramic bearings with composite retainers showed improved torque and wear properties.

  3. Wear and Tear - Mechanical

    NASA Technical Reports Server (NTRS)

    Swanson, Theodore

    2008-01-01

    The focus of this chapter is on the long term wear and tear, or aging, of the mechanical subsystem of a spacecraft. The mechanical subsystem is herein considered to be the primary support structure (as in a skeleton or exoskeleton) upon which all other spacecraft systems rest, and the associated mechanisms. Mechanisms are devices which have some component that moves at least once, in response to some type of passive or active control system. For the structure, aging may proceed as a gradual degradation of mechanical properties and/or function, possibly leading to complete structural failure over an extended period of time. However, over the 50 years of the Space Age such failures appear to be unusual. In contrast, failures for mechanisms are much more frequent and may have a very serious effect on mission performance. Just as on Earth, all moving devices are subject to normal (and possibly accelerated) degradation from mechanical wear due to loss or breakdown of lubricant, misalignment, temperature cycling effects, improper design/selection of materials, fatigue, and a variety of other effects. In space, such environmental factors as severe temperature swings (possibly 100's of degrees C while going in and out of direct solar exposure), hard vacuum, micrometeoroids, wear from operation in a dusty or contaminated environment, and materials degradation from radiation can be much worse. In addition, there are some ground handling issues such as humidity, long term storage, and ground transport which may be of concern. This chapter addresses the elements of the mechanical subsystem subject to wear, and identifies possible causes. The potential impact of such degradation is addressed, albeit with the recognition that the impact of such wear often depends on when it occurs and on what specific components. Most structural elements of the mechanical system typically are conservatively designed (often to a safety factor of greater than approximately 1.25 on yield for

  4. The Impact of Wearing a Face Mask in a High-Stakes Oral Examination: An Exploratory Post-SARS Study in Hong Kong

    ERIC Educational Resources Information Center

    Coniam, David

    2005-01-01

    This article describes a study that emerged as a result of the severe acute respiratory syndrome crisis that struck Hong Kong in 2003. One outcome of the severe acute respiratory syndrome crisis was that all personnel in all educational institutions in Hong Kong were compelled to wear face masks for the period April-August 2003. Consequently, the…

  5. c-axis preferential orientation of hydroxyapatite accounts for the high wear resistance of the teeth of black carp (Mylopharyngodon piceus)

    PubMed Central

    Fu, Jimin; He, Chong; Xia, Biao; Li, Yan; Feng, Qiong; Yin, Qifang; Shi, Xinghua; Feng, Xue; Wang, Hongtao; Yao, Haimin

    2016-01-01

    Biological armors such as mollusk shells have long been recognized and studied for their values in inspiring novel designs of engineering materials with higher toughness and strength. However, no material is invincible and biological armors also have their rivals. In this paper, our attention is focused on the teeth of black carp (Mylopharyngodon piceus) which is a predator of shelled mollusks like snails and mussels. Nanoscratching test on the enameloid, the outermost layer of the teeth, indicates that the natural occlusal surface (OS) has much higher wear resistance compared to the other sections. Subsequent X-ray diffraction analysis reveals that the hydroxyapatite (HAp) crystallites in the vicinity of OS possess c-axis preferential orientation. The superior wear resistance of black carp teeth is attributed to the c-axis preferential orientation of HAp near the OS since the (001) surface of HAp crystal, which is perpendicular to the c-axis, exhibits much better wear resistance compared to the other surfaces as demonstrated by the molecular dynamics simulation. Our results not only shed light on the origin of the good wear resistance exhibited by the black carp teeth but are of great value to the design of engineering materials with better abrasion resistance. PMID:27001150

  6. The Effect of Absorbable Calcium Sulfate on Wear Rates in Ultra-high-Molecular-weight Polyethylene: Potential Implications for Its Use in Treating Arthroplasty Infections.

    PubMed

    Lewicki, Kathleen; Prioreschi, Brandon; Koenig, Karl; Keeney, Benjamin; Bartelstein, Meredith; Moucha, Calin; Van Citters, Douglas

    2017-06-01

    Patients, hospitals, and healthcare systems incur substantial burdens when infections result in total joint revisions. One potential solution to mitigate some of these burdens may be to transition from a two-stage infection treatment to a single-stage procedure. Off-label use of an absorbable calcium sulfate antibiotic carrier has been implemented in single-stage and two-stage procedures globally, with the goal of moving toward more single-stage revisions in the United States. Adverse effects of calcium sulfate on the joint space during articulation are currently unknown. This study aims to determine the impact of calcium sulfate beads on wear of polyethylene during and following exposure. Two phases of in vitro pin-on-disk testing were conducted. The first phase exposed polyethylene pins to calcium sulfate for 500,000 cycles of a 2-million cycle test. The second phase examined the wear of pins that were created from retrieved components exposed to calcium sulfate in vivo. No clinically significant difference was observed between the wear rates of the calcium sulfate-exposed polyethylene pins and the control polyethylene pins. Preliminary results suggest that a substantial increase in the wear rate of polyethylene is not expected with the addition of calcium sulfate beads during treatment of infection.

  7. Effects of a Destabilization Heat Treatment on the Microstructure and Abrasive Wear Behavior of High-Chromium White Cast Iron Investigated Using Different Characterization Techniques

    NASA Astrophysics Data System (ADS)

    Gasan, Hakan; Erturk, Fatih

    2013-11-01

    The hypoeutectic white cast iron was subjected to various destabilization heat treatment temperatures of 1173 K, 1273 K, and 1373 K (900 °C, 1000 °C, and 1100 °C) for 2 hours. The as-cast and destabilized specimens were characterized by optical metallography, classical direct comparison, and the Rietveld method. The volume fractions of carbides were measured by optical metallography. Moreover, the volume fractions of retained austenite and martensite were measured by the classical direct comparison method. Despite the limitations of optical metallography and the classical direct comparison method, the Rietveld method was successively and accurately applied to determine the volume fractions of all phases. In addition, the Rietveld analysis yielded certain results, such as the crystallographic properties of the phases that can be used to explain the relationship between the microstructural parameters and the wear behavior. Abrasive wear tests with different sliding speeds were carried out on the as-cast and destabilized alloys to identify the effect of microstructural parameters on the wear behavior. The results indicated that the morphologies of secondary carbides, the crystallographic properties of the phases, and the proper combination of the amount of martensite, retained austenite, and carbides were the principle parameters that affect the hardness and wear behavior of the alloy.

  8. c-axis preferential orientation of hydroxyapatite accounts for the high wear resistance of the teeth of black carp (Mylopharyngodon piceus)

    NASA Astrophysics Data System (ADS)

    Fu, Jimin; He, Chong; Xia, Biao; Li, Yan; Feng, Qiong; Yin, Qifang; Shi, Xinghua; Feng, Xue; Wang, Hongtao; Yao, Haimin

    2016-03-01

    Biological armors such as mollusk shells have long been recognized and studied for their values in inspiring novel designs of engineering materials with higher toughness and strength. However, no material is invincible and biological armors also have their rivals. In this paper, our attention is focused on the teeth of black carp (Mylopharyngodon piceus) which is a predator of shelled mollusks like snails and mussels. Nanoscratching test on the enameloid, the outermost layer of the teeth, indicates that the natural occlusal surface (OS) has much higher wear resistance compared to the other sections. Subsequent X-ray diffraction analysis reveals that the hydroxyapatite (HAp) crystallites in the vicinity of OS possess c-axis preferential orientation. The superior wear resistance of black carp teeth is attributed to the c-axis preferential orientation of HAp near the OS since the (001) surface of HAp crystal, which is perpendicular to the c-axis, exhibits much better wear resistance compared to the other surfaces as demonstrated by the molecular dynamics simulation. Our results not only shed light on the origin of the good wear resistance exhibited by the black carp teeth but are of great value to the design of engineering materials with better abrasion resistance.

  9. Transparent, superhydrophobic, and wear-resistant coatings on glass and polymer substrates using SiO2, ZnO, and ITO nanoparticles.

    PubMed

    Ebert, Daniel; Bhushan, Bharat

    2012-08-07

    It is of significant interest to create surfaces that simultaneously exhibit high water contact angle, low contact angle hysteresis, and high transmission of visible light, as well as mechanical wear resistance for industrial applications. The fabrication of such surfaces has often involved complex or expensive processes, required techniques that were not suitable for a variety of substrates and particles, required surface post-treatment, or lacked wear resistance. A systematic study has been performed in which transparent superhydrophobic surfaces were created on glass, polycarbonate, and poly(methyl methacrylate) (PMMA) substrates using surface-functionalized SiO(2), ZnO, and indium tin oxide (ITO) nanoparticles. The contact angle, contact angle hysteresis, and optical transmittance were measured for samples using all particle-substrate combinations. To examine wear resistance, multiscale wear experiments were performed using an atomic force microscope (AFM) and a water jet apparatus.

  10. Application of a stereometric structural analysis for an evaluation of surface and for a forecast of the wear of endoprothesis acetabular cups

    SciTech Connect

    Cybo, Jerzy; Maszybrocka, Joanna . E-mail: jmaszybr@us.edu.pl; Cwajna, Jan

    2006-06-15

    To improve the resistance to wear and permanent deformation of polyethylene operating in a polymer/metal friction couple, initial plastic deformation of the polyethylene and its electron irradiation was applied. This contributed to a change of the polymer structure, visible already while machining when the sample surfaces were being prepared for a tribological test. The study shows that the interactions that shape the structure of polyethylene, at the same time cause adequate changes to the stereometric structure of its surface. The parameters of surface microgeometry characterize the future tribological behavior of polyethylene during its operation in a friction couple. It has been shown that an analysis of stereometric parameters may constitute the first projection of polymer wear resistance.

  11. Sliding Wear and Fretting Wear of DLC-Based, Functionally Graded Nanocomposite Coatings

    NASA Technical Reports Server (NTRS)

    Miyoshi, K.; Pohlchuck, B.; Street, Kenneth W.; Zabinski, J. S.; Sanders, J. H.; Voevodin, A. a.; Wu, R. L. C.

    1999-01-01

    Improving the tribological functionality of diamondlike carbon (DLC) films--developing, good wear resistance, low friction, and high load-carrying capacity-was the aim of this investigation. Nanocomposite coatings consisting of an amorphous DLC (a-DLC) top layer and a functionally graded titanium-titanium carbon-diamondlike carbon (Ti-Ti(sub x) C(sub y)-DLC) underlayer were produced on AISI 440C stainless steel substrates by the hybrid technique of magnetron sputtering and pulsed-laser deposition. The resultant DLC films were characterized by Raman spectroscopy, scanning electron microscopy, and surface profilometry. Two types of wear experiment were conducted in this investioation: sliding friction experiments and fretting wear experiments. Unidirectional ball-on-disk sliding friction experiments were conducted to examine the wear behavior of an a-DLC/Ti-Ti(sub x) C(sub y)-DLC-coated AISI 440C stainless steel disk in sliding contact with a 6-mm-diameter AISI 440C stainless steel ball in ultrahigh vacuum, dry nitrogen, and humid air. Although the wear rates for both the coating and ball were low in all three environments, the humid air and dry nitrogen caused mild wear with burnishing, in the a-DLC top layer, and the ultrahigh vacuum caused relatively severe wear with brittle fracture in both the a-DLC top layer and the Ti-Ti(sub x) C(sub y)-DLC underlayer. For reference, amorphous hydrogenated carbon (H-DLC) films produced on a-DLC/Ti-Ti(sub x) C(sub y)-DLC nanocomposite coatings by using an ion beam were also examined in the same manner. The H-DLC films markedly reduced friction even in ultrahigh vacuum without sacrificing wear resistance. The H-DLC films behaved much like the a-DLC/Ti-Ti(sub x) C(sub y)-DLC nanocomposite coating in dry nitrogen and humid air, presenting low friction and low wear. Fretting wear experiments were conducted in humid air (approximately 50% relative humidity) at a frequency of 80 Hz and an amplitude of 75 micron on an a

  12. Generation of physiological parameter sets for hip joint motions and loads during daily life activities for application in wear simulators of the artificial hip joint.

    PubMed

    Fabry, Christian; Herrmann, Sven; Kaehler, Michael; Klinkenberg, Ernst-Dieter; Woernle, Christoph; Bader, Rainer

    2013-01-01

    At present, wear investigations of total hip replacements are performed in accordance with the ISO standard 14242, which is based on simplified kinematic and force data of the gait cycle. The aim of this analytical study was to generate parameter sets of daily life activities in order to replicate more realistic joint load situations in wear testing. Hence, published in vivo motion and force data of daily life activities were evaluated and adjusted using analytical techniques. The created kinematically and dynamically consistent parameter sets comprised time trajectories of three Cardan angles to describe the motion of the femur with respect to the pelvis and time trajectories of three force components, representing the hip joint contact force. The parameter sets include the activities of walking, knee bending, stair climbing and a combined load case of sitting down and standing up. Additionally, a motion sequence following the frequency of daily life activities was presented. Differences of the evaluated angular motions and joint contact forces in comparison to the ISO standard 14242-1 were pointed out. The results of this study offer the possibility to extend the kinematics and dynamics of the ISO standard test protocol and to support the loading conditions of hip wear simulators with a comprehensive set of motions and loads close to reality. Copyright © 2012 IPEM. Published by Elsevier Ltd. All rights reserved.

  13. Multi technical analysis of wear mechanisms in axial piston pumps

    NASA Astrophysics Data System (ADS)

    Schuhler, G.; Jourani, A.; Bouvier, S.; Perrochat, J.-M.

    2017-05-01

    Axial piston pumps convert a motor rotation motion into hydraulic or pneumatic power. Their compactness and efficiency of approximately 0.9 make them suitable for actuation applications especially in aeronautics. However, they suffer a limited life due to the wear of their components. In the literature, studies of axial piston pumps deal with contact between its different elements under lubrication conditions. Nevertheless, they are more focused on analytic or numerical approaches. This study consists in an experimental analysis of worn pump components to highlight and understand wear mechanisms. Piston shoes are central components in the axial piston pump since they are involved in three tribological contacts. These three contacts are thereby studied: piston shoes/swashplate, piston shoes/pistons and piston shoes/shoes hold down plate (SHDP). To perform this analysis, helicopter hydraulic pumps after different operating times have been studied. The wear damage mechanisms and wear debris are analysed using SEM observations. 3D surface roughness measurements are then used to characterize worn surfaces. The observations reveal that in the contact between shoes and swashplate, the main wear mechanism is three-body abrasive wear due to coarse carbides removal. Between shoes and pistons, wear occurs in a less severe way and is mainly due to the debris generated in the first contact and conveyed by the lubricating fluid. In the third contact, the debris are also the prime cause of the abrasive wear and the generation of deep craters in the piston shoes.

  14. Study of Erosive Wear Behaviour on SIC/SIC Composites

    NASA Astrophysics Data System (ADS)

    Suh, Min-Soo

    In the field of aerospace propulsion system, erosive wear on continuous silicon carbide (SiC) fibre-reinforced SiC (SiC/SiC) composites is of significant issue to achieve high energy efficiency. This paper proposes a crucial factor and a design guideline of SiC/SiC composites for higher erosion performance regarding cost effectiveness. Fabrication and evaluation of impacts and wear on SiC/SiC composites are successfully carried out. Erosive wear behaviours of the CVI and the LPS composites evidently show that the crucial fabrication factor against solid particle erosion (SPE). Erosive wear mechanisms on various SiC/SiC composites are determined based on the analysis of erosive wear behaviour. Designing guideline for the SiC/SiC composites for pursuit of high erosion performance is also proposed as focusing on the followings; volume fraction of matrix, strength of the matrix, bonding strength, and PyC interface.

  15. Wear-caused deflection evolution of a slide rail, considering linear and non-linear wear models

    NASA Astrophysics Data System (ADS)

    Kim, Dongwook; Quagliato, Luca; Park, Donghwi; Murugesan, Mohanraj; Kim, Naksoo; Hong, Seokmoo

    2017-05-01

    The research presented in this paper details an experimental-numerical approach for the quantitative correlation between wear and end-point deflection in a slide rail. Focusing the attention on slide rail utilized in white-goods applications, the aim is to evaluate the number of cycles the slide rail can operate, under different load conditions, before it should be replaced due to unacceptable end-point deflection. In this paper, two formulations are utilized to describe the wear: Archard model for the linear wear and Lemaitre damage model for the nonlinear wear. The linear wear gradually reduces the surface of the slide rail whereas the nonlinear one accounts for the surface element deletion (i.e. due to pitting). To determine the constants to use in the wear models, simple tension test and sliding wear test, by utilizing a designed and developed experiment machine, have been carried out. A full slide rail model simulation has been implemented in ABAQUS including both linear and non-linear wear models and the results have been compared with those of the real rails under different load condition, provided by the rail manufacturer. The comparison between numerically estimated and real rail results proved the reliability of the developed numerical model, limiting the error in a ±10% range. The proposed approach allows predicting the displacement vs cycle curves, parametrized for different loads and, based on a chosen failure criterion, to predict the lifetime of the rail.

  16. Friction and wear performance of boron doped, undoped microcrystalline and fine grained composite diamond films

    NASA Astrophysics Data System (ADS)

    Wang, Xinchang; Wang, Liang; Shen, Bin; Sun, Fanghong

    2015-01-01

    Chemical vapor deposition (CVD) diamond films have attracted more attentions due to their excellent mechanical properties. Whereas as-fabricated traditional diamond films in the previous studies don't have enough adhesion or surface smoothness, which seriously impact their friction and wear performance, and thus limit their applications under extremely harsh conditions. A boron doped, undoped microcrystalline and fine grained composite diamond (BD-UM-FGCD) film is f