The role of fiber and matrix in crash energy absorption of composite materials

NASA Technical Reports Server (NTRS)

Farley, G. L.; Bird, R. K.; Modlin, J. T.

1986-01-01

Static crushing tests were conducted on tube specimens fabricated from graphite/epoxy, Kevlar/epoxy and hybrid combinations of graphite-Kevlar/epoxy to examine the influence the fiber and matrix constitutive properties and laminate architecture have on energy absorption. Fiber and matrix ultimate failure strain were determined to significantly effect energy absorption. The energy absorption capability of high ultimate failure strain materials (AS-6/F185 and AS-6/HST-7) was less than materials having lower ultimate failure strain. Lamina stacking sequence had up to a 300 percent change in energy absorption for the materials tested. Hybridizing with graphite and Kevlar reinforcements resulted in materials with high energy absorption capabilities that have postcrushing integrity.

Self-adaptive strain-relaxation optimization for high-energy lithium storage material through crumpling of graphene.

PubMed

Zhao, Yunlong; Feng, Jiangang; Liu, Xue; Wang, Fengchao; Wang, Lifen; Shi, Changwei; Huang, Lei; Feng, Xi; Chen, Xiyuan; Xu, Lin; Yan, Mengyu; Zhang, Qingjie; Bai, Xuedong; Wu, Hengan; Mai, Liqiang

2014-08-01

High-energy lithium battery materials based on conversion/alloying reactions have tremendous potential applications in new generation energy storage devices. However, these applications are limited by inherent large volume variations and sluggish kinetics. Here we report a self-adaptive strain-relaxed electrode through crumpling of graphene to serve as high-stretchy protective shells on metal framework, to overcome these limitations. The graphene sheets are self-assembled and deeply crumpled into pinecone-like structure through a contraction-strain-driven crumpling method. The as-prepared electrode exhibits high specific capacity (2,165 mAh g(-1)), fast charge-discharge rate (20 A g(-1)) with no capacity fading in 1,000 cycles. This kind of crumpled graphene has self-adaptive behaviour of spontaneous unfolding-folding synchronized with cyclic expansion-contraction volumetric variation of core materials, which can release strain and maintain good electric contact simultaneously. It is expected that such findings will facilitate the applications of crumpled graphene and the self-adaptive materials.

Electrical properties of materials for high temperature strain gage applications

NASA Technical Reports Server (NTRS)

Brittain, John O.

1989-01-01

A study was done on the electrical resistance of materials that are potentially useful as resistance strain gages at high temperatures under static strain conditions. Initially a number of binary alloys were investigated. Later, third elements were added to these alloys, all of which were prepared by arc melting. Several transition metals were selected for experimentation, most prepared as thin films. Difficulties with electrical contacts thwarted efforts to extend measurements to the targeted 1000 C, but results obtained did suggest ways of improving the electrical resistance characteristics of certain materials.

Inferring Strength of Tantalum from Hydrodynamic Instability Recovery Experiments

NASA Astrophysics Data System (ADS)

Sternberger, Z.; Maddox, B.; Opachich, Y.; Wehrenberg, C.; Kraus, R.; Remington, B.; Randall, G.; Farrell, M.; Ravichandran, G.

2018-05-01

Hydrodynamic instability experiments allow access to material properties at extreme conditions, where strain rates exceed 105 s-1 and pressures reach 100 GPa. Current hydrodynamic instability experimental methods require in-flight radiography to image the instability growth at high pressure and high strain rate, limiting the facilities where these experiments can be performed. An alternate approach, recovering the sample after loading, allows measurement of the instability growth with profilometry. Tantalum samples were manufactured with different 2D and 3D initial perturbation patterns and dynamically compressed by a blast wave generated by laser ablation. The samples were recovered from peak pressures between 30 and 120 GPa and strain rates on the order of 107 s-1, providing a record of the growth of the perturbations due to hydrodynamic instability. These records are useful validation points for hydrocode simulations using models of material strength at high strain rate. Recovered tantalum samples were analyzed, providing an estimate of the strength of the material at high pressure and strain rate.

Nonlinear Eulerian Thermoelasticity for Anisotropic Crystals

DTIC Science & Technology

2013-08-01

the applied pressure. However, some crystalline materials such as ceramics and hard minerals may retain significant shear strength at finite strain...which elastic properties have been measured. Benefits of using Eulerian strain measures for nonlinear elasticity of isotropic materials were extolled by...highly symmetric anharmonic properties . Deviations may be expected for highly anisotropic materials , as shown in Section 4. This work is focused

Properties of two composite materials made of toughened epoxy resin and high-strain graphite fiber

NASA Technical Reports Server (NTRS)

Dow, Marvin B.; Smith, Donald L.

1988-01-01

Results are presented from an experimental evaluation of IM7/8551-7 and IM6/18081, two new toughened epoxy resin, high strain graphite fiber composite materials. Data include ply-level strengths and moduli, notched tension and compression strengths and compression-after-impact assessments. The measured properties are compared with those of other graphite-epoxy materials.

Brittle materials at high-loading rates: an open area of research

NASA Astrophysics Data System (ADS)

Forquin, Pascal

2017-01-01

Brittle materials are extensively used in many civil and military applications involving high-strain-rate loadings such as: blasting or percussive drilling of rocks, ballistic impact against ceramic armour or transparent windshields, plastic explosives used to damage or destroy concrete structures, soft or hard impacts against concrete structures and so on. With all of these applications, brittle materials are subjected to intense loadings characterized by medium to extremely high strain rates (few tens to several tens of thousands per second) leading to extreme and/or specific damage modes such as multiple fragmentation, dynamic cracking, pore collapse, shearing, mode II fracturing and/or microplasticity mechanisms in the material. Additionally, brittle materials exhibit complex features such as a strong strain-rate sensitivity and confining pressure sensitivity that justify expending greater research efforts to understand these complex features. Currently, the most popular dynamic testing techniques used for this are based on the use of split Hopkinson pressure bar methodologies and/or plate-impact testing methods. However, these methods do have some critical limitations and drawbacks when used to investigate the behaviour of brittle materials at high loading rates. The present theme issue of Philosophical Transactions A provides an overview of the latest experimental methods and numerical tools that are currently being developed to investigate the behaviour of brittle materials at high loading rates. This article is part of the themed issue 'Experimental testing and modelling of brittle materials at high strain rates'.

Brittle materials at high-loading rates: an open area of research

PubMed Central

2017-01-01

Brittle materials are extensively used in many civil and military applications involving high-strain-rate loadings such as: blasting or percussive drilling of rocks, ballistic impact against ceramic armour or transparent windshields, plastic explosives used to damage or destroy concrete structures, soft or hard impacts against concrete structures and so on. With all of these applications, brittle materials are subjected to intense loadings characterized by medium to extremely high strain rates (few tens to several tens of thousands per second) leading to extreme and/or specific damage modes such as multiple fragmentation, dynamic cracking, pore collapse, shearing, mode II fracturing and/or microplasticity mechanisms in the material. Additionally, brittle materials exhibit complex features such as a strong strain-rate sensitivity and confining pressure sensitivity that justify expending greater research efforts to understand these complex features. Currently, the most popular dynamic testing techniques used for this are based on the use of split Hopkinson pressure bar methodologies and/or plate-impact testing methods. However, these methods do have some critical limitations and drawbacks when used to investigate the behaviour of brittle materials at high loading rates. The present theme issue of Philosophical Transactions A provides an overview of the latest experimental methods and numerical tools that are currently being developed to investigate the behaviour of brittle materials at high loading rates. This article is part of the themed issue ‘Experimental testing and modelling of brittle materials at high strain rates’. PMID:27956517

Brittle materials at high-loading rates: an open area of research.

PubMed

Forquin, Pascal

2017-01-28

Brittle materials are extensively used in many civil and military applications involving high-strain-rate loadings such as: blasting or percussive drilling of rocks, ballistic impact against ceramic armour or transparent windshields, plastic explosives used to damage or destroy concrete structures, soft or hard impacts against concrete structures and so on. With all of these applications, brittle materials are subjected to intense loadings characterized by medium to extremely high strain rates (few tens to several tens of thousands per second) leading to extreme and/or specific damage modes such as multiple fragmentation, dynamic cracking, pore collapse, shearing, mode II fracturing and/or microplasticity mechanisms in the material. Additionally, brittle materials exhibit complex features such as a strong strain-rate sensitivity and confining pressure sensitivity that justify expending greater research efforts to understand these complex features. Currently, the most popular dynamic testing techniques used for this are based on the use of split Hopkinson pressure bar methodologies and/or plate-impact testing methods. However, these methods do have some critical limitations and drawbacks when used to investigate the behaviour of brittle materials at high loading rates. The present theme issue of Philosophical Transactions A provides an overview of the latest experimental methods and numerical tools that are currently being developed to investigate the behaviour of brittle materials at high loading rates.This article is part of the themed issue 'Experimental testing and modelling of brittle materials at high strain rates'. © 2016 The Author(s).

Study on the fabricating process monitoring of thermoplastic based materials packaged OFBG and their sensing properties

NASA Astrophysics Data System (ADS)

Wang, Chuan; Zhou, Zhi; Zhang, Zhichun; Ou, Jinping

2007-04-01

As common materials or engineering materials, thermoplastic resin based materials can be used not only directly fabricating products but also FRTP(fiber reinforced thermoplastic polymer) materials for other uses. As one kind of FRTP material, GFRPP(glass fiber reinforced polypropylene) has lots of merits, such as: light weight, high strength, high tenacity, high elongation percentage, good durability, reshaping character and no environmental pollution characters. And they also can be conveniently formed hoop rebar in civil engineering. While a new kind of GFRPP-OFBG smart rod which combined GFRPP and OFBG together can be used as not only structure materials but also sensing materials. Meanwhile, PP packaged OFBG strain sensor can be expected for its low modulus, good sensitivity and good durability. Furthermore, it can be used for large strain measuring. In this paper, we have successfully fabricated a new kind of GFRPP-OFBG(Glass Fiber Reinforced Polypropylene-Optic Fiber Bragg Grating) rod by our own thermoplastic pultrusion production line and a new kind of PP packaged OFBG strain sensor by extruding techniques. And we monitored the inner strain and temperature changes with tow OFBG simultaneously of the fabricating process. The results show that: OFBG can truly reflect the strain and temperature changes in both the GFRPP rod and the PP packaged OFBG, these are very useful to modify our processing parameters. And we also find that because of the shrinkage of PP, this new kind of PP packaged OFBG have -13000μɛ storage, and the strain sensing performance is still very well, so which can be used for large strain measuring. Besides these, GFRPP-OFBG smart rod has good sensing performance in strain sensing just like that of FRSP-OFBG rod, the strain sensitivity coefficient is about1.19pm/μɛ. Besides these, the surface of GFRPP-OFBG rods can be handled just as steel bars and also can be bended and reshaped. These are all very useful and very important for the use of FRP materials in civil engineering structures.

Experimental Techniques for Evaluating the Effects of Aging on Impact and High Strain Rate Properties of Triaxial Braided Composite Materials

NASA Technical Reports Server (NTRS)

Pereira, J. Michael; Roberts, Gary D.; Ruggeri, Charles R.; Gilat, Amos; Matrka, Thomas

2010-01-01

An experimental program is underway to measure the impact and high strain rate properties of triaxial braided composite materials and to quantify any degradation in properties as a result of thermal and hygroscopic aging typically encountered during service. Impact tests are being conducted on flat panels using a projectile designed to induce high rate deformation similar to that experienced in a jet engine fan case during a fan blade-out event. The tests are being conducted on as-fabricated panels and panels subjected to various numbers of aging cycles. High strain rate properties are being measured using a unique Hopkinson bar apparatus that has a larger diameter than conventional Hopkinson bars. This larger diameter is needed to measure representative material properties because of the large unit cell size of the materials examined in this work. In this paper the experimental techniques used for impact and high strain rate testing are described and some preliminary results are presented for both as-fabricated and aged composites.

Dynamic response of polyurea subjected to nanosecond rise-time stress waves

NASA Astrophysics Data System (ADS)

Youssef, George; Gupta, Vijay

2012-08-01

Shaped charges and explosively formed projectiles used in modern warfare can attain speeds as high as 30,000 ft/s. Impacts from these threats are expected to load the armor materials in the 10 to 100 ns timeframe. During this time, the material strains are quite limited but the strain rates are extremely high. To develop armors against such threats it is imperative to understand the dynamic constitutive behavior of materials in the tens of nanoseconds timeframe. Material behavior in this parameter space cannot be obtained by even the most sophisticated plate-impact and split-Hopkinson bar setups that exist within the high energy materials field today. This paper introduces an apparatus and a test method that are based on laser-generated stress waves to obtain such material behaviors. Although applicable to any material system, the test procedures are demonstrated on polyurea which shows unusual dynamic properties. Thin polyurea layers were deformed using laser-generated stress waves with 1-2 ns rise times and 16 ns total duration. The total strain in the samples was less than 3%. Because of the transient nature of the stress wave, the strain rate varied throughout the deformation history of the sample. A peak value of 1.1×105 s-1 was calculated. It was found that the stress-strain characteristics, determined from experimentally recorded incident and transmitted wave profiles, matched satisfactorily with those computed from a 2D wave mechanics simulation in which the polyurea was modeled as a linearly viscoelastic solid with constants derived from the quasi-static experiments. Thus, the test data conformed to the Time-Temperature Superposition (TTS) principle even at extremely high strain rates of our test. This then extends the previous observations of Zhao et al. (Mech. Time-Depend. Mater. 11:289-308, 2007) who showed the applicability of the TTS principle for polyurea in the linearly viscoelastic regime up to peak strain rates of 1200 s-1.

High strain-rate soft material characterization via inertial cavitation

NASA Astrophysics Data System (ADS)

Estrada, Jonathan B.; Barajas, Carlos; Henann, David L.; Johnsen, Eric; Franck, Christian

2018-03-01

Mechanical characterization of soft materials at high strain-rates is challenging due to their high compliance, slow wave speeds, and non-linear viscoelasticity. Yet, knowledge of their material behavior is paramount across a spectrum of biological and engineering applications from minimizing tissue damage in ultrasound and laser surgeries to diagnosing and mitigating impact injuries. To address this significant experimental hurdle and the need to accurately measure the viscoelastic properties of soft materials at high strain-rates (103-108 s-1), we present a minimally invasive, local 3D microrheology technique based on inertial microcavitation. By combining high-speed time-lapse imaging with an appropriate theoretical cavitation framework, we demonstrate that this technique has the capability to accurately determine the general viscoelastic material properties of soft matter as compliant as a few kilopascals. Similar to commercial characterization algorithms, we provide the user with significant flexibility in evaluating several constitutive laws to determine the most appropriate physical model for the material under investigation. Given its straightforward implementation into most current microscopy setups, we anticipate that this technique can be easily adopted by anyone interested in characterizing soft material properties at high loading rates including hydrogels, tissues and various polymeric specimens.

Detecting strain in birefringent materials using spectral polarimetry

NASA Technical Reports Server (NTRS)

Garner, Harold R. (Inventor); Ragucci, Anthony J. (Inventor); Cisar, Alan J. (Inventor); Huebschman, Michael L. (Inventor)

2010-01-01

A method, computer program product and system for analyzing multispectral images from a plurality of regions of birefringent material, such as a polymer film, using polarized light and a corresponding polar analyzer to identify differential strain in the birefringent material. For example, the birefringement material may be low-density polyethylene (LDPE), high-density polyethylene (HDPE), polypropylene, polyethylene terephthalate (PET), polyvinyl chloride (PVC), polyvinylidene chloride, polyester, nylon, or cellophane film. Optionally, the method includes generating a real-time quantitative strain map.

Total strain version of strainrange partitioning for thermomechanical fatigue at low strains

NASA Technical Reports Server (NTRS)

Halford, G. R.; Saltsman, J. F.

1987-01-01

A new method is proposed for characterizing and predicting the thermal fatigue behavior of materials. The method is based on three innovations in characterizing high temperature material behavior: (1) the bithermal concept of fatigue testing; (2) advanced, nonlinear, cyclic constitutive models; and (3) the total strain version of traditional strainrange partitioning.

Material approaches to stretchable strain sensors.

PubMed

Park, Jaeyoon; You, Insang; Shin, Sangbaie; Jeong, Unyong

2015-04-27

With the recent progress made in wearable electronics, devices now require high flexibility and stretchability up to large strain levels (typically larger than 30 % strain). Wearable strain sensors or deformable strain sensors have been gaining increasing research interest because of the rapid development of electronic skins and robotics and because of their biomedical applications. Conventional brittle strain sensors made of metals and piezoresistors are not applicable for such stretchable sensors. This Review summarizes recent advances in stretchable sensors and focuses on material aspects for high stretchability and sensitivity. It begins with a brief introduction to the Wheatstone bridge circuit of conventional resistive strain sensors. Then, studies on the manipulation of materials are reviewed, including waved structural approaches for making metals and semiconductors stretchable, the use of liquid metals, and conductive filler/elastomer composites by using percolation among the fillers. For capacitive strain sensors, the constant conductivity of the electrode is a key factor in obtaining reliable sensors. Possible approaches to developing capacitive strain sensors are presented. This Review concludes with a discussion on the major challenges and perspectives related to stretchable strain sensors. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Biologically inspired crack delocalization in a high strain-rate environment.

PubMed

Knipprath, Christian; Bond, Ian P; Trask, Richard S

2012-04-07

Biological materials possess unique and desirable energy-absorbing mechanisms and structural characteristics worthy of consideration by engineers. For example, high levels of energy dissipation at low strain rates via triggering of crack delocalization combined with interfacial hardening by platelet interlocking are observed in brittle materials such as nacre, the iridescent material in seashells. Such behaviours find no analogy in current engineering materials. The potential to mimic such toughening mechanisms on different length scales now exists, but the question concerning their suitability under dynamic loading conditions and whether these mechanisms retain their energy-absorbing potential is unclear. This paper investigates the kinematic behaviour of an 'engineered' nacre-like structure within a high strain-rate environment. A finite-element (FE) model was developed which incorporates the pertinent biological design features. A parametric study was carried out focusing on (i) the use of an overlapping discontinuous tile arrangement for crack delocalization and (ii) application of tile waviness (interfacial hardening) for improved post-damage behaviour. With respect to the material properties, the model allows the permutation and combination of a variety of different material datasets. The advantage of such a discontinuous material shows notable improvements in sustaining high strain-rate deformation relative to an equivalent continuous morphology. In the case of the continuous material, the shockwaves propagating through the material lead to localized failure while complex shockwave patterns are observed in the discontinuous flat tile arrangement, arising from platelet interlocking. The influence of the matrix properties on impact performance is investigated by varying the dominant material parameters. The results indicate a deceleration of the impactor velocity, thus delaying back face nodal displacement. A final series of FE models considered the identification of an optimized configuration as a function of tile waviness and matrix properties. In the combined model, the optimized configuration was capable of stopping the ballistic threat, thus indicating the potential for bioinspired toughened synthetic systems to defeat high strain-rate threats.

Biologically inspired crack delocalization in a high strain-rate environment

PubMed Central

Knipprath, Christian; Bond, Ian P.; Trask, Richard S.

2012-01-01

Biological materials possess unique and desirable energy-absorbing mechanisms and structural characteristics worthy of consideration by engineers. For example, high levels of energy dissipation at low strain rates via triggering of crack delocalization combined with interfacial hardening by platelet interlocking are observed in brittle materials such as nacre, the iridescent material in seashells. Such behaviours find no analogy in current engineering materials. The potential to mimic such toughening mechanisms on different length scales now exists, but the question concerning their suitability under dynamic loading conditions and whether these mechanisms retain their energy-absorbing potential is unclear. This paper investigates the kinematic behaviour of an ‘engineered’ nacre-like structure within a high strain-rate environment. A finite-element (FE) model was developed which incorporates the pertinent biological design features. A parametric study was carried out focusing on (i) the use of an overlapping discontinuous tile arrangement for crack delocalization and (ii) application of tile waviness (interfacial hardening) for improved post-damage behaviour. With respect to the material properties, the model allows the permutation and combination of a variety of different material datasets. The advantage of such a discontinuous material shows notable improvements in sustaining high strain-rate deformation relative to an equivalent continuous morphology. In the case of the continuous material, the shockwaves propagating through the material lead to localized failure while complex shockwave patterns are observed in the discontinuous flat tile arrangement, arising from platelet interlocking. The influence of the matrix properties on impact performance is investigated by varying the dominant material parameters. The results indicate a deceleration of the impactor velocity, thus delaying back face nodal displacement. A final series of FE models considered the identification of an optimized configuration as a function of tile waviness and matrix properties. In the combined model, the optimized configuration was capable of stopping the ballistic threat, thus indicating the potential for bioinspired toughened synthetic systems to defeat high strain-rate threats. PMID:21880614

Dynamic Tensile Properties of Iron and Steels for a Wide Range of Strain Rates and Strain

NASA Astrophysics Data System (ADS)

Kojima, Nobusato; Hayashi, Hiroyuki; Yamamoto, Terumi; Mimura, Koji; Tanimura, Shinji

The tensile stress-strain curves of iron and a variety of steels, covering a wide range of strength level, over a wide strain rate range on the order of 10-3 ~ 103 s-1, were obtained systematically by using the Sensing Block Type High Speed Material Testing System (SBTS, Saginomiya). Through intensive analysis of these results, the strain rate sensitivity of the flow stress for the large strain region, including the viscous term at high strain rates, the true fracture strength and the true fracture strain were cleared for the material group of the ferrous metals. These systematical data may be useful to develop a practical constitutive model for computer codes, including a fracture criterion for simulations of the dynamic behavior in crash worthiness studies and of work-pieces subjected to dynamic plastic working for a wide strain rate range.

Physical nature of strain rate sensitivity of metals and alloys at high strain rates

NASA Astrophysics Data System (ADS)

Borodin, E. N.; Gruzdkov, A. A.; Mayer, A. E.; Selyutina, N. S.

2018-04-01

The role of instabilities of plastic flow at plastic deformation of various materials is one of the important cross-disciplinary problems which is equally important in physics, mechanics and material science. The strain rate sensitivities under slow and high strain rate conditions of loading have different physical nature. In the case of low strain rate, the sensitivity arising from the inertness of the defect structures evolution can be expressed by a single parameter characterizing the plasticity mechanism. In our approach, this is the value of the characteristic relaxation time. In the dynamic case, there are additional effects of “high-speed sensitivity” associated with the micro-localization of the plastic flow near the stress concentrators. In the frames of mechanical description, this requires to introduce additional strain rate sensitivity parameters, which is realized in numerous modifications of Johnson–Cook and Zerilli–Armstrong models. The consideration of both these factors is fundamental for an adequate description of the problems of dynamic deformation of highly inhomogeneous metallic materials such as steels and alloys. The measurement of the dispersion of particle velocities on the free surface of a shock-loaded material can be regarded as an experimental expression of the effect of micro-localization. This is also confirmed by our results of numerical simulation of the propagation of shock waves in a two-dimensional formulation and analytical estimations.

Use of simulated experiments for material characterization of brittle materials subjected to high strain rate dynamic tension

PubMed Central

Saletti, Dominique

2017-01-01

Rapid progress in ultra-high-speed imaging has allowed material properties to be studied at high strain rates by applying full-field measurements and inverse identification methods. Nevertheless, the sensitivity of these techniques still requires a better understanding, since various extrinsic factors present during an actual experiment make it difficult to separate different sources of errors that can significantly affect the quality of the identified results. This study presents a methodology using simulated experiments to investigate the accuracy of the so-called spalling technique (used to study tensile properties of concrete subjected to high strain rates) by numerically simulating the entire identification process. The experimental technique uses the virtual fields method and the grid method. The methodology consists of reproducing the recording process of an ultra-high-speed camera by generating sequences of synthetically deformed images of a sample surface, which are then analysed using the standard tools. The investigation of the uncertainty of the identified parameters, such as Young's modulus along with the stress–strain constitutive response, is addressed by introducing the most significant user-dependent parameters (i.e. acquisition speed, camera dynamic range, grid sampling, blurring), proving that the used technique can be an effective tool for error investigation. This article is part of the themed issue ‘Experimental testing and modelling of brittle materials at high strain rates’. PMID:27956505

Large strain dynamic compression for soft materials using a direct impact experiment

NASA Astrophysics Data System (ADS)

Meenken, T.; Hiermaier, S.

2006-08-01

Measurement of strain rate dependent material data of low density low strength materials like polymeric foams and rubbers still poses challenges of a different kind to the experimental set up. For instance, in conventional Split Hopkinson Pressure Bar tests the impedance mismatch between the bars and the specimen makes strain measurement almost impossible. Application of viscoelastic bars poses new problems with wave dispersion. Also, maximum achievable strains and strain rates depend directly on the bar lengths, resulting in large experimental set ups in order to measure relevant data for automobile crash applications. In this paper a modified SHPB will be presented for testing low impedance materials. High strains can be achieved with nearly constant strain rate. A thin film stress measurement has been applied to the specimen/bar interfaces to investigate the initial sample ring up process. The process of stress homogeneity within the sample was investigated on EPDM and PU rubber.

High strain rate behavior of a SiC particulate reinforced Al{sub 2}O{sub 3} ceramic matrix composite

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hall, I.W.; Guden, M.

The high strain rate deformation behavior of composite materials is important for several reasons. First, knowledge of the mechanical properties of composites at high strain rates is needed for designing with these materials in applications where sudden changes in loading rates are likely to occur. Second, knowledge of both the dynamic and quasi-static mechanical responses can be used to establish the constitutive equations which are necessary to increase the confidence limits of these materials, particularly if they are to be used in critical structural applications. Moreover, dynamic studies and the knowledge gained form them are essential for the further developmentmore » of new material systems for impact applications. In this study, the high strain rate compressive deformation behavior of a ceramic matrix composite (CMC) consisting of SiC particles and an Al{sub 2}O{sub 3} matrix was studied and compared with its quasi-static behavior. Microscopic observations were conducted to investigate the deformation and fracture mechanism of the composite.« less

High temperature static strain measurement with an electrical resistance strain gage

NASA Technical Reports Server (NTRS)

Lei, Jih-Fen

1992-01-01

An electrical resistance strain gage that can supply accurate static strain measurement for NASP application is being developed both in thin film and fine wire forms. This gage is designed to compensate for temperature effects on substrate materials with a wide range of thermal expansion coefficients. Some experimental results of the wire gage tested on one of the NASP structure materials, i.e., titanium matrix composites, are presented.

High Throughput Assay for Bacterial Adhesion on Acellular Dermal Matrices and Synthetic Surgical Materials

PubMed Central

Nyame, Theodore T.; Lemon, Katherine P.; Kolter, Roberto; Liao, Eric C.

2013-01-01

Background There has been increasing use of various synthetic and biologically derived materials in surgery. Biologic surgical materials are used in many plastic surgery procedures, ranging from breast reconstruction to hernia repairs. In particular, acellular dermal matrix (ADM) material has gained popularity in these applications. There is a paucity of data on how ADM compares to other surgical materials as a substrate for bacterial adhesion, the first step in formation biofilm, which occurs in prosthetic wound infections. We have designed a high throughput assay to evaluate Staphylococcus aureus adherence on various synthetic and biologically derived materials. Methods Clinical isolates of Staphylococcus aureus (strains SC-1 and UAMS-1) were cultured with different materials and bacterial adherence was measured using a resazurin cell vitality reporter microtiter assay. Four materials that are commonly utilized in reconstructive procedures were evaluated: prolene mesh, vicryl mesh, and two different ADM preparations (AlloDerm®, FlexHD®). We were able to develop a high throughput and reliable assay for quantifying bacterial adhesion on synthetic and biologically derived materials. Results The resazurin vitality assay can be reliably used to quantify bacterial adherence to acellular dermal matrix material, as well as synthetic material. S. aureus strains SC-1 and UAMS-1 both adhered better to ADM materials (AlloDerm® vs. FlexHD®) than to the synthetic material prolene. S. aureus also adhered better to vicryl than to prolene. Strain UAMS-1 adhered better to vicryl and ADM materials than did strain SC-1. Conclusion Our results suggest that S. aureus adheres more readily to ADM material than to synthetic material. We have developed an assay to rapidly test bacterial formation on surgical materials, using two S. aureus bacterial strains. This provides a standard method to evaluate existing and new materials with regard to bacterial adherence and potential propensity for infection. This assay is particularly important in the clinical context of the severe sequelae of post-operative infection. PMID:22030489

Highly Sensitive and Very Stretchable Strain Sensor Based on a Rubbery Semiconductor.

PubMed

Kim, Hae-Jin; Thukral, Anish; Yu, Cunjiang

2018-02-07

There is a growing interest in developing stretchable strain sensors to quantify the large mechanical deformation and strain associated with the activities for a wide range of species, such as humans, machines, and robots. Here, we report a novel stretchable strain sensor entirely in a rubber format by using a solution-processed rubbery semiconductor as the sensing material to achieve high sensitivity, large mechanical strain tolerance, and hysteresis-less and highly linear responses. Specifically, the rubbery semiconductor exploits π-π stacked poly(3-hexylthiophene-2,5-diyl) nanofibrils (P3HT-NFs) percolated in silicone elastomer of poly(dimethylsiloxane) to yield semiconducting nanocomposite with a large mechanical stretchability, although P3HT is a well-known nonstretchable semiconductor. The fabricated strain sensors exhibit reliable and reversible sensing capability, high gauge factor (gauge factor = 32), high linearity (R 2 > 0.996), and low hysteresis (degree of hysteresis <12%) responses at the mechanical strain of up to 100%. A strain sensor in this format can be scalably manufactured and implemented as wearable smart gloves. Systematic investigations in the materials design and synthesis, sensor fabrication and characterization, and mechanical analysis reveal the key fundamental and application aspects of the highly sensitive and very stretchable strain sensors entirely from rubbers.

Structure/property development in aPET during large strain, solid phase polymer processing

NASA Astrophysics Data System (ADS)

Martin, Peter; Mohamed, Raja Roslan Raja

2015-12-01

Amorphous Polyethylene terephthalate (aPET) is increasingly of interest for the polymer packaging industry due to its blend of excellent mechanical properties and most importantly its ease of recyclability. Among the major commercial polymers it is almost unique in the degree of improvement in mechanical properties that can be obtained through process-induced strain. For many years these unique properties have been very successfully exploited in the injection stretch blow molding process, where it is deliberately stretched to very large strains using extremely high pressures. However, the material is now also being used in much lower pressure processes such as thermoforming where its properties are often not fully exploited. In this work the change in structure and properties of aPET with strain is systematically investigated using a high speed biaxial stretching machine. The aim was to demonstrate how the properties of the material could be controlled by large strain, high temperature biaxial stretching processes such as thermoforming and blow molding. The results show that property changes in the material are driven by orientation and the onset of rapid strain hardening at large strains. This in turn is shown to vary strongly with process-induced parameters such as the strain rate and the mode and magnitude of biaxial deformation.

3D printing of highly elastic strain sensors using polyurethane/multiwall carbon nanotube composites

NASA Astrophysics Data System (ADS)

Christ, Josef F.; Hohimer, Cameron J.; Aliheidari, Nahal; Ameli, Amir; Mo, Changki; Pötschke, Petra

2017-04-01

As the desire for wearable electronics increases and the soft robotics industry advances, the need for novel sensing materials has also increased. Recently, there have been many attempts at producing novel materials, which exhibit piezoresistive behavior. However, one of the major shortcomings in strain sensing technologies is in the fabrication of such sensors. While there is significant research and literature covering the various methods for developing piezoresistive materials, fabricating complex sensor platforms is still a manufacturing challenge. Here, we report a facile method to fabricate multidirectional embedded strain sensors using additive manufacturing technology. Pure thermoplastic polyurethane (TPU) and TPU/multiwall carbon nanotubes (MWCNT) nanocomposites were 3D printed in tandem using a low-cost multi-material FDM printer to fabricate uniaxial and biaxial strain sensors with conductive paths embedded within the insulative TPU platform. The sensors were then subjected to a series of cyclic strain loads. The results revealed excellent piezoresistive responses of the sensors with cyclic repeatability in both the axial and transverse directions and in response to strains as high as 50%. Further, while strain-softening did occur in the embedded printed strain sensors, it was predictable and similar to the results found in the literature for bulk polymer nanocomposites. This works demonstrates the possibility of manufacturing embedded and multidirectional flexible strain sensors using an inexpensive and versatile method, with potential applications in soft robotics and flexible electronics and health monitoring.

Computational Simulation of the High Strain Rate Tensile Response of Polymer Matrix Composites

NASA Technical Reports Server (NTRS)

Goldberg, Robert K.

2002-01-01

A research program is underway to develop strain rate dependent deformation and failure models for the analysis of polymer matrix composites subject to high strain rate impact loads. Under these types of loading conditions, the material response can be highly strain rate dependent and nonlinear. State variable constitutive equations based on a viscoplasticity approach have been developed to model the deformation of the polymer matrix. The constitutive equations are then combined with a mechanics of materials based micromechanics model which utilizes fiber substructuring to predict the effective mechanical and thermal response of the composite. To verify the analytical model, tensile stress-strain curves are predicted for a representative composite over strain rates ranging from around 1 x 10(exp -5)/sec to approximately 400/sec. The analytical predictions compare favorably to experimentally obtained values both qualitatively and quantitatively. Effective elastic and thermal constants are predicted for another composite, and compared to finite element results.

Strain rate effects on the mechanical behavior of two Dual Phase steels in tension

NASA Astrophysics Data System (ADS)

Cadoni, E.; Singh, N. K.; Forni, D.; Singha, M. K.; Gupta, N. K.

2016-05-01

This paper presents an experimental investigation on the strain rate sensitivity of Dual Phase steel 1200 (DP1200) and Dual Phase steel 1400 (DP1400) under uni-axial tensile loads in the strain rate range from 0.001 s-1 to 600 s-1. These materials are advanced high strength steels (AHSS) having high strength, high capacity to dissipate crash energy and high formability. Flat sheet specimens of the materials having gauge length 10 mm, width 4 mm and thickness 2 mm (DP1200) and 1.25 mm (DP1400), are tested at room temperature (20∘C) on electromechanical universal testing machine to obtain their stress-strain relation under quasi-static condition (0.001 s-1), and on Hydro-Pneumatic machine and modified Hopkinson bar to study their mechanical behavior at medium (3 s-1, and 18 s-1) and high strain rates (200 s-1, 400 s-1, and 600 s-1) respectively. Tests under quasi-static condition are performed at high temperature (200∘C) also, and found that tensile flow stress is a increasing function of temperature. The stress-strain data has been analysed to determine the material parameters of the Cowper-Symonds and the Johnson-Cook models. A simple modification of the Johnson-Cook model has been proposed in order to obtain a better fit of tests at high temperatures. Finally, the fractographs of the broken specimens are taken by scanning electron microscope (SEM) to understand the fracture mechanism of these advanced high strength steels at different strain rates.

An Investigation of a Vertical Test Method for Large Deformation Bending of High Strain Composite Laminates

NASA Astrophysics Data System (ADS)

Herrmann, Kelsey M.

Research to date indicates that traditional composite material failure analysis methods are not appropriate for thin laminates in flexure. Thin composite structures subjected to large bending deformations often attain significantly higher strain-to-failure than previously anticipated tensile and compression coupon test data and linear material model assumption predict. At NASA Langley Research Center, a new bend test method is being developed for High Strain Composite (HSC) structures. This method provides an adequate approximation of a pure moment, large deformation bend test for thin-ply, high strain composites to analyze the large strain flexure response of the laminates. The objective of this research was to further develop this new test method to measure the true bending stiffness and strain-to-failure of high strain composite materials. Of primary importance is the ability to characterize composite laminates that are of interest for current NASA deployable structures in both materials and layups. Two separate testing campaigns were performed for the development of the testing procedure. Initially six laminates were bend tested in three different fiber orientations. These laminates were some combination of unidirectional intermediate modulus (IM) carbon, high tenacity (HT) carbon plain weave, and astroquartz plain weave composite materials. The second test campaign was performed as a more detailed look into the simplest composite laminates at thicknesses that better represented deployable boom structures. The second campaign tested three basic, thinner laminates, again in three different fiber orientations. All testing was monotonic loading to failure. The thickness of the laminates tested ranged from 0.166mm (campaign 2) to 0.45mm (campaign 1). The measured strains at failure for the unidirectional material were approximately 2.1% and 1.4% at the compression and tension sides, respectively, failing as fiber tensile fracture. Both of these values differ from what would be expected from considering much thicker coupons tested under pure compression and tension, that show a strain-to-failure of 1.0-1.1% and 1.6-1.7%, respectively. The significant differences in strain values obtained at the outer surfaces of the coupon is thought to be related to the shift in neutral axis that the specimen experiences during the large deformation bending test as a result of fiber material nonlinearities at higher strains. The vertical test nature of the CBT when compared to other test methods proves to be helpful for visually capturing with Digital Image Correlation the distinct behavior of the flexure on both the compressive and tensile sides. It was found that the thinner the laminate tested, the more confirmation of a nonlinear response of this classification of composites. The moment versus curvature curves were predominantly nonlinear resulting in a near linear bending stiffness versus curvature response. At these large strains, carbon fibers are highly nonlinear resulting in the laminate flexure modulus increasing by up to 5x. The theoretical bending stiffness values calculated using Classical Lamination Theory analysis are within small differences with respect to the experimentally measured values: errors of approximately 5-10% for both D11 and D22. The error between the finite element model computed strain response and the experimental values was on average around 22%, with 35% of the laminates and orientation having errors less than 7%. Comparison between CLT, FEA, and experimentation show that the Column Bend Test appears to be a promising candidate for characterization of large deformation bending behavior of thin-ply high strain composite laminates.

Enhanced tolerance to stretch-induced performance degradation of stretchable MnO2-based supercapacitors.

PubMed

Huang, Yan; Huang, Yang; Meng, Wenjun; Zhu, Minshen; Xue, Hongtao; Lee, Chun-Sing; Zhi, Chunyi

2015-02-04

The performance of many stretchable electronics, such as energy storage devices and strain sensors, is highly limited by the structural breakdown arising from the stretch imposed. In this article, we focus on a detailed study on materials matching between functional materials and their conductive substrate, as well as enhancement of the tolerance to stretch-induced performance degradation of stretchable supercapacitors, which are essential for the design of a stretchable device. It is revealed that, being widely utilized as the electrode material of the stretchable supercapacitor, metal oxides such as MnO2 nanosheets have serious strain-induced performance degradation due to their rigid structure. In comparison, with conducting polymers like a polypyrrole (PPy) film as the electrochemically active material, the performance of stretchable supercapacitors can be well preserved under strain. Therefore, a smart design is to combine PPy with MnO2 nanosheets to achieve enhanced tolerance to strain-induced performance degradation of MnO2-based supercapacitors, which is realized by fabricating an electrode of PPy-penetrated MnO2 nanosheets. The composite electrodes exhibit a remarkable enhanced tolerance to strain-induced performance degradation with well-preserved performance over 93% under strain. The detailed morphology and electrochemical impedance variations are investigated for the mechanism analyses. Our work presents a systematic investigation on the selection and matching of electrode materials for stretchable supercapacitors to achieve high performance and great tolerance to strain, which may guide the selection of functional materials and their substrate materials for the next-generation of stretchable electronics.

Suggested Procedures for Installing Strain Gauges on Langley Research Center Wind Tunnel Balances, Custom Force Measuring Transducers, Metallic and Composite Structural Test Articles

NASA Technical Reports Server (NTRS)

Moore, Thomas C., Sr.

2004-01-01

The character of force and strain measurement testing at LaRC is such that the types of strain gauge installations, the materials upon which the strain gauges are applied, and the test environments encountered, require many varied approaches. In 1997, a NASA Technical Memorandum (NASA TM 110327) was generated to provide the strain gauge application specialist with a listing of recommended procedures for strain gauging various transducers and test articles at LaRC. The technical memorandum offered here is an effort to keep the strain gauge user informed of new technological enhancements in strain-gauging methodology while preserving the strain-gauging guidelines set forth in the 1997 TM. This document provides detailed recommendations for strain gauging LaRC-designed balances and custom transducers, composite materials, cryogenic and high-temperature test articles, and selected non-typical or unique materials or test conditions. Additionally, one section offers details for installing Bragg-Grating type fiber-optic strain sensors for non-typical test scenarios.

The effect of strain rate on the evolution of microstructure in aluminium alloys.

PubMed

Leszczyńska-Madej, B; Richert, M

2010-03-01

Intensive deformations influence strongly microstructure. The very well-known phenomenon is the diminishing dimension of grain size by the severe plastic deformation (SPD) methods. The nanometric features of microstructure were discovered after the SPD deformation of various materials, such as aluminium alloys, iron and others. The observed changes depended on the kind of the deformed material, amount of deformation, strain rate, existence of different phases and stacking fault energy. The influence of the strain and strain rate on the microstructure is commonly investigated nowadays. It was found that the high strain rates activate deformation in shear bands, microbands and adiabatic shear bands. It was observed that bands were places of the nucleation of nanograins in the material deformed by SPD methods. In the work, the refinement of microstructure of the aluminium alloys influenced by the high strain rate was investigated. The samples were compressed by a specially designed hammer to the deformation of phi= 0/0.62 with the strain rate in the range of [Formula in text]. The highest reduction of microbands width with the increase of the strain was found in the AlCu4Zr alloy. The influence of the strain rate on the microstructure refinement indicated that the increase of the strain rate caused the reduction of the microbands width in the all investigated materials (Al99.5, AlCu4Zr, AlMg5, AlZn6Mg2.5CuZr). A characteristic feature of the microstructure of the compressed material was large density of the shear bands and microbands. It was found that the microbands show a large misorientation to the surrounds and, except Al99.5, the large density of dislocation.

Investigation of a Coupled Arrhenius-Type/Rossard Equation of AH36 Material.

PubMed

Qin, Qin; Tian, Ming-Liang; Zhang, Peng

2017-04-13

High-temperature tensile testing of AH36 material in a wide range of temperatures (1173-1573 K) and strain rates (10 -4 -10 -2 s -1 ) has been obtained by using a Gleeble system. These experimental stress-strain data have been adopted to develop the constitutive equation. The constitutive equation of AH36 material was suggested based on the modified Arrhenius-type equation and the modified Rossard equation respectively. The results indicate that the constitutive equation is strongly influenced by temperature and strain, especially strain. Moreover, there is a good agreement between the predicted data of the modified Arrhenius-type equation and the experimental results when the strain is greater than 0.02. There is also good agreement between the predicted data of the Rossard equation and the experimental results when the strain is less than 0.02. Therefore, a coupled equation where the modified Arrhenius-type equation and Rossard equation are combined has been proposed to describe the constitutive equation of AH36 material according to the different strain values in order to improve the accuracy. The correlation coefficient between the computed and experimental flow stress data was 0.998. The minimum value of the average absolute relative error shows the high accuracy of the coupled equation compared with the two modified equations.

Methods of producing strain in a semiconductor waveguide and related devices

DOEpatents

Cox, Johathan Albert; Rakich, Peter Thomas

2016-02-16

Quasi-phase matched (QPM), semiconductor photonic waveguides include periodically-poled alternating first and second sections. The first sections exhibit a high degree of optical coupling (abbreviated "X.sup.2"), while the second sections have a low X.sup.2. The alternating first and second sections may comprise high-strain and low-strain sections made of different material states (such as crystalline and amorphous material states) that exhibit high and low X.sup.2 properties when formed on a particular substrate, and/or strained corrugated sections of different widths. The QPM semiconductor waveguides may be implemented as silicon-on-insulator (SOI), or germanium-on-silicon structures compatible with standard CMOS processes, or as silicon-on-sapphire (SOS) structures.

Thermal Output of WK-Type Strain Gauges on Various Materials at Cryogenic and Elevated Temperatures

NASA Technical Reports Server (NTRS)

Kowalkowski, Matthew K.; Rivers, H. Kevin; Smith, Russell W.

1998-01-01

Strain gage apparent strain (thermal output) is one of the largest sources of error associated with the measurement of strain when temperatures and mechanical loads are varied. In this paper, experimentally determined apparent strains of WK-type strain gages, installed on both metallic and composite-laminate materials of various lay-ups and resin systems for temperatures ranging from -450 F to 230 F are presented. For the composite materials apparent strain in both the 0 ply orientation angle and the 90 ply orientation angle were measured. Metal specimens tested included: aluminum-lithium alloy (Al-LI 2195-T87), aluminum alloy (Al 2219-T87), and titanium alloy. Composite materials tested include: graphite-toughened-epoxy (IM7/997- 2), graphite-bismaleimide (IM7/5260), and graphite-K3 (IM7/K3B). The experimentally determined apparent strain data are curve fit with a fourth-order polynomial for each of the materials studied. The apparent strain data and the polynomials that are fit to the data are compared with those produced by the strain gage manufacturer, and the results and comparisons are presented. Unacceptably high errors between the manufacture's data and the experimentally determined data were observed (especially at temperatures below - 270-F).

Non-Destructive Measurement of Residual Strain in Connecting Rods Using Neutrons

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ikeda, Tomohiro; Bunn, Jeffrey R.; Fancher, Christopher M.

Increasing the strength of materials is effective in reducing weight and boosting structural part performance, but there are cases in where the residual strain generated during the process of manufacturing of high-strength materials results in a decline of durability. It is therefore important to understand how the residual strain in a manufactured component changes due to processing conditions. In the case of a connecting rod, because the strain load on the connecting rod rib sections is high, it is necessary to clearly understand the distribution of strain in the ribs. However, because residual strain is generally measured by using X-raymore » diffractometers or strain gauges, measurements are limited to the surface layer of the parts. Neutron beams, however, have a higher penetration depth than X-rays, allowing for strain measurement in the bulk material. The research discussed within this paper consists of non-destructive residual strain measurements in the interior of connecting rods using the 2nd Generation Neutron Residual Stress Mapping Facility (NRSF2) at Oak Ridge National Laboratory, measuring the Fe (211) diffraction peak position of the ferrite phase. The interior strain distribution of connecting rod, which prepared under different manufacturing processes, was revealed. By the visualization of interior strains, clear understandings of differences in various processing conditions were obtained. In addition, it is known that the peak width, which is also obtained during measurement, is suggestive of the size of crystallites in the structure; however the peak width can additionally be caused by microstresses and material dislocations.« less

Combination of Universal Mechanical Testing Machine with Atomic Force Microscope for Materials Research

PubMed Central

Zhong, Jian; He, Dannong

2015-01-01

Surface deformation and fracture processes of materials under external force are important for understanding and developing materials. Here, a combined horizontal universal mechanical testing machine (HUMTM)-atomic force microscope (AFM) system is developed by modifying UMTM to combine with AFM and designing a height-adjustable stabilizing apparatus. Then the combined HUMTM-AFM system is evaluated. Finally, as initial demonstrations, it is applied to analyze the relationship among macroscopic mechanical properties, surface nanomorphological changes under external force, and fracture processes of two kinds of representative large scale thin film materials: polymer material with high strain rate (Parafilm) and metal material with low strain rate (aluminum foil). All the results demonstrate the combined HUMTM-AFM system overcomes several disadvantages of current AFM-combined tensile/compression devices including small load force, incapability for large scale specimens, disability for materials with high strain rate, and etc. Therefore, the combined HUMTM-AFM system is a promising tool for materials research in the future. PMID:26265357

Combination of Universal Mechanical Testing Machine with Atomic Force Microscope for Materials Research.

PubMed

Zhong, Jian; He, Dannong

2015-08-12

Surface deformation and fracture processes of materials under external force are important for understanding and developing materials. Here, a combined horizontal universal mechanical testing machine (HUMTM)-atomic force microscope (AFM) system is developed by modifying UMTM to combine with AFM and designing a height-adjustable stabilizing apparatus. Then the combined HUMTM-AFM system is evaluated. Finally, as initial demonstrations, it is applied to analyze the relationship among macroscopic mechanical properties, surface nanomorphological changes under external force, and fracture processes of two kinds of representative large scale thin film materials: polymer material with high strain rate (Parafilm) and metal material with low strain rate (aluminum foil). All the results demonstrate the combined HUMTM-AFM system overcomes several disadvantages of current AFM-combined tensile/compression devices including small load force, incapability for large scale specimens, disability for materials with high strain rate, and etc. Therefore, the combined HUMTM-AFM system is a promising tool for materials research in the future.

On the cyclic stress-strain behavior and low cycle fatigue of aerospace materials

NASA Technical Reports Server (NTRS)

Burbach, J.

1972-01-01

The elastic-plastic deformation behavior under cyclic stress of a number of different engineering materials was experimentally investigated with the aid of high-precision methods of measuring, some of which had been newly developed. Experiments made with a variety of steels, the titanium alloy Ti-A16-V4, a cobalt (tungsten) alloy, the high-temperature material Nimonic 90 and Dural (A1-Cu) are reported. The theory given in an attempt to explain these experiments is aimed at finding general formulas for the cyclic stress-strain behavior materials.

Recommended Strain Gage Application Procedures for Various Langley Research Center Balances and Test Articles

NASA Technical Reports Server (NTRS)

Moore, Thomas C., Sr.

1997-01-01

The NASA Langley Research Center uses more than 10000 strain gages per year in supporting its various research programs. The character of the testing at LaRC is such that the types of strain gage installations, the materials they are applied to, and the test environments encountered, require many varied approaches for installing strain gages. These installations must be accomplished in the most technically discerning and appropriate manner. This technical memorandum is offered as an assisting guide in helping the strain gage user to determine the appropriate approach for a given strain gage application requirement. Specifically, this document offers detailed recommendations for strain gaging the following: LaRC-Designed balances, LARC custom transducers, certain composite materials and alloys, high-temperature test articles, and selected non-typical or unique materials or test conditions.

The influence of matrix microstructure

NASA Astrophysics Data System (ADS)

Vyletel, G. M.; Allison, J. E.; Aken, D. C.

1993-11-01

The low-cycle and high-cycle fatigue behavior and cyclic response of naturally aged and artificially aged 2219/TiC/15p and unreinforced 2219 Al were investigated utilizing plastic strain-controlled and stress-controlled testing. The cyclic response of both the reinforced and un-reinforced materials was similar for all plastic strain amplitudes tested except that the saturation stress level for the composite was always greater than that of the unreinforced material. The cyclic response of the naturally aged materials exhibited cyclic hardening and, in some cases, cyclic softening, while the cyclic response for the artificially aged materials showed no evidence of either cyclic hardening or softening. The higher ductility of the unreinforced material made it more resistant to fatigue failure at high strains, and thus, at a given plastic strain, it had longer fatigue life. It should be noted that the tensile ductilities of the 2219/TiC/15p were significantly higher than those previously reported for 2XXX-series composites. During stress-controlled test-ing at stresses below 220 MPa, the presence of TiC particles lead to an improvement in fatigue life. Above 220 MPa, no influence of TiC reinforcement on fatigue life could be detected. In both the composite and unreinforced materials, the low-cycle and high-cycle fatigue lives were found to be virtually independent of matrix microstructure.

Super-stretchable metallic interconnects on polymer with a linear strain of up to 100%

DOE Office of Scientific and Technical Information (OSTI.GOV)

Arafat, Yeasir; Dutta, Indranath; Panat, Rahul, E-mail: Rahul.panat@wsu.edu

Metal interconnects in flexible and wearable devices are heterogeneous metal-polymer systems that are expected to sustain large deformation without failure. The principal strategy to make strain tolerant interconnect lines on flexible substrates has comprised of creating serpentine structures of metal films with either in-plane or out-of-plane waves, using porous substrates, or using highly ductile materials such as gold. The wavy and helical serpentine patterns preclude high-density packing of interconnect lines on devices, while ductile materials such as Au are cost prohibitive for real world applications. Ductile copper films can be stretched if bonded to the substrate, but show high levelmore » of cracking beyond few tens of % strain. In this paper, we demonstrate a material system consisting of Indium metal film over an elastomer (PDMS) with a discontinuous Cr layer such that the metal interconnect can be stretched to extremely high linear strain (up to 100%) without any visible cracks. Such linear strain in metal interconnects exceeds that reported in literature and is obtained without the use of any geometrical manipulations or porous substrates. Systematic experimentation is carried out to explain the mechanisms that allow the Indium film to sustain the high strain level without failure. The islands forming the discontinuous Cr layer are shown to move apart from each other during stretching without delamination, providing strong adhesion to the Indium film while accommodating the large strain in the system. The Indium film is shown to form surface wrinkles upon release from the large strain, confirming its strong adhesion to PDMS. A model is proposed based upon the observations that can explain the high level of stretch-ability of the Indium metal film over the PDMS substrate.« less

Sinuous Flow in Cutting of Metals

NASA Astrophysics Data System (ADS)

Yeung, Ho; Viswanathan, Koushik; Udupa, Anirudh; Mahato, Anirban; Chandrasekar, Srinivasan

2017-11-01

Using in situ high-speed imaging, we unveil details of a highly unsteady plastic flow mode in the cutting of annealed and highly strain-hardening metals. This mesoscopic flow mode, termed sinuous flow, is characterized by repeated material folding, large rotation, and energy dissipation. Sinuous flow effects a very large shape transformation, with local strains of ten or more, and results in a characteristic mushroomlike surface morphology that is quite distinct from the well-known morphologies of metal-cutting chips. Importantly, the attributes of this unsteady flow are also fundamentally different from other well-established unsteady plastic flows in large-strain deformation, like adiabatic shear bands. The nucleation and development of sinuous flow, its dependence on material properties, and its manifestation across material systems are demonstrated. Plastic buckling and grain-scale heterogeneity are found to play key roles in triggering this flow at surfaces. Implications for modeling and understanding flow stability in large-strain plastic deformation, surface quality, and preparation of near-strain-free surfaces by cutting are discussed. The results point to the inadequacy of the widely used shear-zone models, even for ductile metals.

Structural heredity influence upon principles of strain wave hardening

NASA Astrophysics Data System (ADS)

Kiricheck, A. V.; Barinov, S. V.; Yashin, A. V.

2017-02-01

It was established experimentally that by penetration of a strain wave through material hardened not only the technological modes of processing, but also a technological heredity - the direction of the fibers of the original macrostructure have an influence upon the diagram of microhardness. By penetration of the strain wave along fibers, the degree of hardening the material is less, however, a product is hardened throughout its entire section mainly along fibers. In the direction of the strain waves across fibers of the original structure of material, the degree of material hardening is much higher, the depth of the hardened layer with the degree of hardening not less than 50% makes at least 3 mm. It was found that under certain conditions the strain wave can completely change the original structure of the material. Thus, a heterogeneously hardened structure characterized by the interchange of harder and more viscous areas is formed, which is beneficial for assurance of high operational properties of material.

Tensile behavior of glass/ceramic composite materials at elevated temperatures

NASA Technical Reports Server (NTRS)

Mandell, J. F.; Grande, D. H.; Jacobs, J.

1987-01-01

This paper describes the tensile behavior of high-temperature composite materials containing continuous Nicalon ceramic fiber reinforcement and glass and glass/ceramic matrices. The longitudinal properties of these materials can approach theoretical expectations for brittle matrix composites, failing at a strength and ultimate strain level consistent with those of the fibers. The brittle, high-modulus matrices result in a nonlinear stress-strain curve due to the onset of stable matrix cracking at 10 to 30 percent of the fiber strain to failure, and at strains below this range in off-axis plies. Current fibers and matrices can provide attractive properties well above 1000 C, but composites experience embrittlement in oxidizing atmospheres at 800 to 1000 C due to oxidation of a carbon interface reaction layer.The oxidation effect greatly increases the interface bond strength, causing composite embrittlement.

Determination of Strain Rate Sensitivity of Micro-struts Manufactured Using the Selective Laser Melting Method

NASA Astrophysics Data System (ADS)

Gümrük, Recep; Mines, R. A. W.; Karadeniz, Sami

2018-03-01

Micro-lattice structures manufactured using the selective laser melting (SLM) process provides the opportunity to realize optimal cellular materials for impact energy absorption. In this paper, strain rate-dependent material properties are measured for stainless steel 316L SLM micro-lattice struts in the strain rate range of 10-3 to 6000 s-1. At high strain rates, a novel version of the split Hopkinson Bar has been developed. Strain rate-dependent materials data have been used in Cowper-Symonds material model, and the scope and limit of this model in the context of SLM struts have been discussed. Strain rate material data and the Cowper-Symonds model have been applied to the finite element analysis of a micro-lattice block subjected to drop weight impact loading. The model output has been compared to experimental results, and it has been shown that the increase in crush stress due to impact loading is mainly the result of strain rate material behavior. Hence, a systematic methodology has been developed to investigate the impact energy absorption of a micro-lattice structure manufactured using additive layer manufacture (SLM). This methodology can be extended to other micro-lattice materials and configurations, and to other impact conditions.

Plate and butt-weld stresses beyond elastic limit, material and structural modeling

NASA Technical Reports Server (NTRS)

Verderaime, V.

1991-01-01

Ultimate safety factors of high performance structures depend on stress behavior beyond the elastic limit, a region not too well understood. An analytical modeling approach was developed to gain fundamental insights into inelastic responses of simple structural elements. Nonlinear material properties were expressed in engineering stresses and strains variables and combined with strength of material stress and strain equations similar to numerical piece-wise linear method. Integrations are continuous which allows for more detailed solutions. Included with interesting results are the classical combined axial tension and bending load model and the strain gauge conversion to stress beyond the elastic limit. Material discontinuity stress factors in butt-welds were derived. This is a working-type document with analytical methods and results applicable to all industries of high reliability structures.

High-Temperature Strain Sensing for Aerospace Applications

NASA Technical Reports Server (NTRS)

Piazza, Anthony; Richards, Lance W.; Hudson, Larry D.

2008-01-01

Thermal protection systems (TPS) and hot structures are utilizing advanced materials that operate at temperatures that exceed abilities to measure structural performance. Robust strain sensors that operate accurately and reliably beyond 1800 F are needed but do not exist. These shortcomings hinder the ability to validate analysis and modeling techniques and hinders the ability to optimize structural designs. This presentation examines high-temperature strain sensing for aerospace applications and, more specifically, seeks to provide strain data for validating finite element models and thermal-structural analyses. Efforts have been made to develop sensor attachment techniques for relevant structural materials at the small test specimen level and to perform laboratory tests to characterize sensor and generate corrections to apply to indicated strains. Areas highlighted in this presentation include sensors, sensor attachment techniques, laboratory evaluation/characterization of strain measurement, and sensor use in large-scale structures.

Strategy for reliable strain measurement in InAs/GaAs materials from high-resolution Z-contrast STEM images

NASA Astrophysics Data System (ADS)

Vatanparast, Maryam; Vullum, Per Erik; Nord, Magnus; Zuo, Jian-Min; Reenaas, Turid W.; Holmestad, Randi

2017-09-01

Geometric phase analysis (GPA), a fast and simple Fourier space method for strain analysis, can give useful information on accumulated strain and defect propagation in multiple layers of semiconductors, including quantum dot materials. In this work, GPA has been applied to high resolution Z-contrast scanning transmission electron microscopy (STEM) images. Strain maps determined from different g vectors of these images are compared to each other, in order to analyze and assess the GPA technique in terms of accuracy. The SmartAlign tool has been used to improve the STEM image quality getting more reliable results. Strain maps from template matching as a real space approach are compared with strain maps from GPA, and it is discussed that a real space analysis is a better approach than GPA for aberration corrected STEM images.

Joining Chemical Pressure and Epitaxial Strain to Yield Y-doped BiFeO3 Thin Films with High Dielectric Response

PubMed Central

Scarisoreanu, N. D.; Craciun, F.; Birjega, R.; Ion, V.; Teodorescu, V. S.; Ghica, C.; Negrea, R.; Dinescu, M.

2016-01-01

BiFeO3 is one of the most promising multiferroic materials but undergoes two major drawbacks: low dielectric susceptibility and high dielectric loss. Here we report high in-plane dielectric permittivity (ε’ ∼2500) and low dielectric loss (tan δ < 0.01) obtained on Bi0.95Y0.05FeO3 films epitaxially grown on SrTiO3 (001) by pulsed laser deposition. High resolution transmission electron microscopy and geometric phase analysis evidenced nanostripe domains with alternating compressive/tensile strain and slight lattice rotations. Nanoscale mixed phase/domain ensembles are commonly found in different complex materials with giant dielectric/electromechanical (ferroelectric/ relaxors) or magnetoresistance (manganites) response. Our work brings insight into the joined role of chemical pressure and epitaxial strain on the appearance of nanoscale stripe structure which creates conditions for easy reorientation and high dielectric response, and could be of more general relevance for the field of materials science where engineered materials with huge response to external stimuli are a highly priced target. PMID:27157090

High-Temperature Extensometry and PdCr Temperature-Compensated Wire Resistance Strain Gages Compared

NASA Technical Reports Server (NTRS)

1996-01-01

A detailed experimental evaluation is underway at the NASA Lewis Research Center to compare and contrast the performance of the PdCr/Pt dual-element temperature-compensated wire resistance strain gage with that of conventional high-temperature extensometry. The advanced PdCr gage, developed by researchers at Lewis, exhibits desirable properties and a relatively small and repeatable apparent strain to 800 C. This gage represents a significant advance in technology because existing commercial resistance strain gages are not reliable for quasi-static strain measurements above approximately 400 C. Various thermal and mechanical loading spectra are being applied by a high-temperature thermomechanical uniaxial testing system to evaluate the two strain-measurement systems. This is being done not only to compare and contrast the two strain sensors, but also to investigate the applicability of the PdCr strain gage to the coupon-level specimen testing environment typically employed when the high-temperature mechanical behavior of structural materials is characterized. Strain measurement capabilities to 800 C are being investigated with a nickel-base superalloy, Inconel 100 (IN 100), substrate material and application to TMC's is being examined with the model system, SCS-6/Ti-15-3. Furthermore, two gage application techniques are being investigated in the comparison study: namely, flame-sprayed and spot welding.

Incorporating 2D Materials with Micro-electromechanical Systems to Explore Strain Physics and Devices

NASA Astrophysics Data System (ADS)

Christopher, Jason; Vutukuru, Mounika; Kohler, Travis; Bishop, David; Swan, Anna; Goldberg, Bennett

2D materials can withstand an order of magnitude more strain than their bulk counterparts which can be used to dramatically change electrical, thermal and optical properties or even cause unconventional behavior such as generating pseudo-magnetic fields. Here we present micro-electromechanical systems (MEMS) as a platform for straining 2D materials to make such novel phenomena accessible. Unlike other strain techniques, MEMS are capable of precisely controlling the magnitude and orientation of the strain field and are readily integrated with current technology facilitating a path from lab bench to application. In this study, we use graphene as our prototypical 2D material, and determine strain via micro-Raman spectroscopy making extensive use of graphene's well-characterized phonon strain response. We report on the strength of various techniques for affixing graphene to MEMS, and investigate the role of surface morphology and chemistry in creating a high friction interface capable of inducing large strain. This work is supported by NSF DMR Grant 1411008, and author J. Christopher thanks the NDSEG program for its support.

Synthesis and electromechanical characterization of a new acrylic dielectric elastomer with high actuation strain and dielectric strength

NASA Astrophysics Data System (ADS)

Hu, Wei; Niu, Xiaofan; Yang, Xinguo; Zhang, Naifang; Pei, Qibing

2013-04-01

Dielectric Elastomers (DEs) can be actuated under high electric field to produce large strains. Most high-performing DE materials such as the 3M™ VHB™ membranes are commercial products designed for industrial pressure-sensitive adhesives. The limited knowledge of the exact chemical structures of these commercial materials has made it difficult to understand the relationship between molecular structures and electromechanical properties. In this work, new acrylic elastomers based on n-butyl acrylate and acrylic acid were synthesized from monomer solutions by UV-initiated bulk polymerization. The new acrylic copolymers have a potential to obtain high dielectric constant, actuation strain, dielectric strength, and a high energy density. Silicone and ester oligomer diacrylates were also added onto the copolymer structures to suppress crystallization and to crosslink the polymer chains. Four acrylic formulations were developed with different amounts of acrylic acid. This gives a tunable stiffness, while the dielectric constant is varied from 4.3 to 7.1. The figure-of-merit performance of the best formulation is 186 % area strain, 222 MV/m of dielectric strength, and 2.7 MJ/m3 of energy density. To overcome electromechanical instability, different prestrain ratios were investigated, and under the optimized prestrain, the material has a lifetime of thousands of cycles at 120 % area strain.

Crash simulation of hybrid structures considering the stress and strain rate dependent material behavior of thermoplastic materials

NASA Astrophysics Data System (ADS)

Hopmann, Ch.; Schöngart, M.; Weber, M.; Klein, J.

2015-05-01

Thermoplastic materials are more and more used as a light weight replacement for metal, especially in the automotive industry. Since these materials do not provide the mechanical properties, which are required to manufacture supporting elements like an auto body or a cross bearer, plastics are combined with metals in so called hybrid structures. Normally, the plastics components are joined to the metal structures using different technologies like welding or screwing. Very often, the hybrid structures are made of flat metal parts, which are stiffened by a reinforcement structure made of thermoplastic materials. The loads on these structures are very often impulsive, for example in the crash situation of an automobile. Due to the large stiffness variation of metal and thermoplastic materials, complex states of stress and very high local strain rates occur in the contact zone under impact conditions. Since the mechanical behavior of thermoplastic materials is highly dependent on these types of load, the crash failure of metal plastic hybrid parts is very complex. The problem is that the normally used strain rate dependent elastic/plastic material models are not capable to simulate the mechanical behavior of thermoplastic materials depended on the state of stress. As part of a research project, a method to simulate the mechanical behavior of hybrid structures under impact conditions is developed at the IKV. For this purpose, a specimen for the measurement of mechanical properties dependet on the state of stress and a method for the strain rate depended characterization of thermoplastic materials were developed. In the second step impact testing is performed. A hybrid structure made from a metal sheet and a reinforcement structure of a Polybutylenterephthalat Polycarbonate blend is tested under impact conditions. The measured stress and strain rate depended material data are used to simulate the mechanical behavior of the hybrid structure under highly dynamic load with impact velocities up to 5 m/s. The mechanical behavior of the plastics structure is simulated using a quadratic yield surface, which takes the state of stress and the strain rate into account. The FE model is made from mid surface elements to reduce the computing time.

Interaction of heat production, strain rate and stress power in a plastically deforming body under tensile test

NASA Technical Reports Server (NTRS)

Paglietti, A.

1982-01-01

At high strain rates the heat produced by plastic deformation can give rise to a rate dependent response even if the material has rate independent constitutive equations. This effect has to be evaluated when interpreting a material test, or else it could erroneously be ascribed to viscosity. A general thermodynamic theory of tensile testing of elastic-plastic materials is given in this paper; it is valid for large strain at finite strain rates. It enables discovery of the parameters governing the thermodynamic strain rate effect, provides a method for proper interpretation of the results of the tests of dynamic plasticity, and suggests a way of planning experiments in order to detect the real contribution of viscosity.

Microbial specificity of metallic surfaces exposed to ambient seawater

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zaidi, B.R.; Bard, R.F.; Tosteson, T.R.

1984-09-01

High-molecular-weight materials associated with the extracellular matrix and film found on titanium and aluminum surfaces after exposure to flowing coastal seawater were isolated. This material was purified by hydroxylapatite chromatography and subsequently employed to produce antibodies in the toad, Bufo marinus. The antibodies were immobilized on a solid support and employed to isolate adhesion-enhancing, high-molecular-weight materials from the laboratory culture media of bacterial strains recovered from the respective metallic surfaces during the course of their exposure to seawater. The adhesion-enhancing materials produced by the surface-associated bacterial strains were immunologically related to the extracellular biofouling matrix material found on the surfacesmore » from which these bacteria were isolated. The surface selectivity of these bacterial strains appeared to be based on the specificity of the interaction between adhesion-enhancing macromolecules produced by these bacteria and the surfaces in question. 30 references, 6 tables.« less

Microstructure and Strain Rate-Dependent Tensile Deformation Behavior of Fiber Laser-Welded Butt Joints of Dual-Phase Steels

NASA Astrophysics Data System (ADS)

Liu, Yang; Dong, Danyang; Han, Zhiqiang; Yang, Zhibin; Wang, Lu; Dong, Qingwei

2018-05-01

The microstructure and tensile deformation behavior of the fiber laser-welded similar and dissimilar dual-phase (DP) steel joints over a wide range of strain rates from 10-3 to 103 s-1 were investigated for the further applications on the lightweight design of vehicles. The high strain rate dynamic tensile deformation process and full-field strain distribution of the base metals and welded joints were examined using the digital image correlation method and high-speed photography. The strain rate effects on the stress-strain responses, tensile properties, deformation, and fracture behavior of the investigated materials were analyzed. The yield stress (YS) and ultimate tensile strength (UTS) of the dissimilar DP780/DP980 welded joints were lying in-between those of the DP780 and DP980 base metals, and all materials exhibited positive strain rate dependence on the YS and UTS. Owing to the microstructure heterogeneity, the welded joints showed relatively lower ductility in terms of total elongation (TE) than those of the corresponding base metals. The strain localization started before the maximum load was reached, and the strain localization occurred earlier during the whole deformation process with increasing strain rate. As for the dissimilar welded joint, the strain localization tended to occur in the vicinity of the lowest hardness value across the welded joint, which was in the subcritical HAZ at the DP780 side. As the strain rate increased, the typical ductile failure characteristic of the investigated materials did not change.

Microstructure and Strain Rate-Dependent Tensile Deformation Behavior of Fiber Laser-Welded Butt Joints of Dual-Phase Steels

NASA Astrophysics Data System (ADS)

Liu, Yang; Dong, Danyang; Han, Zhiqiang; Yang, Zhibin; Wang, Lu; Dong, Qingwei

2018-04-01

The microstructure and tensile deformation behavior of the fiber laser-welded similar and dissimilar dual-phase (DP) steel joints over a wide range of strain rates from 10-3 to 103 s-1 were investigated for the further applications on the lightweight design of vehicles. The high strain rate dynamic tensile deformation process and full-field strain distribution of the base metals and welded joints were examined using the digital image correlation method and high-speed photography. The strain rate effects on the stress-strain responses, tensile properties, deformation, and fracture behavior of the investigated materials were analyzed. The yield stress (YS) and ultimate tensile strength (UTS) of the dissimilar DP780/DP980 welded joints were lying in-between those of the DP780 and DP980 base metals, and all materials exhibited positive strain rate dependence on the YS and UTS. Owing to the microstructure heterogeneity, the welded joints showed relatively lower ductility in terms of total elongation (TE) than those of the corresponding base metals. The strain localization started before the maximum load was reached, and the strain localization occurred earlier during the whole deformation process with increasing strain rate. As for the dissimilar welded joint, the strain localization tended to occur in the vicinity of the lowest hardness value across the welded joint, which was in the subcritical HAZ at the DP780 side. As the strain rate increased, the typical ductile failure characteristic of the investigated materials did not change.

Final Report Auto/Steel Partnership Phase II

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cady, C.M.; Chen, S.R.; Gray, G.T. III

1999-06-09

This is the final report in which effects of strain-rate, temperature, and stress-state on the yield stress and the strain hardening behavior of many common steels used in automobile construction were investigated. The yield and flow stresses were found to exhibit very high rate sensitivities for most of the steels while the hardening rates were found to be insensitive to strain rate and temperature at lower temperatures or at higher strain rates. This behavior is consistent with the observation that overcoming the intrinsic Peierls stress is shown to be the rate-controlling mechanism in these materials at low temperatures. The dependencemore » of the yield stress on temperature and strain rate was found to decrease while the strain hardening rate increased. The Mechanical Threshold Stress (MTS) model was adopted to model the stress-strain behavior of the steels. Parameters for the constitutive relations were derived for the MTS model and also for the Johnson-Cook (JC) and the Zerilli-Armstrong (ZA) models. The results of this study substantiate the applicability of these models for describing the high strain-rate deformation of these materials. The JC and ZA models, however, due to their use of a power strain hardening law were found to yield constitutive relations for the materials which are strongly dependent on the range of strains for which the models were optimized.« less

High-Temperature Extensometry and PdCr Temperature-Compensated Wire Resistance Strain Gages Compared

NASA Technical Reports Server (NTRS)

1997-01-01

A detailed experimental evaluation is underway at the NASA Lewis Research Center to compare and contrast the performance of the PdCr/Pt dual-element temperature-compensated wire resistance strain gage with that of conventional high-temperature extensometry. The advanced PdCr gage, developed by researchers at Lewis, exhibits desirable properties and a relatively small and repeatable apparent strain to 800 C. This gage represents a significant advance in technology because existing commercial resistance strain gages are not reliable for quasi-static strain measurements above approx. 400 C. Various thermal and mechanical loading spectra are being applied by a high-temperature thermomechanical uniaxial testing system to evaluate the two strain-measurement systems. This is being done not only to compare and contrast the two strain sensors, but also to investigate the applicability of the PdCr strain gage to the coupon-level specimen testing environment typically employed when the high-temperature mechanical behavior of structural materials is characterized. Strain measurement capabilities to 800 C are being investigated with a nickel-base superalloy, Inconel 100 (IN 100), substrate material and application to TMC's is being examined with the model system, SCS-6/Ti-15-3. Furthermore, two gage application techniques are being investigated in the comparison study: namely, flame-sprayed and spot welding. The apparent strain responses of both the weldable and flame-sprayed PdCr wire strain gages were found to be cyclically repeatable on both IN 100 and SCS-6/Ti-15-3 [0]_8. In general, each gage exhibited some uniqueness with respect to apparent strain behavior. Gages mounted on the IN 100 specimens tended to show a repeatable apparent strain within the first few cycles, because the thermal response of IN 100 was stable. This was not the case, however, for the TMC specimens, which typically required several thermal cycles to stabilize the thermal strain response. Thus, progressive changes in the apparent strain behavior were corroborated by the extensometer, which unlike the mounted gage can distinguish quantitative changes in the material's thermal strain response. One specimen was instrumented with both a fixed and floating gage. From the difference in output of these two gages, the thermal expansion strains were calculated. These data, which are given in the figure, show excellent agreement with the values measured by the high-temperature extensometry.

Life prediction of l6 steel using strain-life curve and cyclic stress-strain curve by means of low cycle fatigue testing

NASA Astrophysics Data System (ADS)

Inamdar, Sanket; Ukhande, Manoj; Date, Prashant; Lomate, Dattaprasad; Takale, Shyam; Singh, RKP

2017-05-01

L6 Steel is used as die material in closed die hot forging process. This material is having some unique properties. These properties are due to its composition. Strain softening is the noticeable property of this material. Due to this in spite of cracking at high stress this material gets plastically deformed and encounters loss in time as well as money. Studies of these properties are necessary to nurture this material at fullest extent. In this paper, numerous experiments have been carried on L6 material to evaluate cyclic Stress - strain behavior as swell as strain-life behavior of the material. Low cycle fatigue test is carried out on MTS fatigue test machine at fully reverse loading condition R=-1. Also strain softening effect on forging metal forming process is explained in detail. The failed samples during low cycle fatigue test further investigated metallurgically on scanning electron microscopy. Based on this study, life estimation of hot forging die is carried out and it’s correlation with actual shop floor data is found out. This work also concludes about effect of pre-treatments like nitro-carburizing and surface coating on L6 steel material, to enhance its fatigue life to certain extent.

Strain-rate dependence of ramp-wave evolution and strength in tantalum

DOE PAGES

Lane, J. Matthew D.; Foiles, Stephen M.; Lim, Hojun; ...

2016-08-25

We have conducted molecular dynamics (MD) simulations of quasi-isentropic ramp-wave compression to very high pressures over a range of strain rates from 10 11 down to 10 8 1/s. Using scaling methods, we collapse wave profiles from various strain rates to a master profile curve, which shows deviations when material response is strain-rate dependent. Thus, we can show with precision where, and how, strain-rate dependence affects the ramp wave. We find that strain rate affects the stress-strain material response most dramatically at strains below 20%, and that above 30% strain the material response is largely independent of strain rate. Wemore » show good overall agreement with experimental stress-strain curves up to approximately 30% strain, above which simulated response is somewhat too stiff. We postulate that this could be due to our interatomic potential or to differences in grain structure and/or size between simulation and experiment. Strength is directly measured from per-atom stress tensor and shows significantly enhanced elastic response at the highest strain rates. As a result, this enhanced elastic response is less pronounced at higher pressures and at lower strain rates.« less

Investigation of a Coupled Arrhenius-Type/Rossard Equation of AH36 Material

PubMed Central

Qin, Qin; Tian, Ming-Liang; Zhang, Peng

2017-01-01

High-temperature tensile testing of AH36 material in a wide range of temperatures (1173–1573 K) and strain rates (10−4–10−2 s−1) has been obtained by using a Gleeble system. These experimental stress-strain data have been adopted to develop the constitutive equation. The constitutive equation of AH36 material was suggested based on the modified Arrhenius-type equation and the modified Rossard equation respectively. The results indicate that the constitutive equation is strongly influenced by temperature and strain, especially strain. Moreover, there is a good agreement between the predicted data of the modified Arrhenius-type equation and the experimental results when the strain is greater than 0.02. There is also good agreement between the predicted data of the Rossard equation and the experimental results when the strain is less than 0.02. Therefore, a coupled equation where the modified Arrhenius-type equation and Rossard equation are combined has been proposed to describe the constitutive equation of AH36 material according to the different strain values in order to improve the accuracy. The correlation coefficient between the computed and experimental flow stress data was 0.998. The minimum value of the average absolute relative error shows the high accuracy of the coupled equation compared with the two modified equations. PMID:28772767

TRANSTRAIN: A program to compute strain transformations in composite materials

NASA Technical Reports Server (NTRS)

Ahmed, Rafiq

1990-01-01

Over the years, the solid rocket motor community has made increasing use of composite materials for thermal and structural applications. This is particularly true of solid rocket nozzles, which have used carbon phenolic and, increasingly, carbon-carbon materials to provide structural integrity and thermal protection at the high temperatures encountered during motor burn. To evaluate the degree of structural performance of nozzles and their materials and to verify analysis models, many subscale and full-scale tests are run. These provide engineers with valuable data needed to optimize design and to analyze nozzle hardware. Included among these data are strains, pressures, thrust, temperatures, and displacements. Recent nozzle test hardware has made increasing use of strain gauges embedded in the carbon composite material to measure internal strains. In order to evaluate strength, these data must be transformed into strains along the fiber directions. The fiber-direction stresses can then be calculated. A computer program written to help engineers correctly manipulate the strain data into a form that can be used to evaluate structural integrity of the nozzle is examined.

Identification of Deformation Mechanisms During Bi-Axial Straining of Superplastic AA5083 Material

DTIC Science & Technology

2004-06-01

equiaxed grain structure in FSS along with the prevalence of high - energy boundaries accommodates sliding under the proper shearing conditions. Figure...by a randomized texture and a higher concentration of high disorientation angles. Dislocation creep, which dominates at higher strain rates, is...concentration of high disorientation angles. Dislocation creep, which dominates at higher strain rates, is characterized by fiber texture formation

Design of Strain-Limiting Substrate Materials for Stretchable and Flexible Electronics

PubMed Central

Ma, Yinji; Jang, Kyung-In; Wang, Liang; Jung, Han Na; Kwak, Jean Won; Xue, Yeguang; Chen, Hang; Yang, Yiyuan; Shi, Dawei; Feng, Xue

2017-01-01

Recently developed classes of electronics for biomedical applications exploit substrates that offer low elastic modulus and high stretchability, to allow intimate, mechanically biocompatible integration with soft biological tissues. A challenge is that such substrates do not generally offer protection of the electronics from high peak strains that can occur upon large-scale deformation, thereby creating a potential for device failure. The results presented here establish a simple route to compliant substrates with strain-limiting mechanics based on approaches that complement those of recently described alternatives. Here, a thin film or mesh of a high modulus material transferred onto a prestrained compliant substrate transforms into wrinkled geometry upon release of the prestrain. The structure formed by this process offers a low elastic modulus at small strain due to the small effective stiffness of the wrinkled film or mesh; it has a high tangent modulus (e.g., >1000 times the elastic modulus) at large strain, as the wrinkles disappear and the film/mesh returns to a flat geometry. This bilinear stress–strain behavior has an extremely sharp transition point, defined by the magnitude of the prestrain. A theoretical model yields analytical expressions for the elastic and tangent moduli and the transition strain of the bilinear stress–strain relation, with quantitative correspondence to finite element analysis and experiments. PMID:29033714

Design of Strain-Limiting Substrate Materials for Stretchable and Flexible Electronics.

PubMed

Ma, Yinji; Jang, Kyung-In; Wang, Liang; Jung, Han Na; Kwak, Jean Won; Xue, Yeguang; Chen, Hang; Yang, Yiyuan; Shi, Dawei; Feng, Xue; Rogers, John A; Huang, Yonggang

2016-08-02

Recently developed classes of electronics for biomedical applications exploit substrates that offer low elastic modulus and high stretchability, to allow intimate, mechanically biocompatible integration with soft biological tissues. A challenge is that such substrates do not generally offer protection of the electronics from high peak strains that can occur upon large-scale deformation, thereby creating a potential for device failure. The results presented here establish a simple route to compliant substrates with strain-limiting mechanics based on approaches that complement those of recently described alternatives. Here, a thin film or mesh of a high modulus material transferred onto a prestrained compliant substrate transforms into wrinkled geometry upon release of the prestrain. The structure formed by this process offers a low elastic modulus at small strain due to the small effective stiffness of the wrinkled film or mesh; it has a high tangent modulus (e.g., >1000 times the elastic modulus) at large strain, as the wrinkles disappear and the film/mesh returns to a flat geometry. This bilinear stress-strain behavior has an extremely sharp transition point, defined by the magnitude of the prestrain. A theoretical model yields analytical expressions for the elastic and tangent moduli and the transition strain of the bilinear stress-strain relation, with quantitative correspondence to finite element analysis and experiments.

Super-elastic and fatigue resistant carbon material with lamellar multi-arch microstructure

NASA Astrophysics Data System (ADS)

Gao, Huai-Ling; Zhu, Yin-Bo; Mao, Li-Bo; Wang, Feng-Chao; Luo, Xi-Sheng; Liu, Yang-Yi; Lu, Yang; Pan, Zhao; Ge, Jin; Shen, Wei; Zheng, Ya-Rong; Xu, Liang; Wang, Lin-Jun; Xu, Wei-Hong; Wu, Heng-An; Yu, Shu-Hong

2016-09-01

Low-density compressible materials enable various applications but are often hindered by structure-derived fatigue failure, weak elasticity with slow recovery speed and large energy dissipation. Here we demonstrate a carbon material with microstructure-derived super-elasticity and high fatigue resistance achieved by designing a hierarchical lamellar architecture composed of thousands of microscale arches that serve as elastic units. The obtained monolithic carbon material can rebound a steel ball in spring-like fashion with fast recovery speed (~580 mm s-1), and demonstrates complete recovery and small energy dissipation (~0.2) in each compress-release cycle, even under 90% strain. Particularly, the material can maintain structural integrity after more than 106 cycles at 20% strain and 2.5 × 105 cycles at 50% strain. This structural material, although constructed using an intrinsically brittle carbon constituent, is simultaneously super-elastic, highly compressible and fatigue resistant to a degree even greater than that of previously reported compressible foams mainly made from more robust constituents.

A laser-engraved glass duplicating the structure, mechanics and performance of natural nacre.

PubMed

Valashani, Seyed Mohammad Mirkhalaf; Barthelat, Francois

2015-03-30

Highly mineralized biological materials such as nacre (mother of pearl), tooth enamel or conch shell boast unique and attractive combinations of stiffness, strength and toughness. The structures of these biological materials and their associated mechanisms are now inspiring new types of advanced structural materials. However, despite significant efforts, no bottom up fabrication method could so far match biological materials in terms of microstructural organization and mechanical performance. Here we present a new 'top down' strategy to tackling this fabrication problem, which consists in carving weak interfaces within a brittle material using a laser engraving technique. We demonstrate the method by fabricating and testing borosilicate glasses containing nacre-like microstructures infiltrated with polyurethane. When deformed, these materials properly duplicate the mechanisms of natural nacre: combination of controlled sliding of the tablets, accompanied with geometric hardening, strain hardening and strain rate hardening. The nacre-like glass is composed of 93 volume % (vol%) glass, yet 700 times tougher and breaks at strains as high as 20%.

Hydrostatic Stress Effects Incorporated Into the Analysis of the High-Strain-Rate Deformation of Polymer Matrix Composites

NASA Technical Reports Server (NTRS)

Goldberg, Robert K.; Roberts, Gary D.

2003-01-01

Procedures for modeling the effect of high strain rate on composite materials are needed for designing reliable composite engine cases that are lighter than the metal cases in current use. The types of polymer matrix composites that are likely to be used in such an application have a deformation response that is nonlinear and that varies with strain rate. The nonlinearity and strain rate dependence of the composite response is primarily due to the matrix constituent. Therefore, in developing material models to be used in the design of impact-resistant composite engine cases, the deformation of the polymer matrix must be correctly analyzed. However, unlike in metals, the nonlinear response of polymers depends on the hydrostatic stresses, which must be accounted for within an analytical model. An experimental program has been carried out through a university grant with the Ohio State University to obtain tensile and shear deformation data for a representative polymer for strain rates ranging from quasi-static to high rates of several hundred per second. This information has been used at the NASA Glenn Research Center to develop, characterize, and correlate a material model in which the strain rate dependence and nonlinearity (including hydrostatic stress effects) of the polymer are correctly analyzed. To obtain the material data, Glenn s researchers designed and fabricated test specimens of a representative toughened epoxy resin. Quasi-static tests at low strain rates and split Hopkinson bar tests at high strain rates were then conducted at the Ohio State University. The experimental data confirmed the strong effects of strain rate on both the tensile and shear deformation of the polymer. For the analytical model, Glenn researchers modified state variable constitutive equations previously used for the viscoplastic analysis of metals to allow for the analysis of the nonlinear, strain-rate-dependent polymer deformation. Specifically, we accounted for the effects of hydrostatic stresses. An important discovery in the course of this work was that the hydrostatic stress effects varied during the loading process, which needed to be accounted for within the constitutive equations. The model is characterized primarily by shear data, with tensile data used to characterize the hydrostatic stress effects.

Graphene-based smart materials

NASA Astrophysics Data System (ADS)

Yu, Xiaowen; Cheng, Huhu; Zhang, Miao; Zhao, Yang; Qu, Liangti; Shi, Gaoquan

2017-09-01

The high specific surface area and the excellent mechanical, electrical, optical and thermal properties of graphene make it an attractive component for high-performance stimuli-responsive or 'smart' materials. Complementary to these inherent properties, functionalization or hybridization can substantially improve the performance of these materials. Typical graphene-based smart materials include mechanically exfoliated perfect graphene, chemical vapour deposited high-quality graphene, chemically modified graphene (for example, graphene oxide and reduced graphene oxide) and their macroscopic assemblies or composites. These materials are sensitive to a range of stimuli, including gas molecules or biomolecules, pH value, mechanical strain, electrical field, and thermal or optical excitation. In this Review, we outline different graphene-based smart materials and their potential applications in actuators, chemical or strain sensors, self-healing materials, photothermal therapy and controlled drug delivery. We also introduce the working mechanisms of graphene-based smart materials and discuss the challenges facing the realization of their practical applications.

Ultrasensitive tunability of the direct bandgap of 2D InSe flakes via strain engineering

NASA Astrophysics Data System (ADS)

Li, Yang; Wang, Tianmeng; Wu, Meng; Cao, Ting; Chen, Yanwen; Sankar, Raman; Ulaganathan, Rajesh K.; Chou, Fangcheng; Wetzel, Christian; Xu, Cheng-Yan; Louie, Steven G.; Shi, Su-Fei

2018-04-01

InSe, a member of the layered materials family, is a superior electronic and optical material which retains a direct bandgap feature from the bulk to atomically thin few-layers and high electronic mobility down to a single layer limit. We, for the first time, exploit strain to drastically modify the bandgap of two-dimensional (2D) InSe nanoflakes. We demonstrated that we could decrease the bandgap of a few-layer InSe flake by 160 meV through applying an in-plane uniaxial tensile strain to 1.06% and increase the bandgap by 79 meV through applying an in-plane uniaxial compressive strain to 0.62%, as evidenced by photoluminescence (PL) spectroscopy. The large reversible bandgap change of ~239 meV arises from a large bandgap change rate (bandgap strain coefficient) of few-layer InSe in response to strain, ~154 meV/% for uniaxial tensile strain and ~140 meV/% for uniaxial compressive strain, representing the most pronounced uniaxial strain-induced bandgap strain coefficient experimentally reported in 2D materials. We developed a theoretical understanding of the strain-induced bandgap change through first-principles DFT and GW calculations. We also confirmed the bandgap change by photoconductivity measurements using excitation light with different photon energies. The highly tunable bandgap of InSe in the infrared regime should enable a wide range of applications, including electro-mechanical, piezoelectric and optoelectronic devices.

Simulation of cemented granular materials. I. Macroscopic stress-strain response and strain localization.

PubMed

Estrada, Nicolas; Lizcano, Arcesio; Taboada, Alfredo

2010-07-01

This is the first of two papers investigating the mechanical response of cemented granular materials by means of contact dynamics simulations. In this paper, a two-dimensional polydisperse sample with high-void ratio is constructed and then sheared in a simple shear numerical device at different confinement levels. We study the macroscopic response of the material in terms of mean and deviatoric stresses and strains. We show that the introduction of a local force scale, i.e., the tensile strength of the cemented bonds, causes the material to behave in a rigid-plastic fashion, so that a yield surface can be easily determined. This yield surface has a concave-down shape in the mean:deviatoric stress plane and it approaches a straight line, i.e., a Coulomb strength envelope, in the limit of a very dense granular material. Beyond yielding, the cemented structure gradually degrades until the material eventually behaves as a cohesionless granular material. Strain localization is also investigated, showing that the strains concentrate in a shear band whose thickness increases with the confining stress. The void ratio inside the shear band at the steady state is shown to be a material property that depends only on contact parameters.

Revisit of the relationship between the elastic properties and sound velocities at high pressures

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Chenju; Yan, Xiaozhen; Institute of Atomic and Molecular Sciences, Sichuan University, Chengdu 610065

2014-09-14

The second-order elastic constants and stress-strain coefficients are defined, respectively, as the second derivatives of the total energy and the first derivative of the stress with respect to strain. Since the Lagrangian and infinitesimal strain are commonly used in the two definitions above, the second-order elastic constants and stress-strain coefficients are separated into two categories, respectively. In general, any of the four physical quantities is employed to characterize the elastic properties of materials without differentiation. Nevertheless, differences may exist among them at non-zero pressures, especially high pressures. Having explored the confusing issue systemically in the present work, we find thatmore » the four quantities are indeed different from each other at high pressures and these differences depend on the initial stress applied on materials. Moreover, the various relations between the four quantities depicting elastic properties of materials and high-pressure sound velocities are also derived from the elastic wave equations. As examples, we calculated the high-pressure sound velocities of cubic tantalum and hexagonal rhenium using these nexus. The excellent agreement of our results with available experimental data suggests the general applicability of the relations.« less

Fully integrated carbon nanotube composite thin film strain sensors on flexible substrates for structural health monitoring

NASA Astrophysics Data System (ADS)

Burton, A. R.; Lynch, J. P.; Kurata, M.; Law, K. H.

2017-09-01

Multifunctional thin film materials have opened many opportunities for novel sensing strategies for structural health monitoring. While past work has established methods of optimizing multifunctional materials to exhibit sensing properties, comparatively less work has focused on their integration into fully functional sensing systems capable of being deployed in the field. This study focuses on the advancement of a scalable fabrication process for the integration of multifunctional thin films into a fully integrated sensing system. This is achieved through the development of an optimized fabrication process that can create a broad range of sensing systems using multifunctional materials. A layer-by-layer deposited multifunctional composite consisting of single walled carbon nanotubes (SWNT) in a polyvinyl alcohol and polysodium-4-styrene sulfonate matrix are incorporated with a lithography process to produce a fully integrated sensing system deposited on a flexible substrate. To illustrate the process, a strain sensing platform consisting of a patterned SWNT-composite thin film as a strain-sensitive element within an amplified Wheatstone bridge sensing circuit is presented. Strain sensing is selected because it presents many of the design and processing challenges that are core to patterning multifunctional thin film materials into sensing systems. Strain sensors fabricated on a flexible polyimide substrate are experimentally tested under cyclic loading using standard four-point bending coupons and a partial-scale steel frame assembly under lateral loading. The study reveals the material process is highly repeatable to produce fully integrated strain sensors with linearity and sensitivity exceeding 0.99 and 5 {{V}}/{ε }, respectively. The thin film strain sensors are robust and are capable of high strain measurements beyond 3000 μ {ε }.

Palladium-chromium static strain gage for high temperature propulsion systems

NASA Technical Reports Server (NTRS)

Lei, Jih-Fen

1991-01-01

The present electrical strain gage for high temperature static strain measurements is in its fine-wire and thin-film forms designed to be temperature-compensated on any substrate material. The gage element is of Pd-Cr alloy, while the compensator is of Pt. Because the thermally-induced apparent strain of this compensated wire strain gage is sufficiently small, with good reproducibility between thermal cycles to 800 C, output figures can be corrected within a reasonable margin of error.

Anisotropic effects on constitutive model parameters of aluminum alloys

NASA Astrophysics Data System (ADS)

Brar, Nachhatter S.; Joshi, Vasant S.

2012-03-01

Simulation of low velocity impact on structures or high velocity penetration in armor materials heavily rely on constitutive material models. Model constants are determined from tension, compression or torsion stress-strain at low and high strain rates at different temperatures. These model constants are required input to computer codes (LS-DYNA, DYNA3D or SPH) to accurately simulate fragment impact on structural components made of high strength 7075-T651 aluminum alloy. Johnson- Cook model constants determined for Al7075-T651 alloy bar material failed to simulate correctly the penetration into 1' thick Al-7075-T651plates. When simulation go well beyond minor parameter tweaking and experimental results show drastically different behavior it becomes important to determine constitutive parameters from the actual material used in impact/penetration experiments. To investigate anisotropic effects on the yield/flow stress of this alloy quasi-static and high strain rate tensile tests were performed on specimens fabricated in the longitudinal "L", transverse "T", and thickness "TH" directions of 1' thick Al7075 Plate. While flow stress at a strain rate of ~1/s as well as ~1100/s in the thickness and transverse directions are lower than the longitudinal direction. The flow stress in the bar was comparable to flow stress in the longitudinal direction of the plate. Fracture strain data from notched tensile specimens fabricated in the L, T, and Thickness directions of 1' thick plate are used to derive fracture constants.

Fatigue properties of JIS H3300 C1220 copper for strain life prediction

NASA Astrophysics Data System (ADS)

Harun, Muhammad Faiz; Mohammad, Roslina

2018-05-01

The existing methods for estimating strain life parameters are dependent on the material's monotonic tensile properties. However, a few of these methods yield quite complicated expressions for calculating fatigue parameters, and are specific to certain groups of materials only. The Universal Slopes method, Modified Universal Slopes method, Uniform Material Law, the Hardness method, and Medians method are a few existing methods for predicting strain-life fatigue based on monotonic tensile material properties and hardness of material. In the present study, nine methods for estimating fatigue life and properties are applied on JIS H3300 C1220 copper to determine the best methods for strain life estimation of this ductile material. Experimental strain-life curves are compared to estimations obtained using each method. Muralidharan-Manson's Modified Universal Slopes method and Bäumel-Seeger's method for unalloyed and low-alloy steels are found to yield batter accuracy in estimating fatigue life with a deviation of less than 25%. However, the prediction of both methods only yield much better accuracy for a cycle of less than 1000 or for strain amplitudes of more than 1% and less than 6%. Manson's Original Universal Slopes method and Ong's Modified Four-Point Correlation method are found to predict the strain-life fatigue of copper with better accuracy for a high number of cycles of strain amplitudes of less than 1%. The differences between mechanical behavior during monotonic and cyclic loading and the complexity in deciding the coefficient in an equation are probably the reason for the lack of a reliable method for estimating fatigue behavior using the monotonic properties of a group of materials. It is therefore suggested that a differential approach and new expressions be developed to estimate the strain-life fatigue parameters for ductile materials such as copper.

Design with high strength steel: A case of failure and its implications

NASA Astrophysics Data System (ADS)

Rahka, Klaus

1992-10-01

A recent proof test failure of a high strength steel pressure vessel is scrutinized. Apparent deficiencies in the procedures to account for elasto-plastic local strain are indicated for the applicable routine (code) strength calculations. Tentative guidance is given for the use of material tensile fracture strain and its strain state (plane strain) correction in fracture margin estimation. A hypothesis that the calculated local strain is comparable with a gauge length weighted tensile ductility for fracture to initiate at a notch root is given. A discussion about the actual implications of the failure case and the suggested remedy in the light of the ASME Boiler and Pressure Vessel Code section 3 and 8 is presented. Further needs for research and development are delineated. Possible yield and ductility related design limits and their use as material quality indices are discussed.

Identification of a thermo-elasto-viscoplastic behavior law for the simulation of thermoforming of high impact polystyrene

NASA Astrophysics Data System (ADS)

Atmani, O.; Abbès, B.; Abbès, F.; Li, Y. M.; Batkam, S.

2018-05-01

Thermoforming of high impact polystyrene sheets (HIPS) requires technical knowledge on material behavior, mold type, mold material, and process variables. Accurate thermoforming simulations are needed in the optimization process. Determining the behavior of the material under thermoforming conditions is one of the key parameters for an accurate simulation. The aim of this work is to identify the thermomechanical behavior of HIPS in the thermoforming conditions. HIPS behavior is highly dependent on temperature and strain rate. In order to reproduce the behavior of such material, a thermo-elasto-viscoplastic constitutive law was implement in the finite element code ABAQUS. The proposed model parameters are considered as thermo-dependent. The strain-dependence effect is introduced using Prony series. Tensile tests were carried out at different temperatures and strain rates. The material parameters were then identified using a NSGA-II algorithm. To validate the rheological model, experimental blowing tests were carried out on a thermoforming pilot machine. To compare the numerical results with the experimental ones the thickness distribution and the bubble shape were investigated.

Dielectric Actuation of Polymers

NASA Astrophysics Data System (ADS)

Niu, Xiaofan

Dielectric polymers are widely used in a plurality of applications, such as electrical insulation, dielectric capacitors, and electromechanical actuators. Dielectric polymers with large strain deformations under an electric field are named dielectric elastomers (DE), because of their relative low modulus, high elongation at break, and outstanding resilience. Dielectric elastomer actuators (DEA) are superior to traditional transducers as a muscle-like technology: large strains, high energy densities, high coupling efficiency, quiet operation, and light weight. One focus of this dissertation is on the design of DE materials with high performance and easy processing. UV radiation curing of reactive species is studied as a generic synthesis methodology to provide a platform for material scientists to customize their own DE materials. Oligomers/monomers, crosslinkers, and other additives are mixed and cured at appropriate ratios to control the stress-strain response, suppress electromechanical instability of the resulting polymers, and provide stable actuation strains larger than 100% and energy densities higher than 1 J/g. The processing is largely simplified in the new material system by removal of the prestretching step. Multilayer stack actuators with 11% linear strain are demonstrated in a procedure fully compatible with industrial production. A multifunctional DE derivative material, bistable electroactive polymer (BSEP), is invented enabling repeatable rigid-to-rigid deformation without bulky external structures. Bistable actuation allows the polymer actuator to have two distinct states that can support external load without device failure. Plasticizers are used to lower the glass transition temperature to 45 °C. Interpenetrating polymer network structure is established inside the BSEP to suppress electromechanical instability, providing a breakdown field of 194 MV/m and a stable bistable strain as large as 228% with a 97% strain fixity. The application of BSEP in tactile display is investigated by the prototyping of a large scale refreshable Braille display device. Braille is a critical way for the vision impaired community to learn literacy and improve life quality. Current piezoelectrics-based refreshable Braille display technologies are limited to up to 1 line of Braille text, due to the bulky size of bimorph actuators. Based on the unique actuation feature of BSEP, refreshable Braille display devices up to smartphone-size have been demonstrated by polymer sheet laminates. Dots in the devices can be individually controlled via incorporated field-driven BSEP actuators and Joule heater units. A composite material consisting of silver nanowires (AgNW) embedded in a polymer substrate is brought up as a compliant electrode candidate for BSEP application. The AgNW composite is highly conductive (Rs: 10 Ω/sq) and remains conductive at strains as high as 140% (Rs: <10 3 Ω/sq). The baseline conductivity has only small changes up to 90% strain, which makes it low enough for both field driving and stretchable Joule heating. An out-of-plane bistable area strain up to 68% under Joule heating is achieved.

High average power pockels cell

DOEpatents

Daly, Thomas P.

1991-01-01

A high average power pockels cell is disclosed which reduces the effect of thermally induced strains in high average power laser technology. The pockels cell includes an elongated, substantially rectangular crystalline structure formed from a KDP-type material to eliminate shear strains. The X- and Y-axes are oriented substantially perpendicular to the edges of the crystal cross-section and to the C-axis direction of propagation to eliminate shear strains.

A Continuum Model for the Effect of Dynamic Recrystallization on the Stress⁻Strain Response.

PubMed

Kooiker, H; Perdahcıoğlu, E S; van den Boogaard, A H

2018-05-22

Austenitic Stainless Steels and High-Strength Low-Alloy (HSLA) steels show significant dynamic recovery and dynamic recrystallization (DRX) during hot forming. In order to design optimal and safe hot-formed products, a good understanding and constitutive description of the material behavior is vital. A new continuum model is presented and validated on a wide range of deformation conditions including high strain rate deformation. The model is presented in rate form to allow for the prediction of material behavior in transient process conditions. The proposed model is capable of accurately describing the stress⁻strain behavior of AISI 316LN in hot forming conditions, also the high strain rate DRX-induced softening observed during hot torsion of HSLA is accurately predicted. It is shown that the increase in recrystallization rate at high strain rates observed in experiments can be captured by including the elastic energy due to the dynamic stress in the driving pressure for recrystallization. Furthermore, the predicted resulting grain sizes follow the power-law dependence with steady state stress that is often reported in literature and the evolution during hot deformation shows the expected trend.

On the relationships between hardness and the elastic and plastic properties of isotropic power-law hardening materials

NASA Astrophysics Data System (ADS)

Lan, Hongzhi; Venkatesh, T. A.

2014-01-01

A comprehensive understanding of the relationship between the hardness and the elastic and plastic properties for a wide range of materials is obtained by analysing the hardness characteristics (that are predicted by experimentally verified indentation analyses) of over 9000 distinct combinations of material properties that represent isotropic, homogeneous, power-law hardening metallic materials. Finite element analysis has been used to develop the indentation algorithms that provide the relationships between the elastic and plastic properties of the indented material and its indentation hardness. Based on computational analysis and virtual testing, the following observations are made. The hardness (H) of a material tends to increase with an increase in the elastic modulus (E), yield strength (σy) and the strain-hardening exponent (n). Several materials with different combinations of elastic and plastic properties can exhibit identical true hardness (for a particular indenter geometry/apex angle). In general, combinations of materials that exhibit relatively low elastic modulus and high yield strength or strain-hardening exponents and those that exhibit relatively high elastic modulus and low yield strength or strain-hardening exponents exhibit similar hardness properties. Depending on the strain-hardening characteristics of the indented material, (i.e. n = 0 or ?), the ratio H/σy ranges, respectively, from 2.2 to 2.6 or 2 to 20 (for indentations with a cone angle of 70.3°). The materials that have lower σy/E and higher n exhibit higher H/σy ratios. The commonly invoked relationship between hardness and the yield strength, i.e. H ≈ 3σy, is not generally valid or applicable for all power-law hardening materials. The indentation hardness of a power law hardening material can be taken as following the relationship H ≈ (2.1-2.8)σr where σr is the representative stress based on Tabor's representative strain for a wide range of materials.

Acoustic Performance of Resilient Materials Using Acrylic Polymer Emulsion Resin.

PubMed

Kim, Haseog; Park, Sangki; Lee, Seahyun

2016-07-19

There have been frequent cases of civil complaints and disputes in relation to floor impact noises over the years. To solve these issues, a substantial amount of sound resilient material is installed between the concrete slab and the foamed concrete during construction. A new place-type resilient material is made from cement, silica powder, sodium sulfate, expanded-polystyrene, anhydrite, fly ash, and acrylic polymer emulsion resin. Its physical characteristics such as density, compressive strength, dynamic stiffness, and remanent strain are analyzed to assess the acoustic performance of the material. The experimental results showed the density and the dynamic stiffness of the proposed resilient material is increased with proportional to the use of cement and silica powder due to the high contents of the raw materials. The remanent strain, related to the serviceability of a structure, is found to be inversely proportional to the density and strength. The amount of reduction in the heavyweight impact noise is significant in a material with high density, high strength, and low remanent strain. Finally, specimen no. R4, having the reduction level of 3 dB for impact ball and 1 dB for bang machine in the single number quantity level, respectively, is the best product to obtain overall acoustic performance.

Acoustic Performance of Resilient Materials Using Acrylic Polymer Emulsion Resin

PubMed Central

Kim, Haseog; Park, Sangki; Lee, Seahyun

2016-01-01

There have been frequent cases of civil complaints and disputes in relation to floor impact noises over the years. To solve these issues, a substantial amount of sound resilient material is installed between the concrete slab and the foamed concrete during construction. A new place-type resilient material is made from cement, silica powder, sodium sulfate, expanded-polystyrene, anhydrite, fly ash, and acrylic polymer emulsion resin. Its physical characteristics such as density, compressive strength, dynamic stiffness, and remanent strain are analyzed to assess the acoustic performance of the material. The experimental results showed the density and the dynamic stiffness of the proposed resilient material is increased with proportional to the use of cement and silica powder due to the high contents of the raw materials. The remanent strain, related to the serviceability of a structure, is found to be inversely proportional to the density and strength. The amount of reduction in the heavyweight impact noise is significant in a material with high density, high strength, and low remanent strain. Finally, specimen no. R4, having the reduction level of 3 dB for impact ball and 1 dB for bang machine in the single number quantity level, respectively, is the best product to obtain overall acoustic performance. PMID:28773711

Texture developed during deformation of Transformation Induced Plasticity (TRIP) steels

NASA Astrophysics Data System (ADS)

Bhargava, M.; Shanta, C.; Asim, T.; Sushil, M.

2015-04-01

Automotive industry is currently focusing on using advanced high strength steels (AHSS) due to its high strength and formability for closure applications. Transformation Induced Plasticity (TRIP) steel is promising material for this application among other AHSS. The present work is focused on the microstructure development during deformation of TRIP steel sheets. To mimic complex strain path condition during forming of automotive body, Limit Dome Height (LDH) tests were conducted and samples were deformed in servo hydraulic press to find the different strain path. FEM Simulations were done to predict different strain path diagrams and compared with experimental results. There is a significant difference between experimental and simulation results as the existing material models are not applicable for TRIP steels. Micro texture studies were performed on the samples using EBSD and X-RD techniques. It was observed that austenite is transformed to martensite and texture developed during deformation had strong impact on limit strain and strain path.

SVAS3: Strain Vector Aided Sensorization of Soft Structures.

PubMed

Culha, Utku; Nurzaman, Surya G; Clemens, Frank; Iida, Fumiya

2014-07-17

Soft material structures exhibit high deformability and conformability which can be useful for many engineering applications such as robots adapting to unstructured and dynamic environments. However, the fact that they have almost infinite degrees of freedom challenges conventional sensory systems and sensorization approaches due to the difficulties in adapting to soft structure deformations. In this paper, we address this challenge by proposing a novel method which designs flexible sensor morphologies to sense soft material deformations by using a functional material called conductive thermoplastic elastomer (CTPE). This model-based design method, called Strain Vector Aided Sensorization of Soft Structures (SVAS3), provides a simulation platform which analyzes soft body deformations and automatically finds suitable locations for CTPE-based strain gauge sensors to gather strain information which best characterizes the deformation. Our chosen sensor material CTPE exhibits a set of unique behaviors in terms of strain length electrical conductivity, elasticity, and shape adaptability, allowing us to flexibly design sensor morphology that can best capture strain distributions in a given soft structure. We evaluate the performance of our approach by both simulated and real-world experiments and discuss the potential and limitations.

High-Strain-Rate Compression Testing of Ice

NASA Technical Reports Server (NTRS)

Shazly, Mostafa; Prakash, Vikas; Lerch, Bradley A.

2006-01-01

In the present study a modified split Hopkinson pressure bar (SHPB) was employed to study the effect of strain rate on the dynamic material response of ice. Disk-shaped ice specimens with flat, parallel end faces were either provided by Dartmouth College (Hanover, NH) or grown at Case Western Reserve University (Cleveland, OH). The SHPB was adapted to perform tests at high strain rates in the range 60 to 1400/s at test temperatures of -10 and -30 C. Experimental results showed that the strength of ice increases with increasing strain rates and this occurs over a change in strain rate of five orders of magnitude. Under these strain rate conditions the ice microstructure has a slight influence on the strength, but it is much less than the influence it has under quasi-static loading conditions. End constraint and frictional effects do not influence the compression tests like they do at slower strain rates, and therefore the diameter/thickness ratio of the samples is not as critical. The strength of ice at high strain rates was found to increase with decreasing test temperatures. Ice has been identified as a potential source of debris to impact the shuttle; data presented in this report can be used to validate and/or develop material models for ice impact analyses for shuttle Return to Flight efforts.

Characterization of mechanical damage mechanisms in ceramic composite materials. Technical report, 23 May 1987-24 May 1988

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lankford, J.

High-strain-rate compressive failure mechanisms in fiber-reinforced ceramic-matrix composite materials were characterized. These are contrasted with composite damage development at low-strain rates, and with the dynamic failure of monolithic ceramics. It is shown that it is possible to derive major strain-rate strengthening benefits if a major fraction of the fiber reinforcement is aligned with the load axis. This effect considerably exceeds the inertial microfracture strengthening observed in monolithic ceramics, and non-aligned composites. Its basis is shown to be the trans-specimen propagation time period for heterogeneously-nucleated, high-strain kink bands. A brief study on zirconia focused on the remarkable inverse strength-strain rate resultmore » previously observed for both fully and partially-stabilized zirconia single crystals, whereby the strength decreased with increasing strain rate. Based on the hypothesis that the suppression of microplastic flow, hence, local stress relaxation, might be responsible for this behavior, fully stabilized (i.e., non-transformable) specimens were strain-gaged and subjected to compressive microstrain. The rather stunning observation was that the crystals are highly microplastic, exhibiting plastic yield on loading and anelasticity and reverse plasticity upon unloading. These results clearly support the hypothesis that with increasing strain rate, microcracking is favored at the expense of microplasticity.« less

Strain Rate and Anisotropic Microstructure Dependent Mechanical Behaviors of Silkworm Cocoon Shells

PubMed Central

Xu, Jun; Zhang, Wen; Gao, Xiang; Meng, Wanlin; Guan, Juan

2016-01-01

Silkworm cocoons are multi-layered composite structures comprised of high strength silk fiber and sericin, and their mechanical properties have been naturally selected to protect pupas during metamorphosis from various types of external attacks. The present study attempts to gain a comprehensive understanding of the mechanical properties of cocoon shell materials from wild silkworm species Antheraea pernyi under dynamic loading rates. Five dynamic strain rates from 0.00625 s-1 to 12.5 s-1 are tested to show the strain rate sensitivity of the cocoon shell material. In the meantime, the anisotropy of the cocoon shell is considered and the cocoon shell specimens are cut along 0°, 45° and 90° orientation to the short axis of cocoons. Typical mechanical properties including Young’s modulus, yield strength, ultimate strength and ultimate strain are extracted and analyzed from the stress-strain curves. Furthermore, the fracture morphologies of the cocoon shell specimens are observed under scanning electron microscopy to help understand the relationship between the mechanical properties and the microstructures of the cocoon material. A discussion on the dynamic strain rate effect on the mechanical properties of cocoon shell material is followed by fitting our experimental results to two previous models, and the effect could be well explained. We also compare natural and dried cocoon materials for the dynamic strain rate effect and interestingly the dried cocoon shells show better overall mechanical properties. This study provides a different perspective on the mechanical properties of cocoon material as a composite material, and provides some insight for bio-inspired engineering materials. PMID:26939063

Flat-band superconductivity in strained Dirac materials

NASA Astrophysics Data System (ADS)

Kauppila, V. J.; Aikebaier, F.; Heikkilä, T. T.

2016-06-01

We consider superconducting properties of a two-dimensional Dirac material such as graphene under strain that produces a flat-band spectrum in the normal state. We show that in the superconducting state, such a model results in a highly increased critical temperature compared to the case without the strain, inhomogeneous order parameter with two-peak shaped local density of states and yet a large and almost uniform and isotropic supercurrent. This model could be realized in strained graphene or ultracold atom systems and could be responsible for unusually strong superconductivity observed in some graphite interfaces and certain IV-VI semiconductor heterostructures.

Variation of strain rate sensitivity index of a superplastic aluminum alloy in different testing methods

NASA Astrophysics Data System (ADS)

Majidi, Omid; Jahazi, Mohammad; Bombardier, Nicolas; Samuel, Ehab

2017-10-01

The strain rate sensitivity index, m-value, is being applied as a common tool to evaluate the impact of the strain rate on the viscoplastic behaviour of materials. The m-value, as a constant number, has been frequently taken into consideration for modeling material behaviour in the numerical simulation of superplastic forming processes. However, the impact of the testing variables on the measured m-values has not been investigated comprehensively. In this study, the m-value for a superplastic grade of an aluminum alloy (i.e., AA5083) has been investigated. The conditions and the parameters that influence the strain rate sensitivity for the material are compared with three different testing methods, i.e., monotonic uniaxial tension test, strain rate jump test and stress relaxation test. All tests were conducted at elevated temperature (470°C) and at strain rates up to 0.1 s-1. The results show that the m-value is not constant and is highly dependent on the applied strain rate, strain level and testing method.

Interactions between creep, fatigue and strain aging in two refractory alloys

NASA Technical Reports Server (NTRS)

Sheffler, K. D.

1972-01-01

The application of low-amplitude, high-frequency fatigue vibrations during creep testing of two strain-aging refractory alloys (molybdenum-base TZC and tantalum-base T-111) significantly reduced the creep strength of these materials. This strength reduction caused dramatic increases in both the first stage creep strain and the second stage creep rate. The magnitude of the creep rate acceleration varied directly with both frequency and A ratio (ratio of alternating to mean stress), and also varied with temperature, being greatest in the range where the strain-aging phenomenon was most prominent. It was concluded that the creep rate acceleration resulted from a negative strain rate sensitivity which is associated with the strain aging phenomenon in these materials. (A negative rate sensitivity causes flow stress to decrease with increasing strain rate, instead of increasing as in normal materials). By combining two analytical expressions which are normally used to describe creep and strain aging behavior, an expression was developed which correctly described the influence of temperature, frequency, and A ratio on the TZC creep rate acceleration.

Mechanism-Based Modeling for Low Cycle Fatigue of Cast Austenitic Steel

NASA Astrophysics Data System (ADS)

Wu, Xijia; Quan, Guangchun; Sloss, Clayton

2017-09-01

A mechanism-based approach—the integrated creep-fatigue theory (ICFT)—is used to model low cycle fatigue behavior of 1.4848 cast austenitic steel over the temperature range from room temperature (RT) to 1173 K (900 °C) and the strain rate range from of 2 × 10-4 to 2 × 10-2 s-1. The ICFT formulates the material's constitutive equation based on the physical strain decomposition into mechanism strains, and the associated damage accumulation consisting of crack nucleation and propagation in coalescence with internally distributed damage. At room temperature, the material behavior is controlled by plasticity, resulting in a rate-independent and cyclically stable behavior. The material exhibits significant cyclic hardening at intermediate temperatures, 673 K to 873 K (400 °C to 600 °C), with negative strain rate sensitivity, due to dynamic strain aging. At high temperatures >1073 K (800 °C), time-dependent deformation is manifested with positive rate sensitivity as commonly seen in metallic materials at high temperature. The ICFT quantitatively delineates the contribution of each mechanism in damage accumulation, and predicts the fatigue life as a result of synergistic interaction of the above identified mechanisms. The model descriptions agree well with the experimental and fractographic observations.

A numerical and experimental study of temperature effects on deformation behavior of carbon steels at high strain rates

NASA Astrophysics Data System (ADS)

Pouya, M.; Winter, S.; Fritsch, S.; F-X Wagner, M.

2017-03-01

Both in research and in the light of industrial applications, there is a growing interest in methods to characterize the mechanical behavior of materials at high strain rates. This is particularly true for steels (the most important structural materials), where often the strain rate-dependent material behavior also needs to be characterized in a wide temperature range. In this study, we use the Finite Element Method (FEM), first, to model the compressive deformation behavior of carbon steels under quasi-static loading conditions. The results are then compared to experimental data (for a simple C75 steel) at room temperature, and up to testing temperatures of 1000 °C. Second, an explicit FEM model that captures wave propagation phenomena during dynamic loading is developed to closely reflect the complex loading conditions in a Split-Hopkinson Pressure Bar (SHPB) - an experimental setup that allows loading of compression samples with strain rates up to 104 s-1 The dynamic simulations provide a useful basis for an accurate analysis of dynamically measured experimental data, which considers reflected elastic waves. By combining numerical and experimental investigations, we derive material parameters that capture the strain rate- and temperature-dependent behavior of the C75 steel from room temperature to 1000 °C, and from quasi-static to dynamic loading.

Finite Element Modeling of the Behavior of Armor Materials Under High Strain Rates and Large Strains

NASA Astrophysics Data System (ADS)

Polyzois, Ioannis

For years high strength steels and alloys have been widely used by the military for making armor plates. Advances in technology have led to the development of materials with improved resistance to penetration and deformation. Until recently, the behavior of these materials under high strain rates and large strains has been primarily based on laboratory testing using the Split Hopkinson Pressure Bar apparatus. With the advent of sophisticated computer programs, computer modeling and finite element simulations are being developed to predict the deformation behavior of these metals for a variety of conditions similar to those experienced during combat. In the present investigation, a modified direct impact Split Hopkinson Pressure Bar apparatus was modeled using the finite element software ABAQUS 6.8 for the purpose of simulating high strain rate compression of specimens of three armor materials: maraging steel 300, high hardness armor (HHA), and aluminum alloy 5083. These armor materials, provided by the Canadian Department of National Defence, were tested at the University of Manitoba by others. In this study, the empirical Johnson-Cook visco-plastic and damage models were used to simulate the deformation behavior obtained experimentally. A series of stress-time plots at various projectile impact momenta were produced and verified by comparison with experimental data. The impact momentum parameter was chosen rather than projectile velocity to normalize the initial conditions for each simulation. Phenomena such as the formation of adiabatic shear bands caused by deformation at high strains and strain rates were investigated through simulations. It was found that the Johnson-Cook model can accurately simulate the behavior of body-centered cubic (BCC) metals such as steels. The maximum shear stress was calculated for each simulation at various impact momenta. The finite element model showed that shear failure first occurred in the center of the cylindrical specimen and propagated outwards diagonally towards the front and back edges forming an hourglass pattern. This pattern matched the failure behavior of specimens tested experimentally, which also exhibited failure through the formation of adiabatic shear bands. Adiabatic shear bands are known to lead to a complete shear failure. Both mechanical and thermal mechanisms contribute to the formation of shear bands. However, the finite element simulations did not show the effects of temperature rise within the material, a phenomenon which is known to contribute to thermal instabilities, whereby strain hardening effects are outweighed by thermal softening effects and adiabatic shear bands begin to form. In the simulations, the purely mechanical maximum shear stress failure, nucleating from the center of the specimens, was used as an indicator of the time at which these shear bands begin to form. The time and compressive stress at the moment of thermal instability in experimental results which have shown to form adiabatic shear bands, matched closely to those at which shear failure was first observed in the simulations. Although versatile in modeling BCC behavior, the Johnson-Cook model did not show the correct stress response in face-centered cubic (FCC) metals, such as aluminum 5083, where effects of strain rate and temperature depend on strain. Similar observations have been reported in literature. In the Johnson-Cook model, temperature, strain rate and strain" parameters are independent of each other. To this end, a more physical-based model based on dislocation mechanics, namely the Feng and Bassim constitutive model, would be more appropriate.

Implementation of Improved Transverse Shear Calculations and Higher Order Laminate Theory Into Strain Rate Dependent Analyses of Polymer Matrix Composites

NASA Technical Reports Server (NTRS)

Zhu, Lin-Fa; Kim, Soo; Chattopadhyay, Aditi; Goldberg, Robert K.

2004-01-01

A numerical procedure has been developed to investigate the nonlinear and strain rate dependent deformation response of polymer matrix composite laminated plates under high strain rate impact loadings. A recently developed strength of materials based micromechanics model, incorporating a set of nonlinear, strain rate dependent constitutive equations for the polymer matrix, is extended to account for the transverse shear effects during impact. Four different assumptions of transverse shear deformation are investigated in order to improve the developed strain rate dependent micromechanics model. The validities of these assumptions are investigated using numerical and theoretical approaches. A method to determine through the thickness strain and transverse Poisson's ratio of the composite is developed. The revised micromechanics model is then implemented into a higher order laminated plate theory which is modified to include the effects of inelastic strains. Parametric studies are conducted to investigate the mechanical response of composite plates under high strain rate loadings. Results show the transverse shear stresses cannot be neglected in the impact problem. A significant level of strain rate dependency and material nonlinearity is found in the deformation response of representative composite specimens.

Operando Synchrotron Measurement of Strain Evolution in Individual Alloying Anode Particles within Lithium Batteries

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cortes, Francisco Javier Quintero; Boebinger, Matthew G.; Xu, Michael

Alloying anode materials offer high capacity for next-generation batteries, but the performance of these materials often decays rapidly with cycling because of volume changes and associated mechanical degradation or fracture. The direct measurement of crystallographic strain evolution in individual particles has not been reported, however, and this level of insight is critical for designing mechanically resilient materials. Here, we use operando X-ray diffraction to investigate strain evolution in individual germanium microparticles during electrochemical reaction with lithium. The diffraction peak was observed to shift in position and diminish in intensity during reaction because of the disappearance of the crystalline Ge phase.more » The compressive strain along the [111] direction was found to increase monotonically to a value of -0.21%. This finding is in agreement with a mechanical model that considers expansion and plastic deformation during reaction. This new insight into the mechanics of large-volume-change transformations in alloying anodes is important for improving the durability of high-capacity batteries.« less

Application of the time-temperature superposition principle to the mechanical characterization of elastomeric adhesives for crash simulation purposes

NASA Astrophysics Data System (ADS)

Rauh, A.; Hinterhölzl, R.; Drechsler, K.

2012-05-01

In the automotive industry, finite element simulation is widely used to ensure crashworthiness. Mechanical material data over wide strain rate and temperature ranges are required as a basis. This work proposes a method reducing the cost of mechanical material characterization by using the time-temperature superposition principle on elastomeric adhesives. The method is based on the time and temperature interdependence which is characteristic for mechanical properties of polymers. Based on the assumption that polymers behave similarly at high strain rates and at low temperatures, a temperature-dominated test program is suggested, which can be used to deduce strain rate dependent material behavior at different reference temperatures. The temperature shift factor is found by means of dynamic mechanical analysis according to the WLF-equation, named after Williams, Landel and Ferry. The principle is applied to the viscoelastic properties as well as to the failure properties of the polymer. The applicability is validated with high strain rate tests.

Comparison of epoxy-based encapsulating materials over temperature and strain rate

NASA Astrophysics Data System (ADS)

Khan, Amnah S.; Wilgeroth, James; Balzer, Jens; Proud, William G.

2017-01-01

The highly insulating, adhesive and bonding properties of thermosetting epoxies, their ability to be injection moulded in an uncured state, as well as their presence in a wide number of composites, has resulted in their widespread use in both electrical and aerospace applications. There is thus a need to understand the compressive response of epoxies over the range of temperatures likely to be experienced within their working environment. The effects of varying strain rates and temperatures on an epoxy resin (Scotchcast 8) and an epoxy-based syntactic foam (Stycast 1090) were investigated. The samples were studied from -20 °C to +80 °C over a range of strain rates (10-4 - 10+3 s-1). Stress-strain data was obtained, with further analysis from high-speed images. Dynamic Mechanical Analysis (DMA) was also performed on the two materials. Data obtained from these experiments demonstrated key differences in the behaviour of the two materials, forming a basis for comparison with numerical simulations.

Calculation of Debye-Scherrer diffraction patterns from highly stressed polycrystalline materials

DOE PAGES

MacDonald, M. J.; Vorberger, J.; Gamboa, E. J.; ...

2016-06-07

Calculations of Debye-Scherrer diffraction patterns from polycrystalline materials have typically been done in the limit of small deviatoric stresses. Although these methods are well suited for experiments conducted near hydrostatic conditions, more robust models are required to diagnose the large strain anisotropies present in dynamic compression experiments. A method to predict Debye-Scherrer diffraction patterns for arbitrary strains has been presented in the Voigt (iso-strain) limit. Here, we present a method to calculate Debye-Scherrer diffraction patterns from highly stressed polycrystalline samples in the Reuss (iso-stress) limit. This analysis uses elastic constants to calculate lattice strains for all initial crystallite orientations, enablingmore » elastic anisotropy and sample texture effects to be modeled directly. Furthermore, the effects of probing geometry, deviatoric stresses, and sample texture are demonstrated and compared to Voigt limit predictions. An example of shock-compressed polycrystalline diamond is presented to illustrate how this model can be applied and demonstrates the importance of including material strength when interpreting diffraction in dynamic compression experiments.« less

Mechanical Properties of Transgenic Silkworm Silk Under High Strain Rate Tensile Loading

NASA Astrophysics Data System (ADS)

Chu, J.-M.; Claus, B.; Chen, W.

2017-12-01

Studies have shown that transgenic silkworm silk may be capable of having similar properties of spider silk while being mass-producible. In this research, the tensile stress-strain response of transgenic silkworm silk fiber is systematically characterized using a quasi-static load frame and a tension Kolsky bar over a range of strain-rates between 10^{-3} and 700/s. The results show that transgenic silkworm silk tends to have higher overall ultimate stress and failure strain at high strain rate (700/s) compared to quasi-static strain rates, indicating rate sensitivity of the material. The failure strain at the high strain rate is higher than that of spider silk. However, the stress levels are significantly below that of spider silk, and far below that of high-performance fiber. Failure surfaces are examined via scanning electron microscopy and reveal that the failure modes are similar to those of spider silk.

Tensile behaviour of geopolymer-based materials under medium and high strain rates

NASA Astrophysics Data System (ADS)

Menna, Costantino; Asprone, Domenico; Forni, Daniele; Roviello, Giuseppina; Ricciotti, Laura; Ferone, Claudio; Bozza, Anna; Prota, Andrea; Cadoni, Ezio

2015-09-01

Geopolymers are a promising class of inorganic materials typically obtained from an alluminosilicate source and an alkaline solution, and characterized by an amorphous 3-D framework structure. These materials are particularly attractive for the construction industry due to mechanical and environmental advantages they exhibit compared to conventional systems. Indeed, geopolymer-based concretes represent a challenge for the large scale uses of such a binder material and many research studies currently focus on this topic. However, the behaviour of geopolymers under high dynamic loads is rarely investigated, even though it is of a fundamental concern for the integrity/vulnerability assessment under extreme dynamic events. The present study aims to investigate the effect of high dynamic loading conditions on the tensile behaviour of different geopolymer formulations. The dynamic tests were performed under different strain rates by using a Hydro-pneumatic machine and a modified Hopkinson bar at the DynaMat laboratory of the University of Applied Sciences of Southern Switzerland. The results are processed in terms of stress-strain relationships and strength dynamic increase factor at different strain-rate levels. The dynamic increase factor was also compared with CEB recommendations. The experimental outcomes can be used to assess the constitutive laws of geopolymers under dynamic load conditions and implemented into analytical models.

A Facile and General Approach to Recoverable High-Strain Multishape Shape Memory Polymers.

PubMed

Li, Xingjian; Pan, Yi; Zheng, Zhaohui; Ding, Xiaobin

2018-03-01

Fabricating a single polymer network with no need to design complex structures to achieve an ideal combination of tunable high-strain multiple-shape memory effects and highly recoverable shape memory property is a great challenge for the real applications of advanced shape memory devices. Here, a facile and general approach to recoverable high-strain multishape shape memory polymers is presented via a random copolymerization of acrylate monomers and a chain-extended multiblock copolymer crosslinker. As-prepared shape memory networks show a large width at the half-peak height of the glass transition, far wider than current classical multishape shape memory polymers. A combination of tunable high-strain multishape memory effect and as high as 1000% recoverable strain in a single chemical-crosslinking network can be obtained. To the best of our knowledge, this is the first thermosetting material with a combination of highly recoverable strain and tunable high-strain multiple-shape memory effects. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Electrical Properties of Materials for Elevated Temperature Resistance Strain Gage Application. Ph.D. Thesis

NASA Technical Reports Server (NTRS)

Lei, Jih-Fen

1987-01-01

The objective was to study the electrical resistances of materials that are potentially useful as resistance strain gages at 1000 C. Transition metal carbides and nitrides, boron carbide and silicon carbide were selected for the experimental phase of this research. Due to their low temperature coefficient of resistance and good stability, TiC, ZrC, B sub 4 C and beta-SiC are suggested as good candidates for high temperature resistance strain gage applications.

Dynamic Behavior of AA2519-T8 Aluminum Alloy Under High Strain Rate Loading in Compression

NASA Astrophysics Data System (ADS)

Olasumboye, A. T.; Owolabi, G. M.; Odeshi, A. G.; Yilmaz, N.; Zeytinci, A.

2018-06-01

In this study, the effects of strain rate on the dynamic behavior, microstructure evolution and hence, failure of the AA2519-T8 aluminum alloy were investigated under compression at strain rates ranging from 1000 to 3500 s-1. Cylindrical specimens of dimensions 3.3 mm × 3.3 mm (L/D = 1) were tested using the split-Hopkinson pressure bar integrated with a digital image correlation system. The microstructure of the alloy was assessed using optical and scanning electron microscopes. Results showed that the dynamic yield strength of the alloy is strain rate dependent, with the maximum yield strength attained by the material being 500 MPa. The peak flow stress of 562 MPa was attained by the material at 3500 s-1. The alloy also showed a significant rate of strain hardening that is typical of other Al-Cu alloys; the rate of strain hardening, however, decreased with increase in strain rate. It was determined that the strain rate sensitivity coefficient of the alloy within the range of high strain rates used in this study is approximately 0.05 at 0.12 plastic strain; a more significant value than what was reported in literature under quasi-static loading. Micrographs obtained showed potential sites for the evolution of adiabatic shear band at 3500 s-1, with a characteristic circular-shaped surface profile comprising partially dissolved second phase particles in the continuous phase across the incident plane of the deformed specimen. The regions surrounding the site showed little or no change in the size of particles. However, the constituent coarse particles were observed as agglomerations of fractured pieces, thus having a shape factor different from those contained in the as-received alloy. Since the investigated alloy is a choice material for military application where it can be exposed to massive deformation at high strain rates, this study provides information on its microstructural and mechanical responses to such extreme loading condition.

Dynamic Behavior of AA2519-T8 Aluminum Alloy Under High Strain Rate Loading in Compression

NASA Astrophysics Data System (ADS)

Olasumboye, A. T.; Owolabi, G. M.; Odeshi, A. G.; Yilmaz, N.; Zeytinci, A.

2018-02-01

In this study, the effects of strain rate on the dynamic behavior, microstructure evolution and hence, failure of the AA2519-T8 aluminum alloy were investigated under compression at strain rates ranging from 1000 to 3500 s-1. Cylindrical specimens of dimensions 3.3 mm × 3.3 mm (L/D = 1) were tested using the split-Hopkinson pressure bar integrated with a digital image correlation system. The microstructure of the alloy was assessed using optical and scanning electron microscopes. Results showed that the dynamic yield strength of the alloy is strain rate dependent, with the maximum yield strength attained by the material being 500 MPa. The peak flow stress of 562 MPa was attained by the material at 3500 s-1. The alloy also showed a significant rate of strain hardening that is typical of other Al-Cu alloys; the rate of strain hardening, however, decreased with increase in strain rate. It was determined that the strain rate sensitivity coefficient of the alloy within the range of high strain rates used in this study is approximately 0.05 at 0.12 plastic strain; a more significant value than what was reported in literature under quasi-static loading. Micrographs obtained showed potential sites for the evolution of adiabatic shear band at 3500 s-1, with a characteristic circular-shaped surface profile comprising partially dissolved second phase particles in the continuous phase across the incident plane of the deformed specimen. The regions surrounding the site showed little or no change in the size of particles. However, the constituent coarse particles were observed as agglomerations of fractured pieces, thus having a shape factor different from those contained in the as-received alloy. Since the investigated alloy is a choice material for military application where it can be exposed to massive deformation at high strain rates, this study provides information on its microstructural and mechanical responses to such extreme loading condition.

Influence of subsolvus thermomechanical processing on the low-cycle fatigue properties of haynes 230 alloy

NASA Astrophysics Data System (ADS)

Vecchio, Kenneth S.; Fitzpatrick, Michael D.; Klarstrom, Dwaine

1995-03-01

Strain-controlled low-cycle fatigue tests have been conducted in air at elevated temperature to determine the influence of subsolvus thermomechanical processing on the low-cycle fatigue (LCF) behavior of HAYNES 230 alloy. A series of tests at various strain ranges was conducted on material experimentally processed at 1121 °C, which is below the M23C6 carbide solvus temperature, and on material fully solution annealed at 1232 °C. A comparative strain-life analysis was performed on the LCF results, and the cyclic hardening/softening characteristics were examined. At 760 °C and 871 °C, the fatigue life of the experimental 230/1121 material was improved relative to the standard 230/1232 material up to a factor of 3. The fatigue life advantage of the experimental material was related primarily to a lower plastic (inelastic) strain amplitude response for a given imposed total strain range. It appears the increase in monotonic flow stress exhibited by the finer grain size experimental material has been translated into an increase in cyclic flow stress at the 760 °C and 871 °C test temperatures. Both materials exhibited entirely transgranular fatigue crack initiation and propagation modes at these temperatures. The LCF performance of the experimental material in tests performed at 982 °C was improved relative to the standard material up to a factor as high as 2. The life advantage of the 230/1121 material occurred despite having a larger plastic strain amplitude than the standard 230/1232 material for a given total strain range. Though not fully understood at present, it is suspected that this behavior is related to the deleterious influence of grain boundaries in the fatigue crack initiations of the standard processed material relative to the experimental material, and ultimately to differences in carbide morphology as a result of thermomechanical processing.

Strain-induced phenomenon in complex oxide thin films

NASA Astrophysics Data System (ADS)

Haislmaier, Ryan

Complex oxide materials wield an immense spectrum of functional properties such as ferroelectricity, ferromagnetism, magnetoelectricity, optoelectricity, optomechanical, magnetoresistance, superconductivity, etc. The rich coupling between charge, spin, strain, and orbital degrees of freedom makes this material class extremely desirable and relevant for next generation electronic devices and technologies which are trending towards nanoscale dimensions. Development of complex oxide thin film materials is essential for realizing their integration into nanoscale electronic devices, where theoretically predicted multifunctional capabilities of oxides could add tremendous value. Employing thin film growth strategies such as epitaxial strain and heterostructure interface engineering can greatly enhance and even unlock novel material properties in complex oxides, which will be the main focus of this work. However, physically incorporating oxide materials into devices remains a challenge. While advancements in molecular beam epitaxy (MBE) of thin film oxide materials has led to the ability to grow oxide materials with atomic layer precision, there are still major limitations such as controlling stoichiometric compositions during growth as well as creating abrupt interfaces in multi-component layered oxide structures. The work done in this thesis addresses ways to overcome these limitations in order to harness intrinsic material phenomena. The development of adsorption-controlled stoichiometric growth windows of CaTiO3 and SrTiO3 thin film materials grown by hybrid MBE where Ti is supplied using metal-organic titanium tetraisopropoxide material is thoroughly outlined. These growth windows enable superior epitaxial strain-induced ferroelectric and dielectric properties to be accessed as demonstrated by chemical, structural, electrical, and optical characterization techniques. For tensile strained CaTiO3 and compressive strained SrTiO 3 films, the critical effects of nonstoichiometry on ferroelectric properties are investigated, where enhanced ferroelectric responses are only found for stoichiometric films grown inside of the growth windows, whereas outside of the optimal growth window conditions, ferroelectric properties are greatly deteriorated and eventually disappear for highly nonstoichiometric film compositions. Utilizing these stoichiometric growth windows, high temperature polar phase transitions are discovered for compressively strained CaTiO3 films with transition temperatures in excess of 700 K, rendering this material as a strong candidate for high temperature electronic applications. Beyond the synthesis of single phase materials using hybrid MBE, a methodology is presented for constructing layered (SrTiO3)n/(CaTiO 3)n superlattice structures, where precise control over the unit cell layering thickness (n) is demonstrated using in-situ reflection high energy electron diffraction. The effects of interface roughness and layering periodicity (n) on the strain-induced ferroelectric properties for a series of n=1-10 (SrTiO3)n/(CaTiO3) n superlattice films are investigated. It is found that the stabilization of a ferroelectric phase is independent of n, but is however strongly dominated by the degree of interface roughness which is quantified by measuring the highest nth order X-ray diffraction peak splitting of each superlattice film. A counter-intuitive realization is made whereby a critical amount of interface roughness is required in order to enable the formation of the predicted strain-stabilized ferroelectric phase, whereas sharp interfaces actually suppress this ferroelectric phase from manifesting. It is shown how high-quality complex oxide superlattices can be constructed using hybrid MBE technique, allowing the ability to control layered materials at the atomic scale. Furthermore, a detailed growth methodology is provided for constructing a layered n=4 SrO(SrTiO3)n Ruddlesden-Popper (RP) phase by hybrid MBE, where the ability to deposit single monolayers of SrO and TiO2 is utilized to build the RP film structure over a time period of 5 hours. This is the first time that a thin film RP phase has been grown using hybrid MBE, where an a stable control over the fluxes is demonstrated during relatively long time periods of growth, which advantageously facilitates the synthesis of high-quality RP materials with excellent structural and chemical homogeneity. Additionally, this work demonstrates some major advancements in optical second harmonic generation (SHG) characterization techniques of ferroelectric thin film materials. The SHG characterization techniques developed here proved to be the 'bread-and-butter' for most of the work performed in this thesis, providing a powerful tool for identifying the existence of strain-induced ferroelectric phases, including their temperature dependence and polar symmetry. The work presented in this dissertation will hopefully provide a preliminary road map for future hybrid MBE growers, scientists and researchers, to develop and investigate epitaxial strain and heterostructure layering induced phenomena in other complex oxide systems.

Identification of strained black phosphorous by Raman spectroscopy

NASA Astrophysics Data System (ADS)

Wan, Jiawei; Guo, Junhong; Hu, Fangren

2017-04-01

Phosphorene has a very high hole mobility and can be a tuned band structure, and has become an ideal material for electronic devices. For this new type of two-dimensional material, in the applied strain, black phosphorus (BP) can be changed into an indirect band gap and metallic materials from the direct band gap semiconductor material, which greatly affect its inherent physical characteristics. How to identify strained microstructure changes becomes an important problem. The calculated Raman spectra disclose that the A{}{{g}}2 mode and B{}2{{g}} mode will split and the Raman spectra appear, while the A{}{{g}}1 mode is shifted to low-frequency region. The deformation induced by strain will effectively change the Raman mode position and intensity, this can be used to identify phosphorus changes. Project supported by the National Science Foundation of China (Nos. 61505085, 61574080, 61274127) and the Innovation Project of Jiangsu Graduate Student, China (No. SJLX15_0379).

Revisit to three-dimensional percolation theory: Accurate analysis for highly stretchable conductive composite materials

PubMed Central

Kim, Sangwoo; Choi, Seongdae; Oh, Eunho; Byun, Junghwan; Kim, Hyunjong; Lee, Byeongmoon; Lee, Seunghwan; Hong, Yongtaek

2016-01-01

A percolation theory based on variation of conductive filler fraction has been widely used to explain the behavior of conductive composite materials under both small and large deformation conditions. However, it typically fails in properly analyzing the materials under the large deformation since the assumption may not be valid in such a case. Therefore, we proposed a new three-dimensional percolation theory by considering three key factors: nonlinear elasticity, precisely measured strain-dependent Poisson’s ratio, and strain-dependent percolation threshold. Digital image correlation (DIC) method was used to determine actual Poisson’s ratios at various strain levels, which were used to accurately estimate variation of conductive filler volume fraction under deformation. We also adopted strain-dependent percolation threshold caused by the filler re-location with deformation. When three key factors were considered, electrical performance change was accurately analyzed for composite materials with both isotropic and anisotropic mechanical properties. PMID:27694856

High Strain Rate Deformation Modeling of a Polymer Matrix Composite. Part 2; Composite Micromechanical Model

NASA Technical Reports Server (NTRS)

Goldberg, Robert K.; Stouffer, Donald C.

1998-01-01

Recently applications have exposed polymer matrix composite materials to very high strain rate loading conditions, requiring an ability to understand and predict the material behavior under these extreme conditions. In this second paper of a two part report, a three-dimensional composite micromechanical model is described which allows for the analysis of the rate dependent, nonlinear deformation response of a polymer matrix composite. Strain rate dependent inelastic constitutive equations utilized to model the deformation response of a polymer are implemented within the micromechanics method. The deformation response of two representative laminated carbon fiber reinforced composite materials with varying fiber orientation has been predicted using the described technique. The predicted results compare favorably to both experimental values and the response predicted by the Generalized Method of Cells, a well-established micromechanics analysis method.

Strain engineering of van der Waals heterostructures.

PubMed

Vermeulen, Paul A; Mulder, Jefta; Momand, Jamo; Kooi, Bart J

2018-01-18

Modifying the strain state of solids allows control over a plethora of functional properties. The weak interlayer bonding in van der Waals (vdWaals) materials such as graphene, hBN, MoS 2 , and Bi 2 Te 3 might seem to exclude strain engineering, since strain would immediately relax at the vdWaals interfaces. Here we present direct observations of the contrary by showing growth of vdWaals heterostructures with persistent in-plane strains up to 5% and we show that strain relaxation follows a not yet reported process distinctly different from strain relaxation in three-dimensionally bonded (3D) materials. For this, 2D bonded Bi 2 Te 3 -Sb 2 Te 3 and 2D/3D bonded Bi 2 Te 3 -GeTe multilayered films are grown using Pulsed Laser Deposition (PLD) and their structure is monitored in situ using Reflective High Energy Electron Diffraction (RHEED) and post situ analysis is performed using Transmission Electron Microscopy (TEM). Strain relaxation is modeled and found to solely depend on the layer being grown and its initial strain. This insight demonstrates that strain engineering of 2D bonded heterostructures obeys different rules than hold for epitaxial 3D materials and opens the door to precise tuning of the strain state of the individual layers to optimize functional performance of vdWaals heterostructures.

Channeling techniques to study strains and defects in heterostructures and multi quantum wells

NASA Astrophysics Data System (ADS)

Pathak, A. P.; Dhamodaran, S.; Sathish, N.

2005-08-01

The importance and advantages of heterostructures and Quantum Wells (QWs) in device technology has made research challenging due to lack of direct techniques for their characterization. Particularly the characterization of strain and defects at the interfaces has become important due to their dominance in the electrical and optical properties of materials and devices. RBSiC has been used to study variety of defects in single crystalline materials, for nearly four decades now. Channeling based experiments play a crucial role in giving depth information of strain and defects. Ion beams are used for both material characterizations as well as for modifications. Hence it is also possible to monitor the modifications online, which are discussed in detail. In the present work, Swift Heavy Ion (SHI) modification of III-V semiconductor heterostnictures and MQWs and the results of subsequent strain measurements by RBSiC in initially strained as well as lattice matched systems are discussed. We find that the compressive strain decreases due to SHI irradiation and a tensile strain is induced in an initially lattice matched system. The incident ion fluence dependence of strain modifications in the heterostructures will also be discussed. The use of high energy channeling for better sensitivity of strain measurements in low mismatch materials will be discussed in detail. Wherever possible, a comparison of results with those obtained by other techniques like HRXRD is given.

Viscoelastic Response Of A Highly Filled Polymer

NASA Technical Reports Server (NTRS)

Peng, Steven T. J.; Landel, Robert F.

1992-01-01

Report describes experimental and theoretical studies of nonlinear viscoelastic response of elastomeric binder material filled with small particles of different material. Studies characterize response with sufficient accuracy for use in designing parts subjected to high strains.

Multifunctional carbon nano-paper composite

NASA Astrophysics Data System (ADS)

Zhang, Zhichun; Chu, Hetao; Wang, Kuiwen; Liu, Yanjv; Leng, Jinsong

2013-08-01

Carbon Nanotube (CNT), for its excellent mechanical, electrical properties and nano size, large special surface physical property, become the most promising material. But carbon nanotube can still fabricated in micro dimension, and can't be made into macro size, so to the carbon nanotube filled composite can't explore the properties of the CNT. Carbon nano-paper is made of pure CNT, with micro pore, and it turn micro sized CNT into macro shaped membrane. Based on the piezo-resistivity and electrical conductivity of the carbon nano-paper, we used the carbon nano-paper as functional layers fabricate functional composite, and studies its strain sensing, composite material deicing and shape memory polymer (SMP) material electric actuation performance. The results shown that the resin can pregnant the nano paper, and there was good bond for nano paper and composite. The functional composite can monitoring the strain with high sensitivity comparing to foil strain gauge. The functional composite can be heated via the carbon nano paper with low power supply and high heating rate. The composite has good deicing and heat actuation performance to composite material. For the good strain sensing, electric conductivity and self-heating character of the carbon nano-paper composite, it can be used for self sensing, anti lightning strike and deicing of composite materials in aircrafts and wind turbine blades.

A stretchable strain sensor based on a metal nanoparticle thin film for human motion detection

NASA Astrophysics Data System (ADS)

Lee, Jaehwan; Kim, Sanghyeok; Lee, Jinjae; Yang, Daejong; Park, Byong Chon; Ryu, Seunghwa; Park, Inkyu

2014-09-01

Wearable strain sensors for human motion detection are being highlighted in various fields such as medical, entertainment and sports industry. In this paper, we propose a new type of stretchable strain sensor that can detect both tensile and compressive strains and can be fabricated by a very simple process. A silver nanoparticle (Ag NP) thin film patterned on the polydimethylsiloxane (PDMS) stamp by a single-step direct transfer process is used as the strain sensing material. The working principle is the change in the electrical resistance caused by the opening/closure of micro-cracks under mechanical deformation. The fabricated stretchable strain sensor shows highly sensitive and durable sensing performances in various tensile/compressive strains, long-term cyclic loading and relaxation tests. We demonstrate the applications of our stretchable strain sensors such as flexible pressure sensors and wearable human motion detection devices with high sensitivity, response speed and mechanical robustness.Wearable strain sensors for human motion detection are being highlighted in various fields such as medical, entertainment and sports industry. In this paper, we propose a new type of stretchable strain sensor that can detect both tensile and compressive strains and can be fabricated by a very simple process. A silver nanoparticle (Ag NP) thin film patterned on the polydimethylsiloxane (PDMS) stamp by a single-step direct transfer process is used as the strain sensing material. The working principle is the change in the electrical resistance caused by the opening/closure of micro-cracks under mechanical deformation. The fabricated stretchable strain sensor shows highly sensitive and durable sensing performances in various tensile/compressive strains, long-term cyclic loading and relaxation tests. We demonstrate the applications of our stretchable strain sensors such as flexible pressure sensors and wearable human motion detection devices with high sensitivity, response speed and mechanical robustness. Electronic supplementary information (ESI) available. See DOI: 10.1039/c4nr03295k

Nondestructive strain depth profiling with high energy X-ray diffraction: System capabilities and limitations

NASA Astrophysics Data System (ADS)

Zhang, Zhan; Wendt, Scott; Cosentino, Nicholas; Bond, Leonard J.

2018-04-01

Limited by photon energy, and penetration capability, traditional X-ray diffraction (XRD) strain measurements are only capable of achieving a few microns depth due to the use of copper (Cu Kα1) or molybdenum (Mo Kα1) characteristic radiation. For deeper strain depth profiling, destructive methods are commonly necessary to access layers of interest by removing material. To investigate deeper depth profiles nondestructively, a laboratory bench-top high-energy X-ray diffraction (HEXRD) system was previously developed. This HEXRD method uses an industrial 320 kVp X-Ray tube and the Kα1 characteristic peak of tungsten, to produces a higher intensity X-ray beam which enables depth profiling measurement of lattice strain. An aluminum sample was investigated with deformation/load provided using a bending rig. It was shown that the HEXRD method is capable of strain depth profiling to 2.5 mm. The method was validated using an aluminum sample where both the HEXRD method and the traditional X-ray diffraction method gave data compared with that obtained using destructive etching layer removal, performed by a commercial provider. The results demonstrate comparable accuracy up to 0.8 mm depth. Nevertheless, higher attenuation capabilities in heavier metals limit the applications in other materials. Simulations predict that HEXRD works for steel and nickel in material up to 200 µm, but experiment results indicate that the HEXRD strain profile is not practical for steel and nickel material, and the measured diffraction signals are undetectable when compared to the noise.

Mechanical metamaterials at the theoretical limit of isotropic elastic stiffness

NASA Astrophysics Data System (ADS)

Berger, J. B.; Wadley, H. N. G.; McMeeking, R. M.

2017-02-01

A wide variety of high-performance applications require materials for which shape control is maintained under substantial stress, and that have minimal density. Bio-inspired hexagonal and square honeycomb structures and lattice materials based on repeating unit cells composed of webs or trusses, when made from materials of high elastic stiffness and low density, represent some of the lightest, stiffest and strongest materials available today. Recent advances in 3D printing and automated assembly have enabled such complicated material geometries to be fabricated at low (and declining) cost. These mechanical metamaterials have properties that are a function of their mesoscale geometry as well as their constituents, leading to combinations of properties that are unobtainable in solid materials; however, a material geometry that achieves the theoretical upper bounds for isotropic elasticity and strain energy storage (the Hashin-Shtrikman upper bounds) has yet to be identified. Here we evaluate the manner in which strain energy distributes under load in a representative selection of material geometries, to identify the morphological features associated with high elastic performance. Using finite-element models, supported by analytical methods, and a heuristic optimization scheme, we identify a material geometry that achieves the Hashin-Shtrikman upper bounds on isotropic elastic stiffness. Previous work has focused on truss networks and anisotropic honeycombs, neither of which can achieve this theoretical limit. We find that stiff but well distributed networks of plates are required to transfer loads efficiently between neighbouring members. The resulting low-density mechanical metamaterials have many advantageous properties: their mesoscale geometry can facilitate large crushing strains with high energy absorption, optical bandgaps and mechanically tunable acoustic bandgaps, high thermal insulation, buoyancy, and fluid storage and transport. Our relatively simple design can be manufactured using origami-like sheet folding and bonding methods.

Mechanical metamaterials at the theoretical limit of isotropic elastic stiffness.

PubMed

Berger, J B; Wadley, H N G; McMeeking, R M

2017-03-23

A wide variety of high-performance applications require materials for which shape control is maintained under substantial stress, and that have minimal density. Bio-inspired hexagonal and square honeycomb structures and lattice materials based on repeating unit cells composed of webs or trusses, when made from materials of high elastic stiffness and low density, represent some of the lightest, stiffest and strongest materials available today. Recent advances in 3D printing and automated assembly have enabled such complicated material geometries to be fabricated at low (and declining) cost. These mechanical metamaterials have properties that are a function of their mesoscale geometry as well as their constituents, leading to combinations of properties that are unobtainable in solid materials; however, a material geometry that achieves the theoretical upper bounds for isotropic elasticity and strain energy storage (the Hashin-Shtrikman upper bounds) has yet to be identified. Here we evaluate the manner in which strain energy distributes under load in a representative selection of material geometries, to identify the morphological features associated with high elastic performance. Using finite-element models, supported by analytical methods, and a heuristic optimization scheme, we identify a material geometry that achieves the Hashin-Shtrikman upper bounds on isotropic elastic stiffness. Previous work has focused on truss networks and anisotropic honeycombs, neither of which can achieve this theoretical limit. We find that stiff but well distributed networks of plates are required to transfer loads efficiently between neighbouring members. The resulting low-density mechanical metamaterials have many advantageous properties: their mesoscale geometry can facilitate large crushing strains with high energy absorption, optical bandgaps and mechanically tunable acoustic bandgaps, high thermal insulation, buoyancy, and fluid storage and transport. Our relatively simple design can be manufactured using origami-like sheet folding and bonding methods.

Ductility of Advanced High-Strength Steel in the Presence of a Sheared Edge

NASA Astrophysics Data System (ADS)

Ruggles, Tim; Cluff, Stephen; Miles, Michael; Fullwood, David; Daniels, Craig; Avila, Alex; Chen, Ming

2016-07-01

The ductility of dual-phase (DP) 980 and transformation-induced plasticity (TRIP) assisted bainitic ferritic (TBF) 980 steels was studied in the presence of a sheared edge. Specimens were tested in uniaxial tension in a standard test frame as well as in situ in the scanning electron microscope (SEM). Incremental tensile straining was done in the SEM with images taken at each strain increment. Then digital image correlation (DIC) was used to compute the effective strain at the level of the individual phases in the microstructure. Shear banding across multiple phases was seen in strained TBF specimens, while the DP specimens exhibited more of a patchwork strain pattern, with high strains concentrated in ferrite and low strains observed in the martensite. Two-point statistics were applied to the strain data from the DIC work and the corresponding microstructure images to evaluate the effect of phase hardness on localization and fracture. It was observed that the DP 980 material had a greater tendency for localization around hard phases compared to the TBF 980. This at least partially explains the greater ductility of the TBF material, especially in specimens where a sheared edge was present.

Modeling Strain Rate Effect of Heterogeneous Materials Using SPH Method

NASA Astrophysics Data System (ADS)

Ma, G. W.; Wang, X. J.; Li, Q. M.

2010-11-01

The strain rate effect on the dynamic compressive failure of heterogeneous material based on the smoothed particle hydrodynamics (SPH) method is studied. The SPH method employs a rate-insensitive elasto-plastic damage model incorporated with a Weibull distribution law to reflect the mechanical behavior of heterogeneous rock-like materials. A series of simulations are performed for heterogeneous specimens by applying axial velocity conditions, which induce different strain-rate loadings to the specimen. A detailed failure process of the specimens in terms of microscopic crack-activities and the macro-mechanical response are discussed. Failure mechanisms between the low and high strain rate cases are compared. The result shows that the strain-rate effects on the rock strength are mainly caused by the changing internal pressure due to the inertial effects as well as the material heterogeneity. It also demonstrates that the inertial effect becomes significant only when the induced strain rate exceeds a threshold, below which, the dynamic strength enhancement can be explained due to the heterogeneities in the material. It also shows that the dynamic strength is affected more significantly for a relatively more heterogeneous specimen, which coincides with the experimental results showing that the poor quality specimen had a relatively larger increase in the dynamic strength.

Measurement at low strain rates of the elastic properties of dental polymeric materials.

PubMed

Chabrier, F; Lloyd, C H; Scrimgeour, S N

1999-01-01

To evaluate a simple static test (i.e. a slow strain rate test) designed to measure Young's modulus and the bulk modulus of polymeric materials (The NOL Test). Though it is a 'mature' test as yet it has never been applied to dental materials. A small cylindrical specimen is contained in a close-fitting steel constraining ring and compressive force applied to the ends by steel pistons. The initial (unconstrained) deformation is controlled by Young's modulus. Lateral spreading leads to constraint from the ring and subsequent deformation is controlled by the bulk modulus. A range of dental materials and reference polymers were selected and both moduli measured. From these data Poisson's ratios were calculated. The test proved be a simple reliable method for obtaining values for these properties. For composite the value of Young's modulus was lower, bulk modulus relatively similar and Poisson's ratio higher than that obtained from high strain rate techniques (as expected for a strain rate sensitive material). This test does fulfil a requirement for a simple test to define fully the elastic properties of dental polymeric materials. Measurements are made at the strain rates used in conventional static tests and values reflect this test condition. The higher values obtained for Poisson's ratio at this slow strain rate has implications for FEA, in that analysis is concerned with static or slow rate loading situations.

Room Temperature Shear Band Development in Highly Twinned Wrought Magnesium AZ31B Sheet

NASA Astrophysics Data System (ADS)

Scott, Jon; Miles, Michael; Fullwood, David; Adams, Brent; Khosravani, Ali; Mishra, Raja K.

2013-01-01

Failure mechanisms were studied in wrought AZ31B magnesium alloy after forming under different strain paths. Optical micrographs were used to observe the shear band formation and regions of high twin density in samples strained under uniaxial, biaxial, and plane strain conditions. Interrupted testing at 4 pct effective strain increments, until failure, was used to observe the evolution of the microstructure. The results showed that shear bands, with a high percentage of twinned grains, appeared early in the samples strained under biaxial or plane strain tension. These bands are similar to those seen in uniaxial tension specimens just prior to failure where the uniaxial tensile ductility was much greater than that observed for plane strain or biaxial tension conditions. A forming limit diagram for AZ31B, which was developed from the strain data, showed that plane strain and biaxial tension had very similar limit strains; this contrasts with materials like steel or aluminum alloys, which typically have greater ductility in biaxial tension compared to plane strain tension.

A Continuum Model for the Effect of Dynamic Recrystallization on the Stress–Strain Response

PubMed Central

Perdahcıoğlu, E. S.; van den Boogaard, A. H.

2018-01-01

Austenitic Stainless Steels and High-Strength Low-Alloy (HSLA) steels show significant dynamic recovery and dynamic recrystallization (DRX) during hot forming. In order to design optimal and safe hot-formed products, a good understanding and constitutive description of the material behavior is vital. A new continuum model is presented and validated on a wide range of deformation conditions including high strain rate deformation. The model is presented in rate form to allow for the prediction of material behavior in transient process conditions. The proposed model is capable of accurately describing the stress–strain behavior of AISI 316LN in hot forming conditions, also the high strain rate DRX-induced softening observed during hot torsion of HSLA is accurately predicted. It is shown that the increase in recrystallization rate at high strain rates observed in experiments can be captured by including the elastic energy due to the dynamic stress in the driving pressure for recrystallization. Furthermore, the predicted resulting grain sizes follow the power-law dependence with steady state stress that is often reported in literature and the evolution during hot deformation shows the expected trend. PMID:29789492

SVAS3: Strain Vector Aided Sensorization of Soft Structures

PubMed Central

Culha, Utku; Nurzaman, Surya G.; Clemens, Frank; Iida, Fumiya

2014-01-01

Soft material structures exhibit high deformability and conformability which can be useful for many engineering applications such as robots adapting to unstructured and dynamic environments. However, the fact that they have almost infinite degrees of freedom challenges conventional sensory systems and sensorization approaches due to the difficulties in adapting to soft structure deformations. In this paper, we address this challenge by proposing a novel method which designs flexible sensor morphologies to sense soft material deformations by using a functional material called conductive thermoplastic elastomer (CTPE). This model-based design method, called Strain Vector Aided Sensorization of Soft Structures (SVAS3), provides a simulation platform which analyzes soft body deformations and automatically finds suitable locations for CTPE-based strain gauge sensors to gather strain information which best characterizes the deformation. Our chosen sensor material CTPE exhibits a set of unique behaviors in terms of strain length electrical conductivity, elasticity, and shape adaptability, allowing us to flexibly design sensor morphology that can best capture strain distributions in a given soft structure. We evaluate the performance of our approach by both simulated and real-world experiments and discuss the potential and limitations. PMID:25036332

The structure and mechanical design of rhinoceros dermal armour.

PubMed

Shadwick, R E; Russell, A P; Lauff, R F

1992-09-29

The collagenous dermis of the white rhinoceros forms a thick, protective armour that is highly specialized in its structure and material properties compared with other mammalian skin. Rhinoceros skin is three times thicker than predicted allometrically, and it contains a dense and highly ordered three-dimensional array of relatively straight and highly crosslinked collagen fibres. The skin of the back and flanks exhibits a steep stress-strain curve with very little 'toe' region, a high elastic modulus (240 MPa), a high tensile strength (30 MPa), a low breaking strain (0.24) and high breaking energy (3 MJm-3) and work of fracture (78 kJm-2). By comparison, the belly skin is somewhat less stiff, weaker, and more extensible. In compression, rhinoceros skin withstands average stresses and strains of 170 MPa and 0.7, respectively, before yielding. As a biological material, rhinoceros dorsolateral skin has properties that are intermediate between those of 'normal' mammalian skin and tendons. This study shows that the dermal armour of the rhinoceros is very well adapted to resist blows from the horns of conspecifics, as might occur during aggressive behaviour, due to specialized material properties as well as its great thickness.

Material model validation for laser shock peening process simulation

NASA Astrophysics Data System (ADS)

Amarchinta, H. K.; Grandhi, R. V.; Langer, K.; Stargel, D. S.

2009-01-01

Advanced mechanical surface enhancement techniques have been used successfully to increase the fatigue life of metallic components. These techniques impart deep compressive residual stresses into the component to counter potentially damage-inducing tensile stresses generated under service loading. Laser shock peening (LSP) is an advanced mechanical surface enhancement technique used predominantly in the aircraft industry. To reduce costs and make the technique available on a large-scale basis for industrial applications, simulation of the LSP process is required. Accurate simulation of the LSP process is a challenging task, because the process has many parameters such as laser spot size, pressure profile and material model that must be precisely determined. This work focuses on investigating the appropriate material model that could be used in simulation and design. In the LSP process material is subjected to strain rates of 106 s-1, which is very high compared with conventional strain rates. The importance of an accurate material model increases because the material behaves significantly different at such high strain rates. This work investigates the effect of multiple nonlinear material models for representing the elastic-plastic behavior of materials. Elastic perfectly plastic, Johnson-Cook and Zerilli-Armstrong models are used, and the performance of each model is compared with available experimental results.

Strain-rate/temperature behavior of high density polyethylene in compression

NASA Technical Reports Server (NTRS)

Clements, L. L.; Sherby, O. D.

1978-01-01

The compressive strain rate/temperature behavior of highly linear, high density polyethylene was analyzed in terms of the predictive relations developed for metals and other crystalline materials. For strains of 5 percent and above, the relationship between applied strain rate, dotted epsilon, and resulting flow stress, sigma, was found to be: dotted epsilon exp times (Q sub f/RT) = k'(sigma/sigma sub c) to the nth power; the left-hand side is the activation-energy-compensated strain rate, where Q sub f is activation energy for flow, R is gas constant, and T is temperature; k is a constant, n is temperature-independent stress exponent, and sigma/sigma sub c is structure-compensated stress. A master curve resulted from a logarithmic plot of activation-energy-compensated strain rate versus structure-compensated stress.

Bismuth Sodium Titanate Based Materials for Piezoelectric Actuators

PubMed Central

Reichmann, Klaus; Feteira, Antonio; Li, Ming

2015-01-01

The ban of lead in many electronic products and the expectation that, sooner or later, this ban will include the currently exempt piezoelectric ceramics based on Lead-Zirconate-Titanate has motivated many research groups to look for lead-free substitutes. After a short overview on different classes of lead-free piezoelectric ceramics with large strain, this review will focus on Bismuth-Sodium-Titanate and its solid solutions. These compounds exhibit extraordinarily high strain, due to a field induced phase transition, which makes them attractive for actuator applications. The structural features of these materials and the origin of the field-induced strain will be revised. Technologies for texturing, which increases the useable strain, will be introduced. Finally, the features that are relevant for the application of these materials in a multilayer design will be summarized. PMID:28793724

Utilizing Photogrammetry and Strain Gage Measurement to Characterize Pressurization of Inflatable Modules

NASA Technical Reports Server (NTRS)

Mohammed, Anil

2011-01-01

This paper focuses on integrating a large hatch penetration into inflatable modules of various constructions. This paper also compares load predictions with test measurements. The strain was measured by utilizing photogrammetric methods and strain gages mounted to select clevises that interface with the structural webbings. Bench testing showed good correlation between strain data collected from an extensometer and photogrammetric measurements, even when the material transitioned from the low load to high load strain region of the curve. The full-scale torus design module showed mixed results as well in the lower load and high strain regions. After thorough analysis of photogrammetric measurements, strain gage measurements, and predicted load, the photogrammetric measurements seem to be off by a factor of two.

Calculation of Debye-Scherrer diffraction patterns from highly stressed polycrystalline materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

MacDonald, M. J., E-mail: macdonm@umich.edu; SLAC National Accelerator Laboratory, Menlo Park, California 94025; Vorberger, J.

2016-06-07

Calculations of Debye-Scherrer diffraction patterns from polycrystalline materials have typically been done in the limit of small deviatoric stresses. Although these methods are well suited for experiments conducted near hydrostatic conditions, more robust models are required to diagnose the large strain anisotropies present in dynamic compression experiments. A method to predict Debye-Scherrer diffraction patterns for arbitrary strains has been presented in the Voigt (iso-strain) limit [Higginbotham, J. Appl. Phys. 115, 174906 (2014)]. Here, we present a method to calculate Debye-Scherrer diffraction patterns from highly stressed polycrystalline samples in the Reuss (iso-stress) limit. This analysis uses elastic constants to calculate latticemore » strains for all initial crystallite orientations, enabling elastic anisotropy and sample texture effects to be modeled directly. The effects of probing geometry, deviatoric stresses, and sample texture are demonstrated and compared to Voigt limit predictions. An example of shock-compressed polycrystalline diamond is presented to illustrate how this model can be applied and demonstrates the importance of including material strength when interpreting diffraction in dynamic compression experiments.« less

Flexible strain sensors with high performance based on metallic glass thin film

NASA Astrophysics Data System (ADS)

Xian, H. J.; Cao, C. R.; Shi, J. A.; Zhu, X. S.; Hu, Y. C.; Huang, Y. F.; Meng, S.; Gu, L.; Liu, Y. H.; Bai, H. Y.; Wang, W. H.

2017-09-01

Searching strain sensitive materials for electronic skin is of crucial significance because of the restrictions of current materials such as poor electrical conductivity, large energy consumption, complex manufacturing process, and high cost. Here, we report a flexible strain sensor based on the Zr55Cu30Ni5Al10 metallic glass thin film which we name metallic glass skin. The metallic glass skin, synthesized by ion beam deposition, exhibits piezoresistance effects with a gauge factor of around 2.86, a large detectable strain range (˜1% or 180° bending angle), and good conductivity. Compared to other e-skin materials, the temperature coefficient of resistance of the metallic glass skin is extremely low (9.04 × 10-6 K-1), which is essential for the reduction in thermal drift. In addition, the metallic glass skin exhibits distinct antibacterial behavior desired for medical applications, also excellent reproducibility and repeatability (over 1000 times), nearly perfect linearity, low manufacturing cost, and negligible energy consumption, all of which are required for electronic skin for practical applications.

Thin Film Ceramic Strain Sensor Development for Harsh Environments: Interim Report on Identification of Candidate Thin Film Ceramics to Test for Viability for Static Strain Sensor Development

NASA Technical Reports Server (NTRS)

Wrbanek, John D.; Fralick, Gustave C.; Hunter, Gary W.

2006-01-01

The need to consider ceramic sensing elements is brought about by the temperature limits of metal thin film sensors in propulsion system applications. In order to have a more passive method of negating changes of resistance due to temperature, an effort is underway at NASA Glenn to develop high temperature thin film ceramic static strain gauges for application in turbine engines, specifically in the fan and compressor modules on blades. Other applications can be on aircraft hot section structures and on thermal protection systems. The near-term interim goal of the research effort was to identify candidate thin film ceramic sensor materials to test for viability and provide a list of possible thin film ceramic sensor materials and corresponding properties to test for viability. This goal was achieved by a thorough literature search for ceramics that have the potential for application as high temperature thin film strain gauges, reviewing potential candidate materials for chemical and physical compatibility with our microfabrication procedures and substrates.

Thin Film Ceramic Strain Sensor Development for Harsh Environments: Identification of Candidate Thin Film Ceramics to Test for Viability for Static Strain Sensor Development

NASA Technical Reports Server (NTRS)

Wrbanek, John D.; Fralick, Gustave C.; Hunter, Gary W.

2006-01-01

The need to consider ceramic sensing elements is brought about by the temperature limits of metal thin film sensors in propulsion system applications. In order to have a more passive method of negating changes of resistance due to temperature, an effort is underway at NASA GRC to develop high temperature thin film ceramic static strain gauges for application in turbine engines, specifically in the fan and compressor modules on blades. Other applications include on aircraft hot section structures and on thermal protection systems. The near-term interim goal of this research effort was to identify candidate thin film ceramic sensor materials to test for viability and provide a list of possible thin film ceramic sensor materials and corresponding properties to test for viability. This goal was achieved by a thorough literature search for ceramics that have the potential for application as high temperature thin film strain gauges, reviewing potential candidate materials for chemical & physical compatibility with NASA GRC's microfabrication procedures and substrates.

Tensile strength and failure mechanisms of tantalum at extreme strain rates

NASA Astrophysics Data System (ADS)

Hahn, Eric; Fensin, Saryu; Germann, Timothy; Meyers, Marc

Non-equilibrium molecular dynamics simulations are used to probe the tensile response of monocrystalline, bicrystalline, and nanocrystalline tantalum over six orders of magnitude of strain rate. Our analysis of the strain rate dependence of strength is extended to over nine orders of magnitude by bridging the present simulations to recent laser-driven shock experiments. Tensile strength shows a power-law dependence with strain rate over this wide range, with different relationships depending on the initial microstructure and active deformation mechanism. At high strain rates, multiple spall events occur independently and continue to occur until communication occurs by means of relaxation waves. Temperature plays a significant role in the reduction of spall strength as the initial shock required to achieve such large strain rates also contributes to temperature rise, through pressure-volume work as well as visco-plastic heating, which leads to softening and sometimes melting upon release. At ultra-high strain rates, those approaching or exceeding the atomic vibrational frequency, spall strength saturates at the ultimate cohesive strength of the material. UC Research Laboratories Grant (09-LR-06-118456-MEYM); Department of Energy NNSA/SSAP (DE-NA0002080); DOE ASCR Exascale Co-design Center for Materials in Extreme Environments.

Modeling of NiTiHf using finite difference method

NASA Astrophysics Data System (ADS)

Farjam, Nazanin; Mehrabi, Reza; Karaca, Haluk; Mirzaeifar, Reza; Elahinia, Mohammad

2018-03-01

NiTiHf is a high temperature and high strength shape memory alloy with transformation temperatures above 100oC. A constitutive model based on Gibbs free energy is developed to predict the behavior of this material. Two different irrecoverable strains including transformation induced plastic strain (TRIP) and viscoplastic strain (VP) are considered when using high temperature shape memory alloys (HTSMAs). The first one happens during transformation at high levels of stress and the second one is related to the creep which is rate-dependent. The developed model is implemented for NiTiHf under uniaxial loading. Finite difference method is utilized to solve the proposed equations. The material parameters in the equations are calibrated from experimental data. Simulation results are captured to investigate the superelastic behavior of NiTiHf. The extracted results are compared with experimental tests of isobaric heating and cooling at different levels of stress and also superelastic tests at different levels of temperature. More results are generated to investigate the capability of the proposed model in the prediction of the irrecoverable strain after full transformation in HTSMAs.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Song, Bo; Nelson, Kevin; Jin, Helena

Iridium alloys have been utilized as structural materials for certain high-temperature applications, due to their superior strength and ductility at elevated temperatures. The mechanical properties, including failure response at high strain rates and elevated temperatures of the iridium alloys need to be characterized to better understand high-speed impacts at elevated temperatures. A DOP-26 iridium alloy has been dynamically characterized in compression at elevated temperatures with high-temperature Kolsky compression bar techniques. However, the dynamic high-temperature compression tests were not able to provide sufficient dynamic high-temperature failure information of the iridium alloy. In this study, we modified current room-temperature Kolsky tension barmore » techniques for obtaining dynamic tensile stress-strain curves of the DOP-26 iridium alloy at two different strain rates (~1000 and ~3000 s-1) and temperatures (~750°C and ~1030°C). The effects of strain rate and temperature on the tensile stress-strain response of the iridium alloy were determined. The DOP-26 iridium alloy exhibited high ductility in stress-strain response that strongly depended on both strain rate and temperature.« less

A high temperature testing system for ceramic composites

NASA Technical Reports Server (NTRS)

Hemann, John

1994-01-01

Ceramic composites are presently being developed for high temperature use in heat engine and space power system applications. The operating temperature range is expected to be 1090 to 1650 C (2000 F to 3000 F). Very little material data is available at these temperatures and, therefore, it is desirable to thoroughly characterize the basic unidirectional fiber reinforced ceramic composite. This includes testing mainly for mechanical material properties at high temperatures. The proper conduct of such characterization tests requires the development of a tensile testing system includes unique gripping, heating, and strain measuring devices which require special considerations. The system also requires an optimized specimen shape. The purpose of this paper is to review various techniques for measuring displacements or strains, preferably at elevated temperatures. Due to current equipment limitations it is assumed that the specimen is to be tested at a temperature of 1430 C (2600F) in an oxidizing atmosphere. For the most part, previous high temperature material characterization tests, such as flexure and tensile tests, have been performed in inert atmospheres. Due to the harsh environment in which the ceramic specimen is to be tested, many conventional strain measuring techniques can not be applied. Initially a brief description of the more commonly used mechanical strain measuring techniques is given. Major advantages and disadvantages with their application to high temperature tensile testing of ceramic composites are discussed. Next, a general overview is given for various optical techniques. Advantages and disadvantages which are common to these techniques are noted. The optical methods for measuring strain or displacement are categorized into two sections. These include real-time techniques. Finally, an optical technique which offers optimum performance with the high temperature tensile testing of ceramic composites is recommended.

Analytical Modeling of the High Strain Rate Deformation of Polymer Matrix Composites

NASA Technical Reports Server (NTRS)

Goldberg, Robert K.; Roberts, Gary D.; Gilat, Amos

2003-01-01

The results presented here are part of an ongoing research program to develop strain rate dependent deformation and failure models for the analysis of polymer matrix composites subject to high strain rate impact loads. State variable constitutive equations originally developed for metals have been modified in order to model the nonlinear, strain rate dependent deformation of polymeric matrix materials. To account for the effects of hydrostatic stresses, which are significant in polymers, the classical 5 plasticity theory definitions of effective stress and effective plastic strain are modified by applying variations of the Drucker-Prager yield criterion. To verify the revised formulation, the shear and tensile deformation of a representative toughened epoxy is analyzed across a wide range of strain rates (from quasi-static to high strain rates) and the results are compared to experimentally obtained values. For the analyzed polymers, both the tensile and shear stress-strain curves computed using the analytical model correlate well with values obtained through experimental tests. The polymer constitutive equations are implemented within a strength of materials based micromechanics method to predict the nonlinear, strain rate dependent deformation of polymer matrix composites. In the micromechanics, the unit cell is divided up into a number of independently analyzed slices, and laminate theory is then applied to obtain the effective deformation of the unit cell. The composite mechanics are verified by analyzing the deformation of a representative polymer matrix composite (composed using the representative polymer analyzed for the correlation of the polymer constitutive equations) for several fiber orientation angles across a variety of strain rates. The computed values compare favorably to experimentally obtained results.

Strain induced optical properties of BaReO3

NASA Astrophysics Data System (ADS)

Kumavat, Sandip R.; Kansara, Shivam; Gupta, Sanjeev K.; Sonvane, Yogesh

2018-05-01

Here, we have performed strain induce optical properties of BaReO3 by using density functional theory (DFT). We noticed that after applying intrinsic and extrinsic strain to the BaReO3, it shows the metallic behavior. We also studied optical properties, which show good activity in the ultraviolet region. The results show that after applying intrinsic and extrinsic strain to BaReO3 the absorption peaks are shifted towards the high UV region of the spectrum. Thus, we concluded that, BaReO3 material with extrinsic strain can be useful for high frequency UV device and optoelectronic devices.

Verification of Experimental Techniques for Flow Surface Determination

NASA Technical Reports Server (NTRS)

Lissenden, Cliff J.; Lerch, Bradley A.; Ellis, John R.; Robinson, David N.

1996-01-01

The concept of a yield surface is central to the mathematical formulation of a classical plasticity theory. However, at elevated temperatures, material response can be highly time-dependent, which is beyond the realm of classical plasticity. Viscoplastic theories have been developed for just such conditions. In viscoplastic theories, the flow law is given in terms of inelastic strain rate rather than the inelastic strain increment used in time-independent plasticity. Thus, surfaces of constant inelastic strain rate or flow surfaces are to viscoplastic theories what yield surfaces are to classical plasticity. The purpose of the work reported herein was to validate experimental procedures for determining flow surfaces at elevated temperatures. Since experimental procedures for determining yield surfaces in axial/torsional stress space are well established, they were employed -- except inelastic strain rates were used rather than total inelastic strains. In yield-surface determinations, the use of small-offset definitions of yield minimizes the change of material state and allows multiple loadings to be applied to a single specimen. The key to the experiments reported here was precise, decoupled measurement of axial and torsional strain. With this requirement in mind, the performance of a high-temperature multi-axial extensometer was evaluated by comparing its results with strain gauge results at room temperature. Both the extensometer and strain gauges gave nearly identical yield surfaces (both initial and subsequent) for type 316 stainless steel (316 SS). The extensometer also successfully determined flow surfaces for 316 SS at 650 C. Furthermore, to judge the applicability of the technique for composite materials, yield surfaces were determined for unidirectional tungsten/Kanthal (Fe-Cr-Al).

The Use of Particle/Substrate Material Models in Simulation of Cold-Gas Dynamic-Spray Process

NASA Astrophysics Data System (ADS)

Rahmati, Saeed; Ghaei, Abbas

2014-02-01

Cold spray is a coating deposition method in which the solid particles are accelerated to the substrate using a low temperature supersonic gas flow. Many numerical studies have been carried out in the literature in order to study this process in more depth. Despite the inability of Johnson-Cook plasticity model in prediction of material behavior at high strain rates, it is the model that has been frequently used in simulation of cold spray. Therefore, this research was devoted to compare the performance of different material models in the simulation of cold spray process. Six different material models, appropriate for high strain-rate plasticity, were employed in finite element simulation of cold spray process for copper. The results showed that the material model had a considerable effect on the predicted deformed shapes.

Nanoporous carbon-based electrodes for high strain ionomeric bending actuators

NASA Astrophysics Data System (ADS)

Palmre, Viljar; Brandell, Daniel; Mäeorg, Uno; Torop, Janno; Volobujeva, Olga; Punning, Andres; Johanson, Urmas; Kruusmaa, Maarja; Aabloo, Alvo

2009-09-01

Ionic polymer metal composites (IPMCs) are electroactive material devices that bend at low applied voltage (1-4 V). Inversely, a voltage is generated when the materials are deformed, which makes them useful both as sensors and actuators. In this paper, we propose two new highly porous carbon materials as electrodes for IPMC actuators, generating a high specific area, and compare their electromechanical performance with recently reported RuO2 electrodes and conventional IPMCs. Using a direct assembly process (DAP), we synthesize ionic liquid (Emi-Tf) actuators with either carbide-derived carbon (CDC) or coconut-shell-based activated carbon-based electrodes. The carbon electrodes were applied onto ionic liquid-swollen Nafion membranes using a direct assembly process. The study demonstrates that actuators based on carbon electrodes derived from TiC have the greatest peak-to-peak strain output, reaching up to 20.4 mɛ (equivalent to>2%) at a 2 V actuation signal, exceeding that of the RuO2 electrodes by more than 100%. The electrodes synthesized from TiC-derived carbon also exhibit significantly higher maximum strain rate. The differences between the materials are discussed in terms of molecular interactions and mechanisms upon actuation in the different electrodes.

Phenomenological study of a cellular material behaviour under dynamic loadings

NASA Astrophysics Data System (ADS)

Bouix, R.; Viot, Ph.; Lataillade, J.-L.

2006-08-01

Polypropylene foams are cellular materials, which are often use to fill structures subjected to crash or violent impacts. Therefore, it is necessary to know and to characterise in experiments their mechanical behaviour in compression at high strain rates. So, several apparatus have been used in order to highlight the influence of strain rate, material density and also temperature. A split Hopkinson Pressure Bar has been used for impact tests, a fly wheel to test theses materials at medium strain rate and an electro-mechanical testing machine associated to a climatic chamber for temperature tests. Then, a rheological model has been used in order to describe the material behaviour. The mechanical response to compression of these foams presents three typical domains: a linear elastic step, a wide collapse plateau stress, which leads to a densification, which are related to a standard rheological model.

FAST TRACK COMMUNICATION High rate straining of tantalum and copper

NASA Astrophysics Data System (ADS)

Armstrong, R. W.; Zerilli, F. J.

2010-12-01

High strain rate measurements reported recently for several tantalum and copper crystal/polycrystal materials are shown to follow dislocation mechanics-based constitutive relations, first at lower strain rates, for dislocation velocity control of the imposed plastic deformations and, then at higher rates, transitioning to nano-scale dislocation generation control by twinning or slip. For copper, there is the possibility of added-on slip dislocation displacements to be accounted for from the newly generated dislocations.

Law of damage accumulation and fracture criteria in highly filled polymer materials

NASA Astrophysics Data System (ADS)

Bykov, D. L.; Kazakov, A. V.; Konovalov, D. N.; Mel'nikov, V. P.; Milyokhin, Yu. M.; Peleshko, V. A.; Sadovnichii, D. N.

2014-09-01

We present the results of a large series of experiments aimed at the study of laws of damage accumulation and fracture in highly filled polymer materials under loading conditions of various types: monotone, repeated, low- and high-cycle, with varying type of stress state, dynamic (in general, more than 50 programs implemented on specimens from one lot of material). The data obtained in these test allow one to make conclusions about the constitutive role of the attained maximum of strain intensity when estimating the accumulated damage in the process of uniaxial tension by various programs (in particular, an additional cyclic deformation below the preliminary attained strain maximum does not affect the limit values of strain and stress in the subsequent active extension), about the strong influence of the stress state on the deformation and fracture, about the specific features of the nonlinear behavior of the material under the shock loading conditions and its influence on the repeated deformation. All tests are described (with an accuracy acceptable in practical calculations, both with respect to stresses and strains in the process of loading and at the moment of fracture) in the framework of the same model of nonlinear viscoelasticity with the same set of constants. The constants of the proposed model are calculated according to a relatively simple algorithm by using the results of standard uniaxial tension tests with constant values of the strain rate and hydrostatic pressure (each test for 2-3 levels of these parameters chosen from the ranges proposed in applications, each loading lasts until the fracture occurs, and one of the tests contains an intermediate interval of total loading and repeated loading) and one axial shock compression test if there are dynamic problems in the applications. The model is based on the use of the criterion fracture parameter which, in the class of proportional loading processes, is the sum of partial increments of the strain intensity on active segments of the process (where the strain intensity is at its historical maximum) with the form of the stress state and the intensity of strain rates taken into account.

Unraveling submicron-scale mechanical heterogeneity by three-dimensional X-ray microdiffraction

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, Runguang; Xie, Qingge; Wang, Yan-Dong

Shear banding is a ubiquitous phenomenon of severe plastic deformation, and damage accumulation in shear bands often results in the catastrophic failure of a material. Despite extensive studies, the microscopic mechanisms of strain localization and deformation damage in shear bands remain elusive due to their spatial-temporal complexities embedded in bulk materials. Here we conducted synchrotron-based X-ray microdiffraction (μXRD) experiments to map out the 3D lattice strain field with a submicron resolution around fatigue shear bands in a stainless steel. Both in situ and postmortem μXRD results revealed large lattice strain gradients at intersections of the primary and secondary shear bands.more » Such strain gradients resulted in severe mechanical heterogeneities across the fatigue shear bands, leading to reduced fatigue limits in the high-cycle regime. The ability to spatially quantify the localized strain gradients with submicron resolution through μXRD opens opportunities for understanding the microscopic mechanisms of damage and failure in bulk materials.« less

Unraveling submicron-scale mechanical heterogeneity by three-dimensional X-ray microdiffraction

DOE PAGES

Li, Runguang; Xie, Qingge; Wang, Yan-Dong; ...

2017-12-28

Shear banding is a ubiquitous phenomenon of severe plastic deformation, and damage accumulation in shear bands often results in the catastrophic failure of a material. Despite extensive studies, the microscopic mechanisms of strain localization and deformation damage in shear bands remain elusive due to their spatial-temporal complexities embedded in bulk materials. Here we conducted synchrotron-based X-ray microdiffraction (μXRD) experiments to map out the 3D lattice strain field with a submicron resolution around fatigue shear bands in a stainless steel. Both in situ and postmortem μXRD results revealed large lattice strain gradients at intersections of the primary and secondary shear bands.more » Such strain gradients resulted in severe mechanical heterogeneities across the fatigue shear bands, leading to reduced fatigue limits in the high-cycle regime. The ability to spatially quantify the localized strain gradients with submicron resolution through μXRD opens opportunities for understanding the microscopic mechanisms of damage and failure in bulk materials.« less

Unraveling submicron-scale mechanical heterogeneity by three-dimensional X-ray microdiffraction

PubMed Central

Li, Runguang; Xie, Qingge; Wang, Yan-Dong; Liu, Wenjun; Wang, Mingguang; Wu, Guilin; Li, Xiaowu; Zhang, Minghe; Lu, Zhaoping; Geng, Chang; Zhu, Ting

2018-01-01

Shear banding is a ubiquitous phenomenon of severe plastic deformation, and damage accumulation in shear bands often results in the catastrophic failure of a material. Despite extensive studies, the microscopic mechanisms of strain localization and deformation damage in shear bands remain elusive due to their spatial−temporal complexities embedded in bulk materials. Here we conducted synchrotron-based X-ray microdiffraction (μXRD) experiments to map out the 3D lattice strain field with a submicron resolution around fatigue shear bands in a stainless steel. Both in situ and postmortem μXRD results revealed large lattice strain gradients at intersections of the primary and secondary shear bands. Such strain gradients resulted in severe mechanical heterogeneities across the fatigue shear bands, leading to reduced fatigue limits in the high-cycle regime. The ability to spatially quantify the localized strain gradients with submicron resolution through μXRD opens opportunities for understanding the microscopic mechanisms of damage and failure in bulk materials. PMID:29284751

A nonlinear mechanics model of bio-inspired hierarchical lattice materials consisting of horseshoe microstructures

PubMed Central

Ma, Qiang; Cheng, Huanyu; Jang, Kyung-In; Luan, Haiwen; Hwang, Keh-Chih; Rogers, John A.; Huang, Yonggang; Zhang, Yihui

2016-01-01

Development of advanced synthetic materials that can mimic the mechanical properties of non-mineralized soft biological materials has important implications in a wide range of technologies. Hierarchical lattice materials constructed with horseshoe microstructures belong to this class of bio-inspired synthetic materials, where the mechanical responses can be tailored to match the nonlinear J-shaped stress-strain curves of human skins. The underlying relations between the J-shaped stress-strain curves and their microstructure geometry are essential in designing such systems for targeted applications. Here, a theoretical model of this type of hierarchical lattice material is developed by combining a finite deformation constitutive relation of the building block (i.e., horseshoe microstructure), with the analyses of equilibrium and deformation compatibility in the periodical lattices. The nonlinear J-shaped stress-strain curves and Poisson ratios predicted by this model agree very well with results of finite element analyses (FEA) and experiment. Based on this model, analytic solutions were obtained for some key mechanical quantities, e.g., elastic modulus, Poisson ratio, peak modulus, and critical strain around which the tangent modulus increases rapidly. A negative Poisson effect is revealed in the hierarchical lattice with triangular topology, as opposed to a positive Poisson effect in hierarchical lattices with Kagome and honeycomb topologies. The lattice topology is also found to have a strong influence on the stress-strain curve. For the three isotropic lattice topologies (triangular, Kagome and honeycomb), the hierarchical triangular lattice material renders the sharpest transition in the stress-strain curve and relative high stretchability, given the same porosity and arc angle of horseshoe microstructure. Furthermore, a demonstrative example illustrates the utility of the developed model in the rapid optimization of hierarchical lattice materials for reproducing the desired stress-strain curves of human skins. This study provides theoretical guidelines for future designs of soft bio-mimetic materials with hierarchical lattice constructions. PMID:27087704

A nonlinear mechanics model of bio-inspired hierarchical lattice materials consisting of horseshoe microstructures

NASA Astrophysics Data System (ADS)

Ma, Qiang; Cheng, Huanyu; Jang, Kyung-In; Luan, Haiwen; Hwang, Keh-Chih; Rogers, John A.; Huang, Yonggang; Zhang, Yihui

2016-05-01

Development of advanced synthetic materials that can mimic the mechanical properties of non-mineralized soft biological materials has important implications in a wide range of technologies. Hierarchical lattice materials constructed with horseshoe microstructures belong to this class of bio-inspired synthetic materials, where the mechanical responses can be tailored to match the nonlinear J-shaped stress-strain curves of human skins. The underlying relations between the J-shaped stress-strain curves and their microstructure geometry are essential in designing such systems for targeted applications. Here, a theoretical model of this type of hierarchical lattice material is developed by combining a finite deformation constitutive relation of the building block (i.e., horseshoe microstructure), with the analyses of equilibrium and deformation compatibility in the periodical lattices. The nonlinear J-shaped stress-strain curves and Poisson ratios predicted by this model agree very well with results of finite element analyses (FEA) and experiment. Based on this model, analytic solutions were obtained for some key mechanical quantities, e.g., elastic modulus, Poisson ratio, peak modulus, and critical strain around which the tangent modulus increases rapidly. A negative Poisson effect is revealed in the hierarchical lattice with triangular topology, as opposed to a positive Poisson effect in hierarchical lattices with Kagome and honeycomb topologies. The lattice topology is also found to have a strong influence on the stress-strain curve. For the three isotropic lattice topologies (triangular, Kagome and honeycomb), the hierarchical triangular lattice material renders the sharpest transition in the stress-strain curve and relative high stretchability, given the same porosity and arc angle of horseshoe microstructure. Furthermore, a demonstrative example illustrates the utility of the developed model in the rapid optimization of hierarchical lattice materials for reproducing the desired stress-strain curves of human skins. This study provides theoretical guidelines for future designs of soft bio-mimetic materials with hierarchical lattice constructions.

A nonlinear mechanics model of bio-inspired hierarchical lattice materials consisting of horseshoe microstructures.

PubMed

Ma, Qiang; Cheng, Huanyu; Jang, Kyung-In; Luan, Haiwen; Hwang, Keh-Chih; Rogers, John A; Huang, Yonggang; Zhang, Yihui

2016-05-01

Development of advanced synthetic materials that can mimic the mechanical properties of non-mineralized soft biological materials has important implications in a wide range of technologies. Hierarchical lattice materials constructed with horseshoe microstructures belong to this class of bio-inspired synthetic materials, where the mechanical responses can be tailored to match the nonlinear J-shaped stress-strain curves of human skins. The underlying relations between the J-shaped stress-strain curves and their microstructure geometry are essential in designing such systems for targeted applications. Here, a theoretical model of this type of hierarchical lattice material is developed by combining a finite deformation constitutive relation of the building block (i.e., horseshoe microstructure), with the analyses of equilibrium and deformation compatibility in the periodical lattices. The nonlinear J-shaped stress-strain curves and Poisson ratios predicted by this model agree very well with results of finite element analyses (FEA) and experiment. Based on this model, analytic solutions were obtained for some key mechanical quantities, e.g., elastic modulus, Poisson ratio, peak modulus, and critical strain around which the tangent modulus increases rapidly. A negative Poisson effect is revealed in the hierarchical lattice with triangular topology, as opposed to a positive Poisson effect in hierarchical lattices with Kagome and honeycomb topologies. The lattice topology is also found to have a strong influence on the stress-strain curve. For the three isotropic lattice topologies (triangular, Kagome and honeycomb), the hierarchical triangular lattice material renders the sharpest transition in the stress-strain curve and relative high stretchability, given the same porosity and arc angle of horseshoe microstructure. Furthermore, a demonstrative example illustrates the utility of the developed model in the rapid optimization of hierarchical lattice materials for reproducing the desired stress-strain curves of human skins. This study provides theoretical guidelines for future designs of soft bio-mimetic materials with hierarchical lattice constructions.

High variability in strain estimation errors when using a commercial ultrasound speckle tracking algorithm on tendon tissue.

PubMed

Fröberg, Åsa; Mårtensson, Mattias; Larsson, Matilda; Janerot-Sjöberg, Birgitta; D'Hooge, Jan; Arndt, Anton

2016-10-01

Ultrasound speckle tracking offers a non-invasive way of studying strain in the free Achilles tendon where no anatomical landmarks are available for tracking. This provides new possibilities for studying injury mechanisms during sport activity and the effects of shoes, orthotic devices, and rehabilitation protocols on tendon biomechanics. To investigate the feasibility of using a commercial ultrasound speckle tracking algorithm for assessing strain in tendon tissue. A polyvinyl alcohol (PVA) phantom, three porcine tendons, and a human Achilles tendon were mounted in a materials testing machine and loaded to 4% peak strain. Ultrasound long-axis cine-loops of the samples were recorded. Speckle tracking analysis of axial strain was performed using a commercial speckle tracking software. Estimated strain was then compared to reference strain known from the materials testing machine. Two frame rates and two region of interest (ROI) sizes were evaluated. Best agreement between estimated strain and reference strain was found in the PVA phantom (absolute error in peak strain: 0.21 ± 0.08%). The absolute error in peak strain varied between 0.72 ± 0.65% and 10.64 ± 3.40% in the different tendon samples. Strain determined with a frame rate of 39.4 Hz had lower errors than 78.6 Hz as was the case with a 22 mm compared to an 11 mm ROI. Errors in peak strain estimation showed high variability between tendon samples and were large in relation to strain levels previously described in the Achilles tendon. © The Foundation Acta Radiologica 2016.

Analysis of heterogeneities in strain and microstructure in aluminum alloy and magnesium processed by high-pressure torsion

DOE Office of Scientific and Technical Information (OSTI.GOV)

Panda, Subrata, E-mail: subrata.panda@univ-lorrain

2017-01-15

Two distinct bulk light metals were opted to study the shear strain evolution and associated heterogeneities in texture/microstructure development during torsional straining by high pressure torsion (HPT): a face centered cubic Al alloy (A5086) and a hexagonal commercial purity Mg. Relatively thick disk samples - four times thicker than usually employed in HPT process - were processed to 180° and 270° rotations. With the help of X-ray tomography, the shear strain gradients were examined in the axial direction. The results showed strongly localized shear deformation in the middle plane of the disks in both materials. These gradients involved strong heterogeneitiesmore » in texture, microstructure and associated hardness, in particular through the thickness direction at the periphery of the disk where the interplay between significant strain hardening and possible dynamic recrystallization could occur. - Highlights: •HPT processing was conducted on bulk specimens thicker than the usual thin-disks. •The Al alloy (A5086) and commercial purity magnesium samples were compared. •Distributions of strain and microhardness were evaluated in the radial and axial direction. •Plastic deformation is highly localized in the middle plane at outer edge in both materials. •Different DRX rates governed the differences in microstructure and hardening behavior.« less

Optical Method for Detecting Displacements and Strains at Ultra-High Temperatures During Thermo-Mechanical Testing

NASA Technical Reports Server (NTRS)

Roth, Mark C. (Inventor); Smith, Russell W. (Inventor); Sikora, Joseph G. (Inventor); Rivers, H. Kevin (Inventor); Johnston, William M. (Inventor)

2016-01-01

An ultra-high temperature optical method incorporates speckle optics for sensing displacement and strain measurements well above conventional measurement techniques. High temperature pattern materials are used which can endure experimental high temperature environments while simultaneously having a minimum optical aberration. A purge medium is used to reduce or eliminate optical distortions and to reduce, and/or eliminate oxidation of the target specimen.

High pressure phase transformations revisited

NASA Astrophysics Data System (ADS)

Levitas, Valery I.

2018-04-01

High pressure phase transformations play an important role in the search for new materials and material synthesis, as well as in geophysics. However, they are poorly characterized, and phase transformation pressure and pressure hysteresis vary drastically in experiments of different researchers, with different pressure transmitting media, and with different material suppliers. Here we review the current state, challenges in studying phase transformations under high pressure, and the possible ways in overcoming the challenges. This field is critically compared with fields of phase transformations under normal pressure in steels and shape memory alloys, as well as plastic deformation of materials. The main reason for the above mentioned discrepancy is the lack of understanding that there is a fundamental difference between pressure-induced transformations under hydrostatic conditions, stress-induced transformations under nonhydrostatic conditions below yield, and strain-induced transformations during plastic flow. Each of these types of transformations has different mechanisms and requires a completely different thermodynamic and kinetic description and experimental characterization. In comparison with other fields the following challenges are indicated for high pressure phase transformation: (a) initial and evolving microstructure is not included in characterization of transformations; (b) continuum theory is poorly developed; (c) heterogeneous stress and strain fields in experiments are not determined, which leads to confusing material transformational properties with a system behavior. Some ways to advance the field of high pressure phase transformations are suggested. The key points are: (a) to take into account plastic deformations and microstructure evolution during transformations; (b) to formulate phase transformation criteria and kinetic equations in terms of stress and plastic strain tensors (instead of pressure alone); (c) to develop multiscale continuum theories, and (d) to couple experimental, theoretical, and computational studies of the behavior of a tested sample to extract information about fields of stress and strain tensors and concentration of high pressure phase, transformation criteria and kinetics. The ideal characterization should contain complete information which is required for simulation of the same experiments.

High pressure phase transformations revisited.

PubMed

Levitas, Valery I

2018-04-25

High pressure phase transformations play an important role in the search for new materials and material synthesis, as well as in geophysics. However, they are poorly characterized, and phase transformation pressure and pressure hysteresis vary drastically in experiments of different researchers, with different pressure transmitting media, and with different material suppliers. Here we review the current state, challenges in studying phase transformations under high pressure, and the possible ways in overcoming the challenges. This field is critically compared with fields of phase transformations under normal pressure in steels and shape memory alloys, as well as plastic deformation of materials. The main reason for the above mentioned discrepancy is the lack of understanding that there is a fundamental difference between pressure-induced transformations under hydrostatic conditions, stress-induced transformations under nonhydrostatic conditions below yield, and strain-induced transformations during plastic flow. Each of these types of transformations has different mechanisms and requires a completely different thermodynamic and kinetic description and experimental characterization. In comparison with other fields the following challenges are indicated for high pressure phase transformation: (a) initial and evolving microstructure is not included in characterization of transformations; (b) continuum theory is poorly developed; (c) heterogeneous stress and strain fields in experiments are not determined, which leads to confusing material transformational properties with a system behavior. Some ways to advance the field of high pressure phase transformations are suggested. The key points are: (a) to take into account plastic deformations and microstructure evolution during transformations; (b) to formulate phase transformation criteria and kinetic equations in terms of stress and plastic strain tensors (instead of pressure alone); (c) to develop multiscale continuum theories, and (d) to couple experimental, theoretical, and computational studies of the behavior of a tested sample to extract information about fields of stress and strain tensors and concentration of high pressure phase, transformation criteria and kinetics. The ideal characterization should contain complete information which is required for simulation of the same experiments.

High Strain Rate Material Behavior

DTIC Science & Technology

1985-12-01

data. iii Mr. Dennis Paisely conducted the single plate impact test. Mr. Danny Yaziv is responsible for developing the double flyer plate technique and...neck developed . The sharp rise in the flow stress is due to the increased strain-rates during necking. The maximum observed value of effective stress...for the material modeling. Computer programs and special purpose subroutines were developed to use the Bodner-Partom model in the STEALTH finite

Environmental and High-Strain Rate effects on composites for engine applications

NASA Technical Reports Server (NTRS)

Chamis, C. C.; Smith, G. T.

1982-01-01

The Lewis Research Center is conducting a series of programs intended to investigate and develop the application of composite materials to structural components for turbojet engines. A significant part of that effort is directed to establishing resistance, defect growth, and strain rate characteristics of composite materials over the wide range of environmental and load conditions found in commercial turbojet engine operations. Both analytical and experimental efforts are involved.

Low-Cycle Fatigue Behavior of 10CrNi3MoV High Strength Steel and Its Undermatched Welds

PubMed Central

Liu, Xuesong; Berto, Filippo

2018-01-01

The use of high strength steel allows the design of lighter, more slender and simpler structures due to high strength and favorable ductility. Nevertheless, the increase of yield strength does not guarantee the corresponding improvement of fatigue resistance, which becomes a major concern for engineering structure design, especially for the welded joints. The paper presents a comparison of the low cycle fatigue behaviors between 10CrNi3MoV high strength steel and its undermatched weldments. Uniaxial tension tests, Push-pull, strain-controlled fatigue tests were conducted on base metal and weldments in the strain range of 0.2–1.2%. The monotonic and cyclic stress-strain curves, stress-life, strain-life and energy-life in terms of these materials were analyzed for fatigue assessment of materials discrepancy. The stress-life results of base metal and undermatched weld metal exhibit cyclic softening behaviors. Furthermore, the shapes of 10CrNi3MoV steel hysteresis loops show a satisfactory Masing-type behavior, while the weld metal shows a non-Masing type behavior. Strain, plastic and total strain energy density amplitudes against the number of reversals to failure results demonstrate that the undermatched weld metal presents a higher resistance to fatigue crack initiation than 10CrNi3MoV high strength steel. Finally, fatigue fracture surfaces of specimens were compared by scanning electron microscopy to identify the differences of crack initiation and the propagation between them. PMID:29695140

Low-Cycle Fatigue Behavior of 10CrNi3MoV High Strength Steel and Its Undermatched Welds.

PubMed

Song, Wei; Liu, Xuesong; Berto, Filippo; Razavi, S M J

2018-04-24

The use of high strength steel allows the design of lighter, more slender and simpler structures due to high strength and favorable ductility. Nevertheless, the increase of yield strength does not guarantee the corresponding improvement of fatigue resistance, which becomes a major concern for engineering structure design, especially for the welded joints. The paper presents a comparison of the low cycle fatigue behaviors between 10CrNi3MoV high strength steel and its undermatched weldments. Uniaxial tension tests, Push-pull, strain-controlled fatigue tests were conducted on base metal and weldments in the strain range of 0.2⁻1.2%. The monotonic and cyclic stress-strain curves, stress-life, strain-life and energy-life in terms of these materials were analyzed for fatigue assessment of materials discrepancy. The stress-life results of base metal and undermatched weld metal exhibit cyclic softening behaviors. Furthermore, the shapes of 10CrNi3MoV steel hysteresis loops show a satisfactory Masing-type behavior, while the weld metal shows a non-Masing type behavior. Strain, plastic and total strain energy density amplitudes against the number of reversals to failure results demonstrate that the undermatched weld metal presents a higher resistance to fatigue crack initiation than 10CrNi3MoV high strength steel. Finally, fatigue fracture surfaces of specimens were compared by scanning electron microscopy to identify the differences of crack initiation and the propagation between them.

Thrust chamber life prediction. Volume 1: Mechanical and physical properties of high performance rocket nozzle materials

NASA Technical Reports Server (NTRS)

Esposito, J. J.; Zabora, R. F.

1975-01-01

Pertinent mechanical and physical properties of six high conductivity metals were determined. The metals included Amzirc, NARloy Z, oxygen free pure copper, electroformed copper, fine silver, and electroformed nickel. Selection of these materials was based on their possible use in high performance reusable rocket nozzles. The typical room temperature properties determined for each material included tensile ultimate strength, tensile yield strength, elongation, reduction of area, modulus of elasticity, Poisson's ratio, density, specific heat, thermal conductivity, and coefficient of thermal expansion. Typical static tensile stress-strain curves, cyclic stress-strain curves, and low-cycle fatigue life curves are shown. Properties versus temperature are presented in graphical form for temperatures from 27.6K (-410 F) to 810.9K (1000 F).

Optical Fiber Strain Instrumentation for High Temperature Aerospace Structural Monitoring

NASA Technical Reports Server (NTRS)

Wang, A.

2002-01-01

The objective of the program is the development and laboratory demonstration of sensors based on silica optical fibers for measurement of high temperature strain for aerospace materials evaluations. A complete fiber strain sensor system based on white-light interferometry was designed and implemented. An experiment set-up was constructed to permit testing of strain measurement up to 850 C. The strain is created by bending an alumina cantilever beam to which is the fiber sensor is attached. The strain calibration is provided by the application of known beam deflections. To ensure the high temperature operation capability of the sensor, gold-coated single-mode fiber is used. Moreover, a new method of sensor surface attachment which permits accurate sensor gage length determination is also developed. Excellent results were obtained at temperatures up to 800-850 C.

Deformation twinning: Influence of strain rate

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gray, G.T. III

Twins in most crystal structures, including advanced materials such as intermetallics, form more readily as the temperature of deformation is decreased or the rate of deformation is increased. Both parameters lead to the suppression of thermally-activated dislocation processes which can result in stresses high enough to nucleate and grow deformation twins. Under high-strain rate or shock-loading/impact conditions deformation twinning is observed to be promoted even in high stacking fault energy FCC metals and alloys, composites, and ordered intermetallics which normally do not readily deform via twinning. Under such conditions and in particular under the extreme loading rates typical of shockmore » wave deformation the competition between slip and deformation twinning can be examined in detail. In this paper, examples of deformation twinning in the intermetallics TiAl, Ti-48Al-lV and Ni{sub 3}A as well in the cermet Al-B{sub 4}C as a function of strain rate will be presented. Discussion includes: (1) the microstructural and experimental variables influencing twin formation in these systems and twinning topics related to high-strain-rate loading, (2) the high velocity of twin formation, and (3) the influence of deformation twinning on the constitutive response of advanced materials.« less

Photoelastic colloidal gel for a high-sensitivity strain sensor.

PubMed

Pan, Hui; Chen, Zhixin; Zhu, Shenmin; Jiang, Chun; Zhang, Di

2018-04-27

Nanoparticles, having the ability to self-assemble into an ordered structure in their suspensions, analogous to liquid crystals, have attracted extensive attention. Herein, we report a new type of colloidal gel with an ordered crystal structure assembled from 1D and 2D nanoparticles. The material has high elasticity and, more interestingly, it shows significant photoelasticity. Its refractive index can be tuned under external stress and exhibits an ultra-wide dynamic range (Δn) of the order of 10 -2 . Due to the large Δn, the material shows an extremely high strain sensibility of 720 nm/ε, an order of magnitude higher than the reported ones.

Photoelastic colloidal gel for a high-sensitivity strain sensor

NASA Astrophysics Data System (ADS)

Pan, Hui; Chen, Zhixin; Zhu, Shenmin; Jiang, Chun; Zhang, Di

2018-04-01

Nanoparticles, having the ability to self-assemble into an ordered structure in their suspensions, analogous to liquid crystals, have attracted extensive attention. Herein, we report a new type of colloidal gel with an ordered crystal structure assembled from 1D and 2D nanoparticles. The material has high elasticity and, more interestingly, it shows significant photoelasticity. Its refractive index can be tuned under external stress and exhibits an ultra-wide dynamic range (Δn) of the order of 10-2. Due to the large Δn, the material shows an extremely high strain sensibility of 720 nm/ɛ, an order of magnitude higher than the reported ones.

Characterization of the dynamic behaviour of ALGOTUF armour steel during impact and in torsion

NASA Astrophysics Data System (ADS)

Bassim, Nabil; Boakye-Yiadom, Solomon; Toussaint, Genevieve; Bolduc, Manon

2015-09-01

Algotuf is a new steel which is proposed as a candidate for armour material. To assess this application, a study of the impact properties of this steel was conducted at the University of Manitoba using two types of Hopkinson Bar systems, namely a torsional bar equipment and a direct impact system capable of producing high strain rates and large strains. Stress strain curves for the steels were obtained in pure shear and in compression. Temperatures of 25 ∘C, 200 ∘C and 500 ∘C were used in the testing. Following the testing, a microstructural examination of the specimens tested was carried out to investigate the effect of microstructure on the mechanism of failure of this material. It was found that, above a value of impact momentum corresponding to a high strain rate, adiabatic shear bands are formed. The microscopic examination showed that the initiation of these shear bands corresponded at locations where martensitic laths were present and around regions of maximum shear stresses. Generally, the shear bands act as precursors to the formation of microcracks that may lead to failure. On the other hand, the high strength and formability of the steel makes it suitable for use as an armour material.

Epitaxial growth of highly strained antimonene on Ag(111)

NASA Astrophysics Data System (ADS)

Mao, Ya-Hui; Zhang, Li-Fu; Wang, Hui-Li; Shan, Huan; Zhai, Xiao-Fang; Hu, Zhen-Peng; Zhao, Ai-Di; Wang, Bing

2018-06-01

The synthesis of antimonene, which is a promising group-V 2D material for both fundamental studies and technological applications, remains highly challenging. Thus far, it has been synthesized only by exfoliation or growth on a few substrates. In this study, we show that thin layers of antimonene can be grown on Ag(111) by molecular beam epitaxy. High-resolution scanning tunneling microscopy combined with theoretical calculations revealed that the submonolayer Sb deposited on a Ag(111) surface forms a layer of AgSb2 surface alloy upon annealing. Further deposition of Sb on the AgSb2 surface alloy causes an epitaxial layer of Sb to form, which is identified as antimonene with a buckled honeycomb structure. More interestingly, the lattice constant of the epitaxial antimonene (5 Å) is much larger than that of freestanding antimonene, indicating a high tensile strain of more than 20%. This kind of large strain is expected to make the antimonene a highly promising candidate for roomtemperature quantum spin Hall material.

Characterization of Impact Damage in Ultra-High Performance Concrete Using Spatially Correlated Nanoindentation/SEM/EDX

NASA Astrophysics Data System (ADS)

Moser, R. D.; Allison, P. G.; Chandler, M. Q.

2013-12-01

Little work has been done to study the fundamental material behaviors and failure mechanisms of cement-based materials including ordinary Portland cement concrete and ultra-high performance concretes (UHPCs) under high strain impact and penetration loads at lower length scales. These high strain rate loadings have many possible effects on UHPCs at the microscale and nanoscale, including alterations in the hydration state and bonding present in phases such as calcium silicate hydrate, in addition to fracture and debonding. In this work, the possible chemical and physical changes in UHPCs subjected to high strain rate impact and penetration loads were investigated using a novel technique wherein nanoindentation measurements were spatially correlated with images using scanning electron microscopy and chemical composition using energy dispersive x-ray microanalysis. Results indicate that impact degrades both the elastic modulus and indentation hardness of UHPCs, and in particular hydrated phases, with damage likely occurring due to microfracturing and debonding.

Use of atomic force microscopy for characterizing damage evolution during fatigue

NASA Astrophysics Data System (ADS)

Cretegny, Laurent

2000-10-01

A study of the development of surface fatigue damage in PH 13-8 Mo stainless steel and copper by atomic force microscopy (AFM) was performed. AFM observations allow highly automated, quantitative characterization of surface deformation with a resolution of 5 nm or better, which is ideal for understanding fatigue damage evolution. A secondary objective was to establish a correlation between fatigue life exhausted and impedance spectroscopy. Strain controlled fatigue tests were conducted both in high and low cycle fatigue regimes, and interruptions of the fatigue tests allowed characterizing the evolution of the surface upset at various life-fractions. In the low strain amplitude tests on stainless steel (Deltaepsilonpl/2 = 0.0026%), surface damage occurred in the shape of narrow streaks at the interface between martensite laths where reverted austenite was present. The streaks eventually coalesced to form crack nuclei. In high strain amplitude tests (Deltaepsilon pl/2 = 0.049%), fatigue surface damage was essentially dominated by the formation of extrusions. In copper, both low (Deltaepsilonpl/2 = 0.061%) and high (Deltaepsilonpl/2 = 0.134%) strain amplitude tests showed the formation of slip bands (mainly extrusions) across entire grains. Protrusions were present only in copper specimens tested at the high strain amplitude. Crack nucleation in the low strain amplitude tests occurred in both materials at the interface between a region that sustained a high level of deformation and one with little evidence of surface upset. This commonality between these two materials that are otherwise very dissimilar in nature suggests a universal scheme for location of fatigue crack nucleation sites during HCF. A procedure was developed in this study to quantitatively characterize the amount of irreversible surface strain. The proposed formalism is applicable to any material, independently of the type of surface damage, and leads to a criterion for crack nucleation based on physical evidence of surface damage. A correlation between fatigue damage and impedance spectroscopy measurements was shown in copper, in particular during the primary cyclic hardening stage. The measurements were however less sensitive to the development of surface upset that occurred beyond that stage.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Le, K. C.; Tran, T. M.; Langer, J. S.

The statistical-thermodynamic dislocation theory developed in previous papers is used here in an analysis of high-temperature deformation of aluminum and steel. Using physics-based parameters that we expect theoretically to be independent of strain rate and temperature, we are able to fit experimental stress-strain curves for three different strain rates and three different temperatures for each of these two materials. Here, our theoretical curves include yielding transitions at zero strain in agreement with experiment. We find that thermal softening effects are important even at the lowest temperatures and smallest strain rates.

Constitutive response of Rene 80 under thermal mechanical loads

NASA Technical Reports Server (NTRS)

Kim, K. S.; Cook, T. S.; Mcknight, R. L.

1988-01-01

The applicability of a classical constitutive model for stress-strain analysis of a nickel base superalloy, Rene' 80, in the gas turbine thermomechanical fatigue (TMF) environment is examined. A variety of tests were conducted to generate basic material data and to investigate the material response under cyclic thermomechanical loading. Isothermal stress-strain data were acquired at a variety of strain rates over the TMF temperature range. Creep curves were examined at 2 temperature ranges, 871 to 982 C and 760 to 871 C. The results provide optimism on the ability of the classical constitutive model for high temperature applications.

Persistently Auxetic Materials: Engineering the Poisson Ratio of 2D Self-Avoiding Membranes under Conditions of Non-Zero Anisotropic Strain.

PubMed

Ulissi, Zachary W; Govind Rajan, Ananth; Strano, Michael S

2016-08-23

Entropic surfaces represented by fluctuating two-dimensional (2D) membranes are predicted to have desirable mechanical properties when unstressed, including a negative Poisson's ratio ("auxetic" behavior). Herein, we present calculations of the strain-dependent Poisson ratio of self-avoiding 2D membranes demonstrating desirable auxetic properties over a range of mechanical strain. Finite-size membranes with unclamped boundary conditions have positive Poisson's ratio due to spontaneous non-zero mean curvature, which can be suppressed with an explicit bending rigidity in agreement with prior findings. Applying longitudinal strain along a singular axis to this system suppresses this mean curvature and the entropic out-of-plane fluctuations, resulting in a molecular-scale mechanism for realizing a negative Poisson's ratio above a critical strain, with values significantly more negative than the previously observed zero-strain limit for infinite sheets. We find that auxetic behavior persists over surprisingly high strains of more than 20% for the smallest surfaces, with desirable finite-size scaling producing surfaces with negative Poisson's ratio over a wide range of strains. These results promise the design of surfaces and composite materials with tunable Poisson's ratio by prestressing platelet inclusions or controlling the surface rigidity of a matrix of 2D materials.

Finite element formulation with embedded weak discontinuities for strain localization under dynamic conditions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jin, Tao; Mourad, Hashem M.; Bronkhorst, Curt A.

Here, we present an explicit finite element formulation designed for the treatment of strain localization under highly dynamic conditions. We also used a material stability analysis to detect the onset of localization behavior. Finite elements with embedded weak discontinuities are employed with the aim of representing subsequent localized deformation accurately. The formulation and its algorithmic implementation are described in detail. Numerical results are presented to illustrate the usefulness of this computational framework in the treatment of strain localization under highly dynamic conditions, and to examine its performance characteristics in the context of two-dimensional plane-strain problems.

Finite element formulation with embedded weak discontinuities for strain localization under dynamic conditions

DOE PAGES

Jin, Tao; Mourad, Hashem M.; Bronkhorst, Curt A.; ...

2017-09-13

Here, we present an explicit finite element formulation designed for the treatment of strain localization under highly dynamic conditions. We also used a material stability analysis to detect the onset of localization behavior. Finite elements with embedded weak discontinuities are employed with the aim of representing subsequent localized deformation accurately. The formulation and its algorithmic implementation are described in detail. Numerical results are presented to illustrate the usefulness of this computational framework in the treatment of strain localization under highly dynamic conditions, and to examine its performance characteristics in the context of two-dimensional plane-strain problems.

Limits on rock strength under high confinement

NASA Astrophysics Data System (ADS)

Renshaw, Carl E.; Schulson, Erland M.

2007-06-01

Understanding of deep earthquake source mechanisms requires knowledge of failure processes active under high confinement. Under low confinement the compressive strength of rock is well known to be limited by frictional sliding along stress-concentrating flaws. Under higher confinement strength is usually assumed limited by power-law creep associated with the movement of dislocations. In a review of existing experimental data, we find that when the confinement is high enough to suppress frictional sliding, rock strength increases as a power-law function only up to a critical normalized strain rate. Within the regime where frictional sliding is suppressed and the normalized strain rate is below the critical rate, both globally distributed ductile flow and localized brittle-like failure are observed. When frictional sliding is suppressed and the normalized strain rate is above the critical rate, failure is always localized in a brittle-like manner at a stress that is independent of the degree of confinement. Within the high-confinement, high-strain rate regime, the similarity in normalized failure strengths across a variety of rock types and minerals precludes both transformational faulting and dehydration embrittlement as strength-limiting mechanisms. The magnitude of the normalized failure strength corresponding to the transition to the high-confinement, high-strain rate regime and the observed weak dependence of failure strength on strain rate within this regime are consistent with a localized Peierls-type strength-limiting mechanism. At the highest strain rates the normalized strengths approach the theoretical limit for crystalline materials. Near-theoretical strengths have previously been observed only in nano- and micro-scale regions of materials that are effectively defect-free. Results are summarized in a new deformation mechanism map revealing that when confinement and strain rate are sufficient, strengths approaching the theoretical limit can be achieved in cm-scale sized samples of rocks rich in defects. Thus, non-frictional failure processes must be considered when interpreting rock deformation data collected under high confinement and low temperature. Further, even at higher temperatures the load-bearing ability of crustal rocks under high confinement may not be limited by a frictional process under typical geologic strain rates.

Strain effects on oxygen migration in perovskites.

PubMed

Mayeshiba, Tam; Morgan, Dane

2015-01-28

Fast oxygen transport materials are necessary for a range of technologies, including efficient and cost-effective solid oxide fuel cells, gas separation membranes, oxygen sensors, chemical looping devices, and memristors. Strain is often proposed as a method to enhance the performance of oxygen transport materials, but the magnitude of its effect and its underlying mechanisms are not well-understood, particularly in the widely-used perovskite-structured oxygen conductors. This work reports on an ab initio prediction of strain effects on migration energetics for nine perovskite systems of the form LaBO3, where B = [Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Ga]. Biaxial strain, as might be easily produced in epitaxial systems, is predicted to lead to approximately linear changes in migration energy. We find that tensile biaxial strain reduces the oxygen vacancy migration barrier across the systems studied by an average of 66 meV per percent strain for a single selected hop, with a low of 36 and a high of 89 meV decrease in migration barrier per percent strain across all systems. The estimated range for the change in migration barrier within each system is ±25 meV per percent strain when considering all hops. These results suggest that strain can significantly impact transport in these materials, e.g., a 2% tensile strain can increase the diffusion coefficient by about three orders of magnitude at 300 K (one order of magnitude at 500 °C or 773 K) for one of the most strain-responsive materials calculated here (LaCrO3). We show that a simple elasticity model, which assumes only dilative or compressive strain in a cubic environment and a fixed migration volume, can qualitatively but not quantitatively model the strain dependence of the migration energy, suggesting that factors not captured by continuum elasticity play a significant role in the strain response.

Intrinsically stretchable and healable semiconducting polymer for organic transistors

NASA Astrophysics Data System (ADS)

Oh, Jin Young; Rondeau-Gagné, Simon; Chiu, Yu-Cheng; Chortos, Alex; Lissel, Franziska; Wang, Ging-Ji Nathan; Schroeder, Bob C.; Kurosawa, Tadanori; Lopez, Jeffrey; Katsumata, Toru; Xu, Jie; Zhu, Chenxin; Gu, Xiaodan; Bae, Won-Gyu; Kim, Yeongin; Jin, Lihua; Chung, Jong Won; Tok, Jeffrey B.-H.; Bao, Zhenan

2016-11-01

Thin-film field-effect transistors are essential elements of stretchable electronic devices for wearable electronics. All of the materials and components of such transistors need to be stretchable and mechanically robust. Although there has been recent progress towards stretchable conductors, the realization of stretchable semiconductors has focused mainly on strain-accommodating engineering of materials, or blending of nanofibres or nanowires into elastomers. An alternative approach relies on using semiconductors that are intrinsically stretchable, so that they can be fabricated using standard processing methods. Molecular stretchability can be enhanced when conjugated polymers, containing modified side-chains and segmented backbones, are infused with more flexible molecular building blocks. Here we present a design concept for stretchable semiconducting polymers, which involves introducing chemical moieties to promote dynamic non-covalent crosslinking of the conjugated polymers. These non-covalent crosslinking moieties are able to undergo an energy dissipation mechanism through breakage of bonds when strain is applied, while retaining high charge transport abilities. As a result, our polymer is able to recover its high field-effect mobility performance (more than 1 square centimetre per volt per second) even after a hundred cycles at 100 per cent applied strain. Organic thin-film field-effect transistors fabricated from these materials exhibited mobility as high as 1.3 square centimetres per volt per second and a high on/off current ratio exceeding a million. The field-effect mobility remained as high as 1.12 square centimetres per volt per second at 100 per cent strain along the direction perpendicular to the strain. The field-effect mobility of damaged devices can be almost fully recovered after a solvent and thermal healing treatment. Finally, we successfully fabricated a skin-inspired stretchable organic transistor operating under deformations that might be expected in a wearable device.

Intrinsically stretchable and healable semiconducting polymer for organic transistors.

PubMed

Oh, Jin Young; Rondeau-Gagné, Simon; Chiu, Yu-Cheng; Chortos, Alex; Lissel, Franziska; Wang, Ging-Ji Nathan; Schroeder, Bob C; Kurosawa, Tadanori; Lopez, Jeffrey; Katsumata, Toru; Xu, Jie; Zhu, Chenxin; Gu, Xiaodan; Bae, Won-Gyu; Kim, Yeongin; Jin, Lihua; Chung, Jong Won; Tok, Jeffrey B-H; Bao, Zhenan

2016-11-17

Thin-film field-effect transistors are essential elements of stretchable electronic devices for wearable electronics. All of the materials and components of such transistors need to be stretchable and mechanically robust. Although there has been recent progress towards stretchable conductors, the realization of stretchable semiconductors has focused mainly on strain-accommodating engineering of materials, or blending of nanofibres or nanowires into elastomers. An alternative approach relies on using semiconductors that are intrinsically stretchable, so that they can be fabricated using standard processing methods. Molecular stretchability can be enhanced when conjugated polymers, containing modified side-chains and segmented backbones, are infused with more flexible molecular building blocks. Here we present a design concept for stretchable semiconducting polymers, which involves introducing chemical moieties to promote dynamic non-covalent crosslinking of the conjugated polymers. These non-covalent crosslinking moieties are able to undergo an energy dissipation mechanism through breakage of bonds when strain is applied, while retaining high charge transport abilities. As a result, our polymer is able to recover its high field-effect mobility performance (more than 1 square centimetre per volt per second) even after a hundred cycles at 100 per cent applied strain. Organic thin-film field-effect transistors fabricated from these materials exhibited mobility as high as 1.3 square centimetres per volt per second and a high on/off current ratio exceeding a million. The field-effect mobility remained as high as 1.12 square centimetres per volt per second at 100 per cent strain along the direction perpendicular to the strain. The field-effect mobility of damaged devices can be almost fully recovered after a solvent and thermal healing treatment. Finally, we successfully fabricated a skin-inspired stretchable organic transistor operating under deformations that might be expected in a wearable device.

Fatigue behavior and life prediction of a SiC/Ti-24Al-11Nb composite under isothermal conditions. Ph.D. Thesis

NASA Technical Reports Server (NTRS)

Bartolotta, Paul A.

1991-01-01

Metal Matrix Composites (MMC) and Intermetallic Matrix Composites (IMC) were identified as potential material candidates for advanced aerospace applications. They are especially attractive for high temperature applications which require a low density material that maintains its structural integrity at elevated temperatures. High temperature fatigue resistance plays an important role in determining the structural integrity of the material. This study attempts to examine the relevance of test techniques, failure criterion, and life prediction as they pertain to an IMC material, specifically, unidirectional SiC fiber reinforced titanium aluminide. A series of strain and load controlled fatigue tests were conducted on unidirectional SiC/Ti-24Al-11Nb composite at 425 and 815 C. Several damage mechanism regimes were identified by using a strain-based representation of the data, Talreja's fatigue life diagram concept. Results of these tests were then used to address issues of test control modes, definition of failure, and testing techniques. Finally, a strain-based life prediction method was proposed for an IMC under tensile cyclic loadings at elevated temperatures.

Controlled removal of ceramic surfaces with combination of ions implantation and ultrasonic energy

DOEpatents

Boatner, Lynn A.; Rankin, Janet; Thevenard, Paul; Romana, Laurence J.

1995-01-01

A method for tailoring or patterning the surface of ceramic articles is provided by implanting ions to predetermined depth into the ceramic material at a selected surface location with the ions being implanted at a fluence and energy adequate to damage the lattice structure of the ceramic material for bi-axially straining near-surface regions of the ceramic material to the predetermined depth. The resulting metastable near-surface regions of the ceramic material are then contacted with energy pulses from collapsing, ultrasonically-generated cavitation bubbles in a liquid medium for removing to a selected depth the ion-damaged near-surface regions containing the bi-axially strained lattice structure from the ceramic body. Additional patterning of the selected surface location on the ceramic body is provided by implanting a high fluence of high-energy, relatively-light ions at selected surface sites for relaxing the bi-axial strain in the near-surface regions defined by these sites and thereby preventing the removal of such ion-implanted sites by the energy pulses from the collapsing ultrasonic cavitation bubbles.

Coherent diffraction imaging of nanoscale strain evolution in a single crystal under high pressure

PubMed Central

Yang, Wenge; Huang, Xiaojing; Harder, Ross; Clark, Jesse N.; Robinson, Ian K.; Mao, Ho-kwang

2013-01-01

The evolution of morphology and internal strain under high pressure fundamentally alters the physical property, structural stability, phase transition and deformation mechanism of materials. Until now, only averaged strain distributions have been studied. Bragg coherent X-ray diffraction imaging is highly sensitive to the internal strain distribution of individual crystals but requires coherent illumination, which can be compromised by the complex high-pressure sample environment. Here we report the successful de-convolution of these effects with the recently developed mutual coherent function method to reveal the three-dimensional strain distribution inside a 400 nm gold single crystal during compression within a diamond-anvil cell. The three-dimensional morphology and evolution of the strain under pressures up to 6.4 GPa were obtained with better than 30 nm spatial resolution. In addition to providing a new approach for high-pressure nanotechnology and rheology studies, we draw fundamental conclusions about the origin of the anomalous compressibility of nanocrystals. PMID:23575684

Coherent diffraction imaging of nanoscale strain evolution in a single crystal under high pressure.

PubMed

Yang, Wenge; Huang, Xiaojing; Harder, Ross; Clark, Jesse N; Robinson, Ian K; Mao, Ho-kwang

2013-01-01

The evolution of morphology and internal strain under high pressure fundamentally alters the physical property, structural stability, phase transition and deformation mechanism of materials. Until now, only averaged strain distributions have been studied. Bragg coherent X-ray diffraction imaging is highly sensitive to the internal strain distribution of individual crystals but requires coherent illumination, which can be compromised by the complex high-pressure sample environment. Here we report the successful de-convolution of these effects with the recently developed mutual coherent function method to reveal the three-dimensional strain distribution inside a 400 nm gold single crystal during compression within a diamond-anvil cell. The three-dimensional morphology and evolution of the strain under pressures up to 6.4 GPa were obtained with better than 30 nm spatial resolution. In addition to providing a new approach for high-pressure nanotechnology and rheology studies, we draw fundamental conclusions about the origin of the anomalous compressibility of nanocrystals.

Cyclic deformation and phase transformation of 6Mo superaustenitic stainless steel

NASA Astrophysics Data System (ADS)

Wang, Shing-Hoa; Wu, Chia-Chang; Chen, Chih-Yuan; Yang, Jer-Ren; Chiu, Po-Kay; Fang, Jason

2007-08-01

A fatigue behavior analysis was performed on superaustenitic stainless steel UNS S31254 (Avesta Sheffield 254 SMO), which contains about 6wt.% molybdenum, to examine the cyclic hardening/softening trend, hysteresis loops, the degree of hardening, and fatigue life during cyclic straining in the total strain amplitude range from 0.2 to 1.5%. Independent of strain rate, hardening occurs first, followed by softening. The degree of hardening is dependent on the magnitude of strain amplitude. The cyclic stress-strain curve shows material softening. The lower slope of the degree of hardening versus the strain amplitude curve at a high strain rate is attributed to the fast development of dislocation structures and quick saturation. The ɛ martensite formation, either in band or sheath form, depending on the strain rate, leads to secondary hardening at the high strain amplitude of 1.5%.

On the Effects of the Lateral Strains on the Fiber Bragg Grating Response

PubMed Central

Lai, Marco; Karalekas, Dimitris; Botsis, John

2013-01-01

In this paper, a combined experimental-numerical based work was undertaken to investigate the Bragg wavelength shift response of an embedded FBG sensor when subjected to different conditions of multi-axial loading (deformation). The following cases are examined: (a) when an isotropic host material with no constrains on planes normal to the embedded sensor's axis is biaxially loaded, (b) when the same isotropic host material is subjected to hydrostatic pressure and (c) when the hydrostatically loaded host material is an anisotropic one, as in the case of a composite material, where the optical fiber is embedded along the reinforcing fibers. The comparison of the experimental results and the finite element simulations shows that, when the axial strain on the FBG sensor is the dominant component, the standard wavelength-shift strain relation can be used even if large lateral strains apply on the sensor. However when this is not the case, large errors may be introduced in the conversion of the wavelength to axial strains on the fiber. This situation arises when the FBG is placed parallel to high modulus reinforcing fibers of a polymer composite. PMID:23429580

Fracture behavior of the Fe-8Al alloy FAP-Y

DOE Office of Scientific and Technical Information (OSTI.GOV)

Alexander, D.J.

The tensile and impact properties of two heats of the reduced aluminum alloy FAP-Y have been measured and compared to the Fe{sub 3}Al alloy FA-129. The FAP-Y material has similar yield strengths up to 400{degrees}C, and much better ductility and impact properties, as compared to the FA-129. Despite excellent room-temperature ductility, the ductile-to-brittle transition temperature is still quite high, around 150{degrees}C. The material is found to be strain-rate sensitive, with a significant increase in the yield strength at strain rates of about 10{sup 3} s{sup {minus}1}. It is believed that this strain-rate sensitivity is responsible, at least in part, formore » the high ductile-to-brittle transition temperature.« less

Residual Strain in PCBs with Cu-Plated Holes

NASA Astrophysics Data System (ADS)

Rudajevova, A.; Dušek, K.

2017-12-01

The residual strain in pure printed circuit boards (PCBs) and PCBs with Cu-plated holes has been obtained by measurement of the temperature dependence of their dilatational characteristics in the x, y, and z directions up to 240°C. Shrinkage in all directions was observed for all samples of both materials in the first thermal cycle. No permanent length changes were observed in the second or subsequent thermal cycles. The residual strain was determined from the difference in relative elongation between the first and second thermal cycles. Relaxation of residual strain occurred only in the first thermal cycle, as a thermally activated process. The highest value of relaxed residual strain was found in the z direction for both materials. Relaxation of residual strain in the z direction of the pure PCB occurred only in the negative strain range, whereas relaxation of the PCB with Cu-plated holes occurred in both the positive and negative strain ranges. The relaxation of the positive strain in the PCB with Cu-plated holes in the z direction implies that this part of the PCB was under pressure during its preparation. This relaxation is a consequence of the high coefficient of thermal expansion of PCB laminate in this direction, which can also lead to cracks in Cu holes when the material is heated above the glass-transition temperature.

Strain analysis of SiGe microbridges

NASA Astrophysics Data System (ADS)

Anthony, Ross; Gilbank, Ashley; Crowe, Iain; Knights, Andrew

2018-02-01

We present the analysis of UV (325 nm) Raman scattering spectra from silicon-germanium (SiGe) microbridges where the SiGe has been formed using the so-called "condensation technique". As opposed to the conventional condensation technique in which SiGe is grown epitaxially, we use high-dose ion implantation of Ge ions into SOI as a means to introduce the initial Ge profile. The subsequent oxidation both repairs implantation induced damage, and forms epitaxial Ge. Using Si-Si and Si-Ge optical phonon modes, as well as the ratio of integrated intensities for Ge-Ge and Si-Si, we can determine both the composition and strain of the material. We show that although the material is compressively strained following condensation, by fabricating microbridge structures we can create strain relaxed or tensile strained structures, with subsequent interest for photonic applications.

Achieving high aspect ratio wrinkles by modifying material network stress.

PubMed

Chen, Yu-Cheng; Wang, Yan; McCarthy, Thomas J; Crosby, Alfred J

2017-06-07

Wrinkle aspect ratio, or the amplitude divided by the wavelength, is hindered by strain localization transitions when an increasing global compressive stress is applied to synthetic material systems. However, many examples from living organisms show extremely high aspect ratios, such as gut villi and flower petals. We use three experimental approaches to demonstrate that these high aspect ratio structures can be achieved by modifying the network stress in the wrinkle substrate. We modify the wrinkle stress and effectively delay the strain localization transition, such as folding, to larger aspect ratios by using a zero-stress initial wavy substrate, creating a secondary network with post-curing, or using chemical stress relaxation materials. A wrinkle aspect ratio as high as 0.85, almost three times higher than common values of synthetic wrinkles, is achieved, and a quantitative framework is presented to provide understanding the different strategies and predictions for future investigations.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Josefsson, Gabriella; Gamstedt, E. Kristofer; Ahvenainen, Patrik

The mechanical performance of materials reinforced by cellulose nanofibrils is highly affected by the orientation of these fibrils. This paper investigates the nanofibril orientation distribution of films of partly oriented cellulose nanofibrils. Stripes of hydrogel films were subjected to different amount of strain and, after drying, examined with X-ray diffraction to obtain the orientation of the nanofibrils in the films, caused by the stretching. The cellulose nanofibrils had initially a random in-plane orientation in the hydrogel films and the strain was applied to the films before the nanofibrils bond tightly together, which occurs during drying. The stretching resulted in amore » reorientation of the nanofibrils in the films, with monotonically increasing orientation towards the load direction with increasing strain. Estimation of nanofibril reorientation by X-ray diffraction enables quantitative comparison of the stretch-induced orientation ability of different cellulose nanofibril systems. The reorientation of nanofibrils as a consequence of an applied strain is also predicted by a geometrical model of deformation of nanofibril hydrogels. Conversely, in high-strain cold-drawing of wet cellulose nanofibril materials, the enhanced orientation is promoted by slipping of the effectively stiff fibrils.« less

Three-Axis Distributed Fiber Optic Strain Measurement in 3D Woven Composite Structures

NASA Technical Reports Server (NTRS)

Castellucci, Matt; Klute, Sandra; Lally, Evan M.; Froggatt, Mark E.; Lowry, David

2013-01-01

Recent advancements in composite materials technologies have broken further from traditional designs and require advanced instrumentation and analysis capabilities. Success or failure is highly dependent on design analysis and manufacturing processes. By monitoring smart structures throughout manufacturing and service life, residual and operational stresses can be assessed and structural integrity maintained. Composite smart structures can be manufactured by integrating fiber optic sensors into existing composite materials processes such as ply layup, filament winding and three-dimensional weaving. In this work optical fiber was integrated into 3D woven composite parts at a commercial woven products manufacturing facility. The fiber was then used to monitor the structures during a VARTM manufacturing process, and subsequent static and dynamic testing. Low cost telecommunications-grade optical fiber acts as the sensor using a high resolution commercial Optical Frequency Domain Reflectometer (OFDR) system providing distributed strain measurement at spatial resolutions as low as 2mm. Strain measurements using the optical fiber sensors are correlated to resistive strain gage measurements during static structural loading. Keywords: fiber optic, distributed strain sensing, Rayleigh scatter, optical frequency domain reflectometry

Evolution of plastic anisotropy for high-strain-rate computations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Schiferl, S.K.; Maudlin, P.J.

1994-12-01

A model for anisotropic material strength, and for changes in the anisotropy due to plastic strain, is described. This model has been developed for use in high-rate, explicit, Lagrangian multidimensional continuum-mechanics codes. The model handles anisotropies in single-phase materials, in particular the anisotropies due to crystallographic texture--preferred orientations of the single-crystal grains. Textural anisotropies, and the changes in these anisotropies, depend overwhelmingly no the crystal structure of the material and on the deformation history. The changes, particularly for a complex deformations, are not amenable to simple analytical forms. To handle this problem, the material model described here includes a texturemore » code, or micromechanical calculation, coupled to a continuum code. The texture code updates grain orientations as a function of tensor plastic strain, and calculates the yield strength in different directions. A yield function is fitted to these yield points. For each computational cell in the continuum simulation, the texture code tracks a particular set of grain orientations. The orientations will change due to the tensor strain history, and the yield function will change accordingly. Hence, the continuum code supplies a tensor strain to the texture code, and the texture code supplies an updated yield function to the continuum code. Since significant texture changes require relatively large strains--typically, a few percent or more--the texture code is not called very often, and the increase in computer time is not excessive. The model was implemented, using a finite-element continuum code and a texture code specialized for hexagonal-close-packed crystal structures. The results for several uniaxial stress problems and an explosive-forming problem are shown.« less

Analysis of the Lankford coefficient evolution at different strain rates for AA6016-T4, DP800 and DC06

NASA Astrophysics Data System (ADS)

Lenzen, Matthias; Merklein, Marion

2017-10-01

In the automotive sector, a major challenge is the deep-drawing of modern lightweight sheet metals with limited formability. Thus, conventional material models lack in accuracy due to the complex material behavior. A current field of research takes into account the evolution of the Lankford coefficient. Today, changes in anisotropy under increasing degree of deformation are not considered. Only a consolidated average value of the Lankford coefficient is included in conventional material models. This leads to an increasing error in prediction of the flow behavior and therefore to an inaccurate prognosis of the forming behavior. To increase the accuracy of the prediction quality, the strain dependent Lankford coefficient should be respected, because the R-value has a direct effect on the contour of the associated flow rule. Further, the investigated materials show a more or less extinct rate dependency of the yield stress. For this reason, the rate dependency of the Lankford coefficient during uniaxial tension is focused within this contribution. To quantify the influence of strain rate on the Lankford coefficient, tensile tests are performed for three commonly used materials, the aluminum alloy AA6016-T4, the advanced high strength steel DP800 and the deep drawing steel DC06 at three different strain rates. The strain measurement is carried out by an optical strain measurement system. An evolution of the Lankford coefficient was observed for all investigated materials. Also, an influence of the deformation velocity on the anisotropy could be detected.

Microscopic Electronic and Mechanical Properties of Ultra-Thin Layered Materials

DTIC Science & Technology

2016-07-25

Graphene single layers grown by chemical vapor deposition on single crystal Cu substrates are subject to nonuniform physisorption strains that...the observed highly nonuniform strains. 4. Connecting dopant bond type with electronic structure in N-doped graphene (reference [4]) Robust methods

NASA Astrophysics Data System (ADS)

Scapin, M.; Peroni, L.; Fichera, C.; Cambriani, A.

2014-08-01

High chromium ferritic/martensitic steel T91 (9% Cr, 1% Mo), on account of its radiation resistance, is a candidate material for nuclear reactor applications. Its joining by an impact method to create a cold joint is tested in the realm of scoping tests toward the safe operation of nuclear fuels, encapsulated in representative T91 materials. Hitherto, T91 mechanical characterization at high strain rates is relatively unknown, particularly, in relation to impact joining and also to nuclear accidents. In this study, the mechanical characterization of T91 steel was performed in tension by varying the strain-rate (10-3 up to 104 s-1) and temperature (20-800°C) on dog-bone specimens, using standard testing machines or Hopkinson Bar apparati. As expected, the material is both temperature and strain-rate sensitive and different sets of parameters for the Johnson-Cook strength model were extracted via a numerical inverse procedure, in order to obtain the most suitable set to be used in this field of applications.

Stress-strain time-dependent behavior of A356.0 aluminum alloy subjected to cyclic thermal and mechanical loadings

NASA Astrophysics Data System (ADS)

Farrahi, G. H.; Ghodrati, M.; Azadi, M.; Rezvani Rad, M.

2014-08-01

This article presents the cyclic behavior of the A356.0 aluminum alloy under low-cycle fatigue (or isothermal) and thermo-mechanical fatigue loadings. Since the thermo-mechanical fatigue (TMF) test is time consuming and has high costs in comparison to low-cycle fatigue (LCF) tests, the purpose of this research is to use LCF test results to predict the TMF behavior of the material. A time-independent model, considering the combined nonlinear isotropic/kinematic hardening law, was used to predict the TMF behavior of the material. Material constants of this model were calibrated based on room-temperature and high-temperature low-cycle fatigue tests. The nonlinear isotropic/kinematic hardening law could accurately estimate the stress-strain hysteresis loop for the LCF condition; however, for the out-of-phase TMF, the condition could not predict properly the stress value due to the strain rate effect. Therefore, a two-layer visco-plastic model and also the Johnson-Cook law were applied to improve the estimation of the stress-strain hysteresis loop. Related finite element results based on the two-layer visco-plastic model demonstrated a good agreement with experimental TMF data of the A356.0 alloy.

High Electromechanical Response of Ionic Polymer Actuators with Controlled-Morphology Aligned Carbon Nanotube/Nafion Nanocomposite Electrodes

PubMed Central

Liu, Sheng; Liu, Yang; Cebeci, Hülya; de Villoria, Roberto Guzmán; Lin, Jun-Hong

2011-01-01

Recent advances in fabricating controlled-morphology vertically aligned carbon nanotubes (VA-CNTs) with ultrahigh volume fraction create unique opportunities for markedly improving the electromechanical performance of ionic polymer conductor network composite (IPCNC) actuators. Continuous paths through inter-VA-CNT channels allow fast ion transport, and high electrical conduction of the aligned CNTs in the composite electrodes lead to fast device actuation speed (>10% strain/second). One critical issue in developing advanced actuator materials is how to suppress the strain that does not contribute to the actuation (unwanted strain) thereby reducing actuation efficiency. Here our experiments demonstrate that the VA-CNTs give an anisotropic elastic response in the composite electrodes, which suppresses the unwanted strain and markedly enhances the actuation strain (>8% strain under 4 volts). The results reported here suggest pathways for optimizing the electrode morphology in IPCNCs using ultra-high volume fraction VA-CNTs to further enhanced performance. PMID:21765822

The effect of matrix microstructure on cyclic response and fatigue behavior of particle- reinforced 2219 aluminum: Part I. room temperature behavior

NASA Astrophysics Data System (ADS)

Vyletel, G. M.; Allison, J. E.; van Aken, D. C.

1995-12-01

The low-cycle and high-cycle fatigue behavior and cyclic response of naturally aged and overaged 2219/TiC/15p and unreinforced 2219 Al were investigated using plastic strain-controlled and stress-controlled testing. In addition, the influence of grain size on the particle-reinforced materials was examined. In both reinforced and unreinforced materials, the naturally aged conditions were cyclically unstable, exhibiting an initial hardening behavior followed by an extended region of cyclic stability and ultimately a softening region. The overaged reinforced material was cyclically stable for the plastic strains examined, while the overaged unreinforced material exhibited cyclic hardening at plastic strains greater than 2.5 × 10-4. Decreasing grain size of particle-reinforced materials modestly increased the cyclic flow stress of both naturally aged and overaged materials. Reinforced and unreinforced materials exhibited similar fatigue life behaviors; however, the reinforced and unreinforced naturally aged materials had superior fatigue lives in comparison to the overaged materials. Grain size had no effect on the fatigue life behavior of the particle-reinforced materials. The fatigue lives were strongly influenced by the presence of clusters of TiC particles and exogenous Al3Ti intermetallics.

Properties of a Ni(sub 19.5)Pd(sub 30)Ti(sub 50.5) high-temperature shape memory alloy in tension and compression

NASA Technical Reports Server (NTRS)

Noebe, Ronald; Padula, Santo, II; Bigelow, Glen; Rios, Orlando; Garg, Anita; Lerch, Brad

2006-01-01

Potential applications involving high-temperature shape memory alloys have been growing in recent years. Even in those cases where promising new alloys have been identified, the knowledge base for such materials contains gaps crucial to their maturation and implementation in actuator and other applications. We begin to address this issue by characterizing the mechanical behavior of a Ni19.5Pd30Ti50.5 high-temperature shape memory alloy in both uniaxial tension and compression at various temperatures. Differences in the isothermal uniaxial deformation behavior were most notable at test temperatures below the martensite finish temperature. The elastic modulus of the material was very dependent on strain level; therefore, dynamic Young#s Modulus was determined as a function of temperature by an impulse excitation technique. More importantly, the performance of a thermally activated actuator material is dependent on the work output of the alloy. Consequently, the strain-temperature response of the Ni19.5Pd30Ti50.5 alloy under various loads was determined in both tension and compression and the specific work output calculated and compared in both loading conditions. It was found that the transformation strain and thus, the specific work output were similar regardless of the loading condition. Also, in both tension and compression, the strain-temperature loops determined under constant load conditions did not close due to the fact that the transformation strain during cooling was always larger than the transformation strain during heating. This was apparently the result of permanent plastic deformation of the martensite phase with each cycle. Consequently, before this alloy can be used under cyclic actuation conditions, modification of the microstructure or composition would be required to increase the resistance of the alloy to plastic deformation by slip.

Strain monitoring of bismaleimide composites using embedded microcavity sensor

NASA Astrophysics Data System (ADS)

Kaur, Amardeep; Anandan, Sudharshan; Yuan, Lei; Watkins, Steve E.; Chandrashekhara, K.; Xiao, Hai; Phan, Nam

2016-03-01

A type of extrinsic Fabry-Perot interferometer (EFPI) fiber optic sensor, i.e., the microcavity strain sensor, is demonstrated for embedded, high-temperature applications. The sensor is fabricated using a femtosecond (fs) laser. The fs-laser-based fabrication makes the sensor thermally stable to sustain operating temperatures as high as 800°C. The sensor has low sensitivity toward the temperature as compared to its response toward the applied strain. The performance of the EFPI sensor is tested in an embedded application. The host material is carbon fiber/bismaleimide (BMI) composite laminate that offer thermally stable characteristics at high ambient temperatures. The sensor exhibits highly linear response toward the temperature and strain. Analytical work done with embedded optical-fiber sensors using the out-of-autoclave BMI laminate was limited until now. The work presented in this paper offers an insight into the strain and temperature interactions of the embedded sensors with the BMI composites.

Strain gradient drives shear banding in metallic glasses

NASA Astrophysics Data System (ADS)

Tian, Zhi-Li; Wang, Yun-Jiang; Chen, Yan; Dai, Lan-Hong

2017-09-01

Shear banding is a nucleation-controlled process in metallic glasses (MGs) involving multiple temporal-spatial scales, which hinders a concrete understanding of its structural origin down to the atomic scale. Here, inspired by the morphology of composite materials, we propose a different perspective of MGs as a hard particle-reinforced material based on atomic-scale structural heterogeneity. The local stable structures indicated by a high level of local fivefold symmetry (L5FS) act as hard "particles" which are embedded in the relatively soft matrix. We demonstrate this concept by performing atomistic simulations of shear banding in CuZr MG. A shear band is prone to form in a sample with a high degree of L5FS which is slowly quenched from the liquid. An atomic-scale analysis on strain and the structural evolution reveals that it is the strain gradient effect that has originated from structural heterogeneity that facilitates shear transformation zones (STZs) to mature shear bands. An artificial composite model with a high degree of strain gradient, generated by inserting hard MG strips into a soft MG matrix, demonstrates a great propensity for shear banding. It therefore confirms the critical role strain gradient plays in shear banding. The strain gradient effect on shear banding is further quantified with a continuum model and a mechanical instability analysis. These physical insights might highlight the strain gradient as the hidden driving force in transforming STZs into shear bands in MGs.

A wearable strain sensor based on a carbonized nano-sponge/silicone composite for human motion detection.

PubMed

Yu, Xiao-Guang; Li, Yuan-Qing; Zhu, Wei-Bin; Huang, Pei; Wang, Tong-Tong; Hu, Ning; Fu, Shao-Yun

2017-05-25

Melamine sponge, also known as nano-sponge, is widely used as an abrasive cleaner in our daily life. In this work, the fabrication of a wearable strain sensor for human motion detection is first demonstrated with a commercially available nano-sponge as a starting material. The key resistance sensitive material in the wearable strain sensor is obtained by the encapsulation of a carbonized nano-sponge (CNS) with silicone resin. The as-fabricated CNS/silicone sensor is highly sensitive to strain with a maximum gauge factor of 18.42. In addition, the CNS/silicone sensor exhibits a fast and reliable response to various cyclic loading within a strain range of 0-15% and a loading frequency range of 0.01-1 Hz. Finally, the CNS/silicone sensor as a wearable device for human motion detection including joint motion, eye blinking, blood pulse and breathing is demonstrated by attaching the sensor to the corresponding parts of the human body. In consideration of the simple fabrication technique, low material cost and excellent strain sensing performance, the CNS/silicone sensor is believed to have great potential in the next-generation of wearable devices for human motion detection.

Use of photostress to characterize the mechanical behavior of weldments

NASA Technical Reports Server (NTRS)

Gambrell, S. C., Jr.

1992-01-01

Welded aluminum is an important part of many space structures. Knowledge of the properties and behavior of weld material and the material surrounding the weld is important for modeling and design of the structures. Photoelastic coatings (Photostress) and strain gages were used to determine behavior of heat treated and as welded joints made from 2219T87 parent material and 2319 weld material subjected to tensile loads. TIG welds of 1/8, 1/2, and 1.4 inches thickness were investigated. Discontinuous yielding was observed in all tests and highly non-uniform behavior through the weld thickness was observed in joints having welds 1.4 inches thick. Joints having welds 1/8 and 1/2 inches thick had only small differences in behavior through the thickness of the weld. Joints in the 1/2 inch thick material contained distinct zones of constant strain within the normal strain gradient extending outward from the weld centerline. These zones had different thickness and locations. Points at the weld centerline, and for a distance of nearly one inch from the centerline, exhibited very nonlinear behavior during the first loading but exhibited near perfect strain hardening during the second loading.

Predicting the Highly Nonlinear Mechanical Properties of Polymeric Materials

NASA Astrophysics Data System (ADS)

Porter, David

2009-06-01

Over the past few years, we have developed models that calculate the highly nonlinear mechanical properties of polymers as a function of temperature, strain and strain rate from their molecular and morphological structure. A review of these models is presented here, with emphasis on combining the fundamental aspects of molecular physics that dictate these properties and the pragmatic need to make realistic predictions for our customers; the designer of new materials and the engineers who use these materials. The models calculate the highly nonlinear mechanical properties of polymers as a function of temperature, strain and strain rate from their molecular structure. The model is based upon the premise that mechanical properties are a direct consequence of energy stored and energy dissipated during deformation of a material. This premise is transformed into a consistent set of structure-property relations for the equation of state, EoS, and the engineering constitutive relations in a polymer by quantifying energy storage and loss at the molecular level of interactions between characteristic groups of atoms in a polymer. These relations are derived from a simple volumetric mean field Lennard-Jones potential function for the potential energy of intermolecular interactions in a polymer. First, properties such as temperature-volume relations and glass transition temperature are calculated directly from the potential function. Then, the `shock' EoS is derived simply by differentiating the potential function with respect to volume, assuming that the molecules cannot relax in the time scales of the deformation. The energy components are then used to predict the dynamic mechanical spectrum of a polymer in terms of temperature and rate. This can be transformed directly into the highly nonlinear stress-strain relations through yield. The constitutive relations are formulated as a set of analytical equations that predict properties directly in terms of a small set of structural parameters that can be calculated directly and independently from the chemical composition and morphology of a polymer. A number of examples are given to illustrate the model and also to show that the method can be applied, with appropriate modifications, to other materials.

High-Strain-Rate Material Behavior and Adiabatic Material Instability in Impact of Micron-Scale Al-6061 Particles

NASA Astrophysics Data System (ADS)

Chen, Qiyong; Alizadeh, Arash; Xie, Wanting; Wang, Xuemei; Champagne, Victor; Gouldstone, Andrew; Lee, Jae-Hwang; Müftü, Sinan

2018-04-01

Impact of spherical particles onto a flat sapphire surface was investigated in 50-950 m/s impact speed range experimentally and theoretically. Material parameters of the bilinear Johnson-Cook model were determined based on comparison of deformed particle shapes from experiment and simulation. Effects of high-strain-rate plastic flow, heat generation due to plasticity, material damage, interfacial friction and heat transfer were modeled. Four distinct regions were identified inside the particle by analyzing temporal variation of material flow. A relatively small volume of material near the impact zone becomes unstable due to plasticity-induced heating, accompanied by severe drop in the flow stress for impact velocity that exceeds 500 m/s. Outside of this region, flow stress is reduced due to temperature effects without the instability. Load carrying capacity of the material degrades and the material expands horizontally leading to jetting. The increase in overall plastic and frictional dissipation with impact velocity was found to be inherently lower than the increase in the kinetic energy at high speeds, leading to the instability. This work introduces a novel method to characterize HSR (109 s-1) material properties and also explains coupling between HSR material behavior and mechanics that lead to extreme deformation.

Modeling of yield surface evolution in uniaxial and biaxial loading conditions using a prestrained large scale specimen

NASA Astrophysics Data System (ADS)

Zaman, Shakil Bin; Barlat, Frédéric; Kim, Jin Hwan

2018-05-01

Large-scale advanced high strength steel (AHSS) sheet specimens were deformed in uniaxial tension, using a novel grip system mounted on a MTS universal tension machine. After pre-strain, they were used as a pre-strained material to examine the anisotropic response in the biaxial tension tests with various load ratios, and orthogonal tension tests at 45° and 90° from the pre-strain axis. The flow curve and the instantaneous r-value of the pre-strained steel in each of the aforementioned uniaxial testing conditions were also measured and compared with those of the undeformed steel. Furthermore, an exhaustive analysis of the yield surface was also conducted and the results, prior and post-prestrain were represented and compared. The homogeneous anisotropic hardening (HAH) model [1] was employed to predict the behavior of the pre-strained material. It was found that the HAH-predicted flow curves after non-linear strain path change and the yield loci after uniaxial pre-strain were in good agreement with the experiments, while the r-value evolution after strain path change was qualitatively well predicted.

Grain-size-independent plastic flow at ultrahigh pressures and strain rates.

PubMed

Park, H-S; Rudd, R E; Cavallo, R M; Barton, N R; Arsenlis, A; Belof, J L; Blobaum, K J M; El-dasher, B S; Florando, J N; Huntington, C M; Maddox, B R; May, M J; Plechaty, C; Prisbrey, S T; Remington, B A; Wallace, R J; Wehrenberg, C E; Wilson, M J; Comley, A J; Giraldez, E; Nikroo, A; Farrell, M; Randall, G; Gray, G T

2015-02-13

A basic tenet of material science is that the flow stress of a metal increases as its grain size decreases, an effect described by the Hall-Petch relation. This relation is used extensively in material design to optimize the hardness, durability, survivability, and ductility of structural metals. This Letter reports experimental results in a new regime of high pressures and strain rates that challenge this basic tenet of mechanical metallurgy. We report measurements of the plastic flow of the model body-centered-cubic metal tantalum made under conditions of high pressure (>100  GPa) and strain rate (∼10(7)  s(-1)) achieved by using the Omega laser. Under these unique plastic deformation ("flow") conditions, the effect of grain size is found to be negligible for grain sizes >0.25  μm sizes. A multiscale model of the plastic flow suggests that pressure and strain rate hardening dominate over the grain-size effects. Theoretical estimates, based on grain compatibility and geometrically necessary dislocations, corroborate this conclusion.

Contrastive thermoelectric properties of strained SnSe crystals from the first-principles calculations

NASA Astrophysics Data System (ADS)

Tang, Yu; Cheng, Feng; Li, Decong; Deng, Shuping; Chen, Zhong; Sun, Luqi; Liu, Wenting; Shen, Lanxian; Deng, Shukang

2018-06-01

SnSe is a promising thermoelectric material with a record high dimensionless figure of merit ZT at high temperature ∼923 K. However, the ZT values for low-Temperature Pnma phase SnSe are just 0.1-0.9. Here, we use First-principle combine with Boltzmann transport theory methods to study the effect of tensile and compressible strain on the thermoelectric transport properties. The power factor of SnSe with -4% strain have a large boost along b and c directions of 7.7 and 3.9 μW cm-1 K-2, respectively, which are 2.5 and 2 times as large as those pristine SnSe. The charge density distributions reveal that the overlap of wave function has significant change due to the changed bond lengths and bond angles under different strain, which lead to the change of band gap and band dispersion. Our work provides a new effective strategy to enhance the thermoelectric properties of materials.

Synthesis of Germanium-Tin Alloys by Ion Implantation and Pulsed Laser Melting: Towards a Group IV Direct Band Gap Semiconductor

NASA Astrophysics Data System (ADS)

Tran, Tuan Thien

The germanium-tin (Ge1-xSnx) material system is expected to be a direct bandgap group IV semiconductor at a Sn content of 6.5-11 at.%. Hence there has been much interest in preparing such alloys since they are compatible with silicon and they raise the possibility of integrating photonics functionality into silicon circuitry. However, the maximum solid solubility of Sn in Ge is around 0.5 at.% and non-equilibrium deposition techniques such as molecular beam epitaxy or chemical vapour deposition have been used to achieve the desired high Sn concentrations. In this PhD work, the combination of ion implantation and pulsed laser melting (PLM) is demonstrated to be an alternative promising method to produce a highly Sn concentrated alloy with good crystal quality. In initial studies, it was shown that 100 keV Sn implants followed by PLM produced high quality alloys with up to 6.2 at.%Sn but above these Sn concentrations the crystal quality was poor. The structural properties of the ≤6.2 at.% alloys such as soluble Sn concentration, strain distribution and crystal quality have been characterised by Rutherford backscattering spectrometry (RBS), Raman spectroscopy, X-ray diffraction (XRD) and transmission electron microscopy (TEM). The optical properties and electronic band structure have been studied by spectroscopic ellipsometry. The introduction of substitutional Sn into Ge is shown to either induce a splitting between light and heavy hole subbands or lower the conduction band at the Gamma valley. However, at higher implant doses needed to achieve >6.2 at.% Sn, ion-beam-induced porosity in Ge starts to occur, which drastically reduces the retained amount of the implanted Sn and such microstructure also hinders good crystallisation of the material during PLM. To solve this problem, it was shown that a nanometer thick SiO2 layer deposited on the Ge substrate prior to the implantation can largely eliminate the formation of porosity. This capping SiO2 layer also helps to increase the retained Sn concentration up to 15 at.% after implantation, as well as significantly improving the crystal quality of the Ge-Sn layer after PLM. With the use of the capping layer, a good quality Ge-Sn layer with 9 at.% Sn has been achieved using Sn implants at an energy of 120 keV. However, the thin film alloys produced by 100 keV or 120 keV Sn implantation and PLM are shown to contain compressive strain as a result of the large lattice mismatch between Ge and high Sn content alloys. Such strain compromises the tendency towards a direct bandgap material and hence strain relaxation is highly desirable. A thermal stability study showed that the thin film strained material is metastable up to 400°C, but thereafter Sn comes out of solution and diffuses to the material surface. To investigate a possible pathway to the synthesis of strain-relaxed material, a higher Sn implant energy of 350 keV was used to produce thicker alloy layers. XRD/reciprocal space mapping showed that this thicker alloy material is largely relaxed after PLM, which is beneficial for the direct band gap transition and solves the trade-off between higher Sn concentration and compressive strain. However, RBS indicates a sub-surface band of disorder which suggested a possible mechanism for the strain relaxation. Indeed, TEM examination of such material showed the material relaxed via the generation of non-equilibrium threading defects. Despite such defects, a PL study of this relaxed material found photon emission at a wavelength of 2150 nm for 6-9 at.% Sn alloys. However, the intensity of the emission was variable across different Sn content alloys, presumably as a result of the threading defects. A possible pathway to removing such defects is given that may enable both photodetectors and lasers to be fabricated at wavelengths above 2mum.

Shell-binary nanoparticle materials with variable electrical and electro-mechanical properties.

PubMed

Zhang, P; Bousack, H; Dai, Y; Offenhäusser, A; Mayer, D

2018-01-18

Nanoparticle (NP) materials with the capability to adjust their electrical and electro-mechanical properties facilitate applications in strain sensing technology. Traditional NP materials based on single component NPs lack a systematic and effective means of tuning their electrical and electro-mechanical properties. Here, we report on a new type of shell-binary NP material fabricated by self-assembly with either homogeneous or heterogeneous arrangements of NPs. Variable electrical and electro-mechanical properties were obtained for both materials. We show that the electrical and electro-mechanical properties of these shell-binary NP materials are highly tunable and strongly affected by the NP species as well as their corresponding volume fraction ratio. The conductivity and the gauge factor of these shell-binary NP materials can be altered by about five and two orders of magnitude, respectively. These shell-binary NP materials with different arrangements of NPs also demonstrate different volume fraction dependent electro-mechanical properties. The shell-binary NP materials with a heterogeneous arrangement of NPs exhibit a peaking of the sensitivity at medium mixing ratios, which arises from the aggregation induced local strain enhancement. Studies on the electron transport regimes and micro-morphologies of these shell-binary NP materials revealed the different mechanisms accounting for the variable electrical and electro-mechanical properties. A model based on effective medium theory is used to describe the electrical and electro-mechanical properties of such shell-binary nanomaterials and shows an excellent match with experiment data. These shell-binary NP materials possess great potential applications in high-performance strain sensing technology due to their variable electrical and electro-mechanical properties.

Real-time sonoelastography using an external reference material: test-retest reliability of healthy Achilles tendons.

PubMed

Schneebeli, Alessandro; Del Grande, Filippo; Vincenzo, Gabriele; Cescon, Corrado; Clijsen, Ron; Biordi, Fulvio; Barbero, Marco

2016-08-01

To establish the test-retest reliability of sonoelastography (SE) on healthy Achilles tendons in contracted and relaxed states using an external reference system. Forty-eight Achilles tendons from 24 healthy volunteers were assessed using ultrasound and real-time SE with an external reference material. Tendons were analyzed under relaxed and contracted conditions. Strain ratios between the tendons and the reference material were calculated. The intraclass correlation coefficient (ICC2.k) and Bland-Altman plot were used to assess test-retest reliability. The reliability of SE measurements under relaxed conditions ranged from high to very high, with an ICC2.k of 0.84 (95 % CI: 0.64-0.92) for reference material, 0.91 (95 % CI: 0.83-0.95) for Achilles tendons and 0.95 (95 % CI: 0.91-0.97) for Kager fat pads (KFP). The ICC2.k value for skin was 0.30 (95 % CI: -0.26 to 0.61). Reliability for measurements in the contracted state ranged from high to very high, with an ICC2.k of 0.93 (95 % CI: 0.87-0.96) for reference material, 0.72 (95 % CI: 0.50-0.84) for skin, 0.93 (95 % CI: 0.87-0.96) for Achilles tendons, and 0.81 (95 % CI: 0.66-0.89) for KFP. Reliability of the strain ratio (tendon/reference) under relaxed conditions was high with an ICC2.k of 0.87 (95 % CI: 0.75-0.93), and in the contracted state, it was very high with an ICC2.k of 0.94 (95 % CI: 0.90-0.97). Sonoelastography using an external reference material is a reliable and simple technique for the assessment of the elasticity of healthy Achilles tendons. The use of an external material as a reference, along with strain ratios, could provide a quantitative measure of elasticity.

Biodeuterated Materials: High-Temperature Lubricants from Algae.

DTIC Science & Technology

1986-01-06

to obtain significant growth in D20 media. 1. Chlorella vulgaris (UTEX 397) 2. Chlorella vulgaris (Arg) 3. Scenedesmus obliquus (Arg) 4. Scenedesmus...the other two strains, and almost half of the total fatty acids of strain 1237 was 18:1. Effect of Nitrogen-Deficient Media Chlorella vulgaris (Arg...2.3 36 18 4.5 strain 1237 D20 31 2.9 -- 46 14 5.7 Chlorella vulgaris strain 397 H20 53 9.3 -- 1.6 5.6 19 12 strain 397 D20 28 2.3 -- 6.4 30 23 9.5

Hinge-like structure induced unusual properties of black phosphorus and new strategies to improve the thermoelectric performance

PubMed Central

Qin, Guangzhao; Yan, Qing-Bo; Qin, Zhenzhen; Yue, Sheng-Ying; Cui, Hui-Juan; Zheng, Qing-Rong; Su, Gang

2014-01-01

We systematically investigated the geometric, electronic and thermoelectric (TE) properties of bulk black phosphorus (BP) under strain. The hinge-like structure of BP brings unusual mechanical responses such as anisotropic Young's modulus and negative Poisson's ratio. A sensitive electronic structure of BP makes it transform among metal, direct and indirect semiconductors under strain. The maximal figure of merit ZT of BP is found to be 0.72 at 800 K that could be enhanced to 0.87 by exerting an appropriate strain, revealing BP could be a potential medium-high temperature TE material. Such strain-induced enhancements of TE performance are often observed to occur at the boundary of the direct-indirect band gap transition, which can be attributed to the increase of degeneracy of energy valleys at the transition point. By comparing the structure of BP with SnSe, a family of potential TE materials with hinge-like structure are suggested. This study not only exposes various novel properties of BP under strain, but also proposes effective strategies to seek for better TE materials. PMID:25374306

Biaxial experiments supporting the development of constitutive theories for advanced high-temperature materials

NASA Technical Reports Server (NTRS)

Ellis, J. R.

1988-01-01

Complex states of stress and strain are introduced into components during service in engineering applications. It follows that analysis of such components requires material descriptions, or constitutive theories, which reflect the tensorial nature of stress and strain. For applications involving stress levels above yield, the situation is more complex in that material response is both nonlinear and history dependent. This has led to the development of viscoplastic constitutive theories which introduce time by expressing the flow and evolutionary equation in the form of time derivatives. Models were developed here which can be used to analyze high temperature components manufactured from advanced composite materials. In parallel with these studies, effort was directed at developing multiaxial testing techniques to verify the various theories. Recent progress in the development of constitutive theories from both the theoretical and experimental viewpoints are outlined. One important aspect is that material descriptions for advanced composite materials which can be implemented in general purpose finite element codes and used for practical design are verified.

The Constitutive Modeling of Thin Films with Randon Material Wrinkles

NASA Technical Reports Server (NTRS)

Murphey, Thomas W.; Mikulas, Martin M.

2001-01-01

Material wrinkles drastically alter the structural constitutive properties of thin films. Normally linear elastic materials, when wrinkled, become highly nonlinear and initially inelastic. Stiffness' reduced by 99% and negative Poisson's ratios are typically observed. This paper presents an effective continuum constitutive model for the elastic effects of material wrinkles in thin films. The model considers general two-dimensional stress and strain states (simultaneous bi-axial and shear stress/strain) and neglects out of plane bending. The constitutive model is derived from a traditional mechanics analysis of an idealized physical model of random material wrinkles. Model parameters are the directly measurable wrinkle characteristics of amplitude and wavelength. For these reasons, the equations are mechanistic and deterministic. The model is compared with bi-axial tensile test data for wrinkled Kaptong(Registered Trademark) HN and is shown to deterministically predict strain as a function of stress with an average RMS error of 22%. On average, fitting the model to test data yields an RMS error of 1.2%

Ultrasonic cavitation erosion-corrosion behavior of friction stir processed stainless steel.

PubMed

Selvam, Karthikeyan; Mandal, Priya; Grewal, Harpreet Singh; Arora, Harpreet Singh

2018-06-01

Cavitation erosion remains the primary cause of material degradation in fluid machinery components operating at high speed. Micro-jets/shock waves caused by implosion of bubbles on material surface results in significant material loss and premature failure of the components. The presence of corrosive medium further exuberates this effect, causing rapid degradation. Here, we demonstrate a novel pathway to control cavitation erosion-corrosion by tailoring the surface properties using submerged friction stir processing (FSP), a severe plastic deformation process. FSP parameters were varied over wide range of strain-rates to generate tailored microstructures. High strain-rate processing resulted in nearly single phase fine grained structure while low strain-rate processing resulted in phase transformation in addition to grain refinement. As-received and processed samples were subjected to ultrasonic cavitation in distilled water as well as in corrosive environment of 3.5% NaCl solution. Individual roles of cavitation erosion, corrosion and their synergistic effects were analyzed. Depending on the microstructure, processed samples showed nearly 4-6 times higher cavitation erosion resistance compared to as-received alloy. Superior cavitation erosion-corrosion resistance of processed samples was attributed to surface strengthening, higher strain-hardening ability and quick passivation kinetics. The results of current study could be potentially transformative in designing robust materials for hydro-dynamic applications. Copyright © 2018 Elsevier B.V. All rights reserved.

Methodology for Mechanical Property Testing on Fuel Cladding Using an Expanded Plug Wedge Test

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Jy-An John; Jiang, Hao

To determine the tensile properties of irradiated fuel cladding in a hot cell, a simple test was developed at ORNL and is described fully in US Patent Application 20060070455, Expanded plug method for developing circumferential mechanical properties of tubular materials. This method is designed for testing fuel rod cladding ductility in a hot cell utilizing an expandable plug to stretch a small ring of irradiated cladding material. The specimen strain is determined using the measured diametrical expansion of the ring. This method removes many complexities associated with specimen preparation and testing. The advantages are the simplicity of measuring the testmore » component assembly in the hot cell and the direct measurement of specimen strain. It was also found that cladding strength could be determined from the test results. The basic approach of this test method is to apply an axial compressive load to a cylindrical plug of polyurethane (or other materials) fitted inside a short ring of the test material to achieve radial expansion of the specimen. The diameter increase of the specimen is used to calculate the circumferential strain accrued during the test. The other two basic measurements are total applied load and amount of plug compression (extension). A simple procedure is used to convert the load circumferential strain data from the ring tests into material pseudo-stress-strain curves. However, several deficiencies exist in this expanded-plug loading ring test, which will impact accuracy of test results and introduce potential shear failure of the specimen due to inherited large axial compressive stress from the expansion plug test. First of all, the highly non-uniform stress and strain distribution resulted in the gage section of the clad. To ensure reliable testing and test repeatability, the potential for highly non-uniform stress distribution or displacement/strain deformation has to be eliminated at the gage section of the specimen. Second, significant compressive stresses were induced by clad bending deformation due to a clad bulging effect (or the barreling effect). The barreling effect caused very large localized shear stress in the clad and left testing material at a high risk of shear failure. The above combined effects will result in highly non-conservative predictions both in strength and ductility of the tested clad, and the associated mechanical properties as well. To overcome/mitigate the mentioned deficiencies associated with the current expansion plug test, systematic studies have been conducted. Through detailed parameter investigation on specific geometry designs, careful filtering of material for the expansion plug, as well as adding newly designed parts to the testing system, a method to reconcile the potential non-conservatism embedded in the expansion plug test system has been discovered. A modified expansion plug testing protocol has been developed based on the method. In order to closely resemble thin-wall theory, a general procedure was also developed to determine the hoop stress in the tested ring specimen. A scaling factor called -factor is defined to correlate the ring load P into hoop stress . , = . The generated stress-strain curve agrees very well with tensile test data in both the elastic and plastic regions.« less

Analysis and interpretation of diffraction data from complex, anisotropic materials

NASA Astrophysics Data System (ADS)

Tutuncu, Goknur

Most materials are elastically anisotropic and exhibit additional anisotropy beyond elastic deformation. For instance, in ferroelectric materials the main inelastic deformation mode is via domains, which are highly anisotropic crystallographic features. To quantify this anisotropy of ferroelectrics, advanced X-ray and neutron diffraction methods were employed. Extensive sets of data were collected from tetragonal BaTiO3, PZT and other ferroelectric ceramics. Data analysis was challenging due to the complex constitutive behavior of these materials. To quantify the elastic strain and texture evolution in ferroelectrics under loading, a number of data analysis techniques such as the single peak and Rietveld methods were used and their advantages and disadvantages compared. It was observed that the single peak analysis fails at low peak intensities especially after domain switching while the Rietveld method does not account for lattice strain anisotropy although it overcomes the low intensity problem via whole pattern analysis. To better account for strain anisotropy the constant stress (Reuss) approximation was employed within the Rietveld method and new formulations to estimate lattice strain were proposed. Along the way, new approaches for handling highly anisotropic lattice strain data were also developed and applied. All of the ceramics studied exhibited significant changes in their crystallographic texture after loading indicating non-180° domain switching. For a full interpretation of domain switching the spherical harmonics method was employed in Rietveld. A procedure for simultaneous refinement of multiple data sets was established for a complete texture analysis. To further interpret diffraction data, a solid mechanics model based on the self-consistent approach was used in calculating lattice strain and texture evolution during the loading of a polycrystalline ferroelectric. The model estimates both the macroscopic average response of a specimen and its hkl-dependent lattice strains for different reflections. It also tracks the number of grains (or domains) contributing to each reflection and allows for domain switching. The agreement between the model and experimental data was found to be satisfactory.

Finite element stress analysis of polymers at high strains

NASA Technical Reports Server (NTRS)

Durand, M.; Jankovich, E.

1973-01-01

A numerical analysis is presented for the problem of a flat rectangular rubber membrane with a circular rigid inclusion undergoing high strains due to the action of an axial load. The neo-hookean constitutive equations are introduced into the general purpose TITUS program by means of equivalent hookean constants and initial strains. The convergence is achieved after a few iterations. The method is not limited to any specific program. The results are in good agreement with those of a company sponsored photoelastic stress analysis. The theoretical and experimental deformed shapes also agree very closely with one another. For high strains it is demonstrated that using the conventional HOOKE law the stress concentration factor obtained is unreliable in the case of rubberlike material.

European Science Notes Information Bulletin Reports on Current European/Middle Eastern Science,

DTIC Science & Technology

1989-07-01

behavior at high rates of strain, and composite materials at high rates of strain. ESNIB 89-07 International Conference on Interaction of Steels with... drug mole-armacology,. ture will be the sterility, energy and mass transfer, shearcults possess N-alkyl functions, usually in saturated struc- tures...tnerapcutic agents. This is usually cell densities and high metabolically active cells, the achieved by N-dcalklyating the parent drug molecule to

Mechanical Components from Highly Recoverable, Low Apparent Modulus Materials

NASA Technical Reports Server (NTRS)

Padula, Santo, II (Inventor); Noebe, Ronald D. (Inventor); Stanford, Malcolm K. (Inventor); DellaCorte, Christopher (Inventor)

2015-01-01

A material for use as a mechanical component is formed of a superelastic intermetallic material having a low apparent modulus and a high hardness. The superelastic intermetallic material is conditioned to be dimensionally stable, devoid of any shape memory effect and have a stable superelastic response without irrecoverable deformation while exhibiting strains of at least 3%. The method of conditioning the superelastic intermetallic material is described. Another embodiment relates to lightweight materials known as ordered intermetallics that perform well in sliding wear applications using conventional liquid lubricants and are therefore suitable for resilient, high performance mechanical components such as gears and bearings.

Thin Film Ceramic Strain Sensor Development for High Temperature Environments

NASA Technical Reports Server (NTRS)

Wrbanek, John D.; Fralick, Gustave C.; Gonzalez, Jose M.; Laster, Kimala L.

2008-01-01

The need for sensors to operate in harsh environments is illustrated by the need for measurements in the turbine engine hot section. The degradation and damage that develops over time in hot section components can lead to catastrophic failure. At present, the degradation processes that occur in the harsh hot section environment are poorly characterized, which hinders development of more durable components, and since it is so difficult to model turbine blade temperatures, strains, etc, actual measurements are needed. The need to consider ceramic sensing elements is brought about by the temperature limits of metal thin film sensors in harsh environments. The effort at the NASA Glenn Research Center (GRC) to develop high temperature thin film ceramic static strain gauges for application in turbine engines is described, first in the fan and compressor modules, and then in the hot section. The near-term goal of this research effort was to identify candidate thin film ceramic sensor materials and provide a list of possible thin film ceramic sensor materials and corresponding properties to test for viability. A thorough literature search was conducted for ceramics that have the potential for application as high temperature thin film strain gauges chemically and physically compatible with the NASA GRCs microfabrication procedures and substrate materials. Test results are given for tantalum, titanium and zirconium-based nitride and oxynitride ceramic films.

Constitutive equations for multiphase TRIP steels at high rates of strain

NASA Astrophysics Data System (ADS)

van Slycken, J.; Verleysen, P.; Degrieck, J.; Bouquerel, J.

2006-08-01

Multiphase TRansformation Induced Plasticity (TRIP) steels show an excellent combination of high strength and high strain values, making them ideally suited for use in vehicle body structures. A complex synergy of three different phases (ferrite, bainite and austenite) on the one hand, and the meta-stable character of the austenite on the other hand, give the material indeed a high energy absorption potential. The knowledge and understanding of the dynamic behaviour of these sheet steels is essential to investigate the impact-dynamic characteristics of the structures. Therefore split Hopkinson tensile tests are performed in a strain rate range of 500 to 2000 s-1. Three TRIP steel grades with a different Al and Si content were studied. The experimental results show that these steels preserve their excellent shock-absorbing properties in dynamic conditions. The typical high strain rate loading conditions and the complex behaviour of TRIP steels offer a unique investigation opportunity. This behaviour can be described with phenomenological material models that can be used for numerical simulations of car crashes. The Johnson-Cook model, a frequently used model in finite element codes, is well-suited to describe the dynamic behaviour of the investigated TRIP steels. This model is compared to the Rusinek-Klepaczko model.

Effect of Creep and Oxidation on Reduced Creep-Fatigue life of Ni-based Alloy 617 at 850 C

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, Xiang; Yang, Zhiqing; Sokolov, Mikhail A

Low cycle fatigue (LCF) and creep fatigue testing of Ni-based alloy 617 was carried out at 850 C. Compared with its LCF life, the material s creep fatigue life decreases to different extents depending on test conditions. To elucidate the microstructure-fatigue property relationship for alloy 617 and the effect of creep and oxidation on its fatigue life, systematic microstructural investigations were carried out using scanning electron microscopy, energy-dispersive X-ray spectroscopy, and electron backscatter diffraction (EBSD). In LCF tests, as the total strain range increased, deformations concentrated near high angle grain boundaries (HAGBs). The strain hold period in the creep fatiguemore » tests introduced additional creep damage to the material, which revealed the detrimental effect of the strain hold time on the material fatigue life in two ways. First, the strain hold time enhanced the localized deformation near HAGBs, resulting in the promotion of intergranular cracking of alloy 617. Second, the strain hold time encouraged grain boundary sliding, which resulted in interior intergranular cracking of the material. Oxidation accelerated the initiation of intergranular cracking in alloy 617. In the crack propagation stage, if oxidation was promoted and the cyclic oxidation damage was greater than the fatigue damage, oxidation-assisted intergranular crack growth resulted in a significant reduction in the material s fatigue life.« less

Flexible gas sensor based on graphene/ethyl cellulose nanocomposite with ultra-low strain response for volatile organic compounds rapid detection

NASA Astrophysics Data System (ADS)

Zhang, Qiankun; An, Chunhua; Fan, Shuangqing; Shi, Sigang; Zhang, Rongjie; Zhang, Jing; Li, Quanning; Zhang, Daihua; Hu, Xiaodong; Liu, Jing

2018-07-01

Minimizing the strain-induced undesirable effects is one of the major efforts to be made for flexible electronics. This work demonstrates a highly sensitive flexible gas sensor with ultra-low strain response, which is potentially suitable for wearable electronics applications. The gas sensing material is a free-standing and flexible thin film made of graphene/ethyl cellulose (EC) nanocomposite, which is then integrated with flexible substrate of polyethylene terephthalate. The sensor exhibits relative resistance change within 0.3% at a minimum bending radius of 3.18 mm and 0.2% at the bending radius of 5 mm after 400 bending cycles. The limited strain response attributes to several applied strategies, including using EC with high Young’s modulus as the matrix material, maintaining high graphene concentration and adopting suspended device structure. In contrast to the almost negligible strain sensitivity, the sensor presents large and rapid responses toward volatile organic compounds (VOCs) at room temperature. Specifically, the sensor resistance rapidly increases upon the exposure to VOCs with detection limits ranging from 37 to 167 ppm. A preliminary demo of wearable gas sensing capability is also implemented by wearing the sensor on human hand, which successfully detects several VOCs, instead of normal hand gestures.

Flexible gas sensor based on graphene/ethyl cellulose nanocomposite with ultra-low strain response for volatile organic compounds rapid detection.

PubMed

Zhang, Qiankun; An, Chunhua; Fan, Shuangqing; Shi, Sigang; Zhang, Rongjie; Zhang, Jing; Li, Quanning; Zhang, Daihua; Hu, Xiaodong; Liu, Jing

2018-04-18

Minimizing the strain-induced undesirable effects is one of the major efforts to be made for flexible electronics. This work demonstrates a highly sensitive flexible gas sensor with ultra-low strain response, which is potentially suitable for wearable electronics applications. The gas sensing material is a free-standing and flexible thin film made of graphene/ethyl cellulose (EC) nanocomposite, which is then integrated with flexible substrate of polyethylene terephthalate. The sensor exhibits relative resistance change within 0.3% at a minimum bending radius of 3.18 mm and 0.2% at the bending radius of 5 mm after 400 bending cycles. The limited strain response attributes to several applied strategies, including using EC with high Young's modulus as the matrix material, maintaining high graphene concentration and adopting suspended device structure. In contrast to the almost negligible strain sensitivity, the sensor presents large and rapid responses toward volatile organic compounds (VOCs) at room temperature. Specifically, the sensor resistance rapidly increases upon the exposure to VOCs with detection limits ranging from 37 to 167 ppm. A preliminary demo of wearable gas sensing capability is also implemented by wearing the sensor on human hand, which successfully detects several VOCs, instead of normal hand gestures.

A novel method of fabricating laminated silicone stack actuators with pre-strained dielectric layers

NASA Astrophysics Data System (ADS)

Hinitt, Andrew D.; Conn, Andrew T.

2014-03-01

In recent studies, stack based Dielectric Elastomer Actuators (DEAs) have been successfully used in haptic feedback and sensing applications. However, limitations in the fabrication method, and materials used to con- struct stack actuators constrain their force and displacement output per unit volume. This paper focuses on a fabrication process enabling a stacked elastomer actuator to withstand the high tensile forces needed for high power applications, such as mimetics for mammalian muscle contraction (i.e prostheses), whilst requiring low voltage for thickness-mode contractile actuation. Spun elastomer layers are bonded together in a pre-strained state using a conductive adhesive filler, forming a Laminated Inter-Penetrating Network (L-IPN) with repeatable and uniform electrode thickness. The resulting structure utilises the stored strain energy of the dielectric elas- tomer to compress the cured electrode composite material. The method is used to fabricate an L-IPN example, which demonstrated that the bonded L-IPN has high tensile strength normal to the lamination. Additionally, the uniformity and retained dielectric layer pre-strain of the L-IPN are confirmed. The described method is envisaged to be used in a semi-automated assembly of large-scale multi-layer stacks of pre-strained dielectric layers possessing a tensile strength in the range generated by mammalian muscle.

Strain sensing technology for high temperature applications

NASA Technical Reports Server (NTRS)

Williams, W. Dan

1993-01-01

This review discusses the status of strain sensing technology for high temperature applications. Technologies covered are those supported by NASA such as required for applications in hypersonic vehicles and engines, advanced subsonic engines, as well as material and structure development. The applications may be at temperatures of 540 C (1000 F) to temperatures in excess of 1400 C (2500 F). The most promising technologies at present are the resistance strain gage and remote sensing schemes. Resistance strain gages discussed include the BCL gage, the LaRC compensated gage, and the PdCr gage. Remote sensing schemes such as laser based speckle strain measurement, phase-shifling interferometry, and x-ray extensometry are discussed. Present status and limitations of these technologies are presented.

LS-DYNA Implementation of Polymer Matrix Composite Model Under High Strain Rate Impact

NASA Technical Reports Server (NTRS)

Zheng, Xia-Hua; Goldberg, Robert K.; Binienda, Wieslaw K.; Roberts, Gary D.

2003-01-01

A recently developed constitutive model is implemented into LS-DYNA as a user defined material model (UMAT) to characterize the nonlinear strain rate dependent behavior of polymers. By utilizing this model within a micromechanics technique based on a laminate analogy, an algorithm to analyze the strain rate dependent, nonlinear deformation of a fiber reinforced polymer matrix composite is then developed as a UMAT to simulate the response of these composites under high strain rate impact. The models are designed for shell elements in order to ensure computational efficiency. Experimental and numerical stress-strain curves are compared for two representative polymers and a representative polymer matrix composite, with the analytical model predicting the experimental response reasonably well.

High-resolution high-sensitivity and truly distributed optical frequency domain reflectometry for structural crack detection

NASA Astrophysics Data System (ADS)

Li, Wenhai; Bao, Xiaoyi; Chen, Liang

2014-05-01

Optical Frequency Domain Reflectometry (OFDR) with the use of polarization maintaining fiber (PMF) is capable of distinguishing strain and temperature, which is critical for successful field applications such as structural health monitoring (SHM) and smart material. Location-dependent measurement sensitivities along PMF are compensated by cross- and auto-correlations measurements of the spectra form a distributed parameter matrix. Simultaneous temperature and strain measurement accuracy of 1μstrain and 0.1°C is achieved with 2.5mm spatial resolution in over 180m range.

Synthesis and Crystal Structure of Highly Strained [4]Cyclofluorene: Green-Emitting Fluorophore.

PubMed

Liu, Yu-Yu; Lin, Jin-Yi; Bo, Yi-Fan; Xie, Ling-Hai; Yi, Ming-Dong; Zhang, Xin-Wen; Zhang, Hong-Mei; Loh, Teck-Peng; Huang, Wei

2016-01-15

[4]Cyclo-9,9-dipropyl-2,7-fluorene ([4]CF) with the strain energy of 79.8 kcal/mol is synthesized in high quantum yield. Impressively, hoop-shaped [4]CF exhibits a green fluorescence emission around 512 nm offering a new explanation for the green band (g-band) in polyfluorenes. The solution-processed [4]CF-based organic light emitting diode (OLED) has also been fabricated with the a stronger green band emission. Strained semiconductors offer a promising approach to fabricating multifunctional optoelectronic materials in organic electronics and biomedicine.

A high temperature fatigue life prediction computer code based on the total strain version of StrainRange Partitioning (SRP)

NASA Technical Reports Server (NTRS)

Mcgaw, Michael A.; Saltsman, James F.

1993-01-01

A recently developed high-temperature fatigue life prediction computer code is presented and an example of its usage given. The code discussed is based on the Total Strain version of Strainrange Partitioning (TS-SRP). Included in this code are procedures for characterizing the creep-fatigue durability behavior of an alloy according to TS-SRP guidelines and predicting cyclic life for complex cycle types for both isothermal and thermomechanical conditions. A reasonably extensive materials properties database is included with the code.

Experiments on the rheology of vesicle-bearing magmas

NASA Astrophysics Data System (ADS)

Vona, Alessandro; Ryan, Amy G.; Russell, James K.; Romano, Claudia

2016-04-01

We present a series of high temperature uniaxial deformation experiments designed to investigate the effect of bubbles on the magma bulk viscosity. Starting materials having variable vesicularity (φ = 0 - 66%) were synthesized by high-temperature foaming (T = 900 - 1050 ° C and P = 1 bar) of cores of natural rhyolitic obsidian from Hrafntinnuhryggur, Krafla, Iceland. These cores were subsequently deformed using a high-temperature uniaxial press at dry atmospheric conditions. Each experiment involved deforming vesicle-bearing cores isothermally (T = 750 ° C), at constant displacement rates (strain rates between 0.5-1 x 10-4 s-1), and to total strains (ɛ) of 10-40%. The viscosity of the bubble-free melt (η0) was measured by micropenetration and parallel plate methods and establishes a baseline for comparing data derived from experiments on vesicle rich cores. At the experimental conditions, the presence of vesicles has a major impact on the rheological response, producing a marked decrease of bulk viscosity (maximum decrease of 2 log units Pa s) that is best described by a two-parameter empirical equation: log ηBulk = log η0 - 1.47 * [φ/(1-φ)]0.48. Our model provides a means to compare the diverse behaviour of vesicle-bearing melts reported in the literature and reflecting material properties (e.g., analogue vs. natural), geometry and distribution of pores (e.g. foamed/natural vs. unconsolidated/sintered materials), and flow regime. Lastly, we apply principles of Maxwell relaxation theory, combined with our parameterization of bubble-melt rheology, to map the potential onset of non-Newtonian behaviour (strain localization) in vesiculated magmas and lavas as a function of melt viscosity, vesicularity, strain rate, and geological condition. Increasing vesicularity in magmas can initiate non-Newtonian behaviour at constant strain rates. Lower melt viscosity sustains homogeneous Newtonian flow in vesiculated magmas even at relatively high strain rates.

Determining the tensile response of materials at high temperature using DIC and the Virtual Fields Method

NASA Astrophysics Data System (ADS)

Valeri, Guillermo; Koohbor, Behrad; Kidane, Addis; Sutton, Michael A.

2017-04-01

An experimental approach based on Digital Image Correlation (DIC) is successfully applied to predict the uniaxial stress-strain response of 304 stainless steel specimens subjected to nominally uniform temperatures ranging from room temperature to 900 °C. A portable induction heating device equipped with custom made water-cooled copper coils is used to heat the specimen. The induction heater is used in conjunction with a conventional tensile frame to enable high temperature tension experiments. A stereovision camera system equipped with appropriate band pass filters is employed to facilitate the study of full-field deformation response of the material at elevated temperatures. Using the temperature and load histories along with the full-field strain data, a Virtual Fields Method (VFM) based approach is implemented to identify constitutive parameters governing the plastic deformation of the material at high temperature conditions. Results from these experiments confirm that the proposed method can be used to measure the full field deformation of materials subjected to thermo-mechanical loading.

Finite element analysis of the high strain rate testing of polymeric materials

NASA Astrophysics Data System (ADS)

Gorwade, C. V.; Alghamdi, A. S.; Ashcroft, I. A.; Silberschmidt, V. V.; Song, M.

2012-08-01

Advanced polymer materials are finding an increasing range of industrial and defence applications. Ultra-high molecular weight polymers (UHMWPE) are already used in lightweight body armour because of their good impact resistance with light weight. However, a broader use of such materials is limited by the complexity of the manufacturing processes and the lack of experimental data on their behaviour and failure evolution under high-strain rate loading conditions. The current study deals with an investigation of the internal heat generation during tensile of UHMWPE. A 3D finite element (FE) model of the tensile test is developed and validated the with experimental work. An elastic-plastic material model is used with adiabatic heat generation. The temperature and stresses obtained with FE analysis are found to be in a good agreement with the experimental results. The model can be used as a simple and cost effective tool to predict the thermo-mechanical behaviour of UHMWPE part under various loading conditions.

High Vacuum Creep Facility in the Materials Processing Laboratory

NASA Image and Video Library

1973-01-21

Technicians at work in the Materials Processing Laboratory’s Creep Facility at the National Aeronautics and Space Administration (NASA) Lewis Research Center. The technicians supported the engineers’ studies of refractory materials, metals, and advanced superalloys. The Materials Processing Laboratory contained laboratories and test areas equipped to prepare and develop these metals and materials. The ultra-high vacuum lab, seen in this photograph, contained creep and tensile test equipment. Creep testing is used to study a material’s ability to withstand long durations under constant pressure and temperatures. The equipment measured the strain over a long period of time. Tensile test equipment subjects the test material to strain until the material fails. The two tests were used to determine the strength and durability of different materials. The Materials Processing Laboratory also housed arc and electron beam melting furnaces, a hydraulic vertical extrusion press, compaction and forging equipment, and rolling mills and swagers. There were cryogenic and gas storage facilities and mechanical and oil diffusion vacuum pumps. The facility contained both instrumental and analytical chemistry laboratories for work on radioactive or toxic materials and the only shop to machine toxic materials in the Midwest.

Giant strain with ultra-low hysteresis and high temperature stability in grain oriented lead-free K0.5Bi0.5TiO3-BaTiO3-Na0.5Bi0.5TiO3 piezoelectric materials

PubMed Central

Maurya, Deepam; Zhou, Yuan; Wang, Yaojin; Yan, Yongke; Li, Jiefang; Viehland, Dwight; Priya, Shashank

2015-01-01

We synthesized grain-oriented lead-free piezoelectric materials in (K0.5Bi0.5TiO3-BaTiO3-xNa0.5Bi0.5TiO3 (KBT-BT-NBT) system with high degree of texturing along the [001]c (c-cubic) crystallographic orientation. We demonstrate giant field induced strain (~0.48%) with an ultra-low hysteresis along with enhanced piezoelectric response (d33 ~ 190pC/N) and high temperature stability (~160°C). Transmission electron microscopy (TEM) and piezoresponse force microscopy (PFM) results demonstrate smaller size highly ordered domain structure in grain-oriented specimen relative to the conventional polycrystalline ceramics. The grain oriented specimens exhibited a high degree of non-180° domain switching, in comparison to the randomly axed ones. These results indicate the effective solution to the lead-free piezoelectric materials. PMID:25716551

Giant strain with ultra-low hysteresis and high temperature stability in grain oriented lead-free K₀̣₅Bi₀̣₅TiO₃-BaTiO₃-Na₀̣₅Bi₀̣₅TiO₃ piezoelectric materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Maurya, Deepam; Zhou, Yuan; Wang, Yaojin

2015-02-26

We synthesized grain-oriented lead-free piezoelectric materials in (K₀̣₅Bi₀̣₅TiO₃-BaTiO₃-xNa₀̣₅Bi₀̣₅TiO₃ (KBT-BT-NBT) system with high degree of texturing along the [001]c (c-cubic) crystallographic orientation. We demonstrate giant field induced strain (~0.48%) with an ultra-low hysteresis along with enhanced piezoelectric response (d₃₃ ~ 190pC/N) and high temperature stability (~160°C). Transmission electron microscopy (TEM) and piezoresponse force microscopy (PFM) results demonstrate smaller size highly ordered domain structure in grain-oriented specimen relative to the conventional polycrystalline ceramics. The grain oriented specimens exhibited a high degree of non-180° domain switching, in comparison to the randomly axed ones. These results indicate the effective solution to the lead-free piezoelectricmore » materials.« less

Certification Issues Relating to ABDR

DTIC Science & Technology

2010-05-01

design techniques, among them increased utilization of advanced fibre reinforced materials or advanced metal alloys with higher material allowables for...most cases as a combination of a high strength/modulus carbon fibre and a hot curing thermoset resin. A high percentage of modern fighter aircraft’s...34Limited Fibre Strain Approach" at ultimate design loadcases, where the reduced material allowables account for a low energy impact damage level

The inhomogeneous microstructure and deformation of similar and dissimilar Al-Zn containing Mg friction stir welds

NASA Astrophysics Data System (ADS)

Hiscocks, Jessica

The magnesium-based aluminum-zinc alloys have excellent stiffness to weight ratios, and may be combined by friction stir welding to expand the possible applications. The high aluminum alloy AZ80 in particular has the advantage of being relatively stiff but still extrudable. However limited friction stir welding research is available for this alloy and extrapolation from the extensive work in aluminum alloys is impractical due differences in precipitation behaviour, and magnesium's high plastic anisotropy and tendency to form strong textures during friction stir welding. This work investigates the correlations between local friction stir welded microstructures, textures, residual strains, and the local deformation behaviour based on strain mapping during tensile tests. Covering bead-on-plate and butt configurations, joining of similar and dissimilar materials, and a range of processing conditions, many findings of interest for deformation modelling and industrial applications are presented. Synchrotron x-ray diffraction study of an entire friction stir weld was used to determine texture, residual strain and dislocation density data from a single experiment. A number of unique findings were made, mainly related to the asymmetric distribution of properties both between sides of the weld and through the depth. Particularly in the case of strain measurements, features not detectable at coarser measurement spacing or by line scan are presented and compared for multiple processing conditions. Investigation of the longitudinal material flow during welding showed that even when periodicity in grain size, precipitate distribution, or texture was not observed, periodic changes in texture intensity resulting from compaction of material behind the tool were present, providing evidence that movement of nugget material remained periodic. Strain localisation and fracture behaviour were found to be completely different between good quality similar and dissimilar friction stir welds. For similar magnesium friction stir welds, higher heat input was shown to improve mechanical performance by reducing the residual strain, while for dissimilar friction stir welds, deformation behaviour was found to be more sensitive to the final material distribution in the friction stir weld nugget. For dissimilar welds, even minor changes to the material flow were shown to have a major impact on the tensile performance.

An Objective Approach for Burkholderia pseudomallei Strain Selection as Challenge Material for Medical Countermeasures Efficacy Testing

PubMed Central

Van Zandt, Kristopher E.; Tuanyok, Apichai; Keim, Paul S.; Warren, Richard L.; Gelhaus, H. Carl

2012-01-01

Burkholderia pseudomallei is the causative agent of melioidosis, a rare disease of biodefense concern with high mortality and extreme difficulty in treatment. No human vaccines are available that protect against B. pseudomallei infection, and with the current limitations of antibiotic treatment, the development of new preventative and therapeutic interventions is crucial. Although clinical trials could be used to test the efficacy of new medical countermeasures (MCMs), the high mortality rates associated with melioidosis raises significant ethical issues concerning treating individuals with new compounds with unknown efficacies. The US Food and Drug Administration (FDA) has formulated a set of guidelines for the licensure of new MCMs to treat diseases in which it would be unethical to test the efficacy of these drugs in humans. The FDA “Animal Rule” 21 CFR 314 calls for consistent, well-characterized B. pseudomallei strains to be used as challenge material in animal models. In order to facilitate the efficacy testing of new MCMs for melioidosis using animal models, we intend to develop a well-characterized panel of strains for use. This panel will comprise of strains that were isolated from human cases, have a low passage history, are virulent in animal models, and are well-characterized phenotypically and genotypically. We have reviewed published and unpublished data on various B. pseudomallei strains to establish an objective method for selecting the strains to be included in the panel of B. pseudomallei strains with attention to five categories: animal infection models, genetic characterization, clinical and passage history, and availability of the strain to the research community. We identified 109 strains with data in at least one of the five categories, scored each strain based on the gathered data and identified six strains as candidate for a B. pseudomallei strain panel. PMID:23057010

An objective approach for Burkholderia pseudomallei strain selection as challenge material for medical countermeasures efficacy testing.

PubMed

Van Zandt, Kristopher E; Tuanyok, Apichai; Keim, Paul S; Warren, Richard L; Gelhaus, H Carl

2012-01-01

Burkholderia pseudomallei is the causative agent of melioidosis, a rare disease of biodefense concern with high mortality and extreme difficulty in treatment. No human vaccines are available that protect against B. pseudomallei infection, and with the current limitations of antibiotic treatment, the development of new preventative and therapeutic interventions is crucial. Although clinical trials could be used to test the efficacy of new medical countermeasures (MCMs), the high mortality rates associated with melioidosis raises significant ethical issues concerning treating individuals with new compounds with unknown efficacies. The US Food and Drug Administration (FDA) has formulated a set of guidelines for the licensure of new MCMs to treat diseases in which it would be unethical to test the efficacy of these drugs in humans. The FDA "Animal Rule" 21 CFR 314 calls for consistent, well-characterized B. pseudomallei strains to be used as challenge material in animal models. In order to facilitate the efficacy testing of new MCMs for melioidosis using animal models, we intend to develop a well-characterized panel of strains for use. This panel will comprise of strains that were isolated from human cases, have a low passage history, are virulent in animal models, and are well-characterized phenotypically and genotypically. We have reviewed published and unpublished data on various B. pseudomallei strains to establish an objective method for selecting the strains to be included in the panel of B. pseudomallei strains with attention to five categories: animal infection models, genetic characterization, clinical and passage history, and availability of the strain to the research community. We identified 109 strains with data in at least one of the five categories, scored each strain based on the gathered data and identified six strains as candidate for a B. pseudomallei strain panel.

Large strain cruciform biaxial testing for FLC detection

NASA Astrophysics Data System (ADS)

Güler, Baran; Efe, Mert

2017-10-01

Selection of proper test method, specimen design and analysis method are key issues for studying formability of sheet metals and detection of their forming limit curves (FLC). Materials with complex microstructures may need an additional micro-mechanical investigation and accurate modelling. Cruciform biaxial test stands as an alternative to standard tests as it achieves frictionless, in-plane, multi-axial stress states with a single sample geometry. In this study, we introduce a small-scale (less than 10 cm) cruciform sample allowing micro-mechanical investigation at stress states ranging from plane strain to equibiaxial. With successful specimen design and surface finish, large forming limit strains are obtained at the test region of the sample. The large forming limit strains obtained by experiments are compared to the values obtained from Marciniak-Kuczynski (M-K) local necking model and Cockroft-Latham damage model. This comparison shows that the experimental limiting strains are beyond the theoretical values, approaching to the fracture strain of the two test materials: Al-6061-T6 aluminum alloy and DC-04 high formability steel.

Carbon nanotube-embedded advanced aerospace composites for early-stage damage sensing

NASA Astrophysics Data System (ADS)

Nataraj, Latha; Coatney, Michael; Cain, Jason; Hall, Asha

2018-03-01

Fiber reinforced polymer (FRP) composites featuring outstanding fatigue performance, high specific stiffness and strength, and low density have evolved as critical structural materials in aerospace applications. Microscale damage such as fiber breakage, matrix cracking, and delamination could occur in layered composites compromising structural integrity, emphasizing the critical need to monitor structural health. Early damage detection would lead to enhanced reliability, lifetime, and performance while minimizing maintenance time, leading to enormous scientific and technical interest in realizing physically stable, quick responding, and cost effective strain sensing materials, devices, and techniques with high sensitivity over a broad range of the practical strain spectrum. Today's most commonly used strain sensing techniques are metal foil strain gauges and optical fiber sensors. Metal foil gauges offer high stability and cost-effectiveness but can only be surface-mounted and have a low gauge factor. Optical fibers require expensive instrumentation, are mostly insensitive to cracks parallel to the fiber orientation and may lead to crack initiation as the diameter is larger than that of the reinforcement fibers. Carbon nanotubes (CNTs) have attracted much attention due to high aspect ratio and superior electrical, thermal, and mechanical properties. CNTs embedded in layered composites have improved performance. A variety of CNT architectures and configurations have shown improved piezoresistive behavior and stability for sensing applications. However, scaling up and commercialization remain serious challenges. The current study investigates a simple, cost effective and repeatable technique for highly sensitive, stable, linear and repeatable strain sensing for damage detection by integrating CNT laminates into composites.

High-resolution spatiotemporal strain mapping reveals non-uniform deformation in micropatterned elastomers

NASA Astrophysics Data System (ADS)

Aksoy, B.; Rehman, A.; Bayraktar, H.; Alaca, B. E.

2017-04-01

Micropatterns are generated on a vast selection of polymeric substrates for various applications ranging from stretchable electronics to cellular mechanobiological systems. When these patterned substrates are exposed to external loading, strain field is primarily affected by the presence of microfabricated structures and similarly by fabrication-related defects. The capturing of such nonhomogeneous strain fields is of utmost importance in cases where study of the mechanical behavior with a high spatial resolution is necessary. Image-based non-contact strain measurement techniques are favorable and have recently been extended to scanning tunneling microscope and scanning electron microscope images for the characterization of mechanical properties of metallic materials, e.g. steel and aluminum, at the microscale. A similar real-time analysis of strain heterogeneity in elastomers is yet to be achieved during the entire loading sequence. The available measurement methods for polymeric materials mostly depend on cross-head displacement or precalibrated strain values. Thus, they suffer either from the lack of any real-time analysis, spatiotemporal distribution or high resolution in addition to a combination of these factors. In this work, these challenges are addressed by integrating a tensile stretcher with an inverted optical microscope and developing a subpixel particle tracking algorithm. As a proof of concept, the patterns with a critical dimension of 200 µm are generated on polydimethylsiloxane substrates and strain distribution in the vicinity of the patterns is captured with a high spatiotemporal resolution. In the field of strain measurement, there is always a tradeoff between minimum measurable strain value and spatial resolution. Current noncontact techniques on elastomers can deliver a strain resolution of 0.001% over a minimum length of 5 cm. More importantly, inhomogeneities within this quite large region cannot be captured. The proposed technique can overcome this challenge and provides a displacement measurement resolution of 116 nm and a strain resolution of 0.04% over a gage length of 300 µm. Similarly, the ability to capture inhomogeneities is demonstrated by mapping strain around a thru-hole. The robustness of the technique is also evaluated, where no appreciable change in strain measurement is observed despite the significant variations imposed on the measurement mesh. The proposed approach introduces critical improvements for the determination of displacement and strain gradients in elastomers regarding the real-time nature of strain mapping with a microscale spatial resolution.

A methodology to determine the elastic moduli of crystals by matching experimental and simulated lattice strain pole figures using discrete harmonics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wielewski, Euan; Boyce, Donald E.; Park, Jun-Sang

Determining reliable single crystal material parameters for complex polycrystalline materials is a significant challenge for the materials community. In this work, a novel methodology for determining those parameters is outlined and successfully applied to the titanium alloy, Ti-6Al-4V. Utilizing the results from a lattice strain pole figure experiment conducted at the Cornell High Energy Synchrotron Source, an iterative approach is used to optimize the single crystal elastic moduli by comparing experimental and simulated lattice strain pole figures at discrete load steps during a uniaxial tensile test. Due to the large number of unique measurements taken during the experiments, comparisons weremore » made by using the discrete spherical harmonic modes of both the experimental and simulated lattice strain pole figures, allowing the complete pole figures to be used to determine the single crystal elastic moduli. (C) 2016 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.« less

Polymer-coated FBG sensor for simultaneous temperature and strain monitoring in composite materials under cryogenic conditions.

PubMed

Sampath, Umesh; Kim, Daegil; Kim, Hyunjin; Song, Minho

2018-01-20

A polymer-coated fiber Bragg grating (PCFBG) is examined for real-time temperature and strain monitoring in composite materials at cryogenic temperatures. The proposed sensor enables the simultaneous measurement of temperature and strain at extremely low temperatures by tracking the changes in the reflected center wavelengths from a pair of PCFBGs embedded in a composite material. The cryogenic temperature sensing was realized by introducing polymer coatings onto bare FBGs, which resulted in high temperature sensitivity under cryogenic conditions. A comparison of wavelength responses of the Bragg grating with and without a polymer coating toward temperatures ranging from 25°C to -180°C was performed. The polymer-coated FBG exhibited a sensitivity of 48 pm/°C, which is 10 times greater than that of the bare FBGs. In addition, the encapsulation of the FBG in a capillary tube made it possible to evaluate the strain accumulated within the composite during operation under cryogenic conditions.

Shrinkage of Dental Composite in Simulated Cavity Measured with Digital Image Correlation

PubMed Central

Li, Jianying; Thakur, Preetanjali; Fok, Alex S. L.

2014-01-01

Polymerization shrinkage of dental resin composites can lead to restoration debonding or cracked tooth tissues in composite-restored teeth. In order to understand where and how shrinkage strain and stress develop in such restored teeth, Digital Image Correlation (DIC) was used to provide a comprehensive view of the displacement and strain distributions within model restorations that had undergone polymerization shrinkage. Specimens with model cavities were made of cylindrical glass rods with both diameter and length being 10 mm. The dimensions of the mesial-occlusal-distal (MOD) cavity prepared in each specimen measured 3 mm and 2 mm in width and depth, respectively. After filling the cavity with resin composite, the surface under observation was sprayed with first a thin layer of white paint and then fine black charcoal powder to create high-contrast speckles. Pictures of that surface were then taken before curing and 5 min after. Finally, the two pictures were correlated using DIC software to calculate the displacement and strain distributions. The resin composite shrunk vertically towards the bottom of the cavity, with the top center portion of the restoration having the largest downward displacement. At the same time, it shrunk horizontally towards its vertical midline. Shrinkage of the composite stretched the material in the vicinity of the “tooth-restoration” interface, resulting in cuspal deflections and high tensile strains around the restoration. Material close to the cavity walls or floor had direct strains mostly in the directions perpendicular to the interfaces. Summation of the two direct strain components showed a relatively uniform distribution around the restoration and its magnitude equaled approximately to the volumetric shrinkage strain of the material. PMID:25079865

Shock structures at ultrahigh strain rates: what can they tell us about material behavior on very fast time scales?

NASA Astrophysics Data System (ADS)

Crowhurst, Jonathan

2013-06-01

In recent years, techniques based on table-top laser systems have shown promise for investigating dynamic material behavior at high rates of both compressive and tensile strain. Common to these techniques is a laser pulse that is used in some manner to rapidly deliver energy to the sample; while the energy itself is often comparatively very small, the intensity can be made high by tightly focusing the pump light. In this way pressures or stresses can be obtained that are sufficiently large to have relevance to a wide range of basic and applied fields. Also, when combined with established ultrafast diagnostics these experiments provide very high time resolution which is particularly desirable when studying, for example shock waves, in which the time for the material to pass from undisturbed to fully compressed (the ``rise time'') can be extremely short (order 10 ps or less) even at fairly small peak stresses. Since much of the most interesting physics comes into play during this process it is important to be able to adequately resolve the shock rise. In this context I will discuss our measurements on aluminum and iron thin films and compare the results with known behavior observed at lower strain rates. Specifically, for aluminum, I will compare our assumed steady wave data at strain rates of up to 1010 s-1 to literature data up to ~107 s-1 and show that the well-known fourth power scaling relation of strain rate to shock stress is maintained even at these very high strain rates. For iron, I will show how we have used our nonsteady data (up to ~109 s-1) to infer a number of important properties of the alpha to epsilon polymorphic transition: 1. The transition can occur on the tens of ps time scale at sufficiently high strain rates and corresponding very large deviatoric stresses, and 2, most of the material appears to transform at a substantially higher stress than the nominal value usually inferred from shock wave experiments of about 13 GPa. This work was performed under the auspices of the U.S. Department of Energy by Lawrence Livermore National Laboratory under Contract No. DE-AC52-07NA27344 with Laboratory directed Research and Development funding (12ERD042), as well as being based on work supported as part of the EFree, an Energy Frontier Research Center funded by the U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences under Award No. DESC0001057.

Evaluation of industrial Saccharomyces cerevisiae strains as the chassis cell for second-generation bioethanol production

PubMed Central

Li, Hongxing; Wu, Meiling; Xu, Lili; Hou, Jin; Guo, Ting; Bao, Xiaoming; Shen, Yu

2015-01-01

To develop a suitable Saccharomyces cerevisiae industrial strain as a chassis cell for ethanol production using lignocellulosic materials, 32 wild-type strains were evaluated for their glucose fermenting ability, their tolerance to the stresses they might encounter in lignocellulosic hydrolysate fermentation and their genetic background for pentose metabolism. The strain BSIF, isolated from tropical fruit in Thailand, was selected out of the distinctly different strains studied for its promising characteristics. The maximal specific growth rate of BSIF was as high as 0.65 h−1 in yeast extract peptone dextrose medium, and the ethanol yield was 0.45 g g−1 consumed glucose. Furthermore, compared with other strains, this strain exhibited superior tolerance to high temperature, hyperosmotic stress and oxidative stress; better growth performance in lignocellulosic hydrolysate; and better xylose utilization capacity when an initial xylose metabolic pathway was introduced. All of these results indicate that this strain is an excellent chassis strain for lignocellulosic ethanol production. PMID:25616171

Development of a Hopkinson Bar Apparatus for Testing Soft Materials: Application to a Closed-Cell Aluminum Foam.

PubMed

Peroni, Marco; Solomos, George; Babcsan, Norbert

2016-01-05

An increasing interest in lightweight metallic foams for automotive, aerospace, and other applications has been observed in recent years. This is mainly due to the weight reduction that can be achieved using foams and for their mechanical energy absorption and acoustic damping capabilities. An accurate knowledge of the mechanical behavior of these materials, especially under dynamic loadings, is thus necessary. Unfortunately, metal foams and in general "soft" materials exhibit a series of peculiarities that make difficult the adoption of standard testing techniques for their high strain-rate characterization. This paper presents an innovative apparatus, where high strain-rate tests of metal foams or other soft materials can be performed by exploiting the operating principle of the Hopkinson bar methods. Using the pre-stress method to generate directly a long compression pulse (compared with traditional SHPB), a displacement of about 20 mm can be applied to the specimen with a single propagating wave, suitable for evaluating the whole stress-strain curve of medium-sized cell foams (pores of about 1-2 mm). The potential of this testing rig is shown in the characterization of a closed-cell aluminum foam, where all the above features are amply demonstrated.

Mechanical behavior of precipitation hardenable steels exposed to highly corrosive environment

NASA Technical Reports Server (NTRS)

Rosa, Ferdinand

1994-01-01

Unexpected occurrences of failures, due to stress corrosion cracking (SCC) of structural components, indicate a need for improved characterization of materials and more advanced analytical procedures for reliably predicting structures performance. Accordingly, the purpose of this study was to determine the stress corrosion susceptibility of 15 - 5 PH steel over a wide range of applied strain rates in a highly corrosive environment. The selected environment for this investigation was a 3.5 percent NaCl aqueous solution. The material selected for the study was 15 - 5 PH steel in the H 900 condition. The Slow Strain Rate technique was used to test the metallic specimens.

Advanced Strain-Isolation-Pad Material with Bonded Fibrous Construction

NASA Technical Reports Server (NTRS)

Seibold, R. W.; Saito, C. A.; Buller, B. W.

1982-01-01

The feasibility of utilizing air lay and liquid lay felt deposition techniques to fabricate strain isolation pad (SIP) materials for the Space Shuttle Orbiter was demonstrated. These materials were developed as candidate replacements for the present needled felt SIP used between the ceramic tiles and the aluminum skin on the undersurface of the Orbiter. The SIP materials that were developed consisted of high temperature aramid fibers deposited by controlled fluid (air or liquid) carriers to form low density unbonded felts. The deposited felts were then bonded at the fiber intersections with a small amount of high temperature polyimide resin. This type of bonded felt construction can potentially eliminate two of the problems associated with the present SIP, viz., transmittal of localized stresses into the tiles and load history dependent mechanical response. However, further work is needed to achieve adequate through thickness tensile strength in the bonded felts.

The effect of yield strength and ductility to fatigue damage

NASA Technical Reports Server (NTRS)

Yeh, H. Y.

1973-01-01

The cumulative damage of aluminium alloys with different yield strength and various ductility due to seismic loads was studied. The responses of an idealized beam with a centered mass at one end and fixed at the other end to El Centro's and Taft's earthquakes are computed by assuming that the alloys are perfectly elastoplastic materials and by using numerical technique. Consequently, the corresponding residual plastic strain can be obtained from the stress-strain relationship. The revised Palmgren-Miner cumulative damage theorem is utilized to calculate the fatigue damage. The numerical results show that in certain cases, the high ductility materials are more resistant to seismic loads than the high yield strength materials. The results also show that if a structure collapse during the earthquake, the collapse always occurs in the very early stage.

Microstructured Optical Fiber Sensors Embedded in a Laminate Composite for Smart Material Applications

PubMed Central

Sonnenfeld, Camille; Sulejmani, Sanne; Geernaert, Thomas; Eve, Sophie; Lammens, Nicolas; Luyckx, Geert; Voet, Eli; Degrieck, Joris; Urbanczyk, Waclaw; Mergo, Pawel; Becker, Martin; Bartelt, Hartmut; Berghmans, Francis; Thienpont, Hugo

2011-01-01

Fiber Bragg gratings written in highly birefringent microstructured optical fiber with a dedicated design are embedded in a composite fiber-reinforced polymer. The Bragg peak wavelength shifts are measured under controlled axial and transversal strain and during thermal cycling of the composite sample. We obtain a sensitivity to transversal strain that exceeds values reported earlier in literature by one order of magnitude. Our results evidence the relevance of using microstructured optical fibers for structural integrity monitoring of composite material structures. PMID:22163755

Development of tube-packaged FBG strain sensor and application in the vibration experiment of submarine pipeline model

NASA Astrophysics Data System (ADS)

Ren, Liang; Li, Hong-Nan; Sun, Li; Li, Dong-Sheng

2005-05-01

Optical fiber sensors have received increasing attention in the fields of aeronautic and civil engineering for their superior ability of explosion proof, immunity to electromagnetic interference and high accuracy, especially fitting for measurement applications in harsh environment. In this paper, a novel FBG (fiber Bragg grating) strain sensor, which was packaged in a 1.2mm stainless steel tube by epoxy resin, was developed. Experiments were conducted on the universal material testing machine to calibrate its strain transferring characteristics. The sensor has the advantages of small size, high precision and flexible use, and demonstrates promising potentials. Ten of tube-packaged strain FBG sensors were applied in the vibration experiment of submarine pipeline model. The strain measured by FBG sensor agrees well with the electric resistance strain sensor.

Development of tube-packaged FBG strain sensor and application in the vibration experiment of submarine pipeline model

NASA Astrophysics Data System (ADS)

Ren, Liang; Li, Hong-Nan; Sun, Li; Li, Dong-Sheng

2005-02-01

Optical fiber sensors have received increasing attention in the fields of aeronautic and civil engineering for their superior ability of explosion proof, immunity to electromagnetic interference and high accuracy, especially fitting for measurement applications in harsh environment. In this paper, a novel FBG (fiber Bragg grating) strain sensor, which was packaged in a 1.2mm stainless steel tube by epoxy resin, was developed. Experiments were conducted on the universal material testing machine to calibrate its strain transferring characteristics. The sensor has the advantages of small size, high precision and flexible use, and demonstrates promising potentials. Ten of tube-packaged strain FBG sensors were applied in the vibration experiment of submarine pipeline model. The strain measured by FBG sensor agrees well with the electric resistance strain sensor.

High strain rate characterization of soft materials: past, present and possible futures

NASA Astrophysics Data System (ADS)

Siviour, Clive

2015-06-01

The high strain rate properties of low impedance materials have long been of interest to the community: the very first paper by Kolsky on his eponymous bars included data from man-made polymers and natural rubber. However, it has also long been recognized that characterizing soft or low impedance specimens under dynamic loading presents a number of challenges, mainly owing to the low sound speed in, and low stresses supported by, these materials. Over the past 20 years, significant progress has been made in high rate testing techniques, including better experimental design, more sensitive data acquisition and better understanding of specimen behavior. Further, a new generation of techniques, in which materials are characterized using travelling waves, rather than in a state of static equilibrium, promise to turn those properties that were previously a drawback into an advantage. This paper will give an overview of the history of high rate characterization, the current state of the art after an exciting couple of decades and some of the techniques currently being developed that have the potential to offer increased quality data in the future.

Impact tensile properties and strength development mechanism of glass for reinforcement fiber

NASA Astrophysics Data System (ADS)

Kim, T.; Oshima, K.; Kawada, H.

2013-07-01

In this study, impact tensile properties of E-glass were investigated by fiber bundle testing under a high strain rate. The impact tests were performed employing two types of experiments. One is the tension-type split Hopkinson pressure bar system, and the other is the universal high-speed tensile-testing machine. As the results, it was found that not only the tensile strength but also the fracture strain of E-glass fiber improved with the strain rate. The absorbed strain energy of this material significantly increased. It was also found that the degree of the strain rate dependency of E-glass fibers on the tensile strength was varied according to fiber diameter. As for the strain rate dependency of the glass fiber under tensile loading condition, change of the small crack-propagation behaviour was considered to clarify the development of the fiber strength. The tensile fiber strength was estimated by employing the numerical simulation based on the slow crack-growth model (SCG). Through the parametric study against the coefficient of the crack propagation rate, the numerical estimation value was obtained for the various testing conditions. It was concluded that the slow crack-growth behaviour in the glass fiber was an essential for the increase in the strength of this material.

Poisson's ratio of collagen fibrils measured by small angle X-ray scattering of strained bovine pericardium

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wells, Hannah C.; Sizeland, Katie H.; Kayed, Hanan R.

Type I collagen is the main structural component of skin, tendons, and skin products, such as leather. Understanding the mechanical performance of collagen fibrils is important for understanding the mechanical performance of the tissues that they make up, while the mechanical properties of bulk tissue are well characterized, less is known about the mechanical behavior of individual collagen fibrils. In this study, bovine pericardium is subjected to strain while small angle X-ray scattering (SAXS) patterns are recorded using synchrotron radiation. The change in d-spacing, which is a measure of fibril extension, and the change in fibril diameter are determined frommore » SAXS. The tissue is strained 0.25 (25%) with a corresponding strain in the collagen fibrils of 0.045 observed. The ratio of collagen fibril width contraction to length extension, or the Poisson's ratio, is 2.1 ± 0.7 for a tissue strain from 0 to 0.25. This Poisson's ratio indicates that the volume of individual collagen fibrils decreases with increasing strain, which is quite unlike most engineering materials. This high Poisson's ratio of individual fibrils may contribute to high Poisson's ratio observed for tissues, contributing to some of the remarkable properties of collagen-based materials.« less

Macro-architectured cellular materials: Properties, characteristic modes, and prediction methods

NASA Astrophysics Data System (ADS)

Ma, Zheng-Dong

2017-12-01

Macro-architectured cellular (MAC) material is defined as a class of engineered materials having configurable cells of relatively large (i.e., visible) size that can be architecturally designed to achieve various desired material properties. Two types of novel MAC materials, negative Poisson's ratio material and biomimetic tendon reinforced material, were introduced in this study. To estimate the effective material properties for structural analyses and to optimally design such materials, a set of suitable homogenization methods was developed that provided an effective means for the multiscale modeling of MAC materials. First, a strain-based homogenization method was developed using an approach that separated the strain field into a homogenized strain field and a strain variation field in the local cellular domain superposed on the homogenized strain field. The principle of virtual displacements for the relationship between the strain variation field and the homogenized strain field was then used to condense the strain variation field onto the homogenized strain field. The new method was then extended to a stress-based homogenization process based on the principle of virtual forces and further applied to address the discrete systems represented by the beam or frame structures of the aforementioned MAC materials. The characteristic modes and the stress recovery process used to predict the stress distribution inside the cellular domain and thus determine the material strengths and failures at the local level are also discussed.

Design, analysis, and applications of cellular contact-aided compliant mechanisms

NASA Astrophysics Data System (ADS)

Mehta, Vipul

A new class of compliant mechanisms utilizing the benefits of cellular geometry and contact are addressed in this work. The design, analysis, fabrication and testing of such structures for high-strain and high-strength applications is the focus of the present research. Cellular structures have relatively good strength-to-weight ratios. They also have a higher strain capability than solid structures. Contact during deformation reduces failure-causing bending stresses through stress relief, thereby enabling such cellular structures to be stretched more than the corresponding structures without contact. Both analytical and numerical models are developed to represent one specific mechanism. Several candidate materials are investigated for such mechanisms. Although the allowable strain of all these materials is small, the overall strain of the contact-aided cellular mechanisms is at least an order of magnitude greater than that of the constitutive material. Application of contact to different materials yields an improvement in the global strain capacity by more than 100% relative to cellular structures without contact. Experiments are conducted to validate the models, and good agreement is found. Size optimization is carried out to maximize the stress relief and the overall strain. Two main applications are considered in the present work. One application consists of a morphing aircraft skin for adaptive structures. Different material models such as linearly elastic and multi-linear elastic are examined. For linearly elastic materials, contact-induced stress-relief is advantageous and for nonlinear elastic materials, reduction of transverse deflection due to contact is useful. The proposed contact-aided skin structure is compared with a cellular skin without contact. The contact mechanism helps to increase the morphing capacity while decreasing the structural mass. Using contact-aided cellular mechanisms, the global strain capability is increased by as much as 37%. For a fixed global strain, the optimum contact-aided structure is 15% lighter than an optimum non-contact structure. Another application involves investigation of meso-scaled cellular structures. Two different materials are considered---nanoparticulate zirconia and particulate stainless steel. The lost mold rapid infiltration forming process is utilized to fabricate free standing cellular mechanisms. The analytical model is employed to address the tradeoffs between the manufacturing constraints and to design suitable contact-aided cellular mechanisms. A custom rig is developed to test these meso-scaled parts. Force displacement characteristics are experimentally obtained and compared against those found using the analytical model. Topology optimization tools are applied to the design of compliant cellular mechanisms with and without a contact mechanism. A two-step procedure is developed. For cellular structures without contact, an inverse homogenization method is employed. The compliant mechanism is optimized to yield prescribed elasticity coefficients and achieve a large effective elastic strain. To implement a contact mechanism in the second step, the continuum model of a non-contact structure is converted into a frame model. Only the non-overlapping designs are investigated exhaustively for stress relief. A differential evolution optimizer is used to maximize the stress relief. Four cell topologies are found for different effective properties corresponding to different structural requirements. For each such topology, a contact mechanism is devised that demonstrates stress relief. One such topology resulted a stress relief as high as 36%.

Uniaxial Strain Redistribution in Corrugated Graphene: Clamping, Sliding, Friction, and 2D Band Splitting.

PubMed

Wang, Xuanye; Tantiwanichapan, Khwanchai; Christopher, Jason W; Paiella, Roberto; Swan, Anna K

2015-09-09

Graphene is a promising material for strain engineering based on its excellent flexibility and elastic properties, coupled with very high electrical mobility. In order to implement strain devices, it is important to understand and control the clamping of graphene to its support. Here, we investigate the limits of the strong van der Waals interaction on friction clamping. We find that the friction of graphene on a SiO2 substrate can support a maximum local strain gradient and that higher strain gradients result in sliding and strain redistribution. Furthermore, the friction decreases with increasing strain. The system used is graphene placed over a nanoscale SiO2 grating, causing strain and local strain variations. We use a combination of atomic force microscopy and Raman scattering to determine the friction coefficient, after accounting for compression and accidental charge doping, and model the local strain variation within the laser spot size. By using uniaxial strain aligned to a high crystal symmetry direction, we also determine the 2D Raman Grüneisen parameter and deformation potential in the zigzag direction.

Full Piezoelectric Multilayer-Stacked Hybrid Actuation/Transduction Systems

NASA Technical Reports Server (NTRS)

Su, Ji; Jiang, Xiaoning; Zu, Tian-Bing

2011-01-01

The Stacked HYBATS (Hybrid Actuation/Transduction system) demonstrates significantly enhanced electromechanical performance by using the cooperative contributions of the electromechanical responses of multilayer, stacked negative strain components and positive strain components. Both experimental and theoretical studies indicate that, for Stacked HYBATS, the displacement is over three times that of a same-sized conventional flextensional actuator/transducer. The coupled resonance mode between positive strain and negative strain components of Stacked HYBATS is much stronger than the resonance of a single element actuation only when the effective lengths of the two kinds of elements match each other. Compared with the previously invented hybrid actuation system (HYBAS), the multilayer Stacked HYBATS can be designed to provide high mechanical load capability, low voltage driving, and a highly effective piezoelectric constant. The negative strain component will contract, and the positive strain component will expand in the length directions when an electric field is applied on the device. The interaction between the two elements makes an enhanced motion along the Z direction for Stacked-HYBATS. In order to dominate the dynamic length of Stacked-HYBATS by the negative strain component, the area of the cross-section for the negative strain component will be much larger than the total cross-section areas of the two positive strain components. The transverse strain is negative and longitudinal strain positive in inorganic materials, such as ceramics/single crystals. Different piezoelectric multilayer stack configurations can make a piezoelectric ceramic/single-crystal multilayer stack exhibit negative strain or positive strain at a certain direction without increasing the applied voltage. The difference of this innovation from the HYBAS is that all the elements can be made from one-of-a-kind materials. Stacked HYBATS can provide an extremely effective piezoelectric constant at both resonance and off resonance frequencies. The effective piezoelectric constant can be alternated by varying the size of each component, the degree of the pre-curvature of the positive strain components, the thickness of each layer in the multilayer stacks, and the piezoelectric constant of the material used. Because all of the elements are piezoelectric components, Stacked HYBATS can serve as projector and receiver for underwater detection. The performance of this innovation can be enhanced by improving the piezoelectric properties.

Antiferroelectric Materials, Applications and Recent Progress on Multiferroic Heterostructures

NASA Astrophysics Data System (ADS)

Zhou, Ziyao; Yang, Qu; Liu, Ming; Zhang, Zhiguo; Zhang, Xinyang; Sun, Dazhi; Nan, Tianxiang; Sun, Nianxiang; Chen, Xing

2015-04-01

Antiferroelectric (AFE) materials with adjacent dipoles oriented in antiparallel directions have a double polarization hysteresis loops. An electric field (E-field)-induced AFE-ferroelectric (FE) phase transition takes place in such materials, leading to a large lattice strain and energy change. The high dielectric constant and the distinct phase transition in AFE materials provide great opportunities for the realization of energy storage devices like super-capacitors and energy conversion devices such as AFE MEMS applications. Lots of work has been done in this field since 60-70 s. Recently, the strain tuning of the spin, charge and orbital orderings and their interactions in complex oxides and multiferroic heterostructures have received great attention. In these systems, a single control parameter of lattice strain is used to control lattice-spin, lattice-phonon, and lattice-charge interactions and tailor properties or create a transition between distinct magnetic/electronic phases. Due to the large strain/stress arising from the phase transition, AFE materials are great candidates for integrating with ferromagnetic (FM) materials to realize in situ manipulation of magnetism and lattice-ordered parameters by voltage. In this paper, we introduce the AFE material and it's applications shortly and then review the recent progress in AFEs based on multiferroic heterostructures. These new multiferroic materials could pave a new way towards next generation light, compact, fast and energy efficient voltage tunable RF/microwave, spintronic and memory devices promising approaches to in situ manipulation of lattice-coupled order parameters is to grow epitaxial oxide films on FE/ferroelastic substrates.

Development of a strain rate dependent material model of human cortical bone for computer-aided reconstruction of injury mechanisms.

PubMed

Asgharpour, Zahra; Zioupos, Peter; Graw, Matthias; Peldschus, Steffen

2014-03-01

Computer-aided methods such as finite-element simulation offer a great potential in the forensic reconstruction of injury mechanisms. Numerous studies have been performed on understanding and analysing the mechanical properties of bone and the mechanism of its fracture. Determination of the mechanical properties of bones is made on the same basis used for other structural materials. The mechanical behaviour of bones is affected by the mechanical properties of the bone material, the geometry, the loading direction and mode and of course the loading rate. Strain rate dependency of mechanical properties of cortical bone has been well demonstrated in literature studies, but as many of these were performed on animal bones and at non-physiological strain rates it is questionable how these will apply in the human situations. High strain-rates dominate in a lot of forensic applications in automotive crashes and assault scenarios. There is an overwhelming need to a model which can describe the complex behaviour of bone at lower strain rates as well as higher ones. Some attempts have been made to model the viscoelastic and viscoplastic properties of the bone at high strain rates using constitutive mathematical models with little demonstrated success. The main objective of the present study is to model the rate dependent behaviour of the bones based on experimental data. An isotropic material model of human cortical bone with strain rate dependency effects is implemented using the LS-DYNA material library. We employed a human finite element model called THUMS (Total Human Model for Safety), developed by Toyota R&D Labs and the Wayne State University, USA. The finite element model of the human femur is extracted from the THUMS model. Different methods have been employed to develop a strain rate dependent material model for the femur bone. Results of one the recent experimental studies on human femur have been employed to obtain the numerical model for cortical femur. A forensic application of the model is explained in which impacts to the arm have been reconstructed using the finite element model of THUMS. The advantage of the numerical method is that a wide range of impact conditions can be easily reconstructed. Impact velocity has been changed as a parameter to find the tolerance levels of injuries to the lower arm. The method can be further developed to study the assaults and the injury mechanism which can lead to severe traumatic injuries in forensic cases. Copyright © 2013 Elsevier Ireland Ltd. All rights reserved.

Coherent X-Ray Diffraction Imaging and Characterization of Strain in Silicon-on-Insulator Nanostructures

PubMed Central

Xiong, Gang; Moutanabbir, Oussama; Reiche, Manfred; Harder, Ross; Robinson, Ian

2014-01-01

Coherent X-ray diffraction imaging (CDI) has emerged in the last decade as a promising high resolution lens-less imaging approach for the characterization of various samples. It has made significant technical progress through developments in source, algorithm and imaging methodologies thus enabling important scientific breakthroughs in a broad range of disciplines. In this report, we will introduce the principles of forward scattering CDI and Bragg geometry CDI (BCDI), with an emphasis on the latter. BCDI exploits the ultra-high sensitivity of the diffraction pattern to the distortions of crystalline lattice. Its ability of imaging strain on the nanometer scale in three dimensions is highly novel. We will present the latest progress on the application of BCDI in investigating the strain relaxation behavior in nanoscale patterned strained silicon-on-insulator (sSOI) materials, aiming to understand and engineer strain for the design and implementation of new generation semiconductor devices. PMID:24955950

Strain-induced oxygen vacancies in ultrathin epitaxial CaMnO3 films

NASA Astrophysics Data System (ADS)

Chandrasena, Ravini; Yang, Weibing; Lei, Qingyu; Delgado-Jaime, Mario; de Groot, Frank; Arenholz, Elke; Kobayashi, Keisuke; Aschauer, Ulrich; Spaldin, Nicola; Xi, Xiaoxing; Gray, Alexander

Dynamic control of strain-induced ionic defects in transition-metal oxides is considered to be an exciting new avenue towards creating materials with novel electronic, magnetic and structural properties. Here we use atomic layer-by-layer laser molecular beam epitaxy to synthesize high-quality ultrathin single-crystalline CaMnO3 films with systematically varying coherent tensile strain. We then utilize a combination of high-resolution soft x-ray absorption spectroscopy and bulk-sensitive hard x-ray photoemission spectroscopy in conjunction with first-principles theory and core-hole multiplet calculations to establish a direct link between the coherent in-plane strain and the oxygen-vacancy content. We show that the oxygen vacancies are highly mobile, which necessitates an in-situ-grown capping layer in order to preserve the original strain-induced oxygen-vacancy content. Our findings open the door for designing and controlling new ionically active properties in strongly-correlated transition-metal oxides.

Strain analysis of nanowire interfaces in multiscale composites

NASA Astrophysics Data System (ADS)

Malakooti, Mohammad H.; Zhou, Zhi; Spears, John H.; Shankwitz, Timothy J.; Sodano, Henry A.

2016-04-01

Recently, the reinforcement-matrix interface of fiber reinforced polymers has been modified through grafting nanostructures - particularly carbon nanotubes and ZnO nanowires - on to the fiber surface. This type of interface engineering has made a great impact on the development of multiscale composites that have high stiffness, interfacial strength, toughness, and vibrational damping - qualities that are mutually exclusive to a degree in most raw materials. Although the efficacy of such nanostructured interfaces has been established, the reinforcement mechanisms of these multiscale composites have not been explored. Here, strain transfer across a nanowire interphase is studied in order to gain a heightened understanding of the working principles of physical interface modification and the formation of a functional gradient. This problem is studied using a functionally graded piezoelectric interface composed of vertically aligned lead zirconate titanate nanowires, as their piezoelectric properties can be utilized to precisely control the strain on one side of the interface. The displacement and strain across the nanowire interface is captured using digital image correlation. It is demonstrated that the material gradient created through nanowires cause a smooth strain transfer from reinforcement phase into matrix phase that eliminates the stress concentration between these phases, which have highly mismatched elasticity.

Finite Element Modeling of Reheat Stretch Blow Molding of PET

NASA Astrophysics Data System (ADS)

Krishnan, Dwarak; Dupaix, Rebecca B.

2004-06-01

Poly (ethylene terephthalate) or PET is a polymer used as a packaging material for consumer products such as beverages, food or other liquids, and in other applications including drawn fibers and stretched films. Key features that make it widely used are its transparency, dimensional stability, gas impermeability, impact resistance, and high stiffness and strength in certain preferential directions. These commercially useful properties arise from the fact that PET crystallizes upon deformation above the glass transition temperature. Additionally, this strain-induced crystallization causes the deformation behavior of PET to be highly sensitive to processing conditions. It is thus crucial for engineers to be able to predict its performance at various process temperatures, strain rates and strain states so as to optimize the manufacturing process. In addressing these issues; a finite element analysis of the reheat blow molding process with PET has been carried out using ABAQUS. The simulation employed a constitutive model for PET developed by Dupaix and Boyce et al.. The model includes the combined effects of molecular orientation and strain-induced crystallization on strain hardening when the material is deformed above the glass transition temperature. The simulated bottles were also compared with actual blow molded bottles to evaluate the validity of the simulation.

A study of deformation and strain induced in bulk by the oxide layers formation on a Fe-Cr-Al alloy in high-temperature liquid Pb-Bi eutectic

DOE PAGES

Popovic, M. P.; Chen, K.; Shen, H.; ...

2018-03-29

At elevated temperatures, heavy liquid metals and their alloys are known to create a highly corrosive environment that causes irreversible degradation of most iron-based materials. In this paper, it has been found that an appropriate concentration of oxygen in the liquid alloy can significantly reduce this issue by creating a passivating oxide scale that controls diffusion, especially if Al is present in Fe-based materials (by Al-oxide formation). However, the increase of the temperature and of oxygen content in liquid phase leads to the increase of oxygen diffusion into bulk, and to promotion of the internal Al oxidation. This can causemore » a strain in bulk near the oxide layer, due either to mismatch between the thermal expansion coefficients of the oxides and bulk material, or to misfit of the crystal lattices (bulk vs. oxides). This work investigates the strain induced into proximal bulk of a Fe-Cr-Al alloy by oxide layers formation in liquid lead-bismuth eutectic utilizing synchrotron X-ray Laue microdiffraction. Finally, it is found that internal oxidation is the most likely cause for the strain in the metal rather than thermal expansion mismatch as a two-layer problem.« less

A study of deformation and strain induced in bulk by the oxide layers formation on a Fe-Cr-Al alloy in high-temperature liquid Pb-Bi eutectic

DOE Office of Scientific and Technical Information (OSTI.GOV)

Popovic, M. P.; Chen, K.; Shen, H.

At elevated temperatures, heavy liquid metals and their alloys are known to create a highly corrosive environment that causes irreversible degradation of most iron-based materials. In this paper, it has been found that an appropriate concentration of oxygen in the liquid alloy can significantly reduce this issue by creating a passivating oxide scale that controls diffusion, especially if Al is present in Fe-based materials (by Al-oxide formation). However, the increase of the temperature and of oxygen content in liquid phase leads to the increase of oxygen diffusion into bulk, and to promotion of the internal Al oxidation. This can causemore » a strain in bulk near the oxide layer, due either to mismatch between the thermal expansion coefficients of the oxides and bulk material, or to misfit of the crystal lattices (bulk vs. oxides). This work investigates the strain induced into proximal bulk of a Fe-Cr-Al alloy by oxide layers formation in liquid lead-bismuth eutectic utilizing synchrotron X-ray Laue microdiffraction. Finally, it is found that internal oxidation is the most likely cause for the strain in the metal rather than thermal expansion mismatch as a two-layer problem.« less

Novel Slide-Ring Material/Natural Rubber Composites with High Damping Property

PubMed Central

Wang, Wencai; Zhao, Detao; Yang, Jingna; Nishi, Toshio; Ito, Kohzo; Zhao, Xiuying; Zhang, Liqun

2016-01-01

A novel class of polymers called “slide-ring” (SR) materials with slideable junctions were used for high damping composites for the first time. The SR acts as the high damping phase dispersed in the natural rubber (NR) matrix, and epoxidized natural rubber (ENR) acts as the compatibilizer. The morphological, structural, and mechanical properties of the composites were investigated by atomic force microscope (AFM), transmission electron microscope (TEM), dynamic mechanical thermal analyzer (DMTA), rubber processing analyzer (RPA), and tensile tester. AFM and TEM results showed that the SR phase was uniformly dispersed in the composites, in a small size that is a function of ENR. DMTA and RPA results showed that the damping factor of the composites is much higher than that of NR, especially at room temperatures. Stretch hysteresis was used to study the energy dissipation of the composites at large strains. The results showed that SR and ENR can significantly improve the dissipation efficiency at strains lower than 200% strain. Wide-angle X-ray diffraction was used to study the strain-induced crystallization of the composites. The results indicated that the impact of the SR on the crystallization of NR is mitigated by the insulating effect of ENR. PMID:26949077

Unleashing elastic energy: dynamics of energy release in rubber bands and impulsive biological systems

NASA Astrophysics Data System (ADS)

Ilton, Mark; Cox, Suzanne; Egelmeers, Thijs; Patek, S. N.; Crosby, Alfred J.

Impulsive biological systems - which include mantis shrimp, trap-jaw ants, and venus fly traps - can reach high speeds by using elastic elements to store and rapidly release energy. The material behavior and shape changes critical to achieving rapid energy release in these systems are largely unknown due to limitations of materials testing instruments operating at high speed and large displacement. In this work, we perform fundamental, proof-of-concept measurements on the tensile retraction of elastomers. Using high speed imaging, the kinematics of retraction are measured for elastomers with varying mechanical properties and geometry. Based on the kinematics, the rate of energy dissipation in the material is determined as a function of strain and strain-rate, along with a scaling relation which describes the dependence of maximum velocity on material properties. Understanding this scaling relation along with the material failure limits of the elastomer allows the prediction of material properties required for optimal performance. We demonstrate this concept experimentally by optimizing for maximum velocity in our synthetic model system, and achieve retraction velocities that exceed those in biological impulsive systems. This model system provides a foundation for future work connecting continuum performance to molecular architecture in impulsive systems.

Machining and grinding: High rate deformation in practice

DOE Office of Scientific and Technical Information (OSTI.GOV)

Follansbee, P.S.

1993-04-01

Machining and grinding are well-established material-working operations involving highly non-uniform deformation and failure processes. A typical machining operation is characterized by uncertain boundary conditions (e.g.,surface interactions), three-dimensional stress states, large strains, high strain rates, non-uniform temperatures, highly localized deformations, and failure by both nominally ductile and brittle mechanisms. While machining and grinding are thought to be dominated by empiricism, even a cursory inspection leads one to the conclusion that this results more from necessity arising out of the complicated and highly interdisciplinary nature of the processes than from the lack thereof. With these conditions in mind, the purpose of thismore » paper is to outline the current understanding of strain rate effects in metals.« less

Machining and grinding: High rate deformation in practice

DOE Office of Scientific and Technical Information (OSTI.GOV)

Follansbee, P.S.

1993-01-01

Machining and grinding are well-established material-working operations involving highly non-uniform deformation and failure processes. A typical machining operation is characterized by uncertain boundary conditions (e.g.,surface interactions), three-dimensional stress states, large strains, high strain rates, non-uniform temperatures, highly localized deformations, and failure by both nominally ductile and brittle mechanisms. While machining and grinding are thought to be dominated by empiricism, even a cursory inspection leads one to the conclusion that this results more from necessity arising out of the complicated and highly interdisciplinary nature of the processes than from the lack thereof. With these conditions in mind, the purpose of thismore » paper is to outline the current understanding of strain rate effects in metals.« less

Chirped fiber Bragg grating written in highly birefringent fiber in simultaneous strain and temperature monitoring.

PubMed

Bieda, Marcin S; Sobotka, Piotr; Woliński, Tomasz R

2017-02-20

A new sensor configuration is proposed for simultaneous strain and temperature monitoring in a composite material that is based on a chirped fiber Bragg grating (CFBG) written in a highly birefringent (HB) polarization-maintaining fiber. The sensor is designed in the reflective configuration in which the CFBG acts both as a reflector and a sensing element. Since CFBG and HB fiber induce changes in the state of polarization (SOP), interference between polarization modes in the reflected spectrum is observed and analyzed. We used a simple readout setup to enable fast, linear operation of strain sensing as well simultaneous strain and temperature measurements in the composite.

Maximizing Tensile Strain in Germanium Nanomembranes for Enhanced Optoelectronic Properties

NASA Astrophysics Data System (ADS)

Sanchez Perez, Jose Roberto

Silicon, germanium, and their alloys, which provide the leading materials platform of microelectronics, are extremely inefficient light emitters because of their indirect fundamental energy band gap. This basic materials property has so far hindered the development of group-IV photonic-active devices, including light emitters and diode lasers, thereby significantly limiting our ability to integrate electronic and photonic functionalities at the chip level. Theoretical studies have predicted that tensile strain in Ge lowers the direct energy band gap relative to the indirect one, and that, with sufficient strain, Ge becomes direct-band gap, thus enabling facile interband light emission and the fabrication of Group IV lasers. It has, however, not been possible to impart sufficient strain to Ge to reach the direct-band gap goal, because bulk Ge fractures at much lower strains. Here it is shown that very thin sheets of Ge(001), called nanomembranes (NMs), can be used to overcome this materials limitation. Germanium nanomembranes (NMs) in the range of thicknesses from 20nm to 100nm were fabricated and then transferred and mounted to a flexible substrate [a polyimide (PI) sheet]. An apparatus was developed to stress the PI/NM combination and provide for in-situ Raman measurements of the strain as a function of applied stress. This arrangement allowed for the introduction of sufficient biaxial tensile strain (>1.7%) to transform Ge to a direct-band gap material, as determined by photoluminescence (PL) measurements and theory. Appropriate shifts in the emission spectrum and increases in PL intensities were observed. The advance in this work was nanomembrane fabrication technology; i.e., making thin enough Ge sheets to accept sufficiently high levels of strain without fracture. It was of interest to determine if the strain at which fracture ultimately does occur can be raised, by evaluating factors that initiate fracture. Attempts to assess the effect of free edges (enchant access holes) on the NM were made and an increase of 35% in the strain to at which crack first formed was found on NMs that lack etchant access holes. Ge NMs were used as a platform to investigate the relationships between surface passivation / functionalization and the physical properties of the material.

Conformational locking by design: relating strain energy with luminescence and stability in rigid metal-organic frameworks.

PubMed

Shustova, Natalia B; Cozzolino, Anthony F; Dincă, Mircea

2012-12-05

Minimization of the torsional barrier for phenyl ring flipping in a metal-organic framework (MOF) based on the new ethynyl-extended octacarboxylate ligand H(8)TDPEPE leads to a fluorescent material with a near-dark state. Immobilization of the ligand in the rigid structure also unexpectedly causes significant strain. We used DFT calculations to estimate the ligand strain energies in our and all other topologically related materials and correlated these with empirical structural descriptors to derive general rules for trapping molecules in high-energy conformations within MOFs. These studies portend possible applications of MOFs for studying fundamental concepts related to conformational locking and its effects on molecular reactivity and chromophore photophysics.

Dynamic 3D strain measurements with embedded micro-structured optical fiber Bragg grating sensors during impact on a CFRP coupon

NASA Astrophysics Data System (ADS)

Goossens, Sidney; Geernaert, Thomas; De Pauw, Ben; Lamberti, Alfredo; Vanlanduit, Steve; Luyckx, Geert; Chiesura, Gabriele; Thienpont, Hugo; Berghmans, Francis

2017-04-01

Composite materials are increasingly used in aerospace applications, owing to their high strength-to-mass ratio. Such materials are nevertheless vulnerable to impact damage. It is therefore important to investigate the effects of impacts on composites. Here we embed specialty microstructured optical fiber Bragg grating based sensors inside a carbon fiber reinforced polymer, providing access to the 3D strain evolution within the composite during impact. We measured a maximum strain of -655 μɛ along the direction of impact, and substantially lower values in the two in-plane directions. Such in-situ characterization can trigger insight in the development of impact damage in composites.

Optimized structural designs for stretchable silicon integrated circuits.

PubMed

Kim, Dae-Hyeong; Liu, Zhuangjian; Kim, Yun-Soung; Wu, Jian; Song, Jizhou; Kim, Hoon-Sik; Huang, Yonggang; Hwang, Keh-Chih; Zhang, Yongwei; Rogers, John A

2009-12-01

Materials and design strategies for stretchable silicon integrated circuits that use non-coplanar mesh layouts and elastomeric substrates are presented. Detailed experimental and theoretical studies reveal many of the key underlying aspects of these systems. The results shpw, as an example, optimized mechanics and materials for circuits that exhibit maximum principal strains less than 0.2% even for applied strains of up to approximately 90%. Simple circuits, including complementary metal-oxide-semiconductor inverters and n-type metal-oxide-semiconductor differential amplifiers, validate these designs. The results suggest practical routes to high-performance electronics with linear elastic responses to large strain deformations, suitable for diverse applications that are not readily addressed with conventional wafer-based technologies.

Correlation between Mechanical Behavior and Actuator-type Performance of Ni-Ti-Pd High-temperature Shape Memory Alloys

NASA Technical Reports Server (NTRS)

Bigelow, Glen S.; Padula, Santo A., II; Garg, Anita; Noebe, Ronald D.

2007-01-01

High-temperature shape memory alloys in the NiTiPd system are being investigated as lower cost alternatives to NiTiPt alloys for use in compact solid-state actuators for the aerospace, automotive, and power generation industries. A range of ternary NiTiPd alloys containing 15 to 46 at.% Pd has been processed and actuator mimicking tests (thermal cycling under load) were used to measure transformation temperatures, work behavior, and dimensional stability. With increasing Pd content, the work output of the material decreased, while the amount of permanent strain resulting from each load-biased thermal cycle increased. Monotonic isothermal tension testing of the high-temperature austenite and low temperature martensite phases was used to partially explain these behaviors, where a mismatch in yield strength between the austenite and martensite phases was observed at high Pd levels. Moreover, to further understand the source of the permanent strain at lower Pd levels, strain recovery tests were conducted to determine the onset of plastic deformation in the martensite phase. Consequently, the work behavior and dimensional stability during thermal cycling under load of the various NiTiPd alloys is discussed in relation to the deformation behavior of the materials as revealed by the strain recovery and monotonic tension tests.

Correlation between mechanical behavior and actuator-type performance of Ni-Ti-Pd high-temperature shape memory alloys

NASA Astrophysics Data System (ADS)

Bigelow, Glen S.; Padula, Santo A., II; Garg, Anita; Noebe, Ronald D.

2007-04-01

High-temperature shape memory alloys in the NiTiPd system are being investigated as lower cost alternatives to NiTiPt alloys for use in compact solid-state actuators for the aerospace, automotive, and power generation industries. A range of ternary NiTiPd alloys containing 15 to 46 at.% Pd has been processed and actuator mimicking tests (thermal cycling under load) were used to measure transformation temperatures, work behavior, and dimensional stability. With increasing Pd content, the work output of the material decreased, while the amount of permanent strain resulting from each load-biased thermal cycle increased. Monotonic isothermal tension testing of the high-temperature austenite and low temperature martensite phases was used to partially explain these behaviors, where a mismatch in yield strength between the austenite and martensite phases was observed at high Pd levels. Moreover, to further understand the source of the permanent strain at lower Pd levels, strain recovery tests were conducted to determine the onset of plastic deformation in the martensite phase. Consequently, the work behavior and dimensional stability during thermal cycling under load of the various NiTiPd alloys is discussed in relation to the deformation behavior of the materials as revealed by the strain recovery and monotonic tension tests.

An internal variable constitutive model for the large deformation of metals at high temperatures

NASA Technical Reports Server (NTRS)

Brown, Stuart; Anand, Lallit

1988-01-01

The advent of large deformation finite element methodologies is beginning to permit the numerical simulation of hot working processes whose design until recently has been based on prior industrial experience. Proper application of such finite element techniques requires realistic constitutive equations which more accurately model material behavior during hot working. A simple constitutive model for hot working is the single scalar internal variable model for isotropic thermal elastoplasticity proposed by Anand. The model is recalled and the specific scalar functions, for the equivalent plastic strain rate and the evolution equation for the internal variable, presented are slight modifications of those proposed by Anand. The modified functions are better able to represent high temperature material behavior. The monotonic constant true strain rate and strain rate jump compression experiments on a 2 percent silicon iron is briefly described. The model is implemented in the general purpose finite element program ABAQUS.

Flexible wire-shaped strain sensor from cotton thread for human health and motion detection.

PubMed

Li, Yuan-Qing; Huang, Pei; Zhu, Wei-Bin; Fu, Shao-Yun; Hu, Ning; Liao, Kin

2017-03-21

In this work, a wire-shaped flexible strain sensor was fabricated by encapsulating conductive carbon thread (CT) with polydimethylsiloxane (PDMS) elastomer. The key strain sensitive material, CT, was prepared by pyrolysing cotton thread in N 2 atmosphere. The CT/PDMS composite wire shows a typical piezo-resistive behavior with high strain sensitivity. The gauge factors (GF) calculated at low strain of 0-4% and high strain of 8-10% are 8.7 and 18.5, respectively, which are much higher than that of the traditional metallic strain sensor (GF around 2). The wire-shaped CT/PDMS composite sensor shows excellent response to cyclic tensile loading within the strain range of 0-10%, the frequency range of 0.01-10 Hz, to up to 2000 cycles. The potential of the wire senor as wearable strain sensor is demonstrated by the finger motion and blood pulse monitoring. Featured by the low costs of cotton wire and PDMS resin, the simple structure and fabrication technique, as well as high performance with miniaturized size, the wire-shaped sensor based on CT/PDMS composite is believed to have a great potential for application in wearable electronics for human health and motion monitoring.

DETERMINATION OF THE CREEP–FATIGUE INTERACTION DIAGRAM FOR ALLOY 617

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wright, J. K.; Carroll, L. J.; Sham, T. -L.

Alloy 617 is the leading candidate material for an intermediate heat exchanger for the very high temperature reactor. To evaluate the behavior of this material in the expected service conditions, creep-fatigue testing was performed. Testing has been performed primarily on a single heat of material at 850 and 950°C for total strain ranges of 0.3 to 1% and tensile hold times as long as 240 minutes. At 850°C, increases in the tensile hold duration degraded the creep fatigue resistance, at least to the investigated strain-controlled hold time of up to 60 minutes at the 0.3% strain range and 240 minutesmore » at the 1.0% strain range. At 950°C, the creep-fatigue cycles to failure becomes constant with increasing hold times, indicating saturation occurs at relatively short hold times. The creep and fatigue damage fractions have been calculated and plotted on a creep-fatigue interaction D-diagram. Results from earlier creep-fatigue tests at 800 and 1000°C on an additional heat of Alloy 617 are also plotted on the D-diagram. The methodology for calculating the damage fractions will be presented, and the effects of strain rate, strain range, temperature, hold time, and strain profile (i.e. holds in tension, compression or both) on the creep-fatigue damage will be explored.« less

Dynamic shear rheology of colloidal suspensions of surface-modified silica nanoparticles in PEG

NASA Astrophysics Data System (ADS)

Swarna; Pattanayek, Sudip Kumar; Ghosh, Anup Kumar

2018-03-01

The present work illustrates the effect of surface modification of silica nanoparticles (500 nm) with 3-(glycidoxypropyl)trimethoxy silane which was carried out at different reaction times. The suspensions prepared from modified and unmodified silica nanoparticles were evaluated for their shear rate-dependent viscosity and strain-frequency-dependent modulus. The linear viscoelastic moduli, viz., storage modulus and loss modulus, were compared with those of nonlinear moduli. The shear-thickened suspensions displayed strain thinning at low-frequency smaller strains and a strong strain overshoot at higher strains, characteristics of a continuous shear thickening fluids. The shear-thinned suspension, conversely, exhibited a strong elastic dominance at smaller strains, but at higher strains, its strain softened observed in the steady shear viscosity plot indicating characteristics of yielding material. Considering higher order harmonic components, the decomposed elastic and viscous stress revealed a pronounced elastic response up to 10% strain and a high viscous damping at larger strains. The current work is one of a kind in demonstrating the effect of silica surface functionalization on the linear and nonlinear viscoelasticity of suspensions showing a unique rheological fingerprint. The suspensions can thus be predicted through rheological studies for their applicability in energy absorbing and damping materials with respect to their mechanical properties.

Polydimethylsiloxane-fabricated optical fiber sensor capable of measuring both large axial and shear strain

NASA Astrophysics Data System (ADS)

Shen, Yu; Wang, Ziyuan; Wen, Huaihai; Zhou, Zhi

2014-11-01

Fiber optic sensor (FOS) has received much attention in the field of Structure Health Monitoring (SHM) due to its advantages of low weight, small size, high sensitivity multiplexing ability, free of electromagnetic interference and long durability. However, in harsh environments, structures often undergo large strain where few traditional fiber optic sensors could survive. This paper report a novel material with features of light-transparent, chemically inert, thermally stable material Polydimethylsiloxane(PDMS) fabricated large axial/shearing strain sensor. The sensor was fabricated by directly coupling a conventional signal mode fiber into half cured PDMS material using a translation stage under the inspection of a microscope. Meanwhile, a laser diode and a photo detector were used in the fabrication process to make sure the sensor achieved minimum light loss. An experiment was conducted later to investigate the sensor's transmission characteristic in 1310nm infrared laser relating with the applied axial/shearing strain. The results show that the proposed sensor survived an axial strain of 6 7.79 x 106 μɛ ; a shear of 4 6.49 x 104 μɛ with good linearity and repetition. The experiment indicates that the proposed sensor can potentially be used as strain sensing elements in Structure Health Monitoring systems under earthquake or explosion.

Fracto-mechanoluminescent light emission of EuD4TEA-PDMS composites subjected to high strain-rate compressive loading

NASA Astrophysics Data System (ADS)

Ryu, Donghyeon; Castaño, Nicolas; Bhakta, Raj; Kimberley, Jamie

2017-08-01

The objective of this study is to understand light emission characteristics of fracto-mechanoluminescent (FML) europium tetrakis(dibenzoylmethide)-triethylammonium (EuD4TEA) crystals under high strain-rate compressive loading. As a sensing material that can play a pivotal role for the self-powered impact sensor technology, it is important to understand transformative light emission characteristics of the FML EuD4TEA crystals under high strain-rate compressive loading. First, EuD4TEA crystals were synthesized and embedded into polydimethylsiloxane (PDMS) elastomer to fabricate EuD4TEA-PDMS composite test specimens. Second, the prepared EuD4TEA-PDMS composites were tested using the modified Kolsky bar setup equipped with a high-speed camera. Third, FML light emission was captured to yield 12 bit grayscale video footage, which was processed to quantify the FML light emission. Finally, quantitative parameters were generated by taking into account pixel values and population of pixels of the 12 bit grayscale images to represent FML light intensity. The FML light intensity was correlated with high strain-rate compressive strain and strain rate to understand the FML light emission characteristics under high strain-rate compressive loading that can result from impact occurrences.

Characterization of the behavior under impact loading of a maraging steel strengthened by nano-precipitates

NASA Astrophysics Data System (ADS)

Lach, E.; Redjaïmia, A.; Leitner, H.; Clemens, H.

2006-08-01

Nanometer-sized precipitates are responsible for the high strength of steel alloys well known as maraging steels. The term maraging relates to aging reactions in very low-carbon martensitic steels. Due to precipitation hardening 0.2% yield stress values of up to 2.4 GPa can be achieved. The class of stainless maraging steels exhibits an excellent combination of very high strength and hardness, ductility and toughness, combined with good corrosion resistance. In many applications like crash worthiness or ballistic protection the materials are loaded at high strain-rates. The most important characteristic of material behavior under dynamic load is the dynamic yield stress. In this work compression tests had been conducted at strain-rates in the order of 5 x 10 - 3 s - 1 up to 3 x 103 s - 1 to study the materials behaviour. Additionally high dynamic compression tests had been performed in the temperature range from -40circC up to 300circC.

The nano-epsilon dot method for strain rate viscoelastic characterisation of soft biomaterials by spherical nano-indentation.

PubMed

Mattei, G; Gruca, G; Rijnveld, N; Ahluwalia, A

2015-10-01

Nano-indentation is widely used for probing the micromechanical properties of materials. Based on the indentation of surfaces using probes with a well-defined geometry, the elastic and viscoelastic constants of materials can be determined by relating indenter geometry and measured load and displacement to parameters which represent stress and deformation. Here we describe a method to derive the viscoelastic properties of soft hydrated materials at the micro-scale using constant strain rates and stress-free initial conditions. Using a new self-consistent definition of indentation stress and strain and corresponding unique depth-independent expression for indentation strain rate, the epsilon dot method, which is suitable for bulk compression testing, is transformed to nano-indentation. We demonstrate how two materials can be tested with a displacement controlled commercial nano-indentor using the nano-espilon dot method (nano-ε̇M) to give values of instantaneous and equilibrium elastic moduli and time constants with high precision. As samples are tested in stress-free initial conditions, the nano-ε̇M could be useful for characterising the micro-mechanical behaviour of soft materials such as hydrogels and biological tissues at cell length scales. Copyright © 2015 Elsevier Ltd. All rights reserved.

Bi-Axial Strain Response of Structural Materials and Superconducting NB3SN Wires at 295 K, 7 K, and 4 K

NASA Astrophysics Data System (ADS)

Nyilas, A.; Weiss, K. P.

2008-03-01

A new extensometer capable of measuring diametral strains during axial loading of structural materials and superconducting composite wires has been developed. Using this new transducer it is possible to determine both the averaged axial strain and the transverse strain. The diametral extensometer with a mass of around 1 g is foreseen to be clamped onto the wire inside the averaging double extensometer sensing device system. The sensitivity of this new diametral extensometer is very high, nearly a factor of ten higher than the axial extensometer system. In addition, for structural materials and for composite materials an adjustable diametral extensometer enabling to test specimens between 5 mm and 15 mm diameter has been also developed and tested successfully at 4 K. For materials 304 L, Inconel 718, and modified Type 316LN stainless steel cast alloy the Poisson's coefficient could be determined at 295 K. Type 310 S stainless steel has been investigated at 7 K and at 4 K using the adjustable extensometer to determine the Poisson's coefficient, too. Furthermore, different types of superconducting A15 phase composite wires with diameters between 0.8 and 1.3 mm's were characterized in axial and diametral orientation.

Finite element analysis of composites materials for aerospace applications

NASA Astrophysics Data System (ADS)

Nurhaniza, M.; Ariffin, M. K. A.; Ali, Aidy; Mustapha, F.; Noraini, A. W.

2010-05-01

Composites materials are intended to be used more extensively as an alternative of aluminum structure in aircraft and aerospace applications. This is due to their attractive properties as high strength-to-weight ratio and stiffness-to-weight ratio. Besides that it clarifies the growing interest for composites materials due to advantages of lightweight, high strength, high stiffness, superior fatigue life, tremendous corrosion resistance and low cost manufacturing. In this study, a finite element analysis (FEA) of fiberglass unidirectional E-type was analyzed in the framework of ABAQUS finite element commercial software. The analysis was done to quantify the mechanical properties and response of unidirectional E-glass in term of tensile, compression and thermal responses. From the analysis, the maximum and minimum values of stress and strain for E-glass 21xK43 Gevetex and Silenka E-glass 1200tex were obtained and stress-strain curve is presented. The ultimate load of failure, elastic behavior, tensile strength and other properties for each laminated plates under tensile and thermal-stress are determined from stress-strain curves. The simulation will run twice for each material where the first simulation based on orientation angles of 45° for ply-1, -45° for ply-2 and 90° for ply-3 while the second simulation, the orientation angles is 0° for all plies. The simulation is successfully conducted and verified by experimental data.

Pathogenicity of exopolysaccharide-producing Actinomyces oris isolated from an apical abscess lesion

PubMed Central

Yamane, K; Nambu, T; Yamanaka, T; Ishihara, K; Tatami, T; Mashimo, C; Walker, C B; Leung, K-P; Fukushima, H

2013-01-01

Aim To demonstrate a capacity for producing exopolysaccharides (EPSs) and an ability to form biofilm on abiotic materials of Actinomyces oris strain K20. Methodology The productivity of EPSs and the ability to form biofilm of strain K20 were evaluated by measuring viscosity of spent culture media and by scanning electron microscopy (SEM) and the biofilm assay on microtitre plates, respectively. High-performance liquid chromatography was used to determine the chemical composition of the viscous materials. To examine the role of the viscous materials attributable to the pathogenicity in this organism, the ability of strain K20 to induce abscess formation was compared in mice to that of ATCC 27044. Results The viscosity of the spent culture media of K20 was significantly higher than that of ATCC 27044. Strain K20 showed dense meshwork structures around the cells and formed biofilms on microtitre plates, whereas ATCC 27044 did not. Chemical analysis of the viscous materials revealed that they were mainly composed of neutral sugars with mannose constituting 77.5% of the polysaccharides. Strain K20 induced persistent abscesses in mice lasting at least 5 days at a concentration of 108 cells mL−1, whereas abscesses induced by ATCC 27044 healed and disappeared or decreased in size at day 5. Conclusions Strain K20 produced EPSs, mainly consisting of mannose, and formed biofilms. This phenotype might play an important role for A. oris to express virulence through the progression of apical periodontitis. PMID:22900599

Pathogenicity of exopolysaccharide-producing Actinomyces oris isolated from an apical abscess lesion.

PubMed

Yamane, K; Nambu, T; Yamanaka, T; Ishihara, K; Tatami, T; Mashimo, C; Walker, C B; Leung, K-P; Fukushima, H

2013-02-01

To demonstrate a capacity for producing exopolysaccharides (EPSs) and an ability to form biofilm on abiotic materials of Actinomyces oris strain K20. The productivity of EPSs and the ability to form biofilm of strain K20 were evaluated by measuring viscosity of spent culture media and by scanning electron microscopy (SEM) and the biofilm assay on microtitre plates, respectively. High-performance liquid chromatography was used to determine the chemical composition of the viscous materials. To examine the role of the viscous materials attributable to the pathogenicity in this organism, the ability of strain K20 to induce abscess formation was compared in mice to that of ATCC 27044. The viscosity of the spent culture media of K20 was significantly higher than that of ATCC 27044. Strain K20 showed dense meshwork structures around the cells and formed biofilms on microtitre plates, whereas ATCC 27044 did not. Chemical analysis of the viscous materials revealed that they were mainly composed of neutral sugars with mannose constituting 77.5% of the polysaccharides. Strain K20 induced persistent abscesses in mice lasting at least 5 days at a concentration of 10(8) cells mL(-1), whereas abscesses induced by ATCC 27044 healed and disappeared or decreased in size at day 5. Strain K20 produced EPSs, mainly consisting of mannose, and formed biofilms. This phenotype might play an important role for A. oris to express virulence through the progression of apical periodontitis. © 2012 International Endodontic Journal.

Stress-dependent crystal structure of lanthanum strontium cobalt ferrite by in situ synchrotron X-ray diffraction

NASA Astrophysics Data System (ADS)

Geiger, Philipp T.; Khansur, Neamul H.; Riess, Kevin; Martin, Alexander; Hinterstein, Manuel; Webber, Kyle G.

2018-02-01

Lanthanum strontium cobalt ferrite La1-xSrxCo1-yFeyO3-δ (LSCF) is one of the most studied mixed ionic-electronic conductor materials due to electrical and transport properties, which are attractive for intermediate temperature solid oxide fuel cells (SOFCs), oxygen permeation membranes, and catalysis. The integration of such materials, however, depends on the thermal as well as mechanical behavior. LSCF exhibits nonlinear hysteresis during compressive stress-strain measurements, marked by a remanent strain and coercive stress, i.e., ferroelasticity. However, the origin of ferroelastic behavior has not been investigated under high compressive stress. This study, therefore, investigates the microscopic origin of stress-induced mechanical behavior in polycrystalline (La0.6Sr0.4)0.95Co0.2Fe0.8O3-δ using in situ synchrotron x-ray diffraction. The data presented here reveals that the strain response originates from the intrinsic lattice strain as well as the extrinsic domain switching strain without any apparent change in crystallographic symmetry. A comparison of the calculated microscopic strain contribution with that of a macroscopic measurement indicates a significant change in the relative contributions of intrinsic and extrinsic strain depending on the applied stress state, i.e., under maximum stress and after unloading. Direct evidence of the microscopic origin of stress-strain response outlined in this paper may assist in guiding materials design with the improved mechanical reliability of SOFCs.

From Modeling of Plasticity in Single-Crystal Superalloys to High-Resolution X-rays Three-Crystal Diffractometer Peaks Simulation

NASA Astrophysics Data System (ADS)

Jacques, Alain

2016-12-01

The dislocation-based modeling of the high-temperature creep of two-phased single-crystal superalloys requires input data beyond strain vs time curves. This may be obtained by use of in situ experiments combining high-temperature creep tests with high-resolution synchrotron three-crystal diffractometry. Such tests give access to changes in phase volume fractions and to the average components of the stress tensor in each phase as well as the plastic strain of each phase. Further progress may be obtained by a new method making intensive use of the Fast Fourier Transform, and first modeling the behavior of a representative volume of material (stress fields, plastic strain, dislocation densities…), then simulating directly the corresponding diffraction peaks, taking into account the displacement field within the material, chemical variations, and beam coherence. Initial tests indicate that the simulated peak shapes are close to the experimental ones and are quite sensitive to the details of the microstructure and to dislocation densities at interfaces and within the soft γ phase.

Methodology for Mechanical Property Testing of Fuel Cladding Using a Expanded Plug Wedge Test

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jiang, Hao; Wang, Jy-An John

2014-01-01

An expanded plug method was developed earlier for determining the tensile properties of irradiated fuel cladding. This method tests fuel rod cladding ductility by utilizing an expandable plug to radially stretch a small ring of irradiated cladding material. The circumferential or hoop strain is determined from the measured diametrical expansion of the ring. A developed procedure is used to convert the load circumferential strain data from the ring tests into material pseudo-stress-strain curves, from which material properties of the cladding can be extracted. However, several deficiencies existed in this expanded-plug test that can impact the accuracy of test results, suchmore » as that the large axial compressive stress resulted from the expansion plug test can potentially induce the shear failure mode of the tested specimen. Moreover, highly nonuniform stress and strain distribution in the deformed clad gage section and significant compressive stresses, induced by bending deformation due to clad bulging effect, will further result in highly nonconservative estimates of the mechanical properties for both strength and ductility of the tested clad. To overcome the aforementioned deficiencies associated with the current expansion plug test, systematic studies have been conducted. By optimizing the specific geometry designs, selecting the appropriate material for the expansion plug, and adding new components into the testing system, a modified expansion plug testing protocol has been developed. A general procedure was also developed to determine the hoop stress in the tested ring specimen. A scaling factor, -factor, was used to convert the ring load Fring into hoop stress , and is written as _ = F_ring/tl , where t is the clad thickness and l is the clad length. The generated stress-strain curve agrees well with the associated tensile test data in both elastic and plastic deformation regions.« less

Two phase modeling of the influence of plastic strain on the magnetic and magnetostrictive behaviors of ferromagnetic materials

NASA Astrophysics Data System (ADS)

Hubert, Olivier; Lazreg, Said

2017-02-01

A growing interest of automotive industry in the use of high performance steels is observed. These materials are obtained thanks to complex manufacturing processes whose parameters fluctuations lead to strong variations of microstructure and mechanical properties. The on-line magnetic non-destructive monitoring is a relevant response to this problem but it requires fast models sensitive to different parameters of the forming process. The plastic deformation is one of these important parameters. Indeed, ferromagnetic materials are known to be sensitive to stress application and especially to plastic strains. In this paper, a macroscopic approach using the kinematic hardening is proposed to model this behavior, considering a plastic strained material as a two phase system. Relationship between kinematic hardening and residual stress is defined in this framework. Since stress fields are multiaxial, an uniaxial equivalent stress is calculated and introduced inside the so-called magneto-mechanical multidomain modeling to represent the effect of plastic strain. The modeling approach is complemented by many experiments involving magnetic and magnetostrictive measurements. They are carried out with or without applied stress, using a dual-phase steel deformed at different levels. The main interest of this material is that the mechanically hard phase, soft phase and the kinematic hardening can be clearly identified thanks to simple experiments. It is shown how this model can be extended to single phase materials.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Weaver, Jordan S.; Pathak, Siddhartha; Reichardt, Ashley

Experimentally quantifying the mechanical effects of radiation damage in reactor materials is necessary for the development and qualification of new materials for improved performance and safety. This can be achieved in a high-throughput fashion through a combination of ion beam irradiation and small scale mechanical testing in contrast to the high cost and laborious nature of bulk testing of reactor irradiated samples. The current paper focuses on using spherical nanoindentation stress-strain curves on unirradiated and proton irradiated (10 dpa at 360 °C) 304 stainless steel to quantify the mechanical effects of radiation damage. Spherical nanoindentation stress-strain measurements show a radiation-inducedmore » increase in indentation yield strength from 1.36 GPa to 2.72 GPa and a radiation-induced increase in indentation work hardening rate of 10 GPa–30 GPa. These measurements are critically compared against Berkovich nanohardness, micropillar compression, and micro-tension measurements on the same material and similar grain orientations. The ratio of irradiated to unirradiated yield strength increases by a similar factor of 2 when measured via spherical nanoindentation or Berkovich nanohardness testing. A comparison of spherical indentation stress-strain curves to uniaxial (micropillar and micro-tension) stress-strain curves was achieved using a simple scaling relationship which shows good agreement for the unirradiated condition and poor agreement in post-yield behavior for the irradiated condition. Finally, the disagreement between spherical nanoindentation and uniaxial stress-strain curves is likely due to the plastic instability that occurs during uniaxial tests but is absent during spherical nanoindentation tests.« less

Numerical simulation of systems of shear bands in ductile metal with inclusions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Plohr, JeeYeon N., E-mail: jplohr@lanl.gov; Plohr, Bradley J.

2016-02-15

We develop a method for numerical simulations of high strain-rate loading of mesoscale samples of ductile metal with inclusions. Because of its small-scale inhomogeneity, the composite material is prone to localized shear deformation (adiabatic shear bands). This method employs the Generalized Method of Cells of Paley and Aboudi [Mech. Materials, vol. 14, pp. 127–139, 1992] to ensure that the micro mechanical behavior of the metal and inclusions is reflected properly in the behavior of the composite at the mesoscale. To find the effective plastic strain rate when shear bands are present, we extend and apply the analytic and numerical analysismore » of shear bands of Glimm, Plohr, and Sharp [Mech. Materials, vol. 24, pp. 31–41, 1996]. Our tests of the method focus on the stress/strain response in uniaxial-strain flow, both compressive and tensile, of depleted uranium metal containing silicon carbide inclusions. We use the Preston-Tonks-Wallace viscoplasticity model [J. Appl. Phys., vol. 93, pp. 211–220, 2003], which applies to the high strain-rate regime of an isotropic viscoplastic solid. In results, we verify the elevated temperature and thermal softening at shear bands in our simulations of pure DU and DU/SiC composites. We also note that in composites, due the asymmetry caused by the inclusions, shear band form at different times in different subcells. In particular, in the subcells near inclusions, shear band form much earlier than they do in pure DU.« less

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hansen, Benjamin L; Bronkhorst, Curt; Beyerlein, Irene

The goal of this work is to formulate a constitutive model for the deformation of metals over a wide range of strain rates. Damage and failure of materials frequently occurs at a variety of deformation rates within the same sample. The present state of the art in single crystal constitutive models relies on thermally-activated models which are believed to become less reliable for problems exceeding strain rates of 10{sup 4} s{sup -1}. This talk presents work in which we extend the applicability of the single crystal model to the strain rate region where dislocation drag is believed to dominate. Themore » elastic model includes effects from volumetric change and pressure sensitive moduli. The plastic model transitions from the low-rate thermally-activated regime to the high-rate drag dominated regime. The direct use of dislocation density as a state parameter gives a measurable physical mechanism to strain hardening. Dislocation densities are separated according to type and given a systematic set of interactions rates adaptable by type. The form of the constitutive model is motivated by previously published dislocation dynamics work which articulated important behaviors unique to high-rate response in fcc systems. The proposed material model incorporates thermal coupling. The hardening model tracks the varying dislocation population with respect to each slip plane and computes the slip resistance based on those values. Comparisons can be made between the responses of single crystals and polycrystals at a variety of strain rates. The material model is fit to copper.« less

Numerical simulation of systems of shear bands in ductile metal with inclusions

NASA Astrophysics Data System (ADS)

Plohr, JeeYeon N.; Plohr, Bradley J.

2016-02-01

We develop a method for numerical simulations of high strain-rate loading of mesoscale samples of ductile metal with inclusions. Because of its small-scale inhomogeneity, the composite material is prone to localized shear deformation (adiabatic shear bands). This method employs the Generalized Method of Cells of Paley and Aboudi [Mech. Materials, vol. 14, pp. 127-139, 1992] to ensure that the micro mechanical behavior of the metal and inclusions is reflected properly in the behavior of the composite at the mesoscale. To find the effective plastic strain rate when shear bands are present, we extend and apply the analytic and numerical analysis of shear bands of Glimm, Plohr, and Sharp [Mech. Materials, vol. 24, pp. 31-41, 1996]. Our tests of the method focus on the stress/strain response in uniaxial-strain flow, both compressive and tensile, of depleted uranium metal containing silicon carbide inclusions. We use the Preston-Tonks-Wallace viscoplasticity model [J. Appl. Phys., vol. 93, pp. 211-220, 2003], which applies to the high strain-rate regime of an isotropic viscoplastic solid. In results, we verify the elevated temperature and thermal softening at shear bands in our simulations of pure DU and DU/SiC composites. We also note that in composites, due the asymmetry caused by the inclusions, shear band form at different times in different subcells. In particular, in the subcells near inclusions, shear band form much earlier than they do in pure DU.

On stress/strain shielding and the material stiffness paradigm for dental implants.

PubMed

Korabi, Raoof; Shemtov-Yona, Keren; Rittel, Daniel

2017-10-01

Stress shielding considerations suggest that the dental implant material's compliance should be matched to that of the host bone. However, this belief has not been confirmed from a general perspective, either clinically or numerically. To characterize the influence of the implant stiffness on its functionality using the failure envelope concept that examines all possible combinations of mechanical load and application angle for selected stress, strain and displacement-based bone failure criteria. Those criteria represent bone yielding, remodeling, and implant primary stability, respectively MATERIALS AND METHODS: We performed numerical simulations to generate failure envelopes for all possible loading configurations of dental implants, with stiffness ranging from very low (polymer) to extremely high, through that of bone, titanium, and ceramics. Irrespective of the failure criterion, stiffer implants allow for improved implant functionality. The latter reduces with increasing compliance, while the trabecular bone experiences higher strains, albeit of an overall small level. Micromotions remain quite small irrespective of the implant's stiffness. The current paradigm favoring reduced implant material's stiffness out of concern for stress or strain shielding, or even excessive micromotions, is not supported by the present calculations, that point exactly to the opposite. © 2017 Wiley Periodicals, Inc.

Laboratory experiments from the toy store

NASA Technical Reports Server (NTRS)

Mcclelland, H. T.

1992-01-01

The following is a laboratory experiment designed to further understanding of materials science. This material could be taught to a typical student of materials science or manufacturing at the high school level or above. The objectives of this experiment are as follows: (1) to qualitatively demonstrate the concepts of elasticity, plasticity, and the strain rate and temperature dependence of the mechanical properties of engineering materials; (2) to qualitatively demonstrate the basics of extrusion including material flow, strain rate dependence of defects, lubrication effects, and the making of hollow shapes by extrusion (the two parts may be two separate experiments done at different times when the respective subjects are covered); and (3) to demonstrate the importance of qualitative observations and the amount of information which can be gathered without quantitative measurements.

Characterization of mechanical properties of pseudoelastic shape memory alloys under harmonic excitation

NASA Astrophysics Data System (ADS)

Böttcher, J.; Jahn, M.; Tatzko, S.

2017-12-01

Pseudoelastic shape memory alloys exhibit a stress-induced phase transformation which leads to high strains during deformation of the material. The stress-strain characteristic during this thermomechanical process is hysteretic and results in the conversion of mechanical energy into thermal energy. This energy conversion allows for the use of shape memory alloys in vibration reduction. For the application of shape memory alloys as vibration damping devices a dynamic modeling of the material behavior is necessary. In this context experimentally determined material parameters which accurately represent the material behavior are essential for a reliable material model. Subject of this publication is the declaration of suitable material parameters for pseudoelastic shape memory alloys and the methodology of their identification from experimental investigations. The used test rig was specifically designed for the characterization of pseudoelastic shape memory alloys.

3D modeling of unconstrained HPT process: role of strain gradient on high deformed microstructure formation

NASA Astrophysics Data System (ADS)

Ben Kaabar, A.; Aoufi, A.; Descartes, S.; Desrayaud, C.

2017-05-01

During tribological contact’s life, different deformation paths lead to the formation of high deformed microstructure, in the near-surface layers of the bodies. The mechanical conditions (high pressure, shear) occurring under contact, are reproduced through unconstrained High Pressure Torsion configuration. A 3D finite element model of this HPT test is developed to study the local deformation history leading to high deformed microstructure with nominal pressure and friction coefficient. For the present numerical study the friction coefficient at the interface sample/anvils is kept constant at 0.3; the material used is high purity iron. The strain distribution in the sample bulk, as well as the main components of the strain gradients according to the spatial coordinates are investigated, with rotation angle of the anvil.

ON THE DEGREE OF CONVERSION AND COEFFICIENT OF THERMAL EXPANSION OF A SINGLE FIBER COMPOSITE USING A FBG SENSOR

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lai, M.; Botsis, J.; Coric, D.

2008-08-28

The increasing needs of extending the lifetime in high-technology fields, such as space and aerospace, rail transport and naval systems, require quality enhancing of the composite materials either from a processing standing point or in the sense of resistance to service conditions. It is well accepted that the final quality of composite materials and structures is strongly influenced by processing parameters like curing and post-curing temperatures, rate of heating and cooling, applied vacuum, etc. To optimize manufacturing cycles, residual strains evolution due to chemical shrinkage and other physical parameters of the constituent materials must be characterized in situ. Such knowledgemore » can lead to a sensible reduction in defects and to improved physical and mechanical properties of final products. In this context continuous monitoring of strains distribution developed during processing is important in understanding and retrieving components' and materials' characteristics such as local strains gradients, degree of curing, coefficient of thermal expansion, moisture absorption, etc.« less

Relationship of compressive stress-strain response of engineering materials obtained at constant engineering and true strain rates

DOE PAGES

Song, Bo; Sanborn, Brett

2018-05-07

In this paper, a Johnson–Cook model was used as an example to analyze the relationship of compressive stress-strain response of engineering materials experimentally obtained at constant engineering and true strain rates. There was a minimal deviation between the stress-strain curves obtained at the same constant engineering and true strain rates. The stress-strain curves obtained at either constant engineering or true strain rates could be converted from one to the other, which both represented the intrinsic material response. There is no need to specify the testing requirement of constant engineering or true strain rates for material property characterization, provided that eithermore » constant engineering or constant true strain rate is attained during the experiment.« less

Relationship of compressive stress-strain response of engineering materials obtained at constant engineering and true strain rates

DOE Office of Scientific and Technical Information (OSTI.GOV)

Song, Bo; Sanborn, Brett

In this paper, a Johnson–Cook model was used as an example to analyze the relationship of compressive stress-strain response of engineering materials experimentally obtained at constant engineering and true strain rates. There was a minimal deviation between the stress-strain curves obtained at the same constant engineering and true strain rates. The stress-strain curves obtained at either constant engineering or true strain rates could be converted from one to the other, which both represented the intrinsic material response. There is no need to specify the testing requirement of constant engineering or true strain rates for material property characterization, provided that eithermore » constant engineering or constant true strain rate is attained during the experiment.« less

Progress in speckle-shift strain measurement

NASA Technical Reports Server (NTRS)

Lant, Christian T.; Barranger, John P.; Oberle, Lawrence G.; Greer, Lawrence C., III

1991-01-01

The Instrumentation and Control Technology Division of the Lewis Research Center has been developing an in-house capability to make one dimensional and two dimensional optical strain measurements on high temperature test specimens. The measurements are based on a two-beam speckle-shift technique. The development of composite materials for use in high temperature applications is generating interest in using the speckle-shift technique to measure strains on small diameter fibers and wires of various compositions. The results of preliminary speckle correlation tests on wire and fiber specimens are covered, and the advanced system currently under development is described.

A Coupled Experiment-finite Element Modeling Methodology for Assessing High Strain Rate Mechanical Response of Soft Biomaterials.

PubMed

Prabhu, Rajkumar; Whittington, Wilburn R; Patnaik, Sourav S; Mao, Yuxiong; Begonia, Mark T; Williams, Lakiesha N; Liao, Jun; Horstemeyer, M F

2015-05-18

This study offers a combined experimental and finite element (FE) simulation approach for examining the mechanical behavior of soft biomaterials (e.g. brain, liver, tendon, fat, etc.) when exposed to high strain rates. This study utilized a Split-Hopkinson Pressure Bar (SHPB) to generate strain rates of 100-1,500 sec(-1). The SHPB employed a striker bar consisting of a viscoelastic material (polycarbonate). A sample of the biomaterial was obtained shortly postmortem and prepared for SHPB testing. The specimen was interposed between the incident and transmitted bars, and the pneumatic components of the SHPB were activated to drive the striker bar toward the incident bar. The resulting impact generated a compressive stress wave (i.e. incident wave) that traveled through the incident bar. When the compressive stress wave reached the end of the incident bar, a portion continued forward through the sample and transmitted bar (i.e. transmitted wave) while another portion reversed through the incident bar as a tensile wave (i.e. reflected wave). These waves were measured using strain gages mounted on the incident and transmitted bars. The true stress-strain behavior of the sample was determined from equations based on wave propagation and dynamic force equilibrium. The experimental stress-strain response was three dimensional in nature because the specimen bulged. As such, the hydrostatic stress (first invariant) was used to generate the stress-strain response. In order to extract the uniaxial (one-dimensional) mechanical response of the tissue, an iterative coupled optimization was performed using experimental results and Finite Element Analysis (FEA), which contained an Internal State Variable (ISV) material model used for the tissue. The ISV material model used in the FE simulations of the experimental setup was iteratively calibrated (i.e. optimized) to the experimental data such that the experiment and FEA strain gage values and first invariant of stresses were in good agreement.

A Coupled Experiment-finite Element Modeling Methodology for Assessing High Strain Rate Mechanical Response of Soft Biomaterials

PubMed Central

Prabhu, Rajkumar; Whittington, Wilburn R.; Patnaik, Sourav S.; Mao, Yuxiong; Begonia, Mark T.; Williams, Lakiesha N.; Liao, Jun; Horstemeyer, M. F.

2015-01-01

This study offers a combined experimental and finite element (FE) simulation approach for examining the mechanical behavior of soft biomaterials (e.g. brain, liver, tendon, fat, etc.) when exposed to high strain rates. This study utilized a Split-Hopkinson Pressure Bar (SHPB) to generate strain rates of 100-1,500 sec-1. The SHPB employed a striker bar consisting of a viscoelastic material (polycarbonate). A sample of the biomaterial was obtained shortly postmortem and prepared for SHPB testing. The specimen was interposed between the incident and transmitted bars, and the pneumatic components of the SHPB were activated to drive the striker bar toward the incident bar. The resulting impact generated a compressive stress wave (i.e. incident wave) that traveled through the incident bar. When the compressive stress wave reached the end of the incident bar, a portion continued forward through the sample and transmitted bar (i.e. transmitted wave) while another portion reversed through the incident bar as a tensile wave (i.e. reflected wave). These waves were measured using strain gages mounted on the incident and transmitted bars. The true stress-strain behavior of the sample was determined from equations based on wave propagation and dynamic force equilibrium. The experimental stress-strain response was three dimensional in nature because the specimen bulged. As such, the hydrostatic stress (first invariant) was used to generate the stress-strain response. In order to extract the uniaxial (one-dimensional) mechanical response of the tissue, an iterative coupled optimization was performed using experimental results and Finite Element Analysis (FEA), which contained an Internal State Variable (ISV) material model used for the tissue. The ISV material model used in the FE simulations of the experimental setup was iteratively calibrated (i.e. optimized) to the experimental data such that the experiment and FEA strain gage values and first invariant of stresses were in good agreement. PMID:26067742

Stretchable conductors by kirigami patterning of aramid-silver nanocomposites with zero conductance gradient

NASA Astrophysics Data System (ADS)

Lyu, Jing; Hammig, Mark D.; Liu, Lehao; Xu, Lizhi; Chi, Hang; Uher, Ctirad; Li, Tiehu; Kotov, Nicholas A.

2017-10-01

Materials that are both stretchable and electrically conductive enable a broad spectrum of applications in sensing, actuating, electronics, optics and energy storage. The materials engineering concept of stretchable conductors is primarily based on combining nanowires, nanoribbons, nanoparticles, or nanocarbons with rubbery polymers to obtain composites with different abilities to transport charge and alter their nanoscale organization under strain. Although some of these composites reveal remarkably interesting multiscale reconfigurability and self-assembly phenomena, decreasing conductance with increased strain has restricted their widespread implementation. In a broader physical sense, the dependence of conductance on stress is undesirable because it requires a correlated change of electrical inputs. In this paper, we describe highly conductive and deformable sheets with a conductivity as high as 230 000 S cm-1, composed of silver nanoparticles, infiltrated within a porous aramid nanofiber (ANF) matrix. By forming a kirigami pattern, consisting of a regularized network of notches cut within the films, their ultimate tensile strain is improved from ˜2% to beyond 100%. The use of ANFs derived from well-known ultrastrong Kevlar™ fibers imparts high mechanical performance to the base composite. Importantly, the conductance of the films remains constant, even under large deformation resulting in a material with a zero conductance gradient. Unlike other nanocomposites for which strain and conductance are strongly coupled, the kirigami nanocomposite provides a pathway to demanding applications for flexible and stretchable electronics with power/voltage being unaffected by the deformation mode and temperature.

Development of Specifications for Engineered Cementitious Composites for Use in Bridge Deck Overlays

DOT National Transportation Integrated Search

2016-02-01

Engineered cementitious composite (ECC) material is a high strength, fiber-reinforced, ductile mortar mixture that can exhibit tensile strains of up to 5%. ECC has a dense matrix, giving the material exceptional durability characteristics. The durabi...

Bistable electroactive polymers (BSEP): large-strain actuation of rigid polymers

NASA Astrophysics Data System (ADS)

Yu, Zhibin; Niu, Xiaofan; Brochu, Paul; Yuan, Wei; Li, Huafeng; Chen, Bin; Pei, Qibing

2010-04-01

Reversible, large-strain, bistable actuation has been a lasting puzzle in the pursuit of smart materials and structures. Conducting polymers are bistable, but the achievable strain is small. Large deformations have been achieved in dielectric elastomers at the expense of mechanical strength. The gel or gel-like soft polymers generally have elastic moduli around or less than 10 MPa. The deformed polymer relaxes to its original shape once the applied electric field is removed. We report new, bistable electroactive polymers (BSEP) that are capable of electrically actuated strains as high as 335% area strain. The BSEP could be useful for constructing rigid structures. The structures can support high mechanical loads, and be actuated to large-strain deformations. We will present one unique application of the BSEP for Braille displays that can be quickly refreshed and maintain the displayed contents without a bias voltage.

Genome Sequence of the Alkaline-Tolerant Cellulomonas sp. Strain FA1

DOE PAGES

Cohen, Michael F.; Hu, Ping; Nguyen, My Vu; ...

2015-06-18

We present the genome of the cellulose-degrading Cellulomonas sp. strain FA1 isolated from an actively serpentinizing highly alkaline spring. Knowledge of this genome will enable studies into the molecular basis of plant material degradation in alkaline environments and inform the development of lignocellulose bioprocessing procedures for biofuel production.

High Strain Rate Deformation Modeling of a Polymer Matrix Composite. Part 1; Matrix Constitutive Equations

NASA Technical Reports Server (NTRS)

Goldberg, Robert K.; Stouffer, Donald C.

1998-01-01

Recently applications have exposed polymer matrix composite materials to very high strain rate loading conditions, requiring an ability to understand and predict the material behavior under these extreme conditions. In this first paper of a two part report, background information is presented, along with the constitutive equations which will be used to model the rate dependent nonlinear deformation response of the polymer matrix. Strain rate dependent inelastic constitutive models which were originally developed to model the viscoplastic deformation of metals have been adapted to model the nonlinear viscoelastic deformation of polymers. The modified equations were correlated by analyzing the tensile/ compressive response of both 977-2 toughened epoxy matrix and PEEK thermoplastic matrix over a variety of strain rates. For the cases examined, the modified constitutive equations appear to do an adequate job of modeling the polymer deformation response. A second follow-up paper will describe the implementation of the polymer deformation model into a composite micromechanical model, to allow for the modeling of the nonlinear, rate dependent deformation response of polymer matrix composites.

Modern magnetostrictive materials: classical and nonclassical alloys

NASA Astrophysics Data System (ADS)

Clark, Arthur E.; Wun-Fogle, Marilyn

2002-07-01

Magnetostrictive materials have not changed greatly from their discovery by Joule in 1842 through the 1960's. Their saturation strains remained small and their magnetomechanical couplings were only moderate. The separation of the rare earth elements during World War II and the subsequent measurement of their magnetic properties, created the groundwork for the development of 'giant' magnetostrictive materials during the 1960's. Magnetically anisotropic Tb and Dy became the generators of unprecedented classical magnetostrictions of nearly 1 percent. Coupling factors increased to approximately 0.8. During the same period, a remarkable 5-fold increase of magnetostriction of commonplace b.c.c. Fe with concentrations of Al near 1 18 percent was discovered. More recently, measurements in b.c.c. Fe-Ga alloys have shown a still greater enhancement of the magnetostriction, yielding strains of nearly 400 X 10-6 over the wide range in temperature from 4 K to far above room temperature. In the Fe alloys, as well as in the rare earth alloys, there is no known stress limit to the magnetostriction. Power output is limited by magnetic field generation and mechanical sample failure. Within the last few years, a new class of magnetostrictive materials, ferromagnetic shape memory alloys (FSMA's), have been introduced. These materials have huge magnetically induced strains. However, unlike the classical magnetostrictive alloys, these strains may be stress limited. While all the above materials have been introduced primarily for their high power electrical to mechanical energy conversion capability, they also function in the reciprocal mode, as magnetomechanical sensing materials.

Basalt fiber reinforced porous aggregates-geopolymer based cellular material

NASA Astrophysics Data System (ADS)

Luo, Xin; Xu, Jin-Yu; Li, Weimin

2015-09-01

Basalt fiber reinforced porous aggregates-geopolymer based cellular material (BFRPGCM) was prepared. The stress-strain curve has been worked out. The ideal energy-absorbing efficiency has been analyzed and the application prospect has been explored. The results show the following: fiber reinforced cellular material has successively sized pore structures; the stress-strain curve has two stages: elastic stage and yielding plateau stage; the greatest value of the ideal energy-absorbing efficiency of BFRPGCM is 89.11%, which suggests BFRPGCM has excellent energy-absorbing property. Thus, it can be seen that BFRPGCM is easy and simple to make, has high plasticity, low density and excellent energy-absorbing features. So, BFRPGCM is a promising energy-absorbing material used especially in civil defense engineering.

Coupled modeling and simulation of electro-elastic materials at large strains

NASA Astrophysics Data System (ADS)

Possart, Gunnar; Steinmann, Paul; Vu, Duc-Khoi

2006-03-01

In the recent years various novel materials have been developed that respond to the application of electrical loading by large strains. An example is the class of so-called electro-active polymers (EAP). Certainly these materials are technologically very interesting, e.g. for the design of actuators in mechatronics or in the area of artificial tissues. This work focuses on the phenomenological modeling of such materials within the setting of continuum-electro-dynamics specialized to the case of electro-hyperelastostatics and the corresponding computational setting. Thereby a highly nonlinear coupled problem for the deformation and the electric potential has to be considered. The finite element method is applied to solve the underlying equations numerically and some exemplary applications are presented.

Development of ultra-high temperature material characterization capabilities using digital image correlation analysis

NASA Astrophysics Data System (ADS)

Cline, Julia Elaine

2011-12-01

Ultra-high temperature deformation measurements are required to characterize the thermo-mechanical response of material systems for thermal protection systems for aerospace applications. The use of conventional surface-contacting strain measurement techniques is not practical in elevated temperature conditions. Technological advancements in digital imaging provide impetus to measure full-field displacement and determine strain fields with sub-pixel accuracy by image processing. In this work, an Instron electromechanical axial testing machine with a custom-designed high temperature gripping mechanism is used to apply quasi-static tensile loads to graphite specimens heated to 2000°F (1093°C). Specimen heating via Joule effect is achieved and maintained with a custom-designed temperature control system. Images are captured at monotonically increasing load levels throughout the test duration using an 18 megapixel Canon EOS Rebel T2i digital camera with a modified Schneider Kreutznach telecentric lens and a combination of blue light illumination and narrow band-pass filter system. Images are processed using an open-source Matlab-based digital image correlation (DIC) code. Validation of source code is performed using Mathematica generated images with specified known displacement fields in order to gain confidence in accurate software tracking capabilities. Room temperature results are compared with extensometer readings. Ultra-high temperature strain measurements for graphite are obtained at low load levels, demonstrating the potential for non-contacting digital image correlation techniques to accurately determine full-field strain measurements at ultra-high temperature. Recommendations are given to improve the experimental set-up to achieve displacement field measurements accurate to 1/10 pixel and strain field accuracy of less than 2%.

Modelling of Mechanical Behavior at High Strain Rate of Ti-6al-4v Manufactured By Means of Direct Metal Laser Sintering Technique

NASA Astrophysics Data System (ADS)

Iannitti, Gianluca; Bonora, Nicola; Gentile, Domenico; Ruggiero, Andrew; Testa, Gabriel; Gubbioni, Simone

2017-06-01

In this work, the mechanical behavior of Ti-6Al-4V obtained by additive manufacturing technique was investigated, also considering the build direction. Dog-bone shaped specimens and Taylor cylinders were machined from rods manufactured by means of the EOSSINT M2 80 machine, based on Direct Metal Laser Sintering technique. Tensile tests were performed at strain rate ranging from 5E-4 s-1 to 1000 s-1 using an Instron electromechanical machine for quasistatic tests and a Direct-Tension Split Hopkinson Bar for dynamic tests. The mechanical strength of the material was described by a Johnson-Cook model modified to account for stress saturation occurring at high strain. Taylor cylinder tests and their corresponding numerical simulations were carried out in order to validate the constitutive model under a complex deformation path, high strain rates, and high temperatures.

Orbiter thermal pressure drop characteristics for shuttle orbiter thermal protection system components: High density tile, low density tile, densified low density tile, and strain isolation pad

NASA Technical Reports Server (NTRS)

Lawing, P. L.; Nystrom, D. M.

1980-01-01

Pressure drop tests were conducted on available samples of low and high density tile, densified low density tile, and strain isolation pads. The results are presented in terms of pressure drop, material thickness and volume flow rate. Although the test apparatus was only capable of a small part of the range of conditions to be encountered in a Shuttle Orbiter flight, the data serve to determine the type of flow characteristics to be expected for each material type tested; the measured quantities also should serve as input for initial venting and flow through analysis.

Effects of Phase Transformations and Dynamic Material Strength on Hydrodynamic Instability Evolution in Metals

NASA Astrophysics Data System (ADS)

Opie, Saul

Hydrodynamic phenomena such as the Rayleigh-Taylor (RT) and Richtmyer-Meshkov (RM) instabilities can be described by exponential/linear growth of surface perturbations at a bimaterial interface when subjected to constant/impulsive acceleration. A challenge in designing systems to mitigate or exploit these effects is the lack of accurate material models at large dynamic strain rates and pressures. In particular, little stress-strain constitutive information at large strain rates and pressures is available for transient material phases formed at high pressures, and the continuum effect the phase transformation process has on the instability evolution. In this work, a phase-aware isotropic strength model is developed and partially validated with a novel RM-based instability experiment in addition to existing data from the literature. With the validated material model additional simulations are performed to provide insight into to the role that robust material constitutive behavior (e.g., pressure, temperature, rate dependence) has on RM instability and how RM instability experiments can be used to characterize and validated expected material behavior. For phase aware materials, particularly iron in this work, the simulations predict a strong dependence on the Atwood number that single phase materials do not have. At Atwood numbers close to unity, and pressures in the high pressure stability region, the high pressure phase dominates the RM evolution. However, at Atwood numbers close to negative one, the RM evolution is only weakly affected by the high-pressure phase even for shocks well above the phase transformation threshold. In addition to RM evolution this work looks at the closely related shock front perturbation evolution. Existing analytical models for isentropic processes in gases and liquids are modified for metal equation of states and plastic behavior for the first time. It is found that the presence of a volume collapsing phase transformation with increased pressure causes shock front perturbations to decay sooner, while plastic strength has the opposite effect which is significantly different from the effect viscosity has. These results suggest additional experimental setups to validate material models, or relevant material parameters that can be optimized for system design objectives, e.g., minimize feed through perturbations in inertial confinement fusion capsules.

A Membrane Model from Implicit Elasticity Theory

PubMed Central

Freed, A. D.; Liao, J.; Einstein, D. R.

2014-01-01

A Fungean solid is derived for membranous materials as a body defined by isotropic response functions whose mathematical structure is that of a Hookean solid where the elastic constants are replaced by functions of state derived from an implicit, thermodynamic, internal-energy function. The theory utilizes Biot’s (1939) definitions for stress and strain that, in 1-dimension, are the stress/strain measures adopted by Fung (1967) when he postulated what is now known as Fung’s law. Our Fungean membrane model is parameterized against a biaxial data set acquired from a porcine pleural membrane subjected to three, sequential, proportional, planar extensions. These data support an isotropic/deviatoric split in the stress and strain-rate hypothesized by our theory. These data also demonstrate that the material response is highly non-linear but, otherwise, mechanically isotropic. These data are described reasonably well by our otherwise simple, four-parameter, material model. PMID:24282079

Unified constitutive material models for nonlinear finite-element structural analysis. [gas turbine engine blades and vanes

NASA Technical Reports Server (NTRS)

Kaufman, A.; Laflen, J. H.; Lindholm, U. S.

1985-01-01

Unified constitutive material models were developed for structural analyses of aircraft gas turbine engine components with particular application to isotropic materials used for high-pressure stage turbine blades and vanes. Forms or combinations of models independently proposed by Bodner and Walker were considered. These theories combine time-dependent and time-independent aspects of inelasticity into a continuous spectrum of behavior. This is in sharp contrast to previous classical approaches that partition inelastic strain into uncoupled plastic and creep components. Predicted stress-strain responses from these models were evaluated against monotonic and cyclic test results for uniaxial specimens of two cast nickel-base alloys, B1900+Hf and Rene' 80. Previously obtained tension-torsion test results for Hastelloy X alloy were used to evaluate multiaxial stress-strain cycle predictions. The unified models, as well as appropriate algorithms for integrating the constitutive equations, were implemented in finite-element computer codes.

Semi-brittle flow of granitoid fault rocks in experiments

NASA Astrophysics Data System (ADS)

Pec, Matej; Stünitz, Holger; Heilbronner, Renée.; Drury, Martyn

2016-03-01

Field studies and seismic data show that semi-brittle flow of fault rocks probably is the dominant deformation mechanism at the base of the seismogenic zone at the so-called frictional-viscous transition. To understand the physical and chemical processes accommodating semi-brittle flow, we have performed an experimental study on synthetic granitoid fault rocks exploring a broad parameter space (temperature, T = 300, 400, 500, and 600°C, confining pressure, Pc ≈ 300, 500, 1000, and 1500 MPa, shear strain rate, γṡ ≈ 10-3, 10-4, 10-5, and 10-6 s-1, to finite shear strains, γ = 0-5). The experiments have been carried out using a granular material with grain size smaller than 200 µm with a little H2O added (0.2 wt %). Only two experiments (performed at the fastest strain rates and lowest temperatures) have failed abruptly right after reaching peak strength (τ ~ 1400 MPa). All other samples reach high shear stresses (τ ~ 570-1600 MPa) then weaken slightly (by Δτ ~ 10-190 MPa) and continue to deform at a more or less steady state stress level. Clear temperature dependence and a weak strain rate dependence of the peak as well as steady state stress levels are observed. In order to express this relationship, the strain rate-stress sensitivity has been fit with a stress exponent, assuming γ˙ ∝ τn and yields high stress exponents (n ≈ 10-140), which decrease with increasing temperature. The microstructures show widespread comminution, strain partitioning, and localization into slip zones. The slip zones contain at first nanocrystalline and partly amorphous material. Later, during continued deformation, fully amorphous material develops in some of the slip zones. Despite the mechanical steady state conditions, the fabrics in the slip zones and outside continue to evolve and do not reach a steady state microstructure below γ = 5. Within the slip zones, the fault rock material progressively transforms from a crystalline solid to an amorphous material. We present and interpret the experimental results both in terms of sliding friction and viscous flow, and we discuss the possible effect that the formation of nanocrystalline and amorphous layers may have on earthquake nucleation.

Stretchable, High-k Dielectric Elastomers through Liquid-Metal Inclusions.

PubMed

Bartlett, Michael D; Fassler, Andrew; Kazem, Navid; Markvicka, Eric J; Mandal, Pratiti; Majidi, Carmel

2016-05-01

An all-soft-matter composite with exceptional electro-elasto properties is demonstrated by embedding liquid-metal inclusions in an elastomer matrix. This material exhibits a unique combination of high dielectric constant, low stiffness, and large strain limit (ca. 600% strain). The elasticity, electrostatics, and electromechanical coupling of the composite are investigated, and strong agreement with predictions from effective medium theory is found. © 2016 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Configuration and Calibration of High Temperature Furnaces for Testing Ceramic Matrix Composites

DTIC Science & Technology

2014-10-01

Actual Furnace Cavity Stainless Steel Mesh Cage For Electrical Connections (both sides) High Temperature Power Lead Clamp Furnace Control TC’s Power... tests generate the basic properties such as modulus (E), ultimate tensile strength (UTS), proportional limit (PL), strain at failure (f), as well as...stress- strain behavior. Each material was tested at room temperature, at the maximum use temperature for the CMC system (as determined by the CMC

Gauge Factor and Stretchability of Silicon-on-Polymer Strain Gauges

PubMed Central

Yang, Shixuan; Lu, Nanshu

2013-01-01

Strain gauges are widely applied to measure mechanical deformation of structures and specimens. While metallic foil gauges usually have a gauge factor slightly over 2, single crystalline silicon demonstrates intrinsic gauge factors as high as 200. Although silicon is an intrinsically stiff and brittle material, flexible and even stretchable strain gauges have been achieved by integrating thin silicon strips on soft and deformable polymer substrates. To achieve a fundamental understanding of the large variance in gauge factor and stretchability of reported flexible/stretchable silicon-on-polymer strain gauges, finite element and analytically models are established to reveal the effects of the length of the silicon strip, and the thickness and modulus of the polymer substrate. Analytical results for two limiting cases, i.e., infinitely thick substrate and infinitely long strip, have found good agreement with FEM results. We have discovered that strains in silicon resistor can vary by orders of magnitude with different substrate materials whereas strip length or substrate thickness only affects the strain level mildly. While the average strain in silicon reflects the gauge factor, the maximum strain in silicon governs the stretchability of the system. The tradeoff between gauge factor and stretchability of silicon-on-polymer strain gauges has been proposed and discussed. PMID:23881128

Effect of Strengthening Mechanism on Strain-Rate Related Tensile Properties of Low-Carbon Sheet Steels for Automotive Application

NASA Astrophysics Data System (ADS)

Das, Anindya; Biswas, Pinaki; Tarafder, S.; Chakrabarti, D.; Sivaprasad, S.

2018-05-01

In order to ensure crash resistance of the steels used in automotive components, the ensile deformation behavior needs to be studied and predicted not only under quasi-static condition, but also under dynamic loading rates. In the present study, tensile tests have been performed on four different automobile grade sheet steels, namely interstitial free steel, dual-phase 600 and 800, and a carbon manganese steel over the strain rate regime of 0.001-800/s. Apart from the variation in strength (which always increased with strain rate), the effect of strengthening mechanism on strain rate sensitivity and strain hardening behavior has been evaluated. Strain rate sensitivity was found to increase at high-strain rate regime for all the steels. Contribution of solid solution hardening on strain rate sensitivity at lower plastic strains was found to be higher compared to dislocation strengthening and second-phase hardening. However, precipitation hardening coupled with solid solution hardening produced the highest strain rate sensitivity, in C-Mn-440 steel at high strain rates. Different strain-rate-sensitive models which take into account the change in yield stress and strain hardening behavior with strain rate for ductile materials were used to predict the flow behavior of these sheet steels at strain rates up to 800/s.

Flexible Carbon Nanotube Films for High Performance Strain Sensors

PubMed Central

Kanoun, Olfa; Müller, Christian; Benchirouf, Abderahmane; Sanli, Abdulkadir; Dinh, Trong Nghia; Al-Hamry, Ammar; Bu, Lei; Gerlach, Carina; Bouhamed, Ayda

2014-01-01

Compared with traditional conductive fillers, carbon nanotubes (CNTs) have unique advantages, i.e., excellent mechanical properties, high electrical conductivity and thermal stability. Nanocomposites as piezoresistive films provide an interesting approach for the realization of large area strain sensors with high sensitivity and low manufacturing costs. A polymer-based nanocomposite with carbon nanomaterials as conductive filler can be deposited on a flexible substrate of choice and this leads to mechanically flexible layers. Such sensors allow the strain measurement for both integral measurement on a certain surface and local measurement at a certain position depending on the sensor geometry. Strain sensors based on carbon nanostructures can overcome several limitations of conventional strain sensors, e.g., sensitivity, adjustable measurement range and integral measurement on big surfaces. The novel technology allows realizing strain sensors which can be easily integrated even as buried layers in material systems. In this review paper, we discuss the dependence of strain sensitivity on different experimental parameters such as composition of the carbon nanomaterial/polymer layer, type of polymer, fabrication process and processing parameters. The insights about the relationship between film parameters and electromechanical properties can be used to improve the design and fabrication of CNT strain sensors. PMID:24915183

Micromechanics Modeling of Composites Subjected to Multiaxial Progressive Damage in the Constituents

NASA Technical Reports Server (NTRS)

Bednarcyk, Brett A.; Aboudi, Jacob; Amold, Steven M.

2010-01-01

The high-fidelity generalized method of cells composite micromechanics model is extended to include constituent-scale progressive damage via a proposed damage model. The damage model assumes that all material nonlinearity is due to damage in the form of reduced stiffness, and it uses six scalar damage variables (three for tension and three for compression) to track the damage. Damage strains are introduced that account for interaction among the strain components and that also allow the development of the damage evolution equations based on the constituent material uniaxial stress strain response. Local final-failure criteria are also proposed based on mode-specific strain energy release rates and total dissipated strain energy. The coupled micromechanics-damage model described herein is applied to a unidirectional E-glass/epoxy composite and a proprietary polymer matrix composite. Results illustrate the capability of the coupled model to capture the vastly different character of the monolithic (neat) resin matrix and the composite in response to far-field tension, compression, and shear loading.

Multi-scale predictive modeling of nano-material and realistic electron devices

NASA Astrophysics Data System (ADS)

Palaria, Amritanshu

Among the challenges faced in further miniaturization of electronic devices, heavy influence of the detailed atomic configuration of the material(s) involved, which often differs significantly from that of the bulk material(s), is prominent. Device design has therefore become highly interrelated with material engineering at the atomic level. This thesis aims at outlining, with examples, a multi-scale simulation procedure that allows one to integrate material and device aspects of nano-electronic design to predict behavior of novel devices with novel material. This is followed in four parts: (1) An approach that combines a higher time scale reactive force field analysis with density functional theory to predict structure of new material is demonstrated for the first time for nanowires. Novel stable structures for very small diameter silicon nanowires are predicted. (2) Density functional theory is used to show that the new nanowire structures derived in 1 above have properties different from diamond core wires even though the surface bonds in some may be similar to the surface of bulk silicon. (3) Electronic structure of relatively large-scale germanium sections of realistically strained Si/strained Ge/ strained Si nanowire heterostructures is computed using empirical tight binding and it is shown that the average non-homogeneous strain in these structures drives their interesting non-conventional electronic characteristics such as hole effective masses which decrease as the wire cross-section is reduced. (4) It is shown that tight binding, though empirical in nature, is not necessarily limited to the material and atomic structure for which the parameters have been empirically derived, but that simple changes may adapt the derived parameters to new bond environments. Si (100) surface electronic structure is obtained from bulk Si parameters.

Progress Report on Long Hold Time Creep Fatigue of Alloy 617 at 850°C

DOE Office of Scientific and Technical Information (OSTI.GOV)

Carroll, Laura Jill

Alloy 617 is the leading candidate material for an intermediate heat exchanger for the very high temperature reactor. To evaluate the behavior of this material in the expected service conditions, strain-controlled cyclic tests that include long hold times up to 240 minutes at maximum tensile strain were conducted at 850°C. In terms of the total number of cycles to failure, the fatigue resistance decreased when a hold time was added at peak tensile strain. Increases in the tensile hold duration degraded the creep-fatigue resistance, at least to the investigated strain controlled hold time of up to 60 minutes at themore » 0.3% strain range and 240 minutes at the 1.0% strain range. The creep-fatigue deformation mode is considered relative to the lack of saturation, or continually decreasing number of cycles to failure with increasing hold times. Additionally, preliminary values from the 850°C creep-fatigue data are calculated for the creep-fatigue damage diagram and have higher values of creep damage than those from tests at 950°C.« less

Strain-engineered growth of two-dimensional materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ahn, Geun Ho; Amani, Matin; Rasool, Haider

The application of strain to semiconductors allows for controlled modification of their band structure. This principle is employed for the manufacturing of devices ranging from high-performance transistors to solid-state lasers. Traditionally, strain is typically achieved via growth on lattice-mismatched substrates. For two-dimensional (2D) semiconductors, this is not feasible as they typically do not interact epitaxially with the substrate. Here in this paper, we demonstrate controlled strain engineering of 2D semiconductors during synthesis by utilizing the thermal coefficient of expansion mismatch between the substrate and semiconductor. Using WSe 2 as a model system, we demonstrate stable built-in strains ranging from 1%more » tensile to 0.2% compressive on substrates with different thermal coefficient of expansion. Consequently, we observe a dramatic modulation of the band structure, manifested by a strain-driven indirect-to-direct bandgap transition and brightening of the dark exciton in bilayer and monolayer WSe 2, respectively. The growth method developed here should enable flexibility in design of more sophisticated devices based on 2D materials.« less

Strain-engineered growth of two-dimensional materials

DOE PAGES

Ahn, Geun Ho; Amani, Matin; Rasool, Haider; ...

2017-09-20

The application of strain to semiconductors allows for controlled modification of their band structure. This principle is employed for the manufacturing of devices ranging from high-performance transistors to solid-state lasers. Traditionally, strain is typically achieved via growth on lattice-mismatched substrates. For two-dimensional (2D) semiconductors, this is not feasible as they typically do not interact epitaxially with the substrate. Here in this paper, we demonstrate controlled strain engineering of 2D semiconductors during synthesis by utilizing the thermal coefficient of expansion mismatch between the substrate and semiconductor. Using WSe 2 as a model system, we demonstrate stable built-in strains ranging from 1%more » tensile to 0.2% compressive on substrates with different thermal coefficient of expansion. Consequently, we observe a dramatic modulation of the band structure, manifested by a strain-driven indirect-to-direct bandgap transition and brightening of the dark exciton in bilayer and monolayer WSe 2, respectively. The growth method developed here should enable flexibility in design of more sophisticated devices based on 2D materials.« less

Evolution of thermo-physical properties and annealing of fast neutron irradiated boron carbide

NASA Astrophysics Data System (ADS)

Gosset, Dominique; Kryger, Bernard; Bonal, Jean-Pierre; Verdeau, Caroline; Froment, Karine

2018-03-01

Boron carbide is widely used as a neutron absorber in most nuclear reactors, in particular in fast neutron ones. The irradiation leads to a large helium production (up to 1022/cm3) together with a strong decrease of the thermal conductivity. In this paper, we have performed thermal diffusivity measurements and X-ray diffraction analyses on boron carbide samples coming from control rods of the French Phenix LMFBR reactor. The burnups range from 1021 to 8.1021/cm3. We first confirm the strong decrease of the thermal conductivity at the low burnup, together with high microstructural modifications: swelling, large micro-strains, high defects density, and disordered-like material conductivity. We observe the microstructural parameters are highly anisotropic, with high micro-strains and flattened coherent diffracting domains along the (00l) direction of the hexagonal structure. Performing heat treatments up to high temperature (2200 °C) allows us to observe the material thermal conductivity and microstructure restoration. It then appears the thermal conductivity healing is correlated to the micro-strain relaxation. We then assume the defects responsible for most of the damage are the helium bubbles and the associated stress fields.

Dynamic tensile fracture of mortar at ultra-high strain-rates

NASA Astrophysics Data System (ADS)

Erzar, B.; Buzaud, E.; Chanal, P.-Y.

2013-12-01

During the lifetime of a structure, concrete and mortar may be exposed to highly dynamic loadings, such as impact or explosion. The dynamic fracture at high loading rates needs to be well understood to allow an accurate modeling of this kind of event. In this work, a pulsed-power generator has been employed to conduct spalling tests on mortar samples at strain-rates ranging from 2 × 104 to 4 × 104 s-1. The ramp loading allowed identifying the strain-rate anytime during the test. A power law has been proposed to fit properly the rate-sensitivity of tensile strength of this cementitious material over a wide range of strain-rate. Moreover, a specimen has been recovered damaged but unbroken. Micro-computed tomography has been employed to study the characteristics of the damage pattern provoked by the dynamic tensile loading.

Numerical-graphical method for describing the creep of damaged highly filled polymer materials

NASA Astrophysics Data System (ADS)

Bykov, D. L.; Martynova, E. D.; Mel'nikov, V. P.

2015-09-01

A method for describing the creep behavior until fracture of a highly filled polymer material previously damaged in preliminary tests is proposed. The constitutive relations are the relations of nonlinear endochronic theory of aging viscoelastic materials (NETAVEM) [1]. The numerical-graphical method for identifying the functions occurring in NETAVEM, which was proposed in [2] for describing loading processes at a constant strain rate, is used here for the first time in creep theory. We use the results of experiments with undamaged and preliminary damaged specimens under the action of the same constant tensile loads. The creep kernel is determined in experiments with an undamaged specimen. The reduced time function contained in NETAVEM is determined from the position of points corresponding to the same values of strain on the creep curves of the damaged and undamaged specimens. An integral equation is solved to obtain the aging function, and then the viscosity function is determined. The knowledge of all functions contained in the constitutive relations permits solving the creep problem for products manufactured from a highly filled polymer material.

Topologic connection between 2-D layered structures and 3-D diamond structures for conventional semiconductors

PubMed Central

Wang, Jianwei; Zhang, Yong

2016-01-01

When coming to identify new 2D materials, our intuition would suggest us to look from layered instead of 3D materials. However, since graphite can be hypothetically derived from diamond by stretching it along its [111] axis, many 3D materials can also potentially be explored as new candidates for 2D materials. Using a density functional theory, we perform a systematic study over the common Group IV, III–V, and II–VI semiconductors along different deformation paths to reveal new structures that are topologically connected to but distinctly different from the 3D parent structure. Specifically, we explore two major phase transition paths, originating respectively from wurtzite and NiAs structure, by applying compressive and tensile strain along the symmetry axis, and calculating the total energy changes to search for potential metastable states, as well as phonon spectra to examine the structural stability. Each path is found to further split into two branches under tensile strain–low buckled and high buckled structures, which respectively lead to a low and high buckled monolayer structure. Most promising new layered or planar structures identified include BeO, GaN, and ZnO on the tensile strain side, Ge, Si, and GaP on the compressive strain side. PMID:27090430

Numerical analysis of back pressure equal channel angular pressing of an Al-Mg alloy

NASA Astrophysics Data System (ADS)

Comăneci, R.

2017-08-01

Ultrafine grain size provides enhanced mechanical and/or physical properties such as strength and high ductility, superplasticity at relatively low temperatures and high strain rate and better corrosion resistance. Well-known as one of the most promising and effective structure refining method among other severe plastic deformation (SPD) techniques, equal channel angular pressing (ECAP) has been intensively investigated due to spectacular improvements in structure and therefore properties of bulk ultrafine grained/nanostructured materials. A successful ECAP requires surpassing two obstacles: the necessary load level which directly affects tools and a favourable stress distribution so the material withstanding the accumulated strain of repeated deformation. Materials could withstand more passes if a back pressure (BP) is applied. In traditional ECAP, tensile stress along the contact surface between the work piece and the upper wall of the outlet channel leads to crack initiation, while in the presence of BP, a negative (compressive) stress appears during the process balancing the tensile stress. In this study a comparative tridimensional finite element analysis (FEA) is performed to evaluate the flow of an Al-Mg alloy depending on different BP levels and process parameters. The results in terms of load level and strain distribution show the influence of BP on the material behaviour, opening opportunities for industrial applications.

The mathematical formulation of a generalized Hooke's law for blood vessels.

PubMed

Zhang, Wei; Wang, Chong; Kassab, Ghassan S

2007-08-01

It is well known that the stress-strain relationship of blood vessels is highly nonlinear. To linearize the relationship, the Hencky strain tensor is generalized to a logarithmic-exponential (log-exp) strain tensor to absorb the nonlinearity. A quadratic nominal strain potential is proposed to derive the second Piola-Kirchhoff stresses by differentiating the potential with respect to the log-exp strains. The resulting constitutive equation is a generalized Hooke's law. Ten material constants are needed for the three-dimensional orthotropic model. The nondimensional constant used in the log-exp strain definition is interpreted as a nonlinearity parameter. The other nine constants are the elastic moduli with respect to the log-exp strains. In this paper, the proposed linear stress-strain relation is shown to represent the pseudoelastic Fung model very well.

Carbon nanotube film interlayer for strain and damage sensing in composites during dynamic compressive loading

NASA Astrophysics Data System (ADS)

Wu, A. S.; Na, W.-J.; Yu, W.-R.; Byun, J.-H.; Chou, T.-W.

2012-11-01

A major challenge in the damage assessment of materials under dynamic, high strain rate loading lies in the inability to apply most health monitoring methodologies to the analysis and evaluation of damage incurred on short timescales. Here, we present a resistance-based sensing method utilizing an electrically conductive carbon nanotube film in a fiberglass/vinyl ester composite. This method reveals that applied strain and damage in the form of matrix cracking and delamination give rise to electrical resistance increases across the composite specimen; these can be measured in real-time during high strain rate loading. Damage within the composite specimens is confirmed through pre- and post-mortem x-ray micro computed tomography imaging.

Strain control of oxygen kinetics in the Ruddlesden-Popper oxide La 1.85Sr 0.15CuO 4

DOE Office of Scientific and Technical Information (OSTI.GOV)

Meyer, Tricia L.; Jacobs, Ryan; Lee, Dongkyu

Oxygen defect control has long been considered an important route to functionalizing complex oxide films. However, the nature of oxygen defects in thin films is often not investigated beyond basic redox chemistry. One of the model examples for oxygen-defect studies is the layered Ruddlesden–Popper phase La 2-xSr x CuO 4-δ (LSCO), in which the superconducting transition temperature is highly sensitive to epitaxial strain. However, previous observations of strain-superconductivity coupling in LSCO thin films were mainly understood in terms of elastic contributions to mechanical buckling, with minimal consideration of kinetic or thermodynamic factors. Here, we report that the oxygen nonstoichiometry commonlymore » reported for strained cuprates is mediated by the strain-modified surface exchange kinetics, rather than reduced thermodynamic oxygen formation energies. Remarkably, tensile-strained LSCO shows nearly an order of magnitude faster oxygen exchange rate than a compressively strained film, providing a strategy for developing high-performance energy materials.« less

Strain control of oxygen kinetics in the Ruddlesden-Popper oxide La 1.85Sr 0.15CuO 4

DOE PAGES

Meyer, Tricia L.; Jacobs, Ryan; Lee, Dongkyu; ...

2018-01-08

Oxygen defect control has long been considered an important route to functionalizing complex oxide films. However, the nature of oxygen defects in thin films is often not investigated beyond basic redox chemistry. One of the model examples for oxygen-defect studies is the layered Ruddlesden–Popper phase La 2-xSr x CuO 4-δ (LSCO), in which the superconducting transition temperature is highly sensitive to epitaxial strain. However, previous observations of strain-superconductivity coupling in LSCO thin films were mainly understood in terms of elastic contributions to mechanical buckling, with minimal consideration of kinetic or thermodynamic factors. Here, we report that the oxygen nonstoichiometry commonlymore » reported for strained cuprates is mediated by the strain-modified surface exchange kinetics, rather than reduced thermodynamic oxygen formation energies. Remarkably, tensile-strained LSCO shows nearly an order of magnitude faster oxygen exchange rate than a compressively strained film, providing a strategy for developing high-performance energy materials.« less

Characterization of Multifunctional Carbon Nanotube Yarns: In-situ Strain Sensing and Composite Reinforcement

NASA Astrophysics Data System (ADS)

Page, Christian David

A large body of scientific research and development worldwide has focused on the unprecedented structural/functional properties of carbon nanotubes (CNT), yet translation of these unique properties of CNTs to macroscopic materials has been slow to develop. CNT yarns are an appealing application for CNTs; their lightweight and small diameter can allow for them to be embedded into composite materials. Since the individual nanotubes have shown to have incredibly high strength, stiffness, and strain sensitivity, CNT yarns have the potential to be highly effective for in-situ structural health monitoring of advanced materials and structures. This work identifies the sources for losses in strength and electromechanical sensitivity. This is done by first understanding the physics involved with a CNT yarn under axial strain. Since this material is not a Newtonian solid, the stress-strain relationships are dissimilar to conventional materials, exhibiting a three zone behavior. This is present in both the stress-strain and resistance-strain relationships. A tensile test performed in-situ within a scanning electron microscope showed that the diameter of the yarn reduced greatly during tension, which indicates that the volume is not constant; therefore, the intratube/intrabundle load transfer efficiency and electrical conductivity change significantly under strain. Observation of this phenomenon helps elucidate the source for loss in the translation from nanoscopic CNTs to the macroscopic CNT yarns. Following the observation that the CNT yarn is not a solid body mechanics system, investigation into the long-standing field of textile engineering helped to identify that the CNT yarn structural hierarchy should be re-evaluated. Literary review reveals that the predominant base morphology of CNT yarns is bundles of CNTs as opposed to individual CNTs. Furthermore, in conventional textiles, it is well known that the base morphology (in textiles this is the "fiber") will bundle together during twisting. For CNT yarns, this level is referred to as packs since the title "bundle" has already been widely used as the grouping of individual CNTs. The utilization of conventional textile mechanics is supported by the congruent stress strain curves of cotton/wool yarns and CNT yarns. With this new perspective, sources of strength losses can be identified and, in most cases, quantified. Deterministic and statistical textile models are used to enumerate three top-level parameters which affect the yarn's strength. This approach offers guidance for future work to be done in the field of CNT yarns, including the growth of raw CNT forests, the spinning procedures involved, and any post-processing steps that may arise that can mitigate these losses that are extremely degrading to the CNT yarn mechanical strength. The strength of the yarn is a direct reflection of the quality of the yarn's structure. These morphological properties across the nano, meso, and macro scales have an effect on other physical properties such as electromechanical sensitivity. Improving the strength will also improve the yarn's ability to serve as a strain gage. Coupled with its appealing size, these yarns will be an effective in-situ embedded strain sensor. In conclusion, high quality CNT yarns with minimized strength losses show promise for structural health monitoring of advanced materials and structures since they can be both strongly reinforcing and electromechanically sensitive.

Molecular and biological characterization of the 5 human-bovine rotavirus (WC3)-based reassortant strains of the pentavalent rotavirus vaccine, RotaTeq (registered)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Matthijnssens, Jelle; Joelsson, Daniel B.; Warakomski, Donald J.

RotaTeq (registered) is a pentavalent rotavirus vaccine that contains five human-bovine reassortant strains (designated G1, G2, G3, G4, and P1) on the backbone of the naturally attenuated tissue culture-adapted parental bovine rotavirus (BRV) strain WC3. The viral genomes of each of the reassortant strains were completely sequenced and compared pairwise and phylogenetically among each other and to human rotavirus (HRV) and BRV reference strains. Reassortants G1, G2, G3, and G4 contained the VP7 gene from their corresponding HRV parent strains, while reassortants G1 and G2 also contained the VP3 gene (genotype M1) from the HRV parent strain. The P1 reassortantmore » contained the VP4 gene from the HRV parent strain and all the other gene segments from the BRV WC3 strain. The human VP7s had a high level of overall amino acid identity (G1: 95-99%, G2: 94-99% G3: 96-100%, G4: 93-99%) when compared to those of representative rotavirus strains of their corresponding G serotypes. The VP4 of the P1 reassortant had a high identity (92-97%) with those of serotype P1A[8] HRV reference strains, while the BRV VP7 showed identities ranging from 91% to 94% to those of serotype G6 HRV strains. Sequence analyses of the BRV or HRV genes confirmed that the fundamental structure of the proteins in the vaccine was similar to those of the HRV and BRV references strains. Sequences analyses showed that RotaTeq (registered) exhibited a high degree of genetic stability as no mutations were identified in the material of each reassortant, which undergoes two rounds of replication cycles in cell culture during the manufacturing process, when compared to the final material used to fill the dosing tubes. The infectivity of each of the reassortant strains of RotaTeq (registered) , like HRV strains, did not require the presence of sialic acid residues on the cell surface. The molecular and biologic characterization of RotaTeq (registered) adds to the significant body of clinical data supporting the consistent efficacy, immunogenicity, and safety of RotaTeq (registered) .« less

A Linear Viscoelastic Model Calibration of Sylgard 184.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Long, Kevin Nicholas; Brown, Judith Alice

2017-04-01

We calibrate a linear thermoviscoelastic model for solid Sylgard 184 (90-10 formulation), a lightly cross-linked, highly flexible isotropic elastomer for use both in Sierra / Solid Mechanics via the Universal Polymer Model as well as in Sierra / Structural Dynamics (Salinas) for use as an isotropic viscoelastic material. Material inputs for the calibration in both codes are provided. The frequency domain master curve of oscillatory shear was obtained from a report from Los Alamos National Laboratory (LANL). However, because the form of that data is different from the constitutive models in Sierra, we also present the mapping of the LANLmore » data onto Sandia’s constitutive models. Finally, blind predictions of cyclic tension and compression out to moderate strains of 40 and 20% respectively are compared with Sandia’s legacy cure schedule material. Although the strain rate of the data is unknown, the linear thermoviscoelastic model accurately predicts the experiments out to moderate strains for the slower strain rates, which is consistent with the expectation that quasistatic test procedures were likely followed. This good agreement comes despite the different cure schedules between the Sandia and LANL data.« less

Structure and Compressive Properties of Invar-Cenosphere Syntactic Foams.

PubMed

Luong, Dung; Lehmhus, Dirk; Gupta, Nikhil; Weise, Joerg; Bayoumi, Mohamed

2016-02-18

The present study investigates the mechanical performance of syntactic foams produced by means of the metal powder injection molding process having an Invar (FeNi36) matrix and including cenospheres as hollow particles at weight fractions (wt.%) of 5 and 10, respectively, corresponding to approximately 41.6 and 60.0 vol.% in relation to the metal content and at 0.6 g/cm³ hollow particle density. The synthesis process results in survival of cenospheres and provides low density syntactic foams. The microstructure of the materials is investigated as well as the mechanical performance under quasi-static and high strain rate compressive loads. The compressive stress-strain curves of syntactic foams reveal a continuous strain hardening behavior in the plastic region, followed by a densification region. The results reveal a strain rate sensitivity in cenosphere-based Invar matrix syntactic foams. Differences in properties between cenosphere- and glass microsphere-based materials are discussed in relation to the findings of microstructural investigations. Cenospheres present a viable choice as filler material in iron-based syntactic foams due to their higher thermal stability compared to glass microspheres.

Material degradation due to moisture and temperature. Part 1: mathematical model, analysis, and analytical solutions

NASA Astrophysics Data System (ADS)

Xu, C.; Mudunuru, M. K.; Nakshatrala, K. B.

2016-11-01

The mechanical response, serviceability, and load-bearing capacity of materials and structural components can be adversely affected due to external stimuli, which include exposure to a corrosive chemical species, high temperatures, temperature fluctuations (i.e., freezing-thawing), cyclic mechanical loading, just to name a few. It is, therefore, of paramount importance in several branches of engineering—ranging from aerospace engineering, civil engineering to biomedical engineering—to have a fundamental understanding of degradation of materials, as the materials in these applications are often subjected to adverse environments. As a result of recent advancements in material science, new materials such as fiber-reinforced polymers and multi-functional materials that exhibit high ductility have been developed and widely used, for example, as infrastructural materials or in medical devices (e.g., stents). The traditional small-strain approaches of modeling these materials will not be adequate. In this paper, we study degradation of materials due to an exposure to chemical species and temperature under large strain and large deformations. In the first part of our research work, we present a consistent mathematical model with firm thermodynamic underpinning. We then obtain semi-analytical solutions of several canonical problems to illustrate the nature of the quasi-static and unsteady behaviors of degrading hyperelastic solids.

Experimental Investigation of Textile Composite Materials Using Moire Interferometry

NASA Technical Reports Server (NTRS)

Ifju, Peter G.

1995-01-01

The viability as an efficient aircraft material of advanced textile composites is currently being addressed in the NASA Advanced Composites Technology (ACT) Program. One of the expected milestones of the program is to develop standard test methods for these complex material systems. Current test methods for laminated composites may not be optimum for textile composites, since the architecture of the textile induces nonuniform deformation characteristics on the scale of the smallest repeating unit of the architecture. The smallest repeating unit, also called the unit cell, is often larger than the strain gages used for testing of tape composites. As a result, extending laminated composite test practices to textiles can often lead to pronounced scatter in material property measurements. It has been speculated that the fiber architectures produce significant surface strain nonuniformities, however, the magnitudes were not well understood. Moire interferometry, characterized by full-field information, high displacement sensitivity, and high spatial resolution, is well suited to document the surface strain on textile composites. Studies at the NASA Langley Research Center on a variety of textile architectures including 2-D braids and 3-D weaves, has evidenced the merits of using moire interferometry to guide in test method development for textile composites. Moire was used to support tensile testing by validating instrumentation practices and documenting damage mechanisms. It was used to validate shear test methods by mapping the full-field deformation of shear specimens. Moire was used to validate open hole tension experiments to determine the strain concentration and compare then to numeric predictions. It was used for through-the-thickness tensile strength test method development, to verify capabilities for testing of both 2-D and 3-D material systems. For all of these examples, moire interferometry provided vision so that test methods could be developed with less speculation and more documentation.

Influence of the composite material thermal expansion on embedded highly birefringent polymer microstructured optical fibers

NASA Astrophysics Data System (ADS)

SzelÄ g, M.; Lesiak, P.; Kuczkowski, M.; Domański, A. W.; Woliński, T. R.

2013-05-01

Results of our research on embedded highly birefringent polymer microstructured fibers are presented. A composite material sample with fibers embedded between two layers of a multi-layer composite structure is fabricated and characterized. Temperature sensitivities of the polymer fibers are measured in a free space and compared with the fibers embedded in the composite material. It appeared that highly birefringent polymer microstructured fibers exhibit a strong increase in temperature sensitivity when embedded in the composite material, which is due to the stress-induced changes in birefringence created by thermally-induced strain.

A pulse-shaping technique to investigate the behaviour of brittle materials subjected to plate-impact tests.

PubMed

Forquin, Pascal; Zinszner, Jean-Luc

2017-01-28

Owing to their significant hardness and compressive strengths, ceramic materials are widely employed for use with protective systems subjected to high-velocity impact loadings. Therefore, their mechanical behaviour along with damage mechanisms need to be significantly investigated as a function of loading rates. However, the classical plate-impact testing procedures produce shock loadings in the brittle sample material which cause unrealistic levels of loading rates. Additionally, high-pulsed power techniques and/or functionally graded materials used as flyer plates to smooth the loading pulse remain costly, and are generally difficult to implement. In this study, a shockless plate-impact technique based on the use of either a wavy-machined flyer plate or buffer plate that can be produced by chip-forming is proposed. A series of numerical simulations using an explicit transient dynamic finite-element code have been performed to design and validate the experimental testing configuration. The calculations, conducted in two-dimensional (2D) plane-strain or in 2D axisymmetric modes, prove that the 'wavy' contact surface will produce a pulse-shaping effect, whereas the buffer plate will produce a homogenizing effect of the stress field along the transverse direction of the sample. In addition, 'wavy-shape' geometries of different sizes provide an easy way to change the level of loading rate and rise time in an experimentally tested ceramic specimen. Finally, when a shockless compression loading method is applied to the sample, a Lagrangian analysis of data is made possible by considering an assemblage of ceramic plates of different thicknesses in the target, so the axial stress-strain response of the brittle sample material can be provided.This article is part of the themed issue 'Experimental testing and modelling of brittle materials at high strain rates'. © 2016 The Author(s).

A pulse-shaping technique to investigate the behaviour of brittle materials subjected to plate-impact tests

NASA Astrophysics Data System (ADS)

Forquin, Pascal; Zinszner, Jean-Luc

2017-01-01

Owing to their significant hardness and compressive strengths, ceramic materials are widely employed for use with protective systems subjected to high-velocity impact loadings. Therefore, their mechanical behaviour along with damage mechanisms need to be significantly investigated as a function of loading rates. However, the classical plate-impact testing procedures produce shock loadings in the brittle sample material which cause unrealistic levels of loading rates. Additionally, high-pulsed power techniques and/or functionally graded materials used as flyer plates to smooth the loading pulse remain costly, and are generally difficult to implement. In this study, a shockless plate-impact technique based on the use of either a wavy-machined flyer plate or buffer plate that can be produced by chip-forming is proposed. A series of numerical simulations using an explicit transient dynamic finite-element code have been performed to design and validate the experimental testing configuration. The calculations, conducted in two-dimensional (2D) plane-strain or in 2D axisymmetric modes, prove that the `wavy' contact surface will produce a pulse-shaping effect, whereas the buffer plate will produce a homogenizing effect of the stress field along the transverse direction of the sample. In addition, `wavy-shape' geometries of different sizes provide an easy way to change the level of loading rate and rise time in an experimentally tested ceramic specimen. Finally, when a shockless compression loading method is applied to the sample, a Lagrangian analysis of data is made possible by considering an assemblage of ceramic plates of different thicknesses in the target, so the axial stress-strain response of the brittle sample material can be provided. This article is part of the themed issue 'Experimental testing and modelling of brittle materials at high strain rates'.

Laser-induced Microparticle Impact Experiments on Soft Materials

NASA Astrophysics Data System (ADS)

Kooi, Steven; Veysset, David; Maznev, Alexei; Yang, Yun Jung; Olsen, Bradley; Nelson, Keith

High-velocity impact testing is used to study fundamental aspects of materials behavior under high strain rates as well as in applications ranging from armor testing to the development of novel drug delivery platforms. In this work, we study high-velocity impact of micron-size projectiles on soft viscoelastic materials including synthetic hydrogels and gelatin samples. In an all optical laser-induced projectile impact test (LIPIT), a monolayer of microparticles is placed on a transparent substrate coated with a laser absorbing polymer layer. Ablation of a laser-irradiated polymer region accelerates the microparticles which are ejected from the launching pad into free space, reaching controllable speeds up to 1.5 km/s depending on the laser pulse energy and particle characteristics. The particles are monitored while in free space and after impact on the target surface with an ultrahigh-speed multi-frame camera that can record up to 16 images with time resolution of each frame as short as 3 ns. We present images and movies capturing individual particle impact and penetration in gels, and discuss the observed dynamics in the case of high Reynolds and Weber numbers. The results can provide direct input for modeling of high-velocity impact responses and high strain rate deformation in gels and other soft materials..

Experimental Study on Dynamic Mechanical Properties of 30CrMnSiNi2A Steel.

NASA Astrophysics Data System (ADS)

Huang, Fenglei; Yao, Wei; Wu, Haijun; Zhang, Liansheng

2009-06-01

Under dynamic conditions, the strain-rate dependence of material response and high levels of hydrostatic pressure cause the material behavior to be significantly different from what is observed under quasi-static condition. The curves of stress and strain of 30CrMnSiNi2A steel in different strain rates are obtained with SHPB experiments. Metallographic analyses show that 30CrMnSiNi2A steel is sensitive to strain rate, and dynamic compression leads to shear failure with the angle 45^o as the small carbide which precipitates around grain boundary changes the properties of 30CrMnSiNi2A steel. From the SHPB experiments and quasi-static results, the incomplete Johnson-Cook model has been obtained: σ=[1587+382.5(ɛ^p)^0.245][1+0.017ɛ^*], which can offer parameters for theory application and numerical simulation.

Creep-Fatigue Behavior of Alloy 617 at 850 and 950°C, Revision 2

DOE Office of Scientific and Technical Information (OSTI.GOV)

Carroll, L.; Carroll, M.

Alloy 617 is the leading candidate material for an Intermediate Heat Exchanger (IHX) of the Very High Temperature Reactor (VHTR). To evaluate the behavior of this material in the expected service conditions, strain-controlled cyclic tests including hold times up to 9000 s at maximum tensile strain were conducted at 850 and 950 degrees C. At both temperatures, the fatigue resistance decreased when a hold time was added at peak tensile strain. The magnitude of this effect depended on the specific mechanisms and whether they resulted in a change in fracture mode from transgranular in pure fatigue to intergranular in creep-fatiguemore » for a particular temperature and strain range combination. Increases in the tensile hold duration beyond an initial value were not detrimental to the creep-fatigue resistance at 950 degrees C but did continue to degrade the lifetimes at 850 degrees C.« less

High Temperature Uniaxial Compression and Stress-Relaxation Behavior of India-Specific RAFM Steel

NASA Astrophysics Data System (ADS)

Shah, Naimish S.; Sunil, Saurav; Sarkar, Apu

2018-07-01

India-specific reduced activity ferritic martensitic steel (INRAFM), a modified 9Cr-1Mo grade, has been developed by India as its own structural material for fabrication of the Indian Test Blanket Module (TBM) to be installed in the International Thermonuclear Energy Reactor (ITER). The extensive study on mechanical and physical properties of this material has been currently going on for appraisal of this material before being put to use in the ITER. High temperature compression, stress-relaxation, and strain-rate change behavior of the INRAFM steel have been investigated. The optical microscopic and scanning electron microscopic characterizations were carried out to observe the microstructural changes that occur during uniaxial compressive deformation test. Comparable true plastic stress values at 300 °C and 500 °C and a high drop in true plastic stress at 600 °C were observed during the compression test. Stress-relaxation behaviors were investigated at 500 °C, 550 °C, and 600 °C at a strain rate of 10-3 s-1. The creep properties of the steel at different temperatures were predicted from the stress-relaxation test. The Norton's stress exponent ( n) was found to decrease with the increasing temperature. Using Bird-Mukherjee-Dorn relationship, the temperature-compensated normalized strain rate vs stress was plotted. The stress exponent ( n) value of 10.05 was obtained from the normalized plot. The increasing nature of the strain rate sensitivity ( m) with the test temperature was found from strain-rate change test. The low plastic stability with m 0.06 was observed at 600 °C. The activation volume ( V *) values were obtained in the range of 100 to 300 b3. By comparing the experimental values with the literature, the rate-controlling mechanisms at the thermally activated region of high temperature were found to be the nonconservative movement of jogged screw dislocations and thermal breaking of attractive junctions.

High Temperature Uniaxial Compression and Stress-Relaxation Behavior of India-Specific RAFM Steel

NASA Astrophysics Data System (ADS)

Shah, Naimish S.; Sunil, Saurav; Sarkar, Apu

2018-05-01

India-specific reduced activity ferritic martensitic steel (INRAFM), a modified 9Cr-1Mo grade, has been developed by India as its own structural material for fabrication of the Indian Test Blanket Module (TBM) to be installed in the International Thermonuclear Energy Reactor (ITER). The extensive study on mechanical and physical properties of this material has been currently going on for appraisal of this material before being put to use in the ITER. High temperature compression, stress-relaxation, and strain-rate change behavior of the INRAFM steel have been investigated. The optical microscopic and scanning electron microscopic characterizations were carried out to observe the microstructural changes that occur during uniaxial compressive deformation test. Comparable true plastic stress values at 300 °C and 500 °C and a high drop in true plastic stress at 600 °C were observed during the compression test. Stress-relaxation behaviors were investigated at 500 °C, 550 °C, and 600 °C at a strain rate of 10-3 s-1. The creep properties of the steel at different temperatures were predicted from the stress-relaxation test. The Norton's stress exponent (n) was found to decrease with the increasing temperature. Using Bird-Mukherjee-Dorn relationship, the temperature-compensated normalized strain rate vs stress was plotted. The stress exponent (n) value of 10.05 was obtained from the normalized plot. The increasing nature of the strain rate sensitivity (m) with the test temperature was found from strain-rate change test. The low plastic stability with m 0.06 was observed at 600 °C. The activation volume (V *) values were obtained in the range of 100 to 300 b3. By comparing the experimental values with the literature, the rate-controlling mechanisms at the thermally activated region of high temperature were found to be the nonconservative movement of jogged screw dislocations and thermal breaking of attractive junctions.

Isolation Characterization and Fermented Research of High Producing Saccharamyces Cerevisae

NASA Astrophysics Data System (ADS)

Zhaochunhai

In order to improve to alcoholic production,this paper researched on 122 strains of yeast isolated from orchard and vegetable plot through morphology and molecular biology, screening 17 strains of Saccharomyces cerevisiae through NCBI-blast, selected four yeasts to ferment,amongof them T13 used sorghum as raw material production capacity of 12.48% (v/v).

Measurement and Interpretation of Flow Stress Data for the Simulation of Metal-Forming Processes

DTIC Science & Technology

2010-01-01

fitting constants that differ in each equation): Ludwik Equation: c)εb(aσ += , (29) Voce Equation: )]εcexp([1*a][baσ −−−+= (30) Swift...stress at low strains (ɘ.2) and to overestimate the stress for high strains. For heavily prestrained materials, c ~ 1. The Voce and Swift equations tend

Integration of graphene sensor with electrochromic device on modulus-gradient polymer for instantaneous strain visualization

NASA Astrophysics Data System (ADS)

Yang, Tingting; Zhong, Yujia; Tao, Dashuai; Li, Xinming; Zang, Xiaobei; Lin, Shuyuan; Jiang, Xin; Li, Zhihong; Zhu, Hongwei

2017-09-01

In nature, some animals change their deceptive coloration for camouflage, temperature preservation or communication. This astonishing function has inspired scientists to replicate the color changing abilities of animals with artificial skin. Recently, some studies have focused on the smart materials and devices with reversible color changing or light-emitting properties for instantaneous strain visualization. However, most of these works only show eye-detectable appearance change when subjected to large mechanical deformation (100%-500% strain), and conspicuous color change at small strain remains rarely explored. In the present study, we developed a user-interactive electronic skin with human-readable optical output by assembling a highly sensitive resistive strain sensor with a stretchable organic electrochromic device (ECD) together. We explored the substrate effect on the electromechanical behavior of graphene and designed a strategy of modulus-gradient structure to employ graphene as both the highly sensitive strain sensing element and the insensitive stretchable electrode of the ECD layer. Subtle strain (0-10%) was enough to evoke an obvious color change, and the RGB value of the color quantified the magnitude of the applied strain. Such high sensitivity to smaller strains (0-10%) with color changing capability will potentially enhance the function of wearable devices, robots and prosthetics in the future.

Evaluation of Strain-Life Fatigue Curve Estimation Methods and Their Application to a Direct-Quenched High-Strength Steel

NASA Astrophysics Data System (ADS)

Dabiri, M.; Ghafouri, M.; Rohani Raftar, H. R.; Björk, T.

2018-03-01

Methods to estimate the strain-life curve, which were divided into three categories: simple approximations, artificial neural network-based approaches and continuum damage mechanics models, were examined, and their accuracy was assessed in strain-life evaluation of a direct-quenched high-strength steel. All the prediction methods claim to be able to perform low-cycle fatigue analysis using available or easily obtainable material properties, thus eliminating the need for costly and time-consuming fatigue tests. Simple approximations were able to estimate the strain-life curve with satisfactory accuracy using only monotonic properties. The tested neural network-based model, although yielding acceptable results for the material in question, was found to be overly sensitive to the data sets used for training and showed an inconsistency in estimation of the fatigue life and fatigue properties. The studied continuum damage-based model was able to produce a curve detecting early stages of crack initiation. This model requires more experimental data for calibration than approaches using simple approximations. As a result of the different theories underlying the analyzed methods, the different approaches have different strengths and weaknesses. However, it was found that the group of parametric equations categorized as simple approximations are the easiest for practical use, with their applicability having already been verified for a broad range of materials.

Electromechanical Behavior of Chemically Reduced Graphene Oxide and Multi-walled Carbon Nanotube Hybrid Material

NASA Astrophysics Data System (ADS)

Benchirouf, Abderrahmane; Müller, Christian; Kanoun, Olfa

2016-01-01

In this paper, we propose strain-sensitive thin films based on chemically reduced graphene oxide (GO) and multi-walled carbon nanotubes (MWCNTs) without adding any further surfactants. In spite of the insulating properties of the thin-film-based GO due to the presence functional groups such as hydroxyl, epoxy, and carbonyl groups in its atomic structure, a significant enhancement of the film conductivity was reached by chemical reduction with hydro-iodic acid. By optimizing the MWCNT content, a significant improvement of electrical and mechanical thin film sensitivity is realized. The optical properties and the morphology of the prepared thin films were studied using ultraviolet-visible spectroscopy (UV-Vis) and scanning electron microscope (SEM). The UV-Vis spectra showed the ability to tune the band gap of the GO by changing the MWCNT content, whereas the SEM indicated that the MWCNTs were well dissolved and coated by the GO. Investigations of the piezoresistive properties of the hybrid nanocomposite material under mechanical load show a linear trend between the electrical resistance and the applied strain. A relatively high gauge factor of 8.5 is reached compared to the commercial metallic strain gauges. The self-assembled hybrid films exhibit outstanding properties in electric conductivity, mechanical strength, and strain sensitivity, which provide a high potential for use in strain-sensing applications.

Electromechanical Behavior of Chemically Reduced Graphene Oxide and Multi-walled Carbon Nanotube Hybrid Material.

PubMed

Benchirouf, Abderrahmane; Müller, Christian; Kanoun, Olfa

2016-12-01

In this paper, we propose strain-sensitive thin films based on chemically reduced graphene oxide (GO) and multi-walled carbon nanotubes (MWCNTs) without adding any further surfactants. In spite of the insulating properties of the thin-film-based GO due to the presence functional groups such as hydroxyl, epoxy, and carbonyl groups in its atomic structure, a significant enhancement of the film conductivity was reached by chemical reduction with hydro-iodic acid. By optimizing the MWCNT content, a significant improvement of electrical and mechanical thin film sensitivity is realized. The optical properties and the morphology of the prepared thin films were studied using ultraviolet-visible spectroscopy (UV-Vis) and scanning electron microscope (SEM). The UV-Vis spectra showed the ability to tune the band gap of the GO by changing the MWCNT content, whereas the SEM indicated that the MWCNTs were well dissolved and coated by the GO. Investigations of the piezoresistive properties of the hybrid nanocomposite material under mechanical load show a linear trend between the electrical resistance and the applied strain. A relatively high gauge factor of 8.5 is reached compared to the commercial metallic strain gauges. The self-assembled hybrid films exhibit outstanding properties in electric conductivity, mechanical strength, and strain sensitivity, which provide a high potential for use in strain-sensing applications.

Constitutive modeling for isotropic materials (HOST)

NASA Technical Reports Server (NTRS)

Lindholm, Ulric S.; Chan, Kwai S.; Bodner, S. R.; Weber, R. M.; Walker, K. P.; Cassenti, B. N.

1984-01-01

The results of the first year of work on a program to validate unified constitutive models for isotropic materials utilized in high temperature regions of gas turbine engines and to demonstrate their usefulness in computing stress-strain-time-temperature histories in complex three-dimensional structural components. The unified theories combine all inelastic strain-rate components in a single term avoiding, for example, treating plasticity and creep as separate response phenomena. An extensive review of existing unified theories is given and numerical methods for integrating these stiff time-temperature-dependent constitutive equations are discussed. Two particular models, those developed by Bodner and Partom and by Walker, were selected for more detailed development and evaluation against experimental tensile, creep and cyclic strain tests on specimens of a cast nickel base alloy, B19000+Hf. Initial results comparing computed and test results for tensile and cyclic straining for temperature from ambient to 982 C and strain rates from 10(exp-7) 10(exp-3) s(exp-1) are given. Some preliminary date correlations are presented also for highly non-proportional biaxial loading which demonstrate an increase in biaxial cyclic hardening rate over uniaxial or proportional loading conditions. Initial work has begun on the implementation of both constitutive models in the MARC finite element computer code.

InAs/GaInSb strained layer superlattice as an infrared detector material: an overview

NASA Astrophysics Data System (ADS)

Johnson, Jeffrey L.

2000-04-01

The investigation of the InAs/Ga1-xInxSb strained layer superlattice (SLS) has been largely motivated by the promise of overcoming limitations of current mature high-performance IR detectors, such as those using HgCdTe and extrinsic silicon. It also offers fundamentally superior performance over other newly emerging III-V bandgap- engineered materials such as QWIPs. The inherent properties of the InAs/GaInSb SLS have identified it as an attractive alternative for niche VLWIR applications requiring high performance under low backgrounds at operating temperatures > 40K. If this material system proves to meet the stringent demands of VLWIR applications, it will most certainly play a significant role as an alternative materials for photovoltaic focal pane arrays operating in the LWIR and MWIR regimes as well. This paper is an overview of SLS technology development, and focuses on critical development needs as seen from the perspective of the IR detector industry.

Engineering control of bacterial cellulose production using a genetic toolkit and a new cellulose-producing strain

PubMed Central

Florea, Michael; Hagemann, Henrik; Santosa, Gabriella; Micklem, Chris N.; Spencer-Milnes, Xenia; de Arroyo Garcia, Laura; Paschou, Despoina; Lazenbatt, Christopher; Kong, Deze; Chughtai, Haroon; Jensen, Kirsten; Freemont, Paul S.; Kitney, Richard; Reeve, Benjamin; Ellis, Tom

2016-01-01

Bacterial cellulose is a strong and ultrapure form of cellulose produced naturally by several species of the Acetobacteraceae. Its high strength, purity, and biocompatibility make it of great interest to materials science; however, precise control of its biosynthesis has remained a challenge for biotechnology. Here we isolate a strain of Komagataeibacter rhaeticus (K. rhaeticus iGEM) that can produce cellulose at high yields, grow in low-nitrogen conditions, and is highly resistant to toxic chemicals. We achieved external control over its bacterial cellulose production through development of a modular genetic toolkit that enables rational reprogramming of the cell. To further its use as an organism for biotechnology, we sequenced its genome and demonstrate genetic circuits that enable functionalization and patterning of heterologous gene expression within the cellulose matrix. This work lays the foundations for using genetic engineering to produce cellulose-based materials, with numerous applications in basic science, materials engineering, and biotechnology. PMID:27247386

Engineering control of bacterial cellulose production using a genetic toolkit and a new cellulose-producing strain.

PubMed

Florea, Michael; Hagemann, Henrik; Santosa, Gabriella; Abbott, James; Micklem, Chris N; Spencer-Milnes, Xenia; de Arroyo Garcia, Laura; Paschou, Despoina; Lazenbatt, Christopher; Kong, Deze; Chughtai, Haroon; Jensen, Kirsten; Freemont, Paul S; Kitney, Richard; Reeve, Benjamin; Ellis, Tom

2016-06-14

Bacterial cellulose is a strong and ultrapure form of cellulose produced naturally by several species of the Acetobacteraceae Its high strength, purity, and biocompatibility make it of great interest to materials science; however, precise control of its biosynthesis has remained a challenge for biotechnology. Here we isolate a strain of Komagataeibacter rhaeticus (K. rhaeticus iGEM) that can produce cellulose at high yields, grow in low-nitrogen conditions, and is highly resistant to toxic chemicals. We achieved external control over its bacterial cellulose production through development of a modular genetic toolkit that enables rational reprogramming of the cell. To further its use as an organism for biotechnology, we sequenced its genome and demonstrate genetic circuits that enable functionalization and patterning of heterologous gene expression within the cellulose matrix. This work lays the foundations for using genetic engineering to produce cellulose-based materials, with numerous applications in basic science, materials engineering, and biotechnology.

Constitutive Modelling and Deformation Band Angle Predictions for High Porosity Sandstones

NASA Astrophysics Data System (ADS)

Richards, M. C.; Issen, K. A.; Ingraham, M. D.

2017-12-01

The development of a field-scale deformation model requires a constitutive framework that is capable of representing known material behavior and able to be calibrated using available mechanical response data. This work employs the principle of hyperplasticity (e.g., Houlsby and Puzrin, 2006) to develop such a constitutive framework for high porosity sandstone. Adapting the works of Zimmerman et al. (1986) and Collins and Houlsby (1997), the mechanical data set of Ingraham et al. (2013 a, b) was used to develop a specific constitutive framework for Castlegate sandstone, a high porosity fluvial-deposited reservoir analog rock. Using the mechanical data set of Ingraham et al. (2013 a, b), explicit expressions and material parameters of the elastic moduli and strain tensors were obtained. With these expressions, analytical and numerical techniques were then employed to partition the total mechanical strain into elastic, coupled, and plastic strain components. With the partitioned strain data, yield surfaces in true-stress space, coefficients of internal friction, dilatancy factors, along with the theorectical predictions of the deformation band angles were obtained. These results were also evaluated against band angle values obtained from a) measurements on specimen jackets (Ingraham et al., 2013a), b) plane fits through located acoustic emissions (AE) events (Ingraham et al. 2013b), and c) X-ray micro-computed tomography (micro-CT) calculations.

High-dielectric-constant polymers as high-energy-density (HED) field effect actuator and capacitor materials

NASA Astrophysics Data System (ADS)

Huang, Cheng; Zhang, Qiming

2004-07-01

The development of high dielectric constant polymers as active materials in high-performance devices is one of the challenges in polymeric electronics and opto-electronics such as flexible thin-film capacitors, memory devices and microactuators for deformable micromirror technology. A group of poly(vinylidene fluoridetrifluoroethylene) P(VDF-TrFE) based high-dielectric-constant fluoroterpolymers have been developed, which have high room-temperature dielectric constant (K>60) and very high strain level and high energy density. The longitudinal and transverse strain of these materials can reach about -7% and 4.5%, respectively, and the elastic energy density is around 1.1 J/cm^3 under a high electric field of 150 MV/m. The influence on the electromechanical properties of copolymerizing poly(vinylidene fluoride-trifluoroethylene) (PVDF-TrFE) with a third monomer, chlorofluoroethylene (CFE), was investigated. It was found that increasing the CFE content from 0 to 8.5% slowly converts the ferroelectric structure of the copolymer to a relaxor ferroelectric system. This allows for a greatly decreased polarization and dielectric hysteresis and a much higher strain. Above 8.5%, increased CFE content substantially degrades the bulk crystallinity and the Young's modulus. These terpolymers have the potential to achieve above 10 J/cm^3 whole capacity energy density, which makes them good candidates for applications in pulse power capacitors. An all-polymer percolative composite by the combination of conductive polyaniline particles (K>10^5) within a fluoroterpolymer matrix, is introduced which exhibits very high dielectric constant (>7,000). The experimental results show that the dielectric behavior of this new class of percolative composites follows the prediction of the percolation theory and the analysis of the conductive percolation phenomena. The very high dielectric constant of the all-polymer composites which are also very flexible and possess elastic modulus not very much different from that of the insulation polymer matrix makes it possible to induce a high electromechanical response under a much reduced electric field (a strain of 2.65% with an elastic energy density of 0.18 J/cm^3 can be achieved under a low field of 16 MV/m). Data analysis also suggests that in these composites, the non-uniform local field distribution as well as interface effects can significantly enhance the strain responses. Furthermore, the experimental data as well as the data analysis indicate that the conduction loss in these composites will not affect the strain hysteresis. Flexible high dielectric constant electroactive polymers provide potential applications in high-energy-density (HED) energy storage and conversion systems such as lightweight field effect actuators and capacitors.

Design, Fabrication, and Calibration of an Embedded Piezoceramic Actuator for Active Control Applications

NASA Technical Reports Server (NTRS)

Koopmann, Gary H.; Lesieutre, George A.; Yoshikawa, Shoko; Chen, Weicheng; Fahnline, John B.; Pai, Suresh; Dershem, Brian

1996-01-01

In this presentation, the authors describe the design and fabrication processes for a PZT strain actuator that evolved during the initial stages of a research effort to synthesize and process intelligent, cost effective structures (SPICES). The actuator performance requirements were similar to those of conventional actuators, e.g., it had to be robust, highly efficient with adequate force and stroke, as lightweight as possible, and most importantly, affordable. Further, since the actuator was to be integrated within a composite structure, it had to be compatible with the host material and easily embeddable during the fabrication process. In control applications employing strain devices as actuators, a good bond between this actuator and host material is critical to their successful operation. This criterion is often difficult to achieve when attempting to join ceramics with metals or polymers with dissimilar properties such as Young's moduli, thermal expansion coefficients, etc. One unique feature of the actuator design that evolved in this project is that the need for direct bonding between the PZT ceramic and polymers was circumvented, i.e. the strain transfer to the host material was achieved via a frame surrounding the ceramic. Consequently, the frame material could be selected (or coated) for compatibility with the host material. A second feature is that the frame enclosed a co-fired, multilayered, PZT stack that was used to minimize the voltage requirements while maximizing the output strain.

Modeling of grain size strengthening in tantalum at high pressures and strain rates

DOE PAGES

Rudd, Robert E.; Park, H. -S.; Cavallo, R. M.; ...

2017-01-01

Laser-driven ramp wave compression experiments have been used to investigate the strength (flow stress) of tantalum and other metals at high pressures and high strain rates. Recently this kind of experiment has been used to assess the dependence of the strength on the average grain size of the material, finding no detectable variation with grain size. The insensitivity to grain size has been understood theoretically to result from the dominant effect of the high dislocation density generated at the extremely high strain rates of the experiment. Here we review the experiments and describe in detail the multiscale strength model usedmore » to simulate them. The multiscale strength model has been extended to include the effect of geometrically necessary dislocations generated at the grain boundaries during compatible plastic flow in the polycrystalline metal. Lastly, we use the extended model to make predictions of the threshold strain rates and grain sizes below which grain size strengthening would be observed in the laser-driven Rayleigh-Taylor experiments.« less

METALLURGY OF ZIRCALOY-2. PART II. THE EFFECTS OF FABRICATION VARIABLES ON THE PREFERRED ORIENTATION AND ANISOTROPY OF STRAIN BEHAVIOR

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rittenhouse, P.L.; Picklesimer, M.L.

1961-02-01

The preferred orientation and anisotropy of strain behavior of Zircaloy- 2 were studied as functions of fabrication variables. An inverse-pole-figure technique was used for the preferred orientation determinations. Evaluation of the effects of the fabrication variables on the anisotropy of strain behavior was accomplished by a contractile strainaxial strain analysis. An analysis of strain behavior in the normal direction was developed on the basis of theory of plastic flow of anisotropic metals. A simple intuitively derivable relation was found to exist between the strainstrain analysis and the preferred orientation data. Correlations of the strain-strain data with true-stress-truestrain diagrams and mechanicalmore » properties were attempted. The preferred orientation of Zircaloy-2 produced by the Oak Ridge National Laboratory-Homogeneous Reactor Project (ORNL- HRP) metallurgy fabrication schedule (ingot breakdown at 1500 to 1900 deg F, major reduction at 1800 to 1900 deg F or 1350 to 1450 deg F, a heat treatment of 30 min at 1800 at 1550 deg F followed by a water quench or rapid air cool to below 1200 deg F, a final reduction of 25 to 40% at 1000 deg F. and a 3O-min anneal at 1400 to 1425 deg F) was weak compared to that of most of the other schedules investigated. Elimination of the beta heat treatment (1800 to 1850 deg F for 30 min) between the major reduction and final reduction steps resulted in a material with a high degree of preferred orienation and with a state of pseudoisotropy in ihe rolling plane. A unique and quite high degree of preferred orientaion was developed when the ORNL-HRP metallurgy fabrication procedure was used, but the ingot axis was in the transverse rather than the rolling direction of the finished plate permitting more contractile sirain to occur in the normal direction than in either the rolling or transverse directions. The strain-strain analyses of the materials were consistent with the conclusions reached by the preferred orientation analyses. The effects of cross rolling on the anisotropy of strain behavior of Zircaloy-2 were found to depend on the type of cross rolling (unidirectional or rotational), the temperature of cross rolling, and the stage of fabrication at which the cross rolling was done. Unidirectional cross rolling at 1000 deg F after beta heat treatment caused only a slight increase in anisotropy of strain behavior over that for straight-rolled material, but roiational cross rolling at 1000 deg F after beta heat treatment resulted in a material with a state of isotropy of strain behavior only in the rolling plane. Rotational cross rolling before beta heat treatment, for one material at 1450 deg F and for another from 1900 deg F, produced different states or degrees of anisotropy of strain behavior. Because of flow constraints which exist in sheettype tensile specimens with width-to-thickness ratios > 1.0, it is imperative that round tensile specimens be used in the contractile strain-axial strain analysis. Since the principal axes of anisotropy are generally not the major sheet directions, they must be found by the preferred orientation analysis. (auth)« less

Coherent X-ray diffraction imaging and characterization of strain in silicon-on-insulator nanostructures

DOE PAGES

Xiong, Gang; Moutanabbir, Oussama; Reiche, Manfred; ...

2014-12-06

Coherent X-ray diffraction imaging (CDI) has emerged in the last decade as a promising high resolution lens-less imaging approach for the characterization of various samples. It has made significant technical progress through developments in source, algorithm and imaging methodologies thus enabling important scientific breakthroughs in a broad range of disciplines. In this report, we will introduce the principles of forward scattering CDI and Bragg geometry CDI (BCDI), with an emphasis on the latter. BCDI exploits the ultra-high sensitivity of the diffraction pattern to the distortions of crystalline lattice. Its ability of imaging strain on the nanometer scale in three dimensionsmore » is highly novel. In this study, we will present the latest progress on the application of BCDI in investigating the strain relaxation behavior in nanoscale patterned strained silicon-on-insulator (sSOI) materials, aiming to understand and engineer strain for the design and implementation of new generation semiconductor devices.« less

Coherent X-ray diffraction imaging and characterization of strain in silicon-on-insulator nanostructures.

PubMed

Xiong, Gang; Moutanabbir, Oussama; Reiche, Manfred; Harder, Ross; Robinson, Ian

2014-12-10

Coherent X-ray diffraction imaging (CDI) has emerged in the last decade as a promising high resolution lens-less imaging approach for the characterization of various samples. It has made significant technical progress through developments in source, algorithm and imaging methodologies thus enabling important scientific breakthroughs in a broad range of disciplines. In this report, we will introduce the principles of forward scattering CDI and Bragg geometry CDI (BCDI), with an emphasis on the latter. BCDI exploits the ultra-high sensitivity of the diffraction pattern to the distortions of crystalline lattice. Its ability of imaging strain on the nanometer scale in three dimensions is highly novel. We will present the latest progress on the application of BCDI in investigating the strain relaxation behavior in nanoscale patterned strained silicon-on-insulator (sSOI) materials, aiming to understand and engineer strain for the design and implementation of new generation semiconductor devices. © 2014 The Authors. Published by WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Application of CCG Sensors to a High-Temperature Structure Subjected to Thermo-Mechanical Load.

PubMed

Xie, Weihua; Meng, Songhe; Jin, Hua; Du, Chong; Wang, Libin; Peng, Tao; Scarpa, Fabrizio; Xu, Chenghai

2016-10-13

This paper presents a simple methodology to perform a high temperature coupled thermo-mechanical test using ultra-high temperature ceramic material specimens (UHTCs), which are equipped with chemical composition gratings sensors (CCGs). The methodology also considers the presence of coupled loading within the response provided by the CCG sensors. The theoretical strain of the UHTCs specimens calculated with this technique shows a maximum relative error of 2.15% between the analytical and experimental data. To further verify the validity of the results from the tests, a Finite Element (FE) model has been developed to simulate the temperature, stress and strain fields within the UHTC structure equipped with the CCG. The results show that the compressive stress exceeds the material strength at the bonding area, and this originates a failure by fracture of the supporting structure in the hot environment. The results related to the strain fields show that the relative error with the experimental data decrease with an increase of temperature. The relative error is less than 15% when the temperature is higher than 200 °C, and only 6.71% at 695 °C.

Strain engineered pyrochlore at high pressure

DOE PAGES

Rittman, Dylan R.; Turner, Katlyn M.; Park, Sulgiye; ...

2017-05-22

Strain engineering is a promising method for next-generation materials processing techniques. Here, we use mechanical milling and annealing followed by compression in diamond anvil cell to tailor the intrinsic and extrinsic strain in pyrochlore, Dy 2Ti 2O 7 and Dy 2Zr 2O 7. Raman spectroscopy, X-ray pair distribution function analysis, and X-ray diffraction were used to characterize atomic order over short-, medium-, and long-range spatial scales, respectively, under ambient conditions. Raman spectroscopy and X-ray diffraction were further employed to interrogate the material in situ at high pressure. High-pressure behavior is found to depend on the species and concentration of defectsmore » in the sample at ambient conditions. Overall, we show that defects can be engineered to lower the phase transformation onset pressure by ~50% in the ordered pyrochlore Dy 2Ti 2O 7, and lower the phase transformation completion pressure by ~20% in the disordered pyrochlore Dy 2Zr 2O 7. Lastly, these improvements are achieved without significantly sacrificing mechanical integrity, as characterized by bulk modulus.« less

Advances in Thin Film Sensor Technologies for Engine Applications

NASA Technical Reports Server (NTRS)

Lei, Jih-Fen; Martin, Lisa C.; Will, Herbert A.

1997-01-01

Advanced thin film sensor techniques that can provide accurate surface strain and temperature measurements are being developed at NASA Lewis Research Center. These sensors are needed to provide minimally intrusive characterization of advanced materials (such as ceramics and composites) and structures (such as components for Space Shuttle Main Engine, High Speed Civil Transport, Advanced Subsonic Transports and General Aviation Aircraft) in hostile, high-temperature environments and for validation of design codes. This paper presents two advanced thin film sensor technologies: strain gauges and thermocouples. These sensors are sputter deposited directly onto the test articles and are only a few micrometers thick; the surface of the test article is not structurally altered and there is minimal disturbance of the gas flow over the surface. The strain gauges are palladium-13% chromium based and the thermocouples are platinum-13% rhodium vs. platinum. The fabrication techniques of these thin film sensors in a class 1000 cleanroom at the NASA Lewis Research Center are described. Their demonstration on a variety of engine materials, including superalloys, ceramics and advanced ceramic matrix composites, in several hostile, high-temperature test environments are discussed.

Coherent pulse interrogation system for fiber Bragg grating sensing of strain and pressure in dynamic extremes of materials.

PubMed

Rodriguez, George; Jaime, Marcelo; Balakirev, Fedor; Mielke, Chuck H; Azad, Abul; Marshall, Bruce; La Lone, Brandon M; Henson, Bryan; Smilowitz, Laura

2015-06-01

A 100 MHz fiber Bragg grating (FBG) interrogation system is described and applied to strain and pressure sensing. The approach relies on coherent pulse illumination of the FBG sensor with a broadband short pulse from a femtosecond modelocked erbium fiber laser. After interrogation of the FBG sensor, a long multi-kilometer run of single mode fiber is used for chromatic dispersion to temporally stretch the spectral components of the reflected pulse from the FBG sensor. Dynamic strain or pressure induced spectral shifts in the FBG sensor are detected as a pulsed time domain waveform shift after encoding by the chromatic dispersive line. Signals are recorded using a single 35 GHz photodetector and a 50 G Samples per second, 25 GHz bandwidth, digitizing oscilloscope. Application of this approach to high-speed strain sensing in magnetic materials in pulsed magnetic fields to ~150 T is demonstrated. The FBG wavelength shifts are used to study magnetic field driven magnetostriction effects in LaCoO₃. A sub-microsecond temporal shift in the FBG sensor wavelength attached to the sample under first order phase change appears as a fractional length change (strain: ΔL/L<10^-4) in the material. A second application used FBG sensing of pressure dynamics to nearly 2 GPa in the thermal ignition of the high explosive PBX-9501 is also demonstrated. Both applications demonstrate the use of this FBG interrogation system in dynamical extreme conditions that would otherwise not be possible using traditional FBG interrogation approaches that are deemed too slow to resolve such events.

Spherical nanoindentation of proton irradiated 304 stainless steel: A comparison of small scale mechanical test techniques for measuring irradiation hardening

DOE PAGES

Weaver, Jordan S.; Pathak, Siddhartha; Reichardt, Ashley; ...

2017-06-27

Experimentally quantifying the mechanical effects of radiation damage in reactor materials is necessary for the development and qualification of new materials for improved performance and safety. This can be achieved in a high-throughput fashion through a combination of ion beam irradiation and small scale mechanical testing in contrast to the high cost and laborious nature of bulk testing of reactor irradiated samples. The current paper focuses on using spherical nanoindentation stress-strain curves on unirradiated and proton irradiated (10 dpa at 360 °C) 304 stainless steel to quantify the mechanical effects of radiation damage. Spherical nanoindentation stress-strain measurements show a radiation-inducedmore » increase in indentation yield strength from 1.36 GPa to 2.72 GPa and a radiation-induced increase in indentation work hardening rate of 10 GPa–30 GPa. These measurements are critically compared against Berkovich nanohardness, micropillar compression, and micro-tension measurements on the same material and similar grain orientations. The ratio of irradiated to unirradiated yield strength increases by a similar factor of 2 when measured via spherical nanoindentation or Berkovich nanohardness testing. A comparison of spherical indentation stress-strain curves to uniaxial (micropillar and micro-tension) stress-strain curves was achieved using a simple scaling relationship which shows good agreement for the unirradiated condition and poor agreement in post-yield behavior for the irradiated condition. Finally, the disagreement between spherical nanoindentation and uniaxial stress-strain curves is likely due to the plastic instability that occurs during uniaxial tests but is absent during spherical nanoindentation tests.« less

Spherical nanoindentation of proton irradiated 304 stainless steel: A comparison of small scale mechanical test techniques for measuring irradiation hardening

NASA Astrophysics Data System (ADS)

Weaver, Jordan S.; Pathak, Siddhartha; Reichardt, Ashley; Vo, Hi T.; Maloy, Stuart A.; Hosemann, Peter; Mara, Nathan A.

2017-09-01

Experimentally quantifying the mechanical effects of radiation damage in reactor materials is necessary for the development and qualification of new materials for improved performance and safety. This can be achieved in a high-throughput fashion through a combination of ion beam irradiation and small scale mechanical testing in contrast to the high cost and laborious nature of bulk testing of reactor irradiated samples. The current work focuses on using spherical nanoindentation stress-strain curves on unirradiated and proton irradiated (10 dpa at 360 °C) 304 stainless steel to quantify the mechanical effects of radiation damage. Spherical nanoindentation stress-strain measurements show a radiation-induced increase in indentation yield strength from 1.36 GPa to 2.72 GPa and a radiation-induced increase in indentation work hardening rate of 10 GPa-30 GPa. These measurements are critically compared against Berkovich nanohardness, micropillar compression, and micro-tension measurements on the same material and similar grain orientations. The ratio of irradiated to unirradiated yield strength increases by a similar factor of 2 when measured via spherical nanoindentation or Berkovich nanohardness testing. A comparison of spherical indentation stress-strain curves to uniaxial (micropillar and micro-tension) stress-strain curves was achieved using a simple scaling relationship which shows good agreement for the unirradiated condition and poor agreement in post-yield behavior for the irradiated condition. The disagreement between spherical nanoindentation and uniaxial stress-strain curves is likely due to the plastic instability that occurs during uniaxial tests but is absent during spherical nanoindentation tests.

Complexity in modeling of residual stresses and strains during polymerization of bone cement: effects of conversion, constraint, heat transfer, and viscoelastic property changes.

PubMed

Gilbert, Jeremy L

2006-12-15

Aseptic loosening of cemented joint prostheses remains a significant concern in orthopedic biomaterials. One possible contributor to cement loosening is the development of porosity, residual stresses, and local fracture of the cement that may arise from the in-situ polymerization of the cement. In-situ polymerization of acrylic bone cement is a complex set of interacting processes that involve polymerization reactions, heat generation and transfer, full or partial mechanical constraint, evolution of conversion- and temperature-dependent viscoelastic material properties, and thermal and conversion-driven changes in the density of the cement. Interactions between heat transfer and polymerization can lead to polymerization fronts moving through the material. Density changes during polymerization can, in the presence of mechanical constraint, lead to the development of locally high residual strain energy and residual stresses. This study models the interactions during bone cement polymerization and determines how residual stresses develop in cement and incorporates temperature and conversion-dependent viscoelastic behavior. The results show that the presence of polymerization fronts in bone cement result in locally high residual strain energies. A novel heredity integral approach is presented to track residual stresses incorporating conversion and temperature dependent material property changes. Finally, the relative contribution of thermal- and conversion-dependent strains to residual stresses is evaluated and it is found that the conversion-based strains are the major contributor to the overall behavior. This framework provides the basis for understanding the complex development of residual stresses and can be used as the basis for developing more complex models of cement behavior.

Spherical nanoindentation of proton irradiated 304 stainless steel: A comparison of small scale mechanical test techniques for measuring irradiation hardening

DOE Office of Scientific and Technical Information (OSTI.GOV)

Weaver, Jordan S.; Pathak, Siddhartha; Reichardt, Ashley

Experimentally quantifying the mechanical effects of radiation damage in reactor materials is necessary for the development and qualification of new materials for improved performance and safety. This can be achieved in a high-throughput fashion through a combination of ion beam irradiation and small scale mechanical testing in contrast to the high cost and laborious nature of bulk testing of reactor irradiated samples. The current paper focuses on using spherical nanoindentation stress-strain curves on unirradiated and proton irradiated (10 dpa at 360 °C) 304 stainless steel to quantify the mechanical effects of radiation damage. Spherical nanoindentation stress-strain measurements show a radiation-inducedmore » increase in indentation yield strength from 1.36 GPa to 2.72 GPa and a radiation-induced increase in indentation work hardening rate of 10 GPa–30 GPa. These measurements are critically compared against Berkovich nanohardness, micropillar compression, and micro-tension measurements on the same material and similar grain orientations. The ratio of irradiated to unirradiated yield strength increases by a similar factor of 2 when measured via spherical nanoindentation or Berkovich nanohardness testing. A comparison of spherical indentation stress-strain curves to uniaxial (micropillar and micro-tension) stress-strain curves was achieved using a simple scaling relationship which shows good agreement for the unirradiated condition and poor agreement in post-yield behavior for the irradiated condition. Finally, the disagreement between spherical nanoindentation and uniaxial stress-strain curves is likely due to the plastic instability that occurs during uniaxial tests but is absent during spherical nanoindentation tests.« less

Implementation of an Associative Flow Rule Including Hydrostatic Stress Effects Into the High Strain Rate Deformation Analysis of Polymer Matrix Composites

NASA Technical Reports Server (NTRS)

Goldberg, Robert K.; Roberts, Gary D.; Gilat, Amos

2003-01-01

A previously developed analytical formulation has been modified in order to more accurately account for the effects of hydrostatic stresses on the nonlinear, strain rate dependent deformation of polymer matrix composites. State variable constitutive equations originally developed for metals have been modified in order to model the nonlinear, strain rate dependent deformation of polymeric materials. To account for the effects of hydrostatic stresses, which are significant in polymers, the classical J2 plasticity theory definitions of effective stress and effective inelastic strain, along with the equations used to compute the components of the inelastic strain rate tensor, are appropriately modified. To verify the revised formulation, the shear and tensile deformation of two representative polymers are computed across a wide range of strain rates. Results computed using the developed constitutive equations correlate well with experimental data. The polymer constitutive equations are implemented within a strength of materials based micromechanics method to predict the nonlinear, strain rate dependent deformation of polymer matrix composites. The composite mechanics are verified by analyzing the deformation of a representative polymer matrix composite for several fiber orientation angles across a variety of strain rates. The computed values compare well to experimentally obtained results.

Ultratransparent and stretchable graphene electrodes

PubMed Central

Liu, Nan; Chortos, Alex; Lei, Ting; Jin, Lihua; Kim, Taeho Roy; Bae, Won-Gyu; Zhu, Chenxin; Wang, Sihong; Pfattner, Raphael; Chen, Xiyuan; Sinclair, Robert; Bao, Zhenan

2017-01-01

Two-dimensional materials, such as graphene, are attractive for both conventional semiconductor applications and nascent applications in flexible electronics. However, the high tensile strength of graphene results in fracturing at low strain, making it challenging to take advantage of its extraordinary electronic properties in stretchable electronics. To enable excellent strain-dependent performance of transparent graphene conductors, we created graphene nanoscrolls in between stacked graphene layers, referred to as multilayer graphene/graphene scrolls (MGGs). Under strain, some scrolls bridged the fragmented domains of graphene to maintain a percolating network that enabled excellent conductivity at high strains. Trilayer MGGs supported on elastomers retained 65% of their original conductance at 100% strain, which is perpendicular to the direction of current flow, whereas trilayer films of graphene without nanoscrolls retained only 25% of their starting conductance. A stretchable all-carbon transistor fabricated using MGGs as electrodes exhibited a transmittance of >90% and retained 60% of its original current output at 120% strain (parallel to the direction of charge transport). These highly stretchable and transparent all-carbon transistors could enable sophisticated stretchable optoelectronics. PMID:28913422

The Dynamic Flow and Failure Behavior of Magnesium and Magnesium Alloys

NASA Astrophysics Data System (ADS)

Eswar Prasad, K.; Li, B.; Dixit, N.; Shaffer, M.; Mathaudhu, S. N.; Ramesh, K. T.

2014-01-01

We review the dynamic behavior of magnesium alloys through a survey of the literature and a comparison with our own high-strain-rate experiments. We describe high-strain-rate experiments (at typical strain rates of 103 s-1) on polycrystalline pure magnesium as well as two magnesium alloys, AZ31B and ZK60. Both deformation and failure are considered. The observed behaviors are discussed in terms of the fundamental deformation and failure mechanisms in magnesium, considering the effects of grain size, strain rate, and crystallographic texture. A comparison of current results with the literature studies on these and other Mg alloys reveals that the crystallographic texture, grain size, and alloying elements continue to have a profound influence on the high-strain-rate deformation behavior. The available data set suggests that those materials loaded so as to initiate extension twinning have relatively rate-insensitive strengths up to strain rates of several thousand per second. In contrast, some rate dependence of the flow stress is observed for loading orientations in which the plastic flow is dominated by dislocation mechanisms.

Clostridium species strain BOH3 tolerates and transforms inhibitors from horticulture waste hydrolysates.

PubMed

Yan, Yu; He, Jianzhong

2017-08-01

Conversion of lignocellulosic hydrolysate to biofuels is impeded by the toxic effects of inhibitors that are generated during pretreatment and hydrolysis processes. Here we describe a wild-type Clostridium sp. strain BOH3 with high tolerance to the lignocellulose-derived inhibitors and its capability to transform these inhibitors. Strain BOH3 is capable of tolerating over 60 mM furfural, 60 mM hydroxymethylfurfural, and 6.6 mM vanillin, respectively, and is able to convert 53.74 ± 0.37 mM furfural into furfuryl alcohol within 90 h. The high furfural tolerance and its biotransformation by strain BOH3, which is correlated to the high transcription levels of two short-chain dehydrogenase/reductases, enable strain BOH3 to produce 5.15 ± 0.52 g/L butanol from dilute sulfuric acid pretreated horticultural waste hydrolysate (HWH) that bypassed the detoxification step. The capability of strain BOH3 to produce butanol from un-detoxified HWH lays the foundation of cost-effective biofuel production from lignocellulosic materials.

Residual stresses in high temperature corrosion of pure zirconium using elasto-viscoplastic model: Application to the deflection test in monofacial oxidation

NASA Astrophysics Data System (ADS)

Fettré, D.; Bouvier, S.; Favergeon, J.; Kurpaska, L.

2015-12-01

The paper is devoted to modeling residual stresses and strains in an oxide film formed during high temperature oxidation. It describes the deflection test in isothermal high-temperature monofacial oxidation (DTMO) of pure zirconium. The model incorporates kinetics and mechanism of oxidation and takes into account elastic, viscoplastic, growth and chemical strains. Different growth strains models are considered, namely, isotropic growth strains given by Pilling-Bedworth ratio, anisotropic growth strains defined by Parise and co-authors and physically based model for growth strain proposed by Clarke. Creep mechanisms based on dislocation slip and core diffusion, are used. A mechanism responsible for through thickness normal stress gradient in the oxide film is proposed. The material parameters are identified using deflection tests under 400 °C, 500 °C and 600 °C. The effect of temperature on creep and stress relaxation is analyzed. Numerical sensitivity study of the DTMO experiment is proposed in order to investigate the effects of the initial foil thickness and platinum coating on the deflection curves.

Epitaxial strain relaxation by provoking edge dislocation dipoles

NASA Astrophysics Data System (ADS)

Soufi, A.; El-Hami, K.

2018-02-01

Thin solid films have been used in various devices and engineering systems such as rapid development of highly integrated electronic circuits, the use of surface coatings to protect structural materials in high temperature environments, and thin films are integral parts of many micro-electro-mechanical systems designed to serve as sensors, actuators. Among techniques of ultra-thin films deposition, the heteroepitaxial method becomes the most useful at nanoscale level to obtain performed materials in various applications areas. On the other hand, stresses that appeared during the elaboration of thin films could rise deformations and fractures in materials. The key solution to solve this problem at the nanoscale level is the nucleation of interface dislocations from free surfaces. By provoking edge dislocation dipoles we obtained a strain relaxation in thin films. Moreover, the dynamic of nucleation in edge dislocations from free lateral surfaces was also studied.

A study on the strength of an armour-grade aluminum under high strain-rate loading

NASA Astrophysics Data System (ADS)

Appleby-Thomas, G. J.; Hazell, P. J.

2010-06-01

The aluminum alloy 5083 in tempers such as H32 and H131 is an established light-weight armour material. While its dynamic response under high strain-rates has been investigated elsewhere, little account of the effect of material orientation has been made. In addition, little information on its strength under such loadings is available in the literature. Here, both the longitudinal and lateral components of stress have been measured using embedded manganin stress gauges during plate-impact experiments on samples with the rolling direction aligned both orthogonal and parallel to the impact axis. The Hugoniot elastic limit, spall, and shear strengths were investigated for incident pressures in the range 1-8 GPa, providing an insight into the response of this alloy under shock loading. Further, the time dependence of lateral stress behind the shock front was investigated to give an indication of material response.

Submicron x-ray diffraction and its applications to problems in materials and environmental science

NASA Astrophysics Data System (ADS)

Tamura, N.; Celestre, R. S.; MacDowell, A. A.; Padmore, H. A.; Spolenak, R.; Valek, B. C.; Meier Chang, N.; Manceau, A.; Patel, J. R.

2002-03-01

The availability of high brilliance third generation synchrotron sources together with progress in achromatic focusing optics allows us to add submicron spatial resolution to the conventional century-old x-ray diffraction technique. The new capabilities include the possibility to map in situ, grain orientations, crystalline phase distribution, and full strain/stress tensors at a very local level, by combining white and monochromatic x-ray microbeam diffraction. This is particularly relevant for high technology industry where the understanding of material properties at a microstructural level becomes increasingly important. After describing the latest advances in the submicron x-ray diffraction techniques at the Advanced Light Source, we will give some examples of its application in material science for the measurement of strain/stress in metallic thin films and interconnects. Its use in the field of environmental science will also be discussed.

Effects of Heat Treatment on the Ballistic Impact Properties of Inconel 718 for Jet Engine Fan Containment Applications

NASA Technical Reports Server (NTRS)

Pereira, J. Michael; Lerch, Bradley A.

2001-01-01

The effects of heat treating Inconel 718 on the ballistic impact response and failure mechanisms were studied. Two different annealing conditions and an aged condition were considered. Large differences in the static properties were found between the annealed and the aged material, with the annealed condition having lower strength and hardness and greater elongation than the aged. High strain rate tests show similar results. Correspondingly large differences were found in the velocity required to penetrate material in the two conditions in impact tests involving 12.5 mm diameter, 25.4 mm long cylindrical Ti-6-4 projectiles impacting flat plates at velocities in the range of 150 to 300 m/sec. The annealed material was able to absorb over 25 percent more energy than the aged. This is contrary to results observed for ballistic impact response for higher velocity impacts typically encountered in military applications where it has been shown that there exists a correlation between target hardness and ballistic impact strength. Metallographic examination of impacted plates showed strong indication of failure due to adiabatic shear. In both materials localized bands of large shear deformation were apparent, and microhardness measurements indicated an increase in hardness in these bands compared to the surrounding material. These bands were more localized in the aged material than in the annealed material. In addition the annealed material underwent significantly greater overall deformation before failure. The results indicate that lower elongation and reduced strain hardening behavior lead to a transition from shear to adiabatic shear failure, while high elongation and better strain hardening capabilities reduce the tendency for shear to localize and result in an unstable adiabatic shear failure. This supports empirical containment design methods that relate containment thickness to the static toughness.

Effects of Heat Treatment on the Ballistic Impact Properties of Inconel 718 for Jet Engine Fan Containment Applications

NASA Technical Reports Server (NTRS)

Pereira, J. Michael; Lerch, Bradley A.

1999-01-01

The effects of heat treating Inconel 718 on the ballistic impact response and failure mechanisms were studied. Two different annealing conditions and an aged condition were considered. Large differences in the static properties were found between the annealed and the aged material, with the annealed condition having lower strength and hardness and greater elongation than the aged. High strain rate tests show similar results. Correspondingly large differences were found in the velocity required to penetrate material in the two conditions in impact tests involving 12.5 mm diameter, 25.4 mm long cylindrical Ti-6-4 projectiles impacting flat plates at velocities in the range of 150 to 300 m/sec. The annealed material was able to absorb over 25 percent more energy than the aged. This is contrary to results observed for ballistic impact response for higher velocity impacts typically encountered in military applications where it has been shown that there exists a correlation between target hardness and ballistic impact strength. Metallographic examination of impacted plates showed strong indication of failure due to adiabatic shear. In both materials localized bands of large shear deformation were apparent, and microhardness measurements indicated an increase in hardness in these bands compared to the surrounding material. These bands were more localized in the aged material than in the annealed material. In addition the annealed material underwent significantly greater overall deformation before failure. The results indicate that lower elongation and reduced strain hardening behavior lead to a transition from shear to adiabatic shear failure, while high elongation and better strain hardening capabilities reduce the tendency for shear to localize and result in an unstable adiabatic shear failure. This supports empirical containment design methods that relate containment thickness to the static toughness.

Effect of strain and deformation route on grain boundary characteristics and recrystallization behavior of aluminum

NASA Astrophysics Data System (ADS)

Sakai, Tetsuo; Utsunomiya, Hiroshi; Takahashi, Yasuo

2014-08-01

The effect of strain and deformation route on the recrystallization behavior of aluminum sheets has been investigated using well lubricated cold rolling and continuous equal channel angular extrusion. Three different deformation routes in plane strain corresponding to (1) simple shear, (2) compression, and (3) the combination of simple shear and compression were performed on 1100 aluminum sheet. Fixed amounts of the equivalent strain of 1.28 and 1.06 were accumulated in each route. In case of the combined deformation route, the ratio of shear strain to the total equivalent strain was varied. The recrystallized grain size was finer if the combined deformation route was employed instead of the monotonic route under the same amount of equivalent strain at either strain level. The density of high angle grain boundaries that act as nucleation sites for recrystallization was higher in materials deformed by the combined route. The orientation imaging micrographs revealed that the change in deformation route is effective for introducing a larger number of new high angle grain boundaries with relatively low misorientation angle.

Strain-cycling fatigue behavior of ten structural metals tested in liquid helium (4 K), in liquid nitrogen (78 K), and in ambient air (300 K)

NASA Technical Reports Server (NTRS)

Nachtigall, A. J.

1974-01-01

Strain-cycling fatigue behavior of 10 different structural alloys and metals was investigated in liquid helium (4 K), in liquid nitrogen (78 K), and in ambient air (300 K). At high cyclic lives, fatigue resistance increased with decreasing temperature for all the materials investigated. At low cyclic lives, fatigue resistance generally decreased with decreasing temperature for the materials investigated. Only for Inconel 718 did fatigue resistance increase with decreasing temperature over the entire life range investigated. Comparison of the experimental fatigue behavior with that predicted by the Manson method of universal slopes showed that the fatigue behavior of these materials can be predicted for cryogenic temperatures by using material tensile properties obtained at those same temperatures.

On the Processing of Spalling Experiments. Part I: Identification of the Dynamic Tensile Strength of Concrete

NASA Astrophysics Data System (ADS)

Forquin, P.; Lukić, B.

2017-11-01

The spalling technique based on the use of a single Hopkinson bar put in contact with the tested sample has been widely adopted as a reliable method for obtaining the tensile response of concrete and rock-like materials at strain rates up-to 200 s- 1. However, the traditional processing method, based on the use of Novikov acoustic approach and the rear face velocity measurement, remains quite questionable due to strong approximations of this data processing method. Recently a new technique for deriving cross-sectional stress fields of a spalling sample filmed with an ultra-high speed camera and based on using the full field measurements and the virtual fields method (VFM) was proposed. In the present work, this topic is perused by performing several spalling tests on ordinary concrete at high acquisition speed of 1Mfps to accurately measure the tensile strength, Young's modulus, strain-rate at failure and stress-strain response of concrete at high strain-rate. The stress-strain curves contain more measurement points for a more reliable identification. The observed tensile stiffness is up-to 50% lower than the initial compressive stiffness and the obtained peak stress was about 20% lower than the one obtained by applying the Novikov method. In order to support this claim, numerical simulations were performed to show that the change of stiffness between compression and tension highly affects the rear-face velocity profile. This further suggests that the processing based only on the velocity "pullback" is quite sensitive and can produce an overestimate of the tensile strength in concrete and rock-like materials.

Lightweight, compressible and electrically conductive polyurethane sponges coated with synergistic multiwalled carbon nanotubes and graphene for piezoresistive sensors.

PubMed

Ma, Zhonglei; Wei, Ajing; Ma, Jianzhong; Shao, Liang; Jiang, Huie; Dong, Diandian; Ji, Zhanyou; Wang, Qian; Kang, Songlei

2018-04-19

Lightweight, compressible and highly sensitive pressure/strain sensing materials are highly desirable for the development of health monitoring, wearable devices and artificial intelligence. Herein, a very simple, low-cost and solution-based approach is presented to fabricate versatile piezoresistive sensors based on conductive polyurethane (PU) sponges coated with synergistic multiwalled carbon nanotubes (MWCNTs) and graphene. These sensor materials are fabricated by convenient dip-coating layer-by-layer (LBL) electrostatic assembly followed by in situ reduction without using any complicated microfabrication processes. The resultant conductive MWCNT/RGO@PU sponges exhibit very low densities (0.027-0.064 g cm-3), outstanding compressibility (up to 75%) and high electrical conductivity benefiting from the porous PU sponges and synergistic conductive MWCNT/RGO structures. In addition, the MWCNT/RGO@PU sponges present larger relative resistance changes and superior sensing performances under external applied pressures (0-5.6 kPa) and a wide range of strains (0-75%) compared with the RGO@PU and MWCNT@PU sponges, due to the synergistic effect of multiple mechanisms: "disconnect-connect" transition of nanogaps, microcracks and fractured skeletons at low compression strain and compressive contact of the conductive skeletons at high compression strain. The electrical and piezoresistive properties of MWCNT/RGO@PU sponges are strongly associated with the dip-coating cycle, suspension concentration, and the applied pressure and strain. Fully functional applications of MWCNT/RGO@PU sponge-based piezoresistive sensors in lighting LED lamps and detecting human body movements are demonstrated, indicating their excellent potential for emerging applications such as health monitoring, wearable devices and artificial intelligence.

Experimental stress analysis of large plastic deformations in a hollow sphere deformed by impact against a concrete block

NASA Technical Reports Server (NTRS)

Morris, R. E.

1973-01-01

An experimental plastic strain measurement system is presented for use on the surface of high velocity impact test models. The system was used on a hollow sphere tested in impact against a reinforced concrete block. True strains, deviatoric stresses, and true stresses were calculated from experimental measurements. The maximum strain measured in the model was small compared to the true failure strain obtained from static tensile tests of model material. This fact suggests that a much greater impact velocity would be required to cause failure of the model shell structure.

Hostile environments and high temperature measurements; Proceedings of the Conference, Kansas City, MO, Nov. 6-8, 1989

NASA Astrophysics Data System (ADS)

Topics presented include the identification of stagnant region in a fluidized bed combustor, high sensitivity objective grating speckle, an X-ray beam method for displacement and strain distributions using the moire method, and high-temperature deformation of a Ti-alloy composite under complex loading. Also addressed are a hybrid procedure for dynamic characterization of ceramics at elevated temperature, thermo-structural measurements in a SiC coated carbon-carbon hypersonic glide vehicle, and recent experience with elevated-temperature foil strain gages with application to thin-gage materials.

Deformation field heterogeneity in punch indentation

PubMed Central

Murthy, Tejas G.; Saldana, Christopher; Hudspeth, Matthew; M'Saoubi, Rachid

2014-01-01

Plastic heterogeneity in indentation is fundamental for understanding mechanics of hardness testing and impression-based deformation processing methods. The heterogeneous deformation underlying plane-strain indentation was investigated in plastic loading of copper by a flat punch. Deformation parameters were measured, in situ, by tracking the motion of asperities in high-speed optical imaging. These measurements were coupled with multi-scale analyses of strength, microstructure and crystallographic texture in the vicinity of the indentation. Self-consistency is demonstrated in description of the deformation field using the in situ mechanics-based measurements and post-mortem materials characterization. Salient features of the punch indentation process elucidated include, among others, the presence of a dead-metal zone underneath the indenter, regions of intense strain rate (e.g. slip lines) and extent of the plastic flow field. Perhaps more intriguing are the transitions between shear-type and compression-type deformation modes over the indentation region that were quantified by the high-resolution crystallographic texture measurements. The evolution of the field concomitant to the progress of indentation is discussed and primary differences between the mechanics of indentation for a rigid perfectly plastic material and a strain-hardening material are described. PMID:24910521

Experiment and Modeling of Simultaneous Creep, Plasticity and Transformation of High Temperature Shape Memory Alloys During Cyclic Actuation

NASA Technical Reports Server (NTRS)

Kumar, Parikshith K.; Desai, Uri; Chatzigeorgiou, George; Lagoudas, Dimitris C.; Monroe, James; Karaman, Ibrahim; Noebe, Ron; Bigelow, Glen

2010-01-01

The present work is focused on studying the cycling actuation behavior of HTSMAs undergoing simultaneous creep and transformation. For the thermomechanical testing, a high temperature test setup was assembled on a MTS frame with the capability to test up to temperatures of 600 C. Constant stress thermal cycling tests were conducted to establish the actuation characteristics and the phase diagram for the chosen HTSMA. Additionally, creep tests were conducted at constant stress levels at different test temperatures to characterize the creep behavior of the alloy over the operational range. A thermodynamic constitutive model is developed and extended to take into account a) the effect of multiple thermal cycling on the generation of plastic strains due to transformation (TRIP strains) and b) both primary and secondary creep effects. The model calibration is based on the test results. The creep tests and the uniaxial tests are used to identify the viscoplastic behavior of the material. The parameters for the SMA properties, regarding the transformation and transformation induced plastic strain evolutions, are obtained from the material phase diagram and the thermomechanical tests. The model is validated by predicting the material behavior at different thermomechanical test conditions.

High rate constitutive modeling of aluminium alloy tube

NASA Astrophysics Data System (ADS)

Salisbury, C. P.; Worswick, M. J.; Mayer, R.

2006-08-01

As the need for fuel efficient automobiles increases, car designers are investigating light-weight materials for automotive bodies that will reduce the overall automobile weight. Aluminium alloy tube is a desirable material to use in automotive bodies due to its light weight. However, aluminium suffers from lower formability than steel and its energy absorption ability in a crash event after a forming operation is largely unknown. As part of a larger study on the relationship between crashworthiness and forming processes, constitutive models for 3mm AA5754 aluminium tube were developed. A nominal strain rate of 100/s is often used to characterize overall automobile crash events, whereas strain rates on the order of 1000/s can occur locally. Therefore, tests were performed at quasi-static rates using an Instron test fixture and at strain rates of 500/s to 1500/s using a tensile split Hopkinson bar. High rate testing was then conducted at rates of 500/s, 1000/s and 1500/s at 21circC, 150circC and 300circC. The generated data was then used to determine the constitutive parameters for the Johnson-Cook and Zerilli-Armstrong material models.

Using plastic instability to validate and test the strength law of a material under pressure

NASA Astrophysics Data System (ADS)

Bolis, Cyril; Counilh, Denis; Savale, Brice

2015-09-01

In dynamical experiments (pressures higher than 10 GPa, strain rate around 104-106 s-1), metals are classically described using an equation of state and a strength law which is usually set using data from compression or traction tests at low pressure (few MPa) and low strain rates (less than 103 s-1). In consequence, it needs to be extrapolated during dynamical experiments. Classical shock experiments do not allow a fine validation of the stress law due to the interaction with the equation of state. To achieve this aim, we propose to use a dedicated experiment. We started from the works of Barnes et al. (1974 and 1980) where plastic instabilities initiated by a sinusoidal perturbation at the surface of the metal develop with the pressure. We adapted this principle to a new shape of initial perturbation and realized several experiments. We will present the setup and its use on a simple material: gold. We will detail how the interpretation of the experiments, coupled with previous characterization experiments helps us to test the strength lax of this material at high pressure and high strain rate.

Thin Film Sensors for Surface Measurements

NASA Technical Reports Server (NTRS)

Martin, Lisa C.; Wrbanek, John D.; Fralick, Gustave C.

2001-01-01

Advanced thin film sensors that can provide accurate surface temperature, strain, and heat flux measurements have been developed at NASA Glenn Research Center. These sensors provide minimally intrusive characterization of advanced propulsion materials and components in hostile, high-temperature environments as well as validation of propulsion system design codes. The sensors are designed for applications on different material systems and engine components for testing in engine simulation facilities. Thin film thermocouples and strain gauges for the measurement of surface temperature and strain have been demonstrated on metals, ceramics and advanced ceramic-based composites of various component configurations. Test environments have included both air-breathing and space propulsion-based engine and burner rig environments at surface temperatures up to 1100 C and under high gas flow and pressure conditions. The technologies developed for these sensors as well as for a thin film heat flux gauge have been integrated into a single multifunctional gauge for the simultaneous real-time measurement of surface temperature, strain, and heat flux. This is the first step toward the development of smart sensors with integrated signal conditioning and high temperature electronics that would have the capability to provide feedback to the operating system in real-time. A description of the fabrication process for the thin film sensors and multifunctional gauge will be provided. In addition, the material systems on which the sensors have been demonstrated, the test facilities and the results of the tests to-date will be described. Finally, the results will be provided of the current effort to demonstrate the capabilities of the multifunctional gauge.

Mechanical Behavior of a Low-Cost Ti-6Al-4V Alloy

NASA Astrophysics Data System (ADS)

Casem, D. T.; Weerasooriya, T.; Walter, T. R.

2018-01-01

Mechanical compression tests were performed on an economical Ti-6Al-4V alloy over a range of strain-rates and temperatures. Low rate experiments (0.001-0.1/s) were performed with a servo-hydraulic load frame and high rate experiments (1000-80,000/s) were performed with the Kolsky bar (Split Hopkinson pressure bar). Emphasis is placed on the large strain, high-rate, and high temperature behavior of the material in an effort to develop a predictive capability for adiabatic shear bands. Quasi-isothermal experiments were performed with the Kolsky bar to determine the large strain response at elevated rates, and bars with small diameters (1.59 mm and 794 µm, instrumented optically) were used to study the response at the higher strain-rates. Experiments were also conducted at temperatures ranging from 81 to 673 K. Two constitutive models are used to represent the data. The first is the Zerilli-Armstrong recovery strain model and the second is a modified Johnson-Cook model which uses the recovery strain term from the Zerilli-Armstrong model. In both cases, the recovery strain feature is critical for capturing the instability that precedes localization.

FUNDAMENTAL PROPERTIES OF ULTRA HIGH PERFORMANCE-STRAIN HARDENING CEMENTITIOUS COMPOSITES AND USAGE FOR REPAIR

NASA Astrophysics Data System (ADS)

Kunieda, Minoru; Shimizu, Kosuke; Eguchi, Teruyuki; Ueda, Naoshi; Nakamura, Hikaru

This paper presents the fundamental properties of Ultra High Performance-Strain Hardening Cementitious Composites (UHP-SHCC), which were depeloped for repair applications. In particular, mechanical properties such as tensile response, shrinkage and bond strength were investigated experimentally. Protective performance of the material such as air permeability, water permeability and penetration of chloride ion was also confirmed comparing to that of ordinary concrete. This paper also introduces the usage of the material in repair of concrete st ructures. Laboratory tests concerining the deterioration induced by corrosion were conducted. The UHP-SHCC that coverd the RC beam resisted not only crack opening along the rebar due to corrosion but also crack opening due to loading tests.

High spatial resolution grain orientation and strain mapping in thin films using polychromatic submicron x-ray diffraction

NASA Astrophysics Data System (ADS)

Tamura, N.; MacDowell, A. A.; Celestre, R. S.; Padmore, H. A.; Valek, B.; Bravman, J. C.; Spolenak, R.; Brown, W. L.; Marieb, T.; Fujimoto, H.; Batterman, B. W.; Patel, J. R.

2002-05-01

The availability of high brilliance synchrotron sources, coupled with recent progress in achromatic focusing optics and large area two-dimensional detector technology, has allowed us to develop an x-ray synchrotron technique that is capable of mapping orientation and strain/stress in polycrystalline thin films with submicron spatial resolution. To demonstrate the capabilities of this instrument, we have employed it to study the microstructure of aluminum thin film structures at the granular and subgranular levels. Due to the relatively low absorption of x-rays in materials, this technique can be used to study passivated samples, an important advantage over most electron probes given the very different mechanical behavior of buried and unpassivated materials.

Achieving large linear elasticity and high strength in bulk nanocompsite via synergistic effect

DOE PAGES

Hao, Shijie; Cui, Lishan; Guo, Fangmin; ...

2015-03-09

Elastic strain in bulk metallic materials is usually limited to only a fraction of 1%. Developing bulk metallic materials showing large linear elasticity and high strength has proven to be difficult. Here, based on the synergistic effect between nanowires and orientated martensite NiTi shape memory alloy, we developed an in-situ Nb nanowires-orientated martensitic NiTi matrix composite showing an ultra-large linear elastic strain of 4% and an ultrahigh yield strength of 1.8 GPa. This material also has a high mechanical energy storage efficiency of 96% and a high energy storage density of 36 J/cm 3 that is almost one order ofmore » larger than that of spring steel. It is demonstrated that the synergistic effect allows the exceptional mechanical properties of nanowires to be harvested at macro scale and the mechanical properties of matrix to be greatly improved, resulting in these superior properties. This research provides new avenues for developing advanced composites with superior properties by using effective synergistic effect between components.« less

Polymeric Helical Microactuators: Achieving High Speed and High Extension.

NASA Astrophysics Data System (ADS)

Kim, Yongjin; Crosby, Alfred

We proposed novel concepts of actuation mechanism and fabrication method to induce fast and highly extensional motion in polymeric actuators. Exceptionally high extensional strain over 1400% was realized by the geometric transformation from a helix to a stretched ribbon in a responsive and reversible manner. As a model system, sub-micron sized helices were fabricated from a self-assembled, UV-cured, thermo-responsive polymer. By controlling the size and the geometrical asymmetries in the system, a combined effect of surface tension and differential volumetric strain during the transition between swollen-deswollen state induced by phase transition of the material was successfully utilized to generate torsional stresses in the system. For the full understanding of the results, a finite element analysis and measurements on the poroelastic properties of the material were conducted as well as a demonstration on macroscopic system made with PDMS. Finally, remaining questions on the chirality of helices were presented. This material is based upon work supported by, or in part by, the U. S. Army Research Laboratory and the U. S. Army Research Office under contract/Grant Number W911NF-15-1-0358.

Dynamic tensile fracture of mortar at ultra-high strain-rates

DOE Office of Scientific and Technical Information (OSTI.GOV)

Erzar, B., E-mail: benjamin.erzar@cea.fr; Buzaud, E.; Chanal, P.-Y.

2013-12-28

During the lifetime of a structure, concrete and mortar may be exposed to highly dynamic loadings, such as impact or explosion. The dynamic fracture at high loading rates needs to be well understood to allow an accurate modeling of this kind of event. In this work, a pulsed-power generator has been employed to conduct spalling tests on mortar samples at strain-rates ranging from 2 × 10{sup 4} to 4 × 10{sup 4} s{sup −1}. The ramp loading allowed identifying the strain-rate anytime during the test. A power law has been proposed to fit properly the rate-sensitivity of tensile strength of thismore » cementitious material over a wide range of strain-rate. Moreover, a specimen has been recovered damaged but unbroken. Micro-computed tomography has been employed to study the characteristics of the damage pattern provoked by the dynamic tensile loading.« less

Impact deformation behavior of duplex and superaustenitic stainless steels welds by split Hopkinson pressure bar

NASA Astrophysics Data System (ADS)

Wang, Shing-Hoa; Huang, Chih-Sheng; Lee, Woei-Shyan; Chen, Tao-Hsing; Wu, Chia-Chang; Lien, Charles; Tsai, Hung-Yin

2009-12-01

A considerable volume of γ phase increases in the fusion zone (weld metal) for two duplex stainless steels after a high-strain-rate impact. The strain-induced γ phase formation in the fusion zone results in local hardness variation depending on the strain rate. The α phase content in the fusion zone decreases as the impact strain rate increases for SAF 2205 DSS and SAF 2507 DSS. The results of the two-phase content measured by Ferritoscope correspond to that assessed by image analyses. In contrast, superaustenite stainless steel is unaffected by such an impact owing to its fully stable austenization. Impacted welds at a high strain rate of 5 × 103 s-1 reveal feather-like surface creases along the solidified curved columnar grain boundaries. The apparent surface creases are formed due to the presence of diffuse Lüders bands, which are caused by heavy plastic deformation in coarse-grain materials.

A potential drop strain sensor for in-situ power station creep monitoring

NASA Astrophysics Data System (ADS)

Corcoran, Joseph; Cawley, Peter; Nagy, Peter B.

2014-02-01

Creep is a high temperature damage mechanism of interest to the power industry and at present lacks a satisfactory inspection technique. Existing material inspection techniques are extremely laborious while strain measurements rely on often infrequent off-load measurements. A quasi-DC directional potential drop technique has been suggested that is able to suppress the effects of permeability and is primarily sensitive to changes in resistivity and also the geometry that will develop through strain. The change in creep related resistivity is shown by an equivalent effective resistivity approach to be small at <2% change when compared to the >100% change in transfer resistance that occurs due to strain as observed in laboratory tests. A biaxial inversion is then presented and demonstrated on in-lab samples showing good performance. The result is a sensor that performs as a very robust high temperature strain gauge.

Intergranular stress study of TC11 titanium alloy after laser shock peening by synchrotron-based high-energy X-ray diffraction

NASA Astrophysics Data System (ADS)

Su, R.; Li, L.; Wang, Y. D.; Nie, Z. H.; Ren, Y.; Zhou, X.; Wang, J.

2018-05-01

The distribution of residual lattice strain as a function of depth were carefully investigated by synchrotron-based high energy X-ray diffraction (HEXRD) in TC11 titanium alloy after laser shock peening (LSP). The results presented big compressive residual lattice strains at surface and subsurface, then tensile residual lattice strains in deeper region, and finally close to zero lattice strains in further deep interior with no plastic deformation thereafter. These evolutions in residual lattice strains were attributed to the balance of direct load effect from laser shock wave and the derivative restriction force effect from surrounding material. Significant intergranular stress was evidenced in the processed sample. The intergranular stress exhibited the largest value at surface, and rapidly decreased with depth increase. The magnitude of intergranular stress was proportional to the severity of the plastic deformation caused by LSP. Two shocks generated larger intergranular stress than one shock.

Bulk & Interfacial Contributions to the Adhesion of Acrylic Emulsion-Based Pressure Sensitive Adhesives

NASA Astrophysics Data System (ADS)

Wang, Qifeng

The performance of pressure sensitive adhesives (PSAs) depends strongly on the viscoelastic properties of the adhesive material itself and the surface that it is placed into contact with. In this work we use a multiple- oscillatory test with microindentation apparatus that is able to quantify the mechanical response of adhesive materials in the linear regime, and also in the highly strained regime where the adhesive layer has cavitated to form mechanically isolated brils. The experiments involved the use of hemispherical indenters made of glass or polyethylene, brought into contact with a thin adhesive layer and then retracted, with comprehensive displacement history. A set of model acrylic emulsion-based PSAs were used in the experiments which show a suprising degree of elastic character at high strain. The experiment result suggest that an adhesive failure criterion based on the stored elastic energy is appropriate for these systems. The primary effect of the substrate is to modify the maximum strain where adhesive detachment from the indenter occurs.

Model For Bending Actuators That Use Electrostrictive Graft Elastomers

NASA Technical Reports Server (NTRS)

Costen, Robert C.; Su, Ji; Harrison, Joycelyn S.

2001-01-01

Recently, it was reported that an electrostrictive graft elastomer exhibits large electric field-induced strain (4%). Combined with its high mechanical modulus, the elastomer can offer very promising electromechanical properties, in terms of output mechanical energy density, for an electroactive polymeric material. Therefore, it has been considered as one of the candidates that can be used in high performance, low mass actuation devices in many aerospace applications. Various bilayer- based bending actuators have been designed and fabricated. An analytic model based on beam theory in the strength of materials has been derived for the transverse deflection, or curvature, and the longitudinal strain of the bi-layer beam. The curvature and strain are functions of the applied voltage and the thickness, width, and Young s modulus of the active and passive layers. The model can be used to optimize the performance of electrostrictive graft elastomer-based actuators to meet the requirements of various applications. In this presentation, optimization and sensitivity studies are applied to the bending performance of such actuators.

Formation of Highly Twisted Ribbons in a Carboxymethylcellulase Gene-Disrupted Strain of a Cellulose-Producing Bacterium

PubMed Central

Sugano, Yasushi; Shoda, Makoto; Sakakibara, Hitoshi; Oiwa, Kazuhiro; Tuzi, Satoru; Imai, Tomoya; Sugiyama, Junji; Takeuchi, Miyuki; Yamauchi, Daisuke

2013-01-01

Cellulases are enzymes that normally digest cellulose; however, some are known to play essential roles in cellulose biosynthesis. Although some endogenous cellulases of plants and cellulose-producing bacteria are reportedly involved in cellulose production, their functions in cellulose production are unknown. In this study, we demonstrated that disruption of the cellulase (carboxymethylcellulase) gene causes irregular packing of de novo-synthesized fibrils in Gluconacetobacter xylinus, a cellulose-producing bacterium. Cellulose production was remarkably reduced and small amounts of particulate material were accumulated in the culture of a cmcax-disrupted G. xylinus strain (F2-2). The particulate material was shown to contain cellulose by both solid-state 13C nuclear magnetic resonance analysis and Fourier transform infrared spectroscopy analysis. Electron microscopy revealed that the cellulose fibrils produced by the F2-2 cells were highly twisted compared with those produced by control cells. This hypertwisting of the fibrils may reduce cellulose synthesis in the F2-2 strains. PMID:23243308

Finite element analysis of residual stress field induced by laser shock peening

NASA Astrophysics Data System (ADS)

Nam, Taeksun

The finite element method is applied to analyze the laser shock peening process (LSP) for thick parts (considered as a semi-infinite half space) and thin parts (finite thickness domain). The technology of LSP is used to enhance mechanical properties such as fatigue life, fretting fatigue life, resistance to stress corrosion cracking and surface hardness. These enhanced material properties are directly related to the magnitude and distribution of the plastic strain and associated residual stresses due to shockwaves induced by LSP. To reduce the process development cost and time, the prediction of residual stress field is very useful to provide a base design guideline for selecting appropriate LSP conditions for evaluation. An axisymmetric Finite Element Analysis (FEA) code, named SHOCKWAVE, is developed in order to complement shortcomings of applying commercial FEA codes at extremely high strain rates (as high as 104 -106/sec). The rate dependent plasticity theory is applied along with the small strain assumption. The solution process consists of an explicit dynamic loading analysis for shock loading stage and a static unloading analysis (implicit) to determine the equilibrium state for the residual stress and plastic strain fields. Some of the highlights explored in this investigation entail: (i) overstress power law models for the rate dependence, (ii) various hardening models, (iii) a second-order accurate implicit algorithm for the plastic consistency condition, (iv) an adaptively expanding domain scheme to trace the stress-free boundary condition in a simple way, (v) a special uniform meshing scheme to avoid the usual assembly process and repeated calculations for the stiffness matrix, (vi) mesh sensitivity study, (vii) comparisons with measured data provided and supported by the LSP Technologies, Inc. The dynamic behavior of Ti-6Al-4V at high strain rates can be investigated by using the split torsional Hopkinson bar experiment and by a longitudinal shock loading simulation in uniaxial strain to obtain material parameters representing rate dependent plasticity. In case of the double-sided laser peening for a thin part, reversal in loading plays a significant role. The stress waves repeatedly recompose the pre-accumulated plastic strains because of the interaction of the primary and reflected stress waves. In an attempt to better represent the material behavior under repeated reversals and collapses in loading, a sequence of bend-reverse bend tests is performed to identify the material parameters of TI-6Al-4V needed for a nonlinear kinematic hardening model (Chaboche model). For a thick part (a semi-infinite domain), single shot as well as multiple shots (at the same location) cases are simulated and compared with measured data for two different loading magnitudes and three different hardening models. Some of the simulation results agree well with the measured data, depending on the choice of hardening model and the treatment of rate dependent material behavior at high strain rates. Only a single shot (on both sides) case is investigated for a thin part (a finite thickness domain) in terms of residual stress distribution. The disagreement between the computed results and the measured data is more pronounced in this case, needing further investigations on both sides of the fields.

The Impact Response of Composite Materials Involved in Helicopter Vulnerability Assessment: Literature Review - Part 1

DTIC Science & Technology

2006-04-01

contraction) caused by a load when deforming the material; which takes the form of a stress-strain curve . The stress- strain curve is the key information...anisotropy associated with large variability of the mechanical properties of its constituents. Therefore, every experimental stress-strain curve for...these materials is closely associated with the load direction with respect to the material symmetry axes. Under static conditions, stress-strain curves

Impact compaction of a granular material

DOE PAGES

Fenton, Gregg; Asay, Blaine; Dalton, Devon

2015-05-19

The dynamic behavior of granular materials has importance to a variety of engineering applications. Structural seismic coupling, planetary science, and earth penetration mechanics, are just a few of the application areas. Although the mechanical behavior of granular materials of various types have been studied extensively for several decades, the dynamic behavior of such materials remains poorly understood. High-quality experimental data are needed to improve our general understanding of granular material compaction physics. This study will describe how an instrumented plunger impact system can be used to measure pressure-density relationships for model materials at high and controlled strain rates and subsequentlymore » used for computational modeling.« less

Nanocomposite Strain Gauges Having Small TCRs

NASA Technical Reports Server (NTRS)

Gregory, Otto; Chen, Ximing

2009-01-01

Ceramic strain gauges in which the strain-sensitive electrically conductive strips made from nanocomposites of noble metal and indium tin oxide (ITO) are being developed for use in gas turbine engines and other power-generation systems in which gas temperatures can exceed 1,500 F (about 816 C). In general, strain gauges exhibit spurious thermally induced components of response denoted apparent strain. When temperature varies, a strain-gauge material that has a nonzero temperature coefficient of resistance (TCR) exhibits an undesired change in electrical resistance that can be mistaken for the change in resistance caused by a change in strain. It would be desirable to formulate straingauge materials having TCRs as small as possible so as to minimize apparent strain. Most metals exhibit positive TCRs, while most semiconductors, including ITO, exhibit negative TCRs. The present development is based on the idea of using the negative TCR of ITO to counter the positive TCRs of noble metals and of obtaining the benefit of the ability of both ITO and noble metals to endure high temperatures. The noble metal used in this development thus far has been platinum. Combinatorial libraries of many ceramic strain gauges containing nanocomposites of various proportions of ITO and platinum were fabricated by reactive co-sputtering from ITO and platinum targets onto alumina- and zirconia-based substrates mounted at various positions between the targets.

In-Plane Heterostructures Enable Internal Stress Assisted Strain Engineering in 2D Materials.

PubMed

Liu, Feng; Wang, Tzu-Chiang; Tang, Qiheng

2018-04-01

Conventional methods to induce strain in 2D materials can hardly catch up with the sharp increase in requirements to design specific strain forms, such as the pseudomagnetic field proposed in graphene, funnel effect of excitons in MoS 2 , and also the inverse funnel effect reported in black phosphorus. Therefore, a long-standing challenge in 2D materials strain engineering is to find a feasible scheme that can be used to design given strain forms. In this article, combining the ability of experimentally synthetizing in-plane heterostructures and elegant Eshelby inclusion theory, the possibility of designing strain fields in 2D materials to manipulate physical properties, which is called internal stress assisted strain engineering, is theoretically demonstrated. Particularly, through changing the inclusion's size, the stress or strain gradient can be controlled precisely, which is never achieved. By taking advantage of it, the pseudomagnetic field as well as the funnel effect can be accurately designed, which opens an avenue to practical applications for strain engineering in 2D materials. © 2018 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Strain-tuned optoelectronic properties of hollow gallium sulphide microspheres

NASA Astrophysics Data System (ADS)

Zhang, Yin; Chen, Chen; Liang, C. Y.; Liu, Z. W.; Li, Y. S.; Che, Renchao

2015-10-01

Sulfide semiconductors have attracted considerable attention. The main challenge is to prepare materials with a designable morphology, a controllable band structure and optoelectronic properties. Herein, we report a facile chemical transportation reaction for the synthesis of Ga2S3 microspheres with novel hollow morphologies and partially filled volumes. Even without any extrinsic dopant, photoluminescence (PL) emission wavelength could be facilely tuned from 635 to 665 nm, depending on its intrinsic inhomogeneous strain distribution. Geometric phase analysis (GPA) based on high-resolution transmission electron microscopy (HRTEM) imaging reveals that the strain distribution and the associated PL properties can be accurately controlled by changing the growth temperature gradient, which depends on the distance between the boats used for raw material evaporation and microsphere deposition. The stacking-fault density, lattice distortion degree and strain distribution at the shell interfacial region of the Ga2S3 microspheres could be readily adjusted. Ab initio first-principles calculations confirm that the lowest conductive band (LCB) is dominated by S-3s and Ga-4p states, which shift to the low-energy band as a result of the introduction of tensile strain, well in accordance with the observed PL evolution. Therefore, based on our strain driving strategy, novel guidelines toward the reasonable design of sulfide semiconductors with tunable photoluminescence properties are proposed.Sulfide semiconductors have attracted considerable attention. The main challenge is to prepare materials with a designable morphology, a controllable band structure and optoelectronic properties. Herein, we report a facile chemical transportation reaction for the synthesis of Ga2S3 microspheres with novel hollow morphologies and partially filled volumes. Even without any extrinsic dopant, photoluminescence (PL) emission wavelength could be facilely tuned from 635 to 665 nm, depending on its intrinsic inhomogeneous strain distribution. Geometric phase analysis (GPA) based on high-resolution transmission electron microscopy (HRTEM) imaging reveals that the strain distribution and the associated PL properties can be accurately controlled by changing the growth temperature gradient, which depends on the distance between the boats used for raw material evaporation and microsphere deposition. The stacking-fault density, lattice distortion degree and strain distribution at the shell interfacial region of the Ga2S3 microspheres could be readily adjusted. Ab initio first-principles calculations confirm that the lowest conductive band (LCB) is dominated by S-3s and Ga-4p states, which shift to the low-energy band as a result of the introduction of tensile strain, well in accordance with the observed PL evolution. Therefore, based on our strain driving strategy, novel guidelines toward the reasonable design of sulfide semiconductors with tunable photoluminescence properties are proposed. Electronic supplementary information (ESI) available: Crystal structure pattern; calculated DOS diagram. See DOI: 10.1039/c5nr05528h

Improvement of Reusable Surface Insulation (RSI) materials

NASA Technical Reports Server (NTRS)

Blome, J. C.

1972-01-01

The mullite fiber based hardened compacted fibers (HCF) type of reusable surface insulation was further developed for use in the Space Shuttle Program. Two hundred fifty formulations of fiber mixtures, fillers, binders, and organic processing aids were made using mullite fibers as the basic ingredient. Most of the work was accomplished on 15-lb/cu ft material. It was established that higher density materials are stronger with strength values as high as 250 lb/sq in. in tension. New measurement techniques and equipment were developed for accurate determination of strength and strain to failure. Room temperature to 2300 F stress-strain relationships were made. The room temperature tensile modulus of elasticity is 61,700 lb/sq in. and the strain at failure is 0.165 percent, typically, when measured longitudinally parallel to the long axes of the fibers. Thermal insulating effectiveness was increased 20 percent by reducing the diameter of some of the fibers in the material. Improvements were made in density uniformity and strength uniformity in a block of HCF by mixing improvements and by the use of organic additives. Specifications were established on the materials and processes used in making the insulation.

Relationship between fatigue life in the creep-fatigue region and stress-strain response

NASA Technical Reports Server (NTRS)

Berkovits, A.; Nadiv, S.

1988-01-01

On the basis of mechanical tests and metallographic studies, strainrange partitioned lives were predicted by introducing stress-strain materials parameters into the Universal Slopes Equation. This was the result of correlating fatigue damage mechanisms and deformation mechanisms operating at elevated temperatures on the basis of observed mechanical and microstructural behavior. Correlation between high temperature fatigue and stress strain properties for nickel base superalloys and stainless steel substantiated the method. Parameters which must be evaluated for PP- and CC- life are the maximum stress achievable under entirely plastic and creep conditions respectively and corresponding inelastic strains, and the two more pairs of stress strain parameters must be ascertained.

Mechanical Properties of Elastomeric Impression Materials: An In Vitro Comparison

PubMed Central

De Angelis, Francesco; Caputi, Sergio; D'Amario, Maurizio; D'Arcangelo, Camillo

2015-01-01

Purpose. Although new elastomeric impression materials have been introduced into the market, there are still insufficient data about their mechanical features. The tensile properties of 17 hydrophilic impression materials with different consistencies were compared. Materials and Methods. 12 vinylpolysiloxane, 2 polyether, and 3 hybrid vinylpolyether silicone-based impression materials were tested. For each material, 10 dumbbell-shaped specimens were fabricated (n = 10), according to the ISO 37:2005 specifications, and loaded in tension until failure. Mean values for tensile strength, yield strength, strain at break, and strain at yield point were calculated. Data were statistically analyzed using one-way ANOVA and Tukey's tests (α = 0.05). Results. Vinylpolysiloxanes consistently showed higher tensile strength values than polyethers. Heavy-body materials showed higher tensile strength than the light bodies from the same manufacturer. Among the light bodies, the highest yield strength was achieved by the hybrid vinylpolyether silicone (2.70 MPa). Polyethers showed the lowest tensile (1.44 MPa) and yield (0.94 MPa) strengths, regardless of the viscosity. Conclusion. The choice of an impression material should be based on the specific physical behavior of the elastomer. The light-body vinylpolyether silicone showed high tensile strength, yield strength, and adequate strain at yield/brake; those features might help to reduce tearing phenomena in the thin interproximal and crevicular areas. PMID:26693227

Rate- and Temperature-Dependent Material Behavior of a Multilayer Polymer Battery Separator

NASA Astrophysics Data System (ADS)

Avdeev, Ilya; Martinsen, Michael; Francis, Alex

2014-01-01

Designing battery packs for safety in automotive applications requires multiscale modeling, as macroscopic deformations due to impact cause the mechanical failure of individual cells on a sub-millimeter level. The separator material plays a critical role in this process, as the thinning or perforating of the separator can lead to thermal runaway and catastrophic failure of an entire battery pack. The electrochemical properties of various polymer separators have been extensively investigated; however, the dependency of mechanical properties of these thin films on various factors, such as high temperature and strain rate, has not been sufficiently characterized. In this study, the macroscopic mechanical properties of a multilayer polymer thin film used as a battery separator are studied experimentally at various temperatures, strain rates, and solvent saturations. Due to the anisotropy of the material, material testing was conducted in two perpendicular directions (machine and transverse directions). Material samples were tested in both dry and saturated conditions at several temperatures, and it was found that temperature and strain rate have a nearly linear effect on the stress experienced by the material. Additionally, saturating the separator material in a common lithium-ion solvent had softened it and had a positive effect on its toughness. The experimental results obtained in this study can be used to develop mathematical constitutive models of the multilayer separator material for subsequent numerical simulations and design.

Stability of surface plastic flow in large strain deformation of metals

NASA Astrophysics Data System (ADS)

Viswanathan, Koushik; Udapa, Anirduh; Sagapuram, Dinakar; Mann, James; Chandrasekar, Srinivasan

We examine large-strain unconstrained simple shear deformation in metals using a model two-dimensional cutting system and high-speed in situ imaging. The nature of the deformation mode is shown to be a function of the initial microstructure state of the metal and the deformation geometry. For annealed metals, which exhibit large ductility and strain hardening capacity, the commonly assumed laminar flow mode is inherently unstable. Instead, the imposed shear is accommodated by a highly rotational flow-sinuous flow-with vortex-like components and large-amplitude folding on the mesoscale. Sinuous flow is triggered by a plastic instability on the material surface ahead of the primary region of shear. On the other hand, when the material is extensively strain-hardened prior to shear, laminar flow again becomes unstable giving way to shear banding. The existence of these flow modes is established by stability analysis of laminar flow. The role of the initial microstructure state in determining the change in stability from laminar to sinuous / shear-banded flows in metals is elucidated. The implications for cutting, forming and wear processes for metals, and to surface plasticity phenomena such as mechanochemical Rehbinder effects are discussed.

Short-period cyclic loading system for in situ X-ray observation of anelastic properties at high pressure.

PubMed

Yoshino, Takashi; Yamazaki, Daisuke; Tange, Yoshinori; Higo, Yuji

2016-10-01

To determine the anelastic properties of materials of the Earth's interior, a short-period cyclic loading system was installed for in situ X-ray radiographic observation under high pressure to the multi-anvil deformation DIA press at the bending magnet beam line BL04B1 at SPring-8. The hydraulic system equipped with a piston controlled by a solenoid was designed so as to enable producing smooth sinusoidal stress in a wide range of oscillation period from 0.2 to 100 s and generating variable amplitudes. Time resolved X-ray radiography imaging of the sample and reference material provides their strain as a function of time during cyclic loading. A synchrotron X-ray radiation source allows us to resolve their strain variation with time even at the short period (<1 s). The minimum resolved strain is as small as 10 -4 , and the shortest oscillation period to detect small strain is 0.5 s. Preliminary experimental results exhibited that the new system can resolve attenuation factor Q -1 at upper mantle conditions. These results are in quantitative agreement with previously reported data obtained at lower pressures.

Stretchable and reversibly deformable radio frequency antennas based on silver nanowires.

PubMed

Song, Lingnan; Myers, Amanda C; Adams, Jacob J; Zhu, Yong

2014-03-26

We demonstrate a class of microstrip patch antennas that are stretchable, mechanically tunable, and reversibly deformable. The radiating element of the antenna consists of highly conductive and stretchable material with screen-printed silver nanowires embedded in the surface layer of an elastomeric substrate. A 3-GHz microstrip patch antenna and a 6-GHz 2-element patch array are fabricated. Radiating properties of the antennas are characterized under tensile strain and agree well with the simulation results. The antenna is reconfigurable because the resonant frequency is a function of the applied tensile strain. The antenna is thus well suited for applications like wireless strain sensing. The material and fabrication technique reported here could be extended to achieve other types of stretchable antennas with more complex patterns and multilayer structures.

Observations of Dynamic Strain Aging in Polycrystalline NiAl

NASA Technical Reports Server (NTRS)

Weaver, M. L.; Noebe, R. D.; Kaufman, M. J.

1996-01-01

Dynamic strain aging has been investigated at temperatures between 77 and 1100 K in eight polycrystalline NiAl alloys. The 0.2% offset yield stress and work hardening rates for these alloys generally decreased with increasing temperature. However, local plateaus or maxima were observed in conventional purity and carbon doped alloys at intermediate temperatures (600-900 K). This anomalous behavior was not observed in low interstitial high-purity, nitrogen doped, or in titanium doped materials. Low or negative strain rate sensitivities (SRS) were also observed in all eight alloys in this intermediate temperature range. Coincident with the occurrence of negative SRS was the occurrence of serrated flow in conventional purity alloys containing high concentrations of Si in addition to C. These phenomena have been attributed to dynamic strain aging (DSA). Chemical analysis of the alloys used in this study suggests that the main species causing strain aging in polycrystalline NiAl is C but indicate that residual Si impurities can enhance the strain aging effect.

Silicon strain gages bonded on stainless steel using glass frit for strain sensor applications

NASA Astrophysics Data System (ADS)

Zhang, Zongyang; Cheng, Xingguo; Leng, Yi; Cao, Gang; Liu, Sheng

2014-05-01

In this paper, a steel pressure sensor using strain gages bonded on a 17-4 PH stainless steel (SS) diaphragm based on glass frit technology is proposed. The strain gages with uniform resistance are obtained by growing an epi-silicon layer on a single crystal silicon wafer using epitaxial deposition technique. The inorganic glass frits are used as the bonding material between the strain gages and the 17-4 PH SS diaphragm. Our results show that the output performances of sensors at a high temperature of 125 °C are almost equal those at room temperature, which indicates that the glass frit bonding is a good method and may lead to a significant advance in the high temperature applicability of silicon strain gage sensors. Finally, the microstructure of the cured organic adhesive and the fired glass frit are compared. It may be concluded that the defects of the cured organic adhesive deteriorate the hysteresis and repeatability errors of the sensors.

Strain-optic voltage monitor wherein strain causes a change in the optical absorption of a crystalline material

DOEpatents

Weiss, Jonathan D.

1997-01-01

A voltage monitor which uses the shift in absorption edge of crystalline material to measure strain resulting from electric field-induced deformation of piezoelectric or electrostrictive material, providing a simple and accurate means for measuring voltage applied either by direct contact with the crystalline material or by subjecting the material to an electric field.

A High Strain-Rate Investigation of a Zr-Based Bulk Metallic Glass and an HTPB Polymer Composite

DTIC Science & Technology

2011-03-01

95 8. Lankford J. (1977) Compressive strength and microplasticity in polycrystalline alumina. Journal of Materials Science 12, 791-796. 9...Letters 45, 615-616. 59. Lankford J. (1977) Compressive strength and microplasticity in polycrystalline alumina. Journal of Materials Science 12, 791

Understanding the rheology of two and three-phase magmas

NASA Astrophysics Data System (ADS)

Coats, R.; Cai, B.; Kendrick, J. E.; Wallace, P. A.; Hornby, A. J.; Miwa, T.; von Aulock, F. W.; Ashworth, J. D.; Godinho, J.; Atwood, R. C.; Lee, P. D.; Lavallée, Y.

2017-12-01

The rheology of magma plays a fundamental role in determining the style of a volcanic eruption, be it explosive or effusive. Understanding how magmas respond to changes in stress/ strain conditions may help to enhance eruption forecast models. The presence of crystals and bubbles in magmas alter the viscosity of suspensions and favor a non-Newtonian response. Thus, with the aim of grasping the rheological behavior of volcanic materials, uniaxial compressive tests were performed on natural and synthetic samples. A suite of variably porous (10-32 vol.%), highly crystalline ( 50 vol.%) dacite from the 1991-95 eruption of Mt Unzen, Japan, was selected as the natural material, while synthetic samples were sintered with desired porosities (<3, 20 and 30 vol.%) and TiO2 particles (0-50 vol.%). Tests were carried out at both room temperature and above the glass transition temperature (Tg) of the different materials to cover the entirety of the extrusion process. Room temperature tests were performed at constant strain rates of 10-1, 10-3, and 10-5 s-1. The response was brittle and peak stresses reached were positively correlated to strain rate and negatively correlated to porosity. At temperatures above Tg, strain rates of 10-3, 10-4, and 10-5 s-1 were imposed resulting in dominantly brittle, transitional and dominantly viscous responses, respectively. Samples with a brittle response reached higher peak stresses, and strain-to-failure values, at high temperature than at room temperature. In both materials, non-Newtonian, shear-thinning behavior was observed and while synthetic samples showed an expected increase in apparent viscosity with increasing crystal content, surprisingly natural samples did not show a correlation between apparent viscosity and porosity. We hypothesise this is due to crystal content being the governing factor for the volume fractions explored. In situ, high temperature synchrotron X-ray tomography was performed on selected crystal/pore volume fractions at Diamond Light Source. Unexpectedly, these observations suggest that fractures nucleate in crystals due to crystal interactions, before propagating through the interstitial melt. This ongoing study promises to uncover the way crystal-bearing magmas flow or fail, necessary to constrain magmatic processes and volcanic hazards.

Development of III-V p-MOSFETs with high-kappa gate stack for future CMOS applications

NASA Astrophysics Data System (ADS)

Nagaiah, Padmaja

As the semiconductor industry approaches the limits of traditional silicon CMOS scaling, non-silicon materials and new device architectures are gradually being introduced to improve Si integrated circuit performance and continue transistor scaling. Recently, the replacement of SiO2 with a high-k material (HfO2) as gate dielectric has essentially removed one of the biggest advantages of Si as channel material. As a result, alternate high mobility materials are being considered to replace Si in the channel to achieve higher drive currents and switching speeds. III-V materials in particular have become of great interest as channel materials, owing to their superior electron transport properties. However, there are several critical challenges that need to be addressed before III-V based CMOS can replace Si CMOS technology. Some of these challenges include development of a high quality, thermally stable gate dielectric/III-V interface, and improvement in III-V p-channel hole mobility to complement the n-channel mobility, low source/drain resistance and integration onto Si substrate. In this thesis, we would be addressing the first two issues i.e. the development high performance III-V p-channels and obtaining high quality III-V/high-k interface. We start with using the device architecture of the already established InGaAs n-channels as a baseline to understand the effect of remote scattering from the high-k oxide and oxide/semiconductor interface on channel transport properties such as electron mobility and channel electron concentration. Temperature dependent Hall electron mobility measurements were performed to separate various scattering induced mobility limiting factors. Dependence of channel mobility on proximity of the channel to the oxide interface, oxide thickness, annealing conditions are discussed. The results from this work will be used in the design of the p-channel MOSFETs. Following this, InxGa1-xAs (x>0.53) is chosen as channel material for developing p-channel MOSFETs. Band engineering, strain induced valence band splitting and quantum confinement is used to improve channel hole mobility. Experimental results on the Hall hole mobility is presented for InxGa1-xAs channels with varying In content, thickness of the quantum well and temperature. Then, high mobility InxGa 1-xAs heterostructure thus obtained are integrated with in-situ deposited high-k gate oxide required for high performance p-MOSFET and discuss the challenges associated with the gated structure and draw conclusions on this material system. Antimonide based channel materials such as GaSb and InxGa 1-xSb are explored for III-V based p-MOSFETs in last two chapters. Options for Sb based strained QW channels to obtain maximum hole mobility by varying the strain, channel and barrier material, thickness of the layers etc. is discussed followed by the growth of these Sb channels on GaAs and InP substrates using molecular beam epitaxy. The physical properties of the structures such as the heterostructure quality, alloy content and surface roughness are examined via TEM, XRD and AFM. Following this, electrical measurement results on Hall hole mobility is presented. The effect of strain, alloy content, temperature and thickness on channel mobility and concentration is reported. Development of GaSb n- and p-MOS capacitor structures with in-situ deposited HfO2 gate oxide dielectric using in-situ deposited amorphous Si (a-Si) interface passivation layer (IPL) to improve the interface quality of high-k oxide and (In)GaSb surface is presented. In-situ deposited gate oxides such as Al2O3 and combination oxide of Al 2O3 and HfO2 with and without the a-Si IPL are also explored as alternate gate dielectrics. Subsequently, MOS capacitor structures using buried InGaSb QWs are demonstrated. Development of an inversion type bulk GaSb with implanted source-drain contacts and in-situ deposited gate oxide HfO2 gate oxide is discussed. The merits of biaxial compressive strain is demonstrated on strained surface and buried channel In0.36 Ga0.64Sb QW MOSFETs with thin top barrier and in-situ deposited a-Si IPL and high-k HfO2 as well as combination Al 2O3+HfO2 gate stacks and ex-situ atomic layer deposited (ALD) combination gate oxide and with thin 2 nm InAs surface passivation layer is presented. Finally, summary of the salient results from the different chapters is provided with recommendations for future research.

Strain rate effects for spallation of concrete

NASA Astrophysics Data System (ADS)

Häussler-Combe, Ulrich; Panteki, Evmorfia; Kühn, Tino

2015-09-01

Appropriate triaxial constitutive laws are the key for a realistic simulation of high speed dynamics of concrete. The strain rate effect is still an open issue within this context. In particular the question whether it is a material property - which can be covered by rate dependent stress strain relations - or mainly an effect of inertia is still under discussion. Experimental and theoretical investigations of spallation of concrete specimen in a Hopkinson Bar setup may bring some evidence into this question. For this purpose the paper describes the VERD model, a newly developed constitutive law for concrete based on a damage approach with included strain rate effects [1]. In contrast to other approaches the dynamic strength increase is not directly coupled to strain rate values but related to physical mechanisms like the retarded movement of water in capillary systems and delayed microcracking. The constitutive law is fully triaxial and implemented into explicit finite element codes for the investigation of a wide range of concrete structures exposed to impact and explosions. The current setup models spallation experiments with concrete specimen [2]. The results of such experiments are mainly related to the dynamic tensile strength and the crack energy of concrete which may be derived from, e.g., the velocity of spalled concrete fragments. The experimental results are compared to the VERD model and two further constitutive laws implemented in LS-Dyna. The results indicate that both viscosity and retarded damage are required for a realistic description of the material behaviour of concrete exposed to high strain effects [3].

Embedding of Superelastic SMA Wires into Composite Structures: Evaluation of Impact Properties

NASA Astrophysics Data System (ADS)

Pappadà, Silvio; Rametta, Rocco; Toia, Luca; Coda, Alberto; Fumagalli, Luca; Maffezzoli, Alfonso

2009-08-01

Shape memory alloy (SMA) represents the most versatile way to realize smart materials with sensing, controlling, and actuating functions. Due to their unique mechanical and thermodynamic properties and to the possibility to obtain SMA wires with very small diameters, they are used as smart components embedded into the conventional resins or composites, obtaining active abilities, tunable properties, self-healing properties, and damping capacity. Moreover, superelastic SMAs are used to increase the impact resistance properties of composite materials. In this study, the influence of the integration of thin superelastic wires to suppress propagating damage of composite structures has been investigated. Superelastic SMAs have very high strain to failure and recoverable elastic strain, due to a stress-induced martensitic phase transition creating a plateau region in the stress-strain curve. NiTi superelastic wires ( A f = -15 °C fully annealed) of 0.10 mm in diameter have been produced and characterized by SAES Getters. The straight annealed wire shows the typical flag stress-strain behavior. The measured loading plateau is about 450 MPa at ambient temperature with a recoverable elastic strain of more than 6%. For these reasons superelastic SMA fibers can absorb much more strain energy than other fibers before their failure, partly with a constant stress level. In this paper, the improvement of composite laminates impact properties by embedding SMA wires is evaluated and indications for design and manufacturing of SMA composites with high-impact properties are also given.

Mechanics of hard films on soft substrates

NASA Astrophysics Data System (ADS)

Lu, Nanshu

2009-12-01

Flexible electronics have been developed for various applications, including paper-like electronic readers, rollable solar cells, electronic skins etc., with the merits of light weight, low cost, large area, and ruggedness. The systems may be subject to one-time or repeated large deformation during manufacturing and application. Although organic materials can be highly deformable, currently they are not able to fulfill every electronic function. Therefore flexible electronic devices are usually made as organic/inorganic hybrids, with diverse materials, complex architecture, and micro features. While the polymer substrates can recover from large deformations, thin films of electronic materials such as metals, silicon, oxides, and nitrides fracture at small strains, usually less than a few percent. Mechanics of hard films on soft substrates hence holds the key to build high-performance and highly reliable flex circuits. This thesis investigates the deformability and failure mechanisms of thin films of metallic and ceramic materials supported by soft polymeric substrates through combined experimental, theoretical, and numerical methods. When subject to tension, micron-thick metal films with stable microstructure and strong interfacial adhesion to the substrate can be stretched beyond 50% without forming cracks. They eventually rupture by a ductile transgranular fracture which involves simultaneous necking and debonding. When metal films become nanometer-thick, intergranular fracture dominates the failure mode at elongations of only a few percent. Unannealed films show unstable microstructure at room temperature when subject to mechanical loading. In this case, films also rupture at small strains but by three concurrent mechanisms: deformation-induced grain growth, strain localization at large grains, and simultaneous debonding. In contrast to metal films, ceramic films rupture by brittle mechanisms. The only way to prevent rupture of ceramic films is to reduce the strain they are subject to. Instead of using blanket films that fail at strains less than i%, we have patterned ceramic films into a lattice of periodic, isolated islands. Failure modes such as channel cracking, debonding, and wrinkling have been identified. Island behaviors are controlled by factors such as island size, thickness, and elastic mismatch with the substrate. A very soft interlayer between the islands and the underlying polyimide substrate reduces strains in the islands by orders of magnitude. Using this approach, substrates with arrays of 200 x 200 mum2 large SiNx islands were stretched beyond 20% without cracking or debonding the islands. In summary, highly stretchable thin metal films and ceramic island arrays supported by polymer substrates have been achieved, along with mechanistic understandings of their deformation and failure mechanisms.

Draft ASME Boiler and Pressure Vessel Code Section III, Division 5, Section HB, Subsection B, Code Case for Alloy 617 and Background Documentation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wright, Julie Knibloe

2015-08-01

Alloy 617 is the leading candidate material for an intermediate heat exchanger for the very high temperature reactor. To evaluate the behavior of this material in the expected service conditions, strain controlled cyclic tests that include long hold times up to 240 minutes at maximum tensile strain were conducted at 850°C. In terms of the total number of cycles to failure, the fatigue resistance decreased when a hold time was added at peak tensile strain. Increases in the tensile hold duration degraded the creep fatigue resistance, at least to the investigated strain controlled hold time of up to 60 minutesmore » at the 0.3% strain range and 240 minutes at the 1.0% strain range. The creep fatigue deformation mode is considered relative to the lack of saturation, or continually decreasing number of cycles to failure with increasing hold times. Additionally, preliminary values from the 850°C creep fatigue data are calculated for the creep fatigue damage diagram and have higher values of creep damage than those from tests at 950°C.« less

Specimen dimensions influence the measurement of material properties in tendon fascicles.

PubMed

Legerlotz, Kirsten; Riley, Graham P; Screen, Hazel R C

2010-08-26

Stress, strain and modulus are regularly used to characterize material properties of tissue samples. However, when comparing results from different studies it is evident the reported material properties, particularly failure strains, vary hugely. The aim of our study was to characterize how and why specimen length and cross-sectional area (CSA) appear to influence failure stress, strain and modulus in fascicles from two functionally different tendons. Fascicles were dissected from five rat tails and five bovine foot extensors, their diameters determined by a laser micrometer, and loaded to failure at a range of grip-to-grip lengths. Strain to failure significantly decreased with increasing in specimen length in both rat and bovine fascicles, while modulus increased. Specimen length did not influence failure stress in rat tail fascicles, although in bovine fascicles it was significantly lower in the longer 40 mm specimens compared to 5 and 10mm specimens. The variations in failure strain and modulus with sample length could be predominantly explained by end-effects. However, it was also evident that strain fields along the sample length were highly variable and notably larger towards the ends of the sample than the mid-section even at distances in excess of 5mm from the gripping points. Failure strain, stress and modulus correlated significantly with CSA at certain specimen lengths. Our findings have implications for the mechanical testing of tendon tissue: while it is not always possible to control for fascicle length and/or CSA, these parameters have to be taken into account when comparing samples of different dimensions. 2010 Elsevier Ltd. All rights reserved.

Microstructural effects on ignition sensitivity in Ni/Al systems subjected to high strain rate impacts

NASA Astrophysics Data System (ADS)

Reeves, Robert; Mukasyan, Alexander; Son, Steven

2011-06-01

The effect of microstructural refinement on the sensitivity of the Ni/Al (1:1 at%) system to ignition via high strain rate impacts is investigated. The tested microstructures include compacts of irregularly convoluted lamellar structures with nanometric features created through high-energy ball milling (HEBM) of micron size Ni/Al powders and compacts of nanometric Ni and Al powders. The test materials were subjected to high strain rate impacts through Asay shear experiments powered by a light gas gun. Muzzle velocities up to 1.1 km/s were used. It was found that the nanometric powder exhibited a greater sensitivity to ignition via impact than the HEBM material, despite greater thermal sensitivity of the HEBM. A previously unseen fast reaction mode where the reaction front traveled at the speed of the input stress wave was also observed in the nanometric mixtures at high muzzle energies. This fast mode is considered to be a mechanically induced thermal explosion mode dependent on the magnitude of the traveling stress wave, rather than a self-propagating detonation, since its propagation rate decreases rapidly across the sample. A similar mode is not exhibited by HEBM samples, although local, nonpropagating reaction zones occur in shear bands formed during the impact event.

Microstructural effects on ignition sensitivity in Ni/Al systems subjected to high strain rate impacts

NASA Astrophysics Data System (ADS)

Reeves, Robert V.; Mukasyan, Alexander S.; Son, Steven

2012-03-01

The effect of microstructural refinement on the sensitivity of the Ni/Al (1:1 mol%) system to ignition via high strain rate impacts is investigated. The tested microstructures include compacts of irregularly convoluted lamellar structures with nanometric features created through high-energy ball milling (HEBM) of micron size Ni/Al powders and compacts of nanometric Ni and Al powders. The test materials were subjected to high strain rate impacts through Asay shear experiments powered by a light gas gun. Muzzle velocities up to 1.1 km/s were used. It was found that the nanometric powder exhibited a greater sensitivity to ignition via impact than the HEBM material, despite greater thermal sensitivity of the HEBM. A previously unseen fast reaction mode where the reaction front traveled at the speed of the input stress wave was also observed in the nanometric mixtures at high muzzle energies. This fast mode is considered to be a mechanically induced thermal explosion mode dependent on the magnitude of the traveling stress wave, rather than a self-propagating detonation, since its propagation rate decreases rapidly across the sample. A similar mode is not exhibited by HEBM samples, although local, nonpropagating reaction zones shear bands formed during the impact event are observed.

Electric-field-induced strain contributions in morphotropic phase boundary composition of (Bi{sub 1/2}Na{sub 1/2})TiO{sub 3}-BaTiO{sub 3} during poling

DOE Office of Scientific and Technical Information (OSTI.GOV)

Khansur, Neamul H.; Daniels, John E.; Hinterstein, Manuel

2015-12-14

The microscopic contributions to the electric-field-induced macroscopic strain in a morphotropic 0.93(Bi{sub 1/2}Na{sub 1/2}TiO{sub 3})−0.07(BaTiO{sub 3}) with a mixed rhombohedral and tetragonal structure have been quantified using full pattern Rietveld refinement of in situ high-energy x-ray diffraction data. The analysis methodology allows a quantification of all strain mechanisms for each phase in a morphotropic composition and is applicable to use in a wide variety of piezoelectric compositions. It is shown that during the poling of this material 24%, 44%, and 32% of the total macroscopic strain is generated from lattice strain, domain switching, and phase transformation strains, respectively. The resultsmore » also suggest that the tetragonal phase contributes the most to extrinsic domain switching strain, whereas the lattice strain primarily stems from the rhombohedral phase. The analysis also suggests that almost 32% of the total strain is lost or is a one-time effect due to the irreversible nature of the electric-field-induced phase transformation in the current composition. This information is relevant to on-going compositional development strategies to harness the electric-field-induced phase transformation strain of (Bi{sub 1/2}Na{sub 1/2})TiO{sub 3}-based lead-free piezoelectric materials for actuator applications.« less

Strain Sensitivity in Single Walled Carbon Nanotubes for Multifunctional Materials

NASA Technical Reports Server (NTRS)

Heath, D. M. (Technical Monitor); Smits, Jan M., VI

2005-01-01

Single walled carbon nanotubes represent the future of structural aerospace vehicle systems due to their unparalleled strength characteristics and demonstrated multifunctionality. This multifunctionality rises from the CNT's unique capabilities for both metallic and semiconducting electron transport, electron spin polarizability, and band gap modulation under strain. By incorporating the use of electric field alignment and various lithography techniques, a single wall carbon nanotube (SWNT) test bed for measurement of conductivity/strain relationships has been developed. Nanotubes are deposited at specified locations through dielectrophoresis. The circuit is designed such that the central, current carrying section of the nanotube is exposed to enable atomic force microscopy and manipulation in situ while the transport properties of the junction are monitored. By applying this methodology to sensor development a flexible single wall carbon nanotube (SWNT) based strain sensitive device has been developed. Studies of tensile testing of the flexible SWNT device vs conductivity are also presented, demonstrating the feasibility of using single walled HiPCO (high-pressure carbon monoxide) carbon nanotubes as strain sensing agents in a multi-functional materials system.

Test and Analysis of Sub-Components of Aluminum-Lithium Alloy Cylinders

NASA Technical Reports Server (NTRS)

Haynie, Waddy T.; Chunchu, Prasad B.; Satyanarayana, Arunkumar; Hilburger, Mark W.; Smith, Russell W.

2012-01-01

Integrally machined blade-stiffened panels subjected to an axial compressive load were tested and analyzed to observe the buckling, crippling, and postcrippling response of the panels. The panels were fabricated from aluminum-lithium alloys 2195 and 2050, and both alloys have reduced material properties in the short transverse material direction. The tests were designed to capture a failure mode characterized by the stiffener separating from the panel in the postbuckling range. This failure mode is attributed to the reduced properties in the short transverse direction. Full-field measurements of displacements and strains using three-dimensional digital image correlation systems and local measurements using strain gages were used to capture the deformation of the panel leading up to the failure of the panel for specimens fabricated from 2195. High-speed cameras were used to capture the initiation of the failure. Finite element models were developed using an isotropic strain-hardening material model. Good agreement was observed between the measured and predicted responses for both alloys.

A Membrane Model from Implicit Elasticity Theory. Application to Visceral Pleura

DOE Office of Scientific and Technical Information (OSTI.GOV)

Freed, Alan D.; Liao, Jun; Einstein, Daniel R.

2013-11-27

A Fungean solid is derived for membranous materials as a body defined by isotropic response functions whose mathematical structure is that of a Hookean solid where the elastic constants are replaced by functions of state derived from an implicit, thermodynamic, internal energy function. The theory utilizes Biot’s (Lond Edinb Dublin Philos Mag J Sci 27:468–489, 1939) definitions for stress and strain that, in one-dimension, are the stress/strain measures adopted by Fung (Am J Physiol 28:1532–1544, 1967) when he postulated what is now known as Fung’s law. Our Fungean membrane model is parameterized against a biaxial data set acquired from amore » porcine pleural membrane subjected to three, sequential, proportional, planar extensions. These data support an isotropic/deviatoric split in the stress and strain-rate hypothesized by our theory. These data also demonstrate that the material response is highly nonlinear but, otherwise, mechanically isotropic. These data are described reasonably well by our otherwise simple, four-parameter, material model.« less

Single Hit Energy-resolved Laue Diffraction

DOE Office of Scientific and Technical Information (OSTI.GOV)

Patel, Shamim; Suggit, Matthew J.; Stubley, Paul G.

2015-05-15

In situ white light Laue diffraction has been successfully used to interrogate the structure of single crystal materials undergoing rapid (nanosecond) dynamic compression up to megabar pressures. However, information on strain state accessible via this technique is limited, reducing its applicability for a range of applications. We present an extension to the existing Laue diffraction platform in which we record the photon energy of a subset of diffraction peaks. This allows for a measurement of the longitudinal and transverse strains in situ during compression. Consequently, we demonstrate measurement of volumetric compression of the unit cell, in addition to the limitedmore » aspect ratio information accessible in conventional white light Laue. We present preliminary results for silicon, where only an elastic strain is observed. VISAR measurements show the presence of a two wave structure and measurements show that material downstream of the second wave does not contribute to the observed diffraction peaks, supporting the idea that this material may be highly disordered, or has undergone large scale rotation.« less

SLS complementary logic devices with increase carrier mobility

DOEpatents

Chaffin, R.J.; Osbourn, G.C.; Zipperian, T.E.

1991-07-09

In an electronic device comprising a semiconductor material and having at least one performance characteristic which is limited by the mobility of holes in the semiconductor material, said mobility being limited because of a valence band degeneracy among high-mobility and low-mobility energy levels accessible to said holes at the energy-momentum space maximum, an improvement is provided wherein the semiconductor material is a strained layer superlattice (SLS) whose layer compositions and layer thicknesses are selected so that the strain on the layers predominantly containing said at least one carrier type splits said degeneracy and modifies said energy levels around said energy-momentum space maximum in a manner whereby said limitation on the mobility of said holes is alleviated. 5 figures.

SLS complementary logic devices with increase carrier mobility

DOEpatents

Chaffin, Roger J.; Osbourn, Gordon C.; Zipperian, Thomas E.

1991-01-01

In an electronic device comprising a semiconductor material and having at least one performance characteristic which is limited by the mobility of holes in the semiconductor material, said mobility being limited because of a valence band degeneracy among high-mobility and low-mobility energy levels accessible to said holes at the energy-momentum space maximum, an improvement is provided wherein the semiconductor material is a strained layer superlattice (SLS) whose layer compositions and layer thicknesses are selected so that the strain on the layers predominantly containing said at least one carrier type splits said degeneracy and modifies said energy levels around said energy-momentum space maximum in a manner whereby said limitation on the mobility of said holes is alleviated.

Strain-optic voltage monitor wherein strain causes a change in the optical absorption of a crystalline material

DOEpatents

Weiss, J.D.

1997-01-14

A voltage monitor which uses the shift in absorption edge of crystalline material to measure strain resulting from electric field-induced deformation of piezoelectric or electrostrictive material, providing a simple and accurate means for measuring voltage applied either by direct contact with the crystalline material or by subjecting the material to an electric field. 6 figs.

3D printed high performance strain sensors for high temperature applications

NASA Astrophysics Data System (ADS)

Rahman, Md Taibur; Moser, Russell; Zbib, Hussein M.; Ramana, C. V.; Panat, Rahul

2018-01-01

Realization of high temperature physical measurement sensors, which are needed in many of the current and emerging technologies, is challenging due to the degradation of their electrical stability by drift currents, material oxidation, thermal strain, and creep. In this paper, for the first time, we demonstrate that 3D printed sensors show a metamaterial-like behavior, resulting in superior performance such as high sensitivity, low thermal strain, and enhanced thermal stability. The sensors were fabricated using silver (Ag) nanoparticles (NPs), using an advanced Aerosol Jet based additive printing method followed by thermal sintering. The sensors were tested under cyclic strain up to a temperature of 500 °C and showed a gauge factor of 3.15 ± 0.086, which is about 57% higher than that of those available commercially. The sensor thermal strain was also an order of magnitude lower than that of commercial gages for operation up to a temperature of 500 °C. An analytical model was developed to account for the enhanced performance of such printed sensors based on enhanced lateral contraction of the NP films due to the porosity, a behavior akin to cellular metamaterials. The results demonstrate the potential of 3D printing technology as a pathway to realize highly stable and high-performance sensors for high temperature applications.

Coral-Inspired Nanoengineering Design for Long-Cycle and Flexible Lithium-Ion Battery Anode.

PubMed

Sun, Yangyong; Wang, Cheng; Xue, Yinghui; Zhang, Qin; Mendes, Rafael G; Chen, Linfeng; Zhang, Tao; Gemming, Thomas; Rümmeli, Mark H; Ai, Xinping; Fu, Lei

2016-04-13

Conversion reaction electrode materials (CREMs) have gained significant interest in lithium-ion batteries (LIBs) owing to their high theoretical gravimetric capacity. However, traditional CREMs-based electrodes, with large strain arising from Li(+) intercalation/deintercalation causes pulverization or electrical breakdown and cracking of the active materials which leads to structural collapse, limiting performance. Therefore, in order to construct electrodes with a strong tolerance to the strain incurred during the conversion reaction process, we design a coral-like three-dimensional (3D) hierarchical heterostructure by using cross-linked nanoflakes interspersed with nanoparticles (NPs) standing vertically on graphene foam (GF). The coral-like 3D hierarchical heterostructures can efficiently disperse the strain from both internal and external forces as well as increase the specific surface area for enhanced electrochemical reactions. These features lead to long-cycle stability and excellent flexibility in LIBs. Fe3O4 NPs and CoO NFs are utilized as a model system to demonstrate our strategy. The as-prepared coral-like hierarchical electrode is studied as an anode in LIBs for the first time and is shown to deliver a high reversible specific gravimetric capacity of ∼1200 mA h g(-1) at a rate of 0.5 A g(-1) for 400 cycles. In addition, our batteries can even power a green light-emitting diode when bent to high degrees confirming the excellent flexibility of the material.

Phonon dispersion evolution in uniaxially strained aluminum crystal

NASA Astrophysics Data System (ADS)

Parthasarathy, Ranganathan; Misra, Anil; Aryal, Sitaram; Ouyang, Lizhi

2018-04-01

The influence of loading upon the phonon dispersion of crystalline materials could be highly nonlinear with certain particular trends that depend upon the loading path. In this paper, we have calculated the influence of [100] uniaxial strain on the phonon dispersion and group velocities in fcc aluminum using second moments of position obtained from molecular dynamics (MD) simulation at 300 K. In contrast to nonlinear monotonic variation of both longitudinal and transverse phonon frequencies along the Δ , Λ and Σ lines of the first Brillouin zone under tension, transverse phonon branches along the Λ line show inflection at specific wavevectors when the compressive strain exceeds 5%. Further, the longitudinal group velocities along the high-symmetry Δ line vary non-monotonically with strain, reaching a minimum at 5% compressive strain. Throughout the strain range studied, the equilibrium positions of atoms displace in an affine manner preserving certain static structural symmetry. We attribute the anomalies in the phonon dispersion to the non-affine evolution of second moments of atomic position, and the associated plateauing of force constants under the applied strain path.

Thermal stability and relaxation mechanisms in compressively strained Ge{sub 0.94}Sn{sub 0.06} thin films grown by molecular beam epitaxy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Fleischmann, C.; Lieten, R. R.; Shimura, Y.

Strained Ge{sub 1-x}Sn{sub x} thin films have recently attracted a lot of attention as promising high mobility or light emitting materials for future micro- and optoelectronic devices. While they can be grown nowadays with high crystal quality, the mechanism by which strain energy is relieved upon thermal treatments remains speculative. To this end, we investigated the evolution (and the interplay) of composition, strain, and morphology of strained Ge{sub 0.94}Sn{sub 0.06} films with temperature. We observed a diffusion-driven formation of Sn-enriched islands (and their self-organization) as well as surface depressions (pits), resulting in phase separation and (local) reduction in strain energy,more » respectively. Remarkably, these compositional and morphological instabilities were found to be the dominating mechanisms to relieve energy, implying that the relaxation via misfit generation and propagation is not intrinsic to compressively strained Ge{sub 0.94}Sn{sub 0.06} films grown by molecular beam epitaxy.« less

A Modified Constitutive Model for Tensile Flow Behaviors of BR1500HS Ultra-High-Strength Steel at Medium and Low Temperature Regions

NASA Astrophysics Data System (ADS)

Zhao, Jun; Quan, Guo-Zheng; Pan, Jia; Wang, Xuan; Wu, Dong-Sen; Xia, Yu-Feng

2018-01-01

Constitutive model of materials is one of the most requisite mathematical model in the finite element analysis, which describes the relationships of flow behaviors with strain, strain rate and temperature. In order to construct such constitutive relationships of ultra-high-strength BR1500HS steel at medium and low temperature regions, the true stress-strain data over a wide temperature range of 293-873 K and strain rate range of 0.01-10 s-1 were collected from a series of isothermal uniaxial tensile tests. The experimental results show that stress-strain relationships are highly non-linear and susceptible to three parameters involving temperature, strain and strain rate. By considering the impacts of strain rate and temperature on strain hardening, a modified constitutive model based on Johnson-Cook model was proposed to characterize flow behaviors in medium and low temperature ranges. The predictability of the improved model was also evaluated by the relative error (W(%)), correlation coefficient (R) and average absolute relative error (AARE). The R-value and AARE-value for modified constitutive model at medium and low temperature regions are 0.9915 & 1.56 % and 0.9570 & 5.39 %, respectively, which indicates that the modified constitutive model can precisely estimate the flow behaviors for BR1500HS steel in the medium and low temperature regions.

Measurement of strain distribution in bonded joints by fiber Bragg gratings

NASA Astrophysics Data System (ADS)

Guemes, J. Alfredo; Diaz-Carrillo, Sebastian; Menendez, Jose M.

1998-07-01

Due to the small dimensions of the adhesive layer, the high non-uniformity of the strain field and the non linear elastic behavior of the adhesive material, the strain distribution at an adhesive joint can be predicted by FEM, but can not be experimentally obtained with classical approaches; only non standard procedures like Moire interferometry, or special artifacts like KGR extensometers may afford some insights on the behavior of the adhesive. Due to their small size, ensuring low perturbation of the strain field, and their innate ability to measure strain and strain gradient along the sensor, fiber Bragg gratings offer a good opportunity to solve this problem, and it is a good example of situations that may benefit from these new sensors. Fiber Bragg gratings may be placed or at the interface, within the adhesive layer, or embedded at the adherents, if these were made of composite material. Tests may be run at different temperatures, changing the adhesive characteristics from brittle to pseudoplastic without additional difficulties. When loading the joint, the strain field is obtained by analyzing the distorted spectrum of the reflected light pulse; the algorithm for doing it has already been published. A comparison with theoretical results is done, and the validity and utility of these sensors for this and similar applications is demonstrated.

Effects of Adiabatic Heating on the High Strain Rate Deformation of Polymer Matrix Composites

NASA Technical Reports Server (NTRS)

Sorini, Chris; Chattopadhyay, Aditi; Goldberg, Robert K.

2017-01-01

Polymer matrix composites (PMCs) are increasingly being used in aerospace structures that are expected to experience complex dynamic loading conditions throughout their lifetime. As such, a detailed understanding of the high strain rate behavior of the constituents, particularly the strain rate, temperature, and pressure dependent polymer matrix, is paramount. In this paper, preliminary efforts in modeling experimentally observed temperature rises due to plastic deformation in PMCs subjected to dynamic loading are presented. To this end, an existing isothermal viscoplastic polymer constitutive formulation is extended to model adiabatic conditions by incorporating temperature dependent elastic properties and modifying the components of the inelastic strain rate tensor to explicitly depend on temperature. It is demonstrated that the modified polymer constitutive model is capable of capturing strain rate and temperature dependent yield as well as thermal softening associated with the conversion of plastic work to heat at high rates of strain. The modified constitutive model is then embedded within a strength of materials based micromechanics framework to investigate the manifestation of matrix thermal softening, due to the conversion of plastic work to heat, on the high strain rate response of a T700Epon 862 (T700E862) unidirectional composite. Adiabatic model predictions for high strain rate composite longitudinal tensile, transverse tensile, and in-plane shear loading are presented. Results show a substantial deviation from isothermal conditions; significant thermal softening is observed for matrix dominated deformation modes (transverse tension and in-plane shear), highlighting the importance of accounting for the conversion of plastic work to heat in the polymer matrix in the high strain rate analysis of PMC structures.

Free-standing nanocomposites with high conductivity and extensibility.

PubMed

Chun, Kyoung-Yong; Kim, Shi Hyeong; Shin, Min Kyoon; Kim, Youn Tae; Spinks, Geoffrey M; Aliev, Ali E; Baughman, Ray H; Kim, Seon Jeong

2013-04-26

The prospect of electronic circuits that are stretchable and bendable promises tantalizing applications such as skin-like electronics, roll-up displays, conformable sensors and actuators, and lightweight solar cells. The preparation of highly conductive and highly extensible materials remains a challenge for mass production applications, such as free-standing films or printable composite inks. Here we present a nanocomposite material consisting of carbon nanotubes, ionic liquid, silver nanoparticles, and polystyrene-polyisoprene-polystyrene having a high electrical conductivity of 3700 S cm(-1) that can be stretched to 288% without permanent damage. The material is prepared as a concentrated dispersion suitable for simple processing into free-standing films. For the unstrained state, the measured thermal conductivity for the electronically conducting elastomeric nanoparticle film is relatively high and shows a non-metallic temperature dependence consistent with phonon transport, while the temperature dependence of electrical resistivity is metallic. We connect an electric fan to a DC power supply using the films to demonstrate their utility as an elastomeric electronic interconnect. The huge strain sensitivity and the very low temperature coefficient of resistivity suggest their applicability as strain sensors, including those that operate directly to control motors and other devices.

Anisotropic Effects on Constitutive Model Parameters of Aluminum Alloys

NASA Astrophysics Data System (ADS)

Brar, Nachhatter; Joshi, Vasant

2011-06-01

Simulation of low velocity impact on structures or high velocity penetration in armor materials heavily rely on constitutive material models. The model constants are required input to computer codes (LS-DYNA, DYNA3D or SPH) to accurately simulate fragment impact on structural components made of high strength 7075-T651 aluminum alloys. Johnson-Cook model constants determined for Al7075-T651 alloy bar material failed to simulate correctly the penetration into 1' thick Al-7075-T651plates. When simulations go well beyond minor parameter tweaking and experimental results are drastically different it is important to determine constitutive parameters from the actual material used in impact/penetration experiments. To investigate anisotropic effects on the yield/flow stress of this alloy we performed quasi-static and high strain rate tensile tests on specimens fabricated in the longitudinal, transverse, and thickness directions of 1' thick Al7075-T651 plate. Flow stresses at a strain rate of ~1100/s in the longitudinal and transverse direction are similar around 670MPa and decreases to 620 MPa in the thickness direction. These data are lower than the flow stress of 760 MPa measured in Al7075-T651 bar stock.

Recent progress in distributed fiber optic sensors.

PubMed

Bao, Xiaoyi; Chen, Liang

2012-01-01

Rayleigh, Brillouin and Raman scatterings in fibers result from the interaction of photons with local material characteristic features like density, temperature and strain. For example an acoustic/mechanical wave generates a dynamic density variation; such a variation may be affected by local temperature, strain, vibration and birefringence. By detecting changes in the amplitude, frequency and phase of light scattered along a fiber, one can realize a distributed fiber sensor for measuring localized temperature, strain, vibration and birefringence over lengths ranging from meters to one hundred kilometers. Such a measurement can be made in the time domain or frequency domain to resolve location information. With coherent detection of the scattered light one can observe changes in birefringence and beat length for fibers and devices. The progress on state of the art technology for sensing performance, in terms of spatial resolution and limitations on sensing length is reviewed. These distributed sensors can be used for disaster prevention in the civil structural monitoring of pipelines, bridges, dams and railroads. A sensor with centimeter spatial resolution and high precision measurement of temperature, strain, vibration and birefringence can find applications in aerospace smart structures, material processing, and the characterization of optical materials and devices.

Recent Progress in Distributed Fiber Optic Sensors

PubMed Central

Bao, Xiaoyi; Chen, Liang

2012-01-01

Rayleigh, Brillouin and Raman scatterings in fibers result from the interaction of photons with local material characteristic features like density, temperature and strain. For example an acoustic/mechanical wave generates a dynamic density variation; such a variation may be affected by local temperature, strain, vibration and birefringence. By detecting changes in the amplitude, frequency and phase of light scattered along a fiber, one can realize a distributed fiber sensor for measuring localized temperature, strain, vibration and birefringence over lengths ranging from meters to one hundred kilometers. Such a measurement can be made in the time domain or frequency domain to resolve location information. With coherent detection of the scattered light one can observe changes in birefringence and beat length for fibers and devices. The progress on state of the art technology for sensing performance, in terms of spatial resolution and limitations on sensing length is reviewed. These distributed sensors can be used for disaster prevention in the civil structural monitoring of pipelines, bridges, dams and railroads. A sensor with centimeter spatial resolution and high precision measurement of temperature, strain, vibration and birefringence can find applications in aerospace smart structures, material processing, and the characterization of optical materials and devices. PMID:23012508

Strain Gauges Based on CVD Graphene Layers and Exfoliated Graphene Nanoplatelets with Enhanced Reproducibility and Scalability for Large Quantities

PubMed Central

Yokaribas, Volkan; Schneider, Daniel S.; Friebertshäuser, Philipp; Lemme, Max C.; Fritzen, Claus-Peter

2017-01-01

The two-dimensional material graphene promises a broad variety of sensing activities. Based on its low weight and high versatility, the sensor density can significantly be increased on a structure, which can improve reliability and reduce fluctuation in damage detection strategies such as structural health monitoring (SHM). Moreover; it initializes the basis of structure–sensor fusion towards self-sensing structures. Strain gauges are extensively used sensors in scientific and industrial applications. In this work, sensing in small strain fields (from −0.1% up to 0.1%) with regard to structural dynamics of a mechanical structure is presented with sensitivities comparable to bulk materials by measuring the inherent piezoresistive effect of graphene grown by chemical vapor deposition (CVD) with a very high aspect ratio of approximately 4.86 × 108. It is demonstrated that the increasing number of graphene layers with CVD graphene plays a key role in reproducible strain gauge application since defects of individual layers may become less important in the current path. This may lead to a more stable response and, thus, resulting in a lower scattering.. Further results demonstrate the piezoresistive effect in a network consisting of liquid exfoliated graphene nanoplatelets (GNP), which result in even higher strain sensitivity and reproducibility. A model-assisted approach provides the main parameters to find an optimum of sensitivity and reproducibility of GNP films. The fabricated GNP strain gauges show a minimal deviation in PRE effect with a GF of approximately 5.6 and predict a linear electromechanical behaviour up to 1% strain. Spray deposition is used to develop a low-cost and scalable manufacturing process for GNP strain gauges. In this context, the challenge of reproducible and reliable manufacturing and operating must be overcome. The developed sensors exhibit strain gauges by considering the significant importance of reproducible sensor performances and open the path for graphene strain gauges for potential usages in science and industry. PMID:29258260

Time-dependent strains and stresses in a pumpkin balloon

NASA Technical Reports Server (NTRS)

Gerngross, T.; Xu, Y.; Pellegrino, S.

2006-01-01

This paper presents a study of pumpkin-shaped superpressure balloons, consisting of gores made from a thin polymeric film attached to high stiffness, meridional tendons. This type of design is being used for the NASA ULDB balloons. The gore film shows considerable time-dependent stress relaxation, whereas the behaviour of the tendons is essentially time-independent. Upon inflation and pressurization, the "instantaneous", i.e. linear-elastic strain and stress distribution in the film show significantly higher values in the meridional direction. However, over time, and due to the biaxial visco-elastic stress relaxation of the the material, the hoop strains increase and the meridional stresses decrease, whereas the remaining strain and stress components remain substantially unchanged. These results are important for a correct assessment of the structural integrity of a pumpkin balloon in a long-duration mission, both in terms of the material performance and the overall stability of the shape of the balloon. An experimental investigation of the time dependence of the biaxial strain distribution in the film of a 4 m diameter, 48 gore pumpkin balloon is presented. The inflated shape of selected gores has been measured using photogrammetry and the time variation in strain components at some particular points of these gores has been measured under constant pressure and temperature. The results show good correlation with a numerical study, using the ABAQUS finite-element package, that includes a widely used model of the visco-elastic response of the gore material:

Measurement of the mechanical properties of car body sheet steels at high strain rates and non ambient temperature

NASA Astrophysics Data System (ADS)

Bleck, W.; Larour, P.

2003-09-01

Crash behaviour and light weight have become the major design criteria for car bodies. Modem high strength steels offer appropriate solutions for these requirements. The prediction of the crash behaviour in simulation programs requires the information on materials behaviour during dynamic testing. The reduction of the signal waviness and the inertia effects at strain rates above 50s^{-1} are major issues in dynamic tensile testing. Damping techniques or load measurement on the sample itself are the common way to reduce oscillations. Strain measurement from the piston displacement or from optical devices on the specimen itself are also compared. Advantages and drawbacks of those various measurement techniques are presented.

Determining the mechanical constitutive properties of metals as a function of strain rate and temperature: A combined experimental and modeling approach

DOE Office of Scientific and Technical Information (OSTI.GOV)

I. M. Robertson; A. Beaudoin; J. Lambros

2004-01-05

OAK-135 Development and validation of constitutive models for polycrystalline materials subjected to high strain rate loading over a range of temperatures are needed to predict the response of engineering materials to in-service type conditions (foreign object damage, high-strain rate forging, high-speed sheet forming, deformation behavior during forming, response to extreme conditions, etc.). To account accurately for the complex effects that can occur during extreme and variable loading conditions, requires significant and detailed computational and modeling efforts. These efforts must be closely coupled with precise and targeted experimental measurements that not only verify the predictions of the models, but also providemore » input about the fundamental processes responsible for the macroscopic response. Achieving this coupling between modeling and experimentation is the guiding principle of this program. Specifically, this program seeks to bridge the length scale between discrete dislocation interactions with grain boundaries and continuum models for polycrystalline plasticity. Achieving this goal requires incorporating these complex dislocation-interface interactions into the well-defined behavior of single crystals. Despite the widespread study of metal plasticity, this aspect is not well understood for simple loading conditions, let alone extreme ones. Our experimental approach includes determining the high-strain rate response as a function of strain and temperature with post-mortem characterization of the microstructure, quasi-static testing of pre-deformed material, and direct observation of the dislocation behavior during reloading by using the in situ transmission electron microscope deformation technique. These experiments will provide the basis for development and validation of physically-based constitutive models, which will include dislocation-grain boundary interactions for polycrystalline systems. One aspect of the program will involve the dire ct observation of specific mechanisms of micro-plasticity, as these will indicate the boundary value problem that should be addressed. This focus on the pre-yield region in the quasi-static effort (the elasto-plastic transition) is also a tractable one from an experimental and modeling viewpoint. In addition, our approach will minimize the need to fit model parameters to experimental data to obtain convergence. These are critical steps to reach the primary objective of simulating and modeling material performance under extreme loading conditions. In this annual report, we describe the progress made in the first year of this program.« less

Giant lateral electrostriction in ferroelectric liquid-crystalline elastomers

NASA Astrophysics Data System (ADS)

Lehmann, W.; Skupin, H.; Tolksdorf, C.; Gebhard, E.; Zentel, R.; Krüger, P.; Lösche, M.; Kremer, F.

2001-03-01

Mechanisms for converting electrical energy into mechanical energy are essential for the design of nanoscale transducers, sensors, actuators, motors, pumps, artificial muscles, and medical microrobots. Nanometre-scale actuation has to date been mainly achieved by using the (linear) piezoelectric effect in certain classes of crystals (for example, quartz), and `smart' ceramics such as lead zirconate titanate. But the strains achievable in these materials are small-less than 0.1 per cent-so several alternative materials and approaches have been considered. These include grafted polyglutamates (which have a performance comparable to quartz), silicone elastomers (passive material-the constriction results from the Coulomb attraction of the capacitor electrodes between which the material is sandwiched) and carbon nanotubes (which are slow). High and fast strains of up to 4 per cent within an electric field of 150MVm-1 have been achieved by electrostriction (this means that the strain is proportional to the square of the applied electric field) in an electron-irradiated poly(vinylidene fluoride-trifluoroethylene) copolymer. Here we report a material that shows a further increase in electrostriction by two orders of magnitude: ultrathin (less than 100nanometres) ferroelectric liquid-crystalline elastomer films that exhibit 4 per cent strain at only 1.5 MVm-1. This giant electrostriction was obtained by combining the properties of ferroelectric liquid crystals with those of a polymer network. We expect that these results, which can be completely understood on a molecular level, will open new perspectives for applications.

Elevated temperature strain gages

NASA Technical Reports Server (NTRS)

Brittain, J. O.; Geslin, D.; Lei, J. F.

1986-01-01

One of the goals of the HOST Program is the development of electrical resistance strain gages for static strain measurements at temperatures equal to or greater than 1273 K. Strain gage materials must have a reproducible or predictable response to temperature, time and strain. It is the objective of this research to investigate criteria for the selection of materials for such applications through electrical properties studies. The results of the investigation of two groups of materials, refractory compounds and binary alloy solid solutions are presented.

Strain rate sensitivity of the tensile strength of two silicon carbides: experimental evidence and micromechanical modelling

NASA Astrophysics Data System (ADS)

Zinszner, Jean-Luc; Erzar, Benjamin; Forquin, Pascal

2017-01-01

Ceramic materials are commonly used to design multi-layer armour systems thanks to their favourable physical and mechanical properties. However, during an impact event, fragmentation of the ceramic plate inevitably occurs due to its inherent brittleness under tensile loading. Consequently, an accurate model of the fragmentation process is necessary in order to achieve an optimum design for a desired armour configuration. In this work, shockless spalling tests have been performed on two silicon carbide grades at strain rates ranging from 103 to 104 s-1 using a high-pulsed power generator. These spalling tests characterize the tensile strength strain rate sensitivity of each ceramic grade. The microstructural properties of the ceramics appear to play an important role on the strain rate sensitivity and on the dynamic tensile strength. Moreover, this experimental configuration allows for recovering damaged, but unbroken specimens, giving unique insight on the fragmentation process initiated in the ceramics. All the collected data have been compared with corresponding results of numerical simulations performed using the Denoual-Forquin-Hild anisotropic damage model. Good agreement is observed between numerical simulations and experimental data in terms of free surface velocity, size and location of the damaged zones along with crack density in these damaged zones. This article is part of the themed issue 'Experimental testing and modelling of brittle materials at high strain rates'.

Johnson-Cook Strength Model for Automotive Steels

NASA Astrophysics Data System (ADS)

Vedantam, K.

2005-07-01

Over the last few years most automotive companies are engaged in performing simulations of the capability of individual components or entire structure of a motor vehicle to adequately sustain the shock (impacts) and to protect the occupants from injuries during crashes. These simulations require constitutive material models (e.g., Johnson-Cook) of the sheet steel and other components based on the compression/tension data obtained in a series of tests performed at quasi-static (˜1/s) to high strain rates (˜2000/s). One such study is undertaken by the recently formed IISI (International Iron and Steel Institute) in organizing the round robin tests to compare the tensile data generated at our Laboratory at strain rates of ˜1/s, ˜300/s, ˜800/s, and ˜2000/s on two grades of automotive steel (Mild steel and Dual Phase-DP 590) using split Hopkinson bar with those generated at high strain rate testing facilities in Germany and Japan. Our tension data on mild steel (flow stress ˜ 500 MPa) suggest a relatively small strain rate sensitivity of the material. The second steel grade (DP-590) tested exhibits significant strain rate sensitivity in that the flow stress increases from about 700 MPa (at ˜1/s) to 900 MPa (at ˜2000/s). J-C strength model constants (A, B, n, and C) for the two steel grades will be presented.

Strain rate sensitivity of the tensile strength of two silicon carbides: experimental evidence and micromechanical modelling.

PubMed

Zinszner, Jean-Luc; Erzar, Benjamin; Forquin, Pascal

2017-01-28

Ceramic materials are commonly used to design multi-layer armour systems thanks to their favourable physical and mechanical properties. However, during an impact event, fragmentation of the ceramic plate inevitably occurs due to its inherent brittleness under tensile loading. Consequently, an accurate model of the fragmentation process is necessary in order to achieve an optimum design for a desired armour configuration. In this work, shockless spalling tests have been performed on two silicon carbide grades at strain rates ranging from 10 3 to 10 4  s -1 using a high-pulsed power generator. These spalling tests characterize the tensile strength strain rate sensitivity of each ceramic grade. The microstructural properties of the ceramics appear to play an important role on the strain rate sensitivity and on the dynamic tensile strength. Moreover, this experimental configuration allows for recovering damaged, but unbroken specimens, giving unique insight on the fragmentation process initiated in the ceramics. All the collected data have been compared with corresponding results of numerical simulations performed using the Denoual-Forquin-Hild anisotropic damage model. Good agreement is observed between numerical simulations and experimental data in terms of free surface velocity, size and location of the damaged zones along with crack density in these damaged zones.This article is part of the themed issue 'Experimental testing and modelling of brittle materials at high strain rates'. © 2016 The Author(s).

Strain rate sensitivity of the tensile strength of two silicon carbides: experimental evidence and micromechanical modelling

PubMed Central

Erzar, Benjamin

2017-01-01

Ceramic materials are commonly used to design multi-layer armour systems thanks to their favourable physical and mechanical properties. However, during an impact event, fragmentation of the ceramic plate inevitably occurs due to its inherent brittleness under tensile loading. Consequently, an accurate model of the fragmentation process is necessary in order to achieve an optimum design for a desired armour configuration. In this work, shockless spalling tests have been performed on two silicon carbide grades at strain rates ranging from 103 to 104 s−1 using a high-pulsed power generator. These spalling tests characterize the tensile strength strain rate sensitivity of each ceramic grade. The microstructural properties of the ceramics appear to play an important role on the strain rate sensitivity and on the dynamic tensile strength. Moreover, this experimental configuration allows for recovering damaged, but unbroken specimens, giving unique insight on the fragmentation process initiated in the ceramics. All the collected data have been compared with corresponding results of numerical simulations performed using the Denoual–Forquin–Hild anisotropic damage model. Good agreement is observed between numerical simulations and experimental data in terms of free surface velocity, size and location of the damaged zones along with crack density in these damaged zones. This article is part of the themed issue ‘Experimental testing and modelling of brittle materials at high strain rates’. PMID:27956504

Deformation twinning of a silver nanocrystal under high pressure. Supplementary materials

DOE PAGES

Huang, X. J.; Yang, W. G.; Harder, R.; ...

2015-10-20

Within a high-pressure environment, crystal deformation is controlled by complex processes such as dislocation motion, twinning, and phase transitions, which change materials’ microscopic morphology and alter their properties. Likewise, understanding a crystal’s response to external stress provides a unique opportunity for rational tailoring of its functionalities. It is very challenging to track the strain evolution and physical deformation from a single nanoscale crystal under high-pressure stress. Here, we report an in situ three-dimensional mapping of morphology and strain evolutions in a single-crystal silver nanocube within a high-pressure environment using the Bragg Coherent Diffractive Imaging (CDI) method. We also observed amore » continuous lattice distortion, followed by a deformation twining process at a constant pressure. The ability to visualize stress-introduced deformation of nanocrystals with high spatial resolution and prominent strain sensitivity provides an important route for interpreting and engineering novel properties of nanomaterials.« less

Coherent pulse interrogation system for fiber Bragg grating sensing of strain and pressure in dynamic extremes of materials

DOE PAGES

Rodriguez, George; Jaime, Marcelo; Balakirev, Fedor; ...

2015-05-21

A 100 MHz fiber Bragg grating (FBG) interrogation system is described and applied to strain and pressure sensing. The approach relies on coherent pulse illumination of the FBG sensor with a broadband short pulse from a femtosecond modelocked erbium fiber laser. After interrogation of the FBG sensor, a long multi-kilometer run of single mode fiber is used for chromatic dispersion to temporally stretch the spectral components of the reflected pulse from the FBG sensor. Dynamic strain or pressure induced spectral shifts in the FBG sensor are detected as a pulsed time domain waveform shift after encoding by the chromatic dispersivemore » line. Signals are recorded using a single 35 GHz photodetector and a 50 GSamples per second, 25 GHz bandwidth, digitizing oscilloscope. Application of this approach to high-speed strain sensing in magnetic materials in pulsed magnetic fields to ~150 T is demonstrated. The FBG wavelength shifts are used to study magnetic field driven magnetostriction effects in LaCoO₃. A sub-microsecond temporal shift in the FBG sensor wavelength attached to the sample under first order phase change appears as a fractional length change (strain: ΔL/L<10⁻⁴) in the material. A second application used FBG sensing of pressure dynamics to nearly 2 GPa in the thermal ignition of the high explosive PBX-9501 is also demonstrated. In conclusion, both applications demonstrate the use of this FBG interrogation system in dynamical extreme conditions that would otherwise not be possible using traditional FBG interrogation approaches that are deemed too slow to resolve such events.« less