Development of Benchmark Examples for Quasi-Static Delamination Propagation and Fatigue Growth Predictions

NASA Technical Reports Server (NTRS)

Krueger, Ronald

2012-01-01

The development of benchmark examples for quasi-static delamination propagation and cyclic delamination onset and growth prediction is presented and demonstrated for Abaqus/Standard. The example is based on a finite element model of a Double-Cantilever Beam specimen. The example is independent of the analysis software used and allows the assessment of the automated delamination propagation, onset and growth prediction capabilities in commercial finite element codes based on the virtual crack closure technique (VCCT). First, a quasi-static benchmark example was created for the specimen. Second, based on the static results, benchmark examples for cyclic delamination growth were created. Third, the load-displacement relationship from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. Fourth, starting from an initially straight front, the delamination was allowed to grow under cyclic loading. The number of cycles to delamination onset and the number of cycles during delamination growth for each growth increment were obtained from the automated analysis and compared to the benchmark examples. Again, good agreement between the results obtained from the growth analysis and the benchmark results could be achieved by selecting the appropriate input parameters. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Selecting the appropriate input parameters, however, was not straightforward and often required an iterative procedure. Overall the results are encouraging, but further assessment for mixed-mode delamination is required.

Delamination growth analysis in quasi-isotropic laminates under loads simulating low-velocity impact

NASA Technical Reports Server (NTRS)

Shivakumar, K. N.; Elber, W.

1984-01-01

A geometrically nonlinear finite-element analysis has been developed to calculate the strain energy released by delaminating plates during impact loading. Only the first mode of deformation, which is equivalent to static deflection, was treated. Both the impact loading and delamination in the plate were assumed to be axisymmetric. The strain energy release rate in peeling, GI, and shear sliding, GII, modes were calculated using the fracture mechanics crack closure technique. Energy release rates for various delamination sizes and locations and for various plate configurations and materials were compared. The analysis indicated that shear sliding was the primary mode of delamination growth. The analysis also indicated that the midplane (maximum transverse shear stress plane) delamination was more critical and would grow first before any other delamination of the same size near the midplane region. The delamination growth rate was higher (neutrally stable) for a low toughness (brittle) matrix and slower (stable) for high toughness matrix. The energy release rate in the peeling mode, GI, for a near-surface delamination can be as high as 0.5GII, and can contribute significantly to the delamination growth.

Analysis of Delamination Growth from Matrix Cracks in Laminates Subjected to Bending Loads

NASA Technical Reports Server (NTRS)

Murri, G. B.; Guynn, E. G.

1986-01-01

A major source of delamination damage in laminated composite materials is from low-velocity impact. In thin composite laminates under point loads, matrix cracks develop first in the plies, and delaminations then grow from these cracks at the ply interfaces. The purpose of this study was to quantify the combined effects of bending and transverse shear loads on delamination initiation from matrix cracks. Graphite-epoxy laminates with 90 deg. plies on the outside were used to provide a two-dimensional simulation of the damage due to low-velocity impact. Three plate bending problems were considered: a 4-point bending, 3-point bending, and an end-clamped center-loaded plate. Under bending, a matrix crack will form on the tension side of the laminate, through the outer 90 deg. plies and parallel to the fibers. Delaminations will then grow in the interface between the cracked 90 deg. ply and the next adjacent ply. Laminate plate theory was used to derive simple equations relating the total strain energy release rate, G, associated with the delamination growth from a 90 deg. ply crack to the applied bending load and laminate stiffness properties. Three different lay-ups were tested and results compared. Test results verified that the delamination always formed at the interface between the cracked 90 deg. ply and the next adjacent ply. Calculated values for total G sub c from the analysis showed good agreement for all configurations. The analysis was able to predict the delamination onset load for the cases considered. The result indicated that the opening mode component (Mode I) for delamination growth from a matrix crack may be much larger than the component due to interlaminar shear (Mode II).

Characterization of Mode 1 and Mode 2 delamination growth and thresholds in graphite/peek composites

NASA Technical Reports Server (NTRS)

Martin, Roderick H.; Murri, Gretchen B.

1988-01-01

Composite materials often fail by delamination. The onset and growth of delamination in AS4/PEEK, a tough thermoplastic matrix composite, was characterized for mode 1 and mode 2 loadings, using the Double Cantilever Beam (DCB) and the End Notched Flexure (ENF) test specimens. Delamination growth per fatigue cycle, da/dN, was related to strain energy release rate, G, by means of a power law. However, the exponents of these power laws were too large for them to be adequately used as a life prediction tool. A small error in the estimated applied loads could lead to large errors in the delamination growth rates. Hence strain energy release rate thresholds, G sub th, below which no delamination would occur were also measured. Mode 1 and 2 threshold G values for no delamination growth were found by monitoring the number of cycles to delamination onset in the DCB and ENF specimens. The maximum applied G for which no delamination growth had occurred until at least 1,000,000 cycles was considered the threshold strain energy release rate. Comments are given on how testing effects, facial interference or delamination front damage, may invalidate the experimental determination of the constants in the expression.

Fractography of composite delamination

NASA Technical Reports Server (NTRS)

Bascom, W. D.

1989-01-01

Delamination is a major failure mode of carbon fiber organic matrix composites. It can occur under a variety of loading conditions. Efforts to develop predictive models of the delamination of carbon fiber composites are hampered by a lack of information about the micromechanics of impact damage and delamination growth. Crack formation and propagation in these materials cannot be observed in sufficient detail to determine micro-damage using currently available nondestructive methods such as acoustic backscattering or x ray imaging. Consequently, destructive methods are required. Delamination of composites in Mode I, Mode II and after low energy impact loads were investigated using metallographic techniques of potting the failed specimens, sectioning and examining the cut sections for damage modes.

Delamination growth in composite materials

NASA Technical Reports Server (NTRS)

Gillespie, J. W., Jr.; Carlsson, L. A.; Pipes, R. B.; Rothschilds, R.; Trethewey, B.; Smiley, A.

1986-01-01

The Double Cantilever Beam (DCB) and the End Notched Flexure (ENF) specimens are employed to characterize MODE I and MODE II interlaminar fracture resistance of graphite/epoxy (CYCOM 982) and graphite/PEEK (APC2) composites. Sizing of test specimen geometries to achieve crack growth in the linear elastic regime is presented. Data reduction schemes based upon beam theory are derived for the ENF specimen and include the effects of shear deformation and friction between crack surfaces on compliance, C, and strain energy release rate, G sub II. Finite element (FE) analyses of the ENF geometry including the contact problem with friction are presented to assess the accuracy of beam theory expressions for C and G sub II. Virtual crack closure techniques verify that the ENF specimen is a pure Mode II test. Beam theory expressions are shown to be conservative by 20 to 40 percent for typical unidirectional test specimen geometries. A FE parametric study investigating the influence of delamination length and depth, span, thickness and material properties on G sub II is presented. Mode I and II interlaminar fracture test results are presented. Important experimental parameters are isolated, such as precracking techniques, rate effects, and nonlinear load-deflection response. It is found that subcritical crack growth and inelastic materials behavior, responsible for the observed nonlinearities, are highly rate-dependent phenomena with high rates generally leading to linear elastic response.

The fatigue growth of internal delaminations under compressive loading of cross-ply composite plates

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pelegri, A.A.; Kardomateas, G.A.; Malik, B.U.

1997-12-31

This study focuses on the mode dependence of delamination growth under cyclic compressive loads in cross-ply composite plates. The model proposed makes use of an initial postbuckling solution derived from a perturbation procedure. A mode-dependent crack growth criterion is introduced. Expressions describing the fatigue crack growth are derived in terms of the distribution of the mode adjusted energy release rate. The resulting crack growth laws are numerically integrated to produce delamination growth versus number of cycles diagrams. The model does not impose any restrictive assumptions on the relative thickness of the delaminated and the base plates, although transverse shear stressmore » effects are not considered. Experimental results are presented for cross-ply graphite/epoxy specimens, and the results are compared with experimental results for unidirectional specimens. The test data are obtained for different delamination locations and for different values of applied compressive strain.« less

Strain energy release rate analysis of cyclic delamination growth in compressively loaded laminates

NASA Technical Reports Server (NTRS)

Whitcomb, J. D.

1983-01-01

Delamination growth in compressively loaded composite laminates was studied analytically and experimentally. The configuration used was a laminate with an across-the-width delamination. An approximate super-position stress analysis was developed to quantify the effects of various geometric, material, and load parameters on mode 2 and mode 2 strain energy release rates G sub/1 and G sub 2, respectively. Calculated values of G sub 1 and G sub 2 were then compared with measured cyclic delamination growth rates to determine the relative importance of G sub 1 and G sub 2. High growth rates were observed only when G sub 1 was large. However, slow growth was observed even when G sub 1 was negligibly small. This growth apparently was due to a large value of G sub 2.

Development and Application of Benchmark Examples for Mode II Static Delamination Propagation and Fatigue Growth Predictions

NASA Technical Reports Server (NTRS)

Krueger, Ronald

2011-01-01

The development of benchmark examples for static delamination propagation and cyclic delamination onset and growth prediction is presented and demonstrated for a commercial code. The example is based on a finite element model of an End-Notched Flexure (ENF) specimen. The example is independent of the analysis software used and allows the assessment of the automated delamination propagation, onset and growth prediction capabilities in commercial finite element codes based on the virtual crack closure technique (VCCT). First, static benchmark examples were created for the specimen. Second, based on the static results, benchmark examples for cyclic delamination growth were created. Third, the load-displacement relationship from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. Fourth, starting from an initially straight front, the delamination was allowed to grow under cyclic loading. The number of cycles to delamination onset and the number of cycles during delamination growth for each growth increment were obtained from the automated analysis and compared to the benchmark examples. Again, good agreement between the results obtained from the growth analysis and the benchmark results could be achieved by selecting the appropriate input parameters. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Selecting the appropriate input parameters, however, was not straightforward and often required an iterative procedure. Overall the results are encouraging, but further assessment for mixed-mode delamination is required.

Development of Benchmark Examples for Delamination Onset and Fatigue Growth Prediction

NASA Technical Reports Server (NTRS)

Krueger, Ronald

2011-01-01

An approach for assessing the delamination propagation and growth capabilities in commercial finite element codes was developed and demonstrated for the Virtual Crack Closure Technique (VCCT) implementations in ABAQUS. The Double Cantilever Beam (DCB) specimen was chosen as an example. First, benchmark results to assess delamination propagation capabilities under static loading were created using models simulating specimens with different delamination lengths. For each delamination length modeled, the load and displacement at the load point were monitored. The mixed-mode strain energy release rate components were calculated along the delamination front across the width of the specimen. A failure index was calculated by correlating the results with the mixed-mode failure criterion of the graphite/epoxy material. The calculated critical loads and critical displacements for delamination onset for each delamination length modeled were used as a benchmark. The load/displacement relationship computed during automatic propagation should closely match the benchmark case. Second, starting from an initially straight front, the delamination was allowed to propagate based on the algorithms implemented in the commercial finite element software. The load-displacement relationship obtained from the propagation analysis results and the benchmark results were compared. Good agreements could be achieved by selecting the appropriate input parameters, which were determined in an iterative procedure.

The Use of Doublers in Delamination Toughness Testing

NASA Technical Reports Server (NTRS)

Reeder, James R.; Demarco, Kevin; Whitley, Karen S.

2002-01-01

In this paper, the data reduction equations for common delamination toughness tests are rederived for use with specimens which have bonded doublers. The common toughness tests considered here are the double cantilever beam (DCB) for mode I toughness; the end notch flexure (3ENF) and 4 point ENF (4ENF) for mode II toughness; and the mixed mode bending (MMB) test for testing under combined mode I and mode II loading. Because the addition of the doublers changes the bending stiffness of the specimens, these data reduction equations may need to be corrected. Doublers were added to the delamination test specimens to solve a premature failure problem. Delamination toughness is normally tested using a beam with an imbedded insert so that one end of the specimen is split into two arms. If the specimen is too thin, or if the toughness of the material is too high, an arm of the specimen may fail in bending before the delamination grows. When this occurs, the toughness of the material cannot be determined. To delay the bending failure so that delamination growth occurs, doubler plates were bonded to both top and bottom surfaces of the specimen. A doubler parameter, beta, which describes how much the use of doubler plates changed the ratio of full thickness to delaminated bending stiffnesses, was defined. When changes to the data reduction equations were required, the changes were minor when written in terms of the beta parameter. The doubler plate technique was demonstrated by measuring the mixed-mode fracture toughness of a carbon-carbon composite using test specimens which would otherwise have failed before delamination growth occurred. The doubler plate technique may solve several problems that can be encountered when testing delamination fracture toughness.

The mechanics of delamination in fiber-reinforced composite materials. I - Stress singularities and solution structure

NASA Technical Reports Server (NTRS)

Wang, S. S.; Choi, I.

1983-01-01

The fundamental mechanics of delamination in fiber composite laminates is studied. Mathematical formulation of the problem is based on laminate anisotropic elasticity theory and interlaminar fracture mechanics concepts. Stress singularities and complete solution structures associated with general composite delaminations are determined. For a fully open delamination with traction-free surfaces, oscillatory stress singularities always appear, leading to physically inadmissible field solutions. A refined model is introduced by considering a partially closed delamination with crack surfaces in finite-length contact. Stress singularities associated with a partially closed delamination having frictional crack-surface contact are determined, and are found to be different from the inverse square-root one of the frictionless-contact case. In the case of a delamination with very small area of crack closure, a simplified model having a square-root stress singularity is employed by taking the limit of the partially closed delamination. The possible presence of logarithmic-type stress singularity is examined; no logarithmic singularity of any kind is found in the composite delamination problem. Numerical examples of dominant stress singularities are shown for delaminations having crack-tip closure with different frictional coefficients between general (1) and (2) graphite-epoxy composites. Previously announced in STAR as N84-13221

Characterizing Delamination Migration in Carbon/Epoxy Tape Laminates

NASA Technical Reports Server (NTRS)

Ratcliffe, James G.; Czabaj, Michael W.; Obrien, Thomas K.

2012-01-01

A new test method is presented for the purpose of investigating migration of a delamination between neighboring ply interfaces in fiber-reinforced, polymer matrix tape laminates. The test is a single cantilever beam configuration consisting of a cross-ply laminate with a polytetrafluoroethylene (PTFE) insert implanted at the mid-plane and spanning part way along the length of the specimen. The insert is located between a 0-degree ply (specimen length direction) and a stack of four 90-degree plies (specimen width direction). The specimen is clamped at both ends onto a rigid baseplate and is loaded on its upper surface via a piano hinge. Tests were conducted with the load-application point located on the intact portion of the specimen in order to initiate delamination growth onset followed by migration of the delamination to a neighboring 90/0 ply interface by kinking through the 90- degree ply stack. Varying this position was found to affect the distance relative to the load-application point at which migration initiated. In each specimen, migration initiated by a gradual transition of the delamination at the 0/90 interface into the 90- degree ply stack. In contrast, transition of the kinked crack into the 90/0 interface was sudden. Fractography of the specimens indicated that delamination prior to migration was generally mixed mode-I/II. Inspection of the kink surface revealed mode-I fracture. In general, use of this test allows for the observation of the growth of a delamination followed by migration of the delamination to another ply interface, and should thus provide a means for validating analyses aimed at simulating migration.

Development and Application of Benchmark Examples for Mixed-Mode I/II Quasi-Static Delamination Propagation Predictions

NASA Technical Reports Server (NTRS)

Krueger, Ronald

2012-01-01

The development of benchmark examples for quasi-static delamination propagation prediction is presented and demonstrated for a commercial code. The examples are based on finite element models of the Mixed-Mode Bending (MMB) specimen. The examples are independent of the analysis software used and allow the assessment of the automated delamination propagation prediction capability in commercial finite element codes based on the virtual crack closure technique (VCCT). First, quasi-static benchmark examples were created for the specimen. Second, starting from an initially straight front, the delamination was allowed to propagate under quasi-static loading. Third, the load-displacement relationship from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. Good agreement between the results obtained from the automated propagation analysis and the benchmark results could be achieved by selecting input parameters that had previously been determined during analyses of mode I Double Cantilever Beam and mode II End Notched Flexure specimens. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Overall the results are encouraging, but further assessment for mixed-mode delamination fatigue onset and growth is required.

Combined effect of matrix cracking and stress-free edge on delamination

NASA Technical Reports Server (NTRS)

Salpekar, S. A.; Obrien, T. K.

1990-01-01

The effect of the stress-free edge on the growth of local delaminations initiating from a matrix crack in (0 sub 2/90 sub 4) sub s and (+ or - 45.90 sub 4) sub s glass epoxy laminates is investigated using 3-D finite element analysis. The presence of high interlaminar normal stresses at the intersection (corner) of the matrix crack with the stress-free edge, suggests that a mode I delamination may initiate at the corners. The strain energy release rates (G) were calculated by modeling a uniform through-width delamination and two inclined delaminations at 10.6 deg and 45 deg to the matrix crack. All components of G have high values near the free edges. The mode I component of G is high at small delamination length and becomes zero for a delamination length of one-ply thickness. The total G values near the free edge agreed well with previously derived closed form solution. The quasi-3D solutions agreed well with the 3-D interior solutions.

Combined effect of matrix cracking and stress-free edge on delamination

NASA Technical Reports Server (NTRS)

Salpekar, Satish A.; O'Brien, T. K.

1991-01-01

The effect of the stress-free edge on the growth of local delaminations initiating from a matrix crack in (O sub 2/90 sub 4) sub s and (+/- 45.90 sub 4) sub s glass epoxy laminates is investigated using 3D finite element analysis. The presence of high interlaminar normal stresses at the intersection (corner) of the matrix crack with the stress-free edge, suggests that a mode I delamination may initiate at the corners. The strain energy release rates (G) were calculated by modeling a uniform through-width delamination and two inclined delaminations at 10.6 deg and 45 deg to the matrix crack. All components of G have high values near the free edges. The mode I component of G is high at small delamination length and becomes zero for a delamination length of one-ply thickness. The total G values near the free edge agreed well with previously derived closed form solution. The quasi-3D solutions agreed well with the 3D interior solutions.

An Enriched Shell Element for Delamination Simulation in Composite Laminates

NASA Technical Reports Server (NTRS)

McElroy, Mark

2015-01-01

A formulation is presented for an enriched shell finite element capable of delamination simulation in composite laminates. The element uses an adaptive splitting approach for damage characterization that allows for straightforward low-fidelity model creation and a numerically efficient solution. The Floating Node Method is used in conjunction with the Virtual Crack Closure Technique to predict delamination growth and represent it discretely at an arbitrary ply interface. The enriched element is verified for Mode I delamination simulation using numerical benchmark data. After determining important mesh configuration guidelines for the vicinity of the delamination front in the model, a good correlation was found between the enriched shell element model results and the benchmark data set.

Strain energy release rate analysis of delamination in a tapered laminate subjected to tension load

NASA Technical Reports Server (NTRS)

Salpekar, S. A.; Raju, I. S.; Obrien, T. K.

1990-01-01

A tapered composite laminate subjected to tension load was analyzed using the finite-element method. The glass/epoxy laminate has a (+ or - 45)sub 3 group of plies dropped in three distinct steps, each 20 ply-thicknesses apart, thus forming a taper angle of 5.71 degrees. Steep gradients of interlaminar normal and shear stress on a potential delamination interface suggest the existence of stress singularities at the points of material and geometric discontinuities created by the internal plydrops. The delamination was assumed to initiate at the thin end of the taper on a -45/+45 interface and the delamination growth was simulated in both directions, i.e., along the taper and into the thin region. The strain-energy-release rate for a delamination growing into the thin laminate consisted predominantly of mode I (opening) component. For a delamination growing along the tapered region, the strain-energy-release rate was initially all mode I, but the proportion of mode I decreased with increase in delamination size until eventually total G was all mode II. The total G for both delamination tips increased with increase in delamination size, indicating that a delamination initiating at the end of the taper will grow unstably along the taper and into the thin laminate simultaneously.

A Test for Characterizing Delamination Migration in Carbon/Epoxy Tape Laminates

NASA Technical Reports Server (NTRS)

Ratcliffe, James G.; Czabaj, Michael W.; O'Brien, Thomas K.

2013-01-01

A new test method is presented for the purpose of investigating migration of a delamination between neighboring ply interfaces in fiber-reinforced, polymer matrix tape laminates. The test is a single cantilever beam configuration consisting of a cross-ply laminate with a polytetrafluoroethylene insert implanted at the mid-plane and spanning part way along the length of the specimen. The insert is located between a 0- degree ply (specimen length direction) and a stack of four 90-degree plies (specimen width direction). The specimen is clamped at both ends onto a rigid baseplate and is loaded on its upper surface via a piano hinge. Tests were conducted with the load-application point located on the intact portion of the specimen in order to initiate delamination growth onset followed by migration of the delamination to a neighboring 90/0 ply interface by kinking through the 90-degree ply stack. Varying this position was found to affect the distance relative to the load-application point at which migration initiated. In each specimen, migration initiated by a gradual transition of the delamination at the 0/90 interface into the 90-degree ply stack. In contrast, transition of the kinked crack into the 90/0 interface was sudden. Fractography of the specimens indicated that delamination prior to migration was generally mixed mode-I/II. Inspection of the kink surface revealed mode-I fracture. In general, use of this test allows for the observation of the growth of a delamination followed by migration of the delamination to another ply interface, and should thus provide a means for validating analyses aimed at simulating migration.

Compression behavior of delaminated composite plates

NASA Technical Reports Server (NTRS)

Peck, Scott O.; Springer, George S.

1989-01-01

The response of delaminated composite plates to compressive in-plane loads was investigated. The delaminated region may be either circular or elliptical, and may be located between any two plies of the laminate. For elliptical delaminations, the axes of the ellipse may be arbitrarily oriented with respect to the applied loads. A model was developed that describes the stresses, strains, and deformation of the sublaminate created by the delamination. The mathematical model is based on a two dimensional nonlinear plate theory that includes the effects of transverse shear deformation. The model takes into account thermal and moisture induced strains, transverse pressures acting on the sublaminate, and contact between the sublaminate and plate. The solution technique used is the Ritz method. A computationally efficient computer implementation of the model was developed. The code can be used to predict the nonlinear-load-strain behavior of the sublaminate including the buckling load, postbuckling behavior, and the onset of delamination growth. The accuracy of the code was evaluated by comparing the model results to benchmark analytical solutions. A series of experiments was conducted on Fiberite T300/976 graphite/epoxy laminates bonded to an aluminum honeycomb core forming a sandwich panel. Either circles or ellipses made from Teflon film were embedded in the laminates, simulating the presence of a delamination. Each specimen was loaded in compression and the strain history of the sublaminate was recorded far into the postbuckling regime. The extent of delamination growth was evaluated by C-scan examination of each specimen. The experimental data were compared to code predictions. The code was found to describe the data with reasonable accuracy. A sensitivity study examined the relative importance of various material properties, the delamination dimensions, the contact model, the transverse pressure differential, the critical strain energy release rate, and the relative

Micromechanical models of delamination in aluminum-lithium alloys

NASA Astrophysics Data System (ADS)

Messner, Mark Christian

Aluminum lithium (Al-Li) alloys are lighter, stiffer, and tougher than conventional aerospace aluminum alloys. Replacing conventional aluminums with Al-Li could substantially decrease the weight and cost of aerospace structures. However, Al-Li alloys often fracture intergranularly via a mechanism called delamination cracking. While secondary delamination cracks can improve the effective toughness of a component, no current model accurately predicts the initiation and growth of intergranular cracks. Since simulations cannot incorporate delamination into a structural model, designers cannot quantify the effect of delamination cracking on a particular component. This uncertainty limits the application of Al-Li alloys. Previous experiments identify microstructural features linked to delamination. Fractography of failed surfaces indicates plastic void growth triggers intergranular failure. Furthermore, certain types of soft/stiff grain boundaries tend to localize void growth and nucleate delamination cracks. This dissertation develops a mechanism for the initiation of delamination on the microscale that accounts for these experimental observations. Microscale simulations of grain boundaries near a long primary crack explore the delamination mechanism on the mesoscale. In these simulations, a physically-based crystal plasticity (CP) model represents the constitutive response of individual grains. This CP model incorporates plastic voriticity correction terms into a standard objective stress rate integration, to accurately account for the kinematics of lattice deformation. The CP model implements slip system hardening with a modular approach to facilitate quick testing and calibration of different theories of hardening. The microscale models reveal soft/stiff grain boundaries develop elevated mean stress and plastic strain as a consequence of the mechanics of the interface. These elevated stresses and strain drive plastic void growth. The results indicate plastic void

Delamination and debonding of materials

NASA Technical Reports Server (NTRS)

Johnson, W. S. (Editor)

1985-01-01

The general topics consist of stress analysis, mechanical behavior, and fractography/NDI of composite laminates. Papers are presented on a dynamic hybrid finite-element analysis for interfacial cracks in composites, energy release rate during delamination crack growth in composite laminates, matrix deformation and fracture in graphite-reinforced epoxies, and the role of delamination and damage development on the strength of thick notched laminates. In addition, consideration is given to a new ply model for interlaminar stress analysis, a fracture mechanics approach for designing adhesively bonded joints, the analysis of local delaminations and their influence on composite laminate behavior, and moisture and temperature effects on the mixed-mode delamination fracture of unidirectional graphite/epoxy.

Characteristics of laminates with delamination control strips

NASA Technical Reports Server (NTRS)

Sun, C. T.; Goering, J. C.; Alper, J. M.; Gause, L. W.

1992-01-01

Tough resin is needed to resist delamination crack propagation. However, modulus often has to be compromised because it is difficult to retain both high modulus and toughness in a matrix material. A potential solution is to use a hybrid system in which tough resin strips are included within a conventional matrix composite. By adjusting the spacing of the tough resin strips, maximum delamination size can be controlled. Experimental results for impact damage and subsequent damage propagation in laminates containing tough resin strips are reported. Plain adhesive strips and fiber-reinforced tough resin composite strips were used in constructing the hybrid laminates. Test results indicated that size of delamination inflicted by impact was confined between the tough resin strips. As a result, significantly increased residual compressive strength was obtained. Impacted laminates containing tough resin strips were also fatigue tested. It was found that these strips reduced the growth of the impact damage area relative to the growth seen in coupons with no tough resin strips. Damage growth from an open hole under tension fatigue was evaluated using both tough resin strips and glass fiber reinforced tough resin strips. Unreinforced tough resin strips retarded delamination growth from the open hole, but did not stop matrix cracks growing in the fiber direction. Fiber reinforced tough resin strips did not contain axial delamination growth from the open hole. However, they did act as crack arresters, stopping the through-the-thickness tension crack originating from the hole.

Development and Application of Benchmark Examples for Mixed-Mode I/II Quasi-Static Delamination Propagation Predictions

NASA Technical Reports Server (NTRS)

Krueger, Ronald

2012-01-01

The development of benchmark examples for quasi-static delamination propagation prediction is presented. The example is based on a finite element model of the Mixed-Mode Bending (MMB) specimen for 50% mode II. The benchmarking is demonstrated for Abaqus/Standard, however, the example is independent of the analysis software used and allows the assessment of the automated delamination propagation prediction capability in commercial finite element codes based on the virtual crack closure technique (VCCT). First, a quasi-static benchmark example was created for the specimen. Second, starting from an initially straight front, the delamination was allowed to propagate under quasi-static loading. Third, the load-displacement as well as delamination length versus applied load/displacement relationships from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Overall, the results are encouraging, but further assessment for mixed-mode delamination fatigue onset and growth is required.

Dynamic delamination crack propagation in a graphite/epoxy laminate

NASA Technical Reports Server (NTRS)

Grady, J. E.; Sun, C. T.

1991-01-01

Dynamic delamination crack propagation in a (90/0) 5s Graphite/Epoxy laminate with an embedded interfacial crack was investigated experimentally using high speed photography. The dynamic motion was produced by impacting the beamlike laminate specimen with a silicon rubber ball. The threshold impact velocities required to initiate dynamic crack propagation in laminates with varying initial crack positions were determined. The crack propagation speeds were estimated from the photographs. Results show that the through the thickness position of the embedded crack can significantly affect the dominant mechanism and the threshold impact velocity for the onset of crack movement. If the initial delamination is placed near the top of bottom surface of the laminate, local buckling of the delaminated plies may cause instability of the crack. If the initial delamination lies on the midplane, local buckling does not occur and the initiation of crack propagation appears to be dominated by Mode II fracture. The crack propagation and arrest observed was seen to be affected by wave motion within the delamination region.

Three-dimensional analysis of a postbuckled embedded delamination

NASA Technical Reports Server (NTRS)

Whitcomb, John D.

1988-01-01

Delamination growth caused by local buckling of a delaminated group of plies was investigated. Delamination growth was assumed to be governed by the strain energy release rates, G(1), G(2) and G(3). The strain energy release rates were calculated using a geometrically nonlinear three-dimensional finite element analysis. The program is described and several checks of the analysis are discussed. Based on a limited parametric study, the following conclusions were reached: (1) the problem is definitely mixed mode (in some cases G(1) is larger than G(2), for other cases the opposite is true); (2) in general, there is a large gradient in the strain energy release rates along the delamination front; (3) the locations of maximum G(1) and G(2) depend on the delamination shape and the applied strain; (4) the mode 3 component was negligible for all cases considered; and (5) the analysis predicted that parts of the delamination would overlap. The results presented did not impose contact constraints to prevent overlapping. Further work is needed to determine the effects of allowing the overlapping.

Delamination of Composite Cylinders

NASA Astrophysics Data System (ADS)

Davies, Peter; Carlsson, Leif A.

The delamination resistance of filament wound glass/epoxy cylinders has been characterized for a range of winding angles and fracture mode ratios using beam fracture specimens. The results reveal that the delamination fracture resistance increases with increasing winding angle and mode II (shear) fraction (GΠ/G). It was also found that interlaced fiber bundles in the filament wound cylinder wall acted as effective crack arresters in mode I loading. To examine the sensitivity of delamina-tion damage on the strength of the cylinders, external pressure tests were performed on filament-wound glass/epoxy composite cylinders with artificial defects and impact damage. The results revealed that the cylinder strength was insensitive to the presence of single delaminations but impact damage caused reductions in failure pressure. The insensitivity of the failure pressure to a single delamination is attributed to the absence of buckling of the delaminated sublaminates before the cylinder wall collapsed. The impacted cylinders contained multiple delaminations, which caused local reduction in the compressive load capability and reduction in failure pressure. The response of glass/epoxy cylinders was compared to impacted carbon reinforced cylinders. Carbon/epoxy is more sensitive to damage but retains higher implosion resistance while carbon/PEEK shows the opposite trend.

Delamination properity of 2060 aluminium lithium alloy laminate

NASA Astrophysics Data System (ADS)

Guo, Xiang; Huang, Yi; Tong, Dihua; Ma, Shaojun

2018-03-01

Delamination is an significant property of aluminium lithium alloy laminate for damage tolerance design. Double Crack Lap Shear specimens of "2/1" structure are used for testing delamination properity. Experiments of 2 stress ratio conditions R=0.06, 0.5 are conducted, and 5 stress levels for each stress ratio. Delamination growth data b-N are obtained from 4 crack tips’ locations. The energy release rate, Gd, of the "2/1" structure laminate are calculated. Alderliesten modelis used for describing delamination growth db/dN and energy release rate Gd. Parameters Cd and nd in Alderliesten model are determined for R=0.06 and R=0.5 by linear fitting. An analysis is made by comparing the results of different stress ratio conditons.

Analysis of delamination in cross-ply laminates initiating from impact induced matrix cracking

NASA Technical Reports Server (NTRS)

Salpekar, S. A.

1993-01-01

Two-dimensional finite element analyses of (02/90(8)/02) glass/epoxy and graphite/epoxy composite laminates were performed to investigate some of the characteristics of damage development due to an impact load. A cross section through the thickness of the laminate with fixed ends, and carrying a transverse load in the center, was analyzed. Inclined matrix cracks, such as those produced by a low-velocity impact, were modeled in the 90 deg ply group. The introduction of the matrix cracks caused large interlaminar tensile and shear stresses in the vicinity of both crack tips in the 0/90 and 90/0 interfaces, indicating that matrix cracking may give rise to delamination. The ratio of Mode I to total strain energy release rate, G(I)/G(total), at the beginning of delamination, calculated at the two (top and bottom) matrix crack tips was 60 and 28 percent, respectively, in the glass/epoxy laminate. The corresponding ratio was 97 and 77 percent in the graphite/epoxy laminate. Thus, a significant Mode I component of strain energy release rate may be present at the delamination initiation due to an impact load. The value of strain energy release rate at either crack tip increased due to an increase in the delamination length at the other crack tip and may give rise to an unstable delamination growth under constant load.

Predictive Methodology for Delamination Growth in Laminated Composites Part 1: Theoretical Development and Preliminary Experimental Results

DOT National Transportation Integrated Search

1998-04-01

A methodology is presented for the prediction of delamination growth in laminated structures. The methodology is aimed at overcoming computational difficulties in the determination of energy release rate and mode mix. It also addresses the issue that...

Guidelines and Parameter Selection for the Simulation of Progressive Delamination

NASA Technical Reports Server (NTRS)

Song, Kyongchan; Davila, Carlos G.; Rose, Cheryl A.

2008-01-01

Turon s methodology for determining optimal analysis parameters for the simulation of progressive delamination is reviewed. Recommended procedures for determining analysis parameters for efficient delamination growth predictions using the Abaqus/Standard cohesive element and relatively coarse meshes are provided for single and mixed-mode loading. The Abaqus cohesive element, COH3D8, and a user-defined cohesive element are used to develop finite element models of the double cantilever beam specimen, the end-notched flexure specimen, and the mixed-mode bending specimen to simulate progressive delamination growth in Mode I, Mode II, and mixed-mode fracture, respectively. The predicted responses are compared with their analytical solutions. The results show that for single-mode fracture, the predicted responses obtained with the Abaqus cohesive element correlate well with the analytical solutions. For mixed-mode fracture, it was found that the response predicted using COH3D8 elements depends on the damage evolution criterion that is used. The energy-based criterion overpredicts the peak loads and load-deflection response. The results predicted using a tabulated form of the BK criterion correlate well with the analytical solution and with the results predicted with the user-written element.

Development of a Composite Delamination Fatigue Life Prediction Methodology

NASA Technical Reports Server (NTRS)

OBrien, Thomas K.

2009-01-01

Delamination is one of the most significant and unique failure modes in composite structures. Because of a lack of understanding of the consequences of delamination and the inability to predict delamination onset and growth, many composite parts are unnecessarily rejected upon inspection, both immediately after manufacture and while in service. NASA Langley is leading the efforts in the U.S. to develop a fatigue life prediction methodology for composite delamination using fracture mechanics. Research being performed to this end will be reviewed. Emphasis will be placed on the development of test standards for delamination characterization, incorporation of approaches for modeling delamination in commercial finite element codes, and efforts to mature the technology for use in design handbooks and certification documents.

Analysis of local delaminations and their influence on composite laminate behavior

NASA Technical Reports Server (NTRS)

Obrien, T. K.

1985-01-01

An equation was derived for the strain energy release rate, G, associated with local delamination growth from a matrix ply crack. The critical GC for edge delamination onset in 25/902s graphite epoxy laminates was measured and used in this equation to predict local delamination onset strains in 25/90ns, n = 4, 6, 8 laminates. A simple technique for predicting strain concentrations in the primary load bearing plies near local delaminations was developed. These strain concentrations were responsible for reduced laminate nominal failure strains in laminates containing local delaminations. The influence of edge delamination and matrix crack tip delamination on laminate stiffness and strength was compared.

Analysis of local delaminations and their influence on composite laminate behavior

NASA Technical Reports Server (NTRS)

Obrien, T. K.

1984-01-01

An equation was derived for the strain energy release rate, G, associated with local delamination growth from a matrix ply crack. The critical GC for edge delamination onset in 25/902s graphite epoxy laminates was measured and used in this equation to predict local delamination onset strains in 25/90ns, n = 4, 6, 8 laminates. A simple technique for predicting strain concentrations in the primary load bearing plies near local delaminations was developed. These strain concentrations were responsible for reduced laminate nominal failure strains in laminates containing local delaminations. The influence of edge delamination and matrix crack tip delamination on laminate stiffness and strength was compared.

Critical current survival in the YBCO superconducting layer of a delaminated coated conductor

NASA Astrophysics Data System (ADS)

Feng, Feng; Fu, Qishu; Qu, Timing; Mu, Hui; Gu, Chen; Yue, Yubin; Wang, Linli; Yang, Zhirong; Han, Zhenghe; Feng, Pingfa

2018-04-01

A high-temperature superconducting coated conductor can be practically applied in electric equipment due to its favorable mechanical properties and critical current (I c) performance. However, the coated conductor can easily delaminate because of its poor stress tolerance along the thickness direction. It would be interesting to investigate whether the I c of the delaminated YBa2Cu3O7-δ (YBCO) layer can be preserved. In this study, coated conductor samples manufactured through the metal organic deposition route were delaminated by liquid nitrogen immersion. Delaminated samples, including the YBCO layer and silver stabilizer, were obtained. Delamination occurred inside the YBCO layer and near the YBCO-CeO2 interface, as suggested by the results of scanning electron microscopy (SEM) and x-ray diffraction. A scanning Hall probe system was employed to measure the I c distribution of the original sample and the delaminated sample. It was found that approximately 50% of the I c can be preserved after delamination, which was verified by I c measurements using the four-probe method. Dense and crack-free morphologies of the delaminated surfaces were observed by SEM, which accounts for the I c survival of the delaminated YBCO layer. The potential application of the delaminated sample in superconducting joints was discussed based on the oxygen diffusion estimation.

Fatigue delamination onset prediction in tapered composite laminates

NASA Technical Reports Server (NTRS)

Murri, Gretchen Bostaph; Salpekar, Satish A.; Obrien, T. Kevin

1989-01-01

Tapered (0 deg) laminates of S2/CE9000 and S2/SP250 glass/epoxies, and IM6/1827I graphite/epoxy were tested in cyclic tension. The specimens usually showed some initial stable delaminations in the tapered region, but these did not affect the stiffness of the specimens, and loading was continued until the specimens either delaminated unstably, or reached 10(exp 6) to 2 x 10(exp 7) million cycles with no unstable delamination. The final unstable delamination originated at the junction of the thin and tapered regions. A finite-element model was developed for the tapered laminate with and without the initial stable delaminations observed in the tests. The analysis showed that for both cases the most likely place for an opening (Mode 1) delamination to originate is at the junction of the taper and thin regions. For each material type, the models were used to calculate the strain energy release rate, G, associated with delaminations originating at that junction and growing either into the thin region or tapered region. For the materials tested, cyclic G(sub Imax) values from DCB tests were used with the maximum strain energy release rates calculated from the finite-element analysis to predict the onset of unstable delamination at the junction as a function of fatigue cycles. The predictions were compared to experimental values of maximum cyclic load as a function of cycles to unstable delamination from fatigue tests in tapered laminates. For the IM6/1827I and S2/SP250 laminates, the predictions agreed very well with the test data. Predicted values for the S2/CE9000 were conservative compared to the test data.

Impact Induced Delamination Detection and Quantification With Guided Wavefield Analysis

NASA Technical Reports Server (NTRS)

Tian, Zhenhua; Leckey, Cara A. C.; Yu, Lingyu; Seebo, Jeffrey P.

2015-01-01

This paper studies impact induced delamination detection and quantification by using guided wavefield data and spatial wavenumber imaging. The complex geometry impact-like delamination is created through a quasi-static indentation on a CFRP plate. To detect and quantify the impact delamination in the CFRP plate, PZT-SLDV sensing and spatial wavenumber imaging are performed. In the PZT-SLDV sensing, the guided waves are generated from the PZT, and the high spatial resolution guided wavefields are measured by the SLDV. The guided wavefield data acquired from the PZT-SLDV sensing represent guided wave propagation in the composite laminate and include guided wave interaction with the delamination damage. The measured guided wavefields are analyzed through the spatial wavenumber imaging method, which generates an image containing the dominant local wavenumber at each spatial location. The spatial wavenumber imaging result for the simple single layer Teflon insert delamination provided quantitative information on delamination damage size and location. The location of delamination damage is indicated by the area with larger wavenumbers in the spatial wavenumber image. The impact-like delamination results only partially agreed with the damage size and shape. The results also demonstrated the dependence on excitation frequency. Future work will further investigate the accuracy of the wavenumber imaging method for real composite damage and the dependence on frequency of excitation.

Delaminated sodium nonatitanate and a method for producing delaminated sodium nonatitanate

DOEpatents

Nyman, May D.

2016-02-02

A hydrothermal synthesis method of making a delaminated titanate is disclosed. The delaminated titanate has a unique structure or morphology. The delaminated titanate is first formed by forming at a low temperature a layered sodium nonatitanate (SNT), which may be referred to as layered sodium titanate. The layered SNT has a unique morphology. The layered SNT is then synthesized into a delaminated titanate having a unique morphology.

Assessment of Static Delamination Propagation Capabilities in Commercial Finite Element Codes Using Benchmark Analysis

NASA Technical Reports Server (NTRS)

Orifici, Adrian C.; Krueger, Ronald

2010-01-01

With capabilities for simulating delamination growth in composite materials becoming available, the need for benchmarking and assessing these capabilities is critical. In this study, benchmark analyses were performed to assess the delamination propagation simulation capabilities of the VCCT implementations in Marc TM and MD NastranTM. Benchmark delamination growth results for Double Cantilever Beam, Single Leg Bending and End Notched Flexure specimens were generated using a numerical approach. This numerical approach was developed previously, and involves comparing results from a series of analyses at different delamination lengths to a single analysis with automatic crack propagation. Specimens were analyzed with three-dimensional and two-dimensional models, and compared with previous analyses using Abaqus . The results demonstrated that the VCCT implementation in Marc TM and MD Nastran(TradeMark) was capable of accurately replicating the benchmark delamination growth results and that the use of the numerical benchmarks offers advantages over benchmarking using experimental and analytical results.

Mixed-Mode Bending Method for Delamination Testing

NASA Technical Reports Server (NTRS)

Reeder, James R.; Crews, John R., Jr.

1990-01-01

A mixed mode delamination test procedure was developed combining double cantilever beam (DCB) mode I loading and end-notch fixture (ENF) mode II loading on a split unidirectional laminate. By loading with a lever, a single applied load simultaneously produces mode I and mode II bending loads on the specimen. This mixed-mode bending (MMB) test was analyzed using both finite-element procedures and beam theory to calculate the mode I and mode II components of strain-energy release rate G(sub I) and G(sub II), respectively. A wide range of G(sub I)/G(sub II) ratios can be produced by varying the load position on the lever. As the delamination extended, the G(sub I)/G(sub II) ratios varied by less than 5%. Beam theory equations agreed closely with the finite-element results and provide a basis for selection of G(sub I)/G(sub II) test ratios and a basis for computing the mode I and mode II components of measured delamination toughness. The MMB test was demonstrated using AS4/PEEK (APC2) unidirectional laminates. The MMB test introduced in this paper is rather simple and is believed to offer several advantages over most current mixed-mode test.

Predicting the growth of S i3N4 nanowires by phase-equilibrium-dominated vapor-liquid-solid mechanism

NASA Astrophysics Data System (ADS)

Zhang, Yongliang; Cai, Jing; Yang, Lijun; Wu, Qiang; Wang, Xizhang; Hu, Zheng

2017-09-01

Nanomaterial synthesis is experiencing a profound evolution from empirical science ("cook-and-look") to prediction and design, which depends on the deep insight into the growth mechanism. Herein, we report a generalized prediction of the growth of S i3N4 nanowires by nitriding F e28S i72 alloy particles across different phase regions based on our finding of the phase-equilibrium-dominated vapor-liquid-solid (PED-VLS) mechanism. All the predictions about the growth of S i3N4 nanowires, and the associated evolutions of lattice parameters and geometries of the coexisting Fe -Si alloy phases, are experimentally confirmed quantitatively. This progress corroborates the general validity of the PED-VLS mechanism, which could be applied to the design and controllable synthesis of various one-dimensional nanomaterials.

On Delamination Toughening of a 14YWT Nanostructured Ferritic Alloy

DOE PAGES

Alam, M.E.; Pal, S.; Maloy, Stuart Andrew; ...

2017-06-22

The FCRD NFA-1 is a high strength, irradiation tolerant nanostructured ferritic alloy (NFA) produced by ball milling argon atomized Fe-14Cr-3W-0.35Ti-0.25Y (wt.%) and FeO powders, followed by hot extrusion at 850 °C, and subsequent annealing and cross-rolling at 1000 °C. The microstructure of the resulting ≈10 mm thick NFA-1 plate is dominated by ultrafine sub-micron pancake shaped grains, and a large population of microcracks lying on planes parallel to the plate faces. Pre-cracked fracture toughness tests in four different orientations (L-T, T-L, L-S and T-S) show stable crack growth by ductile tearing, with peak load K Jc from ≈ 88 tomore » 154 MPa√m at ambient temperature. Stable crack tearing persists down to ≈ -175 °C and is accompanied by extensive delamination due to the propagation of the microcracks. Depending on the specimen orientation, this unusual toughening mechanism is either due to a reduction of crack tip stresses in thin ligaments formed by the delaminations (L-T and T-L), or 90° deflection of cracks initially running normal to the delaminations (L-S and T-S), thereby suppressing cleavage in both cases. Lastly, understanding the fracture processes in NFA-1 is also important to its irradiation tolerance in nuclear service as well as its fabricability in making defect-free components such as thin-walled tubing.« less

In Search of a Time Efficient Approach to Crack and Delamination Growth Predictions in Composites

NASA Technical Reports Server (NTRS)

Krueger, Ronald; Carvalho, Nelson

2016-01-01

Analysis benchmarking was used to assess the accuracy and time efficiency of algorithms suitable for automated delamination growth analysis. First, the Floating Node Method (FNM) was introduced and its combination with a simple exponential growth law (Paris Law) and Virtual Crack Closure technique (VCCT) was discussed. Implementation of the method into a user element (UEL) in Abaqus/Standard(Registered TradeMark) was also presented. For the assessment of growth prediction capabilities, an existing benchmark case based on the Double Cantilever Beam (DCB) specimen was briefly summarized. Additionally, the development of new benchmark cases based on the Mixed-Mode Bending (MMB) specimen to assess the growth prediction capabilities under mixed-mode I/II conditions was discussed in detail. A comparison was presented, in which the benchmark cases were used to assess the existing low-cycle fatigue analysis tool in Abaqus/Standard(Registered TradeMark) in comparison to the FNM-VCCT fatigue growth analysis implementation. The low-cycle fatigue analysis tool in Abaqus/Standard(Registered TradeMark) was able to yield results that were in good agreement with the DCB benchmark example. Results for the MMB benchmark cases, however, only captured the trend correctly. The user element (FNM-VCCT) always yielded results that were in excellent agreement with all benchmark cases, at a fraction of the analysis time. The ability to assess the implementation of two methods in one finite element code illustrated the value of establishing benchmark solutions.

Delaminated rotator cuff tear: extension of delamination and cuff integrity after arthroscopic rotator cuff repair.

PubMed

Gwak, Heui-Chul; Kim, Chang-Wan; Kim, Jung-Han; Choo, Hye-Jeung; Sagong, Seung-Yeob; Shin, John

2015-05-01

The purpose of this study was to evaluate the extension of delamination and the cuff integrity after arthroscopic repair of delaminated rotator cuff tears. Sixty-five patients with delaminated rotator cuff tears were retrospectively reviewed. The delaminated tears were divided into full-thickness delaminated tears and partial-thickness delaminated tears. To evaluate the medial extension, we calculated the coronal size of the delaminated portion. To evaluate the posterior extension, we checked the tendon involved. Cuff integrity was evaluated by computed tomography arthrography. The mean medial extension in the full-thickness and partial-thickness delaminated tears was 18.1 ± 6.0 mm and 22.7 ± 6.3 mm, respectively (P = .0084). The posterior extension into the supraspinatus and the infraspinatus was 36.9% and 32.3%, respectively, in the full-thickness delaminated tears, and it was 27.7% and 3.1%, respectively, in the partial-thickness delaminated tears (P = .0043). With regard to cuff integrity, 35 cases of anatomic healing, 10 cases of partial healing defects, and 17 cases of retear were detected. Among the patients with retear and partial healing of the defect, all the partially healed defects showed delamination. Three retear patients showed delamination, and 14 retear patients did not show delamination; the difference was statistically significant (P = .0001). The full-thickness delaminated tears showed less medial extension and more posterior extension than the partial-thickness delaminated tears. Delamination did not develop in retear patients, but delamination was common in the patients with partially healed defects. Copyright © 2015 Journal of Shoulder and Elbow Surgery Board of Trustees. Published by Elsevier Inc. All rights reserved.

Mixed-Mode Decohesion Finite Elements for the Simulation of Delamination in Composite Materials

NASA Technical Reports Server (NTRS)

Camanho, Pedro P.; Davila, Carlos G.

2002-01-01

A new decohesion element with mixed-mode capability is proposed and demonstrated. The element is used at the interface between solid finite elements to model the initiation and non-self-similar growth of delaminations. A single relative displacement-based damage parameter is applied in a softening law to track the damage state of the interface and to prevent the restoration of the cohesive state during unloading. The softening law for mixed-mode delamination propagation can be applied to any mode interaction criterion such as the two-parameter power law or the three-parameter Benzeggagh-Kenane criterion. To demonstrate the accuracy of the predictions and the irreversibility capability of the constitutive law, steady-state delamination growth is simulated for quasistatic loading-unloading cycles of various single mode and mixed-mode delamination test specimens.

Simulating Matrix Crack and Delamination Interaction in a Clamped Tapered Beam

NASA Technical Reports Server (NTRS)

De Carvalho, N. V.; Seshadri, B. R.; Ratcliffe, J. G.; Mabson, G. E.; Deobald, L. R.

2017-01-01

Blind predictions were conducted to validate a discrete crack methodology based on the Floating Node Method to simulate matrix-crack/delamination interaction. The main novel aspects of the approach are: (1) the implementation of the floating node method via an 'extended interface element' to represent delaminations, matrix-cracks and their interaction, (2) application of directional cohesive elements to infer overall delamination direction, and (3) use of delamination direction and stress state at the delamination front to determine migration onset. Overall, good agreement was obtained between simulations and experiments. However, the validation exercise revealed the strong dependence of the simulation of matrix-crack/delamination interaction on the strength data (in this case transverse interlaminar strength, YT) used within the cohesive zone approach applied in this work. This strength value, YT, is itself dependent on the test geometry from which the strength measurement is taken. Thus, choosing an appropriate strength value becomes an ad-hoc step. As a consequence, further work is needed to adequately characterize and assess the accuracy and adequacy of cohesive zone approaches to model small crack growth and crack onset. Additionally, often when simulating damage progression with cohesive zone elements, the strength is lowered while keeping the fracture toughness constant to enable the use of coarser meshes. Results from the present study suggest that this approach is not recommended for any problem involving crack initiation, small crack growth or multiple crack interaction.

Delamination of Southern Pine plywood during three years of exterior exposure

Treesearch

Peter Koch

1970-01-01

Plywood was made from eight loblolly pine trees selected to exhibit a range of specific gravity and growth rate. three-ply, 3/8-inch specimens were exposed outdoors for 3 years in central Louisiana; percentage of delamination was measured annually. Rings per inch and tightness of peel had minor effects. A low gluespread resulted in rapid delamination, particularly with...

Delamination Modeling of Composites for Improved Crash Analysis

NASA Technical Reports Server (NTRS)

Fleming, David C.

1999-01-01

Finite element crash modeling of composite structures is limited by the inability of current commercial crash codes to accurately model delamination growth. Efforts are made to implement and assess delamination modeling techniques using a current finite element crash code, MSC/DYTRAN. Three methods are evaluated, including a straightforward method based on monitoring forces in elements or constraints representing an interface; a cohesive fracture model proposed in the literature; and the virtual crack closure technique commonly used in fracture mechanics. Results are compared with dynamic double cantilever beam test data from the literature. Examples show that it is possible to accurately model delamination propagation in this case. However, the computational demands required for accurate solution are great and reliable property data may not be available to support general crash modeling efforts. Additional examples are modeled including an impact-loaded beam, damage initiation in laminated crushing specimens, and a scaled aircraft subfloor structures in which composite sandwich structures are used as energy-absorbing elements. These examples illustrate some of the difficulties in modeling delamination as part of a finite element crash analysis.

The mechanics of delamination in fiber-reinforced composite materials. Part 1: Stress singularities and solution structure

NASA Technical Reports Server (NTRS)

Wang, S. S.; Choi, I.

1983-01-01

The fundamental mechanics of delamination in fiber composite laminates is studied. Mathematical formulation of the problem is based on laminate anisotropic elasticity theory and interlaminar fracture mechanics concepts. Stress singularities and complete solution structures associated with general composite delaminations are determined. For a fully open delamination with traction-free surfaces, oscillatory stress singularities always appear, leading to physically inadmissible field solutions. A refined model is introduced by considering a partially closed delamination with crack surfaces in finite-length contact. Stress singularities associated with a partially closed delamination having frictional crack-surface contact are determined, and are found to be diferent from the inverse square-root one of the frictionless-contact case. In the case of a delamination with very small area of crack closure, a simplified model having a square-root stress singularity is employed by taking the limit of the partially closed delamination. The possible presence of logarithmic-type stress singularity is examined; no logarithmic singularity of any kind is found in the composite delamination problem. Numerical examples of dominant stress singularities are shown for delaminations having crack-tip closure with different frictional coefficients between general (1) and (2) graphite-epoxy composites.

A fiber-resin micromechanics analysis of the delamination front in a DCB specimen

NASA Technical Reports Server (NTRS)

Crews, J. H.; Shivakumar, K. N.; Raju, I. S.

1988-01-01

A 3-D finite element model was developed to analyze the fiber-resin behavior near the delamination front in a graphite-epoxy double cantilever beam (DCB) specimen. The specimen interior was analyzed using a typical one-fiber slice, represented by a local 3-D fiber-resin model. The resin stresses were computed for the resin-rich layer at the ply interface as well as for the regions between the fibers close to the delamination front. However, the computed strain energy release rate G sub I along the delamination front varied by less than two percent, and was within about four percent of the plane-strain value. The von Mises yield criterion was used to estimate the extent of yielding near the delamination front. The yielding extended ahead of the delamination and also developed between the fibers. Although the fibers had only a negligible effect on G sub I, they caused yielding within the ply and therefore could influence delamination fracture toughness. The normal and shear stresses at the fiber-resin interface were computed near the delamination front. These results suggest that multi-axial stress criteria may be required to analyze fiber-resin interfaces.

A Biaxial-Bending Test to Observe the Growth of Interacting Delaminations in a Composite Laminate Plate

NASA Technical Reports Server (NTRS)

McElroy, Mark; Jackson, Wade; Pankow, Mark

2016-01-01

It is not easy to isolate the damage mechanisms associated with low-velocity impact in composites using traditional experiments. In this work, a new experiment is presented with the goal of generating data representative of progressive damage processes caused by low-velocity impact in composite materials. Carbon fiber reinforced polymer test specimens were indented quasi-statically such that a biaxial-bending state of deformation was achieved. As a result, a three-dimensional damage process, involving delamination and delamination-migration, was observed and documented using ultrasonic and x-ray computed tomography. Results from two different layups are presented in this paper. Delaminations occurred at up to three different interfaces and interacted with one another via transverse matrix cracks. Although this damage pattern is much less complex than that of low-velocity impact on a plate, it is more complex than that of a standard delamination coupon test and provides a way to generate delamination, matrix cracking, and delamination-migration in a controlled manner. By limiting the damage process in the experiment to three delaminations, the same damage mechanisms seen during impact could be observed but in a simplified manner. This type of data is useful in stages of model development and validation when the model is capable of simulating simple tests, but not yet capable of simulating more complex and realistic damage scenarios.

Bending strength of delaminated aerospace composites.

PubMed

Kinawy, Moustafa; Butler, Richard; Hunt, Giles W

2012-04-28

Buckling-driven delamination is considered among the most critical failure modes in composite laminates. This paper examines the propagation of delaminations in a beam under pure bending. A pre-developed analytical model to predict the critical buckling moment of a thin sub-laminate is extended to account for propagation prediction, using mixed-mode fracture analysis. Fractography analysis is performed to distinguish between mode I and mode II contributions to the final failure of specimens. Comparison between experimental results and analysis shows agreement to within 5 per cent in static propagation moment for two different materials. It is concluded that static fracture is almost entirely driven by mode II effects. This result was unexpected because it arises from a buckling mode that opens the delamination. For this reason, and because of the excellent repeatability of the experiments, the method of testing may be a promising means of establishing the critical value of mode II fracture toughness, G(IIC), of the material. Fatigue testing on similar samples showed that buckled delamination resulted in a fatigue threshold that was over 80 per cent lower than the static propagation moment. Such an outcome highlights the significance of predicting snap-buckling moment and subsequent propagation for design purposes.

Quantitative characterization of the interfacial adhesion of Ni thin film on steel substrate: A compression-induced buckling delamination test

NASA Astrophysics Data System (ADS)

Zhu, W.; Zhou, Y. C.; Guo, J. W.; Yang, L.; Lu, C.

2015-01-01

A compression-induced buckling delamination test is employed to quantitatively characterize the interfacial adhesion of Ni thin film on steel substrate. It is shown that buckles initiate from edge flaws and surface morphologies exhibit symmetric, half-penny shapes. Taking the elastoplasticity of film and substrate into account, a three-dimensional finite element model for an edge flaw with the finite size is established to simulate the evolution of energy release rates and phase angles in the process of interfacial buckling-driven delamination. The results show that delamination propagates along both the straight side and curved front. The mode II delamination plays a dominant role in the process with a straight side whilst the curved front experiences almost the pure mode I. Based on the results of finite element analysis, a numerical model is developed to evaluate the interfacial energy release rate, which is in the range of 250-315 J/m2 with the corresponding phase angle from -41° to -66°. These results are in agreement with the available values determined by other testing methods, which confirms the effectiveness of the numerical model.

Effect of Elevated Temperature and Loading Rate on Delamination Fracture Toughness

NASA Technical Reports Server (NTRS)

Reeder, J. R.; Allen, D. H.; Bradley, W. L.

2003-01-01

The effects of temperature and loading rate on delamination growth were studied. The delamination fracture toughness of IM7/K3B was measured at 149 C, 177 C, and 204 C. At each temperature the tests were performed with a variety of loading rates so that the delamination initiated over the range of time from 0.5 sec to 24 hrs. The double cantilever beam (DCB) test was used to measure fracture toughness. The results showed that the delamination resistance is a complicated function of both time and temperature with the effect of temperature either increasing or decreasing the fracture toughness depending on the time scale. The results also showed that the fracture toughness changed by as much as a factor of three as the time scale changed over the five orders of magnitude tested.

Analysis of delamination in unidirectional and crossplied fiber composites containing surface cracks

NASA Technical Reports Server (NTRS)

Wang, S. S.; Mandell, J. F.

1977-01-01

A two-dimensional hybrid stress finite element analysis is described which was used to study the local stress field around delamination cracks in composite materials. The analysis employs a crack tip singularity element which is embedded in a matrix interlayer between plies of the laminate. Results are given for a unidirectional graphite/epoxy laminate containing a delamination emanating from a surface crack through the outside ply. The results illustrate several aspects of delamination cracks: (1) the localization of the singular stress domain within the interlayer; (2) the local concentration of stress in the ply adjacent to the crack; (3) the nature of the transverse normal and interlaminar shear stress distributions; and (4) the relative magnitudes of K sub 1 and K sub 2 associated with the delamination. A simple example of the use of the analysis in predicting delamination crack growth is demonstrated for a glass/epoxy laminate. The comparisons with experimental data show good agreement.

An Irreversible Constitutive Law for Modeling the Delamination Process using Interface Elements

NASA Technical Reports Server (NTRS)

Goyal, Vinay K.; Johnson, Eric R.; Davila, Carlos G.; Jaunky, Navin; Ambur, Damodar (Technical Monitor)

2002-01-01

An irreversible constitutive law is postulated for the formulation of interface elements to predict initiation and progression of delamination in composite structures. An exponential function is used for the constitutive law such that it satisfies a multi-axial stress criterion for the onset of delamination, and satisfies a mixed mode fracture criterion for the progression of delamination. A damage parameter is included to prevent the restoration of the previous cohesive state between the interfacial surfaces. To demonstrate the irreversibility capability of the constitutive law, steady-state crack growth is simulated for quasi-static loading-unloading cycle of various fracture test specimens.

An Irreversible Constitutive Law for Modeling the Delamination Process Using Interface Elements

NASA Technical Reports Server (NTRS)

Goyal, Vinay K.; Johnson, Eric R.; Davila, Carlos G.; Jaunky, Navin; Bushnell, Dennis M. (Technical Monitor)

2002-01-01

An irreversible constitutive law is postulated for the formulation of interface elements to predict initiation and progression of delamination in composite structures. An exponential function is used for the constitutive law such that it satisfies a multi-axial stress criterion for the onset of delamination, and satisfies a mixed mode fracture criterion for the progression of delamination. A damage parameter is included to prevent the restoration of the previous cohesive state between the interfacial surfaces. To demonstrate the irreversibility capability of the constitutive law, steady-state crack growth is simulated for quasi-static loading-unloading cycle of various fracture test specimens.

Penalty-Based Interface Technology for Prediction of Delamination Growth in Laminated Structures

NASA Technical Reports Server (NTRS)

Averill, Ronald C.

2004-01-01

An effective interface element technology has been developed for connecting and simulating crack growth between independently modeled finite element subdomains (e.g., composite plies). This method has been developed using penalty constraints and allows coupling of finite element models whose nodes do not necessarily coincide along their common interface. Additionally, the present formulation leads to a computational approach that is very efficient and completely compatible with existing commercial software. The present interface element has been implemented in the commercial finite element code ABAQUS as a User Element Subroutine (UEL), making it easy to test the approach for a wide range of problems. The interface element technology has been formulated to simulate delamination growth in composite laminates. Thanks to its special features, the interface element approach makes it possible to release portions of the interface surface whose length is smaller than that of the finite elements. In addition, the penalty parameter can vary within the interface element, allowing the damage model to be applied to a desired fraction of the interface between the two meshes. Results for double cantilever beam DCB, end-loaded split (ELS) and fixed-ratio mixed mode (FRMM) specimens are presented. These results are compared to measured data to assess the ability of the present damage model to simulate crack growth.

The mechanics of delamination in fiber-reinforced composite materials. Part 2: Delamination behavior and fracture mechanics parameters

NASA Technical Reports Server (NTRS)

Wang, S. S.; Choi, I.

1983-01-01

Based on theories of laminate anisotropic elasticity and interlaminar fracture, the complete solution structure associated with a composite delamination is determined. Fracture mechanics parameters characterizing the interlaminar crack behavior are defined from asymptotic stress solutions for delaminations with different crack-tip deformation configurations. A numerical method employing singular finite elements is developed to study delaminations in fiber composites with any arbitrary combinations of lamination, material, geometric, and crack variables. The special finite elements include the exact delamination stress singularity in its formulation. The method is shown to be computationally accurate and efficient, and operationally simple. To illustrate the basic nature of composite delamination, solutions are shown for edge-delaminated (0/-0/-0/0) and (+ or - 0/+ or - 0/90/90 deg) graphite-epoxy systems under uniform axial extenstion. Three-dimensional crack-tip stress intensity factors, associated energy release rates, and delamination crack-closure are determined for each individual case. The basic mechanics and mechanisms of composite delamination are studied, and fundamental characteristics unique to recently proposed tests for interlaminar fracture toughness of fiber composite laminates are examined.

Development and Applications of Benchmark Examples for Static Delamination Propagation Predictions

NASA Technical Reports Server (NTRS)

Krueger, Ronald

2013-01-01

The development and application of benchmark examples for the assessment of quasistatic delamination propagation capabilities was demonstrated for ANSYS (TradeMark) and Abaqus/Standard (TradeMark). The examples selected were based on finite element models of Double Cantilever Beam (DCB) and Mixed-Mode Bending (MMB) specimens. First, quasi-static benchmark results were created based on an approach developed previously. Second, the delamination was allowed to propagate under quasi-static loading from its initial location using the automated procedure implemented in ANSYS (TradeMark) and Abaqus/Standard (TradeMark). Input control parameters were varied to study the effect on the computed delamination propagation. Overall, the benchmarking procedure proved valuable by highlighting the issues associated with choosing the appropriate input parameters for the VCCT implementations in ANSYS® and Abaqus/Standard®. However, further assessment for mixed-mode delamination fatigue onset and growth is required. Additionally studies should include the assessment of the propagation capabilities in more complex specimens and on a structural level.

The mechanics of delamination in fiber-reinforced composite materials. II - The delamination behavior and fracture mechanics parameters

NASA Technical Reports Server (NTRS)

Wang, S. S.; Choi, I.

1983-01-01

Based on theories of laminate anisotropic elasticity and interlaminar fracture, the complete solution structure associated with a composite delamination is determined. Fracture mechanics parameters characterizing the interlaminar crack behavior are defined from asymptotic stress solutions for delaminations with different crack-tip deformation configurations. A numerical method employing singular finite elements is developed to study delaminations in fiber composites with any arbitrary combinations of lamination, material, geometric, and crack variables. The special finite elements include the exact delamination stress singularity in its formulation. The method is shown to be computationally accurate and efficient, and operationally simple. To illustrate the basic nature of composite delamination, solutions are shown for edge-delaminated (0/-0/-0/0) and (+ or - 0/+ or - 0/90/90 deg) graphite-epoxy systems under uniform axial extension. Three-dimensional crack-tip stress intensity factors, associated energy release rates, and delamination crack-closure are determined for each individual case. The basic mechanics and mechanisms of composite delamination are studied, and fundamental characteristics unique to recently proposed tests for interlaminar fracture toughness of fiber composite laminates are examined. Previously announced in STAR as N84-13222

Numerical Investigation of Delamination in Drilling of Carbon Fiber Reinforced Polymer Composites

NASA Astrophysics Data System (ADS)

Tang, Wenliang; Chen, Yan; Yang, Haojun; Wang, Hua; Yao, Qiwei

2018-03-01

Drilling of carbon fiber reinforced polymer (CFRP) is a challenging task in modern manufacturing sector and machining induced delamination is one of the major problems affecting assembly precision. In this work, a new three-dimensional (3D) finite element model is developed to study the chip formation and entrance delamination in drilling of CFRP composites on the microscopic level. Fiber phase, matrix phase and equivalent homogeneous phase in the multi-phase model have different constitutive behaviors, respectively. A comparative drilling test, in which the cement carbide drill and unidirectional CFRP laminate are employed, is conducted to validate the proposedmodel in terms of the delamination and the similar changing trend is obtained. Microscopic mechanism of entrance delamination together with the chip formation process at four special fiber cutting angles (0°, 45°, 90° and 135°) is investigated. Moreover, the peeling force is also predicted. The results show that the delamination occurrence and the chip formation are both strongly dependent on the fiber cutting angle. The length of entrance delamination rises with increasing fiber cutting angles. Negligible delamination at 0° is attributed to the compression by the minor flank face. For 45° and 90°, the delamination resulted from the mode III fracture. At 135°, serious delamination which is driven by the mode I and III fractures is more inclined to occur and the peeling force reaches its maximum. Such numerical models can help understand the mechanism of hole entrance delamination further and provide guidance for the damage-free drilling of CFRP.

Cyclic delamination behavior of plasma-sprayed hydroxyapatite coating on Ti-6Al-4V substrates in simulated body fluid.

PubMed

Otsuka, Yuichi; Kawaguchi, Hayato; Mutoh, Yoshiharu

2016-10-01

This study aimed to clarify the effect of a simulated body fluid (SBF) on the cyclic delamination behavior of a plasma-sprayed hydroxapatite (HAp) coating. A HAp coating is deposited on the surfaces of surgical metallic materials in order to enhance the bond between human bone and such surfaces. However, the HAp coating is susceptible to delamination by cyclic loading from the patient's gait. Although hip joints are subjected to both positive and negative moments, only the effects of tensile bending stresses on vertical crack propagation behavior have been investigated. Thus, the cyclic delamination behavior of a HAp coating was observed at the stress ratio R=-1 in order to determine the effects of tensile/compressive loading on the delamination behavior. The delamination growth rate increased with SBF immersion, which decreased the delamination life. Raman spectroscopy analysis revealed that the selective phase dissolution in the HAp coating was promoted at interfaces. Finite element analysis revealed that the energy release rate Gmax showed a positive value even in cases with compressive loading, which is a driving force for the delamination of a HAp coating. A prediction model for the delamination growth life was developed that combines a fracture mechanics parameter with the assumed stress-dependent dissolution rate. The predicted delamination life matched the experimental data well in cases of lower stress amplitudes with SBF. Copyright © 2016 Elsevier B.V. All rights reserved.

Q3DG: A computer program for strain-energy-release rates for delamination growth in composite laminates

NASA Technical Reports Server (NTRS)

Raju, I. S.

1986-01-01

The Q3DG is a computer program developed to perform a quasi-three-dimensional stress analysis for composite laminates which may contain delaminations. The laminates may be subjected to mechanical, thermal, and hygroscopic loads. The program uses the finite element method and models the laminates with eight-noded parabolic isoparametric elements. The program computes the strain-energy-release components and the total strain-energy release in all three modes for delamination growth. A rectangular mesh and data file generator, DATGEN, is included. The DATGEN program can be executed interactively and is user friendly. The documentation includes sections dealing with the Q3D analysis theory, derivation of element stiffness matrices and consistent load vectors for the parabolic element. Several sample problems with the input for Q3DG and output from the program are included. The capabilities of the DATGEN program are illustrated with examples of interactive sessions. A microfiche of all the examples is included. The Q3DG and DATGEN programs have been implemented on CYBER 170 class computers. Q3DG and DATGEN were developed at the Langley Research Center during the early eighties and documented in 1984 to 1985.

A continuum damage model for delaminations in laminated composites

NASA Astrophysics Data System (ADS)

Zou, Z.; Reid, S. R.; Li, S.

2003-02-01

Delamination, a typical mode of interfacial damage in laminated composites, has been considered in the context of continuum damage mechanics in this paper. Interfaces where delaminations could occur are introduced between the constituent layers. A simple but appropriate continuum damage representation is proposed. A single scalar damage parameter is employed and the degradation of the interface stiffness is established. Use has been made of the concept of a damage surface to derive the damage evolution law. The damage surface is constructed so that it combines the conventional stress-based and fracture-mechanics-based failure criteria which take account of mode interaction in mixed-mode delamination problems. The damage surface shrinks as damage develops and leads to a softening interfacial constitutive law. By adjusting the shrinkage rate of the damage surface, various interfacial constitutive laws found in the literature can be reproduced. An incremental interfacial constitutive law is also derived for use in damage analysis of laminated composites, which is a non-linear problem in nature. Numerical predictions for problems involving a DCB specimen under pure mode I delamination and mixed-mode delamination in a split beam are in good agreement with available experimental data or analytical solutions. The model has also been applied to the prediction of the failure strength of overlap ply-blocking specimens. The results have been compared with available experimental and alternative theoretical ones and discussed fully.

The effect of fatigue and environment on the adhesion and delamination of thin polymer films

NASA Astrophysics Data System (ADS)

Snodgrass, Jeffrey Matthew

Polymers are increasingly used in the interconnect and packaging levels of microelectronic devices. Thus, adhesion of polymer films to their adjacent inorganic layers is critical to the manufacturability and reliability of microelectronic components. Weak interfacial adhesion can result in delamination, causing a loss of package hermeticity or the failure of electrical contacts. Recently, interface fracture mechanics techniques have been applied to the problem of thin film delamination and are now used to measure interface adhesion. These techniques allow for characterization of interface adhesion in terms of the critical strain energy release rate, GC, in units of J/m2. In this dissertation, studies are described that quantify the effects of fundamental parameters on the critical adhesion and resistance to subcritical (time-dependent) delamination of benzocyclobutene (BCB)/silica and epoxy underfill/polyimide interfaces. Results are presented detailing the action of small-molecule adhesion promoters on the critical interface adhesion energy of BCB/silica. Silane coupling agents with different functional end groups were used to increase chemical bonding at this interface in order to achieve optimized adhesion. Testing was performed at different mode mixities to evaluate the effect of loading mode on the polymer interface fracture. Subcritical debonding data were measured under two different loading conditions and results are presented in terms of the debond growth rate as a function of applied strain energy release rate. Monotonic loading was used to examine environment-assisted delamination processes, while fatigue loading was used to understand the effects of thermomechanical cycling. Debond growth rates over the range of 10-3 to 10-9 m/s were characterized under mode I and mixed-mode loading. Atomic force microscopy and X-ray photoelectron spectroscopy were used to characterize the fracture surfaces of these interfaces and to generate detailed information about

An Effective Electrical Resonance-Based Method to Detect Delamination in Thermal Barrier Coating

NASA Astrophysics Data System (ADS)

Kim, Jong Min; Park, Jae-Ha; Lee, Ho Girl; Kim, Hak-Joon; Song, Sung-Jin; Seok, Chang-Sung; Lee, Young-Ze

2017-12-01

This research proposes a simple yet highly sensitive method based on electrical resonance of an eddy-current probe to detect delamination of thermal barrier coating (TBC). This method can directly measure the mechanical characteristics of TBC compared to conventional ultrasonic testing and infrared thermography methods. The electrical resonance-based method can detect the delamination of TBC from the metallic bond coat by shifting the electrical impedance of eddy current testing (ECT) probe coupling with degraded TBC, and, due to this shift, the resonant frequencies near the peak impedance of ECT probe revealed high sensitivity to the delamination. In order to verify the performance of the proposed method, a simple experiment is performed with degraded TBC specimens by thermal cyclic exposure. Consequently, the delamination with growth of thermally grown oxide in a TBC system is experimentally identified. Additionally, the results are in good agreement with the results obtained from ultrasonic C-scanning.

An Effective Electrical Resonance-Based Method to Detect Delamination in Thermal Barrier Coating

NASA Astrophysics Data System (ADS)

Kim, Jong Min; Park, Jae-Ha; Lee, Ho Girl; Kim, Hak-Joon; Song, Sung-Jin; Seok, Chang-Sung; Lee, Young-Ze

2018-02-01

This research proposes a simple yet highly sensitive method based on electrical resonance of an eddy-current probe to detect delamination of thermal barrier coating (TBC). This method can directly measure the mechanical characteristics of TBC compared to conventional ultrasonic testing and infrared thermography methods. The electrical resonance-based method can detect the delamination of TBC from the metallic bond coat by shifting the electrical impedance of eddy current testing (ECT) probe coupling with degraded TBC, and, due to this shift, the resonant frequencies near the peak impedance of ECT probe revealed high sensitivity to the delamination. In order to verify the performance of the proposed method, a simple experiment is performed with degraded TBC specimens by thermal cyclic exposure. Consequently, the delamination with growth of thermally grown oxide in a TBC system is experimentally identified. Additionally, the results are in good agreement with the results obtained from ultrasonic C-scanning.

Analysis for delamination initiation in postbuckled dropped-ply laminates

NASA Technical Reports Server (NTRS)

Davila, Carlos G.; Johnson, Eric R.

1992-01-01

The compression strength of dropped-ply, graphite-epoxy laminated plates for the delamination mode of failure is studied by analysis and corroborated with experiments. The nonlinear response of the test specimens is modeled by a geometrically nonlinear finite element analysis. The methodology for predicting delamination is based on a quadratic interlaminar stress criterion evaluated at a characteristic distance from the ply drop-off. The compression strength of specimens exhibiting a linear response is greater than the compression strength of specimens with the same layup exhibiting a geometrically nonlinear response. The analyses for both linear and nonlinear response show that severe interlaminar stress gradients occur in the interfaces at the drop-off because of the thickness/stiffness discontinuity. However, these interlaminar stress distributions are altered in the geometrically nonlinear response such that, with increasing load, their growth at the center of the laminate is retarded while their growth near the unloaded supported edge is increased.

Compressive strength of delaminated aerospace composites.

PubMed

Butler, Richard; Rhead, Andrew T; Liu, Wenli; Kontis, Nikolaos

2012-04-28

An efficient analytical model is described which predicts the value of compressive strain below which buckle-driven propagation of delaminations in aerospace composites will not occur. An extension of this efficient strip model which accounts for propagation transverse to the direction of applied compression is derived. In order to provide validation for the strip model a number of laminates were artificially delaminated producing a range of thin anisotropic sub-laminates made up of 0°, ±45° and 90° plies that displayed varied buckling and delamination propagation phenomena. These laminates were subsequently subject to experimental compression testing and nonlinear finite element analysis (FEA) using cohesive elements. Comparison of strip model results with those from experiments indicates that the model can conservatively predict the strain at which propagation occurs to within 10 per cent of experimental values provided (i) the thin-film assumption made in the modelling methodology holds and (ii) full elastic coupling effects do not play a significant role in the post-buckling of the sub-laminate. With such provision, the model was more accurate and produced fewer non-conservative results than FEA. The accuracy and efficiency of the model make it well suited to application in optimum ply-stacking algorithms to maximize laminate strength.

Mechanics of instability-related delimination growth

NASA Technical Reports Server (NTRS)

Whitcomb, John D.

1988-01-01

Local buckling of a delaminated group of plies can lead to higher interlaminar stresses and delamination growth. The mechanics of instability-related delamination growth (IRDG) had been described previously for the through-width delamination. This paper describes the mechanics of IRDG for the embedded delamination subjected to either uniaxial or axisymmetric loads. The mechanics of IRDG are used to explain the dramatic differences in strain-energy release rates observed for the through-width, the axisymmetrically loaded embedded delamination, and the uniaxially loaded embedded delamination.

Delamination detection using methods of computational intelligence

NASA Astrophysics Data System (ADS)

Ihesiulor, Obinna K.; Shankar, Krishna; Zhang, Zhifang; Ray, Tapabrata

2012-11-01

Abstract Reliable delamination prediction scheme is indispensable in order to prevent potential risks of catastrophic failures in composite structures. The existence of delaminations changes the vibration characteristics of composite laminates and hence such indicators can be used to quantify the health characteristics of laminates. An approach for online health monitoring of in-service composite laminates is presented in this paper that relies on methods based on computational intelligence. Typical changes in the observed vibration characteristics (i.e. change in natural frequencies) are considered as inputs to identify the existence, location and magnitude of delaminations. The performance of the proposed approach is demonstrated using numerical models of composite laminates. Since this identification problem essentially involves the solution of an optimization problem, the use of finite element (FE) methods as the underlying tool for analysis turns out to be computationally expensive. A surrogate assisted optimization approach is hence introduced to contain the computational time within affordable limits. An artificial neural network (ANN) model with Bayesian regularization is used as the underlying approximation scheme while an improved rate of convergence is achieved using a memetic algorithm. However, building of ANN surrogate models usually requires large training datasets. K-means clustering is effectively employed to reduce the size of datasets. ANN is also used via inverse modeling to determine the position, size and location of delaminations using changes in measured natural frequencies. The results clearly highlight the efficiency and the robustness of the approach.

Residual thermal and moisture influences on the strain energy release rate analysis of edge delamination

NASA Technical Reports Server (NTRS)

Obrien, T. K.; Raju, I. S.; Garber, D. P.

1985-01-01

A laminated plate theory analysis is developed to calculate the strain energy release rate associated with edge delamination growth in a composite laminate. The analysis includes the contribution of residual thermal and moisture stresses to the strain energy released. The strain energy release rate, G, increased when residual thermal effects were combined with applied mechanical strains, but then decreased when increasing moisture content was included. A quasi-three-dimensional finite element analysis indicated identical trends and demonstrated these same trends for the individual strain energy release rate components, G sub I and G sub II, associated with interlaminar tension and shear. An experimental study indicated that for T300/5208 graphite-epoxy composites, the inclusion of residual thermal and moisture stresses did not significantly alter the calculation of interlaminar fracture toughness from strain energy release rate analysis of edge delamination data taken at room temperature, ambient conditions.

Delamination Behavior of L-Shaped Laminated Composites

NASA Astrophysics Data System (ADS)

Geleta, Tsinuel N.; Woo, Kyeongsik; Lee, Bongho

2018-05-01

We studied the delamination behavior of L-shaped laminated composites numerically and experimentally. In finite-element modeling, cohesive zone modeling was used to simulate the delamination of plies. Cohesive elements were inserted between bulk elements at each interlayer to represent the occurrence of multiple delaminations. The laminated composite models were subjected to several types of loading inducing opening and shearing types of delamination. Numerical results were compared to those in the literature and of experiments conducted in this study. The results were carefully examined to investigate diverse delamination initiation and propagation behaviors. The effect of varying presence and location of pre-crack was also studied.

Detecting severity of delamination in a lap joint using S-parameters

NASA Astrophysics Data System (ADS)

Islam, M. M.; Huang, H.

2018-03-01

The scattering parameters (S-parameters) represent the frequency response of a two-port linear time-invariant network. Treating a lap joint structure instrumented with two piezoelectric wafer active transducers (PWaTs) as such a network, this paper investigates the application of the S-parameters for detecting the severity of delamination in the lap joint. The pulse-echo signal calculated from the reflection coefficients, namely the S 11 and S 22-parameters, can be divided into three signals, i.e. the excitation, resonant, and echo signals, based on their respective time spans. Analyzing the effects of the delamination on the resonant signal enables us to identify the resonance at which the resonant characteristics of the PWaTs are least sensitive to the delamination. Only at this resonance, we found that the reflection coefficients and the amplitude of the first arrival echo signal changed monotonously with the increase of the delamination length. This discovery is further validated by the time-domain pitch-catch signal calculated from the transmission coefficient (i.e. the S 21-parameter). In addition, comparing the pulse-echo signals obtained from both PWaTs enables us to determine the side of the lap joint that the delamination is located at. This work establishes the S-parameters as an effective tool to evaluate the effects of damage on the PWaT resonant characteristics, based on which the PWaT resonance can be selected judiciously for damage severity detection. Correlating the reflection and transmission coefficients also provide addition validations that increase the detection confidence.

Fractography of composite delamination

NASA Technical Reports Server (NTRS)

Bascom, W. D.

1990-01-01

The microdamage that occurs for Mode 1 and Mode 2 delamination was examined by potting delaminated specimens in a clear epoxy, sectioning through the damage, polishing the cut sections and examining using light microscopy. For Mode 1 delamination of unidirectional carbon fiber reinforced plastic (CFRP) composites, the major observation was fiber bridging including large ligaments of fiber bundles. The Mode 2 delamination of unidirectional laminates revealed a very narrow crack opening with only occasional fiber bridging. Impact testing by repetitive impacts with increasing energy was studied and it was found that this technique does not discern changes in the type of damage with increasing cumulative impact energy. Instead, the changes in the impact response, notably stiffness, are the result of changes in the extent of damage. For laminates with a brittle thermoplastic matrix, 3501-6, there were distinct changes in stiffness that corresponded to the development of through the thickness damage and then to the extension of the damage to the specimen edges. For PEEK and polycarbonate, the changes in stiffness were not as abrupt as for the thermoset. None the less, the damage progressed in the same manner.

Analysis of interlaminar stresses in thick composite laminates with and without edge delamination

NASA Technical Reports Server (NTRS)

Whitcomb, J. D.; Raju, I. S.

1984-01-01

The effect of laminate thickness on the interlaminar stresses in rectangular quasi-isotropic laminates under uniform axial strain was studied. Laminates from 8-ply to infinitely thick were analyzed. Thick laminates were synthesized by stacking (45/0/-45/90) ply groups, rather than grouping like plies. Laminates with and without delaminations were studied. In laminates without delaminations, the free-edge interlaminar normal stress distribution in the outer ply groups was insensitive to total laminate thickness. The interlaminar normal stress distribution for the interior ply groups was nearly the same as for an infinitely thick laminate. In contrast, the free-edge inter-laminar shear stress distribution was nearly the same for inner and outer ply groups and was insensitive to laminate thickness. In laminates with delaminations those delaminations near the top and bottom surfaces of a thick laminate have much larger total strain-energy-release rates (G sub t) and mode I-to-total (G sub t/G sub t) ratios than delaminations deep in the interior. Therefore, delaminations can be expected to grow more easily near the surfaces of a laminate than in the interior.

Crack Growth Mechanisms under Anti-Plane Shear in Composite Laminates

NASA Astrophysics Data System (ADS)

Horner, Allison Lynne

The research conducted for this dissertation focuses on determining the mechanisms associated with crack growth in polymer matrix composite laminates subjected to anti-plane shear (mode III) loading. For mode III split-beam test methods were proposed, and initial evaluations were conducted. A single test method was selected for further evaluation. Using this test method, it was determined that the apparent mode III delamination toughness, GIIIc , depended on geometry, which indicated a true material property was not being measured. Transverse sectioning and optical microscopy revealed an array of transverse matrix cracks, or echelon cracks, oriented at approximately 45° and intersecting the plane of the delamination. Subsequent investigations found the echelon array formed prior to the onset of planar delamination advance and that growth of the planar delamination is always coupled to echelon array formation in these specimens. The evolution of the fracture surfaces formed by the echelon array and planar delamination were studied, and it was found that the development was similar to crack growth in homogenous materials subjected to mode III or mixed mode I-III loading, although the composite laminate architecture constrained the fracture surface development differently than homogenous materials. It was also found that, for split-beam specimens such as those used herein, applying an anti-plane shear load results in twisting of the specimen's uncracked region which gives rise to a mixed-mode I-III load condition. This twisting has been related to the apparent mode III toughness as well as the orientation of the transverse matrix cracks. A finite element model was then developed to study the mechanisms of initial echelon array formation. From this, it is shown that an echelon array will develop, but will become self-limiting prior to the onset of planar delamination growth.

Investigating Delamination Migration in Composite Tape Laminates

NASA Technical Reports Server (NTRS)

Ratcliffe, James G.; DeCarvalho, Nelson V.

2014-01-01

A modification to a recently developed test specimen designed to investigate migration of a delamination between neighboring ply interfaces in tape laminates is presented. The specimen is a cross-ply laminated beam consisting of 40 plies with a polytetrafluoroethylene insert spanning part way along its length. The insert is located between a lower 0-degree ply (specimen length direction) and a stack of four 90-degree plies (specimen width direction). The modification involved a stacking sequence that promotes stable delamination growth prior to migration, and included a relocation of the insert from the specimen midplane to the interface between plies 14 and 15. Specimens were clamped at both ends onto a rigid baseplate and loaded on their upper surface via a piano hinge assembly, resulting in a predominantly flexural loading condition. Tests were conducted with the load-application point positioned at various locations along a specimen's span. This position affected the sequence of damage events during a test.

Delamination Analysis Of Composite Curved Bars

NASA Technical Reports Server (NTRS)

Ko, William L.; Jackson, Raymond H.

1990-01-01

Classical anisotropic elasticity theory used to construct "multilayer" composite semicircular curved bar subjected to end forces and end moments. Radial location and intensity of open-mode delamination stress calculated and compared with results obtained from anisotropic continuum theory and from finite element method. Multilayer theory gave more accurate predictions of location and intensity of open-mode delamination stress. Currently being applied to predict open-mode delamination stress concentrations in horse-shoe-shaped composite test coupons.

Fatigue damage prognosis of internal delamination in composite plates under cyclic compression loadings using affine arithmetic as uncertainty propagation tool

NASA Astrophysics Data System (ADS)

Gbaguidi, Audrey J.-M.

Structural health monitoring (SHM) has become indispensable for reducing maintenance costs and increasing the in-service capacity of a structure. The increased use of lightweight composite materials in aircraft structures drastically increased the effects of fatigue induced damage on their critical structural components and thus the necessity to predict the remaining life of those components. Damage prognosis, one of the least investigated fields in SHM, uses the current damage state of the system to forecast its future performance by estimating the expected loading environments. A successful damage prediction model requires the integration of technologies in areas like measurements, materials science, mechanics of materials, and probability theories, but most importantly the quantification of uncertainty in all these areas. In this study, Affine Arithmetic is used as a method for incorporating the uncertainties due to the material properties into the fatigue life prognosis of composite plates subjected to cyclic compressive loadings. When loadings are compressive in nature, the composite plates undergo repeated buckling-unloading of the delaminated layer which induces mixed modes I and II states of stress at the tip of the delamination in the plates. The Kardomateas model-based prediction law is used to predict the growth of the delamination, while the integration of the effects of the uncertainties for modes I and II coefficients in the fatigue life prediction model is handled using Affine arithmetic. The Mode I and Mode II interlaminar fracture toughness and fatigue characterization of the composite plates are first experimentally studied to obtain the material coefficients and fracture toughness, respectively. Next, these obtained coefficients are used in the Kardomateas law to predict the delamination lengths in the composite plates while using Affine Arithmetic to handle their uncertainties. At last, the fatigue characterization of the composite plates during

Dynamic fracture mechanics analysis for an edge delamination crack

NASA Technical Reports Server (NTRS)

Rizzi, Stephen A.; Doyle, James F.

1994-01-01

A global/local analysis is applied to the problem of a panel with an edge delamination crack subject to an impulse loading to ascertain the dynamic J integral. The approach uses the spectral element method to obtain the global dynamic response and local resultants to obtain the J integral. The variation of J integral along the crack front is shown. The crack behavior is mixed mode (Mode 2 and Mode 3), but is dominated by the Mode 2 behavior.

Analysis of delamination related fracture processes in composites

NASA Technical Reports Server (NTRS)

Armanios, Erian A.

1988-01-01

Delamination related fracture processes in composite materials are discussed. Thermal and moisture influences on the free-edge delamination of laminated composites, fracture analysis of local delaminations in laminated composites, and strain energy release rates in belts are among the topics covered.

Edge delamination in angle-ply composite laminates, part 5

NASA Technical Reports Server (NTRS)

Wang, S. S.

1981-01-01

A theoretical method was developed for describing the edge delamination stress intensity characteristics in angle-ply composite laminates. The method is based on the theory of anisotropic elasticity. The edge delamination problem is formulated using Lekhnitskii's complex-variable stress potentials and an especially developed eigenfunction expansion method. The method predicts exact orders of the three-dimensional stress singularity in a delamination crack tip region. With the aid of boundary collocation, the method predicts the complete stress and displacement fields in a finite-dimensional, delaminated composite. Fracture mechanics parameters such as the mixed-mode stress intensity factors and associated energy release rates for edge delamination can be calculated explicity. Solutions are obtained for edge delaminated (theta/-theta theta/-theta) angle-ply composites under uniform axial extension. Effects of delamination lengths, fiber orientations, lamination and geometric variables are studied.

Constitutive Modeling of the Facesheet to Core Interface in Honeycomb Sandwich Panels Subject to Mode I Delamination

NASA Technical Reports Server (NTRS)

Hoewer, Daniel; Lerch, Bradley A.; Bednarcyk, Brett A.; Pineda, Evan Jorge; Reese, Stefanie; Simon, Jaan-Willem

2017-01-01

A new cohesive zone traction-separation law, which includes the effects of fiber bridging, has been developed, implemented with a finite element (FE) model, and applied to simulate the delamination between the facesheet and core of a composite honeycomb sandwich panel. The proposed traction-separation law includes a standard initial cohesive component, which accounts for the initial interfacial stiffness and energy release rate, along with a new component to account for the fiber bridging contribution to the delamination process. Single cantilever beam tests on aluminum honeycomb sandwich panels with carbon fiber reinforced polymer facesheets were used to characterize and evaluate the new formulation and its finite element implementation. These tests, designed to evaluate the mode I toughness of the facesheet to core interface, exhibited significant fiber bridging and large crack process zones, giving rise to a concave downward concave upward pre-peak shape in the load-displacement curve. Unlike standard cohesive formulations, the proposed formulation captures this observed shape, and its results have been shown to be in excellent quantitative agreement with experimental load-displacement and apparent critical energy release rate results, representative of a payload fairing structure, as well as local strain fields measured with digital image correlation.

Patterns of growth dominance in forests of the Rocky Mountains, USA

Treesearch

Dan Binkley; Daniel M. Kashian; Suzanne Boyden; Margot W. Kaye; John B. Bradford; Mary A. Arthur; Paula J. Fornwalt; Michael G. Ryan

2006-01-01

We used data from 142 stands in Colorado andWyoming, USA, to test the expectations of a model of growth dominance and stand development. Growth dominance relates the distribution of growth rates of individual trees within a stand to tree sizes. Stands with large trees that account for a greater share of stand growth than of stand mass exhibit strong growth dominance....

The Inclusion of In-Plane Stresses in Delamination Criteria

NASA Technical Reports Server (NTRS)

Fenske, Matthew T.

1999-01-01

A study of delamination failure was conducted with emphasis on delamination criteria. Evidence is presented which supports the inclusion of the in-plane stresses in addition to the interlaminar stress terms in delamination criteria. The delamination is characterized as the failure of a resin rich region in between ply sets. The entire six component stress state in this resin layer is calculated through a finite element analysis, averaged over a dimension of 1.75 ply thicknesses, and used in a Modified von Mises Delamination Criterion. This criterion builds onto previous criteria by including all six stress components in the interply resin layer. The MVMDC shows good correlation to experimental data. The results show that the treatment of delamination as the failure of a finite interply resin layer is a valid method and that the MVMDC, considering the full stress state, accurately indicates delamination for different laminate families.

Delamination Detection Using Guided Wave Phased Arrays

NASA Technical Reports Server (NTRS)

Tian, Zhenhua; Yu, Lingyu; Leckey, Cara

2016-01-01

This paper presents a method for detecting multiple delaminations in composite laminates using non-contact phased arrays. The phased arrays are implemented with a non-contact scanning laser Doppler vibrometer (SLDV). The array imaging algorithm is performed in the frequency domain where both the guided wave dispersion effect and direction dependent wave properties are considered. By using the non-contact SLDV array with a frequency domain imaging algorithm, an intensity image of the composite plate can be generated for delamination detection. For the proof of concept, a laboratory test is performed using a non-contact phased array to detect two delaminations (created through quasi-static impact test) at different locations in a composite plate. Using the non-contact phased array and frequency domain imaging, the two impact-induced delaminations are successfully detected. This study shows that the non-contact phased array method is a potentially effective method for rapid delamination inspection in large composite structures.

Towards a Delamination Fatigue Methodology for Composite Materials

NASA Technical Reports Server (NTRS)

OBrien, Thomas K.

2007-01-01

A methodology that accounts for both delaminaton onset and growth in composite structural components is proposed for improved fatigue life prediction to reduce life cycle costs and improve accept/reject criteria for manufacturing flaws. The benefits of using a Delamination Onset Threshold (DOT) approach in combination with a Modified Damage Tolerance (MDT) approach is highlighted. The use of this combined approach to establish accept/reject criteria, requiring less conservative initial manufacturing flaw sizes, is illustrated.

Delamination stresses in semicircular laminated composite bars

NASA Technical Reports Server (NTRS)

Ko, William L.

1988-01-01

Using anisotropic elasticity theory, delamination stresses in a semicircular laminated composite curved bar subjected to end forces and end moments were calculated, and their radial locations determined. A family of design curves was presented, showing variation of the intensity of delamination stresses and their radial locations with different geometry and different degrees of anisotropy of the curved bar. The effect of anisotropy on the location of peak delamination stress was found to be small.

Edge effects and delamination failures

NASA Technical Reports Server (NTRS)

Herakovich, C. T.

1989-01-01

The fundamental relationship between the morphology of a composite laminate and the resulting free edge effects is explored and related to delamination failures. Cross-ply, angle-ply, and quasi-isotropic laminates are discussed in detail. It is shown that the local mismatch in elastic properties of adjacent layers and the global stacking sequence of a laminate both have a significant influence on the interlaminar stresses and delamination failures.

The Inclusion of In-Plane Stresses in Delamination Criteria

NASA Technical Reports Server (NTRS)

Vizzini, Anthony J.; Fenske, Matthew T.

1998-01-01

A study of delamination is performed including strength of materials and fracture mechanics approaches with emphasis placed on methods of delamination prediction. Evidence is presented which supports the inclusion of the in-plane stresses in addition to the inter-laminar stress terms in delamination criteria. The delamination can be modeled as a resin rich region in between ply sets. The entire six component stress state in this resin layer is calculated through a finite element analysis and inputted into a new Modified Von Mises Delamination Criterion. This criterion builds onto previous criteria by including all six stress components. The MVMDC shows improved correlation to experimental data.

Local delamination in laminates with angle ply matrix cracks. Part 2: Delamination fracture analysis and fatigue characterization

NASA Technical Reports Server (NTRS)

Obrien, T. Kevin

1991-01-01

Constant amplitude tension-tension fatigue tests were conducted on AS4/3501-6 graphite/epoxy (02/ theta sub 2/ -(theta sub 2))sub s laminates, where theta was 15, 20, 25, or 30 degrees. Fatigue tests were conducted at a frequency of 5 Hz and an R-ratio of 0.1. Dye penetrant enhanced x-radiography was used to document the onset of matrix cracking in the central -(theta) degree plies, and the subsequent onset of local delaminations in the theta/ -(theta) interface at the intersection of the matrix cracks and the free edge, as a function of the number of fatigue cycles. Two strain energy release rate solutions for local delamination from matrix cracks were derived: one for a local delamination growing from an angle ply matrix crack with a uniform delamination growing from an angle ply matrix crack with a triangular shaped delamination area that extended only partially into the laminate width from the free edge. Plots of G(max) vs. N were generated to assess the accuracy of these G solutions. The influence of residual thermal and moisture stresses on G were also quantified. However, a detailed analysis of the G components and a mixed-mode fatigue failure criterion for this material may be needed to predict the fatigue behavior of these laminates.

Numerical simulations of the mantle lithosphere delamination

NASA Astrophysics Data System (ADS)

Morency, C.; Doin, M.-P.

2004-03-01

Sudden uplift, extension, and increased igneous activity are often explained by rapid mechanical thinning of the lithospheric mantle. Two main thinning mechanisms have been proposed, convective removal of a thickened lithospheric root and delamination of the mantle lithosphere along the Moho. In the latter case, the whole mantle lithosphere peels away from the crust by the propagation of a localized shear zone and sinks into the mantle. To study this mechanism, we perform two-dimensional (2-D) numerical simulations of convection using a viscoplastic rheology with an effective viscosity depending strongly on temperature, depth, composition (crust/mantle), and stress. The simulations develop in four steps. (1) We first obtain "classical" sublithospheric convection for a long time period (˜300 Myr), yielding a slightly heterogeneous lithospheric temperature structure. (2) At some time, in some simulations, a strong thinning of the mantle occurs progressively in a small area (˜100 km wide). This process puts the asthenosphere in direct contact with the lower crust. (3) Large pieces of mantle lithosphere then quickly sink into the mantle by the horizontal propagation of a detachment level away from the "asthenospheric conduit" or by progressive erosion on the flanks of the delaminated area. (4) Delamination pauses or stops when the lithospheric mantle part detaches or when small-scale convection on the flanks of the delaminated area is counterbalanced by heat diffusion. We determine the parameters (crustal thicknesses, activation energies, and friction coefficients) leading to delamination initiation (step 2). We find that delamination initiates where the Moho temperature is the highest, as soon as the crust and mantle viscosities are sufficiently low. Delamination should occur on Earth when the Moho temperature exceeds ˜800°C. This condition can be reached by thermal relaxation in a thickened crust in orogenic setting or by corner flow lithospheric erosion in the

Guided Wave Delamination Detection and Quantification With Wavefield Data Analysis

NASA Technical Reports Server (NTRS)

Tian, Zhenhua; Campbell Leckey, Cara A.; Seebo, Jeffrey P.; Yu, Lingyu

2014-01-01

Unexpected damage can occur in aerospace composites due to impact events or material stress during off-nominal loading events. In particular, laminated composites are susceptible to delamination damage due to weak transverse tensile and inter-laminar shear strengths. Developments of reliable and quantitative techniques to detect delamination damage in laminated composites are imperative for safe and functional optimally-designed next-generation composite structures. In this paper, we investigate guided wave interactions with delamination damage and develop quantification algorithms by using wavefield data analysis. The trapped guided waves in the delamination region are observed from the wavefield data and further quantitatively interpreted by using different wavenumber analysis methods. The frequency-wavenumber representation of the wavefield shows that new wavenumbers are present and correlate to trapped waves in the damage region. These new wavenumbers are used to detect and quantify the delamination damage through the wavenumber analysis, which can show how the wavenumber changes as a function of wave propagation distance. The location and spatial duration of the new wavenumbers can be identified, providing a useful means not only for detecting the presence of delamination damage but also allowing for estimation of the delamination size. Our method has been applied to detect and quantify real delamination damage with complex geometry (grown using a quasi-static indentation technique). The detection and quantification results show the location, size, and shape of the delamination damage.

Edge Delamination of Monolayer Transition Metal Dichalcogenides.

PubMed

Ly, Thuc Hue; Yun, Seok Joon; Thi, Quoc Huy; Zhao, Jiong

2017-07-25

Delamination of thin films from the supportive substrates is a critical issue within the thin film industry. The emergent two-dimensional, atomic layered materials, including transition metal dichalcogenides, are highly flexible; thus buckles and wrinkles can be easily generated and play vital roles in the corresponding physical properties. Here we introduce one kind of patterned buckling behavior caused by the delamination from a substrate initiated at the edges of the chemical vapor deposition synthesized monolayer transition metal dichalcogenides, led by thermal expansion mismatch. The atomic force microscopy and optical characterizations clearly showed the puckered structures associated with the strain, whereas the transmission electron microscopy revealed the special sawtooth-shaped edges, which break the geometrical symmetry for the buckling behavior of hexagonal samples. The condition of the edge delamination is in accordance with the fracture behavior of thin film interfaces. This edge delamination and buckling process is universal for most ultrathin two-dimensional materials, which requires more attention in various future applications.

Visualization of delamination in composite materials utilizing advanced X-ray imaging techniques

NASA Astrophysics Data System (ADS)

Vavrik, D.; Jakubek, J.; Jandejsek, I.; Krejci, F.; Kumpova, I.; Zemlicka, J.

2015-04-01

This work is focused on the development of instrumental radiographic methods for detection of delaminations in layered carbon fibre reinforced plastic composites used in the aerospace industry. The main limitation of current visualisation techniques is a very limited possibility to image so-called closed delaminations in which delaminated layers are in contact practically with no physical gap. In this contribution we report the development of innovative methods for closed delamination detection using an X-ray phase contrast technique for which the distance between delamination surfaces is not relevant. The approach is based on the energetic sensitivity of phase-enhanced radiography. Based on the applied methodology, we can distinguish both closed and open delamination. Further we have demonstrated the possibility to visualise open delaminations characterised by a physical gap between delaminated layers. This delamination type was successfully identified and visualized utilizing a high resolution and computed tomography table-top technique based on proper beam-hardening effect correction.

Analysis of delamination in cross ply laminates initiating from impact induced matrix cracking

NASA Technical Reports Server (NTRS)

Salpekar, S. A.

1991-01-01

Several two dimensional finite element analyses of (0 sub 2/90 sub 8/0 sub 2) glass/epoxy and graphite-epoxy composite laminates were performed to study some of the characteristics of damage development due to an impact load. A cross section through the thickness of the laminate with fixed ends, and carrying a transverse load in the center was analyzed. Inclined matrix cracks such as those produced by low velocity impact were modeled in the 90 deg ply group. The introduction of the matrix cracks caused large interlaminar tension and shear stresses in the vicinity of both crack tips in the 0/90 and 90/0 interfaces. The large interlaminar stresses at the ends of the matrix cracks indicate that matrix cracking may give rise to delamination. The ratio of mode I to total strain energy release rate at the beginning of delamination calculated at the two matrix crack tips was 60 and 28 pct., respectively, in the glass/epoxy laminate. The corresponding ratio was 97 and 77 pct. in the graphite-epoxy laminate. Thus, a significant mode I component of strain energy release rate may be present at the delamination initiation due to an impact load.

Delamination modeling of laminate plate made of sublaminates

NASA Astrophysics Data System (ADS)

Kormaníková, Eva; Kotrasová, Kamila

2017-07-01

The paper presents the mixed-mode delamination of plates made of sublaminates. To this purpose an opening load mode of delamination is proposed as failure model. The failure model is implemented in ANSYS code to calculate the mixed-mode delamination response as energy release rate. The analysis is based on interface techniques. Within the interface finite element modeling there are calculated the individual components of damage parameters as spring reaction forces, relative displacements and energy release rates along the lamination front.

A study of delamination buckling of laminates

NASA Technical Reports Server (NTRS)

Mukherjee, Yu-Xie; Xie, Zhi-Cheng; Ingraffea, Anthony

1990-01-01

The subject of this paper is the buckling of laminated plates, with a preexisting delamination, subjected to in-plane loading. Each laminate is modelled as an orthotropic Mindlin plate. The analysis is carried out by a combination of the finite element and asymptotic expansion methods. By applying the finite element method, plates with general delamination regions can be studied. The asymptotic expansion method reduces the number of unknown variables of the eigenvalue equation to that of the equation for a single Kirchhoff plate. Numerical results are presented for several examples. The effects of the shape, size, and position of the delamination on the buckling load are studied through these examples.

Orogenic delamination - dynamics, effects, and geological expression

NASA Astrophysics Data System (ADS)

Ueda, Kosuke; Gerya, Taras

2010-05-01

Unbundling of continental lithosphere and removal of its mantle portion have been described by two mutually rather exclusive models, convective thinning and integral delamination. Either disburdens the remaining lithosphere, weakens the remainder, and causes uplift and extension. Increased heat flux is likely to promote high-degree crustal melting, and has been viewed as a source for voluminous granitic intrusions in late or collapsing orogenic settings. Collapse may be driven by any of gravitational potential differences from orogen to foreland, by stress inversion in the unburdened domain, or by suction of a retreating trench. In this study, we investigate prerequisites, mechanism, and development paths for orogeny-related mantle lithosphere removal. Our experiments numerically reproduce delamination which self-consistently results from the dynamics of a decoupling collision zone. In particular, it succeeds without a seed facilitating initial separation of layers. External shortening of a continent - ocean - continent assembly, such as to initiate oceanic subduction, is lifted before the whole oceanic part is consumed, leaving slab pull to govern further convergence. Once buoyant continental crust enters, the collision zone locks, and convergence diminishes. Under favourable conditions, delamination then initiates close to the edge of the mantle wedge and at deep crustal levels. While it initially separates upper crust from lower crust according to the weakness minimum in the lithospheric strength profile, the lower crust is eventually also delaminated from the subducting lithospheric mantle, owing to buoyancy differences. The level of delamination within the lithosphere seems thus first rheology-controlled, then density-controlled. Subduction-coupled delamination is contingent on retreat and decoupling of the subducting slab, which in turn is dependent on effective rheological weakening of the plate contact. Weakening is a function of shear-heating and hereby of

Effect of initial delamination on Mode 1 and Mode 2 interlaminar fracture toughness and fatigue fracture threshold

NASA Technical Reports Server (NTRS)

Murri, Gretchen Bostaph; Martin, Roderick H.

1991-01-01

Static and fatigue double-cantilever beam (DCB) and end-notch flexure (ENF) tests were conducted to determine the effect of the simulated initial delamination in interlaminar fracture toughness, G(sub c), and fatigue fracture threshold, G(sub th). Unidirectional, 24-ply specimens of S2/SP250 glass/epoxy were tested using Kapton inserts of four different thickness - 13, 25, 75, and 130 microns, at the midplane at one end, or with tension or shear precracks, to simulate an initial delamination. To determine G(sub c), the fatigue fracture threshold below which no delamination growth would occur in less than 1 x 10(exp 6) cycles, fatigue tests were conducted by cyclically loading specimens until delamination growth was detected. Consistent values of model 1 fracture toughness, G(sub Ic), were measured from DCB specimens with inserts of thickness 75 microns or thinner, or with shear precracks. The fatigue DCB tests gave similar values of G(sub Ith) for the 13, 25, and 75 microns specimens. Results for the shear precracked specimens were significantly lower that for specimens without precracks. Results for both the static and fatigue ENF tests showed that measured G(IIc) and G(IIth) values decreased with decreasing insert thickness, so that no limiting thickness could be determined. Results for specimens with inserts of 75 microns or thicker were significantly higher than the results for precracked specimens or specimens with 13 or 25 microns inserts.

Crack detection and fatigue related delamination in FRP composites applied to concrete

NASA Astrophysics Data System (ADS)

Brown, Jeff; Baker, Rebecca; Kallemeyn, Lisa; Zendler, Andrew

2008-03-01

Reinforced concrete beams are designed to allow minor concrete cracking in the tension zone. The severity of cracking in a beam element is a good indicator of how well a structure is performing and whether or not repairs are needed to prevent structural failure. FRP composites are commonly used to increase the flexural and shear capacity of RC beam elements, but one potential disadvantage of this method is that strengthened surfaces are no longer visible and cracks or delaminations that result from excessive loading or fatigue may go undetected. This research investigated thermal imaging techniques for detecting load induced cracking in the concrete substrate and delamination of FRP strengthening systems applied to reinforced concrete (RC). One small-scale RC beam (5 in. x 6 in. x 60 in.) was strengthened with FRP and loaded to failure monotonically. An infrared thermography inspection was performed after failure. A second strengthened beam was loaded cyclically for 1,750,000 cycles to investigate how fatigue might affect substrate cracking and delamination growth throughout the service-life of a repaired element. No changes were observed in the FRP bond during/after the cyclic loading. The thermal imaging component of this research included pixel normalization to enhance detectability and characterization of this specific type of damage.

Magmatism in Lithosphere Delamination process inferred from numerical models

NASA Astrophysics Data System (ADS)

Göǧüş, Oǧuz H.; Ueda, Kosuke; Gerya, Taras

2017-04-01

The peel away of the oceanic/continental slab from the overlying orogenic crust has been suggested as a ubiquitous process in the Alpine-Mediterranean orogenic region (e.g. Carpathians, Apennines, Betics and Anatolia). The process is defined as lithospheric delamination where a slab removal/peel back may allow for the gradual uprising of sub-lithospheric mantle, resulting in high heat flow, transient surface uplift/subsidence and varying types of magma production. Geodynamical modeling studies have adressed the surface response to the delamination in the context of regional tectonic processes and explored wide range of controlling parameters in pre-syn and post collisional stages. However, the amount and styles of melt production in the mantle (e.g. decompression melting, wet melting in the wedge) and the resulting magmatism due to the lithosphere delamination remains uncertain. In this work, by using thermomechanical numerical experiments, designed in the configuration of subduction to collision, we investigated how melting in the mantle develops in the course of delamination. Furthermore, model results are used to decipher the distribution of volumetric melt production, melt extraction and the source of melt and the style of magmatism (e.g. igneous vs. volcanic). The model results suggest that a broad region of decompression melting occurs under the crust, mixing with the melting of the hydrated mantle derived by the delaminating/subducting slab. Depending on the age of the ocean slab, plate convergence velocity and the mantle temperature, the melt production and crust magmatism may concentrate under the mantle wedge or in the far side of the delamination front (where the subduction begins). The slab break-off usually occurs in the terminal stages of the delamination process and it may effectively control the location of the magmatism in the crust. The model results are reconciled with the temporal and spatial distribution of orogenic vs. anorogenic magmatism in

Numerical investigation of the effect of delaminations on fracture characteristics of glare

NASA Astrophysics Data System (ADS)

Bhat, Sunil; Narayanan, S.

2013-10-01

A finite element examination of the effect of delaminations on fracture characteristics of fibre metal laminate (Glare), by comparing energy release rates of normal cracks in laminates with and without delaminations, is presented in the paper. Glare comprising thin cracked 2024-T3 aerospace aluminum alloy layers alternately bonded with E-glass fibre based composite prepregs is considered for the analysis. Delaminations are modeled with interface cohesive elements. Energy release rates of normal cracks in laminates with delaminations are found to be higher than those in the laminates without delaminations.

Dynamic delamination of patterned thin films

NASA Astrophysics Data System (ADS)

Kandula, Soma S. V.; Tran, Phuong; Geubelle, Philippe H.; Sottos, Nancy R.

2008-12-01

We investigate laser-induced dynamic delamination of a patterned thin film on a substrate. Controlled delamination results from our insertion of a weak adhesion region beneath the film. The inertial forces acting on the weakly bonded portion of the film lead to stable propagation of a crack along the film/substrate interface. Through a simple energy balance, we extract the critical energy for interfacial failure, a quantity that is difficult and sometimes impossible to characterize by more conventional methods for many thin film/substrate combinations.

Delamination analysis of metal-ceramic multilayer coatings subject to nanoindentation

DOE PAGES

Jamison, Ryan Dale; Shen, Yu -Lin

2016-01-22

Internal damage has been experimentally observed in aluminum (Al)/silicon carbide (SiC) multilayer coatings subject to nanoindentation loading. Post-indentation characterization has identified that delamination at the coating/substrate interface is the most prominent form of damage. In this study the finite element method is employed to study the effect of delamination on indentation-derived hardness and Young's modulus. The model features alternating Al/SiC nanolayers above a silicon (Si) substrate, in consistence with the actual material system used in earlier experiments. Cohesive elements with a traction–separation relationship are used to facilitate delamination along the coating/substrate interface. Delamination is observed numerically to be sensitive tomore » the critical normal and shear stresses that define the cohesive traction–separation behavior. Axial tensile stress below the edge of indentation contact is found to be the largest contributor to damage initiation and evolution. Delamination results in a decrease in both indentation-derived hardness and Young's modulus. As a result, a unique finding is that delamination can occur during the unloading process of indentation, depending on the loading condition and critical tractions.« less

Spemann organizer gene Goosecoid promotes delamination of neuroblasts from the otic vesicle.

PubMed

Kantarci, Husniye; Gerberding, Andrea; Riley, Bruce B

2016-11-01

Neurons of the Statoacoustic Ganglion (SAG), which innervate the inner ear, originate as neuroblasts in the floor of the otic vesicle and subsequently delaminate and migrate toward the hindbrain before completing differentiation. In all vertebrates, locally expressed Fgf initiates SAG development by inducing expression of Neurogenin1 (Ngn1) in the floor of the otic vesicle. However, not all Ngn1-positive cells undergo delamination, nor has the mechanism controlling SAG delamination been elucidated. Here we report that Goosecoid (Gsc), best known for regulating cellular dynamics in the Spemann organizer, regulates delamination of neuroblasts in the otic vesicle. In zebrafish, Fgf coregulates expression of Gsc and Ngn1 in partially overlapping domains, with delamination occurring primarily in the zone of overlap. Loss of Gsc severely inhibits delamination, whereas overexpression of Gsc greatly increases delamination. Comisexpression of Ngn1 and Gsc induces ectopic delamination of some cells from the medial wall of the otic vesicle but with a low incidence, suggesting the action of a local inhibitor. The medial marker Pax2a is required to restrict the domain of gsc expression, and misexpression of Pax2a is sufficient to block delamination and fully suppress the effects of Gsc The opposing activities of Gsc and Pax2a correlate with repression or up-regulation, respectively, of E-cadherin (cdh1). These data resolve a genetic mechanism controlling delamination of otic neuroblasts. The data also elucidate a developmental role for Gsc consistent with a general function in promoting epithelial-to-mesenchymal transition (EMT).

Spemann organizer gene Goosecoid promotes delamination of neuroblasts from the otic vesicle

PubMed Central

Kantarci, Husniye; Gerberding, Andrea; Riley, Bruce B.

2016-01-01

Neurons of the Statoacoustic Ganglion (SAG), which innervate the inner ear, originate as neuroblasts in the floor of the otic vesicle and subsequently delaminate and migrate toward the hindbrain before completing differentiation. In all vertebrates, locally expressed Fgf initiates SAG development by inducing expression of Neurogenin1 (Ngn1) in the floor of the otic vesicle. However, not all Ngn1-positive cells undergo delamination, nor has the mechanism controlling SAG delamination been elucidated. Here we report that Goosecoid (Gsc), best known for regulating cellular dynamics in the Spemann organizer, regulates delamination of neuroblasts in the otic vesicle. In zebrafish, Fgf coregulates expression of Gsc and Ngn1 in partially overlapping domains, with delamination occurring primarily in the zone of overlap. Loss of Gsc severely inhibits delamination, whereas overexpression of Gsc greatly increases delamination. Comisexpression of Ngn1 and Gsc induces ectopic delamination of some cells from the medial wall of the otic vesicle but with a low incidence, suggesting the action of a local inhibitor. The medial marker Pax2a is required to restrict the domain of gsc expression, and misexpression of Pax2a is sufficient to block delamination and fully suppress the effects of Gsc. The opposing activities of Gsc and Pax2a correlate with repression or up-regulation, respectively, of E-cadherin (cdh1). These data resolve a genetic mechanism controlling delamination of otic neuroblasts. The data also elucidate a developmental role for Gsc consistent with a general function in promoting epithelial-to-mesenchymal transition (EMT). PMID:27791112

A review on mode-I interlaminar fracture toughness of fibre reinforced composites

NASA Astrophysics Data System (ADS)

Nasuha, N.; Azmi, A. I.; Tan, C. L.

2017-10-01

Composite material has been growing rapidly throughout the year for its unique properties in comparisons with metal. Recently, there has been a growth on studying the way to reduce the delamination failure, which is the primary challenge on laminated fibre composite. This failure can degrade the strength of composite materials, hence loses its function. In this review, database search was performed using the keywords search on “interlaminar fracture toughness”, “double cantilever beam”, “delamination resistance” and “Mode-I GIC”. The searches were performed on Google Scholar, Scopus and Web of Science with further cross-referencing with other databases. Most relevant studies were selected for review and referencing by the author. This review paper gives a brief explanation on Mode-I interlaminar fracture toughness of composite material. This fracture mode is the most common modes on studying the delamination failure.

Characterization of Blistering and Delamination in Depleted Uranium Hohlraums

DOE Office of Scientific and Technical Information (OSTI.GOV)

Biobaum, K. J. M.

2013-03-01

Blistering and delamination are the primary failure mechanisms during the processing of depleted uranium (DU) hohlraums. These hohlraums consist of a sputter-deposited DU layer sandwiched between two sputter-deposited layers of gold; a final thick gold layer is electrodeposited on the exterior. The hohlraum is deposited on a copper-coated aluminum mandrel; the Al and Cu are removed with chemical etching after the gold and DU layers are deposited. After the mandrel is removed, blistering and delamination are observed on the interiors of some hohlraums, particularly at the radius region. It is hypothesized that blisters are caused by pinholes in the coppermore » and gold layers; etchant leaking through these holes reaches the DU layer and causes it to oxidize, resulting in a blister. Depending on the residual stress in the deposited layers, blistering can initiate larger-scale delamination at layer interfaces. Scanning electron microscopy indicates that inhomogeneities in the machined aluminum mandrel are replicated in the sputter-deposited copper layer. Furthermore, the Cu layer exhibits columnar growth with pinholes that likely allow etchant to come in contact with the gold layer. Any inhomogeneities or pinholes in this initial gold layer then become nucleation sites for blistering. Using a focused ion beam system to etch through the gold layer and extract a cross-sectional sample for transmission electron microscopy, amorphous, intermixed layers at the gold/DU interfaces are observed. Nanometer-sized bubbles in the sputtered and electrodeposited gold layers are also present. Characterization of the morphology and composition of the deposited layers is the first step in determining modifications to processing parameters, with the goal of attaining a significant improvement in hohlraum yield.« less

EBSD and Nanoindentation-Correlated Study of Delamination Fracture in Al-Li Alloy 2090

NASA Technical Reports Server (NTRS)

Tayon, Wesley A.; Crooks, Roy E.; Domack, Marcia S.; Wagner, John A.; Elmustafa, A. A.

2008-01-01

Al-Li alloys offer attractive combinations of high strength and low density. However, a tendency for delamination fracture has limited their use. A better understanding of the delamination mechanisms may identify methods to control delaminations through processing modifications. A combination of new techniques has been used to evaluate delamination fracture in Al-Li alloys. Both high quality electron backscattered diffraction (EBSD) information and valid nanoindentation measurements were obtained from fractured test specimens. Correlations were drawn between nano-scale hardness variations and local texture along delaminating boundaries. Intriguing findings were observed for delamination fracture through the combined analysis of grain orientation, Taylor factor, and kernel average misorientation.

Convergence of strain energy release rate components for edge-delaminated composite laminates

NASA Technical Reports Server (NTRS)

Raju, I. S.; Crews, J. H., Jr.; Aminpour, M. A.

1987-01-01

Strain energy release rates for edge delaminated composite laminates were obtained using quasi 3 dimensional finite element analysis. The problem of edge delamination at the -35/90 interfaces of an 8-ply composite laminate subjected to uniform axial strain was studied. The individual components of the strain energy release rates did not show convergence as the delamination tip elements were made smaller. In contrast, the total strain energy release rate converged and remained unchanged as the delamination tip elements were made smaller and agreed with that calculated using a classical laminated plate theory. The studies of the near field solutions for a delamination at an interface between two dissimilar isotropic or orthotropic plates showed that the imaginary part of the singularity is the cause of the nonconvergent behavior of the individual components. To evaluate the accuracy of the results, an 8-ply laminate with the delamination modeled in a thin resin layer, that exists between the -35 and 90 plies, was analyzed. Because the delamination exists in a homogeneous isotropic material, the oscillatory component of the singularity vanishes.

Delaminated graphene at silicon carbide facets: atomic scale imaging and spectroscopy.

PubMed

Nicotra, Giuseppe; Ramasse, Quentin M; Deretzis, Ioannis; La Magna, Antonino; Spinella, Corrado; Giannazzo, Filippo

2013-04-23

Atomic-resolution structural and spectroscopic characterization techniques (scanning transmission electron microscopy and electron energy loss spectroscopy) are combined with nanoscale electrical measurements (conductive atomic force microscopy) to study at the atomic scale the properties of graphene grown epitaxially through the controlled graphitization of a hexagonal SiC(0001) substrate by high temperature annealing. This growth technique is known to result in a pronounced electron-doping (∼10(13) cm(-2)) of graphene, which is thought to originate from an interface carbon buffer layer strongly bound to the substrate. The scanning transmission electron microscopy analysis, carried out at an energy below the knock-on threshold for carbon to ensure no damage is imparted to the film by the electron beam, demonstrates that the buffer layer present on the planar SiC(0001) face delaminates from it on the (112n) facets of SiC surface steps. In addition, electron energy loss spectroscopy reveals that the delaminated layer has a similar electronic configuration to purely sp2-hybridized graphene. These observations are used to explain the local increase of the graphene sheet resistance measured around the surface steps by conductive atomic force microscopy, which we suggest is due to significantly lower substrate-induced doping and a resonant scattering mechanism at the step regions. A first-principles-calibrated theoretical model is proposed to explain the structural instability of the buffer layer on the SiC facets and the resulting delamination.

Guided wave energy trapping to detect hidden multilayer delamination damage

NASA Astrophysics Data System (ADS)

Leckey, Cara A. C.; Seebo, Jeffrey P.

2015-03-01

Nondestructive Evaluation (NDE) and Structural Health Monitoring (SHM) simulation tools capable of modeling three-dimensional (3D) realistic energy-damage interactions are needed for aerospace composites. Current practice in NDE/SHM simulation for composites commonly involves over-simplification of the material parameters and/or a simplified two-dimensional (2D) approach. The unique damage types that occur in composite materials (delamination, microcracking, etc) develop as complex 3D geometry features. This paper discusses the application of 3D custom ultrasonic simulation tools to study wave interaction with multilayer delamination damage in carbon-fiber reinforced polymer (CFRP) composites. In particular, simulation based studies of ultrasonic guided wave energy trapping due to multilayer delamination damage were performed. The simulation results show changes in energy trapping at the composite surface as additional delaminations are added through the composite thickness. The results demonstrate a potential approach for identifying the presence of hidden multilayer delamination damage in applications where only single-sided access to a component is available. The paper also describes recent advancements in optimizing the custom ultrasonic simulation code for increases in computation speed.

Growth dominates choice in network percolation

NASA Astrophysics Data System (ADS)

Vijayaraghavan, Vikram S.; Noël, Pierre-André; Waagen, Alex; D'Souza, Raissa M.

2013-09-01

The onset of large-scale connectivity in a network (i.e., percolation) often has a major impact on the function of the system. Traditionally, graph percolation is analyzed by adding edges to a fixed set of initially isolated nodes. Several years ago, it was shown that adding nodes as well as edges to the graph can yield an infinite order transition, which is much smoother than the traditional second-order transition. More recently, it was shown that adding edges via a competitive process to a fixed set of initially isolated nodes can lead to a delayed, extremely abrupt percolation transition with a significant jump in large but finite systems. Here we analyze a process that combines both node arrival and edge competition. If started from a small collection of seed nodes, we show that the impact of node arrival dominates: although we can significantly delay percolation, the transition is of infinite order. Thus, node arrival can mitigate the trade-off between delay and abruptness that is characteristic of explosive percolation transitions. This realization may inspire new design rules where network growth can temper the effects of delay, creating opportunities for network intervention and control.

A Cohesive Zone Approach for Fatigue-Driven Delamination Analysis in Composite Materials

NASA Astrophysics Data System (ADS)

Amiri-Rad, Ahmad; Mashayekhi, Mohammad

2017-08-01

A new model for prediction of fatigue-driven delamination in laminated composites is proposed using cohesive interface elements. The presented model provides a link between cohesive elements damage evolution rate and crack growth rate of Paris law. This is beneficial since no additional material parameters are required and the well-known Paris law constants are used. The link between the cohesive zone method and fracture mechanics is achieved without use of effective length which has led to more accurate results. The problem of unknown failure path in calculation of the energy release rate is solved by imposing a condition on the damage model which leads to completely vertical failure path. A global measure of energy release rate is used for the whole cohesive zone which is computationally more efficient compared to previous similar models. The performance of the proposed model is investigated by simulation of well-known delamination tests and comparison against experimental data of the literature.

Effective Simulation of Delamination in Aeronautical Structures Using Shells and Cohesive Elements

NASA Technical Reports Server (NTRS)

Davila, Carlos G.; Camanho, Pedro P.; Turon, Albert

2007-01-01

A cohesive element for shell analysis is presented. The element can be used to simulate the initiation and growth of delaminations between stacked, non-coincident layers of shell elements. The procedure to construct the element accounts for the thickness offset by applying the kinematic relations of shell deformation to transform the stiffness and internal force of a zero-thickness cohesive element such that interfacial continuity between the layers is enforced. The procedure is demonstrated by simulating the response and failure of the Mixed Mode Bending test and a skin-stiffener debond specimen. In addition, it is shown that stacks of shell elements can be used to create effective models to predict the inplane and delamination failure modes of thick components. The results indicate that simple shell models can retain many of the necessary predictive attributes of much more complex 3D models while providing the computational efficiency that is necessary for design.

Patterns of growth dominance in thinned yellow-poplar stands in the southern Appalachian Mountains, USA

Treesearch

Tara L. Keyser

2012-01-01

Growth dominance provides a quantitative description of the relative contribution of individual trees to stand growth. Positive dominance occurs when the largest individuals account for a greater proportion of growth period increment than total biomass. Conversely, negative dominance occurs when the smallest trees account for a greater proportion of the growth period...

Analysis of local delaminations caused by angle ply matrix cracks

NASA Technical Reports Server (NTRS)

Salpekar, Satish A.; Obrien, T. Kevin; Shivakumar, K. N.

1993-01-01

Two different families of graphite/epoxy laminates with similar layups but different stacking sequences, (0,theta,-theta) sub s and (-theta/theta/0) sub s were analyzed using three-dimensional finite element analysis for theta = 15 and 30 degrees. Delaminations were modeled in the -theta/theta interface, bounded by a matrix crack and the stress free edge. The total strain energy release rate, G, along the delamination front was computed using three different techniques: the virtual crack closure technique (VCCT), the equivalent domain Integral (EDI) technique, and a global energy balance technique. The opening fracture mode component of the strain energy release rate, Gl, along the delamination front was also computed for various delamination lengths using VCCT. The effect of residual thermal and moisture stresses on G was evaluated.

Microscopic mechanisms of graphene electrolytic delamination from metal substrates

DOE Office of Scientific and Technical Information (OSTI.GOV)

Fisichella, G.; Department of Electronic Engineering, University of Catania, Viale A. Doria, 6 – 95125 Catania; Di Franco, S.

In this paper, hydrogen bubbling delamination of graphene (Gr) from copper using a strong electrolyte (KOH) water solution was performed, focusing on the effect of the KOH concentration (C{sub KOH}) on the Gr delamination rate. A factor of ∼10 decrease in the time required for the complete Gr delamination from Cu cathodes with the same geometry was found increasing C{sub KOH} from ∼0.05 M to ∼0.60 M. After transfer of the separated Gr membranes to SiO{sub 2} substrates by a highly reproducible thermo-compression printing method, an accurate atomic force microscopy investigation of the changes in Gr morphology as a function of C{submore » KOH} was performed. Supported by these analyses, a microscopic model of the delamination process has been proposed, where a key role is played by graphene wrinkles acting as nucleation sites for H{sub 2} bubbles at the cathode perimeter. With this approach, the H{sub 2} supersaturation generated at the electrode for different electrolyte concentrations was estimated and the inverse dependence of t{sub d} on C{sub KOH} was quantitatively explained. Although developed in the case of Cu, this analysis is generally valid and can be applied to describe the electrolytic delamination of graphene from several metal substrates.« less

Delamination propensity of pharmaceutical glass containers by accelerated testing with different extraction media.

PubMed

Guadagnino, Emanuel; Zuccato, Daniele

2012-01-01

The delamination of pharmaceutical glass is a serious issue, as it can cause glass particles to appear in vials, a problem that has forced a number of drug product recalls in recent years. In Type I pharmaceutical glass vials, delamination occurs generally at the bottom and shoulder, where extensive flaming during the conversion process can favor a strong evaporation of alkali and borate species and the formation of heavily enriched silica layers. The contact with parenteral preparations dissolved in an alkaline medium increases the rate of glass corrosion, while the differential hydration of these layers can cause the detachment of flakes. The purpose of this study was to investigate the effect of the pH and the composition of the extraction solutions on the propensity of different glass types to delaminate. Repeated autoclave extractions at 121 °C were carried out on different glass types with different extraction media, including organic extractants like citric and glutaric acid. When vials were in contact with alkaline solutions and similarly aggressive media, an increase in silica extraction values indicated glass corrosion and an increasing risk for further delamination. Under such conditions expansion 33 glass is extensively corroded, showing high silica concentration and heavy flaking as compared to other glass types. Sulfur-treated glass also showed early flaking, even if SiO(2) concentration was very low. A similar ranking was observed with extractions carried out with glutaric and citric acids, but at far much higher SiO(2) concentration levels. Extractions with 0.9% KCl solution can be used as an accelerated test to highlight the propensity of a glass to delaminate, but in no case it can be taken as a guarantee that the glass will not delaminate when exposed to the pharmaceutical drug, whose extraction ability requires case-by-case study. How can injectable drug manufacturers prevent glass delamination? The issue of delamination is a serious one, as it

Mechanistic Study of Delamination Fracture in Al-Li Alloy C458 (2099)

NASA Technical Reports Server (NTRS)

Tayon, W. A.; Crooks, R. E.; Domack, M. S.; Wagner, J. A.; Beaudoin, A. J.; McDonald, R. J.

2009-01-01

Delamination fracture has limited the use of lightweight Al-Li alloys. In the present study, electron backscattered diffraction (EBSD) methods were used to characterize crack paths in Al-Li alloy C458 (2099). Secondary delamination cracks in fracture toughness samples showed a pronounced tendency for fracture between grain variants of the same deformation texture component. These results were analyzed by EBSD mapping methods and simulated with finite element analyses. Simulation procedures include a description of material anisotropy, local grain orientations, and fracture utilizing crystal plasticity and cohesive zone elements. Taylor factors computed for each grain orientation subjected to normal and shear stresses indicated that grain pairs with the largest Taylor factor differences were adjacent to boundaries that failed by delamination. Examination of matching delamination fracture surface pairs revealed pronounced slip bands in only one of the grains bordering the delamination. These results, along with EBSD studies, plasticity simulations, and Auger electron spectroscopy observations support a hypothesis that delamination fracture occurs due to poor slip accommodation along boundaries between grains with greatly differing plastic response.

Autosomal Dominant Growth Hormone Deficiency (Type II).

PubMed

Alatzoglou, Kyriaki S; Kular, Dalvir; Dattani, Mehul T

2015-06-01

Isolated growth hormone deficiency (IGHD) is the commonest pituitary hormone deficiency resulting from congenital or acquired causes, although for most patients its etiology remains unknown. Among the known factors, heterozygous mutations in the growth hormone gene (GH1) lead to the autosomal dominant form of GHD, also known as type II GHD. In many cohorts this is the commonest form of congenital isolated GHD and is mainly caused by mutations that affect the correct splicing of GH-1. These mutations cause skipping of the third exon and lead to the production of a 17.5-kDa GH isoform that exerts a dominant negative effect on the secretion of the wild type GH. The identification of these mutations has clinical implications for the management of patients, as there is a well-documented correlation between the severity of the phenotype and the increased expression of the 17.5-kDa isoform. Patients with type II GHD have a variable height deficit and severity of GHD and may develop additional pituitary hormone defiencies over time, including ACTH, TSH and gonadotropin deficiencies. Therefore, their lifelong follow-up is recommended. Detailed studies on the effect of heterozygous GH1 mutations on the trafficking, secretion and action of growth hormone can elucidate their mechanism on a cellular level and may influence future treatment options for GHD type II.

Assessing the Causes of Encapsulant Delamination in PV Modules

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wohlgemuth, John H.; Hacke, Peter; Bosco, Nick

Delamination of the encapsulant is one of the most prevalent PV module field failures. This paper will present examples of various types of delaminations that have been observed in the field. It will then discuss the development of accelerated stress tests designed to duplicate those field failures and thus provide tools for avoiding them in the future.

Structural vibration-based damage classification of delaminated smart composite laminates

NASA Astrophysics Data System (ADS)

Khan, Asif; Kim, Heung Soo; Sohn, Jung Woo

2018-03-01

Separation along the interfaces of layers (delamination) is a principal mode of failure in laminated composites and its detection is of prime importance for structural integrity of composite materials. In this work, structural vibration response is employed to detect and classify delaminations in piezo-bonded laminated composites. Improved layerwise theory and finite element method are adopted to develop the electromechanically coupled governing equation of a smart composite laminate with and without delaminations. Transient responses of the healthy and damaged structures are obtained through a surface bonded piezoelectric sensor by solving the governing equation in the time domain. Wavelet packet transform (WPT) and linear discriminant analysis (LDA) are employed to extract discriminative features from the structural vibration response of the healthy and delaminated structures. Dendrogram-based support vector machine (DSVM) is used to classify the discriminative features. The confusion matrix of the classification algorithm provided physically consistent results.

Detection of Internal Delamination in Composite Mono Leaf Spring based on Vibration Characteristics

NASA Astrophysics Data System (ADS)

Jamadar, Nagendra Iranna; Kivade, S. B.

2017-06-01

Structural health monitoring (SHM) is one of the non destructive evaluations universally accepted to detect defect or damage in composite structures. The paper deals with detection of inter laminar delamination problems in composite mono leaf spring during service conditions by vibration techniques. The delamination detection is crucial issue as it leads to catastrophic failure. The vibration parameters such as natural frequency and modes shapes are evaluated for healthy and delaminated spring. It has been observed that some mode shapes are found to be more sensitive to the delaminated region. The presence, location and severity of delamination are simulated and validated by experimental modal analysis for both the spring and found closer approximation with each other.

Delamination of Pearlitic Steel Wires: The Defining Role of Prior-Drawing Microstructure

NASA Astrophysics Data System (ADS)

Durgaprasad, A.; Giri, S.; Lenka, S.; Sarkar, Sudip Kumar; Biswas, Aniruddha; Kundu, S.; Mishra, S.; Chandra, S.; Doherty, R. D.; Samajdar, I.

2018-06-01

This article reports the occasional (< 10 pct of the actual production) delamination of pearlitic wires subjected to a drawing strain of 2.5. The original wire rods which exhibited post-drawing delamination had noticeably lower axial alignment of the pearlite: 22 ± 5 pct vs 34 ± 4 pct in the nondelaminated wires. Although all wires had similar through-thickness texture and stress gradients, delaminated wires had stronger gradients in composition and higher hardness across the ferrite-cementite interface. Carbide dissolution and formation of supersaturated ferrite were clearly correlated with delamination, which could be effectively mitigated by controlled laboratory annealing at 673 K. Direct observations on samples subjected to simple shear revealed significant differences in shear localizations. These were controlled by pearlite morphology and interlamellar spacing. Prior-drawing microstructure of coarse misaligned pearlite thus emerged as a critical factor in the wire drawing-induced delamination of the pearlitic wires.

Elastic solitons in delaminated bars: splitting leads to fission

NASA Astrophysics Data System (ADS)

Samsonov, A. M.; Dreiden, G. V.; Khusnutdinova, K. R.; Semenova, I. V.

2008-06-01

Recent theoretical and successful experimental studies confirmed existence and demonstrated main properties of bulk strain solitary waves in nonlinearly elastic solid wave guides. Our current research is devoted to nonlinear wave processes in layered elastic wave guides with inhomogeneities modelling delamination. We present first theoretical and experimental results showing the influence of delamination on the parameters of the longitudinal strain solitary wave.

Hygrothermal influence on delamination behavior of graphite/epoxy laminates

NASA Technical Reports Server (NTRS)

Garg, A.; Ishai, O.

1985-01-01

The hygrothermal effect on the fracture behavior of graphite-epoxy laminates was investigated to develop a methodology for damage tolerance predictions in advanced composite materials. Several T300/934 laminates were tested using a number of specimen configurations to evaluate the effects of temperature and humidity on delamination fracture toughness under mode 1 and mode 2 loading. It is indicated that moisture has a slightly beneficial influence on fracture toughness or critical strain energy release rate during mode 1 delamination, but has a slightly deleterious effect on mode 2 delamination, and mode 1 transverse cracking. The failed specimens are examined by SEM and topographical differences due to fracture modes are identified. It is concluded that the effect of moisture on fracture topography can not be distinguished.

Hygrothermal influence on delamination behavior of graphite/epoxy laminates

NASA Technical Reports Server (NTRS)

Garg, A.; Ishai, O.

1984-01-01

The hygrothermal effect on the fracture behavior of graphite-epoxy laminates was investigated to develop a methodology for damage tolerance predictions in advanced composite materials. Several T300/934 laminates were tested using a number of specimen configurations to evaluate the effects of temperature and humidity on delamination fracture toughness under mode 1 and mode 2 loading. It is indicated that moisture has a slightly beneficial influence on fracture toughness or critical strain energy release rate during mode 1 delamination, but has a slightly deleterious effect on mode 2 delamination and mode 1 transverse cracking. The failed specimens are examined by SEM and topographical differences due to fracture modes are identified. It is concluded that the effect of moisture on fracture topography can not be distinguished.

Detection of bondline delaminations in multilayer structures with lossy components

NASA Technical Reports Server (NTRS)

Madaras, Eric I.; Winfree, William P.; Smith, B. T.; Heyman, Joseph H.

1988-01-01

The detection of bondline delaminations in multilayer structures using ultrasonic reflection techniques is a generic problem in adhesively bonded composite structures such as the Space Shuttles's Solid Rocket Motors (SRM). Standard pulse echo ultrasonic techniques do not perform well for a composite resonator composed of a resonant layer combined with attenuating layers. Excessive ringing in the resonant layer tends to mask internal echoes emanating from the attenuating layers. The SRM is made up of a resonant steel layer backed by layers of adhesive, rubber, liner and fuel, which are ultrasonically attenuating. The structure's response is modeled as a lossy ultrasonic transmission line. The model predicts that the acoustic response of the system is sensitive to delaminations at the interior bondlines in a few narrow frequency bands. These predictions are verified by measurements on a fabricated system. Successful imaging of internal delaminations is sensitive to proper selection of the interrogating frequency. Images of fabricated bondline delaminations are presented based on these studies.

Assessment of probability of detection of delaminations in fiber-reinforced composites

NASA Technical Reports Server (NTRS)

Chern, E. J.; Chu, H. P.; Yang, J. N.

1991-01-01

Delamination is one of the critical defects in composite materials and structures. An ultrasonic C-scan imaging technique which maps out the acoustic impedance mismatched areas with respect to the sample coordinates, is particularly well suited for detecting and characterizing delaminations in composites. To properly interpret the results, it is necessary to correlate the indications with the detection limits and probability of detection (POD) of the ultrasonic C-scan imaging technique. The baseline information on the assessment of POD of delaminations in composite materials and structures is very beneficial to the evaluation of spacecraft materials. In this study, we review the principle of POD, describe the laboratory set-up and procedure, and present the experimental results as well as assessment of POD of delaminations in fiber reinforced composite panels using ultrasonic C-scan techniques.

Application of scanning laser Doppler vibrometry for delamination detection in composite structures

NASA Astrophysics Data System (ADS)

Kudela, Pawel; Wandowski, Tomasz; Malinowski, Pawel; Ostachowicz, Wieslaw

2017-12-01

In this paper application of scanning laser Doppler vibrometry for delamination detection in composite structures was presented. Delamination detection was based on a guided wave propagation method. In this papers results from numerical and experimental research were presented. In the case of numerical research, the Spectral Element Method (SEM) was utilized, in which a mesh was composed of 3D spectral elements. SEM model included also a piezoelectric transducer. In the experimental research guided waves were excited using the piezoelectric transducer whereas the sensing process was conducted using scanning laser Doppler vibrometer (SLDV). Analysis of guided wave propagation and its interaction with delamination was based on a full wavefield approach. Attention was focused on interactions of guided waves with delamination manifested by A0 mode reflection, A0 mode entrapment, and S0/A0 mode conversion. Delamination was simulated by a teflon insert located between plies of composite material. Results of interaction with symmetrically and nonsymmetrical placed delamination (in respect to the composite sample thickness) were presented. Moreover, the authors investigated different size of delaminations. Damage detection was based on a new signal processing algorithm proposed by the authors. In this approach the weighted RMS was utilized selectively. It means that the summation in RMS formula was performed only for a specially selected time instances. Results for simple composite panels, panel with honeycomb core, and real stiffened composite panel from the aircraft were presented.

Debonding/Delamination of Composites (Le Decollement et le Delaminage des Materiaux Composites)

DTIC Science & Technology

1992-12-01

augmented by the first cigenmode Z, magnified b% arc related, however, to a finite total potential energy % al- a scale factor ). In the algebraiL ,,stem...strength of cr ack canniit be measured because of the brushike mect- the r3tltl914C-material lapping of fibers. in reality , after a certain crack...the delamination growth This is not true in reality fracture theory the ERR is defined by and, therefor,, some ideas will be discucsed here to over

Cartilage Delamination Flap Mimicking a Torn Medial Meniscus

PubMed Central

Bin Abd Razak, Hamid Rahmatullah; Amit Kanta, Mitra

2016-01-01

We report a case of a chondral delamination lesion due to medial parapatellar plica friction syndrome involving the medial femoral condyle. This mimicked a torn medial meniscus in clinical and radiological presentation. Arthroscopy revealed a chondral delamination flap, which was debrided. Diagnosis of chondral lesions in the knee can be challenging. Clinical examination and MRI have good accuracy for diagnosis and should be used in tandem. Early diagnosis and treatment of chondral lesions are important to prevent progression to early osteoarthritis. PMID:28070434

Detection of Delamination in Composite Beams Using Broadband Acoustic Emission Signatures

NASA Technical Reports Server (NTRS)

Okafor, A. C.; Chandrashekhara, K.; Jiang, Y. P.

1996-01-01

Delamination in composite structure may be caused by imperfections introduced during the manufacturing process or by impact loads by foreign objects during the operational life. There are some nondestructive evaluation methods to detect delamination in composite structures such as x-radiography, ultrasonic testing, and thermal/infrared inspection. These methods are expensive and hard to use for on line detection. Acoustic emission testing can monitor the material under test even under the presence of noise generated under load. It has been used extensively in proof-testing of fiberglass pressure vessels and beams. In the present work, experimental studies are conducted to investigate the use of broadband acoustic emission signatures to detect delaminations in composite beams. Glass/epoxy beam specimens with full width, prescribed delamination sizes of 2 inches and 4 inches are investigated. The prescribed delamination is produced by inserting Teflon film between laminae during the fabrication of composite laminate. The objectives of this research is to develop a method for predicting delamination size and location in laminated composite beams by combining smart materials concept and broadband AE analysis techniques. More specifically, a piezoceramic (PZT) patch is bonded on the surface of composite beams and used as a pulser. The piezoceramic patch simulates the AE wave source as a 3 cycles, 50KHz, burst sine wave. One broadband AE sensor is fixed near the PZT patch to measure the AE wave near the AE source. A second broadband AE sensor, which is used as a receiver, is scanned along the composite beams at 0.25 inch step to measure propagation of AE wave along the composite beams. The acquired AE waveform is digitized and processed. Signal strength, signal energy, cross-correlation of AE waveforms, and tracking of specific cycle of AE waveforms are used to detect delamination size and location.

Evaluation of the split cantilever beam for Mode 3 delamination testing

NASA Technical Reports Server (NTRS)

Martin, Roderick H.

1989-01-01

A test rig for testing a thick split cantilever beam for scissoring delamination (mode 3) fracture toughness was developed. A 3-D finite element analysis was conducted on the test specimen to determine the strain energy release rate, G, distribution along the delamination front. The virtual crack closure technique was used to calculate the G components resulting from interlaminar tension, GI, interlaminar sliding shear, GII, and interlaminar tearing shear, GIII. The finite element analysis showed that at the delamination front no GI component existed, but a GII component was present in addition to a GIII component. Furthermore, near the free edges, the GII component was significantly higher than the GIII component. The GII/GIII ratio was found to increase with delamination length but was insensitive to the beam depth. The presence of GII at the delamination front was verified experimentally by examination of the failure surfaces. At the center of the beam, where the failure was in mode 3, there was significant fiber bridging. However, at the edges of the beam where the failure was in mode 3, there was no fiber bridging and mode 2 shear hackles were observed. Therefore, it was concluded that the split cantilever beam configuration does not represent a pure mode 3 test. The experimental work showed that the mode 2 fracture toughness, GIIc, must be less than the mode 3 fracture toughness, GIIIc. Therefore, a conservative approach to characterizing mode 3 delamination is to equate GIIIc to GIIc.

Early growth, dominance acquisition and lifetime reproductive success in male and female cooperative meerkats

PubMed Central

English, Sinead; Huchard, Elise; Nielsen, Johanna F; Clutton-Brock, Tim H

2013-01-01

In polygynous species, variance in reproductive success is higher in males than females. There is consequently stronger selection for competitive traits in males and early growth can have a greater influence on later fitness in males than in females. As yet, little is known about sex differences in the effect of early growth on subsequent breeding success in species where variance in reproductive success is higher in females than males, and competitive traits are under stronger selection in females. Greater variance in reproductive success has been documented in several singular cooperative breeders. Here, we investigated consequences of early growth for later reproductive success in wild meerkats. We found that, despite the absence of dimorphism, females who exhibited faster growth until nutritional independence were more likely to become dominant, whereas early growth did not affect dominance acquisition in males. Among those individuals who attained dominance, there was no further influence of early growth on dominance tenure or lifetime reproductive success in males or females. These findings suggest that early growth effects on competitive abilities and fitness may reflect the intensity of intrasexual competition even in sexually monomorphic species. PMID:24340181

Monitoring Delamination of Thermal Barrier Coatings by Near-Infrared and Upconversion Luminescence Imaging

NASA Technical Reports Server (NTRS)

Eldridge, J. I.; Martin, R. E.; Singh, Jogender; Wolfe, Doug E.

2008-01-01

Previous work has demonstrated that TBC delamination can be monitored by incorporating a thin luminescent sublayer that produces greatly increased luminescence intensity from delaminated regions of the TBC. Initial efforts utilized visible-wavelength luminescence from either europium or erbium doped sublayers. This approach exhibited good sensitivity to delamination of electron-beam physical-vapor-deposited (EB-PVD) TBCs, but limited sensitivity to delamination of the more highly scattering plasma-sprayed TBCs due to stronger optical scattering and to interference by luminescence from rare-earth impurities. These difficulties have now been overcome by new strategies employing near-infrared (NIR) and upconversion luminescence imaging. NIR luminescence at 1550 nm was produced in an erbium plus ytterbium co-doped yttria-stabilized zirconia (YSZ) luminescent sublayer using 980-nm excitation. Compared to visible-wavelength luminescence, these NIR emission and excitation wavelengths are much more weakly scattered by the TBC and therefore show much improved depth-probing capabilities. In addition, two-photon upconversion luminescence excitation at 980 nm wavelength produces luminescence emission at 562 nm with near-zero fluorescence background and exceptional contrast for delamination indication. The ability to detect TBC delamination produced by Rockwell indentation and by furnace cycling is demonstrated for both EB-PVD and plasma-sprayed TBCs. The relative strengths of the NIR and upconversion luminescence methods for monitoring TBC delamination are discussed.

Local Guided Wavefield Analysis for Characterization of Delaminations in Composites

NASA Technical Reports Server (NTRS)

Rogge, Matthew D.; Campbell Leckey, Cara A.

2012-01-01

Delaminations in composite laminates resulting from impact events may be accompanied by minimal indication of damage at the surface. As such, inspection techniques are required to ensure defects are within allowable limits. Conventional ultrasonic scanning techniques have been shown to effectively characterize the size and depth of delaminations but require physical contact with the structure. Alternatively, a noncontact scanning laser vibrometer may be used to measure guided wave propagation in the laminate structure. A local Fourier domain analysis method is presented for processing guided wavefield data to estimate spatially-dependent wavenumber values, which can be used to determine delamination depth. The technique is applied to simulated wavefields and results are analyzed to determine limitations of the technique with regards to determining defect size and depth. Finally, experimental wavefield data obtained in quasi-isotropic carbon fiber reinforced polymer (CFRP) laminates with impact damage is analyzed and wavenumber is measured to an accuracy of 8.5% in the region of shallow delaminations. Keywords: Ultrasonic wavefield imaging, Windowed Fourier transforms, Guided waves, Structural health monitoring, Nondestructive evaluation

The effects of embedded internal delaminations on composite laminate compression strength; an experimental review

NASA Technical Reports Server (NTRS)

Nettles, Alan T.

1994-01-01

Delaminations in laminated composite materials can degrade the compressive strength of these materials. Delaminations can form as a result of impact damage or processing flaws. In order to better understand the effects of these delaminations on the compressive behavior of laminated composite plates, programs have been conducted to assess the criticality of prescribed delaminations of known size, shape, and location on the compression strength of laminated composites. A review of these programs is presented along with highlights of pertinent findings from each.

Delamination-Indicating Thermal Barrier Coatings

NASA Technical Reports Server (NTRS)

Eldridge, Jeffrey I.

2007-01-01

The risk of premature failure of thermal barrier coatings (TBCs), typically composed of yttria-stabilized zirconia (YSZ), compromises the reliability of TBCs used to provide thermal protection for turbine engine components. Unfortunately, TBC delamination proceeds well beneath the TBC surface and cannot be monitored by visible inspection. Nondestructive diagnostic tools that could reliably probe the subsurface damage state of TBCs would alleviate the risk of TBC premature failure by indicating when the TBC needs to be replaced before the level of TBC damage threatens engine performance or safety. To meet this need, a new coating design for thermal barrier coatings (TBCs) that are self-indicating for delamination has been successfully implemented by incorporating a europium-doped luminescent sublayer at the base of a TBC composed of YSZ. The luminescent sublayer has the same YSZ composition as the rest of the TBC except for the addition of low-level europium doping and therefore does not alter TBC performance.

Large-scale delamination of multi-layers transition metal carbides and carbonitrides “MXenes”

DOE PAGES

Naguib, Michael; Unocic, Raymond R.; Armstrong, Beth L.; ...

2015-04-17

Herein we report on a general approach to delaminate multi-layered MXenes using an organic base to induce swelling that in turn weakens the bonds between the MX layers. Simple agitation or mild sonication of the swollen MXene in water resulted in the large-scale delamination of the MXene layers. The delamination method is demonstrated for vanadium carbide, and titanium carbonitrides MXenes.

Delamination Analysis of a Multilayered Two-Dimensional Functionally Graded Cantilever Beam

NASA Astrophysics Data System (ADS)

Rizov, V.

2017-11-01

Delamination fracture behaviour of a multilayered two-dimensional functionally graded cantilever beam is analyzed in terms of the strain energy release rate. The beam is made of an arbitrary number of layers. Perfect adhesion is assumed between layers. Each layer has individual thickness and material properties. Besides, the material is two-dimensional functionally graded in the cross-section of each layer. There is a delamination crack located arbitrary between layers. The beam is loaded by a bending moment applied at the free end of the lower crack arm. The upper crack arm is free of stresses. The solution to strain energy release rate derived is applied to investigate the influence of the crack location and the material gradient on the delamination fracture. The results obtained can be used to optimize the multilayered two-dimensional functionally graded beam structure with respect to the delamination fracture behaviour.

Multi-frequency local wavenumber analysis and ply correlation of delamination damage.

PubMed

Juarez, Peter D; Leckey, Cara A C

2015-09-01

Wavenumber domain analysis through use of scanning laser Doppler vibrometry has been shown to be effective for non-contact inspection of damage in composites. Qualitative and semi-quantitative local wavenumber analysis of realistic delamination damage and quantitative analysis of idealized damage scenarios (Teflon inserts) have been performed previously in the literature. This paper presents a new methodology based on multi-frequency local wavenumber analysis for quantitative assessment of multi-ply delamination damage in carbon fiber reinforced polymer (CFRP) composite specimens. The methodology is presented and applied to a real world damage scenario (impact damage in an aerospace CFRP composite). The methodology yields delamination size and also correlates local wavenumber results from multiple excitation frequencies to theoretical dispersion curves in order to robustly determine the delamination ply depth. Results from the wavenumber based technique are validated against a traditional nondestructive evaluation method. Published by Elsevier B.V.

Impact Delamination and Fracture in Aluminum/Acrylic Sandwich Plates

NASA Technical Reports Server (NTRS)

Liaw, Benjamin; Zeichner, Glenn; Liu, Yanxiong; Bowles, Kenneth J. (Technical Monitor)

2000-01-01

Impact-induced delamination and fracture in 6061-T6 aluminum/cast acrylic sandwich plates adhered by epoxy were generated in an instrumented drop-weight impact machine. Although only a small dent was produced on the aluminum side when a hemispherical penetrator tup was dropped onto it from a couple of inches, a large ring of delamination at the interface was observed. The delamination damage was often accompanied by severe shattering in the acrylic substratum. Damage patterns in the acrylic layer include radial and ring cracks and, together with delamination at the interface, may cause peeling-off of acrylic material from the sandwich plate. Theory of stress-wave propagation can be used to explain these damage patterns. The impact tests were conducted at various temperatures. The results also show clearly that temperature effect is very important in impact damage. For pure cast acrylic nil-ductile transition (NDT) occurs between 185-195 F. Excessive impact energy was dissipated into fracture energy when tested at temperature below this range or through plastic deformation when tested at temperature above the NDT temperature. Results from this study will be used as baseline data for studying fiber-metal laminates, such as GLARE and ARALL for advanced aeronautical and astronautical applications.

Magnetic resonance imaging with gadolinium arthrography to assess acetabular cartilage delamination.

PubMed

Zaragoza, Edward; Lattanzio, Pierre-Jean; Beaule, Paul E

2009-01-01

Recent reports have demonstrated magnetic resonance imaging (MRI) as a promising technique in detecting articular cartilage lesions of the hip joint. The purpose of our study was to evaluate the diagnostic performance of MRI with gadolinium arthrography in detecting acetabular cartilage delamination in patients with pre-arthritic hip pain. 46 patients (48 hips) underwent surgical dislocation of the hip. Mean age was 38.8 (range 17-56). There were 26 males and 20 females. All patients had Magnetic Resonance Imaging with gadolinium arthrography (MRA) before undergoing open hip surgery where the acetabular cartilage was inspected. Acetabular cartilage delamination on MRA was seen on sagittal images as a linear intra-articular filling defect of low signal intensity >1mm in thickness on T1 weighted images and surrounded by contrast. On MRA all hips had a labral tear confirmed at surgery. At surgery 30 hips had evidence of acetabular cartilage delamination, 4 hips had ulceration and 14 had no articular cartilage damage. The majority of labral tears and cartilage damage were located in the antero-superior quadrant. The sensitivity and specificity of MRA detection of cartilage delamination confirmed at surgery were 97% and 84%, respectively. The positive and negative predictive values of the MRA finding were 90% and 94%, respectively. The presence of the acetabular cartilage delamination represents an early stage of articular cartilage degeneration. When evaluating a young adult with hip pain, labral tears in association with cartilage delamination should be considered. MRA represents an effective diagnostic tool.

Modeling Quasi-Static and Fatigue-Driven Delamination Migration

NASA Technical Reports Server (NTRS)

De Carvalho, N. V.; Ratcliffe, J. G.; Chen, B. Y.; Pinho, S. T.; Baiz, P. M.; Tay, T. E.

2014-01-01

An approach was proposed and assessed for the high-fidelity modeling of progressive damage and failure in composite materials. It combines the Floating Node Method (FNM) and the Virtual Crack Closure Technique (VCCT) to represent multiple interacting failure mechanisms in a mesh-independent fashion. Delamination, matrix cracking, and migration were captured failure and migration criteria based on fracture mechanics. Quasi-static and fatigue loading were modeled within the same overall framework. The methodology proposed was illustrated by simulating the delamination migration test, showing good agreement with the available experimental data.

Aerogel to simulate delamination and porosity defects in carbon-fiber reinforced polymer composites

NASA Astrophysics Data System (ADS)

Juarez, Peter; Leckey, Cara A. C.

2018-04-01

Representative defect standards are essential for the validation and calibration of new and existing inspection techniques. However, commonly used methods of simulating delaminations in carbon-fiber reinforced polymer (CFRP) composites do not accurately represent the behavior of the real-world defects for several widely-used NDE techniques. For instance, it is common practice to create a delamination standard by inserting Polytetrafluoroethylene (PTFE) in between ply layers. However, PTFE can transmit more ultrasonic energy than actual delaminations, leading to an unrealistic representation of the defect inspection. PTFE can also deform/wrinkle during the curing process and has a thermal effusivity two orders of magnitude higher than air (almost equal to that of a CFRP). It is therefore not effective in simulating a delamination for thermography. Currently there is also no standard practice for producing or representing a known porosity in composites. This paper presents a novel method of creating delamination and porosity standards using aerogel. Insertion of thin sheets of solid aerogel between ply layers during layup is shown to produce air-gap-like delaminations creating realistic ultrasonic and thermographic inspection responses. Furthermore, it is shown that depositing controlled amounts of aerogel powder can represent porosity. Micrograph data verifies the structural integrity of the aerogel through the composite curing process. This paper presents data from multiple NDE methods, including X-ray computed tomography, immersion ultrasound, and flash thermography to the effectiveness of aerogel as a delamination and porosity simulant.

Quantitative Evaluation of Delamination in Composites Using Lamb Waves

NASA Astrophysics Data System (ADS)

Michalcová, L.; Hron, R.

2018-03-01

Ultrasonic guided wave monitoring has become very popular in the area of structural health monitoring (SHM) of aerospace structures. Any possible type of damage must be reliably assessed. The paper deals with delamination length determination in DCB specimens using Lamb waves. An analytical equation based on the velocity dependence on variable thickness is utilized. The group velocity of the fundamental antisymmetric A0 mode rapidly changes in a particular range of the frequency-thickness product. Using the same actuation frequency the propagation velocity is different for delaminated structure. Lamb wave based delamination lengths were compared to the visually determined lengths. The method of the wave velocity determination proved to be essential. More accurate results were achieved by tracking the maximum amplitude of A0 mode than the first signal arrival. These findings are considered as the basis for the damage evaluation of complex structures.

Piecewise delamination of Moroccan lithosphere from beneath the Atlas Mountains

NASA Astrophysics Data System (ADS)

Bezada, M. J.; Humphreys, E. D.; Davila, J. M.; Carbonell, R.; Harnafi, M.; Palomeras, I.; Levander, A.

2014-04-01

The elevation of the intracontinental Atlas Mountains of Morocco and surrounding regions requires a mantle component of buoyancy, and there is consensus that this buoyancy results from an abnormally thin lithosphere. Lithospheric delamination under the Atlas Mountains and thermal erosion caused by upwelling mantle have each been suggested as thinning mechanisms. We use seismic tomography to image the upper mantle of Morocco. Our imaging resolves the location and shape of lithospheric cavities and of delaminated lithosphere ˜400 km beneath the Middle Atlas. We propose discontinuous delamination of an intrinsically unstable Atlas lithosphere, enabled by the presence of anomalously hot mantle, as a mechanism for producing the imaged structures. The Atlas lithosphere was made unstable by a combination of tectonic shortening and eclogite loading during Mesozoic rifting and Cenozoic magmatism. The presence of hot mantle sourced from regional upwellings in northern Africa or the Canary Islands enhanced the instability of this lithosphere. Flow around the retreating Alboran slab focused upwelling mantle under the Middle Atlas, which we infer to be the site of the most recent delamination. The Atlas Mountains of Morocco stand as an example of large-scale lithospheric loss in a mildly contractional orogen.

Edge delamination of composite laminates subject to combined tension and torsional loading

NASA Technical Reports Server (NTRS)

Hooper, Steven J.

1990-01-01

Delamination is a common failure mode of laminated composite materials. Edge delamination is important since it results in reduced stiffness and strength of the laminate. The tension/torsion load condition is of particular significance to the structural integrity of composite helicopter rotor systems. Material coupons can easily be tested under this type of loading in servo-hydraulic tension/torsion test stands using techniques very similar to those used for the Edge Delamination Tensile Test (EDT) delamination specimen. Edge delamination of specimens loaded in tension was successfully analyzed by several investigators using both classical laminate theory and quasi-three dimensional (Q3D) finite element techniques. The former analysis technique can be used to predict the total strain energy release rate, while the latter technique enables the calculation of the mixed-mode strain energy release rates. The Q3D analysis is very efficient since it produces a three-dimensional solution to a two-dimensional domain. A computer program was developed which generates PATRAN commands to generate the finite element model. PATRAN is a pre- and post-processor which is commonly used with a variety of finite element programs such as MCS/NASTRAN. The program creates a sufficiently dense mesh at the delamination crack tips to support a mixed-mode fracture mechanics analysis. The program creates a coarse mesh in those regions where the gradients in the stress field are low (away from the delamination regions). A transition mesh is defined between these regions. This program is capable of generating a mesh for an arbitrarily oriented matrix crack. This program significantly reduces the modeling time required to generate these finite element meshes, thus providing a realistic tool with which to investigate the tension torsion problem.

Monitoring Delamination of Plasma-Sprayed Thermal Barrier Coatings by Reflectance-Enhanced Luminescence

NASA Technical Reports Server (NTRS)

Eldridge, Jeffrey I.; Bencic, Timothy J.

2006-01-01

Highly scattering plasma-sprayed thermal barrier coatings (TBCs) present a challenge for optical diagnostic methods to monitor TBC delamination because scattering attenuates light transmitted through the TBC and usually degrades contrast between attached and delaminated regions of the TBC. This paper presents a new approach where reflectance-enhanced luminescence from a luminescent sublayer incorporated along the bottom of the TBC is used to identify regions of TBC delamination. Because of the higher survival rate of luminescence reflecting off the back surface of a delaminated TBC, the strong scattering exhibited by plasma-sprayed TBCs actually accentuates contrast between attached and delaminated regions by making it more likely that multiple reflections of luminescence off the back surface occur before exiting the top surface of the TBC. A freestanding coating containing sections designed to model an attached or delaminated TBC was prepared by depositing a luminescent Eu-doped or Er-doped yttria-stabilized zirconia (YSZ) luminescent layer below a plasma-sprayed undoped YSZ layer and utilizing a NiCr backing layer to represent an attached substrate. For specimens with a Eu-doped YSZ luminescent sublayer, luminescence intensity maps showed excellent contrast between unbacked and NiCr-backed sections even at a plasma-sprayed overlayer thickness of 300 m. Discernable contrast between unbacked and NiCr-backed sections was not observed for specimens with a Er-doped YSZ luminescent sublayer because luminescence from Er impurities in the undoped YSZ layer overwhelmed luminescence originating form the Er-doped YSZ sublayer.

Delamination detection in smart composite beams using Lamb waves

NASA Astrophysics Data System (ADS)

Ip, Kim-Ho; Mai, Yiu-Wing

2004-06-01

This paper presents a feasibility study on using Lamb waves to detect and locate through-width delamination in fiber-reinforced plastic beams. An active diagnostic system is proposed for clamped-free specimens. It consists of a piezoelectric patch and an accelerometer both mounted near the support. Such a system can locate damage in an absolute sense, that is, a priori knowledge on the response from pristine specimens is not required. The fundamental anti-symmetric Lamb wave mode is chosen as the diagnostic wave. It is generated by applying a voltage in the form of sinusoidal bursts to the piezoelectric patch. The proposed system was applied to locate delaminations in some fabricated Kevlar/epoxy beam specimens. With an appropriate actuating frequency, distortions of waveforms due to boundary reflections can be reduced. Based on their arrival times and the known propagating speed of Lamb waves, the delaminations can be located. The errors associated with the predicted damage positions range from 4.5% to 8.5%.

Using glass-graded zirconia to increase delamination growth resistance in porcelain/zirconia dental structures.

PubMed

Chai, Herzl; Mieleszko, Adam J; Chu, Stephen J; Zhang, Yu

2018-01-01

Porcelain fused to zirconia (PFZ) restorations are widely used in prosthetic dentistry. However, their tendency to delaminate along the P/Z interface remains a practical problem so that assessing and improving the interfacial strength are important design aspects. This work examines the effect of modifying the zirconia veneering surface with an in-house felspathic glass on the interfacial fracture resistance of fused P/Z. Three material systems are studied: porcelain fused to zirconia (control) and porcelain fused to glass-graded zirconia with and without the presence of a glass interlayer. The specimens were loaded in a four-point-bend fixture with the porcelain veneer in tension. The evolution of damage is followed with the aid of a video camera. The interfacial fracture energy G C was determined with the aid of a FEA, taking into account the stress shielding effects due to the presence of adjacent channel cracks. Similarly to a previous study on PFZ specimens, the fracture sequence consisted of unstable growth of channel cracks in the veneer followed by stable cracking along the P/Z interface. However, the value of GC for the graded zirconia was approximately 3 times that of the control zirconia, which is due to the good adhesion between porcelain and the glass network structure on the zirconia surface. Combined with its improved bonding to resin-based cements, increased resistance to surface damage and good esthetic quality, graded zirconia emerges as a viable material concept for dental restorations. Copyright © 2017 The Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.

Simulation of Thermographic Responses of Delaminations in Composites with Quadrupole Method

NASA Technical Reports Server (NTRS)

Winfree, William P.; Zalameda, Joseph N.; Howell, Patricia A.; Cramer, K. Elliott

2016-01-01

The application of the quadrupole method for simulating thermal responses of delaminations in carbon fiber reinforced epoxy composites materials is presented. The method solves for the flux at the interface containing the delamination. From the interface flux, the temperature at the surface is calculated. While the results presented are for single sided measurements, with ash heating, expansion of the technique to arbitrary temporal flux heating or through transmission measurements is simple. The quadrupole method is shown to have two distinct advantages relative to finite element or finite difference techniques. First, it is straight forward to incorporate arbitrary shaped delaminations into the simulation. Second, the quadrupole method enables calculation of the thermal response at only the times of interest. This, combined with a significant reduction in the number of degrees of freedom for the same simulation quality, results in a reduction of the computation time by at least an order of magnitude. Therefore, it is a more viable technique for model based inversion of thermographic data. Results for simulations of delaminations in composites are presented and compared to measurements and finite element method results.

Delaminations in composite plates under transverse static loads - Experimental results

NASA Technical Reports Server (NTRS)

Finn, Scott R.; He, Yi-Fei; Springer, George S.

1992-01-01

Tests were performed measuring the damage initiation loads and the locations, shapes, and sizes of delaminations in Fiberite T300/976 graphite/epoxy, Fiberite IM7/977-2 graphite-toughened epoxy, and ICI APC-2 graphite-PEEK plates subjected to transverse static loads. The data were compared to the results of the Finn-Springer model, and good agreements were found between the measured and calculated delamination lengths and widths.

Inter-dependent apical microtubule and actin dynamics orchestrate centrosome retention and neuronal delamination

PubMed Central

Kasioulis, Ioannis

2017-01-01

Detachment of newborn neurons from the neuroepithelium is required for correct neuronal architecture and functional circuitry. This process, also known as delamination, involves adherens-junction disassembly and acto-myosin-mediated abscission, during which the centrosome is retained while apical/ciliary membranes are shed. Cell-biological mechanisms mediating delamination are, however, poorly understood. Using live-tissue and super-resolution imaging, we uncover a centrosome-nucleated wheel-like microtubule configuration, aligned with the apical actin cable and adherens-junctions within chick and mouse neuroepithelial cells. These microtubules maintain adherens-junctions while actin maintains microtubules, adherens-junctions and apical end-foot dimensions. During neuronal delamination, acto-myosin constriction generates a tunnel-like actin-microtubule configuration through which the centrosome translocates. This movement requires inter-dependent actin and microtubule activity, and we identify drebrin as a potential coordinator of these cytoskeletal dynamics. Furthermore, centrosome compromise revealed that this organelle is required for delamination. These findings identify new cytoskeletal configurations and regulatory relationships that orchestrate neuronal delamination and may inform mechanisms underlying pathological epithelial cell detachment. PMID:29058679

Buckling Analysis of Single and Multi Delamination In Composite Beam Using Finite Element Method

NASA Astrophysics Data System (ADS)

Simanjorang, Hans Charles; Syamsudin, Hendri; Giri Suada, Muhammad

2018-04-01

Delamination is one type of imperfection in structure which found usually in the composite structure. Delamination may exist due to some factors namely in-service condition where the foreign objects hit the composite structure and creates inner defect and poor manufacturing that causes the initial imperfections. Composite structure is susceptible to the compressive loading. Compressive loading leads the instability phenomenon in the composite structure called buckling. The existence of delamination inside of the structure will cause reduction in buckling strength. This paper will explain the effect of delamination location to the buckling strength. The analysis will use the one-dimensional modelling approach using two- dimensional finite element method.

Delaminated Transfer of CVD Graphene

NASA Astrophysics Data System (ADS)

Clavijo, Alexis; Mao, Jinhai; Tilak, Nikhil; Altvater, Michael; Andrei, Eva

Single layer graphene is commonly synthesized by dissociation of a carbonaceous gas at high temperatures in the presence of a metallic catalyst in a process known as Chemical Vapor Deposition or CVD. Although it is possible to achieve high quality graphene by CVD, the standard transfer technique of etching away the metallic catalyst is wasteful and jeopardizes the quality of the graphene film by contamination from etchants. Thus, development of a clean transfer technique and preservation of the parent substrate remain prominent hurdles to overcome. In this study, we employ a copper pretreatment technique and optimized parameters for growth of high quality single layer graphene at atmospheric pressure. We address the transfer challenge by utilizing the adhesive properties between a polymer film and graphene to achieve etchant-free transfer of graphene films from a copper substrate. Based on this concept we developed a technique for dry delamination and transferring of graphene to hexagonal boron nitride substrates, which produced high quality graphene films while at the same time preserving the integrity of the copper catalyst for reuse. DOE-FG02-99ER45742, Ronald E. McNair Postbaccalaureate Achievement Program.

Detection of Delamination in Concrete Bridge Decks Using Mfcc of Acoustic Impact Signals

NASA Astrophysics Data System (ADS)

Zhang, G.; Harichandran, R. S.; Ramuhalli, P.

2010-02-01

Delamination of the concrete cover is a commonly observed damage in concrete bridge decks. The delamination is typically initiated by corrosion of the upper reinforcing bars and promoted by freeze-thaw cycling and traffic loading. The detection of delamination is important for bridge maintenance and acoustic non-destructive evaluation (NDE) is widely used due to its low cost, speed, and easy implementation. In traditional acoustic approaches, the inspector sounds the surface of the deck by impacting it with a hammer or bar, or by dragging a chain, and assesses delamination by the "hollowness" of the sound. The detection of the delamination is subjective and requires extensive training. To improve performance, this paper proposes an objective method for delamination detection. In this method, mel-frequency cepstral coefficients (MFCC) of the signal are extracted. Some MFCC are then selected as features for detection purposes using a mutual information criterion. Finally, the selected features are used to train a classifier which is subsequently used for detection. In this work, a simple quadratic Bayesian classifier is used. Different numbers of features are used to compare the performance of the detection method. The results show that the performance first increases with the number of features, but then decreases after an optimal value. The optimal number of features based on the recorded signals is four, and the mean error rate is only 3.3% when four features are used. Therefore, the proposed algorithm has sufficient accuracy to be used in field detection.

Incorporation of plasma-functionalized carbon nanostructures in composite laminates for interlaminar reinforcement and delamination crack monitoring

NASA Astrophysics Data System (ADS)

Kravchenko, O. G.; Pedrazzoli, D.; Kovtun, D.; Qian, X.; Manas-Zloczower, I.

2018-01-01

A new approach employing carbon nanostructure (CNS) buckypapers (BP) was used to prepare glass fiber/epoxy composite materials with enhanced resistance to delamination along with damage monitoring capability. The CNS-BP was subjected to plasma treatment to improve its wettability by epoxy and to promote stronger interfacial bonding. An increase up to 20% in interlaminar fracture toughness in mode I and mode II was observed in composite laminates incorporating CNS BP. Morphological analysis of the fracture surfaces indicated that failure in the conductive CNS layer provided a more effective energy dissipation mechanism, resulting in interlaminar fracture toughness increase. Moreover, fracture of the conductive CNS layer enabled damage monitoring of the composite by electrical resistance measurements upon delamination. The proposed approach provides multifunctional ply interphases, allowing to couple damage monitoring with interlaminar reinforcement of composite laminates.

Application of the Refined Zigzag Theory to the Modeling of Delaminations in Laminated Composites

NASA Technical Reports Server (NTRS)

Groh, Rainer M. J.; Weaver, Paul M.; Tessler, Alexander

2015-01-01

The Refined Zigzag Theory is applied to the modeling of delaminations in laminated composites. The commonly used cohesive zone approach is adapted for use within a continuum mechanics model, and then used to predict the onset and propagation of delamination in five cross-ply composite beams. The resin-rich area between individual composite plies is modeled explicitly using thin, discrete layers with isotropic material properties. A damage model is applied to these resin-rich layers to enable tracking of delamination propagation. The displacement jump across the damaged interfacial resin layer is captured using the zigzag function of the Refined Zigzag Theory. The overall model predicts the initiation of delamination to within 8% compared to experimental results and the load drop after propagation is represented accurately.

Apical constriction is driven by a pulsatile apical myosin network in delaminating Drosophila neuroblasts.

PubMed

An, Yanru; Xue, Guosheng; Shaobo, Yang; Mingxi, Deng; Zhou, Xiaowei; Yu, Weichuan; Ishibashi, Toyotaka; Zhang, Lei; Yan, Yan

2017-06-15

Cell delamination is a conserved morphogenetic process important for the generation of cell diversity and maintenance of tissue homeostasis. Here, we used Drosophila embryonic neuroblasts as a model to study the apical constriction process during cell delamination. We observe dynamic myosin signals both around the cell adherens junctions and underneath the cell apical surface in the neuroectoderm. On the cell apical cortex, the nonjunctional myosin forms flows and pulses, which are termed medial myosin pulses. Quantitative differences in medial myosin pulse intensity and frequency are crucial to distinguish delaminating neuroblasts from their neighbors. Inhibition of medial myosin pulses blocks delamination. The fate of a neuroblast is set apart from that of its neighbors by Notch signaling-mediated lateral inhibition. When we inhibit Notch signaling activity in the embryo, we observe that small clusters of cells undergo apical constriction and display an abnormal apical myosin pattern. Together, these results demonstrate that a contractile actomyosin network across the apical cell surface is organized to drive apical constriction in delaminating neuroblasts. © 2017. Published by The Company of Biologists Ltd.

Numerical investigation of nonlinear interactions between multimodal guided waves and delamination in composite structures

NASA Astrophysics Data System (ADS)

Shen, Yanfeng

2017-04-01

This paper presents a numerical investigation of the nonlinear interactions between multimodal guided waves and delamination in composite structures. The elastodynamic wave equations for anisotropic composite laminate were formulated using an explicit Local Interaction Simulation Approach (LISA). The contact dynamics was modeled using the penalty method. In order to capture the stick-slip contact motion, a Coulomb friction law was integrated into the computation procedure. A random gap function was defined for the contact pairs to model distributed initial closures or openings to approximate the nature of rough delamination interfaces. The LISA procedure was coded using the Compute Unified Device Architecture (CUDA), which enables the highly parallelized computation on powerful graphic cards. Several guided wave modes centered at various frequencies were investigated as the incident wave. Numerical case studies of different delamination locations across the thickness were carried out. The capability of different wave modes at various frequencies to trigger the Contact Acoustic Nonlinearity (CAN) was studied. The correlation between the delamination size and the signal nonlinearity was also investigated. Furthermore, the influence from the roughness of the delamination interfaces was discussed as well. The numerical investigation shows that the nonlinear features of wave delamination interactions can enhance the evaluation capability of guided wave Structural Health Monitoring (SHM) system. This paper finishes with discussion, concluding remarks, and suggestions for future work.

Simulation of Delamination-Migration and Core Crushing in a CFRP Sandwich Structure

NASA Technical Reports Server (NTRS)

McElroy, M.; Leone, F.; Ratcliffe, J.; Czabaj, M.; Yuan, F. G.

2015-01-01

Following the onset of damage caused by an impact load on a composite laminate structure, delaminations often form propagating outwards from the point of impact and in some cases can migrate via matrix cracks between plies as they grow. The goal of the present study is to develop an accurate finite element modeling technique for simulation of the delamination-migration phenomena in laminate impact damage processes. An experiment was devised where, under a quasi-static indentation load, an embedded delamination in the facesheet of a laminate sandwich specimen migrates via a transverse matrix crack and then continues to grow on a new ply interface. The quasistatic nature of the indentation results in structural behavior equivalent to that seen in low-velocity impact and also allows for highly detailed real time damage characterization. Several finite element damage simulation methods were investigated. Comparing the experimental results with those of the different models reveals certain modeling features that are important to include in a numerical simulation of delamination-migration and some that may be neglected.

An analytical and experimental investigation of edge delamination in laminates subjected to tension, bending, and torsion

NASA Technical Reports Server (NTRS)

Chan, Wen S.

1989-01-01

An integrated two-dimensional finite element was developed to calculate interlaminar stresses and strain energy release rates for the study of delamination in composite laminates subjected to uniaxial tension, bending, and torsion loads. Addressed are the formulation, implementation, and verification of the model. Parametric studies were conducted on the effect of Poisson's ratio mismatch between plies and the stacking sequence on interlaminar stress, and on the effect of delamination opening height and delamination length, due to bending, on strain energy release rate for various laminates. A comparison of strain energy release rates in all-graphite and graphite/glass hybrid laminates is included. The preliminary results of laminates subjected to torsion are also included. Fatigue tension tests were conducted on Mode 1 and mixed mode edge-delamination coupons to establish the relationship between fatigue load vs. onset of delamination cycle. The effect on the fatigue delamination onset of different frequencies (1 and 5 Hz) was investigated for glass, graphite,and their hybrid laminates. Although a 20 percent increase in the static onset-of-delamination strength and a 10 percent increase in ultimate strength resulted from hybridizing the all-graphite laminate with a 90 deg glass ply, the fatigue onset is lower in the hybrid laminate than in the all-graphite laminate.

Growth and metabolic response of premature infants fed whey- or casein-dominant formulas after hospital discharge.

PubMed

Bernbaum, J C; Sasanow, S R; Churella, H R; Daft, A

1989-10-01

We conducted a double-blind, randomized study to test the hypothesis that a whey-dominant formula permits a growth and metabolic advantage over a casein-dominant formula in preterm infants after hospital discharge. Nineteen low birth weight infants were studied for 6 months from the time of discharge. Ten received a casein-dominant formula, and nine received a whey-dominant formula. Growth (weight, length, head circumference, mid-arm circumference, and skin-fold thickness), biochemical measurements (alkaline phosphatase activity, acid-base status, and hemoglobin, serum total protein, albumin, and urea nitrogen levels), and quantity of formula intake did not differ significantly between the groups over a 6-month study period. Serum transthyretin and urea nitrogen concentrations differed significantly between the two feeding groups at the day of entry into the study only. The results indicate that, after hospital discharge, premature infants fed a whey-dominant formula do not differ in growth or biochemical measurements from those fed a casein-dominant formula.

A Mixed-Mode (I-II) Fracture Criterion for AS4/8552 Carbon/Epoxy Composite Laminate

NASA Astrophysics Data System (ADS)

Karnati, Sidharth Reddy

A majority of aerospace structures are subjected to bending and stretching loads that introduce peel and shear stresses between the plies of a composite laminate. These two stress components cause a combination of mode I and II fracture modes in the matrix layer of the composite laminate. The most common failure mode in laminated composites is delamination that affects the structural integrity of composite structures. Damage tolerant designs of structures require two types of materials data: mixed-mode (I-II) delamination fracture toughness that predicts failure and delamination growth rate that predicts the life of the structural component. This research focuses determining mixed-mode (I-II) fracture toughness under a combination of mode I and mode II stress states and then a fracture criterion for AS4/8552 composite laminate, which is widely used in general aviation. The AS4/8552 prepreg was supplied by Hexcel Corporation and autoclave fabricated into a 20-ply unidirectional laminate with an artificial delamination by a Fluorinated Ethylene Propylene (FEP) film at the mid-plane. Standard split beam specimens were prepared and tested in double cantilever beam (DCB) and end notched flexure modes to determine mode I (GIC) and II (GIIC) fracture toughnesses, respectively. The DCB specimens were also tested in a modified mixed-mode bending apparatus at GIIm /GT ratios of 0.18, 0.37, 0.57 and 0.78, where GT is total and GIIm is the mode II component of energy release rates. The measured fracture toughness, GC, was found to follow the locus a power law equation. The equation was validated for the present and literature experimental data.

Effect of Assumed Damage and Location on the Delamination Onset Predictions for Skin-Stiffener Debonding

NASA Technical Reports Server (NTRS)

Paris, Isabelle L.; Krueger, Ronald; OBrien, T. Kevin

2004-01-01

The difference in delamination onset predictions based on the type and location of the assumed initial damage are compared in a specimen consisting of a tapered flange laminate bonded to a skin laminate. From previous experimental work, the damage was identified to consist of a matrix crack in the top skin layer followed by a delamination between the top and second skin layer (+45 deg./-45 deg. interface). Two-dimensional finite elements analyses were performed for three different assumed flaws and the results show a considerable reduction in critical load if an initial delamination is assumed to be present, both under tension and bending loads. For a crack length corresponding to the peak in the strain energy release rate, the delamination onset load for an assumed initial flaw in the bondline is slightly higher than the critical load for delamination onset from an assumed skin matrix crack, both under tension and bending loads. As a result, assuming an initial flaw in the bondline is simpler while providing a critical load relatively close to the real case. For the configuration studied, a small delamination might form at a lower tension load than the critical load calculated for a 12.7 mm (0.5") delamination, but it would grow in a stable manner. For the bending case, assuming an initial flaw of 12.7 mm (0.5") is conservative, the crack would grow unstably.

Contrasting growth responses of dominant peatland plants to warming and vegetation composition.

PubMed

Walker, Tom N; Ward, Susan E; Ostle, Nicholas J; Bardgett, Richard D

2015-05-01

There is growing recognition that changes in vegetation composition can strongly influence peatland carbon cycling, with potential feedbacks to future climate. Nevertheless, despite accelerated climate and vegetation change in this ecosystem, the growth responses of peatland plant species to combined warming and vegetation change are unknown. Here, we used a field warming and vegetation removal experiment to test the hypothesis that dominant species from the three plant functional types present (dwarf-shrubs: Calluna vulgaris; graminoids: Eriophorum vaginatum; bryophytes: Sphagnum capillifolium) contrast in their growth responses to warming and the presence or absence of other plant functional types. Warming was accomplished using open top chambers, which raised air temperature by approximately 0.35 °C, and we measured air and soil microclimate as potential mechanisms through which both experimental factors could influence growth. We found that only Calluna growth increased with experimental warming (by 20%), whereas the presence of dwarf-shrubs and bryophytes increased growth of Sphagnum (46%) and Eriophorum (20%), respectively. Sphagnum growth was also negatively related to soil temperature, which was lower when dwarf-shrubs were present. Dwarf-shrubs may therefore promote Sphagnum growth by cooling the peat surface. Conversely, the effect of bryophyte presence on Eriophorum growth was not related to any change in microclimate, suggesting other factors play a role. In conclusion, our findings reveal contrasting abiotic and biotic controls over dominant peatland plant growth, suggesting that community composition and carbon cycling could be modified by simultaneous climate and vegetation change.

The macroscopic delamination of thin films from elastic substrates

PubMed Central

Vella, Dominic; Bico, José; Boudaoud, Arezki; Roman, Benoit; Reis, Pedro M.

2009-01-01

The wrinkling and delamination of stiff thin films adhered to a polymer substrate have important applications in “flexible electronics.” The resulting periodic structures, when used for circuitry, have remarkable mechanical properties because stretching or twisting of the substrate is mostly accommodated through bending of the film, which minimizes fatigue or fracture. To date, applications in this context have used substrate patterning to create an anisotropic substrate-film adhesion energy, thereby producing a controlled array of delamination “blisters.” However, even in the absence of such patterning, blisters appear spontaneously, with a characteristic size. Here, we perform well-controlled experiments at macroscopic scales to study what sets the dimensions of these blisters in terms of the material properties and explain our results by using a combination of scaling and analytical methods. Besides pointing to a method for determining the interfacial toughness, our analysis suggests a number of design guidelines for the thin films used in flexible electronic applications. Crucially, we show that, to avoid the possibility that delamination may cause fatigue damage, the thin film thickness must be greater than a critical value, which we determine. PMID:19556551

Open-mode delamination stress concentrations in horseshoe and elliptic composite curved bars subjected to end forces

NASA Technical Reports Server (NTRS)

Ko, William L.; Jackson, Raymond H.

1990-01-01

The multilayer theory of anisotropic elasticity and a finite element method were used to analyze the open-mode delamination stress concentrations in horseshoe and elliptic laminated composite curved bars. Two types of laminations, solid laminations and sandwich laminations, were analyzed. It was found that the open-mode delamination stress concentration could be greatly increased in these two types of curved bars by decreasing their aspect ratios. The open-mode delamination stress concentration generated in the solid laminations was found to be far more severe than that generated in the sandwich laminations. The horseshoe curved bar may be used to determine both the open-mode delamination strength of solidly laminated composites and the open-mode debonding strength of sandwiched laminated composites. However, the elliptic curved bar is only good for determining the open-mode delamination strength of solidly laminated composites.

Fiber Optic Thermal Detection of Composite Delaminations

NASA Technical Reports Server (NTRS)

Wu, Meng-Chou; Winfree, William P.

2011-01-01

A recently developed technique is presented for thermographic detection of delaminations in composites by performing temperature measurements with fiber optic Bragg gratings. A single optical fiber with multiple Bragg gratings employed as surface temperature sensors was bonded to the surface of a composite with subsurface defects. The investigated structure was a 10-ply composite specimen with prefabricated delaminations of various sizes and depths. Both during and following the application of a thermal heat flux to the surface, the individual Bragg grating sensors measured the temporal and spatial temperature variations. The data obtained from grating sensors were analyzed with thermal modeling techniques of conventional thermography to reveal particular characteristics of the interested areas. Results were compared and found to be consistent with the calculations using numerical simulation techniques. Also discussed are methods including various heating sources and patterns, and their limitations for performing in-situ structural health monitoring.

A grain boundary damage model for delamination

NASA Astrophysics Data System (ADS)

Messner, M. C.; Beaudoin, A. J.; Dodds, R. H.

2015-07-01

Intergranular failure in metallic materials represents a multiscale damage mechanism: some feature of the material microstructure triggers the separation of grain boundaries on the microscale, but the intergranular fractures develop into long cracks on the macroscale. This work develops a multiscale model of grain boundary damage for modeling intergranular delamination—a failure of one particular family of grain boundaries sharing a common normal direction. The key feature of the model is a physically-consistent and mesh independent, multiscale scheme that homogenizes damage at many grain boundaries on the microscale into a single damage parameter on the macroscale to characterize material failure across a plane. The specific application of the damage framework developed here considers delamination failure in modern Al-Li alloys. However, the framework may be readily applied to other metals or composites and to other non-delamination interface geometries—for example, multiple populations of material interfaces with different geometric characteristics.

Mixed-Mode Decohesion Elements for Analyses of Progressive Delamination

NASA Technical Reports Server (NTRS)

Davila, Carlos G.; Camanho, Pedro P.; deMoura, Marcelo F.

2001-01-01

A new 8-node decohesion element with mixed mode capability is proposed and demonstrated. The element is used at the interface between solid finite elements to model the initiation and propagation of delamination. A single displacement-based damage parameter is used in a strain softening law to track the damage state of the interface. The method can be used in conjunction with conventional material degradation procedures to account for inplane and intra-laminar damage modes. The accuracy of the predictions is evaluated in single mode delamination tests, in the mixed-mode bending test, and in a structural configuration consisting of the debonding of a stiffener flange from its skin.

A new method for evaluating forest thinning: growth dominance in managed Pinus resinosa stands

Treesearch

John B. Bradford; Anthony W. D' Amato; Brian J. Palik; Shawn Fraver

2010-01-01

Growth dominance is a relatively new, simple, quantitative metric of within-stand individual tree growth patterns, and is defined as positive when larger trees in the stand display proportionally greater growth than smaller trees, and negative when smaller trees display proportionally greater growth than larger trees. We examined long-term silvicultural experiments in...

Effects of different excitation waveforms on detection and characterisation of delamination in PV modules by active infrared thermography

NASA Astrophysics Data System (ADS)

Sinha, Archana; Gupta, Rajesh

2017-10-01

Delamination significantly affects the performance and reliability of photovoltaic (PV) modules. Recently, an active infrared thermography approach using step heating has been exploited for the detection and characterisation of delamination in PV modules. However, step heating takes longer observation time and causes overheating problems. This paper presents the effects of different thermal excitation waveforms namely rectangular, half-sine and short pulse, on the detection and characterisation of delamination in PV module by experiments and simulations. For simulation, a 3-dimensional electro-thermal model of heat conduction, based on resistance-capacitance network approach, has been exploited to study the variation in maximum thermal contrast and peak contrast time with the delamination thickness and heating parameters. Results show that the rectangular waveform provides better detection of delamination due to higher absolute contrast, while the half-sine waveform allows better characterisation of delamination in the PV modules with low-cost and low-power heat source. The high-energy short pulse enabled quick visualisation of delamination, but has limited practical implementation. The advantages and limitations of each waveform have been highlighted to assess the specific requirement for appropriate choice in the non-destructive thermographic inspection of delamination in PV modules at the manufacturing units or outdoor fields.

A non-cell-autonomous role for Ras signaling in C. elegans neuroblast delamination

PubMed Central

Parry, Jean M.; Sundaram, Meera V.

2014-01-01

Receptor tyrosine kinase (RTK) signaling through Ras influences many aspects of normal cell behavior, including epithelial-to-mesenchymal transition, and aberrant signaling promotes both tumorigenesis and metastasis. Although many such effects are cell-autonomous, here we show a non-cell-autonomous role for RTK-Ras signaling in the delamination of a neuroblast from an epithelial organ. The C. elegans renal-like excretory organ is initially composed of three unicellular epithelial tubes, namely the canal, duct and G1 pore cells; however, the G1 cell later delaminates from the excretory system to become a neuroblast and is replaced by the G2 cell. G1 delamination and G2 intercalation involve cytoskeletal remodeling, interconversion of autocellular and intercellular junctions and migration over a luminal extracellular matrix, followed by G1 junction loss. LET-23/EGFR and SOS-1, an exchange factor for Ras, are required for G1 junction loss but not for initial cytoskeletal or junction remodeling. Surprisingly, expression of activated LET-60/Ras in the neighboring duct cell, but not in the G1 or G2 cells, is sufficient to rescue sos-1 delamination defects, revealing that Ras acts non-cell-autonomously to permit G1 delamination. We suggest that, similarly, oncogenic mutations in cells within a tumor might help create a microenvironment that is permissive for other cells to detach and ultimately metastasize. PMID:25371363

Detection of delamination defects in CFRP materials using ultrasonic signal processing.

PubMed

Benammar, Abdessalem; Drai, Redouane; Guessoum, Abderrezak

2008-12-01

In this paper, signal processing techniques are tested for their ability to resolve echoes associated with delaminations in carbon fiber-reinforced polymer multi-layered composite materials (CFRP) detected by ultrasonic methods. These methods include split spectrum processing (SSP) and the expectation-maximization (EM) algorithm. A simulation study on defect detection was performed, and results were validated experimentally on CFRP with and without delamination defects taken from aircraft. Comparison of the methods for their ability to resolve echoes are made.

Characterization of the Edge Crack Torsion (ECT) Test for Mode III Fracture Toughness Measurement of Laminated Composites

NASA Technical Reports Server (NTRS)

Ratcliffe, James G.

2004-01-01

The edge crack torsion (ECT) test is designed to initiate mode III delamination growth in composite laminates. An ECT specimen is a rectangular laminate, containing an edge delamination at the laminate mid-plane. Torsion load is applied to the specimens, resulting in relative transverse shear sliding of the delaminated faces. The test data reduction schemes are intended to yield initiation values of critical mode III strain energy release rate, G(sub IIIc), that are constant with delamination length. The test has undergone several design changes during its development. The objective of this paper was to determine the suitability of the current ECT test design as a mode III fracture test. To this end, ECT tests were conducted on specimens manufactured from IM7/8552 and specimens made from S2/8552 tape laminates. Several specimens, each with different delamination lengths are tested. Detailed, three-dimensional finite element analyses of the specimens were performed. The analysis results were used to calculate the distribution of mode I, mode II, and mode III strain energy release rate along the delamination front. The results indicated that mode III-dominated delamination growth would be initiated from the specimen center. However, in specimens of both material types, the measured values of G(sub IIIc) exhibited significant dependence on delamination length. Furthermore, there was a large amount of scatter in the data. Load-displacement response of the specimens exhibited significant deviation from linearity before specimen failure. X-radiographs of a sample of specimens revealed that damage was initiated in the specimens prior to failure. Further inspection of the failure surfaces is required to identify the damage and determine that mode III delamination is initiated in the specimens.

Strain-energy release rate analysis of a laminate with a postbuckled delamination

NASA Technical Reports Server (NTRS)

Whitcomb, John D.; Shivakumar, K. N.

1987-01-01

The objectives are to present the derivation of the new virtual crack closure technique, evaluate the accuracy of the technique, and finally to present the results of a limited parametric study of laminates with a postbuckled delamination. Although the new virtual crack closure technique is general, only homogeneous, isotropic laminates were analyzed. This was to eliminate the variation of flexural stiffness with orientation, which occurs even for quasi-isotropic laminates. This made it easier to identify the effect of geometrical parameters on G. The new virtual crack closure technique is derived. Then the specimen configurations are described. Next, the stress analyses is discussed. Finally, the virtual crack closure technique is evaluated and then used to calculate the distribution of G along the delamination front of several laminates with a postbuckled delamination.

Mechanism of Electrochemical Delamination of Two-Dimensional Materials from Their Native Substrates by Bubbling.

PubMed

Sun, Jie; Fan, Xing; Guo, Weiling; Liu, Lihui; Liu, Xin; Deng, Jun; Xu, Chen

2015-12-16

A capacitor-based circuit model is proposed to explain the electrochemical delamination of two-dimensional materials from their native substrates where produced gas bubbles squeeze into the interface. The delamination is actually the electric breakdown of the capacitor formed between the solution and substrate. To facilitate the procedure, the backside of the ubstrate has to be shielded so that the capacitor breakdown voltage can be reached. The screening effect can be induced either by nonreactive ions around the electrode or, more effectively, by an undetachable insulator. This mechanism serves as a guideline for the surface science and applications involving the bubbling delamination.

Fracture mechanics of matrix cracking and delamination in glass/epoxy laminates

NASA Technical Reports Server (NTRS)

Caslini, M.; Zanotti, C.; Obrien, T. K.

1986-01-01

This study focused on characterizing matrix cracking and delamination behavior in multidirectional laminates. Static tension and tension-tension fatigue tests were conducted on two different layups. Damage onset, accumulation, and residual properties were measured. Matrix cracking was shown to have a considerable influence on residual stiffness of glass epoxy laminates, and could be predicted reasonably well for cracks in 90 deg piles using a simple shear lag analysis. A fracture mechanics analysis for the strain energy release rate associated with 90 deg ply-matrix crack formation was developed and was shown to correlate the onset of 90 deg ply cracks in different laminates. The linear degradation of laminate modulus with delamination area, previously observed for graphite epoxy laminates, was predicted for glass epoxy laminates using a simple rule of mixtures analysis. The strain energy release rate associated with edge delamination formation under static and cyclic loading was difficult to analyze because of the presence of several contemporary damage phenomena.

Using guided ultrasonic wave inspection to quantify the length of delaminations in composite laminates

NASA Astrophysics Data System (ADS)

Feng, Bo; Ribeiro, Artur Lopes; Ramos, Helena Geirinhas

2018-04-01

This paper presents a study of the characteristics of Lamb wave (S0 mode) testing signals in carbon fiber composite laminates containing delaminations. The study was implemented by using commercial finite element simulation software - ANSYS. The delamination signal is proven to be the superposition of the two waves travelling from upper and lower sub-laminates. Dispersion curves for the two sub-laminates were calculated to show the difference between phase velocities of the waves in the sub-laminates. Two models are specifically designed to get the phase difference between the waves that travel in each of the two sub-laminates. From the simulation results, it was found that the phase difference increases with the delamination length. Furthermore, the amplitude of delamination signal decreases first, then it starts to increase after reaching the minimum value. The minimum is reached when the waves from the two sub-laminates are 180° out of phase.

Detecting Thermal Barrier Coating Delamination Using Visible and Near-Infrared Luminescence from Erbium-Doped Sublayers

NASA Technical Reports Server (NTRS)

Eldridge, J. I.; Bencic, T. J.; Martin, R. E.; Singh, J.; Wolfe, D. E.

2007-01-01

Nondestructive diagnostic tools are needed to monitor early stages of delamination progression in thermal barrier coatings (TBCs) because the risk of delamination induced coating failure will compromise engine performance and safety. Previous work has demonstrated that for TBCs composed of yttria-stabilized zirconia (YSZ), luminescence from a buried europium-doped sublayer can be utilized to identify the location of TBC delamination from the substantially higher luminescence intensity observed from the delaminated regions of the TBC. Luminescence measurements from buried europium-doped layers depend on sufficient transmittance of the 532 nm excitation and 606 nm emission wavelengths through the attenuating undoped YSZ overlayer to produce easily detected luminescence. In the present work, improved delamination indication is demonstrated using erbium-doped YSZ sublayers. For visible-wavelength luminescence, the erbium-doped sublayer offers the advantage of a very strong excitation peak at 517 nm that can be conveniently excited a 514 nm Ar ion laser. More importantly, the erbium-doped sublayer also produces near-infrared luminescence at 1550 nm that is effectively excited by a 980 nm laser diode. Both the 980 nm excitation and the 1550 nm emission are transmitted through the TBC with much less attenuation than visible wavelengths and therefore show great promise for delamination monitoring through thicker or more highly scattering TBCs. The application of this approach for both electron beam physical vapor deposited (EB-PVD) and plasma-sprayed TBCs is discussed.

Numerical models of delamination behavior in 2G HTS tapes under transverse tension and peel

NASA Astrophysics Data System (ADS)

Duan, Yujie; Ta, Wurui; Gao, Yuanwen

2018-02-01

In extreme operating environments, delamination in 2G HTS tapes occurs within and/or near the superconductor layer from high transverse tensile stresses caused by fabrication, Lorentz forces and thermal mismatch, etc. Generally, transverse opening and peeling off are the main delamination modes, and are always studied in anvil and peel tests, respectively. Numerical models of these modes for 2G HTS tape are presented wherein the mixed-mode traction-separation law at the interface of the silver and superconductor layers is considered. Plastic deformations of copper, silver, and Hastelloy® in the HTS tape are taken into account. The results obtained from the transverse opening model show that the maximum average tensile stress is smaller than the delamination tensile strength because delamination is asynchronous in the tape. When a crack appears in the tape, only a small stress ( ≤ 1 MPa) is required to expand the crack to other stress free areas through peeling. Using the peeling model, the dependency of the peel strength on peeling angle is investigated under constant fracture toughness. Peel strength decreases with the peeling angle until the minimum value is reached at 150°, and thereafter increases slightly. Other results indicate that peel strength depends strongly on delamination strength, fracture toughness, and thickness of copper layer. The fracture toughness of the delamination interface, which is difficult to obtain by experiment, can be extracted using the present model.

Peeling back the lithosphere: Controlling parameters, surface expressions and the future directions in delamination modeling

NASA Astrophysics Data System (ADS)

Göğüş, Oğuz H.; Ueda, Kosuke

2018-06-01

Geodynamical models investigate the rheological and physical properties of the lithosphere that peels back (delaminates) from the upper-middle crust. Meanwhile, model predictions are used to relate to a set of observations in the geological context to the test the validity of delamination. Here, we review numerical and analogue models of delamination from these perspectives and provide a number of first-order topics which future modeling studies may address. Models suggest that the presence of the weak lower crust that resides between the strong mantle lithosphere (at least 100 times more viscous/stronger) and the strong upper crust is necessary to develop delamination. Lower crustal weakening may be induced by melt infiltration, shear heating or it naturally occurs through the jelly sandwich type strength profile of the continental lithosphere. The negative buoyancy of the lithosphere required to facilitate the delamination is induced by the pre-existing ocean subduction and/or the lower crustal eclogitization. Surface expression of the peeling back lithosphere has a distinct transient and migratory imprint on the crust, resulting in rapid surface uplift/subsidence, magmatism, heating and shortening/extension. New generation of geodynamical experiments can explain how different types of melting (e.g hydrated, dry melting) occurs with delamination. Reformation of the lithosphere after removal, three dimensional aspects, and the termination of the process are key investigation areas for future research. The robust model predictions, as with other geodynamic modeling studies should be reconciled with observations.

Piecewise Delamination Drives Uplift in the Atlas Mountains Region of Morocco

NASA Astrophysics Data System (ADS)

Bezada, M. J.; Humphreys, E.; Martin Davila, J.; mimoun, H.; Josep, G.; Palomeras, I.

2013-12-01

The elevation of the intra-continental Atlas Mountains of Morocco and surrounding regions requires a mantle component of buoyancy, and there is consensus that this buoyancy results from an abnormally thin lithosphere. Lithospheric delamination under the Atlas Mountains and thermal erosion caused by upwelling mantle have each been suggested as thinning mechanisms. We use seismic tomography to image the upper mantle of Morocco by inverting teleseimic p-wave delay times, complemented with local delays, recorded on a dense array of stations in the Iberian peninsula and Morocco. A surface wave model provides constraint on the shallower layers. We determine the geometry of lithospheric cavities and mantle upwelling beneath the Middle Atlas and central High Atlas, and image delaminated lithosphere at ~400 km beneath the Middle Atlas. We propose discontinuous delamination of an intrinsically unstable Atlas lithosphere, enabled by the presence of anomalously hot mantle, as a mechanism for producing the imaged structures. The Atlas lithosphere was made unstable by a combination of tectonic shortening and eclogite loading during Mesozoic rifting and Cenozoic magmatism. The presence of hot mantle, sourced from regional upwellings in northern Africa or the Canary Islands, enabled the mobilization of this lithosphere. Flow around the retreating Alboran slab focused upwelling mantle under the Middle Atlas, where we image the most recent delamination. The Atlas Mountains of Morocco stand as an example of mantle-generated uplift and large-scale lithospheric loss in a mildly contractional orogen.

Mechanism of Electrochemical Delamination of Two-Dimensional Materials from Their Native Substrates by Bubbling

PubMed Central

Sun, Jie; Fan, Xing; Guo, Weiling; Liu, Lihui; Liu, Xin; Deng, Jun; Xu, Chen

2015-01-01

A capacitor-based circuit model is proposed to explain the electrochemical delamination of two-dimensional materials from their native substrates where produced gas bubbles squeeze into the interface. The delamination is actually the electric breakdown of the capacitor formed between the solution and substrate. To facilitate the procedure, the backside of the ubstrate has to be shielded so that the capacitor breakdown voltage can be reached. The screening effect can be induced either by nonreactive ions around the electrode or, more effectively, by an undetachable insulator. This mechanism serves as a guideline for the surface science and applications involving the bubbling delamination. PMID:26694406

Desorption to Delamination: Dynamics of Detachment in a Colloidal Thin Film

NASA Astrophysics Data System (ADS)

Varshney, Atul; Sharma, P.; Sane, A.; Ghosh, S.; Bhattacharya, S.

2010-10-01

Colloidal thin films of varying rigidity detaching from a substrate under an electric field induced stress are studied by video microscopy. For soft films, the process of detachment shows single-particle dynamics, analogous to desorption. For rigid films, a collective delamination spanning hundreds of particles occurs. A competition among the rigidity of the film, the interaction with the substrate, and the external stress leads to a correlation length over which the film delaminates at a critical stress. The phenomenon is described as a dynamical transition in a disordered elastic medium.

Progressive delamination in polymer matrix composite laminates: A new approach

NASA Technical Reports Server (NTRS)

Chamis, C. C.; Murthy, P. L. N.; Minnetyan, L.

1992-01-01

A new approach independent of stress intensity factors and fracture toughness parameters has been developed and is described for the computational simulation of progressive delamination in polymer matrix composite laminates. The damage stages are quantified based on physics via composite mechanics while the degradation of the laminate behavior is quantified via the finite element method. The approach accounts for all types of composite behavior, laminate configuration, load conditions, and delamination processes starting from damage initiation, to unstable propagation, and to laminate fracture. Results of laminate fracture in composite beams, panels, plates, and shells are presented to demonstrate the effectiveness and versatility of this new approach.

Detection of rebar delamination using modal analysis

NASA Astrophysics Data System (ADS)

Blodgett, David W.

2003-08-01

A non-destructive method for early detection of reinforcement steel bars (re-bar) delamination in concrete structures has been developed. This method, termed modal analysis, has been shown effective in both laboratory and field experiments. In modal analysis, an audio speaker is used to generate flexural resonant modes in the re-bar in reinforced concrete structures. Vibrations associated with these modes are coupled to the surrounding concrete and propagate to the surface where they are detected using a laser vibrometer and/or accelerometer. Monitoring both the frequency and amplitude of these vibrations provides information on the bonding state of the embedded re-bar. Laboratory measurements were performed on several specially prepared concrete blocks with re-bar of varying degrees of simulated corrosion. Field measurements were performed on an old bridge about to be torn down in Howard County, Maryland and the results compared with those obtained using destructive analysis of the bridge after demolition. Both laboratory and field test results show this technique to be sensitive to re-bar delamination.

Characterization of delamination and transverse cracking in graphite/epoxy laminates by acoustic emission

NASA Technical Reports Server (NTRS)

Garg, A.; Ishaei, O.

1983-01-01

Efforts to characterize and differentiate between two major failure processes in graphite/epoxy composites - transverse cracking and Mode I delamination are described. Representative laminates were tested in uniaxial tension and flexure. The failure processes were monitored and identified by acoustic emission (AE). The effect of moisture on AE was also investigated. Each damage process was found to have a distinctive AE output that is significantly affected by moisture conditions. It is concluded that AE can serve as a useful tool for detecting and identifying failure modes in composite structures in laboratory and in service environments.

A whole genome association study to detect additive and dominant single nucleotide polymorphisms for growth and carcass traits in Korean native cattle, Hanwoo.

PubMed

Li, Yi; Gao, Yuxuan; Kim, You-Sam; Iqbal, Asif; Kim, Jong-Joo

2017-01-01

A whole genome association study was conducted to identify single nucleotide polymorphisms (SNPs) with additive and dominant effects for growth and carcass traits in Korean native cattle, Hanwoo. The data set comprised 61 sires and their 486 Hanwoo steers that were born between spring of 2005 and fall of 2007. The steers were genotyped with the 35,968 SNPs that were embedded in the Illumina bovine SNP 50K beadchip and six growth and carcass quality traits were measured for the steers. A series of lack-of-fit tests between the models was applied to classify gene expression pattern as additive or dominant. A total of 18 (0), 15 (3), 12 (8), 15 (18), 11 (7), and 21 (1) SNPs were detected at the 5% chromosome (genome) - wise level for weaning weight (WWT), yearling weight (YWT), carcass weight (CWT), backfat thickness (BFT), longissimus dorsi muscle area (LMA) and marbling score, respectively. Among the significant 129 SNPs, 56 SNPs had additive effects, 20 SNPs dominance effects, and 53 SNPs both additive and dominance effects, suggesting that dominance inheritance mode be considered in genetic improvement for growth and carcass quality in Hanwoo. The significant SNPs were located at 33 quantitative trait locus (QTL) regions on 18 Bos Taurus chromosomes (i.e. BTA 3, 4, 5, 6, 7, 9, 11, 12, 13, 14, 16, 17, 18, 20, 23, 26, 28, and 29) were detected. There is strong evidence that BTA14 is the key chromosome affecting CWT. Also, BTA20 is the key chromosome for almost all traits measured (WWT, YWT, LMA). The application of various additive and dominance SNP models enabled better characterization of SNP inheritance mode for growth and carcass quality traits in Hanwoo, and many of the detected SNPs or QTL had dominance effects, suggesting that dominance be considered for the whole-genome SNPs data and implementation of successive molecular breeding schemes in Hanwoo.

Nondestructive testing of delaminated interfaces between two materials using electromagnetic interrogation

NASA Astrophysics Data System (ADS)

Cakoni, Fioralba; de Teresa, Irene; Monk, Peter

2018-06-01

We consider the problem of detecting whether two materials that should be in contact have separated or delaminated using electromagnetic radiation. The interface damage is modeled as a thin opening between two materials of different electromagnetic properties. To derive a reconstruction algorithm that focuses on testing for the delamination at the interface between the two materials, we use the approximate asymptotic model for the forward problem derived in de Teresa (2017 PhD Thesis University of Delaware). In this model, the differential equations in the small opening are replaced by approximate transmission conditions for the electromagnetic fields across the interface. We also assume that the undamaged or background state is known and it is desired to find where the delamination has opened. We adapt the linear sampling method to this configuration in order to locate the damaged part of the interface from a knowledge of the scattered field and the undamaged configuration, but without needing to know the electromagnetic properties of the opening. Numerical examples are presented to validate our algorithm.

Delamination onset in polymeric composite laminates under thermal and mechanical loads

NASA Technical Reports Server (NTRS)

Martin, Roderick H.

1991-01-01

A fracture mechanics damage methodology to predict edge delamination is described. The methodology accounts for residual thermal stresses, cyclic thermal stresses, and cyclic mechanical stresses. The modeling is based on the classical lamination theory and a sublaminate theory. The prediction methodology determines the strain energy release rate, G, at the edge of a laminate and compares it with the fatigue and fracture toughness of the composite. To verify the methodology, isothermal static tests at 23, 125, and 175 C and tension-tension fatigue tests at 23 and 175 C were conducted on laminates. The material system used was a carbon/bismaleimide, IM7/5260. Two quasi-isotropic layups were used. Also, 24 ply unidirectional double cantilever beam specimens were tested to determine the fatigue and fracture toughness of the composite at different temperatures. Raising the temperature had the effect of increasing the value of G at the edge for these layups and also to lower the fatigue and fracture toughness of the composite. The static stress to edge delamination was not affected by temperature but the number of cycles to edge delamination decreased.

Enhancement of Impact Toughness by Delamination Fracture in a Low-Alloy High-Strength Steel with Al Alloying

NASA Astrophysics Data System (ADS)

Sun, Junjie; Jiang, Tao; Liu, Hongji; Guo, Shengwu; Liu, Yongning

2016-12-01

The effect of delamination toughening of martensitic steel was investigated both at room and low temperatures [253 K and 233 K (-20 °C and -40 °C)]. Two low-alloy martensitic steels with and without Al alloying were both prepared. Layered structure with white band and black matrix was observed in Al alloyed steel, while a homogeneous microstructure was displayed in the steel without Al. Both steels achieved high strength (tensile strength over 1600 MPa) and good ductility (elongation over 11 pct), but they displayed stark contrasts on impact fracture mode and Charpy impact energy. Delamination fracture occurred in Al alloyed steel and the impact energies were significantly increased both at room temperature (from 75 to 138 J, i.e., nearly improved up to 2 times) and low temperatures [from 47.9 to 71.3 J at 233 K (-40 °C)] compared with the one without Al. Alloying with Al promotes the segregation of Cr, Mn, Si and C elements to form a network structure, which is martensite with higher carbon content and higher hardness than that of the matrix. And this network structure evolved into a band structure during the hot rolling process. The difference of yield stress between the band structure and the matrix gives rise to a delamination fracture during the impact test, which increases the toughness greatly.

Matrix resin effects in composite delamination - Mode I fracture aspects

NASA Technical Reports Server (NTRS)

Hunston, Donald L.; Moulton, Richard J.; Johnston, Norman J.; Bascom, Willard D.

1987-01-01

A number of thermoset, toughened thermoset, and thermoplastic resin matrix systems were characterized for Mode I critical strain energy release rates, and their composites were tested for interlaminar critical strain energy release rates using the double cantilever beam method. A clear correlation is found between the two sets of data. With brittle resins, the interlaminar critical strain energy release rates are somewhat larger than the neat resin values due to a full transfer of the neat resin toughness to the composite and toughening mechanisms associated with crack growth. With tougher matrices, the higher critical strain energy release rates are only partially transferred to the composites, presumably because the fibers restrict the crack-tip deformation zones.

Delamination Fracture Related to Tempering in a High-Strength Low-Alloy Steel

NASA Astrophysics Data System (ADS)

Yan, Wei; Sha, Wei; Zhu, Lin; Wang, Wei; Shan, Yi-Yin; Yang, Ke

2010-01-01

The delamination or splitting of mechanical test specimens of rolled steel plate is a phenomenon that has been studied for many years. In the present study, splitting during fracture of tensile and Charpy V-notch (CVN) test specimens is examined in a high-strength low-alloy plate steel. It is shown that delamination did not occur in test specimens from plate in the as-rolled condition, but was severe in material tempered in the temperature range 500 °C to 650 °C. Minor splitting was seen after heating to 200 °C, 400 °C, and 700 °C. Samples that had been triple quenched and tempered to produce a fine equiaxed grain size also did not exhibit splitting. Microstructural and preferred orientation studies are presented and are discussed as they relate to the splitting phenomenon. It is concluded that the elongated as-rolled grains and grain boundary embrittlement resulting from precipitates (carbides and nitrides) formed during reheating were responsible for the delamination.

Microcracking, microcrack-induced delamination, and longitudinal splitting of advanced composite structures

NASA Technical Reports Server (NTRS)

Nairn, John A.

1992-01-01

A combined analytical and experimental study was conducted to analyze microcracking, microcrack-induced delamination, and longitudinal splitting in polymer matrix composites. Strain energy release rates, calculated by a variational analysis, were used in a failure criterion to predict microcracking. Predictions and test results were compared for static, fatigue, and cyclic thermal loading. The longitudinal splitting analysis accounted for the effects of fiber bridging. Test data are analyzed and compared for longitudinal splitting and delamination under mixed-mode loading. This study emphasizes the importance of using fracture mechanics analyses to understand the complex failure processes that govern composite strength and life.

Growth and Growth hormone - Insulin Like Growth Factor -I (GH-IGF-I) Axis in Chronic Anemias.

PubMed

Soliman, Ashraf T; De Sanctis, Vincenzo; Yassin, Mohamed; Adel, Ashraf

2017-04-28

Anaemia is a global public health problem affecting both developing and developed countries with major consequences for human health as well as social and economic development. It occurs at all stages of the life cycle, but is more prevalent in pregnant women and young children. Iron deficiency anaemia (IDA) was considered to be among the most important contributing factors to the global burden of disease. Prolonged and/or chronic anemia has a negative effect on linear growth especially during the rapid phases (infancy and puberty). Additionally infants with chronic IDA have delayed cognitive, motor, and affective development that may be long-lasting. In view of the significant impact of chronic anemias on growth, pediatricians endocrinologists and hematologists should advocate primary prevention and screening for growth disturbance in these forms of anemias. The extent of the negative effect of different forms of chronic anemias on linear growth and its possible reversibilty is addressed in this review. The possible mechanisms that may impair growth in the different forms of anemias are addressed with special attention to their effect on the growth hormone (GH) - insulin like growth factor -I (IGF-I).

Comparison of Mode II and III Monotonic and Fatigue Delamination Onset Behavior for Carbon/Toughened Epoxy Composites

NASA Technical Reports Server (NTRS)

Li, Jian; OBrien, T. Kevin; Lee, Shaw Ming

1997-01-01

Monotonic and fatigue tests were performed to compare the Mode II and III interlaminar fracture toughness and fatigue delamination onset for Tenax-HTA/R6376 carbon/toughened epoxy composites. The Mode II interlaminar fracture toughness and fatigue delamination onset were characterized using the end-notched flexure (ENF) test while the Mode III interlaminar fracture toughness and fatigue delamination onset were characterized by using the edge crack torsion (ECT) test. Monotonic tests show that the Mode III fracture toughness is higher than the Mode II fracture toughness. Both Mode II and III cyclic loading greatly increases the tendency for a delamination to grow relative to a single monotonically increasing load. Under fatigue loading, the Mode III specimen also has a longer life than the Mode II specimen.

Spontaneous Periodic Delamination of Thin Films To Form Crack-Free Metal and Silicon Ribbons with High Stretchability.

PubMed

Zhang, Qiuting; Tang, Yichao; Hajfathalian, Maryam; Chen, Chunxu; Turner, Kevin T; Dikin, Dmitriy A; Lin, Gaojian; Yin, Jie

2017-12-27

Design of electronic materials with high stretchability is of great importance for realizing soft and conformal electronics. One strategy of realizing stretchable metals and semiconductors is to exploit the buckling of materials bonded to elastomers. However, the level of stretchability is often limited by the cracking and fragmentation of the materials that occurs when constrained buckling occurs while bonded to the substrate. Here, we exploit a failure mechanism, spontaneous buckling-driven periodic delamination, to achieve high stretchability in metal and silicon films that are deposited on prestrained elastomer substrates. We find that both globally periodic buckle-delaminated pattern and ordered cracking patterns over large areas are observed in the spontaneously buckle-delaminated thin films. The geometry of periodic delaminated buckles and cracking periodicity can be predicted by theoretical models. By patterning the films into ribbons with widths smaller than the predicted cracking periodicity, we demonstrate the design of crack-free and spontaneous delaminated ribbons on highly prestrained elastomer substrates, which provides a high stretchability of about 120% and 400% in Si and Au ribbons, respectively. We find that the high stretchability is mainly attributed to the largely relaxed strain in the ribbons via spontaneous buckling-driven delamination, as made evident by the small maximum tensile strain in both ribbons, which is measured to be over 100 times smaller than that of the substrate prestrain.

Delamination toughness characterization of out-of-autoclave vacuum-bag-only polymer matrix composites enhanced by z-aligned carbon nanofibers

NASA Astrophysics Data System (ADS)

Brewer, John S.

Brewer, John S., M. S., University of South Alabama, May 2015. Delamination Toughness Characterization of Out-of-Autoclave Vacuum-Bag-Only Polymer Matrix Composites Enhanced by z-aligned Carbon Nanofibers. Chair of Committee: Kuang-Ting Hsiao, Ph.D. In the last few decades, the use of composite materials has revolutionized materials manufacturing. Now, carbon fiber materials are at the forefront of engineering and manufacturing technology. One of the chief failure modes of composite materials is delamination. For this reason, this study employed the Mode-I Interlaminar Fracture Toughness Test (ASTM D 5528-01) to characterize how the inclusion of z-aligned carbon nanofibers (CNF) in Carbon Fiber Reinforced Polymers (CFRP) affects delamination strength. CFRP with z-aligned CNF in concentrations of 0.3% and 0.6% by weight were compared to control CFRP samples and CFRP samples modified with 0.3 weight percent unaligned CNF. The largest improvement was seen in the 0.3 weight percent aligned composite with a mean interlaminar fracture toughness increase of over 35%, while the uncertainty was decreased. A standard deviation of 3.3% was observed which equates to an uncertainty value 30% better than the control samples. Data and microscopy are included and discussed.

Distributed fiber optic sensor-enhanced detection and prediction of shrinkage-induced delamination of ultra-high-performance concrete overlay

NASA Astrophysics Data System (ADS)

Bao, Yi; Valipour, Mahdi; Meng, Weina; Khayat, Kamal H.; Chen, Genda

2017-08-01

This study develops a delamination detection system for smart ultra-high-performance concrete (UHPC) overlays using a fully distributed fiber optic sensor. Three 450 mm (length) × 200 mm (width) × 25 mm (thickness) UHPC overlays were cast over an existing 200 mm thick concrete substrate. The initiation and propagation of delamination due to early-age shrinkage of the UHPC overlay were detected as sudden increases and their extension in spatial distribution of shrinkage-induced strains measured from the sensor based on pulse pre-pump Brillouin optical time domain analysis. The distributed sensor is demonstrated effective in detecting delamination openings from microns to hundreds of microns. A three-dimensional finite element model with experimental material properties is proposed to understand the complete delamination process measured from the distributed sensor. The model is validated using the distributed sensor data. The finite element model with cohesive elements for the overlay-substrate interface can predict the complete delamination process.

Delaminating and restacking MgAl-layered double hydroxide monitored and characterized by a range of instrumental methods

NASA Astrophysics Data System (ADS)

Muráth, Szabolcs; Somosi, Zoltán; Tóth, Ildikó Y.; Tombácz, Etelka; Sipos, Pál; Pálinkó, István

2017-07-01

The delamination-restacking properties of MgAl-layered double hydroxide (MgAl-LDH) were studied in various solvents. The LDH samples were successfully delaminated in polar amides (formamide, N-methylformamide, N-methylacetamide). Usually, delamination was finalized by ultrasonic treatment. As rehydrating solutions, numerous Na-salts with single-, double- and triple-charged anions were used. Reconstruction was accomplished with anions of one or two negative charges, but triple-charged ones generally disrupted the rebuilding process, likely, because their salts with the metals of the LDH are very stable, and the thin layers can more readily transform to salts than the ordered materials. Samples and delamination-restacking processes were characterized by X-ray diffractometry (XRD), infrared spectroscopy (IR), dynamic light scattering (DLS), scanning electron microscopy (SEM) and energy-dispersive X-ray analysis (EDX).

Continental Delamination of the Romanian Eastern Carpathians: A Lower Crustal Origin of the Vrancea Seismogenic Zone?

NASA Astrophysics Data System (ADS)

Fillerup, M. A.; Knapp, J. H.; Knapp, C. C.

2006-12-01

Two lithosphere-scale, explosive-source seismic reflection profiles (DRACULA I and DACIA PLAN), inclusive of the hinterland and foreland of the Romanian Eastern Carpathians, provide new evidence for the geodynamic origin of the Vrancea Seismogenic Zone (VSZ) of Romania. These data, collected to evaluate existing subduction-related and delamination geodynamic models proposed to explain the intermediate depth seismicity associated with the Vrancea zone, show evidence of continental crust extending continuously above the VSZ from the Carpathian foreland well into the Transylvanian hinterland. Crustal thicknesses inferred from these data based on reflectivity show a 40-45 km crust below the Transylvanian basin abruptly shallowing to 32 km for ~120 km beneath the fold and thrust belt of the main Carpathian orogen and thickening again to 38-42 km crust in the foreland. This thinned crust outlines an apparent lower crustal sub-orogenic cavity that is overlain by a relatively subhorizontal reflective fabric absent of dipping reflectivity. The northwest dipping Vrancea seismogenic body, a 30x70x200 km volume of intermediate depth earthquakes, is located on the eastern flank of the apparently thin crust beneath the Carpathian orogen. Amplitude decay curves show penetration of seismic energy to a depth of ~60 km in the vicinity of the sub-orogenic cavity, implying this non- reflective zone is a geologic signature. Rotation of the VSZ about a hinge beneath the foreland basin at a depth of ~50 km restores to fill the lower-crustal cavity under the orogen, suggesting the VSZ represents a portion of brittle lower crust delaminated during continental lithospheric delamination which may have caused regional uplift of the Transylvanian basin. The lack of through-going, dipping crustal-scale boundaries along this composite lithospheric transect would appear to preclude subduction as an explanation for seismicity in the VSZ, consistent with abundant surface geologic data. These

Monitoring of non-homogeneous strains in wood glued joints with embedded FBG optical sensors in mode I delamination tests

NASA Astrophysics Data System (ADS)

Maciel, R. S.; Frazão, O.; Morais, J. J. L.; Fernandes, J. R. A.

2013-11-01

In this work it is presented a study of the reflection spectra yielded by a Fiber Bragg Grating sensor embedded into an epoxy glue line between two wood arms, in a double cantilever beam (DCB) Mode I delamination test. The reflection spectra were obtained using a Spectral Analyzer Fibersensing Bragmeter FS2200SA in regular time intervals, as the stress applied to the laminates is continuously increased until fracture occurs. They initially show a typical Bragg grating reflection spectrum, which gradually changes into more complicated, multiple-peak spectra, resulting from a non-homogenous strain distribution along the board line. Based on these results, a model was derived for the variation of the grating effective index which fits the observed spectra when the irregular strain distribution is observed. This model consists of usual cosine description of Bragg grating effective index with linear phase variation, plus a logarithmic phase change along the fiber length, resulting in the increment of the grating wavelength with increasing distance from the load application point. Moreover, from this model the strain distribution along the grating is found, yielding the expected result.

Multiscale Analysis of Delamination of Carbon Fiber-Epoxy Laminates with Carbon Nanotubes

NASA Technical Reports Server (NTRS)

Riddick, Jaret C.; Frankland, SJV; Gates, TS

2006-01-01

A multi-scale analysis is presented to parametrically describe the Mode I delamination of a carbon fiber/epoxy laminate. In the midplane of the laminate, carbon nanotubes are included for the purposes of selectively enhancing the fracture toughness of the laminate. To analyze carbon fiber epoxy carbon nanotube laminate, the multi-scale methodology presented here links a series of parameterizations taken at various length scales ranging from the atomistic through the micromechanical to the structural level. At the atomistic scale molecular dynamics simulations are performed in conjunction with an equivalent continuum approach to develop constitutive properties for representative volume elements of the molecular structure of components of the laminate. The molecular-level constitutive results are then used in the Mori-Tanaka micromechanics to develop bulk properties for the epoxy-carbon nanotube matrix system. In order to demonstrate a possible application of this multi-scale methodology, a double cantilever beam specimen is modeled. An existing analysis is employed which uses discrete springs to model the fiber bridging affect during delamination propagation. In the absence of empirical data or a damage mechanics model describing the effect of CNTs on fracture toughness, several tractions laws are postulated, linking CNT volume fraction to fiber bridging in a DCB specimen. Results from this demonstration are presented in terms of DCB specimen load-displacement responses.

The Effect of Temperature on Faceplate/Core Delamination in Composite/Titanium Sandwich Plates

NASA Technical Reports Server (NTRS)

Liechti, Kenneth M.; Marton, Balazs

2000-01-01

A study was made of the delamination behavior of sandwich beams made of titanium core bonded to face-plates that consisted of carbon fiber reinforced polymer composite. Nominally mode I behavior was considered at 23C and 180C, by making use of a specially reinforced double cantilever (DCB) specimens. The toughness of the bond between the faceplate and the core was determined on the basis of a beam on elastic foundation analysis. The specimen compliance, and toughness were all independent of temperature in these relatively short-term experiments. The fracture mechanism showed temperature dependence, due to the hygrothermal sensitivity of the adhesive.

A Damage Model for the Simulation of Delamination in Advanced Composites under Variable-Mode Loading

NASA Technical Reports Server (NTRS)

Turon, A.; Camanho, P. P.; Costa, J.; Davila, C. G.

2006-01-01

A thermodynamically consistent damage model is proposed for the simulation of progressive delamination in composite materials under variable-mode ratio. The model is formulated in the context of Damage Mechanics. A novel constitutive equation is developed to model the initiation and propagation of delamination. A delamination initiation criterion is proposed to assure that the formulation can account for changes in the loading mode in a thermodynamically consistent way. The formulation accounts for crack closure effects to avoid interfacial penetration of two adjacent layers after complete decohesion. The model is implemented in a finite element formulation, and the numerical predictions are compared with experimental results obtained in both composite test specimens and structural components.

Challenges in Modelling of Lightning-Induced Delamination; Effect of Temperature-Dependent Interfacial Properties

NASA Technical Reports Server (NTRS)

Naghipour, P.; Pineda, E. J.; Arnold, S.

2014-01-01

Lightning is a major cause of damage in laminated composite aerospace structures during flight. Due to the dielectric nature of Carbon fiber reinforced polymers (CFRPs), the high energy induced by lightning strike transforms into extreme, localized surface temperature accompanied with a high-pressure shockwave resulting in extensive damage. It is crucial to develop a numerical tool capable of predicting the damage induced from a lightning strike to supplement extremely expensive lightning experiments. Delamination is one of the most significant failure modes resulting from a lightning strike. It can be extended well beyond the visible damage zone, and requires sophisticated techniques and equipment to detect. A popular technique used to model delamination is the cohesive zone approach. Since the loading induced from a lightning strike event is assumed to consist of extreme localized heating, the cohesive zone formulation should additionally account for temperature effects. However, the sensitivity to this dependency remains unknown. Therefore, the major focus point of this work is to investigate the importance of this dependency via defining various temperature dependency profiles for the cohesive zone properties, and analyzing the corresponding delamination area. Thus, a detailed numerical model consisting of multidirectional composite plies with temperature-dependent cohesive elements in between is subjected to lightning (excessive amount of heat and pressure) and delamination/damage expansion is studied under specified conditions.

Mechanical perturbation-induced ethylene releases apical dominance in Pharbitis nil by restricting shoot growth

NASA Technical Reports Server (NTRS)

Prasad, T. K.; Cline, M. G.

1985-01-01

Mechanical perturbation (MP, rubbing) or internodes of Pharbitis nil shoots initiates release of lateral buds (LB) from apical dominance within 48 h. Evidence is presented which suggests that MP promotion of LB outgrowth is mediated by ethylene-induced restriction of main shoot growth. Ethylene production in the internodes is stimulated by MP within 2 h. Effects of MP are mimicked by treatments with 1-aminocyclopropane-1-carboxylic acid (ACC) and are negated by the inhibitors of ethylene production or action, aminoethoxy vinylglycine (AVG) and AgNO3. The fact that effects of MP, ACC, and ethylene inhibitors are observed to occur on main shoot growth at least 24 h before they are observed to occur on LB growth suggests a possible cause and effect relationship. MP also causes an increase in internode diameter. MP stimulation of ethylene production appears to be mediated by ACC synthase. The results of this study and our previous studies suggest that apical dominance may be released by any mechanism which induces ethylene restriction of main shoot growth.

Winter feeding, growth and condition of brown trout Salmo trutta in a groundwater-dominated stream

USGS Publications Warehouse

French, William E.; Vondracek, Bruce C.; Ferrington, Leonard C.; Finlay, Jacques C.; Dieterman, Douglas J.

2014-01-01

Winter can be a stressful period for stream-dwelling salmonid populations, often resulting in reduced growth and survival. Stream water temperatures have been identified as a primary mechanism driving reductions in fitness during winter. However, groundwater inputs can moderate water temperature and may reduce winter severity. Additionally, seasonal reductions in prey availability may contribute to decreased growth and survival, although few studies have examined food webs supporting salmonids under winter conditions. This study employed diet, stable isotope, and mark-recapture techniques to examine winter (November through March) feeding, growth, and condition of brown troutSalmo trutta in a groundwater-dominated stream (Badger Creek, Minnesota, USA). Growth was greater for fish ≤ 150 mm (mean = 4.1 mg g−1 day−1) than for those 151–276 mm (mean = 1.0 mg g−1 day−1) during the winter season. Overall condition from early winter to late winter did not vary for fish ≤150 mm (mean relative weight (Wr) = 89.5) and increased for those 151–276 mm (mean Wr = 85.8 early and 89.4 late). Although composition varied both temporally and by individual, brown trout diets were dominated by aquatic invertebrates, primarily Amphipods, Dipterans, and Trichopterans. Stable isotope analysis supported the observations of the dominant prey taxa in stomach contents and indicated the winter food web was supported by a combination of allochthonous inputs and aquatic macrophytes. Brown trout in Badger Creek likely benefited from the thermal regime and increased prey abundance present in this groundwater-dominated stream during winter.

Monitoring Delamination of Thermal Barrier Coatings During Interrupted High-Heat-Flux Laser Testing using Luminescence Imaging

NASA Technical Reports Server (NTRS)

Eldridge, Jeffrey I.; Zhu, Dongming; Wolfe, Douglas E.

2011-01-01

This presentation showed progress made in extending luminescence-base delamination monitoring to TBCs exposed to high heat fluxes, which is an environment that much better simulates actual turbine engine conditions. This was done by performing upconversion luminescence imaging during interruptions in laser testing, where a high-power CO2 laser was employed to create the desired heat flux. Upconverison luminescence refers to luminescence where the emission is at a higher energy (shorter wavelength) than the excitation. Since there will be negligible background emission at higher energies than the excitation, this methods produces superb contrast. Delamination contrast is produced because both the excitation and emission wavelengths are reflected at delamination cracks so that substantially higher luminescence intensity is observed in regions containing delamination cracks. Erbium was selected as the dopant for luminescence specifically because it exhibits upconversion luminescence. The high power CO2 10.6 micron wavelength laser facility at NASA GRC was used to produce the heat flux in combination with forced air backside cooling. Testing was performed at a lower (95 W/sq cm) and higher (125 W/sq cm) heat flux as well as furnace cycling at 1163C for comparison. The lower heat flux showed the same general behavior as furnace cycling, a gradual, "spotty" increase in luminescence associated with debond progression; however, a significant difference was a pronounced incubation period followed by acceleration delamination progression. These results indicate that extrapolating behavior from furnace cycling measurements will grossly overestimate remaining life under high heat flux conditions. The higher heat flux results were not only accelerated, but much different in character. Extreme bond coat rumpling occurred, and delamination propagation extended over much larger areas before precipitating macroscopic TBC failure. This indicates that under the higher heat flux (and

An Approach for Assessing Delamination Propagation Capabilities in Commercial Finite Element Codes

NASA Technical Reports Server (NTRS)

Krueger, Ronald

2007-01-01

An approach for assessing the delamination propagation capabilities in commercial finite element codes is presented and demonstrated for one code. For this investigation, the Double Cantilever Beam (DCB) specimen and the Single Leg Bending (SLB) specimen were chosen for full three-dimensional finite element simulations. First, benchmark results were created for both specimens. Second, starting from an initially straight front, the delamination was allowed to propagate. Good agreement between the load-displacement relationship obtained from the propagation analysis results and the benchmark results could be achieved by selecting the appropriate input parameters. Selecting the appropriate input parameters, however, was not straightforward and often required an iterative procedure. Qualitatively, the delamination front computed for the DCB specimen did not take the shape of a curved front as expected. However, the analysis of the SLB specimen yielded a curved front as may be expected from the distribution of the energy release rate and the failure index across the width of the specimen. Overall, the results are encouraging but further assessment on a structural level is required.

Identification of delamination interface in composite laminates using scattering characteristics of lamb wave: numerical and experimental studies

NASA Astrophysics Data System (ADS)

Singh, Rakesh Kumar; Ramadas, C.; Balachandra Shetty, P.; Satyanarayana, K. G.

2017-04-01

Considering the superior strength properties of polymer based composites over metallic materials, they are being used in primary structures of aircrafts. However, these polymeric materials are much more complex in behaviour due to their structural anisotropy along with existence of different materials unlike in metallic alloys. These pose challenge in flaw detection, residual strength determination and life of a structure with their high susceptibility to impact damage in the form of delaminations/disbonds or cracks. This reduces load-bearing capability and potentially leads to structural failure. With this background, this study presents a method to identify location of delamination interface along thickness of a laminate. Both numerical and experimental studies have been carried out with a view to identify the defect, on propagation, mode conversion and scattering characteristics of fundamental anti-symmetric Lamb mode (Ao) when it passed through a semi-infinite delamination. Further, the reflection and transmission scattering coefficients based on power and amplitude ratios of the scattered waves have been computed. The methodology was applied on numerically simulated delaminations to illustrate the efficacy of the method. Results showed that it could successfully identify delamination interface.

Multilayer theory for delamination analysis of a composite curved bar subjected to end forces and end moments

NASA Technical Reports Server (NTRS)

Ko, William L.; Jackson, Raymond H.

1989-01-01

A composite test specimen in the shape of a semicircular curved bar subjected to bending offers an excellent stress field for studying the open-mode delamination behavior of laminated composite materials. This is because the open-mode delamination nucleates at the midspan of the curved bar. The classical anisotropic elasticity theory was used to construct a 'multilayer' theory for the calculations of the stress and deformation fields induced in the multilayered composite semicircular curved bar subjected to end forces and end moments. The radial location and intensity of the open-mode delamination stress were calculated and were compared with the results obtained from the anisotropic continuum theory and from the finite element method. The multilayer theory gave more accurate predictions of the location and the intensity of the open-mode delamination stress than those calculated from the anisotropic continuum theory.

Multilayer theory for delamination analysis of a composite curved bar subjected to end forces and end moments

NASA Technical Reports Server (NTRS)

Ko, William L.; Jackson, Raymond H.

1989-01-01

A composite test specimen in the shape of a semicircular curved bar subjected to bending offers an excellent stress field for studying the open-mode delamination behavior of laminated composite materials. This is because the open-mode delamination nucleates at the midspan of the curved bar. The classical anisotropic elasticity theory was used to construct a multilayer theory for the calculations of the stress and deformation fields induced in the multilayered composite semicircular curved bar subjected to end forces and end moments. The radial location and intensity of the open-mode delamination stress were calculated and were compared with the results obtained from the anisotropic continuum theory and from the finite element method. The multilayer theory gave more accurate predictions of the location and the intensity of the open-mode delamination stress than those calculated from the anisotropic continuum theory.

Effect of tool geometry and cutting parameters on delamination and thrust forces in drilling CFRP/Al-Li

NASA Astrophysics Data System (ADS)

El Bouami, Souhail; Habak, Malek; Franz, Gérald; Velasco, Raphaël; Vantomme, Pascal

2016-10-01

Composite materials are increasingly used for structural parts in the aeronautic industries. Carbon Fiber-Reinforced Plastics (CFRP) are often used in combination with metallic materials, mostly aluminium alloys. This raises new problems in aircraft assembly. Delamination is one of these problems. In this study, CFRP/Al-Li stacks is used as experimental material for investigation effect of interaction of cutting parameters (cutting speed and feed rate) and tool geometry on delamination and thrust forces in drilling operation. A plan of experiments, based on Taguchi design method, was employed to investigate the influence of tool geometry and in particular the point angle and cutting parameters on delamination and axial effort. The experimental results demonstrate that the feed rate is the major parameter and the importance of tool point angle in delamination and thrust forces in the stacks were shown.

The Effect of Delamination on Damage Path and Failure Load Prediction for Notched Composite Laminates

NASA Technical Reports Server (NTRS)

Satyanarayana, Arunkumar; Bogert, Philip B.; Chunchu, Prasad B.

2007-01-01

The influence of delamination on the progressing damage path and initial failure load in composite laminates is investigated. Results are presented from a numerical and an experimental study of center-notched tensile-loaded coupons. The numerical study includes two approaches. The first approach considers only intralaminar (fiber breakage and matrix cracking) damage modes in calculating the progression of the damage path. In the second approach, the model is extended to consider the effect of interlaminar (delamination) damage modes in addition to the intralaminar damage modes. The intralaminar damage is modeled using progressive damage analysis (PDA) methodology implemented with the VUMAT subroutine in the ABAQUS finite element code. The interlaminar damage mode has been simulated using cohesive elements in ABAQUS. In the experimental study, 2-3 specimens each of two different stacking sequences of center-notched laminates are tensile loaded. The numerical results from the two different modeling approaches are compared with each other and the experimentally observed results for both laminate types. The comparisons reveal that the second modeling approach, where the delamination damage mode is included together with the intralaminar damage modes, better simulates the experimentally observed damage modes and damage paths, which were characterized by splitting failures perpendicular to the notch tips in one or more layers. Additionally, the inclusion of the delamination mode resulted in a better prediction of the loads at which the failure took place, which were higher than those predicted by the first modeling approach which did not include delaminations.

Ammonia oxidation-dependent growth of group I.1b Thaumarchaeota in acidic red soil microcosms.

PubMed

Wu, Yucheng; Conrad, Ralf

2014-07-01

Accumulating evidence suggests that Thaumarchaeota may control nitrification in acidic soils. However, the composition of the thaumarchaeotal communities and their functioning is not well known. Therefore, we studied nitrification activity in relation to abundance and composition of Thaumarchaeota in an acidic red soil from China, using microcosms incubated with and without cellulose amendment. Cellulose was selected to simulate the input of crop residues used to increase soil fertility by local farming. Accumulation of NO3-(-N) was correlated with the growth of Thaumarchaeota as determined by qPCR of 16S rRNA and ammonia monooxygenase (amoA) genes. Both nitrification activity and thaumarchaeotal growth were inhibited by acetylene. They were also inhibited by cellulose amendment, possibly due to the depletion of ammonium by enhanced heterotrophic assimilation. These results indicated that growth of Thaumarchaeota was dependent on ammonia oxidation. The thaumarchaeotal 16S rRNA gene sequences in the red soil were dominated by a clade related to soil fosmid clone 29i4 within the group I.1b, which is widely distributed but so far uncultured. The archaeal amoA sequences were mainly related to the Nitrososphaera sister cluster. These observations suggest that fosmid clone 29i4 and Nitrososphaera sister cluster represent the same group of Thaumarchaeota and dominate ammonia oxidation in acidic red soil. © 2014 Federation of European Microbiological Societies. Published by John Wiley & Sons Ltd. All rights reserved.

Time dependent response of low velocity impact induced composite conical shells under multiple delamination

NASA Astrophysics Data System (ADS)

Dey, Sudip; Karmakar, Amit

2014-02-01

This paper presents the time dependent response of multiple delaminated angle-ply composite pretwisted conical shells subjected to low velocity normal impact. The finite element formulation is based on Mindlin's theory incorporating rotary inertia and effects of transverse shear deformation. An eight-noded isoparametric plate bending element is employed to satisfy the compatibility of deformation and equilibrium of resultant forces and moments at the delamination crack front. A multipoint constraint algorithm is incorporated which leads to asymmetric stiffness matrices. The modified Hertzian contact law which accounts for permanent indentation is utilized to compute the contact force, and the time dependent equations are solved by Newmark's time integration algorithm. Parametric studies are conducted with respect to triggering parameters like laminate configuration, location of delamination, angle of twist, velocity of impactor, and impactor's displacement for centrally impacted shells.

Characterization of Delaminations and Transverse Matrix Cracks in Composite Laminates Using Multiple-Angle Ultrasonic Inspection

NASA Technical Reports Server (NTRS)

Johnston, Patrick H.; Appleget, Chelsea D.; Odarczenko, Michael T.

2012-01-01

Delaminations and transverse matrix cracks often appear concurrently in composite laminates. Normal-incidence ultrasound is excellent at detecting delaminations, but is not optimum for matrix cracks. Non-normal incidence, or polar backscattering, has been shown to optimally detect matrix cracks oriented perpendicular to the ultrasonic plane of incidence. In this work, a series of six composite laminates containing slots were loaded in tension to achieve various levels of delamination and ply cracking. Ultrasonic backscattering was measured over a range of incident polar and azimuthal angles, in order to characterize the relative degree of damage of the two types. Sweptpolar- angle measurements were taken with a curved phased array, as a step toward an array-based approach to simultaneous measurement of combined flaws.

Layered zinc hydroxide salts: delamination, preferred orientation of hydroxide lamellae, and formation of ZnO nanodiscs.

PubMed

Demel, Jan; Pleštil, Josef; Bezdička, Petr; Janda, Pavel; Klementová, Mariana; Lang, Kamil

2011-08-15

Delamination of layered zinc hydroxide salts (LZH) into hydroxide layers provides nanobuilding blocs of a two-dimensional anisotropy. The methodology, extent of delamination, the size and stability of hydroxide lamellae are described in detail. The ability of lamellae to restack to form oriented hydroxide films depends on the solvent, original LZH salt, and conditions used for delamination. The most interesting results were obtained using LZH intercalated with dodecyl sulfate anions and LZH nitrate delaminated in butanol at 60 °C and in formamide at room temperature, respectively. The former method produces hydroxide lamellae of a lateral size of ca. 10-20 nm. The inner structure of the hydroxide layers is conserved and separated lamellae restack to the original layered structure of LZH dodecyl sulfate. The latter method yields lamellae with a size decreasing from 73.3 nm to 10 nm after a 2-week aging, while their thickness is nearly constant (2.6-3.8 nm). However, the use of formamide is complicated by the formation of Zn(II) formate. The major part of LZH intercalated with dodecyl sulfate anions is transformed during the delamination procedure to anisotropic ZnO nanoparticles, either needle-like particles prolonged in the [0 0 1] direction or disc-like particles flattened along the (0 0 1) plane. Copyright © 2011 Elsevier Inc. All rights reserved.

Modeling Delamination in Postbuckled Composite Structures Under Static and Fatigue Loads

NASA Technical Reports Server (NTRS)

Bisagni, Chiara; Brambilla, Pietro; Bavila, Carlos G.

2013-01-01

The ability of the Abaqus progressive Virtual Crack Closure Technique (VCCT) to model delamination in composite structures was investigated for static, postbuckling, and fatigue loads. Preliminary evaluations were performed using simple Double Cantilever Beam (DCB) and Mixed-Mode Bending (MMB) specimens. The nodal release sequences that describe the propagation of the delamination front were investigated. The effect of using a sudden or a gradual nodal release was evaluated by considering meshes aligned with the crack front as well as misaligned meshes. Fatigue simulations were then performed using the Direct Cyclic Fatigue (DCF) algorithm. It was found that in specimens such as the DCB, which are characterized by a nearly linear response and a pure fracture mode, the algorithm correctly predicts the Paris Law rate of propagation. However, the Abaqus DCF algorithm does not consider different fatigue propagation laws in different fracture modes. Finally, skin/stiffener debonding was studied in an aircraft fuselage subcomponent in which debonding occurs deep into post-buckling deformation. VCCT was shown to be a robust tool for estimating the onset propagation. However, difficulties were found with the ability of the current implementation of the Abaqus progressive VCCT to predict delamination propagation within structures subjected to postbuckling deformations or fatigue loads.

Ultrasonic Detection of Delamination and Material Characterization of Thermal Barrier Coatings

NASA Astrophysics Data System (ADS)

Chen, Hung-Liang Roger; Zhang, Binwei; Alvin, Mary Anne; Lin, Yun

2012-12-01

This article describes ultrasonic nondestructive evaluation (NDE) to detect the changes of material properties and provide early warning of delamination in thermal barrier coating (TBC) systems. NDE tests were performed on single-crystal René N5 superalloy coupons that were coated with a commercially available MCrAlY bond coat and an air plasma sprayed 7% yttria-stabilized zirconia (YSZ) top coat deposited by Air Plasma Spray method, as well as Haynes 230 superalloy coupons coated with MCrA1Y bond coat, and an electron beam physical vapor deposit of 7% YSZ top coat. The TBC coupons were subjected to either cyclic or isothermal exposure for various lengths of time at temperatures ranging from 900 to 1100 °C. The ultrasonic measurements performed on the coupons had provided an early warning of delamination along the top coat/TGO interface before exposure time, when delamination occurred. The material's property (Young's modulus) of the top coat was estimated using the measured wave speeds. Finite element analysis (FEA) of the ultrasonic wave propagation was conducted on a simplified TBC system to verify experimental observations. The technique developed was also demonstrated on an as-manufactured turbine blade to estimate normalized top coat thickness measurements.

Cohesive finite element modeling of the delamination of HTPB binder and HMX crystals under tensile loading

DOE Office of Scientific and Technical Information (OSTI.GOV)

Walters, David J.; Luscher, Darby J.; Yeager, John D.

Accurately modeling the mechanical behavior of the polymer binders and the degradation of interfaces between binder and crystal is important to science-based understanding of the macro-scale response of polymer bonded explosives. The paper presents a description of relatively a simple bi-crystal HMX-HTPB specimen and associated tensile loading experiment including computed tomography imaging, the pertinent constitutive theory, and details of numerical simulations used to infer the behavior of the material during the delamination process. Within this work, mechanical testing and direct numerical simulation of this relatively simple bi-crystal system enabled reasonable isolation of binder-crystal interface delamination, in which the effects ofmore » the complicated thermomechanical response of explosive crystals were minimized. Cohesive finite element modeling of the degradation and delamination of the interface between a modified HTPB binder and HMX crystals was used to reproduce observed results from tensile loading experiments on bi-crystal specimens. Several comparisons are made with experimental measurements in order to identify appropriate constitutive behavior of the binder and appropriate parameters for the cohesive traction-separation behavior of the crystal-binder interface. This research demonstrates the utility of directly modeling the delamination between binder and crystal within crystal-binder-crystal tensile specimen towards characterizing the behavior of these interfaces in a manner amenable to larger scale simulation of polycrystalline PBX materials. One critical aspect of this approach is micro computed tomography imaging conducted during the experiments, which enabled comparison of delamination patterns between the direct numerical simulation and actual specimen. In addition to optimizing the cohesive interface parameters, one important finding from this investigation is that understanding and representing the strain-hardening plasticity of HTPB

Cohesive finite element modeling of the delamination of HTPB binder and HMX crystals under tensile loading

DOE PAGES

Walters, David J.; Luscher, Darby J.; Yeager, John D.; ...

2018-02-27

Accurately modeling the mechanical behavior of the polymer binders and the degradation of interfaces between binder and crystal is important to science-based understanding of the macro-scale response of polymer bonded explosives. The paper presents a description of relatively a simple bi-crystal HMX-HTPB specimen and associated tensile loading experiment including computed tomography imaging, the pertinent constitutive theory, and details of numerical simulations used to infer the behavior of the material during the delamination process. Within this work, mechanical testing and direct numerical simulation of this relatively simple bi-crystal system enabled reasonable isolation of binder-crystal interface delamination, in which the effects ofmore » the complicated thermomechanical response of explosive crystals were minimized. Cohesive finite element modeling of the degradation and delamination of the interface between a modified HTPB binder and HMX crystals was used to reproduce observed results from tensile loading experiments on bi-crystal specimens. Several comparisons are made with experimental measurements in order to identify appropriate constitutive behavior of the binder and appropriate parameters for the cohesive traction-separation behavior of the crystal-binder interface. This research demonstrates the utility of directly modeling the delamination between binder and crystal within crystal-binder-crystal tensile specimen towards characterizing the behavior of these interfaces in a manner amenable to larger scale simulation of polycrystalline PBX materials. One critical aspect of this approach is micro computed tomography imaging conducted during the experiments, which enabled comparison of delamination patterns between the direct numerical simulation and actual specimen. In addition to optimizing the cohesive interface parameters, one important finding from this investigation is that understanding and representing the strain-hardening plasticity of HTPB

Delamination of neural crest cells requires transient and reversible Wnt inhibition mediated by Dact1/2.

PubMed

Rabadán, M Angeles; Herrera, Antonio; Fanlo, Lucia; Usieto, Susana; Carmona-Fontaine, Carlos; Barriga, Elias H; Mayor, Roberto; Pons, Sebastián; Martí, Elisa

2016-06-15

Delamination of neural crest (NC) cells is a bona fide physiological model of epithelial-to-mesenchymal transition (EMT), a process that is influenced by Wnt/β-catenin signalling. Using two in vivo models, we show that Wnt/β-catenin signalling is transiently inhibited at the time of NC delamination. In attempting to define the mechanism underlying this inhibition, we found that the scaffold proteins Dact1 and Dact2, which are expressed in pre-migratory NC cells, are required for NC delamination in Xenopus and chick embryos, whereas they do not affect the motile properties of migratory NC cells. Dact1/2 inhibit Wnt/β-catenin signalling upstream of the transcriptional activity of T cell factor (TCF), which is required for EMT to proceed. Dact1/2 regulate the subcellular distribution of β-catenin, preventing β-catenin from acting as a transcriptional co-activator to TCF, yet without affecting its stability. Together, these data identify a novel yet important regulatory element that inhibits β-catenin signalling, which then affects NC delamination. © 2016. Published by The Company of Biologists Ltd.

Intracellular processing of epidermal growth factor. I. Acidification of 125I-epidermal growth factor in intracellular organelles.

PubMed

Matrisian, L M; Planck, S R; Magun, B E

1984-03-10

We previously reported that 125I-labeled epidermal growth factor is processed intracellularly to acidic macromolecules in Rat-1 fibroblasts. The present study defines the precursor-product relationship and localization of the processing steps to subcellular organelles by the use of a single isoelectric species of 125I-epidermal growth factor and Percoll gradient fractionation. The native pI 4.55 125I-epidermal growth factor was rapidly processed to a pI 4.2 species on or near the cell surface and in organelles corresponding to clathrin-coated vesicles, Golgi, and endoplasmic reticulum. This species was then processed to a pI 4.35 species in similar organelles. The pI 4.2 and 4.35 species were converted to a pI 4.0 species in dense, lysosome-like organelles. This species was ultimately degraded and exocytosed from the cell as low molecular weight products.

Study on drilling induced delamination of woven kenaf fiber reinforced epoxy composite using carbide drills

NASA Astrophysics Data System (ADS)

Suhaily, M.; Hassan, C. H. Che; Jaharah, A. G.; Azmi, H.; Afifah, M. A.; Khairusshima, M. K. Nor

2018-04-01

In this research study, it presents the influences of drilling parameters on the delamination factor during the drilling of woven kenaf fiber reinforced epoxy composite laminates when using the carbide drill bits. The purpose of this study is to investigate the influence of drilling parameters such as cutting speed, feed rate and drill sizes on the delamination produced when drilling woven kenaf reinforced epoxy composite using the non-coated carbide drill bits. The damage generated on the woven kenaf reinforced epoxy composite laminates were observed both at the entrance and exit surface during the drilling operation. The experiments were conducted according to the Box Behnken experimental designs. The results indicated that the drill diameter has a significant influence on the delamination when drilling the woven kenaf fiber reinforced epoxy composites.

Cryosalt Formation in Delaminated Clays

NASA Astrophysics Data System (ADS)

Yeşilbaş, Merve; Boily, Jean-François

2017-04-01

Hydrohalite (NaClṡ2H2O) forms by evaporation, sublimation and freezing of aqueous solutions of NaCl. Although this process is traditionally deemed to occur in aqueous solutions little attention has been paid on whether this is possible with minerals. Smectite minerals are particularly interesting in this regard for their ability to accommodate water between aluminosilicate sheets, allowing them to swell and even delaminate. In particular, montmorillonite possesses high affinities for water and can play important roles in water retention and ice formation in nature, as well as in strategies for nuclear waste storage and even for technological applications. [1,2] For this study, we aimed to develop insight into the molecular-level nature of hydrohalite formation at surfaces of montmorillonite particles as well as in their interlayers. Thin films of Na+ and Ca2+ exchanged montmorillonites deposited on a diamond-based Attenuated Total Reflectance (ATR) cell were interacted with (0.01, 0.1, 1 and 5M) NaCl solutions, and then frozen to -10˚ C. The resulting frozen montmorillonites pastes were then probed by ATR Fourier Transform Infrared (FTIR) spectroscopy, which is a highly sensitive technique for probing hydrogen bonding in minerals and water. Our results on Na-montmorillonite showed that hydrohalite, with its characteristic O-H stretching (νOH ˜ 3245-3265, 3408, 3462, 3555 cm-1) and bending (δOH ˜ 1614 and 1641 cm-1) bands, formed from solutions of at least 0.1 M NaCl, yet well below the typical homogeneous crystallization of this phase from pure aqueous solutions.[3] Further analysis of the O-H stretching and silicate (νSi-O ˜1000 cm-1) regions of frozen paste of montmorillonites revealed that hydrohalite formed within interlayers and at surfaces of Na-montmorillonite. Ca-montmorillonite did not, on the other hand, promote hydrohalite formation but did undergo Ca2+/Na+ ion exchange due to exposure of the NaCl solutions. Given the inability of Ca

An Approach to Assess Delamination Propagation Simulation Capabilities in Commercial Finite Element Codes

NASA Technical Reports Server (NTRS)

Krueger, Ronald

2008-01-01

An approach for assessing the delamination propagation simulation capabilities in commercial finite element codes is presented and demonstrated. For this investigation, the Double Cantilever Beam (DCB) specimen and the Single Leg Bending (SLB) specimen were chosen for full three-dimensional finite element simulations. First, benchmark results were created for both specimens. Second, starting from an initially straight front, the delamination was allowed to propagate. The load-displacement relationship and the total strain energy obtained from the propagation analysis results and the benchmark results were compared and good agreements could be achieved by selecting the appropriate input parameters. Selecting the appropriate input parameters, however, was not straightforward and often required an iterative procedure. Qualitatively, the delamination front computed for the DCB specimen did not take the shape of a curved front as expected. However, the analysis of the SLB specimen yielded a curved front as was expected from the distribution of the energy release rate and the failure index across the width of the specimen. Overall, the results are encouraging but further assessment on a structural level is required.

Fibroblast Growth Factor 23 and Kidney Disease Progression in Autosomal Dominant Polycystic Kidney Disease.

PubMed

Chonchol, Michel; Gitomer, Berenice; Isakova, Tamara; Cai, Xuan; Salusky, Isidro; Pereira, Renata; Abebe, Kaleab; Torres, Vicente; Steinman, Theodor I; Grantham, Jared J; Chapman, Arlene B; Schrier, Robert W; Wolf, Myles

2017-09-07

Increases in fibroblast growth factor 23 precede kidney function decline in autosomal dominant polycystic kidney disease; however, the role of fibroblast growth factor 23 in autosomal dominant polycystic kidney disease has not been well characterized. We measured intact fibroblast growth factor 23 levels in baseline serum samples from 1002 participants in the HALT-PKD Study A ( n =540; mean eGFR =91±17 ml/min per 1.73 m 2 ) and B ( n =462; mean eGFR =48±12 ml/min per 1.73 m 2 ). We used linear mixed and Cox proportional hazards models to test associations between fibroblast growth factor 23 and eGFR decline, percentage change in height-adjusted total kidney volume, and composite of time to 50% reduction in eGFR, onset of ESRD, or death. Median (interquartile range) intact fibroblast growth factor 23 was 44 (33-56) pg/ml in HALT-PKD Study A and 69 (50-93) pg/ml in Study B. In adjusted models, annualized eGFR decline was significantly faster in the upper fibroblast growth factor 23 quartile (Study A: quartile 4, -3.62; 95% confidence interval, -4.12 to -3.12 versus quartile 1, -2.51; 95% confidence interval, -2.71 to -2.30 ml/min per 1.73 m 2 ; P for trend <0.001; Study B: quartile 4, -3.74; 95% confidence interval, -4.14 to -3.34 versus quartile 1, -2.78; 95% confidence interval, -2.92 to -2.63 ml/min per 1.73 m 2 ; P for trend <0.001). In Study A, higher fibroblast growth factor 23 quartiles were associated with greater longitudinal percentage increase in height-adjusted total kidney volume in adjusted models (quartile 4, 6.76; 95% confidence interval, 5.57 to 7.96 versus quartile 1, 6.04; 95% confidence interval, 5.55 to 6.54; P for trend =0.03). In Study B, compared with the lowest quartile, the highest fibroblast growth factor 23 quartile was associated with elevated risk for the composite outcome (hazard ratio, 3.11; 95% confidence interval, 1.84 to 5.25). Addition of fibroblast growth factor 23 to a model of annualized decline in eGFR≥3.0 ml/min per 1.73 m

Simulation of Delamination Propagation in Composites Under High-Cycle Fatigue by Means of Cohesive-Zone Models

NASA Technical Reports Server (NTRS)

Turon, Albert; Costa, Josep; Camanho, Pedro P.; Davila, Carlos G.

2006-01-01

A damage model for the simulation of delamination propagation under high-cycle fatigue loading is proposed. The basis for the formulation is a cohesive law that links fracture and damage mechanics to establish the evolution of the damage variable in terms of the crack growth rate dA/dN. The damage state is obtained as a function of the loading conditions as well as the experimentally-determined coefficients of the Paris Law crack propagation rates for the material. It is shown that by using the constitutive fatigue damage model in a structural analysis, experimental results can be reproduced without the need of additional model-specific curve-fitting parameters.

Identification of delaminations in composite: structural health monitoring software based on spectral estimation and hierarchical genetic algorithm

NASA Astrophysics Data System (ADS)

Nag, A.; Mahapatra, D. Roy; Gopalakrishnan, S.

2003-10-01

A hierarchical Genetic Algorithm (GA) is implemented in a high peformance spectral finite element software for identification of delaminations in laminated composite beams. In smart structural health monitoring, the number of delaminations (or any other modes of damage) as well as their locations and sizes are no way completely known. Only known are the healthy structural configuration (mass, stiffness and damping matrices updated from previous phases of monitoring), sensor measurements and some information about the load environment. To handle such enormous complexity, a hierarchical GA is used to represent heterogeneous population consisting of damaged structures with different number of delaminations and their evolution process to identify the correct damage configuration in the structures under monitoring. We consider this similarity with the evolution process in heterogeneous population of species in nature to develop an automated procedure to decide on what possible damaged configuration might have produced the deviation in the measured signals. Computational efficiency of the identification task is demonstrated by considering a single delamination. The behavior of fitness function in GA, which is an important factor for fast convergence, is studied for single and multiple delaminations. Several advantages of the approach in terms of computational cost is discussed. Beside tackling different other types of damage configurations, further scope of research for development of hybrid soft-computing modules are highlighted.

On a generalized laminate theory with application to bending, vibration, and delamination buckling in composite laminates

DOE Office of Scientific and Technical Information (OSTI.GOV)

Barbero, E.J.

1989-01-01

In this study, a computational model for accurate analysis of composite laminates and laminates with including delaminated interfaces is developed. An accurate prediction of stress distributions, including interlaminar stresses, is obtained by using the Generalized Laminate Plate Theory of Reddy in which layer-wise linear approximation of the displacements through the thickness is used. Analytical as well as finite-element solutions of the theory are developed for bending and vibrations of laminated composite plates for the linear theory. Geometrical nonlinearity, including buckling and postbuckling are included and used to perform stress analysis of laminated plates. A general two dimensional theory of laminatedmore » cylindrical shells is also developed in this study. Geometrical nonlinearity and transverse compressibility are included. Delaminations between layers of composite plates are modelled by jump discontinuity conditions at the interfaces. The theory includes multiple delaminations through the thickness. Geometric nonlinearity is included to capture layer buckling. The strain energy release rate distribution along the boundary of delaminations is computed by a novel algorithm. The computational models presented herein are accurate for global behavior and particularly appropriate for the study of local effects.« less

From underplating to delamination-retreat in the northern Apennines

NASA Astrophysics Data System (ADS)

Chiarabba, C.; Giacomuzzi, G.; Bianchi, I.; Agostinetti, N. P.; Park, J.

2014-10-01

Recordings of teleseismic earthquakes from a dense set of temporary and permanent broadband seismic stations reveal the lithospheric structure of the northern Apennines and support the scenario of a retreating detachment within the mid-crust. Lithospheric delamination appears crucial to the formation and evolution of the Apennines orogen. Receiver-function (RF) stacks outline a continuous west-dipping Ps converted phase from a positive velocity jump that we interpret as the top of the lower crust and mantle of the Adria continental lithosphere, which is descending into the shallow mantle. The correlation of seismicity with two RF profiles across the northern Apennines suggests distinct stages of lithospheric delamination. Active penetration of the detachment into the Adria lithosphere seems evident in the south/east, with induced shallow-mantle flow facilitated by slab dehydration. Penetration of the detachment in the north/west seems to have arrested, and is possibly marked by crustal underplating. This layer atop the Apennines slab is visible only down to 80 km depth and suspends above an oppositely-dipping paired positive/negative Ps converted phase in stacked receiver functions. The break in the west-dipping Adria lithosphere conflicts with a westward-subduction scenario continuous from the Oligocene. Lateral changes of deep structure and seismicity along the northern Apennines suggest that underplating of crustal material and delamination-retreat are distinct mechanisms active today in the western and eastern sectors, respectively, of the northern Apennines. Negative Ps-pulses at 100-120 km depth help to define a seismic lithosphere-asthenosphere boundary (LAB), but cross-cut a volume of high-velocity mantle rock, as inferred from tomographic models. We hypothesize that this seismic LAB is a rheological discontinuity that affects the frequency band of seismic body waves, but not the long-term viscous response that governs the evolution and eventual detachment

Modeling the Effects of Beam Size and Flaw Morphology on Ultrasonic Pulse/Echo Sizing of Delaminations in Carbon Composites

NASA Technical Reports Server (NTRS)

Margetan, Frank J.; Leckey, Cara A.; Barnard, Dan

2012-01-01

The size and shape of a delamination in a multi-layered structure can be estimated in various ways from an ultrasonic pulse/echo image. For example the -6dB contours of measured response provide one simple estimate of the boundary. More sophisticated approaches can be imagined where one adjusts the proposed boundary to bring measured and predicted UT images into optimal agreement. Such approaches require suitable models of the inspection process. In this paper we explore issues pertaining to model-based size estimation for delaminations in carbon fiber reinforced laminates. In particular we consider the influence on sizing when the delamination is non-planar or partially transmitting in certain regions. Two models for predicting broadband sonic time-domain responses are considered: (1) a fast "simple" model using paraxial beam expansions and Kirchhoff and phase-screen approximations; and (2) the more exact (but computationally intensive) 3D elastodynamic finite integration technique (EFIT). Model-to-model and model-to experiment comparisons are made for delaminations in uniaxial composite plates, and the simple model is then used to critique the -6dB rule for delamination sizing.

High acidity unilamellar zeolite MCM-56 and its pillared and delaminated derivatives.

PubMed

Gil, Barbara; Makowski, Wacław; Marszalek, Bartosz; Roth, Wieslaw J; Kubu, Martin; Čejka, Jiři; Olejniczak, Zbigniew

2014-07-21

The unilamellar form of zeolite MWW, MCM-56, which is obtained by direct hydrothermal synthesis has been studied with regard to acidity and porosity in its original and post-synthesis modified pillared and delaminated forms. The acidity measured by FTIR was found to be only slightly lower than the highly active 3-D MWW forms, MCM-22 and MCM-49. Pivalonitrile adsorption, which is a measure of spatial openness, showed 50% accessibility vs. <30% for MCM-22/49. It highlights the potential of MCM-56 as a layered material with increased access to acid sites because it does not entail laborious post-synthesis modification. Swelling, pillaring and delamination of MCM-56 are facile but result in a reduction in the number of Brønsted acid sites (BAS) while increasing accessibility to pivalonitrile. The delamination procedure involving sonication and acidification of the highly basic mother liquor produces the most visible increase in surface area and access to all BAS. The accompanying doubling of the solid yield and the decrease in absolute number of BAS suggest significant precipitation of dissolved silica generated during swelling and sonication in high pH medium. The viability of separating surfactant covered layers upon sonication with the consequence of exposing hydrophobic hydrocarbon tails to aqueous environment is addressed.

The control of apical dominance: localization of the growth region of the Pharbitis nil shoot

NASA Technical Reports Server (NTRS)

Prasad, T. K.; Cline, M. G.

1986-01-01

The growing region of the upright Pharbitis nil shoot extends over a distance 13 cm basipetal to the shoot apex. When the shoot is inverted, ethylene production in this region is greatly enhanced whereas stem elongation is significantly inhibited. This growth region is ethylene-sensitive and the restriction of its growth by shoot inversion-induced ethylene may mediate the release of apical dominance.

An Interface Damage Model for the Simulation of Delamination Under Variable-Mode Ratio in Composite Materials

NASA Technical Reports Server (NTRS)

Turon, Albert; Camanho, Pedro P.; Costa, Josep; Davila, Carlos G.

2004-01-01

A thermodynamically consistent damage model for the simulation of progressive delamination under variable mode ratio is presented. The model is formulated in the context of the Damage Mechanics (DM). The constitutive equations that result from the variation of the free energy with damage are used to model the initiation and propagation of delamination. A new delamination initiation criterion is developed to assure that the formulation can account for changes in the loading mode in a thermodynamically consistent way. Interfacial penetration of two adjacent layers after complete decohesion is prevented by the formulation of the free energy. The model is implemented into the commercial finite element code ABAQUS by means of a user-written decohesion element. Finally, the numerical predictions given by the model are compared with experimental results.

Floating Node Method and Virtual Crack Closure Technique for Modeling Matrix Cracking-Delamination Interaction

NASA Technical Reports Server (NTRS)

DeCarvalho, N. V.; Chen, B. Y.; Pinho, S. T.; Baiz, P. M.; Ratcliffe, J. G.; Tay, T. E.

2013-01-01

A novel approach is proposed for high-fidelity modeling of progressive damage and failure in composite materials that combines the Floating Node Method (FNM) and the Virtual Crack Closure Technique (VCCT) to represent multiple interacting failure mechanisms in a mesh-independent fashion. In this study, the approach is applied to the modeling of delamination migration in cross-ply tape laminates. Delamination, matrix cracking, and migration are all modeled using fracture mechanics based failure and migration criteria. The methodology proposed shows very good qualitative and quantitative agreement with experiments.

Floating Node Method and Virtual Crack Closure Technique for Modeling Matrix Cracking-Delamination Migration

NASA Technical Reports Server (NTRS)

DeCarvalho, Nelson V.; Chen, B. Y.; Pinho, Silvestre T.; Baiz, P. M.; Ratcliffe, James G.; Tay, T. E.

2013-01-01

A novel approach is proposed for high-fidelity modeling of progressive damage and failure in composite materials that combines the Floating Node Method (FNM) and the Virtual Crack Closure Technique (VCCT) to represent multiple interacting failure mechanisms in a mesh-independent fashion. In this study, the approach is applied to the modeling of delamination migration in cross-ply tape laminates. Delamination, matrix cracking, and migration are all modeled using fracture mechanics based failure and migration criteria. The methodology proposed shows very good qualitative and quantitative agreement with experiments.

A new multi-layer approach for progressive damage simulation in composite laminates based on isogeometric analysis and Kirchhoff-Love shells. Part I: basic theory and modeling of delamination and transverse shear

NASA Astrophysics Data System (ADS)

Bazilevs, Y.; Pigazzini, M. S.; Ellison, A.; Kim, H.

2017-11-01

In this two-part paper we introduce a new formulation for modeling progressive damage in laminated composite structures. We adopt a multi-layer modeling approach, based on Isogeometric Analysis (IGA), where each ply or lamina is represented by a spline surface, and modeled as a Kirchhoff-Love thin shell. Continuum Damage Mechanics is used to model intralaminar damage, and a new zero-thickness cohesive-interface formulation is introduced to model delamination as well as permitting laminate-level transverse shear compliance. In Part I of this series we focus on the presentation of the modeling framework, validation of the framework using standard Mode I and Mode II delamination tests, and assessment of its suitability for modeling thick laminates. In Part II of this series we focus on the application of the proposed framework to modeling and simulation of damage in composite laminates resulting from impact. The proposed approach has significant accuracy and efficiency advantages over existing methods for modeling impact damage. These stem from the use of IGA-based Kirchhoff-Love shells to represent the individual plies of the composite laminate, while the compliant cohesive interfaces enable transverse shear deformation of the laminate. Kirchhoff-Love shells give a faithful representation of the ply deformation behavior, and, unlike solids or traditional shear-deformable shells, do not suffer from transverse-shear locking in the limit of vanishing thickness. This, in combination with higher-order accurate and smooth representation of the shell midsurface displacement field, allows us to adopt relatively coarse in-plane discretizations without sacrificing solution accuracy. Furthermore, the thin-shell formulation employed does not use rotational degrees of freedom, which gives additional efficiency benefits relative to more standard shell formulations.

Delamination failure of multilaminated adhesively bonded joints at low temperatures

NASA Astrophysics Data System (ADS)

Lee, Chi-Seung; Chun, Min-Sung; Kim, Myung-Hyun; Lee, Jae-Myung

2011-08-01

A series of experimental investigations of multilaminated joints adhesively bonded by epoxy/polyurethane (PU) glue were conducted in order to examine the delamination failure characteristics under in-plane shear loading at low temperatures. In order to observe these phenomena, a series of lap-shear tests were carried out at various low temperatures (20 °C, -110 °C and -163 °C) and various adhesion areas (15 mm × 50 mm, 30 mm × 50 mm, 50 mm × 50 mm, 75 mm × 50 mm and 100 mm × 50 mm). The test results were used to investigate the delamination and material characteristics, as well as the material properties, e.g., ultimate shear stress and shear elongation. Furthermore, the dependencies of the characteristics of multilaminated adhesively bonded joints (MABJs) on temperature and adhesion area was analyzed using the stress-strain relationship, and closed form formulas that are functions of the dependent parameters are proposed.

Potential-Induced Degradation-Delamination Mode in Crystalline Silicon Modules: Preprint

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hacke, Peter L; Kempe, Michael D; Wohlgemuth, John

A test sequence producing potential-induced degradation-delamination (PID-d) in crystalline silicon modules has been tested and found comparable under visual inspection to cell/encapsulant delamination seen in some fielded modules. Four commercial modules were put through this sequence, 85 degrees C, 85%, 1000 h damp heat, followed by an intensive PID stress sequence of 72 degrees C, 95% RH, and -1000 V, with the module face grounded using a metal foil. The 60 cell c-Si modules exhibiting the highest current transfer (4.4 center dot 10-4 A) exhibited PID-d at the first inspection after 156 h of PID stress. Effects promoting PID-d aremore » reduced adhesion caused by damp heat, sodium migration further reducing adhesion to the cells, and gaseous products of electrochemical reactions driven by the applied system voltage. A new work item proposal for an IEC test standard to evaluate for PID-d is anticipated.« less

Biophysical controls on soil respiration in the dominant patch types of an old-growth, mixed-conifer forest

Treesearch

Siyan Ma; Jiquan Chen; John R. Butnor; Malcolm North; Eugénie S. Euskirchen; Brian Oakley

2005-01-01

Little is known about biophysical controls on soil respiration in California's Sierra Nevada old-growth, mixed-conifer forests. Using portable and automated soil respiration sampling units, we measured soil respiration rate (SRR) in three dominant patch types: closed canopy (CC), ceanothus-dominated patches (CECO), and open canopy (OC). SRR varied significantly...

Finite element modeling of laminated composite plates with locally delaminated interface subjected to impact loading.

PubMed

Abo Sabah, Saddam Hussein; Kueh, Ahmad Beng Hong

2014-01-01

This paper investigates the effects of localized interface progressive delamination on the behavior of two-layer laminated composite plates when subjected to low velocity impact loading for various fiber orientations. By means of finite element approach, the laminae stiffnesses are constructed independently from their interface, where a well-defined virtually zero-thickness interface element is discreetly adopted for delamination simulation. The present model has the advantage of simulating a localized interfacial condition at arbitrary locations, for various degeneration areas and intensities, under the influence of numerous boundary conditions since the interfacial description is expressed discretely. In comparison, the model shows good agreement with existing results from the literature when modeled in a perfectly bonded state. It is found that as the local delamination area increases, so does the magnitude of the maximum displacement history. Also, as top and bottom fiber orientations deviation increases, both central deflection and energy absorption increase although the relative maximum displacement correspondingly decreases when in contrast to the laminates perfectly bonded state.

Laser Structuring of Thin Layers for Flexible Electronics by a Shock Wave-induced Delamination Process

NASA Astrophysics Data System (ADS)

Lorenz, Pierre; Ehrhardt, Martin; Zimmer, Klaus

The defect-free laser-assisted structuring of thin films on flexible substrates is a challenge for laser methods. However, solving this problem exhibits an outstanding potential for a pioneering development of flexible electronics. Thereby, the laser-assisted delamination method has a great application potential. At the delamination process: the localized removal of the layer is induced by a shock wave which is produced by a laser ablation process on the rear side of the substrate. In this study, the thin-film patterning process is investigated for different polymer substrates dependent on the material and laser parameters using a KrF excimer laser. The resultant structures were studied by optical microscopy and white light interferometry (WLI). The delamination process was tested at different samples (indium tin oxide (ITO) on polyethylene terephthalate (PET), epoxy-based negative photoresist (SU8) on polyimide (PI) and indium tin oxide/copper indium gallium selenide/molybdenum (ITO/CIGS/Mo) on PI.

Application of guided acoustic waves to delamination detection

NASA Technical Reports Server (NTRS)

Sun, Keun J.

1992-01-01

Guided plate waves are able to interact with structural flaws such as delaminations and cracks due to their propagation properties highly sensitive to the thickness change in materials. A technique which employs an acoustic damper to probe the results of this interaction and then to locate flaws in a relatively short period of time is developed. With its technical advantages, this technique shows its potential application to large area structural integrity assessment.

Residual thermal and moisture influences on the strain energy release rate analysis of local delaminations from matrix cracks

NASA Technical Reports Server (NTRS)

Obrien, T. K.

1991-01-01

An analysis utilizing laminated plate theory is developed to calculate the strain energy release rate associated with local delaminations originating at off-axis, single ply, matrix cracks in laminates subjected to uniaxial loads. The analysis includes the contribution of residual thermal and moisture stresses to the strain energy released. Examples are calculated for the strain energy release rate associated with local delaminations originating at 90 degrees and angle-ply (non-90 degrees) matrix ply cracks in glass epoxy and graphite epoxy laminates. The solution developed may be used to assess the relative contribution of mechanical, residual thermal, and moisture stresses on the strain energy release rate for local delamination for a variety of layups and materials.

3-D Mixed Mode Delamination Fracture Criteria - An Experimentalist's Perspective

NASA Technical Reports Server (NTRS)

Reeder, James R.

2006-01-01

Many delamination failure criteria based on fracture toughness have been suggested over the past few decades, but most only covered the region containing mode I and mode II components of loading because that is where toughness data existed. With new analysis tools, more 3D analyses are being conducted that capture a mode III component of loading. This has increased the need for a fracture criterion that incorporates mode III loading. The introduction of a pure mode III fracture toughness test has also produced data on which to base a full 3D fracture criterion. In this paper, a new framework for visualizing 3D fracture criteria is introduced. The common 2D power law fracture criterion was evaluated to produce unexpected predictions with the introduction of mode III and did not perform well in the critical high mode I region. Another 2D criterion that has been shown to model a wide range of materials well was used as the basis for a new 3D criterion. The new criterion is based on assumptions that the relationship between mode I and mode III toughness is similar to the relation between mode I and mode II and that a linear interpolation can be used between mode II and mode III. Until mixed-mode data exists with a mode III component of loading, 3D fracture criteria cannot be properly evaluated, but these assumptions seem reasonable.

Size- and food-dependent growth drives patterns of competitive dominance along productivity gradients.

PubMed

Huss, Magnus; Gårdmark, Anna; Van Leeuwen, Anieke; de Roos, André M

2012-04-01

Patterns of coexistence among competing species exhibiting size- and food-dependent growth remain largely unexplored. Here we studied mechanisms behind coexistence and shifts in competitive dominance in a size-structured fish guild, representing sprat and herring stocks in the Baltic Sea, using a physiologically structured model of competing populations. The influence of degree of resource overlap and the possibility of undergoing ontogenetic diet shifts were studied as functions of zooplankton and zoobenthos productivity. By imposing different size-dependent mortalities, we could study the outcome of competition under contrasting environmental regimes representing poor and favorable growth conditions. We found that the identity of the dominant species shifted between low and high productivity. Adding a herring-exclusive benthos resource only provided a competitive advantage over sprat when size-dependent mortality was high enough to allow for rapid growth in the zooplankton niche. Hence, the importance of a bottom-up effect of varying productivity was dependent on a strong top-down effect. Although herring could depress shared resources to lower levels than could sprat and also could access an exclusive resource, the smaller size at maturation of sprat allowed it to coexist with herring and, in some cases, exclude it. Our model system, characterized by interactions among size cohorts, allowed for consumer coexistence even at full resource overlap at intermediate productivities when size-dependent mortality was low. Observed shifts in community patterns were crucially dependent on the explicit consideration of size- and food-dependent growth. Accordingly, we argue that accounting for food-dependent growth and size-dependent interactions is necessary to better predict changes in community structure and dynamics following changes in major ecosystem drivers such as resource productivity and mortality, which are fundamental for our ability to manage exploitation of

Normal growth and development in the absence of hepatic insulin-like growth factor I

PubMed Central

Yakar, Shoshana; Liu, Jun-Li; Stannard, Bethel; Butler, Andrew; Accili, Domenici; Sauer, Brian; LeRoith, Derek

1999-01-01

The somatomedin hypothesis proposed that insulin-like growth factor I (IGF-I) was a hepatically derived circulating mediator of growth hormone and is a crucial factor for postnatal growth and development. To reassess this hypothesis, we have used the Cre/loxP recombination system to delete the igf1 gene exclusively in the liver. igf1 gene deletion in the liver abrogated expression of igf1 mRNA and caused a dramatic reduction in circulating IGF-I levels. However, growth as determined by body weight, body length, and femoral length did not differ from wild-type littermates. Although our model proves that hepatic IGF-I is indeed the major contributor to circulating IGF-I levels in mice it challenges the concept that circulating IGF-I is crucial for normal postnatal growth. Rather, our model provides direct evidence for the importance of the autocrine/paracrine role of IGF-I. PMID:10377413

Delamination Fracture in Graphite/Epoxy Materials.

DTIC Science & Technology

1986-06-01

stress fields for the two loading conditions. Figures 7-10 indicate the results of a finite element analysis % for the test coupons loaded in mode I and...results somewhat approximate, the difference in the shape of the Srespective stress fields and the different rates of decay of the _ stress fields...Shear deformation is dominant feature .: observed. 1000x (all). 7. ay stress contour plot of split laminate beam tested under . mode I conditions. 8

Impaired growth in Rabson-Mendenhall syndrome: lack of effect of growth hormone and insulin-like growth factor-I.

PubMed

Longo, N; Singh, R; Griffin, L D; Langley, S D; Parks, J S; Elsas, L J

1994-09-01

Mutations in the insulin receptor gene cause the severe insulin-resistant syndromes leprechaunism and Rabson-Mendenhall syndrome. There is no accepted therapy for these inherited conditions. Here we report the results of recombinant human GH (rhGH) and recombinant human insulin-like growth factor-I (rhIGF-I) treatment of a male patient, Atl-2, with Rabson-Mendenhall syndrome. The patient was small for gestational age, had premature dentition, absence of sc fat, acanthosis nigricans, fasting hypoglycemia and postprandial hyperglycemia, and extremely high concentrations of circulating insulin (up to 8500 microU/mL). Fibroblasts and lymphoblasts established from this patient had reduced insulin binding, which was 20-30% of the control value. Binding of epidermal growth factor, IGF-I, and GH to the patient's fibroblasts was normal. The growth of fibroblasts cultured from patient Atl-2 in vitro was intermediate between that of fibroblasts from patients with leprechaunism and control values. The patient's growth curve in vivo was far below the fifth percentile despite adequate nutrition. To stimulate growth, therapy with rhGH was initiated, the rationale being to stimulate hepatic IGF-I production and IGF-I receptor signaling, and bypass the inherited block in insulin receptor signaling. Therapy with rhGH (up to 0.5 mg/kg.week) did not improve growth and failed to increase the levels of circulating IGF-I and IGF-binding protein-3 over a 14-month period. As rhGH could not stimulate growth, rhIGF-I (up to 100 micrograms/kg.day) was given by daily sc injection. No increase in growth velocity was observed over a 14-month period. These results indicate that both GH and IGF-I fail to correct growth in a patient with severe inherited insulin resistance. The lack of efficacy of IGF-I treatment may be related to multiple factors, such as the poor metabolic state of the patient, the deficiency of serum carrier protein for IGF-I, an increased clearance of the growth factor, IGF-I

Feedback amplification loop drives malignant growth in epithelial tissues.

PubMed

Muzzopappa, Mariana; Murcia, Lada; Milán, Marco

2017-08-29

Interactions between cells bearing oncogenic mutations and the surrounding microenvironment, and cooperation between clonally distinct cell populations, can contribute to the growth and malignancy of epithelial tumors. The genetic techniques available in Drosophila have contributed to identify important roles of the TNF-α ligand Eiger and mitogenic molecules in mediating these interactions during the early steps of tumor formation. Here we unravel the existence of a tumor-intrinsic-and microenvironment-independent-self-reinforcement mechanism that drives tumor initiation and growth in an Eiger-independent manner. This mechanism relies on cell interactions between two functionally distinct cell populations, and we present evidence that these cell populations are not necessarily genetically different. Tumor-specific and cell-autonomous activation of the tumorigenic JNK stress-activated pathway drives the expression of secreted signaling molecules and growth factors to delaminating cells, which nonautonomously promote proliferative growth of the partially transformed epithelial tissue. We present evidence that cross-feeding interactions between delaminating and nondelaminating cells increase each other's sizes and that these interactions can explain the unlimited growth potential of these tumors. Our results will open avenues toward our molecular understanding of those social cell interactions with a relevant function in tumor initiation in humans.

Minimizing and predicting delamination of southern plywood in exterior exposure

Treesearch

Peter Koch

1967-01-01

Southern pine plywood is substantially all being manufactured with phenolic glue for exterior use. Because panels must not delaminate in service, a reliable predictor of glueline durability is required. Drawing on the experience of the Douglas-fir plywood industry, southern manufacutrers have adopted as a predictor the percentage of wood failure(% WF) observed in...

Insulin-like growth factor-I and insulin-like growth factor binding protein-3 cotreatment versus insulin-like growth factor-I alone in two brothers with growth hormone insensitivity syndrome: effects on insulin sensitivity, body composition and linear growth.

PubMed

Ekström, Klas; Carlsson-Skwirut, Christine; Ritzén, E Martin; Bang, Peter

2011-01-01

Growth hormone insensitivity syndrome (GHIS) is caused by a defective growth hormone receptor (GHR) and is associated with insulin-like growth factor-I (IGF-I) deficiency, severely short stature and, from adolescence, fasting hyperglycemia and obesity. We studied the effects of treatment with IGF-I in either a 1:1 molar complex with IGFBP-3 (IGF-I/BP-3-Tx) or with IGF-I alone (IGF-I-Tx) on metabolism and linear growth. Two brothers, compound heterozygous for a GHR gene defect, were studied. After 8 months without treatment, we examined the short- and long-term effects of IGF-I/BP-3-Tx and, subsequently, IGF-I-Tx on 12-hour overnight levels of IGF-I, GH, insulin, IGFBP-1, insulin sensitivity by hyperinsulinemic euglycemic clamp, body composition by dual-energy X-ray absorptiometry and linear growth. Mean overnight levels of insulin decreased and IGFBP-1, a measure of hepatic insulin sensitivity, increased on both regimens, but was more pronounced on IGF-I-Tx. Insulin sensitivity by clamp showed no consistent changes. Lean body mass increased and abdominal fat mass decreased in both subjects on IGF-I-Tx. However, the changes were inconsistent during IGF-I/BP-3-Tx. Height velocity was low without treatment, increased slightly on IGF-I/BP-3-Tx and doubled on IGF-I-Tx. Both modalities of IGF-I improved determinants of hepatic insulin sensitivity, body composition and linear growth rate; however, IGF-I alone seemed to be more efficient. Copyright © 2011 S. Karger AG, Basel.

Growth hormone transgenesis does not influence territorial dominance or growth and survival of first-feeding Atlantic salmon Salmo salar in food-limited stream microcosms.

PubMed

Moreau, D T R; Fleming, I A; Fletcher, G L; Brown, J A

2011-03-01

This study explored the relative competitive ability and performance of first-feeding growth hormone (GH) transgenic and non-transgenic Atlantic salmon Salmo salar fry under low food conditions. Pair-wise dominance trials indicated a strong competitive advantage for residents of a contested foraging territory. Transgenic and non-transgenic individuals, however, were equally likely to be dominant. Similarly, in stream environments with limited food, the transgene did not influence the growth in mass or survival at high or low fry densities. Fry in low-density treatments, however, performed better than fry in high-density treatments. These results indicate that, under the environment examined, the growth performance of GH-transgenic and non-transgenic S. salar may be similar during first feeding, an intense period of selection in their life history. Similarities in competitive ability and growth performance with wild-type fish suggest that the capacity of transgenic S. salar to establish in natural streams may not be inhibited during early life history. © 2011 The Authors. Journal of Fish Biology © 2011 The Fisheries Society of the British Isles.

Finite Element Modeling of Laminated Composite Plates with Locally Delaminated Interface Subjected to Impact Loading

PubMed Central

Abo Sabah, Saddam Hussein; Kueh, Ahmad Beng Hong

2014-01-01

This paper investigates the effects of localized interface progressive delamination on the behavior of two-layer laminated composite plates when subjected to low velocity impact loading for various fiber orientations. By means of finite element approach, the laminae stiffnesses are constructed independently from their interface, where a well-defined virtually zero-thickness interface element is discreetly adopted for delamination simulation. The present model has the advantage of simulating a localized interfacial condition at arbitrary locations, for various degeneration areas and intensities, under the influence of numerous boundary conditions since the interfacial description is expressed discretely. In comparison, the model shows good agreement with existing results from the literature when modeled in a perfectly bonded state. It is found that as the local delamination area increases, so does the magnitude of the maximum displacement history. Also, as top and bottom fiber orientations deviation increases, both central deflection and energy absorption increase although the relative maximum displacement correspondingly decreases when in contrast to the laminates perfectly bonded state. PMID:24696668

Delamination Mechanisms of Thermal and Environmental Barrier Coatings on SiC/SiC Ceramic Matrix Composites

NASA Technical Reports Server (NTRS)

Zhu, Dongming; Choi, Sung R.; Lee, Kang N.; Miller, Robert A.

2003-01-01

Advanced ceramic thermal harrier coatings will play an increasingly important role In future gas turbine engines because of their ability to effectively protect the engine components and further raise engine temperatures. However, the coating durability issue remains a major concern with the ever-increasing temperature requirements. In this paper, thermal cyclic response and delamination failure modes of a ZrO2-8wt%Y2O3 and mullite/BSAS thermaVenvironmenta1 barrier coating system on SiC/SiC ceramic matrix composites were investigated using a laser high-heat-flux technique. The coating degradation and delamination processes were monitored in real time by measuring coating apparent conductivity changes during the cyclic tests under realistic engine temperature and stress gradients, utilizing the fact that delamination cracking causes an apparent decrease in the measured thermal conductivity. The ceramic coating crack initiation and propagation driving forces under the cyclic thermal loads, in conjunction with the mechanical testing results, will be discussed.

Delamination Mechanisms of Thermal and Environmental Barrier Coatings on SiC/SiC Ceramic Matrix Composites

NASA Technical Reports Server (NTRS)

Zhu, Dongming; Choi, Sung R.; Lee, Kang N.; Miller, Robert A.

1990-01-01

Advanced ceramic thermal barrier coatings will play an increasingly important role in future gas turbine engines because of their ability to effectively protect the engine components and further raise engine temperatures. However, the coating durability issue remains a major concern with the ever-increasing temperature requirements. In this paper, thermal cyclic response and delamination failure modes of a ZrO2-8wt%Y2O3 and mullite/BSAS thermal/environmental barrier coating system on SiC/SiC ceramic matrix composites were investigated using a laser high-heat-flux technique. The coating degradation and delamination processes were monitored in real time by measuring coating apparent conductivity changes during the cyclic tests under realistic engine temperature and stress gradients, utilizing the fact that delamination cracking causes an apparent decrease in the measured thermal conductivity. The ceramic coating crack initiation and propagation driving forces under the cyclic thermal loads, in conjunction with the mechanical testing results, will be discussed.

Delamination Assessment Tool for Spacecraft Composite Structures

NASA Astrophysics Data System (ADS)

Portela, Pedro; Preller, Fabian; Wittke, Henrik; Sinnema, Gerben; Camanho, Pedro; Turon, Albert

2012-07-01

Fortunately only few cases are known where failure of spacecraft structures due to undetected damage has resulted in a loss of spacecraft and launcher mission. However, several problems related to damage tolerance and in particular delamination of composite materials have been encountered during structure development of various ESA projects and qualification testing. To avoid such costly failures during development, launch or service of spacecraft, launcher and reusable launch vehicles structures a comprehensive damage tolerance verification approach is needed. In 2009, the European Space Agency (ESA) initiated an activity called “Delamination Assessment Tool” which is led by the Portuguese company HPS Lda and includes academic and industrial partners. The goal of this study is the development of a comprehensive damage tolerance verification approach for launcher and reusable launch vehicles (RLV) structures, addressing analytical and numerical methodologies, material-, subcomponent- and component testing, as well as non-destructive inspection. The study includes a comprehensive review of current industrial damage tolerance practice resulting from ECSS and NASA standards, the development of new Best Practice Guidelines for analysis, test and inspection methods and the validation of these with a real industrial case study. The paper describes the main findings of this activity so far and presents a first iteration of a Damage Tolerance Verification Approach, which includes the introduction of novel analytical and numerical tools at an industrial level. This new approach is being put to the test using real industrial case studies provided by the industrial partners, MT Aerospace, RUAG Space and INVENT GmbH

Sheet on a deformable sphere: Wrinkle patterns suppress curvature-induced delamination

NASA Astrophysics Data System (ADS)

Hohlfeld, Evan; Davidovitch, Benny

2015-01-01

The adhesion of a stiff film onto a curved substrate often generates elastic stresses in the film that eventually give rise to its delamination. Here we predict that delamination of very thin films can be dramatically suppressed through tiny, smooth deformations of the substrate, dubbed here "wrinklogami," that barely affect the macro-scale topography. This "prolamination" effect reflects a surprising capability of smooth wrinkles to suppress compression in elastic films even when spherical or other doubly curved topography is imposed, in a similar fashion to origami folds that enable construction of curved structures from an unstretchable paper. We show that the emergence of a wrinklogami pattern signals a nontrivial isometry of the sheet to its planar, undeformed state, in the doubly asymptotic limit of small thickness and weak tensile load exerted by the adhesive substrate. We explain how such an "asymptotic isometry" concept broadens the standard usage of isometries for describing the response of elastic sheets to geometric constraints and mechanical loads.

Contribution to interplay between a delamination test and a sensory analysis of mid-range lipsticks.

PubMed

Richard, C; Tillé-Salmon, B; Mofid, Y

2016-02-01

Lipstick is currently one of the most sold products of cosmetics industry, and the competition between the various manufacturers is significant. Customers mainly seek products with high spreadability, especially long-lasting or long wear on the lips. Evaluation tests of cosmetics are usually performed by sensory analysis. This can then represent a considerable cost. The object of this study was to develop a fast and simple test of delamination (objective method with calibrated instruments) and to interplay the obtained results with those of a discriminative sensory analysis (subjective method) in order to show the relevance of the instrumental test. Three mid-range lipsticks were randomly chosen and were tested. They were made of compositions as described by the International Nomenclature of Cosmetic Ingredients (INCI). Instrumental characterization was performed by texture profile analysis and by a special delamination test. The sensory analysis was voluntarily conducted with an untrained panel as blind test to confirm or reverse the possible interplay. The two approaches or methods gave the same type of classification. The high-fat lipstick had the worst behaviour with the delamination test and the worst notation of the intensity of descriptors with the sensory analysis. There is a high correlation between the sensory analysis and the instrumental measurements in this study. The delamination test carried out should permit to quickly determine the lasting (screening test) and in consequence optimize the basic formula of lipsticks. © 2015 Society of Cosmetic Scientists and the Société Française de Cosmétologie.

Why large cells dominate estuarine phytoplankton

USGS Publications Warehouse

Cloern, James E.

2018-01-01

Surveys across the world oceans have shown that phytoplankton biomass and production are dominated by small cells (picoplankton) where nutrient concentrations are low, but large cells (microplankton) dominate when nutrient-rich deep water is mixed to the surface. I analyzed phytoplankton size structure in samples collected over 25 yr in San Francisco Bay, a nutrient-rich estuary. Biomass was dominated by large cells because their biomass selectively grew during blooms. Large-cell dominance appears to be a characteristic of ecosystems at the land–sea interface, and these places may therefore function as analogs to oceanic upwelling systems. Simulations with a size-structured NPZ model showed that runs of positive net growth rate persisted long enough for biomass of large, but not small, cells to accumulate. Model experiments showed that small cells would dominate in the absence of grazing, at lower nutrient concentrations, and at elevated (+5°C) temperatures. Underlying these results are two fundamental scaling laws: (1) large cells are grazed more slowly than small cells, and (2) grazing rate increases with temperature faster than growth rate. The model experiments suggest testable hypotheses about phytoplankton size structure at the land–sea interface: (1) anthropogenic nutrient enrichment increases cell size; (2) this response varies with temperature and only occurs at mid-high latitudes; (3) large-cell blooms can only develop when temperature is below a critical value, around 15°C; (4) cell size diminishes along temperature gradients from high to low latitudes; and (5) large-cell blooms will diminish or disappear where planetary warming increases temperature beyond their critical threshold.

Study on Fatigue Performance of Composite Bolted Joints with Bolt-Hole Delamination

NASA Astrophysics Data System (ADS)

Liu, M. J.; Yu, S.; Zhao, Q. Y.

2018-03-01

Fatigue performance of composite structure with imperfections is a challenging subject at present. Based on cohesive zone method and multi-continuum theory, delamination evolution response and fatigue life prediction of a 3D composite single-lap joint with a bolt-hole have been investigated through computer codes Abaqus and Fe-safe. Results from the comparison of a perfect composite bolted joint with another defect one indicates that a relatively small delamination damage around the bolt hole brings about significant degradation of local material performance. More notably, fatigue life of stress concentration region of composite bolted joints is highly sensitive to external loads, as an increase of 67% cyclic load amplitude leads to an decrease of 99.5% local fatigue life in this study. However, the numerical strategy for solving composite fatigue problems is meaningful to engineering works.

Delamination measurement of a laminates composite panel due to hole punching based on the focus variation technique

NASA Astrophysics Data System (ADS)

Abdullah, A. B.; Zain, M. S. M.; Abdullah, M. S.; Samad, Z.

2017-07-01

Structural materials, such as composite panels, must be assembled, and such panels are typically constructed via the insertion of a fastener through a drilled hole. The main problem encountered in drilling is delamination, which affects assembly strength. The cost of drilling is also high because of the severe wear on drill bits. The main goal of this research is to develop a new punching method as an alternative to drilling during hole preparation. In this study, the main objective is to investigate the effect of different puncher profiles on the quality of holes punched into carbon fiber reinforcement polymer (CFRP) composite panels. Six types of puncher profiles were fabricated with minimum die clearance (1%), and two quality aspects, namely, incomplete shearing and delamination factor, were measured. The conical puncher incurred the least defects in terms of delamination and yielded an acceptable amount of incomplete shearing in comparison with the other punchers.

Zr-doped TiO2 supported on delaminated clay materials for solar photocatalytic treatment of emerging pollutants.

PubMed

Belver, C; Bedia, J; Rodriguez, J J

2017-01-15

Solar light-active Zr-doped TiO 2 nanoparticles were successfully immobilized on delaminated clay materials by a one-step sol-gel route. Fixing the amount of TiO 2 at 65wt.%, this work studies the influence of Zr loading (up to 2%) on the photocatalytic activity of the resulting Zr-doped TiO 2 /clay materials. The structural characterization demonstrates that all samples were formed by a delaminated clay with nanostructured anatase assembled on its surface. The Zr dopant was successfully incorporated into the anatase lattice, resulting in a slight deformation of the anatase crystal and the reduction of the band gap. These materials exhibit high surface area with a disordered mesoporous structure formed by TiO 2 particles (15-20nm) supported on a delaminated clay. They were tested in the solar photodegradation of antipyrine, usually used as an analgesic drug and selected as an example of emerging pollutant. High degradation rates have been obtained at low antipyrine concentrations and high solar irradiation intensities with the Zr-doped TiO 2 /clay catalyst, more effective than the undoped one. This work demonstrates the potential application of the synthesis method for preparing novel and efficient solar-light photocatalysts based on metal-doped anatase and a delaminated clay. Copyright © 2016 Elsevier B.V. All rights reserved.

Selective role of bainitic lath boundary in influencing slip systems and consequent deformation mechanisms and delamination in high-strength low-alloy steel

NASA Astrophysics Data System (ADS)

Liu, S.; Li, X.; Guo, H.; Yang, S.; Wang, X.; Shang, C.; Misra, R. D. K.

2018-04-01

We elucidate here the deformation behaviour and delamination phenomenon in a high-strength low-alloy bainitic steel, in terms of microstructure, texture and stress evolution during deformation via in situ electron back-scattered diffraction and electron microscopy. Furthermore, the selective role of bainitic lath boundary on slip systems was studied in terms of dislocation pile-up and grain boundary energy models. During tensile deformation, the texture evolution was concentrated at {1 1 0}<1 1 1> and the laths were turn parallel to loading direction. The determining role of lath on the deformation behaviour is governed by length/thickness (l/t) ratio. When l/t > 28, the strain accommodates along the bainite lath rather than along the normal direction. The delamination crack initiated normal to (0 1 1) plane, and become inclined to (0 1 1) plane with continued strain along (0 1 1) plane and lath plane. This indicated that the delamination is not brittle process but plastic process. The lack of dimples at the delaminated surface is because of lack of strain normal to the direction of lath. The delaminated (0 1 1) planes were associated with cleavage along the (1 0 0) plane.

Insulin-like growth factor I gene deletion causing intrauterine growth retardation and severe short stature.

PubMed

Woods, K A; Camacho-Hübner, C; Barter, D; Clark, A J; Savage, M O

1997-11-01

The first human case of a homozygous molecular defect in the gene encoding insulin-like growth factor I (IGF-I) is described. The patient was a 15-year-old boy from a consanguineous pedigree who presented with severe intrauterine growth failure, sensorineural deafness and mild mental retardation. Endocrine evaluation of the growth hormone (GH)--IGF-I axis revealed elevated GH secretion, undetectable serum IGF-I and normal serum IGF-binding protein-3, acid-labile subunit, and GH-binding activity. Analysis of the IGF-I gene revealed a homozygous partial IGF-I gene deletion involving exons 4 and 5, which encodes a severely truncated mature IGF-I peptide. This patient demonstrates that complete disruption of the IGF-I gene in man is compatible with life, and indicates a major role for IGF-I in human fetal growth. In addition, his neurological abnormalities suggest that IGF-I may be involved in central nervous system development.

Predictions of Poisson's ratio in cross-ply laminates containing matrix cracks and delaminations

NASA Technical Reports Server (NTRS)

Harris, Charles E.; Allen, David H.; Nottorf, Eric W.

1989-01-01

A damage-dependent constitutive model for laminated composites has been developed for the combined damage modes of matrix cracks and delaminations. The model is based on the concept of continuum damage mechanics and uses second-order tensor valued internal state variables to represent each mode of damage. The internal state variables are defined as the local volume average of the relative crack face displacements. Since the local volume for delaminations is specified at the laminate level, the constitutive model takes the form of laminate analysis equations modified by the internal state variables. Model implementation is demonstrated for the laminate engineering modulus E(x) and Poisson's ratio nu(xy) of quasi-isotropic and cross-ply laminates. The model predictions are in close agreement to experimental results obtained for graphite/epoxy laminates.

Effect of Shear Deformation and Continuity on Delamination Modelling with Plate Elements

NASA Technical Reports Server (NTRS)

Glaessgen, E. H.; Riddell, W. T.; Raju, I. S.

1998-01-01

The effects of several critical assumptions and parameters on the computation of strain energy release rates for delamination and debond configurations modeled with plate elements have been quantified. The method of calculation is based on the virtual crack closure technique (VCCT), and models that model the upper and lower surface of the delamination or debond with two-dimensional (2D) plate elements rather than three-dimensional (3D) solid elements. The major advantages of the plate element modeling technique are a smaller model size and simpler geometric modeling. Specific issues that are discussed include: constraint of translational degrees of freedom, rotational degrees of freedom or both in the neighborhood of the crack tip; element order and assumed shear deformation; and continuity of material properties and section stiffness in the vicinity of the debond front, Where appropriate, the plate element analyses are compared with corresponding two-dimensional plane strain analyses.

Fractography of composite delamination

NASA Technical Reports Server (NTRS)

1988-01-01

Studies were made of the fractography of mode 2 delamination and the impact damage of carbon fiber reinforced polymer composites. Laminates fractured under mode 2 loading were potted in a clear epoxy polymer, sectioned and polished and examined using transmission and reflection light microscopy. There were only occasional fibers bridging the mode 2 cracks. These cracks were not always visible probably because the crack opening displacement was too small as to be resolved using light microscopy. A study was made of the effect of repetitive impacts on laminates of AS4/3501-6 and IM6/3501-6. Plots of cumulative impact energy vs cumulative absorbed energy exhibited a sharp change in slope which corresponded to the damage area reaching the edges of the specimen. The initial slope was highly reproducible for both composite materials. On the other hand, the intersection point between the two slopes, where the damage area reaches the specimen edges, was highly variable between specimens. This variability is tentatively ascribed to differences in laminate quality.

Assessing skeletal maturity by using blood spot insulin-like growth factor I (IGF-I) testing.

PubMed

Masoud, Mohamed; Masoud, Ibrahim; Kent, Ralph L; Gowharji, Nour; Cohen, Laurie E

2008-08-01

Accurate determination of skeletal maturity and remaining growth is crucial to many orthodontic, orthognathic, and dental-implant timing decisions. Cervical vertebral stages and hand-wrist radiographs are currently used to identify peak mandibular bone growth. These are highly subjective techniques that not only involve radiographic exposure but also lack the ability to determine the intensity of the growth spurt and the end of growth. Insulin-like growth factor I (IGF-I) is a circulating growth hormone-dependent factor whose level correlates with sexual maturity; it is used to diagnose growth hormone deficiency and excess. We hypothesized that IGF-I levels would also correlate with cervical skeletal maturity and would be highest at the cervical stages that correspond to the greatest amount of facial growth. We measured mean blood spot IGF-I levels in a cross-sectional study of 83 patients (44 female, 39 male) on recall to begin orthodontic treatment, in active treatment, or in posttreatment follow-up. Mean blood spot IGF-I levels were significantly higher in the late pubertal stages than in the prepubertal, early pubertal, and postpubertal stages. Linear correlation showed that IGF-I levels had a significant positive correlation with cervical skeletal maturity from the prepubertal to the late pubertal stages, and a significant negative correlation from the late pubertal to the postpubertal stages. In the postpubertal stage, IGF-I levels had a negative linear correlation with increasing time since the onset of puberty and with chronological age. Blood spot IGF-I could be used as a skeletal maturity indicator and might be useful in detecting residual mandibular growth in young adults.

A Three Dimensional Finite Element Analysis of Delamination Growth in Composite Laminates. I. The Energy Methods and Case-Study Problems.

DTIC Science & Technology

1983-09-01

34 2nd. Ed. McGraw Hill , New York, 1976, p. 419. [32] Odom, E. M. and Adams, D. E.,"A Study of Polymer Matrix Fatigue Proper- ties," NADC-TR-83053-60...Compression," Ph.D. Thesis, Drexel University, Phila- delphia, PA. 1984 . [34] Crossman, F. W., Warren, W. J . and Wang, A. S. D.,"Influence of Ply...II :2 3____ 4’ F-i7-E-i- 4S-57F* II 0. 1____ 10 ’ G , - I I ’ ’ " 2!___ I ! I I I I 1tILL II I hILL J l 0. 1 1 10 G, (in-lb/in ) Figure 18. Mixed

Development of a finite element based delamination analysis for laminates subject to extension, bending, and torsion

NASA Technical Reports Server (NTRS)

Hooper, Steven J.

1989-01-01

Delamination is a common failure mode of laminated composite materials. This type of failure frequently occurs at the free edges of laminates where singular interlaminar stresses are developed due to the difference in Poisson's ratios between adjacent plies. Typically the delaminations develop between 90 degree plies and adjacent angle plies. Edge delamination has been studied by several investigators using a variety of techniques. Recently, Chan and Ochoa applied the quasi-three-dimensional finite element model to the analysis of a laminate subject to bending, extension, and torsion. This problem is of particular significance relative to the structural integrity of composite helicopter rotors. The task undertaken was to incorporate Chan and Ochoa's formulation into a Raju Q3DG program. The resulting program is capable of modeling extension, bending, and torsional mechanical loadings as well as thermal and hygroscopic loadings. The addition of the torsional and bending loading capability will provide the capability to perform a delamination analysis of a general unsymmetric laminate containing four cracks, each of a different length. The solutions obtained using this program are evaluated by comparing them with solutions from a full three-dimensional finite element solution. This comparison facilitates the assessment of three dimensional affects such as the warping constraint imposed by the load frame grips. It wlso facilitates the evaluation of the external load representation employed in the Q3D formulation. Finally, strain energy release rates computed from the three-dimensional results are compared with those predicted using the quasi-three-dimensional formulation.

Wave energy trapping and localization in a plate with a delamination

NASA Astrophysics Data System (ADS)

Glushkov, Evgeny; Glushkova, Natalia; Golub, Mikhail V.; Moll, Jochen; Fritzen, Claus-Peter

2012-12-01

The research aims at an experimental approval of the trapping mode effect theoretically predicted for an elastic plate-like structure with a horizontal crack. The effect is featured by a sharp capture of incident wave energy at certain resonance frequencies with its localization between the crack and plate surfaces in the form of energy vortices yielding long-enduring standing waves. The trapping modes are eigensolutions of the related diffraction problem associated with nearly real complex points of its discrete frequency spectrum. To detect such resonance motion, a laser vibrometer based system has been employed for the acquisition and appropriate visualization of piezoelectrically actuated out-of-plane surface motion of a two-layer aluminum plate with an artificial strip-like delamination. The measurements at resonance and off-resonance frequencies have revealed a time-harmonic oscillation of good quality above the delamination in the resonance case. It lasts for a long time after the scattered waves have left that area. The measured frequency of the trapped standing-wave oscillation is in a good agreement with that predicted using the integral equation based mathematical model.

Surface folding in metals: a mechanism for delamination wear in sliding

PubMed Central

Mahato, Anirban; Guo, Yang; Sundaram, Narayan K.; Chandrasekar, Srinivasan

2014-01-01

Using high-resolution, in situ imaging of a hard, wedge-shaped model asperity sliding against a metal surface, we demonstrate a new mechanism for particle formation and delamination wear. Damage to the residual surface is caused by the occurrence of folds on the free surface of the prow-shaped region ahead of the wedge. This damage manifests itself as shallow crack-like features and surface tears, which are inclined at very acute angles to the surface. The transformation of folds into cracks, tears and particles is directly captured. Notably, a single sliding pass is sufficient to damage the surface, and subsequent passes result in the generation of platelet-like wear particles. Tracking the folding process at every stage from surface bumps to folds to cracks/tears/particles ensures that there is no ambiguity in capturing the mechanism of wear. Because fold formation and consequent delamination are quite general, our findings have broad applicability beyond wear itself, including implications for design of surface generation and conditioning processes. PMID:25197251

Dominant behaviours in the expression of human carbonic anhydrase hCA I activity.

PubMed

Abdelrahim, M Yahia M; Tanc, Muhammet; Winum, Jean-Yves; Supuran, Claudiu T; Barboiu, Mihail

2014-07-28

Here we describe the screening via Dynamic Deconvolution of DCLs of inhibitors (CAIs) and activators (CAAs) of hCA I. The inhibitory effects dominate over the activating ones, while the CAAs may be identified in the absence of CAIs.

Failure Predictions of Out-of-Autoclave Sandwich Joints with Delaminations under Flexure Loads

NASA Technical Reports Server (NTRS)

Nordendale, Nikolas; Goyal, Vinay; Lundgren, Eric; Patel, Dhruv; Farrokh, Babak; Jones, Justin; Fischetti, Grace; Segal, Kenneth

2015-01-01

An analysis and a test program was conducted to investigate the damage tolerance of composite sandwich joints. The joints contained a single circular delamination between the face-sheet and the doubler. The coupons were fabricated through out-of-autoclave (OOA) processes, a technology NASA is investigating for joining large composite sections. The four-point bend flexure test was used to induce compression loading into the side of the joint where the delamination was placed. The compression side was chosen since it tends to be one of the most critical loads in launch vehicles. Autoclave cure was used to manufacture the composite sandwich sections, while the doubler was co-bonded onto the sandwich face-sheet using an OOA process after sandwich panels were cured. A building block approach was adopted to characterize the mechanical properties of the joint material, including the fracture toughness between the doubler and facesheet. Twelve four-point-bend samples were tested, six in the sandwich core ribbon orientation and six in sandwich core cross-ribbon direction. Analysis predicted failure initiation and propagation at the pre-delaminated location, consistent with experimental observations. A building block approach using fracture analyses methods predicted failure loads in close agreement with tests. This investigation demonstrated a small strength reduction due to a flaw of significant size compared to the width of the sample. Therefore, concerns of bonding an OOA material to an in-autoclave material was mitigated for the geometries, materials, and load configurations considered.

Failure Predictions of Out-of-Autoclave Sandwich Joints with Delaminations Under Flexure Loads

NASA Technical Reports Server (NTRS)

Nordendale, Nikolas A.; Goyal, Vinay K.; Lundgren, Eric C.; Patel, Dhruv N.; Farrokh, Babak; Jones, Justin; Fischetti, Grace; Segal, Kenneth N.

2015-01-01

An analysis and a test program was conducted to investigate the damage tolerance of composite sandwich joints. The joints contained a single circular delamination between the face-sheet and the doubler. The coupons were fabricated through out-of-autoclave (OOA) processes, a technology NASA is investigating for joining large composite sections. The four-point bend flexure test was used to induce compression loading into the side of the joint where the delamination was placed. The compression side was chosen since it tends to be one of the most critical loads in launch vehicles. Autoclave cure was used to manufacture the composite sandwich sections, while the doubler was co-bonded onto the sandwich face-sheet using an OOA process after sandwich panels were cured. A building block approach was adopted to characterize the mechanical properties of the joint material, including the fracture toughness between the doubler and face-sheet. Twelve four-point-bend samples were tested, six in the sandwich core ribbon orientation and six in sandwich core cross-ribbon direction. Analysis predicted failure initiation and propagation at the pre-delaminated location, consistent with experimental observations. A building block approach using fracture analyses methods predicted failure loads in close agreement with tests. This investigation demonstrated a small strength reduction due to a flaw of significant size compared to the width of the sample. Therefore, concerns of bonding an OOA material to an in-autoclave material was mitigated for the geometries, materials, and load configurations considered.

Failure Predictions of Out-of-Autoclave Sandwich Joints with Delaminations Under Flexure Loads

NASA Technical Reports Server (NTRS)

Nordendale, Nikolas; Goyal, Vinay; Lundgren, Eric; Patel, Dhruv; Farrokh, Babak; Jones, Justin; Fischetti, Grace; Segal, Kenneth

2015-01-01

An analysis and a test program was conducted to investigate the damage tolerance of composite sandwich joints. The joints contained a single circular delamination between the face-sheet and the doubler. The coupons were fabricated through out-of-autoclave (OOA) processes, a technology NASA is investigating for joining large composite sections. The four-point bend flexure test was used to induce compression loading into the side of the joint where the delamination was placed. The compression side was chosen since it tends to be one of the most critical loads in launch vehicles. Autoclave cure was used to manufacture the composite sandwich sections, while the doubler was co-bonded onto the sandwich face-sheet using an OOA process after sandwich panels were cured. A building block approach was adopted to characterize the mechanical properties of the joint material, including the fracture toughness between the doubler and face-sheet. Twelve four-point-bend samples were tested, six in the sandwich core ribbon orientation and six in sandwich core cross-ribbon direction. Analysis predicted failure initiation and propagation at the pre-delaminated location, consistent with experimental observations. Fracture analyses methods predicted failure loads in close agreement with tests. This investigation demonstrated a strength reduction of 10 percent due to a flaw of significant size compared to the width of the sample. Therefore, concerns of bonding an OOA material to an in-autoclave material was mitigated for the geometries, materials, and load configurations considered.

Surface modified MXene Ti3C2 multilayers by aryl diazonium salts leading to large-scale delamination

NASA Astrophysics Data System (ADS)

Wang, Hongbing; Zhang, Jianfeng; Wu, Yuping; Huang, Huajie; Li, Gaiye; Zhang, Xin; Wang, Zhuyin

2016-10-01

Herein we report a simple and facile method to delaminate MXene Ti3C2 multilayers by the assistance of surface modification using aryl diazonium salts. The basic strategy involved the preparation of layered MAX Ti3AlC2 and the exfoliation of Ti3AlC2 into Ti3C2 multilayers, followed by Na+ intercalation and surface modification using sulfanilic acid diazonium salts. The resulting chemically grafted Ti3C2 flakes were characterized by Fourier transform infrared (FT-IR) spectroscopy and X-ray photoelectron spectroscopy (XPS) to confirm the presence of the surface organic species. Ultraviolet-visible spectroscopy revealed that surface-modified MXene Ti3C2 sheets disperse well in water and the solutions obey Lambert-Beer's law. Scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray diffraction (XRD) were used to demonstrate the morphology and structure of delaminating MXene Ti3C2 flakes. The results indicated that chemical modification for MXene multilayers by aryl diazonium salts induced swelling that conversely weakened the bonds between MX layers, hence leading to large-scale delamination of multilayered MXene Ti3C2via mild sonication. Advantages of the present approach rely not only on the simplicity and efficiency of the delamination procedure but also on the grafting of aryl groups to MXene surfaces, highly suitable for further applications of the newly discovered two-dimensional materials.

Growth responses in a mutant dwarf rat to human growth hormone and recombinant human insulin-like growth factor I.

PubMed

Skottner, A; Clark, R G; Fryklund, L; Robinson, I C

1989-05-01

A new mutant GH-deficient dwarf rat has been used to study the effects of iv infusions of human GH (hGH) and recombinant human insulin-like growth factor I (hIGF-I). This animal has only about 5% of normal pituitary GH content, low circulating GH levels, and no regular GH surges. The defect seems to be specific for GH. Infusions of hIGF-I at 180 micrograms/day for 9 days elevated serum IGF-I concentrations significantly over those in the saline-infused controls (713 +/- 20 ng/ml vs. 395 +/- 31 ng/ml); hGH infusions did not raise IGF-I levels significantly (435 +/- 20 ng/ml). Gel filtration of serum samples showed that the high-dose hIGF-I infusions increased free IGF concentrations, without apparently altering the pattern of IGF-I binding whereas hGH infusions increased the amount of high mol wt IGF-I binding protein. Neither IGF-I nor hGH infusions affected the small amounts of rat GH present in the dwarf rat pituitary glands. Continuous iv infusions of hGH (200 mU/day for 9 days) stimulated body wt gain (2.1 +/- 0.2 g/day) and bone growth (96 +/- 9 microns/day) significantly compared to saline-infused dwarf rats (1.2 +/- 0.3 g/day and 43 +/- 3 microns/day). Infusions of hIGF-I at 180 micrograms/day produced a body wt gain (2.1 +/- 0.5 g/day) similar to that seen in the hGH-infused group but a significantly smaller stimulation of bone growth (63 +/- 3 microns/day). Infusion of a 5-fold lower dose of hIGF-I (36 micrograms/day for 9 days) had no effect on body wt or bone growth. Food intake was unaffected by either hGH or hIGF-I infusions. The pattern of tissue growth was affected differentially by hGH and IGF-I infusions that produced the same overall body wt gain. hGH induced a relatively proportional growth in most of the organs studied, whereas hIGF-I infusion at 180 micrograms/day stimulated a disproportionately greater growth of the kidney, adrenals, and spleen. In some of the animals, tissues were extracted for RIA of IGF-I; the amounts of IGF-I in the liver

Modeling the Influence of Stitching on Delamination Growth in Stitched Warp-Knit Composite Lap Joints

NASA Technical Reports Server (NTRS)

Glaessgen, E. H.; Raju, I. S.; Poe, C. C., Jr.

1999-01-01

The effect of stitches on the failure of a single lap joint configuration was determined in a combined experimental and analytical study. The experimental study was conducted to determine debond growth under static monotonic loading. The stitches were shown to delay the initiation of the debond and provide load transfer beyond the load necessary to completely debond the stitched lap joint. The strain energy release rates at the debond front were calculated using a finite element-based technique. Models of the unstitched configuration showed significant values of modes I and II across the width of the joint and showed that mode III is zero at the centerline but increases near the free edge. Models of the stitched configuration showed that the stitches effectively reduced mode I to zero, but had less of an effect on modes II and III.

Impedance Based Detection of Delamination in Composite Structures

NASA Astrophysics Data System (ADS)

Djemana, M.; Hrairi, M.

2017-03-01

Nowadays commercial and military aircrafts are increasingly using composite materials to take advantage of their excellent specific strength and stiffness properties but impacts on composites due to bird-strike, hail-storm cause barely visible impact damage (BVID) that underscores the need for robust structural health monitoring methods. Hence, damage identification in composite materials is a widely researched area that has to deal with problems coming from the anisotropic nature of composites and the fact that much of the damage occurs beneath the top surface of the laminate. This paper focuses on understanding self-sensing piezoelectric wafer active sensors (PWAS) to conduct electromechanical impedance (EMI) in glass fibre reinforced polymer composite to perform structural health monitoring. With the aid of a 3D ANSYS finite element model, an analysis of different techniques for the detection of position and size of a delamination in a composite structure using piezoelectric patches had been performed. The real part of the impedance is used because it is known to be more reactive to damage or changes in the structure’s integrity and less sensitive to ambient temperature changes compared to the imaginary part. Comparison with experimental results is presented to validate the FE results. The experimental setup utilizes as its main apparatus an impedance analyser HP4194 that reads the in-situ EMI of PWAS bonded to the monitored composite structure. A good match between experimental and numerical results has been observed for low and high frequencies. The analysis in this paper provides necessary basis for delamination detection in composite structures using EMI technique

Does social status within a dominance hierarchy mediate individual growth, residency and relocation?

PubMed

Akbaripasand, Abbas; Ramezani, J; Krkosek, Martin; Lokman, P Mark; Closs, Gerard P

2014-11-01

The availability of food, and hence energy, is known to influence the abundance, habitat choice and growth of individuals. In contrast, there is a paucity of knowledge on how the interaction of energy supply and social status determines patterns of residency and movement. This study tests whether the presence of conspecifics and an individual's social status in relation to food supply influence the fitness and movement of a drift-feeding fish (Galaxias fasciatus). Using an information-theoretic approach (AIC), our analysis indicated that the most parsimonious model of fish movement among pools was one that included food supply, social rank and fish relative growth rate. Our results indicated that subordinate fish relocated more frequently compared to dominant fish, most likely as a consequence of intra-specific competition that limited the access of these smaller fish to resources and constrained their growth. Our results suggest that energy constraints may force individuals to explore new habitats in an effort to find more energetically profitable patches. We conclude that intra-specific competition mediated through the social hierarchy amongst closely interacting individuals plays a key role in determining individual growth, residency and relocation.

Elevated levels of insulin-like growth factor (IGF)-I in serum rescue the severe growth retardation of IGF-I null mice.

PubMed

Wu, Yingjie; Sun, Hui; Yakar, Shoshana; LeRoith, Derek

2009-09-01

IGF-I plays a vital role in growth and development and acts in an endocrine and an autocrine/paracrine fashion. The purpose of the current study was to clarify whether elevated levels of IGF-I in serum can rescue the severe growth retardation and organ development and function of igf-I null mice. To address that, we overexpressed a rat igf-I transgene specifically in the liver of igf-I null mice. We found that in the total absence of tissue IGF-I, elevated levels of IGF-I in serum can support normal body size at puberty and after puberty but are insufficient to fully support the female reproductive system (evident by irregular estrous cycle, impaired development of ovarian corpus luteum, reduced number of uterine glands and endometrial hypoplasia, all leading to decreased number of pregnancies and litter size). We conclude that most autocrine/paracrine actions of IGF-I that determine organ growth and function can be compensated by elevated levels of endocrine IGF-I. However, in mice, full compensatory responses are evident later in development, suggesting that autocrine/paracrine IGF-I is critical for neonatal development. Furthermore, we show that tissue IGF-I is necessary for the development of the female reproductive system and cannot be compensated by elevated levels of serum IGF-I.

Human conditions of insulin-like growth factor-I (IGF-I) deficiency

PubMed Central

2012-01-01

Insulin-like growth factor I (IGF-I) is a polypeptide hormone produced mainly by the liver in response to the endocrine GH stimulus, but it is also secreted by multiple tissues for autocrine/paracrine purposes. IGF-I is partly responsible for systemic GH activities although it possesses a wide number of own properties (anabolic, antioxidant, anti-inflammatory and cytoprotective actions). IGF-I is a closely regulated hormone. Consequently, its logical therapeutical applications seems to be limited to restore physiological circulating levels in order to recover the clinical consequences of IGF-I deficiency, conditions where, despite continuous discrepancies, IGF-I treatment has never been related to oncogenesis. Currently the best characterized conditions of IGF-I deficiency are Laron Syndrome, in children; liver cirrhosis, in adults; aging including age-related-cardiovascular and neurological diseases; and more recently, intrauterine growth restriction. The aim of this review is to summarize the increasing list of roles of IGF-I, both in physiological and pathological conditions, underlying that its potential therapeutical options seem to be limited to those proven states of local or systemic IGF-I deficiency as a replacement treatment, rather than increasing its level upper the normal range. PMID:23148873

The growth hormone–insulin-like growth factor-I axis in the diagnosis and treatment of growth disorders

PubMed Central

Blum, Werner F; Alherbish, Abdullah; Alsagheir, Afaf; El Awwa, Ahmed; Kaplan, Walid; Koledova, Ekaterina; Savage, Martin O

2018-01-01

The growth hormone (GH)–insulin-like growth factor (IGF)-I axis is a key endocrine mechanism regulating linear growth in children. While paediatricians have a good knowledge of GH secretion and assessment, understanding and use of measurements of the components of the IGF system are less current in clinical practice. The physiological function of this axis is to increase the anabolic cellular processes of protein synthesis and mitosis, and reduction of apoptosis, with each being regulated in the appropriate target tissue. Measurement of serum IGF-I and IGF-binding protein (IGFBP)-3 concentrations can complement assessment of GH status in the investigation of short stature and contribute to prediction of growth response during GH therapy. IGF-I monitoring during GH therapy also informs the clinician about adherence and provides a safety reference to avoid over-dosing during long-term management. PMID:29724795

The growth hormone-insulin-like growth factor-I axis in the diagnosis and treatment of growth disorders.

PubMed

Blum, Werner; Alherbish, Abdullah; Alsagheir, Afaf; El Awwa, Ahmed; Kaplan, Walid; Koledova, Ekaterina; Savage, Martin O

2018-05-03

The growth hormone (GH)-insulin-like growth factor (IGF)-I axis is a key endocrine mechanism regulating linear growth in children. While paediatricians have a good knowledge of GH secretion and assessment, understanding and use of measurements of the components of the IGF system are less current in clinical practice. The physiological function of this axis is to increase the anabolic cellular processes of protein synthesis and mitosis, and reduction of apoptosis, with each being regulated in the appropriate target tissue. Measurement of serum IGF-I and IGFBP-3 concentrations can complement assessment of GH status in the investigation of short stature and contribute to prediction of growth response during GH therapy. IGF-I monitoring during GH therapy also informs the clinician about adherence and provides a safety reference to avoid over-dosing during long-term management.

Insulin-like growth factor-I stimulates H{sub 4}II rat hepatoma cell proliferation: Dominant role of PI-3'K/Akt signaling

DOE Office of Scientific and Technical Information (OSTI.GOV)

Alexia, Catherine; Fourmatgeat, Pascal; Delautier, Daniele

2006-04-15

Although hepatocytes are the primary source of endocrine IGF-I and -II in mammals, their autocrine/paracrine role in the dysregulation of proliferation and apoptosis during hepatocarcinogenesis and in hepatocarcinomas (HCC) remains to be elucidated. Indeed, IGF-II and type-I IGF receptors are overexpressed in HCC cells, and IGF-I is synthesized in adjacent non-tumoral liver tissue. In the present study, we have investigated the effects of type-I IGF receptor signaling on H{sub 4}II rat hepatoma cell proliferation, as estimated by {sup 3}H-thymidine incorporation into DNA. IGF-I stimulated the rate of DNA synthesis of serum-deprived H{sub 4}II cells, stimulation being maximal 3 h aftermore » the onset of IGF-I treatment and remaining elevated until at least 6 h. The IGF-I-induced increase in DNA replication was abolished by LY294002 and only partially inhibited by PD98059, suggesting that phosphoinositol-3' kinase (PI-3'K) and to a lesser extent MEK/Erk signaling were involved. Furthermore, the 3- to 19-fold activation of the Erks in the presence of LY294002 suggested a down-regulation of the MEK/Erk cascade by PI-3'K signaling. Finally, the effect of IGF-I on DNA replication was almost completely abolished in clones of H{sub 4}II cells expressing a dominant-negative form of Akt but was unaltered by rapamycin treatment of wild-type H{sub 4}II cells. Altogether, these data support the notion that the stimulation of H{sub 4}II rat hepatoma cell proliferation by IGF-I is especially dependent on Akt activation but independent on the Akt/mTOR signal0009i.« less

Autosomal recessive form of isolated growth hormone deficiency is more frequent than the autosomal dominant form in a Brazilian cohort.

PubMed

Lido, Andria C V; França, Marcela M; Correa, Fernanda A; Otto, Aline P; Carvalho, Luciani R; Quedas, Elisangela P S; Nishi, Mirian Y; Mendonca, Berenice B; Arnhold, Ivo J P; Jorge, Alexander A L

2014-10-01

In most studies, the autosomal dominant (type II) form of isolated growth hormone deficiency (IGHD) has been more frequent than the autosomal recessive (type I) form. Our aim was to assess defects in the GH1 in short Brazilian children with different GH secretion status. We selected 135 children with postnatal short stature and classified according to the highest GH peak at stimulation tests in: severe IGHD (peak GH≤3.3 μg/L, n=38, all with normal pituitary magnetic resonance imaging); GH peak between 3.3 and 10 μg/L (n=76); and GH peak >10 μg/L (n=21). The entire coding region of GH1 was sequenced and complete GH1 deletions were assessed by Multiplex Ligation Dependent Probe Amplification and restriction enzyme digestion. Patients with severe IGHD had a higher frequency of consanguinity, were shorter, had lower levels of IGF-1 and IGFBP-3, and despite treatment with lower GH doses had a greater growth response than patients with GH peak ≥3.3 μg/L. Mutations were found only in patients with severe IGHD (GH peak<3.3 μg/L). Eight patients had autosomal recessive IGHD: Seven patients were homozygous for GH1 deletions and one patient was compound heterozygous for a GH1 deletion and the novel c.171+5G>C point mutation in intron 2, predicted to abolish the donor splice site. Only one patient, who was heterozygous for the c.291+1G>T mutation located at the universal donor splice site of intron 3 and predicts exon 3 skipping, had an autosomal dominant form. Analysis of GH1 in a cohort of Brazilian patients revealed that the autosomal recessive form of IGHD was more common than the dominant one, and both were found only in severe IGHD. Copyright © 2014 Elsevier Ltd. All rights reserved.

Evaluation of Delamination of X80 Pipeline Steel Coating Under Alternating Stray Current Via Scanning Electrochemical Microscopy

NASA Astrophysics Data System (ADS)

Wang, Xinhua; Liu, Qiang; Chun, Yingchun; Li, Yingchao; Wang, Zuquan

2018-04-01

The delamination of epoxy coating on X80 pipeline steel was evaluated under various stray alternating current (AC) interferences (0-300 A/m2). Qualitative and quantitative analyses were carried out using scanning electrochemical microscopy (SECM), electrochemical impedance spectroscopy (EIS), and three-dimensional digital microscopy. The results show that the SECM current is directly proportional to the soaking time and applied current density. The variation in SECM current curve shape indicates the delamination distance of epoxy coatings at the defect area. The depths of corrosion pits at 50, 100, and 300 A/m2 stray currents were 140, 160, and 240 μm, respectively. The corrosion pits also became wider with increasing current densities. With increasing stray AC densities, both the coating delamination and pit depth became more severe at the same soaking time. The EIS results show that the change in impedance was not significant without stray current, whereas the impedance first decreased and then increased when stray current was applied. These results are consistent with the SECM measurements.

Correlating bilayer tablet delamination tendencies to micro-environmental thermodynamic conditions during pan coating.

PubMed

Zacour, Brian M; Pandey, Preetanshu; Subramanian, Ganeshkumar; Gao, Julia Z; Nikfar, Faranak

2014-06-01

The objective of this study was to determine the impact that the micro-environment, as measured by PyroButton data loggers, experienced by tablets during the pan coating unit operation had on the layer adhesion of bilayer tablets in open storage conditions. A full factorial design of experiments (DOE) with three center points was conducted to study the impact of final tablet hardness, film coating spray rate and film coating exhaust temperature on the delamination tendencies of bilayer tablets. PyroButton data loggers were placed (fixed) at various locations in a pan coater and were also allowed to freely move with the tablet bed to measure the micro-environmental temperature and humidity conditions of the tablet bed. The variance in the measured micro-environment via PyroButton data loggers accounted for 75% of the variance in the delamination tendencies of bilayer tablets on storage (R(2 )= 0.75). A survival analysis suggested that tablet hardness and coating spray rate significantly impacted the delamination tendencies of the bilayer tablets under open storage conditions. The coating exhaust temperature did not show good correlation with the tablets' propensity to crack indicating that it was not representative of the coating micro-environment. Models created using data obtained from the PyroButton data loggers outperformed models created using primary DOE factors in the prediction of bilayer tablet strength, especially upon equipment or scale transfers. The coating micro-environment experienced by tablets during the pan coating unit operation significantly impacts the strength of the bilayer interface of tablets on storage.

Growth of structure in the Szekeres class-II inhomogeneous cosmological models and the matter-dominated era

NASA Astrophysics Data System (ADS)

Ishak, Mustapha; Peel, Austin

2012-04-01

This study belongs to a series devoted to using the Szekeres inhomogeneous models in order to develop a theoretical framework where cosmological observations can be investigated with a wider range of possible interpretations. While our previous work addressed the question of cosmological distances versus redshift in these models, the current study is a start at looking into the growth rate of large-scale structure. The Szekeres models are exact solutions to Einstein’s equations that were originally derived with no symmetries. We use here a formulation of the Szekeres models that is due to Goode and Wainwright, who considered the models as exact perturbations of a Friedmann-Lemaître-Robertson-Walker (FLRW) background. Using the Raychaudhuri equation we write, for the two classes of the models, exact growth equations in terms of the under/overdensity and measurable cosmological parameters. The new equations in the overdensity split into two informative parts. The first part, while exact, is identical to the growth equation in the usual linearly perturbed FLRW models, while the second part constitutes exact nonlinear perturbations. We integrate numerically the full exact growth rate equations for the flat and curved cases. We find that for the matter-dominated cosmic era, the Szekeres growth rate is up to a factor of three to five stronger than the usual linearly perturbed FLRW cases, reflecting the effect of exact Szekeres nonlinear perturbations. We also find that the Szekeres growth rate with an Einstein-de Sitter background is stronger than that of the well-known nonlinear spherical collapse model, and the difference between the two increases with time. This highlights the distinction when we use general inhomogeneous models where shear and a tidal gravitational field are present and contribute to the gravitational clustering. Additionally, it is worth observing that the enhancement of the growth found in the Szekeres models during the matter-dominated era

A novel method to delaminate nitrate-intercalated MgAl layered double hydroxides in water and application in heavy metals removal from waste water.

PubMed

Rahman, Mir Tamzid; Kameda, Tomohito; Kumagai, Shogo; Yoshioka, Toshiaki

2018-07-01

Nitrate-intercalated MgAl layered double hydroxide (LDH) was successfully delaminated in water by a facile and effective method upon reflux at 120 °C for 24 h followed by sonication at 40 °C for 5 h. This process is environmentally friendly since water is the only solvent used. The delaminated nanosheets were characterized by microscopic, spectroscopic, and particle size analyses. The delamination process successfully produced octahedron-shaped single-layer nanosheets 50-150 nm in size. X-ray photoelectron spectroscopy (XPS) data confirmed that the surface elements and their chemical status are consistent with the basic layer of MgAl LDH. The delaminated nanosheets displayed higher adsorption capacity for removing heavy metals from waste water than the original powdered LDH. After treating the waste water, a sharp and intense peak in the X-ray powder diffraction (XRD) pattern of the precipitate confirms the restacking of the LDH nanosheets. Copyright © 2018 Elsevier Ltd. All rights reserved.

Insulin-like growth factor-I treatment of children with Laron syndrome (primary growth hormone insensitivity).

PubMed

Laron, Zvi

2008-03-01

Laron syndrome (LS, congenital primary GH insensitivity) is caused by deletions or mutations in the GH receptor gene, resulting in an inability to generate insulin-like growth factor-I (IGF-I). If untreated, the deficiency of IGF-I results in severe dwarfism, as well as skeletal and muscular underdevelopment. The only treatment is the daily administration of recombinant IGF-I. This review summarizes the present experience by several groups worldwide. The main conclusions are: A. The one or two injections regimen result in the same growth velocity; B. The growth velocity obtained with IGF-I administration is smaller than that observed with hGH in children with congenital isolated GH deficiency; C. Overdosage of IGF-I causes a series of adverse effects which can be avoided by carefully monitoring the serum IGF-I and GH levels.

Facesheet Delamination of Composite Sandwich Materials at Cryogenic Temperatures

NASA Technical Reports Server (NTRS)

Gates, Thomas S.; Odegard, Gregory M.; Herring, Helen M.

2003-01-01

The next generation of space transportation vehicles will require advances in lightweight structural materials and related design concepts to meet the increased demands on performance. One potential source for significant structural weight reduction is the replacement of traditional metallic cryogenic fuel tanks with new designs for polymeric matrix composite tanks. These new tank designs may take the form of thin-walled sandwich constructed with lightweight core and composite facesheets. Life-time durability requirements imply the materials must safely carry pressure loads, external structural loads, resist leakage and operate over an extremely wide temperature range. Aside from catastrophic events like tank wall penetration, one of the most likely scenarios for failure of a tank wall of sandwich construction is the permeation of cryogenic fluid into the sandwich core and the subsequent delamination of the sandwich facesheet due to the build-up of excessive internal pressure. The research presented in this paper was undertaken to help understand this specific problem of core to facesheet delamination in cryogenic environments and relate this data to basic mechanical properties. The experimental results presented herein provide data on the strain energy release rate (toughness) of the interface between the facesheet and the core of a composite sandwich subjected to simulated internal pressure. A unique test apparatus and associated test methods are described and the results are presented to highlight the effects of cryogenic temperature on the measured material properties.

Dihydrotestosterone inhibits hair growth in mice by inhibiting insulin-like growth factor-I production in dermal papillae.

PubMed

Zhao, Juan; Harada, Naoaki; Okajima, Kenji

2011-10-01

We demonstrated that insulin-like growth factor-I (IGF-I) production in dermal papillae was increased and hair growth was promoted after sensory neuron stimulation in mice. Although the androgen metabolite dihydrotestosterone (DHT) inhibits hair growth by negatively modulating growth-regulatory effects of dermal papillae, relationship between androgen metabolism and IGF-I production in dermal papillae is not fully understood. We examined whether DHT inhibits IGF-I production by inhibiting sensory neuron stimulation, thereby preventing hair growth in mice. Effect of DHT on sensory neuron stimulation was examined using cultured dorsal root ganglion (DRG) neurons isolated from mice. DHT inhibits calcitonin gene-related peptide (CGRP) release from cultured DRG neurons. The non-steroidal androgen-receptor antagonist flutamide reversed DHT-induced inhibition of CGRP release. Dermal levels of IGF-I and IGF-I mRNA, and the number of IGF-I-positive fibroblasts around hair follicles were increased at 6h after CGRP administration. DHT administration for 3weeks decreased dermal levels of CGRP, IGF-I, and IGF-I mRNA in mice. Immunohistochemical expression of IGF-I and the number of proliferating cells in hair follicles were decreased and hair re-growth was inhibited in animals administered DHT. Co-administration of flutamide and CGRP reversed these changes induced by DHT administration. These observations suggest that DHT may decrease IGF-I production in dermal papillae by inhibiting sensory neuron stimulation through interaction with the androgen receptor, thereby inhibiting hair growth in mice. Copyright © 2011 Elsevier Ltd. All rights reserved.

Ductile film delamination from compliant substrates using hard overlayers

PubMed Central

Cordill, M.J.; Marx, V.M.; Kirchlechner, C.

2014-01-01

Flexible electronic devices call for copper and gold metal films to adhere well to polymer substrates. Measuring the interfacial adhesion of these material systems is often challenging, requiring the formulation of different techniques and models. Presented here is a strategy to induce well defined areas of delamination to measure the adhesion of copper films on polyimide substrates. The technique utilizes a stressed overlayer and tensile straining to cause buckle formation. The described method allows one to examine the effects of thin adhesion layers used to improve the adhesion of flexible systems. PMID:25641995

Ductile film delamination from compliant substrates using hard overlayers.

PubMed

Cordill, M J; Marx, V M; Kirchlechner, C

2014-11-28

Flexible electronic devices call for copper and gold metal films to adhere well to polymer substrates. Measuring the interfacial adhesion of these material systems is often challenging, requiring the formulation of different techniques and models. Presented here is a strategy to induce well defined areas of delamination to measure the adhesion of copper films on polyimide substrates. The technique utilizes a stressed overlayer and tensile straining to cause buckle formation. The described method allows one to examine the effects of thin adhesion layers used to improve the adhesion of flexible systems.

Regulating continent growth and composition by chemical weathering

PubMed Central

Lee, Cin-Ty Aeolus; Morton, Douglas M.; Little, Mark G.; Kistler, Ronald; Horodyskyj, Ulyana N.; Leeman, William P.; Agranier, Arnaud

2008-01-01

Continents ride high above the ocean floor because they are underlain by thick, low-density, Si-rich, and Mg-poor crust. However, the parental magmas of continents were basaltic, which means they must have lost Mg relative to Si during their maturation into continents. Igneous differentiation followed by lower crustal delamination and chemical weathering followed by subduction recycling are possible solutions, but the relative magnitudes of each process have never been quantitatively constrained because of the lack of appropriate data. Here, we show that the relative contributions of these processes can be obtained by simultaneous examination of Mg and Li (an analog for Mg) on the regional and global scales in arcs, delaminated lower crust, and river waters. At least 20% of Mg is lost from continents by weathering, which translates into >20% of continental mass lost by weathering (40% by delamination). Chemical weathering leaves behind a more Si-rich and Mg-poor crust, which is less dense and hence decreases the probability of crustal recycling by subduction. Net continental growth is thus modulated by chemical weathering and likely influenced by secular changes in weathering mechanisms. PMID:18362343

Regulating continent growth and composition by chemical weathering

USGS Publications Warehouse

Lee, C.-T.A.; Morton, D.M.; Little, M.G.; Kistler, R.; Horodyskyj, U.N.; Leeman, W.P.; Agranier, A.

2008-01-01

Continents ride high above the ocean floor because they are underlain by thick, low-density, Si-rich, and Mg-poor crust. However, the parental magmas of continents were basaltic, which means they must have lost Mg relative to Si during their maturation into continents. Igneous differentiation followed by lower crustal delamination and chemical weathering followed by subduction recycling are possible solutions, but the relative magnitudes of each process have never been quantitatively constrained because of the lack of appropriate data. Here, we show that the relative contributions of these processes can be obtained by simultaneous examination of Mg and Li (an analog for Mg) on the regional and global scales in arcs, delaminated lower crust, and river waters. At least 20% of Mg is lost from continents by weathering, which translates into >20% of continental mass lost by weathering (40% by delamination). Chemical weathering leaves behind a more Si-rich and Mg-poor crust, which is less dense and hence decreases the probability of crustal recycling by subduction. Net continental growth is thus modulated by chemical weathering and likely influenced by secular changes in weathering mechanisms. ?? 2008 by The National Academy of Sciences of the USA.

Rearing Mozambique tilapia in tidally-changing salinities: Effects on growth and the growth hormone/insulin-like growth factor I axis.

PubMed

Moorman, Benjamin P; Yamaguchi, Yoko; Lerner, Darren T; Grau, E Gordon; Seale, Andre P

2016-08-01

The growth hormone (GH)/insulin-like growth factor (IGF) axis plays a central role in the regulation of growth in teleosts and has been shown to be affected by acclimation salinity. This study was aimed at characterizing the effects of rearing tilapia, Oreochromis mossambicus, in a tidally-changing salinity on the GH/IGF axis and growth. Tilapia were raised in fresh water (FW), seawater (SW), or in a tidally-changing environment, in which salinity is switched between FW (TF) and SW (TS) every 6h, for 4months. Growth was measured over all time points recorded and fish reared in a tidally-changing environment grew significantly faster than other groups. The levels of circulating growth hormone (GH), insulin-like growth factor I (IGF-I), pituitary GH mRNA, gene expression of IGF-I, IGF-II, and growth hormone receptor 2 (GHR) in the muscle and liver were also determined. Plasma IGF-I was higher in FW and TS than in SW and TF tilapia. Pituitary GH mRNA was higher in TF and TS than in FW and SW tilapia. Gene expression of IGF-I in the liver and of GHR in both the muscle and liver changed between TF and TS fish. Fish growth was positively correlated with GH mRNA expression in the pituitary, and GHR mRNA expression in muscle and liver tissues. Our study indicates that rearing fish under tidally-changing salinities elicits a distinct pattern of endocrine regulation from that observed in fish reared in steady-state conditions, and may provide a new approach to increase tilapia growth rate and study the regulation of growth in euryhaline fish. Copyright © 2016 Elsevier Inc. All rights reserved.

Strategic growth decisions in helper cichlids.

PubMed Central

Heg, Dik; Bender, Nicole; Hamilton, Ian

2004-01-01

Recently, it has been shown that group-living subordinate clownfish Amphiprion percula increase their growth rate after acquiring the dominant breeder male position in the group. Evidence was found for strategic growth adjustments of subordinate fishes depending on the threat of eviction, i.e. subordinates adjust their growth rates so they remain smaller than the dominant fish and thereby limit the threat of being expelled from the territory. However, it is impossible to exclude several alternative factors that potentially could have influenced the observed changes in growth, owing to the nature of that experiment (removing the second-ranking fish--the breeder male--caused the third-ranking fish to change sex to become breeder male and change rank). We studied strategic growth decisions in the group-living Lake Tanganyika cichlid Neolamprologus pulcher under controlled laboratory conditions with ad libitum food availability. First, we show that male breeders grow faster than subordinate male helpers of the same initial size and confirm that N. pulcher shows status-dependent growth. Second, we improved on the experimental design by not removing the dominant breeder male in the group; instead we replaced the breeder male with a new breeder male in a full factorial design and measured growth of the subordinate male helpers is a function of the size difference with the old and the new breeder male. As predicted, male helpers showed strategic growth adjustments, i.e. growing faster when the size difference with the breeder male is large. Strategic growth adjustments were less pronounced than status-dependent growth adjustments. PMID:15801617

Strategic growth decisions in helper cichlids.

PubMed

Heg, Dik; Bender, Nicole; Hamilton, Ian

2004-12-07

Recently, it has been shown that group-living subordinate clownfish Amphiprion percula increase their growth rate after acquiring the dominant breeder male position in the group. Evidence was found for strategic growth adjustments of subordinate fishes depending on the threat of eviction, i.e. subordinates adjust their growth rates so they remain smaller than the dominant fish and thereby limit the threat of being expelled from the territory. However, it is impossible to exclude several alternative factors that potentially could have influenced the observed changes in growth, owing to the nature of that experiment (removing the second-ranking fish--the breeder male--caused the third-ranking fish to change sex to become breeder male and change rank). We studied strategic growth decisions in the group-living Lake Tanganyika cichlid Neolamprologus pulcher under controlled laboratory conditions with ad libitum food availability. First, we show that male breeders grow faster than subordinate male helpers of the same initial size and confirm that N. pulcher shows status-dependent growth. Second, we improved on the experimental design by not removing the dominant breeder male in the group; instead we replaced the breeder male with a new breeder male in a full factorial design and measured growth of the subordinate male helpers is a function of the size difference with the old and the new breeder male. As predicted, male helpers showed strategic growth adjustments, i.e. growing faster when the size difference with the breeder male is large. Strategic growth adjustments were less pronounced than status-dependent growth adjustments.

A tropical freshwater wetland: I Structure, growth, and regeneration

Treesearch

James A. Allen; Ken W. Krauss; Katherine C. Ewel; Bobby D Keeland; Erick E. Waguk

2005-01-01

Forested wetlands dominated by (Terminalia carolinensis) are endemic to Micronesia but common only on the island of Kosrae, Federated States of Micronesia. On Kosrae, these forests occur on Nansepsep, Inkosr, and Sonahnpil soil types, which differ in degree of flooding and soil saturation. We compared forest structure, growth, nutrition, and...

Influence of crystallographic texture in X70 pipeline steels on toughness anisotropy and delamination

NASA Astrophysics Data System (ADS)

Al-Jabr, Haytham M.

The effects of microstructure and crystallographic texture in four commercially-produced API X70 pipeline steels and their relation to planar anisotropy of toughness and delamination were evaluated. The experimental steels were processed through either a hot strip mill, a Steckel mill, or a compact strip mill. Different processing routes were selected to obtain plates with potential variations in the microstructure and anisotropic characteristics. Tensile and Charpy impact testing were used to evaluate the mechanical properties in three orientations: longitudinal (L), transverse (T) and diagonal (D) with respect to the rolling direction to evaluate mechanical property anisotropy. The yield and tensile strengths were higher in the T orientation and toughness was lower in the D orientation for all plates. Delamination was observed in some of the ductile fracture surfaces of the impact samples. To further study the splitting behavior and effects on impact toughness, a modified impact test (MCVN) specimen with side grooves was designed to intensify induced stresses parallel to the notch root and thus facilitate evaluation of delamination. Scanning electron microscopy combined with electron backscattered diffraction (EBSD) were used to evaluate the grain size, microstructural constituents, and crystallographic texture to determine the factors leading to delamination and the anisotropy in toughness. The ferrite grain size is mainly responsible for the differences in DBTTs between the L and T orientations. The higher DBTT in the D orientation observed in pipeline steels is attributed to crystallographic texture. The higher DBTT in the D direction is due to the higher volume fraction of grains having their {100} planes parallel or close to the primary fracture plane for the D orientation. An equation based on a new "brittleness parameter," based on an assessment of grain orientations based on EBSD data, was developed to predict the changes in DBTTs with respect to sample

Application of Benchmark Examples to Assess the Single and Mixed-Mode Static Delamination Propagation Capabilities in ANSYS

NASA Technical Reports Server (NTRS)

Krueger, Ronald

2012-01-01

The application of benchmark examples for the assessment of quasi-static delamination propagation capabilities is demonstrated for ANSYS. The examples are independent of the analysis software used and allow the assessment of the automated delamination propagation in commercial finite element codes based on the virtual crack closure technique (VCCT). The examples selected are based on two-dimensional finite element models of Double Cantilever Beam (DCB), End-Notched Flexure (ENF), Mixed-Mode Bending (MMB) and Single Leg Bending (SLB) specimens. First, the quasi-static benchmark examples were recreated for each specimen using the current implementation of VCCT in ANSYS . Second, the delamination was allowed to propagate under quasi-static loading from its initial location using the automated procedure implemented in the finite element software. Third, the load-displacement relationship from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Overall the results are encouraging, but further assessment for three-dimensional solid models is required.

Numerical model of glulam beam delamination in dependence on cohesive strength

NASA Astrophysics Data System (ADS)

Kawecki, Bartosz; Podgórski, Jerzy

2018-01-01

This paper presents an attempt of using a finite element method for predicting delamination of a glue laminated timber beam through a cohesive layer. There were used cohesive finite elements, quadratic stress damage initiation criterion and mixed mode energy release rate failure model. Finite element damage was equal to its complete stiffness degradation. Timber material was considered to be an orthotropic with plastic behaviour after reaching bending limit.

Moisture-Induced Delamination Video of an Oxidized Thermal Barrier Coating

NASA Technical Reports Server (NTRS)

Smialek, James L.; Zhu, Dongming; Cuy, Michael D.

2008-01-01

PVD TBC coatings were thermally cycled to near-failure at 1150 C. Normal failure occurred after 200-300 1-hr cycles with only moderate weight gains (0.5 mg/cm2). Delamination and buckling was often delayed until well after cooldown (desktop spallation), but could be instantly induced by the application of water drops, as shown in an accompanying video-recording. Moisture therefore plays a primary role in delayed desktop TBC failure. Hydrogen embrittlement is proposed as the underlying mechanism.

Surface Cracking and Interface Reaction Associated Delamination Failure of Thermal and Environmental Barrier Coatings

NASA Technical Reports Server (NTRS)

Zhu, Dongming; Choi, Sung R.; Eldridge, Jeffrey I.; Lee, Kang N.; Miller, Robert A.

2003-01-01

In this paper, surface cracking and interface reactions of a BSAS coating and a multi-layer ZTO2-8wt%Y2O3 and mullite/BSAS/Si thermal and environmental barrier coating system on SiC/SiC ceramic matrix composites were characterized after long-term combined laser thermal gradient and furnace cyclic tests in a water vapor containing environment. The surface cracking was analyzed based on the coating thermal gradient sintering behavior and thermal expansion mismatch stress characteristics under the thermal cyclic conditions. The interface reactions, which were largely enhanced by the coating surface cracking in the water vapor environment, were investigated in detail, and the reaction phases were identified for the coating system after the long- term exposure. The accelerated coating delamination failure was attributed to the increased delamination driving force under the thermal gradient cyclic loading and the reduced interface adhesion due to the detrimental interface reactions.

Bone Growth, Mechanical Stimulus and IGF-I

DTIC Science & Technology

2005-10-01

children, stress fractures in military recruits, and osteoporotic fractures in elderly women. Insulin-like growth factor-I (IGF-I), a major regulator...subjects completed the intervention arm of the study and returned for the short-term post-intervention appointment, which included anthropometrie

Transgenic Wuzhishan minipigs designed to express a dominant-negative porcine growth hormone receptor display small stature and a perturbed insulin/IGF-1 pathway.

PubMed

Li, Feida; Li, Yong; Liu, Huan; Zhang, Xingju; Liu, Chuxin; Tian, Kai; Bolund, Lars; Dou, Hongwei; Yang, Wenxian; Yang, Huanming; Staunstrup, Nicklas Heine; Du, Yutao

2015-12-01

Growth hormone (GH) is an anabolic mitogen with widespread influence on cellular growth and differentiation as well as on glucose and lipid metabolism. GH binding to the growth hormone receptor (GHR) on hepatocytes prompts expression of insulin growth factor I (IGF-1) involved in nutritionally induced compensatory hyperplasia of pancreatic β-cell islets and insulin release. A prolonged hyperactivity of the IGF-1/insulin axis in the face of insulinotropic nutrition, on the other hand, can lead to collapse of the pancreatic islets and glucose intolerance. Individuals with Laron syndrome carry mutations in the GHR gene resulting in severe congenital IGF-1 deficiency and elevated GH serum levels leading to short stature as well as perturbed lipid and glucose metabolism. However, these individuals enjoy a reduced prevalence of acne, cancer and possibly diabetes. Minipigs have become important biomedical models for human conditions due to similarities in organ anatomy, physiology, and metabolism relative to humans. The purpose of this study was to generate transgenic Wuzhishan minipigs by handmade cloning with impaired systemic GHR activity and assess their growth profile and glucose metabolism. Transgenic minipigs featuring overexpression of a dominant-negative porcine GHR (GHR(dm)) presented postnatal growth retardation and proportionate dwarfism. Molecular changes included elevated GH serum levels and mild hyperglycemia. We believe that this model may prove valuable in the study of GH functions in relation to cancer, diabetes and longevity.

Does impaction of titanium-coated interbody fusion cages into the disc space cause wear debris or delamination?

PubMed

Kienle, Annette; Graf, Nicolas; Wilke, Hans-Joachim

2016-02-01

A large number of interbody fusion cages are made of polyetheretherketone (PEEK). To improve bone on-growth, some are coated with a thin layer of titanium. This coating may fail when subjected to shear loading. The purpose of this testing was to investigate whether impaction of titanium-coated PEEK cages into the disc space can result in wear or delamination of the coating, and whether titanium cages with subtractive surface etching (no coating) are less susceptible to such failure. A biomechanical study was carried out to simulate the impaction process in clinical practice and to evaluate if wear or delamination may result from impaction. Two groups of posterior lumbar interbody fusion cages with a similar geometry were tested: n=6 titanium-coated PEEK and n=6 surface-etched titanium cages. The cages were impacted into the space in between two vertebral body substitutes (polyurethane foam blocks). The two vertebral body substitutes were fixed in a device, through which a standardized axial preload of 390 N was applied. The anterior tip of the cage was positioned at the posterior border of the space between the two vertebral body substitutes. The cages were then inserted using a drop weight with a mass representative of a surgical hammer. The drop weight impacted the insertion instrument at a maximum speed of about 2.6 m/s, which is in the range of the impaction speed in vivo. This was repeated until the cages were fully inserted. The wear particles were captured and analyzed according to the pertinent standards. The surface-etched titanium cages did not show any signs of wear debris or surface damage. In contrast, the titanium-coated PEEK cages resulted in detached wear particles of different sizes (1-191 µm). Over 50% of these particles had a size <10 µm. In median, on 26% of the implants' teeth, the coating was abraded. Full delamination was not observed. In contrast to the surface-etched implants, the titanium-coated PEEK implants lost some coating material

Effects of fasting on growth hormone, growth hormone receptor, and insulin-like growth factor-I axis in seawater-acclimated tilapia, Oreochromis mossambicus.

PubMed

Fox, B K; Riley, L G; Hirano, T; Grau, E G

2006-09-15

Effects of fasting on the growth hormone (GH)--growth hormone receptor (GHR)-insulin-like growth factor-I (IGF-I) axis were characterized in seawater-acclimated tilapia (Oreochromis mossambicus). Fasting for 4 weeks resulted in significant reductions in body weight and specific growth rate. Plasma GH and pituitary GH mRNA levels were significantly elevated in fasted fish, whereas significant reductions were observed in plasma IGF-I and hepatic IGF-I mRNA levels. There was a significant negative correlation between plasma levels of GH and IGF-I in the fasted fish. No effect of fasting was observed on hepatic GHR mRNA levels. Plasma glucose levels were reduced significantly in fasted fish. The fact that fasting elicited increases in GH and decreases in IGF-I production without affecting GHR expression indicates a possible development of GH resistance.

Numerical simulations and experimental measurements of steel and ice impacts on concrete for acoustic interrogation of delaminations in bridge decks

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mazzeo, Brian A.; Patil, Anjali N.; Klis, Jeffrey M.

2014-02-18

Delaminations in bridge decks typically result from corrosion of the top mat of reinforcing steel, which leads to a localized separation of the concrete cover from the underlying concrete. Because delaminations cannot be detected using visual inspection, rapid, large-area interrogation methods are desired to characterize bridge decks without disruption to traffic, without the subjectivity inherent in existing methods, and with increased inspector safety. To this end, disposable impactors such as water droplets or ice chips can be dropped using automatic dispensers onto concrete surfaces to excite mechanical vibrations while acoustic responses can be recorded using air-coupled microphones. In this work,more » numerical simulations are used to characterize the flexural response of a model concrete bridge deck subject to both steel and ice impactors, and the results are compared with similar experiments performed in the laboratory on a partially delaminated concrete bridge deck slab. The simulations offer greater understanding of the kinetics of impacts and the responses of materials.« less

Evaluating Embedded Heater Bonding for Composites

NASA Astrophysics Data System (ADS)

Carte, Casey

Out-of-autoclave bonding of high-strength carbon-fiber composites structures can reduce costs associated with autoclaves. Nevertheless, a concern is whether out-of-autoclave bonding results in a loss of delamination toughness. The main contribution of this paper is to comparatively evaluate the delamination toughness of adhesively bonded composite parts using carbon fiber embedded heaters and those bonded in an autoclave. Carbon Fiber Reinforced Polymer (CFRP) adherends were bonded by passing an electrical current through a layer of carbon fiber prepreg embedded at the bondline between two electrically insulating thin film adhesives. The delamination toughness was evaluated under mode I dominated loading conditions using a modified single cantilever beam test. Experimental results show that the delamination toughness of specimens bonded using a carbon fiber embedded heater was comparable to that of samples bonded in an autoclave.

Delamination Effect on Impact Properties of Ultrafine-Grained Low-Carbon Steel Processed by Warm Caliber Rolling

NASA Astrophysics Data System (ADS)

Inoue, Tadanobu; Yin, Fuxing; Kimura, Yuuji; Tsuzaki, Kaneaki; Ochiai, Shojiro

2010-02-01

Bulk ultrafine-grained (UFG) low-carbon steel bars were produced by caliber rolling, and the impact and tensile properties were investigated. Initial samples with two different microstructures, ferrite-pearlite and martensite (or bainite), were prepared and then caliber rolling was conducted at 500 °C. The microstructures in the rolled bars consisted of an elongated UFG structure with a strong α-fiber texture. The rolled bar consisting of spheroidal cementite particles that distributed uniformly in the elongated ferrite matrix of transverse grain sizes 0.8 to 1.0 μm exhibited the best strength-ductility balance and impact properties. Although the yield strength in the rolled bar increased 2.4 times by grain refinement, the upper-shelf energy did not change, and its value was maintained from 100 °C to -40 °C. In the rolled bars, cracks during an impact test branched parallel to the longitudinal direction of the test samples as temperatures decreased. Delamination caused by such crack branching appeared, remarkably, near the ductile-to-brittle transition temperature (DBTT). The effect of delamination on the impact properties was associated with crack propagation on the basis of the microstructural features in the rolled bars. In conclusion, the strength-toughness balance is improved by refining crystal grains and controlling their shape and orientation; in addition, delamination effectively enhances the low-temperature toughness.

Differential effects of insulin-like growth factor I and growth hormone on developmental stages of rat growth plate chondrocytes in vivo.

PubMed Central

Hunziker, E B; Wagner, J; Zapf, J

1994-01-01

Skeletal growth depends upon enchondral ossification in growth plate cartilage, within which chondrocytes undergo well defined stages of maturation. We infused IGF-I or growth hormone (GH), two key regulators of skeletal growth, into hypophysectomized rats and compared their effects on growth plate chondrocyte differentiation using qualitative and quantitative autoradiography, stereology, and incident light fluorescence microscopy. Stem cell cycle time was shortened from 50 to 15 and 8 d after treatment with IGF-I and GH, respectively. Proliferating cell cycle time decreased from 11 to 4.5 and 3 d, and duration of the hypertrophic phase decreased from 6 to 4 and 2.8 d. Average matrix volume per cell at each differentiation stage was similar for normal, hormone-treated, and untreated hypophysectomized groups. Mean cell volume and cell height were significantly reduced by hypophysectomy at the proliferative and hypertrophic stages, but were restored to physiological values by IGF-I and GH. In contrast, cell productivity, i.e., increases in cell volume, height, and matrix production per unit of time, did not reach normal values with either IGF-I or GH, and this parameter was inversely proportional to cell cycle time or phase duration. IGF-I and GH are thus capable of stimulating growth plate chondrocytes at all stages of differentiation, albeit to variable degrees with respect to individual cell activities. Although it is generally accepted that GH acts at both the stem and proliferating phases of chondrocyte differentiation, our data represent the first evidence in vivo that IGF-I is also capable of stimulating stem cells. Images PMID:8132746

Surface Cracking and Interface Reaction Associated Delamination Failure of Thermal and Environmental Barrier Coatings

NASA Technical Reports Server (NTRS)

Zhu, Dong-Ming; Choi, Sung R.; Eldridge, Jeffrey I.; Lee, Kang N.; Miller, Robert A.

2003-01-01

In this paper, surface cracking and interface reactions of a BSAS coating and a multi-layer ZrO2-8wt%Y2O3 and mullite/BSAS/Si thermal and environmental barrier coating system on SiC/SiC ceramic matrix composites were characterized after long-term combined laser thermal gradient and furnace cyclic tests in a water vapor containing environment. The surface cracking was analyzed based on the coating thermal gradient sintering behavior and thermal expansion mismatch stress characteristics under the thermal cyclic conditions. The interface reactions, which were largely enhanced by the coating surface cracking in the water vapor environment, were investigated in detail, and the reaction phases were identified for the coating system after the long-term exposure. The accelerated coating delamination failure was attributed to the increased delamination driving force under the thermal gradient cyclic loading and the reduced interface adhesion due to the detrimental interface reactions.

Insulin-like growth factor I gene polymorphism associated with growth and carcass traits in Thai synthetic chickens.

PubMed

Promwatee, N; Laopaiboon, B; Vongpralub, T; Phasuk, Y; Kunhareang, S; Boonkum, W; Duangjinda, M

2013-03-15

Four Thai synthetic chicken lines (Kaen Thong, Khai Mook Esarn, Soi Nin, and Soi Pet) originated from Thai native and exotic commercial chickens were evaluated for their growth and carcass traits with the purpose of developing a Thai broiler breeding program. Insulin-like growth factor I (IGF-I) gene is known to play an important role in growth, proliferation and differentiation. Consequently, we investigated the possibility of using the IGF-I gene for marker-assisted selection in Thai synthetic chickens. We looked for variations in the IGF-I gene and studied their association with growth and carcass traits; 1046 chickens were genotyped using PCR-RFLP methods. A general linear model was used to analyze associations of the IGF-I polymorphism with growth and carcass traits. Kaen Thong, Khai Mook Esarn, and Soi Nin chickens were found to carry similar frequencies of alleles A and C (0.40-0.60), while Soi Pet chickens had high frequencies of allele C (0.75). The IGF-I gene was significantly associated with some growth traits (body weight at hatching, and at 4, 8, 12, and 14 weeks of age; average daily gain during 0-12 and 0-14 weeks of age) in all synthetic chickens. Carcass traits (the percentage of dressing and pectoralis major) were significantly different only in Khai Mook Esarn chickens. We conclude that IGF-I can be used as a marker gene for the selection of growth and carcass traits of synthetic chickens in a marker-assisted selection program.

Ultrasonic Monitoring of Ply Crack and Delamination Formation in Composite Tube Under Torsion Load

NASA Technical Reports Server (NTRS)

Johnston, P. H.; Wright, C. W.; Zalameda, J. N.; Seebo, J. P.

2010-01-01

As a simple model of a rotor spar, a circular graphite-epoxy composite laminate cylinder was subjected to cyclic torsional load. The test section of the cylindrical specimen varied from four to six plies of plus or minus 45 degree fibers, due to intentional ply overlaps and gaps. A layer of 13-micrometer Teflon film was inserted between plies at three locations to serve as delamination initiators. A commercial X-Y scanner was mounted to the load frame to enable ultrasonic inspection without removing the specimen. A focused immersion probe was mounted in a captive water column with a rugged Nitrile membrane tip, which was coupled to the cylinder using a mist of soapy water. The transducer was aligned normal to the cylinder surface using the X-axis. Scanning was performed along the length of the specimen with the Y-axis and the specimen was incrementally rotated by the torsion head of the load frame. After 350k cycles of torsion, several linear 45 degree diagonal indications appeared as 5-40% attenuation of the back wall echo, with no apparent echoes from the interior of the composite, suggesting through-ply cracks in the innermost ply. Crack indications grew and new cracks appeared as torsion cycling continued. Internal reflections from delaminations associated with the growing ply cracks appeared after 500k cycles. Three areas of extensive multi-layer delaminations appeared after 1150k cycles. Failure of the specimen occurred at 1600k cycles. The observed progressive damage was not associated with the Teflon inclusions. Concurrent thermographic measurements provided lower resolution confirmation of the damage observed.

Delaminations in composite plates under transverse impact loads - Experimental results

NASA Technical Reports Server (NTRS)

Finn, Scott R.; He, Ye-Fei; Springer, George S.

1993-01-01

Tests were performed measuring the locations and geometries of delaminations in Fiberite T300/976 graphite/epoxy, Fiberite IM7/977-2 graphite-toughened epoxy, and ICI APC-2 graphite/PEEK plates subjected to transverse impact loads. The data provide specific information on the effects of impactor velocity, impactor mass, material, thickness of back ply group, difference in fiber orientation between adjacent ply groups, plate thickness, and impactor nose radius. The data were compared to the results of the Finn-Springer model. The model was found to describe the data with reasonable accuracy.

Moisture-Induced Delamination Video of an Oxidized Thermal Barrier Coating

NASA Technical Reports Server (NTRS)

Smialek, James L.; Zhu, Dongming; Cuy, Michael D.

2008-01-01

PVD TBC coatings were thermally cycled to near-failure at 1150 C. Normal failure occurred after 200 to 300 1-hr cycles with only moderate weight gains (0.5 mg/sq cm). Delamination and buckling was often delayed until well after cooldown (desktop spallation), but could be instantly induced by the application of water drops, as shown in a video clip which can be viewed by clicking on figure 2 of this report. Moisture therefore plays a primary role in delayed desktop TBC failure. Hydrogen embrittlement is proposed as the underlying mechanism.

Strain energy release rate as a function of temperature and preloading history utilizing the edge delamination fatique test method

NASA Technical Reports Server (NTRS)

Zimmerman, Richard S.; Adams, Donald F.

1989-01-01

Static laminate and tension-tension fatigue tests of IM7/8551-7 composite materials was performed. The Edge Delamination Test (EDT) was utilized to evaluate the temperature and preloading history effect on the critical strain energy release rate. Static and fatigue testing was performed at room temperature and 180 F (82 C). Three preloading schemes were used to precondition fatigue test specimens prior to performing the normal tension-tension fatigue EDT testing. Computer software was written to perform all fatigue testing while monitoring the dynamic modulus to detect the onset of delamination and record the test information for later retrieval and reduction.

Behavioral responses to annual temperature variation alter the dominant energy pathway, growth, and condition of a cold-water predator

PubMed Central

Blanchfield, Paul J.; Rennie, Michael D.

2017-01-01

There is a pressing need to understand how ecosystems will respond to climate change. To date, no long-term empirical studies have confirmed that fish populations exhibit adaptive foraging behavior in response to temperature variation and the potential implications this has on fitness. Here, we use an unparalleled 11-y acoustic telemetry, stable isotope, and mark–recapture dataset to test if a population of lake trout (Salvelinus namaycush), a cold-water stenotherm, adjusted its use of habitat and energy sources in response to annual variations in lake temperatures during the open-water season and how these changes translated to the growth and condition of individual fish. We found that climate influenced access to littoral regions in spring (data from telemetry), which in turn influenced energy acquisition (data from isotopes), and growth (mark–recapture data). In more stressful years, those with shorter springs and longer summers, lake trout had reduced access to littoral habitat and assimilated less littoral energy, resulting in reduced growth and condition. Annual variation in prey abundance influenced lake trout foraging tactics (i.e., the balance of the number and duration of forays) but not the overall time spent in littoral regions. Lake trout greatly reduced their use of littoral habitat and occupied deep pelagic waters during the summer. Together, our results provide clear evidence that climate-mediated behavior can influence the dominant energy pathways of top predators, with implications ranging from individual fitness to food web stability. PMID:28808011

Old-growth definition for western juniper woodlands: Texas ashe juniper dominated or codominated communities. Forest Service general technical report

DOE Office of Scientific and Technical Information (OSTI.GOV)

Diamond, D.D.

1997-09-01

Ashe juniper dominated or codominated woodlands are extensive within the Edwards Plateu in Texas. Almost all contemporary woodlands are the result of various disturbances, especially grazing and fire suppression. Old-growth examples are rare. Several different geomorphic situations once supported natural Ashe juniper communities with different dynamics and composition. These included mesic slopes and canyon systems, shallow-soiled uplands (hardscrabble), and deeper-soiled uplants. The most extensive and most diverse woodlands were in canyon systems, where Ashe juniper shared dominance with a diversity of oaks and other broad-leaved trees, Drier upland woodlands were less diverse, with live oak, shin oak, and Vasey oakmore » variously important. Ashe junipr woodlands harbor a diverse biota, including rare and endemic species, and, thus, preservation of representative old-growth examples is an important conservation concern.« less

The Role of Growth Hormone and Insulin-Like Growth Factor-I in the Liver.

PubMed

Takahashi, Yutaka

2017-07-05

Adult growth hormone deficiency (GHD) is characterized by metabolic abnormalities associated with visceral obesity, impaired quality of life, and increased mortality. Patients with adult GHD show increased prevalence of non-alcoholic fatty liver disease (NAFLD)/non-alcoholic steatohepatitis (NASH), and growth hormone (GH) replacement therapy has been shown to improve these conditions. It has also been demonstrated that a decrease in the GH insulin-like growth factor-I (IGF-I) axis is closely associated with the progression of general NAFLD, suggesting a physiological role of these hormones for the maintenance of the liver. NASH histologically demonstrates inflammation, necrosis, and fibrosis, in addition to steatosis (and is a serious disease because it can progress to liver cirrhosis and hepatocellular carcinoma in a subset of cases). While fibrosis determines the prognosis of the patient, efficacious treatment for fibrosis is crucial; however, it has not yet been established. Recent studies have clarified the essential roles of GH and IGF-I in the liver. GH profoundly reduces visceral fat, which plays an important role in the development of NAFLD. Furthermore, GH directly reduces lipogenesis in the hepatocytes. IGF-I induces cellular senescence and inactivates hepatic stellate cells, therefore ameliorating fibrosis. IGF-I treatment has been shown to improve animal models of NASH and cirrhosis, suggesting potential clinical applications of IGF-I in these conditions. In this review, I will focus on the important roles of GH and IGF-I in the liver, their underlying mechanisms, and their potential therapeutic applications.

Does increasing intrinsic water use efficiency (iWUE) stimulate tree growth at natural alpine timberline on the southeastern Tibetan Plateau?

NASA Astrophysics Data System (ADS)

Huang, Ru; Zhu, Haifeng; Liu, Xiaohong; Liang, Eryuan; Grießinger, Jussi; Wu, Guoju; Li, Xiaoxia; Bräuning, Achim

2017-01-01

Little is known about whether increasing iWUE (intrinsic water use efficiency) can stimulate tree growth in the temperature-limited natural timberlines. Here, we presented the basal area increment (BAI) and iWUE chronologies of Smith fir (Abies georgei var. smithii) from 1900 to 2006 at a high-elevation (ca. 4400 m a.s.l.) timberline in the humid Sygera Mountains, southeastern Tibetan Plateau (TP). The commonality analysis model was applied to investigate the relationships among BAI, temperatures, atmospheric CO2 concentration (Ca) and iWUE during 1961-2006, taking into account of both pure and joint effects. As illustrated by the commonality analysis model, the pure effect of Ca (39.15%) had more stronger influence on iWUE than that of the Tmean (annul mean temperature, 0.12%), but the joint effect between Ca and Tmean (49.79%) on iWUE was stronger than any pure effect for the raw data with an increasing trend. For the first-difference data with year-to-year variations, the pure effect of Ca (7.72%) on iWUE was stronger than that of Tmean (0.59%) and the joint effect between them (0.59%). All above imply the Ca is the dominant factor for iWUE both for the 46-year trend and interannual variations. In addition, as showed by the commonality analysis model, the pure effect of iWUE (17.57%) played a much more important role on BAI than that of temperatures (smt, mean temperature during June, July, August of current year, 5.92%; amt, mean temperature during September, October, November of previous year, 3.04%), while joint effects of iWUE and temperatures contributed more (27.96%; 13.90%; 16.47%) to the BAI than their pure effects for the raw data with an increasing linear trend. For the first-difference data with interannual variations, the pure effect of smt (12.45%) had much more effect on BAI than that of iWUE (5.49%), at the same time the joint iWUE and temperatures contributed less (3.56%; 1.9%; 1.31%) to the BAI than their pure effects. These results suggest that

Modeling delamination of FRP laminates under low velocity impact

NASA Astrophysics Data System (ADS)

Jiang, Z.; Wen, H. M.; Ren, S. L.

2017-09-01

Fiber reinforced plastic laminates (FRP) have been increasingly used in various engineering such as aeronautics, astronautics, transportation, naval architecture and their impact response and failure are a major concern in academic community. A new numerical model is suggested for fiber reinforced plastic composites. The model considers that FRP laminates has been constituted by unidirectional laminated plates with adhesive layers. A modified adhesive layer damage model that considering strain rate effects is incorporated into the ABAQUS / EXPLICIT finite element program by the user-defined material subroutine VUMAT. It transpires that the present model predicted delamination is in good agreement with the experimental results for low velocity impact.

Enoyl-Acyl Carrier Protein Reductase I (FabI) Is Essential for the Intracellular Growth of Listeria monocytogenes

PubMed Central

Ericson, Megan E.; Frank, Matthew W.

2016-01-01

Enoyl-acyl carrier protein reductase catalyzes the last step in each elongation cycle of type II bacterial fatty acid synthesis and is a key regulatory protein in bacterial fatty acid synthesis. Genes of the facultative intracellular pathogen Listeria monocytogenes encode two functional enoyl-acyl carrier protein isoforms based on their ability to complement the temperature-sensitive growth phenotype of Escherichia coli strain JP1111 [fabI(Ts)]. The FabI isoform was inactivated by the FabI selective inhibitor AFN-1252, but the FabK isoform was not affected by the drug, as expected. Inhibition of FabI by AFN-1252 decreased endogenous fatty acid synthesis by 80% and lowered the growth rate of L. monocytogenes in laboratory medium. Robust exogenous fatty acid incorporation was not detected in L. monocytogenes unless the pathway was partially inactivated by AFN-1252 treatment. However, supplementation with exogenous fatty acids did not restore normal growth in the presence of AFN-1252. FabI inactivation prevented the intracellular growth of L. monocytogenes, showing that neither FabK nor the incorporation of host cellular fatty acids was sufficient to support the intracellular growth of L. monocytogenes. Our results show that FabI is the primary enoyl-acyl carrier protein reductase of type II bacterial fatty acid synthesis and is essential for the intracellular growth of L. monocytogenes. PMID:27736774

Enoyl-Acyl Carrier Protein Reductase I (FabI) Is Essential for the Intracellular Growth of Listeria monocytogenes.

PubMed

Yao, Jiangwei; Ericson, Megan E; Frank, Matthew W; Rock, Charles O

2016-12-01

Enoyl-acyl carrier protein reductase catalyzes the last step in each elongation cycle of type II bacterial fatty acid synthesis and is a key regulatory protein in bacterial fatty acid synthesis. Genes of the facultative intracellular pathogen Listeria monocytogenes encode two functional enoyl-acyl carrier protein isoforms based on their ability to complement the temperature-sensitive growth phenotype of Escherichia coli strain JP1111 [fabI(Ts)]. The FabI isoform was inactivated by the FabI selective inhibitor AFN-1252, but the FabK isoform was not affected by the drug, as expected. Inhibition of FabI by AFN-1252 decreased endogenous fatty acid synthesis by 80% and lowered the growth rate of L. monocytogenes in laboratory medium. Robust exogenous fatty acid incorporation was not detected in L. monocytogenes unless the pathway was partially inactivated by AFN-1252 treatment. However, supplementation with exogenous fatty acids did not restore normal growth in the presence of AFN-1252. FabI inactivation prevented the intracellular growth of L. monocytogenes, showing that neither FabK nor the incorporation of host cellular fatty acids was sufficient to support the intracellular growth of L. monocytogenes Our results show that FabI is the primary enoyl-acyl carrier protein reductase of type II bacterial fatty acid synthesis and is essential for the intracellular growth of L. monocytogenes. Copyright © 2016, American Society for Microbiology. All Rights Reserved.

Analytical Solution for the Free Vibration Analysis of Delaminated Timoshenko Beams

PubMed Central

Abedi, Maryam

2014-01-01

This work presents a method to find the exact solutions for the free vibration analysis of a delaminated beam based on the Timoshenko type with different boundary conditions. The solutions are obtained by the method of Lagrange multipliers in which the free vibration problem is posed as a constrained variational problem. The Legendre orthogonal polynomials are used as the beam eigenfunctions. Natural frequencies and mode shapes of various Timoshenko beams are presented to demonstrate the efficiency of the methodology. PMID:24574879

Insulin-like growth factor-I receptor activity is essential for Kaposi's sarcoma growth and survival.

PubMed

Catrina, S-B; Lewitt, M; Massambu, C; Dricu, A; Grünler, J; Axelson, M; Biberfeld, P; Brismar, K

2005-04-25

Kaposi's sarcoma (KS) is a highly vascular tumour and is the most common neoplasm associated with human immunodeficiency virus (HIV-1) infection. Growth factors, in particular vascular endothelial growth factor (VEGF), have been shown to play an important role in its development. The role of insulin-like growth factors (IGFs) in the pathophysiology of different tumours led us to evaluate the role of IGF system in KS. The IGF-I receptors (IGF-IR) were identified by immunohistochemistry in biopsies taken from patients with different AIDS/HIV-related KS stages and on KSIMM cells (an established KS-derived cell line). Insulin-like growth factor-I is a growth factor for KSIMM cells with a maximum increase of 3H-thymidine incorporation of 130 +/- 27.6% (P < 0.05) similar to that induced by VEGF and with which it is additive (281 +/- 13%) (P < 0.05). Moreover, specific blockade of the receptor (either by alpha IR3 antibody or by picropodophyllin, a recently described selective IGF-IR tyrosine phosphorylation inhibitor) induced KSIMM apoptosis, suggesting that IGF-IR agonists (IGF-I and -II) mediate antiapoptotic signals for these cells. We were able to identify an autocrine loop essential for KSIMM cell survival in which IGF-II is the IGF-IR agonist secreted by the cells. In conclusion, IGF-I pathway inhibition is a promising therapeutical approach for KS tumours.

Solvent Assisted Delamination Crack Growth Behavior of Amorphous Thermoplastic Materials

DTIC Science & Technology

1989-02-01

72CRD285. October 1972. 4. Standard Method of Test for Plane- Strain Fracture Toughness of Metallic Materials. 1988 Annual Book of ASTM Standards, Technical...intensity factor K I or the associated strain energy release rate, G I . ASTM compact tension test yields stress intensity factor, KI, via Equation 1...are such that a constant deadweight load results in increasing strain energy release rate with increasing crack length. Figure 3 shows the neat resin

Characterization of the Edge Crack Torsion (ECT) Test for Mode III Fracture Toughness Measurement of Laminated Composites

NASA Technical Reports Server (NTRS)

Ratcliffe, James G.

2004-01-01

The edge crack torsion (ECT) test is designed to initiate mode III delamination growth in composite laminates. The test has undergone several design changes during its development. The objective of this paper was to determine the suitability of the current ECT test design a mode III fracture test. To this end, ECT tests were conducted on specimens manufactured from IM7/8552 and S2/8552 tape laminates. Three-dimensional finite element analyses were performed. The analysis results were used to calculate the distribution of mode I, mode II, and mode III strain energy release rate along the delamination front. The results indicated that mode IIIdominated delamination growth would be initiated from the specimen center. However, in specimens of both material types, the measured values of GIIIc exhibited significant dependence on delamination length. Load-displacement response of the specimens exhibited significant deviation from linearity before specimen failure. X-radiographs of a sample of specimens revealed that damage was initiated in the specimens prior to failure. Further inspection of the failure surfaces is required to identify the damage and determine that mode III delamination is initiated in the specimens.

Slab detachment during continental collision: Influence of crustal rheology and interaction with lithospheric delamination

NASA Astrophysics Data System (ADS)

Duretz, T.; Gerya, T. V.

2013-08-01

Collision between continents can lead to the subduction of continental material. If the crust remains coupled to the downgoing slab, a large buoyancy force is generated. This force slows down convergence and promotes slab detachment. If the crust resists to subduction, it may decouple from the downgoing slab and be subjected to buoyant extrusion. We employ two-dimensional thermo-mechanical modelling to study the importance of crustal rheology on the evolution of subduction-collision systems. We propose simple quantifications of the mechanical decoupling between lithospheric levels (σ*) and the potential for buoyant extrusion of the crust (ξ*). The modelling results indicate that a variable crustal rheological structure results in slab detachment, delamination, or the combination of both mechanisms. A strong crust provides coupling at the Moho (low σ*) and remains coherent during subduction (low ξ). It promotes deep subduction of the crust (180 km) and slab detachment. Exhumation occurs in coherent manners via eduction and thrusting. Slab detachment triggers the development of topography (> 4.5 km) close to the suture. A contrasting style of collision occurs using a weak crustal rheology. Mechanical decoupling at the Moho (high σ*) promotes the extrusion of the crust (high ξ), disabling slab detachment. Ongoing shortening leads to buckling of the crust and development of topography on the lower plate. Collisions involving rheologically layered crust allow decoupling at mid-crustal depths. This structure favours both the extrusion of upper crust and the subduction of the lower crust. Such collisions are successively affected by delamination and slab detachment. Topography develops together with the buoyant extrusion of crust onto the foreland and is further amplified by slab detachment. Our results suggest that the occurrence of both delamination (Apennines) and slab detachment (Himalayas) in orogens may indicate differences in the initial crustal structure of

Edge Delamination and Residual Properties of Drilled Carbon Fiber Composites with and without Short-Aramid-Fiber Interleaf

NASA Astrophysics Data System (ADS)

Sun, Zhi; Hu, Xiaozhi; Shi, Shanshan; Guo, Xu; Zhang, Yupeng; Chen, Haoran

2016-10-01

Edge delamination is frequently observed in carbon fiber reinforced plastic (CFRP) laminates after machining, due to the low fracture toughness of the resin interfaces between carbon fiber plies. In this study, the effects of incorporating tough aramid fibers into the brittle CFRP system are quantified by measuring the residual properties of bolted CFRP. By adding short-aramid-fiber interleaves in CFRP laminates, the residual tensile strength have been substantially increased by 14 % for twill-weave laminates and 45 % for unidirectional laminates respectively. Moreover, tensile failure was observed as the major mode of toughened laminates, in contrast to shear failure of plain laminates. The qualitative FEM results agreed well with the experimental results that edge delamination would cause relatively higher shear stress and therefore alter the failure mode from tensile failure to shear failure.

Separation of crack extension modes in orthotropic delamination models

NASA Technical Reports Server (NTRS)

Beuth, Jack L.

1995-01-01

In the analysis of an interface crack between dissimilar elastic materials, the mode of crack extension is typically not unique, due to oscillatory behavior of near-tip stresses and displacements. This behavior currently limits the applicability of interfacial fracture mechanics as a means to predict composite delamination. The Virtual Crack Closure Technique (VCCT) is a method used to extract mode 1 and mode 2 energy release rates from numerical fracture solutions. The mode of crack extension extracted from an oscillatory solution using the VCCT is not unique due to the dependence of mode on the virtual crack extension length, Delta. In this work, a method is presented for using the VCCT to extract Delta-independent crack extension modes for the case of an interface crack between two in-plane orthotropic materials. The method does not involve altering the analysis to eliminate its oscillatory behavior. Instead, it is argued that physically reasonable, Delta-independent modes of crack extension can be extracted from oscillatory solutions. Knowledge of near-tip fields is used to determine the explicit Delta dependence of energy release rate parameters. Energy release rates are then defined that are separated from the oscillatory dependence on Delta. A modified VCCT using these energy release rate definitions is applied to results from finite element analyses, showing that Delta-independent modes of crack extension result. The modified technique has potential as a consistent method for extracting crack extension modes from numerical solutions. The Delta-independent modes extracted using this technique can also serve as guides for testing the convergence of finite element models. Direct applications of this work include the analysis of planar composite delamination problems, where plies or debonded laminates are modeled as in-plane orthotropic materials.

Operation DOMINIC I-1962.

DTIC Science & Technology

1983-02-01

ISLAND DANGER AREA IS A CIRCLE WITH RADII" JOHNSTON ISLAND (1) 470 nm- ( 871 km) 30 APRIL-12 JUNE 1962 AND DANGER AREA 22 SEPTEMBER-1S OCTOBER 1962 (21...AFCRL. Prolect Report: Reference C. 2018 . .I Project 6.4 -- E- and F-Region Physical Chemistry Agencies: Air Force Cambtidge Research Laboratory (AFCRL...1076) USS RECLAIMER (ARS-42) LISSTO LOVANA (AO- 64) 0USS GURKE (00-783) 2 - USS HALSEY POWELL (DO-686) aJ H I TM SI L N SURFACE ZERO S10- 0 30 60 Go

Analysis of delamination related fracture processes in composites

NASA Technical Reports Server (NTRS)

Armanios, Erian A.

1992-01-01

This is a final report that summarizes the results achieved under this grant. The first major accomplishment is the development of the sublaminate modeling approach and shear deformation theory. The sublaminate approach allows the flexibility of considering one ply or groups of plies as a single laminated unit with effective properties. This approach is valid when the characteristic length of the response is small compared to the sublaminate thickness. The sublaminate approach was validated comparing its predictions with a finite element solution. A shear deformation theory represents an optimum compromise between accuracy and computational effort in delamination analysis of laminated composites. This conclusion was reached by applying several theories with increasing level of complexity to the prediction of interlaminar stresses and strain energy release rate in a double cracked-lap-shear configuration.

Capillary wave propagation during the delamination of graphene by the precursor films in electro-elasto-capillarity

PubMed Central

Zhu, Xueyan; Yuan, Quanzi; Zhao, Ya-Pu

2012-01-01

Molecular dynamics simulations were carried out to explore the capillary wave propagation induced by the competition between one upper precursor film (PF) on the graphene and one lower PF on the substrate in electro-elasto-capillarity (EEC). During the wave propagation, the graphene was gradually delaminated from the substrate by the lower PF. The physics of the capillary wave was explored by the molecular kinetic theory. Besides, the dispersion relation of the wave was obtained theoretically. The theory showed that the wave was controlled by the driving work difference of the two PFs. Simulating the EEC process under different electric field intensities (E), the wave velocity was found insensitive to E. We hope this research could expand our knowledge on the wetting, electrowetting and EEC. As a potential application, the electrowetting of the PF between the graphene and the substrate is a promising candidate for delaminating graphene from substrate. PMID:23226593

Arthroscopic repair of delaminated acetabular articular cartilage using fibrin adhesive. Results at one to three years.

PubMed

Stafford, Giles H; Bunn, Jonathan R; Villar, Richard N

2011-01-01

We describe one- to three-year results of a novel use of fibrin glue in the treatment of cartilage damage by arthroscopy in the hip. This technique uses the microfracture technique and fibrin adhesive to bond delaminated articular cartilage to the underlying subchondral bone. This is generally performed in conjunction with treatment of underlying pathology such as femoroacetabular impingement. Patients were assessed using the modified Harris Hip Score (MHHS) pre- and post-operatively, and statistical significance determined by Student's t-test. We report the mid-term results of 43 patients with femoroacetabular impingement who have undergone this technique for re-attachment of delaminated chondral flaps. There was a statistically significant improvement in MHHS at a mean of 28 months (16 to 42 months) after surgery (p<0.0001). The MHHS for pain improved significantly from 21.8 (95% CI 19.0 to 24.7) pre-operatively to 35.8 (95% CI 32.6 to 38.9) post-operatively (p<0.0001). The MHHS for function also showed significant, although more modest, improvements from 40.0 (95% CI 37.7 to 42.3) pre-operatively to 43.6 (95% CI 41.4 to 45.8) post-operatively (p=0.0006). There were three patients who had early (within 12 months of the index procedure) revision arthroscopy for iliopsoas pathology. Arthroscopic repair of delaminated acetabular articular cartilage using fibrin adhesive is a useful technique in the treatment of early cartilage damage. We have seen encouraging mid-term results, although further studies are warranted.

Some notes on the Roman domination number and Italian domination number in graphs

NASA Astrophysics Data System (ADS)

Hajibaba, Maryam; Jafari Rad, Nader

2017-09-01

An Italian dominating function (or simply, IDF) on a graph G = (V, E) is a function f : V → {0, 1, 2} that satisfies the property that for every vertex v ∈ V, with f(v) = 0, Σ u∈N(v) f(u) ≥ 2. The weight of an Italian dominating function f is defined as w(f) = f(V ) = Σ u∈V f(u). The minimum weight among all of the Italian dominating functions on a graph G is called the Italian domination number of G, and is denoted by γI (G). A double Roman dominating function (or simply, DRDF) is a function f : V → {0, 1, 2, 3} having the property that if f(v) = 0 for a vertex v, then v has at least two adjacent vertices assigned 2 under f or one adjacent vertex assigned 3 under f, and if f(v) = 1, then v has at least one neighbor with f(w) ≥ 2. The weight of a DRDF f is defined as the sum f(V) = Σ v∈V f(v), and the minimum weight of a DRDF on G is the double Roman domination number of G, denoted by γdR (G). In this paper we show that γdR (G)/2 ≤ γI (G) ≤ 2γdR (G)/3, and characterize all trees T with γI (T) = 2γdR (T)/3.

Effect of insulin-like growth factor-I during the early postnatal period in intrauterine growth-restricted rats.

PubMed

Ikeda, Naho; Shoji, Hiromichi; Suganuma, Hiroki; Ohkawa, Natsuki; Kantake, Masato; Murano, Yayoi; Sakuraya, Koji; Shimizu, Toshiaki

2016-05-01

Insulin-like growth factor-I (IGF-I) is essential for perinatal growth and development; low serum IGF-I has been observed during intrauterine growth restriction (IUGR). We investigated the effects of recombinant human (rh) IGF-I in IUGR rats during the early postnatal period. Intrauterine growth restriction was induced by bilateral uterine artery ligation in pregnant rats. IUGR pups were divided into two groups injected daily with rhIGF-I (2 mg/kg; IUGR/IGF-I, n = 16) or saline (IUGR/physiologic saline solution (PSS), n = 16) from postnatal day (PND) 7 to 13. Maternal sham-operated pups injected with saline were used as controls (control, n = 16). Serum IGF-I and IGF binding proteins (IGFBP) 3 and 5 were measured on PND25. The expression of Igf-i, IGF-I receptor (Igf-ir), Igfbp3, and 5 mRNA in the liver and brain was measured using real-time polymerase chain reaction on PND25. Immunohistochemical staining of the liver for IGF expression was performed. Mean bodyweight on PND3 and PND25 in the IUGR pups (IUGR/IGF-I and IUGR/PSS) was significantly lower than that of the control pups. Serum IGF-I and hepatic Igf-ir mRNA in the IUGR pups were significantly lower than those in the control pups. In the IUGR/IGF-I group, hepatic Igfbp3 mRNA and liver immunohistochemical staining were increased. In the IUGR/PSS and control pups, there were no significant differences between these two groups in serum IGFBP3 and IGFBP5, hepatic Igf-i and Igfbp-5 mRNA, or brain Igf mRNA. No benefits on body and brain weight gain but an effective increase in hepatic IGFBP-3 was observed after treatment with 2 mg/kg rhIGF-I during the early postnatal period. © 2015 Japan Pediatric Society.

Intermediate mass black holes in AGN discs - I. Production and growth

NASA Astrophysics Data System (ADS)

McKernan, B.; Ford, K. E. S.; Lyra, W.; Perets, H. B.

2012-09-01

Here we propose a mechanism for efficiently growing intermediate mass black holes (IMBH) in discs around supermassive black holes. Stellar mass objects can efficiently agglomerate when facilitated by the gas disc. Stars, compact objects and binaries can migrate, accrete and merge within discs around supermassive black holes. While dynamical heating by cusp stars excites the velocity dispersion of nuclear cluster objects (NCOs) in the disc, gas in the disc damps NCO orbits. If gas damping dominates, NCOs remain in the disc with circularized orbits and large collision cross-sections. IMBH seeds can grow extremely rapidly by collisions with disc NCOs at low relative velocities, allowing for super-Eddington growth rates. Once an IMBH seed has cleared out its feeding zone of disc NCOs, growth of IMBH seeds can become dominated by gas accretion from the active galactic nucleus (AGN) disc. However, the IMBH can migrate in the disc and expand its feeding zone, permitting a super-Eddington accretion rate to continue. Growth of IMBH seeds via NCO collisions is enhanced by a pile-up of migrators. We highlight the remarkable parallel between the growth of IMBH in AGN discs with models of giant planet growth in protoplanetary discs. If an IMBH becomes massive enough it can open a gap in the AGN disc. IMBH migration in AGN discs may stall, allowing them to survive the end of the AGN phase and remain in galactic nuclei. Our proposed mechanisms should be more efficient at growing IMBH in AGN discs than the standard model of IMBH growth in stellar clusters. Dynamical heating of disc NCOs by cusp stars is transferred to the gas in an AGN disc helping to maintain the outer disc against gravitational instability. Model predictions, observational constraints and implications are discussed in a companion paper (Paper II).

A new failure mechanism in thin film by collaborative fracture and delamination: Interacting duos of cracks

NASA Astrophysics Data System (ADS)

Marthelot, Joël; Bico, José; Melo, Francisco; Roman, Benoît

2015-11-01

When a thin film moderately adherent to a substrate is subjected to residual stress, the cooperation between fracture and delamination leads to unusual fracture patterns, such as spirals, alleys of crescents and various types of strips, all characterized by a robust characteristic length scale. We focus on the propagation of a duo of cracks: two fractures in the film connected by a delamination front and progressively detaching a strip. We show experimentally that the system selects an equilibrium width on the order of 25 times the thickness of the coating and independent of both fracture and adhesion energies. We investigate numerically the selection of the width and the condition for propagation by considering Griffith's criterion and the principle of local symmetry. In addition, we propose a simplified model based on the criterion of maximum of energy release rate, which provides insights of the physical mechanisms leading to these regular patterns, and predicts the effect of material properties on the selected width of the detaching strip.

Local delamination in laminates with angle ply matrix cracks. Part 1: Tension tests and stress analysis

NASA Technical Reports Server (NTRS)

Obrien, T. Kevin; Hooper, S. J.

1991-01-01

Quasi-static tension tests were conducted on AS4/3501-6 graphite epoxy laminates. Dye penetrant enhanced x-radiography was used to document the onset of matrix cracking and the onset of local delaminations at the intersection of the matrix cracks and the free edge. Edge micrographs taken after the onset of damage were used to verify the location of the matrix cracks and local delamination through the laminate thickness. A quasi-3D finite element analysis was conducted to calculate the stresses responsible for matrix cracking in the off-axis plies. Laminated plate theory indicated that the transverse normal stresses were compressive. However, the finite element analysis yielded tensile transverse normal stresses near the free edge. Matrix cracks formed in the off-axis plies near the free edge where in-plane transverse stresses were tensile and had their greatest magnitude. The influence of the matrix crack on interlaminar stresses is also discussed.

Geochemical and petrological evidence of the subduction of delaminated Adriatic continental lithosphere in the genesis of the Neogene-Quaternary magmatism of central Italy

NASA Astrophysics Data System (ADS)

Serri, G.; Innocenti, F.; Manetti, P.

1993-07-01

Serri, G., Innocenti, F. and Manetti, P., 1993. Geochemical and petrological evidence of the subduction of delaminated Adriatic continental lithosphere in the genesis of the Neogene-Quaternary magmatism of central Italy. In: M.J.R. Wortel, U. Hansen and R. Sabadini (Editors), Relationships between Mantle Processes and Geological Processes at or near The Earth's Surface. Tectonophysics, 223: 117-147. The Neogene-Quaternary magmatism of the northern Apenninic arc took place in four phases separated in space and time which become progressively younger from west to east: Phase I, 14 Ma; Phase II, 7.3-6.0 Ma; Phase III, 5.1-2.2 Ma; Phase IV, 1.3-0.1 Ma. This magmatism is the result of the activation of three physically separate sources: (1) the Adriatic continental crust, extracted from the mantle in the late Proterozoic; (2) a strongly refractory, recently K-enriched harzburgitic mantle located in the mechanical boundary layer (MBL) of the lithosphere; and (3) a recently metasomatized, cpx-rich mantle, compositionally variable from Iherzolite to wehrlite-clinopyroxenite, interpreted as an ephemerally K-enriched asthenosphere. The Adriatic continental crust is the dominant source of the acid plutonic and volcanic rocks of the Tuscan region. The acid magmatism is mostly found inside an ellipsoidal area (about 150 × 300 km) centred on Giglio Island, here defined as the Tuscan Crustal Dome. Within this area, mantle-derived magmas unaffected by important crustal contamination processes and mixing with crustal anatectic melts have so far not been found. Pure crustal magmas are rare but are represented, for example by some of the San Vincenzo and Roccastrada rhyolites. Virtually all the Tuscan acid centres show evidence of mixing with potassic mantle-derived magmas. Major and trace elements, as well as {87Sr }/{86Sr } and {143Nd }/{144Nd } data, on primitive rocks (Mg# > 65) reveal two groups of mantle-derived magmas. These define two distinct mantle enrichment trends, both

Investigation Analysis of Crack Growth Arresting with Fasteners in Hybrid Laminated Skin-Stiffener Joint

NASA Astrophysics Data System (ADS)

Jeevan Kumar, N.; Ramesh Babu, P.

2018-02-01

In recent years carbon fibre-reinforced polymers (CFRP) emerged its increasing demand in aerospace engineering. Due to their high specific strength to weight ratio, these composites offer more characteristics and considerable advantages compared to metals. Metals, unlike composites, offer plasticity effects to evade high stress concentrations during postbuckling. Under compressive load, composite structures show a wide range of damage mechanisms where a set of damage modes combined together might lead to the eventual structural collapse. Crack is one of the most critical damages in fiber composites, which are being employed in primary aircraft structures. A parametric study is conducted to investigate the arrest mechanism of the delamination or crack growth with installation of multiple fasteners when the delamination is embedded in between the skin and stiffener interface.

Insulin-like growth factor-I induces CLU expression through Twist1 to promote prostate cancer growth.

PubMed

Takeuchi, Ario; Shiota, Masaki; Beraldi, Eliana; Thaper, Daksh; Takahara, Kiyoshi; Ibuki, Naokazu; Pollak, Michael; Cox, Michael E; Naito, Seiji; Gleave, Martin E; Zoubeidi, Amina

2014-03-25

Clusterin (CLU) is cytoprotective molecular chaperone that is highly expressed in castrate-resistant prostate cancer (CRPC). CRPC is also characterized by increased insulin-like growth factor (IGF)-I responsiveness which induces prostate cancer survival and CLU expression. However, how IGF-I induces CLU expression and whether CLU is required for IGF-mediated growth signaling remain unknown. Here we show that IGF-I induced CLU via STAT3-Twist1 signaling pathway. In response to IGF-I, STAT3 was phosphorylated, translocated to the nucleus and bound to the Twist1 promoter to activate Twist1 transcription. In turn, Twist1 bound to E-boxes on the CLU promoter and activated CLU transcription. Inversely, we demonstrated that knocking down Twist1 abrogated IGF-I induced CLU expression, indicating that Twist1 mediated IGF-I-induced CLU expression. When PTEN knockout mice were crossed with lit/lit mice, the resultant IGF-I deficiency suppressed Twist1 as well as CLU gene expression in mouse prostate glands. Moreover, both Twist1 and CLU knockdown suppressed prostate cancer growth accelerated by IGF-I, suggesting the relevance of this signaling not only in an in vitro, but also in an in vivo. Collectively, this study indicates that IGF-I induces CLU expression through sequential activation of STAT3 and Twist1, and suggests that this signaling cascade plays a critical role in prostate cancer pathogenesis. Copyright © 2014 Elsevier Ireland Ltd. All rights reserved.

Fatigue degradation in compressively loaded composite laminates. [graphite-epoxy composites

NASA Technical Reports Server (NTRS)

Ramkumar, R. L.

1981-01-01

The effect of imbedded delaminations on the compression fatigue behavior of quasi-isotropic, T300/5208, graphite/epoxy laminates was investigated. Teflon imbedments were introduced during panel layup to create delaminations. Static and constant amplitude (R=10, omega = 10 Hz) fatigue tests were conducted. S-N data and half life residual strength data were obtained. During static compression loading, the maximum deflection of the buckled delaminated region was recorded. Under compression fatigue, growth of the imbedded delamination was identified as the predominant failure mode in most of the test cases. Specimens that exhibited others failures had a single low stiffness ply above the Teflon imbedment. Delamination growth during fatigue was monitored using DIB enhanced radiography. In specimens with buried delaminations, the dye penetrant (DIB) was introduced into the delaminated region through a minute laser drilled hole, using a hypodermic needle. A low kV, microfocus, X-ray unit was mounted near the test equipment to efficiently record the cyclic growth of buried delaminations on Polaroid film.

Observation of Intralaminar Cracking in the Edge Crack Torsion Specimen

NASA Technical Reports Server (NTRS)

Czabaj, Michael W.; Ratcliffe, James G.; Davidson, Barry D.

2013-01-01

The edge crack torsion (ECT) test is evaluated to determine its suitability for measuring fracture toughness associated with mode III delamination growth onset. A series of ECT specimens with preimplanted inserts with different lengths is tested and examined using nondestructive and destructive techniques. Ultrasonic inspection of all tested specimens reveals that delamination growth occurs at one interface ply beneath the intended midplane interface. Sectioning and optical microscopy suggest that the observed delamination growth results from coalescence of angled intralaminar matrix cracks that form and extend across the midplane plies. The relative orientation of these cracks is approximately 45 deg with respect to the midplane, suggesting their formation is caused by resolved principal tensile stresses arising due to the global mode-III shear loading. Examination of ECT specimens tested to loads below the level corresponding to delamination growth onset reveals that initiation of intralaminar cracking approximately coincides with the onset of nonlinearity in the specimen's force-displacement response. The existence of intralaminar cracking prior to delamination growth onset and the resulting delamination extension at an unintended interface render the ECT test, in its current form, unsuitable for characterization of mode III delamination growth onset. The broader implications of the mechanisms observed in this study are also discussed with respect to the current understanding of shear-driven delamination in tape-laminate composites.

Strain Rate Sensitivity of Polymer-Matrix Composites under Mode I delamination

DTIC Science & Technology

1990-12-01

unstable growth system requires two values. In reality , the fracture toughness may vary along the length of the specimen due to strain rate effects...18 M. F. Kanninen. An Augmented Double Cantilever Beam Model for Studying Crack Propagation and Arrest. International Journal of Fracture. Vol. 9

Insulin-like growth factor-I, physical activity, and control of cellular anabolism.

PubMed

Nindl, Bradley C

2010-01-01

The underlying mechanisms responsible for mediating the beneficial outcomes of exercise undoubtedly are many, but the insulin-like growth factor-I (IGF-I) system is emerging as an important and central hormonal axis that plays a significant role concerning cellular anabolism. This introductory article summarizes the intent and the content for papers presented as part of a 2008 American College of Sports Medicine national symposium entitled "Insulin-like Growth Factor-I, Physical Activity, and Control of Cellular Anabolism." The individual authors and their papers are as follows: Jan Frystyk authoring "The relationship between exercise and the growth hormone/insulin-like growth factor-I axis," Greg Adams authoring "IGF-I signaling in skeletal muscle and the potential for cytokine interactions," and Brad Nindl authoring "Insulin-like growth factor-I as a biomarker of health, fitness, and training status." These papers focus on 1) different assay methodologies for IGF-I within the paradigm of exercise studies, 2) research demonstrating that intracellular signaling components associated with several proinflammatory cytokines have the potential to interact with anabolic signaling processes in skeletal muscle, and 3) an overview of IGF-I as a biomarker related to exercise training, muscle and bone remodeling, body composition, cognition, and cancer. When summed in total, the contribution that these papers will make will undoubtedly involve bringing attention to the vast regulatory complexity of the IGF-I system and will hopefully convince the reader that the IGF-I system warrants further detailed scientific inquiry to resolve many unanswered questions and paradoxical experimental findings. The IGF-I system remains one of the most intriguing and captivating marvels of human physiology that seems central in mediating numerous adaptations from physical activity.

Berberine slows cell growth in autosomal dominant polycystic kidney disease cells

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bonon, Anna; Mangolini, Alessandra; Pinton, Paolo

Highlights: •Berberine at appropriate doses slows cell proliferation in ADPKD cystic cells. •Reduction of cell growth by berberine occurs by inhibition of ERK and p70-S6 kinase. •Higher doses of berberine cause an overall cytotoxic effect. •Berberine overdose induces apoptotic bodies formation and DNA fragmentation. •Antiproliferative properties of this drug make it a new candidate for ADPKD therapy. -- Abstract: Autosomal dominant polycystic kidney disease (ADPKD) is the most common hereditary monogenic disorder characterized by development and enlargement of kidney cysts that lead to loss of renal function. It is caused by mutations in two genes (PKD1 and PKD2) encoding formore » polycystin-1 and polycystin-2 proteins which regulate different signals including cAMP, mTOR and EGFR pathways. Abnormal activation of these signals following PC1 or PC2 loss of function causes an increased cell proliferation which is a typical hallmark of this disease. Despite the promising findings obtained in animal models with targeted inhibitors able to reduce cystic cell growth, currently, no specific approved therapy for ADPKD is available. Therefore, the research of new more effective molecules could be crucial for the treatment of this severe pathology. In this regard, we have studied the effect of berberine, an isoquinoline quaternary alkaloid, on cell proliferation and apoptosis in human and mouse ADPKD cystic cell lines. Berberine treatment slows cell proliferation of ADPKD cystic cells in a dose-dependent manner and at high doses (100 μg/mL) it induces cell death in cystic cells as well as in normal kidney tubule cells. However, at 10 μg/mL, berberine reduces cell growth in ADPKD cystic cells only enhancing G{sub 0}/G{sub 1} phase of cell cycle and inhibiting ERK and p70-S6 kinases. Our results indicate that berberine shows a selected antiproliferative activity in cellular models for ADPKD, suggesting that this molecule and similar natural compounds could open

Al-Fe interactions and growth enhancement in Melastoma malabathricum and Miscanthus sinensis dominating acid sulphate soils.

PubMed

Watanabe, Toshihiro; Jansen, Steven; Osaki, Mitsuru

2006-12-01

Plants growing in acid sulphate soils are subject to high levels of Al availability, which may have effects on the growth and distribution of these species. Although Fe availability is also high in acid sulphate soils, little is known about the effect of Fe on the growth of native plants in these soils. Two species dominating this soil type in Asia, viz. Melastoma malabathricum and Miscanthus sinensis were grown hydroponically in a nutrient solution with different concentrations of Al and Fe. Melastoma malabathricum is found to be sensitive to Fe (40 and 100 microm). Application of 500 microm Al, however, completely ameliorates Fe toxicity and is associated with a decrease of Fe concentration in shoots and roots. The primary reason for the Al-induced growth enhancement of M. malabathricum is considered to be the Al-induced reduction of toxic Fe accumulation in roots and shoots. Therefore, Al is nearly essential for M. malabathricum when growing in acid sulphate soils. In contrast, application of both Fe and Al does not reduce the growth of M. sinensis, and Al application does not result in lower shoot concentrations of Fe, suggesting that this grass species has developed different mechanisms for adaptation to acid sulphate soils.

Acute Delamination of Commercially Available Decellularized Osteochondral Allograft Plugs

PubMed Central

Degen, Ryan M.; Tetreault, Danielle; Mahony, Greg T.; Williams, Riley J.

2016-01-01

Articular cartilage injuries, and corresponding surgical procedures, are occurring with increasing frequency as identified by a review of recent surgical trends. Concerns have grown in recent years regarding the longevity of results following microfracture, with a shift toward cartilage restoration procedures in recent years. This case report describes 2 cases of acute failure following the use of commercially available osteochondral allograft plugs used for the treatment of osteochondral defects of the distal femur. In both cases the chondral surface of the plug delaminated from the underlying cancellous bone, resulting in persistent pain and swelling requiring reoperation and removal of the loose fragments. Caution should be employed when considering use of these plugs for the treatment of osteochondral lesions, as similar outcomes have not been noted with other cartilage restoration techniques. PMID:27688840

Alps, Carpathians and Dinarides-Hellenides: about plates, micro-plates and delaminated crustal blocks

NASA Astrophysics Data System (ADS)

Schmid, Stefan

2014-05-01

Before the onset of Europe-Africa continental collision in the Dinarides-Hellenides (around 60Ma) and in the Alps and Western Carpathians (around 35 Ma), and at a large scale, the dynamics of orogenic processes in the Mediterranean Alpine chains were governed by Europe-Africa plate convergence leading to the disappearance of large parts of intervening oceanic lithosphere, i.e. the northern branch of Neotethys along the Sava-Izmir-Ankara suture and Alpine Tethys along the Valais-Magura suture (Schmid et al. 2008). In spite of this, two major problems concerning the pre-collisional stage are still poorly understood: (1) by now we only start to understand geometry, kinematics and dynamics of the along-strike changes in the polarity of subduction between Alps-Carpathians and Dinarides-Hellenides, and (2) it is not clear yet during exactly which episodes and to what extent intervening rifted continental fragments such as, for example, Iberia-Briançonnais, Tisza, Dacia, Adria-Taurides moved independently as micro-plates, and during which episodes they remained firmly attached to Europa or Africa from which they broke away. As Europe-Africa plate convergence slowed down well below 1 cm/yr at around 30 Ma ago these pre-collisional processes driven by plate convergence on a global scale gave way to more local processes of combined roll-back and crustal delamination in the Pannonian basin of the Carpathian embayment and in the Aegean (as well as in the Western Mediterranean, not discussed in this contribution). In the case of the Carpathian embayment E-directed roll back totally unrelated to Europe-Africa N-S-directed convergence, started at around 20 Ma ago, due to the presence relict oceanic lithosphere in the future Pannonian basin that remained un-subducted during collision. Due to total delamination of the crust from the eastward rolling back European mantle lithosphere the anticlockwise rotating ALCAPA crustal block, consisting of Eastern Alps and Western Carpathian

Regulation of insulin-like growth factor I receptors on vascular smooth muscle cells by growth factors and phorbol esters.

PubMed

Ververis, J J; Ku, L; Delafontaine, P

1993-06-01

Insulin-like growth factor I (IGF I) is an important mitogen for vascular smooth muscle cells. To characterize regulation of vascular IGF I receptors, we performed radioligand displacement experiments using rat aortic smooth muscle cells (RASMs). Serum deprivation for 48 hours caused a 40% decrease in IGF I receptor number. Exposure of quiescent RASMs to platelet-derived growth factor (PDGF), fibroblast growth factor (FGF), or angiotensin II (Ang II) caused a 1.5-2.0-fold increase in IGF I receptors per cell. After FGF exposure, there was a marked increase in the mitogenic response to IGF I. IGF I downregulated its receptors in the presence of platelet-poor plasma. Stimulation of protein kinase C (PKC) by exposure of quiescent RASMs to phorbol 12-myristate 13-acetate caused a biphasic response in IGF I binding; there was a 42% decrease in receptor number at 45 minutes and a 238% increase at 24 hours. To determine the role of PKC in growth factor-induced regulation of IGF I receptors, we downregulated PKC by exposing RASMs to phorbol 12,13-dibutyrate (PDBu) for 48 hours. PDGF- and FGF- but not Ang II-mediated upregulation of IGF I receptors was completely inhibited in PDBu-treated cells. Thus, acute PKC activation by phorbol esters inhibits IGF I binding, whereas chronic PKC activation increases IGF I binding. PDGF and FGF but not Ang II regulate vascular IGF I receptors through a PKC-dependent pathway. These data provide new insights into the regulation of vascular smooth muscle cell IGF I receptors in vitro and are of potential importance in characterizing vascular proliferative responses in vivo.

Numerical modeling of guided ultrasonic waves generated and received by piezoelectric wafer in a Delaminated composite beam

NASA Astrophysics Data System (ADS)

Xu, G. D.; Xu, B. Q.; Xu, C. G.; Luo, Y.

2017-05-01

A spectral finite element method (SFEM) is developed to analyze guided ultrasonic waves in a delaminated composite beam excited and received by a pair of surface-bonded piezoelectric wafers. The displacements of the composite beam and the piezoelectric wafer are represented by Timoshenko beam and Euler Bernoulli theory respectively. The linear piezoelectricity is used to model the electrical-mechanical coupling between the piezoelectric wafer and the beam. The coupled governing equations and the boundary conditions in time domain are obtained by using the Hamilton's principle, and then the SFEM are formulated by transforming the coupled governing equations into frequency domain via the discrete Fourier transform. The guided waves are analyzed while the interaction of waves with delamination is also discussed. The elements needed in SFEM is far fewer than those for finite element method (FEM), which result in a much faster solution speed in this study. The high accuracy of the present SFEM is verified by comparing with the finite element results.

Towards a damage tolerance philosophy for composite materials and structures

NASA Technical Reports Server (NTRS)

O'Brien, T. Kevin

1990-01-01

A damage-threshold/fail-safe approach is proposed to ensure that composite structures are both sufficiently durable for economy of operation, as well as adequately fail-safe or damage tolerant for flight safety. Matrix cracks are assumed to exist throughout the off-axis plies. Delamination onset is predicted using a strain energy release rate characterization. Delamination growth is accounted for in one of three ways: either analytically, using delamination growth laws in conjunction with strain energy release rate analyses incorporating delamination resistance curves; experimentally, using measured stiffness loss; or conservatively, assuming delamination onset corresponds to catastrophic delamination growth. Fail-safety is assessed by accounting for the accumulation of delaminations through the thickness. A tension fatigue life prediction for composite laminates is presented as a case study to illustrate how this approach may be implemented. Suggestions are made for applying the damage-threshold/fail-safe approach to compression fatigue, tension/compression fatigue, and compression strength following low velocity impact.

Towards a damage tolerance philosophy for composite materials and structures

NASA Technical Reports Server (NTRS)

Obrien, T. Kevin

1988-01-01

A damage-threshold/fail-safe approach is proposed to ensure that composite structures are both sufficiently durable for economy of operation, as well as adequately fail-safe or damage tolerant for flight safety. Matrix cracks are assumed to exist throughout the off-axis plies. Delamination onset is predicted using a strain energy release rate characterization. Delamination growth is accounted for in one of three ways: either analytically, using delamination growth laws in conjunction with strain energy release rate analyses incorporating delamination resistance curves; experimentally, using measured stiffness loss; or conservatively, assuming delamination onset corresponds to catastrophic delamination growth. Fail-safety is assessed by accounting for the accumulation of delaminations through the thickness. A tension fatigue life prediction for composite laminates is presented as a case study to illustrate how this approach may be implemented. Suggestions are made for applying the damage-threshold/fail-safe approach to compression fatigue, tension/compression fatigue, and compression strength following low velocity impact.

Early height growth of ponderosa pine forecasts dominance in plantations

Treesearch

William W. Oliver; Robert F. Powers

1971-01-01

Future crown class may be determined well in advance of intertree competition in plantation grown ponderosa pine. Regardless of site quality, dominant trees in 10 California plantations reached breast height ½ year sooner than codominants and 1-½ years sooner than intermediates. Dominant trees on poor sites reached breast height several years earlier than has been...

Synthesis and structures of ligand-dominated one-dimensional silver(I)–bis(pyridylmethyl)amine coordination chains

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lin, Hung-Jui; Liu, Yu-Chiao; Tseng, Yu-Jui

2016-10-15

Reactants slow diffusion of Ag(I) salts with 3,4′-bis(pyridylmethyl)amine (3,4′-bpma), an unsymmetric bis-pyridyl ligand equipped with a non-innocent amine backbone, afforded polymeric coordination adducts 1–5 having a general formula ([Ag(3,4′-bpma)(solv)]X){sub n} (solv = H{sub 2}O, CH{sub 3}OH, and none; X= CF{sub 3}CO{sub 2}{sup –}, BF{sub 4}{sup –}, ClO{sub 4}{sup –}, CF{sub 3}SO{sub 3}{sup –}, and SbF{sub 6}{sup –}). Single-crystal X-ray diffraction (SCXRD) analyses reveal that colorless crystals of Ag(I) coordination polymers (CPs) 1–5 have very similar one-dimensional (1D) non-flat chain structures, which are preferentially depicted as a “zipper-like” rather than a ladder-like or a double-stranded chain topologies. The 3,4′-bpma ligand inmore » these Ag(I) CPs displays a μ{sub 3}-bridging mode with a gauche–trans (1,4, and 5) and a trans–trans (2 and 3) conformations. Noteworthy, anions do not show strong influence on structural modulation of Ag(I) CPs in the solid state, but really affect CP conformations and packing fashions, indicative of a ligand-dominated assembly process for such a Ag(I)–3,4′-bpma system. Thermal stabilities and solid-state photoluminescence properties of crystalline materials 1–5 were investigated. - Graphical abstract: This work has addressed five ligand-dominated Ag(I)–3,4′-bpma polymeric adducts, which show similar one-dimensional non-flat chain structures depicting a “zipper-like” topology rather than a ladder-like or a double-stranded chain structures.« less

Apical Dominance in Plants

ERIC Educational Resources Information Center

Tucker, D. J.

1974-01-01

Describes a tentative hypothesis for the control of plant branching (apical dominance). Explores the mechanism by which apical buds inhibit the growth of axillary buds on the same shoot. Presents an up-to-date picture of the problem and gives economic implications of the study. (BR)

Autocrine and/or paracrine insulin-like growth factor-I activity in skeletal muscle

NASA Technical Reports Server (NTRS)

Adams, Gregory R.

2002-01-01

Similar to bone, skeletal muscle responds and adapts to changes in loading state via mechanisms that appear to be intrinsic to the muscle. One of the mechanisms modulating skeletal muscle adaptation it thought to involve the autocrine and/or paracrine production of insulinlike growth factor-I. This brief review outlines components of the insulinlike growth factor-I system as it relates to skeletal muscle and provides the rationale for the theory that insulinlike growth factor-I is involved with muscle adaptation.

Reversion of autocrine transformation by a dominant negative platelet-derived growth factor mutant.

PubMed

Vassbotn, F S; Andersson, M; Westermark, B; Heldin, C H; Ostman, A

1993-07-01

A non-receptor-binding mutant of the platelet-derived growth factor (PDGF) A chain, PDGF-0, was generated by exchanging 7 amino acids in the sequence. The mutant chains formed dimers that were similar to wild-type PDGF-AA with regard to stability and rate of processing to the mature 30-kDa secreted forms. Moreover, the mutant chains formed disulfide-bonded heterodimers with the PDGF B chain in NIH 3T3 cells heterodimer underwent the same processing and secretion as PDGF-AB. Transfection of c-sis-expressing 3T3 cells with PDGF-0 significantly inhibited the transformed phenotype of these cells, as determined by the following criteria. (i) Compared with PDGF-0-negative clones, PDGF-0-producing clones showed a reverted morphology. (ii) Clones producing PDGF-0 grew more slowly than PDGF-0-negative clones, with a fivefold difference in cell number after 14 days in culture. (iii) The expression of PDGF-0 completely inhibited the ability of the c-sis-expressing 3T3 cells to form colonies in soft agar; this inhibition was overcome by the addition of recombinant PDGF-BB to the culture medium, showing that the lack of colony formation of these cells was not due to a general unresponsiveness to PDGF. The specific expression of a PDGF-0/PDGF wild-type heterodimer in COS cells revealed that the affinity of the mutant heterodimer for the PDGF alpha receptor was decreased by approximately 50-fold compared with that of PDGF-AA. Thus, we show that a non-receptor-binding PDGF A-chain mutant neutralizes in a trans-dominant manner the autocrine transforming potential of the c-sis/PDGF B chain by forming low-affinity heterodimers with wild-type PDGF chains. This method of specifically antagonizing the effect of PDGF may be useful in investigations of the role of PDGF in normal and pathological conditions.

Correlation of ankle eversion to inversion strength ratio and static balance in dominant and non-dominant limbs of basketball players.

PubMed

Dabadghav, Rachana

2016-04-01

To compare ankle eversion to inversion strength ratio (E/I R) and static balance control between the dominant and non-dominant limbs of basketball players and to correlate ankle E/I R and static balance control in the dominant and non-dominant limbs of basketball players. Twenty-one healthy basketball players in the age-group of 18-25 years participated in this study. Isokinetic ankle eversion and inversion muscle strength was assessed at 30°/s and 120°/s in both dominant and non-dominant limbs using the Biodex isokinetic dynamometer. Similarly balance was assessed on a force platform with eyes open and eyes closed in both dominant and non-dominant limbs. Repeated measure ANOVA for strength measurement, found that there was significant main effect of speed, P=0.001 (P<0.05). However, there was no significant main effect in the sides P=0.099 (P<0.05).There was significant main effect of sides with respect to balance. Balance was affected more in non-dominant limb P=0.000 as compared to dominant limb. However, there was not much of a significant difference with eyes open and eyes closed position. The E/I ratio was >1.0 at the angular velocity of 120°/s increasing the chances of ankle injuries in basketball players. There was no correlation between ankle strength and balance in both dominant and non-dominant limbs.

Comparison of histologic healing and biomechanical characteristics between repair techniques for a delaminated rotator cuff tear in rabbits.

PubMed

Cheon, Sang-Jin; Kim, Jung-Han; Gwak, Heui-Chul; Kim, Chang-Wan; Kim, Jeon-Kyo; Park, Ji-Hwan

2017-05-01

The purpose of this study was to compare histologic healing and biomechanical characteristics between 2 repair techniques (layer by layer, repair of each layer to bone separately; and whole layer, repair of each layer to the bone en masse) for delaminated rotator cuff tear. Rabbits were used as subjects and classified into 2 groups: group A, right side, the layer-by-layer repair group; and group B, left side, the whole-layer repair group. Histologic evaluations were done at 3 weeks (n = 7) and 6 weeks (n = 4) after operation. Biomechanical tests to evaluate the tensile property were done at time 0 (n = 5) and 3 weeks (n = 5) after operation. Histologic healing improved in all groups. A smaller cleft was found between layers in group B compared with the cleft in group A at 3 weeks after operation. At time 0, group A showed a higher yield load and ultimate failure load (67 ± 10.5 N and 80 ± 7.8 N, respectively). However, at 3 weeks after operation, group B showed a higher yield load (48 ± 7.6 N). In the delaminated rotator cuff tear model in the rabbit, the whole-layer repair showed a narrow gap between layers and a higher yield load at 3 weeks after operation. Surgical techniques that unite the cleft in a delaminated tear could improve biomechanical strength after operation. Copyright © 2017 Journal of Shoulder and Elbow Surgery Board of Trustees. Published by Elsevier Inc. All rights reserved.

Differences in xylogenesis between dominant and suppressed trees.

PubMed

Liu, Shushan; Li, Xiaoxia; Rossi, Sergio; Wang, Lily; Li, Wei; Liang, Eryuan; Leavitt, Steven W

2018-05-01

Most dendroecological studies focus on dominant trees, but little is known about the growing season of trees belonging to different size classes and their sensitivity to biotic factors. The objective of this study was to compare the dynamics of xylem formation between dominant and suppressed trees of Abies fabri of similar age growing in the Gongga Mountains, southeastern Tibetan Plateau, and to identify the association between xylem growth and climate. The timing and duration of xylogenesis in histological sections were investigated weekly during the 2013-2015 growing seasons. Our investigation found that timing and duration of xylogenesis varied with canopy position and its associated tree size. Xylogenesis started 6-14 days earlier, and ended 5-11 days later in dominant trees than in suppressed trees, resulting in a significantly longer growing season. Dominant trees also exhibited higher temperature sensitivity of tracheid production rate than suppressed trees. The observed differences in xylogenesis among trees suggested that competition affects tree growth by reducing the growing period in suppressed trees. Representative climate-growth relationships should involve trees of all size classes when evaluating the effects of the environment on forest dynamics. © 2018 Botanical Society of America.

Colocalization of insulin-like growth factor-binding protein with insulin-like growth factor I.

PubMed

Kobayashi, S; Clemmons, D R; Venkatachalam, M A

1991-07-01

We report the localization of insulin-like growth factor I (IGF-I) and a 25-kDa form of insulin-like growth factor-binding protein (IGF-BP-1) in adult rat kidney. The antigens were localized using a rabbit anti-human IGF-I antibody, and a rabbit anti-human IGF-BP-1 antibody raised against human 25-kDa IGF-BP-1 purified from amniotic fluid. Immunohistochemistry by the avidin-biotin peroxidase conjugate technique showed that both peptides are located in the same nephron segments, in the same cell types. The most intense staining was in papillary collecting ducts. There was moderate staining also in cortical collecting ducts and medullary thick ascending limbs of Henle's loop. In collecting ducts the antigens were shown to be present in principal cells but not in intercalated cells. In distal convoluted tubules, cortical thick ascending limbs, and in structures presumptively identified as thin limbs of Henle's loops there was only modest staining. The macula densa, however, lacked immunoreactivity. Colocalization of IGF-I and IGF-BP-1 in the same cells supports the notion, derived from studies on cultured cells, that the actions of IGF-I may be modified by IGF-BPs that are present in the same location.

Elevated temperature crack growth in advanced powder metallurgy aluminum alloys

NASA Technical Reports Server (NTRS)

Porr, William C., Jr.; Gangloff, Richard P.

1990-01-01

Rapidly solidified Al-Fe-V-Si powder metallurgy alloy FVS0812 is among the most promising of the elevated temperature aluminum alloys developed in recent years. The ultra fine grain size and high volume fraction of thermally stable dispersoids enable the alloy to maintain tensile properties at elevated temperatures. In contrast, this alloy displays complex and potentially deleterious damage tolerant and time dependent fracture behavior that varies with temperature. J-Integral fracture mechanics were used to determine fracture toughness (K sub IC) and crack growth resistance (tearing modulus, T) of extruded FVS0812 as a function of temperature. The alloy exhibits high fracture properties at room temperature when tested in the LT orientation, due to extensive delamination of prior ribbon particle boundaries perpendicular to the crack front. Delamination results in a loss of through thickness constraint along the crack front, raising the critical stress intensity necessary for precrack initiation. The fracture toughness and tensile ductility of this alloy decrease with increasing temperature, with minima observed at 200 C. This behavior results from minima in the intrinsic toughness of the material, due to dynamic strain aging, and in the extent of prior particle boundary delaminations. At 200 C FVS0812 fails at K levels that are insufficient to cause through thickness delamination. As temperature increases beyond the minimum, strain aging is reduced and delamination returns. For the TL orientation, K (sub IC) decreased and T increased slightly with increasing temperature from 25 to 316 C. Fracture in the TL orientation is governed by prior particle boundary toughness; increased strain localization at these boundaries may result in lower toughness with increasing temperature. Preliminary results demonstrate a complex effect of loading rate on K (sub IC) and T at 175 C, and indicate that the combined effects of time dependent deformation, environment, and strain aging

Insulin-Like Growth Factor-I is a Marker for the Nutritional State

PubMed Central

Hawkes, Colin P; Grimberg, Adda

2017-01-01

Measurement of the serum concentration of insulin-like growth factor-1 (IGF-I) is generally used as a screening investigation for disorders of the growth hormone (GH)/IGF-I axis in children and adolescents with short stature. IGF-I concentration is sensitive to short-term and chronic alterations in the nutritional state, and the interpretation of IGF-I measurements requires knowledge of the child’s nutritional status. In this review, we summarize the effects of nutrition on the GH/IGF-I axis, and review the clinical implications of these interactions throughout childhood, both in under-nutrition and over-nutrition. PMID:26841638

Long-term auxological and pubertal outcome of patients with hereditary insulin-like growth factor-I deficiency (Laron and growth hormone-gene deletion syndrome) treated with recombinant human insulin-like growth factor-I.

PubMed

Messina, M F; Arrigo, T; Valenzise, M; Ghizzoni, L; Caruso-Nicoletti, M; Zucchini, S; Chiabotto, P; Crisafulli, G; Zirilli, G; De Luca, F

2011-04-01

GH-IGF-I axis is mainly involved in the complex process of somatic growth but emerging evidence suggests that it also influences hypothalamic-pituitary-gonadal (HPG) function. We report some data regarding long-term auxological and pubertal outcome of five female patients with hereditary forms of GH-IGF-I deficiency (Laron and GH-gene deletion syndrome) and a mean age of 23.4±5.3 yr (range 19-32). All the patients received recombinant human IGF-I (rhIGF-I, Pharmacia and Upjohn, Stockholm, Sweden, and rhIGF-I, Genentech, San Francisco, CA, USA) from a mean age of 8.6 yr (range 3.2-14.2) up to the final height. Final height was very disappointing (≤ -5.0 SD scores) and lower than target height in all the patients. Pubertal onset was delayed in most of them but menarche occurred spontaneously in all the patients. Median age at menarche was 15.1 yr. Menstrual cycles were regular for several years. Median duration of gynecological follow- up was 8.3 yr with the longest span of 17.2 yr. We can assert that GH-IGF-I axis has an essential role in promoting linear growth in humans and its physiological action cannot be replaced by pharmacological treatment in most patients with hereditary forms of IGF-I insufficiency as demonstrated by their subnormal final height. Our clinical observations can also support an essential role of IGF-I in genitalia growth but not in the function of HPG axis as demonstrated by the maintenance of regular menstrual cycles in the presence of subnormal levels of IGF-I after treatment discontinuation.

Insulin-like growth factor I: a biologic maturation indicator.

PubMed

Ishaq, Ramy Abdul Rahman; Soliman, Sanaa Abou Zeid; Foda, Manal Yehya; Fayed, Mona Mohamed Salah

2012-11-01

Determination of the maturation level and the subsequent evaluation of growth potential during preadolescence and adolescence are important for optimal orthodontic treatment planning and timing. This study was undertaken to evaluate the applicability of insulin-like growth factor I (IGF-I) blood level as a maturation indicator by correlating it to the cervical vertebral maturation index. The study was conducted with 120 subjects, equally divided into 60 males (ages, 10-18 years) and 60 females (ages, 8-16 years). A lateral cephalometric radiograph and a blood sample were taken from each subject. For each subject, cervical vertebral maturation and IGF-I serum level were assessed. Mean values of IGF-I in each stage of cervical vertebral maturation were calculated, and the means in each stage were statistically compared with those of the other stages. The IGF-I mean value at each cervical vertebral maturation stage was statistically different from the mean values at the other stages. The highest mean values were observed in stage 4, followed by stage 5 in males and stage 3 in females. IGF-I serum level is a reliable maturation indicator that could be applied in orthodontic diagnosis. Copyright © 2012 American Association of Orthodontists. Published by Mosby, Inc. All rights reserved.

[Physiological significance of IGF-I and its binding proteins on fetal growth and maturation].

PubMed

Iwashita, M

1994-08-01

Insulin-like growth factor-I (IGF-I) is one of growth factors that circulates bound to specific, high affinity binding proteins (IGFBPs). Physiological significance of IGF-I and IGFBPs on fetal growth is investigated in this study. In mother, circulating levels of IGF-I are increased during pregnancy in which placental hormones take the place of pituitary GH to regulate IGF-I during pregnancy and correlates with fetal birth weight. IGFBPs except IGFBP-1 in the maternal circulation are markedly reduced compared to those of non pregnant women due to increased activity of protease(s) while IGFBP-1 gradually increased throughout pregnancy and negatively correlates with fetal weight. IGF-I stimulated 3H-AIB uptake and release by cultured trophoblast cells in a dose dependent manner. Furthermore, fetal growth and the transfer of 3H-AIB to fetus is inhibited when IGF-I is neutralized by polyclonal antibody. These results indicate that maternal IGF-I stimulates fetal growth by activating placental transport of nutrients to fetus. In contrast, IGFBP-1 inhibits both 125I-IGF-I binding to placental membrane and 3H-glycine uptake of trophoblast cells by IGF-I in a dose dependent manner. Moreover, fetal growth and the transfer of 3H-AIB to fetus are accelerated when IGFBP-1 is neutralized by polyclonal antibody, suggesting that maternal IGFBP-1 inhibits fetal growth by inhibiting IGF-I action on the placenta. IGF-I and four IGFBPs including IGFBP-1, -2, -3, and -4 are localized in cytotrophoblast of term placenta. Similarly IGFBP-1, -2, and -4 are detected in medium conditioned by term decidua cells by Western ligand blot in which release of IGFBP-1 and -4 are diminished by IGF-I and all three IGFBPs are increased by progesterone. Thus, there is a complicated autocrine/paracrine regulation between decidua and placenta and IGF-I action on fetal growth is presumed to be modified by this local regulation. Fetal levels of IGF-I and IGFBP-1 are positively and negatively correlate

Evolution of the Archean Mohorovičić discontinuity from a synaccretionary 4.5 Ga protocrust

NASA Astrophysics Data System (ADS)

Hamilton, Warren B.

2013-12-01

This review evaluates and rejects the currently dominant dogmas of geodynamics and geochemistry, which are based on 1950s-1970s assumptions of a slowly differentiating Earth. Evidence is presented for evolution of mantle, crust, and early Moho that began with fractionation of most crustal components, synchronously with planetary accretion, into mafic protocrust by ~ 4.5 Ga. We know little about Hadean crustal geology (> 3.9 Ga) except that felsic rocks were then forming, but analogy with Venus, and dating from the Moon, indicate great shallow disruption by large and small impact structures, including huge fractionated impact-melt constructs, throughout that era. The mantle sample and Archean (< 3.9 Ga) crustal geology integrate well. The shallow mantle was extremely depleted by early removal of thick mafic protocrust, which was the primary source of the tonalite, trondhjemite, and granodiorite (TTG) that dominate preserved Archean crust to its base, and of the thick mafic volcanic rocks erupted on that crust. Lower TTG crust, kept mobile by its high radioactivity and by insulating upper crust, rose diapirically into the upper crust as dense volcanic rocks sagged synformally. The mobile lower crust simultaneously flowed laterally to maintain subhorizontal base and surface, and dragged overlying brittler granite-and-greenstone upper crust. Petrologically required garnet-rich residual protocrust incrementally delaminated, sank through low-density high-mantle magnesian dunite, and progressively re-enriched upper mantle, mostly metasomatically. Archean and earliest Proterozoic craton stabilization and development of final Mohos followed regionally complete early delamination of residual protocrust, variously between ~ 2.9 and 2.2 Ga. Where some protocrust remained, Proterozoic basins, filled thickly by sedimentary and volcanic rocks, developed on Archean crust, beneath which delamination of later residual protocrust continued top-down enrichment of upper mantle. That

An Optical Interferometric Triaxial Displacement Sensor for Structural Health Monitoring: Characterization of Sliding and Debonding for a Delamination Process

PubMed Central

Chen, Yizheng; Zhuang, Yiyang; Du, Yang; Gerald, Rex E.; Tang, Yan

2017-01-01

This paper presents an extrinsic Fabry–Perot interferometer-based optical fiber sensor (EFPI) for measuring three-dimensional (3D) displacements, including interfacial sliding and debonding during delamination. The idea employs three spatially arranged EFPIs as the sensing elements. In our sensor, the three EFPIs are formed by three endfaces of three optical fibers and their corresponding inclined mirrors. Two coincident roof-like metallic structures are used to support the three fibers and the three mirrors, respectively. Our sensor was calibrated and then used to monitor interfacial sliding and debonding between a long square brick of mortar and its support structure (i.e., a steel base plate) during the drying/curing process. This robust and easy-to-manufacture triaxial EFPI-based 3D displacement sensor has great potential in structural health monitoring, the construction industry, oil well monitoring, and geotechnology. PMID:29165351

An Optical Interferometric Triaxial Displacement Sensor for Structural Health Monitoring: Characterization of Sliding and Debonding for a Delamination Process.

PubMed

Zhu, Chen; Chen, Yizheng; Zhuang, Yiyang; Du, Yang; Gerald, Rex E; Tang, Yan; Huang, Jie

2017-11-22

This paper presents an extrinsic Fabry-Perot interferometer-based optical fiber sensor (EFPI) for measuring three-dimensional (3D) displacements, including interfacial sliding and debonding during delamination. The idea employs three spatially arranged EFPIs as the sensing elements. In our sensor, the three EFPIs are formed by three endfaces of three optical fibers and their corresponding inclined mirrors. Two coincident roof-like metallic structures are used to support the three fibers and the three mirrors, respectively. Our sensor was calibrated and then used to monitor interfacial sliding and debonding between a long square brick of mortar and its support structure (i.e., a steel base plate) during the drying/curing process. This robust and easy-to-manufacture triaxial EFPI-based 3D displacement sensor has great potential in structural health monitoring, the construction industry, oil well monitoring, and geotechnology.

Evidence that insulin-like growth factor I and growth hormone are required for prostate gland development.

PubMed

Ruan, W; Powell-Braxton, L; Kopchick, J J; Kleinberg, D L

1999-05-01

Insulin-like growth factor I (IGF-I) has been implicated as a factor that may predispose one to prostate cancer. However, no specific relationship between IGF-I and prostate development or cancer in vivo has been established. To determine whether IGF-I was important in prostate development, we examined prostate architecture in IGF-I(-/-) null mice and wild-type littermates. Glands from 44-day-old IGF-I-deficient animals were not only smaller than those from wild-type mice, but also had fewer terminal duct tips and branch points and deficits in tertiary and quaternary branching (P < 0.0001), indicating a specific impairment in gland structure. Administration of des(1-3)-IGF-I for 7 days partially reversed the deficit by increasing those parameters of prostate development (P < 0.006). That IGF-I production probably mediates an effect of GH in this process was indicated by the observations that GH antagonist transgenic mice also had significantly impaired prostate development (P < 0.0002) and that bovine GH had no independent effect on stimulating prostate development in IGF-I null animals. The data indicate that IGF-I deficiency is the proximate cause of impaired prostate development and give credence to the idea that, like testosterone, GH and IGF-I may be involved in prostate cancer growth as an extension of a normal process.

Rare co-occurrence of osteogenesis imperfecta type I and autosomal dominant polycystic kidney disease.

PubMed

Hoefele, Julia; Mayer, Karin; Marschall, Christoph; Alberer, Martin; Klein, Hanns-Georg; Kirschstein, Martin

2016-11-01

There are several clinical reports about the co-occurrence of autosomal dominant polycystic kidney disease (ADPKD) and connective tissue disorders. A simultaneous occurrence of osteogenesis imperfecta (OI) type I and ADPKD has not been observed so far. This report presents the first patient with OI type I and ADPKD. Mutational analysis of PKD1 and COL1A1 in the index patient revealed a heterozygous mutation in each of the two genes. Mutational analysis of the parents indicated the mother as a carrier of the PKD1 mutation and the father as a carrier of the COL1A1 mutation. The simultaneous occurrence of both disorders has an estimated frequency of 3.5:100 000 000. In singular cases, ADPKD can occur in combination with other rare disorders, e.g. connective tissue disorders.

MOCVD growth and study of thin films of indium nitride

NASA Astrophysics Data System (ADS)

Jain, Abhishek

This thesis is focused on a study of MOCVD growth of InN with the goal of providing new information on the effects of growth conditions and buffer/substrate materials on InN film properties. Initial studies, using both (111) Si and (0001) sapphire substrates, identified an optimum growth temperature window of 540--560°C for the formation of stable InN films. When attempting to grow InN films on sapphire with thicknesses greater than approximately 150 nanometers using an AlN buffer layer, the InN films were observed to delaminate from the buffer/substrate at growth temperature. The combined effect of compressive stress due to high lattice mismatch between InN and AlN (˜14%) and tensile stress due to grain coalescence along with the relatively weak bond strength of InN compared to GaN and AlN, is believed to cause the InN film to crack along the interface and delaminate. To further investigate the effect of the buffer layer on InN growth, studies were carried out using GaN films grown on sapphire as the growth template. Recent MBE results had indicated a significant difference in the thermal stability and growth mode of In-polar and N-polar InN, with improved properties reported for N-polar material grown on N-polar GaN. MOCVD growth of N-polar GaN is very difficult; consequently, all of the results reported in the literature for InN growth on GaN were likely carried out on Ga-polar material resulting in films with a high surface roughness. By utilizing N-polar and Ga-polar GaN films, it was possible to produce N-polar and In-polar InN films by MOCVD, as determined by convergent beam electron diffraction (CBED) analysis. Furthermore, the polarity was found to dramatically alter the surface roughness and growth mode of the InN films with enhanced lateral growth and reduced surface roughness obtained for N-polar InN. A qualitative model was proposed to explain the different growth mechanisms observed for In-polar and N-polar InN. In spite of the improvements in

Skeletal Effects of Growth Hormone and Insulin-like Growth Factor-I Therapy

PubMed Central

Lindsey, Richard C.; Mohan, Subburaman

2015-01-01

The growth hormone/insulin-like growth factor (GH/IGF) axis is critically important for the regulation of bone formation, and deficiencies in this system have been shown to contribute to the development of osteoporosis and other diseases of low bone mass. The GH/IGF axis is regulated by a complex set of hormonal and local factors which can act to regulate this system at the level of the ligands, receptors, IGF binding proteins (IGFBPs), or IGFBP proteases. A combination of in vitro studies, transgenic animal models, and clinical human investigations has provided ample evidence of the importance of the endocrine and local actions of both GH and IGF-I, the two major components of the GH/IGF axis, in skeletal growth and maintenance. GH- and IGF-based therapies provide a useful avenue of approach for the prevention and treatment of diseases such as osteoporosis. PMID:26408965

Conventional En Masse Repair Versus Separate Double-Layer Double-Row Repair for the Treatment of Delaminated Rotator Cuff Tears.

PubMed

Kim, Yang-Soo; Lee, Hyo-Jin; Jin, Hong-Ki; Kim, Sung-Eun; Lee, Jin-Woo

2016-05-01

The rotator cuff tendon is known to exert a shear force between the superficial and deep layers. Owing to this characteristic, separate repair of delaminated rotator cuff tears has been introduced for the restoration of the physiological biomechanics of the rotator cuff. However, whether conventional en masse repair or separate repair is superior is controversial in terms of outcomes. To compare clinical outcomes between conventional en masse repair and separate double-layer double-row repair for the treatment of delaminated rotator cuff tears. Randomized controlled study; Level of evidence, 2. Between August 2007 and March 2014, a total of 82 patients who underwent arthroscopic rotator cuff repair of a delaminated tear were enrolled and randomized into 2 groups. In group 1 (n = 48), arthroscopic conventional en masse repair was performed. In group 2 (n = 34), separate double-layer double-row repair was performed. The American Shoulder and Elbow Surgeons score, Constant score, Simple Shoulder Test score, and visual analog scale (VAS) score for pain and range of motion (ROM) were assessed before surgery; at 3, 6, and 12 months after surgery; and at the last follow-up visit. Magnetic resonance imaging (MRI) was performed at 12 months postoperatively to examine the retear rate and pattern. There was no significant difference between groups in the preoperative demographic data, including patient age, sex, symptom duration, tear size, and functional scores (P > .05). The mean follow-up period was 25.9 ± 1.2 months. Significant improvements in functional and pain scores were observed in both groups at the last follow-up visit. However, no significant differences in functional scores and ROM were found between the 2 groups at each time point, except that group 2 had significantly lower VAS pain scores (P < .05) at 3, 6, and 12 months postoperatively. Eight (17%) of 48 patients in group 1 and 6 (18%) of 34 patients in group 2 showed retears on MRI at 12-month follow-up (P

Modeling of delamination in carbon/epoxy composite laminates under four point bending for damage detection and sensor placement optimization

NASA Astrophysics Data System (ADS)

Adu, Stephen Aboagye

Laminated carbon fiber-reinforced polymer composites (CFRPs) possess very high specific strength and stiffness and this has accounted for their wide use in structural applications, most especially in the aerospace industry, where the trade-off between weight and strength is critical. Even though they possess much larger strength ratio as compared to metals like aluminum and lithium, damage in the metals mentioned is rather localized. However, CFRPs generate complex damage zones at stress concentration, with damage progression in the form of matrix cracking, delamination and fiber fracture or fiber/matrix de-bonding. This thesis is aimed at performing; stiffness degradation analysis on composite coupons, containing embedded delamination using the Four-Point Bend Test. The Lamb wave-based approach as a structural health monitoring (SHM) technique is used for damage detection in the composite coupons. Tests were carried-out on unidirectional composite coupons, obtained from panels manufactured with pre-existing defect in the form of embedded delamination in a laminate of stacking sequence [06/904/0 6]T. Composite coupons were obtained from panels, fabricated using vacuum assisted resin transfer molding (VARTM), a liquid composite molding (LCM) process. The discontinuity in the laminate structure due to the de-bonding of the middle plies caused by the insertion of a 0.3 mm thick wax, in-between the middle four (4) ninety degree (90°) plies, is detected using lamb waves generated by surface mounted piezoelectric (PZT) actuators. From the surface mounted piezoelectric sensors, response for both undamaged (coupon with no defect) and damaged (delaminated coupon) is obtained. A numerical study of the embedded crack propagation in the composite coupon under four-point and three-point bending was carried out using FEM. Model validation was then carried out comparing the numerical results with the experimental. Here, surface-to-surface contact property was used to model the

Growth on ATP elicits a P-stress response in the picoeukaryote Micromonas pusilla

DOE PAGES

Whitney, LeAnn P.; Lomas, Michael W.

2016-05-11

The surface waters of oligotrophic oceans have chronically low phosphate (P i) concentrations, which renders dissolved organic phosphorus (DOP) an important nutrient source. In the subtropical North Atlantic, cyanobacteria are often numerically dominant, but picoeukaryotes can dominate autotrophic biomass and productivity making them important contributors to the ocean carbon cycle. Despite their importance, little is known regarding the metabolic response of picoeukaryotes to changes in phosphorus (P) source and availability. To understand the molecular mechanisms that regulate P utilization in oligotrophic environments, we evaluated transcriptomes of the picoeukaryote Micromonas pusilla grown under P i-replete and -deficient conditions, with an additionalmore » investigation of growth on DOP in replete conditions. Genes that function in sulfolipid substitution and P i uptake increased in expression with P i-deficiency, suggesting cells were reallocating cellular P and increasing P acquisition capabilities. P i-deficient M. pusilla cells also increased alkaline phosphatase activity and reduced their cellular P content. Cells grown with DOP were able to maintain relatively high growth rates, however the transcriptomic response was more similar to the P i-deficient response than that seen in cells grown under P i-replete conditions. The results demonstrate that not all P sources are the same for growth; while M. pusilla, a model picoeukaryote, may grow well on DOP, the metabolic demand is greater than growth on P i. Lastly, these findings provide insight into the cellular strategies which may be used to support growth in a stratified future ocean predicted to favor picoeukaryotes.« less

Temperature cycling vapor deposition HgI.sub.2 crystal growth

DOEpatents

Schieber, Michael M.; Beinglass, Israel; Dishon, Giora

1977-01-01

A method and horizontal furnace for vapor phase growth of HgI.sub.2 crystals which utilizes controlled axial and radial airflow to maintain the desired temperature gradients. The ampoule containing the source material is rotated while axial and radial air tubes are moved in opposite directions during crystal growth to maintain a desired distance and associated temperature gradient with respect to the growing crystal, whereby the crystal interface can advance in all directions, i.e., radial and axial according to the crystallographic structure of the crystal. Crystals grown by this method are particularly applicable for use as room-temperature nuclear radiation detectors.

Growth of arachnoid cysts in patients with autosomal dominant polycystic kidney disease: serial imaging and clinical relevance

PubMed Central

Krauer, Fabienne; Ahmadli, Uzeyir; Kollias, Spyros; Bleisch, Jörg; Wüthrich, Rudolf P.; Serra, Andreas L.; Poster, Diane

2012-01-01

Background Autosomal dominant polycystic kidney disease (ADPKD) is an inherited disorder that results in the growth of cysts in the kidneys and other organs. Multisystemic involvement is common including affection of the central nervous system with cerebral aneurysms and arachnoid cysts. Methods This is a prospective cohort study to investigate the prevalence and growth rate of arachnoid cysts in ADPKD patients. Participants enrolled in the SUISSE ADPKD cohort were offered cranial imaging for the detection of intracranial alterations. In the case of identified arachnoid cysts, patients were suggested to undergo follow-up imaging to assess the growth rate of the cysts. Volume of arachnoid cysts at the baseline and at follow-up visits was assessed by manual segmentation on a dedicated workstation. Results A total of 109 ADPKD patients agreed to undergo cranial imaging. In 14 (12.8%) patients (9 males and 5 females), 18 singular arachnoid cysts were identified. The baseline volumes of individual cysts ranged from 1.8 to 337.6 cm3. During a mean follow-up period of 24 months, the volume changes of 12 individual arachnoid cysts of nine patients ranged from −3.1 to 3.7 cm3. Cystic lesions were mostly localized in the middle fossa. All affected patients were clinically asymptomatic. Conclusions We found a higher prevalence of arachnoid cysts in ADPKD patients with more advanced disease. There was a large variability in size and growth. These arachnoid cysts were clinically silent and their growth pattern was subtle and unpredictable, in contrast to the much more foreseeable growth of the renal cysts. PMID:26019816

PERK eIF2alpha kinase regulates neonatal growth by controlling the expression of circulating insulin-like growth factor-I derived from the liver.

PubMed

Li, Yulin; Iida, Kaori; O'Neil, Jeff; Zhang, Peichuan; Li, Sheng'ai; Frank, Ami; Gabai, Aryn; Zambito, Frank; Liang, Shun-Hsin; Rosen, Clifford J; Cavener, Douglas R

2003-08-01

Humans afflicted with the Wolcott-Rallison syndrome and mice deficient for PERK (pancreatic endoplasmic reticulum eIF2alpha kinase) show severe postnatal growth retardation. In mice, growth retardation in Perk-/- mutants is manifested within the first few days of neonatal development. Growth parameters of Perk-/- mice, including comparison of body weight to length and organ weights, are consistent with proportional dwarfism. Tibia growth plates exhibited a reduction in proliferative and hypertrophic chondrocytes underlying the longitudinal growth retardation. Neonatal Perk-/- deficient mice show a 75% reduction in liver IGF-I mRNA and serum IGF-I within the first week, whereas the expression of IGF-I mRNA in most other tissues is normal. Injections of IGF-I partially reversed the growth retardation of the Perk-/- mice, whereas GH had no effect. Transgenic rescue of PERK activity in the insulin- secreting beta-cells of the Perk-/- mice reversed the juvenile but not the neonatal growth retardation. We provide evidence that circulating IGF-I is derived from neonatal liver but is independent of GH at this stage. We propose that PERK is required to regulate the expression of IGF-I in the liver during the neonatal period, when IGF-I expression is GH-independent, and that the lack of this regulation results in severe neonatal growth retardation.

The behavior of delaminations in composite materials - experimental results

NASA Astrophysics Data System (ADS)

Chermoshentseva, A. S.; Pokrovskiy, A. M.; Bokhoeva, L. A.

2016-02-01

Delamination is one of the most common failure modes of composite materials. It may occur as a consequence of imperfections in the production process or the effects of external factors during the operational life of the composite laminates, such as the impact by foreign objects. This paper presents the results of mechanical tests and the optimum degrees of filling the composite materials (CM) with hydrophobic powder (Tarkosil T-20) depending on the latter mass concentration. The results present test samples of the CM with the underlying interlayer defects. The samples were fabricated of twenty-ply pre-preg (fiberglass or carbon fiber). The industrial grade glass is T-25 (VM) specification 6-11-380-76. The composite materials have nanosized additives in structure. The volume concentration of nanopowders is varying from 0.1% to 0.5%. This kind of research has been done for the first time.

Few-Layer MXenes Delaminated via High-Energy Mechanical Milling for Enhanced Sodium-Ion Batteries Performance.

PubMed

Wu, Yuting; Nie, Ping; Wang, Jiang; Dou, Hui; Zhang, Xiaogang

2017-11-15

The global availability of sodium makes the exploration of superior sodium-ion batteries attractive for energy storage application. MXenes, as one of the most promising anodes for sodium-ion batteries, have been reported to have many advantages, such as high electronic conductivity and a hydrophilic surface. However, the compact multilayer structure and deficient delamination significantly inhibits their application, requiring high energy and showing decreased storage capacity and poor rate capabilities. Few-layer MXene has been proved to benefit superior electrochemical properties with a better ionic conductivity and two-dimensional layer structure. Herein, we report scale delamination of few-layer MXene nanosheets as anodes for sodium-ion batteries, which are prepared via an organic solvent assist high-energy mechanical-milling method. This approach efficiently prevents the oxidation of MXene and produces few-layer nanosheets structure, facilitating fast electron transport and Na + diffusion. Electrochemical tests demonstrate that the few-layer MXenes show high specific capacity, excellent cycle stability, and good rate performance. Specifically, few-layer MXene nanosheets deliver a high reversible capacity of 267 mA h g -1 at a current density of 0.1 A g -1 . After cycling 1500 cycles at a high rate of 1 A g -1 , a reversible capacity of 76 mA h g -1 could be maintained.

Insulin-like growth factor-I (lGF-l): safety and efficacy.

PubMed

Laron, Zvi

2004-11-01

Insulin-like growth factor I (IGF-I) is a peptide synthesized mainly in the liver by stimulation by pituitary growth hormone (GH). It circulates almost entirely bound to its binding proteins. It is the anabolic effector hormone of GH. It is the only treatment in states of GH resistance such as Laron syndrome and blocking antibodies to human GH. As it suppresses insulin and GH secretion it has been used in states of insulin resistance including Type II diabetes mellitus. IGF-I is administered by once or twice daily injections. Adverse effects are mostly caused by overdosage. The usual daily dose in children ranges from 100-200 microg/kg.

Domination of hillslope denudation by tree uprooting in an old-growth forest

NASA Astrophysics Data System (ADS)

Phillips, Jonathan D.; Šamonil, Pavel; Pawlik, Łukasz; Trochta, Jan; Daněk, Pavel

2017-01-01

Razula forest preserve in the Carpathian Mountains of the Czech Republic is an unmanaged forest that has not been logged or otherwise anthropically disturbed for at least 83 years, preceded by only infrequent selective logging. We examined this 25 ha area to determine the dominant geomorphological processes on the hillslope. Tree uprooting displaces about 2.9 m3 of soil and regolith per year, representing about 1.5 uprooted trees ha- 1 yr- 1, based on forest inventory records dating back to 1972, and contemporary measurements of displaced soil and pit-mound topography resulting from uprooting. Pits and mounds occupy > 14% of the ground surface. Despite typical slope gradients of 0.05 mm- 1, and up to 0.41, little evidence of mass wasting (e.g., slump or flow scars or deposits, colluvial deposits) was noted in the field, except in association with pit-mound pairs. Small avalanche and ravel features are common on the upslope side of uproot pits. Surface runoff features were rare and poorly connected, but do include stemwash erosion associated with stemflow. No rills or channels were found above the valley bottom area, and only small, localized areas of erosion and forest litter debris indicating overland flow. Where these features occurred, they either disappeared a short distance downslope (indicating infiltration), or indicate flow into tree throw pits. Surface erosion is also inhibited by surface armoring of coarse rock fragments associated with uprooting, as well as by the nearly complete vegetation and litter cover. These results show that the combination of direct and indirect impacts of tree uprooting can dominate slope processes in old-growth, unmanaged forests. The greater observed expression of different hillslope processes in adjacent managed forests (where tree uprooting dynamics are blocked by management activities) suggests that human interventions can change the slope process regime in forest ecosystems.

The skeletal structure of insulin-like growth factor I-deficient mice

NASA Technical Reports Server (NTRS)

Bikle, D.; Majumdar, S.; Laib, A.; Powell-Braxton, L.; Rosen, C.; Beamer, W.; Nauman, E.; Leary, C.; Halloran, B.

2001-01-01

The importance of insulin-like growth factor I (IGF-I) for growth is well established. However, the lack of IGF-I on the skeleton has not been examined thoroughly. Therefore, we analyzed the structural properties of bone from mice rendered IGF-I deficient by homologous recombination (knockout [k/o]) using histomorphometry, peripheral quantitative computerized tomography (pQCT), and microcomputerized tomography (muCT). The k/o mice were 24% the size of their wild-type littermates at the time of study (4 months). The k/o tibias were 28% and L1 vertebrae were 26% the size of wild-type bones. Bone formation rates (BFR) of k/o tibias were 27% that of the wild-type littermates. The k/o bones responded normally to growth hormone (GH; 1.7-fold increase) and supranormally to IGF-I (5.2-fold increase) with respect to BFR. Cortical thickness of the proximal tibia was reduced 17% in the k/o mouse. However, trabecular bone volume (bone volume/total volume [BV/TV]) was increased 23% (male mice) and 88% (female mice) in the k/o mice compared with wild-type controls as a result of increased connectivity, increased number, and decreased spacing of the trabeculae. These changes were either less or not found in L1. Thus, lack of IGF-I leads to the development of a bone structure, which, although smaller, appears more compact.

Cutting Modeling of Hybrid CFRP/Ti Composite with Induced Damage Analysis

PubMed Central

Xu, Jinyang; El Mansori, Mohamed

2016-01-01

In hybrid carbon fiber reinforced polymer (CFRP)/Ti machining, the bi-material interface is the weakest region vulnerable to severe damage formation when the tool cutting from one phase to another phase and vice versa. The interface delamination as well as the composite-phase damage is the most serious failure dominating the bi-material machining. In this paper, an original finite element (FE) model was developed to inspect the key mechanisms governing the induced damage formation when cutting this multi-phase material. The hybrid composite model was constructed by establishing three disparate physical constituents, i.e., the Ti phase, the interface, and the CFRP phase. Different constitutive laws and damage criteria were implemented to build up the entire cutting behavior of the bi-material system. The developed orthogonal cutting (OC) model aims to characterize the dynamic mechanisms of interface delamination formation and the affected interface zone (AIZ). Special focus was made on the quantitative analyses of the parametric effects on the interface delamination and composite-phase damage. The numerical results highlighted the pivotal role of AIZ in affecting the formation of interface delamination, and the significant impacts of feed rate and cutting speed on delamination extent and fiber/matrix failure. PMID:28787824

Effects of sand burial on the survival and growth of two shrubs dominant in different habitats of northern China.

PubMed

Qu, Hao; Zhao, Ha-Lin; Zhao, Xue-Yong; Zuo, Xiao-An; Wang, Shao-Kun; Chen, Min

2017-04-01

Plants that grow in dune ecosystems always suffer from sand burial. Shrubs play implications on the healthy functioning of dune ecosystems due to control blowing sand. However, the survival and growth responses of shrubs to sand burial remain poorly understood. The survival rate and seedling height of two shrubs (Artemisia halodendron and Lespedeza davurica) along with the soil properties under different burial depths were examined in order to reveal the causing ecophysiological attributes of sand burial on shrubs in the desertified region. It was found that A. halodendron can survive a burial depth of 6 cm greater than its seedling height, which is a dominant shrub in mobile dunes with intense burial, whereas a burial depth equivalent to three fourths of its seedling height is detrimental to L. davurica, which is dominant in fixed dunes with less burial. The reasons for the shrub death under sand burial were associated with the physical barrier to vertical growth and the reduction in photosynthetic area. In conclusion, A. halodendron can facilitate the stabilization of mobile dunes because of their high tolerance to the frequent and intensive sand burial, while L. davurica can be beneficial for the recovery process because of their higher survival rates under shallow burial following restoration of mobile dunes.

Assessment of Composite Delamination Self-Healing Via Micro-Encapsulation

NASA Technical Reports Server (NTRS)

O'Brien, T. Kevin; White, Scott R.

2008-01-01

Composite skin/stringer flange debond specimens manufactured from composite prepreg containing interleaf layers with a polymer based healing agent encapsulated in thin walled spheres were tested. As a crack develops and grows in the base polymer, the spheres fracture releasing the healing agent. The agent reacts with catalyst and polymerizes healing the crack. In addition, through-thickness reinforcement, in the form of pultruded carbon z-pins were included near the flange tips to improve the resistance to debonding. Specimens were manufactured with 14 plies in the skin and 10 plies in the stiffener flange. Three-point bend tests were performed to measure the skin/stiffener debonding strength and the recovered strength after healing. The first three tests performed indicated no healing following unloading and reloading. Micrographs showed that delaminations could migrate to the top of the interleaf layer due to the asymmetric loading, and hence, bypass most of the embedded capsules. For two subsequent tests, specimens were clamped in reverse bending before reloading. In one case, healing was observed as evidenced by healing agent that leaked to the specimen edge forming a visible "scar". The residual strength measured upon reloading was 96% of the original strength indicating healing had occurred. Hence, self-healing is possible in fiber reinforced composite material under controlled conditions, i.e., given enough time and contact with pressure on the crack surfaces. The micro-encapsulation technique may prove more robust when capsule sizes can be produced that are small enough to be embedded in the matrix resin without the need for using an interleaf layer. However, in either configuration, the amount of healing that can occur may be limited to the volume of healing agent available relative to the crack volume that must be filled.

Growth of InSb and InI Crystals on Earth and in Microgravity

NASA Technical Reports Server (NTRS)

Ostrogorsky, A. G.; Churilov, A.; Volz, M. P.; Riabov, V.; Van den Berg, L.

2015-01-01

During the past 40 years, dozens of semiconductor crystal growth experiments have been conducted in space laboratories. The subsequent analysis of the space-grown crystals revealed (i) that weak convection existed in virtually all melt-growth experiments, (ii) de-wetting significantly reduced the level of stress-induced defects, and (iii) particularly encouraging results were obtained in vapor-growth experiments. In 2002, following a decade of ground based research in growing doped Ge and GaSb crystals, a series of crystal growth experiments was performed at the ISS, within the SUBSA (Solidification Using a Baffle in Sealed Ampoules) investigation. Te- and Zn-doped InSb crystals were grown from the melt. The specially designed furnace provided a side-view of the melt and precise seeding measurement of the growth rate. At present, under sponsorship of CASIS (Center for the Advancement of Science in Space, www.iss-casis.org), we are conducting ground-based experiments with indium mono-iodide (InI) in preparation for the "SUBSA II" ISS investigation, planned for 2017. The experiments include: i) Horizontal Bridgman (HB) growth and ii) Vapor Transport (VT) growth. Finite element modeling will also be conducted, to optimize the design of the flight ampoules, for vapor and melt growth.

Evolution of dominance in sporophytic self-incompatibility systems: I. Genetic load and coevolution of levels of dominance in pollen and pistil.

PubMed

Llaurens, Violaine; Billiard, Sylvain; Castric, Vincent; Vekemans, Xavier

2009-09-01

Recent theoretical advances have suggested that various forms of balancing selection may promote the evolution of dominance through an increase of the proportion of heterozygote genotypes. We test whether dominance can evolve in the sporophytic self-incompatibility (SSI) system in plants. SSI prevents mating between individuals expressing identical SI phenotypes by recognition of pollen by pistils, which avoids selfing and inbreeding depression. SI phenotypes depend on a complex network of dominance relationships between alleles at the self-incompatibility locus (S-locus). Empirical studies suggest that these relationships are not random, but the exact evolutionary processes shaping these relationships remain unclear. We investigate the expected patterns of dominance under the hypothesis that dominance is a direct target of natural selection. We follow the fate of a mutant allele at the S-locus whose dominance relationships are changed but whose specificity remains unaltered. We show that strict codominance is not evolutionarily stable in SSI, and that inbreeding depression due to deleterious mutations linked or unlinked to the S-locus exerts strong constraints on changes in relative levels of dominance in pollen and pistil. Our results provide a general adaptive explanation for most patterns of dominance relationships empirically observed in natural plant populations.

The Effect of Veneer Layers on the Bending Shear Strength and Delamination of Laminated Veneer Lumber (LVL) from Oil Palm Trunk (OPT)

NASA Astrophysics Data System (ADS)

Jamaludin, M. A.; Nordin, K.; Bahari, S. A.; Ahmad, M.

2010-03-01

The aim of this study was to evaluate the effects of the number of veneer layers on the bending shear strength and delamination of Laminated Veneer Lumber (LVL) from oil palm trunk (OPT). Five (5), Six (6) and Seven (7) veneer layers of OPT LVL were manufactured. The dimension of the boards was 45 cm by 45 cm by 1.9 cm. The boards were hot pressed for 13 minutes at a pressure of 31 kgf per m2. Urea formaldehyde (UF) supplied by a local adhesive manufacturer was used as the binder for the boards. The bending shear tests consisted of the edgewise and flatwise tests, whereas the delamination test consisted of the cold and hot water boil tests. The preparation of the test specimens and tests set-up was in accordance to the Japanese Standards, JAS-1991 [1]. Six replications were used for each test. The results were analyzed by Analysis of Variance (ANOVA) using the Duncan's Multiple Range Test to test for significant differences. The results indicated that as the number of layers increased the strength also increased. All the boards passed the standard. The difference in strength between the different types of samples was significant at 95 percent confidence level. Bending shear failures were primarily in the veneers. It is possible to use the boards as light weight interior building and furniture components. Over the years, the supply of quality timber resources from the natural forest has decrease as the wood-based industry experienced rapid growth. The supply of rubberwood for the furniture industry is also decreasing as a result of increase latex price. Accordingly, OPT LVL can be an alternative or supplementary raw material for the wood-based industry.

CO2 induced growth response in a diatom dominated phytoplankton community from SW Bay of Bengal coastal water

NASA Astrophysics Data System (ADS)

Biswas, Haimanti; Shaik, Aziz Ur Rahman; Bandyopadhyay, Debasmita; Chowdhury, Neha

2017-11-01

The ongoing increase in surface seawater CO2 level could potentially impact phytoplankton primary production in coastal waters; however, CO2 sensitivity studies on tropical coastal phytoplankton assemblages are rare. The present study investigated the interactive impacts of variable CO2 level, light and zinc (Zn) addition on the diatom dominated phytoplankton assemblages from the western coastal Bay of Bengal. Increased CO2 supply enhanced particulate organic matter (POC) production; a concomitant depletion in δ13CPOM values at elevated CO2 suggested increased CO2 diffusive influx inside the cell. Trace amount of Zn added under low CO2 level accelerated growth probably by accelerating Zn-Carbonic Anhydrase activity which helps in converting bicarbonate ion to CO2. Almost identical values of δ13CPOM in the low CO2 treated cells grown with and without Zn indicated a low discrimination between 13C and 12C probably due to bicarbonate uptake. These evidences collectively indicated the existence of the carbon concentration mechanisms (CCMs) at low CO2. A minimum growth rate was observed at low CO2 and light limited condition indicating light dependence of CCMs activity. Upon the increase of light and CO2 level, growth response was maximum. The cells grown in the low CO2 levels showed higher light stress (higher values of both diatoxanthin index and the ratio of photo-protective to light-harvesting pigments) that was alleviated by both increasing CO2 supply and Zn addition (probably by efficient light energy utilization in presence of adequate CO2). This is likely that the diatom dominated phytoplankton communities benefited from the increasing CO2 supply and thus may enhance primary production in response to any further increase in coastal water CO2 levels and can have large biogeochemical consequences in the study area.

Radial growth of two dominant montane conifer tree species in response to climate change in North-Central China.

PubMed

Jiang, Yuan; Zhang, Wentao; Wang, Mingchang; Kang, Muyi; Dong, Manyu

2014-01-01

North-Central China is a region in which the air temperature has clearly increased for several decades. Picea meyeri and Larix principis-rupprechtii are the most dominant co-occurring tree species within the cold coniferous forest belt ranging vertically from 1800 m to 2800 m a.s.l. in this region. Based on a tree-ring analysis of 292 increment cores sampled from 146 trees at different elevations, this study aimed to examine if the radial growth of the two species in response to climate is similar, whether the responses are consistent along altitudinal gradients and which species might be favored in the future driven by the changing climate. The results indicated the following: (1) The two species grew in different rhythms at low and high elevation respectively; (2) Both species displayed inconsistent relationships between radial growth and climate data along altitudinal gradients. The correlation between radial growth and the monthly mean temperature in the spring or summer changed from negative at low elevation into positive at high elevation, whereas those between the radial growth and the total monthly precipitation displayed a change from positive into negative along the elevation gradient. These indicate the different influences of the horizontal climate and vertical mountainous climate on the radial growth of the two species; (3) The species-dependent different response to climate in radial growth appeared mainly in autumn of the previous year. The radial growth of L. principis-rupprechtii displayed negative responses both to temperature and to precipitation in the previous September, October or November, which was not observed in the radial growth of P. meyeri. (4) The radial growth of both species will tend to be increased at high elevation and limited at low elevation, and L. principis-rupprechtii might be more favored in the future, if the temperature keeps rising.

The relationship between salivary insulin-like growth factor I and quantitative cervical maturational stages of skeletal maturity.

PubMed

Nayak, Subash; Bhad Patil, Wasundhara A; Doshi, Umal Hiralal

2014-09-01

Insulin-like growth factor (IGF-I) has been used as an indicator of growth hormone levels and hence can also be used as a marker of growth. The main objective of the study was to quantify salivary IGF-I levels and its secretion rate at different quantitative cervical maturation (QCVM) stages and evaluate a possible role for salivary IGF-I in evaluating skeletal growth. Forty-five subjects (24 female, 21 male) between the ages of 7 and 23 years were included in the study. Each subject had personal information, a lateral cephalogram, and a parotid saliva sample collected on the same day. Salivary IGF-I levels and salivary secretion rates were lowest at QCVM skeletal stages previously associated with the acceleration phase of mandibular growth. Highest levels were found at the high velocity stage. After this there was gradual drop in salivary IGF-I levels and secretion rate at deceleration and completing velocity stages. Relatively high levels in the decelerating velocity stage may be an indication of residual skeletal growth. There was a negative correlation between patient age and levels of IGF-I and its secretion rate, once growth velocity decreased. Salivary IGF-I levels or its secretion rate can be used as an indicator of skeletal growth but longitudinal data are necessary to confirm salivary IGF-I as a marker for skeletal growth prediction and residual mandibular growth. © 2014 British Orthodontic Society.

Dominant inheritance of cerebral gigantism.

PubMed

Zonana, J; Sotos, J F; Romshe, C A; Fisher, D A; Elders, M J; Rimoin, D L

1977-08-01

Cerebral gigantism is a syndrome consisting of characteristic dysmorphic features, accelerated growth in early childhood, and variable degrees of mental retardation. Its etiology and pathogenesis have not been defined. Three families are presented with multiple affected members. The vertical transmission of the trait and equal expression in both sexes in these families indicates a genetic etiology with a dominant pattern of inheritance, probably autosomal. As in previously reported cases, extensive endocrine evaluation failed to define the pathogenesis of the accelerated growth present in this disorder.

Decohesion Elements using Two and Three-Parameter Mixed-Mode Criteria

NASA Technical Reports Server (NTRS)