Sample records for interlayer penetration depth

  1. Fusion welding studies using laser on Ti-SS dissimilar combination

    NASA Astrophysics Data System (ADS)

    Shanmugarajan, B.; Padmanabham, G.

    2012-11-01

    Laser welding investigations were carried out on dissimilar Ti-SS combination. The study is aimed to improve the weld strength and ductility by minimizing harmful intermetallics and taking advantage of high cooling rates in laser welding. Results of continuous wave 3.5 kW CO2 laser welding of totally dissimilar combination of Titanium and stainless steel (304) have been discussed. Bead on plate welding experiments were conducted to identify the laser welding parameters using depth of penetration as criteria. The welding of dissimilar combination has been attempted both autogenously and with interlayers such as Vanadium (V) and Tantalum (Ta) in the form of laser cladding as well as strip. Autogenous welds were carried out by varying the laser power, welding speed and position of the laser beam with respect to the joint centre. The resultant welds are characterized by macrostructure analysis, SEM/EDAX and XRD and as welded tensile test in UTM. The autogenous welds have exhibited extensive cracking even when welded at high speeds or by manipulating the beam position with respect to the joint. Similarly Vandaium as interlayer could not achieve crack free joint. A joint with 40 MPa strength could be made with Ta as interlayer. Results and analysis of these variants of laser welded joints are reported and discussed.

  2. Cost-effectiveness and performance of overlay systems in Illinois, volume 1 : effectiveness assessment of HMA overlay interlayer systems used to retard reflective cracking.

    DOT National Transportation Integrated Search

    2009-05-01

    This project evaluated the ability of interlayer systems used in HMA overlays to retard reflective cracking. Field : crack surveys and forensic investigation, including video imaging and ground penetrating radar surveys as well : as laboratory testin...

  3. Lightning Damage of Carbon Fiber/Epoxy Laminates with Interlayers Modified by Nickel-Coated Multi-Walled Carbon Nanotubes

    NASA Astrophysics Data System (ADS)

    Dong, Qi; Wan, Guoshun; Xu, Yongzheng; Guo, Yunli; Du, Tianxiang; Yi, Xiaosu; Jia, Yuxi

    2017-12-01

    The numerical model of carbon fiber reinforced polymer (CFRP) laminates with electrically modified interlayers subjected to lightning strike is constructed through finite element simulation, in which both intra-laminar and inter-laminar lightning damages are considered by means of coupled electrical-thermal-pyrolytic analysis method. Then the lightning damage extents including the damage volume and maximum damage depth are investigated. The results reveal that the simulated lightning damages could be qualitatively compared to the experimental counterparts of CFRP laminates with interlayers modified by nickel-coated multi-walled carbon nanotubes (Ni-MWCNTs). With higher electrical conductivity of modified interlayer and more amount of modified interlayers, both damage volume and maximum damage depth are reduced. This work provides an effective guidance to the anti-lightning optimization of CFRP laminates.

  4. Dimensionless numbers in additive manufacturing

    NASA Astrophysics Data System (ADS)

    Mukherjee, T.; Manvatkar, V.; De, A.; DebRoy, T.

    2017-02-01

    The effects of many process variables and alloy properties on the structure and properties of additively manufactured parts are examined using four dimensionless numbers. The structure and properties of components made from 316 Stainless steel, Ti-6Al-4V, and Inconel 718 powders for various dimensionless heat inputs, Peclet numbers, Marangoni numbers, and Fourier numbers are studied. Temperature fields, cooling rates, solidification parameters, lack of fusion defects, and thermal strains are examined using a well-tested three-dimensional transient heat transfer and fluid flow model. The results show that lack of fusion defects in the fabricated parts can be minimized by strengthening interlayer bonding using high values of dimensionless heat input. The formation of harmful intermetallics such as laves phases in Inconel 718 can be suppressed using low heat input that results in a small molten pool, a steep temperature gradient, and a fast cooling rate. Improved interlayer bonding can be achieved at high Marangoni numbers, which results in vigorous circulation of liquid metal, larger pool dimensions, and greater depth of penetration. A high Fourier number ensures rapid cooling, low thermal distortion, and a high ratio of temperature gradient to the solidification growth rate with a greater tendency of plane front solidification.

  5. Comparative Study of HfTa-based gate-dielectric Ge metal-oxide-semiconductor capacitors with and without AlON interlayer

    NASA Astrophysics Data System (ADS)

    Xu, J. P.; Zhang, X. F.; Li, C. X.; Chan, C. L.; Lai, P. T.

    2010-04-01

    The electrical properties and high-field reliability of HfTa-based gate-dielectric metal-oxide-semiconductor (MOS) devices with and without AlON interlayer on Ge substrate are investigated. Experimental results show that the MOS capacitor with HfTaON/AlON stack gate dielectric exhibits low interface-state/oxide-charge densities, low gate leakage, small capacitance equivalent thickness (˜1.1 nm), and high dielectric constant (˜20). All of these should be attributed to the blocking role of the ultrathin AlON interlayer against interdiffusions of Ge, Hf, and Ta and penetration of O into the Ge substrate, with the latter effectively suppressing the unintentional formation of unstable poor-quality low- k GeO x and giving a superior AlON/Ge interface. Moreover, incorporation of N into both the interlayer and high- k dielectric further improves the device reliability under high-field stress through the formation of strong N-related bonds.

  6. A comparison of observed and analytically derived remote sensing penetration depths for turbid water

    NASA Technical Reports Server (NTRS)

    Morris, W. D.; Usry, J. W.; Witte, W. G.; Whitlock, C. H.; Guraus, E. A.

    1981-01-01

    The depth to which sunlight will penetrate in turbid waters was investigated. The tests were conducted in water with a single scattering albedo range, and over a range of solar elevation angles. Two different techniques were used to determine the depth of light penetration. It showed little change in the depth of sunlight penetration with changing solar elevation angle. A comparison of the penetration depths indicates that the best agreement between the two methods was achieved when the quasisingle scattering relationship was not corrected for solar angle. It is concluded that sunlight penetration is dependent on inherent water properties only.

  7. Spin-triplet electron transport in hybrid superconductor heterostructures with a composite ferromagnetic interlayer

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Sheyerman, A. E., E-mail: karen@hitech.cplire.ru; Constantinian, K. Y.; Ovsyannikov, G. A.

    2015-06-15

    Hybrid YBa{sub 2}Cu{sub 3}O{sub 7−x}/SrRuO{sub 3}/La{sub 0.7}Sr{sub 0.3}MnO{sub 3}/Au-Nb superconductor mesastructures with a composite manganite-ruthenate ferromagnetic interlayer are studied using electrophysical, magnetic, and microwave methods. The supercurrent in the mesastructure is observed when the interlayer thickness is much larger than the coherence length of ferromagnetic materials. The peak on the dependence of the critical current density on the interlayer material thickness corresponds to the coherence length, which is in qualitative agreement with theoretical predictions for a system with spit-triplet superconducting correlations. The magnetic-field dependence of the critical current is determined by penetration of magnetic flux quanta and by the magneticmore » domain structure, as well as by the field dependence of disorientation of the magnetization vectors of the layers in the composite magnetic interlayer. It is found that the supercurrent exists in magnetic fields two orders of magnitude stronger than the field corresponding to entry of a magnetic flux quantum into the mesastructure. The current-phase relation (CPR) of the supercurrent of mesastructures is investigated upon a change in the magnetic field from zero to 30 Oe; the ratio of the second CPR harmonic to the first, determined from the dependence of the Shapiro steps on the microwave radiation amplitude, does not exceed 50%.« less

  8. Prediction of soil frost penetration depth in northwest of Iran using air freezing indices

    NASA Astrophysics Data System (ADS)

    Mohammadi, H.; Moghbel, M.; Ranjbar, F.

    2016-11-01

    Information about soil frost penetration depth can be effective in finding appropriate solutions to reduce the agricultural crop damage, transportations, and building facilities. Amongst proper methods to achieve this information are the statistical and empirical models capable of estimating soil frost penetration depth. Therefore, the main objective of this research is to calculate soil frost penetration depth in northwest of Iran during the year 2007-2008 to validate two different models accuracy. To do so, the relationship between air and soil temperature in different depths (5-10-20-30-50-100 cm) at three times of the day (3, 9, and 15 GMT) for 14 weather stations over 7 provinces was analyzed using linear regression. Then, two different air freezing indices (AFIs) including Norwegian and Finn AFI was implemented. Finally, the frost penetration depth was calculated by McKeown method and the accuracy of models determined by actual soil frost penetration depth. The results demonstrated that there is a significant correlation between air and soil depth temperature in all studied stations up to the 30 cm under the surface. Also, according to the results, Norwegian index can be effectively used for determination of soil frost depth penetration and the correlation coefficient between actual and estimated soil frost penetration depth is r = 0.92 while the Finn index overestimates the frost depth in all stations with correlation coefficient r = 0.70.

  9. Turbid water measurements of remote sensing penetration depth at visible and near-infrared wavelength

    NASA Technical Reports Server (NTRS)

    Morris, W. D.; Witte, W. G.; Whitlock, C. H.

    1980-01-01

    Remote sensing of water quality is dicussed. Remote sensing penetration depth is a function both of water type and wavelength. Results of three tests to help demonstrate the magnitude of this dependence are presented. The water depth to which the remote-sensor data was valid was always less than that of the Secchi disk depth, although not always the same fraction of that depth. The penetration depths were wavelength dependent and showed the greatest variation for the water type with largest Secchi depth. The presence of a reflective plate, simulating a reflective subsurface, increased the apparent depth of light penetration from that calculated for water of infinite depth.

  10. An Experimental Study of Dependence of Optimum TBM Cutter Spacing on Pre-set Penetration Depth in Sandstone Fragmentation

    NASA Astrophysics Data System (ADS)

    Han, D. Y.; Cao, P.; Liu, J.; Zhu, J. B.

    2017-12-01

    Cutter spacing is an essential parameter in the TBM design. However, few efforts have been made to study the optimum cutter spacing incorporating penetration depth. To investigate the influence of pre-set penetration depth and cutter spacing on sandstone breakage and TBM performance, a series of sequential laboratory indentation tests were performed in a biaxial compression state. Effects of parameters including penetration force, penetration depth, chip mass, chip size distribution, groove volume, specific energy and maximum angle of lateral crack were investigated. Results show that the total mass of chips, the groove volume and the observed optimum cutter spacing increase with increasing pre-set penetration depth. It is also found that the total mass of chips could be an alternative means to determine optimum cutter spacing. In addition, analysis of chip size distribution suggests that the mass of large chips is dominated by both cutter spacing and pre-set penetration depth. After fractal dimension analysis, we found that cutter spacing and pre-set penetration depth have negligible influence on the formation of small chips and that small chips are formed due to squeezing of cutters and surface abrasion caused by shear failure. Analysis on specific energy indicates that the observed optimum spacing/penetration ratio is 10 for the sandstone, at which, the specific energy and the maximum angle of lateral cracks are smallest. The findings in this paper contribute to better understanding of the coupled effect of cutter spacing and pre-set penetration depth on TBM performance and rock breakage, and provide some guidelines for cutter arrangement.

  11. Depth of penetration of a 785nm wavelength laser in food powders

    NASA Astrophysics Data System (ADS)

    Chao, Kuanglin; Dhakal, Sagar; Qin, Jianwei; Kim, Moon S.; Peng, Yankun; Schmidt, Walter F.

    2015-05-01

    Raman spectroscopy is a useful, rapid, and non-destructive method for both qualitative and quantitative evaluation of chemical composition. However it is important to measure the depth of penetration of the laser light to ensure that chemical particles at the very bottom of a sample volume is detected by Raman system. The aim of this study was to investigate the penetration depth of a 785nm laser (maximum power output 400mw) into three different food powders, namely dry milk powder, corn starch, and wheat flour. The food powders were layered in 5 depths between 1 and 5 mm overtop a Petri dish packed with melamine. Melamine was used as the subsurface reference material for measurement because melamine exhibits known and identifiable Raman spectral peaks. Analysis of the sample spectra for characteristics of melamine and characteristics of milk, starch and flour allowed determination of the effective penetration depth of the laser light in the samples. Three laser intensities (100, 200 and 300mw) were used to study the effect of laser intensity to depth of penetration. It was observed that 785nm laser source was able to easily penetrate through every point in all three food samples types at 1mm depth. However, the number of points that the laser could penetrate decreased with increasing depth of the food powder. ANOVA test was carried out to study the significant effect of laser intensity to depth of penetration. It was observed that laser intensity significantly influences the depth of penetration. The outcome of this study will be used in our next phase of study to detect different chemical contaminants in food powders and develop quantitative analysis models for detection of chemical contaminants.

  12. Closed loop control of penetration depth during CO₂ laser lap welding processes.

    PubMed

    Sibillano, Teresa; Rizzi, Domenico; Mezzapesa, Francesco P; Lugarà, Pietro Mario; Konuk, Ali Riza; Aarts, Ronald; Veld, Bert Huis In 't; Ancona, Antonio

    2012-01-01

    In this paper we describe a novel spectroscopic closed loop control system capable of stabilizing the penetration depth during laser welding processes by controlling the laser power. Our novel approach is to analyze the optical emission from the laser generated plasma plume above the keyhole, to calculate its electron temperature as a process-monitoring signal. Laser power has been controlled by using a quantitative relationship between the penetration depth and the plasma electron temperature. The sensor is able to correlate in real time the difference between the measured electron temperature and its reference value for the requested penetration depth. Accordingly the closed loop system adjusts the power, thus maintaining the penetration depth.

  13. Penetration depth of MgB2 measured using Josephson junctions and SQUIDs

    NASA Astrophysics Data System (ADS)

    Cunnane, Daniel; Zhuang, Chenggang; Chen, Ke; Xi, X. X.; Yong, Jie; Lemberger, T. R.

    2013-02-01

    The penetration depth of MgB2 was measured using two methods of different mechanisms. The first method used MgB2 Josephson junctions and the magnetic field dependence of the junction critical current. The second method deduced the penetration depth from the inductance of a MgB2 microstrip used to modulate the voltage of a MgB2 DC SQUID. The two methods showed a consistent value of the low-temperature penetration depth for MgB2 to be about 40 nm. Both the small penetration depth value and its temperature dependence are in agreement with a microscopic theory for MgB2 in the clean limit.

  14. Closed Loop Control of Penetration Depth during CO2 Laser Lap Welding Processes

    PubMed Central

    Sibillano, Teresa; Rizzi, Domenico; Mezzapesa, Francesco P.; Lugarà, Pietro Mario; Konuk, Ali Riza; Aarts, Ronald; Veld, Bert Huis in 't; Ancona, Antonio

    2012-01-01

    In this paper we describe a novel spectroscopic closed loop control system capable of stabilizing the penetration depth during laser welding processes by controlling the laser power. Our novel approach is to analyze the optical emission from the laser generated plasma plume above the keyhole, to calculate its electron temperature as a process-monitoring signal. Laser power has been controlled by using a quantitative relationship between the penetration depth and the plasma electron temperature. The sensor is able to correlate in real time the difference between the measured electron temperature and its reference value for the requested penetration depth. Accordingly the closed loop system adjusts the power, thus maintaining the penetration depth. PMID:23112646

  15. Controlling Force and Depth in Friction Stir Welding

    NASA Technical Reports Server (NTRS)

    Adams, Glynn; Loftus, Zachary; McCormac, Nathan; Venable, Richard

    2005-01-01

    Feedback control of the penetration force applied to a pin tool in friction stir welding has been found to be a robust and reliable means for controlling the depth of penetration of the tool. This discovery has made it possible to simplify depth control and to weld with greater repeatability, even on workpieces with long weld joints. Prior to this discovery, depths of penetration in friction stir welding were controlled by hard-tooled roller assemblies or by depth actuators controlled by feedback from such external sensors as linear variable-differential transformers or laser-based devices. These means of control are limited: A hard-tooled roller assembly confines a pin tool to a preset depth that cannot be changed easily during the welding process. A measurement by an external sensor is only an indirect indicative of the depth of penetration, and computations to correlate such a measurement with a depth of penetration are vulnerable to error. The present force-feedback approach exploits the proportionality between the depth and the force of penetration Unlike a depth measurement taken by an external sensor, a force measurement can be direct because it can be taken by a sensor coupled directly to the pin tool. The reading can be processed through a modern electronic servo control system to control an actuator to keep the applied penetration force at the desired level. In comparison with the older depth-control methods described above, this method offers greater sensitivity to plasticizing of the workpiece metal and is less sensitive to process noise, resulting in a more consistent process. In an experiment, a tapered panel was friction stir welded while controlling the force of penetration according to this method. The figure is a plot of measurements taken during the experiment, showing that force was controlled with a variation of 200 lb (890 N), resulting in control of the depth of penetration with a variation of 0.004 in. (0.1 mm).

  16. Calculation of effective penetration depth in X-ray diffraction for pharmaceutical solids.

    PubMed

    Liu, Jodi; Saw, Robert E; Kiang, Y-H

    2010-09-01

    The use of the glancing incidence X-ray diffraction configuration to depth profile surface phase transformations is of interest to pharmaceutical scientists. The Parratt equation has been used to depth profile phase changes in pharmaceutical compacts. However, it was derived to calculate 1/e penetration at glancing incident angles slightly below the critical angle of condensed matter and is, therefore, applicable to surface studies of materials such as single crystalline nanorods and metal thin films. When the depth of interest is 50-200 microm into the surface, which is typical for pharmaceutical solids, the 1/e penetration depth, or skin depth, can be directly calculated from an exponential absorption law without utilizing the Parratt equation. In this work, we developed a more relevant method to define X-ray penetration depth based on the signal detection limits of the X-ray diffractometer. Our definition of effective penetration depth was empirically verified using bilayer compacts of varying known thicknesses of mannitol and lactose.

  17. Surface area of montmorillonite from the dynamic sorption of nitrogen and carbon dioxide

    USGS Publications Warehouse

    Thomas, Josephus; Bohor, Bruce F.

    1968-01-01

    Surface area determinations were made on a montmorillonite with various cations emplaced on the exchangeable sites, utilizing nitrogen and carbon dioxide as adsorbates at 77°K and 195°K, respectively, in a dynamic system. From the fraction of a Mississippi montmorillonite less than about 1 μ in size, samples were prepared by replacing the original exchangeable cations with Li+, Na+, K+, Rb+, Cs+, Mg++, Ca++, Ba++, and NH4+, forming a series of homoionic montmorillonite species.Surface areas from 3-point B.E.T. plots (half-hour adsorption points), with nitrogen as the adsorbate, ranged from 61 m2/g for Li-montmorillonite to 138 m2/g for Cs-montmorillonite, thus reflecting a certain degree of nitrogen penetration between layers. Complete penetration should theoretically result in a surface area of over 300 m2/g for this clay with a nitrogen monolayer between each pair of platelets. The experimental data indicate that the extent of penetration is time-dependent and is also a function of the interlayer forces as governed by the size and charge of the replaceable cation. This finding negates the generally accepted concept that nitrogen at 77°K does not penetrate the layers and provides a measure only of the external surface of expandable clay minerals.A further measure of the variation of interlayer forces is provided by the adsorption of carbon dioxide at 195°K. Surface area values ranged from 99 m2/g for Li-montmorillonite to 315 m2/g for Csmontmorillonite. Although the carbon dioxide molecule is larger than the nitrogen molecule, its greater penetration apparently is a result of its being kinetically more energetic (with a larger diffusion coefficient) at its higher adsorption temperature. Similar differences have been found with both adsorbates in the study of microporous substances, such as coal, where activated diffusion is of considerable significance.

  18. Ground-penetrating radar--A tool for mapping reservoirs and lakes

    USGS Publications Warehouse

    Truman, C.C.; Asmussen, L.E.; Allison, H.D.

    1991-01-01

    Ground-penetrating radar was evaluated as a tool for mapping reservoir and lake bottoms and providing stage-storage information. An impulse radar was used on a 1.4-ha (3.5-acre) reservoir with 31 transects located 6.1 m (20 feet) apart. Depth of water and lateral extent of the lake bottom were accurately measured by ground-penetrating radar. A linear (positive) relationship existed between measured water depth and ground-penetrating radar-determined water depth (R2=0.989). Ground-penetrating radar data were used to create a contour map of the lake bottom. Relationships between water (contour) elevation and water surface area and volume were established. Ground-penetrating radar proved to be a useful tool for mapping lakes, detecting lake bottom variations, locating old stream channels, and determining water depths. The technology provides accurate, continuous profile data in a relatively short time compared to traditional surveying and depth-sounding techniques.

  19. Dynamic OCT monitoring and quantification of light penetration enhancement for normal, benign and cancerous human lung tissues at different concentrations of glycerol

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Shu-wen Tan; Ying Jin; Hui Yu

    2013-10-31

    We have evaluated the dynamic effects of the analyte diffusion on the 1/e light penetration depths of normal, benign and cancerous human lung tissue in vitro, as well as have monitored and quantified the dynamic change in the light penetration depths of the mentioned human lung tissue after application of 25 % and 50 % glycerol solution, respectively. The light penetration depths of the analyte diffusion in the lung tissue are measured using the Fourierdomain optical coherence tomography (FD-OCT). Experimental results show that the application of glycerol as a chemical agent can significantly enhance light penetration depths into the humanmore » normal lung (NL), lung benign granulomatosis (LBG) and lung squamous cell carcinoma (LSCC) tissue. In-depth transport of the glycerol molecules in the NL, LBG and LSCC tissue at a lower glycerol concentration (25 %) are faster than those at a higher glycerol concentration (50 %), and the 1/e light penetration depths at a lower glycerol concentration (25 %) are smaller than those at a higher glycerol concentration (50 %), respectively. Their differences in the maximal 1/e light penetration depths of the NL, LBG and LSCC tissue at a higher and a lower glycerol concentrations were only 8.8 %, 6.8 % and 4.7 %, respectively. (biophotonics)« less

  20. Effect of Nd:YAG laser parameters on the penetration depth of a representative Ni-Cr dental casting alloy.

    PubMed

    Al Jabbari, Youssef S; Koutsoukis, Theodoros; Barmpagadaki, Xanthoula; El-Danaf, Ehab A; Fournelle, Raymond A; Zinelis, Spiros

    2015-02-01

    The effects of voltage and laser beam (spot) diameter on the penetration depth during laser beam welding in a representative nickel-chromium (Ni-Cr) dental alloy were the subject of this study. The cast alloy specimens were butted against each other and laser welded at their interface using various voltages (160-390 V) and spot diameters (0.2-1.8 mm) and a constant pulse duration of 10 ms. After welding, the laser beam penetration depths in the alloy were measured. The results were plotted and were statistically analyzed with a two-way ANOVA, employing voltage and spot diameter as the discriminating variables and using Holm-Sidak post hoc method (a = 0.05). The maximum penetration depth was 4.7 mm. The penetration depth increased as the spot diameter decreased at a fixed voltage and increased as the voltage increased at a fixed spot diameter. Varying the parameters of voltage and laser spot diameter significantly affected the depth of penetration of the dental cast Ni-Cr alloy. The penetration depth of laser-welded Ni-Cr dental alloys can be accurately adjusted based on the aforementioned results, leading to successfully joined/repaired dental restorations, saving manufacturing time, reducing final cost, and enhancing the longevity of dental prostheses.

  1. Investigation of molecular penetration depth variation with SMBI fluxes

    NASA Astrophysics Data System (ADS)

    Zhou, Yu-Lin; Wang, Zhan-Hui; Xu, Min; Wang, Qi; Nie, Lin; Feng, Hao; Sun, Wei-Guo

    2016-09-01

    We study the molecular penetration depth variation with the SMBI fluxes. The molecular transport process and the penetration depth during SMBI with various injection velocities and densities are simulated and compared. It is found that the penetration depth of molecules strongly depends on the radial convective transport of SMBI and it increases with the increase of the injection velocity. The penetration depth does not vary much once the SMBI injection density is larger than a critical value due to the dramatic increase of the dissociation rate on the fueling path. An effective way to improve the SMBI penetration depth has been predicted, which is SMBI with a large radial injection velocity and a lower molecule injection density than the critical density. Project supported by the National Natural Science Foundation of China (Grant Nos. 11375053, 11575055, 11405022, and 11405112), the Chinese National Fusion Project for ITER (Grant Nos. 2013GB107001 and 2013GB112005), the International S&T Cooperation Program of China (Grant No. 2015DFA61760), and the Funds of the Youth Innovation Team of Science and Technology in Sichuan Province of China (Grant No. 2014TD0023).

  2. Is Grey Level a Suitable Alternative to Low-Contrast Penetration as a Serial Measure of Sensitivity in Computerised Ultrasound Quality Assurance?

    PubMed

    Dudley, Nicholas J; Gibson, Nicholas M

    2017-02-01

    The aim of this study was to test the hypothesis that grey levels are a suitable alternative measure of sensitivity in ultrasound imaging quality assurance, as there are several caveats in the use of penetration depth. In a primary cohort of nine probes, where measurements had been made for 6 to 34 mo, both penetration depth and mean grey level fell below tolerance for six probes; both penetration depth and mean grey level remained within tolerance for three probes. In a secondary cohort where a measurement programme had been in place for a shorter period, grey level and/or penetration depth fell below tolerance in 15 of 66 probes; the sensitivity and specificity of at least 10% loss of grey level in predicting >5% loss in penetration depth were 91% and 93%, respectively. A loss of grey level accompanies a loss of penetration and provides a suitable alternative measure of sensitivity. Crown Copyright © 2016. Published by Elsevier Inc. All rights reserved.

  3. Agreement Between Local and Global Measurements of the London Penetration Depth

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Lippman, Thomas M.; Kalisky, Beena; Kim, Hyunsoo

    Recent measurements of the superconducting penetration depth in Ba(Fe{sub 1-x}Co{sub x}){sub 2}As{sub 2} appeared to disagree on the magnitude and curvature of {delta}{lambda}{sub ab}(T), even near optimal doping. These measurements were carried out on different samples grown by different groups. To understand the discrepancy, we use scanning SQUID susceptometry and a tunnel diode resonator to measure the penetration depth in a single sample. The penetration depth observed by the two techniques is identical with no adjustments. We conclude that any discrepancies arise from differences between samples, either in growth or crystal preparation.

  4. Mathematical modeling of intraperitoneal drug delivery: simulation of drug distribution in a single tumor nodule.

    PubMed

    Steuperaert, Margo; Falvo D'Urso Labate, Giuseppe; Debbaut, Charlotte; De Wever, Olivier; Vanhove, Christian; Ceelen, Wim; Segers, Patrick

    2017-11-01

    The intraperitoneal (IP) administration of chemotherapy is an alternative treatment for peritoneal carcinomatosis, allowing for higher intratumor concentrations of the cytotoxic agent compared to intravenous administration. Nevertheless, drug penetration depths are still limited to a few millimeters. It is thus necessary to better understand the limiting factors behind this poor penetration in order to improve IP chemotherapy delivery. By developing a three-dimensional computational fluid dynamics (CFD) model for drug penetration in a tumor nodule, we investigated the impact of a number of key parameters on the drug transport and penetration depth during IP chemotherapy. Overall, smaller tumors showed better penetration than larger ones, which could be attributed to the lower IFP in smaller tumors. Furthermore, the model demonstrated large improvements in penetration depth by subjecting the tumor nodules to vascular normalization therapy, and illustrated the importance of the drug that is used for therapy. Explicitly modeling the necrotic core had a limited effect on the simulated penetration. Similarly, the penetration depth remained virtually constant when the Darcy permeability of the tissue changed. Our findings illustrate that the developed parametrical CFD model is a powerful tool providing more insight in the drug transport and penetration during IP chemotherapy.

  5. NiCrNx interlayer thickness dependence of spectral performance and environmental durability of protected-silver mirrors

    NASA Astrophysics Data System (ADS)

    Xu, Xu; Li, Bincheng; He, Wenyan; Wang, Changjun; Wei, Ming

    2018-04-01

    Gemini-style protected-silver mirror (Sub / NiCrNx / Ag / NiCrNx / SiNx / Air) is a suitable choice for optical instruments requiring both long-term environmental durability and high broadband reflectance. Three Gemini-style protected-silver mirrors with NiCrNx interlayer thicknesses between 0.1 and 0.6 nm were prepared by magnetron sputtering, and the dependences of spectral properties and environmental durability of these protected-silver mirrors on the thickness of NiCrNx interlayer between the silver layer and SiNx layer were investigated in-depth. The reflectance, transmittance and total scattering loss measurements, optical microscope, and scanning electron microscope imaging were employed to characterize the spectral properties and surface morphology, and accelerated environmental tests, including humidity test and salt fog test, were applied to investigate the environmental durability. The experimental results showed that both optical and corrosion-resistant properties of protected-silver mirrors were NiCrNx interlayer thickness dependent, and an optimum NiCrNx interlayer thickness should be ˜0.3 nm for Gemini-style protected-silver mirrors to have reasonably both high reflectance in a broadband spectral range from visible to far infrared and good corrosion resistance for long-lifetime applications in harsh environments.

  6. Effect of integrating straw into agricultural soils on soil infiltration and evaporation.

    PubMed

    Cao, Jiansheng; Liu, Changming; Zhang, Wanjun; Guo, Yunlong

    2012-01-01

    Soil water movement is a critical consideration for crop yield in straw-integrated fields. This study used an indoor soil column experiment to determine soil infiltration and evaporation characteristics in three forms of direct straw-integrated soils (straw mulching, straw mixing and straw inter-layering). Straw mulching is covering the land surface with straw. Straw mixing is mixing straw with the top 10 cm surface soil. Then straw inter-layering is placing straw at the 20 cm soil depth. There are generally good correlations among the mulch integration methods at p < 0.05, and with average errors/biases <10%. Straw mixing exhibited the best effect in terms of soil infiltration, followed by straw mulching. Due to over-burden weight-compaction effect, straw inter-layering somehow retarded soil infiltration. In terms of soil water evaporation, straw mulching exhibited the best effect. This was followed by straw mixing and then straw inter-layering. Straw inter-layering could have a long-lasting positive effect on soil evaporation as it limited the evaporative consumption of deep soil water. The responses of the direct straw integration modes to soil infiltration and evaporation could lay the basis for developing efficient water-conservation strategies. This is especially useful for water-scarce agricultural regions such as the arid/semi-arid regions of China.

  7. Munition Penetration Depth Prediction: SERDP SEED Project MR 2629

    DTIC Science & Technology

    2017-08-01

    ER D C/ CR RE L TR -1 7- 12 Strategic Environmental Research and Development Program (SERDP) Munition Penetration-Depth Prediction...release; distribution is unlimited. The U.S. Army Engineer Research and Development Center (ERDC) solves the nation’s toughest engineering and... Research and Development Program (SERDP) ERDC/CRREL TR-17-12 August 2017 Munition Penetration-Depth Prediction SERDP SEED Project MR-2629 Arnold J

  8. Method for determining transport critical current densities and flux penetration depth in bulk superconductors

    NASA Technical Reports Server (NTRS)

    Israelsson, Ulf E. (Inventor); Strayer, Donald M. (Inventor)

    1992-01-01

    A contact-less method for determining transport critical current density and flux penetration depth in bulk superconductor material. A compressor having a hollow interior and a plunger for selectively reducing the free space area for distribution of the magnetic flux therein are formed of superconductor material. Analytical relationships, based upon the critical state model, Maxwell's equations and geometrical relationships define transport critical current density and flux penetration depth in terms of the initial trapped magnetic flux density and the ratio between initial and final magnetic flux densities whereby data may be reliably determined by means of the simple test apparatus for evaluating the current density and flux penetration depth.

  9. Direct Measurements of the Penetration Depth in a Superconducting Film using Magnetic Force Microscopy

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    E Nazaretski; J Thibodaux; I Vekhter

    2011-12-31

    We report the local measurements of the magnetic penetration depth in a superconducting Nb film using magnetic force microscopy (MFM). We developed a method for quantitative extraction of the penetration depth from single-parameter simultaneous fits to the lateral and height profiles of the MFM signal, and demonstrate that the obtained value is in excellent agreement with that obtained from the bulk magnetization measurements.

  10. Evaluation of penetration depth of 2% chlorhexidine digluconate into root dentinal tubules using confocal laser scanning microscope.

    PubMed

    Vadhana, Sekar; Latha, Jothi; Velmurugan, Natanasabapathy

    2015-05-01

    This study evaluated the penetration depth of 2% chlorhexidine digluconate (CHX) into root dentinal tubules and the influence of passive ultrasonic irrigation (PUI) using a confocal laser scanning microscope (CLSM). Twenty freshly extracted anterior teeth were decoronated and instrumented using Mtwo rotary files up to size 40, 4% taper. The samples were randomly divided into two groups (n = 10), that is, conventional syringe irrigation (CSI) and PUI. CHX was mixed with Rhodamine B dye and was used as the final irrigant. The teeth were sectioned at coronal, middle and apical levels and viewed under CLSM to record the penetration depth of CHX. The data were statistically analyzed using Kruskal-Wallis and Mann-Whitney U tests. The mean penetration depths of 2% CHX in coronal, middle and apical thirds were 138 µm, 80 µm and 44 µm in CSI group, respectively, whereas the mean penetration depths were 209 µm, 138 µm and 72 µm respectively in PUI group. Statistically significant difference was present between CSI group and PUI group at all three levels (p < 0.01 for coronal third and p < 0.001 for middle and apical thirds). On intragroup analysis, both groups showed statistically significant difference among three levels (p < 0.001). Penetration depth of 2% CHX into root dentinal tubules is deeper in coronal third when compared to middle and apical third. PUI aided in deeper penetration of 2% CHX into dentinal tubules when compared to conventional syringe irrigation at all three levels.

  11. Measurement of in-situ strength using projectile penetration: Tests of a new launching system

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Hearst, J.R.; Newmark, R.L.; Charest, J.A.

    1987-10-01

    The Lawrence Livermore National Laboratory has a continuing need to measure rock strength in situ, both for simple prediction of cavity size, and as input to computational models. In a previous report we compared two methods for measuring formation strength in situ: projectile penetration and a cone penetrometer. We determined that the projectile method was more promising for application to our large-diameter (2-4-m) hole environment. A major practical problem has been the development of a launcher and an apparatus for measuring depth of penetration that would be suitable for use in large-diameter holes. We are developing a gas-gun launcher systemmore » that will be capable of measuring both depth of penetration and deceleration of a reusable projectile. The current version of the launcher is trailer-mounted for testing at our Nevada Test Site (NTS) in tunnels and outcrops, but its design is such that it can be readily adapted for emplacement hole use. We test the current launcher on 60-cm cubes of gypsum cement, mixed to provie a range of densities (1.64 to 2.0 g/cc) and strengths (3 to 17 MPa). We compared depth of penetration of a 84-g projectile from a ''Betsy'' seismic gun - traveling on the order of 500 m/s - with the depth of penetration of a 13-kg projectile from the gas gun - traveling on the order of 30 m/s. For projectiles with the same nose size and shape, impacting targets of approximately constant strength, penetration depth was proportional to projectile kinetic energy. The ratio of kinetic energy to penetration depth was approximately proportional to target strength. Tests in tuffs with a wide range of strengths at NTS gave a similar linear relationship between the ratio of kinetic energy to penetration and target strength, and also a linear relationship between deceleration and strength. It appears that penetration can indeed be used as a semiquantitative measure of strength.« less

  12. Penetration tests to study the mechanical tribological properties of chisel type knife

    NASA Astrophysics Data System (ADS)

    Vlăduţoiu, L.; Chişiu, G.; Andrei, T.; Predescu, A.; Muraru, C.; Vlăduţ, V.

    2017-02-01

    The goal of this study was to analyze the behaviour of chisel knife type penetration in a certain type of sand. A series of penetration tests were carried out with chisel knife type, the answer to penetration depending mainly on nature, shape, size of knife and operating parameters such as speed, depth and working conditions. Tests were conducted in work conditions with wet sand and dry sand and determined force of resistance to penetration of the chisel knife type to a certain depth.

  13. Surface area of vermiculite with nitrogen and carbon dioxide as adsorbates

    USGS Publications Warehouse

    Thomas, Josephus; Bohor, Bruce F.

    1969-01-01

    Surface-area studies were made on several homoionic vermiculites with both nitrogen and carbon dioxide as adsorbates. These studies show that only very slight penetration occurs between individual vermiculite platelets. This is in contrast to an earlier investigation of montmorillonite where it was found that the degree of penetration between layers is quite high, particularly for carbon dioxide, and is governed by the size and charge of the interlayer cation. The inability of these adsorbates to penetrate substantially between vermiculite platelets is due primarily to this mineral's high surface-charge density.The extent of penetration of nitrogen and carbon dioxide at the edges of vermiculite platelets, though slight, is influenced by the coordinated water retained within the sample at a given degassing temperature. Forces between layers are weakened with increasing water content, which permits slightly greater penetration by adsorbate gases. Thus, the surface area of vermiculite, as determined by gas adsorption, is larger than the calculated external surface area based upon particle size and shape considerations. In addition, "extra" surface is provided by the lifting and scrolling of terminal platelets. These morphological features are shown in scanning electron micrographs of a naturally occuring vermiculite.

  14. Penetration of silver nanoparticles into porcine skin ex vivo using fluorescence lifetime imaging microscopy, Raman microscopy, and surface-enhanced Raman scattering microscopy.

    PubMed

    Zhu, Yongjian; Choe, Chun-Sik; Ahlberg, Sebastian; Meinke, Martina C; Alexiev, Ulrike; Lademann, Juergen; Darvin, Maxim E

    2015-05-01

    In order to investigate the penetration depth of silver nanoparticles (Ag NPs) inside the skin, porcine ears treated with Ag NPs are measured by two-photon tomography with a fluorescence lifetime imaging microscopy (TPT-FLIM) technique, confocal Raman microscopy (CRM), and surface-enhanced Raman scattering (SERS) microscopy. Ag NPs are coated with poly-N-vinylpyrrolidone and dispersed in pure water solutions. After the application of Ag NPs, porcine ears are stored in the incubator for 24 h at a temperature of 37°C. The TPT-FLIM measurement results show a dramatic decrease of the Ag NPs' signal intensity from the skin surface to a depth of 4 μm. Below 4 μm, the Ag NPs' signal continues to decline, having completely disappeared at 12 to 14 μm depth. CRM shows that the penetration depth of Ag NPs is 11.1 ± 2.1 μm. The penetration depth measured with a highly sensitive SERS microscopy reaches 15.6 ± 8.3 μm. Several results obtained with SERS show that the penetration depth of Ag NPs can exceed the stratum corneum (SC) thickness, which can be explained by both penetration of trace amounts of Ag NPs through the SC barrier and by the measurements inside the hair follicle, which cannot be excluded in the experiment.

  15. Intrinsic pinning and the critical current scaling of clean epitaxial Fe(Se,Te) thin films

    NASA Astrophysics Data System (ADS)

    Iida, Kazumasa; Hänisch, Jens; Reich, Elke; Kurth, Fritz; Hühne, Ruben; Schultz, Ludwig; Holzapfel, Bernhard; Ichinose, Ataru; Hanawa, Masafumi; Tsukada, Ichiro; Schulze, Michael; Aswartham, Saicharan; Wurmehl, Sabine; Büchner, Bernd

    2013-03-01

    We report on the transport properties of clean, epitaxial Fe(Se,Te) thin films prepared on Fe-buffered MgO (001) single crystalline substrates by pulsed laser deposition. Near Tc a steep slope of the upper critical field for H||ab was observed (74.1 T/K), leading to a very short out-of-plane coherence length, ξc(0), of 0.2 nm, yielding 2ξc(0)≈0.4nm. This value is shorter than the interlayer distance (0.605 nm) between the Fe-Se(Te) planes, indicative of modulation of the superconducting order parameter along the c axis. An inverse correlation between the power law exponent N of the electric field-current density(E-J) curve and the critical current density Jc has been observed at 4 K, when the orientation of H was close to the ab plane. These results prove the presence of intrinsic pinning in Fe(Se,Te). A successful scaling of the angular dependent Jc and the corresponding exponent N can be realized by the anisotropic Ginzburg Landau approach with appropriate Γ values 2˜3.5. The temperature dependence of Γ behaves almost identically to that of the penetration depth anisotropy.

  16. Magnetic proximity effect at the interface between a cuprate superconductor and an oxide spin valve

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Ovsyannikov, G. A., E-mail: gena@hitech.cplire.ru; Demidov, V. V.; Khaydukov, Yu. N.

    2016-04-15

    A heterostructure that consists of the YBa{sub 2}Cu{sub 3}O{sub 7–δ} cuprate superconductor and the SrRuO{sub 3}/La{sub 0.7}Sr{sub 0.3}MnO{sub 3} ruthenate/manganite spin valve is investigated using SQUID magnetometry, ferromagnetic resonance, and neutron reflectometry. It is shown that a magnetic moment is induced due to the magnetic proximity effect in the superconducting part of the heterostructure, while the magnetic moment in the composite ferromagnetic interlayer is suppressed. The magnetization emerging in the superconductor coincides in order of magnitude with the results of calculations taking into account the induced magnetic moment of Cu atoms because of orbital reconstruction at the interface between themore » superconductor and the ferromagnet, as well as with the results of the model taking into account the variations in the density of states at a distance on the order of the coherence length in the superconductor. The experimentally obtained characteristic penetration depth of the magnetic moment in the superconductor considerably exceeds the coherence length of the cuprate superconductor, which indicates the predominance of the mechanism of induced magnetic moment of Cu atoms.« less

  17. Comparison of wavelength-dependent penetration depths of lasers in different types of skin in photodynamic therapy

    NASA Astrophysics Data System (ADS)

    Mustafa, F. H.; Jaafar, M. S.

    2013-03-01

    The determination of the penetration depth of laser light with different sources wavelengths into human skin is one of the preconditions of improving the photodynamic therapy (PDT) procedure for skin diseases. This research is planned to explore which wavelengths would be the most advantageous for use in PDT for superficial skin diseases, and to demonstrate that the red laser exposure of 635 nm wavelength is a suitable choice for all skin types in PDT. A realistic skin model (RSM) in the Advanced Systems Analysis Program (ASAP) software has been used to create different types of skin and to simulate laser sources with wavelengths of 635, 532, 405, 365, 308 and 295 nm. The penetration depths of different kinds of laser into the skin as well as their transmission have been calculated. Comparison of the depth of penetration of different wavelengths for all types of skin has been made. A large variation is found in the penetration depth of laser lights in all skin types. The transmission of lasers on the epidermis and dermis in different skin types occur, and the transmission dose changes significantly with the skin depths. The results of the present study provide a basis for understanding the penetration depth of laser in various skin colors and the responses of the skin to laser to improve dose-drug activation in PDT. The differences in spectral transmission between the red laser and the other lasers suggest that the red laser could be a suitable laser for all skin types.

  18. Infiltration and Selective Interactions at the Interface in Polymer-Oxide Hybrid Solar Cells

    NASA Astrophysics Data System (ADS)

    Ferragut, R.; Aghion, S.; Moia, F.; Binda, M.; Canesi, E. V.; Lanzani, G.; Petrozza, A.

    2013-06-01

    Positron annihilation spectroscopy was used to characterize polymer-based hybrid solar cells formed by poly(3-hexylthiophene) (P3HT) finely infiltrated in a porous TiO2 skeleton. A step-change improvement in the device performance is enabled by engineering the hybrid interface by the insertion of a proper molecular interlayer namely 4-mercaptopyridine (4-MP). In order to obtain depth-resolved data, positrons were implanted in the sample using a variable-energy positron beam. The characteristics of the partially filled nanoporous structures were evaluated in terms of the depth profile of the positronium yield and the S-parameter. A quantitative evaluation of the pore filling in the deep region is given from the analysis of Coincidence Doppler Broadening taken at fixed implantation energy. We note a remarkable difference in terms of the positronium yield when the 4-MP interlayer is introduced, which means a better covering of P3HT on the porous surface.

  19. Magnetic field penetration in niobium- and vanadium-based Josephson junctions

    NASA Astrophysics Data System (ADS)

    Cucolo, A. M.; Pace, S.; Vaglio, R.; di Chiara, A.; Peluso, G.; Russo, M.

    1983-02-01

    Measurements on the temperature dependence of the magnetic field penetration in Nb-NbxOy-Pb and V-VxOy-Pb Josephson junctions have been performed. Results on the zero-temperature penetration depth in niobium films are far above the bulk values although consistent with other measurements on junctions reported in the literature. For vanadium junctions anomalously large penetration depth values are obtained at low temperatures. Nevertheless, the temperature dependence is in reasonable agreement with the local dirty limit model.

  20. Preservation and storage of prepared ballistic gelatine.

    PubMed

    Mattijssen, E J A T; Alberink, I; Jacobs, B; van den Boogaard, Y

    2016-02-01

    The use of ballistic gelatine, generally accepted as a human muscle tissue simulant in wound ballistic studies, might be improved by adding a preservative (Methyl 4-hydroxybenzoate) which inhibits microbial growth. This study shows that replacing a part of the gelatine powder by the preservative does not significantly alter the penetration depth of projectiles. Storing prepared blocks of ballistic gelatine over time decreased the penetration depth of projectiles. Storage of prepared gelatine for 4 week already showed a significant effect on the penetration depth of projectiles. Copyright © 2016 Elsevier Ireland Ltd. All rights reserved.

  1. Monte Carlo analysis on probe performance for endoscopic diffuse optical spectroscopy of tubular organ

    NASA Astrophysics Data System (ADS)

    Zhang, Yunyao; Zhu, Jingping; Cui, Weiwen; Nie, Wei; Li, Jie; Xu, Zhenghong

    2015-03-01

    We investigated the performance of endoscopic diffuse optical spectroscopy probes with circular or linear fiber arrangements for tubular organ cancer detection. Probe performance was measured by penetration depth. A Monte Carlo model was employed to simulate light transport in the hollow cylinder that both emits and receives light from the inner boundary of the sample. The influence of fiber configurations and tissue optical properties on penetration depth was simulated. The results show that under the same condition, probes with circular fiber arrangement penetrate deeper than probes with linear fiber arrangement, and the difference between the two probes' penetration depth decreases with an increase in the 'distance between source and detector (SD)' and the radius of the probe. Other results show that the penetration depths and their differences both decrease with an increase in the absorption coefficient and the reduced scattering coefficient but remain constant with changes in the anisotropy factor. Moreover, the penetration depth was more affected by the absorption coefficient than the reduced scattering coefficient. It turns out that in NIR band, probes with linear fiber arrangements are more appropriate for diagnosing superficial cancers, whereas probes with circular fiber arrangements should be chosen for diagnosing adenocarcinoma. But in UV-VIS band, the two probe configurations exhibit nearly the same. These results are useful in guiding endoscopic diffuse optical spectroscopy-based diagnosis for esophageal, cervical, colorectal and other cancers.

  2. Effect of chitosan nanoparticle, QMix, and EDTA on TotalFill BC sealers' dentinal tubule penetration: a confocal laser scanning microscopy study.

    PubMed

    Aydın, Zeliha Uğur; Özyürek, Taha; Keskin, Büşra; Baran, Talat

    2018-04-12

    The aim of the present study was to compare the effect of chitosan nanoparticle, QMix, and 17% EDTA on the penetrability of a calcium silicate-based sealer into dentinal tubules using a confocal laser scanning microscope (CLSM). Sixty mandibular premolar teeth were selected and randomly divided into three groups (n = 20) before root canal preparation according to the solution used in the final rinse protocol: chitosan, QMix, and EDTA groups. Twenty teeth of each group were filled with a TotalFill BC sealers' single gutta-percha cone and with 0.1% rhodamine B. The specimens were horizontally sectioned at 3 and 5 mm from the apex, and the slices were analyzed in CLSM (4×). Total percentage and maximum depth of sealer penetration were measured using confocal laser scanning microscopy with using Image J analysis software. Dentinal tubule's penetration depth, percentage, and area were measured using imaging software. Kruskal-Wallis test was used for statistical analysis. The level of significance was set at 5%. Results of Kruskal-Wallis analysis showed that there was a significant difference in the percentage and depth of sealer penetration among all groups at 3 and 5 mm level sections (P < 0.05). Within the groups, the minimum sealer penetration depth was recorded for chitosan nanoparticle group. Greater depth of sealer penetration was recorded at 5 mm as compared to 3 mm in all the groups. Within the limitation of the present study, it can be concluded that QMix and EDTA promoted sealer penetration superior to that achieved by chitosan nanoparticle.

  3. Adaptive Neuro-Fuzzy Inference System (ANFIS)-Based Models for Predicting the Weld Bead Width and Depth of Penetration from the Infrared Thermal Image of the Weld Pool

    NASA Astrophysics Data System (ADS)

    Subashini, L.; Vasudevan, M.

    2012-02-01

    Type 316 LN stainless steel is the major structural material used in the construction of nuclear reactors. Activated flux tungsten inert gas (A-TIG) welding has been developed to increase the depth of penetration because the depth of penetration achievable in single-pass TIG welding is limited. Real-time monitoring and control of weld processes is gaining importance because of the requirement of remoter welding process technologies. Hence, it is essential to develop computational methodologies based on an adaptive neuro fuzzy inference system (ANFIS) or artificial neural network (ANN) for predicting and controlling the depth of penetration and weld bead width during A-TIG welding of type 316 LN stainless steel. In the current work, A-TIG welding experiments have been carried out on 6-mm-thick plates of 316 LN stainless steel by varying the welding current. During welding, infrared (IR) thermal images of the weld pool have been acquired in real time, and the features have been extracted from the IR thermal images of the weld pool. The welding current values, along with the extracted features such as length, width of the hot spot, thermal area determined from the Gaussian fit, and thermal bead width computed from the first derivative curve were used as inputs, whereas the measured depth of penetration and weld bead width were used as output of the respective models. Accurate ANFIS models have been developed for predicting the depth of penetration and the weld bead width during TIG welding of 6-mm-thick 316 LN stainless steel plates. A good correlation between the measured and predicted values of weld bead width and depth of penetration were observed in the developed models. The performance of the ANFIS models are compared with that of the ANN models.

  4. Microleakage and penetration depth of different fissure sealant materials after cyclic thermo-mechanic and brushing simulation.

    PubMed

    Hatirli, Hüseyin; Yasa, Bilal; Yasa, Elif

    2018-01-30

    The aim of the study was to evaluate microleakage and the penetration-depths of different fissure-sealant materials applied with/without enameloplasty after cyclic aging. One-hundred-sixty mandibular molars were divided into non-invasive and enameloplasty preparation groups and eight material subgroups, including: flowable composites (microhyrid, nanohybrid, and nanofilled), three resin-based (unfilled, filled, and highly-filled), a giomer-based, and a glass-ionomer-based fissure sealant. Specimens were subjected to two-year cyclic chewing and brushing simulation. After 5% basic-fuchsin dye penetration, specimens were sectioned and scored under stereomicroscope. Kruskal-Wallis statistical data showed that preparation type significantly affected the penetration of all tested materials (p<0.05), but not significantly affected microleakage (p>0.05). Flowable composites showed the best and the glass-ionomer-based sealant showed the worst penetration and microleakage. Slight preparation of fissures is not important in microleakage. However, enameloplasty significantly enhanced the depth of penetration of the sealants. Flowable composites offer promising results at the fissure sealing.

  5. The synthesis and characterization of xerogel silica films for interlayer dielectric applications

    NASA Astrophysics Data System (ADS)

    Chow, Loren Anton

    1999-11-01

    Lowering the dielectric constant, k, of the interlayer dielectric in microprocessors leads to a decrease in power consumption, crosstalk between interconnects and RC time delay. Because of its low density, porous silica, as derived from the sol-gel process, has been widely praised as having the lowest dielectric constant of all viable "low-k" materials. Presented in this work are the results of an investigation featuring the synthesis and characterization of xerogel silica films. Synthesized were xerogel films derived from a tetrafanctional precursor. Such a material was found to be brittle and given to cracking and delamination during curing. it was found, however, that organic modification of the xerogel film led to a compliant material that remained crack-free throughout the curing process. This "hybrid" material filled 0.35 mum trenches without voids, cracks or delamination. The dielectric constant was found to be extremely sensitive to moisture. Although the moisture content was lower than that detectable by Fourier-transform infrared spectroscopy, the dielectric constant in ambient conditions was 80% higher than a dry film. The voltage breakdown was 3.4 MV/cm and the leakage current during bias temperature stressing (at 200 V and 200°C) was negligibly low. There was a critical film thickness at which the film cracked. This critical film thickness was dependent on the elastic constants of the substrate and the film. Because the strain energy released by the cracking film is commensurate with the compliance of the substrate, cracks formed preferentially in the <100> directions; that is, the directions of lowest substrate modulus. The critical thickness for the <100> direction for the hybrid film cured at 500°C was found to be 1.10 mum. Furthermore, it was found that cracks from the xerogel penetrated into the Si substrate to a depth of 0.8 mum. Using substrates of different elastic constants, the biaxial modulus and the coefficient of thermal expansion were found to be respectively 56 GPa and 2.11 x 10-6/°C. With knowledge of the biaxial modulus, the depth of cracking into the Si substrate and an assumption on Poisson's ratio, the critical crack energy release rate of the film was found to be 1.8 J/m2.

  6. Application of welding science to welding engineering: A lumped parameter gas metal arc welding dynamic process model

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Murray, P.E.; Smartt, H.B.; Johnson, J.A.

    1997-12-31

    We develop a model of the depth of penetration of the weld pool in gas metal arc welding (GMAW) which demonstrates interaction between the arc, filler wire and weld pool. This model is motivated by the observations of Essers and Walter which suggest a relationship between droplet momentum and penetration depth. A model of gas metal arc welding was augmented to include an improved model of mass transfer and a simple model of accelerating droplets in a plasma jet to obtain the mass and momentum of impinging droplets. The force of the droplets and depth of penetration is correlated bymore » a dimensionless linear relation used to predict weld pool depth for a range of values of arc power and contact tip to workpiece distance. Model accuracy is examined by comparing theoretical predictions and experimental measurements of the pool depth obtained from bead on plate welds of carbon steel in an argon rich shielding gas. Moreover, theoretical predictions of pool depth are compared to the results obtained from the heat conduction model due to Christensen et al. which suggest that in some cases the momentum of impinging droplets is a better indicator of the depth of the weld pool and the presence of a deep, narrow penetration.« less

  7. Intercalation of p-methycinnamic acid anion into Zn-Al layered double hydroxide to improve UV aging resistance of asphalt

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Peng, Chao; State Key Laboratory of Silicate Materials for Architectures, Wuhan University of Technology, Wuhan 430070; Dai, Jing

    2015-02-15

    A UV absorber, p-methycinnamic acid (PMCA), was intercalated into Zn-Al layered double hydroxide (LDH) by calcination recovery. Fourier transform infrared spectroscopy showed that the PMCA anions completely replaced the CO{sub 3}{sup 2−} anions in the interlayer galleries of Zn-Al-LDH containing PMCA anions (Zn-Al-PMCA-LDH). X-ray diffraction and transmission electron microscopy showed that the interlayer distance increased from 0.78 nm to 1.82 nm after the substitution of PMCA anions for CO{sub 3}{sup 2−} anions. The similar diffraction angles of the CO{sub 3}{sup 2−} anion-containing Zn-Al-LDH (Zn-Al-CO{sub 3}{sup 2−}-LDH) and the Zn-Al-CO{sub 3}{sup 2−}-LDH/styrene–butadiene–styrene (SBS) modified asphalt implied that the asphalt molecules domore » not enter into the LDH interlayer galleries to form separated-phase structures. The different diffraction angles of Zn-Al-PMCA-LDH and Zn-Al-PMCA-LDH/SBS modified asphalt indicated that the asphalt molecules penetrated into the LDH interlayer galleries to form an expanded-phase structure. UV-Vis absorbance analyses showed that Zn-Al-PMCA-LDH was better able to block UV light due to the synergistic effects of PMCA and Zn-Al-LDH. Conventional physical tests and atomic force microscopy images of the SBS modified asphalt, Zn-Al-CO{sub 3}{sup 2−}-LDH/SBS modified asphalt and Zn-Al-PMCA-LDH/SBS modified asphalt before and after UV aging indicated that Zn-Al-PMCA-LDH improved the UV aging resistance of SBS modified asphalts.« less

  8. Effect of Resin Infiltration on Artificial Caries: An in vitro Evaluation of Resin Penetration and Microhardness.

    PubMed

    Prajapati, Deepesh; Nayak, Rashmi; Pai, Deepika; Upadhya, Nagraj; K Bhaskar, Vipin; Kamath, Pujan

    2017-01-01

    To evaluate the effectiveness of resin infiltration on artificial caries lesion by assessing the depth of resin penetration and the change in microhardness of lesion postinfiltration. Totally 45 human extracted premolars were used to create an artificial demineralized lesion in enamel using demineralizing solution. A total of 15 samples (group I) were infiltrated with resin. The depth of resin penetration was studied using scanning electron microscope (SEM). Other half (n = 30) of samples was equally divided into three subgroups and Vickers hardness number (VHN) values were obtained to measure the surface microhardness as group 11 a-before demineralization, 11 b-after demineralization, IIc-postresin infiltration. Mean depth of penetration in group I was 516.8 urn. There was statistically significant increase in VHN values of demineralized lesion postresin infiltration (independent Student's t-test, p < 0.001). Penetration depth of the resin infiltrant was deep enough to render beneficial effects, while significant increase in microhardness was observed postresin infiltration. Infiltrant used can be considered as a valid treatment option for noncavitated lesions. Prajapati D, Nayak R, Pai D, Upadhya N, Bhaskar VK, Kamath P. Effect of Resin Infiltration on Artificial Caries: An in vitro Evaluation of Resin Penetration and Microhardness. Int J Clin Pediatr Dent 2017;10(3):250-256.

  9. Planetary and Primitive Object Strength Measurements and Sampling Apparatus

    NASA Technical Reports Server (NTRS)

    Ahrens, Thomas J.

    1997-01-01

    We present experimental data and a model for the low-velocity (subsonic, 0 - 1000 m/s) penetration of brittle materials by both solid and hollow (i.e., coring) penetrators. The experiments show that penetration is proportional to momentum/frontal area of the penetrator. Because of the buildup of a cap in front of blunt penetrators, the presence or absence of a streamlined or sharp front end usually has a negligible effect for impact into targets with strength. The model accurately predicts the dependence of penetration depth on the various parameters of the target-penetrator system, as well as the qualitative condition of the target material ingested by a corer. In particular, penetration depth is approximately inversely proportional to the static bearing strength of the target. The bulk density of the target material has only a small effect on penetration, whereas friction can be significant, especially at higher impact velocities, for consolidated materials. This trend is reversed for impacts into unconsolidated materials. The present results suggest that the depth of penetration is a good measure of the strength, but not the density, of a consolidated target. Both experiments and model results show that, if passage through the mouth of a coring penetrator requires initially porous target material to be compressed to less than 26% porosity, the sample collected by the corer will be highly fragmented. If the final porosity remains above 26%, then most materials, except cohesionless materials, such as dry sand, will be collected as a compressed slug of material.

  10. Absorption spectra and light penetration depth of normal and pathologically altered human skin

    NASA Astrophysics Data System (ADS)

    Barun, V. V.; Ivanov, A. P.; Volotovskaya, A. V.; Ulashchik, V. S.

    2007-05-01

    A three-layered skin model (stratum corneum, epidermis, and dermis) and engineering formulas for radiative transfer theory are used to study absorption spectra and light penetration depths of normal and pathologically altered skin. The formulas include small-angle and asymptotic approximations and a layer-addition method. These characteristics are calculated for wavelengths used for low-intensity laser therapy. We examined several pathologies such as vitiligo, edema, erythematosus lupus, and subcutaneous wound, for which the bulk concentrations of melanin and blood vessels or tissue structure (for subcutaneous wound) change compared with normal skin. The penetration depth spectrum is very similar to the inverted blood absorption spectrum. In other words, the depth is minimal at blood absorption maxima. The calculated absorption spectra enable the power and irradiation wavelength providing the required light effect to be selected. Relationships between the penetration depth and the diffuse reflectance coefficient of skin (unambiguously expressed through the absorption coefficient) are analyzed at different wavelengths. This makes it possible to find relationships between the light fields inside and outside the tissue.

  11. Use of a ground-penetrating radar system to detect pre-and post-flood scour at selected bridge sites in New Hampshire, 1996-98

    USGS Publications Warehouse

    Olimpio, Joseph R.

    2000-01-01

    Ground-penetrating radar was used to measure the depth and extent of existing and infilled scour holes and previous scour surfaces at seven bridges in New Hampshire from April 1996 to November 1998. Ground-penetrating-radar survey techniques initially were used by the U.S. Geological Survey to study streambed scour at 30 bridges. Sixteen of the 30 bridges were re-surveyed where floods exceeded a 2-year recurrence interval. A 300-megahertz signal was used in the ground-penetrating radar system that penetrated through depths as great as 20 feet of water and as great as 32 feet of streambed materials. Existing scour-hole dimensions, infilled thickness, previous scour surfaces, and streambed materials were detected using ground-penetrating radar. Depths to riprap materials and pier footings were identified and verified with bridge plans. Post data-collection-processing techniques were applied to assist in the interpretation of the data, and the processed data were displayed and printed as line plots. Processing included distance normalization, migration, and filtering but processing was kept to a minimum and some interference from multiple reflections was left in the record. Of the 16 post-flood bridges, 22 ground-penetrating-radar cross sections at 7 bridges were compared and presented in this report. Existing scour holes were detected during 1996 (pre-flood) data collection in nine cross sections where scour depths ranged from 1 to 3 feet. New scour holes were detected during 1998 (post-flood) data collection in four cross sections where scour depths were as great as 4 feet deep. Infilled scour holes were detected in seven cross sections, where depths of infilling ranged from less than 1 to 4 feet. Depth of infilling by means of steel rod and hammer was difficult to verify in the field because of cobble and boulder streambeds or deep water. Previous scour surfaces in streambed materials were identified in 15 cross sections and the depths to these surfaces ranged from 1 to 10 feet below the streambed. Riprap materials or pier footings were identified in all cross sections. Calculated record depths generally agree with bridge plans. Pier footings were exposed at two bridges and steel pile was exposed at one bridge. Exposures were verified by field observations.

  12. A fully spray-coated fuel cell membrane electrode assembly using Aquivion ionomer with a graphene oxide/cerium oxide interlayer

    NASA Astrophysics Data System (ADS)

    Breitwieser, Matthias; Bayer, Thomas; Büchler, Andreas; Zengerle, Roland; Lyth, Stephen M.; Thiele, Simon

    2017-05-01

    A novel multilayer membrane electrode assembly (MEA) for polymer electrolyte membrane fuel cells (PEMFCs) is fabricated in this work, within a single spray-coating device. For the first time, direct membrane deposition is used to fabricate a PEMFC by spraying the short-side-chain ionomer Aquivion directly onto the gas diffusion electrodes. The fully sprayed MEA, with an Aquivion membrane 10 μm in thickness, achieved a high power density of 1.6 W/cm2 for H2/air operation at 300 kPaabs. This is one of the highest reported values for thin composite membranes operated in H2/air atmosphere. By the means of confocal laser scanning microscopy, individual carbon fibers from the gas diffusion layer are identified to penetrate through the micro porous layer (MPL), likely causing a low electrical cell resistance in the range of 150 Ω cm2 through the thin sprayed membranes. By spraying a 200 nm graphene oxide/cerium oxide (GO/CeO2) interlayer between two layers of Aquivion ionomer, the impact of the electrical short is eliminated and the hydrogen crossover current density is reduced to about 1 mA/cm2. The peak power density of the interlayer-containing MEA drops only by 10% compared to a pure Aquivion membrane of similar thickness.

  13. The Penetration Behavior of an Annular Gas-Solid Jet Impinging on a Liquid Bath: The Effects of the Density and Size of Solid Particles

    NASA Astrophysics Data System (ADS)

    Chang, J. S.; Sohn, H. Y.

    2012-08-01

    Top-blow injection of a gas-solid jet through a circular lance is used in the Mitsubishi Continuous Smelting Process. One problem associated with this injection is the severe erosion of the hearth refractory below the lances. A new configuration of the lance to form an annular gas-solid jet rather than the circular jet was designed in this laboratory. With this new configuration, the solid particles fed through the center tube leave the lance at a much lower velocity than the gas, and the penetration behavior of the jet is significantly different from that with a circular lance where the solid particles leave the lance at the same high velocity as the gas. In previous cold-model investigations in this laboratory, the effects of the gas velocity, particle feed rate, lance height of the annular lance, and the cross-sectional area of the gas jet were studied and compared with the circular lance. This study examined the effect of the density and size of the solid particles on the penetration behavior of the annular gas-solid jet, which yielded some unexpected results. The variation in the penetration depth with the density of the solid particles at the same mass feed rate was opposite for the circular lance and the annular lance. In the case of the circular lance, the penetration depth became shallower as the density of the solid particles increased; on the contrary, for the annular lance, the penetration depth became deeper with the increasing density of particles. However, at the same volumetric feed rate of the particles, the density effect was small for the circular lance, but for the annular lance, the jets with higher density particles penetrated more deeply. The variation in the penetration depth with the particle diameter was also different for the circular and the annular lances. With the circular lance, the penetration depth became deeper as the particle size decreased for all the feed rates, but with the annular lance, the effect of the particle size was small. The overall results including the previous work indicated that the penetration behavior of an annular jet is much less sensitive to the variations in operating variables than that of a circular jet. Correlation equations for the penetration depth that show good agreements with the measured values have been developed.

  14. Long range surface plasmon resonance with ultra-high penetration depth for self-referenced sensing and ultra-low detection limit using diverging beam approach

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Isaacs, Sivan, E-mail: sivan.isaacs@gmail.com; Abdulhalim, Ibrahim; NEW CREATE Programme, School of Materials Science and Engineering, 1 CREATE Way, Research Wing, #02-06/08, Singapore 138602

    2015-05-11

    Using an insulator-metal-insulator structure with dielectric having refractive index (RI) larger than the analyte, long range surface plasmon (SP) resonance exhibiting ultra-high penetration depth is demonstrated for sensing applications of large bioentities at wavelengths in the visible range. Based on the diverging beam approach in Kretschmann-Raether configuration, one of the SP resonances is shown to shift in response to changes in the analyte RI while the other is fixed; thus, it can be used as a built in reference. The combination of the high sensitivity, high penetration depth and self-reference using the diverging beam approach in which a dark linemore » is detected of the high sensitivity, high penetration depth, self-reference, and the diverging beam approach in which a dark line is detected using large number of camera pixels with a smart algorithm for sub-pixel resolution, a sensor with ultra-low detection limit is demonstrated suitable for large bioentities.« less

  15. Collaborative effects of wavefront shaping and optical clearing agent in optical coherence tomography

    NASA Astrophysics Data System (ADS)

    Yu, Hyeonseung; Lee, Peter; Jo, YoungJu; Lee, KyeoReh; Tuchin, Valery V.; Jeong, Yong; Park, YongKeun

    2016-12-01

    We demonstrate that simultaneous application of optical clearing agents (OCAs) and complex wavefront shaping in optical coherence tomography (OCT) can provide significant enhancement of penetration depth and imaging quality. OCA reduces optical inhomogeneity of a highly scattering sample, and the wavefront shaping of illumination light controls multiple scattering, resulting in an enhancement of the penetration depth and signal-to-noise ratio. A tissue phantom study shows that concurrent applications of OCA and wavefront shaping successfully operate in OCT imaging. The penetration depth enhancement is further demonstrated for ex vivo mouse ears, revealing hidden structures inaccessible with conventional OCT imaging.

  16. Magnetic field dependence of Sommerfeld coefficient and penetration depth in NdFeAsO1-XFX single crystal

    NASA Astrophysics Data System (ADS)

    Purohit, Geetanjali; Pattanaik, Anup; Nayak, Pratibindhya

    2018-05-01

    Anisotropic properties of Sommerfeld coefficient and penetration depth for single crystal NdFeAsO1-xFx has been studied by using modified phenomenological Ginzburg-Landau (GL) theory. In the above two-band superconducting system, the calculated value of Sommerfeld coefficient shows very close proximity with the experimental result as reported by Welp. Further, anisotropic ratio of penetration depth also calculated and reported for this system. The results of anisotropic properties of the above superconducting system implied that modified GL-theory in the form presented here can be applicable to the above superconducting system.

  17. Monitoring of copper nanoparticle penetration into dentin of human tooth in vitro

    NASA Astrophysics Data System (ADS)

    Selifonov, Alexey A.; Glukhovskoy, Evgeny G.; Skibina, Yulia S.; Zakharevich, Andrey M.; Begletsova, Nadezhda N.; Tuchin, Valery V.

    2018-04-01

    Study of the penetration depth of synthesized copper nanoparticles into cut samples of human dentin was conducted. The scanning electron microscopy was used to determine the elemental composition of fresh transverse cleavage of the dentin cut for determination of the copper nanoparticles penetration with an effective antiseptic effect. The morphology of the cut surface of the dentin of a human tooth was studied and the lower limit of the diffusion boundary was determined. It was found that copper nanoparticles penetrate into the dentin cut to a depth of 1.8 μm with the diffusion coefficient of 1.8×10-11 cm2/s. Despite the rather small size of the synthesized copper nanoparticles (20-80 nm), a rather small penetration depth can be explained by the high aggregation ability of copper nanoparticles, as well as the ability of a micellar solution of sodium dodecyl sulfate, in which nanoparticles were stabilized, to form conglomerates in micelles of much larger sizes.

  18. Wavelength-dependent penetration depth of near infrared radiation into cartilage.

    PubMed

    Padalkar, M V; Pleshko, N

    2015-04-07

    Articular cartilage is a hyaline cartilage that lines the subchondral bone in the diarthrodial joints. Near infrared (NIR) spectroscopy is emerging as a nondestructive modality for the evaluation of cartilage pathology; however, studies regarding the depth of penetration of NIR radiation into cartilage are lacking. The average thickness of human cartilage is about 1-3 mm, and it becomes even thinner as OA progresses. To ensure that spectral data collected is restricted to the tissue of interest, i.e. cartilage in this case, and not from the underlying subchondral bone, it is necessary to determine the depth of penetration of NIR radiation in different wavelength (frequency) regions. In the current study, we establish how the depth of penetration varies throughout the NIR frequency range (4000-10 000 cm(-1)). NIR spectra were collected from cartilage samples of different thicknesses (0.5 mm to 5 mm) with and without polystyrene placed underneath. A separate NIR spectrum of polystyrene was collected as a reference. It was found that the depth of penetration varied from ∼1 mm to 2 mm in the 4000-5100 cm(-1) range, ∼3 mm in the 5100-7000 cm(-1) range, and ∼5 mm in the 7000-9000 cm(-1) frequency range. These findings suggest that the best NIR region to evaluate cartilage with no subchondral bone contribution is in the range of 4000-7000 cm(-1).

  19. Anisotropy of the penetration depth in La2-xSrxCuO4 in underdoped and overdoped regions

    NASA Astrophysics Data System (ADS)

    Zaleski, A. J.; Klamut, J.

    1999-12-01

    We present the results of measurements of the penetration depth anisotropy in pulverized, ceramic La2-xSrxCuO4. The measurements were carried out for x = 0.08, 0.1, 0.125, 0.15 and 0.2. The powdered samples, immersed in wax, were magnetically oriented in a static magnetic field of 10 T. The penetration depth in the a-b plane, icons/Journals/Common/lambda" ALT="lambda" ALIGN="TOP"/>ab, and perpendicular to it, icons/Journals/Common/lambda" ALT="lambda" ALIGN="TOP"/>icons/Journals/Common/perp" ALT="perp" ALIGN="MIDDLE"/>, were derived from alternating-current susceptibility measurements. For underdoped samples they both vary linearly with temperature (for the low-temperature region), while for the samples from the overdoped region the measured points can be fitted by an exponential function. These results support Uemura's picture (Uemura Y J 1997 Physica C 282-287 194) of crossover from Bose-Einstein condensation to a Bardeen-Cooper-Schrieffer mechanism of superconductivity. The penetration depth values extrapolated to T = 0 may be described by a quadratic function of the strontium concentration (for both icons/Journals/Common/lambda" ALT="lambda" ALIGN="TOP"/>ab and icons/Journals/Common/lambda" ALT="lambda" ALIGN="TOP"/>icons/Journals/Common/perp" ALT="perp" ALIGN="MIDDLE"/>). The anisotropy of the penetration depth as a function of the substitution shows a similar dependence to the critical temperature Tc(x).

  20. Demonstration of UXO-PenDepth for the Estimation of Projectile Penetration Depth

    DTIC Science & Technology

    2010-08-01

    Effects (JTCG/ME) in August 2001. The accreditation process included verification and validation (V&V) by a subject matter expert (SME) other than...Within UXO-PenDepth, there are three sets of input parameters that are required: impact conditions (Fig. 1a), penetrator properties , and target... properties . The impact conditions that need to be defined are projectile orientation and impact velocity. The algorithm has been evaluated against

  1. Prediction methods of spudcan penetration for jack-up units

    NASA Astrophysics Data System (ADS)

    Zhang, Ai-xia; Duan, Meng-lan; Li, Hai-ming; Zhao, Jun; Wang, Jian-jun

    2012-12-01

    Jack-up units are extensively playing a successful role in drilling engineering around the world, and their safety and efficiency take more and more attraction in both research and engineering practice. An accurate prediction of the spudcan penetration depth is quite instrumental in deciding on whether a jack-up unit is feasible to operate at the site. The prediction of a too large penetration depth may lead to the hesitation or even rejection of a site due to potential difficulties in the subsequent extraction process; the same is true of a too small depth prediction due to the problem of possible instability during operation. However, a deviation between predictive results and final field data usually exists, especially when a strong-over-soft soil is included in the strata. The ultimate decision sometimes to a great extent depends on the practical experience, not the predictive results given by the guideline. It is somewhat risky, but no choice. Therefore, a feasible predictive method for the spudcan penetration depth, especially in strata with strong-over-soft soil profile, is urgently needed by the jack-up industry. In view of this, a comprehensive investigation on methods of predicting spudcan penetration is executed. For types of different soil profiles, predictive methods for spudcan penetration depth are proposed, and the corresponding experiment is also conducted to validate these methods. In addition, to further verify the feasibility of the proposed methods, a practical engineering case encountered in the South China Sea is also presented, and the corresponding numerical and experimental results are also presented and discussed.

  2. Confocal Raman microscopy and multivariate statistical analysis for determination of different penetration abilities of caffeine and propylene glycol applied simultaneously in a mixture on porcine skin ex vivo.

    PubMed

    Mujica Ascencio, Saul; Choe, ChunSik; Meinke, Martina C; Müller, Rainer H; Maksimov, George V; Wigger-Alberti, Walter; Lademann, Juergen; Darvin, Maxim E

    2016-07-01

    Propylene glycol is one of the known substances added in cosmetic formulations as a penetration enhancer. Recently, nanocrystals have been employed also to increase the skin penetration of active components. Caffeine is a component with many applications and its penetration into the epidermis is controversially discussed in the literature. In the present study, the penetration ability of two components - caffeine nanocrystals and propylene glycol, applied topically on porcine ear skin in the form of a gel, was investigated ex vivo using two confocal Raman microscopes operated at different excitation wavelengths (785nm and 633nm). Several depth profiles were acquired in the fingerprint region and different spectral ranges, i.e., 526-600cm(-1) and 810-880cm(-1) were chosen for independent analysis of caffeine and propylene glycol penetration into the skin, respectively. Multivariate statistical methods such as principal component analysis (PCA) and linear discriminant analysis (LDA) combined with Student's t-test were employed to calculate the maximum penetration depths of each substance (caffeine and propylene glycol). The results show that propylene glycol penetrates significantly deeper than caffeine (20.7-22.0μm versus 12.3-13.0μm) without any penetration enhancement effect on caffeine. The results confirm that different substances, even if applied onto the skin as a mixture, can penetrate differently. The penetration depths of caffeine and propylene glycol obtained using two different confocal Raman microscopes are comparable showing that both types of microscopes are well suited for such investigations and that multivariate statistical PCA-LDA methods combined with Student's t-test are very useful for analyzing the penetration of different substances into the skin. Copyright © 2016 Elsevier B.V. All rights reserved.

  3. Penetration depth measurement of near-infrared hyperspectral imaging light for milk powder

    USDA-ARS?s Scientific Manuscript database

    The increasingly common application of near-infrared (NIR) hyperspectral imaging technique to the analysis of food powders has led to the need for optical characterization of samples. This study was aimed at exploring the feasibility of quantifying penetration depth of NIR hyperspectral imaging ligh...

  4. Projectile penetration into ballistic gelatin.

    PubMed

    Swain, M V; Kieser, D C; Shah, S; Kieser, J A

    2014-01-01

    Ballistic gelatin is frequently used as a model for soft biological tissues that experience projectile impact. In this paper we investigate the response of a number of gelatin materials to the penetration of spherical steel projectiles (7 to 11mm diameter) with a range of lower impacting velocities (<120m/s). The results of sphere penetration depth versus projectile velocity are found to be linear for all systems above a certain threshold velocity required for initiating penetration. The data for a specific material impacted with different diameter spheres were able to be condensed to a single curve when the penetration depth was normalised by the projectile diameter. When the results are compared with a number of predictive relationships available in the literature, it is found that over the range of projectiles and compositions used, the results fit a simple relationship that takes into account the projectile diameter, the threshold velocity for penetration into the gelatin and a value of the shear modulus of the gelatin estimated from the threshold velocity for penetration. The normalised depth is found to fit the elastic Froude number when this is modified to allow for a threshold impact velocity. The normalised penetration data are found to best fit this modified elastic Froude number with a slope of 1/2 instead of 1/3 as suggested by Akers and Belmonte (2006). Possible explanations for this difference are discussed. © 2013 Published by Elsevier Ltd.

  5. Magnetic Penetration Effects in Small Superconducting Devices

    NASA Technical Reports Server (NTRS)

    Stevenson, T. R.; Adams, J. S.; Balvin, M. A.; Bandler, S. R.; Denis, K. L.; Hsieh, W.-T.; Kelly, D. P.; Nagler, P. C.; Porst, J.-P.; Sadleir, J. E.; hide

    2011-01-01

    The temperature dependent behavior of a superconducting body in an applied magnetic field involves flux penetration/expulsion both from screening currents (within a magnetic penetration depth) and variations in the superconducting order parameter (locally to form vortices or a mixed state, or globally in the Meissner effect). The temperature dependence of the magnetic penetration depth, in particular, has been used to make highly sensitive macroscopic thermometers. For the microscopic device volumes required in sensitive low temperature photon detectors, properties of actual thin film materials, non-uniformity of applied magnetic fields, and the influence of measurement circuit dynamics are complicating factors. We discuss the various penetration effects as demonstrated in a particularly promising combination of material and geometry that we have used to make sensitive x-ray microcalorimeters.

  6. Penetration depth, concentration and efficiency of transdermal α-arbutin delivery after ultrasound treatment with albumin-shelled microbubbles in mice.

    PubMed

    Liao, Ai-Ho; Ma, Wan-Chun; Wang, Chih-Hung; Yeh, Ming-Kung

    2016-09-01

    Recently, the feasibility and effects of using microbubbles (MBs) as an ultrasound (US) contrast agent for enhancing the penetration in transdermal delivery in vivo have been demonstrated, but the mechanism and efficiency are unclear. This study demonstrates the penetration depth, concentration and efficiency of transdermal α-arbutin delivery during 4 weeks after US treatment with MBs in mice. Experimental animals were randomly divided into the following four groups (n = 5 animals per group): (1) penetrating α-arbutin alone (C), (2) US combined with penetrating α-arbutin, (3) US combined with MBs and penetrating α-arbutin, and (4) US combined with diluted MBs and penetrating α-arbutin (UBD). The penetration depths in agarose phantoms and pigskin were 47 and 84% greater for group UBD, respectively, than for group C. The in vitro skin penetration by 2% α-arbutin after 3 h was 83% greater in group UBD than in group C. The degree of in vivo skin whitening (quantified as the luminosity index) in group UBD significantly increased by 25% after 1 week, 34% after 2 weeks, and then stabilized after 3 weeks at 37% in C57BL/6J mice over a 4-week experimental period. Our results indicate that combined treatment with optimal US and MBs can increase skin permeability so as to enhance α-arbutin delivery to inhibit melanogenesis without damaging the skin in mice.

  7. Temperature-Enhanced Follicular Penetration of Thermoresponsive Nanogels

    NASA Astrophysics Data System (ADS)

    Jung, Sora; Nagel, Gregor; Giulbudagian, Michael; Calderón, Marcelo; Patzelt, Alexa; Knorr, Fanny; Lademann, Jürgen

    2018-05-01

    Hair follicles can serve as an effective reservoir for dermal drug delivery upon the topical application of particulate substances. Here, the follicular penetration of an indodicarbocyanine-labelled thermoresponsive nanogel (189 nm) having a cloud point temperature of 34°C and linked via an acid-labile linker to the model drug indocarbocyanine was investigated. In total, 227 hair follicles of porcine ear skin were examined after topical application of the thermoresponsive nanogels at room temperature (21°C), physiological skin surface temperature (32°C) and core body temperature (37°C) for the follicular penetration depths of indodicarbocyanine and indocarbocyanine using confocal laser scanning microscopy. The results showed a significantly increased mean follicular penetration of the carrier to a depth of 298.8±85.8 μm after incubation at 37°C compared to samples incubated at 21°C and 32°C with mean follicular penetration depths of 202.7±81.7 μm and 219.4±52.9 μm, respectively (p<0.001). Possibly structural changes in the thermoresponsive nanogel induced by the increased incubation temperature led to an enhancement of follicular penetration. Therefore, thermoresponsive nanogels may be suitable for the temperature-enhanced penetration into the hair follicles under physiological conditions.

  8. Optical penetration sensor for pulsed laser welding

    DOEpatents

    Essien, Marcelino; Keicher, David M.; Schlienger, M. Eric; Jellison, James L.

    2000-01-01

    An apparatus and method for determining the penetration of the weld pool created from pulsed laser welding and more particularly to an apparatus and method of utilizing an optical technique to monitor the weld vaporization plume velocity to determine the depth of penetration. A light source directs a beam through a vaporization plume above a weld pool, wherein the plume changes the intensity of the beam, allowing determination of the velocity of the plume. From the velocity of the plume, the depth of the weld is determined.

  9. Dynamics Modelling of Biolistic Gene Guns

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Zhang, M.; Tao, W.; Pianetta, P.A.

    2009-06-04

    The gene transfer process using biolistic gene guns is a highly dynamic process. To achieve good performance, the process needs to be well understood and controlled. Unfortunately, no dynamic model is available in the open literature for analysing and controlling the process. This paper proposes such a model. Relationships of the penetration depth with the helium pressure, the penetration depth with the acceleration distance, and the penetration depth with the micro-carrier radius are presented. Simulations have also been conducted. The results agree well with experimental results in the open literature. The contribution of this paper includes a dynamic model formore » improving and manipulating performance of the biolistic gene gun.« less

  10. Ion penetration depth in the plant cell wall

    NASA Astrophysics Data System (ADS)

    Yu, L. D.; Vilaithong, T.; Phanchaisri, B.; Apavatjrut, P.; Anuntalabhochai, S.; Evans, P.; Brown, I. G.

    2003-05-01

    This study investigates the depth of ion penetration in plant cell wall material. Based on the biological structure of the plant cell wall, a physical model is proposed which assumes that the wall is composed of randomly orientated layers of cylindrical microfibrils made from cellulose molecules of C 6H 12O 6. With this model, we have determined numerical factors for ion implantation in the plant cell wall to correct values calculated from conventional ion implantation programs. Using these correction factors, it is possible to apply common ion implantation programs to estimate the ion penetration depth in the cell for bioengineering purposes. These estimates are compared with measured data from experiments and good agreement is achieved.

  11. Evidence of unconventional superconductivity in Electron-Doped Cuprates from penetration depth measurements

    NASA Astrophysics Data System (ADS)

    Snezhko, A.; Prozorov, R.; Lawrie, D. D.; Giannetta, R. W.; Gauthier, J.; Renaud, J.; Fournier, P.

    2003-11-01

    The low temperature behavior of magnetic penetration depth provides a powerful tool for probing of order parameter pairing symmetry. In the present work the in-pain London penetration depth, λ(T), measured down to 0.4K is reported for thin films of the Pr_2-xCe_xCuO_4-δ with varying doping levels (x = 0.13, 0.15 and 0.17). Measurements were carried out using a tunnel diode oscillator with excitation fields applied both perpendicular and parallel to the conducting planes. For all systems studied we have found that superfluid density exhibits power law behavior suggestive of a d-wave pairing with impurity scattering.

  12. High-velocity impact loading of thick GFRP blocks

    NASA Astrophysics Data System (ADS)

    Ernst, H.-J.; Merkel, Th.; Wolf, Th.; Hoog, K.

    2003-09-01

    In previous depth of penetration experiments with tungsten long rod projectiles was found that the ballistic resistance of a relatively thick-up to the penetrator length-glass fibre reinforced plastic block grows with increasing penetration depth. This penetration behaviour significantly differs from that of other inert armour materials. Until now, no significant difference between unconfined and totally confined GFRP configurations bas been found. Newest experiments with up to semi-infinite thick GFRP blocks show a change in the penetration process: For thicknesses significantly higher than the penetrator length the protective power may saturate. During the late penetration phase the shortening and deceleration of the projectile induce a change of penetration mechanism from erosion to rigid body penetration. Additionally, the projectile may break into several individually tumbling parts. Reflected tension waves and, probably, pyrolysis effects may cause increasing precursory damage. These effects together are likely to explain the reduction of the ballistic resistance increase during the late penetration phase. Based on these experimental results the published working hypothesis on the governing mechanism of the GFRP penetration behaviour had to be completed. A new approach based on a hyperbolic tangent function seems to satisfactorily describe the observed thickness dependent phenomena.

  13. Multispectral visualization of surgical safety-margins using fluorescent marker seeds

    PubMed Central

    Chin, Patrick TK; Beekman, Chantal AC; Buckle, Tessa; Josephson, Lee; van Leeuwen, Fijs WB

    2012-01-01

    Optical guidance provided by luminescent marker seeds may be suitable for intraoperative determination of appropriate resection margins. In phantom studies we compared the tissue penetration of several organic dyes and inorganic particles (quantum dots; QDs) after incorporation in experimental marker seeds. The tissue penetration of (near infra-) red organic dyes was much better than the penetration of dyes and QDs with an emission in the visible range. By combining 3 dyes in a single marker seed we were able to distinguish four depth ranges. The difference in tissue penetration between the dyes and QDS enabled depth estimation via a ‘traffic light’ approach. PMID:23133810

  14. Depth of penetration of a 785nm laser for Raman spectral measurement in food powders.

    USDA-ARS?s Scientific Manuscript database

    Raman spectroscopy is a useful, rapid, and non-destructive method for both qualitative and quantitative evaluation of chemical composition. However it is important to measure the depth of penetration of the laser light to ensure that chemical particles at the very bottom of a sample volume are detec...

  15. Nonexponential London Penetration Depth of FeAs-Based Superconducting RFeAsO[subscript 0.9]F[subscript 0.1] (R=La, Nd) Single Crystals

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Martin, C.; Tillman, M.E.; Kim, H.

    2009-07-31

    The superconducting penetration depth {lambda}(T) has been measured in RFeAsO{sub 0.9}F{sub 0.1} (R=La, Nd) single crystals (R-1111). In Nd-1111, we find an upturn in {lambda}(T) upon cooling and attribute it to the paramagnetism of the Nd ions, similar to the case of the electron-doped cuprate Nd-Ce-Cu-O. After the correction for paramagnetism, the London penetration depth variation is found to follow a power-law behavior, {Delta}{lambda}L(T) {proportional_to} T{sup 2} at low temperatures. The same T{sup 2} variation of {lambda}(T) was found in nonmagnetic La-1111 crystals. Analysis of the superfluid density and of penetration depth anisotropy over the full temperature range is consistentmore » with two-gap superconductivity. Based on this and on our previous work, we conclude that both the RFeAsO (1111) and BaFe{sub 2}As{sub 2} (122) families of pnictide superconductors exhibit unconventional two-gap superconductivity.« less

  16. Effect of snow cover on soil frost penetration

    NASA Astrophysics Data System (ADS)

    Rožnovský, Jaroslav; Brzezina, Jáchym

    2017-12-01

    Snow cover occurrence affects wintering and lives of organisms because it has a significant effect on soil frost penetration. An analysis of the dependence of soil frost penetration and snow depth between November and March was performed using data from 12 automated climatological stations located in Southern Moravia, with a minimum period of measurement of 5 years since 2001, which belong to the Czech Hydrometeorological institute. The soil temperatures at 5 cm depth fluctuate much less in the presence of snow cover. In contrast, the effect of snow cover on the air temperature at 2 m height is only very small. During clear sky conditions and no snow cover, soil can warm up substantially and the soil temperature range can be even higher than the range of air temperature at 2 m height. The actual height of snow is also important - increased snow depth means lower soil temperature range. However, even just 1 cm snow depth substantially lowers the soil temperature range and it can therefore be clearly seen that snow acts as an insulator and has a major effect on soil frost penetration and soil temperature range.

  17. SHUTTLE IMAGING RADAR: PHYSICAL CONTROLS ON SIGNAL PENETRATION AND SUBSURFACE SCATTERING IN THE EASTERN SAHARA.

    USGS Publications Warehouse

    Schaber, Gerald G.; McCauley, John F.; Breed, Carol S.; Olhoeft, Gary R.

    1986-01-01

    It is found that the Shuttle Imaging Radar A (SIR-A) signal penetration and subsurface backscatter within the upper meter or so of the sediment blanket in the Eastern Sahara of southern Egypt and northern Sudan are enhanced both by radar sensor parameters and by the physical and chemical characteristics of eolian and alluvial materials. The near-surface stratigraphy, the electrical properties of materials, and the types of radar interfaces found to be responsible for different classes of SIR-A tonal response are summarized. The dominant factors related to efficient microwave signal penetration into the sediment blanket include 1) favorable distribution of particle sizes, 2) extremely low moisture content and 3) reduced geometric scattering at the SIR-A frequency (1. 3 GHz). The depth of signal penetration that results in a recorded backscatter, called radar imaging depth, was documented in the field to be a maximum of 1. 5 m, or 0. 25 times the calculated skin depth, for the sediment blanket. The radar imaging depth is estimated to be between 2 and 3 m for active sand dune materials.

  18. Static penetration resistance of soils

    NASA Technical Reports Server (NTRS)

    Durgunoglu, H. T.; Mitchell, J. K.

    1973-01-01

    Model test results were used to define the failure mechanism associated with the static penetration resistance of cohesionless and low-cohesion soils. Knowledge of this mechanism has permitted the development of a new analytical method for calculating the ultimate penetration resistance which explicitly accounts for penetrometer base apex angle and roughness, soil friction angle, and the ratio of penetration depth to base width. Curves relating the bearing capacity factors to the soil friction angle are presented for failure in general shear. Strength parameters and penetrometer interaction properties of a fine sand were determined and used as the basis for prediction of the penetration resistance encountered by wedge, cone, and flat-ended penetrometers of different surface roughness using the proposed analytical method. Because of the close agreement between predicted values and values measured in laboratory tests, it appears possible to deduce in-situ soil strength parameters and their variation with depth from the results of static penetration tests.

  19. Enhanced in vivo visualization of the microcirculation by topical application of fructose solution confirmed with correlation mapping optical coherence tomography

    NASA Astrophysics Data System (ADS)

    Enfield, Joey; McGrath, James; Daly, Susan M.; Leahy, Martin

    2016-08-01

    Changes within the microcirculation can provide an early indication of the onset of a plethora of ailments. Various techniques have thus been developed that enable the study of microcirculatory irregularities. Correlation mapping optical coherence tomography (cmOCT) is a recently proposed technique, which enables mapping of vasculature networks at the capillary level in a noninvasive and noncontact manner. This technique is an extension of conventional optical coherence tomography (OCT) and is therefore likewise limited in the penetration depth of ballistic photons in biological media. Optical clearing has previously been demonstrated to enhance the penetration depth and the imaging capabilities of OCT. In order to enhance the achievable maximum imaging depth, we propose the use of optical clearing in conjunction with the cmOCT technique. We demonstrate in vivo a 13% increase in OCT penetration depth by topical application of a high-concentration fructose solution, thereby enabling the visualization of vessel features at deeper depths within the tissue.

  20. Open-Ended Coaxial Dielectric Probe Effective Penetration Depth Determination.

    PubMed

    Meaney, Paul M; Gregory, Andrew P; Seppälä, Jan; Lahtinen, Tapani

    2016-03-01

    We have performed a series of experiments which demonstrate the effect of open-ended coaxial diameter on the depth of penetration. We used a two layer configuration of a liquid and movable cylindrical piece of either Teflon or acrylic. The technique accurately demonstrates the depth in a sample for which a given probe diameter provides a reasonable measure of the bulk dielectric properties for a heterogeneous volume. In addition we have developed a technique for determining the effective depth for a given probe diameter size. Using a set of simulations mimicking four 50 Ω coaxial cable diameters, we demonstrate that the penetration depth in both water and saline has a clear dependence on probe diameter but is remarkably uniform over frequency and with respect to the intervening liquid permittivity. Two different 50 Ω commercial probes were similarly tested and confirm these observations. This result has significant implications to a range of dielectric measurements, most notably in the area of tissue property studies.

  1. Open-Ended Coaxial Dielectric Probe Effective Penetration Depth Determination

    PubMed Central

    Meaney, Paul M.; Gregory, Andrew P.; Seppälä, Jan; Lahtinen, Tapani

    2016-01-01

    We have performed a series of experiments which demonstrate the effect of open-ended coaxial diameter on the depth of penetration. We used a two layer configuration of a liquid and movable cylindrical piece of either Teflon or acrylic. The technique accurately demonstrates the depth in a sample for which a given probe diameter provides a reasonable measure of the bulk dielectric properties for a heterogeneous volume. In addition we have developed a technique for determining the effective depth for a given probe diameter size. Using a set of simulations mimicking four 50 Ω coaxial cable diameters, we demonstrate that the penetration depth in both water and saline has a clear dependence on probe diameter but is remarkably uniform over frequency and with respect to the intervening liquid permittivity. Two different 50 Ω commercial probes were similarly tested and confirm these observations. This result has significant implications to a range of dielectric measurements, most notably in the area of tissue property studies. PMID:27346890

  2. Tracking ocean heat uptake during the surface warming hiatus

    DOE PAGES

    Liu, Wei; Xie, Shang -Ping; Lu, Jian

    2016-03-30

    Ocean heat uptake is observed to penetrate deep during the recent hiatus1,2,3 of global warming in the Atlantic and Southern Ocean. This has been suggested to indicate that the two regions are the driver of the surface warming hiatus4. We show that the deep heat penetration in the Atlantic and Southern Ocean is not unique to the hiatus but common to the past four decades including the 1970s-90s epoch of accelerated surface warming. Our analyses of a large ensemble simulation5 confirm the deep heat penetration in the Atlantic and Southern Ocean in ensemble members with or without surface warming hiatusmore » in the early 21th century. During the past four decades, the global ocean heat content (OHC) of upper 1500m is dominated by a warming trend, and the depth of anthropogenic heat penetration merely reflects the depth of the mean meridional overturning circulation in the basin. Furthermore, the heat penetration depth is not a valid basis to infer the hiatus mechanism.« less

  3. Tracking ocean heat uptake during the surface warming hiatus

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Liu, Wei; Xie, Shang -Ping; Lu, Jian

    Ocean heat uptake is observed to penetrate deep during the recent hiatus1,2,3 of global warming in the Atlantic and Southern Ocean. This has been suggested to indicate that the two regions are the driver of the surface warming hiatus4. We show that the deep heat penetration in the Atlantic and Southern Ocean is not unique to the hiatus but common to the past four decades including the 1970s-90s epoch of accelerated surface warming. Our analyses of a large ensemble simulation5 confirm the deep heat penetration in the Atlantic and Southern Ocean in ensemble members with or without surface warming hiatusmore » in the early 21th century. During the past four decades, the global ocean heat content (OHC) of upper 1500m is dominated by a warming trend, and the depth of anthropogenic heat penetration merely reflects the depth of the mean meridional overturning circulation in the basin. Furthermore, the heat penetration depth is not a valid basis to infer the hiatus mechanism.« less

  4. Crack propagation and coalescence due to dual non-penetrating surface flaws and their effect on the strength of rock-like material

    NASA Astrophysics Data System (ADS)

    Xu, Jun; Zheng, Zheyuan; Xiao, Xiaochun; Li, Zhaoxia

    2018-06-01

    Non-penetrating surface flaws play a key role in the fracture process of rock-like material, and could cause localized collapse and even failure of the materials. Until now, the mechanism and the effect of surface crack propagation have remained unclear. In this paper, compression tests on gypsum (a soft rock material) are conducted to investigate crack propagation and coalescence due to non-penetrating surface flaws and their effect on the material strength. Specimens are tested under dual pre-existing surface flaws with various combinations of depth and spacing. The results show that when the pre-existing flaws are non-penetrating, the d/t ratio (flaw depth ratio, d is the pre-existing flaw cutting depth and t is the specimen thickness) and the spacing (the distance between the two flaw internal tips) have a strong influence on surface crack patterns and specimen strength. Few cracks emanate from the pre-existing flaws when the flaw depth ratio is equal to 1/3, and more cracks occur with the increase of the flaw depth ratio. When the pre-existing flaw penetrates completely through the specimen, the spacing has a small effect on the specimen strength. A larger flaw depth ratio could advance the occurrence of the peak load (PL) and result in a smaller specimen residual strength. The failure process of the specimen is divided into several stages featured by a stepped decline of the load value after PL, which is closely related to the initiation and propagation of secondary cracks. In addition, the spalling (failure of a portion of the surface caused by coalescence of cracks) can be regarded as indicating the failure of the specimen, and two possible types of spalling formation are briefly discussed.

  5. Magnetic penetration depth in the organic superconductor κ-[BEDT-TTF]2Cu[NCS]2

    NASA Astrophysics Data System (ADS)

    Harshman, D. R.; Kleiman, R. N.; Haddon, R. C.; Chichester-Hicks, S. V.; Kaplan, M. L.; Rupp, L. W., Jr.; Pfiz, T.; Williams, D. Ll.; Mitzi, D. B.

    1990-03-01

    We report the first direct measurement of the effective magnetic penetration depth in oriented single crystals of κ-[BEDT-TTF]2Cu[NCS]2, with Tc(5 G)~=9 K. Results yield an effective in-plane value of λbceff(0)~=9800 Å (for Hext~=3 kG), and a temperature dependence consistent with conventional s-wave pairing. Comparison with the London penetration depth, λL(0) (estimated to be ~=5100 Å), indicates a tendency toward dirty-limit superconductivity, with the ratio of coherence length over mean free path of ξbc0/lbc~=2.7. From our results, it appears unnecessary to invoke any unconventional pairing schemes to explain the superconductivity in this material.

  6. Correction Factor for Determining the London Penetration Depth from Strip Resonators

    NASA Technical Reports Server (NTRS)

    Romanofsky, Robert R.

    1995-01-01

    A significant disagreement is often seen between the theoretical temperature dependent magnetic penetration depth profile and experimentally derived calculations based on stripline type resonators. This short paper shows that the disagreement can be attributed to the susceptance coupled into the resonator from the gap discontinuity as well as the feed line. When the effect is taken into account, the natural resonant frequency of the resonator is increased, and the frequency shift due to kinetic inductance can be calculated much more accurately. While it is necessary to include this effect to determine the penetration depth, it is shown that the impact on unloaded quality factor is generally negligible. The situation when the strip characteristic impedance is not matched to the generator is included.

  7. Improved inter-layer prediction for light field content coding with display scalability

    NASA Astrophysics Data System (ADS)

    Conti, Caroline; Ducla Soares, Luís.; Nunes, Paulo

    2016-09-01

    Light field imaging based on microlens arrays - also known as plenoptic, holoscopic and integral imaging - has recently risen up as feasible and prospective technology due to its ability to support functionalities not straightforwardly available in conventional imaging systems, such as: post-production refocusing and depth of field changing. However, to gradually reach the consumer market and to provide interoperability with current 2D and 3D representations, a display scalable coding solution is essential. In this context, this paper proposes an improved display scalable light field codec comprising a three-layer hierarchical coding architecture (previously proposed by the authors) that provides interoperability with 2D (Base Layer) and 3D stereo and multiview (First Layer) representations, while the Second Layer supports the complete light field content. For further improving the compression performance, novel exemplar-based inter-layer coding tools are proposed here for the Second Layer, namely: (i) an inter-layer reference picture construction relying on an exemplar-based optimization algorithm for texture synthesis, and (ii) a direct prediction mode based on exemplar texture samples from lower layers. Experimental results show that the proposed solution performs better than the tested benchmark solutions, including the authors' previous scalable codec.

  8. Penetration depth of photons in biological tissues from hyperspectral imaging in shortwave infrared in transmission and reflection geometries.

    PubMed

    Zhang, Hairong; Salo, Daniel; Kim, David M; Komarov, Sergey; Tai, Yuan-Chuan; Berezin, Mikhail Y

    2016-12-01

    Measurement of photon penetration in biological tissues is a central theme in optical imaging. A great number of endogenous tissue factors such as absorption, scattering, and anisotropy affect the path of photons in tissue, making it difficult to predict the penetration depth at different wavelengths. Traditional studies evaluating photon penetration at different wavelengths are focused on tissue spectroscopy that does not take into account the heterogeneity within the sample. This is especially critical in shortwave infrared where the individual vibration-based absorption properties of the tissue molecules are affected by nearby tissue components. We have explored the depth penetration in biological tissues from 900 to 1650 nm using Monte–Carlo simulation and a hyperspectral imaging system with Michelson spatial contrast as a metric of light penetration. Chromatic aberration-free hyperspectral images in transmission and reflection geometries were collected with a spectral resolution of 5.27 nm and a total acquisition time of 3 min. Relatively short recording time minimized artifacts from sample drying. Results from both transmission and reflection geometries consistently revealed that the highest spatial contrast in the wavelength range for deep tissue lies within 1300 to 1375 nm; however, in heavily pigmented tissue such as the liver, the range 1550 to 1600 nm is also prominent.

  9. Epiphany sealer penetration into dentinal tubules: Confocal laser scanning microscopic study.

    PubMed

    Ravi, S V; Nageswar, Rao; Swapna, Honwad; Sreekant, Puthalath; Ranjith, Madhavan; Mahidhar, Surabhi

    2014-03-01

    The aim of the following study was to evaluate the percentage and average depth of epiphany sealer penetration into dentinal tubules among the coronal, middle and apical thirds of the root using the confocal laser scanning microscopy (CLSM). A total of 10 maxillary central incisors were prepared and obturated with Resilon-Epiphany system. Sealer was mixed with fluorescent rhodamine B isothiyocyanate dye for visibility under confocal microscope. Teeth were cross-sectioned into coronal, middle and apical sections-2 mm thick. Sections were observed under CLSM. Images were analyzed for percentage and average depth of sealer penetration into dentinal tubules using the lasso tool in Adobe Photoshop CS3 (Adobe systems incorporated, San jose, CA) and laser scanning microscopy (LSM 5) image analyzer. One-way analysis of variance with Student Neuman Keuls post hoc tests, Kruskal-Wallis test and Wilcoxon signed-rank post hoc tests. The results showed that a higher percentage of sealer penetration in coronal section-89.23%, followed by middle section-84.19% and the apical section-64.9%. Average depth of sealer penetration for coronal section was 526.02 μm, middle-385.26 μm and apical-193.49 μm. Study concluded that there was higher epiphany sealer penetration seen in coronal followed by middle and least at apical third of the roots.

  10. Distribution of global fallouts cesium-137 in taiga and tundra catenae at the Ob River basin

    NASA Astrophysics Data System (ADS)

    Semenkov, I. N.; Usacheva, A. A.; Miroshnikov, A. Yu.

    2015-03-01

    The classification of soil catenae at the Ob River basin is developed and applied. This classification reflects the diverse geochemical conditions that led to the formation of certain soil bodies, their combinations and the migration fields of chemical elements. The soil and geochemical diversity of the Ob River basin catenae was analyzed. The vertical and lateral distribution of global fallouts cesium-137 was studied using the example of the four most common catenae types in Western Siberia tundra and taiga. In landscapes of dwarf birches and dark coniferous forests on gleysols, cryosols, podzols, and cryic-stagnosols, the highest 137Cs activity density and specific activity are characteristic of the upper soil layer of over 30% ash, while the moss-grass-shrub cover is characterized by low 137Cs activity density and specific activity. In landscapes of dwarf birches and pine woods on podzols, the maximum specific activity of cesium-137 is typical for moss-grass-shrub cover, while the maximum reserves are concentrated in the upper soil layer of over 30% ash. Bog landscapes and moss-grass-shrub cover are characterized by a minimum activity of 137Cs, and its reserves in soil generally decrease exponentially with depth. The cesium-137 penetration depth increases in oligotrophic histosols from northern to middle taiga landscapes from 10-15 to 40 cm. 137Cs is accumulated in oligotrophic histosols for increases in pH from 3.3 to 4.0 and in concretionary interlayers of pisoplinthic-cryic-histic-stagnosols. Cryogenic movement, on the one hand, leads to burying organic layers enriched in 137Cs and, on the other hand, to deducing specific activity when mixed with low-active material from lower soil layers.

  11. Alaskan frozen soil impact tests of the B83-C/S and Strategic Earth Penetrator

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Dockery, H.A.; Clarke, J.B.; Stull, S.P.

    To assess the penetrability of the B83 strategic bomb and a Strategic Earth Penetrator design into frozen soil and ice, Lawrence Livermore National Laboratory and Sandia National Laboratories, assisted by the US Air Force and US Army, conducted a series of tests in 1987. In April, Strategic Earth Penetrator units were dropped into multi-year sea ice and frozen tundra near Prudhoe Bay, Alaska. Calculated impact velocity ranged from 200 to 308 ft/s into ice and from 200 to 444 ft/s into frozen tundra. Tests in May include drops of a B83 design with specially designed ogive nose shape, a B83more » with a cap over the production ''cookie cutter'' nose, and a Strategic Earth Penetrator. The May tests were conducted near Fairbanks, Alaska, at Eielson Air Force Base and at Donnelly Flats on the Fort Greely Military Reservation. The type of frozen soil encountered at Eielson was very homogeneous in composition; however. Two drops impacted areas with very thin frozen soil layers at depths of about 24 in. below the surface. Velocities of these drops prior to impact ranged from 256 to 308 ft/s, and peak axial deceleration ranged from 160 to 490 g. The units penetrated to depths of 7.5-12 ft. Three other events impacted in a target area where frozen soil averaging 35 in. thick extended essentially to the surface. We calculated velocities prior to impact at 200-256 ft/s; and penetration depths of 3.2-9.6 ft. The geologic material at Donnelly Flats was primarily a very hard, rocky glacial deposit with a variable degree of ice bonding. Here, the test units dropped from 10,000 ft above ground level and achieved an average calculated velocity of 802 ft/s. Depth of penetration ranged from 7.6 to 13.5 ft.« less

  12. Radar attenuation in Europa's ice shell: obstacles and opportunities for constraining shell thickness and thermal structure

    NASA Astrophysics Data System (ADS)

    Kalousova, Klara; Schroeder, Dustin M.; Soderlund, Krista M.; Sotin, Christophe

    2016-10-01

    With its strikingly young surface and possibly recent endogenic activity, Europa is one of the most exciting bodies within our Solar System and a primary target for spacecraft exploration. Future missions to Europa are expected to carry ice penetrating radar instruments which are powerful tools to investigate the subsurface thermophysical structure of its ice shell.Several authors have addressed the 'penetration depth' of radar sounders at icy moons, however, the concept and calculation of a single value penetration depth is a potentially misleading simplification since it ignores the thermal and attenuation structure complexity of a realistic ice shell. Here we move beyond the concept of a single penetration depth by exploring the variation in two-way radar attenuation for a variety of potential thermal structures of Europa's ice shell as well as for a low loss and high loss temperature-dependent attenuation model. The possibility to detect brines is also investigated.Our results indicate that: (i) for all ice shell thicknesses investigated (5-30 km), a nominal satellite-borne radar sounder will penetrate between 15% and 100% of the total thickness, (ii) the maximum penetration depth strongly varies laterally with the deepest penetration possible through the cold downwellings, (iii) the direct detection of the ice/ocean interface might be possible for shells of up to 15 km if the radar signal travels through the cold downwelling, (iv) even if the ice/ocean interface is not detected, the penetration through most of the shell could constrain the deep shell structure through the loss of signal, and (v) for all plausible ice shells the two-way attenuation to the eutectic point is ≤30 dB which shows a robust potential for longitudinal investigation of the ice shell's shallow structure.Part of this work has been performed at the Jet Propulsion Laboratory, California Institute of Technology, under contract to NASA. K.K. acknowledges support by the Grant Agency of the Czech Republic through project 15-14263Y.

  13. Penetration depth of corneal cross-linking with riboflavin and UV-A (CXL) in horses and rabbits.

    PubMed

    Gallhoefer, Nicolin S; Spiess, Bernhard M; Guscetti, Franco; Hilbe, Monika; Hartnack, Sonja; Hafezi, Farhad; Pot, Simon A

    2016-07-01

    CXL penetration depth is an important variable influencing clinical treatment effect and safety. The purposes of this study were to determine the penetration depth of CXL in rabbit and equine corneas in epithelium-on and epithelium-off procedures and to assess an ex vivo fluorescent biomarker staining assay for objective assessment of CXL penetration depth. CXL treatment was performed according to a standardized protocol on 21 and 17 rabbit eyes and on 12 and 10 equine eyes with and without debridement, respectively. Control corneas were treated similarly, but not exposed to CXL. Hemicorneas were stained with either phalloidin and DAPI to visualize intracellular F-actin and nuclei, or with hematoxylin and eosin. Loss of actin staining was measured and compared between groups. Epithelium-off CXL caused a median actin cytoskeleton loss with a demarcation at 274 μm in rabbits and 173 μm in horses. In non-CXL-treated controls, we observed a median actin cytoskeleton loss with a demarcation at 134 μm in rabbits and 149 μm in horses. No effect was detected in the epithelium-on procedure. CXL penetration depth, as determined by a novel ex vivo fluorescent assay, shows clear differences between species. A distinct effect was observed following epithelium-off CXL treatment in the anterior stroma of rabbits, but no different effect was observed in horses in comparison with nontreated controls. Different protocols need to be established to effectively treat equine patients with infectious corneal disease. © 2015 American College of Veterinary Ophthalmologists.

  14. Feasibility of using acoustic method in monitoring the penetration status during the Pulse Mode Laser Welding process

    NASA Astrophysics Data System (ADS)

    Yusof, M. F. M.; Ishak, M.; Ghazali, M. F.

    2017-09-01

    In this paper, the feasibility of using acoustic method to monitor the depth of penetration was investigated by determine the characteristic of the acquired sound throughout the pulse mode laser welding process. To achieve the aim, the sound signal was acquired during the pulsed laser welding process on the 2 mm structural carbon steel plate. During the experiment, the laser peak power and pulse width was set to be varied while welding speed was constantly at 2 mm/s. Result from the experiment revealed that the sound pressure level of the acquired sound was linearly related to the pulse energy as well as the depth of penetration for welding process using 2ms pulse width. However, as the pulse width increase, the sound pressure level show insignificant change with respect to the change in the depth of penetration when the pulse energy reaches certain values. The reported result shows that this was happen due to the occurrence of spatter which suppressed the information associated with the generation of plasma plume as the product of high pulse energy. In this work, it was demonstrated that in some condition, the acoustic method was found to be potentially suitable to be used as a medium to monitor the depth of weld on online basis. To increase the robustness of this method to be used in wider range of parameter, it was believed that some other post processing method is needed in order to extract the specific information associated with the depth of penetration from the acquired sound.

  15. L-band InSAR Penetration Depth Experiment, North Slope Alaska

    NASA Astrophysics Data System (ADS)

    Muskett, Reginald

    2017-04-01

    Since the first spacecraft-based synthetic aperture radar (SAR) mission NASA's SEASAT in 1978 radars have been flown in Low Earth Orbit (LEO) by other national space agencies including the Canadian Space Agency, European Space Agency, India Space Research Organization and the Japanese Aerospace Exploration Agency. Improvements in electronics, miniaturization and production have allowed for the deployment of SAR systems on aircraft for usage in agriculture, hazards assessment, land-use management and planning, meteorology, oceanography and surveillance. LEO SAR systems still provide a range of needful and timely information on large and small-scale weather conditions like those found across the Arctic where ground-base weather radars currently provide limited coverage. For investigators of solid-earth deformation attention must be given to the atmosphere on Interferometric SAR (InSAR) by aircraft and spacecraft multi-pass operations. Because radar has the capability to penetrate earth materials at frequencies from the P- to X-band attention must be given to the frequency dependent penetration depth and volume scattering. This is the focus of our new research project: to test the penetration depth of L-band SAR/InSAR by aircraft and spacecraft systems at a test site in Arctic Alaska using multi-frequency analysis and progressive burial of radar mesh-reflectors at measured depths below tundra while monitoring environmental conditions. Knowledge of the L-band penetration depth on lowland Arctic tundra is necessary to constrain analysis of carbon mass balance and hazardous conditions arising form permafrost degradation and thaw, surface heave and subsidence and thermokarst formation at local and regional scales.

  16. MD and BCA simulations of He and H bombardment of fuzz in bcc elements

    NASA Astrophysics Data System (ADS)

    Klaver, T. P. C.; Zhang, S.; Nordlund, K.

    2017-08-01

    We present results of MD simulations of low energy He ion bombardment of low density fuzz in bcc elements. He ions can penetrate several micrometers into sparse fuzz, which allows for a sufficient He flux through it to grow the fuzz further. He kinetic energy falls off exponentially with penetration depth. A BCA code was used to carry out the same ion bombardment on the same fuzz structures as in MD simulations, but with simpler, 10 million times faster calculations. Despite the poor theoretical basis of the BCA at low ion energies, and the use of somewhat different potentials in MD and BCA calculations, the ion penetration depths predicted by BCA are only ∼12% less than those predicted by MD. The MD-BCA differences are highly systematic and trends in the results of the two methods are very similar. We have carried out more than 200 BCA calculation runs of ion bombardment of fuzz, in which parameters in the ion bombardment process were varied. For most parameters, the results show that the ion bombardment process is quite generic. The ion species (He or H), ion mass, fuzz element (W, Ta, Mo, Fe) and fuzz element lattice parameter turned out to have a modest influence on ion penetration depths at most. An off-normal angle of incidence strongly reduces the ion penetration depth. Increasing the ion energy increases the ion penetration, but the rate by which ion energy drops off at high ion energies follows the same exponential pattern as at lower energies.

  17. Quantification of the vertical translocation rate of soil solid-phase material by the magnetic tracer method

    NASA Astrophysics Data System (ADS)

    Zhidkin, A. P.; Gennadiev, A. N.

    2016-07-01

    Approaches to the quantification of the vertical translocation rate of soil solid-phase material by the magnetic tracer method have been developed; the tracer penetration depth and rate have been determined, as well as the radial distribution of the tracer in chernozems (Chernozems) and dark gray forest soils (Luvisols) of Belgorod oblast under natural steppe and forest vegetation and in arable lands under agricultural use of different durations. It has been found that the penetration depth of spherical magnetic particles (SMPs) during their 150-year-occurrence in soils of a forest plot is 68 cm under forest, 58 cm on a 100-year old plowland, and only 49 cm on a 150-year-old plowland. In the chernozems of the steppe plot, the penetration depth of SMPs exceeds the studied depth of 70 cm both under natural vegetation and on the plowlands. The penetration rates of SMPs deep into the soil vary significantly among the key plots: 0.92-1.32 mm/year on the forest plot and 1.47-1.63 mm/year on the steppe plot, probably because of the more active recent turbation activity of soil animals.

  18. Intelligent Modeling Combining Adaptive Neuro Fuzzy Inference System and Genetic Algorithm for Optimizing Welding Process Parameters

    NASA Astrophysics Data System (ADS)

    Gowtham, K. N.; Vasudevan, M.; Maduraimuthu, V.; Jayakumar, T.

    2011-04-01

    Modified 9Cr-1Mo ferritic steel is used as a structural material for steam generator components of power plants. Generally, tungsten inert gas (TIG) welding is preferred for welding of these steels in which the depth of penetration achievable during autogenous welding is limited. Therefore, activated flux TIG (A-TIG) welding, a novel welding technique, has been developed in-house to increase the depth of penetration. In modified 9Cr-1Mo steel joints produced by the A-TIG welding process, weld bead width, depth of penetration, and heat-affected zone (HAZ) width play an important role in determining the mechanical properties as well as the performance of the weld joints during service. To obtain the desired weld bead geometry and HAZ width, it becomes important to set the welding process parameters. In this work, adaptative neuro fuzzy inference system is used to develop independent models correlating the welding process parameters like current, voltage, and torch speed with weld bead shape parameters like depth of penetration, bead width, and HAZ width. Then a genetic algorithm is employed to determine the optimum A-TIG welding process parameters to obtain the desired weld bead shape parameters and HAZ width.

  19. Quantitative wood–adhesive penetration with X-ray computed tomography

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Paris, Jesse L.; Kamke, Frederick A.

    Micro X-ray computed tomography (XCT) was used to analyze the 3D adhesive penetration behavior of different wood–adhesive bondlines. Three adhesives, a phenol formaldehyde (PF), a polymeric diphenylmethane diisocyanate (pMDI), and a hybrid polyvinyl acetate (PVA), all tagged with iodine for enhanced X-ray attenuation, were used to prepare single-bondline laminates in two softwoods, Douglas-fir and loblolly pine, and one hardwood, a hybrid polar. Adhesive penetration depth was measured with two separate calculations, and results were compared with 2D fluorescent micrographs. A total of 54 XCT scans were collected, representing six replicates of each treatment type; each replicate, however, consisted of approximatelymore » 1500 individual, cross-section slices stacked along the specimen length. As these adhesives were highly modified, the presented results do not indicate typical behavior for their broader adhesive classes. Still, clear penetration differences were observed between each adhesive type, and between wood species bonded with both the PF and pMDI adhesives. Furthermore, penetration results depended on the calculation method used. Two adhesive types with noticeably different resin distributions in the cured bondline, showed relatively similar penetration depths when calculated with a traditional effective penetration equation. However, when the same data was calculated with a weighted penetration calculation, which accounts for both adhesive area and depth, the results appeared to better represent the different distributions depicted in the photomicrographs and tomograms. Additionally, individual replicate comparisons showed variation due to specimen anatomy, not easily observed or interpreted from 2D images. Finally, 3D views of segmented 3D adhesive phases offered unique, in-situ views of the cured adhesive structures. In particular, voids formed by CO 2 bubbles generated during pMDI cure were clearly visible in penetrated columns of the solidified adhesive.« less

  20. Prediction of Weld Penetration in FCAW of HSLA steel using Artificial Neural Networks

    NASA Astrophysics Data System (ADS)

    Asl, Y. Dadgar; Mostafa, N. B.; Panahizadeh R., V.; Seyedkashi, S. M. H.

    2011-01-01

    Flux-cored arc welding (FCAW) is a semiautomatic or automatic arc welding process that requires a continuously-fed consumable tubular electrode containing a flux. The main FCAW process parameters affecting the depth of penetration are welding current, arc voltage, nozzle-to-work distance, torch angle and welding speed. Shallow depth of penetration may contribute to failure of a welded structure since penetration determines the stress-carrying capacity of a welded joint. To avoid such occurrences; the welding process parameters influencing the weld penetration must be properly selected to obtain an acceptable weld penetration and hence a high quality joint. Artificial neural networks (ANN), also called neural networks (NN), are computational models used to express complex non-linear relationships between input and output data. In this paper, artificial neural network (ANN) method is used to predict the effects of welding current, arc voltage, nozzle-to-work distance, torch angle and welding speed on weld penetration depth in gas shielded FCAW of a grade of high strength low alloy steel. 32 experimental runs were carried out using the bead-on-plate welding technique. Weld penetrations were measured and on the basis of these 32 sets of experimental data, a feed-forward back-propagation neural network was created. 28 sets of the experiments were used as the training data and the remaining 4 sets were used for the testing phase of the network. The ANN has one hidden layer with eight neurons and is trained after 840 iterations. The comparison between the experimental results and ANN results showed that the trained network could predict the effects of the FCAW process parameters on weld penetration adequately.

  1. Nonextensive statistics and skin depth of transverse wave in collisional plasma

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Hashemzadeh, M., E-mail: hashemzade@gmail.com

    Skin depth of transverse wave in a collisional plasma is studied taking into account the nonextensive electron distribution function. Considering the kinetic theory for charge particles and using the Bhatnagar-Gross-Krook collision model, a generalized transverse dielectric permittivity is obtained. The transverse dispersion relation in different frequency ranges is investigated. Obtaining the imaginary part of the wave vector from the dispersion relation, the skin depth for these frequency ranges is also achieved. Profiles of the skin depth show that by increasing the q parameter, the penetration depth decreases. In addition, the skin depth increases by increasing the electron temperature. Finally, itmore » is found that in the high frequency range and high electron temperature, the penetration depth decreases by increasing the collision frequency. In contrast, by increasing the collision frequency in a highly collisional frequency range, the skin depth of transverse wave increases.« less

  2. Strategy of topical vaccination with nanoparticles

    NASA Astrophysics Data System (ADS)

    Jung, Sascha; Patzelt, Alexa; Otberg, Nina; Thiede, Gisela; Sterry, Wolfram; Lademann, Juergen

    2009-03-01

    Liposomes in the nanosize range have been recognized as a versatile drug delivery system of both hydrophilic and lipophilic molecules. In order to develop a liposome-based topical vaccination strategy, five different types of liposomes were tested as a putative vaccine delivery system on pig ear skin. The investigated liposomes mainly varied in size, lipid composition, and surface charge. Using hydrophilic and hydrophobic fluorescent dyes as model drugs, penetration behavior was studied by means of confocal laser scanning microscopy of intact skin and histological sections, respectively. Follicular penetration of the liposomes was measured in comparison to a standard, nonliposomal formulation at different time points. Dependent on time but independent of their different characters, the liposomes showed a significantly higher penetration depth into the hair follicles compared to the standard formulation. The standard formulation reached a relative penetration depth of 30% of the full hair follicle length after seven days, whereas amphoteric and cationic liposomes had reached ~70%. Penetration depth of negatively charged liposomes did not exceed 50% of the total follicle length. The fluorescence dyes were mainly detected in the hair follicle; only a small amount of dye was found in the upper parts of the epidermis.

  3. Strategy of topical vaccination with nanoparticles.

    PubMed

    Jung, Sascha; Patzelt, Alexa; Otberg, Nina; Thiede, Gisela; Sterry, Wolfram; Lademann, Juergen

    2009-01-01

    Liposomes in the nanosize range have been recognized as a versatile drug delivery system of both hydrophilic and lipophilic molecules. In order to develop a liposome-based topical vaccination strategy, five different types of liposomes were tested as a putative vaccine delivery system on pig ear skin. The investigated liposomes mainly varied in size, lipid composition, and surface charge. Using hydrophilic and hydrophobic fluorescent dyes as model drugs, penetration behavior was studied by means of confocal laser scanning microscopy of intact skin and histological sections, respectively. Follicular penetration of the liposomes was measured in comparison to a standard, nonliposomal formulation at different time points. Dependent on time but independent of their different characters, the liposomes showed a significantly higher penetration depth into the hair follicles compared to the standard formulation. The standard formulation reached a relative penetration depth of 30% of the full hair follicle length after seven days, whereas amphoteric and cationic liposomes had reached approximately 70%. Penetration depth of negatively charged liposomes did not exceed 50% of the total follicle length. The fluorescence dyes were mainly detected in the hair follicle; only a small amount of dye was found in the upper parts of the epidermis.

  4. Mapping the opacity of paint layers in paintings with coloured grounds using optical coherence tomography

    NASA Astrophysics Data System (ADS)

    Liu, Ping; Hall-Aquitania, Moorea; Hermens, Erma; Groves, Roger M.

    2017-07-01

    Optical diagnostics techniques are becoming important for technical art history (TAH) as well as for heritage conservation. In recent years, optical coherence tomography (OCT) has been increasingly used as a novel technique for the inspection of artwork, revealing the stratigraphy of paintings. It has also shown to be an effective tool for vanish layer inspection. OCT is a contactless and non-destructive technique for microstructural imaging of turbid media, originally developed for medical applications. However current OCT instruments have difficulty in paint layer inspection due to the opacity of most pigments. This paper explores the potential of OCT for the investigation of paintings with coloured grounds. Depth scans were processed to determine the light penetration depth at the optical wavelength based on a 1/e light attenuation calculation. The variation in paint opacity was mapped based on the microstructural images and 3D penetration depth profiles was calculated and related back to the construction of the artwork. By determining the light penetration depth over a range of wavelengths the 3D depth perception of a painting with coloured grounds can be characterized optically.

  5. Explosive shaped charge penetration into tuff rock

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Vigil, M.G.

    1988-10-01

    Analysis and data for the use of Explosive Shaped Charges (ESC) to generate holes in tuff rock formation is presented. The ESCs evaluated include Conical Shaped Charges (CSC) and Explosive Formed Projectiles (EFP). The CSCs vary in size from 0.158 to 9.1 inches inside cone diameter. The EFPs were 5.0 inches in diameter. Data for projectile impact angles of 30 and 90 degrees are presented. Analytically predicted depth of penetration data generally compared favorably with experimental data. Predicted depth of penetration versus ESC standoff data and hole profile dimensions in tuff are also presented. 24 refs., 45 figs., 6 tabs.

  6. Preliminary study of gaseous nitrogen-liquid oxygen mixing and self cleaning

    NASA Technical Reports Server (NTRS)

    Zuckerwar, A. J.

    1985-01-01

    The penetration of gaseous nitrogen into liquid oxygen at a pressure of 150 psi was determined by monitoring the composition of the evaporating liquid in a nitrogen analyzer. For pressurization times of about 1 hr the penetration depth varies between 0.0024 and 0.018 in. at an evaporation rate of about 1 gal/day. These are small compared to the penetration depth of 22.2 in. measured in the 7-inch high temperature tunnel at a pressure of 1500 psi, pressurization time of 5 min, and evaporation rate of 121 gal/day.

  7. Topical dissolved oxygen penetrates skin: model and method.

    PubMed

    Roe, David F; Gibbins, Bruce L; Ladizinsky, Daniel A

    2010-03-01

    It has been commonly perceived that skin receives its oxygen supply from the internal circulation. However, recent investigations have shown that a significant amount of oxygen may enter skin from the external overlying surface. A method has been developed for measuring the transcutaneous penetration of human skin by oxygen as described herein. This method was used to determine both the depth and magnitude of penetration of skin by topically applied oxygen. An apparatus consisting of human skin samples interposed between a topical oxygen source and a fluid filled chamber that registered changes in dissolved oxygen. Viable human skin samples of variable thicknesses with and without epidermis were used to evaluate the depth and magnitude of oxygen penetration from either topical dissolved oxygen (TDO) or topical gaseous oxygen (TGO) devices. This model effectively demonstrates transcutaneous penetration of topically applied oxygen. Topically applied dissolved oxygen penetrates through >700 microm of human skin. Topically applied oxygen penetrates better though dermis than epidermis, and TDO devices deliver oxygen more effectively than TGO devices. Copyright (c) 2010 Elsevier Inc. All rights reserved.

  8. Damage Mechanics Approach to Penetration of Water-filled Surface Crevasses

    NASA Astrophysics Data System (ADS)

    Duddu, R.; Jimenez, S. K.; Bassis, J. N.

    2017-12-01

    Iceberg calving is a natural process that occurs when crevasses penetrate the entire thickness of an ice shelf or a glacier leading to the detachment (birth) of icebergs. Calving from marine-terminating glaciers and floating ice shelves accounts for nearly 50% of the mass lost from both the Greenland and Antarctic ice sheets, which can directly or indirectly contribute to sealevel rise. A widely-accepted hypothesis is that crevasses in ice form due to brittle mode I fracture under the action of tensile stresses. Existing theoretical approaches for modeling crevasse propagation based on the above hypothesis include the Nye zero stress and fracture mechanics approaches. These theoretical approaches assume idealized geometry and boundary conditions, and ignore the effects of viscous creep deformations in ice over longer time scales; however, they still produced interesting results that matched well with sparse field observations available. An alternative is to use the continuum damage mechanics approach for modeling crevasse propagation, which is more easily incorporated into numerical ice sheet models that consider realistic geometries, boundary conditions and viscous creep effects. In this presentation, we describe the damage mechanics approach to penetration of dry and water-filled surface crevasses using the principles of poromechanics and compare our results with those from existing theoretical approaches. We investigate the upper limits on crevasse penetration depth in relation to ice thickness, water depth in the surface crevasse, seawater depth at the ice terminus and ice rheology (i.e., elastic vs. viscous). Our studies on idealized glaciers show that the damage mechanics approach is consistent with the fracture mechanics approach when the seawater depth at the ice terminus is low, but is inconsistent with the theoretical approaches when the seawater depth at the ice terminus is high (i.e., near floatation). Our studies also indicate that the upper limit on surface crevasse penetration depth is minimally sensitive to ice rheology when glacier geometry changes are ignored. However, viscous flow can cause geometry changes and induce stresses (e.g., due to bending) leading to deeper crevasse penetration in numerical ice sheet models.

  9. Erosion of aluminum 6061-T6 under cavitation attack in mineral oil and water

    NASA Technical Reports Server (NTRS)

    Rao, B. C. S.; Buckley, D. H.

    1985-01-01

    Studies of the erosion of aluminum 6061-T6 under cavitation attack in distilled water, ordinary tap water and a viscous mineral oil are presented. The mean depth of penetration for the mineral oil was about 40 percent of that for water at the end of a 40 min test. The mean depth of penetration and its rate did not differ significantly for distilled and tap water. The mean depth of penetration rate for both distilled and tap water increased to a maximum and then decreased with test duration, while that for mineral oil had a maximum during the initial period. The ratio h/2a of the pit depth h to the pit diameter 2a varied from 0.04 to 0.13 in water and from 0.06 to 0.20 in mineral oil. Scanning electron microscopy indicates that the pits are initially formed over the grain boundaries and precipitates while the surface grains are deformed under cavitation attack.

  10. Penetration Depth and Defect Image Contrast Formation in Grazing-Incidence X-ray Topography of 4H-SiC Wafers

    NASA Astrophysics Data System (ADS)

    Yang, Yu; Guo, Jianqiu; Goue, Ouloide Yannick; Kim, Jun Gyu; Raghothamachar, Balaji; Dudley, Michael; Chung, Gill; Sanchez, Edward; Manning, Ian

    2018-02-01

    Synchrotron x-ray topography in grazing-incidence geometry is useful for discerning defects at different depths below the crystal surface, particularly for 4H-SiC epitaxial wafers. However, the penetration depths measured from x-ray topographs are much larger than theoretical values. To interpret this discrepancy, we have simulated the topographic contrast of dislocations based on two of the most basic contrast formation mechanisms, viz. orientation and kinematical contrast. Orientation contrast considers merely displacement fields associated with dislocations, while kinematical contrast considers also diffraction volume, defined as the effective misorientation around dislocations and the rocking curve width for given diffraction vector. Ray-tracing simulation was carried out to visualize dislocation contrast for both models, taking into account photoelectric absorption of the x-ray beam inside the crystal. The results show that orientation contrast plays the key role in determining both the contrast and x-ray penetration depth for different types of dislocation.

  11. Geohydrology of test well USW H-3, Yucca Mountain, Nye County, Nevada

    USGS Publications Warehouse

    Thordarson, William; Rush, F.E.; Waddell, S.J.

    1985-01-01

    Test well USW H-3 is one of several wells drilled in the southwestern part of the Nevada Test Site for hydraulic testing, hydrologic monitoring, and geophysical logging. The work was performed in cooperation with the U.S. Department of Energy. The rocks penetrated by the well to a total depth of 1,219 meters were volcanic tuffs of Tertiary age. The most transmissive zone in this well is in the upper part of the Tram Member of the Crater Flat Tuff that was penetrated at a depth from 809 to 841 meters; transmissivity is about 7 x 10 -1 meter squared per day. The remainder of the rocks penetrated between the depths of 841 to 1,219 meters have a transmissivity of about 4 x 10 -1 meter squared per day and are predominatly in the Tram Member of the Crater Flat Tuff and the Lithic Ridge Tuff in the depths from 841 to 1,219 meters. (USGS)

  12. Penetration depth of photons in biological tissues from hyperspectral imaging in shortwave infrared in transmission and reflection geometries

    PubMed Central

    Zhang, Hairong; Salo, Daniel; Kim, David M.; Komarov, Sergey; Tai, Yuan-Chuan; Berezin, Mikhail Y.

    2016-01-01

    Abstract. Measurement of photon penetration in biological tissues is a central theme in optical imaging. A great number of endogenous tissue factors such as absorption, scattering, and anisotropy affect the path of photons in tissue, making it difficult to predict the penetration depth at different wavelengths. Traditional studies evaluating photon penetration at different wavelengths are focused on tissue spectroscopy that does not take into account the heterogeneity within the sample. This is especially critical in shortwave infrared where the individual vibration-based absorption properties of the tissue molecules are affected by nearby tissue components. We have explored the depth penetration in biological tissues from 900 to 1650 nm using Monte–Carlo simulation and a hyperspectral imaging system with Michelson spatial contrast as a metric of light penetration. Chromatic aberration-free hyperspectral images in transmission and reflection geometries were collected with a spectral resolution of 5.27 nm and a total acquisition time of 3 min. Relatively short recording time minimized artifacts from sample drying. Results from both transmission and reflection geometries consistently revealed that the highest spatial contrast in the wavelength range for deep tissue lies within 1300 to 1375 nm; however, in heavily pigmented tissue such as the liver, the range 1550 to 1600 nm is also prominent. PMID:27930773

  13. L-band InSAR Penetration Depth Experiment, North Slope Alaska

    NASA Astrophysics Data System (ADS)

    Muskett, R. R.

    2017-12-01

    Since the first spacecraft-based synthetic aperture radar (SAR) mission NASA's SEASAT in 1978 radars have been flown in Low Earth Orbit (LEO) by other national space agencies including the Canadian Space Agency, European Space Agency, India Space Research Organization and the Japanese Aerospace Exploration Agency. Improvements in electronics, miniaturization and production have allowed for the deployment of SAR systems on aircraft for usage in agriculture, hazards assessment, land-use management and planning, meteorology, oceanography and surveillance. LEO SAR systems still provide a range of needful and timely information on large and small-scale weather conditions like those found across the Arctic where ground-base weather radars currently provide limited coverage. For investigators of solid-earth deformation attention must be given to the atmosphere on Interferometric SAR (InSAR) by aircraft and spacecraft multi-pass operations. Because radar has the capability to penetrate earth materials at frequencies from the P- to X-band attention must be given to the frequency dependent penetration depth and volume scattering. This is the focus of our new research project: to test the penetration depth of L-band SAR/InSAR by aircraft and spacecraft systems at a test site in Arctic Alaska using multi-frequency analysis and progressive burial of radar mesh-reflectors at measured depths below tundra while monitoring environmental conditions. Knowledge of the L-band penetration depth on lowland Arctic tundra is necessary to constrain analysis of carbon mass balance and hazardous conditions arising form permafrost degradation and thaw, surface heave and subsidence and thermokarst formation at local and regional scales. Ref.: Geoscience and Environment Protection, vol. 5, no. 3, p. 14-30, 2017. DOI: 10.4236/gep.2017.53002.

  14. Split-Ring Resonator Sensor Penetration Depth Assessment Using In Vivo Microwave Reflectivity and Ultrasound Measurements for Lower Extremity Trauma Rehabilitation.

    PubMed

    Shah, Syaiful Redzwan Mohd; Velander, Jacob; Mathur, Parul; Perez, Mauricio D; Asan, Noor Badariah; Kurup, Dhanesh G; Blokhuis, Taco J; Augustine, Robin

    2018-02-21

    In recent research, microwave sensors have been used to follow up the recovery of lower extremity trauma patients. This is done mainly by monitoring the changes of dielectric properties of lower limb tissues such as skin, fat, muscle, and bone. As part of the characterization of the microwave sensor, it is crucial to assess the signal penetration in in vivo tissues. This work presents a new approach for investigating the penetration depth of planar microwave sensors based on the Split-Ring Resonator in the in vivo context of the femoral area. This approach is based on the optimization of a 3D simulation model using the platform of CST Microwave Studio and consisting of a sensor of the considered type and a multilayered material representing the femoral area. The geometry of the layered material is built based on information from ultrasound images and includes mainly the thicknesses of skin, fat, and muscle tissues. The optimization target is the measured S 11 parameters at the sensor connector and the fitting parameters are the permittivity of each layer of the material. Four positions in the femoral area (two at distal and two at thigh) in four volunteers are considered for the in vivo study. The penetration depths are finally calculated with the help of the electric field distribution in simulations of the optimized model for each one of the 16 considered positions. The numerical results show that positions at the thigh contribute the highest penetration values of up to 17.5 mm. This finding has a high significance in planning in vitro penetration depth measurements and other tests that are going to be performed in the future.

  15. Theory for measurements of penetration depth in magnetic superconductors by magnetic force microscopy and scanning SQUID microscopy

    NASA Astrophysics Data System (ADS)

    Lin, Shi-Zeng; Bulaevskii, Lev N.

    2012-07-01

    The working principle of magnetic force microscopy and scanning SQUID microscopy is introducing a magnetic source near a superconductor and measuring the magnetic field distribution near the superconductor, from which one can obtain the penetration depth. We investigate the magnetic field distribution near the surface of a magnetic superconductor when a magnetic source is placed close to the superconductor, which can be used to extract both the penetration depth λL and magnetic susceptibility χ by magnetic force microscopy or scanning SQUID microscopy. When the magnetic moments are parallel to the surface, one extracts λL/1-4πχ. When the moments are perpendicular to the surface, one obtains λL. By changing the orientation of the crystal, one thus is able to extract both χ and λL.

  16. TlCaBaCuO high Tc superconducting microstrip ring resonators designed for 12 GHz

    NASA Technical Reports Server (NTRS)

    Subramanyam, G.; Kapoor, V. J.; Chorey, C. M.; Bhasin, K. B.

    1993-01-01

    Microwave properties of sputtered Tl-Ca-Ba-Cu-O thin films were investigated by designing, fabricating, and testing microstrip ring resonators. Ring resonators designed for 12 GHz fundamental resonance frequency, were fabricated and tested. From the unloaded Q values for the resonators, the surface resistance was calculated by separating the conductor losses from the total losses. The penetration depth was obtained from the temperature dependence of resonance frequency, assuming that the shift in resonance frequency is mainly due to the temperature dependence of penetration depth. The effective surface resistance at 12 GHz and 77 K was determined to be between 1.5 and 2.75 mOmega, almost an order lower than Cu at the same temperature and frequency. The effective penetration depth at 0 K is approximately 7000 A.

  17. Results of the application of seismic-reflection and electromagnetic techniques for near-surface hydrogeologic and environmental investigations at Fort Bragg, North Carolina

    USGS Publications Warehouse

    Meyer, M.T.; Fine, J.M.

    1997-01-01

    As part of the U.S. Geological Survey's Resource Conservation and Recovery Act, Facilities Investigations at Fort Bragg, North Carolina, selected geophysical techniques were evaluated for their usefulness as assessment tools for determining subsurface geology, delineating the areal extent of potentially contaminated landfill sites, and locating buried objects and debris of potential environmental concern. Two shallow seismic-reflection techniques (compression and shear wave) and two electromagnetic techniques (ground-penetrating radar and terrain conductivity) were evaluated at several sites at the U.S. Army Base. The electromagnetic techniques also were tested for tolerance to cultural noise, such as nearby fences, vehicles, and power lines. For the terrain conductivity tests, two instruments were used--the EM31 and EM34, which have variable depths of exploration. The shallowest reflection event was 70 feet below land surface observed in common-depth point, stacked compression-wave data from 24- and 12-fold shallow-seismic-reflection surveys. Several reflection events consistent with clay-sand interfaces between 70 and 120 feet below land surface, along with basement-saprolite surfaces, were imaged in the 24-fold, common- depth-point stacked data. 12-fold, common-depth-point stacked data set contained considerably more noise than the 24-fold, common-depth-point data, due to reduced shot-to-receiver redundancy. Coherent stacked reflection events were not observed in the 24-fold, common-depth-point stacked shear-wave data because of the partial decoupling of the shear- wave generator from the ground. At one site, ground-penetrating radar effectively delineated a shallow, 2- to 5-foot thick sand unit bounded by thin (less than 1 foot) clay layers. The radar signal was completely attenuated where the overlying and underlying clay units thickened and the sand unit thinned. The pene- tration depth of the radar signal was less than 10 feet below land surface. A slight increase in electromagnetic conductivity across shallow sampling EM31 and EM34 profiles provided corroborative evidence of the shallow, thickening clay units. Plots of raw EM31 and EM34 data provided no direct interpretable information to delineate sand and clay units in the shallow subsurface. At two sites, the ground-penetrating radar effectively delineated the lateral continuity of surficial sand units 5 to 25 feet in thickness and the tops of their underlying clay units. The effective exploration depth of the ground-penetrating radar was limited by the proximity of clay units to the subsurface and their thickness. The ground-penetrating radar delineated the areal extent and depth of cover at a previously unrecognized extension of a trench-like landfill underlying a vehicle salvage yard. Attenuation of the radar signal beneath the landfill cover and the adjacent subsurface clays made these two mediums indistinguishable by ground-penetrating radar; however, EM31 data indicated that the electrical conductivity of the landfill was higher than the subsurface material adjacent to the landfill. The EM31 and EM34 conductivity surveys defined the areal extent of a landfill whose boundaries were inaccurately mapped, and also identified the locations of an old dumpsite and waste incinerator site at another landfill. A follow-up ground-penetrating radar survey of the abandoned dumpsite showed incongruities in some of the shallow radar reflections interpreted as buried refuse dispersed throughout the landfill. The ground-penetrating radar and EM31 effectively delineated a shallow buried fuel-oil tank. Of the three electromagnetic instruments, the ground-penetrating radar with the shielded 100-megahertz antenna was the least affected by cultural noise followed, in order, by the EM31 and EM34. The combination of terrain- conductivity and ground-penetrating radar for the site assessment of the landfill provided a powerful means to identify the areal extent of the landfill, potenti

  18. Investigation of Pesticide Penetration and Persistence on Harvested and Live Basil Leaves Using Surface-Enhanced Raman Scattering Mapping.

    PubMed

    Yang, Tianxi; Zhao, Bin; Kinchla, Amanda J; Clark, John M; He, Lili

    2017-05-03

    Understanding pesticide behavior in plants is important for effectively applying pesticides and in reducing pesticide exposures from ingestion. This study aimed to investigate the penetration and persistence of pesticides applied on harvested and live basil leaves. Surface-enhanced Raman scattering (SERS) mapping was applied for in situ and real-time tracking of pesticides over time using gold nanoparticles as probes. The results showed that, after surface exposure of 30 min to 48 h, pesticides (10 mg/L) penetrated more rapidly and deeply into the live leaves than the harvested leaves. The systemic pesticide thiabendazole and the nonsystemic pesticide ferbam can penetrate into the live leaves with depths of 225 and 130 μm, respectively, and the harvested leaves with depths of 180 and 18 μm, respectively, after 48 h of exposure. The effects of leaf integrity and age on thiabendazole penetration were also evaluated on live basil leaves after 24 h of exposure. Thiabendazole (10 mg/L) when applied onto intact leaves penetrated deeper (170 μm) than when applied onto damaged leaves (80 μm) prepared with 20 scrapes on the top surface of the leaves. Older leaves with a wet mass of 0.204 ± 0.019 g per leaf (45 days after leaf out) allowed more rapid and deeper penetration of pesticides (depth of 165 μm) than younger leaves with a wet mass of 0.053 ± 0.007 g per leaf (15 days after leaf out, depth of 95 μm). The degradation of thiabendazole on live leaves was detected after 1 week, whereas the apparent degradation of ferbam was detected after 2 weeks. In addition, the removal of pesticides from basil was more efficient when compared with other fresh produce possibly due to the specific gland structure of basil leaves. The information obtained here provides a better understanding of the behavior and biological fate of pesticides on plants.

  19. Analysis of SIR-B radar illumination of geometry for depth of penetration and surface feature and vegetation detection, Nevada and California

    NASA Technical Reports Server (NTRS)

    Taranik, J. V.; Slemmons, D. B.; Bell, E. J.; Borengasser, M.; Lugaski, T. P.; Vreeland, H.; Vreeland, P.; Kleiner, E.; Peterson, F. F.; Kleiforth, H.

    1984-01-01

    The measurement capability provided by the Shuttle Imaging Radar (SIR-B) was used to determine: (1) the relationships between radar illumination geometry and depth of penetration in different climatic and physiographic environments in Nevada; and, (2) the relationships between radar illumination geometry and detection and analysis of structural features in different climatic and physiographic environments in Nevada.

  20. Application of ground-penetrating radar technique to evaluate the waterfront location in hardened concrete

    NASA Astrophysics Data System (ADS)

    Rodríguez-Abad, Isabel; Klysz, Gilles; Martínez-Sala, Rosa; Balayssac, Jean Paul; Mené-Aparicio, Jesús

    2016-12-01

    The long-term performance of concrete structures is directly tied to two factors: concrete durability and strength. When assessing the durability of concrete structures, the study of the water penetration is paramount, because almost all reactions like corrosion, alkali-silica, sulfate, etc., which produce their deterioration, require the presence of water. Ground-penetrating radar (GPR) has shown to be very sensitive to water variations. On this basis, the objective of this experimental study is, firstly, to analyze the correlation between the water penetration depth in concrete samples and the GPR wave parameters. To do this, the samples were immersed into water for different time intervals and the wave parameters were obtained from signals registered when the antenna was placed on the immersed surface of the samples. Secondly, a procedure has been developed to be able to determine, from those signals, the reliability in the detection and location of waterfront depths. The results have revealed that GPR may have an enormous potential in this field, because excellent agreements were found between the correlated variables. In addition, when comparing the waterfront depths calculated from GPR measurements and those visually registered after breaking the samples, we observed that they totally agreed when the waterfront was more than 4 cm depth.

  1. Supercurrent in ferromagnetic Josephson junctions with heavy metal interlayers

    NASA Astrophysics Data System (ADS)

    Satchell, Nathan; Birge, Norman O.

    2018-06-01

    The length scale over which supercurrent from conventional BCS, s -wave superconductors (S ) can penetrate an adjacent ferromagnetic (F ) layer depends on the ability to convert singlet Cooper pairs into triplet Cooper pairs. Spin-aligned triplet Cooper pairs are not dephased by the ferromagnetic exchange interaction and can thus penetrate an F layer over much longer distances than singlet Cooper pairs. These triplet Cooper pairs carry a dissipationless spin current and are the fundamental building block for the fledgling field of superspintronics. Singlet-triplet conversion by inhomogeneous magnetism is well established. Here, we describe an attempt to use spin-orbit coupling as an alternative mechanism to mediate singlet-triplet conversion in S-F-S Josephson junctions. We report that the addition of thin Pt spin-orbit-coupling layers in our Josephson junctions significantly increases supercurrent transmission, however the decay length of the supercurrent is not found to increase. We attribute the increased supercurrent transmission to Pt acting as a buffer layer to improve the growth of the Co F layer.

  2. Diagnostics of transparent polymer coatings of metal items

    NASA Astrophysics Data System (ADS)

    Varepo, L. G.; Ermakova, I. N.; Nagornova, I. V.; Kondratov, A. P.

    2017-08-01

    The methods of visual and instrumental express diagnostics of safety critical defects and non-uniform thickness of transparent mono- and multilayer polyolefin surface coating of metal items are analyzed in the paper. The instrumental diagnostics method relates to colorimetric measuring based on effects, which appear in the polarized light for extrusion polymer coatings. A color coordinates dependence (in the color system CIE La*b*) on both HDPE / PVC coating thickness fluctuation values (from average ones) and coating interlayer or adhesion layer delaminating is shown. A variation of color characteristics in the polarized light at a liquid penetration into delaminated polymer layers is found. Measuring parameters and critical uncertainties are defined.

  3. Comparison of Vibringe, EndoActivator, and needle irrigation on sealer penetration in extracted human teeth.

    PubMed

    Bolles, Jordan A; He, Jianing; Svoboda, Kathy K H; Schneiderman, Emet; Glickman, Gerald N

    2013-05-01

    Vibringe is a new device that allows continuous sonic irrigation of the canal system during endodontic treatment. The aim of this study was to compare the effect of different irrigation systems on sealer penetration into dentinal tubules of extracted single-rooted teeth. Fifty single-rooted human teeth were instrumented and randomly divided into 4 groups: group 1 (control), saline; group 2 (conventional irrigation), 17% EDTA followed by 6% NaOCl; group 3 (EndoActivator), same irrigants as group 2; group 4 (Vibringe), same irrigants as group 2. Obturation of all teeth was done with gutta-percha and SimpliSeal labeled with fluorescent dye. Transverse sections at 1 mm and 5 mm from the root apex were examined by using confocal laser scanning microscopy. Percentage and maximum depth of sealer penetration were measured by using NIS-Elements Br 3.0 imaging software. Groups 3 and 4 had a significantly greater percentage of the canal wall penetrated by sealer at the 5-mm level than group 1 (P < .0125), but not group 2. No other differences were found between the groups at either section level for both the percentage of sealer penetration and maximum depth. The 5-mm sections in each experimental group had a significantly higher percentage and maximum depth of sealer penetration than did the 1-mm sections (P < .0125). The use of sonic activation with either the EndoActivator or Vibringe did not significantly improve the sealer penetration when compared with conventional irrigation. Copyright © 2013 American Association of Endodontists. Published by Elsevier Inc. All rights reserved.

  4. What Is the Optimal Minimum Penetration Depth for "All-Inside" Meniscal Repairs?

    PubMed

    McCulloch, Patrick C; Jones, Hugh L; Lue, Jeffrey; Parekh, Jesal N; Noble, Philip C

    2016-08-01

    To identify desired minimum depth setting for safe, effective placement of the all-inside meniscal suture anchors. Using 16 cadaveric knees and standard arthroscopic techniques, 3-dimensional surfaces of the meniscocapsular junction and posterior capsule were digitized. Using standard anteromedial and anterolateral portals, the distance from the meniscocapsular junction to the posterior capsule outer wall was measured for 3 locations along the posterior half of medial and lateral menisci. Multiple all-inside meniscal repairs were performed on 7 knees to determine an alternate measure of capsular thickness (X2) and compared with the digitized results. In the digitized group, the distance (X1) from the capsular junction to the posterior capsular wall was averaged in both menisci for 3 regions using anteromedial and anterolateral portals. Mean distances of 6.4 to 8.8 mm were found for the lateral meniscus and 6.5 to 9.1 mm for the medial meniscus. The actual penetration depth was determined in the repair group and labeled X2. It showed a similar pattern to the variation seen in X1 by region, although it exceeded predicted distances an average 1.7 mm in the medial and 1.5 mm in the lateral meniscus owing to visible deformation of the capsule as it pierced. Capsular thickness during arthroscopic repair measures approximately 6 to 9 mm (X1), with 1.5 to 2 mm additional depth needed to ensure penetration rather than bulging of the posterior capsule (X2), resulting in 8 to 10 mm minimum penetration depth range. Surgeons can add desired distance away from the meniscocapsular junction (L) at device implantation, finding optimal minimal setting for penetration depth (X2 + L), which for most repairable tears may be as short as 8 mm and not likely to be greater than 16 mm. Minimum depth setting for optimal placement of all-inside meniscal suture anchors when performing all-inside repair of the medial or lateral meniscus reduces risk of harming adjacent structures secondary to overpenetration and underpenetration of the posterior capsule. Copyright © 2016 Arthroscopy Association of North America. Published by Elsevier Inc. All rights reserved.

  5. Study of motion of optimal bodies in the soil of grid method

    NASA Astrophysics Data System (ADS)

    Kotov, V. L.; Linnik, E. Yu

    2016-11-01

    The paper presents a method of calculating the optimum forms in axisymmetric numerical method based on the Godunov and models elastoplastic soil vedium Grigoryan. Solved two problems in a certain definition of generetrix rotation of the body of a given length and radius of the base, having a minimum impedance and maximum penetration depth. Numerical calculations are carried out by a modified method of local variations, which allows to significantly reduce the number of operations at different representations of generetrix. Significantly simplify the process of searching for optimal body allows the use of a quadratic model of local interaction for preliminary assessments. It is noted the qualitative similarity of the process of convergence of numerical calculations for solving the optimization problem based on local interaction model and within the of continuum mechanics. A comparison of the optimal bodies with absolutely optimal bodies possessing the minimum resistance of penetration below which is impossible to achieve under given constraints on the geometry. It is shown that the conical striker with a variable vertex angle, which equal to the angle of the solution is absolutely optimal body of minimum resistance of penetration for each value of the velocity of implementation will have a final depth of penetration is only 12% more than the traditional body absolutely optimal maximum depth penetration.

  6. Robotic astrobiology - the need for sub-surface penetration of Mars

    NASA Astrophysics Data System (ADS)

    Ellery, A.; Ball, A.; Cockell, C.; Coste, P.; Dickensheets, D.; Edwards, H.; Hu, H.; Kolb, C.; Lammer, H.; Lorenz, R.; McKee, G.; Richter, L.; Winfield, A.; Welch, C.

    2002-11-01

    Recent interest in the astrobiological investigation of Mars has culminated in the only planned astrobiology-focussed robotic mission to Mars - the Beagle2 mission to be carried to Mars by the Mars Express spacecraft in 2003. Beagle2 will be primarily investigating the surface and near-surface environment of Mars. However, the results from the Viking Mars lander indicated that the Martian surface is saturated in peroxides and super-oxides which would rapidly degrade any organic material. Furthermore, recent models of gardening due to meteoritic impacts on the Martian surface suggest that the depth of this oxidising layer could extend to depths of 2-3m. Given that the discovery of organic fossilised residues will be the primary target for astrobiological investigation, this implies that future robotic astrobiology missions to Mars must penetrate to below these depths. The need to penetrate into the sub-surface of Mars has recently been given greater urgency with the discovery of extensive water ice-fields as little as 1m from the surface. We review the different technologies that make this penetration into the sub-surface a practical possibility on robotic missions. We further briefly present one such implementation of these technologies through the use of ground-penetrating moles - The Vanguard Mars mission proposal.

  7. The Tubular Penetration Depth and Adaption of Four Sealers: A Scanning Electron Microscopic Study

    PubMed Central

    Chen, Huan; Zhao, Xinyuan; Qiu, Yu; Xu, Dengyou

    2017-01-01

    Background. The tubular penetration and adaptation of the sealer are important factors for successful root canal filling. The aim of this study was to evaluate the tubular penetration depth of four different sealers in the coronal, middle, and apical third of root canals as well as the adaptation of these sealers to root canal walls. Materials and Methods. 50 single-rooted teeth were prepared in this study. Forty-eight of them were filled with different sealers (Cortisomol, iRoot SP, AH-Plus, and RealSeal SE) and respective core filling materials. Then the specimens were sectioned and scanning electron microscopy was employed to assess the tubular penetration and adaptation of the sealers. Results. Our results demonstrated that the maximum penetration was exhibited by RealSeal SE, followed by AH-Plus, iRoot SP, and Cortisomol. As regards the adaptation property to root canal walls, AH-Plus has best adaptation capacity followed by iRoot SP, RealSeal SE, and Cortisomol. Conclusion. The tubular penetration and adaptation vary with the different sealers investigated. RealSeal SE showed the most optimal tubular penetration, whereas AH-Plus presented the best adaptation to the root canal walls. PMID:29479539

  8. High-frequency Pulse-compression Ultrasound Imaging with an Annular Array

    NASA Astrophysics Data System (ADS)

    Mamou, J.; Ketterling, J. A.; Silverman, R. H.

    High-frequency ultrasound (HFU) allows fine-resolution imaging at the expense of limited depth-of-field (DOF) and shallow acoustic penetration depth. Coded-excitation imaging permits a significant increase in the signal-to-noise ratio (SNR) and therefore, the acoustic penetration depth. A 17-MHz, five-element annular array with a focal length of 31 mm and a total aperture of 10 mm was fabricated using a 25-μm thick piezopolymer membrane. An optimized 8-μs linear chirp spanning 6.5-32 MHz was used to excite the transducer. After data acquisition, the received signals were linearly filtered by a compression filter and synthetically focused. To compare the chirp-array imaging method with conventional impulse imaging in terms of resolution, a 25-μm wire was scanned and the -6-dB axial and lateral resolutions were computed at depths ranging from 20.5 to 40.5 mm. A tissue-mimicking phantom containing 10-μm glass beads was scanned, and backscattered signals were analyzed to evaluate SNR and penetration depth. Finally, ex-vivo ophthalmic images were formed and chirp-coded images showed features that were not visible in conventional impulse images.

  9. Frequency, field, and temperature dependence of the AC penetration depth of a GdBa 2Cu 3O 7-δ film in the mixed state

    NASA Astrophysics Data System (ADS)

    Zeisberger, M.; Klupsch, Th.; Michalke, W.

    1995-02-01

    We report on a systematic mutual induction measurement of the complex AC penetration depth λ of a sputtered high-quality GdBa 2Cu 3O 7-δ film in the mixed state by a very small coil system arranged near the sample surface. The complex penetration depth λ( B, T, ω) for DC inductions B ⩽ 0.65 T (perpendicular to the film), for temperatures 36 K ⩽ T ⩽ 81 K, and for frequencies 1 kHz ⩽ ω/2 π ⩽ 500 kHz was determined from the measured signal by a novel inversion scheme. The results are consistent with theoretical predictions based upon single vortex pinning. The Labusch parameter α, the flux creep relaxation time τ, as well as the effective activation energy U are simulateneously determined.

  10. Single-vortex pinning and penetration depth in superconducting NdFeAsO 1-xF x

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Zhang, Jessie T.; Kim, Jeehoon; Huefner, Magdalena

    2015-10-12

    We use a magnetic force microscope (MFM) to investigate single vortex pinning and penetration depth in NdFeAsO 1-xF x, one of the highest-T c iron-based superconductors. In fields up to 20 Gauss, we observe a disordered vortex arrangement, implying that the pinning forces are stronger than the vortex-vortex interactions. We measure the typical force to depin a single vortex, F depin ≃ 4.5 pN, corresponding to a critical current up to J c ≃ 7×10 5 A/cm 2. As a result, our MFM measurements allow the first local and absolute determination of the superconducting in-plane penetration depth in NdFeAsO 1-xFmore » x, λ ab = 320 ± 60 nm, which is larger than previous bulk measurements.« less

  11. Tritium analysis of divertor tiles used in JET ITER-like wall campaigns by means of β-ray induced x-ray spectrometry

    NASA Astrophysics Data System (ADS)

    Hatano, Y.; Yumizuru, K.; Koivuranta, S.; Likonen, J.; Hara, M.; Matsuyama, M.; Masuzaki, S.; Tokitani, M.; Asakura, N.; Isobe, K.; Hayashi, T.; Baron-Wiechec, A.; Widdowson, A.; contributors, JET

    2017-12-01

    Energy spectra of β-ray induced x-rays from divertor tiles used in ITER-like wall campaigns of the Joint European Torus were measured to examine tritium (T) penetration into tungsten (W) layers. The penetration depth of T evaluated from the intensity ratio of W(Lα) x-rays to W(Mα) x-rays showed clear correlation with poloidal position; the penetration depth at the upper divertor region reached several micrometers, while that at the lower divertor region was less than 500 nm. The deep penetration at the upper part was ascribed to the implantation of high energy T produced by DD fusion reactions. The poloidal distribution of total x-ray intensity indicated higher T retention in the inboard side than the outboard side of the divertor region.

  12. Confocal Raman microscopic investigation of the effectiveness of penetration enhancers for procaine delivery to the skin

    NASA Astrophysics Data System (ADS)

    Lunter, Dominique; Daniels, Rolf

    2014-12-01

    A methodology that employs confocal Raman microscopy (CRM) on ex vivo skin samples is proposed for the investigation of drug content and distribution in the skin. To this end, the influence of the penetration enhancers propylene glycol and polyoxyethylene-23-lauryl ether on the penetration and permeation of procaine as a model substance was investigated. The drug content of skin samples that had been incubated with semisolid formulations containing one of these enhancers was examined after skin segmentation. The experiments showed that propylene glycol did not affect the procaine content that was delivered to the skin, whereas polyoxyethylene-23-lauryl ether led to higher procaine contents and deeper penetration. Neither substance was found to influence the permeation rate of procaine. It is thereby shown that CRM can provide additional information on drug penetration and permeation. Furthermore, the method was found to enhance the depth from which Raman spectra can be collected and to improve the depth resolution compared to previously proposed methods.

  13. Campbell penetration depth in Fe-based superconductors

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Prommapan, Plegchart

    A 'true' critical current density, j c, as opposite to commonly measured relaxed persistent (Bean) current, j B, was extracted from the Campbell penetration depth, Λ c(T,H) measured in single crystals of LiFeAs, and optimally electron-doped Ba(Fe 0.954Ni 0.046) 2As 2 (FeNi122). In LiFeAs, the effective pinning potential is nonparabolic, which follows from the magnetic field - dependent Labusch parameter α. At the equilibrium (upon field - cooling), α(H) is non-monotonic, but it is monotonic at a finite gradient of the vortex density. This behavior leads to a faster magnetic relaxation at the lower fields and provides a natural dynamicmore » explanation for the fishtail (second peak) effect. We also find the evidence for strong pinning at the lower fields.The inferred field dependence of the pinning potential is consistent with the evolution from strong pinning, through collective pinning, and eventually to a disordered vortex lattice. The value of jc(2 K) ≅ 1.22 x 10 6 A/cm 2 provide an upper estimate of the current carrying capability of LiFeAs. Overall, vortex behavior of almost isotropic, fully-gapped LiFeAs is very similar to highly anisotropic d-wave cuprate superconductors, the similarity that requires further studies in order to understand unconventional superconductivity in cuprates and pnictides. In addition to LiFeAs, we also report the magnetic penetration depth in BaFe 2As 2 based superconductors including irradiation of FeNi122. In unirradiated FeNi122, the maximum critical current value is, j c(2K) ≅ 3.3 x 10 6 A/cm 2. The magnetic-dependent feature was observed near the transition temperature in FeTe 0.53Se 0.47 and irradiated FeNi122. Because of this feature, further studies are required in order to properly calibrate the Campbell penetration depth. Finally, we detected the crossing between the magnetic penetration depth and London penetration depth in optimally hold-doped Ba 0.6K 0.4Fe 2As 2 (BaK122) and isovalent doped BaFe 2(As 0.7P 0.3) 2 (BaP122). These phenomena probably coincide with anomalous Meissner effect reported in pnicitde superconductors [Prozorov et al. (2010b)] however more studies are needed in order to clarify this.« less

  14. Campbell penetration depth in iron-based superconductors

    NASA Astrophysics Data System (ADS)

    Prommapan, Plengchart

    2011-12-01

    A "true" critical current density, jc, as opposite to commonly measured relaxed persistent (Bean) current, jB, was extracted from the Campbell penetration depth, lambda C(T, H) measured in single crystals of LiFeAs, and optimally electron-doped Ba (Fe0.954Ni 0.046)2As2 (FeNi122). In LiFeAs, the effective pinning potential is non-parabolic, which follows from the magnetic field - dependent Labusch parameter alpha. At the equilibrium (upon field - cooling), alpha( H) is non-monotonic, but it is monotonic at a finite gradient of the vortex density. This behavior leads to a faster magnetic relaxation at the lower fields and provides a natural dynamic explanation for the fishtail (second peak) effect. We also find the evidence for strong pinning at the lower fields.The inferred field dependence of the pinning potential is consistent with the evolution from strong pinning, through collective pinning, and eventually to a disordered vortex lattice. The value of j c (2 K) ≃ 1:22 x106 A/cm² provide an upper estimate of the current carrying capability of LiFeAs. Overall, vortex behavior of almost isotropic, fully-gapped LiFeAs is very similar to highly anisotropic d-wave cuprate superconductors, the similarity that requires further studies in order to understand unconventional superconductivity in cuprates and pnictides. In addition to LiFeAs, we also report the magnetic penetration depth in BaFe2As2 based superconductors including irradiation of FeNi122. In unirradiated FeNi122, the maximum critical current value is, jc(2 K) ≃ 3.3 x 106 A/cm². The magnetic-dependent feature was observed near the transition temperature in FeTe0.53Se0.47 and irradiated FeNi122. Because of this feature, further studies are required in order to properly calibrate the Campbell penetration depth. Finally, we detected the crossing between the magnetic penetration depth and London penetration depth in optimally hold-doped Ba0.6K 0.4Fe2As2 (BaK122) and isovalent doped BaFe2(As0.7P0.3)2 (BaP122). These phenomena probably coincide with anomalous Meissner effect reported in pnictide superconductors [Prozorov et al. (2010b)] however more studies are needed in order to clarify this.

  15. Skin pre-ablation and laser assisted microjet injection for deep tissue penetration.

    PubMed

    Jang, Hun-Jae; Yeo, Seonggu; Yoh, Jack J

    2017-04-01

    For conventional needless injection, there still remain many unresolved issues such as the potential for cross-contamination, poor reliability of targeted delivery dose, and significantly painstaking procedures. As an alternative, the use of microjets generated with Er:YAG laser for delivering small doses with controlled penetration depths has been reported. In this study, a new system with two stages is evaluated for effective transdermal drug delivery. First, the skin is pre-ablated to eliminate the hard outer layer and second, laser-driven microjet penetrates the relatively weaker and freshly exposed epidermis. Each stage of operation shares a single Er:YAG laser that is suitable for skin ablation as well as for the generation of a microjet. In this study, pig skin is selected for quantification of the injection depth based on the two-stage procedure, namely pre-ablation and microjet injection. The three types of pre-ablation devised here consists of bulk ablation, fractional ablation, and fractional-rotational ablation. The number of laser pulses are 12, 18, and 24 for each ablation type. For fractional-rotational ablation, the fractional beams are rotated by 11.25° at each pulse. The drug permeation in the skin is evaluated using tissue marking dyes. The depth of penetration is quantified by a cross sectional view of the single spot injections. Multi-spot injections are also carried out to control the dose and spread of the drug. The benefits of a pre-ablation procedure prior to the actual microjet injection to the penetration is verified. The four possible combinations of injection are (a) microjet only; (b) bulk ablation and microjet injection; (c) fractional ablation and microjet injection; and (d) fractional-rotational ablation and microjet injection. Accordingly, the total depth increases with injection time for all cases. In particular, the total depth of penetration attained via fractional pre-ablation increased by 8 ∼ 11% and that of fractional-rotational pre-ablation increased by 13 ∼ 33%, when compared with the no pre-ablation or microjet only cases. A noticeable point is that the fraction-rotational pre-ablation and microjet result is comparable to the bulk ablation and microjet result of 11 ∼ 42%. The penetration depth underneath ablated stratum corneum (SC) is also measured in order to verify the pre-ablation effect. The penetration depths for each case are (a) 443 ± 104 µm; (b) 625 ± 98 µm; (c) 523 ± 95 µm; and (d) 595 ± 141 µm for microjet only, bulk ablation and microjet, fractional ablation and microjet, and fractional-rotational ablation and microjet, respectively. This is quite beneficial since any healing time associated with ablation is significantly reduced by avoiding hard-core bulk ablation. Thus the bulk pre-ablation and microjet may well be superseded by the less invasive fractiona-rotational ablation followed by the microjet injection. The density of micro-holes is 1.27 number/mm 2 for fractional ablation and 4.84 number/mm 2 for fractional-rotational ablation. The penetration depths measured underneath the ablated SC are 581 µm (fractional ablation and microjet) and 691 µm (fractional-rotational ablation and microjet). Fractional-rotational ablation increases number of micro-holes in a unit area, enabling fast reepithelialization and high drug delivery efficiency. Optimization of system parameters such as ablation time, number of ablations, and injection time will eventually ensure a macromolecule delivery technique with the potential to include vaccines, insulins, and growth hormones, all of which require deeper penetration into the skin. Lasers Surg. Med. 49:387-394, 2017. © 2016 Wiley Periodicals, Inc. © 2016 Wiley Periodicals, Inc.

  16. Controllably Designed "Vice-Electrode" Interlayers Harvesting High Performance Lithium Sulfur Batteries.

    PubMed

    Hao, Youchen; Xiong, Dongbin; Liu, Wen; Fan, Linlin; Li, Dejun; Li, Xifei

    2017-11-22

    An interlayer has been regarded as a promising mediator to prolong the life span of lithium sulfur batteries because its excellent absorbability to soluble polysulfide efficiently hinders the shuttle effect. Herein, we designed various interlayers and understand the working mechanism of an interlayer for lithium sulfur batteries in detail. It was found that the electrochemical performance of a S electrode for an interlayer located in cathode side is superior to the pristine one without interlayers. Surprisingly, the performance of the S electrode for an interlayer located in anode side is poorer than that of pristine one. For comparison, glass fibers were also studied as a nonconductive interlayer for lithium sulfur batteries. Unlike the two interlayers above, these nonconductive interlayer did displays significant capacity fading because polysulfides were adsorbed onto insulated interlayer. Thus, the nonconductive interlayer function as a "dead zone" upon cycling. Based on our findings, it was for the first time proposed that a controllably optimized interlayer, with electrical conductivity as well as the absorbability of polysulfides, may function as a "vice-electrode" of the anode or cathode upon cycling. Therefore, the cathodic conductive interlayer can enhance lithium sulfur battery performance, and the anodic conductive interlayer may be helpful for the rational design of 3D networks for the protection of lithium metal.

  17. Microplasma effect on skin scaffold for melanoma cancer treatment

    NASA Astrophysics Data System (ADS)

    Abdullah, Zulaika; Zaaba, S. K.; Mustaffa, M. T.; Mohamad, C. W. S. R.; Zakaria, A.

    2017-03-01

    An atmospheric plasma system using Helium gas was developed. The effect of helium plasma treatment on skin scaffold surface was studied by scanning electron microscopy (SEM). The changes of skin scaffold surfaces before and after helium plasma treatment was recorded. The surface of skin scaffold changed with the prolonged of helium plasma treatment time. The depth of helium plasma penetration was studied using methylene blue dye staining method. The methylene blue will detect the presence or absence of an oxygen that was induced from plasma excitation. The presence of the oxygen indicated on the depth of helium plasma penetration. Results showed plasma are able to penetrate 4mm of skin scaffold after 1200 seconds of exposure.

  18. Depth and Motion Prediction for Earth Penetrators

    DTIC Science & Technology

    1978-06-01

    multiple-layer targets. For targets with accurately knowni properties , the final-depth results are accurate ihný pret AM all13 EIIW FINVS S WLT n.- U lass S...Project hAl611o2AT2?, Task A2, Work Unit󈧊, " Effectiveness of Earth Penetrators in Various Geologic Environments." Mr. R. S. Bernard conducted the... effects in the selective destruction of localized targets (airfields, factories, utilities, etc.). The effectiveness of these weapons, however, is

  19. Time and space resolved current density mapping in three dimensions using magnetic field probe array in a high voltage coaxial gap

    NASA Astrophysics Data System (ADS)

    Cordaro, S. W.; Bott-Suzuki, S. C.

    2017-12-01

    We present an experimental analysis of the symmetry of current density in a coaxial geometry, diagnosed using a magnetic field probe array and calculations of the Fowler-Nordheim enhancement factor. Data were collected on the coaxial gap breakdown device (240 A, 25 kV, 150 ns, ˜0.1 Hz), and data from experiments using 2 different gap sizes and different penetration depths are compared over runs comprising 50 shots for each case. The magnetic field probe array quantifies the distribution of current density at three axial locations, on either sides of a vacuum breakdown, and tracks the evolution with time and space. The results show asymmetries in current density, which can be influenced by changes in the gap size and the penetration depth (of the center electrode into the outer electrode). For smaller gap sizes (400 μm), symmetric current profiles were not observed, and the change in the penetration depth changes both the symmetric behavior of the current density and the enhancement factor. For larger gaps (900 μm), current densities were typically more uniform and less influenced by the penetration depth, which is reflected in the enhancement factor values. It is possible that the change in inductance caused by the localization of current densities plays a role in the observed behavior.

  20. Cyclic mechanical loading promotes bacterial penetration along composite restoration marginal gaps

    PubMed Central

    Khvostenko, D.; Salehi, S.; Naleway, S. E.; Hilton, T. J.; Ferracane, J. L.; Mitchell, J. C.; Kruzic, J. J.

    2015-01-01

    Objectives Secondary caries is the most common reason for composite restoration replacement and usually forms between dentin and the filling. The objective of this study was to investigate the combined effect of cyclic loading and bacterial exposure on bacterial penetration into gaps at the interface between dentin and resin composite restorative material using a novel bioreactor system and test specimen design. Methods Human molars were machined into 3 mm thick disks with 2 mm deep × 5 mm diameter cavity preparations into which composite restorations were placed. A ∼15-30 micrometer (small) or ∼300 micrometer wide (large) dentin-restoration gap was introduced along half of the interface between the dentin and restoration. Streptococcus mutans UA 159 biofilms were grown on each sample prior to testing in a bioreactor both with and without cyclic loading. Both groups of samples were tested for 2 weeks and post-test biofilm viability was confirmed with a live-dead assay. Samples were fixed, mounted and cross-sectioned to reveal the gaps and observe the depth of bacterial penetration. Results It was shown that for large gap samples the bacteria easily penetrated to the full depth of the gap independent of loading or non-loading conditions. The results for all cyclically loaded small gap samples show a consistently deep bacterial penetration down 100% of the gap while the average penetration depth was only 67% for the non-loaded samples with only two of six samples reaching 100%. Significance A new bioreactor was developed that allows combining cyclic mechanical loading and bacterial exposure of restored teeth for bacterial biofilm and demineralization studies. Cyclic loading was shown to aid bacterial penetration into narrow marginal gaps, which could ultimately promote secondary caries formation. PMID:25900624

  1. Effect of Irradiation on Tissue Penetration Depth of Doxorubicin after Pressurized Intra-Peritoneal Aerosol Chemotherapy (PIPAC) in a Novel Ex-Vivo Model.

    PubMed

    Khosrawipour, Veria; Giger-Pabst, Urs; Khosrawipour, Tanja; Pour, Yousef Hedayat; Diaz-Carballo, David; Förster, Eckart; Böse-Ribeiro, Hugo; Adamietz, Irenäus Anton; Zieren, Jürgen; Fakhrian, Khashayar

    2016-01-01

    This study was performed to assess the impact of irradiation on the tissue penetration depth of doxorubicin delivered during Pressurized Intra-Peritoneal Aerosol Chemotherapy (PIPAC). Fresh post mortem swine peritoneum was cut into 10 proportional sections. Except for 2 control samples, all received irradiation with 1, 2, 7 and 14 Gy, respectively. Four samples received PIPAC 15 minutes after irradiation and 4 other after 24 hours. Doxorubicin was aerosolized in an ex-vivo PIPAC model at 12 mmHg/36°C. In-tissue doxorubicin penetration was measured using fluorescence microscopy on frozen thin sections. Doxorubicin penetration after PIPAC (15 minutes after irradiation) was 476 ± 74 µm for the control sample, 450 ± 45µm after 1 Gy (p > 0.05), 438 ± 29 µm after 2 Gy (p > 0.05), 396 ± 32 µm after 7 Gy (p = 0.005) and 284 ± 57 after 14 Gy irradiation (p < 0.001). The doxorubicin penetration after PIPAC (24 hours after irradiation) was 428 ± 77 µm for the control sample, 393 ± 41 µm after 1 Gy (p > 0.05), 379 ± 56 µm after 2 Gy (p > 0.05), 352 ± 53 µm after 7 Gy (p = 0.008) and 345 ± 53 after 14 Gy irradiation (p = 0.001). Higher (fractional) radiation dose might reduce the tissue penetration depth of doxorubicin in our ex-vivo model. However, irradiation with lower (fractional) radiation dose does not affect the tissue penetration negatively. Further studies are warranted to investigate if irradiation can be used safely as chemopotenting agent for patients with peritoneal metastases treated with PIPAC.

  2. Computational Transport Modeling of High-Energy Neutrons Found in the Space Environment

    NASA Technical Reports Server (NTRS)

    Cox, Brad; Theriot, Corey A.; Rohde, Larry H.; Wu, Honglu

    2012-01-01

    The high charge and high energy (HZE) particle radiation environment in space interacts with spacecraft materials and the human body to create a population of neutrons encompassing a broad kinetic energy spectrum. As an HZE ion penetrates matter, there is an increasing chance of fragmentation as penetration depth increases. When an ion fragments, secondary neutrons are released with velocities up to that of the primary ion, giving some neutrons very long penetration ranges. These secondary neutrons have a high relative biological effectiveness, are difficult to effectively shield, and can cause more biological damage than the primary ions in some scenarios. Ground-based irradiation experiments that simulate the space radiation environment must account for this spectrum of neutrons. Using the Particle and Heavy Ion Transport Code System (PHITS), it is possible to simulate a neutron environment that is characteristic of that found in spaceflight. Considering neutron dosimetry, the focus lies on the broad spectrum of recoil protons that are produced in biological targets. In a biological target, dose at a certain penetration depth is primarily dependent upon recoil proton tracks. The PHITS code can be used to simulate a broad-energy neutron spectrum traversing biological targets, and it account for the recoil particle population. This project focuses on modeling a neutron beamline irradiation scenario for determining dose at increasing depth in water targets. Energy-deposition events and particle fluence can be simulated by establishing cross-sectional scoring routines at different depths in a target. This type of model is useful for correlating theoretical data with actual beamline radiobiology experiments. Other work exposed human fibroblast cells to a high-energy neutron source to study micronuclei induction in cells at increasing depth behind water shielding. Those findings provide supporting data describing dose vs. depth across a water-equivalent medium. This poster presents PHITS data suggesting an increase in dose, up to roughly 10 cm depth, followed by a continual decrease as neutrons come to a stop in the target.

  3. Piezoelectric control of needle-free transdermal drug delivery.

    PubMed

    Stachowiak, Jeanne C; von Muhlen, Marcio G; Li, Thomas H; Jalilian, Laleh; Parekh, Sapun H; Fletcher, Daniel A

    2007-12-04

    Transdermal drug delivery occurs primarily through hypodermic needle injections, which cause pain, require a trained administrator, and may contribute to the spread of disease. With the growing number of pharmaceutical therapies requiring transdermal delivery, an effective, safe, and simple needle-free alternative is needed. We present and characterize a needle-free jet injector that employs a piezoelectric actuator to accelerate a micron-scale stream of fluid (40-130 microm diameter) to velocities sufficient for skin penetration and drug delivery (50-160 m/s). Existing jet injectors, powered by compressed springs and gases, are not widely used due to painful injections and poor reliability in skin penetration depth and dose. In contrast, our device offers electronic control of the actuator expansion rate, resulting in direct control of jet velocity and thus the potential for more precise injections. We apply a simple fluid-dynamic model to predict the device response to actuator expansion. Further, we demonstrate that injection parameters including expelled volume, jet pressure, and penetration depth in soft materials vary with actuator expansion rate, but are highly coupled. Finally, we discuss how electronically-controlled jet injectors may enable the decoupling of injection parameters such as penetration depth and dose, improving the reliability of needle-free transdermal drug delivery.

  4. London penetration depth measurements in Ba (Fe 1-xT x) 2As 2(T=Co,Ni,Ru,Rh,Pd,Pt,Co+Cu) superconductors

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Gordon, Ryan T.

    2011-01-01

    The London penetration depth has been measured in various doping levels of single crystals of Ba(Fe 1-xT x) 2As 2 (T=Co,Ni,Ru,Rh,Pd,Pt,Co+Cu) superconductors by utilizing a tunnel diode resonator (TDR) apparatus. All in-plane penetration depth measurements exhibit a power law temperature dependence of the form Δλ ab(T) = CT n, indicating the existence of low-temperature, normal state quasiparticles all the way down to the lowest measured temperature, which was typically 500 mK. Several different doping concentrations from the Ba(Fe 1-xT x) 2As 2 (T=Co,Ni) systems have been measured and the doping dependence of the power law exponent, n, is compared tomore » results from measurements of thermal conductivity and specific heat. In addition, a novel method has been developed to allow for the measurement of the zero temperature value of the in-plane penetration depth, λ ab(0), by using TDR frequency shifts. By using this technique, the doping dependence of λ ab(0) has been measured in the Ba(Fe 1-xCo x) 2As 2 series, which has allowed also for the construction of the doping-dependent superfluid phase stiffness, ρ s(T) = [λ(0)/λ(T)] 2. By studying the effects of disorder on these superconductors using heavy ion irradiation, it has been determined that the observed power law temperature dependence likely arises from pair-breaking impurity scattering contributions, which is consistent with the proposed s±-wave symmetry of the superconducting gap in the dirty scattering limit. This hypothesis is supported by the measurement of an exponential temperature dependence of the penetration depth in the intrinsically clean LiFeAs, indicative of a nodeless superconducting gap.« less

  5. Estimation of adhesive bond strength in laminated safety glass using guided mechanical waves

    NASA Astrophysics Data System (ADS)

    Huo, Shihong

    Laminated safety glass is used in the automobile industry and in architectural applications. Laminated safety glass consists of a plastic interlayer, such as a layer of poly vinyl butyral (PVB) or Butacite, surrounded by two adjacent glass plates. The glass can be float glass, plate glass, tempered glass, or sheet glass, and the plastic interlayer is made of a viscoelastic material with relatively high damping. The level of adhesive bond strength between the plastic interlayer and the two adjacent glass plates has a significant role in the penetration resistance against flying objects and is a critical parameter towards ensuring the proper performance of safety glass. Therefore, estimation and control of adhesive bond levels in laminated safety glass is a critical issue. There are several destructive testing procedures used to quantify the adhesion level in laminated safety glass. These tests include the tension test, the peel test, the impact test, and the pummel test. All these tests have drawbacks including the pummel test method, which has been the most widely used in industry for over 80 years. The primary drawbacks of the pummel test method are that it is destructive and subjective (i.e., involves individual human judgment), which precludes this method for use as an on-line test method for quality control. Consequently, a quantitative nondestructive testing method to evaluate adhesion levels would be an asset to the laminated safety glass industry. In this study, adhesion levels in laminated safety glass samples, i.e., windshields, have been assessed using the guided mechanical wave method. To study the adhesive bond strength analytically, the imperfect interfaces between the plastic interlayer and the two adjacent glass plates in laminated safety glass are modeled using a bed of longitudinal and shear springs, and their stiffness characteristics are estimated using fracture mechanics and atomic force microscopy (AFM) surface measurements. The atomic force microscopy measurements are used to estimate the contact area at the imperfect interfaces between the plastic interlayer and the two adjacent glass plates for each of the laminates. The spring layers are then embedded in the global matrix method, which is used to predict the guided wave dispersion behavior of the laminated system. Based upon the guided wave energy velocity predictions for each of the laminates with different levels of adhesion, the S0 mode was selected as the most promising for use in nondestructively estimating adhesion levels in laminated safety glass. The predicted energy velocities (obtained using this multilayered model) were validated using guided wave energy velocity experimental measurements. The experimentally obtained velocity measurements are in good agreement with the predicted values. Guided wave attenuation in laminated safety glass is primarily due to the viscoelastic material properties of the PVB plastic interlayer. The attenuation properties of S1 mode were also explored to estimate the adhesive bond strength between the plastic interlayer and the two adjacent glass plates. Results show that the combination of both the energy velocity and attenuation methods has promise towards replacing the pummel test method to estimate the adhesion level in laminated safety glass.

  6. Ballistics ordnance gelatine - How different concentrations, temperatures and curing times affect calibration results.

    PubMed

    Maiden, Nicholas R; Fisk, Wesley; Wachsberger, Christian; Byard, Roger W

    2015-08-01

    A study was undertaken to determine whether different concentrations of ordnance gelatine, water types, temperatures and curing times would have an effect on projectile penetration of a gelatine tissue surrogate. Both Federal Bureau of Investigation (FBI) and North Atlantic Treaty Organization (NATO) specified gelatines were compared against the FBI calibration standard. 10% w/w and 20% w/w concentrations of gelatine with Bloom numbers of 250 and 285 were prepared and cured at variable temperatures (3-20°C) for 21 hours-3 weeks. Each block was shot on four occasions on the same range using steel calibre 4.5 mm BBs fired from a Daisy(®) air rifle at the required standard velocity of 180 ± 4.5 m/s, to ascertain the mean penetration depth. The results showed no significant difference in mean penetration depth using the three different water types (p > 0.05). Temperature changes and curing times did affect penetration depth. At 10°C, mean penetration depth with 20% gelatine 285 Bloom for the two water types tested was 49.7 ± 1.5 mm after 21 h curing time, whereas the same formulation at 20°C using two different water types was 79.1 ± 2.1 mm after 100 h curing time (p < 0.001). Neither of the NATO 20% concentrations of gelatine at 10°C or a 20% concentration of 285 Bloom gelatine at 10°C met the same calibration standard as the FBI recommended 10% formulation at 4°C. A 20% concentration of 285 Bloom at 20°C met the same calibration/penetration criteria as a 10% concentration of 250 Bloom at 4 °C after 100 h of curing, therefore matching the FBI calibration standard for a soft tissue simulant for wound ballistics research. These results demonstrate significant variability in simulant properties. Failure to standardise ballistic simulants may invalidate experimental results. Copyright © 2015. Published by Elsevier Ltd.

  7. A Double-Blind Study on Acupuncture Sensations with Japanese Style of Acupuncture: Comparison between Penetrating and Placebo Needles.

    PubMed

    Nishiwaki, Masako; Takayama, Miho; Yajima, Hiroyoshi; Nasu, Morihiro; Park, Joel; Kong, Jian; Takakura, Nobuari

    2018-01-01

    To investigate the acupuncture sensations elicited by the Japanese style of acupuncture, penetrating acupuncture and skin-touch placebo needles were randomly administered at various insertion depths (5 and 10 mm for the penetrating needles and 1 and 2 mm for the placebo needles) at LI4 to 50 healthy subjects. Among the 12 acupuncture sensations in the Massachusetts General Hospital Acupuncture Sensation Scale (MASS), "heaviness" was the strongest and most frequently reported sensation with the 10 mm needles, but not with the 5 mm needles. There were no significant differences in number of sensations elicited, MASS index, range of spreading, and intensity of needle pain for 5 mm penetration versus 1 mm skin press and 10 mm penetration versus 2 mm skin press. The MASS index with 2 mm skin-touch needles was significantly larger than that with 1 mm skin-touch and 5 mm penetrating needles. The factor structures in the 12 acupuncture sensations between penetrating and skin-touch needles were different. The acupuncture sensations obtained in this study under satisfactorily performed double-blind (practitioner-patient) conditions suggest that a slight difference in insertion depth and skin press causes significant differences in quantity and quality of acupuncture sensations.

  8. Computed tomographic imaging of stapes implants.

    PubMed

    Warren, Frank M; Riggs, Sterling; Wiggins, Richard H

    2008-08-01

    Computed tomographic (CT) imaging of stapes prostheses is inaccurate. Clinical situations arise in which it would be helpful to determine the depth of penetration of a stapes prosthesis into the vestibule. The accuracy of CT imaging for this purpose has not been defined. This study was aimed to determine the accuracy of CT imaging to predict the depth of intrusion of stapes prostheses into the vestibule. The measurement of stapes prostheses by CT scan was compared with physical measurements in 8 cadaveric temporal bones. The depth of intrusion into the vestibule of the piston was underestimated in specimens with the fluoroplastic piston by a mean of 0.5 mm when compared with the measurements obtained in the temporal bones. The depth of penetration of the stainless steel implant was overestimated by 0.5 mm when compared with that in the temporal bone. The type of implant must be taken into consideration when estimating the depth of penetration into the vestibule using CT scanning because the imaging characteristics of the implanted materials differ. The position of fluoroplastic pistons cannot be accurately measured in the vestibule. Metallic implants are well visualized, and measurements exceeding 2.2 mm increase the suspicion of otolithic impingement. Special reconstructions along the length of the piston may be more accurate in estimating the position of stapes implants.

  9. Possible Gravitational Anomalies in Quantum Materials. Phase 2: Experiment Assembly, Qualification and Test Results

    DTIC Science & Technology

    2007-02-01

    causes the photon to aquire mass via the Higgs mechanism (Ryder, 2003). The London penetration depth that we observe is then just the wavelength of the...Cooper-pair density. Both the penetration depth as well as the graviton wavelength is a complex number, as required by the positive cosmological ...the cosmological constant measurement of i.10-69 kg (De Matos et al, 2005), but it is still a small number. In a recent assessment, Modanese (Modanese

  10. A Study of Crystalline Mechanism of Penetration Sealer Materials.

    PubMed

    Teng, Li-Wei; Huang, Ran; Chen, Jie; Cheng, An; Hsu, Hui-Mi

    2014-01-14

    It is quite common to dispense a topping material like crystalline penetration sealer materials (CPSM) onto the surface of a plastic substance such as concrete to extend its service life span by surface protections from outside breakthrough. The CPSM can penetrate into the existing pores or possible cracks in such a way that it may form crystals to block the potential paths which provide breakthrough for any unknown materials. This study investigated the crystalline mechanism formed in the part of concrete penetrated by the CPSM. We analyzed the chemical composites, in order to identify the mechanism of CPSM and to evaluate the penetrated depth. As shown in the results, SEM observes the acicular-structured crystals filling capillary pores for mortar substrate of the internal microstructure beneath the concrete surface; meanwhile, XRD and FT-IR showed the main hydration products of CPSM to be C-S-H gel and CaCO₃. Besides, MIP also shows CPSM with the ability to clog capillary pores of mortar substrate; thus, it reduces porosity, and appears to benefit in sealing pores or cracks. The depth of CPSM penetration capability indicated by TGA shows 0-10 mm of sealer layer beneath the concrete surface.

  11. There’s plenty of light at the bottom: statistics of photon penetration depth in random media

    PubMed Central

    Martelli, Fabrizio; Binzoni, Tiziano; Pifferi, Antonio; Spinelli, Lorenzo; Farina, Andrea; Torricelli, Alessandro

    2016-01-01

    We propose a comprehensive statistical approach describing the penetration depth of light in random media. The presented theory exploits the concept of probability density function f(z|ρ, t) for the maximum depth reached by the photons that are eventually re-emitted from the surface of the medium at distance ρ and time t. Analytical formulas for f, for the mean maximum depth 〈zmax〉 and for the mean average depth reached by the detected photons at the surface of a diffusive slab are derived within the framework of the diffusion approximation to the radiative transfer equation, both in the time domain and the continuous wave domain. Validation of the theory by means of comparisons with Monte Carlo simulations is also presented. The results are of interest for many research fields such as biomedical optics, advanced microscopy and disordered photonics. PMID:27256988

  12. Inspecting cracks in foam insulation

    NASA Technical Reports Server (NTRS)

    Cambell, L. W.; Jung, G. K.

    1979-01-01

    Dye solution indicates extent of cracking by penetrating crack and showing original crack depth clearly. Solution comprised of methylene blue in denatured ethyl alcohol penetrates cracks completely and evaporates quickly and is suitable technique for usage in environmental or structural tests.

  13. Detection of underground voids in Ohio by use of geophysical methods

    USGS Publications Warehouse

    Munk, Jens; Sheets, R.A.

    1997-01-01

    Geophysical methods are generally classified as electrical, potential field, and seismic methods. Each method type relies on contrasts of physical properties in the subsurface. Forward models based on the physical properties of air- and water-filled voids within common geologic materials indicate that several geophysical methods are technically feasible for detection of subsurface voids in Ohio, but ease of use and interpretation varies widely between the methods. Ground-penetrating radar is the most rapid and cost-effective method for collection of subsurface data in areas associated with voids under roadways. Electrical resistivity, gravity, or seismic reflection methods have applications for direct delineation of voids, but data-collection and analytical procedures are more time consuming. Electrical resistivity, electromagnetic, or magnetic methods may be useful in locating areas where conductive material, such as rail lines, are present in abandoned underground coal mines. Other electrical methods include spontaneous potential and very low frequency (VLF); these latter two methods are considered unlikely candidates for locating underground voids in Ohio. Results of ground-penetrating radar surveys at three highway sites indicate that subsurface penetration varies widely with geologic material type and amount of cultural interference. Two highway sites were chosen over abandoned underground coal mines in eastern Ohio. A third site in western Ohio was chosen in an area known to be underlain by naturally occurring voids in lime stone. Ground-penetrating radar surveys at Interstate 470, in Belmont County, Ohio, indicate subsurface penetration of less than 15 feet over a mined coal seam that was known to vary in depth from 0 to 40 feet. Although no direct observations of voids were made, anomalous areas that may be related to collapse structures above voids were indicated. Cultural interference dominated the radar records at Interstate 70, Guernsey County, Ohio, where coal was mined under the site at a depth of about 50 feet. Interference from overhead powerlines, the field vehicle, and guardrails complicated an interpretation of the radar records where the depth of penetration was estimated to be less than 5 feet. Along State Route 33, in Logan County, Ohio, bedding planes and structures possibly associated with dissolution of limestone were profiled with ground-penetrating radar. Depth of penetration was estimated to be greater than 50 feet.

  14. Al/Cu Dissimilar Friction Stir Welding with Ni, Ti, and Zn Foil as the Interlayer for Flow Control, Enhancing Mechanical and Metallurgical Properties

    NASA Astrophysics Data System (ADS)

    Sahu, Prakash Kumar; Pal, Sukhomay; Pal, Surjya K.

    2017-07-01

    This research investigates the effects of Ni, Ti, and Zn foil as interlayer, inserted between the faying edges of Al and Cu plates, for controlled intermetallic compound (IMC) formation. The weld tensile strength with Ti and Zn as interlayer is superior to Al base metal strength. This is due to controlled flow of IMCs by diffused Ti interlayer and thin, continuous, and uniform IMC formation in the case of Zn interlayer. Improved flexural stress was observed with interlayer. Weld microhardness varied with different interlayers and purely depends on IMCs present at the indentation point, flow of IMCs, and interlayer hardness. Specimens with interlayer failed at the interface of the nugget and thermomechanical-affected zone (TMAZ) with complete and broken three-dimensional (3-D) grains, indicating transgranular fracture. Phase analysis revealed that Al/Cu IMCs are impeded by Ni and Ti interlayer. The minor binary and ternary IMC phases form adjacent to the interlayer due to diffusion of the material with Al/Cu. Line scan and elemental mapping indicate thin, continuous, and uniform IMCs with enhanced weld metallurgical and mechanical properties for the joints with Zn interlayer. Macrostructural analysis revealed IMC flow variations with and without interlayer. Variation in grain size at different zones is also observed for different interlayers.

  15. Investigating skin penetration depth and shape following needle-free injection at different pressures: A cadaveric study.

    PubMed

    Seok, Joon; Oh, Chang Taek; Kwon, Hyun Jung; Kwon, Tae Rin; Choi, Eun Ja; Choi, Sun Young; Mun, Seog Kyun; Han, Seung-Ho; Kim, Beom Joon; Kim, Myeung Nam

    2016-08-01

    The effectiveness of needle-free injection devices in neocollagenesis for treating extended skin planes is an area of active research. It is anticipated that needle-free injection systems will not only be used to inject vaccines or insulin, but will also greatly aid skin rejuvenation when used to inject aesthetic materials such as hyaluronic acid, botulinum toxin, and placental extracts. There has not been any specific research to date examining how materials penetrate the skin when a needle-free injection device is used. In this study, we investigated how material infiltrates the skin when it is injected into a cadaver using a needle-free device. Using a needle-free injector (INNOJECTOR™; Amore Pacific, Seoul, Korea), 0.2 ml of 5% methylene blue (MB) or latex was injected into cheeks of human cadavers. The device has a nozzle diameter of 100 µm and produces a jet with velocity of 180 m/s. This jet penetrates the skin and delivers medicine intradermally via liquid propelled by compressed gasses. Materials were injected at pressures of 6 or 8.5 bars, and the injection areas were excised after the procedure. The excised areas were observed visually and with a phototrichogram to investigate the size, infiltration depth, and shape of the hole created on the skin. A small part of the area that was excised was magnified and stained with H&E (×40) for histological examination. We characterized the shape, size, and depth of skin infiltration following injection of 5% MB or latex into cadaver cheeks using a needle-free injection device at various pressure settings. Under visual inspection, the injection at 6 bars created semi-circle-shaped hole that penetrated half the depth of the excised tissue, while injection at 8.5 bars created a cylinder-shaped hole that spanned the entire depth of the excised tissue. More specific measurements were collected using phototrichogram imaging. The shape of the injection entry point was consistently spherical regardless of the amount of pressure used. When injecting 5% MB at 6 bars, the depth of infiltration reached 2.323 mm, while that at 8.5 bars reached 8.906 mm. The area of the hole created by the 5% MB injection was 0.797 mm(2) at 6 bars and 0.242 mm(2) at 8.5 bars. Latex injections reached a depth of 3.480 mm at 6 bars and 7.558 mm at 8.5 bars, and the areas were measured at 1.043 mm(2) (6 bars) and 0.355 mm(2) (8.5 bars). Histological examination showed that the injection penetrated as deep as the superficial musculoaponeurotic system at 6 bars and the masseter muscle at 8.5 bars. When injecting material into the skin using a pneumatic needle-free injector, higher-pressure injections result in a hole with smaller area than lower-pressure injections. The depth and shape of skin penetration vary according to the amount of pressure applied. For materials of low density and viscosity, there is a greater difference in penetration depth according to the degree of pressure. Lasers Surg. Med. 48:624-628, 2016. © 2016 Wiley Periodicals, Inc. © 2016 Wiley Periodicals, Inc.

  16. Influence of Wind Pressure on the Carbonation of Concrete

    PubMed Central

    Zou, Dujian; Liu, Tiejun; Du, Chengcheng; Teng, Jun

    2015-01-01

    Carbonation is one of the major deteriorations that accelerate steel corrosion in reinforced concrete structures. Many mathematical/numerical models of the carbonation process, primarily diffusion-reaction models, have been established to predict the carbonation depth. However, the mass transfer of carbon dioxide in porous concrete includes molecular diffusion and convection mass transfer. In particular, the convection mass transfer induced by pressure difference is called penetration mass transfer. This paper presents the influence of penetration mass transfer on the carbonation. A penetration-reaction carbonation model was constructed and validated by accelerated test results under high pressure. Then the characteristics of wind pressure on the carbonation were investigated through finite element analysis considering steady and fluctuating wind flows. The results indicate that the wind pressure on the surface of concrete buildings results in deeper carbonation depth than that just considering the diffusion of carbon dioxide. In addition, the influence of wind pressure on carbonation tends to increase significantly with carbonation depth. PMID:28793462

  17. Process parameter effects on material removal in magnetorheological finishing of borosilicate glass.

    PubMed

    Miao, Chunlin; Lambropoulos, John C; Jacobs, Stephen D

    2010-04-01

    We investigate the effects of processing parameters on material removal for borosilicate glass. Data are collected on a magnetorheological finishing (MRF) spot taking machine (STM) with a standard aqueous magnetorheological (MR) fluid. Normal and shear forces are measured simultaneously, in situ, with a dynamic dual load cell. Shear stress is found to be independent of nanodiamond concentration, penetration depth, magnetic field strength, and the relative velocity between the part and the rotating MR fluid ribbon. Shear stress, determined primarily by the material mechanical properties, dominates removal in MRF. The addition of nanodiamond abrasives greatly enhances the material removal efficiency, with the removal rate saturating at a high abrasive concentration. The volumetric removal rate (VRR) increases with penetration depth but is insensitive to magnetic field strength. The VRR is strongly correlated with the relative velocity between the ribbon and the part, as expected by the Preston equation. A modified removal rate model for MRF offers a better estimation of MRF removal capability by including nanodiamond concentration and penetration depth.

  18. Detection and delineation of underground septic tanks in sandy terrain using ground penetrating radar

    NASA Astrophysics Data System (ADS)

    Omolaiye, Gabriel Efomeh; Ayolabi, Elijah A.

    2010-09-01

    A ground penetrating radar (GPR) survey was conducted on the Lekki Peninsula, Lagos State, Nigeria. The primary target of the survey was the delineation of underground septic tanks (ST). A total of four GPR profiles were acquired on the survey site using Ramac X3M GPR equipment with a 250MHz antenna, chosen based on the depth of interest and resolution. An interpretable depth of penetration of 4.5m below the surface was achieved after processing. The method accurately delineated five underground ST. The tops of the ST were easily identified on the radargram based on the strong-amplitude anomalies, the length and the depths to the base of the ST were estimated with 99 and 73 percent confidence respectively. The continuous vertical profiles provide uninterrupted subsurface data along the lines of traverse, while the non-intrusive nature makes it an ideal tool for the accurate mapping and delineation of underground utilities.

  19. Variation of energy absorption and exposure buildup factors with incident photon energy and penetration depth for boro-tellurite (B2O3-TeO2) glasses

    NASA Astrophysics Data System (ADS)

    Sayyed, M. I.; Elhouichet, H.

    2017-01-01

    The gamma ray energy absorption (EABF) and exposure buildup factors (EBF) of (100-x)TeO2-xB2O3 glass systems (where x=5, 10, 15, 20, 22.5 and 25 mol%) have been calculated in the energy region 0.015-15 MeV up to a penetration depth of 40 mfp (mean free path). The five parameters (G-P) fitting method has been used to estimate both EABF and EBF values. Variations of EABF and EBF with incident photon energy and penetration depth have been studied. It was found that EABF and EBF values were higher in the intermediate energy region, for all the glass systems. Furthermore, boro-tellurite glass with 5 mol% B2O3, was found to present the lowest EABF and EBF values, hence it is superior gamma-ray shielding material. The results indicate that the boro-tellurite glasses can be used as radiation shielding materials.

  20. Influence of Wind Pressure on the Carbonation of Concrete.

    PubMed

    Zou, Dujian; Liu, Tiejun; Du, Chengcheng; Teng, Jun

    2015-07-24

    Carbonation is one of the major deteriorations that accelerate steel corrosion in reinforced concrete structures. Many mathematical/numerical models of the carbonation process, primarily diffusion-reaction models, have been established to predict the carbonation depth. However, the mass transfer of carbon dioxide in porous concrete includes molecular diffusion and convection mass transfer. In particular, the convection mass transfer induced by pressure difference is called penetration mass transfer. This paper presents the influence of penetration mass transfer on the carbonation. A penetration-reaction carbonation model was constructed and validated by accelerated test results under high pressure. Then the characteristics of wind pressure on the carbonation were investigated through finite element analysis considering steady and fluctuating wind flows. The results indicate that the wind pressure on the surface of concrete buildings results in deeper carbonation depth than that just considering the diffusion of carbon dioxide. In addition, the influence of wind pressure on carbonation tends to increase significantly with carbonation depth.

  1. Influence of various thickness metallic interlayers on opto-electric and mechanical properties of AZO thin films on PET substrates

    NASA Astrophysics Data System (ADS)

    Chang, R. C.; Li, T. C.; Lin, C. W.

    2012-02-01

    Various thickness metallic interlayers to improve the opto-electric and mechanical properties of aluminum-doped zinc oxide (AZO) thin films deposited on flexible polyethylene terephtalate (PET) substrates are studied. The effects of the interlayers on the resistance and transmittance of the AZO thin films are discussed. The result shows that the metallic interlayers effectively improve the electric resistance but reduce the optical transmittance of the AZO thin films. These phenomena become more obvious as the interlayer thickness increases. However, the AZO with an aluminum interlayer still behaves an acceptable transmittance. Moreover, mechanical tests indicate that the aluminum interlayer increases the hardness and modulus, and reduce the residual stress of the AZO thin films. In contrast, the silver and copper interlayers decrease the AZO's mechanical properties. Comparing to those without any interlayer, the results show that the best interlayer is the 6 nm thick aluminum film.

  2. A miniaturized test method for the mechanical characterization of structural materials for fusion reactors

    NASA Astrophysics Data System (ADS)

    Gondi, P.; Donato, A.; Montanari, R.; Sili, A.

    1996-10-01

    This work deals with a non-destructive method for mechanical tests which is based on the indentation of materials at a constant rate by means of a cylinder with a small radius and penetrating flat surface. The load versus penetration depth curves obtained using this method have shown correspondences with those of tensile tests and have given indications about the mechanical properties on a reduced scale. In this work penetration tests have been carried out on various kinds of Cr martensitic steels (MANET-2, BATMAN and modified F82H) which are of interest for first wall and structural applications in future fusion reactors. The load versus penetration depth curves have been examined with reference to data obtained in tensile tests and to microhardness measurements. Penetration tests have been performed at various temperature (from -180 to 100°C). Conclusions, which can be drawn for the ductile to brittle transition, are discussed for MANET-2 steel. Preliminary results obtained on BATMAN and modified F82H steels are reported. The characteristics of the indenter imprints have been studied by scanning electron microscopy.

  3. The relationship between mechanical properties and ballistic penetration depth in a viscoelastic gel.

    PubMed

    Mrozek, Randy A; Leighliter, Brad; Gold, Christopher S; Beringer, Ian R; Yu, Jian H; VanLandingham, Mark R; Moy, Paul; Foster, Mark H; Lenhart, Joseph L

    2015-04-01

    The fundamental material response of a viscoelastic material when impacted by a ballistic projectile has important implication for the defense, law enforcement, and medical communities particularly for the evaluation of protective systems. In this paper, we systematically vary the modulus and toughness of a synthetic polymer gel to determine their respective influence on the velocity-dependent penetration of a spherical projectile. The polymer gels were characterized using tensile, compression, and rheological testing taking special care to address the unique challenges associated with obtaining high fidelity mechanical data on highly conformal materials. The depth of penetration data was accurately described using the elastic Froude number for viscoelastic gels ranging in Young's modulus from ~60 to 630 kPa. The minimum velocity of penetration was determined to scale with the gel toughness divided by the gel modulus, a qualitative estimate for the zone of deformation size scale upon impact. We anticipate that this work will provide insight into the critical material factors that control ballistic penetration behavior in soft materials and aid in the design and development of new ballistic testing media. Published by Elsevier Ltd.

  4. Estimating maximum depth distribution of seagrass using underwater videography

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Norris, J.G.; Wyllie-Echeverria, S.

    1997-06-01

    The maximum depth distribution of eelgrass (Zostera marina) beds in Willapa Bay, Washington appears to be limited by light penetration which is likely related to water turbidity. Using underwater videographic techniques we estimated that the maximum depth penetration in the less turbid outer bay was -5.85 ft (MILW) and in the more turbid inner bay was only -1.59 ft (MLLW). Eelgrass beds had well defined deepwater edges and no eelgrass was observed in the deep channels of the bay. The results from this study suggest that aerial photographs taken during low tide periods are capable of recording the majority ofmore » eelgrass beds in Willapa Bay.« less

  5. Sub-40 fs, 1060-nm Yb-fiber laser enhances penetration depth in nonlinear optical microscopy of human skin

    NASA Astrophysics Data System (ADS)

    Balu, Mihaela; Saytashev, Ilyas; Hou, Jue; Dantus, Marcos; Tromberg, Bruce J.

    2015-12-01

    Advancing the practical utility of nonlinear optical microscopy requires continued improvement in imaging depth and contrast. We evaluated second-harmonic generation (SHG) and third-harmonic generation images from ex vivo human skin and showed that a sub-40 fs, 1060-nm Yb-fiber laser can enhance SHG penetration depth by up to 80% compared to a >100 fs, 800 nm Ti:sapphire source. These results demonstrate the potential of fiber-based laser systems to address a key performance limitation related to nonlinear optical microscopy (NLOM) technology while providing a low-barrier-to-access alternative to Ti:sapphire sources that could help accelerate the movement of NLOM into clinical practice.

  6. Determination of the neutralization depth of concrete under the aggressive environment influence

    NASA Astrophysics Data System (ADS)

    Morzhukhina, Anastasia; Nikitin, Stanislav; Akimova, Elena

    2018-03-01

    Aggressive environments have a significant impact on destruction of many reinforced concrete structures, such as high-rise constructions or chemical plants. For example, some high-rise constructions are equipped with a swimming pool, so they are exposed to chloride ions in the air. Penetration of aggressive chemical substances into the body of concrete contributes to acceleration of reinforced concrete structure corrosion that in turn leads to load bearing capacity loss and destruction of the building. The article considers and analyzes the main technologies for calculating penetration depth of various aggressive substances into the body of concrete. The calculation of corrosion depth was made for 50-year service life.

  7. Electrical Resistivity and Ground Penetrating Radar Investigation of Presence and Extent of Hardpan Soil Layers

    NASA Astrophysics Data System (ADS)

    Thao, S. J.; Plattner, A.

    2015-12-01

    Farming in the San Joaquin Valley in central California is often impeded by a shallow rock-hard layer of consolidated soil commonly referred to as hardpan. To be able to successfully farm, this layer, if too shallow, needs to be removed either with explosives or heavy equipment. It is therefore of great value to obtain information about depth and presence of such a layer prior to agricultural operations. We tested the applicability of electrical resistivity tomography and ground penetrating radar in hardpan detection. On our test site of known hardpan depth (from trenching) and local absence (prior dynamiting to plant trees), we successfully recovered the known edge of a hardpan layer with both methods, ERT and GPR. The clay-rich soil significantly reduced the GPR penetration depth but we still managed to map the edges at a known gap where prior dynamiting had removed the hardpan. Electrical resistivity tomography with a dipole-dipole electrode configuration showed a clear conductive layer at expected depths with a clearly visible gap at the correct location. In our data analysis and representation we only used either freely available or in-house written software.

  8. Gold nanocage decorated pH-sensitive micelle for highly effective photothermo-chemotherapy and photoacoustic imaging.

    PubMed

    Zhou, Guoyong; Xiao, Hong; Li, Xiaoxia; Huang, Yi; Song, Wei; Song, Liang; Chen, Meiwan; Cheng, Du; Shuai, Xintao

    2017-12-01

    A pH-sensitive copolymer PAsp(DIP)-b-PAsp(MEA) (PDPM) was synthesized and self-assembled to micelle loading chemotherapeutic drug doxorubicin (DOX) and introducing a gold nanocage structure for photothermo-chemotherapy and photoacoustic imaging. After further surface modification with polyethylene glycol (PEG), the DOX-loaded pH-sensitive gold nanocage (D-PGNC) around 100 nm possessed a uniform spherical structure with a pH-sensitive core of PAsp(DIP) incorporating DOX, an interlayer crosslinked via disulfide bonds and decorated with discontinuous gold shell, and a PEG corona. The release of DOX from D-PGNC was turned off in bloodstream due to the cross-linking and gold decoration of interlayer but turned on inside tumor tissue by multiple stimulations including the low pH value of tumor tissue (≈6.8), the low lysosomal pH value of cancer cells (≈5.0) and near-infrared (NIR) irradiation. The gold nanocage receiving NIR irradiation could generate hyperthermia to ablate tumor cells. Moreover, the photoacoustic (PA) imaging and analysis of DOX fluorescence inside tumor tissue demonstrated that photothermal therapy based on the gold nanocage effectively drove DOX penetration inside tumor. Owing to the rapid intratumor release and deep tissue penetration of drug favorable for killing cancer cells survived the photothermal therapy, the combined therapy based on D-PGNC via NIR irradiation exhibited a synergistic treatment effect superior to either chemotherapy or NIR-induced photothermal therapy alone. The novelty of the manuscript is its multifunctional system which incorporates anticancer drug DOX in its pH-sensitive core and acts as a template to introduce a gold nanocage. This nanomedicine presents potentials of sequestrating drug molecules in blood circulation but releasing them inside tumor upon responding to the acidic microenvironment therein. Exposure to NIR laser further expedited the pH-sensitive DOX release and promoted DOX penetration into cancer tissues far away from the vasculature. Consequently, the combined photothermo-chemotherapy showed synergistic effects to inhibit tumor growth and prolong animal survival in nude mice bearing human SKOV-3 ovarian tumor. Moreover, owing to the decoration with gold nanocage, the tumor accumulation and intratumor diffusion of the micelles were easily trackable using photoacoustic imaging. Copyright © 2017 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

  9. Extreme value statistics for two-dimensional convective penetration in a pre-main sequence star

    NASA Astrophysics Data System (ADS)

    Pratt, J.; Baraffe, I.; Goffrey, T.; Constantino, T.; Viallet, M.; Popov, M. V.; Walder, R.; Folini, D.

    2017-08-01

    Context. In the interior of stars, a convectively unstable zone typically borders a zone that is stable to convection. Convective motions can penetrate the boundary between these zones, creating a layer characterized by intermittent convective mixing, and gradual erosion of the density and temperature stratification. Aims: We examine a penetration layer formed between a central radiative zone and a large convection zone in the deep interior of a young low-mass star. Using the Multidimensional Stellar Implicit Code (MUSIC) to simulate two-dimensional compressible stellar convection in a spherical geometry over long times, we produce statistics that characterize the extent and impact of convective penetration in this layer. Methods: We apply extreme value theory to the maximal extent of convective penetration at any time. We compare statistical results from simulations which treat non-local convection, throughout a large portion of the stellar radius, with simulations designed to treat local convection in a small region surrounding the penetration layer. For each of these situations, we compare simulations of different resolution, which have different velocity magnitudes. We also compare statistical results between simulations that radiate energy at a constant rate to those that allow energy to radiate from the stellar surface according to the local surface temperature. Results: Based on the frequency and depth of penetrating convective structures, we observe two distinct layers that form between the convection zone and the stable radiative zone. We show that the probability density function of the maximal depth of convective penetration at any time corresponds closely in space with the radial position where internal waves are excited. We find that the maximal penetration depth can be modeled by a Weibull distribution with a small shape parameter. Using these results, and building on established scalings for diffusion enhanced by large-scale convective motions, we propose a new form for the diffusion coefficient that may be used for one-dimensional stellar evolution calculations in the large Péclet number regime. These results should contribute to the 321D link.

  10. Detour factors in water and plastic phantoms and their use for range and depth scaling in electron-beam dosimetry.

    PubMed

    Fernández-Varea, J M; Andreo, P; Tabata, T

    1996-07-01

    Average penetration depths and detour factors of 1-50 MeV electrons in water and plastic materials have been computed by means of analytical calculation, within the continuous-slowing-down approximation and including multiple scattering, and using the Monte Carlo codes ITS and PENELOPE. Results are compared to detour factors from alternative definitions previously proposed in the literature. Different procedures used in low-energy electron-beam dosimetry to convert ranges and depths measured in plastic phantoms into water-equivalent ranges and depths are analysed. A new simple and accurate scaling method, based on Monte Carlo-derived ratios of average electron penetration depths and thus incorporating the effect of multiple scattering, is presented. Data are given for most plastics used in electron-beam dosimetry together with a fit which extends the method to any other low-Z plastic material. A study of scaled depth-dose curves and mean energies as a function of depth for some plastics of common usage shows that the method improves the consistency and results of other scaling procedures in dosimetry with electron beams at therapeutic energies.

  11. Interaction of trace elements and welding parameters on GTA weld shape. [Variation with penetration and tip angle

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Burgardt, P.; Heiple, C.R.

    1985-01-01

    Good penetration and poor penetration steels have different responses to changes in temperature distribution on the weld pool surface. Penetration of 304 SS was varied using S and Se dopants. The weld parameter investigated was the electrode tip angle. Results of bead-on-plate GTA welds show that there is a difference in response of weld pool shape to tip angle depending on penetration: Low penetration base metal showed no dependence, intermediate penetration steel showed a small linear decrease of weld depth-to-width ratio (d/w) with tip angle, while high penetration steel showed an increase of d/w up to a maximum at aboutmore » 50/sup 0/, followed by a decrease in d/w. (DLC)« less

  12. Global Distribution of Net Electron Acceptance in Subseafloor Sediment

    NASA Astrophysics Data System (ADS)

    Fulfer, V. M.; Pockalny, R. A.; D'Hondt, S.

    2017-12-01

    We quantified the global distribution of net electron acceptance rates (e-/m2/year) in subseafloor sediment (>1.5 meters below seafloor [mbsf]) using (i) a modified version of the chemical-reaction-rate algorithm by Wang et al. (2008), (ii) physical properties and dissolved oxygen and sulfate data from interstitial waters of sediment cores collected by the Ocean Drilling Program, Integrated Ocean Drilling Program, International Ocean Discovery Program, and U.S. coring expeditions, and (iii) correlation of net electron acceptance rates to global oceanographic properties. Calculated net rates vary from 4.8 x 1019 e-/m2/year for slowly accumulating abyssal clay to 1.2 x 1023 e-/m2/year for regions of high sedimentation rate. Net electron acceptance rate correlates strongly with mean sedimentation rate. Where sedimentation rate is very low (e.g., 1 m/Myr), dissolved oxygen penetrates more than 70 mbsf and is the primary terminal electron acceptor. Where sedimentation rate is moderate (e.g., 3 to 60 m/Myr), dissolved sulfate penetrates as far as 700 mbsf and is the principal terminal electron acceptor. Where sedimentation rate is high (e.g., > 60 m/Myr), dissolved sulfate penetrates only meters, but is the principal terminal electron acceptor in subseafloor sediment to the depth of sulfate penetration. Because microbial metabolism continues at greater depths than the depth of sulfate penetration in fast-accumulating sediment, complete quantification of subseafloor metabolic rates will require consideration of other chemical species.

  13. Transcranial light-tissue interaction analysis

    NASA Astrophysics Data System (ADS)

    Aulakh, Kavleen; Zakaib, Scott; Willmore, William G.; Ye, Winnie N.

    2016-03-01

    The penetration depth of light plays a crucial role in therapeutic medical applications. In order to design effective medical photonic devices, an in-depth understanding of light's ability to penetrate tissues (including bone, skin, and fat) is necessary. The amount of light energy absorbed or scattered by tissues affects the intensity of light reaching an intended target in vivo. In this study, we examine the transmittance of light through a variety of cranial tissues for the purpose of determining the efficacy of neuro stimulation using a transcranial laser. Tissue samples collected from a pig were irradiated with a pulsed laser. We first determine the optimal irradiation wavelength of the laser to be 808nm. With varying peak and average power of the laser, we found an inverse and logarithmic relationship between the penetration depth and the intensity of the light. After penetrating the skin and skull of the pig, the light decreases in intensity at a rate of approximately 90.8 (+/-0.4) percent for every 5 mm of brain tissue penetrated. We also found the correlation between the irradiation time and dosage, using three different lasers (with peak power of 500, 1000, and 1500mW respectively). These data will help deduce what laser power is required to achieve a clinically-realistic model for a given irradiation time. This work is fundamental and the experimental data can be used to supplement existing and future research on the effects of laser light on brain tissue for the design of medical devices.

  14. Pre-heating mitigates composite degradation

    PubMed Central

    da SILVA, Jessika Calixto; Rogério Vieira, REGES; REGE, Inara Carneiro Costa; CRUZ, Carlos Alberto dos Santos; VAZ, Luís Geraldo; ESTRELA, Carlos; de CASTRO, Fabrício Luscino Alves

    2015-01-01

    ABSTRACT Dental composites cured at high temperatures show improved properties and higher degrees of conversion; however, there is no information available about the effect of pre-heating on material degradation. Objectives This study evaluated the effect of pre-heating on the degradation of composites, based on the analysis of radiopacity and silver penetration using scanning electron microscopy/energy-dispersive X-ray spectroscopy (SEM/EDS). Material and Methods Thirty specimens were fabricated using a metallic matrix (2x8 mm) and the composites Durafill VS (Heraeus Kulzer), Z-250 (3M/ESPE), and Z-350 (3M/ESPE), cured at 25°C (no pre-heating) or 60°C (pre-heating). Specimens were stored sequentially in the following solutions: 1) water for 7 days (60°C), plus 0.1 N sodium hydroxide (NaOH) for 14 days (60°C); 2) 50% silver nitrate (AgNO3) for 10 days (60°C). Specimens were radiographed at baseline and after each storage time, and the images were evaluated in gray scale. After the storage protocol, samples were analyzed using SEM/EDS to check the depth of silver penetration. Radiopacity and silver penetration data were analyzed using ANOVA and Tukey’s tests (α=5%). Results Radiopacity levels were as follows: Durafill VSZ-350>Z-250 (p<0.05). After storage in water/NaOH, pre-heated specimens presented higher radiopacity values than non-pre-heated specimens (p<0.05). There was a lower penetration of silver in pre-heated specimens (p<0.05). Conclusions Pre-heating at 60°C mitigated the degradation of composites based on analysis of radiopacity and silver penetration depth. PMID:26814459

  15. Interpretation of Stratified Fill, Frost Depths, Water Tables, and Massive Ice within Multi-Frequency Ground-Penetrating Radar Profiles Recorded Beneath Highways in Interior Alaska

    NASA Astrophysics Data System (ADS)

    Arcone, S. A.

    2014-12-01

    Road Radar generally refers to ground-penetrating radar (GPR) surveys intended to investigate pavement construction using pulses centered above 1 GHz. In interior Alaska thick sand and gravel grading and its frozen state by late winter generally afford up to 10 m of signal penetration at lower frequencies. Consequently, this penetration potentially allows identification of pavement issues involving frost heave and thaw settlement, while the smooth surface allows assessment of GPR performance in permafrost areas under ideal survey conditions. Here I discuss profiles using pulse center frequencies from 50 to 360 MHz, recorded over sections of the Steese and Elliott Highways within and just north of Fairbanks, respectively, and of the Tok Highway near Glennallen. Construction fill is easily recognized by its stratification; where marginally present along the Elliott it is replaced by steeply dipping horizons from the underlying schist. The frost depth and water table horizons are recognized by phase attributes of the reflected pulse, as dictated by the contrasts present in dielectric permittivity, their relative depths, and their continuity. Undulating stratification in the sand and gravel fill indicates thaw settlement, as caused by the melting of buried massive ice. The Tok section reveals the top and likely the bottom of massive ice. Generally, signal penetration is greatly reduced beneath the water table and so the highest resolution, at 360 MHz, covers all horizons. There is rare evidence of a permafrost table because it is most likely masked or nearly coincident with the water table. Permafrost penetration in frozen silts is a long-standing problem for GPR, for which I discuss a possible cause related to Maxwell-Wagner dielectric relaxation losses associated with unfrozen water.

  16. Coronal leakage in endodontically treated teeth restored with posts and complete crowns using different luting agent combinations.

    PubMed

    Nissan, Joseph; Rosner, Ofir; Gross, Ora; Pilo, Raphael; Lin, Shaul

    2011-04-01

    To evaluate the influence of different cement combinations on coronal microleakage in restored endodontically treated teeth using dye penetration. Human, noncarious single-rooted extracted premolars (n = 60) were divided into four experimental groups (each n = 15). After endodontic treatment, different combinations of cements were used to lute prefabricated posts and complete crown restorations: zinc phosphate cement applied on posts and cast crowns (Z) or on zinc phosphate cement posts and resin cement applied on cast crowns (ZR); resin cement applied on posts and zinc phosphate cement applied on cast crowns (RZ); and resin cement applied on posts and cast crowns (R). After artificial aging through thermal cycling (5°C to 55°C) for 2,000 cycles at 38 seconds for each cycle and 15 seconds of dwell time, specimens were immersed for 72 hours in basic fuchsin at 37°C. A buccolingual section was made through the vertical axis of specimens. A Toolmaker's microscope (Mitutoyo) was used to measure (um) dye penetration. The Kruskal-Wallis nonparametric test was used to determine intergroup difference. A nonparametric Mann-Whitney test compared each group regarding its maximal linear penetration depths on the mesial and distal aspects of each specimen (a = 0.05). Dye staining was evident to some degree in all specimens. Among groups Z, ZR, and RZ, no significant difference was shown in dye-penetration depths (mean penetration scores 1,518 to 1,807 um). However, dyepenetration depth was significantly lower in group R compared to the other groups (mean penetration score 1,073 um) (P < .05). Under study conditions, the cement combination offering the best coronal sealing was the one using only resin cement for both posts and crown restorations.

  17. The physical foundation of FN = kh(3/2) for conical/pyramidal indentation loading curves.

    PubMed

    Kaupp, G

    2016-01-01

    A physical deduction of the FN = kh(3/2) relation (where FN is normal force, k penetration resistance, and h penetration depth) for conical/pyramidal indentation loading curves has been achieved on the basis of elementary mathematics. The indentation process couples the productions of volume and pressure to the displaced material that often partly plasticizes due to such pressure. As the pressure/plasticizing depends on the indenter volume, it follows that FN = FNp(1/3) · FNV(2/3), where the index p stands for pressure/plasticizing and V for indentation volume. FNp does not contribute to the penetration, only FNV. The exponent 2/3 on FNV shows that while FN is experimentally applied; only FN(2/3) is responsible for the penetration depth h. Thus, FN = kh(3/2) is deduced and the physical reason is the loss of FN(1/3) for the depth. Unfortunately, this has not been considered in teaching, textbooks, and the previous deduction of numerous common mechanical parameters, when the Love/Sneddon deductions of an exponent 2 on h were accepted and applied. The various unexpected experimental verifications and applications of the correct exponent 3/2 are mentioned and cited. Undue mechanical parameters require correction not only for safety reasons. © Wiley Periodicals, Inc.

  18. Modulated Excitation Imaging System for Intravascular Ultrasound.

    PubMed

    Qiu, Weibao; Wang, Xingying; Chen, Yan; Fu, Qiang; Su, Min; Zhang, Lining; Xia, Jingjing; Dai, Jiyan; Zhang, Yaonan; Zheng, Hairong

    2017-08-01

    Advances in methodologies and tools often lead to new insights into cardiovascular diseases. Intravascular ultrasound (IVUS) is a well-established diagnostic method that provides high-resolution images of the vessel wall and atherosclerotic plaques. High-frequency (>50 MHz) ultrasound enables the spatial resolution of IVUS to approach that of optical imaging methods. However, the penetration depth decreases when using higher imaging frequencies due to the greater acoustic attenuation. An imaging method that improves the penetration depth of high-resolution IVUS would, therefore, be of major clinical importance. Modulated excitation imaging is known to allow ultrasound waves to penetrate further. This paper presents an ultrasound system specifically for modulated-excitation-based IVUS imaging. The system incorporates a high-voltage waveform generator and an image processing board that are optimized for IVUS applications. In addition, a miniaturized ultrasound transducer has been constructed using a Pb(Mg 1/3 Nb 2/3 )O 3 -PbTiO 3 single crystal to improve the ultrasound characteristics. The results show that the proposed system was able to provide increases of 86.7% in penetration depth and 9.6 dB in the signal-to-noise ratio for 60 MHz IVUS. In vitro tissue samples were also investigated to demonstrate the performance of the system.

  19. Transcranial magnetic stimulation: Improved coil design for deep brain investigation

    NASA Astrophysics Data System (ADS)

    Crowther, L. J.; Marketos, P.; Williams, P. I.; Melikhov, Y.; Jiles, D. C.; Starzewski, J. H.

    2011-04-01

    This paper reports on a design for a coil for transcranial magnetic stimulation. The design shows potential for improving the penetration depth of the magnetic field, allowing stimulation of subcortical structures within the brain. The magnetic and induced electric fields in the human head have been calculated with finite element electromagnetic modeling software and compared with empirical measurements. Results show that the coil design used gives improved penetration depth, but also indicates the likelihood of stimulation of additional tissue resulting from the spatial distribution of the magnetic field.

  20. Pavement-Transportation Computer Assisted Structural Engineering (PCASE) Implementation of the Modified Berggren (ModBerg) Equation for Computing the Frost Penetration Depth within Pavement Structures

    DTIC Science & Technology

    2012-04-01

    ER D C/ G SL T R -1 2 -1 5 Pavement -Transportation Computer Assisted Structural Engineering (PCASE) Implementation of the Modified...Berggren (ModBerg) Equation for Computing the Frost Penetration Depth within Pavement Structures G eo te ch n ic al a n d S tr u ct u re s La b or at...April 2012 Pavement -Transportation Computer Assisted Structural Engineering (PCASE) Implementation of the Modified Berggren (ModBerg) Equation for

  1. Light penetration structures the deep acoustic scattering layers in the global ocean.

    PubMed

    Aksnes, Dag L; Røstad, Anders; Kaartvedt, Stein; Martinez, Udane; Duarte, Carlos M; Irigoien, Xabier

    2017-05-01

    The deep scattering layer (DSL) is a ubiquitous acoustic signature found across all oceans and arguably the dominant feature structuring the pelagic open ocean ecosystem. It is formed by mesopelagic fishes and pelagic invertebrates. The DSL animals are an important food source for marine megafauna and contribute to the biological carbon pump through the active flux of organic carbon transported in their daily vertical migrations. They occupy depths from 200 to 1000 m at daytime and migrate to a varying degree into surface waters at nighttime. Their daytime depth, which determines the migration amplitude, varies across the global ocean in concert with water mass properties, in particular the oxygen regime, but the causal underpinning of these correlations has been unclear. We present evidence that the broad variability in the oceanic DSL daytime depth observed during the Malaspina 2010 Circumnavigation Expedition is governed by variation in light penetration. We find that the DSL depth distribution conforms to a common optical depth layer across the global ocean and that a correlation between dissolved oxygen and light penetration provides a parsimonious explanation for the association of shallow DSL distributions with hypoxic waters. In enhancing understanding of this phenomenon, our results should improve the ability to predict and model the dynamics of one of the largest animal biomass components on earth, with key roles in the oceanic biological carbon pump and food web.

  2. Nd-glass laser for deep-penetration welding and hardening

    NASA Astrophysics Data System (ADS)

    Kayukov, Serguei V.; Yaresko, Sergey I.; Mikheyev, Pavel A.

    2000-04-01

    Pulsed Nd-glass lasers usually have low beam quality (200 - 300 mm-mrad), and are used only for surface hardening of metals. However, high pulse energy make them feasible for deep penetration welding if their beam quality could be improved. We investigated beam properties of Nd-glass laser with unstable resonator with semitransparent output coupler (URSOC). We had found that beam divergence of the laser with URSOC was an order of magnitude smaller than that of the laser with stable resonator. The achieved beam quality (40 - 50 mm-mrad) permitted to perform deep penetration welding with the aspect ratio of approximately 8. For beam divergence of 3 mrad melt depth of 6.3 mm was achieved with the ratio of depth to pulse energy of 0.27 mm/J.

  3. Unsteady jet in designing innovative drug delivery system

    NASA Astrophysics Data System (ADS)

    Wang, Cong; Mazur, Paul; Cosse, Julia; Rider, Stephanie; Gharib, Morteza

    2014-11-01

    Micro-needle injections, a promising pain-free drug delivery method, is constrained by its limited penetration depth. This deficiency can be overcome by implementing fast unsteady jet that can penetrate sub-dermally. The development of a faster liquid jet would increase the penetration depth and delivery volume of micro-needles. In this preliminary work, the nonlinear transient behavior of an elastic tube balloon in providing fast discharge is analyzed. A physical model that combines the Mooney Rivlin Material model and Young-Lapalce's Law was developed and used to investigate the fast discharging dynamic phenomenon. A proof of concept prototype was constructed to demonstrate the feasibility of a simple thumb-sized delivery system to generate liquid jet with desired speed in the range of 5-10 m/s. This work is supported by ZCUBE Corporation.

  4. Analysis of the penetration of a caffeine containing shampoo into the hair follicles by in vivo laser scanning microscopy

    NASA Astrophysics Data System (ADS)

    Lademann, J.; Richter, H.; Schanzer, S.; Klenk, A.; Sterry, W.; Patzelt, A.

    2010-02-01

    In previous in vitro investigations, it was demonstrated that caffeine is able to stimulate the hair growth. Therefore, a penetration of caffeine into the hair follicle is necessary. In the present study, in vivo laser scanning microscopy (LSM) was used to investigate the penetration and storage of a caffeine containing shampoo into the hair follicles. It was shown that a 2-min contact time of the shampoo with the skin was enough to accumulate significant parts of the shampoo in the hair follicles. A penetration of the shampoo up to a depth of approx. 200 μm could be detected, which represents the detection limit of the LSM. At this depth, the close network of the blood capillaries surrounding the hair follicles commences. Even after 24 h, the substance was still detectable in the hair follicles. This demonstrates the long-term reservoir function of the hair follicles for topically applied substances such as caffeine.

  5. Inter-layered clay stacks in Jurassic shales

    NASA Technical Reports Server (NTRS)

    Pye, K.; Krinsley, D. H.

    1983-01-01

    Scanning electron microscopy in the backscattered electron mode is used together with energy-dispersive X-ray microanalysis to show that Lower Jurassic shales from the North Sea Basin contain large numbers of clay mineral stacks up to 150 microns in size. Polished shale sections are examined to determine the size, shape orientation, textural relationships, and internal compositional variations of the clays. Preliminary evidence that the clay stacks are authigenic, and may have formed at shallow burial depths during early diagenesis, is presented.

  6. Bioactive glass fillers reduce bacterial penetration into marginal gaps for composite restorations

    PubMed Central

    Khvostenko, D.; Hilton, T. J.; Ferracane, J. L.; Mitchell, J. C.; Kruzic, J. J.

    2015-01-01

    Objectives Bioactive glass (BAG) is known to possess antimicrobial and remineralizing properties; however, the use of BAG as a filler for resin based composite restorations to slow recurrent caries has not been studied. Accordingly, the objective of this study was to investigate the effect of 15 wt% BAG additions to a resin composite on bacterial biofilms penetrating into marginal gaps of simulated tooth fillings in vitro during cyclic mechanical loading. Methods Human molars were machined into approximately 3 mm thick disks of dentin and 1.5–2 mm deep composite restorations were placed. A narrow 15–20 micrometer wide dentin-composite gap was allowed to form along half of the margin by not applying dental adhesive to that region. Two different 72 wt% filled composites were used, one with 15 wt% BAG filler (15BAG) and the balance silanated strontium glass and one filled with OX-50 and silanated strontium glass without BAG (0BAG – control). Samples of both groups had Streptococcus mutans biofilms grown on the surface and were tested inside a bioreactor for two weeks while subjected to periods of cyclic mechanical loading. After post-test biofilm viability was confirmed, each specimen was fixed in glutaraldehyde, gram positive stained, mounted in resin and cross-sectioned to reveal the gap profile. Depth of biofilm penetration for 0BAG and 15BAG was quantified as the fraction of gap depth. The data were compared using a Student’s t-test. Results The average depth of bacterial penetration into the marginal gap for the 15BAG samples was significantly smaller (~61%) in comparison to 0BAG, where 100% penetration was observed for all samples with the biofilm penetrating underneath of the restoration in some cases. Significance BAG containing resin dental composites reduce biofilm penetration into marginal gaps of simulated tooth restorations. This suggests BAG containing composites may have the potential to slow the development and propagation of secondary tooth decay at restoration margins. PMID:26621028

  7. Photon excitation enabled large aperture space-charge-controlled potassium tantalate niobate (KTN) beam deflector

    NASA Astrophysics Data System (ADS)

    Zhu, Wenbin; Chao, Ju-Hung; Chen, Chang-Jiang; Shang, Annan; Lee, Yun Goo; Yin, Shizhuo; Dubinskii, Mark; Hoffman, Robert C.

    2018-03-01

    To overcome the depth limitation of the space-charge-controlled (SCC) potassium tantalate niobate (KTN) deflectors, we report in this paper a method of increasing the aperture of SCC-KTN deflectors by harnessing the physical mechanism of blue light photon excitation. The experimental results show that the deflection angle can be increased from 0.7 mrad without the blue light excitation to 2.5 mrad with the blue light excitation at a penetration depth of 5 mm under the same external applied voltage, which is consistent with the theoretical analysis. This represents a substantial increase in the deflection angle at a much deeper penetration depth, which can be very useful for applications such as high speed 3D printings and displays.

  8. Park size and disturbance: impact on soil heterogeneity - a case study Tel-Aviv- Jaffa.

    NASA Astrophysics Data System (ADS)

    Zhevelev, Helena; Sarah, Pariente; Oz, Atar

    2015-04-01

    Parks and gardens are poly-functional elements of great importance in urban areas, and can be used for optimization of physical and social components in these areas. This study aimed to investigate alteration of soil properties with land usages within urban park and with area size of park. Ten parks differed by size (2 - 50 acres) were chosen, in random, in Tel-Aviv- Jaffa city. Soil was sampled in four microenvironments ((lawn, path, picnic and peripheral area (unorganized area) of each the park)), in three points and three depth (0-2, 5-10 and 10-20 cm). Penetration depth was measured in all point of sampling. For each soil sample electrical conductivity and organic matter content were determined. Averages of penetration depth drastically increased from the most disturbed microenvironments (path and picnic) to the less disturbed ones (lawn and peripheral). The maximal heterogeneity (by variances and percentiles) of penetration depth was found in the peripheral area. In this area, penetration depth increased with increasing park size, i.e., from 2.6 cm to 3.7 cm in the small and large parks, respectively. Averages of organic matter content and electrical conductivity decreased with soil depth in all microenvironments and increased with decreasing disturbance of microenvironments. Maximal heterogeneity for both of these properties was found in the picnic area. Increase of park size was accompanied by increasing of organic matter content in the upper depth in the peripheral area, i.e., from 2.4% in the small parks to 4.5% in the large ones. In all microenvironments the increasing of averages of all studied soil properties was accompanied by increasing heterogeneity, i.e., variances and upper percentiles. The increase in the heterogeneity of the studied soil properties is attributed to improved ecological soil status in the peripheral area, on the one hand, and to the high anthropogenic pressure in the picnic area, on the other. This means that the urban park offers "islands" with better ecological conditions which improve the urban system.

  9. Bending-related faulting and mantle serpentinization at the Middle America trench.

    PubMed

    Ranero, C R; Morgan, J Phipps; McIntosh, K; Reichert, C

    2003-09-25

    The dehydration of subducting oceanic crust and upper mantle has been inferred both to promote the partial melting leading to arc magmatism and to induce intraslab intermediate-depth earthquakes, at depths of 50-300 km. Yet there is still no consensus about how slab hydration occurs or where and how much chemically bound water is stored within the crust and mantle of the incoming plate. Here we document that bending-related faulting of the incoming plate at the Middle America trench creates a pervasive tectonic fabric that cuts across the crust, penetrating deep into the mantle. Faulting is active across the entire ocean trench slope, promoting hydration of the cold crust and upper mantle surrounding these deep active faults. The along-strike length and depth of penetration of these faults are also similar to the dimensions of the rupture area of intermediate-depth earthquakes.

  10. Direct evidence for a pressure-induced nodal superconducting gap in the Ba0.65Rb0.35Fe2As2 superconductor

    PubMed Central

    Guguchia, Z.; Amato, A.; Kang, J.; Luetkens, H.; Biswas, P. K.; Prando, G.; von Rohr, F.; Bukowski, Z.; Shengelaya, A.; Keller, H.; Morenzoni, E.; Fernandes, Rafael M.; Khasanov, R.

    2015-01-01

    The superconducting gap structure in iron-based high-temperature superconductors (Fe-HTSs) is non-universal. In contrast to other unconventional superconductors, in the Fe-HTSs both d-wave and extended s-wave pairing symmetries are close in energy. Probing the proximity between these very different superconducting states and identifying experimental parameters that can tune them is of central interest. Here we report high-pressure muon spin rotation experiments on the temperature-dependent magnetic penetration depth in the optimally doped nodeless s-wave Fe-HTS Ba0.65Rb0.35Fe2As2. Upon pressure, a strong decrease of the penetration depth in the zero-temperature limit is observed, while the superconducting transition temperature remains nearly constant. More importantly, the low-temperature behaviour of the inverse-squared magnetic penetration depth, which is a direct measure of the superfluid density, changes qualitatively from an exponential saturation at zero pressure to a linear-in-temperature behaviour at higher pressures, indicating that hydrostatic pressure promotes the appearance of nodes in the superconducting gap. PMID:26548650

  11. Process Parameter Effects on Material Removal in Magnetorheological Finishing of Borosilicate Glass

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Miao, C.; Lambroopulos, J.C.; Jacobs, S.D.

    2010-04-14

    We investigate the effects of processing parameters on material removal for borosilicate glass. Data are collected on a magnetorheological finishing (MRF) spot taking machine (STM) with a standard aqueous magnetorheological (MR) fluid. Normal and shear forces are measured simultaneously, in situ, with a dynamic dual load cell. Shear stress is found to be independent of nanodiamond concentration, penetration depth, magnetic field strength, and the relative velocity between the part and the rotating MR fluid ribbon. Shear stress, determined primarily by the material mechanical properties, dominates removal in MRF. The addition of nanodiamond abrasives greatly enhances the material removal efficiency, withmore » the removal rate saturating at a high abrasive concentration. The volumetric removal rate (VRR) increases with penetration depth but is insensitive to magnetic field strength. The VRR is strongly correlated with the relative velocity between the ribbon and the part, as expected by the Preston equation. A modified removal rate model for MRF offers a better estimation of MRF removal capability by including nanodiamond concentration and penetration depth.« less

  12. London penetration depth and superfluid density of single-crystalline Fe1+y(Te1-xSex) and Fe1+y(Te1-xSx)

    NASA Astrophysics Data System (ADS)

    Kim, H.; Martin, C.; Gordon, R. T.; Tanatar, M. A.; Hu, J.; Qian, B.; Mao, Z. Q.; Hu, Rongwei; Petrovic, C.; Salovich, N.; Giannetta, R.; Prozorov, R.

    2010-05-01

    The in-plane London penetration depth, λ(T) , was measured in single crystals of the iron-chalcogenide superconductors Fe1.03(Te0.63Se0.37) and Fe1.06(Te0.88S0.14) by using a radio-frequency tunnel diode resonator. Similar to the iron-arsenides and in stark contrast to the iron-phosphides, iron-chalcogenides exhibit a nearly quadratic temperature variation of λ(T) at low temperatures. The absolute value of the penetration depth in the T→0 limit was determined for Fe1.03(Te0.63Se0.37) by using an Al coating technique, giving λ(0)≈560±20nm . The superfluid density ρs(T)=λ2(0)/λ2(T) was fitted with a self-consistent two-gap γ model. While two different gaps are needed to describe the full-range temperature variation in ρs(T) , a nonexponential low-temperature behavior requires pair-breaking scattering, and therefore an unconventional (e.g., s± or nodal) order parameter.

  13. Direct evidence for a pressure-induced nodal superconducting gap in the Ba 0.65Rb 0.35Fe 2As 2 superconductor

    DOE PAGES

    Guguchia, Z.; Amato, A.; Kang, J.; ...

    2015-11-09

    The superconducting gap structure in iron-based high-temperature superconductors (Fe-HTSs) is non-universal. Contrasting with other unconventional superconductors, in the Fe-HTSs both d-wave and extended s-wave pairing symmetries are close in energy. Probing the proximity between these very different superconducting states and identifying experimental parameters that can tune them is of central interest. Here we report high-pressure muon spin rotation experiments on the temperature-dependent magnetic penetration depth in the optimally doped nodeless s-wave Fe-HTS Ba 0.65Rb 0.35Fe 2As 2. Upon pressure, a strong decrease of the penetration depth in the zero-temperature limit is observed, while the superconducting transition temperature remains nearly constant.more » More importantly, the low-temperature behaviour of the inverse-squared magnetic penetration depth, which is a direct measure of the superfluid density, changes qualitatively from an exponential saturation at zero pressure to a linear-in-temperature behaviour at higher pressures, indicating that hydrostatic pressure promotes the appearance of nodes in the superconducting gap.« less

  14. Gamma-ray energy buildup factor calculations and shielding effects of some Jordanian building structures

    NASA Astrophysics Data System (ADS)

    Sharaf, J. M.; Saleh, H.

    2015-05-01

    The shielding properties of three different construction styles, and building materials, commonly used in Jordan, were evaluated using parameters such as attenuation coefficients, equivalent atomic number, penetration depth and energy buildup factor. Geometric progression (GP) method was used to calculate gamma-ray energy buildup factors of limestone, concrete, bricks, cement plaster and air for the energy range 0.05-3 MeV, and penetration depths up to 40 mfp. It has been observed that among the examined building materials, limestone offers highest value for equivalent atomic number and linear attenuation coefficient and the lowest values for penetration depth and energy buildup factor. The obtained buildup factors were used as basic data to establish the total equivalent energy buildup factors for three different multilayer construction styles using an iterative method. The three styles were then compared in terms of fractional transmission of photons at different incident photon energies. It is concluded that, in case of any nuclear accident, large multistory buildings with five layers exterior walls, style A, could effectively attenuate radiation more than small dwellings of any construction style.

  15. Interaction of both plasmas in CO2 laser-MAG hybrid welding of carbon steel

    NASA Astrophysics Data System (ADS)

    Kutsuna, Muneharu; Chen, Liang

    2003-03-01

    Researches and developments of laser and arc hybrid welding has been curried out since in 1978. Especially, CO2 laser and TIG hybrid welding has been studied for increasing the penetration depth and welding speed. Recently laser and MIG/MAG/Plasma hybrid welding processes have been developed and applied to industries. It was recognized as a new welding process that promote the flexibility of the process for increasing the penetration depth, welding speed and allowable joint gap and improving the quality of the welds. In the present work, CO2 Laser-MAG hybrid welding of carbon steel (SM490) was investigated to make clear the phenomenon and characteristics of hybrid welding process comparing with laser welding and MAG process. The effects of many process parameters such as welding current, arc voltage, welding speed, defocusing distance, laser-to-arc distance on penetration depth, bead shape, spatter, arc stability and plasma formation were investigated in the present work. Especially, the interaction of laser plasma and MAG arc plasma was considered by changing the laser to arc distance (=DLA).

  16. Model of convection mass transfer in titanium alloy at low energy high current electron beam action

    NASA Astrophysics Data System (ADS)

    Sarychev, V. D.; Granovskii, A. Yu; Nevskii, S. A.; Konovalov, S. V.; Gromov, V. E.

    2017-01-01

    The convection mixing model is proposed for low-energy high-current electron beam treatment of titanium alloys, pre-processed by heterogeneous plasma flows generated via explosion of carbon tape and powder TiB2. The model is based on the assumption vortices in the molten layer are formed due to the treatment by concentrated energy flows. These vortices evolve as the result of thermocapillary convection, arising because of the temperature gradient. The calculation of temperature gradient and penetration depth required solution of the heat problem with taking into account the surface evaporation. However, instead of the direct heat source the boundary conditions in phase transitions were changed in the thermal conductivity equation, assuming the evaporated material takes part in the heat exchange. The data on the penetration depth and temperature distribution are used for the thermocapillary model. The thermocapillary model embraces Navier-Stocks and convection heat transfer equations, as well as the boundary conditions with the outflow of evaporated material included. The solution of these equations by finite elements methods pointed at formation of a multi-vortices structure when electron-beam treatment and its expansion over new zones of material. As the result, strengthening particles are found at the depth exceeding manifold their penetration depth in terms of the diffusion mechanism.

  17. Overcoming sampling depth variations in the analysis of broadband hyperspectral images of breast tissue (Conference Presentation)

    NASA Astrophysics Data System (ADS)

    Kho, Esther; de Boer, Lisanne L.; Van de Vijver, Koen K.; Sterenborg, Henricus J. C. M.; Ruers, Theo J. M.

    2017-02-01

    Worldwide, up to 40% of the breast conserving surgeries require additional operations due to positive resection margins. We propose to reduce this percentage by using hyperspectral imaging for resection margin assessment during surgery. Spectral hypercubes were collected from 26 freshly excised breast specimens with a pushbroom camera (900-1700nm). Computer simulations of the penetration depth in breast tissue suggest a strong variation in sampling depth ( 0.5-10 mm) over this wavelength range. This was confirmed with a breast tissue mimicking phantom study. Smaller penetration depths are observed in wavelength regions with high water and/or fat absorption. Consequently, tissue classification based on spectral analysis over the whole wavelength range becomes complicated. This is especially a problem in highly inhomogeneous human tissue. We developed a method, called derivative imaging, which allows accurate tissue analysis, without the impediment of dissimilar sampling volumes. A few assumptions were made based on previous research. First, the spectra acquired with our camera from breast tissue are mainly shaped by fat and water absorption. Second, tumor tissue contains less fat and more water than healthy tissue. Third, scattering slopes of different tissue types are assumed to be alike. In derivative imaging, the derivatives are calculated of wavelengths a few nanometers apart; ensuring similar penetration depths. The wavelength choice determines the accuracy of the method and the resolution. Preliminary results on 3 breast specimens indicate a classification accuracy of 93% when using wavelength regions characterized by water and fat absorption. The sampling depths at these regions are 1mm and 5mm.

  18. Validation of a measuring technique with computed tomography for cement penetration into trabecular bone underneath the tibial tray in total knee arthroplasty on a cadaver model

    PubMed Central

    2014-01-01

    Background In total knee arthroplasty (TKA), cement penetration between 3 and 5 mm beneath the tibial tray is required to prevent loosening of the tibia component. The objective of this study was to develop and validate a reliable in vivo measuring technique using CT imaging to assess cement distribution and penetration depth in the total area underneath a tibia prosthesis. Methods We defined the radiodensity ranges for trabecular tibia bone, polymethylmethacrylate (PMMA) cement and cement-penetrated trabecular bone and measured the percentages of cement penetration at various depths after cementing two tibia prostheses onto redundant femoral heads. One prosthesis was subsequently removed to examine the influence of the metal tibia prostheses on the quality of the CT images. The percentages of cement penetration in the CT slices were compared with percentages measured with photographs of the corresponding transversal slices. Results Trabecular bone and cement-penetrated trabecular bone had no overlap in quantitative scale of radio-density. There was no significant difference in mean HU values when measuring with or without the tibia prosthesis. The percentages of measured cement-penetrated trabecular bone in the CT slices of the specimen were within the range of percentages that could be expected based on the measurements with the photographs (p = 0.04). Conclusions CT scan images provide valid results in measuring the penetration and distribution of cement into trabecular bone underneath the tibia component of a TKA. Since the proposed method does not turn metal elements into artefacts, it enables clinicians to assess the width and density of the cement mantle in vivo and to compare the results of different cementing methods in TKA. PMID:25158996

  19. Influence of the mole penetrator on measurements of heat flow in lunar subsurface layers

    NASA Astrophysics Data System (ADS)

    Wawrzaszek, Roman; Drogosz, Michal; Seweryn, Karol; Banaszkiewicz, Marek; Grygorczuk, Jerzy

    Measuring the thermal gradient in subsurface layers is a basic method of determination the heat flux from the interior of a planetary body to its surface. In case of the Moon, such measurements complemented with the results of theoretical analysis and modeling can significantly improve our understanding of the thermal and geological evolution of the Moon. In practice, temperature gradient measurements are performed by at least two sensors located at different depths under the surface. These sensors will be attached to a penetrator [1] or to a cable pulled behind the penetrator. In both cases the object that carries the sensors, e.g. penetrator, perturb temperature measurements. In our study we analyze a case of two thermal sensors attached to the ends of 350mm long penetrator made of a composite material. In agreement with the studies of other authors we have found that the penetrator should be placed at the depth of 2-3 meters, where periodic changes of the temperature due to variation of solar flux at the surface are significantly smaller than the error of temperature measurement. The most important result of our analysis is to show how to deconvolve the real gradient of the temperature from the measurements perturbed by the penetrator body. In this way it will be possible to more accurately determine heat flux in the lunar regolith. [1] Grygorczuk J., Seweryn K., Wawrzaszek R., Banaszkiewicz M., Insertion of a Mole Pene-trator -Experimental Results, /39th Lunar and Planetary Science Conference /League City, Texas 2008

  20. A 40-foot static cone penetrometer

    USGS Publications Warehouse

    Beard, R.M.; Lee, H.J.

    1982-01-01

    The Navy needs a lightweight device for testing seafloor soils to sub bottom depths of 12 meters in water depths to 60 meters. To meet this need a quasistatic cone penetration device that uses water jetting to reduce friction on the cone rod has been developed. This device is called the XSP-40. The 5-ton XSP-40 stands 15 meters tall and pushes a standard 5-ton cone into the seafloor. It is remotely controlled with an electronic unit on the deck of the support vessel. All cone outputs are recorded directly as a function of penetration depth with a strip chart recorder. A full suite of gauges is provided. on the electronic unit for monitoring the XSP-40's performance during a test .. About 40 penetration tests have been performed with very good success. The XSP-40 was field tested in Norton Sound, off the west coast of Alaska. The general objective, in addition to evaluation of the device, was to gather geotechnical information on sediments that may be involved in processes potentially hazardous to offshore development. Four example penetration records are presented from gas charged sediment zones and areas near the Yukon River delta. In general it was determined that soil classification from cone data agreed well with classifications from core samples. Relative densities of the silt-sand to sandy-silt soils were usually very high. The significance of these results are discussed with respect to storm wave, liquefaction. It is concluded that the XSP-40 is a durable and reliable piece of equipment capable of achieving penetration beyond that possible when not using the water jet system.

  1. 30 CFR 250.1167 - What information must I submit with forms and for approvals?

    Code of Federal Regulations, 2011 CFR

    2011-07-01

    ..., REGULATION, AND ENFORCEMENT, DEPARTMENT OF THE INTERIOR OFFSHORE OIL AND GAS AND SULPHUR OPERATIONS IN THE... production Downhole commingling Reservoir reclassification Production within 500-ft of a unit or lease line... maps with penetration point and subsea depth for each well penetrating the reservoirs, highlighting...

  2. Optimal Design of Sheet Pile Wall Embedded in Clay

    NASA Astrophysics Data System (ADS)

    Das, Manas Ranjan; Das, Sarat Kumar

    2015-09-01

    Sheet pile wall is a type of flexible earth retaining structure used in waterfront offshore structures, river protection work and temporary supports in foundations and excavations. Economy is an essential part of a good engineering design and needs to be considered explicitly in obtaining an optimum section. By considering appropriate embedment depth and sheet pile section it may be possible to achieve better economy. This paper describes optimum design of both cantilever and anchored sheet pile wall penetrating clay using a simple optimization tool Microsoft Excel ® Solver. The detail methodology and its application with examples are presented for cantilever and anchored sheet piles. The effects of soil properties, depth of penetration and variation of ground water table on the optimum design are also discussed. Such a study will help professional while designing the sheet pile wall penetrating clay.

  3. Laser-welded Dissimilar Steel-aluminum Seams for Automotive Lightweight Construction

    NASA Astrophysics Data System (ADS)

    Schimek, M.; Springer, A.; Kaierle, S.; Kracht, D.; Wesling, V.

    By reducing vehicle weight, a significant increase in fuel efficiency and consequently a reduction in CO 2 emissions can be achieved. Currently a high interest in the production of hybrid weld seams between steel and aluminum exists. Previous methods as laser brazing are possible only by using fluxes and additional materials. Laser welding can be used to join steel and aluminum without the use of additives. With a low penetration depth increases in tensile strength can be achieved. Recent results from laser welded overlap seams show that there is no compromise in strength by decreasing penetration depth in the aluminum.

  4. Atom penetration from a thin film into the substrate during sputtering by polyenergetic Ar{sup +} ion beam with mean energy of 9.4 keV

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Kalin, B.A.; Gladkov, V.P.; Volkov, N.V.

    Penetration of alien atoms (Be, Ni) into Be, Al, Zr, Si and diamond was investigated under Ar{sup +} ion bombardment of samples having thermally evaporated films of 30--50 nm. Sputtering was carried out using a wide energy spectrum beam of Ar{sup +} ions of 9.4 keV to dose D = 1 {times} 10{sup 16}--10{sup 19} ion/cm{sup 2}. Implanted atom distribution in the targets was measured by Rutherford backscattering spectrometry (RBS) of H{sup +} and He{sup +} ions with energy of 1.6 MeV as well as secondary ion mass-spectrometry (SIMS). During the bombardment, the penetration depth of Ar atoms increases withmore » dose linearly. This depth is more than 3--20 times deeper than the projected range of bombarding ions and recoil atoms. This is a deep action effect. The analysis shows that the experimental data for foreign atoms penetration depth are similar to the data calculated for atom migration through the interstitial site in a field of internal (lateral) compressive stresses created in the near-surface layer of the substrate as a result of implantation. Under these experimental conditions atom ratio r{sub i}/r{sub m} (r{sub i} -- radius of dopant, r{sub m} -- radius target of substrate) can play a principal determining role.« less

  5. Fine reservoir structure modeling based upon 3D visualized stratigraphic correlation between horizontal wells: methodology and its application

    NASA Astrophysics Data System (ADS)

    Chenghua, Ou; Chaochun, Li; Siyuan, Huang; Sheng, James J.; Yuan, Xu

    2017-12-01

    As the platform-based horizontal well production mode has been widely applied in petroleum industry, building a reliable fine reservoir structure model by using horizontal well stratigraphic correlation has become very important. Horizontal wells usually extend between the upper and bottom boundaries of the target formation, with limited penetration points. Using these limited penetration points to conduct well deviation correction means the formation depth information obtained is not accurate, which makes it hard to build a fine structure model. In order to solve this problem, a method of fine reservoir structure modeling, based on 3D visualized stratigraphic correlation among horizontal wells, is proposed. This method can increase the accuracy when estimating the depth of the penetration points, and can also effectively predict the top and bottom interfaces in the horizontal penetrating section. Moreover, this method will greatly increase not only the number of points of depth data available, but also the accuracy of these data, which achieves the goal of building a reliable fine reservoir structure model by using the stratigraphic correlation among horizontal wells. Using this method, four 3D fine structure layer models have been successfully built of a specimen shale gas field with platform-based horizontal well production mode. The shale gas field is located to the east of Sichuan Basin, China; the successful application of the method has proven its feasibility and reliability.

  6. Long-wavelength optical coherence tomography at 1.7 µm for enhanced imaging depth

    PubMed Central

    Sharma, Utkarsh; Chang, Ernest W.; Yun, Seok H.

    2009-01-01

    Multiple scattering in a sample presents a significant limitation to achieve meaningful structural information at deeper penetration depths in optical coherence tomography (OCT). Previous studies suggest that the spectral region around 1.7 µm may exhibit reduced scattering coefficients in biological tissues compared to the widely used wavelengths around 1.3 µm. To investigate this long-wavelength region, we developed a wavelength-swept laser at 1.7 µm wavelength and conducted OCT or optical frequency domain imaging (OFDI) for the first time in this spectral range. The constructed laser is capable of providing a wide tuning range from 1.59 to 1.75 µm over 160 nm. When the laser was operated with a reduced tuning range over 95 nm at a repetition rate of 10.9 kHz and an average output power of 12.3 mW, the OFDI imaging system exhibited a sensitivity of about 100 dB and axial and lateral resolution of 24 µm and 14 µm, respectively. We imaged several phantom and biological samples using 1.3 µm and 1.7 µm OFDI systems and found that the depth-dependent signal decay rate is substantially lower at 1.7 µm wavelength in most, if not all samples. Our results suggest that this imaging window may offer an advantage over shorter wavelengths by increasing the penetration depths as well as enhancing image contrast at deeper penetration depths where otherwise multiple scattered photons dominate over ballistic photons. PMID:19030057

  7. Photoacoustic imaging with planoconcave optical microresonator sensors: feasibility studies based on phantom imaging

    NASA Astrophysics Data System (ADS)

    Guggenheim, James A.; Zhang, Edward Z.; Beard, Paul C.

    2017-03-01

    The planar Fabry-Pérot (FP) sensor provides high quality photoacoustic (PA) images but beam walk-off limits sensitivity and thus penetration depth to ≍1 cm. Planoconcave microresonator sensors eliminate beam walk-off enabling sensitivity to be increased by an order-of-magnitude whilst retaining the highly favourable frequency response and directional characteristics of the FP sensor. The first tomographic PA images obtained in a tissue-realistic phantom using the new sensors are described. These show that the microresonator sensors provide near identical image quality as the planar FP sensor but with significantly greater penetration depth (e.g. 2-3cm) due to their higher sensitivity. This offers the prospect of whole body small animal imaging and clinical imaging to depths previously unattainable using the FP planar sensor.

  8. Osteosynthesis for clavicle fractures: How close are we to penetration of neurovascular structures?

    PubMed

    Stillwell, A; Ioannou, C; Daniele, L; Tan, S L E

    2017-02-01

    Risks associated with drill plunging are well recognised in clavicle osteosynthesis. To date no studies have described plunge depth associated with clavicle osteosynthesis. To determine whether plunge depth associated with clavicle osteosynthesis is great enough to penetrate neurovascular structures and whether surgical experience reduces the risk of neurovascular injury METHOD: Cadaveric clavicles were pressed into spongy phenolic foam to allow measurement of drill bit penetration beyond the far cortex (plunge depth). 15 surgeons grouped according to experience were asked to drill a single hole in the medial, middle and lateral clavicle in 2 specimens each. Each surgeon used fully a charged standard Stryker drill with a new 2.6mm drill bit and guide. Plunge depths were measured in 0.5mm increments. Depth measurements were compared amongst groups and to previously documented distances to neurovascular structures as outlined by Robinson et al. Kruskal-Wallis test was used for overall comparison and Mann-Whitney U test was used for comparing the groups individually. Mean plunge depth across all groups was 3.4mm, (0.5-6.5), 4.0mm (1mm-8.5mm) and 4.0mm (0.5mm-15mm) in the medial, middle and lateral clavicle. Plunge depths were greater than previously documented distances to the subclavian vein at the medial clavicle on nine occasions. Plunge depths in the middle and lateral clavicle were well within the previously documented distances from neurovascular structures. There was no correlation between level of experience and median plunge depth (p=0.18). However, inexperienced surgeons plunged 1mm greater than intermediate and experienced surgeons (p=0.026). There was one significant outlier; a 15mm plunge depth by an inexperienced surgeon in the lateral clavicle. Clavicle osteosynthesis has a relatively high risk of neurovascular injury. Plunge depths through the clavicle often exceed the distance of neurovascular structures, especially in the medial clavicle. A thorough understanding of the anatomy of these neurovascular structures and methods to prevent excessive plunging is important prior to undertaking clavicle osteosynthesis. Copyright © 2016 Elsevier Ltd. All rights reserved.

  9. Comparison of sealer penetration using the EndoVac irrigation system and conventional needle root canal irrigation.

    PubMed

    Kara Tuncer, Aysun; Unal, Bayram

    2014-05-01

    The aim of this study was to compare the effect of the EndoVac irrigation system (SybronEndo, Orange, CA) and conventional endodontic needle irrigation on sealer penetration into dentinal tubules. Forty single-rooted, recently extracted human maxillary central incisors were randomly divided into 2 groups according to the irrigation technique used: conventional endodontic needle irrigation and EndoVac irrigation. All teeth were instrumented using the ProFile rotary system (Dentsply Maillefer, Ballaigues, Switzerland) and obturated with gutta-percha and AH Plus sealer (Dentsply DeTrey, Konstanz, Germany) labeled with fluorescent dye. Transverse sections at 1, 3, and 5 mm from the root apex were examined using confocal laser scanning microscopy. The total percentage and maximum depth of sealer penetration were then measured. Mann-Whitney test results showed that EndoVac irrigation resulted in a significantly higher percentage of sealer penetration than conventional irrigation at both the 1- and 3-mm levels (P < .05). However, no difference was found at the 5-mm level. The 5-mm sections in each group showed a significantly higher percentage and maximum depth of sealer penetration than did the 1- and 3-mm sections (P < .05). The EndoVac irrigation system significantly improved the sealer penetration at the 1- to 3-mm level over that of conventional endodontic needle irrigation. Copyright © 2014 American Association of Endodontists. Published by Elsevier Inc. All rights reserved.

  10. Mineralogical, chemical, and physical properties of the regolith overlying crystalline rocks, Fairfax County, Virginia: a preliminary report

    USGS Publications Warehouse

    Leo, Gerhard W.; Pavich, M.J.; Obermeier, Stephen F.

    1977-01-01

    Undisturbed cores of saprolite developed on crystalline rocks of the Piedmont Province in Fairfax County, Virginia have been obtained using a combination of Shelby tubes, Denison sampler, and modified diamond core-drilling. The principal purpose of the core study is to correlate variations in chemistry, mineralogy and texture with engineering properties throughout the weathering profile. Coring sites were chosen to obtain a maximum depth of weathering on diverse lithologies. The rocks investigated include pelitic schist, metagraywacke, granite, diabase and serpentinite. Four to twelve samples per core were selected, depending on thickness of 1) the weathering profile (from about 1 m in serpentinite to more than 30 m in pelitic schist) and on 2) megascopic changes in saprolite character for analysis of petrography, texture, clay mineralogy andd major element chemistry. Shear strength and compressibility were determined on corresponding segments of core. Standard penetration tests were performed adjacent to coring sites to evaluate engineering properties in situ. Geochemical changes of saprolite developed from each rock type follow predictable trends from fresh rock to soil profile, with relative Increases in Si, Ti, Al, Fe3+ and H20; variable K; and relative loss of Fe 2+, Mg, Ca, and Na. These variations are more pronounced in the weathering profiles over mafic and ultramafic rocks than metagraywacke. Clay minerals in granite, schist and metagraywacke saprolite are kaolinite, dioctahedral vermiculite, interlayered micavermiculite, and minor illite. Gibbsite is locally developed in near-surface samples of schist. Standard penetration test data for the upper 7 m of saprolite over schist and metagraywacke suggest alternations between stronger and weaker horizons than probably reflect variations in lithology including the presence of quartz lenses. Results for granite saprolite are most consistent but indicate lower strength. Shear strength increases fairly regularly downward in the weathering profile. The engineering behavior of diabase saprolite is controlled by a dense, plastic, near-surface clay layer (montmorillonite and kaolinite)overlying rock which is weathered to a granular state (grus), while engineering properties of serpentinite are determined by a very thin weathering profile.

  11. Method of producing nano-scaled graphene and inorganic platelets and their nanocomposites

    DOEpatents

    Jang, Bor Z [Centerville, OH; Zhamu, Aruna [Centerville, OH

    2011-02-22

    Disclosed is a method of exfoliating a layered material (e.g., graphite and graphite oxide) to produce nano-scaled platelets having a thickness smaller than 100 nm, typically smaller than 10 nm, and often between 0.34 nm and 1.02 nm. The method comprises: (a) subjecting the layered material in a powder form to a halogen vapor at a first temperature above the melting point or sublimation point of the halogen at a sufficient vapor pressure and for a duration of time sufficient to cause the halogen molecules to penetrate an interlayer space of the layered material, forming a stable halogen-intercalated compound; and (b) heating the halogen-intercalated compound at a second temperature above the boiling point of the halogen, allowing halogen atoms or molecules residing in the interlayer space to exfoliate the layered material to produce the platelets. Alternatively, rather than heating, step (a) is followed by a step of dispersing the halogen-intercalated compound in a liquid medium which is subjected to ultrasonication for exfoliating the halogen-intercalated compound to produce the platelets, which are dispersed in the liquid medium. The halogen can be readily captured and re-used, thereby significantly reducing the impact of halogen to the environment. The method can further include a step of dispersing the platelets in a polymer or monomer solution or suspension as a precursor step to nanocomposite fabrication.

  12. Method of producing nano-scaled graphene and inorganic platelets and their nanocomposites

    DOEpatents

    Jang, Bor Z [Centerville, OH; Zhamu, Aruna [Centerville, OH

    2012-02-14

    Disclosed is a method of exfoliating a layered material (e.g., graphite and graphite oxide) to produce nano-scaled platelets having a thickness smaller than 100 nm, typically smaller than 10 nm, and often between 0.34 nm and 1.02 nm. The method comprises: (a) subjecting the layered material in a powder form to a halogen vapor at a first temperature above the melting point or sublimation point of the halogen at a sufficient vapor pressure and for a duration of time sufficient to cause the halogen molecules to penetrate an interlayer space of the layered material, forming a stable halogen-intercalated compound; and (b) heating the halogen-intercalated compound at a second temperature above the boiling point of the halogen, allowing halogen atoms or molecules residing in the interlayer space to exfoliate the layered material to produce the platelets. Alternatively, rather than heating, step (a) is followed by a step of dispersing the halogen-intercalated compound in a liquid medium which is subjected to ultrasonication for exfoliating the halogen-intercalated compound to produce the platelets, which are dispersed in the liquid medium. The halogen can be readily captured and re-used, thereby significantly reducing the impact of halogen to the environment. The method can further include a step of dispersing the platelets in a polymer or monomer solution or suspension as a precursor step to nanocomposite fabrication.

  13. Grain boundary oxidation and an analysis of the effects of oxidation on fatigue crack nucleation life

    NASA Technical Reports Server (NTRS)

    Oshida, Y.; Liu, H. W.

    1988-01-01

    The effects of preoxidation on subsequent fatigue life were studied. Surface oxidation and grain boundary oxidation of a nickel-base superalloy (TAZ-8A) were studied at 600 to 1000 C for 10 to 1000 hours in air. Surface oxides were identified and the kinetics of surface oxidation was discussed. Grain boundary oxide penetration and morphology were studied. Pancake type grain boundary oxide penetrates deeper and its size is larger, therefore, it is more detrimental to fatigue life than cone-type grain boundary oxide. Oxide penetration depth, a (sub m), is related to oxidation temperature, T, and exposure time, t, by an empirical relation of the Arrhenius type. Effects of T and t on statistical variation of a (sub m) were analyzed according to the Weibull distribution function. Once the oxide is cracked, it serves as a fatigue crack nucleus. Statistical variation of the remaining fatigue life, after the formation of an oxide crack of a critical length, is related directly to the statistical variation of grain boundary oxide penetration depth.

  14. Grain boundary oxidation and an analysis of the effects of pre-oxidation on subsequent fatigue life

    NASA Technical Reports Server (NTRS)

    Oshida, Y.; Liu, H. W.

    1986-01-01

    The effects of preoxidation on subsequent fatigue life were studied. Surface oxidation and grain boundary oxidation of a nickel-base superalloy (TAZ-8A) were studied at 600 to 1000 C for 10 to 1000 hours in air. Surface oxides were identified and the kinetics of surface oxidation was discussed. Grain boundary oxide penetration and morphology were studied. Pancake type grain boundary oxide penetrates deeper and its size is larger, therefore, it is more detrimental to fatigue life than cone-type grain boundary oxide. Oxide penetration depth, a (sub m), is related to oxidation temperature, T, and exposure time, t, by an empirical relation of the Arrhenius type. Effects of T and t on statistical variation of a (sub m) were analyzed according to the Weibull distribution function. Once the oxide is cracked, it serves as a fatigue crack nucleus. Statistical variation of the remaining fatigue life, after the formation of an oxide crack of a critical length, is related directly to the statistical variation of grain boundary oxide penetration depth.

  15. Miniaturization technology for Lunar penetrator mission

    NASA Astrophysics Data System (ADS)

    Hayashi, T.; Saito, H.; Orii, T.; Masumoto, Y.

    1993-10-01

    The ISAS will launch Lunar-A in 1997 to study internal structure of the moon by seismometric measurements. A mother spacecraft which holds three penetrators will be launched by newly developed M-V rocket. Three penetrators will be released from the mother spacecraft orbiting around the moon. These penetrators make hard landing on the moon with shock of about 10,000 G and will penetrate about 1-3 m in depth into the soil. Three axis seismometer, heat flow meter, data handling subsystem, communications subsystem, power subsystem are installed in a penetrator. These penetrators will be placed at three different sites on the moon and expected to operate more than one year using super lithium primary batteries and will send data to the earth via the mother spacecraft. Weight of the penetrator is limited within 13 kg because of the rocket capability. To achieve the mission, it is absolutely necessary to develop miniaturizing technology in the size and power reduction for penetrator equipment in addition to special assembly technique to withstand extremely high-G environment.

  16. Sediment chronology in San Francisco Bay, California, defined by 210Pb, 234Th, 137Cs, and 239,340Pu

    USGS Publications Warehouse

    Fuller, C.C.; van Geen, Alexander; Baskaran, M.; Anima, R.

    1999-01-01

    Sediment chronologies based on radioisotope depth profiles were developed at two sites in the San Francisco Bay estuary to provide a framework for interpreting historical trends in organic compound and metal contaminant inputs. At Richardson Bay near the estuary mouth, sediments are highly mixed by biological and/or physical processes. Excess  penetration ranged from 2 to more than 10 cm at eight coring sites, yielding surface sediment mixing coefficients ranging from 12 to 170 cm2/year. At the site chosen for contaminant analyses, excess  activity was essentially constant over the upper 25 cm of the core with an exponential decrease below to the supported activity between 70 and 90 cm. Both  and  penetrated to 57-cm depth and have broad subsurface maxima between 33 and 41 cm. The best fit of the excess  profile to a steady state sediment accumulation and mixing model yielded an accumulation rate of 0.825 g/cm2/year (0.89 cm/year at sediment surface), surface mixing coefficient of 71 cm2/year, and 33-cm mixed zone with a half-Gaussian depth dependence parameter of 9 cm. Simulations of  and  profiles using these parameters successfully predicted the maximum depth of penetration and the depth of maximum  and  activity. Profiles of successive 1-year hypothetical contaminant pulses were generated using this parameter set to determine the age distribution of sediments at any depth horizon. Because of mixing, sediment particles with a wide range of deposition dates occur at each depth. A sediment chronology was derived from this age distribution to assign the minimum age of deposition and a date of maximum deposition to a depth horizon. The minimum age of sediments in a given horizon is used to estimate the date of first appearance of a contaminant from its maximum depth of penetration. The date of maximum deposition is used to estimate the peak year of input for a contaminant from the depth interval with the highest concentration of that contaminant. Because of the extensive mixing, sediment-bound constituents are rapidly diluted with older material after deposition. In addition, contaminants persist in the mixed zone for many years after deposition. More than 75 years are required to bury 90% of a deposited contaminant below the mixed zone. Reconstructing contaminant inputs is limited to changes occurring on a 20-year time scale. In contrast, mixing is much lower relative to accumulation at a site in San Pablo Bay. Instead, periods of rapid deposition and/or erosion occurred as indicated by frequent sand-silt laminae in the X-radiograph. , , and excess  activity all penetrated to about 120 cm. The distinct maxima in the fallout radionuclides at 105–110 cm yielded overall linear sedimentation rates of 3.9 to 4.1 cm/year, which are comparable to a rate of 4.5±1.5 cm/year derived from the excess  profile.

  17. Plasma sprayed ceria-containing interlayer

    DOEpatents

    Schmidt, Douglas S.; Folser, George R.

    2006-01-10

    A plasma sprayed ceria-containing interlayer is provided. The interlayer has particular application in connection with a solid oxide fuel cell used within a power generation system. The fuel cell advantageously comprises an air electrode, a plasma sprayed interlayer disposed on at least a portion of the air electrode, a plasma sprayed electrolyte disposed on at least a portion of the interlayer, and a fuel electrode applied on at least a portion of the electrolyte.

  18. The Effect of Arrow Mass and Shape on Penetration into a Target

    NASA Astrophysics Data System (ADS)

    Shyam, S.; Gurram, A.; Madireddy, S.

    2016-12-01

    We conducted an archery experiment in order to quantify how aerodynamic design impacted the depth of arrow impact. Research shows that the smaller the surface area of an object, the more easily it travels through the air and the deeper it penetrates a target (Benson 2014). Momentum also affects how far and fast the arrow will go and therefore, how deep it will penetrate into the target. Therefore, a combination of an arrow with greater momentum and better aerodynamics will help the arrow fly faster and penetrate the target deeper. Mass, velocity, momentum, acceleration, force, and drag are the factors that acted on our experiment and produced its results. We hypothesized that the arrow with a thin shaft and pointed arrowhead would penetrate deepest, as opposed to both arrows with no arrowheads or arrows with thick shafts and blunt arrowheads. We tested our hypothesis by having a well-trained archer shoot different types of arrows into a target. We used arrows with shaft lengths of 7 cm and 5.3 cm, coupled with either pointed, blunt, or no arrowhead. We measured the time to target and arrow penetration (in cm) to see which style reached the target the fastest and penetrated the deepest. The results demonstrated that arrows with thin shafts and pointed arrowheads penetrated our target the deepest, followed by arrows with thick shafts and blunt arrowheads. Arrows with thin shafts and blunt arrowheads came after, and arrows with thick shafts and pointed arrowheads came last in depth of penetration. The arrows with no arrowheads either barely penetrated the target, or bounced back. We were able to conclude that the thinner the shaft and the more pointed the arrowhead, the better the arrow cuts the air. This is because, according to the principles of aerodynamics, it creates less drag since the surface area is smaller. However, mass also plays an important role in force through momentum, which also significantly affected our results.

  19. The Flow Induced by the Coalescence of Two Initially Stationary Drops

    NASA Technical Reports Server (NTRS)

    Nobari, M. R.; Tryggvason, G.

    1994-01-01

    The coalescence of two initially stationary drops of different size is investigated by solving the unsteady, axisymmetric Navier-Stokes equations numerically, using a Front-Tracking/Finite Difference method. Initially, the drops are put next to each other and the film between them ruptured. Due to surface tension forces, the drops coalesce rapidly and the fluid from the small drop is injected into the larger one. For low nondimensional viscosity, or Ohnesorge number, little mixing takes place and the small drop fluid forms a blob near the point where the drops touched initially. For low Ohnesorge number, on the other hand, the small drop forms a jet that penetrates far into the large drop. The penetration depth also depends on the size of the drops and shows that for a given fluid of sufficiently low viscosity, there is a maximum penetration depth for intermediate size ratios.

  20. An in vivo confocal Raman study of the delivery of trans retinol to the skin.

    PubMed

    Pudney, Paul D A; Mélot, Mickaël; Caspers, Peter J; Van Der Pol, Andre; Puppels, Gerwin J

    2007-08-01

    The purpose of this study is to monitor in vivo the delivery of trans-retinol into human skin. Delivery to real systems, such as skin, can be extremely difficult to execute and is problematic to confirm and measure. So far, methods for studying the delivery of compounds through the skin are mostly ex vivo and so inherently influence the skin and may not translate directly to the in vivo situation. Raman spectroscopy is uniquely placed to be able to measure biological processes in vivo, and this paper shows that the trans-retinol penetration into the skin can successfully be measured in vivo using this technique. This study measured the volar forearm of volunteers treated with 0.3% trans-retinol in propylene glycol (PG)/ethanol and 0.3% trans-retinol in caprylic/capric acid triglyceride (MYRITOL318), an oil found in skin creams. Solutions were applied and then confocal Raman depth profiles were obtained of the stratum corneum (SC) and into the viable epidermis (VE) up to 10 hours after treatment. Remarkable differences between a penetrating and a nonpenetrating solution can clearly be observed. Treating with trans-retinol in PG/ethanol results in trans-retinol penetrating through the SC and into the VE. Its penetration was also observed to be highly correlated with the depth of penetration of the PG, which is well known as an efficient penetration enhancer. In contrast, while treating with trans-retinol in MYRITOL318, trans-retinol hardly penetrates at all. For the first time, the penetration of trans-retinol has been monitored directly after application of solutions, in vivo without skin excision. Here, the effect of two different solutions on the delivery of trans-retinol into the skin was measured very effectively in vivo by Raman spectroscopy.

  1. A Study to Increase Weld Penetration in P91 Steel During TIG Welding by using Activating Fluxes

    NASA Astrophysics Data System (ADS)

    Singh, Akhilesh Kumar; Kumar, Mayank; Dey, Vidyut; Naresh Rai, Ram

    2017-08-01

    Activated Flux TIG (ATIG) welding is a unique joining process, invented at Paton Institute of electric welding in 1960. ATIG welding process is also known as flux zoned TIG (FZTIG). In this process, a thin layer of activating flux is applied along the line on the surface of the material where the welding is to be carries out. The ATIG process aids to increase the weld penetration in thick materials. Activating fluxes used in the literature show the use of oxides like TiO2, SiO2, Cr2O3, ZnO, CaO, Fe2O3, and MnO2 during welding of steels. In the present study, ATIG was carried out on P-91 steel. Though, Tungsten Inert Gas welding gives excellent quality welds, but the penetration obtained in such welding is still demanding. P91 steel which is ferritic steel is used in high temperature applications. As this steel is, generally, used in thick sections, fabrication of such structures with TIG welding is limited, due to its low depth of penetration. To increase the depth of penetration in P91while welding with ATIG, the role of various oxides were investigated. Apart from the oxides mentioned above, in the present study the role of B2O3, V2O5 and MgO, during ATIG welding of P91 was investigated. It was seen that, compared to TIG welding, there was phenomenal increase in weld penetration during ATIG welding. Amongst all the oxides used in this study, maximum penetration was achieved in case of B2O3. The measurements of weld penetration, bead width and heat affected zone of the weldings were carried out using an image analysis technique.

  2. Interpretation of TOF SIMS depth profiles from ultrashallow high-k dielectric stacks assisted by hybrid collisional computer simulation

    NASA Astrophysics Data System (ADS)

    Ignatova, V. A.; Möller, W.; Conard, T.; Vandervorst, W.; Gijbels, R.

    2005-06-01

    The TRIDYN collisional computer simulation has been modified to account for emission of ionic species and molecules during sputter depth profiling, by introducing a power law dependence of the ion yield as a function of the oxygen surface concentration and by modelling the sputtering of monoxide molecules. The results are compared to experimental data obtained with dual beam TOF SIMS depth profiling of ZrO2/SiO2/Si high-k dielectric stacks with thicknesses of the SiO2 interlayer of 0.5, 1, and 1.5 nm. Reasonable agreement between the experiment and the computer simulation is obtained for most of the experimental features, demonstrating the effects of ion-induced atomic relocation, i.e., atomic mixing and recoil implantation, and preferential sputtering. The depth scale of the obtained profiles is significantly distorted by recoil implantation and the depth-dependent ionization factor. A pronounced double-peak structure in the experimental profiles related to Zr is not explained by the computer simulation, and is attributed to ion-induced bond breaking and diffusion, followed by a decoration of the interfaces by either mobile Zr or O.

  3. Measuring soil frost depth in forest ecosystems with ground penetrating radar

    Treesearch

    John R. Butnor; John L. Campbell; James B. Shanley; Stanley Zarnoch

    2014-01-01

    Soil frost depth in forest ecosystems can be variable and depends largely on early winter air temperatures and the amount and timing of snowfall. A thorough evaluation of ecological responses to seasonally frozen ground is hampered by our inability to adequately characterize the frequency, depth, duration and intensity of soil frost events. We evaluated the use of...

  4. In-situ burning of oil in coastal marshes. 2. Oil spill cleanup efficiency as a function of oil type, marsh type, and water depth.

    PubMed

    Lin, Qianxin; Mendelssohn, Irving A; Carney, Kenneth; Miles, Scott M; Bryner, Nelson P; Walton, William D

    2005-03-15

    In-situ burning of spilled oil, which receives considerable attention in marine conditions, could be an effective way to cleanup wetland oil spills. An experimental in-situ burn was conducted to study the effects of oil type, marsh type, and water depth on oil chemistry and oil removal efficiency from the water surface and sediment. In-situ burning decreased the totaltargeted alkanes and total targeted polycyclic aromatic hydrocarbons (PAHs) in the burn residues as compared to the pre-burn diesel and crude oils. Removal was even more effective for short-chain alkanes and low ring-number PAHs. Removal efficiencies for alkanes and PAHs were >98% in terms of mass balance although concentrations of some long-chain alkanes and high ring-number PAHs increased in the burn residue as compared to the pre-burn oils. Thus, in-situ burning potentially prevents floating oil from drifting into and contaminating adjacent habitats and penetrating the sediment. In addition, in-situ burning significantly removed diesel oil that had penetrated the sediment for all water depths. Furthermore, in-situ burning at a water depth 2 cm below the soil surface significantly removed crude oil that had penetrated the sediment. As a result, in-situ burning may reduce the long-term impacts of oil on benthic organisms.

  5. Laboratory studies on low-energy electron penetration depths into amorphous ice - consequence to astrobiology on icy surfaces

    NASA Astrophysics Data System (ADS)

    Gudipati, M. S.; Li, I.; Lignell, A. A.

    2009-12-01

    Penetration of electrons through icy surfaces plays an important role in radiation processing of solar system icy bodies. However, to date, there is no quantitative data available on the penetration depths of electrons through cryogenic water-ices. Penetration of high-energy incident electrons also results in the in-situ formation of secondary low-energy electrons, such as on the surface of Europa (Herring-Captain et al., 2005; Johnson et al., 2004). Low-energy electrons can also be produced through photoionization process such as on comet surfaces, or through bombardment by solar wind on icy surfaces (Bodewits et al., 2004). Present models use the laboratory penetration data of high-energy (>10 keV) electrons through silicon as a proxy for the ice (Cooper et al., 2001), normalized by the density of the medium. So far no laboratory studies have been conducted that deal with the penetration of electrons through amorphous or crystalline ices. In order to address this issue, we adopted a new experimental strategy by using aromatic molecules as probes. To begin with, we carried out systematic studies on the penetration depths of low-energy electrons (5 eV - 2 keV) through amorphous ice films of defined thickness at cryogenic temperatures (5 - 30 K). The results of these experiments will be analyzed and their relevance to survival of organic material on solar system icy surfaces will be presented. References: Bodewits, D., et al., 2004. X-ray and Far-Ultraviolet emission from comets: Relevant charge exchange processes. Physica Scripta. 70, C17-C20. Cooper, J. F., et al., 2001. Energetic ion and electron irradiation of the icy Galilean satellites. Icarus. 149, 133-159. Herring-Captain, J., et al., 2005. Low-energy (5-250 eV) electron-stimulated desorption of H+, H2+, and H+(H2O)nfrom low-temperature water ice surfaces. Physical Review B. 72, 035431-10. Johnson, R. E., et al., Radiation Effects on the Surfaces of the Galilean Satellites. In: F. Bagenal, et al., Eds.), Jupiter - The Planet, Satellites and Magnetosphere. Cambridge University Press, 2004, pp. 485-512.

  6. A perspective on high-frequency ultrasound for medical applications

    NASA Astrophysics Data System (ADS)

    Mamou, Jonathan; Aristizába, Orlando; Silverman, Ronald H.; Ketterling, Jeffrey A.

    2010-01-01

    High-frequency ultrasound (HFU, >15 MHz) is a rapidly developing field. HFU is currently used and investigated for ophthalmologic, dermatologic, intravascular, and small-animal imaging. HFU offers a non-invasive means to investigate tissue at the microscopic level with resolutions often better than 100 μm. However, fine resolution is only obtained over the limited depth-of-field (˜1 mm) of single-element spherically-focused transducers typically used for HFU applications. Another limitation is penetration depth because most biological tissues have large attenuation at high frequencies. In this study, two 5-element annular arrays with center frequencies of 17 and 34 MHz were fabricated and methods were developed to obtain images with increased penetration depth and depth-of-field. These methods were used in ophthalmologic and small-animal imaging studies. Improved blood sensitivity was obtained when a phantom mimicking a vitreous hemorrhage was imaged. Central-nervous systems of 12.5-day-old mouse embryos were imaged in utero and in three dimensions for the first time.

  7. Pulsed Eddy Current Probe Design Based on Transient Circuit Analysis

    NASA Astrophysics Data System (ADS)

    Cadeau, Trevor J.; Krause, Thomas W.

    2009-03-01

    Probe design parameters affecting depth of penetration of pulsed eddy currents in multi-layer aluminum 2024-T3 were examined. Several probe designs were evaluated for their ability to detect a discontinuity at the bottom of a stack of aluminum plates. The reflection type probes, consisting of pick-up coil and encircling drive coil, were characterized based on their transient response to a square pulse excitation. Probes with longer fundamental time constants, equivalent to a lower driving frequency, generated greater depth of penetration. However, additional factors such as inductive and resistive load, and excessive coil heating were also factors that limited signal-to-noise response with increasing layer thickness.

  8. Microwave (EPR) measurements of the penetration depth measurements of high-Tc superconductors

    NASA Technical Reports Server (NTRS)

    Dalal, N. S.; Rakvin, B.; Mahl, T. A.; Bhalla, A. S.; Sheng, Z. Z.

    1991-01-01

    The use is discussed of electron paramagnetic resonance (EPR) as a quick and easily accessible method for measuring the London penetration depth, lambda for the high T sub c superconductors. The method uses the broadening of the EPR signal, due to the emergence of the magnetic flux lattice, of a free radical adsorbed on the surface of the sample. The second moment, of the EPR signal below T sub c is fitted to the Brandt equation for a simple triangular lattice. The precision of this method compares quite favorably with those of the more standard methods such as micro sup(+)SR, neutron scattering, and magnetic susceptibility.

  9. An EPR methodology for measuring the London penetration depth for the ceramic superconductors

    NASA Technical Reports Server (NTRS)

    Rakvin, B.; Mahl, T. A.; Dalal, N. S.

    1990-01-01

    The use is discussed of electron paramagnetic resonance (EPR) as a quick and easily accessible method for measuring the London penetration depth, lambda for the high T(sub c) superconductors. The method utilizes the broadening of the EPR signal, due to the emergence of the magnetic flux lattice, of a free radical adsorbed on the surface of the sample. The second moment, of the EPR signal below T(sub c) is fitted to the Brandt equation for a simple triangular lattice. The precision of this method compares quite favorably with those of the more standard methods such as micro sup(+)SR, Neutron scattering, and magnetic susceptibility.

  10. Towards multimodal detection of melanoma thickness based on optical coherence tomography and optoacoustics

    NASA Astrophysics Data System (ADS)

    Rahlves, M.; Varkentin, A.; Stritzel, J.; Blumenröther, E.; Mazurenka, M.; Wollweber, M.; Roth, B.

    2016-03-01

    Melanoma skin cancer has one of the highest mortality rates of all types of cancer if not detected at an early stage. The survival rate is highly dependent on its penetration depth, which is commonly determined by histopathology. In this work, we aim at combining optical coherence tomography and optoacoustic as a non-invasive all-optical method to measure the penetration depth of melanoma. We present our recent achievements to setup a handheld multimodal device and also results from first in vivo measurements on healthy and cancerous skin tissue, which are compared to measurements obtained by ultrasound and histopathology.

  11. Carbon monoxide concentration and exposure time effects on the depth of CO penetration and surface color of raw and cooked beef longissimus lumborum steaks.

    PubMed

    Sakowska, A; Guzek, D; Głąbska, D; Wierzbicka, A

    2016-11-01

    This study investigated the influence of carbon monoxide (CO) exposure time (0, 7, 14, and 21days) and concentration in gas mixture on depth of penetration and the surface color of raw and cooked striploin steaks. Seven packaging treatments were evaluated: vacuum, vacuum after 48h of exposure to 0.1%, 0.3% or 0.5% CO (mixed with 30% CO2 and 69.5-69.9% N2), and modified atmosphere packaging (MAP) containing the same gas mixtures. CO penetration depth increased as exposure times and CO concentration in gas mixtures increased (p<0.05). However, the carboxymyoglobin that formed did not always turn brown during thermal treatment. In cooked samples treated with 0.3% and 0.5% CO-MAP, a red carboxymyoglobin border was visible at the cross section, whereas other CO packaging treatments had its partial or total browning. To create a red color in raw and avoid a red boarder in cooked beef, up to 0.5% CO in vacuum packages and only 0.1% for MAP can be recommended. Copyright © 2016 Elsevier Ltd. All rights reserved.

  12. Effect of heavy-ion irradiation on London penetration depth in overdoped Ba(Fe1-xCox)2As2

    NASA Astrophysics Data System (ADS)

    Murphy, J.; Tanatar, M. A.; Kim, Hyunsoo; Kwok, W.; Welp, U.; Graf, D.; Brooks, J. S.; Bud'ko, S. L.; Canfield, P. C.; Prozorov, R.

    2013-08-01

    Irradiation with 1.4 GeV 208Pb ions was used to induce artificial disorder in single crystals of iron-arsenide superconductor Ba(Fe1-xCox)2As2 and to study its effects on the temperature-dependent London penetration depth and transport properties. A study was undertaken on overdoped single crystals with x=0.108 and x=0.127 characterized by notable modulation of the superconducting gap. Irradiation corresponding to the matching fields of Bϕ=6 T and 6.5 T with doses 2.22×1011 d/cm2 and 2.4×1011 d/cm2, respectively, suppresses the superconducting Tc by approximately 0.3 to 1 K. The variation of the low-temperature penetration depth in both pristine and irradiated samples is well described by the power law Δλ(T)=ATn. Irradiation increases the magnitude of the prefactor A and decreases the exponent n, similar to the effect of irradiation in optimally-doped samples. This finding supports universal s± pairing in Ba(Fe1-xCox)2As2 compounds for the entire Co doping range.

  13. Hybrid Welding of 45 mm High Strength Steel Sections

    NASA Astrophysics Data System (ADS)

    Bunaziv, Ivan; Frostevarg, Jan; Akselsen, Odd M.; Kaplan, Alexander F.

    Thick section welding has significant importance for oil and gas industry in low temperature regions. Arc welding is usually employed providing suitable quality joints with acceptable toughness at low temperatures with very limited productivity compared to modern high power laser systems. Laser-arc hybrid welding (LAHW) can enhance the productivity by several times due to higher penetration depth from laser beam and combined advantages of both heat sources. LAHW was applied to join 45 mm high strength steel with double-sided technique and application of metal cored wire. The process was captured by high speed camera, allowing process observation in order to identify the relation of the process stability on weld imperfections and efficiency. Among the results, it was found that both arc power and presence of a gap increased penetration depth, and that higher welding speeds cause unstable processing and limits penetration depth. Over a wide range of heat inputs, the welds where found to consist of large amounts of fine-grained acicular ferrite in the upper 60-75% part of welds. At the root filler wire mixing was less and cooling faster, and thus found to have bainitic transformation. Toughness of deposited welds provided acceptable toughness at -50 °C with some scattering.

  14. Shielding gas selection for increased weld penetration and productivity in GTA welding

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Leinonen, J.I.

    1996-12-31

    The effects of hydrogen and helium additions to the argon shielding gas on GTA weld pool profiles in the case of two austenitic stainless steel sheets 3 mm thick are investigated here in detail. One of the test steels shows good weldability, with a relatively deep, narrow weld pool profile, but the other is poorly weldable, with a shallow, wide weld pool when argon shielding gas is used. Bead-on-plate test welds were produced with arc shields of argon, argon with hydrogen additions of 2 to 18.2% and argon with helium additions of 20 to 80%. The hydrogen additions increases themore » depth of weld penetration in both test steels, but productivity with respect to maximum welding speed can be improved to an accepted level only with steel sheets of good weldability in terms of a relatively high depth/width (D/W) ratio. The depth of penetration in the test steel of good weldability increased somewhat with helium additions and the D/W ratio remained unchanged, while these parameters increased markedly in the poorly weldable steel when a He-20% Ar shielding gas was used and resembled those of the more weldable steel.« less

  15. Application of x-ray nano-particulate markers for the visualization of intermediate layers and interfaces using scanning electron microscopy

    NASA Astrophysics Data System (ADS)

    Bessudnova, Nadezda O.; Bilenko, David I.; Zakharevich, Andrey M.

    2012-03-01

    In this study the methodology of biological sample preparation for dental research using SEM/EDX has been elaborated. (1)The original cutting equipment supplied with 3D user-controlled sample fixation and an adjustable cooling system has been designed and evaluated. (2) A new approach to the root dentine drying procedure has been developed to preserve structure peculiarities of root dentine. (3) A novel adhesive system with embedded X-Ray nanoparticulate markers has been designed. (4)The technique allowing for visualization of bonding resins, interfaces and intermediate layers between tooth hard tissues and restorative materials of endodontically treated teeth using the X-ray nano-particulate markers has been developed and approved. These methods and approaches were used to compare the objective depth of penetration of adhesive systems of different generations in root dentine. It has been shown that the depth of penetration in dentine is less for adhesive systems of generation VI in comparison with bonding resins of generation V, which is in agreement with theoretical evidence. The depth of penetration depends on the correlation between the direction of dentinal tubules, bonding resin delivery and gravity.

  16. Space station integrated wall design and penetration damage control. Task 3: Theoretical analysis of penetration mechanics

    NASA Technical Reports Server (NTRS)

    Bjorkman, M. D.; Geiger, J. D.; Wilhelm, E. E.

    1987-01-01

    The efforts to provide a penetration code called PEN4 version 10 is documented for calculation of projectile and target states for the impact of 2024-T3 aluminum, R sub B 90 1018 steel projectiles and icy meteoroids onto 2024-T3 aluminum plates at impact velocities from 0 to 16 km/s. PEN4 determines whether a plate is perforated by calculating the state of fragmentation of projectile and first plate. Depth of penetration into the second to n sup th plate by fragments resulting from first plate perforation is determined by multiple cratering. The results from applications are given.

  17. Penetration of tungsten-alloy rods into composite ceramic targets: Experiments and 2-D simulations

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Rosenberg, Z.; Dekel, E.; Hohler, V.

    1998-07-10

    A series of terminal ballistics experiments, with scaled tungsten-alloy penetrators, was performed on composite targets consisting of ceramic tiles glued to thick steel backing plates. Tiles of silicon-carbide, aluminum nitride, titanium-dibroide and boron-carbide were 20-80 mm thick, and impact velocity was 1.7 km/s. 2-D numerical simulations, using the PISCES code, were performed in order to simulate these shots. It is shown that a simplified version of the Johnson-Holmquist failure model can account for the penetration depths of the rods but is not enough to capture the effect of lateral release waves on these penetrations.

  18. Endoluminal ultrasound applicator configurations utilizing deployable arrays, reflectors and lenses to augment and dynamically adjust treatment volume, gain, and depth

    NASA Astrophysics Data System (ADS)

    Adams, Matthew S.; Salgaonkar, Vasant A.; Sommer, Graham; Diederich, Chris J.

    2017-02-01

    Endoluminal high-intensity ultrasound offers spatially-precise thermal ablation of tissues adjacent to body lumens, but is constrained in treatment volume and penetration depth by the effective aperture of integrated transducers, which are limited in size to enable delivery through anatomical passages, endoscopic instrumentation, or laparoscopic ports. This study introduced and investigated three distinct endoluminal ultrasound applicator designs that can be delivered in a compact state then deployed or expanded at the target luminal site to increase the effective therapeutic aperture. The first design incorporated an array of planar transducers which could be unfolded at specific angles of convergence between the transducers. Two alternative designs consisted of fixed transducer sources surrounded by an expandable multicompartment balloon that contained acoustic reflector and dynamically-adjustable fluid lenses compartments. Parametric studies of acoustic output were performed across device design parameters via the rectangular radiator and secondary sources methods. Biothermal models were used to simulate resulting temperature distributions in three-dimensional heterogeneous tissue models. Simulations indicate that a deployable transducer array can increase volumetric coverage and penetration depth by 80% and 20%, respectively, while permitting more conformal thermal lesion shapes based on the degree of convergence between the transducers. The applicator designs incorporating reflector and fluid lenses demonstrated enhanced focal gain and penetration depth that increased with the diameter of the expanded reflector-lens balloon. Thermal simulations of assemblies with 12 mm compact profiles and 50 mm expanded balloon diameters demonstrated generation of localized thermal lesions at depths up to 10 cm in liver tissue.

  19. Assessing stapes piston position using computed tomography: a cadaveric study.

    PubMed

    Hahn, Yoav; Diaz, Rodney; Hartman, Jonathan; Bobinski, Matthew; Brodie, Hilary

    2009-02-01

    Temporal bone computed tomographic (CT) scanning in the postoperative stapedotomy patient is inaccurate in assessing stapes piston position within the vestibule. Poststapedotomy patients that have persistent vertigo may undergo CT scanning to assess the position of the stapes piston within the vestibule to rule out overly deep insertion. Vertigo is a recognized complication of the deep piston, and CT evaluation is often recommended. The accuracy of CT scan in this setting is unestablished. Stapedotomy was performed on 12 cadaver ears, and stainless steel McGee pistons were placed. The cadaver heads were then scanned using a fine-cut temporal bone protocol. Temporal bone dissection was performed with microscopic measurement of the piston depth in the vestibule. These values were compared with depth of intravestibular penetration measured on CT scan by 4 independent measurements. The intravestibular penetration as assessed by computed tomography was consistently greater than the value found on cadaveric anatomic dissection. The radiographic bias was greater when piston location within the vestibule was shallower. The axial CT scan measurement was 0.53 mm greater, on average, than the anatomic measurement. On average, the coronal CT measurement was 0.68 mm greater than the anatomic measurement. The degree of overestimation of penetration, however, was highly inconsistent. Standard temporal bone CT scan is neither an accurate nor precise examination of stapes piston depth within the vestibule. We found that CT measurement consistently overstated intravestibular piston depth. Computed tomography is not a useful study in the evaluation of piston depth for poststapedectomy vertigo and is of limited value in this setting.

  20. Geohydrologic data and test results from Well J-13, Nevada Test Site, Nye County, Nevada

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Thordarson, W.

    Well J-13 was drilled to a depth of 1063.1 meters by using air-hydraulic-rotary drilling equipment. The well penetrated 135.6 meters of alluvium of Quaternary and Tertiary age and 927.5 meters of tuff of Tertiary age. The Topopah Spring Member of the Paintbrush Tuff, the principal aquifer, was penetrated from depths of 207.3 to 449.6 meters; a pumping test indicated its transmissivity is 120 meters squared per day, and its hydraulic conductivity is 1.0 meters per day. Below the Topopah Spring Member, tuff units are confining beds; transmissivities range from 0.10 to 4.5 meters squared per day, and hydraulic conductivities rangemore » from 0.0026 to 0.15 meter per day. Confining beds penetrated below a depth of 719.3 meters had the smallest transmissivities (0.10 to 0.63 meter squared per day) and hydraulic conductivities (0.0026 to 0.0056 meter per day). A static water level of about 282.2 meters was measured for the various water-bearing tuff units above a depth of 645.6 meters. Below a depth of 772.7 meters, the static water level was slightly deeper, 283.3 to 283.6 meters. Ground water sampled from well J-13 is a sodium bicarbonate water containing small concentrations of calcium, magnesium, silica, and sulfate, which is a typical analysis of water from tuff. Apparent age of the ground water, derived from carbon-14 age dating, is 9900 years. 15 references, 24 figures, 13 tables.« less

  1. Quantitative estimation of carbonation and chloride penetration in reinforced concrete by laser-induced breakdown spectroscopy

    NASA Astrophysics Data System (ADS)

    Eto, Shuzo; Matsuo, Toyofumi; Matsumura, Takuro; Fujii, Takashi; Tanaka, Masayoshi Y.

    2014-11-01

    The penetration profile of chlorine in a reinforced concrete (RC) specimen was determined by laser-induced breakdown spectroscopy (LIBS). The concrete core was prepared from RC beams with cracking damage induced by bending load and salt water spraying. LIBS was performed using a specimen that was obtained by splitting the concrete core, and the line scan of laser pulses gave the two-dimensional emission intensity profiles of 100 × 80 mm2 within one hour. The two-dimensional profile of the emission intensity suggests that the presence of the crack had less effect on the emission intensity when the measurement interval was larger than the crack width. The chlorine emission spectrum was measured without using the buffer gas, which is usually used for chlorine measurement, by collinear double-pulse LIBS. The apparent diffusion coefficient, which is one of the most important parameters for chloride penetration in concrete, was estimated using the depth profile of chlorine emission intensity and Fick's law. The carbonation depth was estimated on the basis of the relationship between carbon and calcium emission intensities. When the carbon emission intensity was statistically higher than the calcium emission intensity at the measurement point, we determined that the point was carbonated. The estimation results were consistent with the spraying test results using phenolphthalein solution. These results suggest that the quantitative estimation by LIBS of carbonation depth and chloride penetration can be performed simultaneously.

  2. Thermally stable diamond brazing

    DOEpatents

    Radtke, Robert P [Kingwood, TX

    2009-02-10

    A cutting element and a method for forming a cutting element is described and shown. The cutting element includes a substrate, a TSP diamond layer, a metal interlayer between the substrate and the diamond layer, and a braze joint securing the diamond layer to the substrate. The thickness of the metal interlayer is determined according to a formula. The formula takes into account the thickness and modulus of elasticity of the metal interlayer and the thickness of the TSP diamond. This prevents the use of a too thin or too thick metal interlayer. A metal interlayer that is too thin is not capable of absorbing enough energy to prevent the TSP diamond from fracturing. A metal interlayer that is too thick may allow the TSP diamond to fracture by reason of bending stress. A coating may be provided between the TSP diamond layer and the metal interlayer. This coating serves as a thermal barrier and to control residual thermal stress.

  3. Tunneling Photocurrent Assisted by Interlayer Excitons in Staggered van der Waals Hetero-Bilayers.

    PubMed

    Luong, Dinh Hoa; Lee, Hyun Seok; Neupane, Guru Prakash; Roy, Shrawan; Ghimire, Ganesh; Lee, Jin Hee; Vu, Quoc An; Lee, Young Hee

    2017-09-01

    Vertically stacked van der Waals (vdW) heterostructures have been suggested as a robust platform for studying interfacial phenomena and related electric/optoelectronic devices. While the interlayer Coulomb interaction mediated by the vdW coupling has been extensively studied for carrier recombination processes in a diode transport, its correlation with the interlayer tunneling transport has not been elucidated. Here, a contrast is reported between tunneling and drift photocurrents tailored by the interlayer coupling strength in MoSe 2 /MoS 2 hetero-bilayers (HBs). The interfacial coupling modulated by thermal annealing is identified by the interlayer phonon coupling in Raman spectra and the emerging interlayer exciton peak in photoluminescence spectra. In strongly coupled HBs, positive photocurrents are observed owing to the inelastic band-to-band tunneling assisted by interlayer excitons that prevail over exciton recombinations. By contrast, weakly coupled HBs exhibit a negative photovoltaic diode behavior, manifested as a drift current without interlayer excitonic emissions. This study sheds light on tailoring the tunneling transport for numerous optoelectronic HB devices. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

  4. Calculating maximum frost depths at Mn/ROAD : winters 1993-94, 1994-95 and 1995-96

    DOT National Transportation Integrated Search

    1997-03-01

    This effort involved calculating maximum frost penetration depths for each of the 40 test cells at Mn/ROAD, the Minnesota Department of Transportation's pavement testing facility, for the 1993-94, 1994-95, and 1995-96 winters. The report compares res...

  5. Effects of a Ta interlayer on the phase transition of TiSi2 on Si(111)

    NASA Astrophysics Data System (ADS)

    Jeon, Hyeongtag; Jung, Bokhee; Kim, Young Do; Yang, Woochul; Nemanich, R. J.

    2000-09-01

    This study examines the effects of a thin Ta interlayer on the formation of TiSi2 on Si(111) substrate. The Ta interlayer was introduced by depositing Ta and Ti films sequentially on an atomically clean Si(111) substrate in an ultrahigh vacuum (UHV) system. Samples of 100 Å Ti with 5 and 10 Å Ta interlayers were compared to similar structures without an interlayer. After deposition, the substrates were annealed for 10 min, in situ, at temperatures between 500 and 750 °C in 50 °C increments. The TiSi2 formation with and without the Ta interlayer was analyzed with an X-ray diffractometer, Auger electron spectroscopy (AES), Scanning electron microscopy (SEM), transmission electron microscopy (TEM), and a four-point probe. The AES analysis data showed a 1:2 ratio of Ti:Si in the Ti-silicide layer and indicated that the Ta layer remained at the interface between TiSi2 and the Si(111) substrate. The C 49-C 54 TiSi2 phase transition temperature was lowered by ˜200 °C. The C 49-C 54 TiSi2 phase transition temperature was 550 °C for the samples with a Ta interlayer and was 750 °C for the samples with no Ta interlayer. The sheet resistance of the Ta interlayered Ti silicide showed lower values of resistivity at low temperatures which indicated the change in phase transition temperature. The C 54 TiSi2 displayed different crystal orientation when the Ta interlayer was employed. The SEM and TEM micrographs showed that the TiSi2 with a Ta interlayer significantly suppressed the tendency to islanding and surface agglomeration.

  6. Sealer penetration into dentinal tubules in the presence or absence of smear layer: a confocal laser scanning microscopic study.

    PubMed

    Kuçi, Astrit; Alaçam, Tayfun; Yavaş, Ozer; Ergul-Ulger, Zeynep; Kayaoglu, Guven

    2014-10-01

    The aim of this study was to test the dentinal tubule penetration of AH26 (Dentsply DeTrey, Konstanz, Germany) and MTA Fillapex (Angelus, Londrina, PR, Brazil) in instrumented root canals obturated by using cold lateral compaction or warm vertical compaction techniques in either the presence or absence of the smear layer. Forty-five extracted single-rooted human mandibular premolar teeth were used. The crowns were removed, and the root canals were instrumented by using the Self-Adjusting File (ReDent-Nova, Ra'anana, Israel) with continuous sodium hypochlorite (2.6%) irrigation. Final irrigation was either with 5% EDTA or with sodium hypochlorite. The canals were dried and obturated by using rhodamine B-labeled AH26 or MTA Fillapex in combination with the cold lateral compaction or the warm vertical compaction technique. After setting, the roots were sectioned horizontally at 4-, 8-, and 12-mm distances from the apical tip. On each section, sealer penetration in the dentinal tubules was measured by using confocal laser scanning microscopy. Regardless of the usage of EDTA, MTA Fillapex, compared with AH26, was associated with greater sealer penetration when used with the cold lateral compaction technique, and, conversely, AH26, compared with MTA Fillapex, was associated with greater sealer penetration when used with the warm vertical compaction technique (P < .05). Removal of the smear layer increased the penetration depth of MTA Fillapex used with the cold lateral compaction technique (P < .05); however, it had no significant effect on the penetration depth of AH26. Greater sealer penetration could be achieved with either the MTA Fillapex-cold lateral compaction combination or with the AH26-warm vertical compaction combination. Smear layer removal was critical for the penetration of MTA Fillapex; however, the same did not hold for AH26. Copyright © 2014 American Association of Endodontists. Published by Elsevier Inc. All rights reserved.

  7. Ultrasound-mediated transdermal drug delivery of fluorescent nanoparticles and hyaluronic acid into porcine skin in vitro

    NASA Astrophysics Data System (ADS)

    Wang, Huan-Lei; Fan, Peng-Fei; Guo, Xia-Sheng; Tu, Juan; Ma, Yong; Zhang, Dong

    2016-12-01

    Transdermal drug delivery (TDD) can effectively bypass the first-pass effect. In this paper, ultrasound-facilitated TDD on fresh porcine skin was studied under various acoustic parameters, including frequency, amplitude, and exposure time. The delivery of yellow-green fluorescent nanoparticles and high molecular weight hyaluronic acid (HA) in the skin samples was observed by laser confocal microscopy and ultraviolet spectrometry, respectively. The results showed that, with the application of ultrasound exposures, the permeability of the skin to these markers (e.g., their penetration depth and concentration) could be raised above its passive diffusion permeability. Moreover, ultrasound-facilitated TDD was also tested with/without the presence of ultrasound contrast agents (UCAs). When the ultrasound was applied without UCAs, low ultrasound frequency will give a better drug delivery effect than high frequency, but the penetration depth was less likely to exceed 200 μm. However, with the help of the ultrasound-induced microbubble cavitation effect, both the penetration depth and concentration in the skin were significantly enhanced even more. The best ultrasound-facilitated TDD could be achieved with a drug penetration depth of over 600 μm, and the penetration concentrations of fluorescent nanoparticles and HA increased up to about 4-5 folds. In order to get better understanding of ultrasound-facilitated TDD, scanning electron microscopy was used to examine the surface morphology of skin samples, which showed that the skin structure changed greatly under the treatment of ultrasound and UCA. The present work suggests that, for TDD applications (e.g., nanoparticle drug carriers, transdermal patches and cosmetics), protocols and methods presented in this paper are potentially useful. Project partially supported by the National Natural Science Foundation of China (Grant Nos. 81127901, 81227004, 81473692, 81673995, 11374155, 11574156, 11274170, 11274176, 11474001, 11474161, 11474166, and 11674173), the Natural Science Foundation of Jiangsu Province, China (Grant No. BK2011812), the Fundamental Research Funds for the Central Universities, and the National High-Tech Research and Development Program of China (Grant No. 2012AA022702).

  8. Role of low-temperature AlGaN interlayers in thick GaN on silicon by metalorganic vapor phase epitaxy

    NASA Astrophysics Data System (ADS)

    Fritze, S.; Drechsel, P.; Stauss, P.; Rode, P.; Markurt, T.; Schulz, T.; Albrecht, M.; Bläsing, J.; Dadgar, A.; Krost, A.

    2012-06-01

    Thin AlGaN interlayers have been grown into a thick GaN stack on Si substrates to compensate tensile thermal stress and significantly improve the structural perfection of the GaN. In particular, thicker interlayers reduce the density in a-type dislocations as concluded from x-ray diffraction (XRD) measurements. Beyond an interlayer thickness of 28 nm plastic substrate deformation occurs. For a thick GaN stack, the first two interlayers serve as strain engineering layers to obtain a crack-free GaN structure, while a third strongly reduces the XRD ω-(0002)-FWHM. The vertical strain and quality profile determined by several XRD methods demonstrates the individual impact of each interlayer.

  9. A 3D conductive carbon interlayer with ultrahigh adsorption capability for lithium-sulfur batteries

    NASA Astrophysics Data System (ADS)

    Zhao, Qian; Zhu, Qizhen; An, Yabin; Chen, Renjie; Sun, Ning; Wu, Feng; Xu, Bin

    2018-05-01

    To improve the cycling performance of the Li-S batteries, a 3D interwoven hollow interlayer with extremely high electrolyte adsorption capability up to 9.64 g g-1 was simply prepared by carbonization of cotton fabric (CCF). For comparison, an interlayer coated on separator was obtained by the slurry-coating method of powdery CCF. The key role of the adsorption capability is confirmed by comparing the electrochemical performance of Li-S batteries with these two interlayers. In the Li-S batteries with 3D CCF interlayer, massive dissolved polysulfides, together with the electrolyte, can be adsorbed and confined in the 3D CCF interlayer, providing substantial extra active sites and alleviating the shuttle effect effectively. As a result, the Li-S batteries with 3D CCF interlayer show much enhanced utilization of active materials (1346.9 mAh g-1 at 0.1C), prolonged cycle life (capacity retention of 80% after 100 cycles), and improved rate performance (553.2 mAh g-1 at 4C). Even for cathodes with high sulfur loading of 5 mg cm-2, the cells with 3D CCF interlayer perform a high capacity of 1085 mAh g-1 and retain 870.6 mAh g-1 after 75 cycles at 0.5 mA cm-2. These results not only provide a sustainable, low cost and easy-prepared 3D CCF interlayer, but also offer a promising strategy based on interlayer with high adsorption capability in designing high-performance Li-S batteries.

  10. Penetration analysis of projectile with inclined concrete target

    NASA Astrophysics Data System (ADS)

    Kim, S. B.; Kim, H. W.; Yoo, Y. H.

    2015-09-01

    This paper presents numerical analysis result of projectile penetration with concrete target. We applied dynamic material properties of 4340 steels, aluminium and explosive for projectile body. Dynamic material properties were measured with static tensile testing machine and Hopkinson pressure bar tests. Moreover, we used three concrete damage models included in LS-DYNA 3D, such as SOIL_CONCRETE, CSCM (cap model with smooth interaction) and CONCRETE_DAMAGE (K&C concrete) models. Strain rate effect for concrete material is important to predict the fracture deformation and shape of concrete, and penetration depth for projectiles. CONCRETE_DAMAGE model with strain rate effect also applied to penetration analysis. Analysis result with CSCM model shows good agreement with penetration experimental data. The projectile trace and fracture shapes of concrete target were compared with experimental data.

  11. Solar radiation, phytoplankton pigments and the radiant heating of the equatorial Pacific warm pool

    NASA Technical Reports Server (NTRS)

    Siegel, David A.; Ohlmann, J. Carter; Washburn, Libe; Bidigare, Robert R.; Nosse, Craig T.; Fields, Erik; Zhou, Yimei

    1995-01-01

    Recent optical, physical, and biological oceanographic observations are used to assess the magnitude and variability of the penetrating flux of solar radiation through the mixed layer of the warm water pool (WWP) of the western equatorial Pacific Ocean. Typical values for the penetrative solar flux at the climatological mean mixed layer depth for the WWP (30 m) are approx. 23 W/sq m and are a large fraction of the climatological mean net air-sea heat flux (approx. 40 W/sq m). The penetrating solar flux can vary significantly on synoptic timescales. Following a sustained westerly wind burst in situ solar fluxes were reduced in response to a near tripling of mixed layer phytoplankton pigment concentrations. This results in a reduction in the penetrative flux at depth (5.6 W/sq m at 30 m) and corresponds to a biogeochemically mediated increase in the mixed layer radiant heating rate of 0.13 C per month. These observations demonstrate a significant role of biogeochemical processes on WWP thermal climate. We speculate that this biogeochemically mediated feedback process may play an important role in enhancing the rate at which the WWP climate system returns to normal conditions following a westerly wind burst event.

  12. Large Frequency Change with Thickness in Interlayer Breathing Mode—Significant Interlayer Interactions in Few Layer Black Phosphorus

    NASA Astrophysics Data System (ADS)

    Luo, Xin; Lu, Xin; Koon, Gavin Kok Wai; Castro Neto, Antonio H.; Özyilmaz, Barbaros; Xiong, Qihua; Quek, Su Ying

    2015-06-01

    Bulk black phosphorus (BP) consists of puckered layers of phosphorus atoms. Few-layer BP, obtained from bulk BP by exfoliation, is an emerging candidate as a channel material in post-silicon electronics. A deep understanding of its physical properties and its full range of applications are still being uncovered. In this paper, we present a theoretical and experimental investigation of phonon properties in few-layer BP, focusing on the low-frequency regime corresponding to interlayer vibrational modes. We show that the interlayer breathing mode A3g shows a large redshift with increasing thickness; the experimental and theoretical results agreeing well. This thickness dependence is two times larger than that in the chalcogenide materials such as few-layer MoS2 and WSe2, because of the significantly larger interlayer force constant and smaller atomic mass in BP. The derived interlayer out-of-plane force constant is about 50% larger than that in graphene and MoS2. We show that this large interlayer force constant arises from the sizable covalent interaction between phosphorus atoms in adjacent layers, and that interlayer interactions are not merely of the weak van der Waals type. These significant interlayer interactions are consistent with the known surface reactivity of BP, and have been shown to be important for electric-field induced formation of Dirac cones in thin film BP.

  13. Large Frequency Change with Thickness in Interlayer Breathing Mode--Significant Interlayer Interactions in Few Layer Black Phosphorus.

    PubMed

    Luo, Xin; Lu, Xin; Koon, Gavin Kok Wai; Castro Neto, Antonio H; Özyilmaz, Barbaros; Xiong, Qihua; Quek, Su Ying

    2015-06-10

    Bulk black phosphorus (BP) consists of puckered layers of phosphorus atoms. Few-layer BP, obtained from bulk BP by exfoliation, is an emerging candidate as a channel material in post-silicon electronics. A deep understanding of its physical properties and its full range of applications are still being uncovered. In this paper, we present a theoretical and experimental investigation of phonon properties in few-layer BP, focusing on the low-frequency regime corresponding to interlayer vibrational modes. We show that the interlayer breathing mode A(3)g shows a large redshift with increasing thickness; the experimental and theoretical results agree well. This thickness dependence is two times larger than that in the chalcogenide materials, such as few-layer MoS2 and WSe2, because of the significantly larger interlayer force constant and smaller atomic mass in BP. The derived interlayer out-of-plane force constant is about 50% larger than that of graphene and MoS2. We show that this large interlayer force constant arises from the sizable covalent interaction between phosphorus atoms in adjacent layers and that interlayer interactions are not merely of the weak van der Waals type. These significant interlayer interactions are consistent with the known surface reactivity of BP and have been shown to be important for electric-field induced formation of Dirac cones in thin film BP.

  14. Probing the Interlayer Exciton Physics in a MoS2/MoSe2/MoS2 van der Waals Heterostructure.

    PubMed

    Baranowski, M; Surrente, A; Klopotowski, L; Urban, J M; Zhang, N; Maude, D K; Wiwatowski, K; Mackowski, S; Kung, Y C; Dumcenco, D; Kis, A; Plochocka, P

    2017-10-11

    Stacking atomic monolayers of semiconducting transition metal dichalcogenides (TMDs) has emerged as an effective way to engineer their properties. In principle, the staggered band alignment of TMD heterostructures should result in the formation of interlayer excitons with long lifetimes and robust valley polarization. However, these features have been observed simultaneously only in MoSe 2 /WSe 2 heterostructures. Here we report on the observation of long-lived interlayer exciton emission in a MoS 2 /MoSe 2 /MoS 2 trilayer van der Waals heterostructure. The interlayer nature of the observed transition is confirmed by photoluminescence spectroscopy, as well as by analyzing the temporal, excitation power, and temperature dependence of the interlayer emission peak. The observed complex photoluminescence dynamics suggests the presence of quasi-degenerate momentum-direct and momentum-indirect bandgaps. We show that circularly polarized optical pumping results in long-lived valley polarization of interlayer exciton. Intriguingly, the interlayer exciton photoluminescence has helicity opposite to the excitation. Our results show that through a careful choice of the TMDs forming the van der Waals heterostructure it is possible to control the circular polarization of the interlayer exciton emission.

  15. Shape-Dependent Skin Penetration of Silver Nanoparticles: Does It Really Matter?

    PubMed Central

    Tak, Yu Kyung; Pal, Sukdeb; Naoghare, Pravin K.; Rangasamy, Sabarinathan; Song, Joon Myong

    2015-01-01

    Advancements in nano-structured materials have facilitated several applications of nanoparticles (NPs). Skin penetration of NPs is a crucial factor for designing suitable topical antibacterial agents with low systemic toxicity. Available reports focus on size-dependent skin penetration of NPs, mainly through follicular pathways. Herein, for the first time, we demonstrate a proof-of-concept study that entails variations in skin permeability and diffusion coefficients, penetration rates and depth-of-penetration of differently shaped silver NPs (AgNPs) via intercellular pathways using both in vitro and in vivo models. The antimicrobial activity of AgNPs is known. Different shapes of AgNPs may exhibit diverse antimicrobial activities and skin penetration capabilities depending upon their active metallic facets. Consideration of the shape dependency of AgNPs in antimicrobial formulations could help developing an ideal topical agent with the highest efficacy and low systemic toxicity. PMID:26584777

  16. First-principles study on interlayer state in alkali and alkaline earth metal atoms intercalated bilayer graphene

    NASA Astrophysics Data System (ADS)

    Kaneko, Tomoaki; Saito, Riichiro

    2017-11-01

    Energetics and electronic structures of alkali metal (Li, Na, K, Rb, and Cs) and alkaline earth metal (Be, Mg, Ca, Sr, and Ba) atoms intercalated bilayer graphene are systematically investigated using first-principles calculations based on density functional theory. Formation of alkali and alkaline earth metal atoms intercalated bilayer graphene is exothermic except for Be and Mg. The interlayer state between two graphene layers is occupied for K, Rb, Cs, Ca, Sr, and Ba. We find that the energetic position of the interlayer states between bilayer graphene monotonically shifts downward with increasing of interlayer distance. The interlayer distances of more than 4.5 Å and 4.0 Å, respectively, are necessary for the occupation of the interlayer state in bilayer graphene for alkali and alkaline earth metal atoms, which is almost independent of the intercalant metal species. We discuss the relevance to occurrence of superconductivity for the metal intercalated bilayer graphene in terms of the occupation of the interlayer state and the phonon frequency of metal ions.

  17. The graphene oxide membrane immersing in the aqueous solution studied by electrochemical impedance spectroscopy

    NASA Astrophysics Data System (ADS)

    Zhang, Yongjing; Chen, Zhe; Yao, Lei; Wang, Xiao; Fu, Ping; Lin, Zhidong

    2018-04-01

    The interlayer spacing of graphene oxide (GO) is a key property for GO membrane. To probe the variation of interlayer spacing of the GO membrane immersing in KCl aqueous solution, electrochemical impedance spectroscopy (EIS), x-ray diffraction (XRD) and computational calculation was utilized in this study. The XRD patterns show that soaking in KCl aqueous solution leads to an increase of interlayer spacing of GO membrane. And the EIS results indicate that during the immersing process, the charge transfer resistance of GO membrane decreases first and then increases. Computational calculation confirms that intercalated water molecules can result in an increase of interlayer spacing of GO membrane, while the permeation of K+ ions would lead to a decrease of interlayer spacing. All the results are in agreement with each other. It suggests that during the immersing process, the interlayer spacing of GO enlarges first and then decreases. EIS can be a promisingly online method for examining the interlayer spacing of GO in the aqueous solution.

  18. A numerically optimized active shield for improved transcranial magnetic stimulation targeting.

    PubMed

    Hernandez-Garcia, Luis; Hall, Timothy; Gomez, Luis; Michielssen, Eric

    2010-10-01

    Transcranial magnetic stimulation (TMS) devices suffer of poor targeting and penetration depth. A new approach to designing TMS coils is introduced in order to improve the focus of the stimulation region through the use of actively shielded probes. Iterative optimization techniques were used to design different active shielding coils for TMS probes. The new approach aims to increase the amount of energy deposited in a thin cylindrical region below the probe relative to the energy deposited elsewhere in the region ("sharpness"), whereas, simultaneously increase the induced electric field deep in the target region relative to the surface ("penetration"). After convergence, the resulting designs showed that there is a clear tradeoff between sharpness and penetration that can be controlled by the choice of a tuning parameter. The resulting designs were tested on a realistic human head conductivity model, taking the contribution from surface charges into account. The design of choice reduced penetration depths by 16.7%. The activated surface area was reduced by 24.1% and the volume of the activation was reduced from 42.6% by the shield. Restoring the lost penetration could be achieved by increasing the total power to the coil by 16.3%, but in that case, the stimulated volume reduction was only 13.1% and there was a slight increase in the stimulated surface area (2.9%). Copyright © 2010 Elsevier Inc. All rights reserved.

  19. Electron microscopy investigations of purity of AlN interlayer in Al{sub x}Ga{sub 1-x}N/GaN heterostructures grown by plasma assisted molecular beam epitaxy

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Sridhara Rao, D. V.; Jain, Anubha; Lamba, Sushil

    2013-05-13

    The electron microscopy was used to characterize the AlN interlayer in Al{sub x}Ga{sub 1-x}N/AlN/GaN heterostructures grown by plasma assisted molecular beam epitaxy (PAMBE). We show that the AlN interlayer grown by PAMBE is without gallium and oxygen incorporation and the interfaces are coherent. The AlN interlayer has the ABAB stacking of lattice planes as expected for the wurtzite phase. High purity of AlN interlayer with the ABAB stacking leads to larger conduction band offset along with stronger polarization effects. Our studies show that the origin of lower sheet resistance obtained by PAMBE is the purity of AlN interlayer.

  20. Effects of the F₄TCNQ-Doped Pentacene Interlayers on Performance Improvement of Top-Contact Pentacene-Based Organic Thin-Film Transistors.

    PubMed

    Fan, Ching-Lin; Lin, Wei-Chun; Chang, Hsiang-Sheng; Lin, Yu-Zuo; Huang, Bohr-Ran

    2016-01-13

    In this paper, the top-contact (TC) pentacene-based organic thin-film transistor (OTFT) with a tetrafluorotetracyanoquinodimethane (F₄TCNQ)-doped pentacene interlayer between the source/drain electrodes and the pentacene channel layer were fabricated using the co-evaporation method. Compared with a pentacene-based OTFT without an interlayer, OTFTs with an F₄TCNQ:pentacene ratio of 1:1 showed considerably improved electrical characteristics. In addition, the dependence of the OTFT performance on the thickness of the F₄TCNQ-doped pentacene interlayer is weaker than that on a Teflon interlayer. Therefore, a molecular doping-type F₄TCNQ-doped pentacene interlayer is a suitable carrier injection layer that can improve the TC-OTFT performance and facilitate obtaining a stable process window.

  1. An Analytical Means of Determining Mass Loss from High Velocity Rigid Penetrators based on the Thermodynamic and Mechanical Properties of the Penetrator and Target

    NASA Astrophysics Data System (ADS)

    Foster, Joseph C., Jr.; Jones, S. E.; Rule, William; Toness, Odin

    1999-06-01

    Sub-scale experimentation is commonly used as a cost-effective means of conducting terminal ballistics research. Analytical models of the penetration process focus on calculating the depth of penetration based on target density, target strength represented by the unconfined compressive-strength (f”c), the areal density of the penetrator (W/A), and the impact velocity.1 Forrestal, et. al. have documented the mass loss from the penetrator during the penetration process and employed improved equations of motion.2 Various researchers have investigated the upper limits of rigid body penetration and identified the onset of instabilities.3 In an effort to better understand the physical processes associated with this instability, experimental techniques have been developed to capture the details of the penetrator and target and subject them to microscopic analysis.4 These results have served as motivation to explore new forms for the physics included in the penetration equation as a means of identifying the processes associated with high velocity instability. We have included target shear and nose friction in the formulation of the fundamental load function expressions.5 When the resulting equations of motion are integrated and combined with the thermodynamics indicated by microscopic analysis, methods are identified to calculated penetrator mass loss. A comparison of results with experimental data serves as an indicator of the thermodynamic state variables associated with the quasi-steady state penetrator target interface conditions. 1 Young, C. W. , “Depth Predictions for Earth Penetrating Projectiles,” Journal of Soil Mechanics and Foundations, Division of ASCE, May 1998 pp 803-817 2. M.J. Forrestal, D.J. Frew, S.J. Hanchak, amd Brar, “ Pentration of Grout and Concrete Targets with Ogive-Nose Steel Projectiles,” Inrt. J. Impact Engng. Vol 18, pp. 465-476,1996 3. Andrew J. Piekutowski, Michael J. Forrestal, Kevin L. Poormon, and Thomas L. Warren, “Penetration of 6061-T6511 Aluminum Target by Ogive-Nose Projectiles with Striking Velocities between 0.5 and 3.0 Km/s,’ Int. J. Impact Engng. Vol. 23, 1999 4. Joseph C. Foster, Jr., Frank Christopher, Leo Wilson, Dave Jerome, Odin Toness, “Observations concerning the Damage in Concrete Subjected to High Rates of Loading,” Proceedings of Plasticity ’99, Cancun Mexico, 4-14 January 1999 5. S.E. Jones, Joseph C. Foster, Jr. , and William K Rule, “Estimating Target Strength from Penetration Experiments,” (submitted for publication)

  2. Magnetic penetration depth and flux dynamics in single-crystal Bi2Sr2CaCu2O8+δ

    NASA Astrophysics Data System (ADS)

    Harshman, D. R.; Kleiman, R. N.; Inui, M.; Espinosa, G. P.; Mitzi, D. B.; Kapitulnik, A.; Pfiz, T.; Williams, D. Ll.

    1991-11-01

    The muon-spin-relaxation technique has been used to study vortex dynamics in single-phase superconducting single crystals of Bi2Sr2CaCu2O8+δ (Tc~=90 K). The data indicate motional narrowing of the internal field distribution due to vortex motion (on a time scale comparable to the muon lifetime). A field-dependent lattice transition is also observed at Tx~30 K, as evidenced by the onset of an asymmetric line shape below Tx. Narrowing arising from disordering of the vortices along [001] is also discussed with reference to its effect on the measured penetration depth.

  3. Evidence of nodes in the order parameter of the superconducting doped topological insulator Nb x Bi 2 Se 3 via penetration depth measurements

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Smylie, M. P.; Claus, H.; Welp, U.

    2016-11-01

    The low-temperature variation of the London penetration depth lambda(T) in the candidate topological superconductor NbxBi2Se3 (x = 0.25) is reported for several crystals. The measurements were carried out by means of a tunnel-diode oscillator technique in both field orientations (H-rf || c and H-rf || ab planes). All samples exhibited power-law behavior at low temperatures (Delta lambda similar to T-2) clearly indicating the presence of point nodes in the superconducting order parameter. The results presented here are consistent with a nematic odd-parity spin-triplet E-u pairing state in NbxBi2Se3.

  4. Kerr-gated picosecond Raman spectroscopy and Raman photon migration of equine bone tissue with 400-nm excitation

    NASA Astrophysics Data System (ADS)

    Morris, Michael D.; Goodship, Allen E.; Draper, Edward R. C.; Matousek, Pavel; Towrie, Michael; Parker, Anthony W.

    2004-07-01

    We show that Raman spectroscopy with visible lasers, even in the deep blue is possible with time-gated Raman spectroscopy. A 4 picosec time gate allows efficient fluorescence rejection, up to 1000X, and provides almost background-free Raman spectra with low incident laser power. The technology enables spectroscopy with better than 10X higher scattering efficiency than is possible with the NIR (785 nm and 830 nm) lasers that are conventionally used. Raman photon migration is shown to allow depth penetration. We show for the first time that Kerr-gated Raman spectra of bone tissue with blue laser excitation enables both fluorescence rejection and depth penetration.

  5. A millimeter-wave reflectometer for whole-body hydration sensing

    NASA Astrophysics Data System (ADS)

    Zhang, W.-D.; Brown, E. R.

    2016-05-01

    This paper demonstrates a non-invasive method to determine the hydration level of human skin by measuring the reflectance of W-band (75-110 GHz) and Ka-band (26-40 GHz) radiation. Ka-band provides higher hydration accuracy (<1%) and greater depth of penetration (> 1 mm), thereby allowing access to the important dermis layer of skin. W-band provides less depth of penetration but finer spatial resolution (~2 mm). Both the hydration sensing concept and experimental results are presented here. The goal is to make a human hydration sensor that is 1% accurate or better, operable by mechanically scanning, and fast enough to measure large areas of the human body in seconds.

  6. Results of geophysical surveys of glacial deposits near a former waste-disposal site, Nashua, New Hampshire

    USGS Publications Warehouse

    Ayotte, Joseph D.; Dorgan, Tracy H.

    1995-01-01

    Geophysical investigations were done near a former waste-disposal site in Nashua, New Hampshire to determine the thickness and infer hydraulic characteristics of the glacial sediments that underlie the area. Approximately 5 miles of ground- penetrating radar (GPR) data were collected in the study area by use of dual-80 Megahertz antennas. Three distinct radar-reflection signatures were evident from the data and are interpreted to represent (1) glacial lake-bottom sediments, (2) coarse sand and gravel and (or) sandy glacial till, and (3) bedrock. The GPR signal penetrated as much as 70 feet of sediment in coarse-grained areas, but penetration depth was generally less than 40 feet in extensive areas of fine-grained deposits. Geologic features were evident in many of the profiles. Glacial-lake-bottom sediments were the most common features identified. Other features include deltas deposited in glacial Lake Nashua and lobate fans of sediment deposited subaqueously at the distal end of deltaic sediments. Cross-bedded sands were often identifiable in the deltaic sediments. Seismic-refraction data were also collected at five of the GPR data sites. In most cases, depths to the water table and to the till and (or) bedrock surface indicated by the seismic-refraction data compared favorably with depths calculated from the GPR data. Test holes were drilled at three locations to determine the true depths to radar reflectors and to determine the types of geologic material represented by the various reflectors.

  7. Shuttle Imaging Radar - Physical controls on signal penetration and subsurface scattering in the Eastern Sahara

    NASA Technical Reports Server (NTRS)

    Schaber, G. G.; Mccauley, J. F.; Breed, C. S.; Olhoeft, G. R.

    1986-01-01

    Interpretation of Shuttle Imaging Radar-A (SIR-A) images by McCauley et al. (1982) dramatically changed previous concepts of the role that fluvial processes have played over the past 10,000 to 30 million years in shaping this now extremely flat, featureless, and hyperarid landscape. In the present paper, the near-surface stratigraphy, the electrical properties of materials, and the types of radar interfaces found to be responsible for different classes of SIR-A tonal response are summarized. The dominant factors related to efficient microwave signal penetration into the sediment blanket include (1) favorable distribution of particle sizes, (2) extremely low moisture content and (3) reduced geometric scattering at the SIR-A frequency (1.3 GHz). The depth of signal penetration that results in a recorded backscatter, here called 'radar imaging depth', was documented in the field to be a maximum of 1.5 m, or 0.25 of the calculated 'skin depth', for the sediment blanket. Radar imaging depth is estimated to be between 2 and 3 m for active sand dune materials. Diverse permittivity interfaces and volume scatterers within the shallow subsurface are responsible for most of the observed backscatter not directly attributable to grazing outcrops. Calcium carbonate nodules and rhizoliths concentrated in sandy alluvium of Pleistocene age south of Safsaf oasis in south Egypt provide effective contrast in premittivity and thus act as volume scatterers that enhance SIR-A portrayal of younger inset stream channels.

  8. [Comments on the paper by D. Tausch et al. Experiments on the penetration power of various bullets into skin and muscle tissue (author's transl)].

    PubMed

    Dammermann, W

    1979-07-17

    The objections in the following comments on a recent paper by Tausch et al. (1978) are raised principally to the points that the mass of the projectile is given an importance for the penetration which is not justified, and that the inherent uncertainty of the measurement data and the scope of validity of the empirical formulas are not sufficiently taken into account. The discussion on the process of penetration and a discontinuity of the depth of penetration as a function of the velocity of the bullet is of fundamental significance, with consequences for the definition of the critical velocity.

  9. [Morphometric anatomic study and clinical significance of lunate fossa].

    PubMed

    Aldemir, Cengiz; Önder, Merve; Doğan, Ali; Duygun, Fatih; Oğuz, Nurettin

    2015-01-01

    This study aims to investigate the depth, transverse and sagittal diameters of lunate fossa which is a significant structure of the wrist in terms of reducing the risk for volar plate screws, which are administered in distal radius fractures, from penetrating into the joint. Depth, transverse and sagittal diameters of lunate fossa in 50 right and 50 left adult dried radius bones without distal tip damage were measured by using MicroscribeG2X from the MicroScribe G series. Mean lunate fossa depth: left 2.419886±0.51 mm/right 2.543052±0.78 mm, mean lunate fossa sagittal diameter: left 19.656±1.57 mm/right 18.796±1.53 mm, mean lunate fossa transverse diameter: left 11.382±0.65 mm/right 11.106±0.91 mm. There was no statistically significant difference between right and left depth values of lunate fossa (p=0.320), whereas there was statistically significant difference between right and left transverse and sagittal diameters (p=0.006, p=0.048). Measurements involving depth of lunate fossa may guide the development of new anatomic plates and decrease complications like the penetration of screw into joint whilst volar plate administrations.

  10. Effect of particle size on the experimental dissolution and auto-aluminization processes of K-vermiculite

    NASA Astrophysics Data System (ADS)

    Viennet, Jean-Christophe; Hubert, Fabien; Tertre, Emmanuel; Ferrage, Eric; Robin, Valentin; Dzene, Liva; Cochet, Carine; Turpault, Marie-Pierre

    2016-05-01

    In acidic soils, the fixation of Al in the interlayer spaces of 2:1 clay minerals and the subsequent formation of hydroxyl interlayer minerals (HIMs) are known to reduce soil fertility. The resulting crystal structure of HIMs consist of complex mixed-layer minerals (MLMs) with contrasting relative proportions of expandable, hydroxy-interlayers (HI) and illite layers. The present study aims to experimentally assess the influence of particle size on the formation of such complex HIMs for vermiculite saturated with potassium (K). Based on chemical and structural data, this study reports the dissolution and Al-interlayer occupancy of three size fractions (0.1-0.2, 1-2 and 10-20 μm) of K-vermiculite, which were obtained at pH = 3 by using stirred flow-through reactors. The Al-interlayer occupancies were ordered 0.1-0.2 μm < 10-20 μm < 1-2 μm even though the dissolution rate (in molvermiculite g-1 s-1) increases with decreasing particle size. For fine particles (0.1-0.2 μm), a rapid but low Al-interlayer occupancy during the transitory state and a null rate in the steady-state were evidenced and interpreted as indicating (i) a rapid but limited K+ interlayer exchange during the first step of the overall reactions and (ii) a stoichiometric dissolution of the crystal (TOT layer + interlayer) in the steady-state. By contrast, although the stoichiometric dissolution of the TOT layer is reached in the steady-state for the coarsest fractions (10-20 and 1-2 μm), the Al-interlayer occupancies continue to evolve due to the exchange of interlayer K+, which continues to progress for a longer duration. The mechanism of auto-aluminization is interpreted in the present study as multiple processes that involve (i) the dissolution of the mineral under acidic conditions, (ii) the interlayer diffusion of initial interlayer cations and their exchange with those from the aqueous phase and (iii) the fixation of interlayer aluminum. Competition between the kinetics of ion-exchange reactions and that of mineral dissolution is responsible for the above Al-interlayer occupancy order among the particle sizes (i.e., 0.1-0.2 μm < 10-20 μm < 1-2 μm). Moreover, this mechanism may be the cause of complex mineralogical structures such as mixed-layer minerals, which are commonly found in the clay-size fraction of acidic soils.

  11. Magnetic Field Effects and Electromagnetic Wave Propagation in Highly Collisional Plasmas.

    NASA Astrophysics Data System (ADS)

    Bozeman, Steven Paul

    The homogeneity and size of radio frequency (RF) and microwave driven plasmas are often limited by insufficient penetration of the electromagnetic radiation. To investigate increasing the skin depth of the radiation, we consider the propagation of electromagnetic waves in a weakly ionized plasma immersed in a steady magnetic field where the dominant collision processes are electron-neutral and ion-neutral collisions. Retaining both the electron and ion dynamics, we have adapted the theory for cold collisionless plasmas to include the effects of these collisions and obtained the dispersion relation at arbitrary frequency omega for plane waves propagating at arbitrary angles with respect to the magnetic field. We discuss in particular the cases of magnetic field enhanced wave penetration for parallel and perpendicular propagation, examining the experimental parameters which lead to electromagnetic wave propagation beyond the collisional skin depth. Our theory predicts that the most favorable scaling of skin depth with magnetic field occurs for waves propagating nearly parallel to B and for omega << Omega_{rm e} where Omega_{rm e} is the electron cyclotron frequency. The scaling is less favorable for propagation perpendicular to B, but the skin depth does increase for this case as well. Still, to achieve optimal wave penetration, we find that one must design the plasma configuration and antenna geometry so that one generates primarily the appropriate angles of propagation. We have measured plasma wave amplitudes and phases using an RF magnetic probe and densities using Stark line broadening. These measurements were performed in inductively coupled plasmas (ICP's) driven with a standard helical coil, a reverse turn (Stix) coil, and a flat spiral coil. Density measurements were also made in a microwave generated plasma. The RF magnetic probe measurements of wave propagation in a conventional ICP with wave propagation approximately perpendicular to B show an increase in skin depth with magnetic field and a damping of the effect of B with pressure. The flat coil geometry which launches waves more nearly parallel to B allows enhanced wave penetration at higher pressures than the standard helical coil.

  12. In-vivo dynamic characterization of microneedle skin penetration using optical coherence tomography

    NASA Astrophysics Data System (ADS)

    Enfield, Joey; O'Connell, Marie-Louise; Lawlor, Kate; Jonathan, Enock; O'Mahony, Conor; Leahy, Martin

    2010-07-01

    The use of microneedles as a method of circumventing the barrier properties of the stratum corneum is receiving much attention. Although skin disruption technologies and subsequent transdermal diffusion rates are being extensively studied, no accurate data on depth and closure kinetics of microneedle-induced skin pores are available, primarily due to the cumbersome techniques currently required for skin analysis. We report on the first use of optical coherence tomography technology to image microneedle penetration in real time and in vivo. We show that optical coherence tomography (OCT) can be used to painlessly measure stratum corneum and epidermis thickness, as well as microneedle penetration depth after microneedle insertion. Since OCT is a real-time, in-vivo, nondestructive technique, we also analyze skin healing characteristics and present quantitative data on micropore closure rate. Two locations (the volar forearm and dorsal aspect of the fingertip) have been assessed as suitable candidates for microneedle administration. The results illustrate the applicability of OCT analysis as a tool for microneedle-related skin characterization.

  13. Ultrasound-facilitated transport of silver chloride (AgCl) particles in fish skin.

    PubMed

    Frenkel, V; Kimmel, E; Iger, Y

    2000-08-10

    Electron-dense nano-particles in aqueous suspension were administered by immersion into the epidermis of fish using ultrasound in the therapeutic range. Enhanced permeability of the tissues to the particles was achieved by acoustic cavitation, which induced a controlled level of necrosis in the outer cell layers, and by non-cavitational exposures, which widened intercellular spaces of non-necrosed tissue in deeper regions of the epidermis. Both particle concentration and penetration depth were quantified using transmission electron microscopy. While cavitation-induced perforation was necessary for particles to penetrate into the tissues, non-cavitational exposures during immersions increased the particle flux towards the skin surface, as well as the diffusion rate of the particles within the epidermis and their depth of penetration. The technique described above may potentially be applied for non-stressful, mass-administration of substances into aquatic animals, as well as the relatively new field of ultrasound-facilitated delivery in moist epithelial tissues in humans.

  14. Magnetoconductance oscillations at a nanoparticle film-superconductor interface: a means for probing flux penetration depth.

    PubMed

    Dunford, Jeffrey L; Dhirani, Al-Amin

    2008-11-12

    Interfaces between disordered normal materials and superconductors (S) can exhibit 'reflectionless tunnelling' (RT)-a phenomenon that arises from repeated disorder-driven elastic scattering, multiple Andreev reflections, and electron/hole interference. RT has been used to explain zero-bias conductance peaks (ZBCPs) observed using doped semiconductors and evaporated granular metal films as the disordered normal materials. Recently, in addition to ZBCPs, magnetoconductance oscillations predicted by RT theory have been observed using a novel normal disordered material: self-assembled nanoparticle films. In the present study, we find that the period of these oscillations decreases as temperature (T) increases. This suggests that the magnetic flux associated with interfering pathways increases accordingly. We propose that the increasing flux can be attributed to magnetic field penetration into S as [Formula: see text]. This model agrees remarkably well with known T dependence of penetration depth predicted by Bardeen-Cooper-Schrieffer theory. Our study shows that this additional region of flux is significant and must be considered in experimental and theoretical studies of RT.

  15. Confocal Raman microspectrometry: a vectorial electromagnetic treatment of the light focused and collected through a planar interface and its application to the study of a thin coating.

    PubMed

    Sourisseau, C; Maraval, P

    2003-11-01

    In-depth confocal Raman microspectrometry (CRM) studies through a planar interface between materials of mismatched refraction indices are known to be affected by a decrease of both the collected Raman intensity and the axial resolution as a function of the penetration depth. Following a previous model, which takes the refraction, diffraction, and spherical aberration effects into account when focusing a Gaussian incident laser beam with a high numerical aperture objective lens, a complete vectorial treatment of these phenomena is considered. It is demonstrated that off-axis refraction effects cannot be neglected and that the dimension of the confocal pinhole aperture plays a crucial role on the effective focal plane position and on the collection efficiency. We thus propose a more rigorous and complete approach to the problem, and we find a very good agreement between experimental and theoretical Raman intensity variations for a thick polyethylene sample as a function of the penetration depth. As compared with calculations where only refraction was considered, we confirm that the lengthening of the focus even for a large penetration depth is significantly reduced upon diffraction effects. As an illustrative example, the theoretical Raman responses for a thin coating of approximately 20 microns on a polymer substrate were investigated and compared to experimental results already published. Even though the interfacial region is spread over approximately 5-6 microns when using a 100x objective and a confocal pinhole of 200 microns diameter, it is definitively concluded that the apparent axial resolution is not drastically deteriorated with increasing depth and that the coating thickness may be directly estimated with a precision of approximately 1.0 micron (5%).

  16. Geohydrology of rocks penetrated by test well USW H-4, Yucca Mountain, Nye County, Nevada

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Whitfield, M.S. Jr.; Eshom, E.P.; Thordarson, W.

    This report presents the results of hydraulic testing of rocks penetrated by USW H-4, one of several test wells drilled in the southwestern part of the Nevada Test Site, in cooperation with the US Department of Energy, for investigations related to the isolation of high-level radioactive wastes in volcanic tuffs of Tertiary age. All rocks penetrated by the test well to its total depth of 1219 meters were volcanic. Static water level was at a depth of 519 meters below land surface. Hydraulic-head measurements made at successively lower depths during drilling in this test hole indicate no noticeable head change.more » A radioactive-tracer, borehole-flow survey indicated that the two most productive zones in this borehole occurred in the upper part of the Bullfrog Member, depth interval from 721 to 731.5 meters, and in the underlying upper part of the Tram Member, depth interval from 864 to 920 meters, both in the Crater Flat Tuff. Hydraulic coefficients calculated from pumping-test data indicate that transmissivity ranged from 200 to 790 meters squared per day. The hydraulic conductivity ranged from 0.29 to 1.1 meters per day. Chemical analysis of water pumped from the saturated part of the borehole (composite sample) indicates that the water is typical of water produced from tuffaceous rocks in southern Nevada. The water is predominantly a sodium bicarbonate type with small concentrations of calcium, magnesium, and sulfate. The apparent age of this composite water sample was determined by a carbon-14 date to be 17,200 years before present. 24 refs., 10 figs., 8 tabs.« less

  17. Mechanism of nanosecond laser drilling process of 4H-SiC for through substrate vias

    NASA Astrophysics Data System (ADS)

    Kim, Byunggi; Iida, Ryoichi; Doan, Duc Hong; Fushinobu, Kazuyoshi

    2017-06-01

    Role of optical parameters on nanosecond laser drilling of 4H-SiC was experimentally studied. Using ns pulsed Nd:YAG laser, parametric studies on effects of wavelength (1064 nm or 532 nm), beam profile (Gaussian or Bessel), and ambient condition (air or water) were conducted. The wavelengths which have large optical penetration depth were selected as wavefront has to propagate through materials to generate Bessel beam. The experimental results showed that carbonization of SiC surface accelerates thermal ablation of the materials with fluence under the lattice melting threshold. Especially, pattern of side lobes with small fluence was formed by irradiation of Bessel beam. The pattern disturbed penetration of wavefronts through materials. Implementation of water environment was not effective to suppress carbonization and had slight effect on improvement of drilling quality. For this reason, deep drilling with small entrance was not achieved using Bessel beam. Irradiation of 1064 nm Gaussian beam with large fluence led to formation of critical amount of re-solidified silicon due to the large optical penetration depth. Carbonization and silicon formation had a significant effect on unique fluence dependence of drilling depth. Absorption mechanism was studied as well to discuss effect of wavelength on processing characteristics.

  18. Completing the Feedback Loop: The Impact of Chlorophyll Data Assimilation on the Ocean State

    NASA Technical Reports Server (NTRS)

    Borovikov, Anna; Keppenne, Christian; Kovach, Robin

    2015-01-01

    In anticipation of the integration of a full biochemical model into the next generation GMAO coupled system, an intermediate solution has been implemented to estimate the penetration depth (1Kd_PAR) of ocean radiation based on the chlorophyll concentration. The chlorophyll is modeled as a tracer with sources-sinks coming from the assimilation of MODIS chlorophyll data. Two experiments were conducted with the coupled ocean-atmosphere model. In the first, climatological values of Kpar were used. In the second, retrieved daily chlorophyll concentrations were assimilated and Kd_PAR was derived according to Morel et al (2007). No other data was assimilated to isolate the effects of the time-evolving chlorophyll field. The daily MODIS Kd_PAR product was used to validate the skill of the penetration depth estimation and the MERRA-OCEAN re-analysis was used as a benchmark to study the sensitivity of the upper ocean heat content and vertical temperature distribution to the chlorophyll input. In the experiment with daily chlorophyll data assimilation, the penetration depth was estimated more accurately, especially in the tropics. As a result, the temperature bias of the model was reduced. A notably robust albeit small (2-5 percent) improvement was found across the equatorial Pacific ocean, which is a critical region for seasonal to inter-annual prediction.

  19. Magnetic penetration-depth measurements of a suppressed superfluid density of superconducting Ca0.5Na0.5Fe2As2 single crystals by proton irradiation

    NASA Astrophysics Data System (ADS)

    Kim, Jeehoon; Haberkorn, N.; Graf, M. J.; Usov, I.; Ronning, F.; Civale, L.; Nazaretski, E.; Chen, G. F.; Yu, W.; Thompson, J. D.; Movshovich, R.

    2012-10-01

    We report on the dramatic effect of random point defects, produced by proton irradiation, on the superfluid density ρs in superconducting Ca0.5Na0.5Fe2As2 single crystals. The magnitude of the suppression is inferred from measurements of the temperature-dependent magnetic penetration depth λ(T) using magnetic force microscopy. Our findings indicate that a radiation dose of 2×1016 cm-2 produced by 3 MeV protons results in a reduction of the superconducting critical temperature Tc by approximately 10%. In contrast, ρs(0) is suppressed by approximately 60%. This breakdown of the Abrikosov-Gorkov theory may be explained by the so-called “Swiss cheese model,” which accounts for the spatial suppression of the order parameter near point defects similar to holes in Swiss cheese. Both the slope of the upper critical field and the penetration depth λ(T/Tc)/λ(0) exhibit similar temperature dependences before and after irradiation. This may be due to a combination of the highly disordered nature of Ca0.5Na0.5Fe2As2 with large intraband and simultaneous interband scattering as well as the s±-wave nature of short coherence length superconductivity.

  20. Transmission measurement based on STM observation to detect the penetration depth of low-energy heavy ions in botanic samples.

    PubMed

    Liu, Feng; Wang, Yugang; Xue, Jianming; Wang, Sixue; Du, Guanhua; Zhao, Weijiang

    2003-02-01

    The penetration depth of low-energy heavy ions in botanic samples was detected with a new transmission measurement. In the measurement, highly oriented pyrolytic graphite (HOPG) pieces were placed behind the botanic samples with certain thickness. During the irradiation of heavy ions with energy of tens of keV, the energetic particles transmitted from those samples were received by the HOPG pieces. After irradiation, scanning tunneling microscope (STM) was applied to observe protrusion-like damage induced by these transmitted ions on the surface of the HOPG. The statistical average number density of protrusions and the minimum transmission rate of the low-energy heavy ions can be obtained. The detection efficiency of the new method for low-energy heavy ions was about 0.1-1 and the background in the measurement can be reduced to as low as 1.0 x 10(8) protrusions/cm2. With this method, the penetration depth of the energetic particles was detected to be no less than 60 micrometers in kidney bean slices when the slices were irradiated by 100 keVAr+ ion at the fluence of 5 x 10(16) ions/cm2. c2002 Elsevier Science Ltd. All rights reserved.

  1. Effect of heavy-ion irradiation on London penetration depth in overdoped Ba(Fe 1 - x Co x ) 2 As 2

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Murphy, J.; Tanatar, M. A.; Kim, Hyunsoo

    2013-08-01

    Irradiation with 1.4 GeV 208 Pb ions was used to induce artificial disorder in single crystals of iron-arsenide superconductor Ba(Fe 1 - x Co x ) 2 As 2 and to study its effects on the temperature-dependent London penetration depth and transport properties. A study was undertaken on overdoped single crystals with x = 0.108 and x = 0.127 characterized by notable modulation of the superconducting gap. Irradiation corresponding to the matching fields of B Φ = 6 T and 6.5 T with doses 2.22 × 10 11 d /cm 2 and 2.4 × 10 11 d /cm 2 ,more » respectively, suppresses the superconducting T c by approximately 0.3 to 1 K. The variation of the low-temperature penetration depth in both pristine and irradiated samples is well described by the power law Δ λ ( T ) = A T n . Irradiation increases the magnitude of the prefactor A and decreases the exponent n , similar to the effect of irradiation in optimally-doped samples. This finding supports universal s ± pairing in Ba(Fe 1 - x Co x ) 2 As 2 compounds for the entire Co doping range.« less

  2. Influence of laser power on the penetration depth and geometry of scanning tracks in selective laser melting

    NASA Astrophysics Data System (ADS)

    Stopyra, Wojciech; Kurzac, Jarosław; Gruber, Konrad; Kurzynowski, Tomasz; Chlebus, Edward

    2016-12-01

    SLM technology allows production of a fully functional objects from metal and ceramic powders, with true density of more than 99,9%. The quality of manufactured items in SLM method affects more than 100 parameters, which can be divided into fixed and variable. Fixed parameters are those whose value before the process should be defined and maintained in an appropriate range during the process, e.g. chemical composition and morphology of the powder, oxygen level in working chamber, heating temperature of the substrate plate. In SLM technology, five parameters are variables that optimal set allows to produce parts without defects (pores, cracks) and with an acceptable speed. These parameters are: laser power, distance between points, time of exposure, distance between lines and layer thickness. To develop optimal parameters thin walls or single track experiments are performed, to select the best sets narrowed to three parameters: laser power, exposure time and distance between points. In this paper, the effect of laser power on the penetration depth and geometry of scanned single track was shown. In this experiment, titanium (grade 2) substrate plate was used and scanned by fibre laser of 1064 nm wavelength. For each track width, height and penetration depth of laser beam was measured.

  3. Transmission measurement based on STM observation to detect the penetration depth of low-energy heavy ions in botanic samples

    NASA Technical Reports Server (NTRS)

    Liu, Feng; Wang, Yugang; Xue, Jianming; Wang, Sixue; Du, Guanhua; Zhao, Weijiang

    2003-01-01

    The penetration depth of low-energy heavy ions in botanic samples was detected with a new transmission measurement. In the measurement, highly oriented pyrolytic graphite (HOPG) pieces were placed behind the botanic samples with certain thickness. During the irradiation of heavy ions with energy of tens of keV, the energetic particles transmitted from those samples were received by the HOPG pieces. After irradiation, scanning tunneling microscope (STM) was applied to observe protrusion-like damage induced by these transmitted ions on the surface of the HOPG. The statistical average number density of protrusions and the minimum transmission rate of the low-energy heavy ions can be obtained. The detection efficiency of the new method for low-energy heavy ions was about 0.1-1 and the background in the measurement can be reduced to as low as 1.0 x 10(8) protrusions/cm2. With this method, the penetration depth of the energetic particles was detected to be no less than 60 micrometers in kidney bean slices when the slices were irradiated by 100 keVAr+ ion at the fluence of 5 x 10(16) ions/cm2. c2002 Elsevier Science Ltd. All rights reserved.

  4. Characterization of NbN films and tunnel junctions

    NASA Technical Reports Server (NTRS)

    Stern, J. A.; Leduc, H. G.

    1991-01-01

    Properties of NbN films and NbN/MgO/NbN tunnel junctions are discussed. NbN junctions are being developed for use in high-frequency, SIS quasiparticle mixers. To properly design mixer circuits, junction and film properties need to be characterized. The specific capacitance of NbN/MgO/NbN junctions has been measured as a function of the product of the normal-state resistance and the junction area (RnA), and it is found to vary by more than a factor of two (35-85 fF/sq microns) over the range of RnA measured (1000-50 ohm sq microns). This variation is important because the specific capacitance determines the RC speed of the tunnel junction at a given RnA value. The magnetic penetration depth of NbN films deposited under different conditions is also measured. The magnetic penetration depth affects the design of microstrip line used in RF tuning circuits. Control of the magnetic penetration depth is necessary to fabricate reproducible tuning circuits. Additionally, the critical current uniformity for arrays of 100 junctions has been measured. Junction uniformity will affect the design of focal-plane arrays of SIS mixers. Finally, the relevance of these measurements to the design of Josephson electronics is discussed.

  5. Effects of the F4TCNQ-Doped Pentacene Interlayers on Performance Improvement of Top-Contact Pentacene-Based Organic Thin-Film Transistors

    PubMed Central

    Fan, Ching-Lin; Lin, Wei-Chun; Chang, Hsiang-Sheng; Lin, Yu-Zuo; Huang, Bohr-Ran

    2016-01-01

    In this paper, the top-contact (TC) pentacene-based organic thin-film transistor (OTFT) with a tetrafluorotetracyanoquinodimethane (F4TCNQ)-doped pentacene interlayer between the source/drain electrodes and the pentacene channel layer were fabricated using the co-evaporation method. Compared with a pentacene-based OTFT without an interlayer, OTFTs with an F4TCNQ:pentacene ratio of 1:1 showed considerably improved electrical characteristics. In addition, the dependence of the OTFT performance on the thickness of the F4TCNQ-doped pentacene interlayer is weaker than that on a Teflon interlayer. Therefore, a molecular doping-type F4TCNQ-doped pentacene interlayer is a suitable carrier injection layer that can improve the TC-OTFT performance and facilitate obtaining a stable process window. PMID:28787845

  6. Band engineering in twisted molybdenum disulfide bilayers

    NASA Astrophysics Data System (ADS)

    Zhao, Yipeng; Liao, Chengwei; Ouyang, Gang

    2018-05-01

    In order to explore the theoretical relationship between interlayer spacing, interaction and band offset at the atomic level in vertically stacked two-dimensional (2D) van der Waals (vdW) structures, we propose an analytical model to address the evolution of interlayer vdW coupling with random stacking configurations in MoS2 bilayers based on the atomic-bond-relaxation correlation mechanism. We found that interlayer spacing changes substantially with respect to the orientations, and the bandgap increases from 1.53 eV (AB stacking) to 1.68 eV (AA stacking). Our results reveal that the evolution of interlayer vdW coupling originates from the interlayer interaction, leading to interlayer separations and electronic properties changing with stacking configurations. Our predictions constitute a demonstration of twist engineering the band shift in the emergent class of 2D crystals, transition-metal dichalcogenides.

  7. Effect of sputtered titanium interlayers on the properties of nanocrystalline diamond films

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Li, Cuiping, E-mail: licp226@126.com, E-mail: limingji@163.com; Li, Mingji, E-mail: licp226@126.com, E-mail: limingji@163.com; Wu, Xiaoguo

    2016-04-07

    Ti interlayers with different thicknesses were sputtered on Si substrates and then ultrasonically seeded in a diamond powder suspension. Nanocrystalline diamond (NCD) films were deposited using a dc arc plasma jet chemical vapor deposition system on the seeded Ti/Si substrates. Atomic force microscopy and scanning electron microscopy tests showed that the roughness of the prepared Ti interlayer increased with increasing thickness. The effects of Ti interlayers with various thicknesses on the properties of NCD films were investigated. The results show nucleation, growth, and microstructure of the NCD films are strongly influenced by the Ti interlayers. The addition of a Timore » interlayer between the Si substrate and the NCD films can significantly enhance the nucleation rate and reduce the surface roughness of the NCD. The NCD film on a 120 nm Ti interlayer possesses the fastest nucleation rate and the smoothest surface. Raman spectra of the NCD films show trans-polyacetylene relevant peaks reduce with increasing Ti interlayer thickness, which can owe to the improvement of crystalline at grain boundaries. Furthermore, nanoindentation measurement results show that the NCD film on a 120 nm Ti interlayer displays a higher hardness and elastic modulus. High resolution transmission electron microscopy images of a cross-section show that C atoms diffuse into the Ti layer and Si substrate and form TiC and SiC hard phases, which can explain the enhancement of mechanical properties of NCD.« less

  8. Bottom Penetration at Shallow Grazing Angles II

    DTIC Science & Technology

    1992-06-19

    Millwater , "Wave Reflection from a Sediment Layer with Depth-Dependent Properties," J. Acoust. Soc. Am. 77, 1781- 1788 (1985). 35 8. N. P. Chotiros, ’High...Acoust. Soc. Am. 8B1 S131 (1990). 12. M. Stern, A. Bedford, and H. R. Millwater , "Wave Reflection from a Sediment Layer with Depth-Dependent

  9. The effect of cup outer sizes on the contact mechanics and cement fixation of cemented total hip replacements.

    PubMed

    Hua, Xijin; Li, Junyan; Wang, Ling; Wilcox, Ruth; Fisher, John; Jin, Zhongmin

    2015-10-01

    One important loosening mechanism of the cemented total hip arthroplasty is the mechanical overload at the bone-cement interface and consequent failure of the cement fixation. Clinical studies have revealed that the outer diameter of the acetabular component is a key factor in influencing aseptic loosening of the hip arthroplasty. The aim of the present study was to investigate the influence of the cup outer diameter on the contact mechanics and cement fixation of a cemented total hip replacement (THR) with different wear penetration depths and under different cup inclination angles using finite element (FE) method. A three-dimensional FE model was developed based on a typical Charnley hip prosthesis. Two acetabular cup designs with outer diameters of 40 and 43 mm were modelled and the effect of cup outer diameter, penetration depth and cup inclination angle on the contact mechanics and cement fixation stresses in the cemented THR were studied. The results showed that for all penetration depths and cup inclination angles considered, the contact mechanics in terms of peak von Mises stress in the acetabular cup and peak contact pressure at the bearing surface for the two cup designs were similar (within 5%). However, the peak von Mises stress, the peak maximum principal stress and peak shear stress in the cement mantle at the bone-cement interface for the 43 mm diameter cup design were predicted to be lower compared to those for the 40 mm diameter cup design. The differences were predicted to be 15-19%, 15-22% and 18-20% respectively for different cup penetration depths and inclination angles, which compares to the clinical difference of aseptic loosening incidence of about 20% between the two cup designs. Copyright © 2015 IPEM. Published by Elsevier Ltd. All rights reserved.

  10. Penetration Resistance of Armor Ceramics: Dimensional Analysis and Property Correlations

    DTIC Science & Technology

    2015-08-01

    been reported in experimental studies. Particular ceramics analyzed here are low- and high-purity alumina, aluminum nitride, boron carbide, silicon...analyzed here are low- and high-purity alumina, aluminum nitride, boron carbide, silicon carbide, and titanium diboride. Data for penetration depth...include high hardness, high elastic stiffness, high strengths (static/dynamic compressive, shear, and bending), and low density relative to armor steels

  11. Box simulations of rotating magnetoconvection. Effects of penetration and turbulent pumping

    NASA Astrophysics Data System (ADS)

    Ziegler, U.; Rüdiger, G.

    2003-04-01

    Various effects of penetration in rotating magnetoconvection are studied by means of three-dimensional numerical simulations employing the code NIRVANA. A local, 2-layer model is applied dividing the computational domain (which is a rectangular box placed tangentially on a sphere at latitude 45deg) in an unstable polytropic region on top of a stable polytropic region. Different realizations of convection are examined parameterized by Taylor numbers Ta=0,6 x 104, 6x 105 and magnetic field strengths β = 5,50,500,5000,infty . We find a rather distinctive behavior of the penetration depth Delta on the system parameters (Ta,β). In non-rotating convection Delta is a monotonically decreasing function of β-1 which is due to magnetic quenching effects. Also, penetration is subject to rotational quenching, i.e. Delta is reduced for increasing rotation rate. In the intermediate regime of (Ta,β), the effects of rotation and magnetic field on Delta do not simply add (see Fig. 3). We find, nevertheless, a very strong reduction of the penetration depth of overshooting turbulence by both rotation and magnetism. Penetrative convection is closely associated with the mixing of a passive scalar quantity advected with the flow. In the long term, the tracer material penetrates significantly deeper into the stable layer than suggested by Delta which is due to the cumulative effect of isolated, fast-moving plumes. In case of a weak magnetic field, penetrative convection also serves to ensure a downward transport of magnetic flux by turbulent pumping with an average rate gammaz ~ -7x 10-3 measured in units of the sound speed at the top z-boundary. For larger magnetic fields the pumping effect is quenched and even changes sign in the convection zone. This effect is suggested as being due to the effect of ``turbulent buoyancy'' which in density-stratified media transports a given magnetic field upwards if it is not too strong (Kichatinov & Rüdiger \\cite{Kichatinov92}).

  12. The hyperelastic and failure behaviors of skin in relation to the dynamic application of microscopic penetrators in a murine model.

    PubMed

    Meliga, Stefano C; Coffey, Jacob W; Crichton, Michael L; Flaim, Christopher; Veidt, Martin; Kendall, Mark A F

    2017-01-15

    In-depth understanding of skin elastic and rupture behavior is fundamental to enable next-generation biomedical devices to directly access areas rich in cells and biomolecules. However, the paucity of skin mechanical characterization and lack of established fracture models limits their rational design. We present an experimental and numerical study of skin mechanics during dynamic interaction with individual and arrays of micro-penetrators. Initially, micro-indentation of individual skin strata revealed hyperelastic moduli were dramatically rate-dependent, enabling extrapolation of stiffness properties at high velocity regimes (>1ms -1 ). A layered finite-element model satisfactorily predicted the penetration of micro-penetrators using characteristic fracture energies (∼10pJμm -2 ) significantly lower than previously reported (≫100pJμm -2 ). Interestingly, with our standard application conditions (∼2ms -1 , 35gpistonmass), ∼95% of the application kinetic energy was transferred to the backing support rather than the skin ∼5% (murine ear model). At higher velocities (∼10ms -1 ) strain energy accumulated in the top skin layers, initiating fracture before stress waves transmitted deformation to the backing material, increasing energy transfer efficiency to 55%. Thus, the tools developed provide guidelines to rationally engineer skin penetrators to increase depth targeting consistency and payload delivery across patients whilst minimizing penetration energy to control skin inflammation, tolerability and acceptability. The mechanics of skin penetration by dynamically-applied microscopic tips is investigated using a combined experimental-computational approach. A FE model of skin is parameterized using indentation tests and a ductile-failure implementation validated against penetration assays. The simulations shed light on skin elastic and fracture properties, and elucidate the interaction with microprojection arrays for vaccine delivery allowing rational design of next-generation devices. Copyright © 2016 Acta Materialia Inc. Published by Elsevier Ltd. All rights reserved.

  13. Time-varying multiplex network: Intralayer and interlayer synchronization

    NASA Astrophysics Data System (ADS)

    Rakshit, Sarbendu; Majhi, Soumen; Bera, Bidesh K.; Sinha, Sudeshna; Ghosh, Dibakar

    2017-12-01

    A large class of engineered and natural systems, ranging from transportation networks to neuronal networks, are best represented by multiplex network architectures, namely a network composed of two or more different layers where the mutual interaction in each layer may differ from other layers. Here we consider a multiplex network where the intralayer coupling interactions are switched stochastically with a characteristic frequency. We explore the intralayer and interlayer synchronization of such a time-varying multiplex network. We find that the analytically derived necessary condition for intralayer and interlayer synchronization, obtained by the master stability function approach, is in excellent agreement with our numerical results. Interestingly, we clearly find that the higher frequency of switching links in the layers enhances both intralayer and interlayer synchrony, yielding larger windows of synchronization. Further, we quantify the resilience of synchronous states against random perturbations, using a global stability measure based on the concept of basin stability, and this reveals that intralayer coupling strength is most crucial for determining both intralayer and interlayer synchrony. Lastly, we investigate the robustness of interlayer synchronization against a progressive demultiplexing of the multiplex structure, and we find that for rapid switching of intralayer links, the interlayer synchronization persists even when a large number of interlayer nodes are disconnected.

  14. The thickness design of unintentionally doped GaN interlayer matched with background doping level for InGaN-based laser diodes

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Chen, P.; Zhao, D. G., E-mail: dgzhao@red.semi.ac.cn; Jiang, D. S.

    2016-03-15

    In order to reduce the internal optical loss of InGaN laser diodes, an unintentionally doped GaN (u-GaN) interlayer is inserted between InGaN/GaN multiple quantum well active region and Al{sub 0.2}Ga{sub 0.8}N electron blocking layer. The thickness design of u-GaN interlayer matching up with background doping level for improving laser performance is studied. It is found that a suitably chosen u-GaN interlayer can well modulate the optical absorption loss and optical confinement factor. However, if the value of background doping concentration of u-GaN interlayer is too large, the output light power may decrease. The analysis of energy band diagram of amore » LD structure with 100 nm u-GaN interlayer shows that the width of n-side depletion region decreases when the background concentration increases, and may become even too small to cover whole MQW, resulting in a serious decrease of the output light power. It means that a suitable interlayer thickness design matching with the background doping level of u-GaN interlayer is significant for InGaN-based laser diodes.« less

  15. Time-varying multiplex network: Intralayer and interlayer synchronization.

    PubMed

    Rakshit, Sarbendu; Majhi, Soumen; Bera, Bidesh K; Sinha, Sudeshna; Ghosh, Dibakar

    2017-12-01

    A large class of engineered and natural systems, ranging from transportation networks to neuronal networks, are best represented by multiplex network architectures, namely a network composed of two or more different layers where the mutual interaction in each layer may differ from other layers. Here we consider a multiplex network where the intralayer coupling interactions are switched stochastically with a characteristic frequency. We explore the intralayer and interlayer synchronization of such a time-varying multiplex network. We find that the analytically derived necessary condition for intralayer and interlayer synchronization, obtained by the master stability function approach, is in excellent agreement with our numerical results. Interestingly, we clearly find that the higher frequency of switching links in the layers enhances both intralayer and interlayer synchrony, yielding larger windows of synchronization. Further, we quantify the resilience of synchronous states against random perturbations, using a global stability measure based on the concept of basin stability, and this reveals that intralayer coupling strength is most crucial for determining both intralayer and interlayer synchrony. Lastly, we investigate the robustness of interlayer synchronization against a progressive demultiplexing of the multiplex structure, and we find that for rapid switching of intralayer links, the interlayer synchronization persists even when a large number of interlayer nodes are disconnected.

  16. Molecular dynamics simulation of diffusion and electrical conductivity in montmorillonite interlayers

    DOE PAGES

    Greathouse, Jeffery A.; Cygan, Randall T.; Fredrich, Joanne T.; ...

    2016-01-20

    In this study, the diffusion of water and ions in the interlayer region of smectite clay minerals represents a direct probe of the type and strength of clay–fluid interactions. Interlayer diffusion also represents an important link between molecular simulation and macroscopic experiments. Here we use molecular dynamics simulation to investigate trends in cation and water diffusion in montmorillonite interlayers, looking specifically at the effects of layer charge, interlayer cation and cation charge (sodium or calcium), water content, and temperature. For Na-montmorillonite, the largest increase in ion and water diffusion coefficients occurs between the one-layer and two-layer hydrates, corresponding to themore » transition from inner-sphere to outer-sphere surface complexes. Calculated activation energies for ion and water diffusion in Na-montmorillonite are similar to each other and to the water hydrogen bond energy, suggesting the breaking of water–water and water–clay hydrogen bonds as a likely mechanism for interlayer diffusion. A comparison of interlayer diffusion with that of bulk electrolyte solutions reveals a clear trend of decreasing diffusion coefficient with increasing electrolyte concentration, and in most cases the interlayer diffusion results are nearly coincident with the corresponding bulk solutions. Trends in electrical conductivities computed from the ion diffusion coefficients are also compared.« less

  17. Interlayer Exciton Optoelectronics in a 2D Heterostructure p-n Junction.

    PubMed

    Ross, Jason S; Rivera, Pasqual; Schaibley, John; Lee-Wong, Eric; Yu, Hongyi; Taniguchi, Takashi; Watanabe, Kenji; Yan, Jiaqiang; Mandrus, David; Cobden, David; Yao, Wang; Xu, Xiaodong

    2017-02-08

    Semiconductor heterostructures are backbones for solid-state-based optoelectronic devices. Recent advances in assembly techniques for van der Waals heterostructures have enabled the band engineering of semiconductor heterojunctions for atomically thin optoelectronic devices. In two-dimensional heterostructures with type II band alignment, interlayer excitons, where Coulomb bound electrons and holes are confined to opposite layers, have shown promising properties for novel excitonic devices, including a large binding energy, micron-scale in-plane drift-diffusion, and a long population and valley polarization lifetime. Here, we demonstrate interlayer exciton optoelectronics based on electrostatically defined lateral p-n junctions in a MoSe 2 -WSe 2 heterobilayer. Applying a forward bias enables the first observation of electroluminescence from interlayer excitons. At zero bias, the p-n junction functions as a highly sensitive photodetector, where the wavelength-dependent photocurrent measurement allows the direct observation of resonant optical excitation of the interlayer exciton. The resulting photocurrent amplitude from the interlayer exciton is about 200 times smaller than the resonant excitation of intralayer exciton. This implies that the interlayer exciton oscillator strength is 2 orders of magnitude smaller than that of the intralayer exciton due to the spatial separation of electron and hole to the opposite layers. These results lay the foundation for exploiting the interlayer exciton in future 2D heterostructure optoelectronic devices.

  18. Irradiation Does Not Increase the Penetration Depth of Doxorubicin in Normal Tissue After Pressurized Intra-peritoneal Aerosol Chemotherapy (PIPAC) in an Ex Vivo Model.

    PubMed

    Khosrawipour, Veria; Bellendorf, Alexander; Khosrawipour, Carolina; Hedayat-Pour, Yousef; Diaz-Carballo, David; Förster, Eckart; Mücke, Ralph; Kabakci, Burak; Adamietz, Irenäus Anton; Fakhrian, Khashayar

    To compare the impact of single fractional with bi-fractional irradiation on the depth of doxorubicin penetration into the normal tissue after pressurized intra-peritoneal aerosol chemotherapy (PIPAC) in our ex vivo model. Fresh post mortem swine peritoneum was cut into 12 proportional sections. Two control samples were treated with PIPAC only (no irradiation), one sample on day 1, the other on day 2. Five samples were irradiated with 1, 2, 4, 7 or 14 Gy followed by PIPAC. Four samples were treated on day one with 0.5, 1, 2, 3.5 or 7 Gy and with the same radiation dose 24 h later followed by PIPAC. Doxorubicin was aerosolized in an ex vivo PIPAC model at 12 mmHg/36°C. In-tissue doxorubicin penetration was measured using fluorescence microscopy on frozen thin sections. Doxorubicin penetration (DP) after PIPAC for the control samples was 407 μm and 373 μm, respectively. DP for samples with single fraction irradiation was 396 μm after 1 Gy, 384 μm after 2 Gy, 327 μm after 4 Gy, 280 μm after 7 Gy and 243 μm after 14 Gy. DP for samples with 2 fractions of irradiation was 376 μm after 0.5+0.5 Gy, 363 μm after 1+1 Gy, 372 μm after 2+2 Gy, 341 μm after 3.5+3.5 and 301 μm after 7+7 Gy irradiation. Fractionating of the irradiation did not significantly change DP into normal tissue. Irradiation does not increase the penetration depth of doxorubicin into the normal tissue but might have a limiting impact on penetration and distribution of doxorubicin. Further studies are warranted to investigate the impact of addition of irradiation to PIPAC of tumor cells and to find out if irradiation can be used safely as chemopotenting agent for patients with peritoneal metastases treated with PIPAC. Copyright © 2016 International Institute of Anticancer Research (Dr. John G. Delinassios), All rights reserved.

  19. Interlayer interactions in graphites.

    PubMed

    Chen, Xiaobin; Tian, Fuyang; Persson, Clas; Duan, Wenhui; Chen, Nan-xian

    2013-11-06

    Based on ab initio calculations of both the ABC- and AB-stacked graphites, interlayer potentials (i.e., graphene-graphene interaction) are obtained as a function of the interlayer spacing using a modified Möbius inversion method, and are used to calculate basic physical properties of graphite. Excellent consistency is observed between the calculated and experimental phonon dispersions of AB-stacked graphite, showing the validity of the interlayer potentials. More importantly, layer-related properties for nonideal structures (e.g., the exfoliation energy, cleave energy, stacking fault energy, surface energy, etc.) can be easily predicted from the interlayer potentials, which promise to be extremely efficient and helpful in studying van der Waals structures.

  20. Anion-intercalated layered double hydroxides modified test strips for detection of heavy metal ions.

    PubMed

    Wang, Nan; Sun, Jianchao; Fan, Hai; Ai, Shiyun

    2016-01-01

    In this work, a novel approach for facile and rapid detection of heavy metal ions using anion-intercalated layered double hydroxides (LDHs) modified test strips is demonstrated. By intercalating Fe(CN)6(4-) or S(2-) anions into the interlayers of LDHs on the filter paper, various heavy metal ions can be easily detected based on the color change before and after reaction between the anions and the heavy metal ions. Upon the dropping of heavy metal ions solutions to the test strips, the colors of the test strips changed instantly, which can be easily observed by naked eyes. With the decrease of the concentration, the color depth changed obviously. The lowest detection concentration can be up to 1×10(-6) mol L(-1). Due to the easily intercalation of anions into the interlayer of the LDHs on test trips, this procedure provides a general method for the construction of LDHs modified test strips for detection of heavy metal ions. The stability of the prepared test strips is investigated. Furthermore, all the results were highly reproducible. The test strips may have potential applications in environmental monitoring fields. Copyright © 2015 Elsevier B.V. All rights reserved.

  1. Improvement of heavy dopant doped Ni-silicide using ytterbium interlayer for nano-scale MOSFETS with an ultra shallow junction.

    PubMed

    Shin, Hong-Sik; Oh, Se-Kyung; Kang, Min-Ho; Li, Shi-Guang; Lee, Ga-Won; Lee, Hi-Deok

    2011-07-01

    In this paper, a novel Ni silicide with Yb interlayer (Yb/Ni/TiN) on a boron cluster (B18H22) implanted source/drain junction is proposed for the first time, and its thermal stability characteristics are analyzed in depth. The proposed Ni-silicide exhibits a wider RTP temperature window for uniform sheet resistance, surface roughness and better thermal stability than the conventional structure (Ni/TiN). In addition, the cross-sectional profile of the proposed Ni-silicide showed less agglomeration despite the high temperature post-silicidation annealing, and it can be said that the proposed structure was little dependence on the temperature post-silicidation annealing. The improvement of Ni silicide properties is analyzed and found to be due to the formation of the rare earth metal--NiSi (YbNi2Si2), whose peaks were confirmed by XRD. The junction leakage current of the p + -n junction with Yb/Ni/TiN and B18H22 implantation is smaller than that with Ni/TiN by almost one order of magnitude as well as improving the thermal stability of ultra shallow junction.

  2. The time-dependent accumulation of protoporphyrin IX fluorescence in nodular basal cell carcinoma following application of methyl aminolevulinate with an oxygen pressure injection device.

    PubMed

    Blake, E; Campbell, S; Allen, J; Mathew, J; Helliwell, P; Curnow, A

    2012-12-05

    Topical protoporphyrin (PpIX)-induced photodynamic therapy (PDT) relies on the penetration of the prodrug into the skin lesion and subsequent accumulation of the photosensitizer. Methyl aminolevulinate (MAL)-PDT is an established treatment for thinner and superficial non-melanoma skin cancers (NMSCs) but for the treatment of the thicker nodular basal cell carcinoma (nBCC) enhanced penetration of the prodrug is required. This study employed a new higher pressure, oxygen pressure injection (OPI) device, at the time of Metvix® application with a view to enhancing the penetration of MAL into the tumors. Each patient had Metvix® applied to a single nBCC followed by application of a higher pressure OPI device. Following different time intervals (0, 30, 60, 120 or 180 min) the tumors were excised. The maximum depth and area of MAL penetration achieved in each lesion was measured using PpIX fluorescence microscopy. As expected, an increase in the depth of MAL-induced PpIX accumulation and area of tumor sensitized was observed over time; when the Metvix® cream was applied for 0, 30, 60, 120 and 180 min the median depth of PpIX fluorescence was 0%, 21%, 26.5%, 75.5% and 90%, respectively and the median area of tumor sensitized was 0%, 4%, 6%, 19% and 60%, respectively. As the investigation presented here did not include a control arm, the relative depths of fluorescence observed in this study were statistically compared (using the non-parametric Mann Whitney U test) with the results of our previous study where patients had Metvix® cream applied either with or without the standard pressure OPI device. When the higher pressure OPI device was employed compared to without OPI this increase was observed to be greater following 30, 120, and 180 min although overall not significantly (p=0.835). In addition, no significant difference between the higher pressure OPI device employed here and the previously investigated standard pressure OPI device was observed (p=0.403). However, when the results for both OPI devices were combined and compared to the standard treatment (no OPI employed) group, although the difference did not reach significance (p=0.531) a consistent and substantial increase in the depth of PpIX fluorescence was observed, therefore employment of an OPI device during topical MAL-PDT protocols warrants further investigation as a technique for enhancing MAL penetration. Copyright © 2012 Elsevier B.V. All rights reserved.

  3. A comparative study on the transdermal penetration effect of gaseous and aqueous plasma reactive species

    NASA Astrophysics Data System (ADS)

    Liu, Xin; Gan, Lu; Ma, Mingyu; Zhang, Song; Liu, Jingjing; Chen, Hongxiang; Liu, Dawei; Lu, Xinpei

    2018-02-01

    To improve the depth of plasma active species in the skin, it is very important to develop skin disease treatment using plasma. In this article, an air plasma source was used to work directly with the skin of a mouse. A tortuous pathway, hair follicles, electroporation and a microneedle do not aid the transdermal delivery of gaseous plasma active species, therefore these gaseous plasma active species cannot penetrate mouse skin with a thickness of ~0.75 mm. The plasma activated water (PAW) produced by the air plasma source was used to study the transdermal penetration of the aqueous plasma activated species. This aqueous plasma activated species can penetrate the skin through hair follicles, intercellular and transcellular routes. The pH of the PAW did not affect the penetration efficiency of the aqueous plasma active species.

  4. Interlayer‐State‐Coupling Dependent Ultrafast Charge Transfer in MoS2/WS2 Bilayers

    PubMed Central

    Zhang, Jin; Hong, Hao; Lian, Chao; Ma, Wei; Xu, Xiaozhi; Zhou, Xu; Fu, Huixia

    2017-01-01

    Light‐induced interlayer ultrafast charge transfer in 2D heterostructures provides a new platform for optoelectronic and photovoltaic applications. The charge separation process is generally hypothesized to be dependent on the interlayer stackings and interactions, however, the quantitative characteristic and detailed mechanism remain elusive. Here, a systematical study on the interlayer charge transfer in model MoS2/WS2 bilayer system with variable stacking configurations by time‐dependent density functional theory methods is demonstrated. The results show that the slight change of interlayer geometry can significantly modulate the charge transfer time from 100 fs to 1 ps scale. Detailed analysis further reveals that the transfer rate in MoS2/WS2 bilayers is governed by the electronic coupling between specific interlayer states, rather than the interlayer distances, and follows a universal dependence on the state‐coupling strength. The results establish the interlayer stacking as an effective freedom to control ultrafast charge transfer dynamics in 2D heterostructures and facilitate their future applications in optoelectronics and light harvesting. PMID:28932669

  5. Dispersion relations of elastic waves in one-dimensional piezoelectric/piezomagnetic phononic crystal with functionally graded interlayers.

    PubMed

    Guo, Xiao; Wei, Peijun; Lan, Man; Li, Li

    2016-08-01

    The effects of functionally graded interlayers on dispersion relations of elastic waves in a one-dimensional piezoelectric/piezomagnetic phononic crystal are studied in this paper. First, the state transfer equation of the functionally graded interlayer is derived from the motion equation by the reduction of order (from second order to first order). The transfer matrix of the functionally graded interlayer is obtained by solving the state transfer equation with the spatial-varying coefficient. Based on the transfer matrixes of the piezoelectric slab, the piezomagnetic slab and the functionally graded interlayers, the total transfer matrix of a single cell is obtained. Further, the Bloch theorem is used to obtain the resultant dispersion equations of in-plane and anti-plane Bloch waves. The dispersion equations are solved numerically and the numerical results are shown graphically. Five kinds of profiles of functionally graded interlayers between a piezoelectric slab and a piezomagnetic slab are considered. It is shown that the functionally graded interlayers have evident influences on the dispersion curves and the band gaps. Copyright © 2016 Elsevier B.V. All rights reserved.

  6. Depth-resolved measurements with elliptically polarized reflectance spectroscopy

    PubMed Central

    Bailey, Maria J.; Sokolov, Konstantin

    2016-01-01

    The ability of elliptical polarized reflectance spectroscopy (EPRS) to detect spectroscopic alterations in tissue mimicking phantoms and in biological tissue in situ is demonstrated. It is shown that there is a linear relationship between light penetration depth and ellipticity. This dependence is used to demonstrate the feasibility of a depth-resolved spectroscopic imaging using EPRS. The advantages and drawbacks of EPRS in evaluation of biological tissue are analyzed and discussed. PMID:27446712

  7. Magnetic and superconducting phase diagram of Nb/Gd/Nb trilayers

    NASA Astrophysics Data System (ADS)

    Khaydukov, Yu. N.; Vasenko, A. S.; Kravtsov, E. A.; Progliado, V. V.; Zhaketov, V. D.; Csik, A.; Nikitenko, Yu. V.; Petrenko, A. V.; Keller, T.; Golubov, A. A.; Kupriyanov, M. Yu.; Ustinov, V. V.; Aksenov, V. L.; Keimer, B.

    2018-04-01

    We report on a study of the structural, magnetic, and superconducting properties of Nb (25 nm ) /Gd (df) /Nb (25 nm ) hybrid structures of a superconductor/ ferromagnet (S/F) type. The structural characterization of the samples, including careful determination of the layer thickness, was performed using neutron and x-ray scattering with the aid of depth-sensitive mass spectrometry. The magnetization of the samples was determined by superconducting quantum interference device magnetometry and polarized neutron reflectometry, and the presence of magnetic ordering for all samples down to the thinnest Gd(0.8 nm) layer was shown. The analysis of the neutron spin asymmetry allowed us to prove the absence of magnetically dead layers in junctions with Gd interlayer thickness larger than one monolayer. The measured dependence of the superconducting transition temperature Tc(df) has a damped oscillatory behavior with well-defined positions of the minimum at df=3 nm and the following maximum at df=4 nm, in qualitative agreement with prior work [J. S. Jiang et al., Phys. Rev. B 54, 6119 (1996), 10.1103/PhysRevB.54.6119]. We use a theoretical approach based on the Usadel equations to analyze the experimental Tc(df) dependence. The analysis shows that the observed minimum at df=3 nm can be described by the so-called zero to π phase transitions of highly transparent S/F interfaces with a superconducting correlation length ξf≈4 nm in Gd. This penetration length is several times higher than for strong ferromagnets like Fe, Co, and Ni, thus simplifying the preparation of S/F structures with df˜ξf which are of topical interest in superconducting spintronics.

  8. Maximizing synchronizability of duplex networks

    NASA Astrophysics Data System (ADS)

    Wei, Xiang; Emenheiser, Jeffrey; Wu, Xiaoqun; Lu, Jun-an; D'Souza, Raissa M.

    2018-01-01

    We study the synchronizability of duplex networks formed by two randomly generated network layers with different patterns of interlayer node connections. According to the master stability function, we use the smallest nonzero eigenvalue and the eigenratio between the largest and the second smallest eigenvalues of supra-Laplacian matrices to characterize synchronizability on various duplexes. We find that the interlayer linking weight and linking fraction have a profound impact on synchronizability of duplex networks. The increasingly large inter-layer coupling weight is found to cause either decreasing or constant synchronizability for different classes of network dynamics. In addition, negative node degree correlation across interlayer links outperforms positive degree correlation when most interlayer links are present. The reverse is true when a few interlayer links are present. The numerical results and understanding based on these representative duplex networks are illustrative and instructive for building insights into maximizing synchronizability of more realistic multiplex networks.

  9. Influence of in-situ deposited SiNx interlayer on crystal quality of GaN epitaxial films

    NASA Astrophysics Data System (ADS)

    Fan, Teng; Jia, Wei; Tong, Guangyun; Zhai, Guangmei; Li, Tianbao; Dong, Hailiang; Xu, Bingshe

    2018-05-01

    GaN epitaxial films with SiNx interlayers were prepared by metal organic chemical vapor deposition (MOCVD) on c-plane sapphire substrates. The influences of deposition times and locations of SiNx interlayers on crystal quality of GaN epitaxial films were studied. Under the optimal growth time of 120 s for the SiNx interlayer, the dislocation density of GaN film is reduced to 4.05 × 108 cm-2 proved by high resolution X-ray diffraction results. It is found that when the SiNx interlayer deposits on the GaN nucleation islands, the subsequent GaN film has the lowest dislocation density of only 2.89 × 108 cm-2. Moreover, a model is proposed to illustrate the morphological evolution and associated propagation processes of TDs in GaN epi-layers with SiNx interlayers for different deposition times and locations.

  10. Long-Range Interactions Restrict Water Transport in Pyrophyllite Interlayers

    DOE PAGES

    Zarzycki, Piotr; Gilbert, Benjamin

    2016-04-27

    Water diffusion within smectite clay interlayers is reduced by confinement and hence is highly determined by the interlayer spacings that are adopted during swelling. However, a molecular understanding of the short-and long-range forces governing interlayer water structure and dynamics is lacking. Using molecular dynamics simulations of water intercalated between pyrophyllite (smectite prototype) layers we provide a detailed picture of the variation of interlayered water mobility accompanying smectite expansion. Subtle changes in hydrogen bond network structure cause significant changes in water mobility that is greater for stable hydration states and reduced for intermediate separations. By studying pyrophyllite with and without externalmore » water we reveal that long-range electrostatic forces apply a restraining effect upon interlayer water mobility. Our findings are relevant for broad range of confining nanostructures with walls thin enough to permit long-range interactions that could affect the mobility of confined solvent molecules and solute species.« less

  11. Voltage-controlled interlayer coupling in perpendicularly magnetized magnetic tunnel junctions

    DOE PAGES

    Newhouse-Illige, Ty; Liu, Yaohua; Xu, M.; ...

    2017-05-16

    Magnetic interlayer coupling is one of the central phenomena in spintronics. It has been predicted that the sign of interlayer coupling can be manipulated by electric fields, instead of electric currents, thereby offering a promising low energy magnetization switching mechanism. Here we present the experimental demonstration of voltage-controlled interlayer coupling in a new perpendicular magnetic tunnel junction system with a GdO x tunnel barrier, where a large perpendicular magnetic anisotropy and a sizable tunnelling magnetoresistance have been achieved at room temperature. Owing to the interfacial nature of the magnetism, the ability to move oxygen vacancies within the barrier, and amore » large proximity-induced magnetization of GdO x, both the magnitude and the sign of the interlayer coupling in these junctions can be directly controlled by voltage. Lastly, these results pave a new path towards achieving energy-efficient magnetization switching by controlling interlayer coupling.« less

  12. Long-Range Interactions Restrict Water Transport in Pyrophyllite Interlayers

    PubMed Central

    Zarzycki, Piotr; Gilbert, Benjamin

    2016-01-01

    Water diffusion within smectite clay interlayers is reduced by confinement and hence is highly determined by the interlayer spacings that are adopted during swelling. However, a molecular understanding of the short- and long-range forces governing interlayer water structure and dynamics is lacking. Using molecular dynamics simulations of water intercalated between pyrophyllite (smectite prototype) layers we provide a detailed picture of the variation of interlayered water mobility accompanying smectite expansion. Subtle changes in hydrogen bond network structure cause significant changes in water mobility that is greater for stable hydration states and reduced for intermediate separations. By studying pyrophyllite with and without external water we reveal that long-range electrostatic forces apply a restraining effect upon interlayer water mobility. Our findings are relevant for broad range of confining nanostructures with walls thin enough to permit long-range interactions that could affect the mobility of confined solvent molecules and solute species. PMID:27118164

  13. Voltage-controlled interlayer coupling in perpendicularly magnetized magnetic tunnel junctions

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Newhouse-Illige, Ty; Liu, Yaohua; Xu, M.

    Magnetic interlayer coupling is one of the central phenomena in spintronics. It has been predicted that the sign of interlayer coupling can be manipulated by electric fields, instead of electric currents, thereby offering a promising low energy magnetization switching mechanism. Here we present the experimental demonstration of voltage-controlled interlayer coupling in a new perpendicular magnetic tunnel junction system with a GdO x tunnel barrier, where a large perpendicular magnetic anisotropy and a sizable tunnelling magnetoresistance have been achieved at room temperature. Owing to the interfacial nature of the magnetism, the ability to move oxygen vacancies within the barrier, and amore » large proximity-induced magnetization of GdO x, both the magnitude and the sign of the interlayer coupling in these junctions can be directly controlled by voltage. Lastly, these results pave a new path towards achieving energy-efficient magnetization switching by controlling interlayer coupling.« less

  14. Modeling studies for a Mars penetrator heat flow measurement

    NASA Technical Reports Server (NTRS)

    Keihm, S. J.; Langseth, M. G.

    1976-01-01

    There were, two different design concepts considered for the purpose of measuring heat flow as part of a Mars penetrator mission. The first of the tentative designs utilizes temperature sensors emplaced along the trailing umbilicus at regularly spaced intervals, no greater than 1m, which is thermally coupled to the adjacent regolith radiatively and possibly convectively or conductively. The second of the heat flow designs considered requires the radial deployment of two or more low thermal mass temperature sensors outward from the penetrator body over a vertical (depth) range on the order of 1m.

  15. Elemental profiling of laser cladded multilayer coatings by laser induced breakdown spectroscopy and energy dispersive X-ray spectroscopy

    NASA Astrophysics Data System (ADS)

    Lednev, V. N.; Sdvizhenskii, P. A.; Filippov, M. N.; Grishin, M. Ya.; Filichkina, V. A.; Stavertiy, A. Ya.; Tretyakov, R. S.; Bunkin, A. F.; Pershin, S. M.

    2017-09-01

    Multilayer tungsten carbide wear resistant coatings were analyzed by laser induced breakdown spectroscopy (LIBS) and energy dispersive X-ray (EDX) spectroscopy. Coaxial laser cladding technique was utilized to produce tungsten carbide coating deposited on low alloy steel substrate with additional inconel 625 interlayer. EDX and LIBS techniques were used for elemental profiling of major components (Ni, W, C, Fe, etc.) in the coating. A good correlation between EDX and LIBS data was observed while LIBS provided additional information on light element distribution (carbon). A non-uniform distribution of tungsten carbide grains along coating depth was detected by both LIBS and EDX. In contrast, horizontal elemental profiling showed a uniform tungsten carbide particles distribution. Depth elemental profiling by layer-by-layer LIBS analysis was demonstrated to be an effective method for studying tungsten carbide grains distribution in wear resistant coating without any sample preparation.

  16. The efficiency of ceramic-faced metal targets at high-velocity impact

    NASA Astrophysics Data System (ADS)

    Tolkachev, V. F.; Konyaev, A. A.; Pakhnutova, N. V.

    2017-11-01

    The paper represents experimental results and engineering evaluation concerning the efficiency of composite materials to be used as an additional protection during the high- velocity interaction of a tungsten rod with a target in the velocity range of 1...5 km/s. The main parameter that characterizes the high-velocity interaction of a projectile with a layered target is the penetration depth. Experimental data, numerical simulation and engineering evaluation by modified models are used to determine the penetration depth. Boron carbide, aluminum oxide, and aluminum nickelide are applied as a front surface of targets. Based on experimental data and numerical simulation, the main characteristics of ceramics are determined, which allows composite materials to be effectively used as additional elements of protection.

  17. Magnetic penetration depth of YBa2Cu3O(7-delta) thin films determined by the power transmission method

    NASA Technical Reports Server (NTRS)

    Heinen, Vernon O.; Miranda, Felix A.; Bhasin, Kul B.

    1992-01-01

    A power transmission measurement technique was used to determine the magnetic penetration depth (lambda) of YBa2Cu3O(7-delta) superconducting thin films on LaAlO3 within the 26.5 to 40.0 GHz frequency range, and at temperatures from 20 to 300 K. Values of lambda ranging from 1100 to 2500 A were obtained at low temperatures. The anisotropy of lambda was determined from measurements of c-axis and a-axis oriented films. An estimate of the intrinsic value of lambda of 90 +/- 30 nm was obtained from the dependence of lambda on film thickness. The advantage of this technique is that it allows lambda to be determined nondestructively.

  18. Local Measurement of the Penetration Depth in the Pnictide Superconductor Ba(Fe_0.95 Co_0.05)_2 As_2

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Matsushita, Y.

    2010-01-11

    We use magnetic force microscopy (MFM) to measure the local penetration depth {lambda} in Ba(Fe{sub 0.95}Co{sub 0.05}){sub 2}As{sub 2} single crystals and use scanning SQUID susceptometry to measure its temperature variation down to 0.4 K. We observe that superfluid density {rho}{sub s} over the full temperature range is well described by a clean two-band fully gapped model. We demonstrate that MFM can measure the important and hard-to-determine absolute value of {lambda}, as well as obtain its temperature dependence and spatial homogeneity. We find {rho}{sub s} to be uniform on the submicron scale despite the highly disordered vortex pinning.

  19. Penetration Depth Study of Superconducting Gap Structure of 2H-NbSe2

    NASA Astrophysics Data System (ADS)

    Fletcher, J. D.; Carrington, A.; Diener, P.; Rodière, P.; Brison, J. P.; Prozorov, R.; Olheiser, T.; Giannetta, R. W.

    2007-02-01

    We report measurements of the temperature dependence of both in-plane and out-of-plane penetration depths (λa and λc, respectively) in 2H-NbSe2. Measurements were made with a radio-frequency tunnel diode oscillator circuit at temperatures down to 100 mK. Analysis of the anisotropic superfluid density shows that a reduced energy gap is located on one or more of the quasi-two-dimensional Nb Fermi surface sheets rather than on the Se sheet, in contrast with some previous reports. This result suggests that the gap structure is not simply related to the weak electron-phonon coupling on the Se sheet and is therefore important for microscopic models of anisotropic superconductivity in this compound.

  20. Phase-based Bragg intragrating distributed strain sensor

    NASA Astrophysics Data System (ADS)

    Huang, S.; Ohn, M. M.; Measures, R. M.

    1996-03-01

    A strain-distribution sensing technique based on the measurement of the phase spectrum of the reflected light from a fiber-optic Bragg grating is described. When a grating is subject to a strain gradient, the grating will experience a chirp and therefore the resonant wavelength will vary along the grating, causing wavelength-dependent penetration depth. Because the group delay for each wavelength component is related to its penetration depth and the resonant wavelength is determined by strain, a measured phase spectrum can then indicate the local strain as a function of location within the grating. This phase-based Bragg grating sensing technique offers a powerful new means for studying some important effects over a few millimeters or centimeters in smart structures.

  1. Effect of neutron irradiation on the London penetration depth for polycrystalline Bi(1.8)Pb(0.3)Sr2Ca2Cu3O10 superconductor

    NASA Technical Reports Server (NTRS)

    Ossandon, J. G.; Thompson, J. R.; Sun, Yang Ren; Christen, D. K.; Chakoumakos, B. C.

    1995-01-01

    Magnetization studies of polycrystalline Bi(1.8)Pb(0.3)Sr2Ca2Cu3O10 superconductor, prior to and after neutron irradiation, showed an increase in J(sub c) due to irradiation damage. Analysis of the equilibrium magnetization revealed significant increases in other more fundamental properties. In particular, the London penetration depth increased by approximately 15 percent following irradiation with 8 x 10(exp 16) neutrons/sq cm. Corresponding changes were observed in the upper critical magnetic field H(sub c2). However, the most fundamental thermodynamic property, the superconductive condensation energy F(sub c), was unaffected by the moderate level of neutron-induced damage.

  2. Study of gamma ray energy absorption and exposure buildup factors for ferrites by geometric progression fitting method

    NASA Astrophysics Data System (ADS)

    Raut, S. D.; Awasarmol, V. V.; Shaikh, S. F.; Ghule, B. G.; Ekar, S. U.; Mane, R. S.; Pawar, P. P.

    2018-04-01

    The gamma ray energy absorption and exposure buildup factors (EABF and EBF) were calculated for ferrites such as cobalt ferrite (CoFe2O4), zinc ferrite (ZnFe2O4), nickel ferrite (NiFe2O4) and magnesium ferrite (MgFe2O4) using five parametric geometric progression (G-P fitting) formula in the energy range 0.015-15.00 MeV up to the penetration depth 40 mean free path (mfp). The obtained data of absorption and exposure buildup factors have been studied as a function of incident photon energy and penetration depth. The obtained EABF and EBF data are useful for radiation dosimetry and radiation therapy.

  3. Performance of TenCate Paving interlayers in asphalt concrete pavements.

    DOT National Transportation Integrated Search

    2017-08-01

    As a continued effort of a previously completed project entitled Performance of TenCate Mirafi PGM-G4 Interlayer-Reinforced Asphalt Pavements in Alaska, this project evaluated two newly modified paving interlayers (TruPave and Mirapave) through...

  4. Rheological model analysis on depth of toppling deformation in the anti-dip rock slope

    NASA Astrophysics Data System (ADS)

    Zheng, Da

    2017-04-01

    The failure of the toppling deformation occurred in the layered rock mass, it is a kind of mode of deformation and failure, which is bent towards free direction and gradually develops into the slope under the combined forces of in-situ stress, gravity, and groundwater dynamic (hydrostatic) pressure and so on. The most common toppling deformation is the toppling of ductile bending. Obtaining the developmental depth of bending deformation is of great significance for judging the development scale of the plasmodium and the stability of the slope. At present, the developmental depth of toppling deformation mainly depends on the survey and statistic of the exploration adit, or the simulation of the deformation and failure process through the numerical simulation method, there is little research on the developmental depth of toppling deformation from mechanics point of view. In this paper, with the consideration of the time-sensitive characteristics of developmental process of the toppling deformation, the anti-dip layered slope can be considered as a multi-layer superposition cantilever with fixed end and free end, bending under self-weight and inter-layer stress. Under the premise of the initial stage of rheology of the rock slopes, which is considered to be the limit position of the toppling deformation and development, the Kelvin rheological model, which is usually used to describe the decay creep, is chosen to describe the time-sensitive process of rock slopes. The stress-strain analysis calculation is used to obtain the time-varying expression of a certain point on the rock beam. Furthermore, taking the time to infinity, the depth of the layered rock slopes is calculated as x=4Ccosβ/[2γcosαcosβ - γ2(cos (α + β)+2sin(α + β)tanφ)*((1+n) /2+(1-n) cos2α/ 2)] , which is obtained by using the strain reaches zero as the criterion of the depth at toppling deformation development limit position, combining the time-varying expression of a certain point on the beam. we obtain the mathematic analysis conditions by using the constant positive characteristic of depth of the toppling deformation, The result shows that the depth of the slope toppling deformation is influenced by the rock mass, strata inclination, rock thickness, interfacial friction coefficient, interlayer internal friction angle, slope angel and Poisson 's ratio of rock slopes. The toppling deformation only occurs when 2cosαcosβ-[cos(α + β)+2sin(α + β)tanφ][(1+n)/2+(1-n) cos2α/2]≥0. This study is an exploration to explain the time-sensitive characteristics of toppling deformation by using rheological theory. The conclusion is of great significance for the study of the location of the bending zone, the size of the toppling deformation, the stability analysis and the early identification of the toppling deformation based on the deformation characteristics.

  5. Variable Temperature Infrared Spectroscopy Investigation of Benzoic Acid Interactions with Montmorillonite Clay Interlayer Water.

    PubMed

    Nickels, Tara M; Ingram, Audrey L; Maraoulaite, Dalia K; White, Robert L

    2015-07-01

    Molecular interactions between benzoic acid and cations and water contained in montmorillonite clay interlayer spaces are characterized by using variable temperature diffuse reflection infrared Fourier transform spectroscopy (VT-DRIFTS). Using sample perturbation and difference spectroscopy, infrared spectral changes resulting from removal of interlayer water and associated changes in local benzoic acid environments are identified. Difference spectra features can be correlated with changes in specific molecular vibrations that are characteristic of benzoic acid molecular orientation. Results suggest that the carboxylic acid functionality of benzoic acid interacts with interlayer cations through a bridging water molecule and that this interaction is affected by the nature of the cation present in the clay interlayer space.

  6. Bending stiffness and interlayer shear modulus of few-layer graphene

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Chen, Xiaoming; Yi, Chenglin; Ke, Changhong, E-mail: cke@binghamton.edu

    2015-03-09

    Interlayer shear deformation occurs in the bending of multilayer graphene with unconstrained ends, thus influencing its bending rigidity. Here, we investigate the bending stiffness and interlayer shear modulus of few-layer graphene through examining its self-folding conformation on a flat substrate using atomic force microscopy in conjunction with nonlinear mechanics modeling. The results reveal that the bending stiffness of 2–6 layers graphene follows a square-power relationship with its thickness. The interlayer shear modulus is found to be in the range of 0.36–0.49 GPa. The research findings show that the weak interlayer shear interaction has a substantial stiffening effect for multilayer graphene.

  7. Interface amorphization in hexagonal boron nitride films on sapphire substrate grown by metalorganic vapor phase epitaxy

    NASA Astrophysics Data System (ADS)

    Yang, Xu; Nitta, Shugo; Pristovsek, Markus; Liu, Yuhuai; Nagamatsu, Kentaro; Kushimoto, Maki; Honda, Yoshio; Amano, Hiroshi

    2018-05-01

    Hexagonal boron nitride (h-BN) films directly grown on c-plane sapphire substrates by pulsed-mode metalorganic vapor phase epitaxy exhibit an interlayer for growth temperatures above 1200 °C. Cross-sectional transmission electron microscopy shows that this interlayer is amorphous, while the crystalline h-BN layer above has a distinct orientational relationship with the sapphire substrate. Electron energy loss spectroscopy shows the energy-loss peaks of B and N in both the amorphous interlayer and the overlying crystalline h-BN layer, while Al and O signals are also seen in the amorphous interlayer. Thus, the interlayer forms during h-BN growth through the decomposition of the sapphire at elevated temperatures.

  8. Interlayer exciton optoelectronics in a 2D heterostructure p–n junction

    DOE PAGES

    Ross, Jason S.; Rivera, Pasqual; Schaibley, John; ...

    2016-12-22

    Semiconductor heterostructures are backbones for solid-state-based optoelectronic devices. Recent advances in assembly techniques for van der Waals heterostructures have enabled the band engineering of semiconductor heterojunctions for atomically thin optoelectronic devices. In two-dimensional heterostructures with type II band alignment, interlayer excitons, where Coulomb bound electrons and holes are confined to opposite layers, have shown promising properties for novel excitonic devices, including a large binding energy, micron-scale in-plane drift-diffusion, and a long population and valley polarization lifetime. Here, we demonstrate interlayer exciton optoelectronics based on electrostatically defined lateral p–n junctions in a MoSe 2–WSe 2 heterobilayer. Applying a forward bias enablesmore » the first observation of electroluminescence from interlayer excitons. At zero bias, the p–n junction functions as a highly sensitive photodetector, where the wavelength-dependent photocurrent measurement allows the direct observation of resonant optical excitation of the interlayer exciton. The resulting photocurrent amplitude from the interlayer exciton is about 200 times smaller than the resonant excitation of intralayer exciton. This implies that the interlayer exciton oscillator strength is 2 orders of magnitude smaller than that of the intralayer exciton due to the spatial separation of electron and hole to the opposite layers. Lastly, these results lay the foundation for exploiting the interlayer exciton in future 2D heterostructure optoelectronic devices.« less

  9. Quantum-Dot Light-Emitting Diodes with Nitrogen-Doped Carbon Nanodot Hole Transport and Electronic Energy Transfer Layer.

    PubMed

    Park, Young Ran; Jeong, Hu Young; Seo, Young Soo; Choi, Won Kook; Hong, Young Joon

    2017-04-12

    Electroluminescence efficiency is crucial for the application of quantum-dot light-emitting diodes (QD-LEDs) in practical devices. We demonstrate that nitrogen-doped carbon nanodot (N-CD) interlayer improves electrical and luminescent properties of QD-LEDs. The N-CDs were prepared by solution-based bottom up synthesis and were inserted as a hole transport layer (HTL) between other multilayer HTL heterojunction and the red-QD layer. The QD-LEDs with N-CD interlayer represented superior electrical rectification and electroluminescent efficiency than those without the N-CD interlayer. The insertion of N-CD layer was found to provoke the Förster resonance energy transfer (FRET) from N-CD to QD layer, as confirmed by time-integrated and -resolved photoluminescence spectroscopy. Moreover, hole-only devices (HODs) with N-CD interlayer presented high hole transport capability, and ultraviolet photoelectron spectroscopy also revealed that the N-CD interlayer reduced the highest hole barrier height. Thus, more balanced carrier injection with sufficient hole carrier transport feasibly lead to the superior electrical and electroluminescent properties of the QD-LEDs with N-CD interlayer. We further studied effect of N-CD interlayer thickness on electrical and luminescent performances for high-brightness QD-LEDs. The ability of the N-CD interlayer to improve both the electrical and luminescent characteristics of the QD-LEDs would be readily exploited as an emerging photoactive material for high-efficiency optoelectronic devices.

  10. Bulk density and soil resistance to penetration as affected by commercial thinning in northeastern Washington.

    Treesearch

    Johanna D. Landsberg; Richard E. Miller; Harry W. Anderson; Jeffrey S. Tepp

    2003-01-01

    Bulk density and soil resistance to penetration were measured in ten, 3- to 11-ha operational units in overstocked, mixed-conifer stands in northeast Washington. Resistance was measured with a recording penetrometer to the 33-cm depth (13 in) at 10 stations on each of 8 to 17, 30.5-m-long, randomly located transects in each unit. Subsequently, different combinations of...

  11. The effect of aircraft speed on the penetration of sonic boom noise into a flat ocean

    NASA Technical Reports Server (NTRS)

    Sparrow, Victor W.

    1994-01-01

    As U.S. aircraft manufacturers now have focused their HSCT efforts on overwater supersonic flight, a great deal more must be known about sonic booms propagating overwater and interacting with the ocean. For example, it is thought that atmospheric turbulence effects are often much less severe over water than over land. Another important aspect of the overwater flight problems is the penetration of the sonic boom noise into the ocean, where there could be an environmental impact on sea life. This talk will present a brief review on the penetration of sonic boom noise into a large body of water with a flat surface. It has been determined recently that faster supersonic speeds imply greater penetration of sonic boom noise into the ocean. The new theory is derived from the original Sawyers paper and from the knowledge that for level flight a boom's duration is proportional to the quantity M/(M(exp 2)-1)(exp 3/8) where M is the Mach number. It is found that for depths of 10 m or less, the peak SPL varies less than 6 dB over a wide range of M. For greater depths, 100 m for example, increased Mach numbers may increase the SPL by 15 dB or more.

  12. Drilling, sampling, and sample-handling system for China's asteroid exploration mission

    NASA Astrophysics Data System (ADS)

    Zhang, Tao; Zhang, Wenming; Wang, Kang; Gao, Sheng; Hou, Liang; Ji, Jianghui; Ding, Xilun

    2017-08-01

    Asteroid exploration has a significant importance in promoting our understanding of the solar system and the origin of life on Earth. A unique opportunity to study near-Earth asteroid 99942 Apophis will occur in 2029 because it will be at its perigee. In the current work, a drilling, sampling, and sample-handling system (DSSHS) is proposed to penetrate the asteroid regolith, collect regolith samples at different depths, and distribute the samples to different scientific instruments for in situ analysis. In this system, a rotary-drilling method is employed for the penetration, and an inner sampling tube is utilized to collect and discharge the regolith samples. The sampling tube can deliver samples up to a maximum volume of 84 mm3 at a maximum penetration depth of 300 mm to 17 different ovens. To activate the release of volatile substances, the samples will be heated up to a temperature of 600 °C by the ovens, and these substances will be analyzed by scientific instruments such as a mass spectrometer, an isotopic analyzer, and micro-cameras, among other instruments. The DSSHS is capable of penetrating rocks with a hardness value of six, and it can be used for China's asteroid exploration mission in the foreseeable future.

  13. Internal Waves, South China Sea

    NASA Technical Reports Server (NTRS)

    1983-01-01

    Subsurface ocean currents, frequently referred to as internal waves, are frequently seen from space under the right lighting conditions when depth penetration can be achieved. These internal waves observed in the South China Sea off the SE coast of the island of Hainan (18.5N, 110.5E) visibly demonstrate turbidity in the ocean's depths at the confluence of conflicting currents.

  14. The relation of mechanical properties of wood and nosebar pressure in the production of veneer

    Treesearch

    Charles W. McMillin

    1958-01-01

    Observations of checking frequency, depth of check penetration, veneer thickness, and surface quality were made at 20 machining conditions. An inverse relationship between depth of check and frequency of checking was established. The effect of cutting temperature was demonstrated, and strength in compression perpendicular to the grain, tension perpendicular to the...

  15. Synergistic Use of Spacecraft Telecom Links for Collection of Planetary Radar Science Data

    NASA Astrophysics Data System (ADS)

    Asmar, S.; Bell, D. J.; Chahat, N. E.; Decrossas, E.; Dobreva, T.; Duncan, C.; Ellliot, H.; Jin, C.; Lazio, J.; Miller, J.; Preston, R.

    2017-12-01

    On multiple solar system missions, radar instruments have been used to probe subsurface geomorphology and to infer chemical composition based on the dielectric signature derived from the reflected signal. Example spacecraft radar instruments are the 90 MHz CONSERT radar used to probe the interior of Comet 67P/Churyumov-Gerasimenko to a depth of 760m, the 20 MHz SHARAD instrument used to investigate Mars subsurface ice features from Mars orbit at depths of 300 to 3000 meters and the upcoming RIMFAX 150 MHz to 1200 MHz ground penetrating radar that will ride on the Mars 2020 rover investigating to a depth of 10m below the rover. In all of these applications, the radar frequency and signal structures were chosen to match science goals of desired depth of penetration and spatial resolution combined with the expected subsurface materials and structures below the surface. Recently, JPL investigators have proposed a new radar science paradigm, synergistic use of the telecom hardware and telecom links to collect bistatic or monostatic radar signatures. All JPL spacecraft employ telecom hardware that operates at UHF (400 MHz and 900 MHz), X-band (8 GHz) or Ka-band (32 GHz). Using existing open-loop record functions in these radios, the telecom hardware can be used to capture opportunistic radar signatures from telecom signals penetrating the surface and reflecting off of subsurface structures. This paper reports on telecom strategies, radar science applications and recent laboratory and field tests to demonstrate the effectiveness of telecom link based radar data collection.

  16. Penetration of Chlorhexidine into Human Skin ▿

    PubMed Central

    Karpanen, T. J.; Worthington, T.; Conway, B. R.; Hilton, A. C.; Elliott, T. S. J.; Lambert, P. A.

    2008-01-01

    This study evaluated a model of skin permeation to determine the depth of delivery of chlorhexidine into full-thickness excised human skin following topical application of 2% (wt/vol) aqueous chlorhexidine digluconate. Skin permeation studies were performed on full-thickness human skin using Franz diffusion cells with exposure to chlorhexidine for 2 min, 30 min, and 24 h. The concentration of chlorhexidine extracted from skin sections was determined to a depth of 1,500 μm following serial sectioning of the skin using a microtome and analysis by high-performance liquid chromatography. Poor penetration of chlorhexidine into skin following 2-min and 30-min exposures to chlorhexidine was observed (0.157 ± 0.047 and 0.077 ± 0.015 μg/mg tissue within the top 100 μm), and levels of chlorhexidine were minimal at deeper skin depths (less than 0.002 μg/mg tissue below 300 μm). After 24 h of exposure, there was more chlorhexidine within the upper 100-μm sections (7.88 ± 1.37 μg/mg tissue); however, the levels remained low (less than 1 μg/mg tissue) at depths below 300 μm. There was no detectable penetration through the full-thickness skin. The model presented in this study can be used to assess the permeation of antiseptic agents through various layers of skin in vitro. Aqueous chlorhexidine demonstrated poor permeation into the deeper layers of the skin, which may restrict the efficacy of skin antisepsis with this agent. This study lays the foundation for further research in adopting alternative strategies for enhanced skin antisepsis in clinical practice. PMID:18676882

  17. Photothermal optical coherence tomography of epidermal growth factor receptor in live cells using immunotargeted gold nanospheres

    NASA Astrophysics Data System (ADS)

    Skala, Melissa C.; Crow, Matthew J.; Wax, Adam; Izatt, Joseph A.

    2009-02-01

    Molecular imaging is a powerful tool for investigating disease processes and potential therapies in both in vivo and in vitro systems. However, high resolution molecular imaging has been limited to relatively shallow penetration depths that can be accessed with microscopy. Optical coherence tomography (OCT) is an optical analogue to ultrasound with relatively good penetration depth (1-2 mm) and resolution (~1-10 μm). We have developed and characterized photothermal OCT as a molecular contrast mechanism that allows for high resolution molecular imaging at deeper penetration depths than microscopy. Our photothermal system consists of an amplitude-modulated heating beam that spatially overlaps with the focused spot of the sample arm of a spectral-domain OCT microscope. Validation experiments in tissue-like phantoms containing gold nanospheres that absorb at 532 nm revealed a sensitivity of 14 parts per million nanospheres (weight/weight) in a tissue-like environment. The nanospheres were then conjugated to anti-EGFR, and molecular targeting was confirmed in cells that over-express EGFR (MDA-MB-468) and cells that express low levels of EGFR (MDA-MB-435). Molecular imaging in three-dimensional tissue constructs was confirmed with a significantly lower photothermal signal (p<0.0001) from the constructs composed of cells that express low levels of EGFR compared to the over-expressing cell constructs (300% signal increase). This technique could potentially augment confocal and multiphoton microscopy as a method for deep-tissue, depth-resolved molecular imaging with relatively high resolution and target sensitivity, without photobleaching or cytotoxicity.

  18. Evaluation of stone/RAP interlayers under accelerated loading : technical summary.

    DOT National Transportation Integrated Search

    2008-08-01

    The primary objective of this study was to determine the effectiveness of using an untreated RAP interlayer in lieu of a stone interlayer in a soil-cement asphalt pavement structure under accelerated loading. The secondary objective was to investigat...

  19. Structural evolution of Ti destroyable interlayer in large-size diamond film deposition by DC arc plasma jet

    NASA Astrophysics Data System (ADS)

    Guo, Jianchao; Li, Chengming; Liu, Jinlong; Wei, Junjun; Chen, Liangxian; Hua, Chenyi; Yan, Xiongbo

    2016-05-01

    The addition of titanium (Ti) interlayer was verified to reduce the residual stress of diamond films by self-fracturing and facilitate the harvest of a crack-free free-standing diamond film prepared by direct current (DC) arc plasma jet. In this study, the evolution of the Ti interlayer between large-area diamond film and substrate was studied and modeled in detail. The evolution of the interlayer was found to be relevant to the distribution of the DC arc plasma, which can be divided into three areas (arc center, arc main, and arc edge). The formation rate of titanium carbide (TiC) in the arc main was faster than in the other two areas and resulted in the preferred generation of crack in the diamond film in the arc main during cooling. Sandwich structures were formed along with the growth of TiC until the complete transformation of the Ti interlayer. The interlayer released stress via self-fracture. Avoiding uneven fragile regions that formed locally in the interlayer and achieving cooperatively released stress are crucial for the preparation of large crack-free diamond films.

  20. Enhanced performance of solution-processed organic thin-film transistors with a low-temperature-annealed alumina interlayer between the polyimide gate insulator and the semiconductor.

    PubMed

    Yoon, Jun-Young; Jeong, Sunho; Lee, Sun Sook; Kim, Yun Ho; Ka, Jae-Won; Yi, Mi Hye; Jang, Kwang-Suk

    2013-06-12

    We studied a low-temperature-annealed sol-gel-derived alumina interlayer between the organic semiconductor and the organic gate insulator for high-performance organic thin-film transistors. The alumina interlayer was deposited on the polyimide gate insulator by a simple spin-coating and 200 °C-annealing process. The leakage current density decreased by the interlayer deposition: at 1 MV/cm, the leakage current densities of the polyimide and the alumina/polyimide gate insulators were 7.64 × 10(-7) and 3.01 × 10(-9) A/cm(2), respectively. For the first time, enhancement of the organic thin-film transistor performance by introduction of an inorganic interlayer between the organic semiconductor and the organic gate insulator was demonstrated: by introducing the interlayer, the field-effect mobility of the solution-processed organic thin-film transistor increased from 0.35 ± 0.15 to 1.35 ± 0.28 cm(2)/V·s. Our results suggest that inorganic interlayer deposition could be a simple and efficient surface treatment of organic gate insulators for enhancing the performance of solution-processed organic thin-film transistors.

  1. Effects of Electrospun Carbon Nanofibers' Interlayers on High-Performance Lithium-Sulfur Batteries.

    PubMed

    Gao, Tianji; Le, TrungHieu; Yang, Ying; Yu, Zhihao; Huang, Zhenghong; Kang, Feiyu

    2017-03-31

    Two different interlayers were introduced in lithium-sulfur batteries to improve the cycling stability with sulfur loading as high as 80% of total mass of cathode. Melamine was recommended as a nitrogen-rich (N-rich) amine component to synthesize a modified polyacrylic acid (MPAA). The electrospun MPAA was carbonized into N-rich carbon nanofibers, which were used as cathode interlayers, while carbon nanofibers from PAA without melamine was used as an anode interlayer. At the rate of 0.1 C, the initial discharge capacity with two interlayers was 983 mAh g -1 , and faded down to 651 mAh g -1 after 100 cycles with the coulombic efficiency of 95.4%. At the rate of 1 C, the discharge capacity was kept to 380 mAh g -1 after 600 cycles with a coulombic efficiency of 98.8%. It apparently demonstrated that the cathode interlayer is extremely effective at shutting down the migration of polysulfide ions. The anode interlayer induced the lithium ions to form uniform lithium metal deposits confined on the fiber surface and in the bulk to strengthen the cycling stability of the lithium metal anode.

  2. High-Performance Lithium-Sulfur Batteries with a Self-Assembled Multiwall Carbon Nanotube Interlayer and a Robust Electrode-Electrolyte Interface.

    PubMed

    Kim, Hee Min; Hwang, Jang-Yeon; Manthiram, Arumugam; Sun, Yang-Kook

    2016-01-13

    Elemental sulfur electrode has a huge advantage in terms of charge-storage capacity. However, the lack of electrical conductivity results in poor electrochemical utilization of sulfur and performance. This problem has been overcome to some extent previously by using a bare multiwall carbon nanotube (MWCNT) paper interlayer between the sulfur cathode and the polymeric separator, resulting in good electron transport and adsorption of dissolved polysulfides. To advance the interlayer concept further, we present here a self-assembled MWCNT interlayer fabricated by a facile, low-cost process. The Li-S cells fabricated with the self-assembled MWCNT interlayer and a high loading of 3 mg cm(-2) sulfur exhibit a first discharge specific capacity of 1112 mAh g(-1) at 0.1 C rate and retain 95.8% of the capacity at 0.5 C rate after 100 cycles as the self-assembled MWCNT interlayer facilitates good interfacial contact between the interlayer and the sulfur cathode and fast electron and lithium-ion transport while trapping and reutilizing the migrating polysulfides. The approach presented here has the potential to advance the commercialization feasibility of the Li-S batteries.

  3. Effects of Electrospun Carbon Nanofibers’ Interlayers on High-Performance Lithium–Sulfur Batteries

    PubMed Central

    Gao, Tianji; Le, TrungHieu; Yang, Ying; Yu, Zhihao; Huang, Zhenghong; Kang, Feiyu

    2017-01-01

    Two different interlayers were introduced in lithium–sulfur batteries to improve the cycling stability with sulfur loading as high as 80% of total mass of cathode. Melamine was recommended as a nitrogen-rich (N-rich) amine component to synthesize a modified polyacrylic acid (MPAA). The electrospun MPAA was carbonized into N-rich carbon nanofibers, which were used as cathode interlayers, while carbon nanofibers from PAA without melamine was used as an anode interlayer. At the rate of 0.1 C, the initial discharge capacity with two interlayers was 983 mAh g−1, and faded down to 651 mAh g−1 after 100 cycles with the coulombic efficiency of 95.4%. At the rate of 1 C, the discharge capacity was kept to 380 mAh g−1 after 600 cycles with a coulombic efficiency of 98.8%. It apparently demonstrated that the cathode interlayer is extremely effective at shutting down the migration of polysulfide ions. The anode interlayer induced the lithium ions to form uniform lithium metal deposits confined on the fiber surface and in the bulk to strengthen the cycling stability of the lithium metal anode. PMID:28772731

  4. Penetration of ASM 981 in canine skin: a comparative study.

    PubMed

    Gutzwiller, Meret E Ricklin; Reist, Martin; Persohn, Elke; Peel, John E; Roosje, Petra J

    2006-01-01

    ASM 981 has been developed for topical treatment of inflammatory skin diseases. It specifically inhibits the production and release of pro-inflammatory cytokines. We measured the skin penetration of ASM 981 in canine skin and compared penetration in living and frozen skin. To make penetration of ASM 981 visible in dog skin, tritium labelled ASM 981 was applied to a living dog and to defrosted skin of the same dog. Using qualitative autoradiography the radioactive molecules were detected in the lumen of the hair follicles until the infundibulum, around the superficial parts of the hair follicles and into a depth of the dermis of 200 to 500 microm. Activity could not be found in deeper parts of the hair follicles, the dermis or in the sebaceous glands. Penetration of ASM 981 is low in canine skin and is only equally spread in the upper third of the dermis 24 hours after application. Penetration in frozen skin takes even longer than in living canine skin but shows the same distribution.

  5. Optical microangiography reveals collateral blood perfusion dynamics in mouse cerebral cortex after focal stroke

    NASA Astrophysics Data System (ADS)

    Baran, Utku; Li, Yuandong; Wang, Ruikang K.

    2015-03-01

    Arteriolo-arteriolar anastomosis's role in regulating blood perfusion through penetrating arterioles during stroke is yet to be discovered. We apply ultra-high sensitive optical microangiography (UHS-OMAG) and Doppler optical microangiography (DOMAG) techniques to evaluate vessel diameter and red blood cell velocity changes in large number of pial and penetrating arterioles in relation with arteriolo-arteriolar anastomosis (AAA) during and after focal stroke. Thanks to the high sensitivity of UHS-OMAG, we were able to image pial microvasculature up to capillary level through a cranial window (9 mm2), and DOMAG provided clear image of penetrating arterioles up to 500μm depth. Results showed that penetrating arterioles close to a strong AAA connection dilate whereas penetrating arterioles constrict significantly in weaker AAA regions. These results suggest that AAA plays a major role in active regulation of the pial arterioles, and weaker AAA connections lead to poor blood perfusion to penumbra through penetrating arterioles.

  6. Sunlight penetration through the Martian polar caps: Effects on the thermal and frost budgets

    NASA Technical Reports Server (NTRS)

    Lindner, Bernhard Lee

    1992-01-01

    An energy balance model of the seasonal polar caps on Mars is modified to include penetration of solar radiation into and through the ice. Penetration of solar radiation has no effect on subsurface temperature or total frost sublimation if seasonal ice overlies a dust surface. An effect is noted for seasonal ice which overlies the residual polar caps. For the case of an exposed water-ice residual polar cap, the temperature at depth is calculated to be up to several degrees warmer and the calculated lifetime of seasonal CO2 frost is slightly lower when penetration of sunlight is properly treated in the model. For the case of a residual polar cap which is perennially covered by CO2 frost, the calculated lifetime of seasonal CO2 frost is very slightly increased as a result of sunlight penetration through the ice. Hence, penetration of sunlight into the ice helps to stabilize the observed dichotomy in the residual polar caps on Mars, although it is a small effect.

  7. Sunlight penetration through the Martian polar caps - Effects on the thermal and frost budgets

    NASA Technical Reports Server (NTRS)

    Lindner, Bernhard L.

    1992-01-01

    An energy balance model of the seasonal polar caps on Mars is modified to include penetration of solar radiation into and through the ice. Penetration of solar radiation has no effect on subsurface temperature or total frost sublimation if seasonal ice overlies a dust surface. An effect is noted for seasonal ice which overlies the residual polar caps. For the case of an exposed water-ice residual polar cap, the temperature at depth is calculated to be up to several degrees warmer, and the calculated lifetime of seasonal CO2 frost is slightly lower when penetration of sunlight is properly treated in the model. For the case of a residual polar cap which is perennially covered by CO2 frost, the calculated lifetime of seasonal CO2 frost is very slightly increased as a result of sunlight penetration through the ice. Hence, penetration of sunlight into the ice helps to stabilize the observed dichotomy in the residual polar caps on Mars, although it is a small effect.

  8. Application of Airborne Hydrographic Laser Scanning for Mapping Shallow Water Riverine Environments in the Pacific Northwest, United States

    NASA Astrophysics Data System (ADS)

    Cooper, C.; Nayegandhi, A.; Faux, R.

    2013-12-01

    Small-footprint, green wavelength airborne LiDAR systems can provide seamless topography across the land-water interface at very high spatial resolution. These data have the potential to improve floodplain modeling, fisheries habitat assessments, stream restoration efforts, and other applications by continuously mapping shallow water depths that are difficult or impossible to measure using traditional ground-based or water-borne survey techniques. WSI (Corvallis, Oregon) in collaboration with Dewberry, (Tampa, Florida) and Riegl (Orlando, Florida), deployed the Riegl VQ-820-G hydrographic airborne laser scanner to map riverine and lacustrine environments from Oregon to Minnesota. Discussion will focus on the ability to accurately map depth and underwater structure, as well as riparian vegetation and terrain under different conditions. Results indicate that depth penetration varies with both water (i.e. clarity and surface conditions) and bottom conditions (i.e. substrate, depth, and landform). Depth penetration was typically limited to 1 Secchi depth or less across selected project areas. As an example, the green LiDAR system effectively mapped 83% of a shallow water river system, the Sandy River, with typical depths ranging from 0-2.5 meters. WSI will show quantitative comparisons of Green LiDAR surveys against more traditional methods such as rod or sonar surveys. WSI will also discuss advantages and limitations of Green LiDAR surveys for bathymetric modeling including survey accuracy, density, and efficiency along with data processing challenges not inherent with traditional NIR LiDAR processing.

  9. Tidal disruption of inclined or eccentric binaries by massive black holes

    NASA Astrophysics Data System (ADS)

    Brown, Harriet; Kobayashi, Shiho; Rossi, Elena M.; Sari, Re'em

    2018-07-01

    Binary stars that are on close orbits around massive black holes (MBHs) such as Sgr A* in the centre of the Milky Way are liable to undergo tidal disruption and eject a hypervelocity star. We study the interaction between such an MBH and circular binaries for general binary orientations and penetration depths (i.e. binaries penetrate into the tidal radius around the BH). We show that for very deep penetrators, almost all binaries are disrupted when the binary rotation axis is roughly oriented towards the BH or it is in the opposite direction. The surviving chance becomes significant when the angle between the binary rotation axis and the BH direction is between 0.15π and 0.85π. The surviving chance is as high as ˜20 per cent when the binary rotation axis is perpendicular to the BH direction. However, for shallow penetrators, the highest disruption chance is found in such a perpendicular case, especially in the prograde case. This is because the dynamics of shallow penetrators is more sensitive to the relative orientation of the binary and orbital angular momenta. We provide numerical fits to the disruption probability and energy gain at the BH encounter as a function of the penetration depth. The latter can be simply rescaled in terms of binary masses, their initial separation, and the binary-to-BH mass ratio to evaluate the ejection velocity of a binary members in various systems. We also investigate the disruption of coplanar, eccentric binaries by an MBH. It is shown that for highly eccentric binaries retrograde orbits have a significantly increased disruption probability and ejection velocities compared to the circular binaries.

  10. Tidal Disruption of Inclined or Eccentric Binaries by Massive Black Holes

    NASA Astrophysics Data System (ADS)

    Brown, Harriet; Kobayashi, Shiho; Rossi, Elena M.; Sari, Re'em

    2018-04-01

    Binary stars that are on close orbits around massive black holes (MBH) such as Sgr A* in the centre of the Milky Way are liable to undergo tidal disruption and eject a hypervelocity star. We study the interaction between such a MBH and circular binaries for general binary orientations and penetration depths (i.e. binaries penetrate into the tidal radius around the BH). We show that for very deep penetrators, almost all binaries are disrupted when the binary rotation axis is roughly oriented toward the BH or it is in the opposite direction. The surviving chance becomes significant when the angle between the binary rotation axis and the BH direction is between 0.15π and 0.85π. The surviving chance is as high as ˜20% when the binary rotation axis is perpendicular to the BH direction. However, for shallow penetrators, the highest disruption chance is found in such a perpendicular case, especially in the prograde case. This is because the dynamics of shallow penetrators is more sensitive to the relative orientation of the binary and orbital angular momenta. We provide numerical fits to the disruption probability and energy gain at the the BH encounter as a function of the penetration depth. The latter can be simply rescaled in terms of binary masses, their initial separation and the binary-to-BH mass ratio to evaluate the ejection velocity of a binary members in various systems. We also investigate the disruption of coplanar, eccentric binaries by a MBH. It is shown that for highly eccentric binaries retrograde orbits have a significantly increased disruption probability and ejection velocities compared to the circular binaries.

  11. Penetration of fast projectiles into resistant media: From macroscopic to subatomic projectiles

    NASA Astrophysics Data System (ADS)

    Gaite, José

    2017-09-01

    The penetration of a fast projectile into a resistant medium is a complex process that is suitable for simple modeling, in which basic physical principles can be profitably employed. This study connects two different domains: the fast motion of macroscopic bodies in resistant media and the interaction of charged subatomic particles with matter at high energies, which furnish the two limit cases of the problem of penetrating projectiles of different sizes. These limit cases actually have overlapping applications; for example, in space physics and technology. The intermediate or mesoscopic domain finds application in atom cluster implantation technology. Here it is shown that the penetration of fast nano-projectiles is ruled by a slightly modified Newton's inertial quadratic force, namely, F ∼v 2 - β, where β vanishes as the inverse of projectile diameter. Factors essential to penetration depth are ratio of projectile to medium density and projectile shape.

  12. Stability and Process of Destruction of Compressed Plate of Layered Composite Materials With Defects

    NASA Astrophysics Data System (ADS)

    Bokhoeva, L. A.; Rogov, V. E.; Chermoshentseva, A. S.; Lobanov, D. V.

    2016-08-01

    Interlayer defects in composite materials are a pressing problem, which affecting their performance characteristics. In this research, we considered the problem of the stability and of the fracture process of the compressed thin plate made of laminated composite materials with the interlayer defects. In this research we had got a critical equation for a plate with interlayer defect. The experiment showed the effect and the quantity of nano-dispersed additives on the mechanical properties of composite materials with interlayer defects.

  13. Quantitative detection of caffeine in human skin by confocal Raman spectroscopy--A systematic in vitro validation study.

    PubMed

    Franzen, Lutz; Anderski, Juliane; Windbergs, Maike

    2015-09-01

    For rational development and evaluation of dermal drug delivery, the knowledge of rate and extent of substance penetration into the human skin is essential. However, current analytical procedures are destructive, labor intense and lack a defined spatial resolution. In this context, confocal Raman microscopy bares the potential to overcome current limitations in drug depth profiling. Confocal Raman microscopy already proved its suitability for the acquisition of qualitative penetration profiles, but a comprehensive investigation regarding its suitability for quantitative measurements inside the human skin is still missing. In this work, we present a systematic validation study to deploy confocal Raman microscopy for quantitative drug depth profiling in human skin. After we validated our Raman microscopic setup, we successfully established an experimental procedure that allows correlating the Raman signal of a model drug with its controlled concentration in human skin. To overcome current drawbacks in drug depth profiling, we evaluated different modes of peak correlation for quantitative Raman measurements and offer a suitable operating procedure for quantitative drug depth profiling in human skin. In conclusion, we successfully demonstrate the potential of confocal Raman microscopy for quantitative drug depth profiling in human skin as valuable alternative to destructive state-of-the-art techniques. Copyright © 2015 Elsevier B.V. All rights reserved.

  14. Site 766: Sedimentology

    USGS Publications Warehouse

    ,

    1990-01-01

    Site 766 is located at the base of the steep western margin of the Exmouth Plateau. The oldest sediment penetrated at Site 766, in Section 123-766A-49R-4 at 66 cm (466.7 mbsf), is uppermost Valanginian sandstone and siltstone, alternating with inclined basaltic intrusions (see "Igneous Rock Lithostratigraphy" section, this chapter). The uppermost sediment/basalt interface occurs in Section 123-766A-48R-6 at 129 cm (460.6 mbsf) At least 300 m (approximately 65%) of the sediments penetrated accumulated during the Lower Cretaceous, compared with less than 150 m thereafter. At Site 765, on the Argo Abyssal Plain, the Lower Cretaceous also is slightly more than 300 m thick. However, approximately 65% of the total sediment column at this site accumulated after the Lower Cretaceous, primarily during the Neogene. The sedimentation history, based on the age and present depth of basement(?) and time-depth relationship for oceanic crust, suggests that Site 766 began at a depth of about 800 m. However, the presence of shallow marine components in the oldest lithologic unit, if not redeposited, suggests that initial depths were shallower. Site 766 appears to have remained above or near the carbonate compensation depth (CCD) throughout its history, whereas Site 765 may have started near the CCD, but remained below it throughout most of its history.

  15. Hypervelocity penetration against mechanical properties of target materials

    NASA Astrophysics Data System (ADS)

    Kamarudin, Khairul Hasni; Abdullah, Mohamad Faizal; Zaidi, Ahmad Mujahid Ahmad; Nor, Norazman M.; Ismail, Ariffin; Yusof, Mohammed Alias; Hilmi, Ahmad Humaizi

    2018-02-01

    This paper study the mechanical properties behavior of metal plates against hypervelocity penetration caused by shaped charge. Five different materials were used as target specimen fabricated from welded stacks of material plates, namely Rolled Homogeneous Armor (RHA), Hardox-500, mild steel, aluminum and brass. Specimens had undergone an initial monolithic test consist of tensile tests and microstructure observations, followed by series of hydrodynamics penetration blast tests using shape charge mechanism. Results from blast test shows that the least penetrated specimen is RHA (58mm) followed by Hardox-500 (92 mm), mild steel (110 mm), Brass (155 mm) and aluminum 238 mm). Comparing these with the specimen yield strength from the tensile test results shows that Hardox-500 has higher yield strength (Sy) followed by RHA, mild steel, brass and aluminum, which are 1370 MPa, 1320 MPa, 280,221 respectively, which are not inversely proportional to the penetration. However, the ultimate tensile strength (Sut) where the RHA were the highest followed by Hardox-500, mild steel, brass and aluminum, were inversely proportional with the depth of penetration. The penetration results also show consistence relation with energy absorption.

  16. Parametric effect on the mixing of the combination of a hydrogen porthole with an air porthole in transverse gaseous injection flow fields

    NASA Astrophysics Data System (ADS)

    Li, Lang-quan; Huang, Wei; Yan, Li; Li, Shi-bin

    2017-10-01

    The dual transverse injection system with a front hydrogen porthole and a rear air porthole arranged in tandem is proposed, and this is a realistic approach for mixing enhancement and penetration improvement of transverse injection in a scramjet combustor. The influence of this dual transverse injection system on mixing characteristics has been evaluated numerically based on grid independency analysis and code validation. The numerical approach employed in the current study has been validated against the available experimental data in the open literature, and the predicted wall static pressure distributions show reasonable agreement with the experimental data for the cases with different jet-to-crossflow pressure ratios. The obtained results predicted by the three-dimensional Reynolds-average Navier - Stokes (RANS) equations coupled with the two equation k-ω shear stress transport (SST) turbulence model show that the air pothole has an great impact on penetration depth and mixing efficiency, and the effect of air jet on flow field varies with different values of the aspect ratio. The air porthole with larger aspect ratio can increase the fuel penetration depth. However, when the aspect ratio is relatively small, the fuel penetration depth decreases, and even smaller than that of the single injection system. At the same time, the air pothole has a highly remarkable improvement on mixing efficiency, especially in the near field. The smaller the aspect ratio of the air porthole is, the higher the mixing efficiency in the near field is. This is due to its larger circulation in the near field. The dual injection system owns more losses of stagnation pressure than the single injection system.

  17. Regolith stratigraphy at the Chang'E-3 landing site as seen by lunar penetrating radar

    NASA Astrophysics Data System (ADS)

    Fa, Wenzhe; Zhu, Meng-Hua; Liu, Tiantian; Plescia, Jeffrey B.

    2015-12-01

    The Chang'E-3 lunar penetrating radar (LPR) observations at 500 MHz reveal four major stratigraphic zones from the surface to a depth of ~20 m along the survey line: a layered reworked zone (<1 m), an ejecta layer (~2-6 m), a paleoregolith layer (~4-11 m), and the underlying mare basalts. The reworked zone has two to five distinct layers and consists of surface regolith. The paleoregolith buried by the ejecta from a 500 m crater is relatively homogenous and contains only a few rocks. Population of buried rocks increases with depth to ~2 m at first, and then decreases with depth, representing a balance between initial deposition of the ejecta and later turnover of the regolith. Combining with the surface age, the LPR observations indicate a mean accumulation rate of about 5-10 m/Gyr for the surface regolith, which is at least 4-8 times larger than previous estimation.

  18. Fractional laser microablation of skin: increasing the efficiency of transcutaneous delivery of particles

    NASA Astrophysics Data System (ADS)

    Genina, E. A.; Dolotov, L. E.; Bashkatov, A. N.; Tuchin, V. V.

    2016-06-01

    We study several regimes of fractional laser microablation using a pulsed Er : YAG laser for producing microchannels of different depth and incisions that allow transcutaneous delivery of particles of different size, namely, Al2O3 (27 μm), ZrO2 (smaller than 5 μm) and TiO2 (smaller than 100 nm). The shock wave regime was used both for enhancing the penetration of particles into the ablation zones and as an independent method of particle delivery into the skin. Based on optical coherence tomography we assessed the coherent depth of particle detection in the skin in 2 hours, 3 days and 10 days after the administration. The maximal localisation depth (up to 450 μm) was obtained for TiO2 nanoparticles in the regime of incisions with enhancement of particle penetration by pulses of a multiple-beam hydrodynamic shock wave. The results of the study can be useful for developing new methods of transcutaneous delivery of micro- and nanocarriers of medicinal preparations.

  19. Nontrivial Nature and Penetration Depth of Topological Surface States in SmB6 Thin Films

    NASA Astrophysics Data System (ADS)

    Liu, Tao; Li, Yufan; Gu, Lei; Ding, Junjia; Chang, Houchen; Janantha, P. A. Praveen; Kalinikos, Boris; Novosad, Valentyn; Hoffmann, Axel; Wu, Ruqian; Chien, C. L.; Wu, Mingzhong

    2018-05-01

    The nontrivial feature and penetration depth of the topological surface states (TSS) in SmB6 were studied via spin pumping. The experiments used SmB6 thin films grown on the bulk magnetic insulator Y3Fe5O12 (YIG). Upon the excitation of magnetization precession in the YIG, a spin current is generated in the SmB6 that produces, via spin-orbit coupling, a lateral electrical voltage in the film. This spin-pumping voltage signal becomes considerably stronger as the temperature decreases from 150 to 10 K, and such an enhancement most likely originates from the spin-momentum locking of the TSS and may thereby serve as evidence for the nontrivial nature of the TSS. The voltage data also show a unique film thickness dependence that suggests a TSS depth of ˜32 nm . The spin-pumping results are supported by transport measurements and analyses using a tight binding model.

  20. Structural charge site influence on the interlayer hydration of expandable three-sheet clay minerals

    USGS Publications Warehouse

    Kerns, Raymond L.; Mankin, Charles J.

    1968-01-01

    Previous investigations have demonstrated the influences of interlayer cation composition, relative humidity, temperature, and magnitude of interlayer surface charge on the interlayer hydration of montmorillonites and vermiculites. It has been suggested that the sites of layer charge deficiencies may also have an influence upon the amount of hydration that can take place in the interlayers of expandable clay minerals. If the interlayer cation-to-layer bonds are considered as ideally electrostatic, the magnitude of the forces resisting expansion may be expressed as a form of Coulomb's law. If this effect is significant, expandable structures in which the charge-deficiency sites are predominantly in the tetrahedral sheet should have less pronounced swelling properties than should structures possessing charge deficiencies located primarily in the octahedral sheet.Three samples that differed in location of layer charge sites were selected for study. An important selection criterion was a non-correlation between tetrahedral charge sites and high surface-charge density, and between octahedral charge sites and low surface-charge density.The effects of differences in interlayer cation composition were eliminated by saturating portions of each sample with the same cations. Equilibrium (001) d values at controlled constant humidities were used as a measure of the relative degree of interlayer hydration.Although no correlation could be made between the degree of interlayer hydration and total surface-charge density, the investigation does not eliminate total surface-charge density as being significant to the swelling properties of three-sheet clay-mineral structures. The results do indicate a correlation between more intense expandability and predominance of charge deficiencies in the octahedral sheet. Conversely, less intense swelling behavior is associated with predominantly tetrahedral charge deficiencies.

  1. Preparation and Bond Properties of Thermal Barrier Coatings on Mg Alloy with Sprayed Al or Diffused Mg-Al Intermetallic Interlayer

    NASA Astrophysics Data System (ADS)

    Fan, Xizhi; Wang, Ying; Zou, Binglin; Gu, Lijian; Huang, Wenzhi; Cao, Xueqiang

    2014-02-01

    Sprayed Al or diffused Mg-Al layer was designed as interlayer between the thermal barrier coatings (TBCs) and Mg alloy substrate. The effects of the interlayer on the bond properties of the coats were investigated. Al layers were prepared by arc spraying and atmospheric plasma spraying (APS), respectively. Mg-Al diffused layer was obtained after the heat treatment of the sprayed sample (Mg alloy with APS Al coat) at 400 °C. The results show that sprayed Al interlayer does not improve the bond stability of TBCs. The failure of the TBCs on Mg alloy with Al interlayer occurs mainly due to the low strength of Al layer. Mg-Al diffused layer improves corrosion resistance of substrate and the bond interface. The TBCs on Mg alloy with Mg-Al diffused interlayer shows better bond stability than the sample of which the TBCs is directly sprayed on Mg alloy substrate by APS.

  2. Mechanism Responsible for Intercalation of Dimethyl Sulfoxide in Kaolinite: Molecular Dynamics Simulations.

    PubMed

    Zhang, Shuai; Liu, Qinfu; Cheng, Hongfei; Gao, Feng; Liu, Cun; Teppen, Brian J

    2018-01-01

    Intercalation is the promising strategy to expand the interlayer region of kaolinite for their further applications. Herein, the adaptive biasing force (ABF) accelerated molecular dynamics simulations were performed to calculate the free energies involved in the kaolinite intercalation by dimethyl sulfoxide (DMSO). Additionally, the classical all atom molecular dynamics simulations were carried out to calculate the interfacial interactions between kaolinite interlayer surfaces and DMSO with the aim at exploring the underlying force that drives the DMSO to enter the interlayer space. The results showed that the favorable interaction of DMSO with both kaolinite interlayer octahedral surface and tetrahedral surface can help in introducing DMSO enter kaolinite interlayer. The hydroxyl groups on octahedral surface functioned as H-donors attracting the S=O groups of DMSO through hydrogen bonding interaction. The tetrahedral surface featuring hydrophobic property attracted the methyl groups of DMSO through hydrophobic interaction. The results provided a detailed picture of the energetics and interlayer structure of kaolinite-DMSO intercalate.

  3. Interlayer orientation-dependent light absorption and emission in monolayer semiconductor stacks

    PubMed Central

    Heo, Hoseok; Sung, Ji Ho; Cha, Soonyoung; Jang, Bo-Gyu; Kim, Joo-Youn; Jin, Gangtae; Lee, Donghun; Ahn, Ji-Hoon; Lee, Myoung-Jae; Shim, Ji Hoon; Choi, Hyunyong; Jo, Moon-Ho

    2015-01-01

    Two-dimensional stacks of dissimilar hexagonal monolayers exhibit unusual electronic, photonic and photovoltaic responses that arise from substantial interlayer excitations. Interband excitation phenomena in individual hexagonal monolayer occur in states at band edges (valleys) in the hexagonal momentum space; therefore, low-energy interlayer excitation in the hexagonal monolayer stacks can be directed by the two-dimensional rotational degree of each monolayer crystal. However, this rotation-dependent excitation is largely unknown, due to lack in control over the relative monolayer rotations, thereby leading to momentum-mismatched interlayer excitations. Here, we report that light absorption and emission in MoS2/WS2 monolayer stacks can be tunable from indirect- to direct-gap transitions in both spectral and dynamic characteristics, when the constituent monolayer crystals are coherently stacked without in-plane rotation misfit. Our study suggests that the interlayer rotational attributes determine tunable interlayer excitation as a new set of basis for investigating optical phenomena in a two-dimensional hexagonal monolayer system. PMID:26099952

  4. Strain modulation-enhanced Mg acceptor activation efficiency of Al0.14Ga0.86N/GaN superlattices with AlN interlayer

    NASA Astrophysics Data System (ADS)

    Wang, Lei; Li, Rui; Li, Ding; Liu, Ningyang; Liu, Lei; Chen, Weihua; Wang, Cunda; Yang, Zhijian; Hu, Xiaodong

    2010-02-01

    AlN layer was grown as interlayer between undoped GaN and Mg doped Al0.14Ga0.86N/GaN superlattices (SLs) epilayer to modulate the strain distribution between Al0.14Ga0.86N barrier and GaN well layers in SLs sample. Strain relaxation was observed in the SLs sample with AlN interlayer by x-ray diffraction reciprocal space mapping method. The measured hole concentration of SLs sample with AlN interlayer at room temperature was over 1.6×1018 cm-3 but that was only 6.6×1016 cm-3 obtained in SLs sample without AlN interlayer. Variable temperature Hall-effect measurement showed that the acceptor activation energy decreased from 150 to 70 meV after inserting the AlN layer, which indicated that the strain modulation of SLs induced by AlN interlayer was beneficial to the Mg acceptor activation and hole concentration enhancement.

  5. Intercalation of gaseous thiols and sulfides into Ag+ ion-exchanged aluminum dihydrogen triphosphate.

    PubMed

    Hayashi, Aki; Saimen, Hiroki; Watanabe, Nobuaki; Kimura, Hitomi; Kobayashi, Ayumi; Nakayama, Hirokazu; Tsuhako, Mitsutomo

    2005-08-02

    Ag(+) ion-exchanged layered aluminum dihydrogen triphosphate (AlP) with the interlayer distance of 0.85 nm was synthesized by the ion-exchange of proton in triphosphate with Ag(+) ion. The amount of exchanged Ag(+) ion depended on the concentration of AgNO(3) aqueous solution. Ag(+) ion-exchanged AlP adsorbed gaseous thiols and sulfides into the interlayer region. The adsorption amounts of thiols were more than those of sulfides, thiols with one mercapto group > thiol with two mercapto groups > sulfides, and depended on the amount of exchanged Ag(+) ion in the interlayer region. The thiols with one mercapto group were intercalated to expand the interlayer distance of Ag(+) ion-exchanged AlP, whereas there was no expansion in the adsorption of sulfide. In the case of thiol with two mercapto groups, there was observed contraction of the interlayer distance through the bridging with Ag(+) ions of the upper and lower sides of the interlayer region.

  6. Potential of coded excitation in medical ultrasound imaging.

    PubMed

    Misaridis, T X; Gammelmark, K; Jørgensen, C H; Lindberg, N; Thomsen, A H; Pedersen, M H; Jensen, J A

    2000-03-01

    Improvement in signal-to-noise ratio (SNR) and/or penetration depth can be achieved in medical ultrasound by using long coded waveforms, in a similar manner as in radars or sonars. However, the time-bandwidth product (TB) improvement, and thereby SNR improvement is considerably lower in medical ultrasound, due to the lower available bandwidth. There is still space for about 20 dB improvement in the SNR, which will yield a penetration depth up to 20 cm at 5 MHz [M. O'Donnell, IEEE Trans. Ultrason. Ferroelectr. Freq. Contr., 39(3) (1992) 341]. The limited TB additionally yields unacceptably high range sidelobes. However, the frequency weighting from the ultrasonic transducer's bandwidth, although suboptimal, can be beneficial in sidelobe reduction. The purpose of this study is an experimental evaluation of the above considerations in a coded excitation ultrasound system. A coded excitation system based on a modified commercial scanner is presented. A predistorted FM signal is proposed in order to keep the resulting range sidelobes at acceptably low levels. The effect of the transducer is taken into account in the design of the compression filter. Intensity levels have been considered and simulations on the expected improvement in SNR are also presented. Images of a wire phantom and clinical images have been taken with the coded system. The images show a significant improvement in penetration depth and they preserve both axial resolution and contrast.

  7. Doping-dependent anisotropic superconducting gap in Na1-δ(Fe1-xCox)As from London penetration depth

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Cho, Kyuil; Tanatar, Makariy A.; Spyrison, Nicholas

    2012-07-30

    The London penetration depth was measured in single crystals of self-doped Na1-δFeAs (from under doping to optimal doping, Tc from 14 to 27 K) and electron-doped Na(Fe1-xCox)As with x ranging from undoped, x=0, to overdoped, x=0.1. In all samples, the low-temperature variation of the penetration depth exhibits a power-law dependence, Δλ(T)=ATn, with the exponent that varies in a domelike fashion from n˜1.1 in the underdoped, reaching a maximum of n˜1.9 in the optimally doped, and decreasing again to n˜1.3 on the overdoped side. While the anisotropy of the gap structure follows a universal domelike evolution, the exponent at optimal doping,more » n˜1.9, is lower than in other charge-doped Fe-based superconductors (FeSCs). The full-temperature range superfluid density, ρs(T)=λ(0)/λ(T)2, at optimal doping is also distinctly different from other charge-doped FeSCs but is similar to isovalently substituted BaFe2(As1-xPx)2, believed to be a nodal pnictide at optimal doping. These results suggest that the superconducting gap in Na(Fe1-xCox)As is highly anisotropic even at optimal doping.« less

  8. Effects of injection pressure variation on mixing in a cold supersonic combustor with kerosene fuel

    NASA Astrophysics Data System (ADS)

    Liu, Wei-Lai; Zhu, Lin; Qi, Yin-Yin; Ge, Jia-Ru; Luo, Feng; Zou, Hao-Ran; Wei, Min; Jen, Tien-Chien

    2017-10-01

    Spray jet in cold kerosene-fueled supersonic flow has been characterized under different injection pressures to assess the effects of the pressure variation on the mixing between incident shock wave and transverse cavity injection. Based on the real scramjet combustor, a detailed computational fluid dynamics model is developed. The injection pressures are specified as 0.5, 1.0, 2.0, 3.0 and 4.0 MPa, respectively, with the other constant operation parameters (such as the injection diameter, angle and velocity). A three dimensional Couple Level Set & Volume of Fluids approach incorporating an improved Kelvin-Helmholtz & Rayleigh-Taylor model is used to investigate the interaction between kerosene and supersonic air. The numerical simulations primarily concentrate on penetration depth, span expansion area, angle of shock wave and sauter mean diameter distribution of the kerosene droplets with/without evaporation. Validation has been implemented by comparing the calculated against the measured in literature with good qualitative agreement. Results show that the penetration depth, span-wise angle and expansion area of the transverse cavity jet are all increased with the injection pressure. However, when the injection pressure is further increased, the value in either penetration depth or expansion area increases appreciably. This study demonstrates the feasibility and effectiveness of the combination of Couple Level Set & Volume of Fluids approach and an improved Kelvin-Helmholtz & Rayleigh-Taylor model, in turn providing insights into scramjet design improvement.

  9. Evidence for Interlayer Collapse of Nontronite on Mars from Laboratory Visible and Near-IR Reflective Spectra

    NASA Technical Reports Server (NTRS)

    Morris, Richard V.; Ming, D. W.; Golden, D. C.; Graff, T. G.; Achilles, C. N.

    2010-01-01

    Dioctahedral smectites (e.g., nontronite and montmorillionite) are interpreted to occupy the optical surface of Mars at a number of locations on the basis of spectral features derived from interlayer H2O and MOH (M=Fe(3+)2, Fe(3+)Al, Al2, etc.) as observed by orbiting MRO-CRISM and MEx-OMEGA hyperspectral imaging spectrometers. At wavelengths shorter than approximately 2.7 micrometers, the strongest bands from interlayer H2O occur at approximately 1.4 and 1.9 micrometers from 2v1 and v1+v2, respectively, where v1 and v2 are the fundamental stretching and bending vibrations of the H2O molecule. Smectite MOH vibrations occur near 1.4 micrometers (stretching overtone) and in the region between 2.1 and 2.7 micrometers (stretching + bending combination). Because interlayer H2O can exchange with the martian environment, a number of studies have examined the strength of the interlayer H2O spectral features under Mars-like environmental conditions. The relationship between spectral properties and the underlying crystal structure of the smectites was not determined, and the extent of interlayer H2O removal was not established. We report combined visible and near-IR (VNIR), Mossbauer (MB), and powder X-ray diffraction (XRD) data for samples of the Fe-bearing smectite nontronite where the interlayer was collapsed by complete removal of interlayer H2O.

  10. Inferring strength and deformation properties of hot mix asphalt layers from the GPR signal: recent advances

    NASA Astrophysics Data System (ADS)

    Tosti, Fabio; Benedetto, Andrea; Bianchini Ciampoli, Luca; Adabi, Saba; Pajewski, Lara

    2015-04-01

    The great flexibility of ground-penetrating radar has led to consider worldwide this instrument as an effective and efficient geophysical tool in several fields of application. As far as pavement engineering is concerned, ground-penetrating radar is employed in a wide range of applications, including physical and geometrical evaluation of road pavements. Conversely, the mechanical characterization of pavements is generally inferred through traditional (e.g., plate bearing test method) or advanced non-destructive techniques (e.g., falling weight deflectometer). Nevertheless, measurements performed using these methods, inevitably turn out to be both much more time-consuming and low-significant whether compared with ground-penetrating radar's potentials. In such a framework, a mechanical evaluation directly coming from electromagnetic inspections could represent a real breakthrough in the field of road assets management. With this purpose, a ground-penetrating radar system with 600 MHz and 1600 MHz center frequencies of investigation and ground-coupled antennas was employed to survey a 4m×30m flexible pavement test site. The test area was marked by a regular grid mesh of 836 nodes, respectively spaced by a distance of 0.40 m alongside the horizontal and vertical axes. At each node, the elastic modulus was measured using a light falling weight deflectometer. Data processing has provided to reconstruct a 3-D matrix of amplitudes for the surveyed area, considering a depth of around 300 mm, in accord to the influence domain of the light falling weight deflectometer. On the other hand, deflectometric data were employed for both calibration and validation of a semi-empirical model by relating the amplitude of signal reflections through the media along fixed depths within the depth domain considered, and the Young's modulus of the pavement at the evaluated point. This statistically-based model is aimed at continuously taking into account alongside the depth of investigation, of both the different strength provision of each layer composing the hot mix asphalt pavement structure, and of the attenuation occurring to electromagnetic waves during their in-depth propagation. Promising results are achieved by matching modelled and measured elastic modulus data. This continuous statistically-based model enables to consider the whole set of information related to each single depth, in order to provide a more comprehensive prediction of the strength and deformation behavior of such a complex multi-layered medium. Amongst some further developments to be tackled in the near future, a model improvement could be reached through laboratory activities under controlled conditions and by adopting several frequency bandwidths suited for purposes. In addition, the perspective to compare electromagnetic data with mechanical measurements retrieved continuously, i.e., by means of specifically equipped lorries, could pave the way to considerable enhancements in this field of research. Acknowledgements - This work has benefited from networking activities carried out within the EU funded COST Action TU1208 "Civil Engineering Applications of Ground Penetrating Radar".

  11. Performance characteristics of a conformal ultra-wideband multilayer applicator (CUMLA) for hyperthermia in veterinary patients: a pilot evaluation of its use in the adjuvant treatment of non-resectable tumours.

    PubMed

    Smrkovski, O A; Koo, Y; Kazemi, R; Lembcke, L M; Fathy, A; Liu, Q; Phillips, J C

    2013-03-01

    Performance and clinical characteristics of a novel hyperthermia antenna operating at 434 MHz were evaluated for the adjuvant treatment of locally advanced superficial tumours in cats, dogs and horses. Electromagnetic simulations were performed to determine electric field characteristics and compared to simulations for a flat microwave antenna with similar dimensions. Simulation results show a reduced skin surface and backfield irradiation and improved directional irradiation (at broadside) compared to a flat antenna. Radiated power and penetration is notably increased with a penetration depth of 4.59 cm compared to 2.74 cm for the flat antenna. Clinical use of the antenna was then evaluated in six animals with locoregionally advanced solid tumours receiving adjuvant chemotherapy. During clinical applications, therapeutic temperatures were achieved at depths ≥4 cm. Objective responses were seen in all patients; tissue toxicity in one case limited further therapy. This antenna provides compact, efficient, focused and deep-penetrating clinical hyperthermia for the treatment of solid tumours in veterinary patients. © 2011 Blackwell Publishing Ltd.

  12. Quantifying glucose permeability and enhanced light penetration in ex vivo human normal and cancerous esophagus tissues with optical coherence tomography

    NASA Astrophysics Data System (ADS)

    Zhao, Q. L.; Si, J. L.; Guo, Z. Y.; Wei, H. J.; Yang, H. Q.; Wu, G. Y.; Xie, S. S.; Li, X. Y.; Guo, X.; Zhong, H. Q.; Li, L. Q.

    2011-01-01

    We report our pilot results on quantification of glucose (G) diffusion permeability in human normal esophagus and ESCC tissues in vitro by using OCT technique. The permeability coefficient of 40% aqueous solution of G was found to be (1.74±0.04)×10-5 cm/s in normal esophagus and (2.45±0.06)×10-5 cm/s in ESCC tissues. The results from this study indicate that ESCC tissues had a higher permeability coefficient compared to normal esophageal tissues, and the light penetration depths gradually increase with the increase of applied topically with G time for the normal esophageal and ESCC tissues. The results indicate that the permeability coefficient of G in cancer tissues was 1.41-fold than that in normal tissues, and the light penetration depth for the ESCC tissues is significantly smaller than that of normal esophagus tissues in the same time range. These results demonstrate that the optical clearing of normal and cancer esophagus tissues are improved after application of G.

  13. Evaluation of asphalt rubber membrane interlayer (ARMI) using the University of Florida's composite system interface cracking (CSIC) test.

    DOT National Transportation Integrated Search

    2012-05-01

    Since the late 1970s, FDOT : has applied an interlayer : of Asphalt Rubber : Membrane Interlayer : (ARMI) to asphalt roadway : surfaces. ARMI layers are : constructed by spraying : asphalt rubber binder onto : the asphalt, covering the : layer with n...

  14. METHOD AND APPARATUS FOR EARTH PENETRATION

    DOEpatents

    Adams, W.M.

    1963-12-24

    A nuclear reactor apparatus for penetrating into the earth's crust is described. The apparatus comprises a cylindrical nuclear core operating at a temperature that is higher than the melting temperature of rock. A high-density ballast member is coupled to the nuclear core such that the overall density of the core-ballast assembly is greater than the density of molten rock. The nuclear core is thermally insulated so that its heat output is constrained to flow axially, with radial heat flow being minimized. In operation, the apparatus is placed in contact with the earth's crust at the point desired to be penetrated. The heat output of the reactor melts the underlying rock, and the apparatus sinks through the resulting magma. The fuel loading of the reactor core determines the ultimate depth of crust penetration. (AEC)

  15. High Spectral Resolution Lidar Data

    DOE Data Explorer

    Eloranta, Ed

    2004-12-01

    The HSRL provided calibrated vertical profiles of optical depth, backscatter cross section and depoloarization at a wavelength of 532 nm. Profiles were acquired at 2.5 second intervals with 7.5 meter resolution. Profiles extended from an altitude of 100 m to 30 km in clear air. The lidar penetrated to a maximum optical depth of ~ 4 under cloudy conditions. Our data contributed directly to the aims of the M-PACE experiment, providing calibrated optical depth and optical backscatter measurements which were not available from any other instrument.

  16. Comparing Yb-fiber and Ti:Sapphire lasers for depth resolved imaging of human skin (Conference Presentation)

    NASA Astrophysics Data System (ADS)

    Balu, Mihaela; Saytashev, Ilyas; Hou, Jue; Dantus, Marcos; Tromberg, Bruce J.

    2016-02-01

    We report on a direct comparison between Ti:Sapphire and Yb fiber lasers for depth-resolved label-free multimodal imaging of human skin. We found that the penetration depth achieved with the Yb laser was 80% greater than for the Ti:Sapphire. Third harmonic generation (THG) imaging with Yb laser excitation provides additional information about skin structure. Our results indicate the potential of fiber-based laser systems for moving into clinical use.

  17. Evaluation of a pneumatic Martian soil sampler concept

    NASA Technical Reports Server (NTRS)

    Schaefer, John L.; Neathery, James K.; Stencel, John M.

    1994-01-01

    The pneumatic soil sampler concept was successfully demonstrated by penetrating a Martian simulant soil to a depth of 2 meters. Working gas pressure, composition, and pulsing were evaluated with the objective of minimizing gas usage. Also, the probe penetration force was investigated with the objective of minimizing probe weight. Gas and probe penetration force, while not yet optimized, are within the range which make the soil sampler concept feasible. While the tests described in this report did not answer all the questions and address all the variables associated with pneumatic soil sampling, valuable data experience and knowledge were gained which can be used to further develop the concept.

  18. Simultaneous surface and depth neural activity recording with graphene transistor-based dual-modality probes.

    PubMed

    Du, Mingde; Xu, Xianchen; Yang, Long; Guo, Yichuan; Guan, Shouliang; Shi, Jidong; Wang, Jinfen; Fang, Ying

    2018-05-15

    Subdural surface and penetrating depth probes are widely applied to record neural activities from the cortical surface and intracortical locations of the brain, respectively. Simultaneous surface and depth neural activity recording is essential to understand the linkage between the two modalities. Here, we develop flexible dual-modality neural probes based on graphene transistors. The neural probes exhibit stable electrical performance even under 90° bending because of the excellent mechanical properties of graphene, and thus allow multi-site recording from the subdural surface of rat cortex. In addition, finite element analysis was carried out to investigate the mechanical interactions between probe and cortex tissue during intracortical implantation. Based on the simulation results, a sharp tip angle of π/6 was chosen to facilitate tissue penetration of the neural probes. Accordingly, the graphene transistor-based dual-modality neural probes have been successfully applied for simultaneous surface and depth recording of epileptiform activity of rat brain in vivo. Our results show that graphene transistor-based dual-modality neural probes can serve as a facile and versatile tool to study tempo-spatial patterns of neural activities. Copyright © 2018 Elsevier B.V. All rights reserved.

  19. Depth-dependent resistance of granular media to vertical penetration.

    PubMed

    Brzinski, T A; Mayor, P; Durian, D J

    2013-10-18

    We measure the quasistatic friction force acting on intruders moving downwards into a granular medium. By utilizing different intruder geometries, we demonstrate that the force acts locally normal to the intruder surface. By altering the hydrostatic loading of grain contacts by a sub-fluidizing airflow through the bed, we demonstrate that the relevant frictional contacts are loaded by gravity rather than by the motion of the intruder itself. Lastly, by measuring the final penetration depth versus airspeed and using an earlier result for inertial drag, we demonstrate that the same quasistatic friction force acts during impact. Altogether this force is set by a friction coefficient, hydrostatic pressure, projectile size and shape, and a dimensionless proportionality constant. The latter is the same in nearly all experiments, and is surprisingly greater than one.

  20. Probing the superconducting gap symmetry of α - PdBi 2 : A penetration depth study

    DOE PAGES

    Mitra, S.; Okawa, K.; Kunniniyil Sudheesh, S.; ...

    2017-04-27

    Inmore » this paper, we report measurements of the in-plane London penetration depth λ in single crystals of the α - PdBi 2 superconductor—the α-phase counterpart of the putative topological superconductor β - PdBi 2 , down to 0.35 K using a high-resolution tunnel-diode-based technique. Both λ and superfluid density ρ s exhibit an exponential behavior for T ≤ 0.35T c, with Δ(0) /k BT c ~ 2.0, ΔC/γT c ~ 2.0, and λ(0) ~ 140 nm, showing that α - PdBi 2 is a moderately coupling, fully gapped superconductor. Finally, the values of Δ(0) and ΔC/γT c are consistent with each other via strong-coupling corrections.« less

  1. Probing the superconducting gap symmetry of α - PdBi 2 : A penetration depth study

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Mitra, S.; Okawa, K.; Kunniniyil Sudheesh, S.

    Inmore » this paper, we report measurements of the in-plane London penetration depth λ in single crystals of the α - PdBi 2 superconductor—the α-phase counterpart of the putative topological superconductor β - PdBi 2 , down to 0.35 K using a high-resolution tunnel-diode-based technique. Both λ and superfluid density ρ s exhibit an exponential behavior for T ≤ 0.35T c, with Δ(0) /k BT c ~ 2.0, ΔC/γT c ~ 2.0, and λ(0) ~ 140 nm, showing that α - PdBi 2 is a moderately coupling, fully gapped superconductor. Finally, the values of Δ(0) and ΔC/γT c are consistent with each other via strong-coupling corrections.« less

  2. Critical fields and vortex pinning in overdoped Ba 0.2 K 0.8 Fe 2 As 2

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Shen, B.; Leroux, M.; Wang, Y. L.

    2015-05-19

    We determine the upper and lower critical fields, the penetration depth and the vortex pinning characteristics of single crystals of overdoped Ba 0.2K 0.8Fe 2As 2 with T c ~ 10 K. We find that bulk vortex pinning is weak and vortex dynamics to be dominated by the geometrical surface barrier. The temperature dependence of the lower critical field, H c1, displays a distinctive upturn at low temperatures, which is suggestive of two distinct superconducting gaps. Furthermore, the penetration depth, λ, varies linearly with temperature below 4 K indicative of line nodes in the superconducting gap. As a result, thesemore » observations can be well described in a model based on a multi-band nodal superconducting gap.« less

  3. Estimation of the Friction Coefficient of a Nanostructured Composite Coating

    NASA Astrophysics Data System (ADS)

    Shil'ko, S. V.; Chernous, D. A.; Ryabchenko, T. V.; Hat'ko, V. V.

    2017-11-01

    The frictional-mechanical properties of a thin polymer-ceramic coating obtained by gas-phase impregnation of nanoporous anodic alumina with a fluoropolymer (octafluorocyclobutane) have been investigated. The coefficient of sliding friction of the coating is predicted based on an analysis of contact deformation within the framework of the Winkler elastic foundation hypothesis and a three-phase micromechanical model. It is shown that an acceptable prediction accuracy can be obtained considering the uniaxial strain state of the coating. It was found that, on impregnation by the method of plasmachemical treatment, the relative depth of penetration of the polymer increased almost in proportion to the processing time. The rate and maximum possible depth of penetration of the polymer into nanoscale pores grew with increasing porosity of the alumina substrate.

  4. Evaluation of asphalt rubber membrane interlayer (ARMI) using the University of Florida's composite system interface cracking (CSIC) test [summary].

    DOT National Transportation Integrated Search

    2012-01-01

    Since the late 1970s, FDOT : has applied an interlayer : of Asphalt Rubber : Membrane Interlayer : (ARMI) to asphalt roadway : surfaces. ARMI layers are : constructed by spraying : asphalt rubber binder onto : the asphalt, covering the : layer with n...

  5. FAST TRACK COMMUNICATION: Interlayer exchange coupling across a ferroelectric barrier

    NASA Astrophysics Data System (ADS)

    Zhuravlev, M. Ye; Vedyayev, A. V.; Tsymbal, E. Y.

    2010-09-01

    A new magnetoelectric effect is predicted originating from the interlayer exchange coupling between two ferromagnetic layers separated by an ultrathin ferroelectric barrier. It is demonstrated that ferroelectric polarization switching driven by an external electric field leads to a sizable change in the interlayer exchange coupling. The effect occurs in asymmetric ferromagnet/ferroelectric/ferromagnet junctions due to a change in the electrostatic potential profile across the junction affecting the interlayer coupling. The predicted phenomenon indicates the possibility of switching the magnetic configuration by reversing the polarization of the ferroelectric barrier layer.

  6. In0.15Ga0.85N visible-light metal-semiconductor-metal photodetector with GaN interlayers deposited by pulsed NH3

    NASA Astrophysics Data System (ADS)

    Wang, Hongxia; Zhang, Xiaohan; Wang, Hailong; Lv, Zesheng; Li, Yongxian; Li, Bin; Yan, Huan; Qiu, Xinjia; Jiang, Hao

    2018-05-01

    InGaN visible-light metal-semiconductor-metal photodetectors with GaN interlayers deposited by pulsed NH3 were fabricated and characterized. By periodically inserting the GaN thin interlayers, the surface morphology of InGaN active layer is improved and the phase separation is suppressed. At 5 V bias, the dark current reduced from 7.0 × 10-11 A to 7.0 × 10-13 A by inserting the interlayers. A peak responsivity of 85.0 mA/W was measured at 420 nm and 5 V bias, corresponding to an external quantum efficiency of 25.1%. The insertion of GaN interlayers also lead to a sharper spectral response cutoff.

  7. Mechanical characterization and modeling of brazed tungsten and Cu-Cr-Zr alloy using stress relief interlayers

    NASA Astrophysics Data System (ADS)

    Qu, Dandan; Zhou, Zhangjian; Yum, Youngjin; Aktaa, Jarir

    2014-12-01

    A rapidly solidified foil-type Ti-Zr based amorphous filler with a melting temperature of 850 °C was used to braze tungsten to Cu-Cr-Zr alloy for water cooled divertors and plasma facing components application. Brazed joints of dissimilar materials suffer from a mismatch in coefficients of thermal expansion. In order to release the residual stress caused by the mismatch, brazed joints of tungsten and Cu-Cr-Zr alloy using different interlayers were studied. The shear strength tests of brazed W/Cu joints show that the average strength of the joint with a W70Cu30 composite plate interlayer reached 119.8 MPa, and the average strength of the joint with oxygen free high conductivity copper (OFHC Cu)/Mo multi-interlayers reached 140.8 MPa, while the joint without interlayer was only 16.6 MPa. Finite element method (FEM) has been performed to investigate the stress distribution and effect of stress relief interlayers. FEM results show that the maximum von Mises stress occurs in the tungsten/filler interface and that the filler suffers the peak residual stresses and becomes the weakest zone. And the use of OFHC Cu/Mo multi-interlayers can reduce the residual stress significantly, which agrees with the mechanical experiment data.

  8. Fiscal year 1976 progress report on a feasibility study evaluating the use of surface penetrators for planetary exploration

    NASA Technical Reports Server (NTRS)

    Blanchard, M. B.; Oberbeck, V. R.; Bunch, T. E.; Reynolds, R. T.; Canning, T. N.; Jackson, R. W.

    1976-01-01

    The feasibility of employing penetrators for exploring Mars was examined. Eight areas of interest for key scientific experiments were identified. These include: seismic activity, imaging, geochemistry, water measurement, heatflow, meteorology, magnetometry, and biochemistry. In seven of the eight potential experiment categories this year's progress included: conceptual design, instrument fabrication, instrument performance evaluation, and shock loading of important components. Most of the components survived deceleration testing with negligible performance changes. Components intended to be placed inside the penetrator forebody were tested up to 3,500 g and components intended to be placed on the afterbody were tested up to 21,000 g. A field test program was conducted using tentative Mars penetrator mission constraints. Drop tests were performed at two selected terrestrial analog sites to determine the range of penetration depths for anticipated common Martian materials. Minimum penetration occurred in basalt at Amboy, California. Three full-scale penetrators penetrated 0.4 to 0.9 m into the basalt after passing through 0.3 to 0.5 m of alluvial overburden. Maximum penetration occurred in unconsolidated sediments at McCook, Nebraska. Two full-scale penetrators penetrated 2.5 to 8.5 m of sediment. Impact occurred in two kinds of sediment: loess and layered clay. Deceleration g loads of nominally 2,000 for the forebody and 20,000 for the afterbody did not present serious design problems for potential experiments. Penetrators have successfully impacted into terrestrial analogs of the probable extremes of potential Martian sites.

  9. Unusually Deep Bonin Earthquake (M7.9) of May 30, 2015 Suggests that Stagnant Slab Transforms into Penetration Stage

    NASA Astrophysics Data System (ADS)

    Obayashi, M.; Fukao, Y.; Yoshimitsu, J.

    2015-12-01

    A great shock occurred at an unusual depth of 678 km far away from the well-defined Wadati-Benioff zone of the Izu-Bonin arc (Fig.1). To the north of this region the slab is stagnant above the 660 km discontinuity and to the south it penetrates the discontinuity (Fig.2). Thus, the slab in this region can be viewed as in a transitional state from the stagnant to penetrating slab. Here, the steeply dipping part of the slab bends sharply to horizontal and the great shock happened at the lowest corner of this bending. The CMT indicates a pure normal faulting with the trench-normal near horizontal tensional axis and the near vertical compressional axis (Fig.1). We suggest that this mechanism reflects a transitional state of slab deformation from the bending-dominant mode to the penetration-dominant mode. The mechanism is consistent with either of these two two modes. We show that the mechanism is also consistent with the resultant stress field generated by many deep shocks occurring along the Wadati-Benioff zone. The calculated stress field changes rapidly along a trench-normal profile at a depth of 680 km and becomes similar to that generated by the great shock at points near the hypocenter (Fig.3). Thus, the stress field due to the Wadati-Benioff zone earthquakes works to enhance the occurrence of deep shocks of the type of the 2015 great shock, which represents slab deformation associated with the transition from stagnant to penetrating slab.

  10. Indentation of a free-falling lance penetrometer into a poroelastic seabed

    NASA Astrophysics Data System (ADS)

    Elsworth, Derek; Lee, Dae Sung

    2005-02-01

    A solution is developed for the build-up, steady and post-arrest dissipative pore fluid pressure fields that develop around a blunt penetrometer that self-embeds from freefall into the seabed. Arrest from freefall considers deceleration under undrained conditions in a purely cohesive soil, with constant shear strength with depth. The resulting decelerating velocity field is controlled by soil strength, geometric bearing capacity factors, and inertial components. At low impact velocities the embedment process is controlled by soil strength, and at high velocities by inertia. With the deceleration defined, a solution is evaluated for a point normal dislocation penetrating in a poroelastic medium with a prescribed decelerating velocity. Dynamic steady pressures, PD, develop relative to the penetrating tip geometry with their distribution conditioned by the non-dimensional penetration rate, UD, incorporating impacting penetration rate, consolidation coefficient and penetrometer radius, and the non-dimensional strength, ND, additionally incorporating undrained shear strength of the sediment. Pore pressures develop to a steady peak magnitude at the penetrometer tip, and drop as PD=1/xD with distance xD behind the tip and along the shaft. Peak induced pressure magnitudes may be correlated with sediment permeabilities, post-arrest dissipation rates may be correlated with consolidation coefficients, and depths of penetration may be correlated with shear strengths. Together, these records enable strength and transport parameters to be recovered from lance penetrometer data. Penetrometer data recorded off La Palma in the Canary Islands (J. Volcanol. Geotherm. Res. 2000; 101:253) are used to recover permeabilities and consolidation coefficients from peak pressure and dissipation response, respectively. Copyright

  11. Inelastic neutron scattering and molecular simulation of the dynamics of interlayer water in smectite clay minerals

    DOE PAGES

    Cygan, Randall T.; Daemen, Luke L.; Ilgen, Anastasia G.; ...

    2015-11-16

    The study of mineral–water interfaces is of great importance to a variety of applications including oil and gas extraction, gas subsurface storage, environmental contaminant treatment, and nuclear waste repositories. Understanding the fundamentals of that interface is key to the success of those applications. Confinement of water in the interlayer of smectite clay minerals provides a unique environment to examine the interactions among water molecules, interlayer cations, and clay mineral surfaces. Smectite minerals are characterized by a relatively low layer charge that allows the clay to swell with increasing water content. Montmorillonite and beidellite varieties of smectite were investigated to comparemore » the impact of the location of layer charge on the interlayer structure and dynamics. Inelastic neutron scattering of hydrated and dehydrated cation-exchanged smectites was used to probe the dynamics of the interlayer water (200–900 cm –1 spectral region) and identify the shift in the librational edge as a function of the interlayer cation. Molecular dynamics simulations of equivalent phases and power spectra, derived from the resulting molecular trajectories, indicate a general shift in the librational behavior with interlayer cation that is generally consistent with the neutron scattering results for the monolayer hydrates. Both neutron scattering and power spectra exhibit librational structures affected by the location of layer charge and by the charge of the interlayer cation. Furthermore, divalent cations (Ba 2+ and Mg 2+) characterized by large hydration enthalpies typically exhibit multiple broad librational peaks compared to monovalent cations (Cs + and Na +), which have relatively small hydration enthalpies.« less

  12. Estimating soil water content from ground penetrating radar coarse root reflections

    NASA Astrophysics Data System (ADS)

    Liu, X.; Cui, X.; Chen, J.; Li, W.; Cao, X.

    2016-12-01

    Soil water content (SWC) is an indispensable variable for understanding the organization of natural ecosystems and biodiversity. Especially in semiarid and arid regions, soil moisture is the plants primary source of water and largely determine their strategies for growth and survival, such as root depth, distribution and competition between them. Ground penetrating radar (GPR), a kind of noninvasive geophysical technique, has been regarded as an accurate tool for measuring soil water content at intermediate scale in past decades. For soil water content estimation with surface GPR, fixed antenna offset reflection method has been considered to have potential to obtain average soil water content between land surface and reflectors, and provide high resolution and few measurement time. In this study, 900MHz surface GPR antenna was used to estimate SWC with fixed offset reflection method; plant coarse roots (with diameters greater than 5 mm) were regarded as reflectors; a kind of advanced GPR data interpretation method, HADA (hyperbola automatic detection algorithm), was introduced to automatically obtain average velocity by recognizing coarse root hyperbolic reflection signals on GPR radargrams during estimating SWC. In addition, a formula was deduced to determine interval average SWC between two roots at different depths as well. We examined the performance of proposed method on a dataset simulated under different scenarios. Results showed that HADA could provide a reasonable average velocity to estimate SWC without knowledge of root depth and interval average SWC also be determined. When the proposed method was applied to estimation of SWC on a real-field measurement dataset, a very small soil water content vertical variation gradient about 0.006 with depth was captured as well. Therefore, the proposed method could be used to estimate average soil water content from ground penetrating radar coarse root reflections and obtain interval average SWC between two roots at different depths. It is very promising for measuring root-zone-soil-moisture and mapping soil moisture distribution around a shrub or even in field plot scale.

  13. An in situ approach to detect tree root ecology: linking ground-penetrating radar imaging to isotope-derived water acquisition zones

    PubMed Central

    Isaac, Marney E; Anglaaere, Luke C N

    2013-01-01

    Tree root distribution and activity are determinants of belowground competition. However, studying root response to environmental and management conditions remains logistically challenging. Methodologically, nondestructive in situ tree root ecology analysis has lagged. In this study, we tested a nondestructive approach to determine tree coarse root architecture and function of a perennial tree crop, Theobroma cacao L., at two edaphically contrasting sites (sandstone and phyllite–granite derived soils) in Ghana, West Africa. We detected coarse root vertical distribution using ground-penetrating radar and root activity via soil water acquisition using isotopic matching of δ18O plant and soil signatures. Coarse roots were detected to a depth of 50 cm, however, intraspecifc coarse root vertical distribution was modified by edaphic conditions. Soil δ18O isotopic signature declined with depth, providing conditions for plant–soil δ18O isotopic matching. This pattern held only under sandstone conditions where water acquisition zones were identifiably narrow in the 10–20 cm depth but broader under phyllite–granite conditions, presumably due to resource patchiness. Detected coarse root count by depth and measured fine root density were strongly correlated as were detected coarse root count and identified water acquisition zones, thus validating root detection capability of ground-penetrating radar, but exclusively on sandstone soils. This approach was able to characterize trends between intraspecific root architecture and edaphic-dependent resource availability, however, limited by site conditions. This study successfully demonstrates a new approach for in situ root studies that moves beyond invasive point sampling to nondestructive detection of root architecture and function. We discuss the transfer of such an approach to answer root ecology questions in various tree-based landscapes. PMID:23762519

  14. An example of applied structural petrology in the Illinois Basin: Sphalerite kaolinite and their relation to the depth and relative timing of coal jointing

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Ambers, C.P.

    1993-03-01

    Sphalerite is associated with very well crystallized kaolinite (VWCK) in geodes, siderite nodules and coal cleats in the Illinois Basin and allows estimation of the temperature of formation of the VWCK using fluid inclusions. The approximate depth of kaolinite growth and the relative timing of coal fracturing can then be ascertained. Sphalerite associated with VWCK was extracted from Mississippian geodes collected near Keokuk, Iowa, and from Pennsylvanian siderite nodules and coal collected in SW Indiana. Inclusions in the sphalerite consist of VWCK; large, negative crystal, two-phase fluid inclusions; small, fracture-related, two-phase fluid inclusions; and organic inclusions. Homogenization temperatures of 89more » C [+-] 10, 115 C [+-] 15, 89 C [+-] 5 were measured for the two-phase inclusions in sphalerite from the geodes, siderite nodules and coal, respectively. Freezing temperatures of the inclusions in the geode and siderite nodule sphalerite were measured at [minus]13.5 C [+-] 0.5 and [minus]9.4 C [+-] 0.2, indicating moderate salinity. Using a geothermal gradient range of 23--36 C/km and an average surface temperature of 20 C, kaolinite and sphalerite probably grew at depths of about 1.9 to 4.1 km. In SW Indiana, VWCK occurs in vertical, non-penetrative joints in vitrinite layers. Penetrative joint sets rarely contain VWCK. At nearly all of the 28 sites studied, two sets of barren cleats occur oriented N10W to NSE and N80E to N95E. The orientation of barren, penetrative cleats shows that the maximum horizontal stress rotated CW from the earlier stress field. Rare VWCK in the late cleats suggests they also formed at depth after the thermal maxima.« less

  15. 77 FR 21422 - Airworthiness Directives; The Boeing Company Airplanes

    Federal Register 2010, 2011, 2012, 2013, 2014

    2012-04-10

    ... the fail-safe interlayer of certain No. 2 and No. 3 glass windows, which could result in loss of the... would hinder the internal or external detailed inspections for fail-safe interlayer cracks, glass pane... this AD only if the non-clear damage hinders the inspection for fail-safe interlayer cracks, glass pane...

  16. Measuring Interlayer Shear Stress in Bilayer Graphene

    NASA Astrophysics Data System (ADS)

    Wang, Guorui; Dai, Zhaohe; Wang, Yanlei; Tan, PingHeng; Liu, Luqi; Xu, Zhiping; Wei, Yueguang; Huang, Rui; Zhang, Zhong

    2017-07-01

    Monolayer two-dimensional (2D) crystals exhibit a host of intriguing properties, but the most exciting applications may come from stacking them into multilayer structures. Interlayer and interfacial shear interactions could play a crucial role in the performance and reliability of these applications, but little is known about the key parameters controlling shear deformation across the layers and interfaces between 2D materials. Herein, we report the first measurement of the interlayer shear stress of bilayer graphene based on pressurized microscale bubble loading devices. We demonstrate continuous growth of an interlayer shear zone outside the bubble edge and extract an interlayer shear stress of 40 kPa based on a membrane analysis for bilayer graphene bubbles. Meanwhile, a much higher interfacial shear stress of 1.64 MPa was determined for monolayer graphene on a silicon oxide substrate. Our results not only provide insights into the interfacial shear responses of the thinnest structures possible, but also establish an experimental method for characterizing the fundamental interlayer shear properties of the emerging 2D materials for potential applications in multilayer systems.

  17. Connecting the molecular scale to the continuum scale for diffusion processes in smectite-rich porous media.

    PubMed

    Bourg, Ian C; Sposito, Garrison

    2010-03-15

    In this paper, we address the manner in which the continuum-scale diffusive properties of smectite-rich porous media arise from their molecular- and pore-scale features. Our starting point is a successful model of the continuum-scale apparent diffusion coefficient for water tracers and cations, which decomposes it as a sum of pore-scale terms describing diffusion in macropore and interlayer "compartments." We then apply molecular dynamics (MD) simulations to determine molecular-scale diffusion coefficients D(interlayer) of water tracers and representative cations (Na(+), Cs(+), Sr(2+)) in Na-smectite interlayers. We find that a remarkably simple expression relates D(interlayer) to the pore-scale parameter δ(nanopore) ≤ 1, a constrictivity factor that accounts for the lower mobility in interlayers as compared to macropores: δ(nanopore) = D(interlayer)/D(0), where D(0) is the diffusion coefficient in bulk liquid water. Using this scaling expression, we can accurately predict the apparent diffusion coefficients of tracers H(2)0, Na(+), Sr(2+), and Cs(+) in compacted Na-smectite-rich materials.

  18. Penetration of Streptococcus sobrinus and Streptococcus sanguinis into dental enamel.

    PubMed

    Kneist, Susanne; Nietzsche, Sandor; Küpper, Harald; Raser, Gerhard; Willershausen, Brita; Callaway, Angelika

    2015-10-01

    The aim of this pilot study was to assess the difference in virulence of acidogenic and aciduric oral streptococci in an in vitro caries model using their penetration depths into dental enamel. 30 caries-free extracted molars from 11- to 16-year-olds were cleaned ultrasonically for 1 min with de-ionized water and, after air-drying, embedded in epoxy resin. After 8-h of setting at room temperature, the specimens were ground on the buccal side with SiC-paper 1200 (particle size 13-16 μm). Enamel was removed in circular areas sized 3 mm in diameter; the mean depth of removed enamel was 230 ± 60 μm. 15 specimens each were incubated anaerobically under standardized conditions with 24 h-cultures of Streptococcus sanguinis 9S or Streptococcus sobrinus OMZ 176 in Balmelli broth at 37 ± 2 °C; the pH-values of the broths were measured at the beginning and end of each incubation cycle. After 2, 4, 6, 8, and 10 weeks 3 teeth each were fixed in 2.5% glutaraldehyde in cacodylate buffer for 24 h, washed 3× and dehydrated 30-60min by sequential washes through a series of 30-100% graded ethanol. The teeth were cut in half longitudinally; afterward, two slits were made to obtain fracture surfaces in the infected area. After critical-point-drying the fragments were gold-sputtered and viewed in a scanning electron microscope at magnifications of ×20-20,000. After 10 weeks of incubation, penetration of S. sanguinis of 11.13 ± 24.04 μm below the break edges into the enamel was observed. The invasion of S. sobrinus reached depths of 87.53 ± 76.34 μm. The difference was statistically significant (paired t test: p = 0.033). The experimental penetration depths emphasize the importance of S. sanguinis versus S. sobrinus in the context of the extended ecological plaque hypothesis. Copyright © 2015 Elsevier Ltd. All rights reserved.

  19. Formation of lamellar cross bridges in the annulus fibrosus of the intervertebral disc is a consequence of vascular regression.

    PubMed

    Smith, Lachlan J; Elliott, Dawn M

    2011-05-01

    Cross bridges are radial structures within the highly organized lamellar structure of the annulus fibrosus of the intervertebral disc that connect two or more non-consecutive lamellae. Their origin and function are unknown. During fetal development, blood vessels penetrate deep within the AF and recede during postnatal growth. We hypothesized that cross bridges are the pathways left by these receding blood vessels. Initially, the presence of cross bridges was confirmed in cadaveric human discs aged 25 and 53 years. Next, L1-L2 intervertebral discs (n=4) from sheep ranging in age from 75 days fetal gestation to adult were processed for paraffin histology. Mid-sagittal sections were immunostained for endothelial cell marker PECAM-1. The anterior and posterior AF were imaged using differential interference contrast microscopy, and the following parameters were quantified: total number of distinct lamellae, total number of cross bridges, percentage of cross bridges staining positive for PECAM-1, cross bridge penetration depth (% total lamellae), and PECAM-1 positive cross bridge penetration depth. Cross bridges were first observed at 100 days fetal gestation. The overall number peaked in neonates then remained relatively unchanged. The percentage of PECAM-1 positive cross bridges declined progressively from almost 100% at 100 days gestation to less than 10% in adults. Cross bridge penetration depth peaked in neonates then remained unchanged at subsequent ages. Depth of PECAM-1 positive cross bridges decreased progressively after birth. Findings were similar for both the anterior and posterior. The AF lamellar architecture is established early in development. It later becomes disrupted as a consequence of vascularization. Blood vessels then recede, perhaps due to increasing mechanical stresses in the surrounding matrix. In this study we present evidence that the pathways left by receding blood vessels remain as lamellar cross bridges. It is unclear whether the presence of cross bridges in the aging and degenerating intervertebral disc would be advantageous or detrimental, and this question should be addressed by future studies. Copyright © 2011 International Society of Matrix Biology. Published by Elsevier B.V. All rights reserved.

  20. A numerically optimized active shield for improved TMS targeting

    PubMed Central

    Hernandez-Garcia, Luis; Hall, Timothy; Gomez, Luis; Michielssen, Eric

    2010-01-01

    Transcranial magnetic stimulation (TMS) devices suffer of poor targeting and penetration depth. A new approach to designing TMS coils is introduced in order to improve the focus of the stimulation region through the use of actively shielded probes. Iterative optimization techniques were used to design different active shielding coils for TMS probes. The new approach aims to increase the amount of energy deposited in a thin cylindrical region below the probe relative to the energy deposited elsewhere in the region (“sharpness”), while simultaneously increase the induced electric field deep in the target region relative to the surface (“penetration”). After convergence, the resulting designs showed that there is a clear tradeoff between sharpness and penetration that can be controlled by the choice of a tuning parameter. The resulting designs were tested on a realistic human head conductivity model, taking the contribution from surface charges into account. The design of choice reduced penetration depths by 16.7%. The activated surface area was reduced by 24.1 % and the volume of the activation was reduced from 42.6% by the shield. Restoring the lost penetration could be achieved by increasing the total power to the coil by 16.3%, but in that case, the stimulated volume reduction was only 13.1% and there was a slight increase in the stimulated surface area (2.9 %) PMID:20965451

  1. Distribution of phospholipid based formulations in the skin investigated by combined ATR-FTIR and tape stripping experiments.

    PubMed

    Wolf, Martin; Halper, Maria; Pribyl, Raffaela; Baurecht, Dieter; Valenta, Claudia

    2017-03-15

    The spatial distribution of exogenous substances in the stratum corneum (SC) could have an influence on their skin irritation potential. In this study it was possible to monitor the distribution of phospholipids with their phosphatidylcholine scaffold on porcine ear skin by combining tape stripping and in vitro ATR-FTIR spectroscopy. Significant vibrational modes in the spectra could be successfully assigned to the functional groups of the molecules. Thus it was possible to track the phospholipids without the need of their deuterated form by calculating difference spectra from the treated - untreated skin samples. The correlation between four characteristic bands (R 2 ≥0.9909) revealed the excellent suitability of this semi-quantitative method for deep profiling analysis. The penetration capabilities of aqueous suspensions of the different phospholipid compositions as well as two monoacyl-phosphatidylcholine based liposome formulations were investigated using this method. Nevertheless, differences in the distribution of the investigated phospholipid species, having different amounts of monoacyl-phosphatidylcholine, could not be found. It could be clearly shown that the deepest skin penetration was seen in the irritating anionic SDS (sodium dodecyl sulfate) out of the aqueous solution. The aqueous suspensions based on different phospholipid surfactants showed the same range of penetration depth (10-15% of SC), whereas the smallest skin penetration depth was observed after the application of liposomal formulations. Copyright © 2017 Elsevier B.V. All rights reserved.

  2. Helioseismic Constraints on the Depth Dependence of Large-Scale Solar Convection

    NASA Astrophysics Data System (ADS)

    Woodard, Martin F.

    2017-08-01

    A recent helioseismic statistical waveform analysis of subsurface flow based on a 720-day time series of SOHO/MDI Medium-l spherical-harmonic coefficients has been extended to cover a greater range of subphotospheric depths. The latest analysis provides estimates of flow-dependent oscillation-mode coupling-strength coefficients b(s,t;n,l) over the range l = 30 to 150 of mode degree (angular wavenumber) for solar p-modes in the approximate frequency range 2 to 4 mHz. The range of penetration depths of this mode set covers most of the solar convection zone. The most recent analysis measures spherical harmonic (s,t) components of the flow velocity for odd s in the angular wavenumber range 1 to 19 for t not much smaller than s at a given s. The odd-s b(s,t;n,l) coefficients are interpreted as averages over depth of the depth-dependent amplitude of one spherical-harmonic (s,t) component of the toroidal part of the flow velocity field. The depth-dependent weighting function defining the average velocity is the fractional kinetic energy density in radius of modes of the (n,l) multiplet. The b coefficients have been converted to estimates of root velocity power as a function of l0 = nu0*l/nu(n,l), which is a measure of mode penetration depth. (nu(n,l) is mode frequency and nu0 is a reference frequency equal to 3 mHz.) A comparison of the observational results with simple convection models will be presented.

  3. Geohydrology of Test Well USW H-3, Yucca Mountain, Nye County, Nevada

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Thordarson, W.; Rush, F.E.; Waddell, S.J.

    Test well USW H-3 is one of several test wells drilled in the southwestern part of the Nevada Test Site in cooperation with the US Department of Energy for investigations related to the isolation of high-level radioactive wastes. All rocks penetrated by the well to a total depth of 1219 meters are volcanic tuff of Tertiary age. The composite hydraulic head in the zone 751 to 1219 meters was 733 meters above sea level, and at a depth below land surface of 751 meters. Below a depth of 1190 meters, the hydraulic head was 754 meters above sea level ormore » higher, suggesting an upward component of groundwater flow at the site. The most transmissive part of the saturated zone is in the upper part of the Tram Member of the Crater Flat Tuff in the depth interval from 809 to 841 meters, with an apparent transmissivity of about 7 x 10{sup -1} meter squared per day. The remainder of the penetrated rocks in the saturated zone, 841 to 1219 meters, has an apparent transmissivity of about 4 x 10{sup -1} meter squared per day. The most transmissive part of the lower depth interval is in the bedded tuff and Lithic Ridge Tuff, in the depth interval from 1108 to 1120 meters. The apparent hydraulic conductivity of the rocks in the lower depth interval from 841 to 1219 meters commonly ranges from about 10{sup -1} to 10{sup -4} meter per day. 32 references, 20 figures, 4 tables.« less

  4. Numerical investigation of the mechanical properties of the additive manufactured bone scaffolds fabricated by FDM: The effect of layer penetration and post-heating.

    PubMed

    Naghieh, S; Karamooz Ravari, M R; Badrossamay, M; Foroozmehr, E; Kadkhodaei, M

    2016-06-01

    In recent years, thanks to additive manufacturing technology, researchers have gone towards the optimization of bone scaffolds for the bone reconstruction. Bone scaffolds should have appropriate biological as well as mechanical properties in order to play a decisive role in bone healing. Since the fabrication of scaffolds is time consuming and expensive, numerical methods are often utilized to simulate their mechanical properties in order to find a nearly optimum one. Finite element analysis is one of the most common numerical methods that is used in this regard. In this paper, a parametric finite element model is developed to assess the effects of layers penetration׳s effect on inter-layer adhesion, which is reflected on the mechanical properties of bone scaffolds. To be able to validate this model, some compression test specimens as well as bone scaffolds are fabricated with biocompatible and biodegradable poly lactic acid using fused deposition modeling. All these specimens are tested in compression and their elastic modulus is obtained. Using the material parameters of the compression test specimens, the finite element analysis of the bone scaffold is performed. The obtained elastic modulus is compared with experiment indicating a good agreement. Accordingly, the proposed finite element model is able to predict the mechanical behavior of fabricated bone scaffolds accurately. In addition, the effect of post-heating of bone scaffolds on their elastic modulus is investigated. The results demonstrate that the numerically predicted elastic modulus of scaffold is closer to experimental outcomes in comparison with as-built samples. Copyright © 2016 Elsevier Ltd. All rights reserved.

  5. Molecular induced skyhook effect for magnetic interlayer softening

    NASA Astrophysics Data System (ADS)

    Friedrich, Rico; Caciuc, Vasile; Atodiresei, Nicolae; Blügel, Stefan

    2015-11-01

    Our first-principles study demonstrates for the first time that by increasing the molecule-surface binding strength, the interlayer magnetic coupling of a ferromagnetic metal can be drastically reduced with respect to that of a clean substrate. Importantly, for a weakly chemisorbed molecule the rehybridization of metal atomic d states within the molecule-induced surface geometry (geometrical effect) plays a crucial role in obtaining interlayer magnetic softening. On the contrary, for a strongly chemisorbed molecule the interlayer magnetic coupling is further reduced due to an interplay between the geometrical effect and the hybridization of atomic d states with molecular ones.

  6. Partial liquid-penetration inside a deep trench by film flowing over it

    NASA Astrophysics Data System (ADS)

    Nguyen, Phuc-Khanh; Dimakopoulos, Yiannis; Tsamopoulos, John

    2014-11-01

    Liquid film flow along substrates featuring a deep trench may not wet the trench floor, but create a second gas-liquid interface inside the trench. The liquid penetration inside the trench depends on the location and shape of this inner interface. The penetration increases by decreasing the two three-phase contact lines between the inner interface and the two side-walls or the flow rate and depends on the liquid properties. This partial-penetration is studied by employing the Galerkin / finite element method to solve the two-dimensional steady-state Navier-Stokes equations in a physical domain that is adaptively remeshed. Multiple branches of steady solutions connected via turning points are revealed by pseudo arc-length continuation. Flow hysteresis may occur in a certain range of liquid penetration depth, when the interaction of the two interfaces changes qualitatively. This induces an abrupt jump of penetration distance and deformation amplitude of the outer interface. Work supported by the General Secretariat of Research & Technology of Greece through the program ``Excellence'' (Grant No. 1918) in the framework ``Education and Lifelong Learning'' co-funded by the ESF.

  7. Activity and Stability of (Pr 1-xNd x) 2NiO 4 as Cathodes for Solid Oxide Fuel Cells: Part V. In Situ Studies of Phase Evolution

    DOE PAGES

    Dogdibegovic, Emir; Alabri, Nawf S.; Wright, Christopher J.; ...

    2017-08-12

    This study is to complement an early report (the manuscript is attached for review purpose) on the role of interlayer on activity and performance stability in praseodymium nickelates. The aforementioned report showed a remarkable 48% increase in power density while switching from common GDC interlayer to a new interlayer chemistry (PGCO). Furthermore, a stable long-term performance was linked with suppressed reaction between the cathode and PGCO interlayer. In this article, we report in situ studies of the phase evolution. The high energy XRD studies at a synchrotron source showed fully suppressed phase transition in praseodymium nickelates with PGCO interlayer, whilemore » the electrodes on the GDC interlayer undergo substantial phase transformation. Furthermore, in operando and post-test XRD analyses shown fully suppressed structural changes in electrodes operated in full cells at 750°C and 0.80 V for 500 hours. SEM-EDS analysis showed that the formation of PrO x at the cathode-interlayer interface may play a role in a decrease of mechanical integrity of the interfaces, due to thermal expansion mismatch, leading to a local stress between the two phases. Furthermore, phase evolution at a narrow interface may propagate toward the electrode bulk, leading to structural changes Q1 and performance degradation.« less

  8. Activity and Stability of (Pr 1-xNd x) 2NiO 4 as Cathodes for Solid Oxide Fuel Cells: Part V. In Situ Studies of Phase Evolution

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Dogdibegovic, Emir; Alabri, Nawf S.; Wright, Christopher J.

    This study is to complement an early report (the manuscript is attached for review purpose) on the role of interlayer on activity and performance stability in praseodymium nickelates. The aforementioned report showed a remarkable 48% increase in power density while switching from common GDC interlayer to a new interlayer chemistry (PGCO). Furthermore, a stable long-term performance was linked with suppressed reaction between the cathode and PGCO interlayer. In this article, we report in situ studies of the phase evolution. The high energy XRD studies at a synchrotron source showed fully suppressed phase transition in praseodymium nickelates with PGCO interlayer, whilemore » the electrodes on the GDC interlayer undergo substantial phase transformation. Furthermore, in operando and post-test XRD analyses shown fully suppressed structural changes in electrodes operated in full cells at 750°C and 0.80 V for 500 hours. SEM-EDS analysis showed that the formation of PrO x at the cathode-interlayer interface may play a role in a decrease of mechanical integrity of the interfaces, due to thermal expansion mismatch, leading to a local stress between the two phases. Furthermore, phase evolution at a narrow interface may propagate toward the electrode bulk, leading to structural changes Q1 and performance degradation.« less

  9. Carbon felt interlayer derived from rice paper and its synergistic encapsulation of polysulfides for lithium-sulfur batteries

    NASA Astrophysics Data System (ADS)

    Yang, Kai; Zhong, Lei; Guan, Ruiteng; Xiao, Min; Han, Dongmei; Wang, Shuanjin; Meng, Yuezhong

    2018-05-01

    Lithium-sulfur (Li-S) batteries have remarkably high theoretical specific capacity as promising candidates for next-generation energy storage. However, the "polysulfides shuttle" effect hampers its commercial application. Here, we use a kind of rice paper as a raw material to get inorganic oxides doping carbon felt by the facile carbonization method, and then modified by a simple coating process using poly (fluorenyl ether ketone) and Super P slurry. The special structure of the carbon felt derived from rice paper and its modified layer endow the final electronic conductive interlayer with inherent polysulfides absorbents and ion Coulombic repulsion functions, respectively, which show synergistic effect for trapping polysulfides. As an interlayer of Li-S batteries, the obtained carbon felt/poly (fluorenyl ether ketone)& Super P (CFSS) interlayer shows excellent electrochemical performance in improving specific capacity and decreasing polarization. The batteries with CFSS interlayer exhibit a high capacity of 837 mA h g-1 at 2.0 C and a high initial capacity of 1073.4 mA h g-1 and good capacity retention of 824.5 mA h g-1 after 500 cycles at 0.5 C. CFSS interlayer also shows excellent anti-self-discharge performance. Therefore, the simple and economical CFSS interlayer can be considered as a promising component for high performance Li-S batteries.

  10. Effect of sulphur vacancy and interlayer interaction on the electronic structure and spin splitting of bilayer MoS2.

    PubMed

    Dong, Yulan; Zeng, Bowen; Xiao, Jin; Zhang, Xiaojiao; Li, Dongde; Li, Mingjun; He, Jun; Long, Mengqiu

    2018-02-27

    Molybdenum disulfide (MoS 2 ) is one of the candidate materials for nanoelectronics and optoelectronics devices in the future. The electronic and magnetic properties of MoS 2 can be regulated by interlayer interaction and the vacancy effect. Nevertheless, the combined effect of these two factors on MoS 2 is not clearly understood. In this study, we have investigated the impact of a single S vacancy combined with interlayer interaction on the properties of bilayer MoS 2 . Our calculated results show that an S vacancy brings impurity states in the band structure of bilayer MoS 2 , and the energy level of the impurity states can be affected by the interlayer distance, which finally disappears in the bulk state when the layer distance is relatively small. Moreover, during the compression of bilayer MoS 2 , the bottom layer, where the S vacancy stays, gets an additional charge due to interlayer charge transfer, which first increases, and then decreases due to gradually forming the interlayer S-S covalent bond, as interlayer distance decreases. The change of the additional charge is consistent with the change of the total magnetic moment of the bottom layers, no magnetic moment has been found in the top layer. The distribution of magnetic moment mainly concentrates on the three Mo atoms around the S vacancy, for each of which the magnetic moment is very much related to the Mo-Mo length. Our conclusion is that the interlayer charge transfer and S vacancy co-determine the magnetic properties of this system, which may be a useful way to regulate the electronic and magnetic properties of MoS 2 for potential applications.

  11. Effects of exchanged cation and layer charge on the sorption of water and EGME vapors on montmorillonite clays

    USGS Publications Warehouse

    Chiou, Cary T.; Rutherford, David W.

    1997-01-01

    The effects of exchanged cation and layer charge on the sorption of water and ethylene glycol monoethyl ether (EGME) vapors on montmorillonite have been studied on SAz-1 and SWy-1 source clays, each exchanged respectively with Ca, Na, K, Cs and tetramethylammonium (TMA) cations. The corresponding lattice expansions were also determined, and the corresponding N2 adsorption data were provided for comparison. For clays exchanged with cations of low hydrating powers (such as K, Cs and TMA), water shows a notably lower uptake than does N2 at low relative pressures (P/P0). By contrast, EGME shows higher uptakes than N2 on all exchanged clays at all P/P0. The anomaly for water is attributed to its relatively low attraction for siloxane surfaces of montmorillonite because of its high cohesive energy density. In addition to solvating cations and expanding interlayers, water and EGME vapors condense into small clay pores and interlayer voids created by interlayer expansion. The initial (dry) interlayer separation varies more significantly with cation type than with layer charge; the water-saturated interlayer separation varies more with cation type than the EGME-saturated interlayer separation. Because of the differences in surface adsorption and interlayer expansion for water and EGME, no general correspondence is found between the isotherms of water and EGME on exchanged clays, nor is a simple relation observed between the overall uptake of either vapor and the cation solvating power. The excess interlayer capacities of water and of EGME that result from lattice expansion of the exchanged clays are estimated by correcting for amounts of vapor adsorption on planar clay surfaces and of vapor condensation into intrinsic clay pores. The resulting data follow more closely the relative solvating powers of the exchanged cations.

  12. Effect of sulphur vacancy and interlayer interaction on the electronic structure and spin splitting of bilayer MoS2

    NASA Astrophysics Data System (ADS)

    Dong, Yulan; Zeng, Bowen; Xiao, Jin; Zhang, Xiaojiao; Li, Dongde; Li, Mingjun; He, Jun; Long, Mengqiu

    2018-03-01

    Molybdenum disulfide (MoS2) is one of the candidate materials for nanoelectronics and optoelectronics devices in the future. The electronic and magnetic properties of MoS2 can be regulated by interlayer interaction and the vacancy effect. Nevertheless, the combined effect of these two factors on MoS2 is not clearly understood. In this study, we have investigated the impact of a single S vacancy combined with interlayer interaction on the properties of bilayer MoS2. Our calculated results show that an S vacancy brings impurity states in the band structure of bilayer MoS2, and the energy level of the impurity states can be affected by the interlayer distance, which finally disappears in the bulk state when the layer distance is relatively small. Moreover, during the compression of bilayer MoS2, the bottom layer, where the S vacancy stays, gets an additional charge due to interlayer charge transfer, which first increases, and then decreases due to gradually forming the interlayer S-S covalent bond, as interlayer distance decreases. The change of the additional charge is consistent with the change of the total magnetic moment of the bottom layers, no magnetic moment has been found in the top layer. The distribution of magnetic moment mainly concentrates on the three Mo atoms around the S vacancy, for each of which the magnetic moment is very much related to the Mo-Mo length. Our conclusion is that the interlayer charge transfer and S vacancy co-determine the magnetic properties of this system, which may be a useful way to regulate the electronic and magnetic properties of MoS2 for potential applications.

  13. Clinical study assessing the photosensitizer accumulation and light penetration for esophageal cancer prior to treatment by PDT

    NASA Astrophysics Data System (ADS)

    Bargo, Paulo R.; Jacques, Steven L.

    2001-07-01

    The FDA has approved PDT using Photofrin for certain esophageal and lung cancers, specifying an approved prescription of administered drug (mg/kg body weight) and administered light (J/linear cm of cylindrical fiber). This paper describes our development of a multi-optical fiber catheter for endoscopic use which documents the drug accumulated in the target tissues and the light penetration into the target tissues. The catheter uses reflectance to specify the light penetration depth and uses reflectance- corrected fluorescence to document drug accumulation. The goal is to document the variation in drug and light received by patients who are administered the FDA-approved prescription.

  14. High-resolution scanning Hall probe microscopy

    NASA Astrophysics Data System (ADS)

    Hallen, Hans D.; Hess, H. F.; Chang, A. M.; Pfeiffer, Loren N.; West, Kenneth W.; Mitzi, David B.

    1993-06-01

    A high resolution scanning Hall probe microscope is used to spatially resolve vortices in high temperature superconducting Bi2Sr2CaCu2O8+(delta) crystals. We observe a partially ordered vortex lattice at several different applied magnetic fields and temperatures. At higher temperatures, a limited amount of vortex re-arrangement is observed, but most vortices remain fixed for periods long compared to the imaging time of several hours even at temperatures as high as 75 degree(s)K (the superconducting transition temperature for these crystals is approximately 84 degree(s)K). A measure of these local magnetic penetration depth can be obtained from a fit to the surface field of several neighboring vortices, and has been measured as a function of temperature. In particular, we have measured the zero temperature penetration depth and found it to be 275 +/- 40 nm.

  15. DOE Office of Scientific and Technical Information (OSTI.GOV)

    Checco, A.; Hofmann, T.; DiMasi, E.

    The details of air nanobubble trapping at the interface between water and a nanostructured hydrophobic silicon surface are investigated using X-ray scattering and contact angle measurements. Large-area silicon surfaces containing hexagonally packed, 20 nm wide hydrophobic cavities provide ideal model surfaces for studying the morphology of air nanobubbles trapped inside cavities and its dependence on the cavity depth. Transmission small-angle X-ray scattering measurements show stable trapping of air inside the cavities with a partial water penetration of 5-10 nm into the pores, independent of their large depth variation. This behavior is explained by consideration of capillary effects and the cavitymore » geometry. For parabolic cavities, the liquid can reach a thermodynamically stable configuration - a nearly planar nanobubble meniscus - by partially penetrating into the pores. This microscopic information correlates very well with the macroscopic surface wetting behavior.« less

  16. Improved oxidation resistance of organic/inorganic composite atomic layer deposition coated cellulose nanocrystal aerogels

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Smith, Sean W.; Matthews, David J.; Conley, John F., E-mail: jconley@eecs.oregonstate.edu

    2014-07-01

    Cellulose nanocrystal (CNC) aerogels are coated with thin conformal layers of Al{sub 2}O{sub 3} using atomic layer deposition to form hybrid organic/inorganic nanocomposites. Electron probe microanalysis and scanning electron microscopy analysis indicated the Al{sub 2}O{sub 3} penetrated more than 1500 μm into the aerogel for extended precursor pulse and exposure/purge times. The measured profile of coated fiber radius versus depth from the aerogel surface agrees well with simulations of precursor penetration depth in modeled aerogel structures. Thermogravimetric analysis shows that Al{sub 2}O{sub 3} coated CNC aerogel nanocomposites do not show significant thermal degradation below 295 °C as compared with 175 °C for uncoatedmore » CNC aerogels, an improvement of over 100 °C.« less

  17. Biochemical and physical factors affecting discoloration characteristics of 19 bovine muscles.

    PubMed

    McKenna, D R; Mies, P D; Baird, B E; Pfeiffer, K D; Ellebracht, J W; Savell, J W

    2005-08-01

    Steaks from muscles (n=19 from nine beef carcasses) were evaluated over the course of retail display (0-, 1-, 2-, 3-, 4- or 5-d) for objective measures of discoloration (metmyoglobin, oxymyoglobin, L*-, a*-, and b*-values), reducing ability (metmyoglobin reductase activity (MRA), resistance to induced metmyoglobin formation (RIMF), and nitric oxide metmyoglobin reducing ability (NORA)), oxygen consumption rate (OCR), oxygen penetration depth, myoglobin content, oxidative rancidity, and pH. Muscles were grouped according to objective color measures of discoloration. M. longissimus lumborum, M. longissimus thoracis, M. semitendinosus, and M. tensor fasciae latae were grouped as "high" color stability muscles, M. semimembranosus, M. rectus femoris, and M. vastus lateralis were grouped as "moderate" color stability muscles, M. trapezius, M. gluteus medius, and M. latissimus dorsi were grouped as "intermediate" color stability muscles, M. triceps brachi - long head, M. biceps femoris, M. pectoralis profundus, M. adductor, M. triceps brachi - lateral head, and M. serratus ventralis were grouped as "low" color stability muscles, and M. supraspinatus, M. infraspinatus, and M. psoas major were grouped as "very low" color stability muscles. Generally, muscles of high color stability had high RIMF, nitric oxide reducing ability, and oxygen penetration depth and possessed low OCRs, myoglobin content, and oxidative rancidity. In contrast, muscles of low color stability had high MRA, OCRs, myoglobin content, and oxidative rancidity and low RIMF, NORA, and oxygen penetration depth. Data indicate that discoloration differences between muscles are related to the amount of reducing activity relative to the OCR.

  18. Effect of AEM energy applicator configuration on magnetic nanoparticle mediated hyperthermia for breast cancer.

    PubMed

    Sanapala, Krishna K; Hewaparakrama, Kapila; Kang, Kyung A

    2011-01-01

    Magnetic nanoparticle mediated low heat hyperthermia (42~45( o )C) via alternating electromagnetic (AEM) energy is a promising, cancer specific and minimally-invasive cancer therapy. Iron oxide particles frequently used for this therapy are non-toxic and already used as a contrast agent for magnetic resonance imaging. One important issue in the hyperthermia is applying an appropriate amount of energy to the tumor at various sizes and depths, with a minimal damage to normal tissue. For the therapy to be desirable, the AEM energy applicator needs to be non-invasive and user-friendly. To better understand the effect of the probe on the magnetic field distribution, computer simulation was performed for the field distribution by probes with various configurations. In a solenoid-type probe, the field is mainly inside the probe and, therefore, is difficult to use on body. A pancake-shaped probe is easy to use but the field penetration is shallow and, thus, may better serve surface tumor treatment. A sandwich probe, composed of two pancake probes, has a penetration depth deeper than a pancake probe. The results also showed that the spacing between two adjacent coils and the number of coil turns are very important for controlling the field penetration depth and strength. Experiments were also performed to study the effects of the size and concentration of iron oxide nanoparticles on heating. Among the tested particle sizes of 10~50 nm, 30 nm particles showed the best heating for the same mass.

  19. Characterization of scintillator crystals for usage as prompt gamma monitors in particle therapy

    NASA Astrophysics Data System (ADS)

    Roemer, K.; Pausch, G.; Bemmerer, D.; Berthel, M.; Dreyer, A.; Golnik, C.; Hueso-González, F.; Kormoll, T.; Petzoldt, J.; Rohling, H.; Thirolf, P.; Wagner, A.; Wagner, L.; Weinberger, D.; Fiedler, F.

    2015-10-01

    Particle therapy in oncology is advantageous compared to classical radiotherapy due to its well-defined penetration depth. In the so-called Bragg peak, the highest dose is deposited; the tissue behind the cancerous area is not exposed. Different factors influence the range of the particle and thus the target area, e.g. organ motion, mispositioning of the patient or anatomical changes. In order to avoid over-exposure of healthy tissue and under-dosage of cancerous regions, the penetration depth of the particle has to be monitored, preferably already during the ongoing therapy session. The verification of the ion range can be performed using prompt gamma emissions, which are produced by interactions between projectile and tissue, and originate from the same location and time of the nuclear reaction. The prompt gamma emission profile and the clinically relevant penetration depth are correlated. Various imaging concepts based on the detection of prompt gamma rays are currently discussed: collimated systems with counting detectors, Compton cameras with (at least) two detector planes, or the prompt gamma timing method, utilizing the particle time-of-flight within the body. For each concept, the detection system must meet special requirements regarding energy, time, and spatial resolution. Nonetheless, the prerequisites remain the same: the gamma energy region (2 to 10 MeV), high counting rates and the stability in strong background radiation fields. The aim of this work is the comparison of different scintillation crystals regarding energy and time resolution for optimized prompt gamma detection.

  20. High-temperature thermal treatment of the uterus

    NASA Astrophysics Data System (ADS)

    Ryan, Thomas P.; Xiao, Jia Hua; Chung, Juh Yun

    2003-06-01

    More than 200,000 hysterectomies are performed annually in the US due to abnormal uterine bleeding from excessive menstrual flow. A minimally invasive procedure has been developed using thermal treatment combined with pressure to the endometrial lining of the uterus. Results from a 3-D finite element model will be shown, as well as experimental data. Good correlation was seen between simulations and experiments. The study found similar results then temperatures were increased and times for treatment were shortened.More than 200,000 hysterectomies are performed annually in the US due to abnormal uterine bleeding from excessive menstrual flow. A minimally invasive procedure has been developed using a balloon-based thermal treatment combined with pressure to the endometrial lining of the uterus. A 3D finite element model was set up to simulate the balloon ablation device in the human uterus as used in over 150,000 patients to date. Several additional simulations were made at higher temperatures to seek alternative combinations with higher temperature and shorter time intervals for the same depth of penetration, or deeper penetration at longer times and elevated temperatures. A temperature range of 87 to 150°C was explored. The Bioheat Equation was used in the simulations to predict temperature distributions in tissue. The Damage Integral was also used to characterize the location at depth of irreversible damage in the uterus. Treatment safety issues were also analyzed as the simulations showed the depth of penetration into the myometrium, towards the serosa.

  1. Crater Morphology of Engineered and Natural Impactors into Planetary Ice

    NASA Astrophysics Data System (ADS)

    Danner, M.; Winglee, R.; Koch, J.

    2017-12-01

    Crater morphology of engineered impactors, such as those proposed for the Europa Kinetic Ice Penetrator (EKIP) mission, varies drastically from that of natural impactors (i.e. Asteroids, meteoroids). Previous work of natural impact craters in ice have been conducted with the intent to bound the thickness of Europa's ice crust; this work focuses on the depth, size, and compressional effects caused by various impactor designs, and the possible effects to the Europan surface. The present work details results from nine projectiles that were dropped on the Taku Glacier, AK at an altitude of 775 meters above surface; three rocks to simulate natural impactors, and six iterations of engineered steel and aluminum penetrator projectiles. Density measurements were taken at various locations within the craters, as well as through a cross section of the crater. Due to altitude restrictions, projectiles remained below terminal velocity. The natural/rock impact craters displayed typical cratering characteristics such as shallow, half meter scale depth, and orthogonal compressional forcing. The engineered projectiles produced impact craters with depths averaging two meters, with crater widths matching the impactor diameters. Compressional waves from the engineered impactors propagated downwards, parallel to direction of impact. Engineered impactors create significantly less lateral fracturing than natural impactors. Due to the EKIP landing mechanism, sampling of pristine ice closer to the lander is possible than previously thought with classical impact theory. Future work is planned to penetrate older, multiyear ice with higher velocity impacts.

  2. Wide field video-rate two-photon imaging by using spinning disk beam scanner

    NASA Astrophysics Data System (ADS)

    Maeda, Yasuhiro; Kurokawa, Kazuo; Ito, Yoko; Wada, Satoshi; Nakano, Akihiko

    2018-02-01

    The microscope technology with wider view field, deeper penetration depth, higher spatial resolution and higher imaging speed are required to investigate the intercellular dynamics or interactions of molecules and organs in cells or a tissue in more detail. The two-photon microscope with a near infrared (NIR) femtosecond laser is one of the technique to improve the penetration depth and spatial resolution. However, the video-rate or high-speed imaging with wide view field is difficult to perform with the conventional two-photon microscope. Because point-to-point scanning method is used in conventional one, so it's difficult to achieve video-rate imaging. In this study, we developed a two-photon microscope with spinning disk beam scanner and femtosecond NIR fiber laser with around 10 W average power for the microscope system to achieve above requirements. The laser is consisted of an oscillator based on mode-locked Yb fiber laser, a two-stage pre-amplifier, a main amplifier based on a Yb-doped photonic crystal fiber (PCF), and a pulse compressor with a pair of gratings. The laser generates a beam with maximally 10 W average power, 300 fs pulse width and 72 MHz repetition rate. And the beam incident to a spinning beam scanner (Yokogawa Electric) optimized for two-photon imaging. By using this system, we achieved to obtain the 3D images with over 1mm-penetration depth and video-rate image with 350 x 350 um view field from the root of Arabidopsis thaliana.

  3. Observation of van Hove Singularities in Twisted Silicene Multilayers.

    PubMed

    Li, Zhi; Zhuang, Jincheng; Chen, Lan; Ni, Zhenyi; Liu, Chen; Wang, Li; Xu, Xun; Wang, Jiaou; Pi, Xiaodong; Wang, Xiaolin; Du, Yi; Wu, Kehui; Dou, Shi Xue

    2016-08-24

    Interlayer interactions perturb the electronic structure of two-dimensional materials and lead to new physical phenomena, such as van Hove singularities and Hofstadter's butterfly pattern. Silicene, the recently discovered two-dimensional form of silicon, is quite unique, in that silicon atoms adopt competing sp(2) and sp(3) hybridization states leading to a low-buckled structure promising relatively strong interlayer interaction. In multilayer silicene, the stacking order provides an important yet rarely explored degree of freedom for tuning its electronic structures through manipulating interlayer coupling. Here, we report the emergence of van Hove singularities in the multilayer silicene created by an interlayer rotation. We demonstrate that even a large-angle rotation (>20°) between stacked silicene layers can generate a Moiré pattern and van Hove singularities due to the strong interlayer coupling in multilayer silicene. Our study suggests an intriguing method for expanding the tunability of the electronic structure for electronic applications in this two-dimensional material.

  4. Temperature dependence of interlayer coupling in perpendicular magnetic tunnel junctions with GdOx barriers

    DOE PAGES

    Newhouse-Illige, T.; Xu, Y. H.; Liu, Y. H.; ...

    2018-02-13

    Perpendicular magnetic tunnel junctions with GdO X tunneling barriers have shown a unique voltage controllable interlayer magnetic coupling effect. Here we investigate the quality of the GdO X barrier and the coupling mechanism in these junctions by examining the temperature dependence of the tunneling magnetoresistance and the interlayer coupling from room temperature down to 11 K. The barrier is shown to be of good quality with the spin independent conductance only contributing a small portion, 14%, to the total room temperature conductance, similar to AlO X and MgO barriers. The interlayer coupling, however, shows an anomalously strong temperature dependence includingmore » sign changes below 80 K. This non-trivial temperature dependence is not described by previous models of interlayer coupling and may be due to the large induced magnetic moment of the Gd ions in the barrier.« less

  5. Magnetron sputtered zinc oxide nanorods as thickness-insensitive cathode interlayer for perovskite planar-heterojunction solar cells.

    PubMed

    Liang, Lusheng; Huang, Zhifeng; Cai, Longhua; Chen, Weizhong; Wang, Baozeng; Chen, Kaiwu; Bai, Hua; Tian, Qingyong; Fan, Bin

    2014-12-10

    Suitable electrode interfacial layers are essential to the high performance of perovskite planar heterojunction solar cells. In this letter, we report magnetron sputtered zinc oxide (ZnO) film as the cathode interlayer for methylammonium lead iodide (CH3NH3PbI3) perovskite solar cell. Scanning electron microscopy and X-ray diffraction analysis demonstrate that the sputtered ZnO films consist of c-axis aligned nanorods. The solar cells based on this ZnO cathode interlayer showed high short circuit current and power conversion efficiency. Besides, the performance of the device is insensitive to the thickness of ZnO cathode interlayer. Considering the high reliability and maturity of sputtering technique both in lab and industry, we believe that the sputtered ZnO films are promising cathode interlayers for perovskite solar cells, especially in large-scale production.

  6. Temperature dependence of interlayer coupling in perpendicular magnetic tunnel junctions with GdOx barriers

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Newhouse-Illige, T.; Xu, Y. H.; Liu, Y. H.

    Perpendicular magnetic tunnel junctions with GdO X tunneling barriers have shown a unique voltage controllable interlayer magnetic coupling effect. Here we investigate the quality of the GdO X barrier and the coupling mechanism in these junctions by examining the temperature dependence of the tunneling magnetoresistance and the interlayer coupling from room temperature down to 11 K. The barrier is shown to be of good quality with the spin independent conductance only contributing a small portion, 14%, to the total room temperature conductance, similar to AlO X and MgO barriers. The interlayer coupling, however, shows an anomalously strong temperature dependence includingmore » sign changes below 80 K. This non-trivial temperature dependence is not described by previous models of interlayer coupling and may be due to the large induced magnetic moment of the Gd ions in the barrier.« less

  7. Evolution of mechanical response of sodium montmorillonite interlayer with increasing hydration by molecular dynamics.

    PubMed

    Schmidt, Steven R; Katti, Dinesh R; Ghosh, Pijush; Katti, Kalpana S

    2005-08-16

    The mechanical response of the interlayer of hydrated montmorillonite was evaluated using steered molecular dynamics. An atomic model of the sodium montmorillonite was previously constructed. In the current study, the interlayer of the model was hydrated with multiple layers of water. Using steered molecular dynamics, external forces were applied to individual atoms of the clay surface, and the response of the model was studied. The displacement versus applied stress and stress versus strain relationships of various parts of the interlayer were studied. The paper describes the construction of the model, the simulation procedure, and results of the simulations. Some results of the previous work are further interpreted in the light of the current research. The simulations provide quantitative stress deformation relationships as well as an insight into the molecular interactions taking place between the clay surface and interlayer water and cations.

  8. Electronic cooling via interlayer Coulomb coupling in multilayer epitaxial graphene

    PubMed Central

    Mihnev, Momchil T.; Tolsma, John R.; Divin, Charles J.; Sun, Dong; Asgari, Reza; Polini, Marco; Berger, Claire; de Heer, Walt A.; MacDonald, Allan H.; Norris, Theodore B.

    2015-01-01

    In van der Waals bonded or rotationally disordered multilayer stacks of two-dimensional (2D) materials, the electronic states remain tightly confined within individual 2D layers. As a result, electron–phonon interactions occur primarily within layers and interlayer electrical conductivities are low. In addition, strong covalent in-plane intralayer bonding combined with weak van der Waals interlayer bonding results in weak phonon-mediated thermal coupling between the layers. We demonstrate here, however, that Coulomb interactions between electrons in different layers of multilayer epitaxial graphene provide an important mechanism for interlayer thermal transport, even though all electronic states are strongly confined within individual 2D layers. This effect is manifested in the relaxation dynamics of hot carriers in ultrafast time-resolved terahertz spectroscopy. We develop a theory of interlayer Coulomb coupling containing no free parameters that accounts for the experimentally observed trends in hot-carrier dynamics as temperature and the number of layers is varied. PMID:26399955

  9. Sandblasting induced stress release and enhanced adhesion strength of diamond films deposited on austenite stainless steel

    NASA Astrophysics Data System (ADS)

    Li, Xiao; Ye, Jiansong; Zhang, Hangcheng; Feng, Tao; Chen, Jianqing; Hu, Xiaojun

    2017-08-01

    We firstly used sandblasting to treat austenite stainless steel and then deposited a Cr/CrN interlayer by close field unbalanced magnetron sputtering on it. After that, diamond films were prepared on the interlayer. It is found that the sandblasting process induces phase transition from austenite to martensite in the surface region of the stainless steel, which decreases thermal stress in diamond films due to lower thermal expansion coefficient of martensite phase compared with that of austenite phase. The sandblasting also makes stainless steel's surface rough and the Cr/CrN interlayer film inherits the rough surface. This decreases the carburization extent of the interlayer, increases nucleation density and modifies the stress distribution. Due to lower residual stress and small extent of the interlayer's carburization, the diamond film on sandblast treated austenite stainless steel shows enhanced adhesion strength.

  10. Improved Understanding of Permafrost Controls on Hydrology in Interior Alaska by Integration of Ground-Based Geophysical Permafrost Characterization and Numerical Modeling

    DTIC Science & Technology

    2015-05-01

    Horiguchi and Miller, 1983; McCauley et al., 2002) that extended to a maximum depth of 90 m as influenced by the geothermal gradient and determined by... geothermal energy flux were applied to the model boundaries (Figure 5.4.1). The ground surface at 0 m depth consisted of an idealized lake bottom with...deeper saturated zone and the geothermal gradient from below the penetration depth of the annual temperature envelope. The initial condition for

  11. Ultra-hard AlMgB14 coatings fabricated by RF magnetron sputtering from a stoichiometric target

    NASA Astrophysics Data System (ADS)

    Grishin, A. M.; Khartsev, S. I.; Böhlmark, J.; Ahlgren, M.

    2015-01-01

    For the first time hard aluminum magnesium boride films were fabricated by RF magnetron sputtering from a single stoichiometric ceramic AlMgB14 target. Optimized processing conditions (substrate temperature, target sputtering power and target-to-substrate distance) enable fabrication of stoichiometric in-depth compositionally homogeneous films with the peak values of nanohardness 88 GPa and Young's modulus 517 GPa at the penetration depth of 26 nm and, respectively, 35 and 275 GPa at 200 nm depth in 2 μm thick film.

  12. Orbital SAR and Ground-Penetrating Radar for Mars: Complementary Tools in the Search for Water

    NASA Technical Reports Server (NTRS)

    Campbell, B. A.; Grant, J. A.

    2000-01-01

    The physical structure and compositional variability of the upper martian crust is poorly understood. Optical and infrared measurements probe at most the top few cm of the surface layer and indicate the presence of layered volcanics and sediments, but it is likely that permafrost, hydrothermal deposits, and transient liquid water pockets occur at depths of meters to kilometers within the crust. An orbital synthetic aperture radar (SAR) can provide constraints on surface roughness, the depth of fine-grained aeolian or volcanic deposits, and the presence of strongly absorbing near-surface deposits such as carbonates. This information is crucial to the successful landing and operation of any rover designed to search for subsurface water. A rover-based ground-penetrating radar (GPR) can reveal layering in the upper crust, the presence of erosional or other subsurface horizons, depth to a permafrost layer, and direct detection of near-surface transient liquid water. We detail here the radar design parameters likely to provide the best information for Mars, based on experience with SAR and GPR in analogous terrestrial or planetary environments.

  13. Geohydrology of rocks penetrated by test well USW H-4, Yucca Mountain, Nye County, Nevada

    USGS Publications Warehouse

    Whitfield, M.S.; Eshom, E.P.; Thordarson, William; Schaefer, D.H.

    1985-01-01

    Test well USW H-4 is one of several wells drilled in the southwestern part of the Nevada Test Site for hydraulic testing, hydrologic monitoring, and geophysical logging. The work was performed in cooperation with the U.S. Department of Energy. The rocks penetrated by the well to a total depth of 1,219 m were volcanic tuffs of Tertiary age. Hydraulic coefficients calculated from pumping test data indicate that transmissivity ranged from 200 to 790 sq m/day. A radioactive tracer, borehole flow survey indicated that the two most productive zones during this borehole flow survey occurred in the upper part of the Bullfrog Member of the Crater Flat Tuff, depth interval from 721 to 731.5m, and in the underlying part of the Tram Member, depth interval from 864 to 920m. The water is predominantly a sodium biocarbonate type with small concentrations of calcium, magnesium, and sulfate. The apparent age of this composite water sample was determined by carbon-14 date of 17,200 years before present. (USGS)

  14. Comparison of Ecological Impacts of Postulated Oil Spills at Selected Alaskan Locations. Volume 1. Introduction, Summary, Methodology, Evaluation and Appendices

    DTIC Science & Technology

    1975-06-01

    MECHANISM : ALUMINOSILICATE ORGANIC INTERACTION IN SALINE WATERS, A.C.S. Tom M 21 (1969-1970) to be published in Advances in Chemistry Series. 5...recovery mechanisms . Detailed information on various devices is given in Sittig3 and by EPA. (1) WEIR DEVICES Weir devices depend on gravity to... mechanical eguipments. The selection depends on the depth of oil penetration: 1. For oil penetration of up to 1 inch, combined use of road graders and

  15. A comparison study of different RF shields for an 8-element transceive small animal array at 9.4T.

    PubMed

    Jin, Jin; Li, Yu; Liu, Feng; Weber, Ewald; Crozier, Stuart

    2011-01-01

    In this study, three types of radio-frequency shields are studied and compared in the context of ultra-high field small-animal magnetic resonance imaging. It has been demonstrated that the coil penetration depth and mutual coupling between the coils depend heavily on the type of shield employed. The results were used to guide the design of a 9.4T 8-element transceive small animal array, which provides high overall coil penetration.

  16. Imaging calcium carbonate distribution in human sweat pore in vivo using nonlinear microscopy

    NASA Astrophysics Data System (ADS)

    Chen, Xueqin; Gasecka, Alicja; Formanek, Florian; Galey, Jean-Baptiste; Rigneault, Hervé

    2015-03-01

    Nonlinear microscopies, including two-photon excited autofluorescence (TPEF) and coherent anti-Stokes Raman scattering (CARS), were used to study individual human sweat pore morphology and topically applied antiperspirant salt penetration inside sweat pore, in vivo on human palms. Sweat pore inner morphology in vivo was imaged up to the depth of 100 μm by TPEF microscopy. The 3D penetration and distribution of "in situ calcium carbonate" (isCC), an antiperspirant salt model, was investigated using CARS microscopy.

  17. Verification of Sulfate Attack Penetration Rates for Saltstone Disposal Unit Modeling

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Flach, G. P.

    Recent Special Analysis modeling of Saltstone Disposal Units consider sulfate attack on concrete and utilize degradation rates estimated from Cementitious Barriers Partnership software simulations. This study provides an independent verification of those simulation results using an alternative analysis method and an independent characterization data source. The sulfate penetration depths estimated herein are similar to the best-estimate values in SRNL-STI-2013-00118 Rev. 2 and well below the nominal values subsequently used to define Saltstone Special Analysis base cases.

  18. Investigation of rf power absorption in the plasma of helicon ion source.

    PubMed

    Mordyk, S; Alexenko, O; Miroshnichenko, V; Storizhko, V; Stepanov, K; Olshansky, V

    2008-02-01

    The simulations of the spatial distribution of rf power absorbed in a helicon ion source reveal a correlation between the depth of penetration of rf power into the plasma and the tilt angle of lines of force of the outer magnetic field. The deeper field penetration and greater power absorption were observed at large tilt angles of the field line to the plasma surface. The evaluations as to the possibility of excitation of helicon waves in compact rf ion sources were performed.

  19. Transition of Corner Cracks at Holes into Through-The-Thickness Cracks

    DTIC Science & Technology

    1983-12-01

    upon an imaginary crack depth, which is arrived at by allowing the flaw to continually grow in the same elliptical shape it had when it penetrated the...approximately 0.75, and then they deteriorate rapidly . This value of 0.75 agrees with the value selected as the start of the transition region along the bore of...a corner crack emanating from a hole as it grows until it reaches final fracture. However, in a region near where the corner crack penetrates the back

  20. The coherent interlayer resistance of a single, rotated interface between two stacks of AB graphite

    NASA Astrophysics Data System (ADS)

    Habib, K. M. Masum; Sylvia, Somaia S.; Ge, Supeng; Neupane, Mahesh; Lake, Roger K.

    2013-12-01

    The coherent, interlayer resistance of a misoriented, rotated interface between two stacks of AB graphite is determined for a variety of misorientation angles. The quantum-resistance of the ideal AB stack is on the order of 1 to 10 mΩ μm2. For small rotation angles, the coherent interlayer resistance exponentially approaches the ideal quantum resistance at energies away from the charge neutrality point. Over a range of intermediate angles, the resistance increases exponentially with cell size for minimum size unit cells. Larger cell sizes, of similar angles, may not follow this trend. The energy dependence of the interlayer transmission is described.

  1. Inter-layer potential for hexagonal boron nitride

    NASA Astrophysics Data System (ADS)

    Leven, Itai; Azuri, Ido; Kronik, Leeor; Hod, Oded

    2014-03-01

    A new interlayer force-field for layered hexagonal boron nitride (h-BN) based structures is presented. The force-field contains three terms representing the interlayer attraction due to dispersive interactions, repulsion due to anisotropic overlaps of electron clouds, and monopolar electrostatic interactions. With appropriate parameterization, the potential is able to simultaneously capture well the binding and lateral sliding energies of planar h-BN based dimer systems as well as the interlayer telescoping and rotation of double walled boron-nitride nanotubes of different crystallographic orientations. The new potential thus allows for the accurate and efficient modeling and simulation of large-scale h-BN based layered structures.

  2. Plasticized Polymer Interlayer for Low-Temperature Fabrication of a High-Quality Silver Nanowire-Based Flexible Transparent and Conductive Film

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Jo, Wonhee; Kang, Hong Suk; Choi, Jaeho

    Silver nanowires (AgNWs) are one of the most promising materials to replace commercially available indium tin oxide in flexible transparent conductive films (TCFs); however, there are still numerous problems originating from poor AgNW junction formation and improper AgNW embedment into transparent substrates. To mitigate these problems, high-temperature processes have been adopted; however, unwanted substrate deformation prevents the use of these processes for the formation of flexible TCFs. In this work, we present a novel poly(methyl methacrylate) interlayer plasticized by dibutyl phthalate for low-temperature fabrication of AgNW-based TCFs, which does not cause any substrate deformation. By exploiting the viscoelastic properties ofmore » the plasticized interlayer near the lowered glass-transition temperature, a monolithic junction of AgNWs on the interlayer and embedment of the interconnected AgNWs into the interlayer are achieved in a single-step pressing. The resulting AgNW-TCFs are highly transparent (~92% at a wavelength of 550 nm), highly conductive (<90 Ω/sq), and environmentally and mechanically robust. Therefore, the plasticized interlayer provides a simple and effective route to fabricate high-quality AgNW-based TCFs.« less

  3. Results of the mole penetration tests in different materials

    NASA Astrophysics Data System (ADS)

    Wawrzaszek, Roman; Seweryn, Karol; Grygorczuk, Jerzy; Banaszkiewicz, Marek; Rybus, Tomasz; Wisniewski, Lukasz; Neal, Clive R.; Huang, Shaopeng

    2010-05-01

    Mole devices are low velocity, medium to high energy, self-driven penetrators, designed as a carrier of different sensors for in situ investigations of subsurface layers of planetary bodies. The maximum insertion depth of such devices is limited by energy of single mole's stroke and soil resistance for the dynamic penetration. A mole penetrator ‘KRET' has been designed, developed, and successfully tested at Space Research Centre PAS in Poland. The principle of operation of the mole bases on the interaction between three masses: the cylindrical casing, the hammer, and the rest of the mass, acting as a support mass. This approach takes advantage of the MUPUS penetrator (a payload of Philae lander on Rosetta mission) insertion tests knowledge. Main parameters of the mole KRET are listed below: - outer diameter: 20.4mm, - length: 330mm, - total mass: 488g, - energy of the driving spring: 2.2J, - average power consumption: 0.28W, - average insertion progress/stroke: 8.5mm, The present works of Space Research Center PAS team are focused on three different activities. First one includes investigations of the mole penetration effectiveness in the lunar analogues (supported by ESA PECS project). Second activity, supported by Polish national fund, is connected with numerical calculation of the heat flow investigations and designing and developing the Heat Flow Probe Hardware Component (HPHC) for L-GIP NASA project. It's worth noting that L-GIP project refers to ILN activity. Last activity focuses on preparing the second version of the mole ready to work in low thermal and pressure conditions. Progress of a mole penetrator in granular medium depends on the mechanical properties of this medium. The mole penetrator ‘KRET' was tested in different materials: dry quartz sand (0.3 - 0.8 grain size), wet quartz sand, wheat flour and lunar regolith mechanical simulant - Chemically Enhanced OB-1 (CHENOBI). Wheat flour was selected due to its high cohesion rate and small grain size. Influence of the material compaction on the mole progress was also investigated. For these tests the small testbed has been used. It allowed us to test our mole penetrator up to the depth of 0.5 meters. Obtained results show that 'KRET' is able to penetrate even compacted lunar regolith simulant CHENOBI with minimum progress rate about 2mm per stroke. Moreover, we have confirmed that the mole works properly in both materials with low and high cohesion.

  4. How Confocal Is Confocal Raman Microspectroscopy on the Skin? Impact of Microscope Configuration and Sample Preparation on Penetration Depth Profiles.

    PubMed

    Lunter, Dominique Jasmin

    2016-01-01

    The aim of the study was to elucidate the effect of sample preparation and microscope configuration on the results of confocal Raman microspectroscopic evaluation of the penetration of a pharmaceutical active into the skin (depth profiling). Pig ear skin and a hydrophilic formulation containing procaine HCl were used as a model system. The formulation was either left on the skin during the measurement, or was wiped off or washed off prior to the analysis. The microscope configuration was varied with respect to objectives and pinholes used. Sample preparation and microscope configuration had a tremendous effect on the results of depth profiling. Regarding sample preparation, the best results could be observed when the formulation was washed off the skin prior to the analysis. Concerning microscope configuration, the use of a 40 × 0.6 numerical aperture (NA) objective in combination with a 25-µm pinhole or a 100 × 1.25 NA objective in combination with a 50-µm pinhole was found to be advantageous. Complete removal of the sample from the skin before the analysis was found to be crucial. A thorough analysis of the suitability of the chosen microscope configuration should be performed before acquiring concentration depth profiles. © 2016 S. Karger AG, Basel.

  5. Depth-Penetrating Temperature Measurements of Thermal Barrier Coatings Incorporating Thermographic Phosphors

    NASA Technical Reports Server (NTRS)

    Eldridge, Jeffrey I.; Bencic, Timothy J..; Allison, Stephen W.; Beshears, David L.

    2003-01-01

    Thermographic phosphors have been previously demonstrated to provide effective non-contact, emissivity-independent surface temperature measurements. Because of the translucent nature of thermal barrier coatings (TBCs), thermographic phosphor-based temperature measurements can be extended beyond the surface to provide depth-selective temperature measurements by incorporating the thermographic phosphor layer at the depth where the temperature measurement is desired. In this paper, thermographic phosphor (Y2O3:Eu) fluorescence decay time measurements are demonstrated to provide through-the-coating thickness temperature readings up to 1100 C with the phosphor layer residing beneath a 100 micron thick TBC (plasma-sprayed 8wt% yttria-stabilized zirconia). With an appropriately chosen excitation wavelength and detection configuration, it is shown that sufficient phosphor emission is generated to provide effective temperature measurements, despite the attenuation of both the excitation and emission intensities by the overlying TBC. This depth-penetrating temperature measurement capability should prove particularly useful for TBC diagnostics where a large thermal gradient is typically present across the TBC thickness. The fluorescence decay from the Y2O3:Eu layer exhibited both an initial short-term exponential rise and a longer-term exponential decay. The rise time constant was demonstrated to provide better temperature indication below 500 C while the decay time constant was a better indicator at higher temperatures.

  6. Confocal Imaging of the Embryonic Heart: How Deep?

    NASA Astrophysics Data System (ADS)

    Miller, Christine E.; Thompson, Robert P.; Bigelow, Michael R.; Gittinger, George; Trusk, Thomas C.; Sedmera, David

    2005-06-01

    Confocal microscopy allows for optical sectioning of tissues, thus obviating the need for physical sectioning and subsequent registration to obtain a three-dimensional representation of tissue architecture. However, practicalities such as tissue opacity, light penetration, and detector sensitivity have usually limited the available depth of imaging to 200 [mu]m. With the emergence of newer, more powerful systems, we attempted to push these limits to those dictated by the working distance of the objective. We used whole-mount immunohistochemical staining followed by clearing with benzyl alcohol-benzyl benzoate (BABB) to visualize three-dimensional myocardial architecture. Confocal imaging of entire chick embryonic hearts up to a depth of 1.5 mm with voxel dimensions of 3 [mu]m was achieved with a 10× dry objective. For the purpose of screening for congenital heart defects, we used endocardial painting with fluorescently labeled poly-L-lysine and imaged BABB-cleared hearts with a 5× objective up to a depth of 2 mm. Two-photon imaging of whole-mount specimens stained with Hoechst nuclear dye produced clear images all the way through stage 29 hearts without significant signal attenuation. Thus, currently available systems allow confocal imaging of fixed samples to previously unattainable depths, the current limiting factors being objective working distance, antibody penetration, specimen autofluorescence, and incomplete clearing.

  7. Development of a red diode laser system for photodynamic therapy

    NASA Astrophysics Data System (ADS)

    Halkiotis, Konstantinos N.; Yova, Dido M.; Uzunoglou, Nikolaos K.; Papastergiou, Georgios; Matakias, Sotiris; Koukouvinos, Ilias

    1998-07-01

    The effectiveness of photodynamic treatment modality has been proven experimentally for a large variety of tumors, during the last years. This therapy utilizes the combined action of light and photosensitizing drug. Until now, a disadvantage of PDT has be the low tissue penetration of light, at the wavelengths of most commonly available lasers, for clinical studies. The red wavelength offers the advantage of increased penetration depth in tissue, in addition several new wavelength offers the advantage of increased penetration depth in tissue, in addition several new photosensitizers present absorption band at the region 630nm to 690nm. The development of high power red diode laser system for photodynamic therapy, has provided a cost effective alternative to existing lasers for use in PDT. This paper will describe the system design, development and performance of a diode laser system, connected with a fiber optic facility, to be used for PDT. The system was based on a high power semiconductor diode laser emitting at 655nm. The laser output power was approximately 60mW at the output of a 62.5/125/900 micron fiber optic probe. FUll technical details and optical performance characteristics of the system will be discussed in this paper.

  8. Ground Penetrating Radar Survey at Yoros Fortesss,Istanbul

    NASA Astrophysics Data System (ADS)

    Kucukdemirci, M.; Yalçın, A. B.

    2016-12-01

    Geophysical methods are effective tool to detect the archaeological remains and materials, which were hidden under the ground. One of the most frequently used methods for archaeological prospection is Ground Penetrating Radar (GPR). This paper illustrates the small scale GPR survey to determine the buried archaeological features around the Yoros Fortress, located on shores of the Bosporus strait in Istanbul, during the archaeological excavations. The survey was carried out with a GSSI SIR 3000 system, using 400 Mhz center frequency bistatic antenna with the configuration of 16 bits dynamic range and 512 samples per scan. The data were collected along parallel profiles with an interval of 0.50 meters with zigzag profile configuration on the survey grids. The GPR data were processed by GPR-Slice V.7 (Ground Penetrating Radar Imaging Software). As a result, in the first shallow depths, some scattered anomalies were detected. These can be related to a small portion of archaeological ruins close to the surface. In the deeper levels, the geometry of the anomalies related to the possible archaeological ruins, looks clearer. Two horizontal and parallel anomalies were detected, with the direction NS in the depth of 1.45 meters, possibly related to the ancient channels.

  9. Assessing the Penetrating Abilities of Experimental Preparation with Dental Infiltrant Features Using Optical Microscope: Preliminary Study.

    PubMed

    Skucha-Nowak, Małgorzata; Machorowska-Pieniążek, Agnieszka; Tanasiewicz, Marta

    2016-01-01

    The aim of the infiltration technique is to penetrate demineralized enamel with a low viscosity resin. Icon® (DMG) is the first ever and so far the only dental infiltrant. Bacteriostaticity is one of the properties that should be inherent in dental infiltrants, but Icon lacks this feature. The aim of the preliminary study was to properly choose a dye which would allow us to assess the penetrating abilities of our own, experimental preparation with features of a dental infiltrant with bacteriostatic properties and to compare using an optical microscope the depth of infiltration of the designed experimental preparation with the infiltrant available on the market. The preparation is supposed to infiltrate decalcified human enamel and be assessed with an optical microscope. Eosin, neutral fuchsine and methylene blue were added to experimental preparation with dental infiltrant features and to Icon® (DMG) in order to assess the depth of penetration of the experimental solution into the decalcified layers of enamel. The experimental solution mixes well with eosin, neutral fuchsine, and methylene blue. During the preliminary study, the authors concluded that the experimental solution mixes well with methylene blue, neutral fuchsine, and eosin. An addition of eosin to a preparation which infiltrates inner, demineralized enamel layers, facilitates the assessment of such a preparation with an optical microscope. A designed experimental solution with the main ingredients, i.e., 2-hydroxyethyl methacrylate (HEMA) and tetraethylene glycol dimethacrylate (TEGDMA) with a ratio of 75% to 25% penetrates the demineralized (decalcified) inner parts of the enamel and polymerizes when exposed to light. In order to assess the infiltration of the experimental solution into the demineralized enamel layers, it is required to improve the measurement techniques that utilize optical microscopy.

  10. Effect of lavage and brush preparation on cement penetration and primary stability in tibial unicompartmental total knee arthroplasty: An experimental cadaver study.

    PubMed

    Scheele, Christian; Pietschmann, Matthias F; Schröder, Christian; Grupp, Thomas; Holderied, Melanie; Jansson, Volmar; Müller, Peter E

    2017-03-01

    Unicompartmental total knee arthroplasty (UKA) is a well-established treatment option for unicondylar osteoarthritis, and generally leads to better functional results than tricompartimental total knee arthroplasty (TKA). However, revision rates of UKAs are reported as being higher; a major reason for this is aseptic loosening of the tibial component due to implant-cement-bone interface fatigue. The objective of this study was to determine the effects of trabecular bone preparation, prior to implantation of tibial UKAs, on morphological and biomechanical outcomes in a cadaver study. Cemented UKAs were performed in 18 human cadaver knees after the bone bed was cleaned using pulsed lavage (Group A), conventional brush (Group B) or no cleaning at all (Group C, control). Morphologic cement penetration and primary stability were measured. The area proportion under the tibial component without visible cement penetration was significantly higher in Group C (21.9%, SD 11.9) than in both Group A (7.1%, SD 5.8), and Group B (6.5%, SD 4.2) (P=0.007). The overall cement penetration depth did not differ between groups. However, in the posterior part, cement penetration depth was significantly higher in Group B (1.9mm, SD 0.3) than in both Group A (1.3mm, SD 0.3) and Group C (1.4mm, SD 0.3) (P=0.015). The mode of preparation did not show a substantial effect on primary stability tested under dynamic compression-shear test conditions (P=0.910). Bone preparation significantly enhances cement interdigitation. The application of a brush shows similar results compared with the application of pulsed lavage. Copyright © 2016 Elsevier B.V. All rights reserved.

  11. Effect of barrier perturbation on cutaneous penetration of salicylic acid in hairless rats: in vivo pharmacokinetics using microdialysis and non-invasive quantification of barrier function.

    PubMed

    Benfeldt, E; Serup, J

    1999-09-01

    The penetration of topically applied drugs is altered in diseased or barrier-damaged skin. We used microdialysis in the dermis to measure salicylic acid (SA) penetration in hairless rats following application to normal (unmodified) skin (n = 11) or skin with perturbed barrier function from (1) tape-stripping (n = 5), (2) sodium lauryl sulphate (SLS) 2% for 24 h (n = 3) or (3) delipidization by acetone (n = 4). Prior to the experiment, transepidermal water loss (TEWL) and erythema were measured. Two microdialysis probes were inserted into the dermis on the side of the trunk and 5% SA in ethanol was applied in a chamber overlying the probes. Microdialysis sampling was continued for 4 h, followed by measurements of probe depth by ultrasound scanning. SA was detectable in all samples and rapidly increasing up to 130 min. Microdialysates collected between 80 and 200 min showed mean SA concentrations of 3 microg/ml in unmodified and acetone-treated skin, whereas mean SA concentrations were 280 microg/ml in SLS-pretreated skin and 530 microg/ml in tape-stripped skin (P < 0.001). The penetration of SA correlated with barrier perturbation measured by TEWL (P < 0.001) and erythema (P < 0.001). A correlation between dermal probe depth and SA concentration was found in unmodified skin (P = 0.04). Microdialysis sampling in anatomical regions remote from the dosed site excluded the possibility that SA levels measured were due to systemic absorption. Microdialysis sampling of cutaneous penetration was highly reproducible. Impaired barrier function, caused by irritant dermatitis or tape stripping, resulted in an 80- to 170-fold increase in the drug level in the dermis. This dramatic increase in drug penetration could be relevant to humans, in particular to topical treatment of skin diseases and to occupational toxicology.

  12. Direct S -matrix calculation for diffractive structures and metasurfaces

    NASA Astrophysics Data System (ADS)

    Shcherbakov, Alexey A.; Stebunov, Yury V.; Baidin, Denis F.; Kämpfe, Thomas; Jourlin, Yves

    2018-06-01

    The paper presents a derivation of analytical components of S matrices for arbitrary planar diffractive structures and metasurfaces in the Fourier domain. The attained general formulas for S -matrix components can be applied within both formulations in the Cartesian and curvilinear metric. A numerical method based on these results can benefit from all previous improvements of the Fourier domain methods. In addition, we provide expressions for S -matrix calculation in the case of periodically corrugated layers of two-dimensional materials, which are valid for arbitrary corrugation depth-to-period ratios. As an example, the derived equations are used to simulate resonant grating excitation of graphene plasmons and the impact of a silica interlayer on corresponding reflection curves.

  13. Transient liquid phase bonding of titanium-, iron- and nickel-based alloys

    NASA Astrophysics Data System (ADS)

    Rahman, A. H. M. Esfakur

    The operating temperature of land-based gas turbines and jet engines are ever-increasing to increase the efficiency, decrease the emissions and minimize the cost. Within the engines, complex-shaped parts experience extreme temperature, fatigue and corrosion conditions. Ti-based, Ni-based and Fe-based alloys are commonly used in gas turbines and jet engines depending on the temperatures of different sections. Although those alloys have superior mechanical, high temperature and corrosion properties, severe operating conditions cause fast degradation and failure of the components. Repair of these components could reduce lifecycle costs. Unfortunately, conventional fusion welding is not very attractive, because Ti reacts very easily with oxygen and nitrogen at high temperatures, Ni-based superalloys show heat affected zone (HAZ) cracking, and stainless steels show intergranular corrosion and knife-line attack. On the other hand, transient liquid phase (TLP) bonding method has been considered as preferred joining method for those types of alloys. During the initial phase of the current work commercially pure Ti, Fe and Ni were diffusion bonded using commercially available interlayer materials. Commercially pure Ti (Ti-grade 2) has been diffusion bonded using silver and copper interlayers and without any interlayer. With a silver (Ag) interlayer, different intermetallics (AgTi, AgTi2) appeared in the joint centerline microstructure. While with a Cu interlayer eutectic mixtures and Ti-Cu solid solutions appeared in the joint centerline. The maximum tensile strengths achieved were 160 MPa, 502 MPa, and 382 MPa when Ag, Cu and no interlayers were used, respectively. Commercially pure Fe (cp-Fe) was diffusion bonded using Cu (25 m) and Au-12Ge eutectic interlayer (100 microm). Cu diffused predominantly along austenite grain boundaries in all bonding conditions. Residual interlayers appeared at lower bonding temperature and time, however, voids were observed in the joint centerline at higher joining temperature and time. Dispersed Au-rich particles were observed in the base metal near interface. The highest ultimate tensile strengths obtained for the bonded Fe were 291+/-2 MPa using a Cu interlayer at 1030°C for 10 h and 315+/-4 MPa using a Au-12Ge interlayer at 950°C for 15 h. Commercially pure Ni (cp-Ni) was diffusion bonded using a Al, Au-12Ge or Cu interlayer. The formation of intermetallics could not be avoided when Al interlayer was used. Even though no intermetallics were obtained with Au-12Ge or Cu interlayer, appreciable strength of the joint was not found. Next, the simple bonding systems were modeled numerically. It is hoped that the simple models can be extended for higher order alloys. The modeling of TLP joint means to come up with a mathematical model which can predict the concentration profiles of diffusing species. The concentration dependence of diffusivity in a multi-component diffusion system makes it complicated to predict the concentration profiles of diffusing species. The so-called chemical diffusivity can be expressed as a function of thermodynamic and kinetic data. DICTRA software can calculate the concentration profiles using appropriate mobility and thermodynamic data. It can also optimize the diffusivity data using experimental diffusivity data. Then the optimized diffusivity data is stored as mobility data which is a linear function of temperature. In this work, diffusion bonding of commercially pure Ni using Cu interlayers is reported. The mobility parameters of Ni-Cu alloy binary systems were optimized using DICTRA/Thermocalc software from the available self-, tracer and chemical diffusion coefficients. The optimized mobility parameters were used to simulate concentration profiles of Ni-Cu diffusion joints using DICTRA/Thermocalc software. The calculated and experimental concentration profiles agreed well at 1100 °C. This method could not be extended for higher order alloys because of the lack of appropriate thermodynamic and kinetic database. In the third phase industrially important alloys such as SS 321, Inconel 718 and Ti-6Al-4V were diffusion bonded. Diffusion bonded SS 321 with Au-12Ge interlayer provided the best microstructure when bonded in either vacuum or argon at 1050°C for 20 h and cooled in air. The maximum strength obtained of the joint was 387+/-4 MPa bonded in vacuum at 1050°C for 20 h and cooled in air. The microstructure of joint centerline of diffusion bonded Inconel 718 using Au-12Ge interlayer at 1050°C for 15 h and cooled in air consisted of residual interlayer (1.3-2.5 microm). The residual interlayer was disappeared by increasing the bonding time by 5 h, however, pores appeared in the joint centerline. As a result, the strength obtained for bonded Inconel 718 was much lower than that of the base alloy. The joint centerline microstructure of bonded Ti-6Al-4V using Cu interlayer was free of intermetallics and solid solution of Cu and base alloy. The strength of the joint is yet to be determined.

  14. Transdermal delivery of biomacromolecules using lipid-like nanoparticles

    NASA Astrophysics Data System (ADS)

    Bello, Evelyn A.

    The transdermal delivery of biomacromolecules, including proteins and nucleic acids, is challenging, owing to their large size and the penetration-resistant nature of the stratum corneum. Thus, an urgent need exists for the development of transdermal delivery methodologies. This research focuses on the use of cationic lipid-like nanoparticles (lipidoids) for the transdermal delivery of proteins, and establishes an in vitro model for the study. The lipidoids used were first combinatorially designed and synthesized; afterwards, they were employed for protein encapsulation in a vesicular system. A skin penetration study demonstrated that lipidoids enhance penetration depth in a pig skin model, overcoming the barrier that the stratum corneum presents. This research has successfully identified active lipidoids capable of efficiently penetrating the skin; therefore, loading proteins into lipidoid nanoparticles will facilitate the transdermal delivery of proteins. Membrane diffusion experiments were used to confirm the results. This research has confirmed that lipidoids are a suitable material for transdermal protein delivery enhancement.

  15. Benchmarking the SPHINX and CTH shock physics codes for three problems in ballistics

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Wilson, L.T.; Hertel, E.; Schwalbe, L.

    1998-02-01

    The CTH Eulerian hydrocode, and the SPHINX smooth particle hydrodynamics (SPH) code were used to model a shock tube, two long rod penetrations into semi-infinite steel targets, and a long rod penetration into a spaced plate array. The results were then compared to experimental data. Both SPHINX and CTH modeled the one-dimensional shock tube problem well. Both codes did a reasonable job in modeling the outcome of the axisymmetric rod impact problem. Neither code correctly reproduced the depth of penetration in both experiments. In the 3-D problem, both codes reasonably replicated the penetration of the rod through the first plate.more » After this, however, the predictions of both codes began to diverge from the results seen in the experiment. In terms of computer resources, the run times are problem dependent, and are discussed in the text.« less

  16. Asphalt-Rubber SAMI (Stress-Absorbing Membrane Interlayers) Field Evaluation.

    DTIC Science & Technology

    1986-04-01

    revealed that there was promise in using the material as an interlayer to prevent the reflection of cracks from an old pavement to a new asphalt -concrete...reflection cracking , and (2) that asphalt - rubber interlayers should be investigated in conjunction with conventional asphalt -concrete overlays. An... Asphalt -rubber samples were taken and tested and construction activities were documented. The performance has been monitored by conducting crack

  17. Radiofrequency penetration and absorption in the human body: limitations to high-field whole-body nuclear magnetic resonance imaging.

    PubMed

    Röschmann, P

    1987-01-01

    This study presents experimental results about the effective depth of penetration and about the radiofrequency (rf) power absorption in humans as a function of frequency. The frequency range investigated covers 10 up to 220 MHz. For the main part, the results were derived from bench measurements of the quality factor Q, and of the resonance frequency shift due to the loading of the coil. Different types of head-, body-, and surface coils were investigated loaded with volunteers or metallic phantoms. For spin-echo imaging at 2 T (85 MHz), the local specific absorption rate (SAR) was found to be approximately equal to 0.05 W/kg using a pi pulse of 1-ms duration and pulse repetition time TR = 1 s. Measurements of the quality factor Q as a function of frequency show that the SAR depends upon the frequency f according to approximately f2.15. The effective depth of rf penetration as derived drops from 17 cm at 85 MHz to 7 cm at 220 MHz. Head imaging with B1 penetrating from practically all sides into the object should be possible up to 220 MHz (5 T) with SAR values staying within the local limit of 2 W/kg as set by the FDA. Whole-body imaging of large subjects as well as surface coil imaging is depth limited above 100-MHz frequency. Perturbation methods are applied in order to separate the total rf power deposition in the patient into dielectric and magnetic contributions. The observed effects due to interactions of rf magnetic fields with biological tissue contradict predictions based on homogeneous tissue models. A refined tissue model with regions of high electrical conductivity, subdivided by quasi-insulating adipose layers, provides a rationale for a better understanding of the underlying processes. At frequencies below 100 MHz, the rf power deposition in patients is apparently more evenly distributed over the exposed body volume than currently assumed.

  18. The concept of a marine Free-fall CPT systems revisited

    NASA Astrophysics Data System (ADS)

    Kopf, A.; Stegmann, S.

    2005-12-01

    Cone Penetration Tests (CPT) are a widely used method for the geotechnical in situ characterisation of sediments in onshore settings. In the course of enhanced use of the continental shelf and slope by humans impact, the need for time- and cost-efficient solutions in the marine realm is emerging. In order to avoid the challenges of lowering heavy gear to the seafloor for the penetration tests, free drop devices have been developed since the 1970s, however, the use of the majority of them was discontinued owing to technical difficulties in measurement and data interpretation caused by the impact. Based on those experiences, two different free-fall CPT lances were designed for the in situ measurement of strength (tip resistance, sleeve friction), pore pressure and temperature. In addition, deceleration and tilt are monitored for vertical profiling of the penetrated sediment column. Both CPT systems rely on an industry 15 cm2 piezocone with the sensors at the tip and a pressure housing containing a microprocessor at the top. The lightweight (40-100 kg), shallow water (200 m depth) lance works completely autonomous with a volatile memory and battery package, and can be deployed from any platform, even without a winch. The sturdier, deeper water (2500 m depth) system uses both power and telemetry for data transmission from the research vessel. The length and weight of either system can be varied according to the sediment stiffness and hence allow variable penetration depth (usually less than 5 m). Initial use of the CPT systems attests their efficiency and reliability in the measurement of sediment physical properties. While most of the data are collected within the first seconds of the CPT experiments, long term (pore pressure dissipation tests have also been successfully carried out for durations in excess of 6 hours. In a variety of estuarine and marine settings, our studies served objectives such as the assessment of slope stability, navigability of harbours/estuaries, consultancy for cable laying and trenching, or ground-truthing of geophysical data.

  19. Histological Validity and Clinical Evidence for Use of Fractional Lasers for Acne Scars

    PubMed Central

    Sardana, Kabir; Garg, Vijay K; Arora, Pooja; Khurana, Nita

    2012-01-01

    Though fractional lasers are widely used for acne scars, very little clinical or histological data based on the objective clinical assessment or the depth of penetration of lasers on in vivo facial tissue are available. The depth probably is the most important aspect that predicts the improvement in acne scars but the studies on histology have little uniformity in terms of substrate (tissue) used, processing and stains used. The variability of the laser setting (dose, pulses and density) makes comparison of the studies difficult. It is easier to compare the end results, histological depth and clinical results. We analysed all the published clinical and histological studies on fractional lasers in acne scars and analysed the data, both clinical and histological, by statistical software to decipher their significance. On statistical analysis, the depth was found to be variable with the 1550-nm lasers achieving a depth of 679 μm versus 10,600 nm (895 μm) and 2940 nm (837 μm) lasers. The mean depth of penetration (in μm) in relation to the energy used, in millijoules (mj), varies depending on the laser studied. This was statistically found to be 12.9–28.5 for Er:glass, 3–54.38 for Er:YAG and 6.28–53.66 for CO2. The subjective clinical improvement was a modest 46%. The lack of objective evaluation of clinical improvement and scar-specific assessment with the lack of appropriate in vivo studies is a case for combining conventional modalities like subcision, punch excision and needling with fractional lasers to achieve optimal results. PMID:23060702

  20. The Use of Ground Penetrating Radar and Electrical Resistivity Imaging for the Characterisation of Slope Movements in Expansive Marls

    NASA Astrophysics Data System (ADS)

    Rey, Isabel; Martínez, Julián; Cortada, Unai; Hildago, Mª Carmen

    2017-04-01

    Slope movements are one of the natural hazards that most affect linear projects, becoming an important waste of money and time for building companies. Thus, studies to identify the processes that provoke these movements, as well as to characterise the landslides are necessary. For this purpose, geophysical prospecting techniques as Ground Penetrating Radar (GPR) and Electrical Resistivity Imaging (ERI) could become useful. However, the effectiveness of these techniques in slope movement characterisation is affected by many factors, like soil humidity, grain size or failure plane depth. Therefore, studies that determine the usefulness of these techniques in different kind of soils and slope movements are required. In this study, GPR and ERI techniques efficiency for the analysis of slope movements in Upper Miocene expansive marls was evaluated. In particular, two landslides in an old regional road in the province of Jaen (Spain) were studied. A total of 53 GPR profiles were made, 31 with a 250 MHz frequency antenna and 22 with an 800 MHz frequency antenna. Marl facies rapidly attenuated the signal of the electromagnetic waves, which means that this technique only provided information of the first two meters of the subsoil. In spite of this low depth of penetration, it is necessary to point out the precision and detail undertaken. Thus, both GPR antennas gave information of the thicknesses and quality-continuity of the different soil layers. In addition, several restoration phases of the linear work were detected. Therefore, this technique was useful to detect the current state and history of the structure, even though it could not detect the shear surface of the slope movement. On the other hand, two profiles of electrical tomography were made, one in each studied sector. The profiles were configured with a total length of 189 m, with 64 electrodes and a spacing of 3 m. This allowed investigating up to 35 m depth. This penetration capability enabled to detect the depth of the shear surfaces and therefore the minimum depth at which the possible piles should be placed in the design of the restoration structures. Thus, this method was more effective than the GPR for the detection of slope surfaces in uniform expansive marls. Nevertheless, the GPR was efficient for the analysis of the previous restoration phases, which was helpful to determine any relation between them and the causes that provoked the slope movements.

  1. Exploitation of sub-micron cavitation nuclei to enhance ultrasound-mediated transdermal transport and penetration of vaccines.

    PubMed

    Bhatnagar, Sunali; Kwan, James J; Shah, Apurva R; Coussios, Constantin-C; Carlisle, Robert C

    2016-09-28

    Inertial cavitation mediated by ultrasound has been previously shown to enable skin permeabilisation for transdermal drug and vaccine delivery, by sequentially applying the ultrasound then the therapeutic in liquid form on the skin surface. Using a novel hydrogel dosage form, we demonstrate that the use of sub-micron gas-stabilising polymeric nanoparticles (nanocups) to sustain and promote cavitation activity during simultaneous application of both drug and vaccine results in a significant enhancement of both the dose and penetration of a model vaccine, Ovalbumin (OVA), to depths of 500μm into porcine skin. The nanocups themselves exceeded the penetration depth of the vaccine (up to 700μm) due to their small size and capacity to 'self-propel'. In vivo murine studies indicated that nanocup-assisted ultrasound transdermal vaccination achieved significantly (p<0.05) higher delivery doses without visible skin damage compared to the use of a chemical penetration enhancer. Transdermal OVA doses of up to 1μg were achieved in a single 90-second treatment, which was sufficient to trigger an antigen-specific immune response. Furthermore, ultrasound-assisted vaccine delivery in the presence of nanocups demonstrated substantially higher specific anti-OVA IgG antibody levels compared to other transdermal methods. Further optimisation can lead to a viable, safe and non-invasive delivery platform for vaccines with potential use in a primary care setting or personalized self-vaccination at home. Copyright © 2016 The Authors. Published by Elsevier B.V. All rights reserved.

  2. Origins of interlayer formation and misfit dislocation displacement in the vicinity of InAs/GaAs quantum dots

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Huang, S.; Kim, S. J.; Pan, X. Q.

    We have examined the origins of interlayer formation and misfit dislocation (MD) displacement in the vicinity of InAs/GaAs quantum dots (QDs). For QDs formed by the Stranski-Krastanov mode, regularly spaced MDs nucleate at the interface between the QD and the GaAs buffer layer. In the droplet epitaxy case, both In island formation and In-induced “nano-drilling” of the GaAs buffer layer are observed during In deposition. Upon annealing under As flux, the In islands are converted to InAs QDs, with an InGaAs interlayer at the QD/buffer interface. Meanwhile, MDs nucleate at the QD/interlayer interface.

  3. Observation of interlayer excitons in MoSe2 single crystals

    NASA Astrophysics Data System (ADS)

    Horng, Jason; Stroucken, Tineke; Zhang, Long; Paik, Eunice Y.; Deng, Hui; Koch, Stephan W.

    2018-06-01

    Interlayer excitons with direct optical transitions are observed coexisting with intralayer excitons in the same K valleys in bilayer, few-layer, and bulk MoSe2 single crystals by confocal reflection contrast spectroscopy. Quantitative analysis using the Dirac-Bloch equations provides unambiguous state assignment of all the measured resonances. The interlayer excitons in bilayer MoSe2 have a large binding energy of 153 meV and a narrow linewidth of 20 meV. Their spectral weight is comparable to the commonly studied higher-order intralayer excitons. At the same time, the interlayer excitons are characterized by distinct transition energies and permanent dipole moments, providing a promising high temperature and optically accessible platform for dipolar exciton physics.

  4. Multilayer Disk Reduced Interlayer Crosstalk with Wide Disk-Fabrication Margin

    NASA Astrophysics Data System (ADS)

    Hirotsune, Akemi; Miyauchi, Yasushi; Endo, Nobumasa; Onuma, Tsuyoshi; Anzai, Yumiko; Kurokawa, Takahiro; Ushiyama, Junko; Shintani, Toshimichi; Sugiyama, Toshinori; Miyamoto, Harukazu

    2008-07-01

    To reduce interlayer crosstalk caused by the ghost spot which appears in a multilayer optical disk with more than three information layers, a multilayer disk structure which reduces interlayer crosstalk with a wide disk-fabrication margin was proposed in which the backward reflectivity of the information layers is sufficiently low. It was confirmed that the interlayer crosstalk caused by the ghost spot was reduced to less than the crosstalk from the adjacent layer by controlling backward reflectivity. The wide disk-fabrication margin of the proposed disk structure was indicated by experimentally confirming that the tolerance of the maximum deviation of the spacer-layer thickness is four times larger than that in the previous multilayer disk.

  5. Influence of a MoOx interlayer on the open-circuit voltage in organic photovoltaic cells

    NASA Astrophysics Data System (ADS)

    Zou, Yunlong; Holmes, Russell J.

    2013-07-01

    Metal-oxides have been used as interlayers at the anode-organic interface in organic photovoltaic cells (OPVs) to increase the open-circuit voltage (VOC). We examine the role of MoOx in determining the maximum VOC in a planar heterojunction OPV and find that the interlayer strongly affects the temperature dependence of VOC. Boron subphthalocyanine chloride (SubPc)-C60 OPVs that contain no interlayer show a maximum VOC of 1.2 V at low temperature, while those with MoOx show no saturation, reaching VOC > 1.4 V. We propose that the MoOx-SubPc interface forms a Schottky junction that provides an additional contribution to VOC at low temperature.

  6. Investigation of concrete sealer products to extend concrete pavement life : phase 1.

    DOT National Transportation Integrated Search

    2011-12-01

    Five surface applied concrete sealer treatments were evaluated in the laboratory for water vapor transmission, saltwater absorption, alkali resistance, depth of penetration, UV exposure and cyclic saltwater ponding, chloride content, and freeze-thaw ...

  7. Selective reflection by deteriorated phase accumulation in Fabry-Perot cavity with aperiodic metallic nanomesh entry windows

    NASA Astrophysics Data System (ADS)

    Sun, Tianyi; Guo, Chuanfei; Kempa, Krzysztof; Ren, Zhifeng

    2014-03-01

    A Fabry-Perot reflection filter, consisting of semi-transparent metal and dielectric layers on opaque metals, is featured by selective absorption determined by the phase difference of waves from the two interfaces. In such systems, semi-transparency is usually realized by layers of reflective metals thinner than the penetration depth of the light. Here we present a filter cavity with entry windows not made of traditional thin layers, but of aperiodic metallic random nanomeshes thicker than the penetration depth, fabricated by grain boundary lithography. It is shown that due to the deteriorated phase caused by the interface between the random nanomesh and the dielectric layer, the width and location of the resonances can be tuned by metallic coverage. Further experiments show that this phenomenon can be used in designing aperiodic plasmonic metamaterial structures for visible and infrared applications.

  8. Monitoring of tissue modification with optical coherence tomography

    NASA Astrophysics Data System (ADS)

    Zhang, Wei; Luo, Qingming; Yao, Lei; Cheng, Haiying; Zeng, Shaoqun

    2002-04-01

    An experimental monitoring of tissue modification of in vitro and in vivo rabbit dura mater with administration of osmotical agents, 40% glucose solution and glycerol, using optical coherence tomography was presented. The preliminary results of experimental study of influence of osmotical liquids (glucose solutions, glycerol) of rabbit dura mater were reported. The significant decreasing of the light from surface and increasing of the light from the deep of dura mater under action of osmotical solutions and the increasing of OCT imaging depth were demonstrated. Experiments showed that administration of osmolytes to dura mater allowed for effective and temporary control of its optical characteristics, which made dura mater more transparent, increased the ability of light penetrating the tissue, and consequently improved the optical imaging depth. It is a significant study, which can improve penetration of optical imaging of cerebral function and acquire more information of the deep brain tissue.

  9. Relationships between wintering waterbirds and invertebrates, sediments and hydrology of coastal marsh ponds

    USGS Publications Warehouse

    Bolduc, F.; Afton, A.D.

    2004-01-01

    We studied relationships among sediment variables (carbon content, C:N, hardness, oxygen penetration, silt-clay fraction), hydrologic variables (dissolved oxygen, salinity, temperature, transparency, water depth), sizes and biomass of common invertebrate classes, and densities of 15 common waterbird species in ponds of impounded freshwater, oligohaline, mesohaline, and unimpounded mesohaline marshes during winters 1997-98 to 1999-2000 on Rockefeller State Wildlife Refuge, Louisiana, USA. Canonical correspondence analysis and forward selection was used to analyze the above variables. Water depth and oxygen penetration were the variables that best segregated habitat characteristics that resulted in maximum densities of common waterbird species. Most common waterbird species were associated with specific marsh types, except Green-winged Teal (Anas crecca) and Northern Shoveler (Anas clypeata). We concluded that hydrologic manipulation of marsh ponds is the best way to manage habitats for these birds, if the hydrology can be controlled adequately.

  10. Models for selecting GMA Welding Parameters for Improving Mechanical Properties of Weld Joints

    NASA Astrophysics Data System (ADS)

    Srinivasa Rao, P.; Ramachandran, Pragash; Jebaraj, S.

    2016-02-01

    During the process of Gas Metal Arc (GMAW) welding, the weld joints mechanical properties are influenced by the welding parameters such as welding current and arc voltage. These parameters directly will influence the quality of the weld in terms of mechanical properties. Even small variation in any of the cited parameters may have an important effect on depth of penetration and on joint strength. In this study, S45C Constructional Steel is taken as the base metal to be tested using the parameters wire feed rate, voltage and type of shielding gas. Physical properties considered in the present study are tensile strength and hardness. The testing of weld specimen is carried out as per ASTM Standards. Mathematical models to predict the tensile strength and depth of penetration of weld joint have been developed by regression analysis using the experimental results.

  11. In-plane magnetic penetration depth of superconducting CaKFe4As4

    NASA Astrophysics Data System (ADS)

    Khasanov, Rustem; Meier, William R.; Wu, Yun; Mou, Daixiang; Bud'ko, Sergey L.; Eremin, Ilya; Luetkens, Hubertus; Kaminski, Adam; Canfield, Paul C.; Amato, Alex

    2018-04-01

    The temperature dependence of the in-plane magnetic penetration depth (λa b) in an extensively characterized sample of superconducting CaKFe4As4(Tc≃35 K ) was investigated using muon-spin rotation (μ SR ). A comparison of λab -2(T ) measured by μ SR with the one inferred from angle-resolved photoemission spectroscopy (ARPES) data confirms the presence of multiple gaps at the Fermi level. An agreement between μ SR and ARPES requires the presence of additional bands, which are not resolved by ARPES experiments. These bands are characterized by small superconducting gaps with an average zero-temperature value of Δ0=2.4 (2 ) meV . Our data suggest that in CaKFe4As4 the s± order parameter symmetry acquires a more sophisticated form by allowing a sign change not only between electron and hole pockets, but also within pockets of similar type.

  12. Giant optical field enhancement in multi-dielectric stacks by photon scanning tunneling microscopy

    NASA Astrophysics Data System (ADS)

    Ndiaye, C.; Zerrad, M.; Lereu, A. L.; Roche, R.; Dumas, Ph.; Lemarchand, F.; Amra, C.

    2013-09-01

    Dielectric optical thin films, as opposed to metallic, have been very sparsely explored as good candidates for absorption-based optical field enhancement. In such materials, the low imaginary part of the refractive index implies that absorption processes are usually not predominant. This leads to dielectric-based optical resonances mainly via waveguiding modes. We show here that when properly designed, a multi-layered dielectric thin films stack can give rise to optical resonances linked to total absorption. We report here, on such dielectric stack designed to possess a theoretical optical field enhancement above 1000. Using photon scanning tunneling microscopy, we experimentally evaluate the resulting field enhancement of the stack as well as the associated penetration depth. We thus demonstrate the capability of multi-dielectric stacks in generating giant optical field with tunable penetration depth (down to few dozens of nm).

  13. Water penetration study

    NASA Technical Reports Server (NTRS)

    Lockwood, H. E.

    1973-01-01

    Nine film-filter combinations have been tested for effectiveness in recording water subsurface detail when exposed from an aerial platform over a typical water body. An experimental 2-layer positive color film, a 2-layer (minus blue layer) film, a normal 3-layer color film, a panchromatic black-and-white film, and an infrared film with selected filters were tested. Results have been tabulated to show the relative capability of each film-filter combination for: (1) image contrast in shallow water (0 to 5 feet); (2) image contrast at medium depth (5 to 10 feet); (3) image contrast in deep water (10 feet plus); (4) water penetration; maximum depth where detail was discriminated; (5) image color (the spectral range of the image); (6) vegetation visible above a water background; (7) specular reflections visible from the water surface; and (8) visual compatibility; ease of discriminating image detail. Recommendations for future recording over water bodies are included.

  14. Study of buildup factor of gamma ray photons in bismuth-ground granulated blast furnace slag concrete

    NASA Astrophysics Data System (ADS)

    Kumar, Sandeep; Kaur, Ramanpreet; Singh, Tejbir; Singh, Sukhpal

    2018-05-01

    The gamma ray buildup factors of Bismuth-Ground granulated blast furnace slag (Bi-GGBFS) concrete in the composition of (0.6 cement + x Bi2O3+ (0.4-x) GGBFS, x = 0.05, 0.10, 0.15, 0.20 and 0.25) has been calculated by using Geometrical Progression formula in the energy region of 0.015-15 MeV as well as up to a penetration depth of 40 mean free paths, and have been studied as a function of incident photon energy. From the obtained results it is found that the fixed penetration depth values of buildup factor are very large in the medium energy region and in the low and high energy regions are low. The investigation was carried out to explore the advantages of the Bismuth-Ground granulated blast furnace slag (Bi-GGBFS) concrete in different radiation shielding applications.

  15. Spatially resolved penetration depth measurements and vortex manipulation in the ferromagnetic superconductor ErNi 2 B 2 C

    DOE PAGES

    Wulferding, Dirk; Yang, Ilkyu; Yang, Jinho; ...

    2015-07-31

    We present a local probe study of the magnetic superconductor ErNi 2B 2C, using magnetic force microscopy at sub-Kelvin temperatures. ErNi 2B 2C is an ideal system to explore the effects of concomitant superconductivity and ferromagnetism. At 500 mK, far below the transition to a weakly ferromagnetic state, we directly observe a structured magnetic background on the micrometer scale. We determine spatially resolved absolute values of the magnetic penetration depth λ and study its temperature dependence as the system undergoes magnetic phase transitions from paramagnetic to antiferromagnetic, and to weak ferromagnetic, all within the superconducting regime. We estimate the absolutemore » pinning force of Abrikosov vortices, which shows a position dependence and temperature dependence as well, and discuss the possibility of the purported spontaneous vortex formation.« less

  16. Cellular imaging of deep organ using two-photon Bessel light-sheet nonlinear structured illumination microscopy

    PubMed Central

    Zhao, Ming; Zhang, Han; Li, Yu; Ashok, Amit; Liang, Rongguang; Zhou, Weibin; Peng, Leilei

    2014-01-01

    In vivo fluorescent cellular imaging of deep internal organs is highly challenging, because the excitation needs to penetrate through strong scattering tissue and the emission signal is degraded significantly by photon diffusion induced by tissue-scattering. We report that by combining two-photon Bessel light-sheet microscopy with nonlinear structured illumination microscopy (SIM), live samples up to 600 microns wide can be imaged by light-sheet microscopy with 500 microns penetration depth, and diffused background in deep tissue light-sheet imaging can be reduced to obtain clear images at cellular resolution in depth beyond 200 microns. We demonstrate in vivo two-color imaging of pronephric glomeruli and vasculature of zebrafish kidney, whose cellular structures located at the center of the fish body are revealed in high clarity by two-color two-photon Bessel light-sheet SIM. PMID:24876996

  17. Archimedes' law explains penetration of solids into granular media.

    PubMed

    Kang, Wenting; Feng, Yajie; Liu, Caishan; Blumenfeld, Raphael

    2018-03-16

    Understanding the response of granular matter to intrusion of solid objects is key to modelling many aspects of behaviour of granular matter, including plastic flow. Here we report a general model for such a quasistatic process. Using a range of experiments, we first show that the relation between the penetration depth and the force resisting it, transiently nonlinear and then linear, is scalable to a universal form. We show that the gradient of the steady-state part, K ϕ , depends only on the medium's internal friction angle, ϕ, and that it is nonlinear in μ = tan ϕ, in contrast to an existing conjecture. We further show that the intrusion of any convex solid shape satisfies a modified Archimedes' law and use this to: relate the zero-depth intercept of the linear part to K ϕ and the intruder's cross-section; explain the curve's nonlinear part in terms of the stagnant zone's development.

  18. Observation of van Hove Singularities in Twisted Silicene Multilayers

    PubMed Central

    2016-01-01

    Interlayer interactions perturb the electronic structure of two-dimensional materials and lead to new physical phenomena, such as van Hove singularities and Hofstadter’s butterfly pattern. Silicene, the recently discovered two-dimensional form of silicon, is quite unique, in that silicon atoms adopt competing sp2 and sp3 hybridization states leading to a low-buckled structure promising relatively strong interlayer interaction. In multilayer silicene, the stacking order provides an important yet rarely explored degree of freedom for tuning its electronic structures through manipulating interlayer coupling. Here, we report the emergence of van Hove singularities in the multilayer silicene created by an interlayer rotation. We demonstrate that even a large-angle rotation (>20°) between stacked silicene layers can generate a Moiré pattern and van Hove singularities due to the strong interlayer coupling in multilayer silicene. Our study suggests an intriguing method for expanding the tunability of the electronic structure for electronic applications in this two-dimensional material. PMID:27610412

  19. Antiferromagnetic Interlayer Exchange Coupling in All-Semiconducting EuS/PbS/EuS Trilayers

    NASA Technical Reports Server (NTRS)

    Smits, C. J. P.; Filip, A. T.; Swagten, H. J. M.; Koopmans, B.; deJonge, W. J. M.; Chernyshova, M.; Kowalczyk, L.; Grasza, K.; Szczerbakow, A.; Story, T.

    2003-01-01

    A comprehensive experimental study on the antiferromagnetic interlayer exchange coupling in high quality epitaxial all-semiconducting EuSPbSEuS trilayers is reported. The influence of substrates, the thickness of the non-magnetic PbS spacer layer, and of temperature, was investigated by means of SQUID magnetometry. In trilayers with a PbS thickness between 4 and 12 deg A the low temperature hysteresis loops showed the signature of antiferromagnetic coupling. The value of the interlayer exchange coupling energy was determined by simulating the data with a modified Stoner model, including Zeeman, anisotropy, and exchange coupling energies. An important observation was of a strong dependence of the interlayer exchange coupling energy on temperature, consistent with a power law dependence of the exchange coupling constant on the saturation magnetization of the EuS layers. While no theoretical description is readily available, we conjecture that the observed behavior is due to a dependence of the interlayer exchange coupling energy on the exchange splitting of the EuS conduction band.

  20. Electrochemical preparation of carbon films with a Mo2C interlayer in LiCl-NaCl-Na2CO3 melts

    NASA Astrophysics Data System (ADS)

    Ge, Jianbang; Wang, Shuai; Zhang, Feng; Zhang, Long; Jiao, Handong; Zhu, Hongmin; Jiao, Shuqiang

    2015-08-01

    The electrodeposition of carbon films with a Mo2C interlayer was investigated in LiCl-NaCl-Na2CO3 melts at 900 °C. Cyclic voltammetry was applied to study the electrochemical reaction mechanism on Mo and Pt electrodes, indicating that, two reduction reactions including carbon deposition and carbon monoxide evolution, may take place on the two electrodes simultaneously during the cathodic sweep. Carbon films with a continuous Mo2C interlayer were prepared by constant voltage electrolysis, showing a good adhesion between Mo substrate and carbon films. The carbon films with a Mo2C interlayer were characterized using X-ray diffraction measurement, Raman spectroscopy, scanning electron microscopy and transmission electron microscopy. The results reveal that carbon materials deposited on the electrodes are mainly composed of graphite and carbon diffusion in Mo (or Mo2C) leads to the formation and growth of Mo2C interlayer.

  1. Toward Increasing Micropore Volume between Hybrid Layered Perovskites with Silsesquioxane Interlayers.

    PubMed

    Kataoka, Sho; Kamimura, Yoshihiro; Endo, Akira

    2018-04-10

    Hybrid organic-inorganic layered perovskites are typically nonporous solids. However, the incorporation of silsesquioxanes with a cubic cage structure as interlayer materials creates micropores between the perovskite layers. In this study, we increase in the micropore volume in layered perovskites by replacing a portion of the silsesquioxane interlayers with organic amines. In the proposed method, approximately 20% of the silsesquioxane interlayers can be replaced without changing the layer distance owing to the size of the silsesquioxane. When small amines (e.g., ethylamine) are used in this manner, the micropore volume of the obtained hybrid layered perovskites increases by as much as 44%; when large amines (e.g., phenethylamine) are used, their micropore volume decreases by as much as 43%. Through the variation of amine fraction, the micropore volume can be adjusted in the range. Finally, the magnetic moment measurements reveal that the layered perovskites with mixed interlayers exhibit ferromagnetic ordering at temperature below 20 K, thus indicating that the obtained perovskites maintain their functions as layered perovskites.

  2. Effects of GaN interlayer on the transport properties of lattice-matched AlInN/AlN/GaN heterostructures

    DOE Office of Scientific and Technical Information (OSTI.GOV)

    Wu, F.; Gao, K. H., E-mail: khgao@tju.edu.cn; Li, Z. Q.

    2015-04-21

    We study the effects of GaN interlayer on the transport properties of two-dimensional electron gases confined in lattice-matched AlInN/AlN/GaN heterostructures. It is found that the Hall mobility is evidently enhanced when an additional ultrathin GaN interlayer is introduced between AlInN and AlN layers. The enhancement of the Hall mobility is especially remarkable at low temperature. The high Hall mobility results in a low sheet resistance of 23 Ω/◻ at 2 K. Meanwhile, Shubnikov-de Haas oscillations (SdH) are also remarkably enhanced due to the existence of GaN interlayer. The enhancement of the SdH oscillations is related to the larger quantum mobility μ{sub q}more » owing to the suppression of the interface roughness, alloy disorder, and ionized impurity scatterings by the GaN interlayer.« less

  3. Observation of long-lived interlayer excitons in monolayer MoSe 2–WSe 2 heterostructures

    DOE PAGES

    Rivera, Pasqual; Schaibley, John R.; Jones, Aaron M.; ...

    2015-02-24

    Van der Waals bound heterostructures constructed with two-dimensional materials, such as graphene, boron nitride and transition metal dichalcogenides, have sparked wide interest in both device physics and technologies at the two-dimensional limit. One highly coveted heterostructure is that of differing monolayer transition metal dichalcogenides with type-II band alignment, with bound electrons and holes localized in individual monolayers, that is, interlayer excitons. Here, we report the observation of interlayer excitons in monolayer MoSe 2–WSe 2 heterostructures by photoluminescence and photoluminescence excitation spectroscopy. The energy and luminescence intensity are highly tunable by an applied vertical gate voltage. Moreover, we measure an interlayermore » exciton lifetime of ~1.8 ns, an order of magnitude longer than intralayer excitons in monolayers. Ultimately, our work demonstrates optical pumping of interlayer electric polarization, which may provoke further exploration of interlayer exciton condensation, as well as new applications in two-dimensional lasers, light-emitting diodes and photovoltaic devices.« less

  4. Interlayer electron-phonon coupling in WSe2/hBN heterostructures

    NASA Astrophysics Data System (ADS)

    Jin, Chenhao; Kim, Jonghwan; Suh, Joonki; Shi, Zhiwen; Chen, Bin; Fan, Xi; Kam, Matthew; Watanabe, Kenji; Taniguchi, Takashi; Tongay, Sefaattin; Zettl, Alex; Wu, Junqiao; Wang, Feng

    2017-02-01

    Engineering layer-layer interactions provides a powerful way to realize novel and designable quantum phenomena in van der Waals heterostructures. Interlayer electron-electron interactions, for example, have enabled fascinating physics that is difficult to achieve in a single material, such as the Hofstadter's butterfly in graphene/boron nitride (hBN) heterostructures. In addition to electron-electron interactions, interlayer electron-phonon interactions allow for further control of the physical properties of van der Waals heterostructures. Here we report an interlayer electron-phonon interaction in WSe2/hBN heterostructures, where optically silent hBN phonons emerge in Raman spectra with strong intensities through resonant coupling to WSe2 electronic transitions. Excitation spectroscopy reveals the double-resonance nature of such enhancement, and identifies the two resonant states to be the A exciton transition of monolayer WSe2 and a new hybrid state present only in WSe2/hBN heterostructures. The observation of an interlayer electron-phonon interaction could open up new ways to engineer electrons and phonons for device applications.

  5. Photocarrier generation from interlayer charge-transfer transitions in WS2-graphene heterostructures

    PubMed Central

    Yuan, Long; Chung, Ting-Fung; Kuc, Agnieszka; Wan, Yan; Xu, Yang; Chen, Yong P.; Heine, Thomas; Huang, Libai

    2018-01-01

    Efficient interfacial carrier generation in van der Waals heterostructures is critical for their electronic and optoelectronic applications. We demonstrate broadband photocarrier generation in WS2-graphene heterostructures by imaging interlayer coupling–dependent charge generation using ultrafast transient absorption microscopy. Interlayer charge-transfer (CT) transitions and hot carrier injection from graphene allow carrier generation by excitation as low as 0.8 eV below the WS2 bandgap. The experimentally determined interlayer CT transition energies are consistent with those predicted from the first-principles band structure calculation. CT interactions also lead to additional carrier generation in the visible spectral range in the heterostructures compared to that in the single-layer WS2 alone. The lifetime of the charge-separated states is measured to be ~1 ps. These results suggest that interlayer interactions make graphene–two-dimensional semiconductor heterostructures very attractive for photovoltaic and photodetector applications because of the combined benefits of high carrier mobility and enhanced broadband photocarrier generation. PMID:29423439

  6. Microorganism penetration in dentinal tubules of instrumented and retreated root canal walls. In vitro SEM study.

    PubMed

    Al-Nazhan, Saad; Al-Sulaiman, Alaa; Al-Rasheed, Fellwa; Alnajjar, Fatimah; Al-Abdulwahab, Bander; Al-Badah, Abdulhakeem

    2014-11-01

    This in vitro study aimed to investigate the ability of Candida albicans (C. albicans) and Enterococcus faecalis (E. faecalis) to penetrate dentinal tubules of instrumented and retreated root canal surface of split human teeth. Sixty intact extracted human single-rooted teeth were divided into 4 groups, negative control, positive control without canal instrumentation, instrumented, and retreated. Root canals in the instrumented group were enlarged with endodontic instruments, while root canals in the retreated group were enlarged, filled, and then removed the canal filling materials. The teeth were split longitudinally after canal preparation in 3 groups except the negative control group. The teeth were inoculated with both microorganisms separately and in combination. Teeth specimens were examined by scanning electron microscopy (SEM), and the depth of penetration into the dentinal tubules was assessed using the SMILE view software (JEOL Ltd). Penetration of C. albicans and E. faecalis into the dentinal tubules was observed in all 3 groups, although penetration was partially restricted by dentin debris of tubules in the instrumented group and remnants of canal filling materials in the retreated group. In all 3 groups, E. faecalis penetrated deeper into the dentinal tubules by way of cell division than C. albicans which built colonies and penetrated by means of hyphae. Microorganisms can easily penetrate dentinal tubules of root canals with different appearance based on the microorganism size and status of dentinal tubules.

  7. Direct Laser Ice Penetrator for Exploring Icy Ocean Worlds: Design, Modeling and Test Results of a Proof-of-Concept Prototype

    NASA Astrophysics Data System (ADS)

    Hogan, B.; Stone, W.; Bramall, N. E.; Siegel, V.; Lelievre, S.; Rothhammer, B.; Richmond, K.; Flesher, C.

    2016-12-01

    Subsurface exploration of icy ocean worlds requires an efficient method of penetrating ice to significant depths under extreme environment conditions. Searching for extant life dictates descent to a depth which is habitable or where biomarkers can survive and allow detection. It's anticipated that several meters to 10s of meters of shielding is required to prevent cosmic background radiation and other energetic particles from destroying biomarker evidence. We have devised, developed and demonstrated an entirely novel ice penetrating technology utilizing laser light carried by an optical fiber tether and emitted from a probe's optical nose cone and radiated directly into the volume of ice preceding the penetrator. We have termed it a "Direct Laser Penetrator" or DLP. We present design details, modeling, and test data from preliminary proof-of-concept experiments conducted at Stone Aerospace with results exceeding expectations and achieving the fastest reported thermal probe descent rate to date (> 12 m / hr). DLP has critical benefits over conventional "hot point" melt probes, which must generate large temperature gradients to force heat by conduction through the nose cone, and layers of ice and water. Additionally, hot point melt probes tested under vacuum have shown extreme difficulty initiating penetration, as virtually no thermal contact exists between the probe nose and rough ice surface. The ice simply sublimates and any transferred heat is quickly dissipated due to the low power density and extreme cold. DLP requires NO thermal contact between the probe nose and the ice surface since the laser energy is radiated directly into the volume (vs. surface) of ice preceding the penetrator. A proposed key element of the DLP is the fiber optic tether, coupled with a dedicated sensor fiber, enables "optical access" to the subsurface environment by a lander's shared or DLP dedicated on-board instruments (Raman / Fluorescence / fiber / UV / VIS / NIR spectroscopy, etc). These sensors can search for extant life by detecting biomarkers as well as characterizing the radiation / light environment for subsurface habitability. The combination of a laser penetrator w/ integrated fiber coupled instruments could be an important tool for an icy ocean worlds lander. (Supported by NASA funded SAS projects VALKYRIE and SPINDLE)

  8. Carbon with Expanded and Well-Developed Graphene Planes Derived Directly from Condensed Lignin as a High-Performance Anode for Sodium-Ion Batteries.

    PubMed

    Yoon, Dohyeon; Hwang, Jieun; Chang, Wonyoung; Kim, Jaehoon

    2018-01-10

    In this study, we demonstrate that lignin, which constitutes 30-40 wt % of the terrestrial lignocellulosic biomass and is produced from second generation biofuel plants as a cheap byproduct, is an excellent precursor material for sodium-ion battery (NIB) anodes. Because it is rich in aromatic monomers that are highly cross-linked by ether and condensed bonds, the lignin material carbonized at 1300 °C (C-1300) in this study has small graphitic domains with well-developed graphene layers, a large interlayer spacing (0.403 nm), and a high micropore surface area (207.5 m 2 g -1 ). When tested as an anode in an NIB, C-1300 exhibited an initial Coulombic efficiency of 68% and a high reversible capacity of 297 mA h g -1 at 50 mA g -1 after 50 cycles. The high capacity of 199 mA h g -1 at less than 0.1 V with a flat voltage profile and an extremely low charge-discharge voltage hysteresis (<0.03 V) make C-1300 a promising energy-dense electrode material. In addition, C-1300 exhibited an excellent high-rate performance of 116 mA h g -1 at 2.5 A g -1 and showed stable cycling retention (0.2% capacity decay per cycle after 500 cycles). By comparing the properties of the lignin-derived carbon with oak sawdust-derived and sugar-derived carbons and a low-temperature carbonized sample (900 °C), the reasons for the excellent performance of C-1300 were determined to result from facilitated Na + -ion transport to the graphitic layer and the microporous regions that penetrate through the less defective and enlarged interlayer spacings.

  9. Green Rust: Structure, Redox Reaction Mechanisms, Transformation and Colloidal Behaviour

    NASA Astrophysics Data System (ADS)

    Stipp, S.; Skovbjerg, L.; Christiansen, B.; Hansson, E.; Utsunomiya, S.; Schild, D.; Geckeis, H.; Ewing, R.

    2006-05-01

    Green rust (GR) forms where pH is neutral to basic, iron concentration is high and oxidation potential provides a small amount of Fe(III). GR is best known from metallic iron corrosion but it has also been reported in soil. It typically forms nano-particles, so surface area is high. It has a layered structure and is reactive, adsorbing species on its surface, providing exchange of interlayer ions, and allowing reaction of redox active species. Corroding stainless-steel canisters in a concrete and steel radioactive waste repository would offer geochemical conditions for GR formation. We used surface-sensitive and high resolution techniques (atomic force microscopy, AFM, transmission electron microscopy, TEM, X-ray photoelectron spectroscopy, XPS) to supplement data from traditional methods (X-ray diffraction, XRD, and wet chemistry). The purpose was to refine structural and compositional parameters for green rust sulfate; to define trace component uptake mechanisms; and to assess potential mobility of GR colloids and thus, sorbed radionuclides. Green rust reduced dissolved Np(V), Cr(VI) and Se(VI), rapidly decreasing solution concentration. High resolution TEM and AFM images showed that chromate penetrates GR interlayers to a distance of about 100 nm from crystal edges. It reduces to Cr(III), blocking further movement and GR transforms topotactically to Cr- goethite, thus immobilising the contaminant in a phase significantly less soluble than pure goethite. Further oxidation results in dissolution of GR and growth of more Cr-goethite. In-situ AFM imaging showed that GR can nucleate and grow both in solution and on minerals typical of fractures in granite, i.e. graphite, muscovite, biotite, quartz and amorphous silica. Particles are more likely to stick to each other or to a substrate than to remain monodispersed.

  10. Inter-layer synchronization in non-identical multi-layer networks

    NASA Astrophysics Data System (ADS)

    Leyva, I.; Sevilla-Escoboza, R.; Sendiña-Nadal, I.; Gutiérrez, R.; Buldú, J. M.; Boccaletti, S.

    2017-04-01

    Inter-layer synchronization is a dynamical process occurring in multi-layer networks composed of identical nodes. This process emerges when all layers are synchronized, while nodes in each layer do not necessarily evolve in unison. So far, the study of such inter-layer synchronization has been restricted to the case in which all layers have an identical connectivity structure. When layers are not identical, the inter-layer synchronous state is no longer a stable solution of the system. Nevertheless, when layers differ in just a few links, an approximate treatment is still feasible, and allows one to gather information on whether and how the system may wander around an inter-layer synchronous configuration. We report the details of an approximate analytical treatment for a two-layer multiplex, which results in the introduction of an extra inertial term accounting for structural differences. Numerical validation of the predictions highlights the usefulness of our approach, especially for small or moderate topological differences in the intra-layer coupling. Moreover, we identify a non-trivial relationship connecting the betweenness centrality of the missing links and the intra-layer coupling strength. Finally, by the use of multiplexed layers of electronic circuits, we study the inter-layer synchronization as a function of the removed links.

  11. Mechanism of mechanically induced optoelectronic and spintronic phase transitions in 1D graphene spirals: insight into the role of interlayer coupling.

    PubMed

    Xu, Xiaodong; Liu, Bingyi; Zhao, Wenyu; Jiang, Yongyuan; Liu, Linhua; Li, Weiqi; Zhang, Guiling; Tian, Wei Quan

    2017-07-13

    Graphene spirals (GSs), an emerging carbonic nano-material with a Riemann surface, demonstrate extraordinary topological electronic signatures: interlayer coupling similar to van der Waals (vdW) heterojunctions and intralayer coupling within the spiral conformation. Based on the state-of-the-art first-principles technique, the electronic properties of the periphery-modified GSs with geometry deformation are explored under axial strain. For all GSs, there emerges a remarkable phase transition from metal to semiconductor, due to the attenuation of interlayer "σ-bonds" reducing the interlayer tunneling probability for carriers. Analogous to graphene, GSs consist of bipartite sublattices with carbonic sp 2 hybridization as well. Once the balance of the bipartite sublattices is lost, there will emerge intense edge (corner) states, contributed by the p z orbitals. In contrast to isolated graphene nanoflakes, GSs realize the continuous spin-polarized edge (corner) state coupling with 1D morphology. However, the spin-polarization is blocked by the robust interlayer "σ-bonds" so that the spintronic transition takes place until this interlayer coupling is broken. More intriguingly, an indirect-direct bandgap transition is observed, revealing excellent optical on-off features. Their tunable properties provide great potential for their application in optoelectronics, spintronics and chemical or biological sensors.

  12. Development of a Novel Ni-Fe-Cr-B-Si Interlayer Material for Transient Liquid Phase Bonding of Inconel 718

    NASA Astrophysics Data System (ADS)

    Tarai, U. K.; Robi, P. S.; Pal, Sukhomay

    2018-04-01

    A Ni-Cr-Fe-Si-B based interlayer material was developed by mechanical alloying (MA) process in a high-energy planetary ball mill. Equiaxed alloy powders of size 12 µm was obtained after milling for 50 hours. X-ray diffraction analysis of the milled powder revealed that milling of elemental powders initially resulted in microcrystalline alloy powder having face centered cubic structure, which on subsequent milling resulted in nano-crystallice alloy powder with a crystallite size of 3.2 nm. XRD analysis also reveals formation of metastable eutectic alloys resulting in lowering of the melting point of the interlayer material to 1025 °C. IN 718 superalloy samples were joined at 1050°C using the developed interlayer. A homogeneous joint was formed by the newly developed interlayer material. Three different zones were observed at the bond (i) isothermally solidified zone, (ii) diffusion affected zone and (iii) unaffected base metal. In the diffusion-affected zone, boron was present at the grain boundaries of Ni γ matrix in bulky metal borides form. The diffusion of boron from interlayer material into the base material was mechanism of isothermal solidification and bond formation in transient liquid phase bonding of IN 718.

  13. Revealing the preferred interlayer orientations and stackings of two-dimensional bilayer gallium selenide crystals

    DOE PAGES

    Li, Xufan; Basile Carrasco, Leonardo A.; Yoon, Mina; ...

    2015-01-21

    Characterizing and controlling the interlayer orientations and stacking order of bilayer two-dimensional (2D) crystals and van der Waals (vdW) heterostructure is crucial to optimize their electrical and optoelectronic properties. The four polymorphs of layered gallium selenide (GaSe) that result from different layer stacking provide an ideal platform to study the stacking configurations in bilayer 2D crystals. Here, through a controllable vapor-phase deposition method we selectively grow bilayer GaSe crystals and investigate their two preferred 0° or 60° interlayer rotations. The commensurate stacking configurations (AA' and AB-stacking) in as-grown 2D bilayer GaSe crystals are clearly observed at the atomic scale andmore » the Ga-terminated edge structure are identified for the first time by using atomic-resolution scanning transmission electron microscopy (STEM). Theoretical analysis of the interlayer coupling energetics vs. interlayer rotation angle reveals that the experimentally-observed orientations are energetically preferred among the bilayer GaSe crystal polytypes. Here, the combined experimental and theoretical characterization of the GaSe bilayers afforded by these growth studies provide a pathway to reveal the atomistic relationships in interlayer orientations responsible for the electronic and optical properties of bilayer 2D crystals and vdW heterostructures.« less

  14. Layer and doping tunable ferromagnetic order in two-dimensional Cr S2 layers

    NASA Astrophysics Data System (ADS)

    Wang, Cong; Zhou, Xieyu; Pan, Yuhao; Qiao, Jingsi; Kong, Xianghua; Kaun, Chao-Cheng; Ji, Wei

    2018-06-01

    Interlayer coupling is of vital importance for manipulating physical properties, e.g., electronic band gap, in two-dimensional materials. However, tuning magnetic properties in these materials is yet to be addressed. Here, we found the in-plane magnetic orders of Cr S2 mono and few layers are tunable between striped antiferromagnetic (sAFM) and ferromagnetic (FM) orders by manipulating charge transfer between Cr t2 g and eg orbitals. Such charge transfer is realizable through interlayer coupling, direct charge doping, or substituting S with Cl atoms. In particular, the transferred charge effectively reduces a portion of Cr4 + to Cr3 +, which, together with delocalized S p orbitals and their resulting direct S-S interlayer hopping, enhances the double-exchange mechanism favoring the FM rather than sAFM order. An exceptional interlayer spin-exchange parameter was revealed over -10 meV , an order of magnitude stronger than available results of interlayer magnetic coupling. It addition, the charge doping could tune Cr S2 between p - and n -doped magnetic semiconductors. Given these results, several prototype devices were proposed for manipulating magnetic orders using external electric fields or mechanical motion. These results manifest the role of interlayer coupling in modifying magnetic properties of layered materials and shed considerable light on manipulating magnetism in these materials.

  15. Molecular Modeling of the Binding Structures in the Interlayer Adsorption of a Tetracycline Antibiotic by Smectite Clays

    NASA Astrophysics Data System (ADS)

    Aristilde, L.

    2009-12-01

    A controlling factor in the fate of antibiotics in the environment is their sequestration in soil particles including clay minerals. Of special interest is the interlayer adsorption by smectite clays, which has been shown to influence both the bioavailability and persistence of antibiotics in the soil environment. However, the interlayer structures of the bound antibiotics, essential to an accurate understanding of the adsorption mechanisms, are not well understood. Molecular simulations of oxytetracycline (OTC) with a model montmorillonite (MONT) clay were performed to gain insights into these structures for tetracycline antibiotics. Monte Carlo simulations were used for explorations of the clay layer spacing required for the adsorption of the antibiotic under different hydration states of the clay interlayer; these preliminary results were validated with previous X-ray diffraction patterns obtained following sorption experiments of OTC with MONT. Molecular dynamics relaxation simulations were performed subsequently in order to obtain geometry-optimized structures of the binding conformations of the intercalated antibiotic in the model MONT layers. This study contributes to a mechanistic understanding of the factors controlling the interlayer adsorption of the tetracycline antibiotics by the expandable smectite clay minerals. Figure 1. Optimized Monte Carlo simulation cell of OTC in the interlayer of MONT: perspective side view (top) and bottom view (bottom).

  16. Influence of Ni Interlayer on Microstructure and Mechanical Properties of Mg/Al Bimetallic Castings

    NASA Astrophysics Data System (ADS)

    Liu, Ning; Liu, Canchun; Liang, Chunyong; Zhang, Yongguang

    2018-05-01

    Dissimilar joining of magnesium and aluminum using a compound casting process was investigated in the present work. For the first time, a Ni interlayer prepared by plasma spraying was inserted between the two base metals to improve the interfacial characteristics. Examination of the interfacial regions using scanning electron microscopy, energy-dispersive X-ray spectroscopy, electron probe microanalysis, and X-ray diffraction revealed the formation of a three-layered interface between Mg and Al without the interlayer. The thickness of the interface was approximately 600 μm when the casting was performed at 700 °C and increased with increasing casting temperature. However, with the addition of the Ni interlayer, the Al-Mg reaction was successfully prevented, and metallurgical bonding between the Ni interlayer and two base metals was achieved at a casting temperature of 700 °C. Upon increasing this temperature, Mg-Ni and Al-Ni intermetallics were generated at the separate interfaces. The shear strength of the Mg/Al bimetallic castings with the Ni interlayer was substantially improved compared with that of the direct Mg/Al joint, with a maximum value of 25.4 MPa achieved at 700 °C. Fracture occurred mainly along the Mg/Ni interface for the Mg/Ni/Al multilayer structure castings.

  17. Role of interlayer hydration in lincomycin sorption by smectite clays.

    PubMed

    Wang, Cuiping; Ding, Yunjie; Teppen, Brian J; Boyd, Stephen A; Song, Cunyi; Li, Hui

    2009-08-15

    Lincomycin, an antibiotic widely administered as a veterinary medicine, is frequently detected in water. Little is known about the soil-water distribution of lincomycin despite the fact that this is a major determinant of its environmental fate and potential for exposure. Cation exchange was found to be the primary mechanism responsible for lincomycin sorption by soil clay minerals. This was evidenced by pH-dependent sorption, and competition with inorganic cations for sorptive sites. As solution pH increased, lincomycin sorption decreased. The extent of reduction was consistent with the decrease in cationic lincomycin species in solution. The presence of Ca2+ in solution diminished lincomycin sorption. Clay interlayer hydration status strongly influenced lincomycin adsorption. Smectites with the charge deficit from isomorphic substitution in tetrahedral layers (i.e., saponite) manifest a less hydrated interlayer environment resulting in greater sorption than that by octahedrally substituted clays (i.e., montmorillonite). Strongly hydrated exchangeable cations resulted in a more hydrated clay interlayer environment reducing sorption in the order of Ca- < K- < Cs-smectite. X-ray diffraction revealed that lincomycin was intercalated in smectite clay interlayers. Sorption capacity was limited by clay surface area rather than by cation exchange capacity. Smectite interlayer hydration was shown to be a major, yet previously unrecognized, factor influencing the cation exchange process of lincomycin on aluminosilicate mineral surfaces.

  18. DOE Office of Scientific and Technical Information (OSTI.GOV)

    Poletika, T. M., E-mail: poletm@ispms.tsc.ru; Girsova, S. L., E-mail: llm@ispms.tsc.ru; Meisner, L. L., E-mail: girs@ispms.tsc.ru

    The structure of the surface and near-surface layers of single crystals of NiTi, differently oriented relative to the direction of ion beam treatment was investigated. The role of the crystallographic orientation in formation of structure of surface layers after ion-plasma alloying was revealed. It was found that the orientation effects of selective sputtering and channeling determine the thickness of the oxide and amorphous layers, the depth of penetration of ions and impurities, the distribution of Ni with depth.

  19. Cellular uptake and ex vivo urothelial penetration by oligodeoxynucleotides for optimizing treatment of transitional cell carcinoma.

    PubMed

    Bolenz, Christian; Trojan, Lutz; Gabriel, Ute; Honeck, Patrick; Wendt-Nordahl, Gunnar; Schaaf, Axel; Alken, Peter; Michel, Maurice Stephan

    2008-10-01

    To evaluate cellular uptake and urothelial penetration of oligodeoxynucleotides (ODNs) in transitional cell carcinoma (TCC) cell lines and in a porcine ex vivo model, respectively. A panel of human TCC cell lines (RT 112, HT 1197 and UM-UC3) were exposed tofluorescein-labeled ODNs. Transfection rates were assessed byfluorescence microscopy and fluorescence-activated cell sorting (FACS). Intravesical treatment with ODNs was performed in a porcine ex vivo model. Urothelial penetration was evaluated using fluorescence microscopy of cryosections. Treatment with ODNs provided transfection rates of at least 96.8% of TCC cells, irrespective of use of a transfection agent. Effective urothelial penetration by ODNs was detected when compared with controls (p = 0.0325). The addition of a liposomal transfection agent significantly increased the penetration depth, allowing affection of deep urothelial cell layers (p = 0.0082). High transfection rates of ODNs can be achieved in TCC cells. Urothelial penetration of ODNs was observed down to the deepest cell layers when a transfection agent is added, suggesting a high potential for complementing the chemoresection effects on residual tumor areas during intravesical therapy of non-muscle-invasive TCC.

  20. Unsteady penetration of a target by a liquid jet

    PubMed Central

    Uth, Tobias; Deshpande, Vikram S.

    2013-01-01

    It is widely acknowledged that ceramic armor experiences an unsteady penetration response: an impacting projectile may erode on the surface of a ceramic target without substantial penetration for a significant amount of time and then suddenly start to penetrate the target. Although known for more than four decades, this phenomenon, commonly referred to as dwell, remains largely unexplained. Here, we use scaled analog experiments with a low-speed water jet and a soft, translucent target material to investigate dwell. The transient target response, in terms of depth of penetration and impact force, is captured using a high-speed camera in combination with a piezoelectric force sensor. We observe the phenomenon of dwell using a soft (noncracking) target material. The results show that the penetration rate increases when the flow of the impacting water jet is reversed due to the deformation of the jet–target interface––this reversal is also associated with an increase in the force exerted by the jet on the target. Creep penetration experiments with a constant indentation force did not show an increase in the penetration rate, confirming that flow reversal is the cause of the unsteady penetration rate. Our results suggest that dwell can occur in a ductile noncracking target due to flow reversal. This phenomenon of flow reversal is rather widespread and present in a wide range of impact situations, including water-jet cutting, needleless injection, and deposit removal via a fluid jet. PMID:24277818

Top