Johann Spectrometer for High Resolution X-ray Spectroscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Machek, Pavel; Froeba, Michael; Welter, Edmund

2007-01-19

A newly designed vacuum Johann spectrometer with a large focusing analyzer crystal for inelastic x-ray scattering and high resolution fluorescence spectroscopy has been installed at the DORIS III storage ring. Spherically bent crystals with a maximum diameter of 125 mm, and cylindrically bent crystals are employed as dispersive optical elements. Standard radius of curvature of the crystals is 1000 mm, however, the design of the mechanical components also facilitates measurements with smaller and larger bending radii. Up to four crystals are mounted on a revolving crystal changer which enables crystal changes without breaking the vacuum. The spectrometer works at fixedmore » Bragg angle. It is preferably designed for the measurements in non-scanning mode with a broad beam spot, and offers a large flexibility to set the sample to the optimum position inside the Rowland circle. A deep depletion CCD camera is employed as a position sensitive detector to collect the energy-analyzed photons on the circumference of the Rowland circle. The vacuum in the spectrometer tank is typically 10-6 mbar. The sample chamber is separated from the tank either by 25 {mu}m thick Kapton windows, which allows samples to be measured under ambient conditions, or by two gate valves. The spectrometer is currently installed at wiggler beamline W1 whose working range is 4-10.5 keV with typical flux at the sample of 5x1010photons/s/mm2. The capabilities of the spectrometer are illustrated by resonant inelastic experiments on 3d transition metals and rare earth compounds, and by chemical shift measurements on chromium compounds.« less

Charge dynamics of MgO single crystals subjected to KeV electron irradiation

NASA Astrophysics Data System (ADS)

Boughariou, A.; Blaise, G.; Braga, D.; Kallel, A.

2004-04-01

A scanning electron microscope has been equipped to study the fundamental aspects of charge trapping in insulating materials, by measuring the secondary electron emission (SEE) yield σ with a high precision (a few percent), as a function of energy, electron current density, and dose. The intrinsic secondary electron emission yield σ0 of uncharged MgO single crystals annealed at 1000 °C, 2 h, has been studied at four energies 1.1, 5, 15, and 30 keV on three different crystal orientations (100), (110), and (111). At low energies (1.1 and 5 keV) σ0 depends on the crystalline orientation wheras at high energies (30 keV) no differentiation occurs. It is shown that the value of the second crossover energy E2, for which the intrinsic SEE yield σ0=1, is extremely delicate to measure with precision. It is about 15 keV±500 eV for the (100) orientation, 13.5 keV±500 eV for the (110), and 18.5 keV±500 eV for the (111) one. At low current density J⩽105 pA/cm2, the variation of σ with the injected dose makes possible the observation of a self-regulated regime characterized by a steady value of the SEE yield σst=1. At low energies 1.1 and 5 keV, there is no current density effects in MgO, but at high energies ≈30 keV, apparent current density effects come from a bad collect of secondary electrons, due to very high negative surface potential. At 30 keV energy, an intense erratic electron exoemission was observed on the MgO (110) orientation annealed at 1500 °C. This phenomenon is the result of a disruptive process similar to flashover, which takes place at the surface of the material.

Effects of thermal expansion of the crystal lattice on x-ray crystal spectrometers used for fusion research

NASA Astrophysics Data System (ADS)

Delgado-Aparicio, L.; Bitter, M.; Podpaly, Y.; Rice, J.; Burke, W.; Sanchez del Rio, M.; Beiersdorfer, P.; Bell, R.; Feder, R.; Gao, C.; Hill, K.; Johnson, D.; Lee, S. G.; Marmar, E.; Pablant, N.; Reinke, M. L.; Scott, S.; Wilson, R.

2013-12-01

X-ray imaging crystal spectrometers with high spectral and spatial resolution are currently being used on magnetically confined fusion devices to infer the time history profiles of ion and electron temperatures as well as plasma flow velocities. The absolute measurement of flow velocities is important for optimizing various discharge scenarios and evaluating the radial electric field in tokamak and stellarator plasmas. Recent studies indicate that the crystal temperature must be kept constant to within a fraction of a degree to avoid changes of the interplanar 2d-spacing by thermal expansion that cause changes in the Bragg angle, which could be misinterpreted as Doppler shifts. For the instrumental parameters of the x-ray crystal spectrometer on Alcator C-Mod, where those thermal effects were investigated, a change of the crystal temperature by 1 °C causes a change of the lattice spacing of the order of Δd = 1 × 10-5 Å introducing a fictitious velocity drift of the order of ˜3 km s-1. This effect must be considered for x-ray imaging crystals spectrometers installed on LHD, KSTAR, EAST, J-TEXT, NSTX and, in the future, W7-X and ITER.

Absolute activity measurements with the windowless 4π-CsI(Tl)-sandwich spectrometer

NASA Astrophysics Data System (ADS)

Denecke, B.

1994-01-01

The windowless 4π-CsI(Tl)-sandwich spectrometer consists of two scintillation crystals sandwiching radioactive sources deposited on thin plastic foils. This configuration has a solid angle very close to 4π sr. The detectors are sensitive to charged particles with energies > 15 keV and measure photons of 15-200 keV with a probability > 98%. Disintegration rates of samples of radionuclides with complex decay modes can be determined directly from the measured count rates with uncertainties below 0.3%. Radionuclide solutions of 57Co, 109Cd, 125I, 152Eu and 192Ir were standardised, partly in the framework of international comparisons. A detailed description of the spectrometer and the measurement procedure is given.

On the design of the NIF Continuum Spectrometer

NASA Astrophysics Data System (ADS)

Thorn, D. B.; MacPhee, A.; Ayers, J.; Galbraith, J.; Hardy, C. M.; Izumi, N.; Bradley, D. K.; Pickworth, L. A.; Bachmann, B.; Kozioziemski, B.; Landen, O.; Clark, D.; Schneider, M. B.; Hill, K. W.; Bitter, M.; Nagel, S.; Bell, P. M.; Person, S.; Khater, H. Y.; Smith, C.; Kilkenny, J.

2017-08-01

In inertial confinement fusion (ICF) experiments on the National Ignition Facility (NIF), measurements of average ion temperature using DT neutron time of flight broadening and of DD neutrons do not show the same apparent temperature. Some of this may be due to time and space dependent temperature profiles in the imploding capsule which are not taken into account in the analysis. As such, we are attempting to measure the electron temperature by recording the free-free electron-ion scattering-spectrum from the tail of the Maxwellian temperature distribution. This will be accomplished with the new NIF Continuum Spectrometer (ConSpec) which spans the x-ray range of 20 keV to 30 keV (where any opacity corrections from the remaining mass of the ablator shell are negligible) and will be sensitive to temperatures between ˜ 3 keV and 6 keV. The optical design of the ConSpec is designed to be adaptable to an x-ray streak camera to record time resolved free-free electron continuum spectra for direct measurement of the dT/dt evolution across the burn width of a DT plasma. The spectrometer is a conically bent Bragg crystal in a focusing geometry that allows for the dispersion plane to be perpendicular to the spectrometer axis. Additionally, to address the spatial temperature dependence, both time integrated and time resolved pinhole and penumbral imaging will be provided along the same polar angle. The optical and mechanical design of the instrument is presented along with estimates for the dispersion, solid angle, photometric sensitivity, and performance.

Calibration of X-ray spectrometers for opacity experiments at the Orion laser facility (invited).

PubMed

Bentley, C; Allan, P; Brent, K; Bruce, N; Hoarty, D; Meadowcroft, A; Percival, J; Opie, C

2016-11-01

Accurately calibrated and characterised x-ray diagnostics are a key requirement in the fielding of experiments on the Orion laser where absolute measurements of x-ray emission are used to underpin the validity of models of emissivity and opacity. Diffraction crystals are used in spectrometers on Orion to record the dispersed spectral features emitted by the laser produced plasma to obtain a measurement of the plasma conditions. The ability to undertake diffraction crystal calibrations supports the successful outcome of these Orion experiments. This paper details the design and commissioning of a system to undertake these calibrations in the energy range 2.0 keV to approximately 8.5 keV. Improvements to the design are detailed which will extend the commissioned range of energies to below 1 keV.

A 7.2 keV spherical crystal backlighter system for Sandia's Z Pulsed Power Facility

NASA Astrophysics Data System (ADS)

Schollmeier, M.; Knapp, P. F.; Ampleford, D. J.; Loisel, G. P.; Robertson, G.; Shores, J. E.; Smith, I. C.; Speas, C. S.; Porter, J. L.; McBride, R. D.

2016-10-01

Many experiments on Sandia's Z facility, a 30 MA, 100 ns rise-time, pulsed-power driver, use a monochromatic Quartz crystal imaging backlighter system at 1.865 keV (Si Heα) or 6.151 keV (Mn Heα) x-ray energy to radiograph an imploding liner (cylindrical tube) or wire array. The x-ray source is generated by the Z-Beamlet Laser (ZBL), which provides up to 4.5 kJ at 527 nm during a 6 ns window. Radiographs of an imploding thick-walled Beryllium liner at a convergence ratio of about 20 [CR =Rin . (0) /Rin . (t) ] were too opaque to identify the inner surface of the liner with high confidence, demonstrating the need for a higher-energy x-ray backlighter between 6 and 10 keV. We present the design, test and first application of a Ge (335) spherical crystal x-ray backlighter system using the 7.242 keV Co Heα resonance line. The system operates at an almost identical Bragg angle as the existing 1.865 and 6.151 keV backlighters, enhancing our capabilities such as two-color, two-frame radiography, without changing detector shielding hardware. SAND No: SAND2016-6724 A. Sandia National Laboratories is a multi-program laboratory managed and operated by Sandia Corp., a wholly owned subsidiary of Lockheed Martin Corp., for the U.S. DoE NNSA under contract DE-AC04-94AL85000.

Pump–probe spectrometer for measuring x-ray induced strain

DOE PAGES

Loether, A.; Adams, B. W.; DiCharia, A.; ...

2016-04-20

A hard x-ray pump–probe spectrometer using a multi-crystal Bragg reflector is demonstrated at a third generation synchrotron source. This device derives both broadband pump and monochromatic probe pulses directly from a single intense, broadband x-ray pulse centered at 8.767 keV. In conclusion, we present a proof-of-concept experiment which directly measures x-ray induced crystalline lattice strain.

Portable neutron spectrometer and dosimeter

DOEpatents

Waechter, D.A.; Erkkila, B.H.; Vasilik, D.G.

The disclosure relates to a battery operated neutron spectrometer/dosimeter utilizing a microprocessor, a built-in tissue equivalent LET neutron detector, and a 128-channel pulse height analyzer with integral liquid crystal display. The apparatus calculates doses and dose rates from neutrons incident on the detector and displays a spectrum of rad or rem as a function of keV per micron of equivalent tissue and also calculates and displays accumulated dose in millirads and millirem as well as neutron dose rates in millirads per hour and millirem per hour.

Portable neutron spectrometer and dosimeter

DOEpatents

Waechter, David A.; Erkkila, Bruce H.; Vasilik, Dennis G.

1985-01-01

The disclosure relates to a battery operated neutron spectrometer/dosimeter utilizing a microprocessor, a built-in tissue equivalent LET neutron detector, and a 128-channel pulse height analyzer with integral liquid crystal display. The apparatus calculates doses and dose rates from neutrons incident on the detector and displays a spectrum of rad or rem as a function of keV per micron of equivalent tissue and also calculates and displays accumulated dose in millirads and millirem as well as neutron dose rates in millirads per hour and millirem per hour.

Improving a high-efficiency, gated spectrometer for x-ray Thomson scattering experiments at the National Ignition Facility.

PubMed

Döppner, T; Kraus, D; Neumayer, P; Bachmann, B; Emig, J; Falcone, R W; Fletcher, L B; Hardy, M; Kalantar, D H; Kritcher, A L; Landen, O L; Ma, T; Saunders, A M; Wood, R D

2016-11-01

We are developing x-ray Thomson scattering for applications in implosion experiments at the National Ignition Facility. In particular we have designed and fielded MACS, a high-efficiency, gated x-ray spectrometer at 7.5-10 keV [T. Döppner et al., Rev. Sci. Instrum. 85, 11D617 (2014)]. Here we report on two new Bragg crystals based on Highly Oriented Pyrolytic Graphite (HOPG), a flat crystal and a dual-section cylindrically curved crystal. We have performed in situ calibration measurements using a brass foil target, and we used the flat HOPG crystal to measure Mo K-shell emission at 18 keV in 2nd order diffraction. Such high photon energy line emission will be required to penetrate and probe ultra-high-density plasmas or plasmas of mid-Z elements.

A high-resolution imaging x-ray crystal spectrometer for high energy density plasmas

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, Hui, E-mail: chen33@llnl.gov, E-mail: bitter@pppl.gov; Magee, E.; Nagel, S. R.

2014-11-15

Adapting a concept developed for magnetic confinement fusion experiments, an imaging crystal spectrometer has been designed and tested for HED plasmas. The instrument uses a spherically bent quartz [211] crystal with radius of curvature of 490.8 mm. The instrument was tested at the Titan laser at Lawrence Livermore National Laboratory by irradiating titanium slabs with laser intensities of 10{sup 19}–10{sup 20} W/cm{sup 2}. He-like and Li-like Ti lines were recorded, from which the spectrometer performance was evaluated. This spectrometer provides very high spectral resolving power (E/dE > 7000) while acquiring a one-dimensional image of the source.

X-ray Diffraction Crystal Calibration and Characterization

DOE Office of Scientific and Technical Information (OSTI.GOV)

Michael J. Haugh; Richard Stewart; Nathan Kugland

2009-06-05

National Security Technologies’ X-ray Laboratory is comprised of a multi-anode Manson type source and a Henke type source that incorporates a dual goniometer and XYZ translation stage. The first goniometer is used to isolate a particular spectral band. The Manson operates up to 10 kV and the Henke up to 20 kV. The Henke rotation stages and translation stages are automated. Procedures have been developed to characterize and calibrate various NIF diagnostics and their components. The diagnostics include X-ray cameras, gated imagers, streak cameras, and other X-ray imaging systems. Components that have been analyzed include filters, filter arrays, grazing incidencemore » mirrors, and various crystals, both flat and curved. Recent efforts on the Henke system are aimed at characterizing and calibrating imaging crystals and curved crystals used as the major component of an X-ray spectrometer. The presentation will concentrate on these results. The work has been done at energies ranging from 3 keV to 16 keV. The major goal was to evaluate the performance quality of the crystal for its intended application. For the imaging crystals we measured the laser beam reflection offset from the X-ray beam and the reflectivity curves. For the curved spectrometer crystal, which was a natural crystal, resolving power was critical. It was first necessary to find sources of crystals that had sufficiently narrow reflectivity curves. It was then necessary to determine which crystals retained their resolving power after being thinned and glued to a curved substrate.« less

A tandem mass spectrometer for crossed-beam irradiation of mass-selected molecular systems by keV atomic ions

NASA Astrophysics Data System (ADS)

Schwob, Lucas; Lalande, Mathieu; Chesnel, Jean-Yves; Domaracka, Alicja; Huber, Bernd A.; Maclot, Sylvain; Poully, Jean-Christophe; Rangama, Jimmy; Rousseau, Patrick; Vizcaino, Violaine; Adoui, Lamri; Méry, Alain

2018-04-01

In the present paper, we describe a new home-built crossed-beam apparatus devoted to ion-induced ionization and fragmentation of isolated biologically relevant molecular systems. The biomolecular ions are produced by an electrospray ionization source, mass-over-charge selected, accumulated in a 3D ion trap, and then guided to the extraction region of an orthogonal time-of-flight mass spectrometer. Here, the target molecular ions interact with a keV atomic ion beam produced by an electron cyclotron resonance ion source. Cationic products from the collision are detected on a position sensitive detector and analyzed by time-of-flight mass spectrometry. A detailed description of the operation of the setup is given, and early results from irradiation of a protonated pentapeptide (leucine-enkephalin) by a 7 keV He+ ion beam are presented as a proof-of-principle.

The transient gamma-ray spectrometer

NASA Technical Reports Server (NTRS)

Owens, A.; Baker, R.; Cline, T. L.; Gehrels, N.; Jermakian, J.; Nolan, T.; Ramaty, R.; Smith, G.; Stilwell, D. E.; Teegarden, B. J.

1991-01-01

The authors describe the Transient Gamma-Ray Spectrometer (TGRS) to be flown onboard the WIND spacecraft. This instrument is designed to detect cosmic gamma-ray bursts over the energy range of 20 keV to 10 MeV with an expected spectroscopic resolution of 2 keV at 1 MeV (E/Delta-E = 500). The active detection element is a 215-cu cm high-purity n-type Ge crystal cooled to cryogenic temperatures by a passive radiative cooler. The geometric field of view (FOV) defined by the cooler is 170 deg FWFM. Burst data are stored directly in an onboard 2.75-Mb burst memory with an absolute timing accuracy of +/-1.5 ms. This capacity is sufficient to store the entire spectral data set of all but the largest bursts. In addition to burst measurements, the instrument will also study solar flares, search for possible diffuse background lines, and monitor the 511-keV positron annihilation radiation from the galactic center. The experiment is scheduled to be launched on a Delta II launch vehicle from Cape Canaveral on December 31, 1992.

High-resolution crystal spectrometer for the 10-60 (angstrom) EUV region

DOE Office of Scientific and Technical Information (OSTI.GOV)

Beiersdorfer, P; Brown, G V; Goddard, R

2004-02-20

A vacuum crystal spectrometer with nominal resolving power approaching 1000 is described for measuring emission lines with wavelength in the extreme ultraviolet region up to 60 Angstroms. The instrument utilizes a flat octadecyl hydrogen maleate (OHM) crystal and a thin-window 1-D position-sensitive gas proportional detector. This detector employs a 1 {micro}m-thick 100 x8 mm{sup 2} aluminized polyimide window and operates at one atmosphere pressure. The spectrometer has been implemented on the Livermore electron beam ion traps. The performance of the instrument is illustrated in measurements of the newly discovered magnetic field-sensitive line in Ar{sup 8+}.

The spectral archive of cosmic X-ray sources observed by the Einstein Observatory Focal Plane Crystal Spectrometer

NASA Technical Reports Server (NTRS)

Lum, Kenneth S. K.; Canizares, Claude R.; Clark, George W.; Coyne, Joan M.; Markert, Thomas H.; Saez, Pablo J.; Schattenburg, Mark L.; Winkler, P. F.

1992-01-01

The Einstein Observatory Focal Plane Crystal Spectrometer (FPCS) used the technique of Bragg spectroscopy to study cosmic X-ray sources in the 0.2-3 keV energy range. The high spectral resolving power (E/Delta-E is approximately equal to 100-1000) of this instrument allowed it to resolve closely spaced lines and study the structure of individual features in the spectra of 41 cosmic X-ray sources. An archival summary of the results is presented as a concise record the FPCS observations and a source of information for future analysis by the general astrophysics community. For each observation, the instrument configuration, background rate, X-ray flux or upper limit within the energy band observed, and spectral histograms are given. Examples of the contributions the FPCS observations have made to the understanding of the objects observed are discussed.

Advanced X-ray Imaging Crystal Spectrometer for Magnetic Fusion Tokamak Devices

NASA Astrophysics Data System (ADS)

Lee, S. G.; Bak, J. G.; Bog, M. G.; Nam, U. W.; Moon, M. K.; Cheon, J. K.

2008-03-01

An advanced X-ray imaging crystal spectrometer is currently under development using a segmented position sensitive detector and time-to-digital converter (TDC) based delay-line readout electronics for burning plasma diagnostics. The proposed advanced XICS utilizes an eight-segmented position sensitive multi-wire proportional counter and supporting electronics to increase the spectrometer performance includes the photon count-rate capability and spatial resolution.

Improving a high-efficiency, gated spectrometer for x-ray Thomson scattering experiments at the National Ignition Facility

DOE PAGES

Döppner, T.; Kraus, D.; Neumayer, P.; ...

2016-08-03

We are developing x-ray Thomson scattering for applications in implosion experiments at the National Ignition Facility. In particular we have designed and fielded MACS, a high-efficiency, gated x-ray spectrometer at 7.5-10 keV [T. Döppner et al., Rev. Sci. Instrum. 85, 11D617 (2014)]. Here in this paper we report on two new Bragg crystals based on Highly Oriented Pyrolytic Graphite (HOPG), a flat crystal and a dual-section cylindrically curved crystal. We have performed in situ calibration measurements using a brass foil target, and we used the flat HOPG crystal to measure Mo K-shell emission at 18 keV in 2nd order diffraction.more » Such high photon energy line emission will be required to penetrate and probe ultra-high-density plasmas or plasmas of mid-Z elements.« less

Improving a high-efficiency, gated spectrometer for x-ray Thomson scattering experiments at the National Ignition Facility

DOE Office of Scientific and Technical Information (OSTI.GOV)

Döppner, T., E-mail: doeppner1@llnl.gov; Bachmann, B.; Emig, J.

We are developing x-ray Thomson scattering for applications in implosion experiments at the National Ignition Facility. In particular we have designed and fielded MACS, a high-efficiency, gated x-ray spectrometer at 7.5–10 keV [T. Döppner et al., Rev. Sci. Instrum. 85, 11D617 (2014)]. Here we report on two new Bragg crystals based on Highly Oriented Pyrolytic Graphite (HOPG), a flat crystal and a dual-section cylindrically curved crystal. We have performed in situ calibration measurements using a brass foil target, and we used the flat HOPG crystal to measure Mo K-shell emission at 18 keV in 2nd order diffraction. Such high photonmore » energy line emission will be required to penetrate and probe ultra-high-density plasmas or plasmas of mid-Z elements.« less

High-resolution crystal spectrometer for the 10-60 A extreme ultraviolet region

DOE Office of Scientific and Technical Information (OSTI.GOV)

Beiersdorfer, P.; Brown, G.V.; Goddard, R.

2004-10-01

A vacuum crystal spectrometer with nominal resolving power approaching 1000 is described for measuring emission lines with wavelength in the extreme ultraviolet region up to 60 A. The instrument utilizes a flat octadecyl hydrogen maleate crystal and a thin-window 1D position-sensitive gas proportional detector. This detector employs a 1-{mu}m-thick 100x8 mm{sup 2} aluminized polyimide window and operates at one atmosphere pressure. The spectrometer has been implemented on the Livermore electron beam ion traps. The performance of the instrument is illustrated in measurements of the newly discovered magnetic field-sensitive line in Ar{sup 8+}.

A new time and space resolved transmission spectrometer for research in inertial confinement fusion and radiation source development.

PubMed

Knapp, P F; Ball, C; Austin, K; Hansen, S B; Kernaghan, M D; Lake, P W; Ampleford, D J; McPherson, L A; Sandoval, D; Gard, P; Wu, M; Bourdon, C; Rochau, G A; McBride, R D; Sinars, D B

2017-01-01

We describe the design and function of a new time and space resolved x-ray spectrometer for use in Z-pinch inertial confinement fusion and radiation source development experiments. The spectrometer is designed to measure x-rays in the range of 0.5-1.5 Å (8-25 keV) with a spectral resolution λ/Δλ ∼ 400. The purpose of this spectrometer is to measure the time- and one-dimensional space-dependent electron temperature and density during stagnation. These relatively high photon energies are required to escape the dense plasma created at stagnation and to obtain sensitivity to electron temperatures ≳3 keV. The spectrometer is of the Cauchois type, employing a large 30 × 36 mm 2 , transmissive quartz optic for which a novel solid beryllium holder was designed. The performance of the crystal was verified using offline tests, and the integrated system was tested using experiments on the Z pulsed power accelerator.

High-resolution Bent-crystal Spectrometer for the Ultra-soft X-ray Region

DOE R&D Accomplishments Database

Beiersdorfer, P.; von Goeler, S.; Bitter, M.; Hill, K. W.; Hulse, R. A.; Walling, R. S.

1988-10-01

A multichannel vacuum Brag-crystal spectrometer has been developed for high-resolution measurements of the line emission from tokamak plasmas in the wavelength region between 4 and 25 angstrom. The spectrometer employs a bent crystal in Johann geometry and a microchannel-plate intensified photodiode array. The instrument is capable of measuring high-resolution spectra (lambda/..delta..lambda approx. 3000) with fast time resolution (4 msec per spectrum) and good spatial resolution (3 cm). The spectral bandwidth is ..delta..lambda/lambda{sub 0} = 8 angstrom. A simple tilt mechanism allows access to different wavelength intervals. In order to illustrate the utility of the new spectrometer, time- and space-resolved measurements of the n = 3 to n = 2 spectrum of selenium from the Princeton Large Torus tokamak plasmas are presented. The data are used to determine the plasma transport parameters and to infer the radial distribution of fluorinelike, neonlike, and sodiumlike ions of selenium in the plasma. The new ultra-soft x-ray spectrometer has thus enabled us to demonstrate the utility of high-resolution L-shell spectroscopy of neonlike ions as a fusion diagnostic.

A multi-cone x-ray imaging Bragg crystal spectrometer

DOE PAGES

Bitter, M.; Hill, K. W.; Gao, Lan; ...

2016-08-26

This article describes a new x-ray imaging Bragg crystal spectrometer, which—in combination with a streak camera or a gated strip detector—can be used for time-resolved measurements of x-ray line spectra at the National Ignition Facility and other high power laser facilities. The main advantage of this instrument is that it produces perfect images of a point source for each wavelength in a selectable spectral range and that the detector plane can be perpendicular to the crystal surface or inclined by an arbitrary angle with respect to the crystal surface. Furthermore, these unique imaging properties are obtained by bending the x-raymore » diffracting crystal into a certain shape, which is generated by arranging multiple cones with different aperture angles on a common nodal line.« less

X-ray spectrometer with a low-cost SiC photodiode

NASA Astrophysics Data System (ADS)

Zhao, S.; Lioliou, G.; Barnett, A. M.

2018-04-01

A low-cost Commercial-Off-The-Shelf (COTS) 4H-SiC 0.06 mm2 UV p-n photodiode was coupled to a low-noise charge-sensitive preamplifier and used as photon counting X-ray spectrometer. The photodiode/spectrometer was investigated at X-ray energies from 4.95 keV to 21.17 keV: a Mo cathode X-ray tube was used to fluoresce eight high-purity metal foils to produce characteristic X-ray emission lines which were used to characterise the instrument. The energy resolution (full width at half maximum, FWHM) of the spectrometer was found to be 1.6 keV to 1.8 keV, across the energy range. The energy linearity of the detector/spectrometer (i.e. the detector's charge output per photon as a function of incident photon energy across the 4.95 keV to 21.17 keV energy range), as well as the count rate linearity of the detector/spectrometer (i.e. number of detected photons as a function of photon fluence at a specific energy) were investigated. The energy linearity of the detector/spectrometer was linear with an error < ± 0.7 %; the count rate linearity of the detector/spectrometer was linear with an error < ± 2 %. The use of COTS SiC photodiodes as detectors for X-ray spectrometers is attractive for nanosatellite/CubeSat applications (including solar flare monitoring), and for cost sensitive industrial uses.

A short working distance multiple crystal x-ray spectrometer

USGS Publications Warehouse

Dickinson, B.; Seidler, G.T.; Webb, Z.W.; Bradley, J.A.; Nagle, K.P.; Heald, S.M.; Gordon, R.A.; Chou, I.-Ming

2008-01-01

For x-ray spot sizes of a few tens of microns or smaller, a millimeter-sized flat analyzer crystal placed ???1 cm from the sample will exhibit high energy resolution while subtending a collection solid angle comparable to that of a typical spherically bent crystal analyzer (SBCA) at much larger working distances. Based on this observation and a nonfocusing geometry for the analyzer optic, we have constructed and tested a short working distance (SWD) multicrystal x-ray spectrometer. This prototype instrument has a maximum effective collection solid angle of 0.14 sr, comparable to that of 17 SBCA at 1 m working distance. We find good agreement with prior work for measurements of the Mn K?? x-ray emission and resonant inelastic x-ray scattering for MnO, and also for measurements of the x-ray absorption near-edge structure for Dy metal using L??2 partial-fluorescence yield detection. We discuss future applications at third- and fourth-generation light sources. For concentrated samples, the extremely large collection angle of SWD spectrometers will permit collection of high-resolution x-ray emission spectra with a single pulse of the Linac Coherent Light Source. The range of applications of SWD spectrometers and traditional multi-SBCA instruments has some overlap, but also is significantly complementary. ?? 2008 American Institute of Physics.

X-ray crystal spectrometer upgrade for ITER-like wall experiments at JETa)

NASA Astrophysics Data System (ADS)

Shumack, A. E.; Rzadkiewicz, J.; Chernyshova, M.; Jakubowska, K.; Scholz, M.; Byszuk, A.; Cieszewski, R.; Czarski, T.; Dominik, W.; Karpinski, L.; Kasprowicz, G.; Pozniak, K.; Wojenski, A.; Zabolotny, W.; Conway, N. J.; Dalley, S.; Figueiredo, J.; Nakano, T.; Tyrrell, S.; Zastrow, K.-D.; Zoita, V.

2014-11-01

The high resolution X-Ray crystal spectrometer at the JET tokamak has been upgraded with the main goal of measuring the tungsten impurity concentration. This is important for understanding impurity accumulation in the plasma after installation of the JET ITER-like wall (main chamber: Be, divertor: W). This contribution provides details of the upgraded spectrometer with a focus on the aspects important for spectral analysis and plasma parameter calculation. In particular, we describe the determination of the spectrometer sensitivity: important for impurity concentration determination.

X-ray crystal spectrometer upgrade for ITER-like wall experiments at JET.

PubMed

Shumack, A E; Rzadkiewicz, J; Chernyshova, M; Jakubowska, K; Scholz, M; Byszuk, A; Cieszewski, R; Czarski, T; Dominik, W; Karpinski, L; Kasprowicz, G; Pozniak, K; Wojenski, A; Zabolotny, W; Conway, N J; Dalley, S; Figueiredo, J; Nakano, T; Tyrrell, S; Zastrow, K-D; Zoita, V

2014-11-01

The high resolution X-Ray crystal spectrometer at the JET tokamak has been upgraded with the main goal of measuring the tungsten impurity concentration. This is important for understanding impurity accumulation in the plasma after installation of the JET ITER-like wall (main chamber: Be, divertor: W). This contribution provides details of the upgraded spectrometer with a focus on the aspects important for spectral analysis and plasma parameter calculation. In particular, we describe the determination of the spectrometer sensitivity: important for impurity concentration determination.

The Los Alamos National Laboratory precision double crystal spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Morgan, D.V.; Stevens, C.J.; Liefield, R.J.

1994-03-01

This report discusses the following topics on the LANL precision double crystal X-ray spectrometer: Motivation for construction of the instrument; a brief history of the instrument; mechanical systems; motion control systems; computer control system; vacuum system; alignment program; scan programs; observations of the copper K{alpha} lines; and characteristics and specifications.

HYSPEC : A CRYSTAL TIME OF FLIGHT HYBRID SPECTROMETER FOR THE SPALLATION NEUTRON SOURCE.

DOE Office of Scientific and Technical Information (OSTI.GOV)

SHAPIRO,S.M.; ZALIZNYAK,I.A.

2002-12-30

This document lays out a proposal by the Instrument Development Team (IDT) composed of scientists from leading Universities and National Laboratories to design and build a conceptually new high-flux inelastic neutron spectrometer at the pulsed Spallation Neutron Source (SNS) at Oak Ridge. This instrument is intended to supply users of the SNS and scientific community, of which the IDT is an integral part, with a platform for ground-breaking investigations of the low-energy atomic-scale dynamical properties of crystalline solids. It is also planned that the proposed instrument will be equipped with a polarization analysis capability, therefore becoming the first polarized beammore » inelastic spectrometer in the SNS instrument suite, and the first successful polarized beam inelastic instrument at a pulsed spallation source worldwide. The proposed instrument is designed primarily for inelastic and elastic neutron spectroscopy of single crystals. In fact, the most informative neutron scattering studies of the dynamical properties of solids nearly always require single crystal samples, and they are almost invariably flux-limited. In addition, in measurements with polarization analysis the available flux is reduced through selection of the particular neutron polarization, which puts even more stringent limits on the feasibility of a particular experiment. To date, these investigations have mostly been carried out on crystal spectrometers at high-flux reactors, which usually employ focusing Bragg optics to concentrate the neutron beam on a typically small sample. Construction at Oak Ridge of the high-luminosity spallation neutron source, which will provide intense pulsed neutron beams with time-averaged fluxes equal to those at medium-flux reactors, opens entirely new opportunities for single crystal neutron spectroscopy. Drawing upon experience acquired during decades of studies with both crystal and time-of-flight (TOF) spectrometers, the IDT has developed a

Calibration of the OHREX high-resolution imaging crystal spectrometer at the Livermore electron beam ion traps [Calibration of the OHREX high-resolution imaging crystal spectrometer at the Livermore EBIT

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hell, N.; Beiersdorfer, P.; Magee, E. W.

2016-08-04

Here, we report the calibration of the Orion High-Resolution X-ray (OHREX) imaging crystal spectrometer at the EBIT-I electron beam ion trap at Livermore. Two such instruments, dubbed OHREX-1 and OHREX-2, are fielded for plasma diagnostics at the Orion laser facility in the United Kingdom. The OHREX spectrometer can simultaneously house two spherically bent crystals with a radius of curvature of r=67.2 cm. The focusing properties of the spectrometer allow both for larger distance to the source due to the increase in collected light and for observation of extended sources. OHREX is designed to cover a 2.5–3 degree spectral range atmore » Bragg angles around 51.3 degree. The typically high resolving powers at these large Bragg angles are ideally suited for line shape diagnostics. For instance, the nominal resolving power of the instrument (> 10000) is much higher than the effective resolving power associated with the Doppler broadening due to the temperature of the trapped ions in EBIT-I. The effective resolving power is only around 3000 at typical EBIT-I conditions, which nevertheless is sufficient to set up and test the instrument’s spectral characteristics. We have calibrated the spectral range for a number of crystals using well known reference lines in first and second order, and derived the ion temperatures from these lines. We have also made use of the 50µm size of the EBIT-I source width to characterize the spatial focusing of the spectrometer.« less

Double axis, two-crystal x-ray spectrometer.

PubMed

Erez, G; Kimhi, D; Livnat, A

1978-05-01

A two-crystal double axis x-ray spectrometer, capable of goniometric accuracy on the order of 0.1", has been developed. Some of its unique design features are presented. These include (1) a modified commercial thrust bearing which furnishes a precise, full circle theta:2theta coupling, (2) a new tangent drive system design in which a considerable reduction of the lead screw effective pitch is achieved, and (3) an automatic step scanning control which eliminates most of the mechanical deficiencies of the tangent drive by directly reading the tangent arm displacement.

A 7.2 keV spherical x-ray crystal backlighter for two-frame, two-color backlighting at Sandia's Z Pulsed Power Facility

NASA Astrophysics Data System (ADS)

Schollmeier, M. S.; Knapp, P. F.; Ampleford, D. J.; Harding, E. C.; Jennings, C. A.; Lamppa, D. C.; Loisel, G. P.; Martin, M. R.; Robertson, G. K.; Shores, J. E.; Smith, I. C.; Speas, C. S.; Weis, M. R.; Porter, J. L.; McBride, R. D.

2017-10-01

Many experiments on Sandia National Laboratories' Z Pulsed Power Facility—a 30 MA, 100 ns rise-time, pulsed-power driver—use a monochromatic quartz crystal backlighter system at 1.865 keV (Si He α ) or 6.151 keV (Mn He α ) x-ray energy to radiograph an imploding liner (cylindrical tube) or wire array z-pinch. The x-ray source is generated by the Z-Beamlet laser, which provides two 527-nm, 1 kJ, 1-ns laser pulses. Radiographs of imploding, thick-walled beryllium liners at convergence ratios CR above 15 [ C R = r i ( 0 ) / r i ( t ) ] using the 6.151-keV backlighter system were too opaque to identify the inner radius r i of the liner with high confidence, demonstrating the need for a higher-energy x-ray radiography system. Here, we present a 7.242 keV backlighter system using a Ge(335) spherical crystal with the Co He α resonance line. This system operates at a similar Bragg angle as the existing 1.865 keV and 6.151 keV backlighters, enhancing our capabilities for two-color, two-frame radiography without modifying the system integration at Z. The first data taken at Z include 6.2-keV and 7.2-keV two-color radiographs as well as radiographs of low-convergence (CR about 4-5), high-areal-density liner implosions.

X-ray imaging crystal spectrometer for extended X-ray sources

DOEpatents

Bitter, Manfred L.; Fraenkel, Ben; Gorman, James L.; Hill, Kenneth W.; Roquemore, A. Lane; Stodiek, Wolfgang; von Goeler, Schweickhard E.

2001-01-01

Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokomak fusion experiment to provide spatially and temporally resolved data on plasma parameters using the imaging properties for Bragg angles near 45. For a Bragg angle of 45.degree., the spherical crystal focuses a bundle of near parallel X-rays (the cross section of which is determined by the cross section of the crystal) from the plasma to a point on a detector, with parallel rays inclined to the main plain of diffraction focused to different points on the detector. Thus, it is possible to radially image the plasma X-ray emission in different wavelengths simultaneously with a single crystal.

High-energy e- /e+ spectrometer via coherent interaction in a bent crystal

NASA Astrophysics Data System (ADS)

Bagli, Enrico; Guidi, Vincenzo; Howard, Alexander

2018-01-01

We propose a novel spectrometer based on the crystal channeling effect capable of discriminating between positive and negative particles well beyond the TeV energy scale. The atomic order of a crystalline structure generates an electrostatic field built up by all the atoms in the crystals, which confines charged particle trajectories between neighbouring atomic planes. Through such an interaction in a tiny curved crystal, the same dynamical action on the highest energy particles as that of a huge superconducting magnet is achieved. Depending on the charge sign, points of equilibrium of the oscillatory motion under channeling lie between or on atomic planes for positive and negative particles, respectively, forcing positive particles to stably oscillate far from the planes, while negative ones repeatedly cross them. The different interaction rate with atomic planes causes a tremendous discrepancy between the deflection efficiency of positive and negative particles under channeling. We suggest the use of interactions between charged particles and oriented bent crystals as a novel non-cryogenic passive charge spectrometer to aid the search for dark matter in the Universe in satellite-borne experiment. The limited angular acceptance makes this technique particularly suited for directional local sources of energetic charged particles.

SPECTIX, a PETAL+ X-ray spectrometer: design, calibration and preliminary tests

NASA Astrophysics Data System (ADS)

Reverdin, C.; Bastiani, S.; Batani, D.; Brambrink, E.; Boutoux, G.; Duval, A.; Hulin, S.; Jakubowska, K.; Koenig, M.; Lantuéjoul-Thfoin, I.; Lecherbourg, L.; Szabo, C. I.; Vauzour, B.

2018-01-01

The present article describes the design, the calibration and preliminary tests of the X-ray transmission crystal spectrometer SPECTIX (Spectromètre PEtal à Cristaux en Transmission X) built in the framework of the PETAL (PETawatt Aquitaine Laser) project and located in the Laser MégaJoule (LMJ) facility [1,2]. SPECTIX aims at characterizing the hard x-ray Kα emission generated by the interaction of the PETAL ps ultra high-energy laser with a target. The broad spectral range covered by this spectrometer (7 to 150 keV) is achieved by using two measurement channels composed by two distinct crystals. Due to the harsh environment experienced by the spectrometer during a LMJ-PETAL shot, passive detection with image plates is used. Shielding has been dimensioned in order to protect the detector against PETAL shot products. It includes a magnetic dipole to remove electrons entering the spectrometer, a 20 mm thick tungsten frontal collimation and a 6 mm thick lead housing. The SPECTIX performances, including the shielding efficiency, have been tested during an experimental campain performed at the PICO 2000 laser facility at LULI. Improvements inferred from these tests are currently being implemented. Full commissioning of SPECTIX is planned on PETAL shots at the end of 2017.

Performance of the EBIT calorimeter spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Porter, Frederick Scott; Gygax, John; Kelley, Richard L.

The EBIT calorimeter spectrometer (ECS) is a new high-resolution, broadband x-ray spectrometer that has recently been installed at the Electron Beam Ion Trap Facility (EBIT) at the Lawrence Livermore National Laboratory. The ECS is an entirely new production class spectrometer that replaces the XRS/EBIT spectrometer that has been operating at EBIT since 2000. The ECS utilizes a 32-pixel x-ray calorimeter array from the XRS instrument on the Suzaku x-ray observatory. Eighteen of the pixels are optimized for the 0.1-10 keV band and yield 4.5 eV full width at half maximum energy resolution and 95% quantum efficiency at 6 keV. Inmore » addition, the ECS includes 14 detector pixels that are optimized for the high-energy band with a bandpass from 0.5 to over 100 keV with 34 eV resolution and 32% quantum efficiency at 60 keV. The ECS detector array is operated at 50 mK using a five stage cryogenic system that is entirely automated. The instrument takes data continuously for over 65 h with a 2.5 h recycle time. The ECS is a nondispersive, broadband, highly efficient spectrometer that is one of the prime instruments at the EBIT facility. The instrument is used for studies of absolute cross sections, charge exchange recombination, and x-ray emission from nonequilibrium plasmas, among other measurements in our laboratory astrophysics program.« less

A 7.2 keV spherical x-ray crystal backlighter for two-frame, two-color backlighting at Sandia’s Z Pulsed Power Facility

DOE PAGES

Schollmeier, M. S.; Knapp, P. F.; Ampleford, D. J.; ...

2017-10-10

Many experiments on Sandia National Laboratories’ Z Pulsed Power Facility—a 30 MA, 100 ns rise-time, pulsed-power driver—use a monochromatic quartz crystal backlighter system at 1.865 keV (Si He α) or 6.151 keV (Mn He α) x-ray energy to radiograph an imploding liner (cylindrical tube) or wire array z-pinch. The x-ray source is generated by the Z-Beamlet laser, which provides two 527-nm, 1 kJ, 1-ns laser pulses. Radiographs of imploding, thick-walled beryllium liners at convergence ratios C R above 15 [C R=r i(0)/r i(t)] using the 6.151-keV backlighter system were too opaque to identify the inner radius ri of the linermore » with high confidence, demonstrating the need for a higher-energy x-ray radiography system. Here, we present a 7.242 keV backlighter system using a Ge(335) spherical crystal with the Co He α resonance line. This system operates at a similar Bragg angle as the existing 1.865 keV and 6.151 keV backlighters, enhancing our capabilities for two-color, two-frame radiography without modifying the system integration at Z. The first data taken at Z include 6.2-keV and 7.2-keV two-color radiographs as well as radiographs of low-convergence (C R about 4-5), high-areal-density liner implosions.« less

A 7.2 keV spherical x-ray crystal backlighter for two-frame, two-color backlighting at Sandia’s Z Pulsed Power Facility

DOE Office of Scientific and Technical Information (OSTI.GOV)

Schollmeier, M. S.; Knapp, P. F.; Ampleford, D. J.

Many experiments on Sandia National Laboratories’ Z Pulsed Power Facility—a 30 MA, 100 ns rise-time, pulsed-power driver—use a monochromatic quartz crystal backlighter system at 1.865 keV (Si He α) or 6.151 keV (Mn He α) x-ray energy to radiograph an imploding liner (cylindrical tube) or wire array z-pinch. The x-ray source is generated by the Z-Beamlet laser, which provides two 527-nm, 1 kJ, 1-ns laser pulses. Radiographs of imploding, thick-walled beryllium liners at convergence ratios C R above 15 [C R=r i(0)/r i(t)] using the 6.151-keV backlighter system were too opaque to identify the inner radius ri of the linermore » with high confidence, demonstrating the need for a higher-energy x-ray radiography system. Here, we present a 7.242 keV backlighter system using a Ge(335) spherical crystal with the Co He α resonance line. This system operates at a similar Bragg angle as the existing 1.865 keV and 6.151 keV backlighters, enhancing our capabilities for two-color, two-frame radiography without modifying the system integration at Z. The first data taken at Z include 6.2-keV and 7.2-keV two-color radiographs as well as radiographs of low-convergence (C R about 4-5), high-areal-density liner implosions.« less

Hyper-filter-fluorescer spectrometer for x-rays above 120 keV

DOEpatents

Wang, Ching L.

1983-01-01

An apparatus utilizing filter-fluorescer combinations is provided to measure short bursts of high fluence x-rays above 120 keV energy, where there are no practical absorption edges available for conventional filter-fluorescer techniques. The absorption edge of the prefilter is chosen to be less than that of the fluorescer, i.e., E.sub.PRF E.sub.F. In this way, the response function is virtually zero between E.sub.PRF and E.sub.F and well defined and enhanced in an energy band of less than 1000 keV above the 120 keV energy.

X-ray spectrometer based on a bent diamond crystal for high repetition rate free-electron laser applications

DOE PAGES

Boesenberg, Ulrike; Samoylova, Liubov; Roth, Thomas; ...

2017-02-03

A precise spectral characterization of every single pulse is required in many x-ray free-electron laser (XFEL) experiments due to the fluctuating spectral content of self-amplified spontaneous emission (SASE) beams. Bent single-crystal spectrometers can provide sufficient spectral resolution to resolve the SASE spikes while also covering the full SASE bandwidth. To better withstand the high heat load induced by the 4.5 MHz repetition rate of pulses at the forthcoming European XFEL facility, a spectrometer based on single-crystal diamond has been developed. Here, we report a direct comparison of the diamond spectrometer with its Si counterpart in experiments performed at the Linacmore » Coherent Light Source.« less

New Observations of Soft X-ray (0.5-5 keV) Solar Spectra

NASA Astrophysics Data System (ADS)

Caspi, A.; Woods, T. N.; Mason, J. P.; Jones, A. R.; Warren, H. P.

2013-12-01

The solar corona is the brightest source of X-rays in the solar system, and the X-ray emission is highly variable on many time scales. However, the actual solar soft X-ray (SXR) (0.5-5 keV) spectrum is not well known, particularly during solar quiet periods, as, with few exceptions, this energy range has not been systematically studied in many years. Previous observations include high-resolution but very narrow-band spectra from crystal spectrometers (e.g., Yohkoh/BCS), or integrated broadband irradiances from photometers (e.g., GOES/XRS, TIMED/XPS, etc.) that lack detailed spectral information. In recent years, broadband measurements with moderate energy resolution (~0.5-0.7 keV FWHM) were made by SphinX on CORONAS-Photon and SAX on MESSENGER, although they did not extend to energies below ~1 keV. We present observations of solar SXR emission obtained using new instrumentation flown on recent SDO/EVE calibration rocket underflights. The photon-counting spectrometer, a commercial Amptek X123 with a silicon drift detector and an 8 μm Be window, measures the solar disk-integrated SXR emission from ~0.5 to >10 keV with ~0.15 keV FWHM resolution and 1 s cadence. A novel imager, a pinhole X-ray camera using a cooled frame-transfer CCD (15 μm pixel pitch), Ti/Al/C filter, and 5000 line/mm Au transmission grating, images the full Sun in multiple spectral orders from ~0.1 to ~5 nm with ~10 arcsec/pixel and ~0.01 nm/pixel spatial and spectral detector scales, respectively, and 10 s cadence. These instruments are prototypes for future CubeSat missions currently being developed. We present new results of solar observations on 04 October 2013 (NASA sounding rocket 36.290). We compare with previous results from 23 June 2012 (NASA sounding rocket 36.286), during which solar activity was low and no signal was observed above ~4 keV. We compare our spectral and imaging measurements with spectra and broadband irradiances from other instruments, including SDO/EVE, GOES/XRS, TIMED

A high-resolving-power x-ray spectrometer for the OMEGA EP Laser (invited)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nilson, P. M., E-mail: pnil@lle.rochester.edu; Ehrne, F.; Mileham, C.

A high-resolving-power x-ray spectrometer has been developed for the OMEGA EP Laser System based on a spherically bent Si [220] crystal with a radius of curvature of 330 mm and a Spectral Instruments (SI) 800 Series charge-coupled device. The instrument measures time-integrated x-ray emission spectra in the 7.97- to 8.11-keV range, centered on the Cu K{sub α1} line. To demonstrate the performance of the spectrometer under high-power conditions, K{sub α1,2} emission spectra were measured from Cu foils irradiated by the OMEGA EP laser with 100-J, 1-ps pulses at focused intensities above 10{sup 18} W/cm{sup 2}. The ultimate goal is tomore » couple the spectrometer to a picosecond x-ray streak camera and measure temperature-equilibration dynamics inside rapidly heated materials. The plan for these ultrafast streaked x-ray spectroscopy studies is discussed.« less

Development of a flat-field spectrometer with a wideband Ni/C multilayer grating in the 1–3.5 keV range

DOE Office of Scientific and Technical Information (OSTI.GOV)

Imazono, Takashi

2016-07-27

To develop a flat-field spectrometer with coverage of the 1–3.5 keV range, a wideband Ni/C multilayer grating was invented. The multilayer consists of two kinds of layer structures. One is a conventional periodic multilayer of thickness D{sub 1} = 5.6 nm, Ni thickness ratio to the multilayer period γ{sub 1} = 0.5 and the number of layers N{sub 1} = 79. Both the first and last layers are Ni. The other is a C/Ni bilayer of D{sub 2} = 8.4 nm, γ{sub 2} = 0.53 and N{sub 2} = 2. The first layer is C and then Ni. The aperiodicmore » multilayer from the topmost C/Ni bilayer was coated on a laminar-type grating having an effective grating constant of 1/2400 mm, groove depth of 2.8 nm, and duty ratio (land width/groove period) of 0.5. In a preliminary experiment, the diffraction efficiency was in excess of 0.8% in the energy range of 2.1-3.3 keV and the maximum of 5.4% at 3.1 keV at a constant angle of incidence of 88.54°, which is considerably higher than that of an Au-coated grating before deposition of the multilayer.« less

Calibration of the OHREX high-resolution imaging crystal spectrometer at the Livermore electron beam ion traps

NASA Astrophysics Data System (ADS)

Hell, N.; Beiersdorfer, P.; Magee, E. W.; Brown, G. V.

2016-11-01

We report the calibration of the Orion High-Resolution X-ray (OHREX) imaging crystal spectrometer at the EBIT-I electron beam ion trap at Livermore. Two such instruments, dubbed OHREX-1 and OHREX-2, are fielded for plasma diagnostics at the Orion laser facility in the United Kingdom. The OHREX spectrometer can simultaneously house two spherically bent crystals with a radius of curvature of r = 67.2 cm. The focusing properties of the spectrometer allow both for larger distance to the source due to the increase in collected light and for observation of extended sources. OHREX is designed to cover a 2.5°-3° spectral range at Bragg angles around 51.3°. The typically high resolving powers at these large Bragg angles are ideally suited for line shape diagnostics. For instance, the nominal resolving power of the instrument (>10 000) is much higher than the effective resolving power associated with the Doppler broadening due to the temperature of the trapped ions in EBIT-I. The effective resolving power is only around 3000 at typical EBIT-I conditions, which nevertheless is sufficient to set up and test the instrument's spectral characteristics. We have calibrated the spectral range for a number of crystals using well known reference lines in the first and second order and derived the ion temperatures from these lines. We have also made use of the 50 μm size of the EBIT-I source width to characterize the spatial focusing of the spectrometer.

Calibration of the OHREX high-resolution imaging crystal spectrometer at the Livermore electron beam ion traps

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hell, N.; Dr. Remeis-Sternwarte and ECAP, Universität Erlangen-Nürnberg, Bamberg 96049; Beiersdorfer, P.

2016-11-15

We report the calibration of the Orion High-Resolution X-ray (OHREX) imaging crystal spectrometer at the EBIT-I electron beam ion trap at Livermore. Two such instruments, dubbed OHREX-1 and OHREX-2, are fielded for plasma diagnostics at the Orion laser facility in the United Kingdom. The OHREX spectrometer can simultaneously house two spherically bent crystals with a radius of curvature of r = 67.2 cm. The focusing properties of the spectrometer allow both for larger distance to the source due to the increase in collected light and for observation of extended sources. OHREX is designed to cover a 2.5°–3° spectral range atmore » Bragg angles around 51.3°. The typically high resolving powers at these large Bragg angles are ideally suited for line shape diagnostics. For instance, the nominal resolving power of the instrument (>10 000) is much higher than the effective resolving power associated with the Doppler broadening due to the temperature of the trapped ions in EBIT-I. The effective resolving power is only around 3000 at typical EBIT-I conditions, which nevertheless is sufficient to set up and test the instrument’s spectral characteristics. We have calibrated the spectral range for a number of crystals using well known reference lines in the first and second order and derived the ion temperatures from these lines. We have also made use of the 50 μm size of the EBIT-I source width to characterize the spatial focusing of the spectrometer.« less

Design Study of an X-ray Crystal Spectrometer for the HANBIT Mirror Machine

NASA Astrophysics Data System (ADS)

Lee, S. G.; Hwang, S. M.; Bitter, M. L.

1997-11-01

X-ray crystal spectroscopy is expected to play a major role for the diagnostics of the reactor-like plasmas produced in future large tokamaks, such as KSTAR and ITER. However, it is also desirable to extend the observable spectral range to longer wavelengths (7-15 dotA), which is of interest for the diagnostics of plasmas with much lower electron densities (10^11-10^12 cm-3) and electron temperatures (100 - 200 eV) in other magnetic-confinement experiments, such as the HANBIT mirror machine. The construction of crystal spectrometers for this wavelength range and these plasma conditions is challenging because of the low X-ray emissivity and the fact that the low-energy X-rays are strongly attenuated by even very thin foils or windows. New types of detectors other than the presently used multi-wire proportional counters are therefore needed to obtain a high detection efficiency. In this paper, we present a design study for a vacuum spectrometer with a CCD array detector and detailed estimates of the instrument performance for the observation of spectra from O, Ne and Al ions.

Post-flare coronal arches observed with the SMM/XRP flat crystal spectrometer

NASA Technical Reports Server (NTRS)

Hick, Paul; Svestka, Zdenek; Smith, Kermit L.; Strong, Keith T.

1987-01-01

Postflare coronal arch observations made with the SMM Flat Crystal Spectrometer on January 20-23, 1985 are discussed. Results suggest that the arch revival following the dynamic flare of 23:50 UT on January 1 was of the type noted on November 6-8 and June 4, 1980 by the SMM Hard X-ray Imaging Spectrometer (HXIS). Activity different from that of the HXIS observations was found starting at about 23 UT on January 22, with no trigger of the revival being identified, and with the activity being restricted to the coronal regions (without any related disturbance in the chromosphere). The development of the arch enhancement in the corona was shown to be slower than is expected for a flare-associated revival.

Post-flare coronal arches observed with the SMM/XRP flat crystal spectrometer

NASA Astrophysics Data System (ADS)

Hick, Paul; Svestka, Zdenek; Smith, Kermit L.; Strong, Keith T.

1987-09-01

Postflare coronal arch observations made with the SMM Flat Crystal Spectrometer on January 20-23, 1985 are discussed. Results suggest that the arch revival following the dynamic flare of 23:50 UT on January 1 was of the type noted on November 6-8 and June 4, 1980 by the SMM Hard X-ray Imaging Spectrometer (HXIS). Activity different from that of the HXIS observations was found starting at about 23 UT on January 22, with no trigger of the revival being identified, and with the activity being restricted to the coronal regions (without any related disturbance in the chromosphere). The development of the arch enhancement in the corona was shown to be slower than is expected for a flare-associated revival.

Experimental results from an X-ray imaging crystal spectrometer utilizing multi-wire proportional counter for KSTAR

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lee, S. G., E-mail: sglee@nfri.re.kr; Kim, Y. S.; Yoo, J. W.

2016-11-15

The inconsistency of the first experimental results from the X-ray imaging crystal spectrometer for the Korea Superconducting Tokamak Advanced Research device utilizing a multi-wire proportional counter (MWPC) is clarified after improving the photon-count rate of the data acquisition system for the MWPC and ground loop isolator for the whole spectrometer system. The improved MWPC is successfully applied to pure Ohmic plasmas as well as plasmas with high confinement modes.

Systematic search for spherical crystal X-ray microscopes matching 1–25 keV spectral line sources

DOE PAGES

Schollmeier, Marius S.; Loisel, Guillaume P.

2016-12-29

Spherical-crystal microscopes are used as high-resolution imaging devices for monochromatic x-ray radiography or for imaging the source itself. Crystals and Miller indices (hkl) have to be matched such that the resulting lattice spacing d is close to half the spectral wavelength used for imaging, to fulfill the Bragg equation with a Bragg angle near 90° which reduces astigmatism. Only a few suitable crystal and spectral-line combinations have been identified for applications in the literature, suggesting that x-ray imaging using spherical crystals is constrained to a few chance matches. In this paper, after performing a systematic, automated search over more thanmore » 9 × 10 6 possible combinations for x-ray energies between 1 and 25 keV, for six crystals with arbitrary Miller-index combinations hkl between 0 and 20, we show that a matching, efficient crystal and spectral-line pair can be found for almost every He α or K α x-ray source for the elements Ne to Sn. Finally, using the data presented here it should be possible to find a suitable imaging combination using an x-ray source that is specifically selected for a particular purpose, instead of relying on the limited number of existing crystal imaging systems that have been identified to date.« less

A von Hamos x-ray spectrometer based on a segmented-type diffraction crystal for single-shot x-ray emission spectroscopy and time-resolved resonant inelastic x-ray scattering studies

DOE Office of Scientific and Technical Information (OSTI.GOV)

Szlachetko, J.; Institute of Physics, Jan Kochanowski University, 25-406 Kielce; Nachtegaal, M.

2012-10-15

We report on the design and performance of a wavelength-dispersive type spectrometer based on the von Hamos geometry. The spectrometer is equipped with a segmented-type crystal for x-ray diffraction and provides an energy resolution in the order of 0.25 eV and 1 eV over an energy range of 8000 eV-9600 eV. The use of a segmented crystal results in a simple and straightforward crystal preparation that allows to preserve the spectrometer resolution and spectrometer efficiency. Application of the spectrometer for time-resolved resonant inelastic x-ray scattering and single-shot x-ray emission spectroscopy is demonstrated.

Lineshape spectroscopy with a very high resolution, very high signal-to-noise crystal spectrometer

DOE PAGES

Beiersdorfer, P.; Magee, E. W.; Brown, G. V.; ...

2016-06-06

Here, we have developed a high-resolution x-ray spectrometer for measuring the shapes of spectral lines produced from laser-irradiated targets on the Orion laser facility. The instrument utilizes a spherically bent crystal geometry to spatially focus and spectrally analyze photons from foil or microdot targets. The high photon collection efficiency resulting from its imaging properties allows the instrument to be mounted outside the Orion chamber, where it is far less sensitive to particles, hard x-rays, or electromagnetic pulses than instruments housed close to the target chamber center in ten-inch manipulators. Moreover, Bragg angles above 50° are possible, which provide greatly improvedmore » spectral resolution compared to radially viewing, near grazing-incidence crystal spectrometers. These properties make the new instrument an ideal lineshape diagnostic for determining plasma temperature and density. We describe its calibration on the Livermore electron beam ion trap facility and present spectral data of the K-shell emission from highly charged sulfur produced by long-pulse as well as short-pulse beams on the Orion laser in the United Kingdom.« less

Lineshape spectroscopy with a very high resolution, very high signal-to-noise crystal spectrometer

NASA Astrophysics Data System (ADS)

Beiersdorfer, P.; Magee, E. W.; Brown, G. V.; Chen, H.; Emig, J.; Hell, N.; Bitter, M.; Hill, K. W.; Allan, P.; Brown, C. R. D.; Hill, M. P.; Hoarty, D. J.; Hobbs, L. M. R.; James, S. F.

2016-06-01

We have developed a high-resolution x-ray spectrometer for measuring the shapes of spectral lines produced from laser-irradiated targets on the Orion laser facility. The instrument utilizes a spherically bent crystal geometry to spatially focus and spectrally analyze photons from foil or microdot targets. The high photon collection efficiency resulting from its imaging properties allows the instrument to be mounted outside the Orion chamber, where it is far less sensitive to particles, hard x-rays, or electromagnetic pulses than instruments housed close to the target chamber center in ten-inch manipulators. Moreover, Bragg angles above 50° are possible, which provide greatly improved spectral resolution compared to radially viewing, near grazing-incidence crystal spectrometers. These properties make the new instrument an ideal lineshape diagnostic for determining plasma temperature and density. We describe its calibration on the Livermore electron beam ion trap facility and present spectral data of the K-shell emission from highly charged sulfur produced by long-pulse as well as short-pulse beams on the Orion laser in the United Kingdom.

Lineshape spectroscopy with a very high resolution, very high signal-to-noise crystal spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Beiersdorfer, P.; Magee, E. W.; Brown, G. V.

2016-06-15

We have developed a high-resolution x-ray spectrometer for measuring the shapes of spectral lines produced from laser-irradiated targets on the Orion laser facility. The instrument utilizes a spherically bent crystal geometry to spatially focus and spectrally analyze photons from foil or microdot targets. The high photon collection efficiency resulting from its imaging properties allows the instrument to be mounted outside the Orion chamber, where it is far less sensitive to particles, hard x-rays, or electromagnetic pulses than instruments housed close to the target chamber center in ten-inch manipulators. Moreover, Bragg angles above 50° are possible, which provide greatly improved spectralmore » resolution compared to radially viewing, near grazing-incidence crystal spectrometers. These properties make the new instrument an ideal lineshape diagnostic for determining plasma temperature and density. We describe its calibration on the Livermore electron beam ion trap facility and present spectral data of the K-shell emission from highly charged sulfur produced by long-pulse as well as short-pulse beams on the Orion laser in the United Kingdom.« less

The EBIT Calorimeter Spectrometer: A New, Permanent User Facility at the LLNL EBIT

NASA Technical Reports Server (NTRS)

Porter, S.

2007-01-01

The EBIT Calorimeter Spectrometer (ECS) has recently been completed and is currently being installed at the EBIT facility at the Lawrence Livermore National Laboratory. The ECS will replace the smaller XRS/EBIT spectrometer that has been in almost continuous operation since 2000. The XRS/EBIT was based on a spare laboratory cryostat and an engineering model detector system from the Suzaku/XRS observatory. The new ECS spectrometer was built from the ground up to be a low maintenance, high performance microcalorimeter spectrometer with 4 eV resolution at 6 keV, 32 detector channels, 10 us event timing, and capable of uninterrupted acquisition sessions of over 70 hours at 50 mK. The XRSIEBIT program has been extremely successful, producing over two-dozen refereed publications on topics such as laboratory astrophysics, atomic physics, nuclear physics, and calibration of the spectrometers for the National Ignition Facility, with many more publications in preparation. The ECS spectrometer will continue this work into the future with improved spectral resolution, integration times, and ease-of-use. We designed the ECS instrument with TES detectors in mind by using the same highly successful magnetic shielding as our laboratory TES cryostats. This design will lead to a future TES instrument at the LLNL EBIT. This proposed future instrument would include a hybrid detector system with 0.8 eV resolution in the band from 0.1-1.0 keV, 2 eV from 0.1-10 keV, and 30 eV from 0.5-100 keV, with high quantum efficiency in each band. Here we discuss the legacy of the XRS/EBIT program, the performance of the new ECS spectrometer, and plans for a future TES spectrometer.

Correction: Spectroscopic characteristics of the OSIRIS near-backscattering crystal analyser spectrometer on the ISIS pulsed neutron source.

PubMed

Telling, Mark T F; Campbell, Stuart I; Engberg, Dennis; Martín Y Marero, David; Andersen, Ken H

2016-03-21

Correction for 'Spectroscopic characteristics of the OSIRIS near-backscattering crystal analyser spectrometer on the ISIS pulsed neutron source' by Mark T. F. Telling et al., Phys. Chem. Chem. Phys., 2005, 7, 1255-1261.

On the evaluation of the absolute photon energy of Cu Kα, β lines using 4-crystal X -ray spectrometer

NASA Astrophysics Data System (ADS)

Ito, Yoshiaki; Tochio, Tatsunori; Fukushima, Sei

A 4-crystal X-ray spectrometer was designed based on a 2-crystal X-ray spectrometer to be able to perform the absolute measurement of Bragg angle. This basic thought based on 2 crystals dates back to the times to A.Compton etc.. Because a distortion to give the crystal by the adhesive when a crystal was glued, greatly affected the X-rays profile, we changed it to the channel cut crystal without a free distortion as for having made each crystal of 2-crystal a channel cut. The influence of the foot in the spectral profile is more suppressed because four times of reflections reflect it. It is a high resolution so as not to need to consider instrumental function by the reflection degree that a specific atomic analysis can be executed with the chemical state which it is possible for making the placement of the 4-crystal (+, +) setting. This type of spectrum device is first time in the world. Because the absolute measurement of 2 θ angles is enabled by (+,-) and (+, +) setting from the center of gravity position of the rocking curve and the center of gravity position of the X-rays spectrum, we may measure the absolute value of the X-ray photon energy. Because we evaluated the energy of the Cu Kα , β lines, we report it. We acknowledge financial support for the measurements of a part of the data by the REXDAB collaboration that was initiated within the International Fundamental Parameter Initiative.

Hard x-ray broad band Laue lenses (80-600 keV): building methods and performances

NASA Astrophysics Data System (ADS)

Virgilli, E.; Frontera, F.; Rosati, P.; Liccardo, V.; Squerzanti, S.; Carassiti, V.; Caroli, E.; Auricchio, N.; Stephen, J. B.

2015-09-01

We present the status of the LAUE project devoted to develop a technology for building a 20 meter long focal length Laue lens for hard X-/soft gamma-ray astronomy (80-600 keV). The Laue lens is composed of bent crystals of Gallium Arsenide (GaAs, 220) and Germanium (Ge, 111), and, for the first time, the focusing property of bent crystals has been exploited for this field of applications. We show the preliminary results concerning the adhesive employed to fix the crystal tiles over the lens support, the positioning accuracy obtained and possible further improvements. The Laue lens petal that will be completed in a few months has a pass band of 80-300 keV and is a fraction of an entire Laue lens capable of focusing x-rays up to 600 keV, possibly extendable down to ~20-30 keV with suitable low absorption crystal materials and focal length. The final goal is to develop a focusing optics that can improve the sensitivity over current telescopes in this energy band by 2 orders of magnitude.

Experimental Determination of the HPGe Spectrometer Efficiency Calibration Curves for Various Sample Geometry for Gamma Energy from 50 keV to 2000 keV

NASA Astrophysics Data System (ADS)

Saat, Ahmad; Hamzah, Zaini; Yusop, Mohammad Fariz; Zainal, Muhd Amiruddin

2010-07-01

Detection efficiency of a gamma-ray spectrometry system is dependent upon among others, energy, sample and detector geometry, volume and density of the samples. In the present study the efficiency calibration curves of newly acquired (August 2008) HPGe gamma-ray spectrometry system was carried out for four sample container geometries, namely Marinelli beaker, disc, cylindrical beaker and vial, normally used for activity determination of gamma-ray from environmental samples. Calibration standards were prepared by using known amount of analytical grade uranium trioxide ore, homogenized in plain flour into the respective containers. The ore produces gamma-rays of energy ranging from 53 keV to 1001 keV. Analytical grade potassium chloride were prepared to determine detection efficiency of 1460 keV gamma-ray emitted by potassium isotope K-40. Plots of detection efficiency against gamma-ray energy for the four sample geometries were found to fit smoothly to a general form of ɛ = AΕa+BΕb, where ɛ is efficiency, Ε is energy in keV, A, B, a and b are constants that are dependent on the sample geometries. All calibration curves showed the presence of a "knee" at about 180 keV. Comparison between the four geometries showed that the efficiency of Marinelli beaker is higher than cylindrical beaker and vial, while cylindrical disk showed the lowest.

Spatial resolution of a spherical x-ray crystal spectrometer at various magnifications

DOE PAGES

Gao, Lan; Hill, K. W.; Bitter, M.; ...

2016-08-23

Here, a high spatial resolution of a few μm is often required for probing small-scale high-energy-density plasmas using high resolution x-ray imaging spectroscopy. This resolution can be achieved by adjusting system magnification to overcome the inherent limitation of the detector pixel size. Laboratory experiments on investigating the relation between spatial resolution and system magnification for a spherical crystal spectrometer are presented. Tungsten Lβ 2 rays from a tungsten-target micro-focus x-ray tube were diffracted by a Ge 440 crystal, which was spherically bent to a radius of 223 mm, and imaged onto an x-ray CCD with 13-μm pixel size. The source-to-crystalmore » (p) and crystal-to-detector (q) distances were varied to produce spatial magnifications ( M = q/p) ranging from 2 to 10. The inferred instrumental spatial width reduces with increasing system magnification M. However, the experimental measurement at each M is larger than the theoretical value of pixel size divided by M. Future work will focus on investigating possible broadening mechanisms that limit the spatial resolution.« less

THE X-RAY LINE FEATURE AT 3.5 KeV IN GALAXY CLUSTER SPECTRA

DOE Office of Scientific and Technical Information (OSTI.GOV)

Phillips, K. J. H.; Sylwester, B.; Sylwester, J., E-mail: kennethjhphillips@yahoo.com, E-mail: bs@cbk.pan.wroc.pl, E-mail: js@cbk.pan.wroc.pl

2015-08-10

Recent work by Bulbul et al. and Boyarsky et al. has suggested that a line feature at ∼3.5 keV in the X-ray spectra of galaxy clusters and individual galaxies seen with XMM-Newton is due to the decay of sterile neutrinos, a dark matter candidate. This identification has been criticized by Jeltema and Profumo on the grounds that model spectra suggest that atomic transitions in helium-like potassium (K xviii) and chlorine (Cl xvi) are more likely to be the emitters. Here it is pointed out that the K xviii lines have been observed in numerous solar flare spectra at high spectralmore » resolution with the RESIK crystal spectrometer and also appear in Chandra HETG spectra of the coronally active star σ Gem. In addition, the solar flare spectra at least indicate a mean coronal potassium abundance, which is a factor between 9 and 11 higher than the solar photospheric abundance. This fact, together with the low statistical quality of the XMM-Newton spectra, completely account for the ∼3.5 keV feature and there is therefore no need to invoke a sterile neutrino interpretation of the observed line feature at ∼3.5 keV.« less

The hard X-ray burst spectrometer on the solar maximum mission

NASA Technical Reports Server (NTRS)

Orwig, L. E.; Frost, K. J.; Dennis, B. R.

1979-01-01

The primary scientific objective of the spectrometer is to provide a greater understanding of the role of energetic electrons in solar flares. This will be achieved by observations of high energy X-rays in the energy range from 20 to 200 keV with time resolution of 0.128s on a continuous basis and as short as 1 ms for limited intervals. The X-ray detector is an actively shielded CsI(Na) crystal with a thickness of 0.635 cm and a sensitive area of 71 sq cm. In the first year after launch, it is expected that approximately 1000 flares above the sensitivity threshold of 0.2 photons/(sq cm s) lasting for one second, will be detected.

A possible line feature at 73 keV from the Crab Nebula

NASA Technical Reports Server (NTRS)

Ling, J. C.; Mahoney, W. A.; Willett, J. B.; Jacobson, A. S.

1979-01-01

Evidence is reported for a possible line feature at 73 keV from the Crab Nebula. The experiment was conducted with a balloon-borne high-resolution gamma-ray spectrometer on June 10, 1974, over Palestine, Texas. The intensity and the width of the line derived from the fitting of these data are approximately 0.0038 photon per (sq cm-sec) and less than 4.9 keV FWHM, respectively. The line is superposed on a power-law continuum of 11.2 E to the -2.16 photons per (sq cm-keV) in the energy range from 53 to 300 keV, which is consistent with other measurements of the Crab Nebula spectrum.

Applications of Silicon-on-Insulator Photonic Crystal Structures in Miniature Spectrometer Designs

NASA Astrophysics Data System (ADS)

Gao, Boshen

Optical spectroscopy is one of the most important fundamental scientific techniques. It has been widely adopted in physics, chemistry, biology, medicine and many other research fields. However, the size and weight of a spectrometer as well as the difficulty to align and maintain it have long limited spectroscopy to be a laboratory-only procedure. With the recent advancement in semiconductor electronics and photonics, miniaturized spectrometers have been introduced to complete many tasks in daily life where mobility and portability are necessary. This thesis focuses on the study of several photonic crystal (PC) nano-structures potentially suitable for miniaturized on-chip spectrometer designs. Chapter 1 briefly introduces the concept of PCs and their band structures. By analyzing the band structure, the origin of the superprism effect is explained. Defect-based PC nano-cavities are also discussed, as well as a type of coupled cavity waveguides (CCW) composed of PC nano-cavities. Chapter 2 is devoted to the optimization of a flat-band superprism structure for spectroscopy application using numerical simulations. Chapter 3 reports a fabricated broad-band superprism and the experimental characterization of its wavelength resolving performance. In chapter 4, the idea of composing a miniature spectrometer based on a single tunable PC nano-cavity is proposed. The rest of this chapter discusses the experimental study of this design. Chapter 5 examines the slow-light performance of a CCW and discusses its potential application in slow-light interferometry. Chapter 6 serves as a conclusion of this thesis and proposes directions for possible future work to follow up.

Objectives and layout of a high-resolution x-ray imaging crystal spectrometer for the large helical device.

PubMed

Bitter, M; Hill, K; Gates, D; Monticello, D; Neilson, H; Reiman, A; Roquemore, A L; Morita, S; Goto, M; Yamada, H; Rice, J E

2010-10-01

A high-resolution x-ray imaging crystal spectrometer, whose concept was tested on NSTX and Alcator C-Mod, is being designed for the large helical device (LHD). This instrument will record spatially resolved spectra of helium-like Ar(16+) and will provide ion temperature profiles with spatial and temporal resolutions of <2 cm and ≥10 ms, respectively. The spectrometer layout and instrumental features are largely determined by the magnetic field structure of LHD. The stellarator equilibrium reconstruction codes, STELLOPT and PIES, will be used for the tomographic inversion of the spectral data.

The nonlinear light output of NaI(Tl) detectors in the Modular Total Absorption Spectrometer

DOE PAGES

Rasco, B. C.; Fijałkowska, A.; Karny, M.; ...

2015-04-08

New detector array, the Modular Total Absorption Spectrometer (MTAS),was commissioned at the Holifield Radioactive Ion Beam Facility (HRIBF) at Oak Ridge National Lab(ORNL).Total absorption gamma spectra measured with MTAS are expected to improve beta-feeding patterns and beta strength functions in fission products.MTAS is constructed out of hexagonal NaI(Tl) detectors with a unique central module surrounded by 18 identical crystals assembled in three rings. The total NaI(Tl) mass of MTAS is over1000 kg.The response of the central and other 18 MTAS modules to -radiation was simulated using the GEANT4 tool kit modified to analyze the nonlinear light output of NaI(Tl).A detailedmore » description oftheGEANT4modifications madeisdiscussed.SimulatedenergyresolutionofMTAS modules is found to agree well with the measurements for single transitions of 662keV (137Cs) with 8.2% full width half maximum (FWHM),835keV (54Mn) with FWHM of 7.5% FWHM, and 1115keV (65Zn) with FWHM of 6.5%.Simulations of single and multiple -rays from 60Co are also discussed.« less

Use of CLYC spectrometer in counter-terrorism applications

NASA Astrophysics Data System (ADS)

Ing, H.; Smith, M. B.; Koslowsky, M. R.; Andrews, H. R.

2015-05-01

A new scintillator crystal, now known as CLYC (Cs2LiYCl6:Ce), has been under development for over 15 years (1). It was primarily of interest for radiation detection applications because of its good energy resolution for gamma rays (< 4% for 662 keV gamma rays) and its capability for detection of thermal neutrons. The pulse shapes of the signals from the two radiations are different, which allow them to be separated electronically, permitting simultaneous detection of gamma rays and neutrons. The crystal is now commercially available. Early investigations of the neutron response by the current authors (2) revealed that CLYC also responds to fast neutrons. In fact, the good energy resolution of the response under monoenergetic neutron irradiations showed that CLYC was an excellent high-energy neutron spectrometer. This discovery has great impact on the field of neutron spectroscopy, which has numerous, although often specialized, applications. This presentation focuses on applications in counter-terrorism scenarios where neutrons may be involved. The relative importance of the fast neutron response of CLYC, compared to the thermal and gamma-ray response, will be discussed for these scenarios.

A neutron spectrometer for studying giant resonances with (p,n) reactions in inverse kinematics

NASA Astrophysics Data System (ADS)

Stuhl, L.; Krasznahorkay, A.; Csatlós, M.; Algora, A.; Gulyás, J.; Kalinka, G.; Timár, J.; Kalantar-Nayestanaki, N.; Rigollet, C.; Bagchi, S.; Najafi, M. A.

2014-02-01

A neutron spectrometer, the European Low-Energy Neutron Spectrometer (ELENS), has been constructed to study exotic nuclei in inverse-kinematics experiments. The spectrometer, which consists of plastic scintillator bars, can be operated in the neutron energy range of 100 keV-10 MeV. The neutron energy is determined using the time-of-flight technique, while the position of the neutron detection is deduced from the time-difference information from photomultipliers attached to both ends of each bar. A novel wrapping method has been developed for the plastic scintillators. The array has a larger than 25% detection efficiency for neutrons of approximately 500 keV in kinetic energy and an angular resolution of less than 1°. Details of the design, construction and experimental tests of the spectrometer will be presented.

Objectives and Layout of a High-Resolution X-ray Imaging Crystal Spectrometer for the Large Helical Device (LHD)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bitter, M; Gates, D; Monticello, D

A high-resolution X-ray imaging crystal spectrometer, whose concept was tested on NSTX and Alcator C-Mod, is being designed for LHD. This instrument will record spatially resolved spectra of helium-like Ar16+ and provide ion temperature profiles with spatial and temporal resolutions of < 2 cm and ≥ 10 ms. The stellarator equilibrium reconstruction codes, STELLOPT and PIES, will be used for the tomographic inversion of the spectral data. The spectrometer layout and instrumental features are largely determined by the magnetic field structure of LHD.

Photon Throughput Calculations for a Spherical Crystal Spectrometer

NASA Astrophysics Data System (ADS)

Gilman, C. J.; Bitter, M.; Delgado-Aparicio, L.; Efthimion, P. C.; Hill, K.; Kraus, B.; Gao, L.; Pablant, N.

2017-10-01

X-ray imaging crystal spectrometers of the type described in Refs. have become a standard diagnostic for Doppler measurements of profiles of the ion temperature and the plasma flow velocities in magnetically confined, hot fusion plasmas. These instruments have by now been implemented on major tokamak and stellarator experiments in Korea, China, Japan, and Germany and are currently also being designed by PPPL for ITER. A still missing part in the present data analysis is an efficient code for photon throughput calculations to evaluate the chord-integrated spectral data. The existing ray tracing codes cannot be used for a data analysis between shots, since they require extensive and time consuming numerical calculations. Here, we present a detailed analysis of the geometrical properties of the ray pattern. This method allows us to minimize the extent of numerical calculations and to create a more efficient code. This work was performed under the auspices of the U.S. Department of Energy by Princeton Plasma Physics Laboratory under contract DE-AC02-09CH11466.

Crystals for stellar spectrometers

NASA Technical Reports Server (NTRS)

Alexandropoulos, N. G.; Cohen, G. G.

1974-01-01

Crystal evaluation as it applies to instrumentation employed in X-ray astronomy is reviewed, and some solutions are offered to problems that are commonly encountered. A general approach for selecting the most appropriate crystals for a given problem is also suggested. The energy dependence of the diffraction properties of (002) PET, (111) Ge, (101) ADP, (101) KAP, and (001) RAP are reported.

One-shot spectrometer for several elements using an integrated conical crystal analyzer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Morishita, Kohei; Nakajima, Kazuo; Hayashi, Kouichi

Time-resolved x-ray spectrometry using an ultrastrong x-ray source such as an x-ray free electron laser is one of the new trends in the field of x-ray physics. To achieve such time-resolved measurement, the development of an one-shot spectrometer with a wide wavelength range, high efficiency, and good energy resolution is an essential prerequisite. Here we developed an integrated conical Ge crystal analyzer consisting of several conical rings, which were connected using spline surfaces to form a single body using our previously developed hot deformation technique, which can form a Si or Ge wafer into an arbitrary and accurate shape. Wemore » simultaneously focused several characteristic lines from an alloy sample onto different positions on a small x-ray charge-coupled device with very high image brightness (gain relative to planar analyzer: 100) and a good spatial resolution of 9-13 eV. The small radius of curvature of the crystal (28-50 mm) enabled us to realize a very short sample-detector distance of 214.4 mm. The present result shows the possibility of realizing a new focusing x-ray crystal spectrograph that can control the focal position as desired.« less

High Resolution, Non-Dispersive X-Ray Calorimeter Spectrometers on EBITs and Orbiting Observatories

NASA Technical Reports Server (NTRS)

Porter, Frederick S.

2010-01-01

X-ray spectroscopy is the primary tool for performing atomic physics with Electron beam ion trap (EBITs). X-ray instruments have generally fallen into two general categories, 1) dispersive instruments with very high spectral resolving powers but limited spectral range, limited count rates, and require an entrance slit, generally, for EBITs, defined by the electron beam itself, and 2) non-dispersive solid-state detectors with much lower spectral resolving powers but that have a broad dynamic range, high count rate ability and do not require a slit. Both of these approaches have compromises that limit the type and efficiency of measurements that can be performed. In 1984 NASA initiated a program to produce a non-dispersive instrument with high spectral resolving power for x-ray astrophysics based on the cryogenic x-ray calorimeter. This program produced the XRS non-dispersive spectrometers on the Astro-E, Astro-E2 (Suzaku) orbiting observatories, the SXS instrument on the Astro-H observatory, and the planned XMS instrument on the International X-ray Observatory. Complimenting these spaceflight programs, a permanent high-resolution x-ray calorimeter spectrometer, the XRS/EBIT, was installed on the LLNL EBIT in 2000. This unique instrument was upgraded to a spectral resolving power of 1000 at 6 keV in 2003 and replaced by a nearly autonomous production-class spectrometer, the EBIT Calorimeter Spectrometer (ECS), in 2007. The ECS spectrometer has a simultaneous bandpass from 0.07 to over 100 keV with a spectral resolving power of 1300 at 6 keV with unit quantum efficiency, and 1900 at 60 keV with a quantum efficiency of 30%. X-ray calorimeters are event based, single photon spectrometers with event time tagging to better than 10 us. We are currently developing a follow-on instrument based on a newer generation of x-ray calorimeters with a spectral resolving power of 3000 at 6 keV, and improved timing and measurement cadence. The unique capabilities of the x

Multichannel Spectrometer of Time Distribution

NASA Astrophysics Data System (ADS)

Akindinova, E. V.; Babenko, A. G.; Vakhtel, V. M.; Evseev, N. A.; Rabotkin, V. A.; Kharitonova, D. D.

2015-06-01

For research and control of characteristics of radiation fluxes, radioactive sources in particular, for example, in paper [1], a spectrometer and methods of data measurement and processing based on the multichannel counter of time intervals of accident events appearance (impulses of particle detector) MC-2A (SPC "ASPECT") were created. The spectrometer has four independent channels of registration of time intervals of impulses appearance and correspondent amplitude and spectrometric channels for control along the energy spectra of the operation stationarity of paths of each of the channels from the detector to the amplifier. The registration of alpha-radiation is carried out by the semiconductor detectors with energy resolution of 16-30 keV. Using a spectrometer there have been taken measurements of oscillations of alpha-radiation 239-Pu flux intensity with a subsequent autocorrelative statistical analysis of the time series of readings.

OZSPEC-2: an improved broadband high-resolution elliptical crystal x-ray spectrometer for high-energy density physics experiments (invited).

PubMed

Heeter, R F; Anderson, S G; Booth, R; Brown, G V; Emig, J; Fulkerson, S; McCarville, T; Norman, D; Schneider, M B; Young, B K F

2008-10-01

A novel time, space, and energy-resolved x-ray spectrometer has been developed which produces, in a single snapshot, a broadband and relatively calibrated spectrum of the x-ray emission from a high-energy density laboratory plasma. The opacity zipper spectrometer (OZSPEC-1) records a nearly continuous spectrum for x-ray energies from 240 to 5800 eV in a single shot. The second-generation OZSPEC-2, detailed in this work, records fully continuous spectra on a single shot from any two of these three bands: 270-650, 660-1580, and 1960-4720 eV. These instruments thus record thermal and line radiation from a wide range of plasmas. These instruments' single-shot bandwidth is unmatched in a time-gated spectrometer; conversely, other broadband instruments are either time-integrated (using crystals or gratings), lack spectral resolution (diode arrays), or cover a lower energy band (gratings). The OZSPECs are based on the zipper detector, a large-format (100x35 mm) gated microchannel plate detector, with spectra dispersed along the 100 mm dimension. OZSPEC-1 and -2 both use elliptically bent crystals of OHM, RAP, and/or PET. Individual spectra are gated in 100 ps. OZSPEC-2 provides one-dimensional spatial imaging with 30-50 microm resolution over a 1500 microm field of view at the source. The elliptical crystal design yields broad spectral coverage with resolution E/DeltaE>500, strong rejection of hard x-ray backgrounds, and negligible source broadening for extended sources. Near-term applications include plasma opacity measurements, detailed spectra of inertial fusion Hohlraums, and laboratory astrophysics experiments.

Wavelength calibration of x-ray imaging crystal spectrometer on Joint Texas Experimental Tokamak

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yan, W.; Chen, Z. Y., E-mail: zychen@hust.edu.cn; Jin, W.

2014-11-15

The wavelength calibration of x-ray imaging crystal spectrometer is a key issue for the measurements of plasma rotation. For the lack of available standard radiation source near 3.95 Å and there is no other diagnostics to measure the core rotation for inter-calibration, an indirect method by using tokamak plasma itself has been applied on joint Texas experimental tokamak. It is found that the core toroidal rotation velocity is not zero during locked mode phase. This is consistent with the observation of small oscillations on soft x-ray signals and electron cyclotron emission during locked-mode phase.

High-resolution x-ray spectroscopy with the EBIT Calorimeter Spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Porter, F. Scott; Adams, Joseph S.; Kelley, Richard L.

The EBIT Calorimeter Spectrometer (ECS) is a production-class 36 pixel x-ray calorimeter spectrometer that has been continuously operating at the Electron Beam Ion Trap (EBIT) facility at Lawrence Livermore National Laboratory for almost 2 years. The ECS was designed to be a long-lifetime, turn-key spectrometer that couples high performance with ease of operation and minimal operator intervention. To this end, a variant of the Suzaku/XRS spaceflight detector system has been coupled to a low-maintenance cryogenic system consisting of a long-lifetime liquid He cryostat, and a closed cycle, {sup 3}He pre-cooled adiabatic demagnetization refrigerator. The ECS operates for almost 3 weeksmore » between cryogenic servicing and the ADR operates at 0.05 K for more than 60 hours between automatic recycles under software control. Half of the ECS semiconductor detector array is populated with mid-band pixels that have a resolution of 4.5 eV FWHM, a bandpass from 0.05-12 keV, and a quantum efficiency of 95% at 6 keV. The other half of the array has thick HgTe absorbers that have a bandpass from 0.3 to over 100 keV, an energy resolution of 33 eV FWHM, and a quantum efficiency of 32% at 60 keV. In addition, the ECS uses a real-time, autonomous, data collection and analysis system developed for the Suzaku/XRS instrument and implemented in off-the-shelf hardware for the ECS. Here we will discuss the performance of the ECS instrument and its implementation as a turnkey cryogenic detector system.« less

A practical superconducting-microcalorimeter X-ray spectrometer for beamline and laboratory science

DOE PAGES

Doriese, W. B.; Abbamonte, P.; Alpert, B. K.; ...

2017-05-01

We describe a series of microcalorimeter X-ray spectrometers designed for a broad suite of measurement applications. The chief advantage of this type of spectrometer is that it can be orders of magnitude more efficient at collecting X-rays than more traditional high-resolution spectrometers that rely on wavelength-dispersive techniques. This advantage is most useful in applications that are traditionally photon-starved and/or involve radiation-sensitive samples. Each energy-dispersive spectrometer is built around an array of several hundred transition-edge sensors (TESs). TESs are superconducting thin films that are biased into their superconducting-to-normal-metal transitions. The spectrometers share a common readout architecture and many design elements, suchmore » as a compact, 65 mK detector package, 8-column time-division-multiplexed superconducting quantum-interference device readout, and a liquid-cryogen-free cryogenic system that is a two-stage adiabatic-demagnetization refrigerator backed by a pulse-tube cryocooler. We have adapted this flexible architecture to mate to a variety of sample chambers and measurement systems that encompass a range of observing geometries. There are two different types of TES pixels employed. The first, designed for X-ray energies below 10 keV, has a best demonstrated energy resolution of 2.1 eV (full-width-at-half-maximum or FWHM) at 5.9 keV. The second, designed for X-ray energies below 2 keV, has a best demonstrated resolution of 1.0 eV (FWHM) at 500 eV. Our team has now deployed seven of these X-ray spectrometers to a variety of light sources, accelerator facilities, and laboratory-scale experiments; these seven spectrometers have already performed measurements related to their applications. Another five of these spectrometers will come online in the near future. We have applied our TES spectrometers to the following measurement applications: synchrotron-based absorption and emission spectroscopy and energy

A practical superconducting-microcalorimeter X-ray spectrometer for beamline and laboratory science

DOE Office of Scientific and Technical Information (OSTI.GOV)

Doriese, W. B.; Abbamonte, P.; Alpert, B. K.

We describe a series of microcalorimeter X-ray spectrometers designed for a broad suite of measurement applications. The chief advantage of this type of spectrometer is that it can be orders of magnitude more efficient at collecting X-rays than more traditional high-resolution spectrometers that rely on wavelength-dispersive techniques. This advantage is most useful in applications that are traditionally photon-starved and/or involve radiation-sensitive samples. Each energy-dispersive spectrometer is built around an array of several hundred transition-edge sensors (TESs). TESs are superconducting thin films that are biased into their superconducting-to-normal-metal transitions. The spectrometers share a common readout architecture and many design elements, suchmore » as a compact, 65 mK detector package, 8-column time-division-multiplexed superconducting quantum-interference device readout, and a liquid-cryogen-free cryogenic system that is a two-stage adiabatic-demagnetization refrigerator backed by a pulse-tube cryocooler. We have adapted this flexible architecture to mate to a variety of sample chambers and measurement systems that encompass a range of observing geometries. There are two different types of TES pixels employed. The first, designed for X-ray energies below 10 keV, has a best demonstrated energy resolution of 2.1 eV (full-width-at-half-maximum or FWHM) at 5.9 keV. The second, designed for X-ray energies below 2 keV, has a best demonstrated resolution of 1.0 eV (FWHM) at 500 eV. Our team has now deployed seven of these X-ray spectrometers to a variety of light sources, accelerator facilities, and laboratory-scale experiments; these seven spectrometers have already performed measurements related to their applications. Another five of these spectrometers will come online in the near future. We have applied our TES spectrometers to the following measurement applications: synchrotron-based absorption and emission spectroscopy and energy

A practical superconducting-microcalorimeter X-ray spectrometer for beamline and laboratory science

NASA Astrophysics Data System (ADS)

Doriese, W. B.; Abbamonte, P.; Alpert, B. K.; Bennett, D. A.; Denison, E. V.; Fang, Y.; Fischer, D. A.; Fitzgerald, C. P.; Fowler, J. W.; Gard, J. D.; Hays-Wehle, J. P.; Hilton, G. C.; Jaye, C.; McChesney, J. L.; Miaja-Avila, L.; Morgan, K. M.; Joe, Y. I.; O'Neil, G. C.; Reintsema, C. D.; Rodolakis, F.; Schmidt, D. R.; Tatsuno, H.; Uhlig, J.; Vale, L. R.; Ullom, J. N.; Swetz, D. S.

2017-05-01

We describe a series of microcalorimeter X-ray spectrometers designed for a broad suite of measurement applications. The chief advantage of this type of spectrometer is that it can be orders of magnitude more efficient at collecting X-rays than more traditional high-resolution spectrometers that rely on wavelength-dispersive techniques. This advantage is most useful in applications that are traditionally photon-starved and/or involve radiation-sensitive samples. Each energy-dispersive spectrometer is built around an array of several hundred transition-edge sensors (TESs). TESs are superconducting thin films that are biased into their superconducting-to-normal-metal transitions. The spectrometers share a common readout architecture and many design elements, such as a compact, 65 mK detector package, 8-column time-division-multiplexed superconducting quantum-interference device readout, and a liquid-cryogen-free cryogenic system that is a two-stage adiabatic-demagnetization refrigerator backed by a pulse-tube cryocooler. We have adapted this flexible architecture to mate to a variety of sample chambers and measurement systems that encompass a range of observing geometries. There are two different types of TES pixels employed. The first, designed for X-ray energies below 10 keV, has a best demonstrated energy resolution of 2.1 eV (full-width-at-half-maximum or FWHM) at 5.9 keV. The second, designed for X-ray energies below 2 keV, has a best demonstrated resolution of 1.0 eV (FWHM) at 500 eV. Our team has now deployed seven of these X-ray spectrometers to a variety of light sources, accelerator facilities, and laboratory-scale experiments; these seven spectrometers have already performed measurements related to their applications. Another five of these spectrometers will come online in the near future. We have applied our TES spectrometers to the following measurement applications: synchrotron-based absorption and emission spectroscopy and energy-resolved scattering

A practical superconducting-microcalorimeter X-ray spectrometer for beamline and laboratory science.

PubMed

Doriese, W B; Abbamonte, P; Alpert, B K; Bennett, D A; Denison, E V; Fang, Y; Fischer, D A; Fitzgerald, C P; Fowler, J W; Gard, J D; Hays-Wehle, J P; Hilton, G C; Jaye, C; McChesney, J L; Miaja-Avila, L; Morgan, K M; Joe, Y I; O'Neil, G C; Reintsema, C D; Rodolakis, F; Schmidt, D R; Tatsuno, H; Uhlig, J; Vale, L R; Ullom, J N; Swetz, D S

2017-05-01

We describe a series of microcalorimeter X-ray spectrometers designed for a broad suite of measurement applications. The chief advantage of this type of spectrometer is that it can be orders of magnitude more efficient at collecting X-rays than more traditional high-resolution spectrometers that rely on wavelength-dispersive techniques. This advantage is most useful in applications that are traditionally photon-starved and/or involve radiation-sensitive samples. Each energy-dispersive spectrometer is built around an array of several hundred transition-edge sensors (TESs). TESs are superconducting thin films that are biased into their superconducting-to-normal-metal transitions. The spectrometers share a common readout architecture and many design elements, such as a compact, 65 mK detector package, 8-column time-division-multiplexed superconducting quantum-interference device readout, and a liquid-cryogen-free cryogenic system that is a two-stage adiabatic-demagnetization refrigerator backed by a pulse-tube cryocooler. We have adapted this flexible architecture to mate to a variety of sample chambers and measurement systems that encompass a range of observing geometries. There are two different types of TES pixels employed. The first, designed for X-ray energies below 10 keV, has a best demonstrated energy resolution of 2.1 eV (full-width-at-half-maximum or FWHM) at 5.9 keV. The second, designed for X-ray energies below 2 keV, has a best demonstrated resolution of 1.0 eV (FWHM) at 500 eV. Our team has now deployed seven of these X-ray spectrometers to a variety of light sources, accelerator facilities, and laboratory-scale experiments; these seven spectrometers have already performed measurements related to their applications. Another five of these spectrometers will come online in the near future. We have applied our TES spectrometers to the following measurement applications: synchrotron-based absorption and emission spectroscopy and energy-resolved scattering

The NIF x-ray spectrometer calibration campaign at Omega.

PubMed

Pérez, F; Kemp, G E; Regan, S P; Barrios, M A; Pino, J; Scott, H; Ayers, S; Chen, H; Emig, J; Colvin, J D; Bedzyk, M; Shoup, M J; Agliata, A; Yaakobi, B; Marshall, F J; Hamilton, R A; Jaquez, J; Farrell, M; Nikroo, A; Fournier, K B

2014-11-01

The calibration campaign of the National Ignition Facility X-ray Spectrometer (NXS) was carried out at the Omega laser facility. Spherically symmetric, laser-driven, millimeter-scale x-ray sources of K-shell and L-shell emission from various mid-Z elements were designed for the 2-18 keV energy range of the NXS. The absolute spectral brightness was measured by two calibrated spectrometers. We compare the measured performance of the target design to radiation hydrodynamics simulations.

Streaked x-ray spectrometer having a discrete selection of Bragg geometries for Omega

DOE Office of Scientific and Technical Information (OSTI.GOV)

Millecchia, M.; Regan, S. P.; Bahr, R. E.

2012-10-15

The streaked x-ray spectrometer (SXS) is used with streak cameras [D. H. Kalantar, P. M. Bell, R. L. Costa, B. A. Hammel, O. L. Landen, T. J. Orzechowski, J. D. Hares, and A. K. L. Dymoke-Bradshaw, in 22nd International Congress on High-Speed Photography and Photonics, edited by D. L. Paisley and A. M. Frank (SPIE, Bellingham, WA, 1997), Vol. 2869, p. 680] positioned with a ten-inch manipulator on OMEGA [T. R. Boehly et al., Opt. Commun. 133, 495 (1997)] and OMEGA EP [L. J. Waxer et al., Presented at CLEO/QELS 2008, San Jose, CA, 4-9 May 2008 (Paper JThB1)] formore » time-resolved, x-ray spectroscopy of laser-produced plasmas in the 1.4- to 20-keV photon-energy range. These experiments require measuring a portion of this photon-energy range to monitor a particular emission or absorption feature of interest. The SXS relies on a pinned mechanical reference system to create a discrete set of Bragg reflection geometries for a variety of crystals. A wide selection of spectral windows is achieved accurately and efficiently using this technique. It replaces the previous spectrometer designs that had a continuous Bragg angle adjustment and required a tedious alignment calibration procedure. The number of spectral windows needed for the SXS was determined by studying the spectral ranges selected by OMEGA users over the last decade. These selections are easily configured in the SXS using one of the 25 discrete Bragg reflection geometries and one of the six types of Bragg crystals, including two curved crystals.« less

The Solar Flare 4: 10 keV X-ray Spectrum

NASA Technical Reports Server (NTRS)

Phillips, K. J. H.

2004-01-01

The 4-10 keV solar flare spectrum includes highly excited lines of stripped Ca, Fe, and Ni ions as well as a continuum steeply falling with energy. Groups of lines at approximately 7 keV and approximately 8 keV, observed during flares by the broad-band RHESSI spectrometer and called here the Fe-line and Fe/Ni-line features, are formed mostly of Fe lines but with Ni lines contributing to the approximately 8 keV feature. Possible temperature indicators of these line features are discussed - the peak or centroid energies of the Fe-line feature, the line ratio of the Fe-line to the Fe/Ni-line features, and the equivalent width of the Fe-line feature. The equivalent width is by far the most sensitive to temperature. However, results will be confused if, as is commonly believed, the abundance of Fe varies from flare to flare, even during the course of a single flare. With temperature determined from the thermal continuum, the Fe-line feature becomes a diagnostic of the Fe abundance in flare plasmas. These results are of interest for other hot plasmas in coronal ionization equilibrium such as stellar flare plasmas, hot gas in galaxies, and older supernova remnants.

Observations of solar flare photon energy spectra from 20 keV to 7 MeV

NASA Technical Reports Server (NTRS)

Yoshimori, M.; Watanabe, H.; Nitta, N.

1985-01-01

Solar flare photon energy spectra in the 20 keV to 7 MeV range are derived from the Apr. 1, Apr. 4, apr. 27 and May 13, 1981 flares. The flares were observed with a hard X-ray and a gamma-ray spectrometers on board the Hinotori satellite. The results show that the spectral shape varies from flare to flare and the spectra harden in energies above about 400 keV. Effects of nuclear line emission on the continuum and of higher energy electron bremsstrahlung are considered to explain the spectral hardening.

A compact neutron spectrometer for characterizing inertial confinement fusion implosions at OMEGA and the NIF

DOE PAGES

Zylstra, A. B.; Gatu Johnson, M.; Frenje, J. A.; ...

2014-06-04

A compact spectrometer for measurements of the primary deuterium-tritium neutron spectrum has been designed and implemented on the OMEGA laser facility. This instrument uses the recoil spectrometry technique, where neutrons produced in an implosion elastically scatter protons in a plastic foil, which are subsequently detected by a proton spectrometer. This diagnostic is capable of measuring the yield to ~±10% accuracy, and mean neutron energy to ~±50 keV precision. As these compact spectrometers can be readily placed at several locations around an implosion, effects of residual fuel bulk flows during burn can be measured. Future improvements to reduce the neutron energymore » uncertainty to ±15-20 keV are discussed, which will enable measurements of fuel velocities to an accuracy of ~±25-40 km/s.« less

Diffraction of real and virtual photons in a pyrolytic graphite crystal as source of intensive quasimonochromatic X-ray beam

NASA Astrophysics Data System (ADS)

Bogomazova, E. A.; Kalinin, B. N.; Naumenko, G. A.; Padalko, D. V.; Potylitsyn, A. P.; Sharafutdinov, A. F.; Vnukov, I. E.

2003-01-01

A series of experiments on the parametric X-rays radiation (PXR) generation and radiation soft component diffraction of relativistic electrons in pyrolytic graphite (PG) crystals have been carried out at the Tomsk synchrotron. It is shown that the experimental results with PG crystals are explained by the kinematic PXR theory if we take into account a contribution of the real photons diffraction (transition radiation, bremsstrahlung and PXR photons as well). The measurements of the emission spectrum of channeled electrons in the photon energy range much smaller than the characteristic energy of channeling radiation have been performed with a crystal-diffraction spectrometer. For electrons incident along the <1 1 0> axis of a silicon crystal, the radiation intensity in the energy range 30⩽ ω⩽360 keV exceeds the bremsstrahlung one almost by an order of magnitude. Different possibilities to create an effective source of the monochromatic X-ray beam based on the real and virtual photons diffraction in the PG crystals have been considered.

SMM detection of diffuse Galactic 511 keV annihilation radiation

NASA Technical Reports Server (NTRS)

Share, G. H.; Kinzer, R. L.; Kurfess, J. D.; Messina, D. C.; Purcell, W. R.

1988-01-01

Observations of the 511 keV annihilation line from the vicinity of the Galactic center from October to February for 1980/1981, 1981/1982, 1982/1983, 1984/1985, and 1985/1986 are presented. The measurements were made with the gamma-ray spectrometer on the SMM. The design of the instrument and some of its properties used in the analysis are described, and the methods used for accumulating, fitting, and analyzing the data are outlined. It is shown how the Galactic 511 keV line was separated from the intense and variable background observed in orbit. The SMM observations are compared with previous measurements of annihilation radiation from the Galactic center region, and the astrophysical implications are discussed. It is argued that most of the measurements made to date suggest the presence of an extended Galactic source of annihilation radiation.

Research of X-ray curved crystals analyzer

NASA Astrophysics Data System (ADS)

Xiao, Shali; Xong, Xian-cai; Qian, Jia-yu; Zhong, Xian-xin; Yan, Guo-hong; Liu, Zhong-li; Ding, Yong-kun

2005-08-01

X-ray spectrograph has long been used as a means of diagnosing conditions of laser-produced plasmas, as information concerning both the temperature and density can be extracted from the emitted radiation. For the measurement of X-ray lines in the energy range of 0.6-6 keV, A curved crystal X-ray spectrometer of reflection type elliptical geometry is required. In order to obtain both high resolution and collection efficiency the elliptical geometry is more advantageous than the flat configurations. Elliptical curved crystals spectrograph with a relatively wide spectral range are of particular use for deducing electron temperatures by measurement of the ratios of lines associated with different charge states. Curved crystals analyzer was designed and manufactured for use on an experiment to investigate the properties of laser produced plasmas. The spectrograph has 1350mm focal length and for these measurements, utilized PET, LIF, KAP and MICA crystal bent onto an elliptical substrate. This crystal analyzer covers the Bragg angel range from 30 to 67.5. The analyzer based on elliptically geometrical principle, which has self-focusing characteristics. The experiment was carried out on Shanghai Shengguang-II Facility and aimed to investigate the characteristics of a high density plasma. Experimental results using Curved crystal analyzer are described which show spectrum of Ti, Au laser-plasma. The focusing crystal analyzer clearly gave an increase in sensitivity over a flat crystal. Spectra showing the main resonance line were recorded with X-ray CCD and with laser energies 150J laser wavelength 350nm. The calculated wavelength resolution is about 500-1000.

Research on imaging spectrometer using LC-based tunable filter

NASA Astrophysics Data System (ADS)

Shen, Zhixue; Li, Jianfeng; Huang, Lixian; Luo, Fei; Luo, Yongquan; Zhang, Dayong; Long, Yan

2012-09-01

A liquid crystal tunable filter (LCTF) with large aperture is developed using PDLC liquid crystal. A small scale imaging spectrometer is established based on this tunable filter. This spectrometer can continuously tuning, or random-access selection of any wavelength in the visible and near infrared (VNIR) band synchronized with the imaging processes. Notable characteristics of this spectrometer include the high flexibility control of its operating channels, the image cubes with high spatial resolution and spectral resolution and the strong ability of acclimation to environmental temperature. The image spatial resolution of each tuning channel is almost near the one of the same camera without the LCTF. The spectral resolution is about 20 nm at 550 nm. This spectrometer works normally under 0-50°C with a maximum power consumption of 10 Watts (with exclusion of the storage module). Due to the optimization of the electrode structure and the driving mode of the Liquid Crystal cell, the switch time between adjacent selected channels can be reduced to 20 ms or even shorter. Spectral imaging experiments in laboratory are accomplished to verify the performance of this spectrometer, which indicate that this compact imaging spectrometer works reliably, and functionally. Possible applications of this imaging spectrometer include medical science, protection of historical relics, criminal investigation, disaster monitoring and mineral detection by remote sensing.

Ring-patterned plasmonic photonic crystal thermal light source for miniaturized near-infrared spectrometers

NASA Astrophysics Data System (ADS)

Labib, Shady R.; Elsayed, Ahmed A.; Sabry, Yasser M.; Khalil, Diaa

2018-02-01

There is a growing number of spectroscopy applications in the near-infrared (NIR) range including gas sensing, food analysis, pharmaceutical and industrial applications that requires highly efficient, more compact and low-cost miniaturized spectrometers. One of the key components for such systems is the wideband light source that can be fabricated using Silicon technology and hence integrated with other components on the same chip. In this work, we report a ring-patterned plasmonic photonic crystal (PC) thermal light source for miniaturized near-infrared spectrometers. The design is based on silicon and tuned to achieve wavelength selectivity in the emitted spectrum. The design is optimized by using Rigorous Coupled-Wave Analysis (RCWA) simulation, which is used to compute the power reflectance and transmittance that are used to predict the emissivity of the structure. The design consists of a PC of silicon rings coated with platinum. The period of the structure is about 2 μm and the silicon is highly-doped with n-type doping level in the order of 1019-1020 cm-3 to enhance the free-carrier absorption. The ring etching depth, diameter and shell thickness are optimized to increase its emissivity within a specific wavelength range of interest. The simulation results show an emissivity exceeding 0.9 in the NIR range up to 2.5 μm, while the emissivity is decreased significantly for longer wavelengths suppressing the emission out of the range of interest, and hence increasing the efficiency for the source. The reported results open the door for black body radiation engineering in integrated silicon sources for spectrometer miniaturization.

A compact neutron spectrometer for characterizing inertial confinement fusion implosions at OMEGA and the NIF.

PubMed

Zylstra, A B; Gatu Johnson, M; Frenje, J A; Séguin, F H; Rinderknecht, H G; Rosenberg, M J; Sio, H W; Li, C K; Petrasso, R D; McCluskey, M; Mastrosimone, D; Glebov, V Yu; Forrest, C; Stoeckl, C; Sangster, T C

2014-06-01

A compact spectrometer for measurements of the primary deuterium-tritium neutron spectrum has been designed and implemented on the OMEGA laser facility [T. Boehly et al., Opt. Commun. 133, 495 (1997)]. This instrument uses the recoil spectrometry technique, where neutrons produced in an implosion elastically scatter protons in a plastic foil, which are subsequently detected by a proton spectrometer. This diagnostic is currently capable of measuring the yield to ~±10% accuracy, and mean neutron energy to ~±50 keV precision. As these compact spectrometers can be readily placed at several locations around an implosion, effects of residual fuel bulk flows during burn can be measured. Future improvements to reduce the neutron energy uncertainty to ±15-20 keV are discussed, which will enable measurements of fuel velocities to an accuracy of ~±25-40 km/s.

A compact neutron spectrometer for characterizing inertial confinement fusion implosions at OMEGA and the NIF

NASA Astrophysics Data System (ADS)

Zylstra, A. B.; Gatu Johnson, M.; Frenje, J. A.; Séguin, F. H.; Rinderknecht, H. G.; Rosenberg, M. J.; Sio, H. W.; Li, C. K.; Petrasso, R. D.; McCluskey, M.; Mastrosimone, D.; Glebov, V. Yu.; Forrest, C.; Stoeckl, C.; Sangster, T. C.

2014-06-01

A compact spectrometer for measurements of the primary deuterium-tritium neutron spectrum has been designed and implemented on the OMEGA laser facility [T. Boehly et al., Opt. Commun. 133, 495 (1997)]. This instrument uses the recoil spectrometry technique, where neutrons produced in an implosion elastically scatter protons in a plastic foil, which are subsequently detected by a proton spectrometer. This diagnostic is currently capable of measuring the yield to ˜±10% accuracy, and mean neutron energy to ˜±50 keV precision. As these compact spectrometers can be readily placed at several locations around an implosion, effects of residual fuel bulk flows during burn can be measured. Future improvements to reduce the neutron energy uncertainty to ±15-20 keV are discussed, which will enable measurements of fuel velocities to an accuracy of ˜±25-40 km/s.

In-situ wavelength calibration and temperature control for the C-Mod high-resolution x-ray crystal imaging spectrometer

NASA Astrophysics Data System (ADS)

Delgado-Aparicio, Luis F.; Podpaly, Y.; Reinke, M. L.; Gao, C.; Rice, J.; Scott, S.; Bitter, M.; Hill, K.; Beiersdorfer, P.; Johnson, D.; Wilson, J. R.

2010-11-01

An x-ray crystal imaging spectrometer with high spectral and spatial resolution is currently being used on Alcator C-Mod to infer time histories of temperature and velocity profiles. An in-situ wavelength calibration using a 1 μm palladium filter in between the crystal and the detectors of choice is being proposed as a natural wavelength-marker using the transmission changes across the L-II and L-III edges at 3722.9 mA and 3907.1 mA, respectively. Recent results also indicate that the crystal temperature should be kept constant within a fraction of a degree since the thermal expansion of the quartz crystal will change the interplanar (2d) spacing and introduce fictitious velocity measurements of several km/s. A detailed temperature scan indicates a thermal expansion coefficient (α) of 13.5x10-6 /^oC and thus a false Doppler shift of 4.05.δT[^oC] km/s.

Optical transmittance investigation of 1-keV ion-irradiated sapphire crystals as potential VUV to NIR window materials of fusion reactors

NASA Astrophysics Data System (ADS)

Iwano, Keisuke; Yamanoi, Kohei; Iwasa, Yuki; Mori, Kazuyuki; Minami, Yuki; Arita, Ren; Yamanaka, Takuma; Fukuda, Kazuhito; Empizo, Melvin John F.; Takano, Keisuke; Shimizu, Toshihiko; Nakajima, Makoto; Yoshimura, Masashi; Sarukura, Nobuhiko; Norimatsu, Takayoshi; Hangyo, Masanori; Azechi, Hiroshi; Singidas, Bess G.; Sarmago, Roland V.; Oya, Makoto; Ueda, Yoshio

2016-10-01

We investigate the optical transmittances of ion-irradiated sapphire crystals as potential vacuum ultraviolet (VUV) to near-infrared (NIR) window materials of fusion reactors. Under potential conditions in fusion reactors, sapphire crystals are irradiated with hydrogen (H), deuterium (D), and helium (He) ions with 1-keV energy and ˜ 1020-m-2 s-1 flux. Ion irradiation decreases the transmittances from 140 to 260 nm but hardly affects the transmittances from 300 to 1500 nm. H-ion and D-ion irradiation causes optical absorptions near 210 and 260 nm associated with an F-center and an F+-center, respectively. These F-type centers are classified as Schottky defects that can be removed through annealing above 1000 K. In contrast, He-ion irradiation does not cause optical absorptions above 200 nm because He-ions cannot be incorporated in the crystal lattice due to the large ionic radius of He-ions. Moreover, the significant decrease in transmittance of the ion-irradiated sapphire crystals from 140 to 180 nm is related to the light scattering on the crystal surface. Similar to diamond polishing, ion irradiation modifies the crystal surface thereby affecting the optical properties especially at shorter wavelengths. Although the transmittances in the VUV wavelengths decrease after ion irradiation, the transmittances can be improved through annealing above 1000 K. With an optical transmittance in the VUV region that can recover through simple annealing and with a high transparency from the ultraviolet (UV) to the NIR region, sapphire crystals can therefore be used as good optical windows inside modern fusion power reactors in terms of light particle loadings of hydrogen isotopes and helium.

The construction of a high resolution crystal backscattering spectrometer HERMES I

DOE Office of Scientific and Technical Information (OSTI.GOV)

Larese, J.Z.

There is a need in the United States for a state-of-the-art, cold-neutron, crystal backscattering spectrometer (CBS) designed to investigate the structure and dynamics of condensed matter systems by the simultaneous utilization of long wavelength elastic diffraction and high-energy-resolution inelastic scattering. Cold neutron spectroscopy with CBS-type instruments has already made many important contributions to the study of atomic and molecular diffusion in biomaterials, polymers, semiconductors, liquid crystals, superionic conductors and the like. Such instruments have also been invaluable for ultra high resolution investigations of the low-lying quantum tunneling processes that provide direct insight into the dynamical response of solids at themore » lowest energies. Until relatively recently, however, all such instruments were located at steady-state reactors. This proposal describes HERMES I (High Energy Resolution Machines I) a CBS intended for installation at the LANSCE pulsed neutron facility of Los Alamos National Laboratory. As explained in detail in the main text, the authors propose to construct an updated, high-performance CBS which incorporates neutron techniques developed during the decade since IRIS was built, i.e., improved supermirror technology, a larger area crystal analyzer and high efficiency wire gas detectors. The instrument is designed in such a way as to be readily adaptable to future upgrades. HERMES I, they believe, will substantially expand the range and flexibility of neutron investigations in the United States and open new and potentially fruitful directions for condensed matter exploration. This document describes a implementation plan with a direct cost range between $4.5 to 5.6 M and scheduled duration of 39--45 months for identified alternatives.« less

Measurement of helium-like and hydrogen-like argon spectra using double-crystal X-ray spectrometers on EAST

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lyu, B., E-mail: blu@ipp.ac.cn; Hefei Science Center, Chinese Academy of Sciences, Hefei 230031; Chen, J.

2016-11-15

A two-crystal assembly was deployed on the tangential X-ray crystal spectrometer to measure both helium-like and hydrogen-like spectra on EAST. High-quality helium-like and hydrogen-like spectra were observed simultaneously for the first time on one detector for a wide range of plasma parameters. Profiles of line-integrated core ion temperatures inferred from two spectra were consistent. Since tungsten was adopted as the upper divertor material, one tungsten line (W XLIV at 4.017 Å) on the short-wavelength side of the Lyman-α line (Lα1) was identified for typical USN discharges, which was diffracted by a He-like crystal (2d = 4.913 Å). Another possible Femore » XXV line (1.85 Å) was observed to be located on the long-wavelength side of resonance line (w), which was diffracted from a H-like crystal (2d = 4.5622 Å) on the second order. Be-like argon lines were also observable that fill the detector space between the He-like and H-like spectra.« less

Measurement of helium-like and hydrogen-like argon spectra using double-crystal X-ray spectrometers on EAST.

PubMed

Lyu, B; Chen, J; Hu, R J; Wang, F D; Li, Y Y; Fu, J; Shen, Y C; Bitter, M; Hill, K W; Delgado-Aparicio, L F; Pablant, N; Lee, S G; Ye, M Y; Shi, Y J; Wan, B N

2016-11-01

A two-crystal assembly was deployed on the tangential X-ray crystal spectrometer to measure both helium-like and hydrogen-like spectra on EAST. High-quality helium-like and hydrogen-like spectra were observed simultaneously for the first time on one detector for a wide range of plasma parameters. Profiles of line-integrated core ion temperatures inferred from two spectra were consistent. Since tungsten was adopted as the upper divertor material, one tungsten line (W XLIV at 4.017 Å) on the short-wavelength side of the Lyman-α line (Lα1) was identified for typical USN discharges, which was diffracted by a He-like crystal (2d = 4.913 Å). Another possible Fe XXV line (1.85 Å) was observed to be located on the long-wavelength side of resonance line (w), which was diffracted from a H-like crystal (2d = 4.5622 Å) on the second order. Be-like argon lines were also observable that fill the detector space between the He-like and H-like spectra.

A TLD-based few-channel spectrometer for mixed photon, electron, and ion fields with high fluence rates.

PubMed

Behrens, R; Ambrosi, P

2002-01-01

A few-channel spectrometer for mixed photon, electron and ion radiation fields has been developed. It consists of a front layer of an etched-track detector foil for detecting protons and ions, a stack of PMMA with thermoluminescent detectors at different depths for gaining spectral information about electrons, and a stack of metallic filters with increasing cut-off photon energies, interspersed with thermoluminescent detectors for gaining spectral information about photons. From the reading of the TL detectors the spectral fluence of the electrons (400 keV to 9 MeV) and photons (20 keV to 2 MeV) can be determined by an unfolding procedure. The spectrometer can be used in pulsed radiation fields with extremely high momentary values of the fluence rate. Design and calibration of the spectrometer are described.

Response function of single crystal synthetic diamond detectors to 1-4 MeV neutrons for spectroscopy of D plasmas

NASA Astrophysics Data System (ADS)

Rebai, M.; Giacomelli, L.; Milocco, A.; Nocente, M.; Rigamonti, D.; Tardocchi, M.; Camera, F.; Cazzaniga, C.; Chen, Z. J.; Du, T. F.; Fan, T. S.; Giaz, A.; Hu, Z. M.; Marchi, T.; Peng, X. Y.; Gorini, G.

2016-11-01

A Single-crystal Diamond (SD) detector prototype was installed at Joint European Torus (JET) in 2013 and the achieved results have shown its spectroscopic capability of measuring 2.5 MeV neutrons from deuterium plasmas. This paper presents measurements of the SD response function to monoenergetic neutrons, which is a key point for the development of a neutron spectrometer based on SDs and compares them with Monte Carlo simulations. The analysis procedure allows for a good reconstruction of the experimental results. The good pulse height energy resolution (equivalent FWHM of 80 keV at 2.5 MeV), gain stability, insensitivity to magnetic field, and compact size make SDs attractive as compact neutron spectrometers of high flux deuterium plasmas, such as for instance those needed for the ITER neutron camera.

Response function of single crystal synthetic diamond detectors to 1-4 MeV neutrons for spectroscopy of D plasmas

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rebai, M., E-mail: marica.rebai@mib.infn.it; Nocente, M.; Rigamonti, D.

2016-11-15

A Single-crystal Diamond (SD) detector prototype was installed at Joint European Torus (JET) in 2013 and the achieved results have shown its spectroscopic capability of measuring 2.5 MeV neutrons from deuterium plasmas. This paper presents measurements of the SD response function to monoenergetic neutrons, which is a key point for the development of a neutron spectrometer based on SDs and compares them with Monte Carlo simulations. The analysis procedure allows for a good reconstruction of the experimental results. The good pulse height energy resolution (equivalent FWHM of 80 keV at 2.5 MeV), gain stability, insensitivity to magnetic field, and compactmore » size make SDs attractive as compact neutron spectrometers of high flux deuterium plasmas, such as for instance those needed for the ITER neutron camera.« less

Superconducting High Resolution Fast-Neutron Spectrometers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hau, Ionel Dragos

2006-01-01

Superconducting high resolution fast-neutron calorimetric spectrometers based on 6LiF and TiB{sub 2} absorbers have been developed. These novel cryogenic spectrometers measure the temperature rise produced in exothermal (n, α) reactions with fast neutrons in 6Li and 10B-loaded materials with heat capacity C operating at temperatures T close to 0.1 K. Temperature variations on the order of 0.5 mK are measured with a Mo/Cu thin film multilayer operated in the transition region between its superconducting and its normal state. The advantage of calorimetry for high resolution spectroscopy is due to the small phonon excitation energies k BT on the order ofmore » μeV that serve as signal carriers, resulting in an energy resolution ΔE ~ (k BT 2C) 1/2, which can be well below 10 keV. An energy resolution of 5.5 keV has been obtained with a Mo/Cu superconducting sensor and a TiB 2 absorber using thermal neutrons from a 252Cf neutron source. This resolution is sufficient to observe the effect of recoil nuclei broadening in neutron spectra, which has been related to the lifetime of the first excited state in 7Li. Fast-neutron spectra obtained with a 6Li-enriched LiF absorber show an energy resolution of 16 keV FWHM, and a response in agreement with the 6Li(n, α) 3H reaction cross section and Monte Carlo simulations for energies up to several MeV. The energy resolution of order of a few keV makes this novel instrument applicable to fast-neutron transmission spectroscopy based on the unique elemental signature provided by the neutron absorption and scattering resonances. The optimization of the energy resolution based on analytical and numerical models of the detector response is discussed in the context of these applications.« less

A New Observation of the Quiet Sun Soft X-ray (0.5-5 keV) Spectrum

NASA Astrophysics Data System (ADS)

Caspi, A.; Woods, T. N.; Stone, J.

2012-12-01

The solar corona is the brightest source of X-rays in the solar system, and the X-ray emission is highly variable with solar activity. While this is particularly true during solar flares, when emission can be enhanced by many orders of magnitude up to gamma-ray energies, even the so-called "quiet Sun" is bright in soft X-rays (SXRs), as the ~1-2 MK ambient plasma of the corona emits significant thermal bremsstrahlung up to ~5 keV. However, the actual solar SXR (0.5-5 keV) spectrum is not well known, particularly during quiet periods, as, with few exceptions, this energy range has not been systematically studied in many years. Previous observations include ultra-high-resolution but very narrow-band spectra from crystral spectrometers (e.g. Yohkoh/BCS), or integrated broadband irradiances from photometers (e.g. GOES/XRS, TIMED/XPS, etc.) that lack detailed spectral information. In recent years, broadband measurements with fair energy resolution (~0.5-0.7 keV FWHM) were made by SphinX on CORONAS-Photon and XRS on MESSENGER, although they did not extend below ~1 keV. We present observations of the quiet Sun SXR emission obtained using a new SXR spectrometer flown on the third SDO/EVE underflight calibration rocket (NASA 36.286). The commercial off-the-shelf Amptek X123 silicon drift detector, with an 8-micron Be window and custom aperture, measured the solar SXR emission from ~0.5 to >10 keV with ~0.15 keV FWHM resolution (though, due to hardware limitations, with only ~0.12 keV binning) and 2-sec cadence over ~5 minutes on 23 June 2012. Despite the rising solar cycle, activity on 23 June 2012 was abnormally low, with no visible active regions and GOES XRS emission near 2010 levels; we measured no solar counts above ~4 keV during the observation period. We compare our X123 measurements with spectra and broadband irradiances from other instruments, including the SphinX observations during the deep solar minimum of 2009, and with upper limits of >3 keV quiet Sun emission

A New Observation of the Quiet Sun Soft X-ray (0.5-5 keV) Spectrum

NASA Astrophysics Data System (ADS)

Caspi, Amir; Woods, Thomas N.; Stone, Jordan

2013-03-01

The solar corona is the brightest source of X-rays in the solar system, and the X-ray emission is highly variable with solar activity. While this is particularly true during solar flares, when emission can be enhanced by many orders of magnitude up to gamma-ray energies, even the so-called "quiet Sun" is bright in soft X-rays (SXRs), as the 1-2 MK ambient plasma of the corona emits significant thermal bremsstrahlung up to 5 keV. However, the actual solar SXR (0.5-5 keV) spectrum is not well known, particularly during quiet periods, as, with few exceptions, this energy range has not been systematically studied in many years. Previous observations include ultra-high-resolution but very narrow-band spectra from crystral spectrometers (e.g. Yohkoh/BCS), or integrated broadband irradiances from photometers (e.g. GOES/XRS, TIMED/XPS, etc.) that lack detailed spectral information. In recent years, broadband measurements with fair energy resolution ( 0.5-0.7 keV FWHM) were made by SphinX on CORONAS-Photon and XRS on MESSENGER, although they did not extend below 1 keV. We present observations of the quiet Sun SXR emission obtained using a new SXR spectrometer flown on the third SDO/EVE underflight calibration rocket (NASA 36.286). The commercial off-the-shelf Amptek X123 silicon drift detector, with an 8-micron Be window and custom aperture, measured the solar SXR emission from 0.5 to >10 keV with 0.15 keV FWHM resolution (though, due to hardware limitations, with only 0.12 keV binning) and 2-sec cadence over 5 minutes on 23 June 2012. Despite the rising solar cycle, activity on 23 June 2012 was abnormally low, with no visible active regions and GOES XRS emission near 2010 levels; we measured no solar counts above 4 keV during the observation period. We compare our X123 measurements with spectra and broadband irradiances from other instruments, including the SphinX observations during the deep solar minimum of 2009, and with upper limits of >3 keV quiet Sun emission

Key Elements of a Low Voltage, Ultracompact Plasma Spectrometer

NASA Technical Reports Server (NTRS)

Scime, E. E.; Barrie, A.; Dugas, M.; Elliott, D.; Ellison, S.; Keesee, A. M.; Pollock, C. J.; Rager, A.; Tersteeg, J.

2016-01-01

Taking advantage of technological developments in wafer-scale processing over the past two decades, such as deep etching, 3-D chip stacking, and double-sided lithography, we have designed and fabricated the key elements of an ultracompact 1.5cm (exp 3)plasma spectrometer that requires only low-voltage power supplies, has no microchannel plates, and has a high aperture area to instrument volume ratio. The initial design of the instrument targets the measurement of charged particles in the 3-20keV range with a highly directional field of view and a 100 duty cycle; i.e., the entire energy range Is continuously measured. In addition to reducing mass, size, and voltage requirements, the new design will affect the manufacturing process of plasma spectrometers, enabling large quantities of identical instruments to be manufactured at low individual unit cost. Such a plasma spectrometer is ideal for heliophysics plasma investigations, particularly for small satellite and multispacecraft missions. Two key elements of the instrument have been fabricated: the collimator and the energy analyzer. An initial collimator transparency of 20 with 3deg x 3deg angular resolution was achieved. The targeted 40 collimator transparency appears readily achievable. The targeted energy analyzer scaling factor of 1875 was achieved; i.e.20 keV electrons were selected for only a 10.7V bias voltage in the energy analyzer.

Mossbauer spectrometer radiation detector

NASA Technical Reports Server (NTRS)

Singh, J. J. (Inventor)

1973-01-01

A Mossbauer spectrometer with high efficiencies in both transmission and backscattering techniques is described. The device contains a sodium iodide crystal for detecting radiation caused by the Mossbauer effect, and two photomultipliers to collect the radiation detected by the crystal. When used in the transmission technique, the sample or scatterer is placed between the incident radiation source and the detector. When used in a backscattering technique, the detector is placed between the incident radiation source and the sample of scatterer such that the incident radiation will pass through a hole in the crystal and strike the sample. Diagrams of the instrument are provided.

Curved focusing crystals for hard X-ray astronomy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ferrari, C., E-mail: ferrari@imem.cnr.it; Buffagni, E.; Bonnini, E.

A lens made by a properly arranged array of crystals can be used to focus x-rays of energy ranging from 30 to 500 keV for x-ray astronomy. Mosaic or curved crystals can be employed as x-ray optical elements. In this work self standing curved focusing Si and GaAs crystals in which the lattice bending is induced by a controlled damaging process on one side of planar crystals are characterized. Diffraction profiles in Laue geometry have been measured in crystals at x-ray energies E = 17, 59 and 120 keV. An enhancement of diffraction efficiency is found in asymmetric geometries.

The LCLS variable-energy hard X-ray single-shot spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rich, David; Zhu, Diling; Turner, James

2016-01-01

The engineering design, implementation, operation and performance of the new variable-energy hard X-ray single-shot spectrometer (HXSSS) for the LCLS free-electron laser (FEL) are reported. The HXSSS system is based on a cylindrically bent Si thin crystal for dispersing the incident polychromatic FEL beam. A spatially resolved detector system consisting of a Ce:YAG X-ray scintillator screen, an optical imaging system and a low-noise pixelated optical camera is used to record the spectrograph. The HXSSS provides single-shot spectrum measurements for users whose experiments depend critically on the knowledge of the self-amplified spontaneous emission FEL spectrum. It also helps accelerator physicists for themore » continuing studies and optimization of self-seeding, various improved mechanisms for lasing mechanisms, and FEL performance improvements. The designed operating energy range of the HXSSS is from 4 to 20 keV, with the spectral range of order larger than 2% and a spectral resolution of 2 × 10 -5or better. Those performance goals have all been achieved during the commissioning of the HXSSS.« less

The LCLS variable-energy hard X-ray single-shot spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rich, David; Zhu, Diling; Turner, James

The engineering design, implementation, operation and performance of the new variable-energy hard X-ray single-shot spectrometer (HXSSS) for the LCLS free-electron laser (FEL) are reported. The HXSSS system is based on a cylindrically bent Si thin crystal for dispersing the incident polychromatic FEL beam. A spatially resolved detector system consisting of a Ce:YAG X-ray scintillator screen, an optical imaging system and a low-noise pixelated optical camera is used to record the spectrograph. The HXSSS provides single-shot spectrum measurements for users whose experiments depend critically on the knowledge of the self-amplified spontaneous emission FEL spectrum. It also helps accelerator physicists for themore » continuing studies and optimization of self-seeding, various improved mechanisms for lasing mechanisms, and FEL performance improvements. The designed operating energy range of the HXSSS is from 4 to 20 keV, with the spectral range of order larger than 2% and a spectral resolution of 2 × 10 -5or better. Those performance goals have all been achieved during the commissioning of the HXSSS.« less

SMM observation of a cosmic gamma-ray burst from 20 keV to 100 MeV

NASA Technical Reports Server (NTRS)

Share, G. H.; Matz, S. M.; Messina, D. C.; Nolan, P. L.; Chupp, E. L.

1986-01-01

The Solar Maximum Mission gamma-ray spectrometer has detected an intense gamma-ray burst that occurred on August 5, 1984. The burst originated from a source in the constellation Hydra and lasted about 45 s. Its integral fluence at 20 keV was 0.003 erg/sq cm. Spectral evolution similar to other bursts detected by SMM was observed. The overall shape of the spectrum from 20 keV to 100 MeV, on timescales as short as 2 s, is relatively constant. This shape can be fitted by the sum of an exponential-type function and a power law. There is no evidence for narrow or broadened emission lines.

A preliminary design study for a cosmic X-ray spectrometer

NASA Technical Reports Server (NTRS)

1972-01-01

The results are described of theoretical and experimental investigations aimed at the development of a curved crystal cosmic X-ray spectrometer to be used at the focal plane of the large orbiting X-ray telescope on the third High Energy Astronomical Observatory. The effort was concentrated on the development of spectrometer concepts and their evaluation by theoretical analysis, computer simulation, and laboratory testing with breadboard arrangements of crystals and detectors. In addition, a computer-controlled facility for precision testing and evaluation of crystals in air and vacuum was constructed. A summary of research objectives and results is included.

A micro-scale plasma spectrometer for space and plasma edge applications (invited)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Scime, E. E., E-mail: escime@wvu.edu; Keesee, A. M.; Elliott, D.

2016-11-15

A plasma spectrometer design based on advances in lithography and microchip stacking technologies is described. A series of curved plate energy analyzers, with an integrated collimator, is etched into a silicon wafer. Tests of spectrometer elements, the energy analyzer and collimator, were performed with a 5 keV electron beam. The measured collimator transmission and energy selectivity were in good agreement with design targets. A single wafer element could be used as a plasma processing or fusion first wall diagnostic.

A Spatially Resolving X-ray Crystal Spectrometer for Measurement of Ion-temperature and Rotation-velocity Profiles on the AlcatorC-Mod Tokamak

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hill, K. W.; Bitter, M. L.; Scott, S. D.

2009-03-24

A new spatially resolving x-ray crystal spectrometer capable of measuring continuous spatial profiles of high resolution spectra (λ/dλ > 6000) of He-like and H-like Ar Kα lines with good spatial (~1 cm) and temporal (~10 ms) resolutions has been installed on the Alcator C-Mod tokamak. Two spherically bent crystals image the spectra onto four two-dimensional Pilatus II pixel detectors. Tomographic inversion enables inference of local line emissivity, ion temperature (Ti), and toroidal plasma rotation velocity (vφ) from the line Doppler widths and shifts. The data analysis techniqu

New Results from the Solar Maximum Mission/Bent Crystal Spectrometer

NASA Astrophysics Data System (ADS)

Rapley, C. G.; Sylwester, J.; Phillips, K. J. H.

2017-04-01

The Bent Crystal Spectrometer (BCS) onboard the NASA Solar Maximum Mission was part of the X-ray Polychromator, which observed numerous flares and bright active regions from February to November 1980, when operation was suspended as a result of the failure of the spacecraft fine-pointing system. Observations resumed following the Space Shuttle SMM Repair Mission in April 1984 and continued until November 1989. BCS spectra have been widely used in the past to obtain temperatures, emission measures, and turbulent and bulk flows during flares, as well as element abundances. Instrumental details including calibration factors not previously published are given here, and the in-orbit performance of the BCS is evaluated. Some significant changes during the mission are described, and recommendations for future instrumentation are made. Using improved estimates for the instrument parameters and operational limits, it is now possible to obtain de-convolved calibrated spectra that show finer detail than before, providing the means for improved interpretation of the physics of the emitting plasmas. The results indicate how historical archived data can be re-used to obtain enhanced and new, scientifically valuable results.

MULTI-KEV X-RAY YIELDS FROM HIGH-Z GAS TARGETS FIELDED AT OMEGA

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kane, J O; Fournier, K B; May, M J

2010-11-04

The authors report on modeling of x-ray yield from gas-filled targets shot at the OMEGA laser facility. The OMEGA targets were 1.8 mm long, 1.95 mm in diameter Be cans filled with either a 50:50 Ar:Xe mixture, pure Ar, pure Kr or pure Xe at {approx} 1 atm. The OMEGA experiments heated the gas with 20 kJ of 3{omega} ({approx} 350 nm) laser energy delivered in a 1 ns square pulse. the emitted x-ray flux was monitored with the x-ray diode based DANTE instruments in the sub-keV range. Two-dimensional x-ray images (for energies 3-5 keV) of the targets were recordedmore » with gated x-ray detectors. The x-ray spectra were recorded with the HENWAY crystal spectrometer at OMEGA. Predictions are 2D r-z cylindrical with DCA NLTE atomic physics. Models generally: (1) underpredict the Xe L-shell yields; (2) overpredict the Ar K-shell yields; (3) correctly predict the Xe thermal yields; and (4) greatly underpredict the Ar thermal yields. However, there are spreads within the data, e.g. the DMX Ar K-shell yields are correctly predicted. The predicted thermal yields show strong angular dependence.« less

Infrared fiber coupled acousto-optic tunable filter spectrometer

NASA Technical Reports Server (NTRS)

Levin, K. H.; Kindler, E.; Ko, T.; Lee, F.; Tran, D. C.; Tapphorn, R. M.

1990-01-01

A spectrometer design is introduced which combines an acoustooptic tunable filter (AOTF) and IR-transmitting flouride-glass fibers. The AOTF crystal is fabricated from TeO2 and permits random access to any wavelength in less than 50 microseconds, and the resulting spectrometer is tested for the remote analysis of gases and hydrocarbons. The AOTF spectrometer, when operated with a high-speed frequency synthesizer and optimized algorithms, permits accurate high-speed spectroscopy in the mid-IR spectral region.

Micro-X-ray fluorescence spectrometer with x-ray single bounce metallic capillary optics for light element analysis (Conference Presentation)

NASA Astrophysics Data System (ADS)

Mroczka, Robert; Żukociński, Grzegorz; Łopucki, Rafał

2017-05-01

In the last 20 years, , due to the rapid development of X-ray optics, micro X-ray fluorescence spectrometry (micro-XRF) has become a powerful tool to determine the spatial distribution of major, minor, and trace elements within a sample. Micro-X-ray fluorescence (micro-XRF) spectrometers for light element analysis (6 <= Z <= 14) using glass polycapillary optics are usually designed and applied to confocal geometry. Two such X-ray optics systems are used in this setup. The first one focuses the primary beam on the sample; the second restricts the field of view of the detector. In order to be able to analyze a wider range of elements especialy with (6 <= Z <= 14), both sample and detector are under vacuum. Depth resolution varies between 100 μm at 1 keV fluorescence energy (Na-Kα) and 30 μm for 17.5 keV (Mo-Kα) [1,2]. In order to improve resolution at energies below 9 keV, our group designed similar spectrometer (in cooperation with PREVAC) but instead of primary polycapillary optics we applied single bounce metallic capillaries optics , designed and manufactured in our Laboratory. The vacuum chumber is currently under construction and is expected to be fully operational in September this year. Single bounce gold capillaries with elliptic internal shape have recently been redesigned and developed in our Laboratory. Surface roughness was reduced up to 0.5 nm and slope error to 0.3 mrad. For these capillaries an expected depth resolution varies from 3 μm (1 keV) and 10 µm for 9 keV (Cu-Kα). The spectrometer equipped with gold capillaries offers the possibility of elemental analysis with better depth resolution than is offerred by glass polycapillaries at energies below 9 keV. Furthermore, we will compare the capabilities and limitations of this spectrometer with others, that use laboratory and/or synchrotron sources. Acknowledgments: This work was supported and co-funded by the European Union as part of the Operational Programme Development of Eastern Poland for

NEW OBSERVATIONS OF THE SOLAR 0.5–5 KEV SOFT X-RAY SPECTRUM

DOE Office of Scientific and Technical Information (OSTI.GOV)

Caspi, Amir; Woods, Thomas N.; Warren, Harry P.

2015-03-20

The solar corona is orders of magnitude hotter than the underlying photosphere, but how the corona attains such high temperatures is still not understood. Soft X-ray (SXR) emission provides important diagnostics for thermal processes in the high-temperature corona, and is also an important driver of ionospheric dynamics at Earth. There is a crucial observational gap between ∼0.2 and ∼4 keV, outside the ranges of existing spectrometers. We present observations from a new SXR spectrometer, the Amptek X123-SDD, which measured the spatially integrated solar spectral irradiance from ∼0.5 to ∼5 keV, with ∼0.15 keV FWHM resolution, during sounding rocket flights onmore » 2012 June 23 and 2013 October 21. These measurements show that the highly variable SXR emission is orders of magnitude greater than that during the deep minimum of 2009, even with only weak activity. The observed spectra show significant high-temperature (5–10 MK) emission and are well fit by simple power-law temperature distributions with indices of ∼6, close to the predictions of nanoflare models of coronal heating. Observations during the more active 2013 flight indicate an enrichment of low first-ionization potential elements of only ∼1.6, below the usually observed value of ∼4, suggesting that abundance variations may be related to coronal heating processes. The XUV Photometer System Level 4 data product, a spectral irradiance model derived from integrated broadband measurements, significantly overestimates the spectra from both flights, suggesting a need for revision of its non-flare reference spectra, with important implications for studies of Earth ionospheric dynamics driven by solar SXRs.« less

Measurement of DT and DD components in neutron spectrum with a double-crystal time-of-flight spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Okada, K.; Okamoto, A.; Kitajima, S.

To investigate the deuteron and triton density ratio in core plasmas, a new methodology with measurement of tritium (DT) and deuterium (DD) neutron count rate ratio using a double-crystal time-of-flight (TOF) spectrometer is proposed. Multi-discriminator electronic circuits for the first and second detectors are used in addition to the TOF technique. The optimum arrangement of the detectors and discrimination window were examined considering the relations between the geometrical arrangement and deposited energy using a Monte Carlo Code, PHITS (Particle and Heavy Ion Transport Code System). An experiment to verify the calculations was performed using DD neutrons from an accelerator.

New search for double electron capture in {sup 106}Cd decay with the TGV-2 spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Briançon, Ch.; Brudanin, V. B.; Egorov, V. G.

2015-09-15

A new experiment devoted to searches for double electron capture in {sup 106}Cd decay is being performed at the Modane underground laboratory (4800 mwe) with the 32-detector TGV-2 spectrometer. The limit T{sub 1/2}(2νEC/EC) > 2.0×10{sup 20} yr at a 90%confidence level (C.L.) was obtained from a preliminary analysis of data obtained over 2250 h of measurements with about 23.2 g sample enriched in the isotope {sup 106}Cd to 99.57%. The limits T{sub 1/2}(KL, 2741 keV) > 0.9 × 10{sup 20} yr and T{sub 1/2}(KK, 2718 keV) ≫ 1.4 × 10{sup 20} yr at a 90% C.L. on the neutrinoless decaymore » of {sup 106}Cd were obtained from measurements performed with the Obelix low-background spectrometer from high-purity germanium (HPGe spectrometer) for a sample of mass about 23.2 g enriched in the isotope {sup 106}Cd.« less

System Design and Implementation of the Detector Assembly of the Astro-H Soft X-Ray Spectrometer

NASA Technical Reports Server (NTRS)

Chiao, M. P.; Adams, J.; Goodwin, P.; Hobson, C.W.; Kelley, R. L.; Kilbourne, C. A.; McCammom, D.; McGuinness, D. S.; Moseley, S. J.; Porter, F. S.;

The Marshall Grazing Incidence X-ray Spectrometer

NASA Astrophysics Data System (ADS)

Kobayashi, Ken; Winebarger, Amy R.; Savage, Sabrina; Champey, Patrick; Cheimets, Peter N.; Hertz, Edward; Bruccoleri, Alexander R.; Golub, Leon; Ramsey, Brian; Ranganathan, Jaganathan; Marquez, Vanessa; Allured, Ryan; Parker, Theodore; Heilmann, Ralf K.; Schattenburg, Mark L.

2017-08-01

The Marshall Grazing Incidence X-ray Spectrometer (MaGIXS) is a NASA sounding rocket instrument designed to obtain spatially resolved soft X-ray spectra of the solar atmosphere in the 6-24 Å (0.5-2.0 keV) range. The instrument consists of a single shell Wolter Type-I telescope, a slit, and a spectrometer comprising a matched pair of grazing incidence parabolic mirrors and a planar varied-line space diffraction grating. The instrument is designed to achieve a 50 mÅ spectral resolution and 5 arcsecond spatial resolution along a +/-4-arcminute long slit, and launch is planned for 2019. We report on the status and our approaches for fabrication and alignment for this novel optical system. The telescope and spectrometer mirrors are replicated nickel shells, and are currently being fabricated at the NASA Marshall Space Flight Center. The diffraction grating is currently under development by the Massachusetts Institute of Technology (MIT); because of the strong line spacing variation across the grating, it will be fabricated through e-beam lithography.

[Development of X-ray excited fluorescence spectrometer].

PubMed

Ni, Chen; Gu, Mu; Di, Wang; Cao, Dun-Hua; Liu, Xiao-Lin; Huang, Shi-Ming

2009-08-01

An X-ray excited fluorescence spectrometer was developed with an X-ray tube and a spectrometer. The X-ray tube, spectrometer, autocontrol method and data processing selected were roundly evaluated. The wavelength and detecting efficiency of the apparatus were calibrated with the mercury and tungsten bromine standard lamps, and the X-ray excited emission spectra of BaF2, Cs I (Tl) crystals were measured. The results indicate that the apparatus has advantages of good wavelength resolution, high stability, easy to operation and good radioprotection. It is a wery effective tool for exploration of new scintillation materials.

Imaging crystal spectrometer for high-resolution x-ray measurements on electron beam ion traps and tokamaks

DOE PAGES

Beiersdorfer, P.; Magee, E. W.; Hell, N.; ...

2016-09-09

Here, we describe a crystal spectrometer implemented on the Livermore electron beam ion traps that employ two spherically bent quartz crystals and a cryogenically cooled back-illuminated charge-coupled device detector to measure x rays with a nominal resolving power of λ/Δλ ≥ 10 000. Its focusing properties allow us to record x rays either with the plane of dispersion perpendicular or parallel to the electron beam and, thus, to preferentially select one of the two linear x-ray polarization components. Moreover, by choice of dispersion plane and focussing conditions, we use the instrument either to image the distribution of the ions withinmore » the 2 cm long trap region, or to concentrate x rays of a given energy to a point on the detector, which optimizes the signal-to-noise ratio. We demonstrate the operation and utility of the new instrument by presenting spectra of Mo 34+, which prepares the instrument for use as a core impurity diagnostic on the NSTX-U spherical torus and other magnetic fusion devices that employ molybdenum as plasma facing components.« less

Thin-window high-efficiency position sensitive proportional counter for the vacuum flat crystal spectrometers on the Lawrence Livermore National Laboratory electron beam ion trap (abstract)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Brown, G. V.; Beiersdorfer, P.; Goddard, R.

2001-01-01

We have mounted 1 {mu}m thick aluminized polyimide windows onto the position sensitive proportional counters employed by the wide-band flat crystal spectrometers at the Lawrence Livermore National Laboratory electron beam ion trap experiment. The aluminized polyimide, supported by thin wires across the short axis of the window, is used to isolate the detection chamber of the proportional counters, which operate at a pressure of 760 Torr, from the vacuum chamber of the spectrometer. The windows are modified versions of those developed for the proportional counters which were used during ground calibration of the Chandra X-ray Observatory. The transmission properties ofmore » these windows are, therefore, well known. The increased transmission efficiency of the polyimide windows relative to the 4 {mu}m thick polypropylene window material previously employed by our proportional counters has extended the useful range of the spectrometer from roughly 20 to 30 Aa at energies below the carbon edge, as well as increasing detection efficiency at wavelengths beyond the carbon edge. Using an octadecyl hydrogen maleate crystal with 2d=63.5Aa, we demonstrate the increased wavelength coverage by measuring the resonance, intercombination, and forbidden lines in helium-like NVII in two different density regimes. The thin polyimide windows have also increased the efficiency of the spectrometers entire wavelength range. To demonstrate the increased efficiency we compare the FeXVII spectrum in the 15--17 Aa band measured with the 1 {mu}m aluminized polyimide windows to the 4 {mu}m aluminized polypropylene windows. The comparison shows an average increase in efficiency of {approx}40%. The polyimide windows have a significantly lower leak rate than the polypropylene windows making it possible to achieve approximately an order of magnitude lower pressure in the spectrometer vacuum chamber which reduces the gas load on the trap region.« less

In-Flight Performance of the Soft X-Ray Spectrometer Detector System on ASTRO-H

NASA Technical Reports Server (NTRS)

Porter, Frederick S.; Boyce, Kevin R.; Chiao, Meng P.; Eckart, Megan E.; Fujimoto, Ryuichi; Ishisaki, Yoshitaka; Kelley, Richard L.; Kilbourne, Carolina A.; Leutenegger, Maurice A.; McCammon, Dan;

In-flight performance of the soft x-ray spectrometer detector system on Astro-H

NASA Astrophysics Data System (ADS)

Porter, Frederick S.; Boyce, Kevin R.; Chiao, Meng P.; Eckart, Megan E.; Fujimoto, Ryuichi; Ishisaki, Yoshitaka; Kilbourne, Caroline Anne; Leutenegger, Maurice A.; McCammon, Daniel; Mitsuda, Kazuhisa; Sato, Kosuke; Seta, Hiromi; Sawada, Makoto; Sneiderman, Gary A.; Szymkowiak, Andrew E.; Takei, Yoh; Tashiro, Makoto S.; Tsujimoto, Masahiro; Watanabe, Tomomi; Yamada, Shinya

2018-01-01

The soft x-ray spectrometer (SXS) instrument was launched aboard the Astro-H (Hitomi) observatory on February 17, 2016. The SXS is based on a high-sensitivity x-ray calorimeter detector system that has been successfully deployed in many ground and suborbital spectrometers. The instrument was to provide essential diagnostics for nearly every class of x-ray emitting objects from the atmosphere of Jupiter to the outskirts of galaxy clusters, without degradation for spatially extended objects. The SXS detector system consisted of a 36-pixel cryogenic microcalorimeter array operated at a heat sink temperature of 50 mK. In preflight testing, the detector system demonstrated a resolving power of better than 1300 at 6 keV with a simultaneous bandpass from below 0.3 keV to above 12 keV with a timing precision better than 100 μs. In addition, a solid-state anticoincidence detector was placed directly behind the detector array for background suppression. The detector error budget included the measured interference from the SXS cooling system and the spacecraft. Additional margin for on-orbit gain stability and on-orbit spacecraft interference were also included predicting an on-orbit performance that meets or exceeds the 7-eV FWHM at 6-keV requirement. The actual on-orbit spectral resolution was better than 5 eV FWHM at 6 keV, easily satisfying the instrument requirement. Here, we discuss the actual on-orbit performance of the SXS detector system and compare this to performance in preflight testing and the on-orbit predictions. We will also discuss the on-orbit gain stability, additional on-orbit interference, and measurements of the on-orbit background.

BiI 3 Crystals for High Energy Resolution Gamma-Ray Spectroscopy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nino, Juan C.; Baciak, James; Johns, Paul

2017-04-12

BiI 3 had been investigated for its unique properties as a layered compound semiconductor for many decades. However, despite the exceptional atomic, physical, and electronic properties of this material, good resolution gamma ray spectra had never been reported for BiI 3. The shortcomings that previously prevented BiI 3 from reaching success as a gamma ray sensor were, through this project, identified and suppressed to unlock the performance of this promising compound. Included in this work were studies on a number of methods which have, for the first time, enabled BiI 3 to exhibit spectral performance rivaling many other candidate semiconductorsmore » for room temperature gamma ray sensors. New approaches to crystal growth were explored that allow BiI 3 spectrometers to be fabricated with up to 2.2% spectral resolution at 662 keV. Fundamental studies on trap states, dopant incorporation, and polarization were performed to enhance performance of this compound. Additionally, advanced detection techniques were applied to display the capabilities of high quality BiI 3 spectrometers. Overall, through this work, BiI 3 has been revealed as a potentially transformative material for nuclear security and radiation detection sciences.« less

High-energy-resolution monochromator for nuclear resonant scattering of synchrotron radiation by Te-125 at 35.49 keV

NASA Astrophysics Data System (ADS)

Imai, Yasuhiko; Yoda, Yoshitaka; Kitao, Shinji; Masuda, Ryo; Higashitaniguchi, Satoshi; Inaba, Chika; Seto, Makoto

2007-09-01

We have developed a high-resolution monochromator (HRM) for the measurement of nuclear resonant scattering (NRS) of synchrotron radiation by Te-125 at 35.49 keV using the backscattering of sapphire (9 1 -10 68). HRMs for nuclei with excitation energies less than 30 keV have been successfully developed using high angle diffractions by silicon crystals. Nearly perfect silicon crystal, however, is not suitable for high efficient HRMs at higher energy regions because the symmetry of the crystal structure is high and the Debye-temperature is low. Therefore, we used high quality synthetic sapphire crystal, which has low symmetry of crystal structure and high Debye-temperature. The temperature of the crystal was precisely controlled around 218 K to diffract synchrotron radiation with a Bragg angle of π/2 - 0.52 mrad. Energy was tuned by changing the crystal temperature under the condition of constant diffraction angle. Energy resolution was measured by detecting nuclear forward scattering by Te-125 in enriched TeO II. The relative energy resolution of 2.1×10 -7 is achieved, that is 7.5 meV in energy bandwidth. This HRM opens studies on element-specific dynamics and electronic state of substances containing Te-125.

Calibration of the Microcalorimeter Spectrometer On-Board the Hitomi (Astro-H) Observatory (invited)

NASA Technical Reports Server (NTRS)

Eckart, M. E.; Boyce, K. R.; Brown, G. V.; Chiao, M. P.; Fujimoto, R.; Haas, D.; Den Herder, J.-W.; Ishisaki, Y.; Kelley, R. L.; Kilbourne, C. A.;

Design Parameters and Objectives of a High-­Resolution X-­ray Imaging Crystal Spectrometer for the Large Helical Device (LHD)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Bitter, M; Gates, D; Neilson, H

A high-resolution X-ray imaging crystal spectrometer, whose instrumental concept was thoroughly tested on NSTX and Alcator C-Mod, is presently being designed for LHD. The instrument will record spatially resolved spectra of helium-like Ar16+ and provide ion temperature profiles with spatial and temporal resolutions of 1 cm and > 10 ms which are obtained by a tomographic inversion of the spectral data, using the stellarator equilibrium reconstruction codes, STELLOPT and PIES. Since the spectrometer will be equipped with radiation hardened, high count rate, PILATUS detectors,, it is expected to be operational for all experimental conditions on LHD, which include plasmas ofmore » high density and plasmas with auxiliary RF and neutral beam heating. The special design features required by the magnetic field structure at LHD will be described.« less

Measurement of the electron and ion temperatures by the x-ray imaging crystal spectrometer on joint Texas experimental tokamak

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yan, W.; Chen, Z. Y., E-mail: zychen@hust.edu.cn; Huang, D. W.

An x-ray imaging crystal spectrometer has been developed on joint Texas experimental tokamak for the measurement of electron and ion temperatures from the K{sub α} spectra of helium-like argon and its satellite lines. A two-dimensional multi-wire proportional counter has been applied to detect the spectra. The electron and ion temperatures have been obtained from the Voigt fitting with the spectra of helium-like argon ions. The profiles of electron and ion temperatures show the dependence on electron density in ohmic plasmas.

Evidence for solar flare directivity from the Gamma-Ray Spectrometer aboard the SMM satellite

NASA Technical Reports Server (NTRS)

Vestrand, W. T.; Forrest, D. J.; Chupp, E. L.; Rieger, E.; Share, G. H.

1986-01-01

A number of observations from the SMM Gamma-Ray Spectrometer are presented that altogether strongly indicate that the high-energy emission from flares is anisotropic. They are: (1) the fraction of events detected at energies above 300 keV near the limb is significantly higher than is expected for isotropically emitting flares; (2) there is a statistically significant center-to-limb variation in the 300-1000-keV spectra of flares; and (3) nearly all of the events detected at above 10 MeV are located near the limb.

Advanced Laboratory NMR Spectrometer with Applications.

ERIC Educational Resources Information Center

Biscegli, Clovis; And Others

1982-01-01

A description is given of an inexpensive nuclear magnetic resonance (NMR) spectrometer suitable for use in advanced laboratory courses. Applications to the nondestructive analysis of the oil content in corn seeds and in monitoring the crystallization of polymers are presented. (SK)

A balloon-borne instrument for high-resolution astrophysical spectroscopy in the 20-8000 keV energy range

NASA Technical Reports Server (NTRS)

Paciesas, W. S.; Baker, R.; Boclet, D.; Brown, S.; Cline, T.; Costlow, H.; Durouchoux, P.; Ehrmann, C.; Gehrels, N.; Hameury, J. M.

1983-01-01

The Low Energy Gamma ray Spectrometer (LEGS) is designed to perform fine energy resolution measurements of astrophysical sources. The instrument is configured for a particular balloon flight with either of two sets of high purity germanium detectors. In one configuration, the instrument uses an array of three coaxial detectors (effective volume equal to or approximately 230 cubic cm) inside an NaI (T1) shield and collimator (field of view equal to or approximately 16 deg FWHM) and operates in the 80 to 8000 keV energy range. In the other configuration, three planar detectors (effective area equal to or approximately square cm) surrounded by a combination of passive Fe and active NaI for shielding and collimation (field of view equal to or approximately 5 deg x 10 deg FWHM) are optimized for the 20 to 200 keV energy range. In a typical one day balloon flight, LEGS sensitivity limit (3 sigma) for narrow line features is less than or approximately .0008 ph/cm/s square (coaxial array: 80 to 2000 keV) and less than or approximately .0003 ph/square cm/s (planar array: 50 to 150 keV).

Resonant inelastic X-ray scattering spectrometer with 25meV resolution at the Cu K -edge

DOE PAGES

Ketenoglu, Didem; Harder, Manuel; Klementiev, Konstantin; ...

2015-06-27

An unparalleled resolution is reported with an inelastic X-ray scattering instrument at the CuK-edge. Based on a segmented concave analyzer, featuring single-crystal quartz (SiO 2) pixels, the spectrometer delivers a resolution near 25meV (FWHM) at 8981eV. Besides the quartz analyzer, the performance of the spectrometer relies on a four-bounce Si(553) high-resolution monochromator and focusing Kirkpatrick–Baez optics. The measured resolution agrees with the ray-tracing simulation of an ideal spectrometer. The performance of the spectrometer is demonstrated by reproducing the phonon dispersion curve of a beryllium single-crystal.

Ultra compact spectrometer apparatus and method using photonic crystals

NASA Technical Reports Server (NTRS)

Ting, David Z. (Inventor); Hill, Cory J. (Inventor); Bandara, Sumith V. (Inventor); Gunapala, Sarath D. (Inventor)

2009-01-01

The present invention is directed to methods of photonic crystal formation, and to methods and apparatus for using such photonic crystals, particularly in conjunction with detector arrays. Photonic crystal parameters and detector array parameters are compared to optimize the selection and orientation of a photonic crystal shape. A photonic crystal is operatively positioned relative to a plurality of light sensors. The light sensors can be separated by a pitch distance and positioned within one half of the pitch distance of an exit surface of the photonic crystals.

GaAs Spectrometer for Electron Spectroscopy at Europa

NASA Astrophysics Data System (ADS)

Lioliou, G.; Barnett, A. M.

2016-12-01

We propose a GaAs based electron spectrometer for a hypothetical future mission orbiting Europa. Previous observations at Europa's South Pole with the Hubble Space Telescope of hydrogen Lyman-α and oxygen OI 130.4 nm emissions were consistent with water vapor plumes [Roth et al., 2014, Science 343, 171]. Future observations and analysis of plumes on Europa could provide information about its subsurface structure and the distribution of liquid water within its icy shells [Rhoden at al. 2015, Icarus 253, 169]. In situ low energy (1keV - 100keV) electron spectroscopy along with UV imaging either in situ or with the Hubble Space Telescope Wide Field Camera 3 or similar would allow verification of the auroral observations being due to electron impact excitation of water vapor plumes. The proposed spectrometer includes a novel GaAs p+-i-n+ photodiode and a custom-made charge-sensitive preamplifier. The use of an early prototype GaAs detector for direct electron spectroscopy has already been demonstrated in ground based applications [Barnett et al., 2012, J. Instrum. 7, P09012]. Based on previous radiation hardness measurements of GaAs, the expected duration of the mission without degradation of the detector performance is estimated to be 4 months. Simulations and laboratory experiments characterising the detection performance of the proposed system are presented.

Laboratory-based micro-X-ray fluorescence setup using a von Hamos crystal spectrometer and a focused beam X-ray tube

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kayser, Y., E-mail: yves.kayser@psi.ch; Paul Scherrer Institut, 5232 Villigen-PSI; Błachucki, W.

2014-04-15

The high-resolution von Hamos bent crystal spectrometer of the University of Fribourg was upgraded with a focused X-ray beam source with the aim of performing micro-sized X-ray fluorescence (XRF) measurements in the laboratory. The focused X-ray beam source integrates a collimating optics mounted on a low-power micro-spot X-ray tube and a focusing polycapillary half-lens placed in front of the sample. The performances of the setup were probed in terms of spatial and energy resolution. In particular, the fluorescence intensity and energy resolution of the von Hamos spectrometer equipped with the novel micro-focused X-ray source and a standard high-power water-cooled X-raymore » tube were compared. The XRF analysis capability of the new setup was assessed by measuring the dopant distribution within the core of Er-doped SiO{sub 2} optical fibers.« less

Low-temperature THz time domain waveguide spectrometer with butt-coupled emitter and detector crystal.

PubMed

Qiao, W; Stephan, D; Hasselbeck, M; Liang, Q; Dekorsy, T

2012-08-27

A compact high-resolution THz time-domain waveguide spectrometer that is operated inside a cryostat is demonstrated. A THz photo-Dember emitter and a ZnTe electro-optic detection crystal are directly attached to a parallel copper-plate waveguide. This allows the THz beam to be excited and detected entirely inside the cryostat, obviating the need for THz-transparent windows or external THz mirrors. Since no external bias for the emitter is required, no electric feed-through into the cryostat is necessary. Using asynchronous optical sampling, high resolution THz spectra are obtained in the frequency range from 0.2 to 2.0 THz. The THz emission from the photo-Dember emitter and the absorption spectrum of 1,2-dicyanobenzene film are measured as a function of temperature. An absorption peak around 750 GHz of 1,2-dicyanobenzene displays a blue shift with increasing temperature.

The growth of deactivated layers on CsI(Na) scintillating crystals

NASA Technical Reports Server (NTRS)

Goodman, N. B.

1975-01-01

An effective and sensitive measurement of the depth of a deactivated or dead layer can be obtained from the relative attenuation of the 22.162 KeV and 87.9 KeV X-rays emitted by Cd 109. The alpha-particles emitted by Am 241 are also useful in measuring dead layers less than 25 microns. The properties and temporal development of dead layers are discussed in detail. The rate of growth of a deal layer is closely related to the ambient humidity, and the damage to the crystal is irreversible by any known process. The dead layer can be minimized by polishing all crystal surfaces and by keeping the crystal in a vacuum or a dry atmosphere. Since a dead layer seriously inhibits the response of a crystal to X-rays of energies below approximately 20 keV, CsI(Na) detectors should not be used at these energies unless precautions are taken to ensure that no dead layer forms.

Precision mechanical structure of an ultra-high-resolution spectrometer for inelastic X-ray scattering instrument

DOEpatents

Shu, Deming; Shvydko, Yuri; Stoupin, Stanislav A.; Khachatryan, Ruben; Goetze, Kurt A.; Roberts, Timothy

2015-04-14

A method and an ultrahigh-resolution spectrometer including a precision mechanical structure for positioning inelastic X-ray scattering optics are provided. The spectrometer includes an X-ray monochromator and an X-ray analyzer, each including X-ray optics of a collimating (C) crystal, a pair of dispersing (D) element crystals, anomalous transmission filter (F) and a wavelength (W) selector crystal. A respective precision mechanical structure is provided with the X-ray monochromator and the X-ray analyzer. The precision mechanical structure includes a base plate, such as an aluminum base plate; positioning stages for D-crystal alignment; positioning stages with an incline sensor for C/F/W-crystal alignment, and the positioning stages including flexure-based high-stiffness structure.

Ultraviolet Raman Wide-Field Hyperspectral Imaging Spectrometer for Standoff Trace Explosive Detection.

PubMed

Hufziger, Kyle T; Bykov, Sergei V; Asher, Sanford A

2017-02-01

We constructed the first deep ultraviolet (UV) Raman standoff wide-field imaging spectrometer. Our novel deep UV imaging spectrometer utilizes a photonic crystal to select Raman spectral regions for detection. The photonic crystal is composed of highly charged, monodisperse 35.5 ± 2.9 nm silica nanoparticles that self-assemble in solution to produce a face centered cubic crystalline colloidal array that Bragg diffracts a narrow ∼1.0 nm full width at half-maximum (FWHM) UV spectral region. We utilize this photonic crystal to select and image two different spectral regions containing resonance Raman bands of pentaerythritol tetranitrate (PETN) and NH 4 NO 3 (AN). These two deep UV Raman spectral regions diffracted were selected by angle tuning the photonic crystal. We utilized this imaging spectrometer to measure 229 nm excited UV Raman images containing ∼10-1000 µg/cm 2 samples of solid PETN and AN on aluminum surfaces at 2.3 m standoff distances. We estimate detection limits of ∼1 µg/cm 2 for PETN and AN films under these experimental conditions.

Low energy X-ray spectra measured with a mercuric iodide energy dispersive spectrometer in a scanning electron microscope

NASA Technical Reports Server (NTRS)

Iwanczyk, J. S.; Dabrowski, A. J.; Huth, G. C.; Bradley, J. G.; Conley, J. M.

1986-01-01

A mercuric iodide energy dispersive X-ray spectrometer, with Peltier cooling provided for the detector and input field effect transistor, has been developed and tested in a scanning electron microscope. X-ray spectra were obtained with the 15 keV electron beam. An energy resolution of 225 eV (FWHM) for Mn-K(alpha) at 5.9 keV and 195 eV (FWHM) for the Mg-K line at 1.25 keV has been measured. Overall system noise level was 175 eV (FWHM). The detector system characterization with a carbon target demonstrated good energy sensitivity at low energies and lack of significant spectral artifacts at higher energies.

Absolute radiant power measurement for the Au M lines of laser-plasma using a calibrated broadband soft X-ray spectrometer with flat-spectral response.

PubMed

Troussel, Ph; Villette, B; Emprin, B; Oudot, G; Tassin, V; Bridou, F; Delmotte, F; Krumrey, M

2014-01-01

CEA implemented an absolutely calibrated broadband soft X-ray spectrometer called DMX on the Omega laser facility at the Laboratory for Laser Energetics (LLE) in 1999 to measure radiant power and spectral distribution of the radiation of the Au plasma. The DMX spectrometer is composed of 20 channels covering the spectral range from 50 eV to 20 keV. The channels for energies below 1.5 keV combine a mirror and a filter with a coaxial photo-emissive detector. For the channels above 5 keV the photoemissive detector is replaced by a conductive detector. The intermediate energy channels (1.5 keV < photon energy < 5 keV) use only a filter and a coaxial detector. A further improvement of DMX consists in flat-response X-ray channels for a precise absolute measurement of the photon flux in the photon energy range from 0.1 keV to 6 keV. Such channels are equipped with a filter, a Multilayer Mirror (MLM), and a coaxial detector. We present as an example the development of channel for the gold M emission lines in the photon energy range from 2 keV to 4 keV which has been successfully used on the OMEGA laser facility. The results of the radiant power measurements with the new MLM channel and with the usual channel composed of a thin titanium filter and a coaxial detector (without mirror) are compared. All elements of the channel have been calibrated in the laboratory of the Physikalisch-Technische Bundesanstalt, Germany's National Metrology Institute, at the synchrotron radiation facility BESSY II in Berlin using dedicated well established and validated methods.

Inverse time-of-flight spectrometer for beam plasma research

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yushkov, Yu. G., E-mail: yuyushkov@gmail.com; Zolotukhin, D. B.; Tyunkov, A. V.

2014-08-15

The paper describes the design and principle of operation of an inverse time-of-flight spectrometer for research in the plasma produced by an electron beam in the forevacuum pressure range (5–20 Pa). In the spectrometer, the deflecting plates as well as the drift tube and the primary ion beam measuring system are at high potential with respect to ground. This provides the possibility to measure the mass-charge constitution of the plasma created by a continuous electron beam with a current of up to 300 mA and electron energy of up to 20 keV at forevacuum pressures in the chamber placed atmore » ground potential. Research results on the mass-charge state of the beam plasma are presented and analyzed.« less

The differential absorption hard x-ray spectrometer at the Z facility

DOE PAGES

Bell, Kate S.; Coverdale, Christine A.; Ampleford, David J.; ...

2017-08-03

The Differential Absorption Hard X-ray (DAHX) spectrometer is a diagnostic developed to measure time-resolved radiation between 60 keV and 2 MeV at the Z Facility. It consists of an array of 7 Si PIN diodes in a tungsten housing that provides collimation and coarse spectral resolution through differential filters. DAHX is a revitalization of the Hard X-Ray Spectrometer (HXRS) that was fielded on Z prior to refurbishment in 2006. DAHX has been tailored to the present radiation environment in Z to provide information on the power, spectral shape, and time profile of the hard emission by plasma radiation sources drivenmore » by the Z Machine.« less

Development and performance of a suprathermal electron spectrometer to study auroral precipitations

NASA Astrophysics Data System (ADS)

Ogasawara, Keiichi; Grubbs, Guy; Michell, Robert G.; Samara, Marilia; Stange, Jason L.; Trevino, John A.; Webster, James; Jahn, Jörg-Micha

2016-05-01

The design, development, and performance of Medium-energy Electron SPectrometer (MESP), dedicated to the in situ observation of suprathermal electrons in the auroral ionosphere, are summarized in this paper. MESP employs a permanent magnet filter with a light tight structure to select electrons with proper energies guided to the detectors. A combination of two avalanche photodiodes and a large area solid-state detector (SSD) provided 46 total energy bins (1 keV resolution for 3-20 keV range for APDs, and 7 keV resolution for >20 keV range for SSDs). Multi-channel ultra-low power application-specific integrated circuits are also verified for the flight operation to read-out and analyze the detector signals. MESP was launched from Poker Flat Research Range on 3 March 2014 as a part of ground-to-rocket electrodynamics-electrons correlative experiment (GREECE) mission. MESP successfully measured the precipitating electrons from 3 to 120 keV in 120-ms time resolution and characterized the features of suprathermal distributions associated with auroral arcs throughout the flight. The measured electrons were showing the inverted-V type spectra, consistent with the past measurements. In addition, investigations of the suprathermal electron population indicated the existence of the energetic non-thermal distribution corresponding to the brightest aurora.

Development and performance of a suprathermal electron spectrometer to study auroral precipitations.

PubMed

Ogasawara, Keiichi; Grubbs, Guy; Michell, Robert G; Samara, Marilia; Stange, Jason L; Trevino, John A; Webster, James; Jahn, Jörg-Micha

2016-05-01

The design, development, and performance of Medium-energy Electron SPectrometer (MESP), dedicated to the in situ observation of suprathermal electrons in the auroral ionosphere, are summarized in this paper. MESP employs a permanent magnet filter with a light tight structure to select electrons with proper energies guided to the detectors. A combination of two avalanche photodiodes and a large area solid-state detector (SSD) provided 46 total energy bins (1 keV resolution for 3-20 keV range for APDs, and 7 keV resolution for >20 keV range for SSDs). Multi-channel ultra-low power application-specific integrated circuits are also verified for the flight operation to read-out and analyze the detector signals. MESP was launched from Poker Flat Research Range on 3 March 2014 as a part of ground-to-rocket electrodynamics-electrons correlative experiment (GREECE) mission. MESP successfully measured the precipitating electrons from 3 to 120 keV in 120-ms time resolution and characterized the features of suprathermal distributions associated with auroral arcs throughout the flight. The measured electrons were showing the inverted-V type spectra, consistent with the past measurements. In addition, investigations of the suprathermal electron population indicated the existence of the energetic non-thermal distribution corresponding to the brightest aurora.

Development and Performance of a Suprathermal Electron Spectrometer to Study Auroral Precipitations

NASA Technical Reports Server (NTRS)

Ogasawara, Keiichi; Grubbs, Guy, II; Michell, Robert G.; Samara, Maria; Stange, Jason L.; Trevino, John A.; Webster, James; Jahn, Jorg-Micha

2016-01-01

The design, development, and performance of Medium-energy Electron SPectrometer (MESP), dedicated to the in situ observation of suprathermal electrons in the auroral ionosphere, are summarized in this paper. MESP employs a permanent magnet filter with a light tight structure to select electrons with proper energies guided to the detectors. A combination of two avalanche photodiodes and a large area solid-state detector (SSD) provided 46 total energy bins (1 keV resolution for 3-20 keV range for APDs, and 7 keV resolution for greater than 20 keV range for SSDs). Multi-channel ultra-low power application-specific integrated circuits are also verified for the flight operation to read-out and analyze the detector signals. MESP was launched from Poker F1at Research Range on 3 March 2014 as a part of ground-to-rocket electrodynamics-electrons correlative experiment (GREECE) mission. MESP successfully measured the precipitating electrons from 3 to 120 keV in 120-ms time resolution and characterized the features of suprathermal distributions associated with auroral arcs throughout the flight. The measured electrons were showing the inverted-V type spectra, consistent with the past measurements. In addition, investigations of the suprathermal electron population indicated the existence of the energetic non-thermal distribution corresponding to the brightest aurora.

Absolute Calibration of Image Plate for electrons at energy between 100 keV and 4 MeV

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, H; Back, N L; Eder, D C

2007-12-10

The authors measured the absolute response of image plate (Fuji BAS SR2040) for electrons at energies between 100 keV to 4 MeV using an electron spectrometer. The electron source was produced from a short pulse laser irradiated on the solid density targets. This paper presents the calibration results of image plate Photon Stimulated Luminescence PSL per electrons at this energy range. The Monte Carlo radiation transport code MCNPX results are also presented for three representative incident angles onto the image plates and corresponding electron energies depositions at these angles. These provide a complete set of tools that allows extraction ofmore » the absolute calibration to other spectrometer setting at this electron energy range.« less

A spatially resolving x-ray crystal spectrometer for measurement of ion-temperature and rotation-velocity profiles on the Alcator C-Mod tokamak.

PubMed

Hill, K W; Bitter, M L; Scott, S D; Ince-Cushman, A; Reinke, M; Rice, J E; Beiersdorfer, P; Gu, M-F; Lee, S G; Broennimann, Ch; Eikenberry, E F

2008-10-01

A new spatially resolving x-ray crystal spectrometer capable of measuring continuous spatial profiles of high resolution spectra (lambda/d lambda>6000) of He-like and H-like Ar K alpha lines with good spatial (approximately 1 cm) and temporal (approximately 10 ms) resolutions has been installed on the Alcator C-Mod tokamak. Two spherically bent crystals image the spectra onto four two-dimensional Pilatus II pixel detectors. Tomographic inversion enables inference of local line emissivity, ion temperature (T(i)), and toroidal plasma rotation velocity (upsilon(phi)) from the line Doppler widths and shifts. The data analysis techniques, T(i) and upsilon(phi) profiles, analysis of fusion-neutron background, and predictions of performance on other tokamaks, including ITER, will be presented.

A beta-ray spectrometer based on a two-or three silicon detector coincidence telescope

NASA Astrophysics Data System (ADS)

Horowitz, Y. S.; Weizman, Y.; Hirning, C. R.

1996-02-01

This report describes the operation of a beta-ray energy spectrometer based on a silicon detector telescope using two or three elements. The front detector is a planar, totally-depleted, silicon surface barrier detector that is 97 μm thick, the back detector is a room-temperature, lithium compensated, silicon detector that is 5000 μm thick, and the intermediate detector is similar to the front detector but 72 μm thick and intended to be used only in intense photon fields. The three detectors are mounted in a light-tight aluminum housing. The capability of the spectrometer to reject photons is based upon the fact that the incident photon will have a small probability of simultaneously losing detectable energy in two detectors, and an even smaller probability of losing detectable energy in all three detectors. Electrons will, however, almost always record measurable events in either the front two or all three detectors. A coincidence requirement between the detectors thus rejects photon induced events. With a 97 μm thick detector the lower energy coincidence threshold is approximately 110 keV. With an ultra-thin 40 μm thick front detector, and operated at 15°C, the spectrometer is capable of detecting even 60-70 keV electrons with a coincidence efficiency of 60%. The spectrometer has been used to measure beta radiation fields in CANDU reactor working environments, and the spectral information is intended to support dose algorithms for the LiF TLD chips used in the Ontario Hydro dosimetry program.

The average 0.5-200 keV spectrum of local active galactic nuclei and a new determination of the 2-10 keV luminosity function at z ≈ 0

NASA Astrophysics Data System (ADS)

Ballantyne, D. R.

2014-01-01

The broad-band X-ray spectra of active galactic nuclei (AGNs) contains information about the nuclear environment from Schwarzschild radii scales (where the primary power law is generated in a corona) to distances of ˜1 pc (where the distant reflector may be located). In addition, the average shape of the X-ray spectrum is an important input into X-ray background synthesis models. Here, local (z ≈ 0) AGN luminosity functions (LFs) in five energy bands are used as a low-resolution, luminosity-dependent X-ray spectrometer in order to constrain the average AGN X-ray spectrum between 0.5 and 200 keV. The 15-55 keV LF measured by Swift-BAT is assumed to be the best determination of the local LF, and then a spectral model is varied to determine the best fit to the 0.5-2 keV, 2-10 keV, 3-20 keV and 14-195 keV LFs. The spectral model consists of a Gaussian distribution of power laws with a mean photon-index <Γ> and cutoff energy Ecut, as well as contributions from distant and disc reflection. The reflection strength is parametrized by varying the Fe abundance relative to solar, AFe, and requiring a specific Fe Kα equivalent width (EW). In this way, the presence of the X-ray Baldwin effect can be tested. The spectral model that best fits the four LFs has <Γ> = 1.85 ± 0.15, E_{cut}=270^{+170}_{-80} keV, A_{Fe}=0.3^{+0.3}_{-0.15}. The sub-solar AFe is unlikely to be a true measure of the gas-phase metallicity, but indicates the presence of strong reflection given the assumed Fe Kα EW. Indeed, parametrizing the reflection strength with the R parameter gives R=1.7^{+1.7}_{-0.85}. There is moderate evidence for no X-ray Baldwin effect. Accretion disc reflection is included in the best-fitting model, but it is relatively weak (broad iron Kα EW < 100 eV) and does not significantly affect any of the conclusions. A critical result of our procedure is that the shape of the local 2-10 keV LF measured by HEAO-1 and MAXI is incompatible with the LFs measured in the hard X

Data reduction and analysis for the graphite crystal X-ray spectrometer and polarimeter experiment flown aboard OSO-8 spacecraft

NASA Technical Reports Server (NTRS)

Novick, R.

1980-01-01

The documentation and software programs developed for the reception, initial processing (quickbook), and production analysis of data obtained by solar X-ray spectroscopy, stellar spectroscopy, and X-ray polarimetry experiments on OSO-8 are listed. The effectiveness and sensitivity of the Bragg crystal scattering instruments used are assessed. The polarization data polarimetric data obtained shows that some X-ray sources are polarized and that a larger polarimeter of this type is required to perform the measurements necessary to fully understand the physics of X-ray sources. The scanning Bragg crystal spectrometer was ideally suited for studying rapidly changing solar conditions. Observations of the Crab Nebula and pulsar, Cyg X-1, Cyg X-2, Cyg X-3, Sco X-1, Cen X-3, and Her X-1 are discussed as well as of 4U1656-53 and 4U1820-30. Evidence was obtained for iron line emission from Cyg X-3.

Dominance of high-energy (>150 keV) heavy ion intensities in Earth's middle to outer magnetosphere

NASA Astrophysics Data System (ADS)

Cohen, Ian J.; Mitchell, Donald G.; Kistler, Lynn M.; Mauk, Barry H.; Anderson, Brian J.; Westlake, Joseph H.; Ohtani, Shinichi; Hamilton, Douglas C.; Turner, Drew L.; Blake, J. Bernard; Fennell, Joseph F.; Jaynes, Allison N.; Leonard, Trevor W.; Gerrard, Andrew J.; Lanzerotti, Louis J.; Allen, Robert C.; Burch, James L.

2017-09-01

Previous observations have driven the prevailing assumption in the field that energetic ions measured by an instrument using a bare solid state detector (SSD) are predominantly protons. However, new near-equatorial energetic particle observations obtained between 7 and 12 RE during Phase 1 of the Magnetospheric Multiscale mission challenge the validity of this assumption. In particular, measurements by the Energetic Ion Spectrometer (EIS) instruments have revealed that the intensities of heavy ion species (specifically oxygen and helium) dominate those of protons at energies ≳150-220 keV in the middle to outer (>7 RE) magnetosphere. Given that relative composition measurements can drift as sensors degrade in gain, quality cross-calibration agreement between EIS observations and those from the SSD-based Fly's Eye Energetic Particle Spectrometer (FEEPS) sensors provides critical support to the veracity of the measurement. Similar observations from the Radiation Belt Storm Probes Ion Composition Experiment (RBSPICE) instruments aboard the Van Allen Probes spacecraft extend the ion composition measurements into the middle magnetosphere and reveal a strongly proton-dominated environment at L≲6 but decreasing proton intensities at L≳6. It is concluded that the intensity dominance of the heavy ions at higher energies (>150 keV) arises from the existence of significant populations of multiply-charged heavy ions, presumably of solar wind origin.

Neutron molecular spectroscopy using a white beam time-of-flight spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chen, S.; Jorgensen, J.D.; Berney, C.V.

1978-01-01

An inverted-geometry white beam TOF neutron spectrometer using an extended graphite crystal analyzer was constructed at the CP-5 reactor at Argonne. A performance test of the spectrometer for incoherent inelastic scattering studies was made with five selected molecular solids. The results demonstrate the utility of such a spectrometer for investigation of lattice vibrational spectra of hydrogenous compounds in the energy range 0--400 cm/sup -1/. We describe design considerations and energy resolution of the spectrometer, and discuss observed low-frequency spectra of acetic acid (CH/sub 3/COOH, CD/sub 3/COOH, and CH/sub 3/COOD), cyclohexane, and cyclopentane.

Tests of a solution-grown stilbene scintillator in mono-energetic neutron beams of 565 keV and 5 MeV

NASA Astrophysics Data System (ADS)

Dioni, Luca; Gressier, Vincent; Nardin, Gaëlle; Jacqmin, Robert; Stout, Brian; Sumini, Marco

2018-02-01

The results of measurements performed with a solution-grown stilbene scintillator placed in reference mono-energetic neutron fields are presented. The ∅ 25 mm organic scintillator was positioned in 5 MeV and 565 keV neutron fields delivered by the AIFIRA facility at CENBG. The goal of the experiment was to assess the performance of the solution-grown stilbene crystal (n- γ discrimination, response, anisotropy, sensitivity) relative to that of a BC501A liquid scintillator of larger size. Neutron pulse height spectra after gamma discrimination are compared. The results show that the stilbene crystal not only has a better discrimination capability than the BC501A (35% higher FoM) at 5 MeV, but is also able to separate neutrons from gamma-rays at 565 keV and below, a range where the BC501A is inoperative. This study also confirms the anisotropy of the crystal response, as already observed by other groups at different energies.

Stitching Type Large Aperture Depolarizer for Gas Monitoring Imaging Spectrometer

NASA Astrophysics Data System (ADS)

Liu, X.; Li, M.; An, N.; Zhang, T.; Cao, G.; Cheng, S.

2018-04-01

To increase the accuracy of radiation measurement for gas monitoring imaging spectrometer, it is necessary to achieve high levels of depolarization of the incoming beam. The preferred method in space instrument is to introduce the depolarizer into the optical system. It is a combination device of birefringence crystal wedges. Limited to the actual diameter of the crystal, the traditional depolarizer cannot be used in the large aperture imaging spectrometer (greater than 100 mm). In this paper, a stitching type depolarizer is presented. The design theory and numerical calculation model for dual babinet depolarizer were built. As required radiometric accuracies of the imaging spectrometer with 250 mm × 46 mm aperture, a stitching type dual babinet depolarizer was design in detail. Based on designing the optimum structural parmeters the tolerance of wedge angle refractive index, and central thickness were given. The analysis results show that the maximum residual polarization degree of output light from depolarizer is less than 2 %. The design requirements of polarization sensitivity is satisfied.

The High Resolution Microcalorimeter Soft X-Ray Spectrometer for the Astro-H Mission

NASA Technical Reports Server (NTRS)

Kelley, Richard L.; Mitsuda, Kazuhisa; den Herder, Jan-Willem A.; Aarts, Henri J. M.; Azzarello, Philipp; Boyce, Kevin R.; Brown, Gregory V.; Chiao, Meng P.; de Vries, Cor P.; DiPirro, Michael J.;

High-resolution integrated germanium Compton polarimeter for the γ-ray energy range 80 keV-1 MeV

NASA Astrophysics Data System (ADS)

Sareen, R. A.; Urban, W.; Barnett, A. R.; Varley, B. J.

1995-06-01

Parameters which govern the choice of a detection system to measure the linear polarization of γ rays at low energies are discussed. An integrated polarimeter is described which is constructed from a single crystal of germanium. It is a compact planar device with the sectors defined electrically, and which gives an energy resolution in the add-back mode of 1 keV at 300 keV. Its performance is demonstrated in a series of calibration measurements using both unpolarized radiation from radioactive sources and polarized γ rays from the 168Er(α,2n)170Yb reaction at Eα=25 MeV. Polarization measurements at energies as low as 84 keV have been achieved, where the sensitivity was 0.32±0.09. The sensitivity, efficiency, and energy resolution are reported. Our results indicate that energy resolution should be included in the definition of the figure of merit and we relate the new definition to earlier work. The comparisons show the advantages of the present design in the energy range below 300 keV and its competitiveness up to 1500 keV.

The hard X-ray burst spectrometer event listing, 1980 - 1985

NASA Technical Reports Server (NTRS)

Dennis, B. R.; Orwig, L. E.; Kiplinger, A. L.; Gibson, B. R.; Kennard, G. S.; Tolbert, A. K.

1985-01-01

This event listing is a comprehensive reference for the hard X-ray bursts detected with the Hard X-Ray Burst Spectrometer on the Solar Maximum Mission from the time of launch on February 14, 1980 to September 1985. Over 8000 X-ray events were detected in the energy range from 30 to approx. 500 keV with the vast majority being solar flares. The listing includes the start time, peak time, duration and peak rate of each event.

The hard X-ray burst spectrometer event listing 1980-1987

NASA Technical Reports Server (NTRS)

Dennis, B. R.; Orwig, L. E.; Kiplinger, A. L.; Schwartz, R. A.; Gibson, B. R.; Kennard, G. S.; Tolbert, A. K.; Biesecker, D. A.; Labow, G. J.; Shaver, A.

1988-01-01

This event listing is a comprehensive reference for the Hard X-ray bursts detected with the Hard X-ray Burst Spectrometer on the Solar Maximum Mission from the time of launch 14 February 1980 to December 1987. Over 8600 X-ray events were detected in the energy range from 30 to approx. 600 keV with the vast majority being solar flares. The listing includes the start time, peak time, duration and peak rate of each event.

Ground Calibration of the Astro-H (Hitomi) Soft X-Ray Spectrometer

NASA Technical Reports Server (NTRS)

Eckart, M. E.; Adams, J. S.; Boyce, K. R.; Brown, G. V.; Chiao, Meng P.; Fujimoto, R. J.; Haas, D.; Den Herder, J. W.; Ishisaki, Y.; Kelley, R. L.;

Monolithic liquid crystal waveguide Fourier transform spectrometer for gas species sensing

NASA Astrophysics Data System (ADS)

Chao, Tien-Hsin; Lu, Thomas T.; Davis, Scott R.; Rommel, Scott D.; Farca, George; Luey, Ben; Martin, Alan; Anderson, Michael H.

2011-04-01

Jet Propulsion Lab and Vescent Photonics Inc. and are jointly developing an innovative ultracompact (volume < 10 cm3), ultra-low power (<10-3 Watt-hours per measurement and zero power consumption when not measuring), completely non-mechanical Liquid Crystal Waveguide Fourier Transform Spectrometer (LCWFTS) that will be suitable for a variety of remote-platform, in-situ measurements. These devices are made possible by novel electro-evanescent waveguide architecture, enabling "monolithic chip-scale" Electro Optic-FTS (EO-FTS) sensors. The potential performance of these EO-FTS sensors include: i) a spectral range throughout 0.4-5 μm (25000 - 2000 cm-1), ii) high-resolution (Δλ <= 0.1 nm), iii) high-speed (< 1 ms) measurements, and iv) rugged integrated optical construction. This performance potential enables the detection and quantification of a large number of different atmospheric gases simultaneously in the same air mass and the rugged construction will enable deployment on previously inaccessible platforms. The sensor construction is also amenable for analyzing aqueous samples on remote floating or submerged platforms. We will report a proof-of-principle prototype LCWFTS sensor that has been demonstrated in the near-IR (range of 1450-1700 nm) with a 5 nm resolution. This performance is in good agreement with theoretical models, which are being used to design and build the next generation LCWFTS devices.

High efficiency CsI(Tl)/HgI{sub 2} gamma ray spectrometers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Y.J.; Patt, B.E.; Iwanczyk, J.S.

CsI(Tl)/HgI{sub 2} gamma-ray spectrometers have been constructed using 0.5 inch diameter detectors which show excellent energy resolution: 4.58% FWHM for 662 keV {sup 137}Cs gamma-ray photons. Further efforts have been focused on optimization of larger size ({ge} 1 inch diameter) detector structures and improvement of low noise electronics. In order to take full advantage of scintillation detectors for high energy gamma-rays, larger scintillators are always preferred for their higher detection efficiencies. However, the larger capacitance and higher dark current caused by the larger size of the detector could result in a higher FWHM resolution. Also, the increased probability of includingmore » nonuniformities in larger pieces of crystals makes it more difficult to obtain the high resolutions one obtains from small detectors. Thus for very large volume scintillators, it may be necessary to employ a photodiode (PD) with a sensitive area smaller than the cross-section of the scintillator. Monte Carlo simulations of the light collection for various tapered scintillator/PD configuration were performed in order to find those geometries which resulted in the best light collection. According to the simulation results, scintillators with the most favorable geometry, the conical frustum, have been fabricated and evaluated. The response of a large conical frustum (top-2 inch, bottom-1 inch, 2 inch high) CsI(Tl) scintillator coupled with a 1 inch HgI{sub 2} PD was measured. The energy resolution of the 662 keV peak was 5.57%. The spectrum shows much higher detection efficiency than those from smaller scintillators, i.e., much higher peak-to-Compton ratio in the spectrum.« less

Instrumental background in balloon-borne gamma-ray spectrometers and techniques for its reduction

NASA Technical Reports Server (NTRS)

Gehrels, N.

1985-01-01

Instrumental background in balloon-borne gamma-ray spectrometers is presented. The calculations are based on newly available interaction cross sections and new analytic techniques, and are the most detailed and accurate published to date. Results compare well with measurements made in the 20 keV to 10 MeV energy range by the Goddard Low Energy Gamma-ray Spectrometer (LEGS). The principal components of the continuum background in spectrometers with GE detectors and thick active shields are: (1) elastic neutron scattering of atmospheric neutrons on the Ge nuclei; (2) aperture flux of atmospheric and cosmic gamma rays; (3) beta decays of unstable nuclides produced by nuclear interactions of atmospheric protons and neutrons with Ge nuclei; and (4) shield leakage of atmospheric gamma rays. The improved understanding of these components leads to several recommended techniques for reducing the background.

Development of a spatially resolving x-ray crystal spectrometer for measurement of ion-temperature (T(i)) and rotation-velocity (v) profiles in ITER.

PubMed

Hill, K W; Bitter, M; Delgado-Aparicio, L; Johnson, D; Feder, R; Beiersdorfer, P; Dunn, J; Morris, K; Wang, E; Reinke, M; Podpaly, Y; Rice, J E; Barnsley, R; O'Mullane, M; Lee, S G

2010-10-01

Imaging x-ray crystal spectrometer (XCS) arrays are being developed as a US-ITER activity for Doppler measurement of T(i) and v profiles of impurities (W, Kr, and Fe) with ∼7 cm (a/30) and 10-100 ms resolution in ITER. The imaging XCS, modeled after a prototype instrument on Alcator C-Mod, uses a spherically bent crystal and 2D x-ray detectors to achieve high spectral resolving power (E/dE>6000) horizontally and spatial imaging vertically. Two arrays will measure T(i) and both poloidal and toroidal rotation velocity profiles. The measurement of many spatial chords permits tomographic inversion for the inference of local parameters. The instrument design, predictions of performance, and results from C-Mod are presented.

Development and performance of a suprathermal electron spectrometer to study auroral precipitations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ogasawara, Keiichi, E-mail: kogasawara@swri.edu; Stange, Jason L.; Trevino, John A.

2016-05-15

The design, development, and performance of Medium-energy Electron SPectrometer (MESP), dedicated to the in situ observation of suprathermal electrons in the auroral ionosphere, are summarized in this paper. MESP employs a permanent magnet filter with a light tight structure to select electrons with proper energies guided to the detectors. A combination of two avalanche photodiodes and a large area solid-state detector (SSD) provided 46 total energy bins (1 keV resolution for 3−20 keV range for APDs, and 7 keV resolution for >20 keV range for SSDs). Multi-channel ultra-low power application-specific integrated circuits are also verified for the flight operation tomore » read-out and analyze the detector signals. MESP was launched from Poker Flat Research Range on 3 March 2014 as a part of ground-to-rocket electrodynamics-electrons correlative experiment (GREECE) mission. MESP successfully measured the precipitating electrons from 3 to 120 keV in 120-ms time resolution and characterized the features of suprathermal distributions associated with auroral arcs throughout the flight. The measured electrons were showing the inverted-V type spectra, consistent with the past measurements. In addition, investigations of the suprathermal electron population indicated the existence of the energetic non-thermal distribution corresponding to the brightest aurora.« less

Columbia University OSO-8 instrument for stellar and solar X-ray spectroscopy and polarimetry

NASA Technical Reports Server (NTRS)

Wolff, R. S.

1976-01-01

A spectrometer and a polarimeter consisting of large-area panels of mosaic crystals have been constructed and prepared for use in the OSO-8 satellite. The instrumentation is planned for study of stellar and solar X-ray spectra between 1.8-8 keV and stellar X-ray polarization at 2.6 keV. Aspects of the design which enable the instrument to make measurements of the diverse range of stellar and solar phenomena are described. Some of the unique features, such as high sensitivity, high temporal resolution, and spectral range, are discussed. The applicability of the spectrometer and polarimeter to various current problems in X-ray astronomy is considered.

Crystal growth and scintillation properties of potassium strontium bromide

NASA Astrophysics Data System (ADS)

Stand, L.; Zhuravleva, M.; Wei, H.; Melcher, C. L.

2015-08-01

In this work, potassium strontium bromide activated with divalent europium, (KSr2Br5:Eu) has been studied. It has a monoclinic crystal structure and a density of 3.98 g/cm3. Two single crystals of KSr2Br5 doped with 5% Eu2+, with diameters of 13 mm and 22 mm, were grown in a two zone transparent furnace via the Bridgman technique. The X-ray excited emission spectrum consisted of a single peak at ∼427 nm due to the 5d-4f transition in Eu2+. The measured light yield and energy resolution at 662 keV was 75,000 ph/MeV and 3.5%. At low energies KSr2Br5:Eu 5% also displays good energy resolution, 6.7% at 122 keV and 7.9% at 59.5 keV.

The EBIT Calorimeter Spectrometer: a new, permanent user facility at the LLNL EBIT

DOE Office of Scientific and Technical Information (OSTI.GOV)

Porter, F S; Beiersdorfer, P; Brown, G V

The EBIT Calorimeter Spectrometer (ECS) is currently being completed and will be installed at the EBIT facility at the Lawrence Livermore National Laboratory in October 2007. The ECS will replace the smaller XRS/EBIT microcalorimeter spectrometer that has been in almost continuous operation since 2000. The XRS/EBIT was based on a spare laboratory cryostat and an engineering model detector system from the Suzaku/XRS observatory program. The new ECS spectrometer was built to be a low maintenance, high performance implanted silicon microcalorimeter spectrometer with 4 eV resolution at 6 keV, 32 detector channels, 10 {micro}s event timing, and capable of uninterrupted acquisitionmore » sessions of over 60 hours at 50 mK. The XRS/EBIT program has been very successful, producing many results on topics such as laboratory astrophysics, atomic physics, nuclear physics, and calibration of the spectrometers for the National Ignition Facility. The ECS spectrometer will continue this work into the future with improved spectral resolution, integration times, and ease-of-use. We designed the ECS instrument with TES detectors in mind by using the same highly successful magnetic shielding as our laboratory TES cryostats. This design will lead to a future TES instrument at the LLNL EBIT. Here we discuss the legacy of the XRS/EBIT program, the performance of the new ECS spectrometer, and plans for a future TES instrument.« less

The superconducting high-resolution soft X-ray spectrometer at the advanced biological and environmental X-ray facility

NASA Astrophysics Data System (ADS)

Friedrich, S.; Drury, O. B.; George, S. J.; Cramer, S. P.

2007-11-01

We have built a 36-pixel superconducting tunnel junction X-ray spectrometer for chemical analysis of dilute samples in the soft X-ray band. It offers an energy resolution of ˜10-20 eV FWHM below 1 keV, a solid angle coverage of ˜10 -3, and can be operated at total rates of up to ˜10 6 counts/s. Here, we describe the spectrometer performance in speciation measurements by fluorescence-detected X-ray absorption spectroscopy at the Advanced Biological and Environmental X-ray facility at the ALS synchrotron.

A Comprehensive Search for Gamma-Ray Lines in the First Year of Data from the INTEGRAL Spectrometer

NASA Technical Reports Server (NTRS)

Teegarden, B. J.; Watanabe, K.

2006-01-01

Gamma-ray lines are produced in nature by a variety of different physical processes. They can be valuable astrophysical diagnostics providing information the may be unobtainable by other means. We have carried out an extensive search for gamma-ray lines in the first year of public data from the Spectrometer (SPI) on the INTEGRAL mission. INTEGRAL has spent a large fraction of its observing time in the Galactic Plane with particular concentration in the Galactic Center (GC) region (approximately 3 Msec in the first year). Hence the most sensitive search regions are in the Galactic Plane and Center. The phase space of the search spans the energy range 20-8000 keV, and line widths from 0-1000 keV (FWHM) and includes both diffuse and point-like emission. We have searched for variable emission on time scales down to approximately 1000 sec. Diffuse emission has been searched for on a range of different spatial scales from approximately 20 degrees (the approximate field-of-view of the spectrometer) up to the entire Galactic Plane. Our search procedures were verified by the recovery of the known gamma-ray lines at 511 keV and 1809 keV at the appropriate intensities and significances. We find no evidence for any previously unknown gamma-ray lines. The upper limits range from a few x10(exp -5) per square centimeter per second to a few x10(exp -3) per square centimeter per second depending on line width, energy and exposure. Comparison is made between our results and various prior predictions of astrophysical lines

Search for gamma-ray transients using the SMM spectrometer

NASA Technical Reports Server (NTRS)

Share, G. H.; Harris, M. J.; Leising, M. D.; Messina, D. C.

1993-01-01

Observations for transient radiation made by the Gamma Ray Spectrometer on the SMM satellite are summarized. Spectra were obtained from 215 solar flares and 177 gamma-ray bursts. No narrow or moderately broadened lines were observed in any of the bursts. The rate of bursts is consistent with a constant over the mission but is weakly correlated with solar activity. No evidence was found for bursts of 511 keV line emission, unaccompanied by a strong continuum, at levels not less than 0.05 gamma/sq cm s for bursts lasting not more than 16 s. No evidence was found for broad features near 1 MeV from Cyg X-1, the Galactic center, or the Crab in 12-d integrations at levels not less than 0.006 gamma/sq cm s. No evidence was found for transient celestial narrow-line emission from 300 keV to 7 MeV on min-to-hrs-long time scales from 1984 to 1989.

Time Projection Compton Spectrometer (TPCS). User`s guide

DOE Office of Scientific and Technical Information (OSTI.GOV)

Landron, C.O.; Baldwin, G.T.

1994-04-01

The Time Projection Compton Spectrometer (TPCS) is a radiation diagnostic designed to determine the time-integrated energy spectrum between 100 keV -- 2 MeV of flash x-ray sources. This guide is intended as a reference for the routine operator of the TPCS. Contents include a brief overview of the principle of operation, detailed component descriptions, detailed assembly and disassembly procedures, guide to routine operations, and troubleshooting flowcharts. Detailed principle of operation, signal analysis and spectrum unfold algorithms are beyond the scope of this guide; however, the guide makes reference to sources containing this information.

Neutron fluence and energy reconstruction with the IRSN recoil detector μ-TPC at 27 keV, 144 keV and 565 keV

DOE Office of Scientific and Technical Information (OSTI.GOV)

Maire, D.; Lebreton, L.; Richer, J.P.

2015-07-01

The French Institute for Radioprotection and Nuclear Safety (IRSN), associated to the French Metrology Institute (LNE), is developing a time projection chamber using a Micromegas anode: μ-TPC. This work is carried out in collaboration with the Laboratory of Subatomic Physics and Cosmology (LPSC). The aim is to characterize with a primary procedure the energy distribution of neutron fluence in the energy range 8 keV - 1 MeV. The time projection chambers are gaseous detectors, which are able to measure charged particles energy and to reconstruct their track if a pixelated anode is used. In our case, the gas is usedmore » as a (n, p) converter in order to detect neutrons down to few keV. Coming from elastic collisions with neutrons, recoil protons lose a part of their kinetic energy by ionizing the gas. The ionization electrons are drifted toward a pixelated anode (2D projection), read at 50 MHz by a self-triggered electronic system to obtain the third track dimension. The neutron energy is reconstructed event by event thanks to proton scattering angle and proton energy measurements. The scattering angle is deduced from the 3D track. The proton energy is obtained by charge collection measurements, knowing the ionization quenching factor (i.e. the part of proton kinetic energy lost by ionizing the gas). The fluence is calculated thanks to the detected events number and the simulated detector response. The μ-TPC is a new reliable detector which enables to measure energy distribution of the neutron fluence without deconvolution or neutron calibration contrary to usual gaseous counters. The μ-TPC is still being developed and measurements have been carried out at the AMANDE facility, with neutrons energies going from 8 keV to 565 keV. After the context and the μ-TPC working principle presentation, measurements of the neutron energy and fluence at 27.2 keV, 144 keV and 565 keV are shown and compared to the complete detector simulation. This work shows the first direct

A Low-Noise Germanium Ionization Spectrometer for Low-Background Science

DOE Office of Scientific and Technical Information (OSTI.GOV)

Aalseth, Craig E.; Colaresi, Jim; Collar, Juan I.

2016-12-01

Recent progress on the development of very low energy threshold high purity germanium ionization spectrometers has produced an instrument of 1.2 kg mass and excellent noise performance. The detector was installed in a low-background cryostat intended for use in a low mass, WIMP dark matter direct detection search. The integrated detector and low background cryostat achieved noise performance of 98 eV full-width half-maximum of an input electronic pulse generator peak and gamma-ray energy resolution of 1.9 keV full-width half-maximum at the 60Co gamma-ray energy of 1332 keV. This Transaction reports the thermal characterization of the low-background cryostat, specifications of themore » newly prepared 1.2 kg p-type point contact germanium detector, and the ionization spectroscopy – energy resolution and energy threshold – performance of the integrated system.« less

New Solar Irradiance Measurements from the Miniature X-Ray Solar Spectrometer Cubesat

DOE Office of Scientific and Technical Information (OSTI.GOV)

Woods, Thomas N.; Jones, Andrew; Kohnert, Richard

The goal of the Miniature X-ray Solar Spectrometer ( MinXSS ) CubeSat is to explore the energy distribution of soft X-ray (SXR) emissions from the quiescent Sun, active regions, and during solar flares and to model the impact on Earth's ionosphere and thermosphere. The energy emitted in the SXR range (0.1–10 keV) can vary by more than a factor of 100, yet we have limited spectral measurements in the SXRs to accurately quantify the spectral dependence of this variability. The MinXSS primary science instrument is an Amptek, Inc. X123 X-ray spectrometer that has an energy range of 0.5–30 keV withmore » a nominal 0.15 keV energy resolution. Two flight models have been built. The first, MinXSS -1, has been making science observations since 2016 June 9 and has observed numerous flares, including more than 40 C-class and 7 M-class flares. These SXR spectral measurements have advantages over broadband SXR observations, such as providing the capability to derive multiple-temperature components and elemental abundances of coronal plasma, improved irradiance accuracy, and higher resolution spectral irradiance as input to planetary ionosphere simulations. MinXSS spectra obtained during the M5.0 flare on 2016 July 23 highlight these advantages and indicate how the elemental abundance appears to change from primarily coronal to more photospheric during the flare. MinXSS -1 observations are compared to the Geostationary Operational Environmental Satellite ( GOES ) X-ray Sensor (XRS) measurements of SXR irradiance and estimated corona temperature. Additionally, a suggested improvement to the calibration of the GOES XRS data is presented.« less

Interferometric phase-contrast X-ray CT imaging of VX2 rabbit cancer at 35keV X-ray energy

NASA Astrophysics Data System (ADS)

Takeda, Tohoru; Wu, Jin; Tsuchiya, Yoshinori; Yoneyama, Akio; Lwin, Thet-Thet; Hyodo, Kazuyuki; Itai, Yuji

2004-05-01

Imaging of large objects at 17.7-keV low x-ray energy causes huge x-ray exposure to the objects even using interferometric phase-contrast x-ray CT (PCCT). Thus, we tried to obtain PCCT images at high x-ray energy of 35keV and examined the image quality using a formalin-fixed VX2 rabbit cancer specimen with 15-mm in diameter. The PCCT system consisted of an asymmetrically cut silicon (220) crystal, a monolithic x-ray interferometer, a phase-shifter, an object cell and an x-ray CCD camera. The PCCT at 35 keV clearly visualized various inner structures of VX2 rabbit cancer such as necrosis, cancer, the surrounding tumor vessels, and normal liver tissue. Besides, image-contrast was not degraded significantly. These results suggest that the PCCT at 35 KeV is sufficient to clearly depict the histopathological morphology of VX2 rabbit cancer specimen.

Sub-second variations of high energy ( 300 keV) hard X-ray emission from solar flares

NASA Technical Reports Server (NTRS)

Bai, Taeil

1986-01-01

Subsecond variations of hard X-ray emission from solar flares were first observed with a balloon-borne detector. With the launch of the Solar Maximum Mission (SMM), it is now well known that subsecond variations of hard X-ray emission occur quite frequently. Such rapid variations give constraints on the modeling of electron energization. Such rapid variations reported until now, however, were observed at relatively low energies. Fast mode data obtained by the Hard X-ray Burst Spectrometer (HXRBS) has time resolution of approximately 1 ms but has no energy resolution. Therefore, rapid fluctuations observed in the fast-mode HXRBS data are dominated by the low energy hard X-rays. It is of interest to know whether rapid fluctuations are observed in high-energy X-rays. The highest energy band at which subsecond variations were observed is 223 to 1057 keV. Subsecond variations observed with HXRBS at energies greater than 300 keV are reported, and the implications discussed.

Improved growth method of (SN) x single crystals

NASA Astrophysics Data System (ADS)

Nakada, Ichiroh

1981-12-01

The crystal growth of pure and sizable single crystals of polysulfur nitride (SN) x was improved by adopting a monitor system with a quadrapole mass spectrometer and a Pirani gauge. The mass spectrometer helped to find a temperature appropriate for trapping (SN) 2 selectively on a cold finger and removing other unnecessary or harmful materials produced by the thermal decomposition of (SN) 4 as well as out-gassing water vapour from the glass wall. Leakage of gasses in the vessel was monitored with the Pirani gauge. With a heat pipe the crystal tube is cooled locally so that only a small number of nuclei start to grow. (SN) x single crystals with dimensions of 1 to 6 mm in edge size have been obtained. The relation between the crystal habit and the crystallographic axes has also been determined.

In-flight calibration of Hitomi Soft X-ray Spectrometer. (1) Background

NASA Astrophysics Data System (ADS)

Kilbourne, Caroline A.; Sawada, Makoto; Tsujimoto, Masahiro; Angellini, Lorella; Boyce, Kevin R.; Eckart, Megan E.; Fujimoto, Ryuichi; Ishisaki, Yoshitaka; Kelley, Richard L.; Koyama, Shu; Leutenegger, Maurice A.; Loewenstein, Michael; McCammon, Dan; Mitsuda, Kazuhisa; Nakashima, Shinya; Porter, Frederick S.; Seta, Hiromi; Takei, Yoh; Tashiro, Makoto S.; Terada, Yukikatsu; Yamada, Shinya; Yamasaki, Noriko Y.

2018-03-01

The X-Ray Spectrometer (XRS) instrument of Suzaku provided the first measurement of the non-X-ray background (NXB) of an X-ray calorimeter spectrometer, but the data set was limited. The Soft X-ray Spectrometer (SXS) instrument of Hitomi was able to provide a more detailed picture of X-ray calorimeter background, with more than 360 ks of data while pointed at the Earth, and a comparable amount of blank-sky data. These data are important not only for analyzing SXS science data, but also for categorizing the contributions to the NXB in X-ray calorimeters as a class. In this paper, we present the contributions to the SXS NXB, the types and effectiveness of the screening, the interaction of the screening with the broad-band redistribution, and the residual background spectrum as a function of magnetic cut-off rigidity. The orbit-averaged SXS NXB in the range 0.3-12 keV was 4 × 10-2 counts s-1 cm-2. This very low background in combination with groundbreaking spectral resolution gave SXS unprecedented sensitivity to weak spectral lines.

HREM study of irradiation damage in human dental enamel crystals.

PubMed

Brès, E F; Hutchison, J L; Senger, B; Voegel, J C; Frank, R M

1991-06-01

Several phenomena have been observed during the examination of human dental enamel crystals (mainly constituted by hydroxyapatite (OHAP] by high-resolution electron microscopy (HREM) at 300 and 400 keV: orientation-dependent damage in the form of mass loss from voids or uniform destruction of crystal structure, beam-induced diffusion creating outgrowths at the crystal surfaces, recrystallization of the bulk crystal and crystallization of the inorganic components of the matrix surrounding the crystals. These beam-induced crystals have the CaO structure. The phenomena observed are most likely due to various electron-crystal interaction mechanisms (ballistic knock-on damage, electronic excitations, temperature rise, etc.). In this paper, the contribution of the ballistic process to the phenomena observed is discussed. The quantitative description of the knock-on collisions rests on the McKinley-Feshbach cross-section formula. The minimum ion displacement energies which appear in this expression have been estimated on the basis of the electrostatic ion binding energies, and the covalent bond energies if required. It is shown that hydroxyl, calcium and oxygen ions can effectively be displaced by the incident 300 and 400 keV electrons. Thus, the formation of CaO crystals by the combination of calcium and oxygen ions diffusing from their initial sites inside the OHAP lattice can tentatively be explained.

The complete Hard X Ray Burst Spectrometer event list, 1980-1989

NASA Technical Reports Server (NTRS)

Dennis, B. R.; Orwig, L. E.; Kennard, G. S.; Labow, G. J.; Schwartz, R. A.; Shaver, A. R.; Tolbert, A. K.

1991-01-01

This event list is a comprehensive reference for all Hard X ray bursts detected with the Hard X Ray Burst Spectrometer on the Solar Maximum Mission from the time of launch on Feb. 14, 1980 to the end of the mission in Dec. 1989. Some 12,776 events were detected in the energy range 30 to 600 keV with the vast majority being solar flares. This list includes the start time, peak time, duration, and peak rate of each event.

SMM observations of gamma-ray transients. 2: A search for gamma-ray lines between 400 and 600 keV from the Crab Nebula

NASA Technical Reports Server (NTRS)

Harris, Michael J.; Share, Gerald H.; Leising, Mark D.

1994-01-01

We have search spectra obtained by the Solar Maximum Mission Gamma-Ray Spectrometer during 1981-1988 for evidence of transient gamma-ray lines from the Crab Nebula which have been reported by previous experiments at energies 400-460 keV and 539 keV. We find no evidence for significant emission in any of these lines on time scales between aproximately 1 day and approximately 1 yr. Our 3 sigma upper limits on the transient flux during 1 d intervals are approximately equal to 2.2 x 10(exp -3) photons/sq cm/s for narrow lines at any energy, and approximately equal to 2.9 x 10(exp -3) photons/sq cm/s for the 539 keV line if it is as broad as 42 keV Full Width at Half Maximum (FWHM). We also searched our data during the approximately 5 hr period on 1981 June 6 during which Owens, Myers, & Thompson (1985) reported a strong line at 405 keV. We detected no line down to a 3 upper sigma limit of 3.3 x 10(exp -3) photons/sq cm/s in disagreement with the flux 7.2 +/- 2.1 x 10(exp -3) photos/sq cm/s measured by Owens et al.

The hard X-ray burst spectrometer event listing 1980, 1981 and 1982

NASA Technical Reports Server (NTRS)

Dennis, B. R.; Frost, K. J.; Orwig, L. E.; Kiplinger, A.; Dennis, H. E.; Gibson, B. R.; Kennard, G. S.; Tolbert, A. K.

1983-01-01

A comprehensive reference for the hard X-ray bursts detected with the Hard X-Ray Burst Spectrometer on the Solar Maximum Mission for the time of launch on February 14, 1980 to March 1983 is provided. Over 6300 X-ray events were detected in the energy range from 30 to approx 500 keV with the vast majority being solar flares. The listing includes the start time, peak time, duration and peak rate of each event.

New Solar Irradiance Measurements from the Miniature X-Ray Solar Spectrometer CubeSat

NASA Astrophysics Data System (ADS)

Woods, Thomas N.; Caspi, Amir; Chamberlin, Phillip C.; Jones, Andrew; Kohnert, Richard; Mason, James Paul; Moore, Christopher S.; Palo, Scott; Rouleau, Colden; Solomon, Stanley C.; Machol, Janet; Viereck, Rodney

2017-02-01

The goal of the Miniature X-ray Solar Spectrometer (MinXSS) CubeSat is to explore the energy distribution of soft X-ray (SXR) emissions from the quiescent Sun, active regions, and during solar flares and to model the impact on Earth's ionosphere and thermosphere. The energy emitted in the SXR range (0.1-10 keV) can vary by more than a factor of 100, yet we have limited spectral measurements in the SXRs to accurately quantify the spectral dependence of this variability. The MinXSS primary science instrument is an Amptek, Inc. X123 X-ray spectrometer that has an energy range of 0.5-30 keV with a nominal 0.15 keV energy resolution. Two flight models have been built. The first, MinXSS-1, has been making science observations since 2016 June 9 and has observed numerous flares, including more than 40 C-class and 7 M-class flares. These SXR spectral measurements have advantages over broadband SXR observations, such as providing the capability to derive multiple-temperature components and elemental abundances of coronal plasma, improved irradiance accuracy, and higher resolution spectral irradiance as input to planetary ionosphere simulations. MinXSS spectra obtained during the M5.0 flare on 2016 July 23 highlight these advantages and indicate how the elemental abundance appears to change from primarily coronal to more photospheric during the flare. MinXSS-1 observations are compared to the Geostationary Operational Environmental Satellite (GOES) X-ray Sensor (XRS) measurements of SXR irradiance and estimated corona temperature. Additionally, a suggested improvement to the calibration of the GOES XRS data is presented.

Fundamental studies of MALDI with an orthogonal TOF mass spectrometer

NASA Astrophysics Data System (ADS)

Qiao, Hui

The interaction between the matrix and analyte molecules are studied with a high resolution MALDI imaging technique in an orthogonal-injection time of flight (TOF) mass spectrometer. The analyte incorporation and distribution patterns have been clearly demonstrated. Purified protein analytes were found to be homogeneously incorporated in large single crystals of DHB and sinapinic acid matrices, with no evidence for preferred crystal faces. Segregation of some species was observed and appeared to correlate with analyte hydrophobicity, and to a lesser extent analyte mass or mobility. Similar segregation phenomena were observed with confocal laser scanning microscopy of the same analytes labeled with fluorescent dyes in 2,5-DHB single crystals. The above investigations may shed some light on optimizing sample preparation with different matrices. The influence of incident laser parameters on sensitivity in MALDI has been investigated using orthogonal-injection TOF instruments. A qualitative comparison was first made between the beam profiles obtained with a N 2 laser and a Nd:YAG laser using 2-m long optical fibers. The N 2 laser gives better sensitivity, consistent with a more uniform fluence distribution and therefore better coverage of the N2 laser profile. Most of the difference disappears when a 30-m long fiber is used or when the fibers are twisted during irradiation to smooth out the fluence distribution. In more systematic measurements, the total integrated ion yield from a single spot (a measure of sensitivity) was found to increase rapidly with fluence to a maximum, and then saturate or decrease slightly. Thus, the optimum sensitivity is achieved at high fluence. For a fluence near threshold, the integrated yield has a steep (cubic) dependence on the spot size, but the yield saturates at higher fluence for smaller spots. The area dependence is much weaker (close to linear) for fluence values above saturation, with the result that the highest integrated yields

Einstein Observatory solid state spectrometer observations of M87 and the Virgo cluster

NASA Technical Reports Server (NTRS)

Lea, S. M.; Mushotzky, R. F.; Holt, S. S.

1982-01-01

X-ray observations of the galaxy M87 and of a region in the Virgo cluster displaced 7 minutes from the center of M87 are presented. X-ray spectra are obtained at these two locations with the slid state spectrometer onboard the Einstein Observatory. Emission lines were observed in both locations, indicating the presence of heavy elements at abundances approximately solar (to within a factor of 2). A temperature gradient, T increases from approximately 1.4 keV at the position of M87 to T approximately 3.35 keV 7' away, was detected. There is lower temperature thermal emission at the center of M87 with T approximately 0.6 keV, consistent with models for cooling flows in this cluster. In addition to the thermal emission, a power law component in the spectrum of M87, was detected consistent with that observed by HEAO-1, indicating that this component probably originates in the galaxy itself. The presence of intracluster gas having density approximately .001 cu cm and temperature approximately 30 million K is indicated.

A Compton scatter attenuation gamma ray spectrometer

NASA Technical Reports Server (NTRS)

Austin, W. E.

1972-01-01

A Compton scatter attenuation gamma ray spectrometer conceptual design is discussed for performing gamma spectral measurements in monodirectional gamma fields from 100 R per hour to 1,000,000 R per hour. Selectable Compton targets are used to scatter gamma photons onto an otherwise heavily shielded detector with changeable scattering efficiencies such that the count rate is maintained between 500 and 10,000 per second. Use of two sum-Compton coincident detectors, one for energies up to 1.5 MeV and the other for 600 keV to 10 MeV, will allow good peak to tail pulse height ratios to be obtained over the entire spectrum and reduces the neutron recoil background rate.

Soft x-ray spectrometer (SXS): the high-resolution cryogenic spectrometer onboard ASTRO-H

NASA Astrophysics Data System (ADS)

Mitsuda, Kazuhisa; Kelley, Richard L.; Akamatsu, Hiroki; Bialas, Thomas; Boyce, Kevin R.; Brown, Gregory V.; Canavan, Edgar; Chiao, Meng; Costantini, Elisa; den Herder, Jan-Willem; de Vries, Cor; DiPirro, Michael J.; Eckart, Megan E.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Haas, Daniel; Hoshino, Akio; Ishikawa, Kumi; Ishisaki, Yoshitaka; Iyomoto, Naoko; Kilbourne, Caroline A.; Kimball, Mark; Kitamoto, Shunji; Konami, Saori; Leutenegger, Maurice A.; McCammon, Dan; Miko, Joseph; Mitsuishi, Ikuyuki; Murakami, Hiroshi; Murakami, Masahide; Noda, Hirofumi; Ogawa, Mina; Ohashi, Takaya; Okamoto, Atsushi; Ota, Naomi; Paltani, Stéphane; Porter, F. Scott; Sato, Kosuke; Sato, Yoichi; Sawada, Makoto; Seta, Hiromi; Shinozaki, Keisuke; Shirron, Peter J.; Sneiderman, Gary A.; Sugita, Hiroyuki; Szymkowiak, Andrew; Takei, Yoh; Tamagawa, Toru; Tashiro, Makoto S.; Terada, Yukikatsu; Tsujimoto, Masahiro; Yamada, Shinya; Yamasaki, Noriko Y.

2014-07-01

We present the development status of the Soft X-ray Spectrometer (SXS) onboard the ASTRO-H mission. The SXS provides the capability of high energy-resolution X-ray spectroscopy of a FWHM energy resolution of < 7eV in the energy range of 0.3 - 10 keV. It utilizes an X-ray micorcalorimeter array operated at 50 mK. The SXS microcalorimeter subsystem is being developed in an EM-FM approach. The EM SXS cryostat was developed and fully tested and, although the design was generally confirmed, several anomalies and problems were found. Among them is the interference of the detector with the micro-vibrations from the mechanical coolers, which is the most difficult one to solve. We have pursued three different countermeasures and two of them seem to be effective. So far we have obtained energy resolutions satisfying the requirement with the FM cryostat.

A Bonner Sphere Spectrometer with extended response matrix

NASA Astrophysics Data System (ADS)

Birattari, C.; Dimovasili, E.; Mitaroff, A.; Silari, M.

2010-08-01

This paper describes the design, calibration and applications at high-energy accelerators of an extended-range Bonner Sphere neutron Spectrometer (BSS). The BSS was designed by the FLUKA Monte Carlo code, investigating several combinations of materials and diameters of the moderators for the high-energy channels. The system was calibrated at PTB in Braunschweig, Germany, using monoenergetic neutron beams in the energy range 144 keV-19 MeV. It was subsequently tested with Am-Be source neutrons and in the simulated workplace neutron field at CERF (the CERN-EU high-energy reference field facility). Since 2002, it has been employed for neutron spectral measurements around CERN accelerators.

Prototype Ge:Ga detectors for the NASA-Ames cooled grating spectrometer

NASA Technical Reports Server (NTRS)

Houck, J. R.

1981-01-01

The detectors were fabricated from a Ge:Ga wafer from Eagle-Pitcher with a room temperature resistivity of approx. 12ohms cm. The wafer is approximately 2 inches in diameter and 0.061 inches thick. The contact material was ion implanted with Boron using 10 to the 14th power ions/sq cm at 25 Kev and 2 x10 to the 14th power ions/sq cm at 50 Kev. The crystal was then sputter-cleaned and metallized first with sputtered Ti and then sputter Au. In addition to the usual infrared measurements of responsivity and noise, measurements were made of the detectors' response to ionizing radiation.

Overview of the Design, Fabrication and Performance Requirements of Micro-Spec, an Integrated Submillimeter Spectrometer

NASA Technical Reports Server (NTRS)

Barrentine, Emily M.; Noroozian, Omid; Brown, Ari D.; Cataldo, Giuseppe; Ehsan, Negar; Hsieh, Wen-Ting; Stevenson, Thomas R.; U-Yen, Kongpop; Wollack, Edward J.; Moseley, S. Harvey

2015-01-01

Micro-Spec is a compact submillimeter (350-700 GHz) spectrometer which uses low loss superconducting niobium microstrip transmission lines and a single-crystal silicon dielectric to integrate all of the components of a grating-analog spectrometer onto a single chip. Here we present details of the fabrication and design of a prototype Micro-Spec spectrometer with resolution, R64, where we use a high-yield single-flip wafer bonding process to realize instrument components on a 0.45 m single-crystal silicon dielectric. We discuss some of the electromagnetic design concerns (such as loss, stray-light, cross-talk, and fabrication tolerances) for each of the spectrometer components and their integration into the instrument as a whole. These components include a slot antenna with a silicon lens for optical coupling, a phase delay transmission line network, parallel plate waveguide interference region, and aluminum microstrip transmission line kinetic inductance detectors with extremely low cross-talk and immunity to stray light. We have demonstrated this prototype spectrometer with design resolution of R64. Given the optical performance of this prototype, we will also discuss the extension of this design to higher resolutions suitable for balloon-flight.

Multi-Element CZT Array for Nuclear Safeguards Applications

NASA Astrophysics Data System (ADS)

Kwak, S.-W.; Lee, A.-R.; Shin, J.-K.; Park, U.-R.; Park, S.; Kim, Y.; Chung, H.

2016-12-01

Due to its electronic properties, a cadmium zinc telluride (CZT) detector has been used as a hand-held portable nuclear measurement instrument. However, a CZT detector has low detection efficiency because of a limitation of its single crystal growth. To address its low efficiency, we have constructed a portable four-CZT array based gamma-ray spectrometer consisting of a CZT array, electronics for signal processing and software. Its performance has been characterized in terms of energy resolution and detection efficiency using radioactive sources and nuclear materials. Experimental results showed that the detection efficiency of the four-CZT array based gamma-ray spectrometer was much higher than that of a single CZT detector in the array. The FWHMs of the CZT array were 9, 18, and 21 keV at 185.7, 662, and 1,332 keV, respectively. Some gamma-rays in a range of 100 keV to 200 keV were not clear in a single crystal detector while those from the CZT array system were observed to be clear. The energy resolution of the CZT array system was only slightely worse than those of the single CZT detectors. By combining several single crystals and summing signals from each single detector at a digital electronic circuit, the detection efficiency of a CZT array system increased without degradation of its energy resolution. The technique outlined in this paper shows a very promising method for designing a CZT-based gamma-ray spectroscopy that overcomes the fundamental limitations of a small volume CZT detector.

SIKA—the multiplexing cold-neutron triple-axis spectrometer at ANSTO

NASA Astrophysics Data System (ADS)

Wu, C.-M.; Deng, G.; Gardner, J. S.; Vorderwisch, P.; Li, W.-H.; Yano, S.; Peng, J.-C.; Imamovic, E.

2016-10-01

SIKA is a new cold-neutron triple-axis spectrometer receiving neutrons from the cold source CG4 of the 20MW Open Pool Australian Light-water reactor. As a state-of-the-art triple-axis spectrometer, SIKA is equipped with a large double-focusing pyrolytic graphite monochromator, a multiblade pyrolytic graphite analyser and a multi-detector system. In this paper, we present the design, functions, and capabilities of SIKA, and discuss commissioning experimental results from powder and single-crystal samples to demonstrate its performance.

Room temperature X- and gamma-ray detectors using thallium bromide crystals

NASA Astrophysics Data System (ADS)

Hitomi, K.; Muroi, O.; Shoji, T.; Suehiro, T.; Hiratate, Y.

1999-10-01

Thallium bromide (TlBr) is a compound semiconductor with wide band gap (2.68eV) and high X- and γ-ray stopping power. The TlBr crystals were grown by the horizontal travelling molten zone (TMZ) method using purified material. Two types of room temperature X- and γ-ray detectors were fabricated from the TlBr crystals: TlBr detectors with high detection efficiency for positron annihilation γ-ray (511keV) detection and TlBr detectors with high-energy resolution for low-energy X-ray detection. The detector of the former type demonstrated energy resolution of 56keV FWHM (11%) for 511keV γ-rays. Energy resolution of 1.81keV FWHM for 5.9keV was obtained from the detector of the latter type. In order to analyze noise characteristics of the detector-preamplifier assembly, the equivalent noise charge (ENC) was measured as a function of the amplifier shaping time for the high-resolution detector. This analysis shows that parallel white noise and /1/f noise were dominant noise sources in the detector system. Current-voltage characteristics of the TlBr detector with a small Peltier cooler were also measured. Significant reduction of the detector leakage current was observed for the cooled detectors.

Quantitative Kα line spectroscopy for energy transport in ultra-intense laser plasma interaction

NASA Astrophysics Data System (ADS)

Zhang, Z.; Nishimura, H.; Namimoto, T.; Fujioka, S.; Arikawa, Y.; Nakai, M.; Koga, M.; Shiraga, H.; Kojima, S.; Azechi, H.; Ozaki, T.; Chen, H.; Pakr, J.; Williams, G. J.; Nishikino, M.; Kawachi, T.; Sagisaka, A.; Orimo, S.; Ogura, K.; Pirozhkov, A.; Yogo, A.; Kiriyama, H.; Kondo, K.; Okano, Y.

2012-10-01

X-ray line spectra ranging from 17 to 77 keV were quantitatively measured with a Laue spectrometer, composed of a cylindrically curved crystal and a detector. The absolute sensitivity of the spectrometer system was calibrated using pre-characterized laser-produced x-ray sources and radioisotopes, for the detectors and crystal respectively. The integrated reflectivity for the crystal is in good agreement with predictions by an open code for x-ray diffraction. The energy transfer efficiency from incident laser beams to hot electrons, as the energy transfer agency for Au Kα x-ray line emissions, is derived as a consequence of this work. By considering the hot electron temperature, the transfer efficiency from LFEX laser to Au plate target is about 8% to 10%.

Elpasolite Planetary Ice and Composition Spectrometer (EPICS): A Low-Resource Combined Gamma-Ray and Neutron Spectrometer for Planetary Science

NASA Astrophysics Data System (ADS)

Stonehill, L. C.; Coupland, D. D. S.; Dallmann, N. A.; Feldman, W. C.; Mesick, K.; Nowicki, S.; Storms, S.

2017-12-01

The Elpasolite Planetary Ice and Composition Spectrometer (EPICS) is an innovative, low-resource gamma-ray and neutron spectrometer for planetary science missions, enabled by new scintillator and photodetector technologies. Neutrons and gamma rays are produced by cosmic ray interactions with planetary bodies and their subsequent interactions with the near-surface materials produce distinctive energy spectra. Measuring these spectra reveals details of the planetary near-surface composition that are not accessible through any other phenomenology. EPICS will be the first planetary science instrument to fully integrate the neutron and gamma-ray spectrometers. This integration is enabled by the elpasolite family of scintillators that offer gamma-ray spectroscopy energy resolutions as good as 3% FWHM at 662 keV, thermal neutron sensitivity, and the ability to distinguish gamma-ray and neutron signals via pulse shape differences. This new detection technology will significantly reduce size, weight, and power (SWaP) while providing similar neutron performance and improved gamma energy resolution compared to previous scintillator instruments, and the ability to monitor the cosmic-ray source term. EPICS will detect scintillation light with silicon photomultipliers rather than traditional photomultiplier tubes, offering dramatic additional SWaP reduction. EPICS is under development with Los Alamos National Laboratory internal research and development funding. Here we report on the EPICS design, provide an update on the current status of the EPICS development, and discuss the expected sensitivity and performance of EPICS in several potential missions to airless bodies.

Observation of Pulsed Gamma Rays with Energies Greater than 250 keV from the Crab Nebula Pulsar NP 0532. Ph.D. Thesis

NASA Technical Reports Server (NTRS)

Orwig, L. E.

1971-01-01

Data from a balloon flight experiment using an Na I scintillation spectrometer were analyzed for gamma ray pulsation. The payload was carried to a nominal atmospheric depth of 3.5 g/cm2. A superposed epoch analysis was performed on a 12,000 second portion of the data spanning a total time interval of 16,700 seconds at float altitude. A positive pulsed contribution was observed at the expected apparent frequency of NP 0532 having the typical double pulse structure. The results indicate a time-averaged pulse photon flux of 0.00144 + or - 0.00057 photons/sq cm/sec in the energy interval from 250 keV to 2.3 MeV. This represents a time-averaged pulsed power of 0.000649 + or - 0.000257 keV/sq cm/sec/keV. The ratio of interpulse to main pulse was found to be 2.4 + or - 1.9. The analysis indicates a positive photon flux from 250 keV to 725 keV of 0.00120 + or - 0.00052 photons/sq cm/sec.

Radiation measurement above the lunar surface by Kaguya gamma-ray spectrometer

NASA Astrophysics Data System (ADS)

Hasebe, Nobuyuki; Nagaoka, Hiroshi; Kusano, Hiroki; Hareyama, Matoko; Ideguchi, Yusuke; Shimizu, Sota; Shibamura, Eido

The lunar surface is filled with various ionizing radiations such as high energy galactic particles, albedo particles and secondary radiations of neutrons, gamma rays and other elementary particles. A high-resolution Kaguya Gamma-Ray Spectrometer (KGRS) was carried on the Japan’s lunar explorer SELENE (Kaguya), the largest lunar orbiter since the Apollo missions. The KGRS instrument employed, for the first time in lunar exploration, a high-purity Ge crystal to increase the identification capability of elemental gamma-ray lines. The Ge detector is surrounded by BGO and plastic counters as for anticoincidence shields. The KGRS measured gamma rays in the energy range from 200 keV to 13 MeV with high precision to determine the chemical composition of the lunar surface. It provided data on the abundance of major elements over the entire lunar surface. In addition to the gamma-ray observation by the KGRS, it successfully measured the global distribution of fast neutrons. In the energy spectra of gamma-rays observed by the KGRS, several saw-tooth- peaks of Ge are included, which are formed by the collision interaction of lunar fast neutrons with Ge atoms in the Ge crystal. With these saw-tooth-peaks analysis, global distribution of neutrons emitted from the lunara surface was successfully created, which was compared with the previous results obtained by Lunar Prospector neutron maps. Another anticoincidence counter, the plastic counter with 5 mm thickness, was used to veto radiation events mostly generated by charged particles. A single photomultiplier serves to count scintillation light from the plastic scintillation counter. The global map of counting rates observed by the plastic counter was also created, implying that the radiation counting rate implies the geological distribution, in spite that the plastic counter mostly measures high energy charged particles and energetic neutrons. These results are presented and discussed.

Development of Calorimetric Particle Spectrometer and Measurement of Specific Heat at Low Temperature.

NASA Astrophysics Data System (ADS)

Zhou, Jun-Wei

1991-02-01

A dilution refrigerator has been put into work from 30 mK to 300 K to study bolometer characteristics relevant to its potential use as a high resolution X-ray and alpha, beta, gamma particle spectrometer. Tests of the energy deposited in the detector by measuring the temperature rise following absorption of individual nuclear particles or X- or gamma-rays have been done. Essential studies were made of electromagnetic and acoustic noise. A composite-composite bolometer fabricated by the group of N. Coron (Institute of Space Astrophysics, France), with whom we collaborate, was used. This design allows the separate optimization of the absorber and thermistor, and avoids problems with absorption inhomogeneties. A FWHM resolution of 10.5 KeV for 5 to 6 MeV alpha spectra was obtained. This resolution exceeds the best obtainable with surface barrier semiconductor detectors. A broad spectrum recording simultaneously gamma-rays, beta and alpha particles from 15 KeV to 6 MeV was obtained with the same bolometer cooled below 0.1 K. Other bolometers were also tested. 6 KeV X-rays have been observed with a resolution of 472 eV. The bolometers were also used for determination of specific heat of the sapphire at low temperatures. Assuming a specific heat C = AT^3, we find in a 2.3 g sample A ~eq 1.4 times 10^{-8} J/Kcdotg from T = 0.1 K to T = 0.4 K. A discussion of the systematic errors in determining A is given. From our measurements, it was determined that a bolometer designed for a future possible neutrino mass measurement would have a resolution of 7.5 eV at 80 mK under optimal operation. Since tritium was implanted in this detector, systematic errors associated with electron spectrometer beta spectrum measurements can be, in principle, avoided.

Crystal face temperature determination means

DOEpatents

Nason, D.O.; Burger, A.

1994-11-22

An optically transparent furnace having a detection apparatus with a pedestal enclosed in an evacuated ampule for growing a crystal thereon is disclosed. Temperature differential is provided by a source heater, a base heater and a cold finger such that material migrates from a polycrystalline source material to grow the crystal. A quartz halogen lamp projects a collimated beam onto the crystal and a reflected beam is analyzed by a double monochromator and photomultiplier detection spectrometer and the detected peak position in the reflected energy spectrum of the reflected beam is interpreted to determine surface temperature of the crystal. 3 figs.

The Miniature X-ray Solar Spectrometer (MinXSS) CubeSats: New soft X-ray spectrometer to investigate properties of hot plasma in the quiet Sun, active regions, and flares.

NASA Astrophysics Data System (ADS)

Moore, C. S.; Dennis, B. R.; Woods, T. N.

2017-12-01

Detection of soft X-rays from the Sun provides direct information on coronal plasma at temperatures in excess of 1 MK. The Miniature X-ray Solar Spectrometer (MinXSS) CubeSats provides new spectrally resolved measurements from 0.8 -12 keV. The MinXSS spectral resolving power (R 40 at 5.9 keV) allows plasma abundances to be determined for Fe, Mg, Ni, Ca, Si, S, and Ar. Long-term temporal variations during quiet-Sun times allow active region contributions to be extracted from the full solar flux. The MinXSS 10 second time cadence allows short-term variations of the soft X-ray flux, temperature, and abundances to be determined during flares. The MinXSS spectroscopic observations, combined with the imaging spectroscopy from the Hinode X-ray Telescope (XRT) and the Reuven Ramaty Solar Spectroscopic Imager (RHESSI), hold great potential for advancing our understanding of solar dynamics.

Development of a high resolution x-ray spectrometer for the National Ignition Facility (NIF)

DOE PAGES

Hill, K. W.; Bitter, M.; Delgado-Aparicio, L.; ...

2016-09-28

A high resolution (E/ΔE = 1200-1800) Bragg crystal x-ray spectrometer is being developed to measure plasma parameters in National Ignition Facility experiments. The instrument will be a diagnostic instrument manipulator positioned cassette designed mainly to infer electron density in compressed capsules from Stark broadening of the helium-β (1s 2-1s3p) lines of krypton and electron temperature from the relative intensities of dielectronic satellites. Two conically shaped crystals will diffract and focus (1) the Kr Heβ complex and (2) the Heα (1s 2-1s2p) and Lyα (1s-2p) complexes onto a streak camera photocathode for time resolved measurement, and a third cylindrical or conicalmore » crystal will focus the full Heα to Heβ spectral range onto an image plate to provide a time integrated calibration spectrum. Calculations of source x-ray intensity, spectrometer throughput, and spectral resolution are presented. Furthermore, details of the conical-crystal focusing properties as well as the status of the instrumental design are also presented.« less

Development of a high resolution x-ray spectrometer for the National Ignition Facility (NIF).

PubMed

Hill, K W; Bitter, M; Delgado-Aparicio, L; Efthimion, P C; Ellis, R; Gao, L; Maddox, J; Pablant, N A; Schneider, M B; Chen, H; Ayers, S; Kauffman, R L; MacPhee, A G; Beiersdorfer, P; Bettencourt, R; Ma, T; Nora, R C; Scott, H A; Thorn, D B; Kilkenny, J D; Nelson, D; Shoup, M; Maron, Y

2016-11-01

A high resolution (E/ΔE = 1200-1800) Bragg crystal x-ray spectrometer is being developed to measure plasma parameters in National Ignition Facility experiments. The instrument will be a diagnostic instrument manipulator positioned cassette designed mainly to infer electron density in compressed capsules from Stark broadening of the helium-β (1s 2 -1s3p) lines of krypton and electron temperature from the relative intensities of dielectronic satellites. Two conically shaped crystals will diffract and focus (1) the Kr Heβ complex and (2) the Heα (1s 2 -1s2p) and Lyα (1s-2p) complexes onto a streak camera photocathode for time resolved measurement, and a third cylindrical or conical crystal will focus the full Heα to Heβ spectral range onto an image plate to provide a time integrated calibration spectrum. Calculations of source x-ray intensity, spectrometer throughput, and spectral resolution are presented. Details of the conical-crystal focusing properties as well as the status of the instrumental design are also presented.

The Instruments and Capabilities of the Miniature X-Ray Solar Spectrometer (MinXSS) CubeSats

NASA Astrophysics Data System (ADS)

Moore, Christopher S.; Caspi, Amir; Woods, Thomas N.; Chamberlin, Phillip C.; Dennis, Brian R.; Jones, Andrew R.; Mason, James P.; Schwartz, Richard A.; Tolbert, Anne K.

2018-02-01

The Miniature X-ray Solar Spectrometer (MinXSS) CubeSat is the first solar science oriented CubeSat mission flown for the NASA Science Mission Directorate, with the main objective of measuring the solar soft X-ray (SXR) flux and a science goal of determining its influence on Earth's ionosphere and thermosphere. These observations can also be used to investigate solar quiescent, active region, and flare properties. The MinXSS X-ray instruments consist of a spectrometer, called X123, with a nominal 0.15 keV full-width at half-maximum (FWHM) resolution at 5.9 keV and a broadband X-ray photometer, called XP. Both instruments are designed to obtain measurements from 0.5 - 30 keV at a nominal time cadence of 10 s. A description of the MinXSS instruments, performance capabilities, and relation to the Geostationary Operational Environmental Satellite (GOES) 0.1 - 0.8 nm flux is given in this article. Early MinXSS results demonstrate the capability of measuring variations of the solar spectral soft X-ray (SXR) flux between 0.8 - 12 keV from at least GOES A5-M5 (5 × 10^{-8} - 5 ×10^{-5} W m^{-2}) levels and of inferring physical properties (temperature and emission measure) from the MinXSS data alone. Moreover, coronal elemental abundances can be inferred, specifically for Fe, Ca, Si, Mg, S, Ar, and Ni, when the count rate is sufficiently high at each elemental spectral feature. Additionally, temperature response curves and emission measure loci demonstrate the MinXSS sensitivity to plasma emission at different temperatures. MinXSS observations coupled with those from other solar observatories can help address some of the most compelling questions in solar coronal physics. Finally, simultaneous observations by MinXSS and the Reuven Ramaty High Energy Solar Spectroscopic Imager (RHESSI) can provide the most spectrally complete soft X-ray solar flare photon flux measurements to date.

Calibration of hard x-ray (15 - 50 keV) optics at the MPE test facility PANTER

NASA Astrophysics Data System (ADS)

Bräuninger, Heinrich; Burkert, Wolfgang; Hartner, Gisela D.; Citterio, Oberto; Ghigo, Mauro; Mazzoleni, Francesco; Pareschi, Giovanni; Spiga, Daniele

2004-02-01

The Max-Planck-Institut für extraterrestrische Physik (MPE) in Garching, Germany, operates the large X-ray beam line facility PANTER for testing astronomical systems. At PANTER a number of telescopes like EXOSAT, ROSAT, SAX, JET-X, ABRIXAS, XMM and SWIFT operating in the soft energy range (0.02 - 15 keV) have been successfully calibrated. In the present paper we report on an important upgrade recently implemented that enables the calibration of hard X-ray optics (from 15 up to 50 keV). Currently hard X-ray optics based on single and multilayer coating are being developed for several future X-ray missions. The hard X-ray calibrations at PANTER are carried out by a high energy source based on an electron gun and several anodes, able to cover the energy range from 4.5 up to 50 keV. It provides fluxes up to 104 counts/sec/cm2 at the instrument chamber with a stability better than 1%. As detector a pn-CCD camera operating between 0.2 and 50 keV and a collecting area of 36 cm2 is used. Taking into account the high energy resolution of the CCD (145 eV at 6 keV), a very easy way to operate the facility in hard X-ray is in energy-dispersive mode (i.e. with a broad-band beam). A double crystal monochromator is also available providing energies up to 20 keV. In this paper we present the first results obtained by using PANTER for hard X-ray characterizations, performed on prototype multilayer optics developed by the Osservatorio Astronomico di Brera (OAB), Milano, Italy, and the Harvard-Smithsonian Center for Astrophysics (CfA), Cambridge, MA, USA.

Non-proportionality study of CaMoO4 and GAGG:Ce scintillation crystals using Compton coincidence technique.

PubMed

Kaewkhao, J; Limkitjaroenporn, P; Chaiphaksa, W; Kim, H J

2016-09-01

In this study, the CCT technique and nuclear instrument module (NIM) setup for the measurements of coincidence electron energy spectra of calcium molybdate (CaMoO4) and cerium doped gadolinium aluminium gallium garnet (Gd3Al2Ga3O12:Ce or GAGG:Ce) scintillation crystals were carried out. The (137)Cs irradiated gamma rays with an energy (Eγ) of 662keV was used as a radioactive source. The coincidence electron energy spectra were recorded at seven scattering angles of 30°-120°. It was found that seven corresponding electron energies were in the range of 100.5-435.4keV. The results show that, for all electron energies, the electron energy peaks of CaMoO4 crystal yielded higher number of counts than those of GAGG:Ce crystal. The electron energy resolution, the light yield and non-proportionality were also determined. It was found that the energy resolutions are inverse proportional to the square root of electron energy for both crystals. Furthermore, the results show that the light yield of GAGG:Ce crystal is much higher than that of CaMoO4 crystal. It was also found that both CaMoO4 and GAGG:Ce crystals demonstrated good proportional property in the electron energy range of 260-435.4keV. Copyright © 2016 Elsevier Ltd. All rights reserved.

Muonium formation at keV energies

NASA Astrophysics Data System (ADS)

Prokscha, T.; Morenzoni, E.; Garifianov, N.; Glückler, H.; Khasanov, R.; Luetkens, H.; Suter, A.

2003-02-01

Charge differentiation in μ + or muonium (Mu) as a consequence of the slowing down of μ + in matter is of fundamental interest in the μSR method. It is also of relevance for understanding the moderation process of μ + in van der Waals solids like s-Ne, s-Ar or s-N 2, which are the most suitable materials to generate epithermal μ + serving as a source for low-energy μ + (LE-μ +) beams. The LE-μ + beam at the Paul Scherrer Institut (PSI) allows us to study the formation of Mu at low implantation energies (0.5- 30 keV) in insulators and semiconductors. These investigations may help to clarify the interaction between the μ + and the electrons of its ionisation track since the number of track electrons can be tuned by varying the implantation energy. We present the first results of LE-μSR investigations on thin van der Waals solids (s-Ar, s-Xe), fused quartz ( SUPRASIL) and a quartz crystal, where the μ + and Mu fractions were measured as a function of the implantation energy.

Terahertz photonic crystals

NASA Astrophysics Data System (ADS)

Jian, Zhongping

This thesis describes the study of two-dimensional photonic crystals slabs with terahertz time domain spectroscopy. In our study we first demonstrate the realization of planar photonic components to manipulate terahertz waves, and then characterize photonic crystals using terahertz pulses. Photonic crystal slabs at the scale of micrometers are first designed and fabricated free of defects. Terahertz time domain spectrometer generates and detects the electric fields of single-cycle terahertz pulses. By putting photonic crystals into waveguide geometry, we successfully demonstrate planar photonic components such as transmission filters, reflection frequency-selective filters, defects modes as well as superprisms. In the characterization study of out-of-plane properties of photonic crystal slabs, we observe very strong dispersion at low frequencies, guided resonance modes at middle frequencies, and a group velocity anomaly at high frequencies. We employ Finite Element Method and Finite-Difference Time-Domain method to simulate the photonic crystals, and excellent agreement is achieved between simulation results and experimental results.

APES: Acute Precipitating Electron Spectrometer - A High Time Resolution Monodirectional Magnetic Deflection Electron Spectrometer

NASA Technical Reports Server (NTRS)

Michell, R. G.; Samara, M.; Grubbs, G., II; Ogasawara, K.; Miller, G.; Trevino, J. A.; Webster, J.; Stange, J.

2016-01-01

We present a description of the Acute Precipitating Electron Spectrometer (APES) that was designed and built for the Ground-to-Rocket Electron Electrodynamics Correlative Experiment (GREECE) auroral sounding rocket mission. The purpose was to measure the precipitating electron spectrum with high time resolution, on the order of milliseconds. The trade-off made in order to achieve high time resolution was to limit the aperture to only one look direction. The energy selection was done by using a permanent magnet to separate the incoming electrons, such that the different energies would fall onto different regions of the microchannel plate and therefore be detected by different anodes. A rectangular microchannel plate (MCP) was used (15 mm x 100 mm), and there was a total of 50 discrete anodes under the MCP, each one 15 mm x 1.5 mm, with a 0.5 mm spacing between anodes. The target energy range of APES was 200 eV to 30 keV.

Handheld dual thermal neutron detector and gamma-ray spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stowe, Ashley C.; Burger, Arnold; Bhattacharya, Pijush

2017-05-02

A combined thermal neutron detector and gamma-ray spectrometer system, including: a first detection medium including a lithium chalcopyrite crystal operable for detecting neutrons; a gamma ray shielding material disposed adjacent to the first detection medium; a second detection medium including one of a doped metal halide, an elpasolite, and a high Z semiconductor scintillator crystal operable for detecting gamma rays; a neutron shielding material disposed adjacent to the second detection medium; and a photodetector coupled to the second detection medium also operable for detecting the gamma rays; wherein the first detection medium and the second detection medium do not overlapmore » in an orthogonal plane to a radiation flux. Optionally, the first detection medium includes a .sup.6LiInSe.sub.2 crystal. Optionally, the second detection medium includes a SrI.sub.2(Eu) scintillation crystal.« less

Fe XXV temperatures in flares from the Yohkoh Bragg crystal spectrometer

NASA Technical Reports Server (NTRS)

Sterling, Alphonse C.; Doschek, George A.; Pike, C. David

1994-01-01

Studies by Doschek et al. using P78-1 and Solar Maximum Misson (SMM) data have shown that the ratio of intensities of the Fe XXV and Ca XIX resonance lines can be expressed as a function of Fe XXV temperature. Using a more recent data set consisting of 13 flares observed by the Bragg crystal spectrometer (BCS) experiment on board Yohkoh, we find a nearly identical functional relationship between the same resonance line ratios and Fe XXV temperatures. We use this functional relationship to obtain resonance line ratio temperatures (T(sub RLR)) for each flare in our data set, and compare them with temperatures resulting from application of a simple spectral fitting method. (T(sub SSF)) to individal Fe XXV spectra. We also use a more involved free-parameter spectral fitting method to deduce temperatures (T(sub FSF)) from some of these spectra. On average, agreement between T(sub RLR) and T(sub SSF) improves as a flare progresses in time, with average agreements of 10.0% +/- 5.2%, 6.4% +/- 5.4%, and 5.0% +/- 3.9% over the rise, peak, and decay phases, respectively. Deviations between T(sub RLR) and T(sub FSF) are about the same or smaller. Thus, for most analysis purposes, all three methods yield virtually identical temperatures in flares. The somewhat poorer agreement between T(sub SSF) and T(sub RLR) during the earlier phases may be partially a result of difficulties in obtaining precise values for temperatures from spectral fits when blueshifts and large nonthermal broadenings are present in the spectra. Because of the high sensitivity of the Yohkoh BCS compared to that of BCS experiments on earlier spacecraft, we can for the first time consistently observe the heating phase of flares in Fe XXV.

A comparative study of LaBr3(Ce(3+)) and CeBr3 based gamma-ray spectrometers for planetary remote sensing applications.

PubMed

Kozyrev, A; Mitrofanov, I; Owens, A; Quarati, F; Benkhoff, J; Bakhtin, B; Fedosov, F; Golovin, D; Litvak, M; Malakhov, A; Mokrousov, M; Nuzhdin, I; Sanin, A; Tretyakov, V; Vostrukhin, A; Timoshenko, G; Shvetsov, V; Granja, C; Slavicek, T; Pospisil, S

2016-08-01

The recent availability of large volume cerium bromide crystals raises the possibility of substantially improving gamma-ray spectrometer limiting flux sensitivities over current systems based on the lanthanum tri-halides, e.g., lanthanum bromide and lanthanum chloride, especially for remote sensing, low-level counting applications or any type of measurement characterized by poor signal to noise ratios. The Russian Space Research Institute has developed and manufactured a highly sensitive gamma-ray spectrometer for remote sensing observations of the planet Mercury from the Mercury Polar Orbiter (MPO), which forms part of ESA's BepiColombo mission. The Flight Model (FM) gamma-ray spectrometer is based on a 3-in. single crystal of LaBr3(Ce(3+)) produced in a separate crystal development programme specifically for this mission. During the spectrometers development, manufacturing, and qualification phases, large crystals of CeBr3 became available in a subsequent phase of the same crystal development programme. Consequently, the Flight Spare Model (FSM) gamma-ray spectrometer was retrofitted with a 3-in. CeBr3 crystal and qualified for space. Except for the crystals, the two systems are essentially identical. In this paper, we report on a comparative assessment of the two systems, in terms of their respective spectral properties, as well as their suitability for use in planetary mission with respect to radiation tolerance and their propensity for activation. We also contrast their performance with a Ge detector representative of that flown on MESSENGER and show that: (a) both LaBr3(Ce(3+)) and CeBr3 provide superior detection systems over HPGe in the context of minimally resourced spacecraft and (b) CeBr3 is a more attractive system than LaBr3(Ce(3+)) in terms of sensitivities at lower gamma fluxes. Based on the tests, the FM has now been replaced by the FSM on the BepiColombo spacecraft. Thus, CeBr3 now forms the central gamma-ray detection element on the MPO spacecraft.

Venus Measurements by the MESSENGER Gamma-Ray and X-Ray Spectrometers

NASA Astrophysics Data System (ADS)

Rhodes, E. A.; Starr, R. D.; Goldsten, J. O.; Schlemm, C. E.; Boynton, W. V.

2007-12-01

The Gamma-Ray Spectrometer (GRS), which is a part of the Gamma-Ray and Neutron Spectrometer Instrument, and the X-Ray Spectrometer (XRS) on the MESSENGER spacecraft made calibration measurements during the Venus flyby on June 5, 2007. The purpose of these instruments is to determine elemental abundances on the surface of Mercury. The GRS measures gamma-rays emitted from element interactions with cosmic rays impinging on the surface, while the XRS measures X-ray emissions induced on the surface by the incident solar flux. The GRS sensor is a high-resolution high-purity Ge detector cooled by a Stirling cryocooler, surrounded by a borated-plastic anticoincidence shield. The GRS is sensitive to gamma-rays up to ~10 MeV and can identify most major elements, sampling down to depths of about ten centimeters. Only the shield was powered on for this flyby in order to conserve cooler lifetime. Gamma-rays were observed coming from Venus as well as from the spacecraft. Although the Venus gamma-rays originate from its thick atmosphere rather than its surface, the GRS data from this encounter will provide useful calibration data from a source of known composition. In particular, the data will be useful for determining GRS sensitivity and pointing options for the Mercury flybys, the first of which will be in January 2008. The X-ray spectrum of a planetary surface is dominated by a combination of the fluorescence and scattered solar X-rays. The most prominent fluorescent lines are the Kα lines from the major elements Mg, Al, Si, S, Ca, Ti, and Fe (1-10 keV). The sampling depth is less than 100 u m. The XRS is similar in design to experiments flown on Apollo 15 and 16 and the NEAR-Shoemaker mission. Three large-area gas-proportional counters view the planet, and a small Si-PIN detector mounted on the spacecraft sunshade monitors the Sun. The energy resolution of the gas proportional counters (~850 eV at 5.9 keV) is sufficient to resolve the X-ray lines above 2 keV, but Al and Mg

Effects of 160 keV electron irradiation on the optical properties and microstructure of "Panda" type Polarization-Maintaining optical fibers

NASA Astrophysics Data System (ADS)

Hong-Chen, Zhang; Hai, Liu; Hui-Jie, Xue; Wen-Qiang, Qiao; Shi-Yu, He

2012-11-01

In this paper, effects of 160 keV electron irradiated "Panda" type Polarization-Maintaining optical fiber at 1310 nm are investigated by us. Attenuation coefficient induced in optical fiber by electron beams at 1310 nm increases with increase in electron fluence. Electron irradiation-induced damage mechanism are studied by means of CASINO simulation program, the X-ray photoelectron spectroscopy (XPS), electron spin resonance spectrometer (EPR) and Fourier transform infrared spectroscopy (FTIR). The results show that Si-OH impurity defect concentration is the main reason of increasing attenuation coefficient at 1310 nm.

LaBr3γ-ray spectrometer for detecting 10B in debris of melted nuclear fuel

NASA Astrophysics Data System (ADS)

Koizumi, Mitsuo; Tsuchiya, Harufumi; Kitatani, Fumito; Harada, Hideo; Heyse, Jan; Kopecky, Stefan; Mondelaers, Willy; Paradela, Carlos; Schillebeeckx, Peter

2016-11-01

Neutron resonance densitometry has been proposed as a nondestructive analytical method for quantifying special nuclear material (SNM) in the rock- and particle-like debris that is to be removed from the Fukushima Daiichi nuclear power plant. The method is based on neutron resonance transmission analysis (NRTA) and neutron resonance capture analysis combined with prompt-γ-ray analysis (NRCA/PGA). Although quantification of SNM will predominantly rely on NRTA, this will be hampered by the presence of strong neutron-absorbing matrix materials, in particular 10B. Results obtained with NRCA/PGA are used to improve the interpretation of NRTA data. Prompt γ rays originating from the 10B(n, αγ) reaction are used to assess the amount of 10B. The 478 keV γ rays from 10B, however, need to be measured under a high-radiation environment, especially because of 137Cs. To meet this requirement, we developed a well-shaped γ-ray spectrometer consisting of one cylindrical and four rectangular-cuboid LaBr3 scintillators combined with a fast data-acquisition system. Furthermore, to improve the gain stability of the main detector, a special high-voltage divider was developed. Because of the reduction in gain shift, a 3.8% resolution at 662 keV was obtained for long-term measurements. By using the data-acquisition system, which consists of eight 250 MHz digitizers, input signals of over 500 kHz per channel were recorded. The work reported herein demonstrates that, with such a spectrometer, the impact of the Compton edge of 662 keV γ rays from 137Cs is significantly reduced, which allows the 10B amount to be determined with greater sensitivity.

Remarks on a Johann spectrometer for exotic-atom research and more

NASA Astrophysics Data System (ADS)

Gotta, Detlev E.; Simons, Leopold M.

2016-06-01

General properties of a Johann-type spectrometer equipped with spherically bent crystals are described leading to simple rules of thumb for practical use. They are verified by comparing with results from Monte-Carlo studies and demonstrated by selected measurements in exotic-atom and X-ray fluorescence research.

An experiment to measure the mass density of a plasma armature

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rogers, J.W.; Thomas, K.A.; Clothiaux, E.J.

1991-01-01

In this paper a diagnostic technique for determining the mass density, and possibly the plasma composition, of the plasma armature in the MIDI-3 free-running arc device is described. The armature consists primarily of the components of polythylene and copper, and it can reach velocities in excess of 8 km/sec. The approach in this proof-of-principle experiment utilizes a flash x-ray source with x rays having energies from 3 keV to 20 keV, an elliptical x-ray crystal spectrometer, and an appropriate detector array and data acquisition system.

Study of high resolution x-ray spectrometer concepts for NIF experiments

NASA Astrophysics Data System (ADS)

Hill, K. W.; Bitter, M.; Delgado-Aparicio, L.; Efthimion, P.; Gao, L.; Maddox, J.; Pablant, N. A.; Beiersdorfer, P.; Chen, H.; Coppari, F.; Ma, T.; Nora, R.; Scott, H.; Schneider, M.; Mancini, R.

2015-11-01

Options have been investigated for DIM-insertable (Diagnostic Instrument Manipulator) high resolution (E/ ΔE ~ 3000 - 5000) Bragg crystal x-ray spectrometers for experiments on the NIF. Of interest are time integrated Cu K- and Ta L-edge absorption spectra and time resolved Kr He- β emission from compressed symcaps for inference of electron temperature from dielectronic satellites and electron density from Stark broadening. Cylindrical and conical von Hamos, Johann, and advanced high throughput designs have been studied. Predicted x-ray intensities, spectrometer throughputs, spectral resolution, and spatial focusing properties, as well as lab evaluations of some spectrometer candidates will be presented. Performed under the auspices of the US DOE by PPPL under contract DE-AC02-09CH11466 and by LLNL under contract DE-AC52-07NA27344.

X-ray emitting hot plasma in solar active regions observed by the SphinX spectrometer

NASA Astrophysics Data System (ADS)

Miceli, M.; Reale, F.; Gburek, S.; Terzo, S.; Barbera, M.; Collura, A.; Sylwester, J.; Kowalinski, M.; Podgorski, P.; Gryciuk, M.

2012-08-01

Aims: The detection of very hot plasma in the quiescent corona is important for diagnosing heating mechanisms. The presence and the amount of such hot plasma is currently debated. The SphinX instrument on-board the CORONAS-PHOTON mission is sensitive to X-ray emission of energies well above 1 keV and provides the opportunity to detect the hot plasma component. Methods: We analysed the X-ray spectra of the solar corona collected by the SphinX spectrometer in May 2009 (when two active regions were present). We modelled the spectrum extracted from the whole Sun over a time window of 17 days in the 1.34-7 keV energy band by adopting the latest release of the APED database. Results: The SphinX broadband spectrum cannot be modelled by a single isothermal component of optically thin plasma and two components are necessary. In particular, the high statistical significance of the count rates and the accurate calibration of the spectrometer allowed us to detect a very hot component at ~7 million K with an emission measure of ~2.7 × 1044 cm-3. The X-ray emission from the hot plasma dominates the solar X-ray spectrum above 4 keV. We checked that this hot component is invariably present in both the high and low emission regimes, i.e. even excluding resolvable microflares. We also present and discuss the possibility of a non-thermal origin (which would be compatible with a weak contribution from thick-target bremsstrahlung) for this hard emission component. Conclusions: Our results support the nanoflare scenario and might confirm that a minor flaring activity is ever-present in the quiescent corona, as also inferred for the coronae of other stars.

Pseudoslit Spectrometer

NASA Technical Reports Server (NTRS)

Reuter, Dennis C.; McCabe, George H.

2004-01-01

The pseudoslit spectrometer is a conceptual optoelectronic instrument that would offer some of the advantages, without the disadvantages, of prior linear-variable etalon (LVE) spectrometers and prior slit spectrometers. The pseudoslit spectrometer is so named because it would not include a slit, but the combined effects of its optical components would include a spatial filtering effect approximately equivalent to that of a slit. Like a prior LVE spectrometer, the pseudoslit spectrometer would include an LVE (essentially, a wedge-like narrowband- pass filter, the pass wavelength of which varies linearly with position in one dimension) in a focal plane covering an imaging planar array of photodetectors. However, the pseudoslit spectrometer would be more efficient because unlike a prior LVE spectrometer, the pseudoslit spectrometer would not have to be scanned across an entire field of view to obtain the spectrum of an object of interest that may occupy only a small portion of the field of view. Like a prior slit spectrometer, the pseudoslit spectrometer could acquire the entire spectrum of such a small object without need for scanning. However, the pseudoslit spectrometer would be optically and mechanically simpler: it would have fewer components and, hence, would pose less of a problem of alignment of components and would be less vulnerable to misalignment.

Crystal face temperature determination means

DOEpatents

Nason, Donald O.; Burger, Arnold

1994-01-01

An optically transparent furnace (10) having a detection apparatus (29) with a pedestal (12) enclosed in an evacuated ampule (16) for growing a crystal (14) thereon. Temperature differential is provided by a source heater (20), a base heater (24) and a cold finger (26) such that material migrates from a polycrystalline source material (18) to grow the crystal (14). A quartz halogen lamp (32) projects a collimated beam (30) onto the crystal (14) and a reflected beam (34) is analyzed by a double monochromator and photomultiplier detection spectrometer (40) and the detected peak position (48) in the reflected energy spectrum (44) of the reflected beam (34) is interpreted to determine surface temperature of the crystal (14).

Low-energy nuclear reactions in crystal structures

NASA Astrophysics Data System (ADS)

Bagulya, A. V.; Dalkarov, O. D.; Negodaev, M. A.; Rusetskii, A. S.

2017-09-01

Results of studying low-energy nuclear reactions at the HELIS facility (LPI) are presented. Investigations of yields from DD reactions in deuterated crystal structures at deuteron energies of 10 to 25 keV show a considerable enhancement effect. It is shown that exposure of the deuterated targets to the H+ (proton) and Ne+ beams with energies from 10 to 25 keV and an X-ray beam with the energy of 20 to 30 keV stimulates DD reaction yields. For the CVD diamond target, it is shown that its orientation with respect to the deuteron beam affects the neutron yield. The D+ beam is shown to cause much higher heat release in the TiDx target than the H+ and Ne+ beams, and this heat release depends on the deuterium concentration in the target and the current density of the deuteron beam.

A Bonner Sphere Spectrometer based on a large 6LiI(Eu) scintillator: Calibration in reference monoenergetic fields

NASA Astrophysics Data System (ADS)

Bedogni, R.; Pola, A.; Costa, M.; Monti, V.; Thomas, D. J.

2018-07-01

A Bonner Sphere spectrometer employing a large, 11 mm diameter × 3 mm thickness, 6LiI(Eu) scintillator (LL-BSS), was assembled. The purpose was to produce a BSS similar in sensitivity to those based on 3He sensors, but using alternative sensors. With respect to the traditional BSS based on the 4 mm (diameter) × 4 mm (height) 6LiI(Eu), this new BSS is a factor of 3 more sensitive. LL-BSS response matrix, determined with MCNPX, was experimentally evaluated with monoenergetic reference neutron fields of 144 keV, 565 keV and 1.2 MeV available at NPL (Teddington, UK). The results of the experiment confirmed the correctness of the response matrix within an overall uncertainty lower than ±2%.

Einstein Observatory solid state spectrometer observations of M87 and the Virgo cluster

NASA Technical Reports Server (NTRS)

Lea, S. M.; Mushotzky, R.; Holt, S. S.

1982-01-01

X-ray observations of the galaxy M87 and of a region in the Virgo cluster displaced 7 arcmin from the center of M87 are reported. X-ray spectra were obtained at these two locations with the Solid State Spectrometer onboard the Einstein Observatory. Emission lines were observed in both locations, indicating the presence of heavy elements at abundances near solar. There is no strong abundance gradient, within the errors. A temperature gradient has been detected: T increases from about 1.4 keV at the position of M87 to about 3.35 keV 7 arcmin away. There is lower temperature thermal emission at the center of M87 with T about 0.6 keV, consistent with models for cooling flows in this cluster. A mass infall rate of nearly 20 solar masses/yr has been obtained. In addition to the thermal emission, a power-law component has been detected in the spectrum of M87, consistent with that observed by HEAO 1, indicating that this component probably originates in the galaxy itself. Comparison of the results with those of other observers and with theoretical models for this source indicates the presence of intracluster gas having density near 1/1000 per cu cm and temperature of about 30,000,000 K.

Development of portable CdZnTe spectrometers for remote sensing of signatures from nuclear materials

NASA Astrophysics Data System (ADS)

Burger, Arnold; Groza, Michael; Cui, Yunlong; Roy, Utpal N.; Hillman, Damian; Guo, Mike; Li, Longxia; Wright, Gomez W.; James, Ralph B.

2005-03-01

Room temperature cadmium zinc telluride (CZT) gamma-ray spectrometers are being developed for a number for years for medical, space and national security applications where high sensitivity, low operating power and compactness are indispensable. The technology has matured now to the point where large volume (several cubic centimeters) and high energy resolution (approximately 1% at 660 eV) of gamma photons, are becoming available for their incorporation into portable systems for remote sensing of signatures from nuclear materials. The straightforward approach of utilizing a planar CZT device has been excluded due to the incomplete collection arising from the trapping of holes and causing broadening of spectral lines at energies above 80 keV, to unacceptable levels of performance. Solutions are being pursued by developing devices aimed at processing the signal produced primarily by electrons and practically insensitive to the contribution of holes, and recent progress has been made in the areas of material growth as well as electrode and electronics design. Present materials challenges are in the growth of CZT boules from which large, oriented single crystal pieces can be cut to fabricate such sizable detectors. Since virtually all the detector grade CZT boules consist of several grains, the cost of a large, single crystal section is still high. Co-planar detectors, capacitive Frisch-grid detectors and devices taking advantage of the small pixel effect, are configurations with a range of requirements in crystallinity and defect content and involve variable degrees of complexity in the fabrication, surface passivation and signal processing. These devices have been demonstrated by several research groups and will be discussed in terms of their sensitivity and availability.

Copper crystal lens for medical imaging: first results

NASA Astrophysics Data System (ADS)

Roa, Dante E.; Smither, Robert K.

2001-06-01

A copper crystal lens designed to focus gamma ray energies of 100 to 200 keV has been assembled at Argonne National Laboratory. In particular, the lens has been optimized to focus the 140.6 keV gamma rays from technetium-99 m typically used in radioactive tracers. This new approach to medical imaging relies on crystal diffraction to focus incoming gamma rays in a manner similar to a simple convex lens focusing visible light. The lens is envisioned to be part of an array of lenses that can be used as a complementary technique to gamma cameras for localized scans of suspected tumor regions in the body. In addition, a 2- lens array can be used to scan a woman's breast in search of tumors with no discomfort to the patient. The incoming gamma rays are diffracted by a set of 828 copper crystal cubes arranged in 13 concentric rings, which focus the gamma rays into a very small area on a well-shielded NaI detector. Experiments performance with technetium-99 m and cobalt 57 radioactive sources indicate that a 6-lens array should be capable of detecting sources with (mu) Ci strength.

Calibration of a High Resolution X-ray Spectrometer for High-Energy-Density Plasmas on NIF

NASA Astrophysics Data System (ADS)

Kraus, B.; Gao, L.; Hill, K. W.; Bitter, M.; Efthimion, P.; Schneider, M. B.; Chen, H.; Ayers, J.; Beiersdorfer, P.; Liedahl, D.; Macphee, A. G.; Thorn, D. B.; Bettencourt, R.; Kauffman, R.; Le, H.; Nelson, D.

2017-10-01

A high-resolution, DIM-based (Diagnostic Instrument Manipulator) x-ray crystal spectrometer has been calibrated for and deployed at the National Ignition Facility (NIF) to diagnose plasma conditions and mix in ignition capsules near stagnation times. Two conical crystals in the Hall geometry focus rays from the Kr He- α, Ly- α, and He- β complexes onto a streak camera for time-resolved spectra, in order to measure electron density and temperature by observing Stark broadening and relative intensities of dielectronic satellites. Signals from these two crystals are correlated with a third crystal that time-integrates the intervening energy range. The spectrometer has been absolutely calibrated using a microfocus x-ray source, an array of CCD and single-photon-counting detectors, and K- and L-absorption edge filters. Measurements of the integrated reflectivity, energy range, and energy resolution for each crystal will be presented. The implications of the calibration on signal levels from NIF implosions and x-ray filter choices will be discussed. This work was performed under the auspices of the U.S. DoE by Princeton Plasma Physics Laboratory under contract DE-AC02-09CH11466 and by Lawrence Livermore National Laboratory under contract DE-AC52-07NA27344.

Electro-optic imaging Fourier transform spectrometer

NASA Technical Reports Server (NTRS)

Chao, Tien-Hsin (Inventor); Znod, Hanying (Inventor)

2009-01-01

An Electro-Optic Imaging Fourier Transform Spectrometer (EOIFTS) for Hyperspectral Imaging is described. The EOIFTS includes an input polarizer, an output polarizer, and a plurality of birefringent phase elements. The relative orientations of the polarizers and birefringent phase elements can be changed mechanically or via a controller, using ferroelectric liquid crystals, to substantially measure the spectral Fourier components of light propagating through the EIOFTS. When achromatic switches are used as an integral part of the birefringent phase elements, the EIOFTS becomes suitable for broadband applications, with over 1 micron infrared bandwidth.

Set-up of an XAFS beamline for measurements between 2.4-8 keV at DORIS III

DOE Office of Scientific and Technical Information (OSTI.GOV)

Welter, Edmund

2010-06-23

In this paper results from the commissioning phase and from first user experiments of a new EXAFS beamline at the DORIS III storage ring are presented. The bending magnet EXAFS beamline A1 underwent a complete rebuild and now covers the energy range 2.4-8 keV. A Ni-coated toroidal mirror, placed in a 2:1 focusing position and a plane mirror with one Ni coated stripe and one uncoated (SiO{sub 2}) stripe are used for effective higher harmonics suppression and focusing. The UHV-compatible fixed-exit Double Crystal Monochromator (DCM) is equipped with two Si(111) crystal pairs. The second crystal of one of the twomore » crystal pairs is tilted by 90 deg. around the surface normal to shift the position of glitches. It allows Bragg angles between 5 deg. and 55.5 deg. and continuous scans in quick-EXAFS mode. Test measurements during the commissioning phase proved the excellent performance of the monochromator and a high quality of the XAFS spectra over the entire working range.« less

Measuring the x-ray resolving power of bent potassium acid phthalate diffraction crystals

DOE Office of Scientific and Technical Information (OSTI.GOV)

Haugh, M. J., E-mail: haughmj@nv.doe.gov; Jacoby, K. D.; Wu, M.

2014-11-15

This report presents the results from measuring the X-ray resolving power of a curved potassium acid phthalate (KAP(001)) spectrometer crystal using two independent methods. It is part of a continuing effort to measure the fundamental diffraction properties of bent crystals that are used to study various characteristics of high temperature plasmas. Bent crystals like KAP(001) do not usually have the same diffraction properties as corresponding flat crystals. Models that do exist to calculate the effect of bending the crystal on the diffraction properties have simplifying assumptions and their accuracy limits have not been adequately determined. The type of crystals thatmore » we measured is being used in a spectrometer on the Z machine at Sandia National Laboratories in Albuquerque, New Mexico. The first technique for measuring the crystal resolving power measures the X-ray spectral line width of the characteristic lines from several metal anodes. The second method uses a diode X-ray source and a double crystal diffractometer arrangement to measure the reflectivity curve of the KAP(001) crystal. The width of that curve is inversely proportional to the crystal resolving power. The measurement results are analyzed and discussed.« less

Initial Results From The Chandra High Energy Transmission Grating Spectrometer

NASA Technical Reports Server (NTRS)

Canizares, C. R.; Davis, D. S.; Dewey, D.; Flanagan, K. A.; Houck, J.; Huenemoerder, D. P.; Marshall, H. L.; Schattenburg, M. L.; Schulz, N. S.; Wise, M.

2000-01-01

The High Energy Transmission Grating Spectrometer (HETGS) on the Chandra X-ray Observatory provides spectral resolving powers of 200-1000 over the range 0.4-8.0 keV (1.5-30 A) with effective area of 2-200 square centimeters. Initial observations during the activation and calibration phases of the mission show that the HETGS is performing as predicted prior to Chandra launch. The talk presented very preliminary results that illustrate the power of the HETGS for performing detailed studies of a wide range of celestial sources, including plasma diagnostics. This written version gives a brief summary of that talk with examples of preliminary spectra of Capella, the Crab pulsar, SS433 and the SNR E0102-72.

Characteristics of bursts observed by the SMM Gamma-Ray Spectrometer

NASA Technical Reports Server (NTRS)

Share, G. H.; Messina, D. C.; Iadicicco, A.; Matz, S. M.; Rieger, E.; Forrest, D. J.

1992-01-01

The Gamma Ray Spectrometer (GRS) on the SMM completed close to 10 years of highly successful operation when the spacecraft reentered the atmosphere on December 2, 1989. During this period the GRS detected 177 events above 300 keV which have been classified as cosmic gamma-ray bursts. A catalog of these events is in preparation which will include time profiles and spectra for all events. Visual inspection of the spectra indicates that emission typically extends into the MeV range, without any evidence for a high-energy cutoff; 17 of these events are also observed above 10 MeV. We find no convincing evidence for line-like emission features in any of the time-integrated spectra.

High energy resolution, high angular acceptance crystal monochromator

DOEpatents

Alp, E.E.; Mooney, T.M.; Toellner, T.

1996-06-04

A 4-bounce dispersive crystal monochromator reduces the bandpass of synchrotron radiation to a 10-50 meV range without sacrificing angular acceptance. The monochromator includes the combination of an asymmetrical channel-cut single crystal of lower order reflection and a symmetrical channel-cut single crystal of higher order reflection in a nested geometric configuration. In the disclosed embodiment, a highly asymmetrically cut ({alpha}=20) outer silicon crystal (4 2 2) with low order reflection is combined with a symmetrically cut inner silicon crystal (10 6 4) with high order reflection to condition a hard x-ray component (5--30 keV) of synchrotron radiation down to the {micro}eV-neV level. Each of the crystals is coupled to the combination of a positioning inchworm and angle encoder via a respective rotation stage for accurate relative positioning of the crystals and precise energy tuning of the monochromator. 7 figs.

High energy resolution, high angular acceptance crystal monochromator

DOEpatents

Alp, Ercan E.; Mooney, Timothy M.; Toellner, Thomas

1996-06-04

A 4-bounce dispersive crystal monochromator reduces the bandpass of synchrotron radiation to a 10-50 meV range without sacrificing angular acceptance. The monochromator includes the combination of an asymmetrical channel-cut single crystal of lower order reflection and a symmetrical channel-cut single crystal of higher order reflection in a nested geometric configuration. In the disclosed embodiment, a highly asymmetrically cut (.alpha.=20) outer silicon crystal (4 2 2) with low order reflection is combined with a symmetrically cut inner silicon crystal (10 6 4) with high order reflection to condition a hard x-ray component (5-30 keV) of synchrotron radiation down to the .mu.eV-neV level. Each of the crystals is coupled to the combination of a positioning inchworm and angle encoder via a respective rotation stage for accurate relative positioning of the crystals and precise energy tuning of the monochromator.

X-ray spectrum of Cassiopeia A measured with the Einstein SSS. [Solid State Spectrometer

NASA Technical Reports Server (NTRS)

Becker, R. H.; Smith, B. W.; White, N. E.; Holt, S. S.; Boldt, E. A.; Mushotzky, R. F.; Serlemitsos, P. J.

1979-01-01

The solid state spectrometer (SSS) on the Einstein Observatory observed the X-ray spectrum of Cas A between 0.8 and 4.5 keV with a FWHM energy resolution of 160 eV. Line emission consistent with transitions of helium-like ions of Si, S, and Ar was well defined. Comparison between the data and the emission expected from a gas containing two distinct thermal components requires additional line emission from Mg, Al, Ca, and Fe. These results are discussed in the context of both equilibrium and nonequilibrium situations.

Development and characterization of semiconductor ion detectors for plasma diagnostics in the range over 0.3 keV

NASA Astrophysics Data System (ADS)

Cho, T.; Sakamoto, Y.; Hirata, M.; Kohagura, J.; Makino, K.; Kanke, S.; Takahashi, K.; Okamura, T.; Nakashima, Y.; Yatsu, K.; Tamano, T.; Miyoshi, S.

1997-01-01

For the purpose of plasma-ion-energy analyses in a wide-energy range from a few hundred eV to hundreds of keV, upgraded semiconductor detectors are newly fabricated and characterized using a test-ion-beam line from 0.3 to 12 keV. In particular, the detectable lowest-ion energy is drastically improved at least down to 0.3 keV; this energy is one to two orders-of-magnitude better than those for commercially available Si-surface-barrier diodes employed for previous plasma-ion diagnostics. A signal-to-noise ratio of two to three orders-of-magnitude better than that for usual metal-collector detectors is demonstrated for the compact-sized semiconductor along with the availability of the use under conditions of a good vacuum and a strong-magnetic field. Such characteristics are achieved due to the improving methods of the optimization of the thicknesses of a Si dead layer and a SiO2 layer, as well as the nitrogen-doping technique near the depletion layer along with minimizing impurity concentrations in Si. Such an upgraded capability of an extremely low-energy-ion detection with the low-noise characteristics enlarges research regimes of plasma-ion behavior using semiconductor detectors not only in the divertor regions of tokamaks but in wider spectra of open-field plasma devices including tandem mirrors. An application of the semiconductor ion detector for plasma-ion diagnostics is demonstrated in a specially designed ion-spectrometer structure.

Layout and results from the initial operation of the high-resolution x-ray imaging crystal spectrometer on the Large Helical Device.

PubMed

Pablant, N A; Bitter, M; Delgado-Aparicio, L; Goto, M; Hill, K W; Lazerson, S; Morita, S; Roquemore, A L; Gates, D; Monticello, D; Nielson, H; Reiman, A; Reinke, M; Rice, J E; Yamada, H

2012-08-01

First results of ion and electron temperature profile measurements from the x-ray imaging crystal spectrometer (XICS) diagnostic on the Large Helical Device (LHD) are presented. This diagnostic system has been operational since the beginning of the 2011 LHD experimental campaign and is the first application of the XICS diagnostic technique to helical plasma geometry. The XICS diagnostic provides measurements of ion and electron temperature profiles in LHD with a spatial resolution of 2 cm and a maximum time resolution of 5 ms (typically 20 ms). Ion temperature profiles from the XICS diagnostic are possible under conditions where charge exchange recombination spectroscopy (CXRS) is not possible (high density) or is perturbative to the plasma (low density or radio frequency heated plasmas). Measurements are made by using a spherically bent crystal to provide a spectrally resolved 1D image of the plasma from line integrated emission of helium-like Ar(16 +). The final hardware design and configuration are detailed along with the calibration procedures. Line-integrated ion and electron temperature measurements are presented, and the measurement accuracy is discussed. Finally central temperature measurements from the XICS system are compared to measurements from the Thomson scattering and CXRS systems, showing excellent agreement.

A comparative study of LaBr{sub 3}(Ce{sup 3+}) and CeBr{sub 3} based gamma-ray spectrometers for planetary remote sensing applications

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kozyrev, A., E-mail: kozyrev@mx.iki.rssi.ru; Mitrofanov, I.; Bakhtin, B.

The recent availability of large volume cerium bromide crystals raises the possibility of substantially improving gamma-ray spectrometer limiting flux sensitivities over current systems based on the lanthanum tri-halides, e.g., lanthanum bromide and lanthanum chloride, especially for remote sensing, low-level counting applications or any type of measurement characterized by poor signal to noise ratios. The Russian Space Research Institute has developed and manufactured a highly sensitive gamma-ray spectrometer for remote sensing observations of the planet Mercury from the Mercury Polar Orbiter (MPO), which forms part of ESA’s BepiColombo mission. The Flight Model (FM) gamma-ray spectrometer is based on a 3-in. singlemore » crystal of LaBr{sub 3}(Ce{sup 3+}) produced in a separate crystal development programme specifically for this mission. During the spectrometers development, manufacturing, and qualification phases, large crystals of CeBr{sub 3} became available in a subsequent phase of the same crystal development programme. Consequently, the Flight Spare Model (FSM) gamma-ray spectrometer was retrofitted with a 3-in. CeBr{sub 3} crystal and qualified for space. Except for the crystals, the two systems are essentially identical. In this paper, we report on a comparative assessment of the two systems, in terms of their respective spectral properties, as well as their suitability for use in planetary mission with respect to radiation tolerance and their propensity for activation. We also contrast their performance with a Ge detector representative of that flown on MESSENGER and show that: (a) both LaBr{sub 3}(Ce{sup 3+}) and CeBr{sub 3} provide superior detection systems over HPGe in the context of minimally resourced spacecraft and (b) CeBr{sub 3} is a more attractive system than LaBr{sub 3}(Ce{sup 3+}) in terms of sensitivities at lower gamma fluxes. Based on the tests, the FM has now been replaced by the FSM on the BepiColombo spacecraft. Thus, CeBr{sub 3

In-flight calibration of Hitomi Soft X-ray Spectrometer. (3) Effective area

NASA Astrophysics Data System (ADS)

Tsujimoto, Masahiro; Okajima, Takashi; Eckart, Megan E.; Hayashi, Takayuki; Hoshino, Akio; Iizuka, Ryo; Kelley, Richard L.; Kilbourne, Caroline A.; Leutenegger, Maurice A.; Maeda, Yoshitomo; Mori, Hideyuki; Porter, Frederick S.; Sato, Kosuke; Sato, Toshiki; Serlemitsos, Peter J.; Szymkowiak, Andrew; Yaqoob, Tahir

2018-03-01

We present the result of the in-flight calibration of the effective area of the Soft X-ray Spectrometer (SXS) on board the Hitomi X-ray satellite using an observation of the Crab nebula. We corrected for artifacts when observing high count rate sources with the X-ray microcalorimeter. We then constructed a spectrum in the 0.5-20 keV band, which we modeled with a single power-law continuum attenuated by interstellar extinction. We evaluated the systematic uncertainty of the spectral parameters by various calibration items. In the 2-12 keV band, the SXS result is consistent with the literature values in flux (2.20 ± 0.08 × 10-8 erg s-1 cm-2 with a 1 σ statistical uncertainty) but is softer in the power-law index (2.19 ± 0.11). The discrepancy is attributable to the systematic uncertainty of about +6%/-7% and +2%/-5% respectively for the flux and the power-law index. The softer spectrum is affected primarily by the systematic uncertainty of the Dewar gate valve transmission and the event screening.

Measuring the X-ray Resolving Power of Bent Potassium Acid Phthalate Diffraction Crystals

DOE Office of Scientific and Technical Information (OSTI.GOV)

Haugh, M. J.; Wu, M.; Jacoby, K. D.

2014-11-01

This report presents the results from measuring the X-ray resolving power of a curved potassium acid phthalate (KAP(001)) spectrometer crystal using two independent methods. It is part of a continuing effort to measure the fundamental diffraction properties of bent crystals that are used to study various characteristics of high temperature plasmas. Bent crystals like KAP(001) do not usually have the same diffraction properties as corresponding flat crystals. Models that do exist to calculate the effect of bending the crystal on the diffraction properties have simplifying assumptions and their accuracy limits have not been adequately determined. The type of crystals thatmore » we measured is being used in a spectrometer on the Z machine at Sandia National Laboratories (SNL) in Albuquerque, NM. The first technique for measuring the crystal resolving power measures the X-ray spectral line width of the characteristic lines from several metal anodes. The second method uses a diode X-ray source and a dual goniometer arrangement to measure the reflectivity curve of the KAP(001) crystal. The width of that curve is inversely proportional to the crystal resolving power. The measurement results are analyzed and discussed.« less

Alignment and absolute wavelength calibration of imaging Bragg spectrometers.

PubMed

Bertschinger, G; Marchuk, O; Barnsley, R

2016-11-01

In the present and the next generation of fusion devices, imaging Bragg spectrometers are key diagnostics to measure plasma parameters in the hot core, especially ion temperature and plasma rotation. The latter quantities are routinely obtained using the Doppler-width and -shift of the emitted spectral lines, respectively. Line shift measurements require absolute accuracies Δλ/λ of about 10 ppm, where λ-is the observed wavelength. For ITER and the present fusion devices, spectral lines of He-and H-like argon, iron, and krypton as well as Ne-like tungsten are foreseen for the measurements. For these lines, Kα lines can be found, some in higher order, which fit into the narrow energy window of the spectrometers. For arbitrary wavelength settings, Kα lines are also used to measure the miscut of the spherical crystals; afterwards the spectrometers can be set according to the geometrical imaging properties using coordinate measurement machines. For the spectrometers measuring Lyα lines of H-like ions, fluorescence targets can provide in situ localized calibration lines on the spectra. The fluorescence targets are used best in transmission and are excited by the thermal x-ray radiation of the plasma. An analytic theory of fluorescence is worked out.

Polarized neutron scattering on HYSPEC: the HYbrid SPECtrometer at SNS

DOE PAGES

Zaliznyak, Igor A.; Savici, Andrei T.; Ovidiu Garlea, V.; ...

2017-06-20

Here, we describe some of the first polarized neutron scattering measurements performed at HYSPEC [1-4] spectrometer at the Spallation Neutron Source, Oak Ridge National Laboratory. Furthermore, we discuss details of the instrument setup and the experimental procedures in the mode with full polarization analysis. Examples of polarized neutron diffraction and polarized inelastic neutron data obtained on single crystal samples are presented.

Superconducting High Energy Resolution Gamma-ray Spectrometers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chow, D T

2002-02-22

We have demonstrated that a bulk absorber coupled to a TES can serve as a good gamma-ray spectrometer. Our measured energy resolution of 70 eV at 60 keV is among the best measurements in this field. We have also shown excellent agreement between the noise predictions and measured noise. Despite this good result, we noted that our detector design has shortcomings with a low count rate and vulnerabilities with the linearity of energy response. We addressed these issues by implementation of an active negative feedback bias. We demonstrated the effects of active bias such as additional pulse shortening, reduction ofmore » TES change in temperature during a pulse, and linearization of energy response at low energy. Linearization at higher energy is possible with optimized heat capacities and thermal conductivities of the microcalorimeter. However, the current fabrication process has low control and repeatability over the thermal properties. Thus, optimization of the detector performance is difficult until the fabrication process is improved. Currently, several efforts are underway to better control the fabrication of our gamma-ray spectrometers. We are developing a full-wafer process to produce TES films. We are investigating the thermal conductivity and surface roughness of thicker SiN membranes. We are exploring alternative methods to couple the absorber to the TES film for reproducibility. We are also optimizing the thermal conductivities within the detector to minimize two-element phonon noise. We are experimenting with different absorber materials to optimize absorption efficiency and heat capacity. We are also working on minimizing Johnson noise from the E S shunt and SQUID amplifier noise. We have shown that our performance, noise, and active bias models agree very well with measured data from several microcalorimeters. Once the fabrication improvements have been implemented, we have no doubt that our gamma-ray spectrometer will achieve even more spectacular

R and D progress on second-generation crystals for Laue lens applications

NASA Astrophysics Data System (ADS)

Barrière, N.; von Ballmoos, P.; Bastie, P.; Courtois, P.; Abrosimov, N. V.; Andersen, K.; Buslaps, T.; Camus, T.; Halloin, H.; Jentschel, M.; Knödlseder, J.; Roudil, G.; Serre, D.; Skinner, G.

2007-09-01

The concept of a gamma-ray telescope based on a Laue lens offers the possibility to increase the sensitivity by more than an order of magnitude with respect to existing instruments. Laue lenses have been developed by our collaboration for several years : the main achievement of this R&D program was the CLAIRE lens prototype, which has successfully demonstrated the feasibility of the concept in astrophysical conditions. Since then, the endeavour has been oriented towards the development of efficient diffracting elements (crystal slabs) in order to increase both the effective area and the width of the energy bandpass focused, the aim being to step from a technological Laue lens to a scientifically exploitable lens. The latest mission concept featuring a gamma-ray lens is the European Gamma- Ray Imager (GRI) which intends to make use of the Laue lens to cover energies from 200 keV to 1300 keV. Investigations of two promising materials, low mosaicity copper and gradient concentration silicongermanium are presented in this paper. The measurements have been performed during three runs: 6 + 4 days at the European Synchrotron Radiation Facility (Grenoble, France), on beamline ID15A, using a 500 keV monochromatic beam, and 14 days on the GAMS 4 instrument of the Institute Laue Langevin (Grenoble, France) featuring a highly monochromatic beam of 517 keV. Despite it was not perfectly homogeneous, the presented copper crystal has exhibited peak reflectivity of 25 % in accordance with theoretical predictions, and a mosaicity around 26 arcsec, the ideal range for the realization of a Laue lens such as GRI. Silicon-germanium featuring a constant gradient have been measured for the very first time at 500 keV. Two samples showed a quite homogeneous reflectivity reaching 26%, which is far from the 48 % already observed in experimental crystals but a very encouraging beginning. The measured results have been used to estimate the performance of the GRI Laue lens design.

Ion profiling in an ambient drift tube-ion mobility spectrometer using a high pixel density linear array detector IonCCD.

PubMed

Davila, Stephen J; Hadjar, Omar; Eiceman, Gary A

2013-07-16

A linear pixel-based detector array, the IonCCD, is characterized for use under ambient conditions with thermal (<1 eV) positive ions derived from purified air and a 10 mCi (63)Ni foil. The IonCCD combined with a drift tube-ion mobility spectrometer permitted the direct detection of gas phase ions at atmospheric pressure and confirmed a limit of detection of 3000 ions/pixel/frame established previously in both the keV (1-2 keV) and the hyper-thermal (10-40 eV) regimes. Results demonstrate the "broad-band" application of the IonCCD over 10(5) orders in ion energy and over 10(10) in operating pressure. The Faraday detector of a drift tube for an ion mobility spectrometer was replaced with the IonCCD providing images of ion profiles over the cross-section of the drift tube. Patterns in the ion profiles were developed in the drift tube cross-section by control of electric fields between wires of Bradbury Nielson and Tyndall Powell shutter designs at distances of 1-8 cm from the detector. Results showed that ion beams formed in wire sets, retained their shape with limited mixing by diffusion and Coulombic repulsion. Beam broadening determined as 95 μm/cm for hydrated protons in air with moisture of ~10 ppmv. These findings suggest a value of the IonCCD in further studies of ion motion and diffusion of thermalized ions, enhancing computational results from simulation programs, and in the design or operation of ion mobility spectrometers.

Crystal growth and characterization of europium doped KCaI3, a high light yield scintillator

NASA Astrophysics Data System (ADS)

Lindsey, Adam C.; Zhuravleva, Mariya; Stand, Luis; Wu, Yuntao; Melcher, Charles L.

2015-10-01

The presented study reports on the spectroscopic characteristics of a new high performance scintillation material KCaI3:Eu. The growth of ∅ 17 mm boules using the Bridgman-Stockbarger method in fused silica ampoules is demonstrated to produce yellow tinted, yet transparent single crystals suitable for use in spectroscopic applications due to very promising performance. Scintillation light yield of 72,000 ± 3000 ph/MeV and energy resolution of 3% (FWHM) at 662 keV and 6.1% at 122 keV was obtained from small single crystals of approximately 15 mm3. For a much larger 3.8 cm3 detector, 4.4% and 7.3% for the same energy. Proportionality of the scintillation response to the energy of ionizing radiation is within 96% of the ideal response over an energy range of 14-662 keV. The high light yield and energy resolution of KCaI3:Eu make it suitable for potential use in domestic security applications requiring radionuclide identification.

Bragg crystal spectroscopy on the OSO 8 satellite

NASA Technical Reports Server (NTRS)

Long, K. S.; Chanan, G. A.; Helfand, D. J.; Ku, W. H.-M.; Novick, R.

1979-01-01

Results are reported for high-resolution OSO 8 Bragg-crystal spectroscopy of a variety of cosmic X-ray sources in the energy range from 2 to 10 keV. A continuous spectrum of Sco X-1 is examined, and results of a search for narrow line emission due to iron near 6.7 keV are presented for 32 galactic X-ray sources, including Sco X-1, Cyg X-3, and Cen X-3. It is noted that the strongest evidence for iron line emission has been obtained for Cyg X-3 and that evidence for an iron line feature has also been found in the spectrum of Cen X-3.

On the alignment and focusing of the Marshall Grazing Incidence X-ray Spectrometer (MaGIXS)

NASA Astrophysics Data System (ADS)

Champey, Patrick; Winebarger, Amy; Kobayashi, Ken; Savage, Sabrina; Cirtain, Jonathan; Cheimets, Peter; Hertz, Edward; Golub, Leon; Ramsey, Brian; McCracken, Jeff; Marquez, Vanessa; Allured, Ryan; Heilmann, Ralf K.; Schattenburg, Mark; Bruccoleri, Alexander

2016-07-01

The Marshall Grazing Incidence X-ray Spectrometer (MaGIXS) is a NASA sounding rocket instrument that is designed to observe soft X-ray emissions from 24 - 6.0 Å (0.5 - 2.0 keV energies) in the solar atmosphere. For the first time, high-temperature, low-emission plasma will be observed directly with 5 arcsecond spatial resolution and 22 mÅ spectral resolution. The unique optical design consists of a Wolter - I telescope and a 3-optic grazing- incidence spectrometer. The spectrometer utilizes a finite conjugate mirror pair and a blazed planar, varied line spaced grating, which is directly printed on a silicon substrate using e-beam lithography. The grating design is being finalized and the grating will be fabricated by the Massachusetts Institute of Technology (MIT) and Izentis LLC. Marshall Space Flight Center (MSFC) is producing the nickel replicated telescope and spectrometer mirrors using the same facilities and techniques as those developed for the ART-XC and FOXSI mirrors. The Smithsonian Astrophysical Observatory (SAO) will mount and align the optical sub-assemblies based on previous experience with similar instruments, such as the Hinode X-Ray Telescope (XRT). The telescope and spectrometer assembly will be aligned in visible light through the implementation of a theodolite and reference mirrors, in addition to the centroid detector assembly (CDA) - a device designed to align the AXAF-I nested mirrors. Focusing of the telescope and spectrometer will be achieved using the X-ray source in the Stray Light Facility (SLF) at MSFC. We present results from an alignment sensitivity analysis performed on the on the system and we also discuss the method for aligning and focusing MaGIXS.

On the Alignment and Focusing of the Marshall Grazing Incidence X-ray Spectrometer (MaGIXS)

NASA Technical Reports Server (NTRS)

Champey, Patrick; Winebarger, Amy; Kobayashi, Ken; Savage, Sabrina; Cirtain, Jonathan; Cheimets, Peter; Hertz, Edward; Golub, Leon; Ramsey, Brian; McCracken, Jeff

2016-01-01

The Marshall Grazing Incidence X-ray Spectrometer (MaGIXS) is a NASA sounding rocket instrument that is designed to observe soft X-ray emissions from 24 - 6.0 A (0.5 - 2.0 keV energies) in the solar atmosphere. For the rst time, high-temperature, low-emission plasma will be observed directly with 5 arcsecond spatial resolution and 22 mA spectral resolution. The unique optical design consists of a Wolter - I telescope and a 3-optic grazing- incidence spectrometer. The spectrometer utilizes a nite conjugate mirror pair and a blazed planar, varied line spaced grating, which is directly printed on a silicon substrate using e-beam lithography. The grating design is being nalized and the grating will be fabricated by the Massachusetts Institute of Technology (MIT) and Izentis LLC. Marshall Space Flight Center (MSFC) is producing the nickel replicated telescope and spectrometer mirrors using the same facilities and techniques as those developed for the ART-XC and FOXSI mirrors. The Smithsonian Astrophysical Observatory (SAO) will mount and align the optical sub-assemblies based on previous experience with similar instruments, such as the Hinode X-Ray Telescope (XRT). The telescope and spectrometer assembly will be aligned in visible light through the implementation of a theodolite and reference mirrors, in addition to the centroid detector assembly (CDA) { a device designed to align the AXAF-I nested mirrors. Focusing of the telescope and spectrometer will be achieved using the X-ray source in the Stray Light Facility (SLF) at MSFC. We present results from an alignment sensitivity analysis performed on the on the system and we also discuss the method for aligning and focusing MaGIXS.

The Reflection Grating Spectrometer on Board XMM-Newton

NASA Technical Reports Server (NTRS)

denHerder, J. W.; Brinkman, A. C.; Kahn, S. M.; Branduardi-Raymont, G.; Thomsen, K.; Aarts, H.; Audard, M.; Bixler, J. V.; denBoggende, A. J.

2000-01-01

The ESA X-ray Multi Mirror mission, XMM-Newton, carries two identical Reflection Grating Spectrometers (RGS) behind two of its three nested sets of Wolter I type mirrors. The instrument allows high-resolution (E/(Delta)E = 100 to 500) measurements in the soft X-ray range (6 to 38 A or 2.1 to 0.3 keV) with a maximum effective area of about 140 sq cm at 15 A. Its design is optimized for the detection of the K-shell transitions of carbon, nitrogen, oxygen, neon, magnesium, and silicon. as well as the L shell transitions of iron. The present paper gives a full description of the design of the RGS and its operational modes. We also review details of the calibrations and in-orbit performance including the line spread function, the wavelength calibration, the effective area, and the instrumental background.

Airborne Visible/Infrared Imaging Spectrometer (AVIRIS) spectrometer design and performance

NASA Technical Reports Server (NTRS)

Macenka, Steven A.; Chrisp, Michael P.

1987-01-01

The development of the Airborne Visible/Infrared Imaging Spectrometer (AVIRIS) has been completed at JPL. This paper outlines the functional requirements of the spectrometer optics subsystem, and describes the spectrometer optical design. The optical subsystem performance is shown in terms of spectral modulation transfer functions, radial energy distributions, and system transmission at selected wavelengths for the four spectrometers. An outline of the spectrometer alignment is included.

Development of position-sensitive time-of-flight spectrometer for fission fragment research

DOE PAGES

Arnold, C. W.; Tovesson, F.; Meierbachtol, K.; ...

2014-07-09

A position-sensitive, high-resolution time-of-flight detector for fission fragments has been developed. The SPectrometer for Ion DEtermination in fission Research (SPIDER) is a 2E–2v spectrometer designed to measure the mass of light fission fragments to a single mass unit. The time pick-off detector pairs to be used in SPIDER have been tested with α-particles from 229Th and its decay chain and α-particles and spontaneous fission fragments from 252Cf. Each detector module is comprised of thin electron conversion foil, electrostatic mirror, microchannel plates, and delay-line anodes. Particle trajectories on the order of 700 mm are determined accurately to within 0.7 mm. Flightmore » times were measured with 250 ps resolution FWHM. Computed particle velocities are accurate to within 0.06 mm/ns corresponding to a precision of 0.5%. As a result, an ionization chamber capable of 400 keV energy resolution coupled with the velocity measurements described here will pave the way for modestly efficient measurements of light fission fragments with unit mass resolution.« less

Calibration of Ge gamma-ray spectrometers for complex sample geometries and matrices

NASA Astrophysics Data System (ADS)

Semkow, T. M.; Bradt, C. J.; Beach, S. E.; Haines, D. K.; Khan, A. J.; Bari, A.; Torres, M. A.; Marrantino, J. C.; Syed, U.-F.; Kitto, M. E.; Hoffman, T. J.; Curtis, P.

2015-11-01

A comprehensive study of the efficiency calibration and calibration verification of Ge gamma-ray spectrometers was performed using semi-empirical, computational Monte-Carlo (MC), and transfer methods. The aim of this study was to evaluate the accuracy of the quantification of gamma-emitting radionuclides in complex matrices normally encountered in environmental and food samples. A wide range of gamma energies from 59.5 to 1836.0 keV and geometries from a 10-mL jar to 1.4-L Marinelli beaker were studied on four Ge spectrometers with the relative efficiencies between 102% and 140%. Density and coincidence summing corrections were applied. Innovative techniques were developed for the preparation of artificial complex matrices from materials such as acidified water, polystyrene, ethanol, sugar, and sand, resulting in the densities ranging from 0.3655 to 2.164 g cm-3. They were spiked with gamma activity traceable to international standards and used for calibration verifications. A quantitative method of tuning MC calculations to experiment was developed based on a multidimensional chi-square paraboloid.

Preliminary Results from Pyroelectric Crystal Accelerator

DOE Office of Scientific and Technical Information (OSTI.GOV)

Anderson, Tom; Edwards, Ronald; Bright, Kevin

The Nuclear Science and Engineering Research Center (NSERC), a Defense Threat Reduction Agency (DTRA) office located at the United States Military Academy (USMA), sponsors and manages cadet and faculty research in support of DTRA objectives. Cadets in the Department of Physics and Nuclear Engineering at USMA are using pyroelectric crystals to ionize and accelerate residual gas trapped inside a vacuum system. A system using two lithium tantalate crystals with associated diagnostics was designed and is now operational. X-ray energies of approximately 150 keV have been achieved. Future work will focus on developing a portable neutron generator using the D-D nuclearmore » fusion process.« less

Single-Crystal Bismuth Iodide Gamma-Ray Spectrometers

DTIC Science & Technology

2012-02-01

the density of the crystal (g/cm\\ M is the molecular weight of the vapor (g/mole), and R is the gas constant (cai/(K·mole)). Equation (6) indicates...along the vertical axis with a fixed rate. This simulated the downward movement of the ampoule in the conventional vertical Bridgman method. The...3cl512 1.03 4512 4.6 961 Pd Pd3d 336.5 Pd 3d512 1.03 6796 4.6 1477 Pdb N3d 340.3 Pd 3d3J2 1.03 2978 4.6 647 Pd Pd3d 341.7 Pd 3d3J2 1.03 4486 4.6 975

DOE Office of Scientific and Technical Information (OSTI.GOV)

Loether, A.; Adams, B. W.; DiCharia, A.

A hard x-ray pump–probe spectrometer using a multi-crystal Bragg reflector is demonstrated at a third generation synchrotron source. This device derives both broadband pump and monochromatic probe pulses directly from a single intense, broadband x-ray pulse centered at 8.767 keV. In conclusion, we present a proof-of-concept experiment which directly measures x-ray induced crystalline lattice strain.

Single crystal and optical ceramic multicomponent garnet scintillators: A comparative study

NASA Astrophysics Data System (ADS)

Wu, Yuntao; Luo, Zhaohua; Jiang, Haochuan; Meng, Fang; Koschan, Merry; Melcher, Charles L.

2015-04-01

Multicomponent garnet materials can be made in optical ceramic as well as single crystal form due to their cubic crystal structure. In this work, high-quality Gd3Ga3Al2O12:0.2 at% Ce (GGAG:Ce) single crystal and (Gd,Lu)3Ga3Al2O12:1 at% Ce (GLuGAG:Ce) optical ceramics were fabricated by the Czochralski method and a combination of hot isostatic pressing (HIPing) and annealing treatment, respectively. Under optical and X-ray excitation, the GLuGAG:Ce optical ceramic exhibits a broad Ce3+ transition emission centered at 550 nm, while the emission peak of the GGAG:Ce single crystal is centered at 540 nm. A self-absorption effect in GLuGAG:Ce optical ceramic results in this red-shift of the Ce3+ emission peak compared to that in the GGAG:Ce single crystal. The light yield under 662 keV γ-ray excitation was 45,000±2500 photons/MeV and 48,200±2410 photons/MeV for the GGAG:Ce single crystal and GLuGAG:Ce optical ceramic, respectively. An energy resolution of 7.1% for 662 keV γ-rays was achieved in the GLuGAG:Ce optical ceramic with a Hamamatsu R6231 PMT, which is superior to the value of 7.6% for a GGAG:Ce single crystal. Scintillation decay time measurements under 137Cs irradiation show two exponential decay components of 58 ns (47%) and 504 ns (53%) for the GGAG:Ce single crystal, and 84 ns (76%) and 148 ns (24%) for the GLuGAG:Ce optical ceramic. The afterglow level after X-ray cutoff in the GLuGAG:Ce optical ceramic is at least one order of magnitude lower than in the GGAG:Ce single crystal.

Germanium-gated γ-γ fast timing of excited states in fission fragments using the EXILL&FATIMA spectrometer

NASA Astrophysics Data System (ADS)

Régis, J.-M.; Simpson, G. S.; Blanc, A.; de France, G.; Jentschel, M.; Köster, U.; Mutti, P.; Paziy, V.; Saed-Samii, N.; Soldner, T.; Ur, C. A.; Urban, W.; Bruce, A. M.; Drouet, F.; Fraile, L. M.; Ilieva, S.; Jolie, J.; Korten, W.; Kröll, T.; Lalkovski, S.; Mach, H.; Mărginean, N.; Pascovici, G.; Podolyak, Zs.; Regan, P. H.; Roberts, O. J.; Smith, J. F.; Townsley, C.; Vancraeyenest, A.; Warr, N.

2014-11-01

A high-granularity mixed spectrometer consisting of high-resolution Ge and very fast LaBr3(Ce)-scintillator detectors has been installed around a fission target at the cold-neutron guide PF1B of the high-flux reactor of the Institut Laue-Langevin. Lifetimes of excited states in the range of 10 ps to 10 ns can be measured in around 100 exotic neutron-rich fission fragments using Ge-gated LaBr3(Ce)-LaBr3(Ce) or Ge-Ge-LaBr3(Ce)-LaBr3(Ce) coincidences. We report on various characteristics of the EXILL&FATIMA spectrometer for the energy range of 40 keV up to 6.8 MeV and present results of ps-lifetime test measurements in a fission fragment. The results are discussed with respect to possible systematic errors induced by background contributions.

Imaging birefringent crystals using micro optical coherence tomography (Conference Presentation)

NASA Astrophysics Data System (ADS)

Sharma, Gargi; Singh, Kanwarpal; Gardecki, Joseph A.; Tearney, Guillermo J.

2017-02-01

Background: Uric acid crystals have recently been identified as a possible therapeutic target for coronary artery disease. Being subcellular in size, it is difficult to identify these crystals in situ. Micro optical coherence tomography (Micro-OCT) allows one to image subcellular structures with 1-micron resolution. Even though Micro-OCT should be capable of resolving urate crystals, it's difficult to differentiate these structures from other scattering particles within tissue. In this work we developed a novel polarization sensitive micro OCT (ps-Micro-OCT) system for identification of uric acid crystals. Methods: A spectrometer based ps-Micro-OCT system was developed using a broadband light source. The broadband input light was divided into reference and sample signals using a beam splitter. The reference signal was further divided into two polarized signals with different polarization states. Reflected reference and sample signals were combined and sent to a spectrometer that recorded the interference signal. Results: To test the performance of system, a mirror was used as sample and a quarter wave-plate was placed in the sample path. The measured quarter wave-plate angle values matched closely to actual angle values. Next we prepared uric acid crystals in our lab and imaged them using this system.We were able to image and identify these crystals based on polarization measurements. Conclusion: In this work we imaged and identified uric acid crystals using a newly developed ps-Micro-OCT system. The proposed technique will enable imaging uric acid crystals in coronary artery.

Einstein Observatory SSS and MPC observations of the complex X-ray spectra of Seyfert galaxies. [Solid State Spectrometer and Monitor Proportional Counter

NASA Technical Reports Server (NTRS)

Turner, T. J.; Weaver, K. A.; Mushotzky, R. F.; Holt, S. S.; Madejski, G. M.

1991-01-01

The X-ray spectra of 25 Seyfert galaxies measured with the Solid State Spectrometer on the Einstein Observatory have been investigated. This new investigation utilizes simultaneous data from the Monitor Proportional Counter, and automatic correction for systematic effects in the Solid State Spectrometer which were previously handled subjectively. It is found that the best-fit single-power-law indices generally agree with those previously reported, but that soft excesses of some form are inferred for about 48 percent of the sources. One possible explanation of the soft excess emission is a blend of soft X-ray lines, centered around 0.8 keV. The implications of these results for accretion disk models are discussed.

The Fourier Imaging X-ray Spectrometer (FIXS) for the Argentinian, Scout-launched satelite de Aplicaciones Cienficas-1 (SAC-1)

NASA Technical Reports Server (NTRS)

Dennis, Brian R.; Crannell, Carol JO; Desai, Upendra D.; Orwig, Larry E.; Kiplinger, Alan L.; Schwartz, Richard A.; Hurford, Gordon J.; Emslie, A. Gordon; Machado, Marcos; Wood, Kent

1988-01-01

The Fourier Imaging X-ray Spectrometer (FIXS) is one of four instruments on SAC-1, the Argentinian satellite being proposed for launch by NASA on a Scout rocket in 1992/3. The FIXS is designed to provide solar flare images at X-ray energies between 5 and 35 keV. Observations will be made on arcsecond size scales and subsecond time scales of the processes that modify the electron spectrum and the thermal distribution in flaring magnetic structures.

Spherical grating spectrometers

NASA Astrophysics Data System (ADS)

O'Donoghue, Darragh; Clemens, J. Christopher

2014-07-01

We describe designs for spectrometers employing convex dispersers. The Offner spectrometer was the first such instrument; it has almost exclusively been employed on satellite platforms, and has had little impact on ground-based instruments. We have learned how to fabricate curved Volume Phase Holographic (VPH) gratings and, in contrast to the planar gratings of traditional spectrometers, describe how such devices can be used in optical/infrared spectrometers designed specifically for curved diffraction gratings. Volume Phase Holographic gratings are highly efficient compared to conventional surface relief gratings; they have become the disperser of choice in optical / NIR spectrometers. The advantage of spectrometers with curved VPH dispersers is the very small number of optical elements used (the simplest comprising a grating and a spherical mirror), as well as illumination of mirrors off axis, resulting in greater efficiency and reduction in size. We describe a "Half Offner" spectrometer, an even simpler version of the Offner spectrometer. We present an entirely novel design, the Spherical Transmission Grating Spectrometer (STGS), and discuss exemplary applications, including a design for a double-beam spectrometer without any requirement for a dichroic. This paradigm change in spectrometer design offers an alternative to all-refractive astronomical spectrometer designs, using expensive, fragile lens elements fabricated from CaF2 or even more exotic materials. The unobscured mirror layout avoids a major drawback of the previous generation of catadioptric spectrometer designs. We describe laboratory measurements of the efficiency and image quality of a curved VPH grating in a STGS design, demonstrating, simultaneously, efficiency comparable to planar VPH gratings along with good image quality. The stage is now set for construction of a prototype instrument with impressive performance.

Engineering and Characterizing Light-Matter Interactions in Photonic Crystals

DTIC Science & Technology

2010-01-01

photonic crystal effects would occur at wavelengths in the infrared spectrum. These effects would not be easily measured by our available...spectrometers which operate in the visible and near- infrared , at wavelengths shorter than 1.6 microns. Similarly, the majority of interesting luminescent...periodicity of the photonic crystal is defined by the high -throughput method while the low-throughput method performs the complementary task of adding a

Compact liquid crystal waveguide Fourier transform spectrometer for real-time gas sensing in NIR spectral band

NASA Astrophysics Data System (ADS)

Chao, Tien-Hsin; Lu, Thomas T.; Davis, Scott R.; Rommel, Scott D.; Farca, George; Luey, Ben; Martin, Alan; Anderson, Michael H.

2012-04-01

Jet Propulsion Lab and Vescent Photonics Inc. and are jointly developing an innovative ultra-compact (volume < 10 cm3), ultra-low power (<10 -3 Watt-hours per measurement and zero power consumption when not measuring), completely non-mechanical Liquid Crystal Waveguide Fourier Transform Spectrometer (LCWFTS) that will be suitable for a variety of remote-platform, in-situ measurements. These devices are made possible by novel electro-evanescent waveguide architecture, enabling "monolithic chip-scale" Electro Optic-FTS (EO-FTS) sensors. The potential performance of these EO-FTS sensors include: i) a spectral range throughout 0.4-5 μm (25000 - 2000 cm-1), ii) highresolution (Δλ<= 0.1 nm), iii) high-speed (< 1 ms) measurements, and iv) rugged integrated optical construction. This performance potential enables the detection and quantification of a large number of different atmospheric gases simultaneously in the same air mass and the rugged construction will enable deployment on previously inaccessible platforms. The sensor construction is also amenable for analyzing aqueous samples on remote floating or submerged platforms. We have reported [1] a proof-of-principle prototype LCWFTS sensor that has been demonstrated in the near- IR (range of 1450-1600 nm) with a 5 nm resolution. In this paper, we will report the recently built and tested LCWFTS test bed and the demonstration of a real-time gas sensing applications.

The High-energy Burst Spectrometer for SMESE Mission

NASA Astrophysics Data System (ADS)

Gu, Qiang; Chang, Jin

2009-01-01

The SMall Explorer for Solar Eruptions (SMESE) is a small satellite being developed jointly by China and France. It is planed to launch around the next solar maximum year (˜ 2011) for observing simultaneously the two most violent types of eruptive events on the sun (the coronal mass ejection (CME) and the solar flare) and investigating their relationship. As one of the 3 main payloads of the small satellite, the high energy burst spectrometer (HEBS) adopts the upto- date high-resolution LaBr3 scintillation detector to observe the high-energy solar radiation in the range 10 keV—600 MeV. Its energy resolution is better than 3.0% at 662 keV, 2-fold higher than that of current scintillation detectors, promising a breakthrough in the studies of energy release in solar flares and CMEs, particle acceleration and the relationship between solar flares and CMEs.

Carotid dual-energy CT angiography: Evaluation of low keV calculated monoenergetic datasets by means of a frequency-split approach for noise reduction at low keV levels.

PubMed

Riffel, Philipp; Haubenreisser, Holger; Meyer, Mathias; Sudarski, Sonja; Morelli, John N; Schmidt, Bernhard; Schoenberg, Stefan O; Henzler, Thomas

2016-04-01

Calculated monoenergetic ultra-low keV datasets did not lead to improved contrast-to-noise ratio (CNR) due to the dramatic increase in image noise. The aim of the present study was to evaluate the objective image quality of ultra-low keV monoenergetic images (MEIs) calculated from carotid DECT angiography data with a new monoenergetic imaging algorithm using a frequency-split technique. 20 patients (12 male; mean age 53±17 years) were retrospectively analyzed. MEIs from 40 to 120 keV were reconstructed using the monoenergetic split frequency approach (MFSA). Additionally MEIs were reconstructed for 40 and 50 keV using a conventional monoenergetic (CM) software application. Signal intensity, noise, signal-to-noise ratio (SNR) and CNR were assessed in the basilar, common, internal carotid arteries. Ultra-low keV MEIs at 40 keV and 50 keV demonstrated highest vessel attenuation, significantly greater than those of the polyenergetic images (PEI) (all p-values <0.05). The highest SNR level and CNR level was found at 40 keV and 50 keV (all p-values <0.05). MEIs with MFSA showed significantly lower noise levels than those processed with CM (all p-values <0.05) and no significant differences in vessel attenuation (p>0.05). Thus MEIs with MFSA showed significantly higher SNR and CNR compared to MEIs with CM. Combining the lower spatial frequency stack for contrast at low keV levels with the high spatial frequency stack for noise at high keV levels (frequency-split technique) leads to improved image quality of ultra-low keV monoenergetic DECT datasets when compared to previous monoenergetic reconstruction techniques without the frequency-split technique. Copyright © 2016 Elsevier Ireland Ltd. All rights reserved.

Continued development of thallium bromide and related compounds for gamma-ray spectrometers

NASA Astrophysics Data System (ADS)

Kim, H.; Churilov, A.; Ciampi, G.; Cirignano, L.; Higgins, W.; Kim, S.; O'Dougherty, P.; Olschner, F.; Shah, Kanai

2011-02-01

Thallium bromide (TlBr) and related ternary compounds, TlBrI and TlBrCl, have been under development for room temperature gamma-ray spectroscopy due to high density, high Z and wide bandgap of the material. Low melting point and cubic crystal structure of selected compositions of these compounds facilitate crystal growth by melt techniques. Recent advances in material purification, crystal growth, and device processing have led to mobility-lifetime products of electrons in the mid 10 -3 cm 2/V range enabling working detectors of greater than 15 mm thickness to be fabricated. In this paper we report on our recent progress on TlBr detector development and first results from TlBr xCl 1- x devices. Pulse height spectra will be presented from TlBr arrays as thick as 18 mm. Depth corrected spectra will also be presented. For a 5 mm thick TlBr array, energy resolution of less than 1% (FWHM at 662 keV) was obtained after depth correction.

Hard X-ray (greater than 10 keV) telescope for space astronomy from the Moon

NASA Astrophysics Data System (ADS)

Frontera, F.; de Chiara, P.; Pasqualini, G.

1994-06-01

The use of the Moon as site for deep observations of astrophysical sources in hard X-rays (greater than 10 keV) is very exciting, in spite of several technological problems to be solved. A strong limitation to the sensitivity of hard X-ray experiments is imposed by the use of direct-viewing (with or without masks) detectors. We propose a lunar hard X-ray observatory, (LHEXO), that makes use of a hard X-ray concentrator which is based on the use of confocal paraboloidal mirrors made of mosaic crystals of graphite (002). In this paper we describe telescope concept and its expected performances.

Correlation spectrometer

DOEpatents

Sinclair, Michael B [Albuquerque, NM; Pfeifer, Kent B [Los Lunas, NM; Flemming, Jeb H [Albuquerque, NM; Jones, Gary D [Tijeras, NM; Tigges, Chris P [Albuquerque, NM

2010-04-13

A correlation spectrometer can detect a large number of gaseous compounds, or chemical species, with a species-specific mask wheel. In this mode, the spectrometer is optimized for the direct measurement of individual target compounds. Additionally, the spectrometer can measure the transmission spectrum from a given sample of gas. In this mode, infrared light is passed through a gas sample and the infrared transmission signature of the gasses present is recorded and measured using Hadamard encoding techniques. The spectrometer can detect the transmission or emission spectra in any system where multiple species are present in a generally known volume.

CRYSTAL/FACE

NASA Technical Reports Server (NTRS)

Baumgardner, Darrel; Kok, Greg; Anderson, Bruce

2004-01-01

Droplet Measurement Technologies (DMT), under funding from NASA, participated in the CRYSTAL/FACE field campaign in July, 2002 with measurements of cirrus cloud hydrometeors in the size range from 0.5 to 1600 microns. The measurements were made with the DMT Cloud, Aerosol and Precipitation Spectrometer (CAPS) that was flown on NASA's WB57F. With the exception of the first research flight when the data system failed two hours into the mission, the measurement system performed almost flawlessly during the thirteen flights. The measurements from the CAPS have been essential for interpretation of cirrus cloud properties and their impact on climate. The CAPS data set has been used extensively by the CRYSTAL/FACE investigators and as of the date of this report, have been included in five published research articles, 10 conference presentations and six other journal articles currently in preparation.

Curved diamond-crystal spectrographs for x-ray free-electron laser noninvasive diagnostics.

PubMed

Terentyev, Sergey; Blank, Vladimir; Kolodziej, Tomasz; Shvyd'ko, Yuri

2016-12-01

We report on the manufacturing and X-ray tests of bent diamond-crystal X-ray spectrographs, designed for noninvasive diagnostics of the X-ray free-electron laser (XFEL) spectra in the spectral range from 5 to 15 keV. The key component is a curved, 20-μm thin, single crystalline diamond triangular plate in the (110) orientation. The radius of curvature can be varied between R = 0.6 m and R = 0.1 m in a controlled fashion, ensuring imaging in a spectral window of up to 60 eV for ≃8 keV X-rays. All of the components of the bending mechanism (about 10 parts) are manufactured from diamond, thus ensuring safe operations in intense XFEL beams. The spectrograph is transparent to 88% for 5-keV photons and to 98% for 15-keV photons. Therefore, it can be used for noninvasive diagnostics of the X-ray spectra during XFEL operations.

Curved diamond-crystal spectrographs for x-ray free-electron laser noninvasive diagnostics

DOE PAGES

Terentyev, Sergey; Blank, Vladimir; Kolodziej, Tomasz; ...

2016-12-29

Here, we report on the manufacturing and X-ray tests of bent diamond-crystal X-ray spectrographs, designed for noninvasive diagnostics of the X-ray free-electron laser (XFEL) spectra in the spectral range from 5 to 15 keV. The key component is a curved, 20-µm thin, single crystalline diamond triangular plate in the (110) orientation. The radius of curvature can be varied between R = 0.6 m and R = 0.1 m in a controlled fashion, ensuring imaging in a spectral window of up to 60 eV for ' 8 keV X-rays. All of the components of the bending mechanism (about 10 parts) aremore » manufactured from diamond, thus ensuring safe operations in intense XFEL beams. The spectrograph is transparent to 88% for 5-keV photons, and to 98% for 15-keV photons. Therefore, it can be used for noninvasive diagnostics of the X-ray spectra during XFEL operations.« less

Curved diamond-crystal spectrographs for x-ray free-electron laser noninvasive diagnostics

DOE Office of Scientific and Technical Information (OSTI.GOV)

Terentyev, Sergey; Blank, Vladimir; Kolodziej, Tomasz

Here, we report on the manufacturing and X-ray tests of bent diamond-crystal X-ray spectrographs, designed for noninvasive diagnostics of the X-ray free-electron laser (XFEL) spectra in the spectral range from 5 to 15 keV. The key component is a curved, 20-µm thin, single crystalline diamond triangular plate in the (110) orientation. The radius of curvature can be varied between R = 0.6 m and R = 0.1 m in a controlled fashion, ensuring imaging in a spectral window of up to 60 eV for ' 8 keV X-rays. All of the components of the bending mechanism (about 10 parts) aremore » manufactured from diamond, thus ensuring safe operations in intense XFEL beams. The spectrograph is transparent to 88% for 5-keV photons, and to 98% for 15-keV photons. Therefore, it can be used for noninvasive diagnostics of the X-ray spectra during XFEL operations.« less

Interfacing an aspiration ion mobility spectrometer to a triple quadrupole mass spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Adamov, Alexey; Viidanoja, Jyrki; Kaerpaenoja, Esko

2007-04-15

This article presents the combination of an aspiration-type ion mobility spectrometer with a mass spectrometer. The interface between the aspiration ion mobility spectrometer and the mass spectrometer was designed to allow for quick mounting of the aspiration ion mobility spectrometer onto a Sciex API-300 triple quadrupole mass spectrometer. The developed instrumentation is used for gathering fundamental information on aspiration ion mobility spectrometry. Performance of the instrument is demonstrated using 2,6-di-tert-butyl pyridine and dimethyl methylphosphonate.

Inelastic neutron scattering experiments with the monochromatic imaging mode of the RITA-II spectrometer

NASA Astrophysics Data System (ADS)

Bahl, C. R. H.; Lefmann, K.; Abrahamsen, A. B.; Rønnow, H. M.; Saxild, F.; Jensen, T. B. S.; Udby, L.; Andersen, N. H.; Christensen, N. B.; Jakobsen, H. S.; Larsen, T.; Häfliger, P. S.; Streule, S.; Niedermayer, Ch.

2006-05-01

Recently a monochromatic multiple data taking mode has been demonstrated for diffraction experiments using a RITA type cold neutron spectrometer with a multi-bladed analyser and a position-sensitive detector. Here, we show how this mode can be used in combination with a flexible radial collimator to perform real inelastic neutron scattering experiments. We present the results from inelastic powder, single crystal dispersion and single crystal constant energy mapping experiments. The advantages and complications of performing these experiments are discussed along with a comparison between the imaging mode and the traditional monochromatic focussing mode.

Temporal Gain Correction for X-Ray Calorimeter Spectrometers

NASA Technical Reports Server (NTRS)

Porter, F. S.; Chiao, M. P.; Eckart, M. E.; Fujimoto, R.; Ishisaki, Y.; Kelley, R. L.; Kilbourne, C. A.; Leutenegger, M. A.; McCammon, D.; Mitsuda, K.

2016-01-01

Calorimetric X-ray detectors are very sensitive to their environment. The boundary conditions can have a profound effect on the gain including heat sink temperature, the local radiation temperature, bias, and the temperature of the readout electronics. Any variation in the boundary conditions can cause temporal variations in the gain of the detector and compromise both the energy scale and the resolving power of the spectrometer. Most production X-ray calorimeter spectrometers, both on the ground and in space, have some means of tracking the gain as a function of time, often using a calibration spectral line. For small gain changes, a linear stretch correction is often sufficient. However, the detectors are intrinsically non-linear and often the event analysis, i.e., shaping, optimal filters etc., add additional non-linearity. Thus for large gain variations or when the best possible precision is required, a linear stretch correction is not sufficient. Here, we discuss a new correction technique based on non-linear interpolation of the energy-scale functions. Using Astro-HSXS calibration data, we demonstrate that the correction can recover the X-ray energy to better than 1 part in 104 over the entire spectral band to above 12 keV even for large-scale gain variations. This method will be used to correct any temporal drift of the on-orbit per-pixel gain using on-board calibration sources for the SXS instrument on the Astro-H observatory.

Rest-wavelength fiducials for the ITER core imaging x-ray spectrometer.

PubMed

Beiersdorfer, P; Brown, G V; Graf, A T; Bitter, M; Hill, K W; Kelley, R L; Kilbourne, C A; Leutenegger, M A; Porter, F S

2012-10-01

Absolute wavelength references are needed to derive the plasma velocities from the Doppler shift of a given line emitted by a moving plasma. We show that such reference standards exist for the strongest x-ray line in neonlike W(64+), which has become the line of choice for the ITER (Latin "the way") core imaging x-ray spectrometer. Close-by standards are the Hf Lβ(3) line and the Ir Lα(2) line, which bracket the W(64+) line by ±30 eV; other standards are given by the Ir Lα(1) and Lα(2) lines and the Hf Lβ(1) and Lβ(2) lines, which bracket the W(64+) line by ±40 and ±160 eV, respectively. The reference standards can be produced by an x-ray tube built into the ITER spectrometer. We present spectra of the reference lines obtained with an x-ray microcalorimeter and compare them to spectra of the W(64+) line obtained both with an x-ray microcalorimeter and a crystal spectrometer.

Rest-wavelength Fiducials for the ITER Core Imaging X-ray Spectrometer

NASA Technical Reports Server (NTRS)

Beiersdorfer, P.; Brown, G. V.; Graf, A. T.; Bitter, M.; Hill, K. W.; Kelley, R. L.; Kilbourne, C. A.; Leutenegger, M. A.; Porter, F. S.

2012-01-01

Absolute wavelength references are needed to derive the plasma velocities from the Doppler shift of a given line emitted by a moving plasma. We show that such reference standards exist for the strongest x-ray line in neonlike W64+, which has become the line of choice for the ITER (Latin the way) core imaging x-ray spectrometer. Close-by standards are the Hf L3 line and the Ir L2 line, which bracket the W64+ line by 30 eV; other standards are given by the Ir L1 and L2 lines and the Hf L1 and L2 lines, which bracket the W64+ line by 40 and 160 eV, respectively. The reference standards can be produced by an x-ray tube built into the ITER spectrometer. We present spectra of the reference lines obtained with an x-ray microcalorimeter and compare them to spectra of the W64+ line obtained both with an x-ray microcalorimeter and a crystal spectrometer

Single crystal Ce doped scintillator material with garnet structure sensitive to gamma ray and neutron radiation

NASA Astrophysics Data System (ADS)

Solodovnikov, D.; Weber, M. H.; Haven, D. T.; Lynn, K. G.

2012-08-01

A mixed garnet scintillator host material is obtained from the melt—Yttrium Gadolinium Gallium Aluminum Garnet (YGGAG). In addition to the high thermal and chemical stability and radiation hardness found in garnet crystals, it offers sensitivity to neutrons due to the presence of Gd atoms, has lower melting temperature than yttrium aluminum garnet, and similar crystallization behavior suitable for growth of large volume crystals. Crystals of YGGAG doped with Ce of 10×10×10 mm3 have already demonstrated energy resolution of 10% at 662 keV.

Slowing down of 100 keV antiprotons in Al foils

NASA Astrophysics Data System (ADS)

Nordlund, K.

2018-03-01

Using energy degrading foils to slow down antiprotons is of interest for producing antihydrogen atoms. I consider here the slowing down of 100 keV antiprotons, that will be produced in the ELENA storage ring under construction at CERN, to energies below 10 keV. At these low energies, they are suitable for efficient antihydrogen production. I simulate the antihydrogen motion and slowing down in Al foils using a recently developed molecular dynamics approach. The results show that the optimal Al foil thickness for slowing down the antiprotons to below 5 keV is 910 nm, and to below 10 keV is 840 nm. Also the lateral spreading of the transmitted antiprotons is reported and the uncertainties discussed.

A Thomson-type mass and energy spectrometer for characterizing ion energy distributions in a coaxial plasma gun operating in a gas-puff mode

NASA Astrophysics Data System (ADS)

Rieker, G. B.; Poehlmann, F. R.; Cappelli, M. A.

2013-07-01

Measurements of ion energy distribution are performed in the accelerated plasma of a coaxial electromagnetic plasma gun operating in a gas-puff mode at relatively low discharge energy (900 J) and discharge potential (4 kV). The measurements are made using a Thomson-type mass and energy spectrometer with a gated microchannel plate and phosphor screen as the ion sensor. The parabolic ion trajectories are captured from the sensor screen with an intensified charge-coupled detector camera. The spectrometer was designed and calibrated using the Geant4 toolkit, accounting for the effects on the ion trajectories of spatial non-uniformities in the spectrometer magnetic and electric fields. Results for hydrogen gas puffs indicate the existence of a class of accelerated protons with energies well above the coaxial discharge potential (up to 24 keV). The Thomson analyzer confirms the presence of impurities of copper and iron, also of relatively high energies, which are likely erosion or sputter products from plasma-electrode interactions.

Development of a Gamma-Ray Spectrometer for Korean Pathfinder Lunar Orbiter

NASA Astrophysics Data System (ADS)

Kim, Kyeong Ja; Park, Junghun; Choi, Yire; Lee, Sungsoon; Yeon, Youngkwang; Yi, Eung Seok; Jeong, Meeyoung; Sun, Changwan; van Gasselt, Stephan; Lee, K. B.; Kim, Yongkwon; Min, Kyungwook; Kang, Kyungin; Cho, Jinyeon; Park, Kookjin; Hasebe, Nobuyuki; Elphic, Richard; Englert, Peter; Gasnault, Olivier; Lim, Lucy; Shibamura, Eido; GRS Team

2016-10-01

Korea is preparing for a lunar orbiter mission (KPLO) to be developed in no later than 2018. Onboard the spacecraft is a gamma ray spectrometer (KLGRS) allowing to collect low energy gamma-ray signals in order to detect elements by either X-ray fluorescence or by natural radioactive decay in the low as well as higher energy regions of up to 10 MeV. Scientific objectives include lunar resources (water and volatile measurements, rare earth elements and precious metals, energy resources, major elemental distributions for prospective in-situ utilizations), investigation of the lunar geology and studies of the lunar environment (mapping of the global radiation environment from keV to 10 MeV, high energy cosmic ray flux using the plastic scintillator).The Gamma-Ray Spectrometer (GRS) system is a compact low-weight instrument for the chemical analysis of lunar surface materials within a gamma-ray energy range from 10s keV to 10 MeV. The main LaBr3 detector is surrounded by an anti-coincidence counting module of BGO/PS scintillators to reduce both low gamma-ray background from the spacecraft and housing materials and high energy gamma-ray background from cosmic rays. The GRS system will determine the elemental compositions of the near surface of the Moon.The GRS system is a recently developed gamma-ray scintillation based detector which can be used as a replacement for the HPGe GRS sensor with the advantage of being able to operate at a wide range of temperatures with remarkable energy resolution. LaBr3 also has a high photoelectron yield, fast scintillation response, good linearity and thermal stability. With these major advantages, the LaBr3 GRS system will allow us to investigate scientific objectives and assess important research questions on lunar geology and resource exploration.The GRS investigation will help to assess open questions related to the spatial distribution and origin of the elements on the lunar surface and will contribute to unravel geological surface

The JET neutron time-of-flight spectrometer

NASA Astrophysics Data System (ADS)

Elevant, T.; Aronsson, D.; van Belle, P.; Grosshoeg, G.; Hoek, M.; Olsson, M.; Sadler, G.

1991-08-01

An instrument for measuring neutron energy spectra over the interval 1 to 20 MeV has been developed and tested. It is based on time-of-flight measurements in between correlated events in two spatially separated sets of plastic scintillators. This instrument has been installed at the Joint European Tours (JET). We describe here the required operating conditions, performance tests and results of three years of operation during which neutron energy spectra in the 2-3 MeV range from D(d, n) 3He reactions in JET were studied. Some technical details are given and the results from Monte Carlo and analytical model calculations of the spectrometer energy resolution and response function are presented. The efficiency of the system is ≈ 1 × 10 -2 cm 2 counted at the position of the first detector. Together with the geometry conditions at JET this yields 6 × 10 2 counts per 10 15 neutrons emitted. The energy resolution is in the interval from 125 to 133 keV (FWHM) depending on conditions and is known to an accuracy of ±5 keV. Correction for the inevitable random background is dealt with in detail and a reduction procedure valid for fast variations in neutron count-rates is provided. Plasma ion temperatures deduced from the neutron spectra agree within statistical limits with the results from other diagnostic techniques in use at JET. Stable behaviour up to useful count-rates of 3 × 10 3 counts/s have been obtained, making possible the study of neutron spectra on the short time-scales typical of fusion plasmas.

Bridgman-Stockbarger growth of SrI2:Eu2+ single crystal

NASA Astrophysics Data System (ADS)

Raja, A.; Daniel, D. Joseph; Ramasamy, P.; Singh, S. G.; Sen, S.; Gadkari, S. C.

2018-05-01

Strontium Iodide (SrI2): Europium Iodide (EuI2) was purified by Zone-refinement process. Europium doped strontium iodide (SrI2:Eu2+) single crystal was grown by modified vertical Bridgman - Stockbarger technique. Photoluminescence (PL) excitation and emission (PLE) spectra were measured for Eu2+ doped SrI2 crystal. The sharp emission was recorded at 432 nm. Scintillation properties of the SrI2:Eu2+ crystal were checked by the gamma ray spectrometer using 137Cs gamma source.

Retraction: Using the Medipix3 detector for direct electron imaging in the range 60 keV to 200 keV in electron microscopy Retraction: Using the Medipix3 detector for direct electron imaging in the range 60 keV to 200 keV in electron microscopy

NASA Astrophysics Data System (ADS)

Mir, J. A.; Plackett, R.; Shipsey, I.; dos Santos, J. M. F.

2018-01-01

The paper "Using the Medipix3 detector for direct electron imaging in the range 60keV to 200keV in electron microscopy" by J.A. Mir, R. Plackett, I. Shipsey and J.M.F. dos Santos has been retracted following the authors' request on the basis of the existence of a disagreement about the ownership of the data, to prevent conflict between collaborators.

Chemical state analysis of Cl Kα and Kβ1,3 X-ray emission lines using polychromatic WDXRF spectrometer

NASA Astrophysics Data System (ADS)

Kainth, Harpreet Singh; Upmanyu, Arun; Sharma, Hitesh; Singh, Tejbir; Kumar, Sanjeev

2018-02-01

With the support of research projects focusing on sampling and data analysing of different varieties of chemical compounds, wavelength dispersive X-ray fluorescence (WDXRF) technique is commonly used in many research laboratories throughout the world wide to determine the elemental composition of various unknown samples. In the present study, first time we have employed polychromatic S8 TIGER WDXRF spectrometer to study the chemical state analysis in Cl Kα and Kβ1,3 X-ray emission lines. A Voigt function is used to determine the central peak position of the K shell emission lines in all samples. From the present measurements, it is seen that both positive and negative shifts have been observed in Cl Kα (2.622 keV) and Kβ1,3 (2.817 keV) emission peaks. It has been also seen that the effective charge, relative line-width and relative intensity ratio I(Kβ1,3/Kα) are found proportional with the chemical shift. Furthermore, a parabolic relation is also established between them.

Compton spectroscopy in the diagnostic x-ray energy range. I. Spectrometer design.

PubMed

Matscheko, G; Carlsson, G A

1989-02-01

The optimal design of a Compton spectrometer for measuring photon energy spectra from x-ray tubes in a clinical laboratory is analysed. The demands are: (i) coherent and multiple scattering distort the measurements and must be avoided; (ii) the measuring time should be as short as possible to avoid unnecessary wear on the x-ray tube; and (iii) the impairment in energy resolution due to the scattering geometry should be kept minimal. A scattering angle of 90 degrees is advocated. Scatterers (of low-atomic-number material) in the shape of long circular rods (0.5-4 mm diameter, 20-40 mm long) are preferable to scattering foils. Use of a short focus-scatterer distance (approximately 200 mm) is to be preferred compared to using a large detector area (greater than or equal to 4 mm diameter) in order to establish a sufficiently high count rate in the detector. Short focal distances and a 90 degrees scattering angle are advantages in measuring energy spectra in the gantry of CT machines where the available space is limited. To limit the geometrical energy broadening to less than 1 keV, the spread in scattering angles of registered photons must not exceed 1-2 degrees for incident photon energies of 100-150 keV.

Monolithic spectrometer

DOEpatents

Rajic, Slobodan; Egert, Charles M.; Kahl, William K.; Snyder, Jr., William B.; Evans, III, Boyd M.; Marlar, Troy A.; Cunningham, Joseph P.

1998-01-01

A monolithic spectrometer is disclosed for use in spectroscopy. The spectrometer is a single body of translucent material with positioned surfaces for the transmission, reflection and spectral analysis of light rays.

Simulation of background from low-level tritium and radon emanation in the KATRIN spectrometers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Leiber, B.; Collaboration: KATRIN Collaboration

The KArlsruhe TRItium Neutrino (KATRIN) experiment is a large-scale experiment for the model independent determination of the mass of electron anti-neutrinos with a sensitivity of 200 meV/c{sup 2}. It investigates the kinematics of electrons from tritium beta decay close to the endpoint of the energy spectrum at 18.6 keV. To achieve a good signal to background ratio at the endpoint, a low background rate below 10{sup −2} counts per second is required. The KATRIN setup thus consists of a high luminosity windowless gaseous tritium source (WGTS), a magnetic electron transport system with differential and cryogenic pumping for tritium retention, andmore » electro-static retarding spectrometers (pre-spectrometer and main spectrometer) for energy analysis, followed by a segmented detector system for counting transmitted beta-electrons. A major source of background comes from magnetically trapped electrons in the main spectrometer (vacuum vessel: 1240 m{sup 3}, 10{sup −11} mbar) produced by nuclear decays in the magnetic flux tube of the spectrometer. Major contributions are expected from short-lived radon isotopes and tritium. Primary electrons, originating from these decays, can be trapped for hours, until having lost almost all their energy through inelastic scattering on residual gas particles. Depending on the initial energy of the primary electron, up to hundreds of low energetic secondary electrons can be produced. Leaving the spectrometer, these electrons will contribute to the background rate. This contribution describes results from simulations for the various background sources. Decays of {sup 219}Rn, emanating from the main vacuum pump, and tritium from the WGTS that reaches the spectrometers are expected to account for most of the background. As a result of the radon alpha decay, electrons are emitted through various processes, such as shake-off, internal conversion and the Auger deexcitations. The corresponding simulations were done using the

Compact, maintainable 80-KeV neutral beam module

DOEpatents

Fink, Joel H.; Molvik, Arthur W.

1980-01-01

A compact, maintainable 80-keV arc chamber, extractor module for a neutral beam system immersed in a vacuum of <10.sup.-2 Torr, incorporating a nested 60-keV gradient shield located midway between the high voltage ion source and surrounding grounded frame. The shield reduces breakdown or arcing path length without increasing the voltage gradient, tends to keep electric fields normal to conducting surfaces rather than skewed and reduces the peak electric field around irregularities on the 80-keV electrodes. The arc chamber or ion source is mounted separately from the extractor or ion accelerator to reduce misalignment of the accelerator and to permit separate maintenance to be performed on these systems. The separate mounting of the ion source provides for maintaining same without removing the ion accelerator.

Slow light enhanced gas sensing in photonic crystals

NASA Astrophysics Data System (ADS)

Kraeh, Christian; Martinez-Hurtado, J. L.; Popescu, Alexandru; Hedler, Harry; Finley, Jonathan J.

2018-02-01

Infrared spectroscopy allows for highly selective and highly sensitive detection of gas species and concentrations. Conventional gas spectrometers are generally large and unsuitable for on-chip applications. Long absorption path lengths are usually required and impose a challenge for miniaturization. In this work, a gas spectrometer is developed consisting of a microtube photonic crystal structure. This structure of millimetric form factors minimizes the required absorption path length due to slow light effects. The microtube photonic crystal allows for strong transmission in the mid-infrared and, due to its large void space fraction, a strong interaction between light and gas molecules. As a result, enhanced absorption of light increases the gas sensitivity of the device. Slow light enhanced gas absorption by a factor of 5.8 in is experimentally demonstrated at 5400 nm. We anticipate small form factor gas sensors on silicon to be a starting point for on-chip gas sensing architectures.

Cross sections for ionization of tetrahydrofuran by protons at energies between 300 and 3000 keV

NASA Astrophysics Data System (ADS)

Wang, Mingjie; Rudek, Benedikt; Bennett, Daniel; de Vera, Pablo; Bug, Marion; Buhr, Ticia; Baek, Woon Yong; Hilgers, Gerhard; Rabus, Hans

2016-05-01

Double-differential cross sections for ionization of tetrahydrofuran by protons with energies from 300 to 3000 keV were measured at the Physikalisch-Technische Bundesanstalt ion accelerator facility. The electrons emitted at angles between 15∘ and 150∘ relative to the ion-beam direction were detected with an electrostatic hemispherical electron spectrometer. Single-differential and total ionization cross sections have been derived by integration. The experimental results are compared to the semiempirical Hansen-Kocbach-Stolterfoht model as well as to the recently reported method based on the dielectric formalism. The comparison to the latter showed good agreement with experimental data in a broad range of emission angles and energies of secondary electrons. The scaling property of ionization cross sections for tetrahydrofuran was also investigated. Compared to molecules of different size, the ionization cross sections of tetrahydrofuran were found to scale with the number of valence electrons at large impact parameters.

Tropospheric Emission Spectrometer and Airborne Emission Spectrometer

NASA Technical Reports Server (NTRS)

Glavich, T.; Beer, R.

1996-01-01

The Tropospheric Emission Spectrometer (TES) is an instrument being developed for the NASA Earth Observing System Chemistry Platform. TES will measure the distribution of ozone and its precursors in the lower atmosphere. The Airborne Emission Spectrometer (AES) is an aircraft precursor to TES. Applicable descriptions are given of instrument design, technology challenges, implementation and operations for both.

Facilities and Techniques for X-Ray Diagnostic Calibration in the 100-eV to 100-keV Energy Range

NASA Astrophysics Data System (ADS)

Gaines, J. L.; Wittmayer, F. J.

1986-08-01

The Lawrence Livermore National Laboratory (LLNL) has been a pioneer in the field of x-ray diagnostic calibration for more than 20 years. We have built steady state x-ray sources capable of supplying fluorescent lines of high spectral purity in the 100-eV to 100-keV energy range, and these sources have been used in the calibration of x-ray detectors, mirrors, crystals, filters, and film. This paper discusses our calibration philosophy and techniques, and describes some of our x-ray sources. Examples of actual calibration data are presented as well.

Monolithic spectrometer

DOEpatents

Rajic, S.; Egert, C.M.; Kahl, W.K.; Snyder, W.B. Jr.; Evans, B.M. III; Marlar, T.A.; Cunningham, J.P.

1998-05-19

A monolithic spectrometer is disclosed for use in spectroscopy. The spectrometer is a single body of translucent material with positioned surfaces for the transmission, reflection and spectral analysis of light rays. 6 figs.

Performance of the helium dewar and the cryocoolers of the Hitomi soft x-ray spectrometer

NASA Astrophysics Data System (ADS)

Fujimoto, Ryuichi; Takei, Yoh; Mitsuda, Kazuhisa; Yamasaki, Noriko Y.; Tsujimoto, Masahiro; Koyama, Shu; Ishikawa, Kumi; Sugita, Hiroyuki; Sato, Yoichi; Shinozaki, Keisuke; Okamoto, Atsushi; Kitamoto, Shunji; Hoshino, Akio; Sato, Kosuke; Ezoe, Yuichiro; Ishisaki, Yoshitaka; Yamada, Shinya; Seta, Hiromi; Ohashi, Takaya; Tamagawa, Toru; Noda, Hirofumi; Sawada, Makoto; Tashiro, Makoto; Yatsu, Yoichi; Mitsuishi, Ikuyuki; Kanao, Kenichi; Yoshida, Seiji; Miyaoka, Mikio; Tsunematsu, Shoji; Otsuka, Kiyomi; Narasaki, Katsuhiro; DiPirro, Michael J.; Shirron, Peter J.; Sneiderman, Gary A.; Kilbourne, Caroline A.; Porter, Frederick Scott; Chiao, Meng P.; Eckart, Megan E.

2018-01-01

The soft x-ray spectrometer (SXS) was a cryogenic high-resolution x-ray spectrometer onboard the Hitomi (ASTRO-H) satellite that achieved energy resolution of 5 eV at 6 keV, by operating the detector array at 50 mK using an adiabatic demagnetization refrigerator (ADR). The cooling chain from room temperature to the ADR heat sink was composed of two-stage Stirling cryocoolers, a He4 Joule-Thomson cryocooler, and superfluid liquid helium and was installed in a dewar. It was designed to achieve a helium lifetime of more than 3 years with a minimum of 30 L. The satellite was launched on February 17, 2016, and the SXS worked perfectly in orbit, until March 26 when the satellite lost its function. It was demonstrated that the heat load on the helium tank was about 0.7 mW, which would have satisfied the lifetime requirement. This paper describes the design, results of ground performance tests, prelaunch operations, and initial operation and performance in orbit of the flight dewar and the cryocoolers.

Dipeptide Formation from Amino Acid Monomer Induced by keV Ion Irradiation: An Implication for Physicochemical Repair by Radiation Itself

NASA Astrophysics Data System (ADS)

Wang, Wei; Yuan, Hang; Wang, Xiangqin; Yu, Zengliang

2008-02-01

An identification of Phe dipeptide from L-phenylalanine monomers after keV nitrogen and argon ion implantation, by using the HPLC (high performance liquid chromatography) and LC-MS(liquid chromatography mass spectrometer) methods is reported. The results showed a similar yield behavior for both ion species, namely: 1) the yield of dipeptides under alkalescent conditions was distinctly higher than that under acidic or neutral conditions; 2) for different ion species, the dose-yield curves tracked a similar trend which was called a counter-saddle curve. The dipeptide formation may implicate a recombination repair mechanism of damaged biomolecules that energetic ions have left in their wake. Accordingly a physicochemical self-repair mechanism by radiation itself for the ion-beam radiobiological effects is proposed.

Metrology for terahertz time-domain spectrometers

NASA Astrophysics Data System (ADS)

Molloy, John F.; Naftaly, Mira

2015-12-01

In recent years the terahertz time-domain spectrometer (THz TDS) [1] has emerged as a key measurement device for spectroscopic investigations in the frequency range of 0.1-5 THz. To date, almost every type of material has been studied using THz TDS, including semiconductors, ceramics, polymers, metal films, liquid crystals, glasses, pharmaceuticals, DNA molecules, proteins, gases, composites, foams, oils, and many others. Measurements with a TDS are made in the time domain; conversion from the time domain data to a frequency spectrum is achieved by applying the Fourier Transform, calculated numerically using the Fast Fourier Transform (FFT) algorithm. As in many other types of spectrometer, THz TDS requires that the sample data be referenced to similarly acquired data with no sample present. Unlike frequency-domain spectrometers which detect light intensity and measure absorption spectra, a TDS records both amplitude and phase information, and therefore yields both the absorption coefficient and the refractive index of the sample material. The analysis of the data from THz TDS relies on the assumptions that: a) the frequency scale is accurate; b) the measurement of THz field amplitude is linear; and c) that the presence of the sample does not affect the performance characteristics of the instrument. The frequency scale of a THz TDS is derived from the displacement of the delay line; via FFT, positioning errors may give rise to frequency errors that are difficult to quantify. The measurement of the field amplitude in a THz TDS is required to be linear with a dynamic range of the order of 10 000. And attention must be given to the sample positioning and handling in order to avoid sample-related errors.

Neutron capture cross sections of 69Ga and 71Ga at 25 keV and Epeak = 90 keV

NASA Astrophysics Data System (ADS)

Göbel, Kathrin; Beinrucker, Clemens; Erbacher, Philipp; Fiebiger, Stefan; Fonseca, Micaela; Heftrich, Michael; Heftrich, Tanja; Käppeler, Franz; Krása, Antonin; Lederer-Woods, Claudia; Plag, Ralf; Plompen, Arjan; Reifarth, René; Schmidt, Stefan; Sonnabend, Kerstin; Weigand, Mario

2017-09-01

We measured the neutron capture cross sections of 69Ga and 71Ga for a quasi-stellar spectrum at kBT = 25 keV and a spectrum with a peak energy at 90 keV by the activation technique at the Joint Research Centre (JRC) in Geel, Belgium. Protons were provided by an electrostatic Van de Graaff accelerator to produce neutrons via the reaction 7Li(p,n). The produced activity was measured via the γ emission of the product nuclei by high-purity germanium detectors. We present preliminary results.

Using neutrons to measure keV temperatures in highly compressed plastic at multi-Gbar pressures

NASA Astrophysics Data System (ADS)

Nilsen, J.; Bachmann, B.; Zimmerman, G. B.; Hatarik, R.; Döppner, T.; Swift, D.; Hawreliak, J.; Collins, G. W.; Falcone, R. W.; Glenzer, S. H.; Kraus, D.; Landen, O. L.; Kritcher, A. L.

2016-12-01

We have designed an experiment for the National Ignition Facility to measure the Hugoniot of materials such as plastic at extreme pressures. The design employs a strong spherically converging shock launched through a solid ball of material using a hohlraum radiation drive. The shock front conditions can be characterized using X-ray radiography until background from shock coalescence overtakes the backlit signal. Shock coalescence at the center is predicted to reach tens of Gbars and can be further characterized by measuring the X-ray self-emission and 2.45 MeV neutrons emitted from the shock flash region. In this simulation design work the standard plastic sphere is replaced with a deuterated polyethylene sphere, CD2, that reaches sufficiently high densities and temperatures in the central hot spot to produce neutrons from Deuterium-Deuterium (DD) fusion reactions that can be measured by a neutron time of flight spectrometer (nTOF) and act as a temperature diagnostic. This paper focuses on the design of these experiments, based on an extensive suite of radiation-hydrodynamics simulations, and the interpretation of the predicted DD neutron signals. The simulations predict mean temperatures of 1 keV in the central hot spot with mean densities of 33 g/cc and mean pressures of 25 Gbar. A preliminary comparison with early experimental results looks promising with an average ion temperature of 1.06 ± 0.15 keV in the central hot spot estimated from the nTOF spectral width and measured neutron yield of 7.0 (±0.5) × 109 DD neutrons.

Crystal Growth and Scintillation Properties of Ce Doped Gd3Ga,Al5O12 Single Crystals

NASA Astrophysics Data System (ADS)

Kamada, Kei; Yanagida, Takayuki; Pejchal, Jan; Nikl, Martin; Endo, Takanori; Tsutsumi, Kousuke; Fujimoto, Yutaka; Fukabori, Akihiro; Yoshikawa, Akira

2012-10-01

Ce1%, 2% and 3% doped Gd3(Ga,Al)5O12 (GAGG) single crystals were grown by the Cz method. Luminescence and scintillation properties were measured. Light yield change along the growth direction and effects of Ce concentration on scintillation properties in Ce:GAGG were studied. Ce3+ 5d-4f emission within 520-530 nm was observed in the Ce:GAGG crystals. The Ce1%:GAGG sample with 3×3×1 mm size showed the highest light yield of 46000 photon/MeV. The energy resolution was 7.8%@662 keV. With increasing solidification fraction, the LY were decreased. It is proposed that the increase of Ga concentration along the growth direction is the main cause of the decrease of LY. The scintillation decay times were accelerated with increasing Ce concentration in the Ce:GAGG crystals. The scintillation decay times were 92.0 ns, 79.1 ns and 68.3 ns in the Ce1, 2 and 3% GAGG, respectively.

Effects of increasing size and changing europium activator concentration in KCaI3 scintillator crystals

NASA Astrophysics Data System (ADS)

Lindsey, Adam C.; Zhuravleva, Mariya; Wu, Yuntao; Stand, Luis; Loyd, Matthew; Gokhale, Sasmit; Koschan, Merry; Melcher, Charles L.

2016-09-01

KCaI3:Eu crystals have been identified as very promising for use in spectroscopic detector applications related to nuclear nonproliferation and domestic security efforts. Initial studies have shown for small crystals a few mm3 in size with 3% europium dopant concentration, a high light yield of >70,000 ph/MeV and energy resolution of ≈3% at 662 keV is attainable which is comparable with the highest performance scintillators discovered. In this work, single crystals of KCaI3 with a range of Eu2+ doping between 0 and 5 at% substituting for Ca2+ were grown at 22 mm diameter and their performance for gamma-ray spectroscopy studied. Comparisons among crystals approximately Ø22 mm×22 mm (8.4 cm3 or ≈0.5 in3) provide a more accurate understanding of how scintillation performance changes with Eu doping and increased crystal size. KCaI3 in the undoped form is shown to be a highly efficient intrinsic scintillator with a defect-related emission at 404 nm which coexists with the Eu2+ 5d-4f emission in low dopant concentrations and is completely re-absorbed in more heavily doped crystals. For larger crystals, effects from self-absorption due to Eu activation become more evident by a near doubling of decay time for 0.5 in3 crystals as the activator is increased from 0.5 to 5.0 at% Eu. Comparisons of pulse-height spectra obtained for Ø22 mm×22 mm cylinders with varying Eu concentration suggests best performance is achieved using lower Eu additions closer to 0.5-1.0 at%. Using a modified crystal packaging featuring an offset reflector geometry, 0.5 in3 crystals of KCaI3:Eu can attain under 4% energy resolution at 662 keV.

Estimating the flux of the 14.4 keV solar axions

NASA Astrophysics Data System (ADS)

Avignone, F. T., III; Creswick, R. J.; Vergados, J. D.; Pirinen, P.; Srivastava, P. C.; Suhonen, J.

2018-01-01

In this paper we present a calculation of the expected flux of the mono-energetic 14.4 keV solar axions emitted by the M1 type nuclear transition of 57Fe in the Sun. These axions can be detected, e.g., by inverse coherent Bragg-Primakoff conversion in single-crystal TeO2 bolometers. The ingredients of this calculation are i) the axion nucleon coupling, estimated in several popular axion models and ii)the nuclear spin matrix elements involving realistic shell model calculations with both proton and neutron excitations. For the benefit of the experiments we have also calculated the branching ratio involving axion and photon emission. We find the solar axion flux on Earth to be Φa = 0.703×109cm-2s-1 (107 GeV/fa)2 and the branching ratio of axion to photon for the same model to be: wa/wγ = 0.229×10-15 ≈ 2×10-16.

The X-ray Spectrometer - A cryogenic instrument on the Advanced X-ray Astrophysics Facility

NASA Technical Reports Server (NTRS)

Breon, Susan R.; Hopkins, Richard A.; Nieczkoski, Stephen J.

1991-01-01

The X-ray Spectrometer (XRS) is an instrument on the Advanced X-ray Astrophysics Facility (AXAF), the third of NASA's Great Observatories scheduled for launch in 1998. The XRS detectors have a resolution of approximately 10 eV over the range 0.3 - 10 keV. To achieve this resolution, the detectors are maintained at or below 0.1 Kelvin using an adiabatic demagnetization refrigerator inside a superfluid helium dewar. In addition, split-Stirling-cycle mechanical coolers are used to extend the anticipated on-orbit helium lifetime to a minimum of 4 years. This paper describes the challenges of developing this hybrid cryogenic system and presents an overview of the current design of the system.

A view inside the nature of protein crystals

NASA Astrophysics Data System (ADS)

Oswald, R.; Pietzsch, M.; Ulrich, J.

2017-07-01

In this work a fundamental analysis of protein crystal modifications was presented to compare and confirm the components of protein crystal modifications. The result is that a protein crystal contains besides the protein, the precipitant and water. A mass spectrometer coupled to a thermogravimetry device was used to confirm the different waters (free water -the chosen buffer- and bound water) inside the crystals. Here the biggest amount of water is the free water (the buffer) with an amount of approximately 35%. The bound water (in the sense of a hydrate) has only an amount of about 1-1.5%. Furthermore, an x-ray analysis to confirm the influence range of pH value on the stability of one crystal modification for the understanding of effects on dissolution mechanism of protein crystals was investigated. The crystals of the tetragonal modification crystallized at pH 4.7, 4.85, 5.0, 5.15 and 5.3 maintain according to the x-ray measurements the same lattice parameters. The measured data are discussed.

Maskless nano-implant of 20 keV Ga+ in bulk Si(1 0 0) substrates

NASA Astrophysics Data System (ADS)

Milazzo, R. G.; D'Arrigo, G.; Mio, A. M.; Rimini, E.; Spinella, C.; Peto, L.; Nadzeyka, A.; Bauerdick, S.

2014-12-01

Multidirectional SPEG (Solid Phase Epitaxial Growth) of silicon has been investigated in micro and nanoamorphous structures generated on a crystalline substrate by a nano-sized ion beam, Gaussian shaped and with a standard deviation of about 5 nm. The 20 keV Ga+ ions were implanted at a fluence of 5 × 1014 ions cm-2 in a bulk Si(1 0 0) single crystal. Two structures were used for the implants: circular regions of 100 nm and 1 μm diameters respectively and straight lines 10 nm in width and few microns in length along (1 0 0) or (1 1 0) directions. The lateral spread of ions has been taken into account in the damage estimation. Transmission Electron Microscopy indicates that the structures are made of an amorphous core surrounded by a defective and filamentary shell. The recovery of the damaged outer regions promptly occurs during the early stages of the thermal treatment at 500-600 °C for all the structures. By prolonging annealing time, re-crystallization of the amorphous cores is achieved too by the movement of the underneath crystal-amorphous interface. The re-growth is almost defects free when the contribution of the crystalline seed below the structures is present, defective and twin mediated if it misses as in the thinnest regions of the specimen.

The Magnetic Recoil Spectrometer for time-resolved neutron measurements (MRSt) at the NIF

NASA Astrophysics Data System (ADS)

Parker, C. E.; Frenje, J. A.; Wink, C. W.; Gatu Johnson, M.; Lahmann, B.; Li, C. K.; Seguin, F. H.; Petrasso, R. D.; Hilsabeck, T. J.; Kilkenny, J. D.; Bionta, R.; Casey, D. T.; Khater, H. Y.; Forrest, C. J.; Glebov, V. Yu.; Sorce, C.; Hares, J. D.; Siegmund, O. H. W.

2017-10-01

The next-generation Magnetic Recoil Spectrometer, called MRSt, will provide time-resolved measurements of the DT-neutron spectrum. These measurements will provide critical information about the time evolution of the fuel assembly, hot-spot formation, and nuclear burn in Inertial Confinement Fusion (ICF) implosions at the National Ignition Facility (NIF). The neutron spectrum in the energy range 12-16 MeV will be measured with high accuracy ( 5%), unprecedented energy resolution ( 100 keV) and, for the first time ever, time resolution ( 20 ps). An overview of the physics motivation, conceptual design for meeting these performance requirements, and the status of the offline tests for critical components will be presented. This work was supported in part by the U.S. DOE, LLNL, and LLE.

Multidimensional spectrometer

DOEpatents

Zanni, Martin Thomas; Damrauer, Niels H.

2010-07-20

A multidimensional spectrometer for the infrared, visible, and ultraviolet regions of the electromagnetic spectrum, and a method for making multidimensional spectroscopic measurements in the infrared, visible, and ultraviolet regions of the electromagnetic spectrum. The multidimensional spectrometer facilitates measurements of inter- and intra-molecular interactions.

NaI(Tl) scintillator read out with SiPM array for gamma spectrometer

NASA Astrophysics Data System (ADS)

Huang, Tuchen; Fu, Qibin; Lin, Shaopeng; Wang, Biao

2017-04-01

The NaI(Tl) scintillator is widely used in gamma spectrometer with photomultiplier tube (PMT) readout. Recently developed silicon photomultiplier (SiPM) offers gain and efficiency similar to those of PMT, but with merits such as low bias voltage, compact volume, low cost, high ruggedness and magnetic resonance compatibility. In this study, 2-in. and 1-in. NaI(Tl) scintillators were readout with SiPM arrays, which were made by tiling multiple SiPMs each with an active area of 6×6 mm2 on a printed circuit board. The energy resolutions for 661.6 keV gamma rays, obtained with Φ2×2 in. scintillator coupled to 6×6 ch SiPM array and Φ1×1 in. scintillator coupled to 4×4 ch SiPM array were 7.6% and 7.8%, respectively, and were very close to the results obtained with traditional bialkali PMT (7.3% and 7.6%, respectively). Scintillator coupled to photodetector with smaller area was also studied by adding a light guide or using scintillator with tapered head. The latter showed better performance than using light guide. The 1-in. NaI(Tl) scintillator with tapered head coupled to 2×2 ch SiPM array achieved 7.7% energy resolution at 661.6 keV, the same as that obtained with standard Φ1×1 in. scintillator coupled to 4×4 ch SiPM array. While the 2-in. scintillator with similar geometry showed degraded energy resolution, 10.2% at 661.6 keV, but could still be used when high efficiency is preferred over energy resolution.

Chromatic aberrations correction for imaging spectrometer based on acousto-optic tunable filter with two transducers.

PubMed

Zhao, Huijie; Wang, Ziye; Jia, Guorui; Zhang, Ying; Xu, Zefu

2017-10-02

The acousto-optic tunable filter (AOTF) with wide wavelength range and high spectral resolution has long crystal and two transducers. A longer crystal length leads to a bigger chromatic focal shift and the double-transducer arrangement induces angular mutation in diffracted beam, which increase difficulty in longitudinal and lateral chromatic aberration correction respectively. In this study, the two chromatic aberrations are analyzed quantitatively based on an AOTF optical model and a novel catadioptric dual-path configuration is proposed to correct both the chromatic aberrations. The test results exhibit effectiveness of the optical configuration for this type of AOTF-based imaging spectrometer.

Growth of bulk ZnO crystals by self-selecting CVT method

NASA Astrophysics Data System (ADS)

Fan, Long; Jiang, Tao; Xiao, TingTing; Chen, Jie; Peng, Liping; Wang, Xuemin; Yan, Dawei; Wu, Weidong

2018-05-01

Bulk ZnO crystals were grown by self-selecting CVT method using carbon as the transport agent. The crystal growth process took place on the top of the polycrystalline source material, and deep-red colored ZnO crystals of several millimeters were obtained. The as-grown crystals were characterized by X-ray diffraction (XRD), Energy Dispersive Spectrometer (EDS), Raman scattering (RS) spectroscopy, visible-near infrared (VIS-NIR) spectrophotometer and room temperature photoluminescence (PL) spectroscopy. XRD results indicate good crystallinity of the ZnO crystal. The EDS analysis shows that the crystal has a stoichiometry ratio Zn: O = 52: 48. The results suggest the existence of native defects of oxygen vacancies (OV) in the as-grown ZnO samples, which is caused by the stoichiometry shift to Zn-rich.

Intrinsic light yield and light loss coefficient of Bi4Ge3O12 single crystals

NASA Astrophysics Data System (ADS)

Yawai, Nattasuda; Chewpraditkul, Weerapong; Wanarak, Chalerm; Nikl, Martin; Ratanatongchai, Wichian

2014-10-01

In this paper we present the scintillation properties of polished Bi4Ge3O12 (BGO) crystals grown by the Bridgman method. The light yield (LY) and energy resolution were measured using XP5200B photomultiplier. At 662 keV γ-rays, high LY of 9680 photons/MeV and good energy resolution of 8.6% were obtained for a 5 × 5 × 1 mm3 BGO sample. The intrinsic LY and light loss coefficient were evaluated. The photofraction in pulse height spectrum of 662 keV γ-rays and the mass attenuation coefficient at 59.5 and 662 keV γ-rays were also determined and compared with the theoretical ones calculated using the WinXCom program.

Characterization of Pr:LuAG scintillating crystals for X-ray spectroscopy

NASA Astrophysics Data System (ADS)

Bertoni, R.; Bonesini, M.; Cervi, T.; Clemenza, M.; De Bari, A.; Falcone, A.; Mazza, R.; Menegolli, A.; Nastasi, M.; Rossella, M.

2016-07-01

The main features of the Pr doped Lu3Al5O12 (Pr:LuAG) scintillating crystals for X-ray spectroscopy applications have been studied using different radioactive sources and photo-detectors. Pr:LuAG is cheaper, compared to a Germanium detector, but with remarkable properties which make it useful for many applications, from fundamental physics measurements to the PET imaging for medical purposes: high density, elevate light yield, fast response, high energy resolution, no hygroscopicity. A sample of Pr:LuAG crystals with 14 mm×14 mm surface area and 13 mm thickness and a NaI crystal of the same surface and 26 mm thickness used as a reference have been characterized with several radioactive sources, emitting photons in the range 100-1000keV. Different light detectors were adopted for the Pr:LuAG studies, sensitive to its UV emission (peak at 310 nm): a 3 in. PMT (Hamamatsu R11065) and new arrays of Hamamatsu SiPM S13361, with siliconic resin as a window. Preliminary results are presented on the performance of the Pr:LuAG crystals, to be mounted in a 2 × 2 array to be tested in the 2015 run of the FAMU experiment at RIKEN-RAL muon facility. The goal is the detection of the X-rays (around 130 keV) emitted during the de-excitation processes of the muonic hydrogen after the excitation with an IR laser with wavelength set at the resonance of the hyperfine splitting, to measure the muonic atom proton radius with unprecedented precision.

The magnetic recoil spectrometer (MRSt) for time-resolved measurements of the neutron spectrum at the National Ignition Facility (NIF)

DOE PAGES

Frenje, J. A.; Hilsabeck, T. J.; Wink, C. W.; ...

2016-08-02

The next-generation magnetic recoil spectrometer for time-resolved measurements of the neutron spectrum has been conceptually designed for the National Ignition Facility. This spectrometer, called MRSt, represents a paradigm shift in our thinking about neutron spectrometry for inertial confinement fusion applications, as it will provide simultaneously information about the burn history and time evolution of areal density (ρR), apparent ion temperature (T i), yield (Y n), and macroscopic flows during burn. From this type of data, an assessment of the evolution of the fuel assembly, hotspot, and alpha heating can be made. According to simulations, the MRSt will provide accurate datamore » with a time resolution of ~20 ps and energy resolution of ~100 keV for total neutron yields above ~10 16. Lastly, at lower yields, the diagnostic will be operated at a higher-efficiency, lower-energy-resolution mode to provide a time resolution of ~20 ps.« less

The magnetic recoil spectrometer (MRSt) for time-resolved measurements of the neutron spectrum at the National Ignition Facility (NIF).

PubMed

Frenje, J A; Hilsabeck, T J; Wink, C W; Bell, P; Bionta, R; Cerjan, C; Gatu Johnson, M; Kilkenny, J D; Li, C K; Séguin, F H; Petrasso, R D

2016-11-01

The next-generation magnetic recoil spectrometer for time-resolved measurements of the neutron spectrum has been conceptually designed for the National Ignition Facility. This spectrometer, called MRSt, represents a paradigm shift in our thinking about neutron spectrometry for inertial confinement fusion applications, as it will provide simultaneously information about the burn history and time evolution of areal density (ρR), apparent ion temperature (T i ), yield (Y n ), and macroscopic flows during burn. From this type of data, an assessment of the evolution of the fuel assembly, hotspot, and alpha heating can be made. According to simulations, the MRSt will provide accurate data with a time resolution of ∼20 ps and energy resolution of ∼100 keV for total neutron yields above ∼10 16 . At lower yields, the diagnostic will be operated at a higher-efficiency, lower-energy-resolution mode to provide a time resolution of ∼20 ps.

The magnetic recoil spectrometer (MRSt) for time-resolved measurements of the neutron spectrum at the National Ignition Facility (NIF)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Frenje, J. A., E-mail: jfrenje@psfc.mit.edu; Wink, C. W.; Gatu Johnson, M.

The next-generation magnetic recoil spectrometer for time-resolved measurements of the neutron spectrum has been conceptually designed for the National Ignition Facility. This spectrometer, called MRSt, represents a paradigm shift in our thinking about neutron spectrometry for inertial confinement fusion applications, as it will provide simultaneously information about the burn history and time evolution of areal density (ρR), apparent ion temperature (T{sub i}), yield (Y{sub n}), and macroscopic flows during burn. From this type of data, an assessment of the evolution of the fuel assembly, hotspot, and alpha heating can be made. According to simulations, the MRSt will provide accurate datamore » with a time resolution of ∼20 ps and energy resolution of ∼100 keV for total neutron yields above ∼10{sup 16}. At lower yields, the diagnostic will be operated at a higher-efficiency, lower-energy-resolution mode to provide a time resolution of ∼20 ps.« less

Multi-ampoule Bridgman growth of halide scintillator crystals using the self-seeding method

NASA Astrophysics Data System (ADS)

Lindsey, Adam C.; Wu, Yuntao; Zhuravleva, Mariya; Loyd, Matthew; Koschan, Merry; Melcher, Charles L.

2017-07-01

We investigate the multi-ampoule growth at 25 mm diameter of ternary iodide single crystal scintillator KCaI3:Eu using the randomly oriented self-seeded Bridgman method. We compare scintillation performance between cubic inch scale crystals containing small variations of low nominal europium concentrations previously shown to balance light yield with self-absorption in the host crystal. Growth conditions were optimized in the developmental furnace and four 2 in3 KCaI3:Eu crystals were grown simultaneously producing a total of six 25 mm × 25 mm cylinders. Small variations in activator concentration did not result in significant performance differences among the six measured crystals. A range of energy resolutions of 3.5-4.7% at 662 keV was achieved, surpassing that of NaI:Tl crystals commonly used in spectroscopic detection applications. The function and basic design of the multi-ampoule furnace as well as the process of growing single crystals of KCaI3 is included here.

Detailed characterization of the LLNL imaging proton spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rasmus, A. M., E-mail: rasmus@lanl.gov, E-mail: arasmus@umich.edu; University of Michigan, Ann Arbor, Michigan 48109; Hazi, A. U.

2016-11-15

Ultra-intense short pulse lasers incident on solid targets (e.g., thin Au foils) produce well collimated, broad-spectrum proton beams. These proton beams can be used to characterize magnetic fields, electric fields, and density gradients in high energy-density systems. The LLNL-Imaging Proton Spectrometer (L-IPS) was designed and built [H. Chen et al., Rev. Sci. Instrum. 81, 10D314 (2010)] for use with such laser produced proton beams. The L-IPS has an energy range of 50 keV-40 MeV with a resolving power (E/dE) of about 275 at 1 MeV and 21 at 20 MeV, as well as a single spatial imaging axis. In ordermore » to better characterize the dispersion and imaging capability of this diagnostic, a 3D finite element analysis solver is used to calculate the magnetic field of the L-IPS. Particle trajectories are then obtained via numerical integration to determine the dispersion relation of the L-IPS in both energy and angular space.« less

Measurement and models of bent KAP(001) crystal integrated reflectivity and resolution (invited)

NASA Astrophysics Data System (ADS)

Loisel, G. P.; Wu, M.; Stolte, W.; Kruschwitz, C.; Lake, P.; Dunham, G. S.; Bailey, J. E.; Rochau, G. A.

2016-11-01

The Advanced Light Source beamline-9.3.1 x-rays are used to calibrate the rocking curve of bent potassium acid phthalate (KAP) crystals in the 2.3-4.5 keV photon-energy range. Crystals are bent on a cylindrically convex substrate with a radius of curvature ranging from 2 to 9 in. and also including the flat case to observe the effect of bending on the KAP spectrometric properties. As the bending radius increases, the crystal reflectivity converges to the mosaic crystal response. The X-ray Oriented Programs (xop) multi-lamellar model of bent crystals is used to model the rocking curve of these crystals and the calibration data confirm that a single model is adequate to reproduce simultaneously all measured integrated reflectivities and rocking-curve FWHM for multiple radii of curvature in both 1st and 2nd order of diffraction.

Measurement and models of bent KAP(001) crystal integrated reflectivity and resolution (invited)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Loisel, G. P., E-mail: gploise@sandia.gov; Wu, M.; Lake, P.

2016-11-15

The Advanced Light Source beamline-9.3.1 x-rays are used to calibrate the rocking curve of bent potassium acid phthalate (KAP) crystals in the 2.3-4.5 keV photon-energy range. Crystals are bent on a cylindrically convex substrate with a radius of curvature ranging from 2 to 9 in. and also including the flat case to observe the effect of bending on the KAP spectrometric properties. As the bending radius increases, the crystal reflectivity converges to the mosaic crystal response. The X-ray Oriented Programs (XOP) multi-lamellar model of bent crystals is used to model the rocking curve of these crystals and the calibration datamore » confirm that a single model is adequate to reproduce simultaneously all measured integrated reflectivities and rocking-curve FWHM for multiple radii of curvature in both 1st and 2nd order of diffraction.« less

The SPEDE spectrometer

NASA Astrophysics Data System (ADS)

Papadakis, P.; Cox, D. M.; O'Neill, G. G.; Borge, M. J. G.; Butler, P. A.; Gaffney, L. P.; Greenlees, P. T.; Herzberg, R.-D.; Illana, A.; Joss, D. T.; Konki, J.; Kröll, T.; Ojala, J.; Page, R. D.; Rahkila, P.; Ranttila, K.; Thornhill, J.; Tuunanen, J.; Van Duppen, P.; Warr, N.; Pakarinen, J.

2018-03-01

The electron spectrometer, SPEDE, has been developed and will be employed in conjunction with the Miniball spectrometer at the HIE-ISOLDE facility, CERN. SPEDE allows for direct measurement of internal conversion electrons emitted in-flight, without employing magnetic fields to transport or momentum filter the electrons. Together with the Miniball spectrometer, it enables simultaneous observation of γ rays and conversion electrons in Coulomb excitation experiments using radioactive ion beams.

A compact proton spectrometer for measurement of the absolute DD proton spectrum from which yield and pR are determined in thin-shell inertial-confinement-fusion implosions

DOE PAGES

Rosenberg, M. J.; Zylstra, A. B.; Frenje, J. A.; ...

2014-10-10

A compact, step range filter proton spectrometer has been developed for the measurement of the absolute DD proton spectrum, from which yield and areal density (ρR) are inferred for deuterium-filled thin-shell inertial confinement fusion implosions. This spectrometer, which is based on tantalum step-range filters, is sensitive to protons in the energy range 1-9 MeV and can be used to measure proton spectra at mean energies of ~1-3 MeV. It has been developed and implemented using a linear accelerator and applied to experiments at the OMEGA laser facility and the National Ignition Facility (NIF). Modeling of the proton slowing in themore » filters is necessary to construct the spectrum, and the yield and energy uncertainties are ±<10% in yield and ±120 keV, respectively. This spectrometer can be used for in situ calibration of DD-neutron yield diagnostics at the NIF« less

A compact proton spectrometer for measurement of the absolute DD proton spectrum from which yield and ρR are determined in thin-shell inertial-confinement-fusion implosions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rosenberg, M. J., E-mail: mrosenbe@mit.edu; Zylstra, A. B.; Frenje, J. A.

2014-10-01

A compact, step range filter proton spectrometer has been developed for the measurement of the absolute DD proton spectrum, from which yield and areal density (ρR) are inferred for deuterium-filled thin-shell inertial confinement fusion implosions. This spectrometer, which is based on tantalum step-range filters, is sensitive to protons in the energy range 1-9 MeV and can be used to measure proton spectra at mean energies of ~1-3 MeV. It has been developed and implemented using a linear accelerator and applied to experiments at the OMEGA laser facility and the National Ignition Facility (NIF). Modeling of the proton slowing in themore » filters is necessary to construct the spectrum, and the yield and energy uncertainties are ±<10% in yield and ±120 keV, respectively. This spectrometer can be used for in situ calibration of DD-neutron yield diagnostics at the NIF.« less

Using neutrons to measure keV temperatures in highly compressed plastic at multi-Gbar pressures

DOE PAGES

Nilsen, J.; Bachmann, B.; Zimmerman, G. B.; ...

2016-10-27

In this study, we have designed an experiment for the National Ignition Facility to measure the Hugoniot of materials such as plastic at extreme pressures. The design employs a strong spherically converging shock launched through a solid ball of material using a hohlraum radiation drive. The shock front conditions can be characterized using X-ray radiography until background from shock coalescence overtakes the backlit signal. Shock coalescence at the center is predicted to reach tens of Gbars and can be further characterized by measuring the X-ray self-emission and 2.45 MeV neutrons emitted from the shock flash region. In this simulation designmore » work the standard plastic sphere is replaced with a deuterated polyethylene sphere, CD 2, that reaches sufficiently high densities and temperatures in the central hot spot to produce neutrons from Deuterium-Deuterium (DD) fusion reactions that can be measured by a neutron time of flight spectrometer (nTOF) and act as a temperature diagnostic. This paper focuses on the design of these experiments, based on an extensive suite of radiation-hydrodynamics simulations, and the interpretation of the predicted DD neutron signals. The simulations predict mean temperatures of 1 keV in the central hot spot with mean densities of 33 g/cc and mean pressures of 25 Gbar. Lastly, a preliminary comparison with early experimental results looks promising with an average ion temperature of 1.06 ± 0.15 keV in the central hot spot estimated from the nTOF spectral width and measured neutron yield of 7.0 (±0.5) × 10 9 DD neutrons.« less

Design and Performance of A High Resolution Micro-Spec: An Integrated Sub-Millimeter Spectrometer

NASA Technical Reports Server (NTRS)

Barrentine, Emily M.; Cataldo, Giuseppe; Brown, Ari D.; Ehsan, Negar; Noroozian, Omid; Stevenson, Thomas R.; U-Yen, Kongpop; Wollack, Edward J.; Moseley, S. Harvey

2016-01-01

Micro-Spec is a compact sub-millimeter (approximately 100 GHz--1:1 THz) spectrometer which uses low loss superconducting microstrip transmission lines and a single-crystal silicon dielectric to integrate all of the components of a diffraction grating spectrometer onto a single chip. We have already successfully evaluated the performance of a prototype Micro-Spec, with spectral resolving power, R=64. Here we present our progress towards developing a higher resolution Micro-Spec, which would enable the first science returns in a balloon flight version of this instrument. We describe modifications to the design in scaling from a R=64 to a R=256 instrument, as well as the ultimate performance limits and design concerns when scaling this instrument to higher resolutions.

Expected performances of a Laue lens made with bent crystals

NASA Astrophysics Data System (ADS)

Virgilli, Enrico; Valsan, Vineeth; Frontera, Filippo; Caroli, Ezio; Liccardo, Vincenzo; Stephen, John Buchan

2017-10-01

In the context of the Laue project devoted to build a Laue lens prototype for focusing celestial hard x-/soft gamma-rays, a Laue lens made of bent crystal tiles, with 20-m focal length, is simulated. The focusing energy passband is assumed to be 90 to 600 keV. The distortion of the image produced by the lens on the focal plane, due to effects of crystal tile misalignment and radial distortion of the crystal curvature, is investigated. The corresponding effective area of the lens, its point spread function, and sensitivity are calculated and compared with those exhibited by a nominal Laue lens with no misalignment and/or distortion. Such analysis is crucial to estimate the optical properties of a real lens, in which the investigated shortcomings could be present.

Line Emission and X-ray Line Polarization of Multiply Ionized Mo Ions

NASA Astrophysics Data System (ADS)

Petkov, E. E.; Safronova, A. S.; Kantsyrev, V. L.; Shlyaptseva, V. V.; Stafford, A.; Safronova, U. I.; Shrestha, I. K.; Schultz, K. A.; Childers, R.; Cooper, M. C.; Beiersdorfer, P.; Hell, N.; Brown, G. V.

2016-10-01

We present a comprehensive experimental and theoretical study of the line emission from multiply ionized Mo ions produced by two different sets of experiments: at LLNL EBIT and the pulsed power generator Zebra at UNR. Mo line emission and polarization measurements were accomplished at EBIT for the first time. In particular, benchmarking experiments at the LLNL EBIT with Mo ions produced at electron beam energies from 2.75 keV up to 15 keV allowed us to break down these very complicated spectra into spectra with only few ionization stages and to select processes that influence them as well as to measure line polarization. The EBIT data were recorded using the EBIT Calorimeter Spectrometer and a crystal spectrometer with a Ge crystal. X-ray Mo spectra and pinhole images were collected from Z-pinch plasmas produced from various wire loads. Non-LTE modeling, high-precision relativistic atomic and polarization data were used to analyze L-shell Mo spectra. The influence of different plasma processes including electron beams on Mo line radiation is summarized. This work was supported by NNSA under DOE Grant DE-NA0002954. Experiments at the NTF/UNR were funded in part by DE-NA0002075. Work at LLNL was performed under the auspices of the U.S. DOE under contract DE-AC52-07NA27344.

Bent crystal spectrometer for both frequency and wavenumber resolved x-ray scattering at a seeded free-electron laser.

PubMed

Zastrau, Ulf; Fletcher, Luke B; Förster, Eckhart; Galtier, Eric Ch; Gamboa, Eliseo; Glenzer, Siegfried H; Heimann, Philipp; Marschner, Heike; Nagler, Bob; Schropp, Andreas; Wehrhan, Ortrud; Lee, Hae Ja

2014-09-01

We present a cylindrically curved GaAs x-ray spectrometer with energy resolution ΔE/E = 1.1 × 10(-4) and wave-number resolution of Δk/k = 3 × 10(-3), allowing plasmon scattering at the resolution limits of the Linac Coherent Light Source (LCLS) x-ray free-electron laser. It spans scattering wavenumbers of 3.6 to 5.2/Å in 100 separate bins, with only 0.34% wavenumber blurring. The dispersion of 0.418 eV/13.5 μm agrees with predictions within 1.3%. The reflection homogeneity over the entire wavenumber range was measured and used to normalize the amplitude of scattering spectra. The proposed spectrometer is superior to a mosaic highly annealed pyrolytic graphite spectrometer when the energy resolution needs to be comparable to the LCLS seeded bandwidth of 1 eV and a significant range of wavenumbers must be covered in one exposure.

The SPIDER fission fragment spectrometer for fission product yield measurements

DOE PAGES

Meierbachtol, K.; Tovesson, F.; Shields, D.; ...

2015-04-01

We developed the SPectrometer for Ion DEtermination in fission Research (SPIDER) for measuring mass yield distributions of fission products from spontaneous and neutron-induced fission. The 2E–2v method of measuring the kinetic energy (E) and velocity (v) of both outgoing fission products has been utilized, with the goal of measuring the mass of the fission products with an average resolution of 1 atomic mass unit (amu). Moreover, the SPIDER instrument, consisting of detector components for time-of-flight, trajectory, and energy measurements, has been assembled and tested using 229Th and 252Cf radioactive decay sources. For commissioning, the fully assembled system measured fission productsmore » from spontaneous fission of 252Cf. Individual measurement resolutions were met for time-of-flight (250 ps FWHM), spacial resolution (2 mm FHWM), and energy (92 keV FWHM for 8.376 MeV). Finally, these mass yield results measured from 252Cf spontaneous fission products are reported from an E–v measurement.« less

Crystal growth and dislocation etch pits observation of chalcopyrite CdSiP2

NASA Astrophysics Data System (ADS)

He, Zhiyu; Zhao, Beijun; Zhu, Shifu; Chen, Baojun; Huang, Wei; Lin, Li; Feng, Bo

2018-01-01

CdSiP2 is the only crystal that can offer Non-critical Phase Matching (NCPM) for a 1064 nm pumped optical parametric oscillation (OPO) with idler output in the 6 μm range. In this paper, a large, crack-free CdSiP2 single crystal measuring 18 mm in diameter and 65 mm in length was successfully grown by the Vertical Bridgman method (MVB) with an explosion-proof quartz ampoule. The results of lattice parameters, element composition and IR transmittance of the as-grown crystal characterized by X-ray diffraction (XRD), energy dispersive X-ray spectrometer (EDS) and Fourier transformation infrared spectrometer (FTIR) showed the as grown crystal crystallized well and the absorption coefficients at 4878 cm-1 and 2500 cm-1 were 0.14 cm-1 and 0.06 cm-1. Moreover, a new etchant composed of Br2, HCl, HNO3, CH3OH and H2O (1:800:800:400:400 in volume ratio) was prepared and the dislocation etch pits on oriented faces of as-grown CdSiP2 crystal were observed for the first time. It is found the etch pits are in rectangular structure on the (1 0 1) face, but in trigonal pyramid structure on (3 1 2) face. According to the quantities of the etch pits, the average densities of dislocation were evaluated to be 2.28 × 105/cm2 and 1.4 × 105/cm2, respectively.

Performance revaluation of a N-type coaxial HPGe detector with front edges crystal using MCNPX.

PubMed

Azli, Tarek; Chaoui, Zine-El-Abidine

2015-03-01

The MCNPX code was used to determine the efficiency of a N-type HPGe detector after two decades of operation. Accounting for the roundedness of the crystal`s front edges and an inhomogeneous description of the detector's dead layers were shown to achieve better agreement between measurements and simulation efficiency determination. The calculations were experimentally verified using point sources in the energy range from 50keV to 1400keV, and an overall uncertainty less than 2% was achieved. In order to use the detector for different matrices and geometries in radioactivity, the suggested model was validated by changing the counting geometry and by using multi-gamma disc sources. The introduced simulation approach permitted the revaluation of the performance of an HPGe detector in comparison of its initial condition, which is a useful tool for precise determination of the thickness of the inhomogeneous dead layer. Copyright © 2014 Elsevier Ltd. All rights reserved.

X-ray Free Electron Laser Determination of Crystal Structures of Dark and Light States of a Reversibly Photoswitching Fluorescent Protein at Room Temperature

PubMed Central

Hutchison, Christopher D. M.; Cordon-Preciado, Violeta; Morgan, Rhodri M. L.; Dorlhiac, Gabriel; Sanchez-Gonzalez, Alvaro; Fitzpatrick, Ann; Fare, Clyde; Marangos, Jon P.; Hunter, Mark S.; DePonte, Daniel P.; Boutet, Sébastien; Owada, Shigeki; Tanaka, Rie; Tono, Kensuke; Iwata, So; van Thor, Jasper J.

2017-01-01

The photochromic fluorescent protein Skylan-NS (Nonlinear Structured illumination variant mEos3.1H62L) is a reversibly photoswitchable fluorescent protein which has an unilluminated/ground state with an anionic and cis chromophore conformation and high fluorescence quantum yield. Photo-conversion with illumination at 515 nm generates a meta-stable intermediate with neutral trans-chromophore structure that has a 4 h lifetime. We present X-ray crystal structures of the cis (on) state at 1.9 Angstrom resolution and the trans (off) state at a limiting resolution of 1.55 Angstrom from serial femtosecond crystallography experiments conducted at SPring-8 Angstrom Compact Free Electron Laser (SACLA) at 7.0 keV and 10.5 keV, and at Linac Coherent Light Source (LCLS) at 9.5 keV. We present a comparison of the data reduction and structure determination statistics for the two facilities which differ in flux, beam characteristics and detector technologies. Furthermore, a comparison of droplet on demand, grease injection and Gas Dynamic Virtual Nozzle (GDVN) injection shows no significant differences in limiting resolution. The photoconversion of the on- to the off-state includes both internal and surface exposed protein structural changes, occurring in regions that lack crystal contacts in the orthorhombic crystal form. PMID:28880248

Thermal neutron detector and gamma-ray spectrometer utilizing a single material

DOEpatents

Stowe, Ashley; Burger, Arnold; Lukosi, Eric

2017-05-02

A combined thermal neutron detector and gamma-ray spectrometer system, including: a detection medium including a lithium chalcopyrite crystal operable for detecting thermal neutrons in a semiconductor mode and gamma-rays in a scintillator mode; and a photodetector coupled to the detection medium also operable for detecting the gamma rays. Optionally, the detection medium includes a .sup.6LiInSe.sub.2 crystal. Optionally, the detection medium comprises a compound formed by the process of: melting a Group III element; adding a Group I element to the melted Group III element at a rate that allows the Group I and Group III elements to react thereby providing a single phase I-III compound; and adding a Group VI element to the single phase I-III compound and heating; wherein the Group I element includes lithium.

Advanced crystal growth techniques for thallium bromide semiconductor radiation detectors

NASA Astrophysics Data System (ADS)

Datta, Amlan; Becla, Piotr; Guguschev, Christo; Motakef, Shariar

2018-02-01

Thallium Bromide (TlBr) is a promising room-temperature radiation detector candidate with excellent charge transport properties. Currently, Travelling Molten Zone (TMZ) technique is widely used for growth of semiconductor-grade TlBr crystals. However, there are several challenges associated with this type of crystal growth process including lower yield, high thermal stress, and low crystal uniformity. To overcome these shortcomings of the current technique, several different crystal growth techniques have been implemented in this study. These include: Vertical Bridgman (VB), Physical Vapor Transport (PVT), Edge-defined Film-fed Growth (EFG), and Czochralski Growth (Cz). Techniques based on melt pulling (EFG and Cz) were demonstrated for the first time for semiconductor grade TlBr material. The viability of each process along with the associated challenges for TlBr growth has been discussed. The purity of the TlBr crystals along with its crystalline and electronic properties were analyzed and correlated with the growth techniques. Uncorrected 662 keV energy resolutions around 2% were obtained from 5 mm x 5 mm x 10 mm TlBr devices with virtual Frisch-grid configuration.

Study of 1–8 keV K-α x-ray emission from high intensity femtosecond laser produced plasma

DOE Office of Scientific and Technical Information (OSTI.GOV)

Arora, V., E-mail: arora@rrcat.gov.in; Naik, P. A.; Chakera, J. A.

2014-04-15

We report an experimental study on the optimization of a laser plasma based x-ray source of ultra-short duration K-α line radiation. The interaction of pulses from a CPA based Ti:sapphire laser (10 TW, 45 fs, 10 Hz) system with magnesium, titanium, iron and copper solid target generates bright 1-8 keV K-α x-ray radiation. The x-ray yield was optimized with the laser pulse duration (at fixed fluence) which is varied in the range of 45 fs to 1.4 ps. It showed a maximum at laser pulse duration of ∼740 fs, 420 fs, 350 and 250 fs for Mg (1.3 keV), Timore » (4.5 keV), Fe (6.4 keV) and Cu (8.05 keV) respectively. The x-ray yield is observed to be independent of the sign of the chirp. The scaling of the K-α yield (I{sub x} ∝ I{sub L}{sup β}) for 45 fs and optimized pulse duration were measured for laser intensities in the region of 3 × 10{sup 14} – 8 × 10{sup 17}. The x-ray yield shows a much faster scaling exponent β = 1.5, 2.1, 2.4 and 2.6 for Mg, Ti, Fe and Cu respectively at optimized pulse duration compared to scaling exponent of 0.65, 1.3, 1.5, and 1.7 obtained for 45 fs duration laser pulses. The laser to x-ray energy conversion efficiencies obtained for different target materials are η{sub Mg} = 1.2 × 10{sup −5}, η{sub Ti} = 3.1 × 10{sup −5}, η{sub Fe} = 2.7 × 10{sup −5}, η{sub Cu} = 1.9 × 10{sup −5}. The results have been explained from the efficient generation of optimal energy hot electrons at longer laser pulse duration. The faster scaling observed at optimal pulse duration indicates that the x-ray source is generated at the target surface and saturation of x-ray emission would appear at larger laser fluence. An example of utilization of the source for measurement of shock-wave profiles in a silicon crystal by time resolved x-ray diffraction is also presented.« less

Neutron resonance spin-echo upgrade at the three-axis spectrometer FLEXX

DOE Office of Scientific and Technical Information (OSTI.GOV)

Groitl, F., E-mail: felix.groitl@psi.ch; Quintero-Castro, D. L.; Habicht, K.

2015-02-15

We describe the upgrade of the neutron resonance spin-echo setup at the cold neutron triple-axis spectrometer FLEXX at the BER II neutron source at the Helmholtz-Zentrum Berlin. The parameters of redesigned key components are discussed, including the radio frequency (RF) spin-flip coils, the magnetic shield, and the zero field coupling coils. The RF-flippers with larger beam windows allow for an improved neutron flux transfer from the source to the sample and further to the analyzer. The larger beam cross sections permit higher coil inclination angles and enable measurements on dispersive excitations with a larger slope of the dispersion. Due tomore » the compact design of the spin-echo units in combination with the increased coil tilt angles, the accessible momentum-range in the Larmor diffraction mode is substantially enlarged. In combination with the redesigned components of the FLEXX spectrometer, including the guide, the S-bender polarizer, the double focusing monochromator, and a Heusler crystal analyzer, the count rate increased by a factor of 15.5, and the neutron beam polarization is enhanced. The improved performance extends the range of feasible experiments, both for inelastic scattering on excitation lifetimes in single crystals, and for high-resolution Larmor diffraction. The experimental characterization of the instrument components demonstrates the reliable performance of the new neutron resonance spin-echo option, now available for the scientific community at FLEXX.« less

Linear attenuation coefficients of tissues from 1 keV to 150 keV

NASA Astrophysics Data System (ADS)

Böke, Aysun

2014-09-01

The linear attenuation coefficients and three interaction processes have been computed for liver, kidney, muscle, fat and for a range of x-ray energies from 1 keV to 150 keV. Molecular photoelectric absorption cross sections were calculated from atomic cross section data. Total coherent (Rayleigh) and incoherent (Compton) scattering cross sections were obtained by numerical integration over combinations of F2m(x) with the Thomson formula and Sm(x) with the Klein-Nishina formula, respectively. For the coherent (Rayleigh) scattering cross section calculations, molecular form factors were obtained from recent experimental data in the literature for values of x<1 Å-1 and from the relativistic modified atomic form factors for values of x≥1 Å-1. With the inclusion of molecular interference effects in the coherent (Rayleigh) scattering, more accurate knowledge of the scatter from these tissues will be provided. The number of elements involved in tissue composition is 5 for liver, 47 for kidney, 44 for muscle and 3 for fat. The results are compared with previously published experimental and theoretical linear attenuation coefficients. In general, good agreement is obtained. The molecular form factors and scattering functions and cross sections are incorporated into a Monte Carlo program. The energy distributions of x-ray photons scattered from tissues have been simulated and the results are presented.

Bulk and integrated acousto-optic spectrometers for molecular astronomy with heterodyne spectrometers

NASA Technical Reports Server (NTRS)

Chin, G.; Buhl, D.; Florez, J. M.

1981-01-01

A survey of acousto-optic spectrometers for molecular astronomy is presented, noting a technique of combining the acoustic bending of a collimated coherent light beam with a Bragg cell followed by an array of sensitive photodetectors. This acousto-optic spectrometer has a large bandwidth, a large number of channels, high resolution, and is energy efficient. Receiver development has concentrated on high-frequency heterodyne systems for the study of the chemical composition of the interstellar medium. RF spectrometers employing acousto-optic diffraction cells are described. Acousto-optic techniques have been suggested for applications to electronic warfare, electronic countermeasures and electronic support systems. Plans to use integrated optics for the further miniaturization of acousto-optic spectrometers are described. Bulk acousto-optic spectrometers with 300 MHz and 1 GHz bandwidths are being developed for use in the back-end of high-frequency heterodyne receivers for astronomical research.

Compact Infrared Spectrometers

NASA Technical Reports Server (NTRS)

Mouroulis, Pantazis

2009-01-01

Concentric spectrometer forms are advantageous for constructing a variety of systems spanning the entire visible to infrared range. Spectrometer examples are given, including broadband or high resolution forms. Some issues associated with the Dyson catadioptric type are also discussed.

The Astro-H High Resolution Soft X-Ray Spectrometer

NASA Technical Reports Server (NTRS)

Kelley, Richard L.; Akamatsu, Hiroki; Azzarell, Phillip; Bialas, Tom; Boyce, Kevin R.; Brown, Gregory V.; Canavan, Edgar; Chiao, Meng P.; Costantini, Elisa; DiPirro, Michael J.;

The Astro-H high resolution soft x-ray spectrometer

NASA Astrophysics Data System (ADS)

Kelley, Richard L.; Akamatsu, Hiroki; Azzarello, Phillipp; Bialas, Tom; Boyce, Kevin R.; Brown, Gregory V.; Canavan, Edgar; Chiao, Meng P.; Costantini, Elisa; DiPirro, Michael J.; Eckart, Megan E.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Haas, Daniel; den Herder, Jan-Willem; Hoshino, Akio; Ishikawa, Kumi; Ishisaki, Yoshitaka; Iyomoto, Naoko; Kilbourne, Caroline A.; Kimball, Mark O.; Kitamoto, Shunji; Konami, Saori; Koyama, Shu; Leutenegger, Maurice A.; McCammon, Dan; Mitsuda, Kazuhisa; Mitsuishi, Ikuyuki; Moseley, Harvey; Murakami, Hiroshi; Murakami, Masahide; Noda, Hirofumi; Ogawa, Mina; Ohashi, Takaya; Okamoto, Atsushi; Ota, Naomi; Paltani, Stéphane; Porter, F. S.; Sakai, Kazuhiro; Sato, Kosuke; Sato, Yohichi; Sawada, Makoto; Seta, Hiromi; Shinozaki, Keisuke; Shirron, Peter J.; Sneiderman, Gary A.; Sugita, Hiroyuki; Szymkowiak, Andrew E.; Takei, Yoh; Tamagawa, Toru; Tashiro, Makoto; Terada, Yukikatsu; Tsujimoto, Masahiro; de Vries, Cor P.; Yamada, Shinya; Yamasaki, Noriko Y.; Yatsu, Yoichi

2016-07-01

We present the overall design and performance of the Astro-H (Hitomi) Soft X-Ray Spectrometer (SXS). The instrument uses a 36-pixel array of x-ray microcalorimeters at the focus of a grazing-incidence x-ray mirror Soft X-Ray Telescope (SXT) for high-resolution spectroscopy of celestial x-ray sources. The instrument was designed to achieve an energy resolution better than 7 eV over the 0.3-12 keV energy range and operate for more than 3 years in orbit. The actual energy resolution of the instrument is 4-5 eV as demonstrated during extensive ground testing prior to launch and in orbit. The measured mass flow rate of the liquid helium cryogen and initial fill level at launch predict a lifetime of more than 4 years assuming steady mechanical cooler performance. Cryogen-free operation was successfully demonstrated prior to launch. The successful operation of the SXS in orbit, including the first observations of the velocity structure of the Perseus cluster of galaxies, demonstrates the viability and power of this technology as a tool for astrophysics.

Investigation of the unique degradation phenomenon observed in CsSrBr3: Eu 5% scintillator crystals

NASA Astrophysics Data System (ADS)

Gokhale, S. S.; Loyd, M.; Stand, L.; Lindsey, A.; Swider, S.; Zhuravleva, M.; Melcher, C. L.

2016-10-01

CsSrBr3: Eu 5% is a promising compound scintillator for radiation detection and imaging applications. Light output and energy resolution measured for a crystal of volume 5×5×5 mm3 were 55,000±2000 ph/MeV and 5.6% at 662 keV respectively which is a significant improvement over previous reports. The hygroscopicity of the compound and the tendency of the scintillator crystals to degrade when exposed to the atmosphere necessitate the proper encapsulation of the crystals. It was observed that unlike other hygroscopic scintillator crystals CsSrBr3 undergoes a unique degradation while encapsulated in mineral oil. The light output of the crystal decreases over time, but there is no visually observed physical degradation of the crystal. This degradation is a reversible process wherein a degraded crystal can be subjected to annealing in vacuum in order to restore its original performance.

Recent Progress in Thallium Bromide Gamma-Ray Spectrometer Development

NASA Astrophysics Data System (ADS)

Kim, Hadong; Kargar, Alireza; Cirignano, Leonard; Churilov, Alexei; Ciampi, Guido; Higgins, William; Olschner, Fred; Shah, Kanai

2012-02-01

In recent years, progress in processing and crystal growth methods have led to a significant increase in the mobility-lifetime product of electrons in thallium bromide (TlBr). This has enabled single carrier collection devices with thickness greater than 1-cm to be fabricated. In this paper we report on our latest results from pixellated devices with depth correction as well as our initial results with Frisch collar devices. After applying depth corrections, energy resolution of approximately 2% (FWHM at 662 keV) was obtained from a 13-mm thick TlBr array operated at -18°C and under continuous bias and irradiation for more than one month. Energy resolution of 2.4% was obtained at room temperature with an 8.4-mm thick TlBr Frisch collar device.

A new spectroscopic imager for X-rays from 0.5 keV to 150 keV combining a pnCCD and a columnar CsI(Tl) scintillator

NASA Astrophysics Data System (ADS)

Schlosser, D. M.; Hartmann, R.; Kalok, D.; Bechteler, A.; Abboud, A.; Shokr, M.; Çonka, T.; Pietsch, U.; Strüder, L.

2017-04-01

By combining a low noise fully depleted pnCCD detector with a columnar CsI(Tl) scintillator an energy dispersive spatial resolving detector can be realized with a high quantum efficiency in the range from below 0.5 keV to above 150 keV. The used scintillator system increases the pulse height of gamma-rays converted in the CsI(Tl), due to focusing properties of the columnar scintillator structure by reducing the event size in indirect detection mode (conversion in the scintillator). In case of direct detection (conversion in the silicon of the pnCCD) the relative energy resolution is 0.7% at 122 keV (FWHM = 850 eV) and the spatial resolution is less than 75 μm. In case of indirect detection the relative energy resolution, integrated over all event sizes is about 9% at 122 keV with an expected spatial precision of below 75 μm.

ISIS/EPI-Lo: A New Instrument for Measuring keV to MeV Ions and Electrons with Simultaneous Half-Sky Coverage on NASA's Solar Probe Plus Mission

NASA Astrophysics Data System (ADS)

Hill, M. E.; Mitchell, D. G.; McNutt, R. L., Jr.; Cooper, S.; Crew, A. B.; Dupont, A.; Hayes, J.; Hoffer, E.; Nelson, K.; Parker, C.; Schlemm, C., II; Seifert, H.; Stokes, M.; Angold, N. G.; McComas, D. J.; Weidner, S.; Wiedenbeck, M. E.

2016-12-01

The Solar Probe Plus (SPP) Mission's Integrated Science Investigation of the Sun (ISIS) is a suite of two energetic particle instruments, EPI-Lo and EPI-Hi, covering lower ( 10 keV-100 MeV) and higher ( 1-100 MeV/nuc) energies, respectively. The ISIS team will investigate the origins, acceleration, and transport of energetic particles in the corona and inner heliosphere during the planned 7-year, 24-orbit mission, with a perihelion initially of 0.16 AU (36 Solar radii; RS), the three final orbits reaching 0.044 AU (9.9 RS). EPI-Lo has a novel approach to obtaining large angular coverage, well-suited to 3-axis stabilized spacecraft such as SPP, by densely sampling its 2π steradian field of view with 80 apertures organized in eight matching, 10-aperture wedges. Each wedge relies primarily on time-of-flight (TOF) mass spectrometer techniques, employing thin secondary-electron-emitting foils, microchannel plates, and solid state detectors (SSDs), to measure ions from 50 keV - 15 MeV and electrons from 50-500 keV. Signal attenuation, absorbers, TOF-only measurements, and SSD-only techniques are used to extend this energy range higher and lower. In 2015 and 2016 we made measurements with engineering units and flight-spare EPI-Lo wedges at accelerators and with radioactive sources; in addition to presenting the instrument design, we will report the results from these tests to characterize the instrument's measurement performance.

Second-Generation Design of Micro-Spec: A Medium-Resolution, Submillimeter-Wavelength Spectrometer-on-a-Chip

NASA Astrophysics Data System (ADS)

Cataldo, G.; Barrentine, E. M.; Bulcha, B. T.; Ehsan, N.; Hess, L. A.; Noroozian, O.; Stevenson, T. R.; U-Yen, K.; Wollack, E. J.; Moseley, S. H.

2018-04-01

Micro-Spec (µ-Spec) is a direct-detection spectrometer which integrates all the components of a diffraction-grating spectrometer onto a ˜ 10-cm^2 chip through the use of superconducting microstrip transmission lines on a single-crystal silicon substrate. A second-generation µ-Spec is being designed to operate with a spectral resolution of 512 in the submillimeter (500-1000 µm, 300-600 GHz) wavelength range, a band of interest for several spectroscopic applications in astrophysics. High-altitude balloon missions would provide the first test bed to demonstrate the µ-Spec technology in a space-like environment and would be an economically viable venue for multiple observation campaigns. This work reports on the current status of the instrument design and will provide a brief overview of each instrument subsystem. Particular emphasis will be given to the design of the spectrometer's two-dimensional diffractive region, through which the light of different wavelengths is focused on the detectors along the focal plane. An optimization process is employed to generate geometrical configurations of the diffractive region that satisfy specific requirements on spectrometer size, operating spectral range, and performance. An optical design optimized for balloon missions will be presented in terms of geometric layout, spectral purity, and efficiency.

An experimental and numerical study of the light scattering properties of ice crystals with black carbon inclusions

NASA Astrophysics Data System (ADS)

Arienti, Marco; Geier, Manfred; Yang, Xiaoyuan; Orcutt, John; Zenker, Jake; Brooks, Sarah D.

2018-05-01

We investigate the optical properties of ice crystals nucleated on atmospheric black carbon (BC). The parameters examined in this study are the shape of the ice crystal, the volume fraction of the BC inclusion, and its location inside the crystal. We report on new spectrometer measurements of forward scattering and backward polarization from ice crystals nucleated on BC particles and grown under laboratory-controlled conditions. Data from the Cloud and Aerosol Spectrometer with Polarization (CASPOL) are used for direct comparison with single-particle calculations of the scattering phase matrix. Geometrical optics and discrete dipole approximation techniques are jointly used to provide the best compromise of flexibility and accuracy over a broad range of size parameters. Together with the interpretation of the trends revealed by the CASPOL measurements, the numerical results confirm previous reports on absorption cross-section magnification in the visible light range. Even taking into account effects of crystal shape and inclusion position, the ratio between absorption cross-section of the compound particle and the absorption cross-section of the BC inclusion alone (the absorption magnification) has a lower bound of 1.5; this value increases to 1.7 if the inclusion is centered with respect to the crystal. The simple model of BC-ice particle presented here also offers new insights on the effect of the relative position of the BC inclusion with respect to the crystal's outer surfaces, the shape of the crystal, and its size.

The High-Resolution X-Ray Microcalorimeter Spectrometer, SXS, on Astro-H

NASA Technical Reports Server (NTRS)

Mitsuda, Kazuhisa; Kelley, Richard L.; Boyce, Kevin R.; Brown, Gregory V.; Costantini, Elisa; DiPirro, Michael J.; Ezoe, Yuichiro; Fujimoto, Ryuichi; Gendreau, Keith C.; denHerder, Jan-Willem;

Measurement of the mass attenuation coefficient from 81 keV to 1333 keV for elemental materials Al, Cu and Pb

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gjorgieva, Slavica, E-mail: slavicagjorgieva89@gmail.com; Institute of Physics, Faculty of Natural Sciences and Mathematics, Ss Cyril and Methodius University, POB 162, 1000 Skopje; Barandovski, Lambe, E-mail: lambe@pmf.ukim.mk

The mass attenuation coefficients (μ/ρ) for 3 high purity elemental materials Al, Cu and Pb were measured in the γ-ray energy range from 81 keV up to 1333 keV using {sup 22}Na, {sup 60}Co {sup 133}Ba and {sup 133}Cs as sources of gamma radiation. Well shielded detector (NaI (Tl) semiconductor detector) was used to measure the intensity of the transmitted beam. The measurements were made under condition of good geometry, assuring that any photon absorbed or deflected appreciably does not reach the detector. The measured values are compared with the theoretical ones obtained by Seltzer (1993).

Exploring growth conditions and Eu2+ concentration effects for KSr2I5:Eu scintillator crystals II: Ø 25 mm crystals

NASA Astrophysics Data System (ADS)

Stand, L.; Zhuravleva, M.; Johnson, J.; Koschan, M.; Wu, Y.; Donnald, S.; Vaigneur, K.; Lukosi, E.; Melcher, C. L.

2018-02-01

Europium doped potassium strontium iodide is a very promising scintillator for national security applications due to its ease of growth and excellent scintillation properties. For this work the fast crystal growth and scintillation properties of 1-inch diameter single crystals of KSr2I5:Eu2+ (KSI:Eu) were investigated. We focused our efforts on optimizing the growth parameters required to produce one-inch diameter crystals without decreasing the previously reported fast pulling rate of 5 mm/h. Cracking was minimized by replacing the quartz ampoules with carbon coated quartz ampoules; thus, several crack free single crystals of KSI with varying Eu2+ concentrations were grown, including a Ø 1″ by 6″ long boule with 2.5% Eu. The maximum achievable performance of each crystal was measured using small 0.012 cm3 specimens. The volumetric dependencies of the light yield, energy resolution and decay time were evaluated using KSI:Eu 2% specimens with volumes ranging from 0.012 cm3 to 18 cm3. For large volumes (≥ 9 cm3), the performance was comparable to other high performing scintillators, with light yields up to 78,200 ph/MeV and energy resolutions as good as 3.2% at 662 keV. The initial version of a hermetic package has been developed, and the stability of the sealed crystal is promising.

Ice crystals classification using airborne measurements in mixing phase

NASA Astrophysics Data System (ADS)

Sorin Vajaiac, Nicolae; Boscornea, Andreea

2017-04-01

This paper presents a case study of ice crystals classification from airborne measurements in mixed-phase clouds. Ice crystal shadow is recorded with CIP (Cloud Imaging Probe) component of CAPS (Cloud, Aerosol, and Precipitation Spectrometer) system. The analyzed flight was performed in the south-western part of Romania (between Pietrosani, Ramnicu Valcea, Craiova and Targu Jiu), with a Beechcraft C90 GTX which was specially equipped with a CAPS system. The temperature, during the fly, reached the lowest value at -35 °C. These low temperatures allow the formation of ice crystals and influence their form. For the here presented ice crystals classification a special software, OASIS (Optical Array Shadow Imaging Software), developed by DMT (Droplet Measurement Technologies), was used. The obtained results, as expected are influenced by the atmospheric and microphysical parameters. The particles recorded where classified in four groups: edge, irregular, round and small.

Characterization studies of silicon photomultipliers and crystals matrices for a novel time of flight PET detector

NASA Astrophysics Data System (ADS)

Auffray, E.; Ben Mimoun Bel Hadj, F.; Cortinovis, D.; Doroud, K.; Garutti, E.; Lecoq, P.; Liu, Z.; Martinez, R.; Paganoni, M.; Pizzichemi, M.; Silenzi, A.; Xu, C.; Zvolský, M.

2015-06-01

This paper describes the characterization of crystal matrices and silicon photomultiplier arrays for a novel Positron Emission Tomography (PET) detector, namely the external plate of the EndoTOFPET-US system. The EndoTOFPET-US collaboration aims to integrate Time-Of-Flight PET with ultrasound endoscopy in a novel multimodal device, capable to support the development of new biomarkers for prostate and pancreatic tumors. The detector consists in two parts: a PET head mounted on an ultrasound probe and an external PET plate. The challenging goal of 1 mm spatial resolution for the PET image requires a detector with small crystal size, and therefore high channel density: 4096 LYSO crystals individually readout by Silicon Photomultipliers (SiPM) make up the external plate. The quality and properties of these components must be assessed before the assembly. The dark count rate, gain, breakdown voltage and correlated noise of the SiPMs are measured, while the LYSO crystals are evaluated in terms of light yield and energy resolution. In order to effectively reduce the noise in the PET image, high time resolution for the gamma detection is mandatory. The Coincidence Time Resolution (CTR) of all the SiPMs assembled with crystals is measured, and results show a value close to the demanding goal of 200 ps FWHM. The light output is evaluated for every channel for a preliminary detector calibration, showing an average of about 1800 pixels fired on the SiPM for a 511 keV interaction. Finally, the average energy resolution at 511 keV is about 13 %, enough for effective Compton rejection.

Balloon Borne Ultraviolet Spectrometer.

DTIC Science & Technology

1978-12-28

n.c.aaary ond lden lfy by block numb.r) ultraviolet ground support equipment (GSE) spectrometers flight electronics instrumentation balloons \\ solar ...Assembly 4 Fig. 3 Solar Balloon Experiment Ass ’y 7 Fig. 4 Mechanical Interface , UV Spectrometer 8 Fig . 5 Spectrometer Body Assemb ly 10 Fig. 6...Diagram, GSE )bnitor 48 Selector and Battery Charger Fig. 25 Schematic Diagram, GSE Serial to 49 Parallel Data Converter Fig. 26 Schematic Diagram

High-resolution measurements of the DT neutron spectrum using new CD foils in the Magnetic Recoil neutron Spectrometer (MRS) on the National Ignition Facility

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gatu Johnson, M., E-mail: gatu@psfc.mit.edu; Frenje, J. A.; Li, C. K.

2016-11-15

The Magnetic Recoil neutron Spectrometer (MRS) on the National Ignition Facility measures the DT neutron spectrum from cryogenically layered inertial confinement fusion implosions. Yield, areal density, apparent ion temperature, and directional fluid flow are inferred from the MRS data. This paper describes recent advances in MRS measurements of the primary peak using new, thinner, reduced-area deuterated plastic (CD) conversion foils. The new foils allow operation of MRS at yields 2 orders of magnitude higher than previously possible, at a resolution down to ∼200 keV FWHM.

High-resolution measurements of the DT neutron spectrum using new CD foils in the Magnetic Recoil neutron Spectrometer (MRS) on the National Ignition Facility

DOE PAGES

Gatu Johnson, M.; Frenje, J. A.; Bionta, R. M.; ...

2016-08-09

The Magnetic Recoil neutron Spectrometer (MRS) on the National Ignition Facility measures the DT neutron spectrum from cryogenically layered inertial confinement fusion implosions. Yield, areal density, apparent ion temperature, and directional fluid flow are inferred from the MRS data. Here, this paper describes recent advances in MRS measurements of the primary peak using new, thinner, reduced-area deuterated plastic (CD) conversion foils. The new foils allow operation of MRS at yields 2 orders of magnitude higher than previously possible, at a resolution down to ~200 keV FWHM.

High-resolution measurements of the DT neutron spectrum using new CD foils in the Magnetic Recoil neutron Spectrometer (MRS) on the National Ignition Facility.

PubMed

Gatu Johnson, M; Frenje, J A; Bionta, R M; Casey, D T; Eckart, M J; Farrell, M P; Grim, G P; Hartouni, E P; Hatarik, R; Hoppe, M; Kilkenny, J D; Li, C K; Petrasso, R D; Reynolds, H G; Sayre, D B; Schoff, M E; Séguin, F H; Skulina, K; Yeamans, C B

2016-11-01

The Magnetic Recoil neutron Spectrometer (MRS) on the National Ignition Facility measures the DT neutron spectrum from cryogenically layered inertial confinement fusion implosions. Yield, areal density, apparent ion temperature, and directional fluid flow are inferred from the MRS data. This paper describes recent advances in MRS measurements of the primary peak using new, thinner, reduced-area deuterated plastic (CD) conversion foils. The new foils allow operation of MRS at yields 2 orders of magnitude higher than previously possible, at a resolution down to ∼200 keV FWHM.

Teflon impregnated anatase TiO2 nanoparticles irradiated by 80 keV Xe+ ions

NASA Astrophysics Data System (ADS)

Khanam, Rizwin; Paul, Nibedita; Kumar, P.; Kanjilal, D.; Ahmed, Gazi A.; Mohanta, Dambarudhar

2014-10-01

We report the effect of 80 keV Xe+ ion irradiation on the morphological and optical responses of TiO2 nanoparticles spread over commercially available polytetrafluoroethylene (PTFE, Teflon). These nanoparticles were synthesized via a convenient, sol-gel approach with titanium isopropoxide as the main precursor. From X-ray diffraction (XRD) studies we found that, the nanoparticles crystallize in anatase phase and with a preferential orientation of crystallites along (1 0 1) plane. Upon irradiation at a fluence of 1.25 × 1017 ions/cm2, the nanoparticle dimension was found to increase from a value of ∼9 nm to ∼20-30 nm. Essentially, particle growth is predicted as a consequence of swelling behavior accompanied by the formation of Xe van der Waal crystals in isolated regions of nano-titania. Evidence of nanoripples was also witnessed on the surface of the irradiated nano-titania. The morphological evolution was assessed both by atomic force and transmission electron microscopies (AFM and TEM) independently. From the UV-Vis optical absorption studies, the estimated optical band gap was found to drop with increasing fluence, while refractive index exhibited a remarkable improvement. Photoluminescence (PL) studies have revealed that, the band edge emission and those due to the self trapped excitons (STE) and other oxygen vacancy related ones were manifested considerably as a result of Xe ion irradiation.

Development of a High Resolution X-Ray Spectrometer for the National Ignition Facility (NIF)

NASA Astrophysics Data System (ADS)

Hill, K. W.; Bitter, M.; Delgado-Aparicio, L.; Efthimion, P. C.; Ellis, R.; Gao, L.; Maddox, J.; Pablant, N. A.; Schneider, M. B.; Chen, H.; Ayers, S.; Kauffman, R. L.; Macphee, A. G.; Beiersdorfer, P.; Ma, T.; Nora, R. C.; Scott, H. A.; Thorn, D. B.; Kilkenny, J. D.; Nelson, D.; Shoup, M., III; Maron, Y.

2016-10-01

A high resolution (E/ ΔE 2000) Bragg crystal x-ray spectrometer is being developed to measure plasma parameters in NIF experiments. The instrument will be a positioner insertable cassette designed to infer electron density in compressed capsules from Stark broadening of the helium- β (1s2-1s3p) lines of krypton, and electron temperature from the relative intensities of dielectronic satellites. Two conically shaped crystals will diffract and sagittally focus (1) the Kr He β complex and (2) the He α and Ly α complexes onto a streak camera photocathode for time resolved measurement. A third cylindrical crystal will focus the full He α to He β spectrum onto an image plate for a time integrated calibration spectrum. Performance estimates and design status will be presented. Performed under the auspices of the US DOE by PPPL under contract DE-AC02-09CH11466 and by LLNL under contract DE-AC52-07NA27344.

Ion irradiation-induced crystal structure changes in inverse spinel MgIn 2O 4

DOE PAGES

Tang, Ming; Valdez, James A.; Wang, Yongqiang; ...

2016-07-29

We performed 400 keV Ne and 200 keV He ion irradiations on fully inverse MgIn 2O 4 samples at cryogenic temperature (~ 77 K), in order to examine the influence of radiation-induced cation disordering on crystal structure. In the case of MgIn 2O 4 samples irradiated with Ne ions to a peak displacement damage dose of 4 displacements per atom (dpa), a spinel-to-rocksalt phase transformation was observed. Conversely, for MgIn 2O 4 samples irradiated with He ions to a peak displacement damage dose of 5 dpa, the only observed structural effect involved cation rearrangements from an inverse to a “random”more » spinel structure.« less

The CubeSat Imaging X-ray Solar Spectrometer (CubIXSS) Mission Concept

NASA Astrophysics Data System (ADS)

Caspi, Amir; Shih, Albert Y.; Warren, Harry; DeForest, Craig; Laurent, Glenn Thomas; Schwartz, Richard A.; Woods, Thomas N.; Mason, James; Palo, Scott; Steslicki, Marek; Sylwester, Janusz; Gburek, Szymon; Mrozek, Tomasz; Kowalinski, Miroslaw; Torre, Gabriele; Crowley, Geoffrey; Schattenburg, Mark

2017-08-01

Solar soft X-ray (SXR) observations provide important diagnostics of plasma heating, during solar flares and quiescent times. Spectrally- and temporally-resolved measurements are crucial for understanding the dynamics, origins, and evolution of these energetic processes, providing probes both into the temperature distributions and elemental compositions of hot plasmas; spatially-resolved measurements are critical for understanding energy transport and mass flow. A better understanding of the thermal plasma improves our understanding of the relationships between particle acceleration, plasma heating, and the underlying release of magnetic energy during reconnection. We introduce a new proposed small satellite mission, the CubeSat Imaging X-ray Solar Spectrometer (CubIXSS), to measure spectrally- and spatially-resolved SXRs from the quiescent and flaring Sun from a 6U CubeSat platform in low-Earth orbit during a nominal 1-year mission. CubIXSS includes the Amptek X123-FastSDD silicon drift detector, a low-noise, commercial off-the-shelf (COTS) instrument enabling solar SXR spectroscopy from ~0.5 to ~30 keV with ~0.15 keV FWHM spectral resolution with low power, mass, and volume requirements. Multiple detectors and tailored apertures provide sensitivity to a wide range of solar conditions, optimized for a launch during solar minimum. The precise spectra from these instruments will provide detailed measurements of the coronal temperature distribution and elemental abundances from the quiet Sun to active regions and flares. CubIXSS also includes a novel spectro-spatial imager -- the first ever solar imager on a CubeSat -- utilizing a custom pinhole camera and Chandra-heritage X-ray transmission diffraction grating to provide spatially- resolved, full-Sun imaging spectroscopy from ~0.1 to ~10 keV, with ~25 arcsec and ~0.1 Å FWHM spatial and spectral resolutions, respectively. MOXSI’s unique capabilities enable SXR spectroscopy and temperature diagnostics of individual

Crystal growth and analysis of ohmic contact and magneto-optical isolator properties of cadmium manganese telluride

NASA Astrophysics Data System (ADS)

Prakasam, Mythili; Viraphong, Oudomsack; Teulé-Gay, Lionel; Decourt, Rodolphe; Veber, Philippe; Víllora, Encarnación G.; Shimamura, Kiyoshi

2011-03-01

Cd1-xMnxTe (x=0.1, 0.3, 0.5, 0.7 and 0.9) (CMT) single crystals were grown by the vertical Bridgman method. The optical studies reveal that with the increase in Mn concentration, the band gap values increase, which is attributed to s, p-d exchange interaction between the band carriers and Mn ions. Faraday rotation angle of the grown CMT (x=0.5) crystals were measured at the following wavelengths: 825, 1060 and 1575 nm. It was inferred that CMT exhibit larger Faraday effect (3-6 times larger than terbium-gallium garnet (TGG) currently used for optical isolators) making it as an efficient material for optical isolator at longer wavelengths. Field-cooled and zero field-cooled magnetizations of CMT were measured as a function of temperature and magnetic field. The spin-glass like behavior of CMT and their tendency to decrease in magnitude with increasing Mn concentration have been analyzed. The metal contacts on the Cd1-xMnxTe (x=0.1, 0.5, 0.7 and 0.9) crystals have been made with various metals and metal alloys to establish the ohmic contact. The detector characteristics of CMT have been tested using γ-rays with 511 keV (22 Na) and 59.5 keV (241 Am).

The production and sputtering of S2 by keV ion bombardment

NASA Technical Reports Server (NTRS)

Boring, J. W.; Chrisey, D. B.; Oshaughnessy, D. J.; Phipps, J. A.; Zhao, N.

1986-01-01

The ion bombardment of S-containing molecules in comets is simulated experimentally. Mass-analyzed 30-keV beams of Ar(+) and He(+) are directed at solid S, H2S, and CS2 targets at temperatures 15 K, and the neutral molecular species produced are ionized and analyzed using a quadrupole mass spectrometer. The dominant species detected are S1 and S2 for the S target, H2S and S2 for the H2S target, and S, CS, S2, and CS2 for the CS2 target. In the latter case, it is found that after about 10 to the 14th He(+) ions/sq cm have struck the target, further sputtering is prevented by formation of a dark brown deposit which is stable at room temperature; the residue forms more slowly when Ar(+) ions are used. These results, indicating relatively efficient S2 production by ion bombardment, are applied to theoretical models of S2 production and/or ejection by solar-wind, solar-flare, or cosmic-ray ions striking comets. It is found that direct solar-wind production of S2 by sputtering is unlikely at realistic bombardment rates, but that H2S-S2 conversion by energetic ions could be significant, with less stringent ice-temperature and irradiation-flux constraints than in the case of S2 production by photons.

Multilayer diffraction at 104 keV

NASA Technical Reports Server (NTRS)

Krieger, Allen S.; Blake, Richard L.; Siddons, D. P.

1993-01-01

We have measured the diffraction peak of a W:Si synthetic multilayer reflector at 104 keV using the High Energy Bonse-Hart Camera at the X-17B hard X-ray wiggler beam line of the National Synchrotron Light Source at Brookhaven National Laboratory. The characteristics of the diffraction peak are described and compared to theory.

Neutral Kaon Spectrometer 2

NASA Astrophysics Data System (ADS)

Kaneta, M.; Beckford, B.; Fujii, T.; Fujii, Y.; Futatsukawa, K.; Han, Y. C.; Hashimoto, O.; Hirose, K.; Ishikawa, T.; Kanda, H.; Kimura, C.; Maeda, K.; Nakamura, S. N.; Suzuki, K.; Tsukada, K.; Yamamoto, F.; Yamazaki, H.

2018-04-01

A large-acceptance spectrometer, Neutral Kaon Spectrometer 2 (NKS2), was newly constructed to explore various photoproduction reactions in the gigaelectronvolt region at the Laboratory of Nuclear Science (LNS, currently ELPH), Tohoku University. The spectrometer consisted of a dipole magnet, drift chambers, and plastic scintillation counters. NKS2 was designed to separate pions and protons in a momentum range of less than 1 GeV/ c, and was placed in a tagged photon beamline. A cryogenic H2/D2 target fitted to the spectrometer were designed. The design and performance of the detectors are described. The results of the NKS2 experiment on analyzing strangeness photoproduction data using a 0.8-1.1 GeV tagged photon beam are also presented.

Fourier Transform Spectrometer System

NASA Technical Reports Server (NTRS)

Campbell, Joel F. (Inventor)

2014-01-01

A Fourier transform spectrometer (FTS) data acquisition system includes an FTS spectrometer that receives a spectral signal and a laser signal. The system further includes a wideband detector, which is in communication with the FTS spectrometer and receives the spectral signal and laser signal from the FTS spectrometer. The wideband detector produces a composite signal comprising the laser signal and the spectral signal. The system further comprises a converter in communication with the wideband detector to receive and digitize the composite signal. The system further includes a signal processing unit that receives the composite signal from the converter. The signal processing unit further filters the laser signal and the spectral signal from the composite signal and demodulates the laser signal, to produce velocity corrected spectral data.

The RITA spectrometer at Risø - design considerations and recent results

NASA Astrophysics Data System (ADS)

Clausen, K. N.; McMorrow, D. F.; Lefmann, K.; Aeppli, G.; Mason, T. E.; Schröder, A.; Issikii, M.; Nohara, M.; Takagi, H.

In the new cold triple axis spectrometer RITA at Risø we have improved the front end by extensive use of state of the art optical elements and better shielding material. The analyser system is situated in one large open tank and consists of seven individually orientable PG(002) crystal analyser blades, and a 170 mm by 120 mm 2 areas sensitive micro-strip detector. In comparison to the old TAS6 spectrometer we have obtained a factor 2-5 gain in intensity on the sample, a substantially lower background, much more flexibility for optimising the instrument and the possibility to go beyond simple point-by-point inspection. The excellent performance of RITA in the standard TAS mode is exemplified by a study of the dynamics of ≈ 15 nm hematite (α-Fe 2O 3) nano-particles, and utilisation of horizontal and vertical focusing modes to study two dimensional systems is illustrated by a study of the spin fluctuations in the high Tc superconductor La 1.83Sr 0.17CuO 4.

History and current status of strontium iodide scintillators

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cherepy, Nerine J.; Beck, Patrick R.; Payne, Stephen A.

Eu-doped strontium iodide single crystal growth has reached maturity and prototype SrI 2(Eu)-based gamma ray spectrometers provide detection performance advantages over standard detectors. SrI 2(Eu) offers a high, proportional light yield of >80,000 photons/MeV. Energy resolution of <3% at 662 keV with 1.5” x 1.5” SrI2(Eu) crystals is routinely achieved, by employing either a small taper at the top of the crystal or a digital readout technique. These methods overcome light-trapping, in which scintillation light is re-absorbed and re-emitted in Eu 2+-doped crystals. As a result, its excellent energy resolution, lack of intrinsic radioactivity or toxicity, and commercial availability makemore » SrI 2(Eu) the ideal scintillator for use in handheld radioisotope identification devices. A 6-lb SrI 2(Eu) radioisotope identifier is described.« less

History and current status of strontium iodide scintillators

DOE PAGES

Cherepy, Nerine J.; Beck, Patrick R.; Payne, Stephen A.; ...

2017-09-15

Eu-doped strontium iodide single crystal growth has reached maturity and prototype SrI 2(Eu)-based gamma ray spectrometers provide detection performance advantages over standard detectors. SrI 2(Eu) offers a high, proportional light yield of >80,000 photons/MeV. Energy resolution of <3% at 662 keV with 1.5” x 1.5” SrI2(Eu) crystals is routinely achieved, by employing either a small taper at the top of the crystal or a digital readout technique. These methods overcome light-trapping, in which scintillation light is re-absorbed and re-emitted in Eu 2+-doped crystals. As a result, its excellent energy resolution, lack of intrinsic radioactivity or toxicity, and commercial availability makemore » SrI 2(Eu) the ideal scintillator for use in handheld radioisotope identification devices. A 6-lb SrI 2(Eu) radioisotope identifier is described.« less

Lunar orbital mass spectrometer experiment

NASA Technical Reports Server (NTRS)

Lord, W. P.

1971-01-01

The design, development, manufacture, test and calibration of five lunar orbital mass spectrometers with the four associated ground support equipment test sets are discussed. A mass spectrometer was installed in the Apollo 15 and one in the Apollo 16 Scientific Instrument Module within the Service Module. The Apollo 15 mass spectrometer was operated with collection of 38 hours of mass spectra data during lunar orbit and 50 hours of data were collected during transearth coast. The Apollo 16 mass spectrometer was operated with collection of 76 hours of mass spectra data during lunar orbit. However, the Apollo 16 mass spectrometer was ejected into lunar orbit upon malfunction of spacecraft boom system just prior to transearth insection and no transearth coast data was possible.

Solar neutrino flux at keV energies

NASA Astrophysics Data System (ADS)

Vitagliano, Edoardo; Redondo, Javier; Raffelt, Georg

2017-12-01

We calculate the solar neutrino and antineutrino flux in the keV energy range. The dominant thermal source processes are photo production (γ e→ e νbar nu), bremsstrahlung (e+Ze→ Ze+e+νbar nu), plasmon decay (γ→νbar nu), and νbar nu emission in free-bound and bound-bound transitions of partially ionized elements heavier than hydrogen and helium. These latter processes dominate in the energy range of a few keV and thus carry information about the solar metallicity. To calculate their rate we use libraries of monochromatic photon radiative opacities in analogy to a previous calculation of solar axion emission. Our overall flux spectrum and many details differ significantly from previous works. While this low-energy flux is not measurable with present-day technology, it could become a significant background for future direct searches for keV-mass sterile neutrino dark matter.

Development of high resolution x-ray spectrometers for the investigation of bioinorganic chemistry in metalloproteins

NASA Astrophysics Data System (ADS)

Drury, Owen Byron

We have built an X-ray spectrometer for synchrotron-based high-resolution soft X-ray spectroscopy. The spectrometer uses four 9-pixel arrays of superconducting tunnel junctions (STJs) as sensors. They infer the energy of an absorbed X-ray from a temporary increase in tunneling current. The STJs are operated in a two-stage adiabatic demagnetization refrigerator (ADR) that uses liquid nitrogen and helium for precooling to 77 K and 4.2 K, and gallium gadolinium garnet and iron ammonium sulfate to attain a base temperature below 0.1 K. The sensors are held at the end of a 40-cm-long cold finger within ˜1 cm of a sample located inside the vacuum chamber of a synchrotron beam line end station. The spectrometer has an energy resolution between 10 eV and 20 eV FWHM below 1 keV, can be operated at rates up to ˜106 counts/s. STJ spectrometers are suited for chemical analysis of dilute samples by fluorescence-detected X-ray absorption spectroscopy (XAS) in cases where conventional germanium detectors do not have enough energy resolution. We have used this STJ spectrometer at the Advanced Light Source synchrotron for spectroscopy on the lower energy X-ray absorption edges of the elements Mo, S, Fe and N. These elements play an important role in biological nitrogen fixation at the metalloprotein nitrogenase, and we have examined if STJ spectrometers can be used to provide new insights into some of the open questions regarding the reaction mechanism of this protein. We have taken X-ray absorption near-edge spectra (XANES) and extended fine structure spectra (EXAFS) of an Fe 6N(CO)15-compound containing a single N atom inside a cluster of six Fe atoms, as postulated to exist inside the Fe-S cluster of the FeMo-cofactor (FeMo-co) in nitrogenase. The STJ detector has enabled the first-ever extended range EXAFS scans on nitrogen through the oxygen K-edge, enabling a comparison with N EXAFS on FeMo-co. We have taken iron L23-edge spectra of the Fe-S cluster in FeMo-co, which can be

Tropospheric and Airborne Emission Spectrometers

NASA Technical Reports Server (NTRS)

Glavich, Thomas; Beer, Reinhard

1996-01-01

X This paper describes the development of two related instruments, the Tropospheric Emission Spectrometer (TES) and the Airborne Emission Spectrometer (AES). Both instruments are infrared imaging Fourier Transform Spectrometers, used for measuring the state of the lower atmosphere, and in particular the measurement of ozone and ozone sources and sinks.

Nondestructive determination of radionuclides in lunar samples using a large low-background gamma-ray spectrometer and a novel application of least-squares fitting

NASA Technical Reports Server (NTRS)

Eldridge, J. S.; Okelly, G. D.; Northcutt, K. J.; Schonfeld, E.

1972-01-01

Dual-parameter gamma ray spectrometer systems with large volume Nal (Tl) crystals and low backgrounds were used for nondestructive determination of K, Th, U and cosmic ray produced radionuclides in 60 lunar samples. The total weight of samples measured with this system is 28 kg, and the individual sample weights varied from 2 to 2300 g. Samples from Apollo 11, 12, 14, 15 and 16 were measured. Operation of the spectrometers in the coincidence mode and analyzing single coincidence spectra permits the simultaneous determination of 8-10 radionuclides in each lunar sample.

Electronics for a Spectrometer

NASA Image and Video Library

2014-01-24

NASA has provided part of the electronics package for an instrument called the Double Focusing Mass Spectrometer, which is part of the Swiss-built Rosetta Orbiter Spectrometer for Ion and Neutral Analysis ROSINA instrument.

Single crystal CVD diamond membranes as Position Sensitive X-ray Detector

NASA Astrophysics Data System (ADS)

Desjardins, K.; Menneglier, C.; Pomorski, M.

2017-12-01

Transparent X-ray Beam Position Monitor (XBPM) has been specifically developed for low energy X-ray beamlines (1.4 keV < E < 5 keV) allowing to transmit more than 80% of 2 keV energy beam. The detector is based on a free-standing single crystal CVD diamond membrane of 4 μm thickness with position-sensitive DLC (Diamond-Like Carbon) resistive electrodes in duo-lateral configuration. The measured X-ray beam induced current (XBIC) due to the interaction of X-rays with diamond membrane allows precise monitoring of the absolute beam flux and the beam position (by the reconstruction of its center-of-gravity) at beam transmissions reaching 95%. This detector has been installed at SOLEIL synchrotron on the SIRIUS beamline monochromator output and it has shown charge collection efficiency (CCE) reaching 100% with no lag-effects and excellent beam intensity sensitivity monitoring. X-ray beam mapping of the detector showed an XBIC response inhomogeneity of less than 10% across the membrane, corresponding mainly to the measured variation of the diamond plate thickness. The measured beam position resolution is at sub-micron level depending on the beam flux and the readout electronics bandwidth.

On-chip spectroscopy with thermally tuned high-Q photonic crystal cavities

DOE Office of Scientific and Technical Information (OSTI.GOV)

Liapis, Andreas C., E-mail: andreas.liapis@gmail.com; Gao, Boshen; Siddiqui, Mahmudur R.

2016-01-11

Spectroscopic methods are a sensitive way to determine the chemical composition of potentially hazardous materials. Here, we demonstrate that thermally tuned high-Q photonic crystal cavities can be used as a compact high-resolution on-chip spectrometer. We have used such a chip-scale spectrometer to measure the absorption spectra of both acetylene and hydrogen cyanide in the 1550 nm spectral band and show that we can discriminate between the two chemical species even though the two materials have spectral features in the same spectral region. Our results pave the way for the development of chip-size chemical sensors that can detect toxic substances.

Spent Fuel Assay with an Ultra-High Rate HPGe Spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Fast, James; Fulsom, Bryan; Pitts, Karl

2015-07-01

Traditional verification of spent nuclear fuel (SNF) includes determination of initial enrichment, burnup and cool down time (IE, BU, CT). Along with neutron measurements, passive gamma assay provides important information for determining BU and CT. Other gamma-ray-based assay methods such as passive tomography and active delayed gamma offer the potential to measure the spatial distribution of fission products and the fissile isotopic concentration of the fuel, respectively. All fuel verification methods involving gamma-ray spectroscopy require that the spectrometers manage very high count rates while extracting the signatures of interest. PNNL has developed new digital filtering and analysis techniques to producemore » an ultra-high rate gamma-ray spectrometer from a standard coaxial high-purity germanium (HPGe) crystal. This 37% relative efficiency detector has been operated for SNF measurements at input count rates of 500-1300 kcps and throughput in excess of 150 kcps. Optimized filtering algorithms preserve the spectroscopic capability of the system even at these high rates. This paper will present the results of both passive and active SNF measurement performed with this system at PNNL. (authors)« less

Second generation crystals for Laue lens applications

NASA Astrophysics Data System (ADS)

Barrière, N.; von Ballmoos, P.; Bastie, P.; Courtois, P.; Abrosimov, N. V.; Andersen, K.; Halloin, H.; Skinner, G.; Smither, R. K.

2006-06-01

A Laue lens gamma-ray telescope represents an exciting concept for a future high-energy mission. The feasibility of such a lens has been demonstrated by the CLAIRE lens prototype; since then various mission concepts featuring a Laue lens are being developed. The latest, which is also the most ambitious, is the European Gamma-Ray Imager (GRI). However, advancing from the CLAIRE prototype to a scientifically exploitable Laue lens requires still substantial research and development. First and foremost, diffracting elements (crystals) that constitute the Laue lens have to be optimized to offer the best efficiency and imaging capabilities for the resulting telescope. The characteristics of selected candidate crystals were measured at the European Synchrotron Radiation Facility on the high-energy beamline ID 15A using a beam tuned at 292 keV. The studied low mosaicity copper crystals have shown absolute reflectivity reaching 30%. These crystals are promising for the realization of a Laue lens, despite the fact that they produce a diffracted beam featuring a Gaussian intensity profile, which contributes to the spread of the focal spot. A composition gradient Si 1-x-Ge x crystal has been investigated as well, which showed a diffraction efficiency reaching 50% (disregarding absorption) - half of the theoretical maximum - that represents an absolute reflectivity around 39 %, the best that we measured at this energy to date. This gradient crystal also showed a square-shaped rocking curve that is almost the best case to minimize the spread of the focal spot. We also show that bending a gradient crystal could still enhance the focusing. Thanks to the better focusing, a factor of 2 in sensitivity improvement may be achieved.

Synthesis, crystal growth and characterization of bioactive material: 2- Amino-1H-benzimidazolium pyridine-3-carboxylate single crystal- a proton transfer molecular complex

NASA Astrophysics Data System (ADS)

Fathima, K. Saiadali; Kavitha, P.; Anitha, K.

2017-09-01

The 1:1 molecular adducts 2- Amino-1H-benzimidazolium pyridine-3-carboxylate (2ABPC) was synthesized and grown as single crystal where 2-aminobenzimidazole (ABI) acts as a donor and nicotinic acid (NA) acts as an acceptor. The presence of proton and carbon were predicted using 1H and 13C NMR spectral analysis. The molecular structure of the crystal was elucidated by subjecting the grown crystals to the single crystal x-ray diffraction analysis and was refined by full matrix least-squares method to R = 0.038 for 2469 reflections. The vibrational modes of functional group have been studied using FTIR and Raman spectroscopic analysis. The UV-Vis spectrum exhibited a visible band at 246 nm for 2ABPC due to the nicotinate anion of the molecule. Further, the antimicrobial activity of 2ABPC complex against B. subtilis, klebsiella pneumonia, Pseudomonas eruginos and E. coli pathogens was investigated. Minimum Inhibitory Concentration (MIC) for this crystal was obtained using UV spectrometer against MRSA pathogen. It was found that the benzimidazole with aminogroup at position 2 increases the general antimicrobial activities of 2ABPC crystal.

Future Development Trajectories for Imaging X-rays Spectrometers Based on Microcalorimeters

NASA Technical Reports Server (NTRS)

Kilbourne, Caroline A.; Bandler, Simon R.

2013-01-01

Future development trajectories for imaging x-ray spectrometers based on microcalorimeters. Since their invention 30 years ago, the capability of X-ray microcalorimeters has increased steadily, with continual improvements in energy resolution, speed, and array size. Arrays of up to 1024 pixels have been produced, and resolution better than 1 eV at 1.5 keV has been achieved. These detectors can be optimized for the highest priority science, such as designing for the highest resolving power at low energies at the expense of dynamic range, or the greatest focal-plane coverage at the expense of speed. Three types of X-ray microcalorimeters presently dominate the field, each characterized by the thermometer technology. The first two types use temperature-sensitive resistors: semiconductors in the metal-insulator transition and superconductors operated in the superconducting-normal transition. The third type uses a magnetically coupled thermometer, and is at an earlier stage of development than the other two. The Soft X-ray Spectrometer (SXS) on Astro-H, expected to launch in 2015, will use an array of silicon thermistors with HgTe X-ray absorbers that will operate at 50 mK. Both the semiconductor and superconductor calorimeters have been implemented in small arrays. Kilopixel arrays of the superconducting calorimeters are being produced, and much larger arrays may require the non-dissipative advantage of magnetically coupled thermometers. I will project the development trajectories of these detectors and their read-out technologies and assess what their capabilities and limitations will be 10 - 20 years from now.

Regolith X-Ray Imaging Spectrometer (REXIS) Aboard the OSIRIS-REx Asteroid Sample Return Mission

NASA Astrophysics Data System (ADS)

Masterson, R. A.; Chodas, M.; Bayley, L.; Allen, B.; Hong, J.; Biswas, P.; McMenamin, C.; Stout, K.; Bokhour, E.; Bralower, H.; Carte, D.; Chen, S.; Jones, M.; Kissel, S.; Schmidt, F.; Smith, M.; Sondecker, G.; Lim, L. F.; Lauretta, D. S.; Grindlay, J. E.; Binzel, R. P.

2018-02-01

The Regolith X-ray Imaging Spectrometer (REXIS) is the student collaboration experiment proposed and built by an MIT-Harvard team, launched aboard NASA's OSIRIS-REx asteroid sample return mission. REXIS complements the scientific investigations of other OSIRIS-REx instruments by determining the relative abundances of key elements present on the asteroid's surface by measuring the X-ray fluorescence spectrum (stimulated by the natural solar X-ray flux) over the range of energies 0.5 to 7 keV. REXIS consists of two components: a main imaging spectrometer with a coded aperture mask and a separate solar X-ray monitor to account for the Sun's variability. In addition to element abundance ratios (relative to Si) pinpointing the asteroid's most likely meteorite association, REXIS also maps elemental abundance variability across the asteroid's surface using the asteroid's rotation as well as the spacecraft's orbital motion. Image reconstruction at the highest resolution is facilitated by the coded aperture mask. Through this operation, REXIS will be the first application of X-ray coded aperture imaging to planetary surface mapping, making this student-built instrument a pathfinder toward future planetary exploration. To date, 60 students at the undergraduate and graduate levels have been involved with the REXIS project, with the hands-on experience translating to a dozen Master's and Ph.D. theses and other student publications.

Barium iodide and strontium iodide crystals and scintillators implementing the same

DOEpatents

Payne, Stephen A.; Cherepy, Nerine J.; Hull, Giulia E.; Drobshoff, Alexander D.; Burger, Arnold

2016-11-29

In one embodiment, a material comprises a crystal comprising strontium iodide providing at least 50,000 photons per MeV, where the strontium iodide material is characterized by a volume not less than 1 cm.sup.3. In another embodiment, a scintillator optic includes europium-doped strontium iodide providing at least 50,000 photons per MeV, where the europium in the crystal is primarily Eu.sup.2+, and the europium is present in an amount greater than about 1.6%. A scintillator radiation detector in yet another embodiment includes a scintillator optic comprising SrI.sub.2 and BaI.sub.2, where a ratio of SrI.sub.2 to BaI.sub.2 is in a range of between 0:1 and 1.0, the scintillator optic is a crystal that provides at least 50,000 scintillation photons per MeV and energy resolution of less than about 5% at 662 keV, and the crystal has a volume of 1 cm.sup.3 or more; the scintillator optic contains more than about 2% europium.

Polarized Neutron Studies on Antiferromagnetic Single Crystals: Technical Report No. 4

DOE R&D Accomplishments Database

Nathans, R.; Riste, T.; Shirane, G.; Shull, C.G.

1958-11-26

The theory of neutron scattering by magnetic crystals as given by Halpern and Johnson predicts changes in the polarization state of the neutron beam upon scattering which depend upon the relative orientation of the neutron polarization vector and the crystal magnetic axis. This was investigated experimentally with a polarized beam spectrometer using single crystals of Cr{sub 2}O{sub 3} and alpha - Fe{sub 2}O{sub 3} in which reside unique antiferromagnetic axes. Studies were made on several different reflections in both crystals for a number of different temperatures both below and above the Neel point. Results support the theoretical predictions and indicate directions for the moments in these crystals consistent with previous work. A more detailed study of the polarization changes in the (111) reflection in alpha - Fe{sub 2}O{sub 3} at room temperature on application of a magnetic field was carried out, The results indicate that the principal source of the parasitic ferromagnetism in hematite is essentially independent of the orientation of the antiferromagnetic domains within the crystal.

Spatial resolution of a hard x-ray CCD detector.

PubMed

Seely, John F; Pereira, Nino R; Weber, Bruce V; Schumer, Joseph W; Apruzese, John P; Hudson, Lawrence T; Szabo, Csilla I; Boyer, Craig N; Skirlo, Scott

2010-08-10

The spatial resolution of an x-ray CCD detector was determined from the widths of the tungsten x-ray lines in the spectrum formed by a crystal spectrometer in the 58 to 70 keV energy range. The detector had 20 microm pixel, 1700 by 1200 pixel format, and a CsI x-ray conversion scintillator. The spectral lines from a megavolt x-ray generator were focused on the spectrometer's Rowland circle by a curved transmission crystal. The line shapes were Lorentzian with an average width after removal of the natural and instrumental line widths of 95 microm (4.75 pixels). A high spatial frequency background, primarily resulting from scattered gamma rays, was removed from the spectral image by Fourier analysis. The spectral lines, having low spatial frequency in the direction perpendicular to the dispersion, were enhanced by partially removing the Lorentzian line shape and by fitting Lorentzian curves to broad unresolved spectral features. This demonstrates the ability to improve the spectral resolution of hard x-ray spectra that are recorded by a CCD detector with well-characterized intrinsic spatial resolution.

Gamma-ray spectrometer experiment, Apollo 17: NaI(T1) detector crystal activation

NASA Technical Reports Server (NTRS)

Trombka, J. I.; Schmadebeck, R. L.; Bielefeld, M.; Okelley, G. D.; Eldridge, J. S.; Northcutt, K. J.; Metzger, A. E.; Schonfeld, E.; Peterson, L. E.; Arnold, J. R.

1973-01-01

An attempt was made to obtain experimental data on proton induced activity and its effect on gamma ray spectral measurements. A NaI(T1) crystal flown in Apollo 17 command module was used for the experiment.

X-ray characterization of curved crystals for hard x-ray astronomy

NASA Astrophysics Data System (ADS)

Buffagni, Elisa; Bonnini, Elisa; Ferrari, Claudio; Virgilli, Enrico; Frontera, Filippo

2015-05-01

Among the methods to focus photons the diffraction in crystals results as one of the most effective for high energy photons. An assembling of properly oriented crystals can form a lens able to focus x-rays at high energy via Laue diffraction in transmission geometry; this is a Laue lens. The x-ray diffraction theory provides that the maximum diffraction efficiency is achieved in ideal mosaic crystals, but real mosaic crystals show diffraction efficiencies several times lower than the ideal case due to technological problems. An alternative and convenient approach is the use of curved crystals. We have recently optimized an efficient method based on the surface damage of crystals to produce self-standing uniformly curved Si, GaAs and Ge tiles of thickness up to 2-3 mm and curvature radii R down to a few meters. We show that, for curved diffracting planes, such crystals have a diffraction efficiency nearly forty times higher than the diffraction efficiency of perfect similar flat crystals, thus very close to that of ideal mosaic crystals. Moreover, in an alternative configuration where the diffracting planes are perpendicular to the curved ones, a focusing effect occurs and will be shown. These results were obtained for several energies between 17 and 120 keV with lab sources or at high energy facilities such as LARIX at Ferrara (Italy), ESRF at Grenoble (France), and ANKA at Karlsruhe (Germany).

Smoothing metallic glasses without introducing crystallization by gas cluster ion beam

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shao, Lin; Chen, Di; Myers, Michael

2013-03-11

We show that 30 keV Ar cluster ion bombardment of Ni{sub 52.5}Nb{sub 10}Zr{sub 15}Ti{sub 15}Pt{sub 7.5} metallic glass (MG) can remove surface mountain-like features and reduce the root mean square surface roughness from 12 nm to 0.7 nm. X-ray diffraction analysis reveals no crystallization after cluster ion irradiation. Molecular dynamics simulations show that, although damage cascades lead to local melting, the subsequent quenching rate is a few orders of magnitude higher than the critical cooling rate for MG formation, thus the melted zone retains its amorphous nature down to room temperature. These findings can be applied to obtain ultra-smooth MGsmore » without introducing crystallization.« less

Probing dynamics in colloidal crystals with pump-probe experiments at LCLS: Methodology and analysis

DOE PAGES

Mukharamova, Nastasia; Lazarev, Sergey; Meijer, Janne -Mieke; ...

2017-05-19

We present results of the studies of dynamics in colloidal crystals performed by pump-probe experiments using an X-ray free-electron laser (XFEL). Colloidal crystals were pumped with an infrared laser at a wavelength of 800 nm with varying power and probed by XFEL pulses at an energy of 8 keV with a time delay up to 1000 ps. The positions of the Bragg peaks, and their radial and azimuthal widths were analyzed as a function of the time delay. The spectral analysis of the data did not reveal significant enhancement of frequencies expected in this experiment. As a result, this allowedmore » us to conclude that the amplitude of vibrational modes excited in colloidal crystals was less than the systematic error caused by the noise level.« less

The monochromatic imaging mode of a RITA-type neutron spectrometer

NASA Astrophysics Data System (ADS)

Bahl, C. R. H.; Andersen, P.; Klausen, S. N.; Lefmann, K.

2004-12-01

The imaging monochromatic mode of a neutron spectrometer with a multi-bladed RITA analyser system is so far unexplored. We present analytical calculations that define the mode. It is shown that the mode can be realised for PG (0 0 2) analyser crystals, from incident energies of about 3.2 meV and up, allowing the important cases of 3.7, 5.0 and 13.7 meV. Due to beam divergence, the neutron rays from neighbouring analyser blades are found to overlap slightly. Hence, the optimal use of the monochromatic imaging mode would be found by employing an adjustable radial collimator to limit the spread of the ray from each analyser blade.

VEGAS: VErsatile GBT Astronomical Spectrometer

NASA Astrophysics Data System (ADS)

Bussa, Srikanth; VEGAS Development Team

2012-01-01

The National Science Foundation Advanced Technologies and Instrumentation (NSF-ATI) program is funding a new spectrometer backend for the Green Bank Telescope (GBT). This spectrometer is being built by the CICADA collaboration - collaboration between the National Radio Astronomy Observatory (NRAO) and the Center for Astronomy Signal Processing and Electronics Research (CASPER) at the University of California Berkeley.The backend is named as VErsatile GBT Astronomical Spectrometer (VEGAS) and will replace the capabilities of the existing spectrometers. This backend supports data processing from focal plane array systems. The spectrometer will be capable of processing up to 1.25 GHz bandwidth from 8 dual polarized beams or a bandwidth up to 10 GHz from a dual polarized beam.The spectrometer will be using 8-bit analog to digital converters (ADC), which gives a better dynamic range than existing GBT spectrometers. There will be 8 tunable digital sub-bands within the 1.25 GHz bandwidth, which will enhance the capability of simultaneous observation of multiple spectral transitions. The maximum spectral dump rate to disk will be about 0.5 msec. The vastly enhanced backend capabilities will support several science projects with the GBT. The projects include mapping temperature and density structure of molecular clouds; searches for organic molecules in the interstellar medium; determination of the fundamental constants of our evolving Universe; red-shifted spectral features from galaxies across cosmic time and survey for pulsars in the extreme gravitational environment of the Galactic Center.

Resolution-enhanced Mapping Spectrometer

NASA Technical Reports Server (NTRS)

Kumer, J. B.; Aubrun, J. N.; Rosenberg, W. J.; Roche, A. E.

1993-01-01

A familiar mapping spectrometer implementation utilizes two dimensional detector arrays with spectral dispersion along one direction and spatial along the other. Spectral images are formed by spatially scanning across the scene (i.e., push-broom scanning). For imaging grating and prism spectrometers, the slit is perpendicular to the spatial scan direction. For spectrometers utilizing linearly variable focal-plane-mounted filters the spatial scan direction is perpendicular to the direction of spectral variation. These spectrometers share the common limitation that the number of spectral resolution elements is given by the number of pixels along the spectral (or dispersive) direction. Resolution enhancement by first passing the light input to the spectrometer through a scanned etalon or Michelson is discussed. Thus, while a detector element is scanned through a spatial resolution element of the scene, it is also temporally sampled. The analysis for all the pixels in the dispersive direction is addressed. Several specific examples are discussed. The alternate use of a Michelson for the same enhancement purpose is also discussed. Suitable for weight constrained deep space missions, hardware systems were developed including actuators, sensor, and electronics such that low-resolution etalons with performance required for implementation would weigh less than one pound.

Search For Anomalous n-p Scattering At 60 eV-140 keV

DOE Office of Scientific and Technical Information (OSTI.GOV)

Moreh, R.; Block, R. C.; Danon, Y.

2009-01-28

A search for an anomalous n-p scattering from a polyethylene sample (CH{sub 2}) at 8 final energies between 64 eV and 2.5 keV was carried out. The scattering intensities were compared to that from a graphite (C) sample. The results were found to confirm our previous n-p results on H{sub 2}O at a final energy of 24.3 keV where no n-p scattering anomaly was observed. The present results refute all proposed models attempting to explain the occurrence of any n-p scattering anomaly at keV neutron energies.

Electron/proton spectrometer certification documentation analyses

NASA Technical Reports Server (NTRS)

Gleeson, P.

1972-01-01

A compilation of analyses generated during the development of the electron-proton spectrometer for the Skylab program is presented. The data documents the analyses required by the electron-proton spectrometer verification plan. The verification plan was generated to satisfy the ancillary hardware requirements of the Apollo Applications program. The certification of the spectrometer requires that various tests, inspections, and analyses be documented, approved, and accepted by reliability and quality control personnel of the spectrometer development program.

Measuring Transmission Efficiencies Of Mass Spectrometers

NASA Technical Reports Server (NTRS)

Srivastava, Santosh K.

1989-01-01

Coincidence counts yield absolute efficiencies. System measures mass-dependent transmission efficiencies of mass spectrometers, using coincidence-counting techniques reminiscent of those used for many years in calibration of detectors for subatomic particles. Coincidences between detected ions and electrons producing them counted during operation of mass spectrometer. Under certain assumptions regarding inelastic scattering of electrons, electron/ion-coincidence count is direct measure of transmission efficiency of spectrometer. When fully developed, system compact, portable, and used routinely to calibrate mass spectrometers.

Searches for 3.5 keV Absorption Features in Cluster AGN Spectra

NASA Astrophysics Data System (ADS)

Conlon, Joseph P.

2018-06-01

We investigate possible evidence for a spectral dip around 3.5 keV in central cluster AGNs, motivated by previous results for archival Chandra observations of the Perseus cluster and the general interest in novel spectral features around 3.5 keV that may arise from dark matter physics. We use two deep Chandra observations of the Perseus and Virgo clusters that have recently been made public. In both cases, mild improvements in the fit (Δχ2 = 4.2 and Δχ2 = 2.5) are found by including such a dip at 3.5 keV into the spectrum. A comparable result (Δχ2 = 6.5) is found re-analysing archival on-axis Chandra ACIS-S observations of the centre of the Perseus cluster.

15 pixels digital autocorrelation spectrometer system

NASA Astrophysics Data System (ADS)

Lee, Changhoon; Kim, Hyo-Ryung; Kim, Kwang-Dong; Chung, Mun-Hee; Timoc, C.

2006-06-01

In this paper describes the system configuration and the some performance test results of the 15 pixels digital autocorrelation spectrometer to be used at the Taeduk Radio Astronomy Observatory (TRAO) of Korea. This autocorrelation spectrometer instrument enclosed in a 3-slot VXI module and controlled via a USB port by a backend PC. This spectrometer system consists of the 4 band-pass filters unit, the digitizer, the 512 lags correlator, the clock distribution unit, and USB controller. And here we describe the frequency accuracy and the root-mean-square noise characteristic of this spectrometer. After some calibration procedure, this spectrometer can be use as the back-end system at TRAO for the 3x5 focal plane array receivers.

Measurements of the spectrum and energy dependence of X-ray transition radiation

NASA Technical Reports Server (NTRS)

Cherry, M. L.

1978-01-01

The results of experiments designed to test the theory of X-ray transition radiation and to verify the predicted dependence of the characteristic features of the radiation on the radiator dimensions are presented. The X-ray frequency spectrum produced by 5- to 9-GeV electrons over the range 4 to 30 keV was measured with a calibrated single-crystal Bragg spectrometer, and at frequencies up to 100 keV with an NaI scintillator. The interference pattern in the spectrum and the hardening of the radiation with increasing foil thickness are clearly observed. The energy dependence of the total transition-radiation intensity was studied using a radiator with large dimensions designed to yield energy-dependent signals at very high particle energies, up to E/mc-squared approximately equal to 100,000. The results are in good agreement with the theoretical predictions.

Copper doping of ZnO crystals by transmutation of 64Zn to 65Cu: An electron paramagnetic resonance and gamma spectroscopy study

NASA Astrophysics Data System (ADS)

Recker, M. C.; McClory, J. W.; Holston, M. S.; Golden, E. M.; Giles, N. C.; Halliburton, L. E.

2014-06-01

Transmutation of 64Zn to 65Cu has been observed in a ZnO crystal irradiated with neutrons. The crystal was characterized with electron paramagnetic resonance (EPR) before and after the irradiation and with gamma spectroscopy after the irradiation. Major features in the gamma spectrum of the neutron-irradiated crystal included the primary 1115.5 keV gamma ray from the 65Zn decay and the positron annihilation peak at 511 keV. Their presence confirmed the successful transmutation of 64Zn nuclei to 65Cu. Additional direct evidence for transmutation was obtained from the EPR of Cu2+ ions (where 63Cu and 65Cu hyperfine lines are easily resolved). A spectrum from isolated Cu2+ (3d9) ions acquired after the neutron irradiation showed only hyperfine lines from 65Cu nuclei. The absence of 63Cu lines in this Cu2+ spectrum left no doubt that the observed 65Cu signals were due to transmuted 65Cu nuclei created as a result of the neutron irradiation. Small concentrations of copper, in the form of Cu+-H complexes, were inadvertently present in our as-grown ZnO crystal. These Cu+-H complexes are not affected by the neutron irradiation, but they dissociate when a crystal is heated to 900 °C. This behavior allowed EPR to distinguish between the copper initially in the crystal and the copper subsequently produced by the neutron irradiation. In addition to transmutation, a second major effect of the neutron irradiation was the formation of zinc and oxygen vacancies by displacement. These vacancies were observed with EPR.

K-shell photoelectric cross sections for intermediate-Z elements at 26 keV

NASA Astrophysics Data System (ADS)

Kumar, Suresh; Singh, N.; Allawadhi, K. L.; Sood, B. S.

1986-08-01

Our earlier measurements of K-shell photoelectric cross sections for intermediate Z elements at 74 and 37 keV have been extended to 26 keV using external conversion x rays in Sn. The experimental results are found to show fairly good agreement with the theoretical values of Scofield.

Laser Induced Breakdown Spectroscopy of Glass and Crystal Samples

NASA Astrophysics Data System (ADS)

Sharma, Prakash; Sandoval, Alejandra; Carter, Michael; Kumar, Akshaya

2015-03-01

Different types of quartz crystals and rare earth ions doped glasses have been identified using the laser induced breakdown spectroscopy (LIBS) technique. LIBS is a real time technique, can be used to identify samples in solid, liquid and gas phases. The advantage of LIBS technique is that no sample preparation is required and laser causes extremely minimal damage to the sample surface. The LIBS spectrum of silicate glasses, prepared by sol-gel method and doped with different concentration of rare earth ions, has been recorded. The limit of detection of rare earth ions in glass samples has been calculated. Total 10 spectrums of each sample were recorded and then averaged to get a final spectrum. The ocean optics LIBS2500 plus spectrometer along with a Q- switched Nd: YAG laser (Quantel, Big Sky) were used to record the LIBS spectrum. This spectrometer can analyze the sample in the spectral range of 200 nm to 980 nm. The spectrum was processed by OOILIBS-plus (v1.0) software. This study has application in the industry where different crystals can be easily identified before they go for shaping and polishing. Also, concentration of rare earth ions in glass can be monitored in real time for quality control.

Characteristics of pitch angle distributions of hundreds of keV electrons in the slot region and inner radiation belt

NASA Astrophysics Data System (ADS)

Zhao, H.; Li, X.; Blake, J. B.; Fennell, J. F.; Claudepierre, S. G.; Baker, D. N.; Jaynes, A. N.; Malaspina, D. M.

2014-12-01

The pitch angle distribution (PAD) of energetic electrons in the slot region and inner radiation belt received little attention in the past decades due to the lack of quality measurements. Using the state-of-the-art pitch angle-resolved data from the Magnetic Electron Ion Spectrometer instrument onboard the Van Allen Probes, a detailed analysis of hundreds of keV electron PADs below L = 4 is performed, in which the PADs are categorized into three types: normal (flux peaking at 90°), cap (exceedingly peaking narrowly around 90°), and 90° minimum (lower flux at 90°) PADs. By examining the characteristics of the PADs of ˜460 keV electrons for over a year, we find that the 90° minimum PADs are generally present in the inner belt (L<2), while normal PADs dominate at L˜3.5-4. In the region between, 90° minimum PADs dominate during injection times and normal PADs dominate during quiet times. Cap PADs appear mostly at the decay phase of storms in the slot region and are likely caused by the pitch angle scattering of hiss waves. Fitting the normal PADs into sinnα form, the parameter n is much higher below L = 3 than that in the outer belt and relatively constant in the inner belt but changes significantly in the slot region (2 < L < 3) during injection times. As for the 90° minimum PADs, by performing a detailed case study, we find in the slot region this type of PAD is likely caused by chorus wave heating, but this mechanism can hardly explain the formation of 90° minimum PADs at the center of inner belt.

Imaging spectrometer/camera having convex grating

NASA Technical Reports Server (NTRS)

Reininger, Francis M. (Inventor)

2000-01-01

An imaging spectrometer has fore-optics coupled to a spectral resolving system with an entrance slit extending in a first direction at an imaging location of the fore-optics for receiving the image, a convex diffraction grating for separating the image into a plurality of spectra of predetermined wavelength ranges; a spectrometer array for detecting the spectra; and at least one concave sperical mirror concentric with the diffraction grating for relaying the image from the entrance slit to the diffraction grating and from the diffraction grating to the spectrometer array. In one embodiment, the spectrometer is configured in a lateral mode in which the entrance slit and the spectrometer array are displaced laterally on opposite sides of the diffraction grating in a second direction substantially perpendicular to the first direction. In another embodiment, the spectrometer is combined with a polychromatic imaging camera array disposed adjacent said entrance slit for recording said image.

Development of a High Resolution X-ray Spectrometer on the National Ignition Facility

NASA Astrophysics Data System (ADS)

Gao, L.; Kraus, B.; Hill, K. W.; Bitter, M.; Efthimion, P.; Schneider, M. B.; Chen, H.; Ayers, J.; Liedahl, D.; Macphee, A. G.; Le, H. P.; Thorn, D.; Nelson, D.

2017-10-01

A high-resolution x-ray spectrometer has been designed, calibrated, and deployed on the National Ignition Facility (NIF) to measure plasma parameters for a Kr-doped surrogate capsule imploded at NIF conditions. Two conical crystals, each diffracting the He α and He β complexes respectively, focus the spectra onto a steak camera photocathode for time-resolved measurements with a temporal resolution of <20 ps. A third cylindrical crystal focuses the entire He α to He β spectrum onto an image plate for a time-integrated spectrum to correlate the two streaked signals. The instrument was absolutely calibrated by the x-ray group at the Princeton Plasma Physics Laboratory using a micro-focus x-ray source. Detailed calibration procedures, including source and spectrum alignment, energy calibration, crystal performance evaluation, and measurement of the resolving power and the integrated reflectivity will be presented. Initial NIF experimental results will also be discussed. This work was performed under the auspices of the U.S. Department of Energy by Princeton Plasma Physics Laboratory under contract DE-AC02-09CH11466 and by Lawrence Livermore National Laboratory under contract DE-AC52-07NA27344.

0.2 to 10 keV electrons interacting with water ice: Radiolysis, sputtering, and sublimation

NASA Astrophysics Data System (ADS)

Galli, A.; Vorburger, A.; Wurz, P.; Pommerol, A.; Cerubini, R.; Jost, B.; Poch, O.; Tulej, M.; Thomas, N.

2018-06-01

We present new laboratory experiments investigating various water ice samples, ranging from thin ice films to porous thick ice layers, that are irradiated with electrons. The molecules leaving the ice are monitored with a pressure gauge and a mass spectrometer. Most particles released from the ice are H2 and O2, the observed ratio of 2:1 is consistent with H2O being radiolysed into H2 + 1/2 O2 upon irradiation. H2O2 is likely a minor contribution of radiolysis, amounting to 0.001 ± 0.001 of the total gas release from the ice sample. Neither the physical properties of the ice, nor the energy, nor the electron impact angle have any obvious effect on the relative abundances of the radiolysis products. The absolute sputtering yield (i.e., the ratio of produced O2 or destroyed H2O per impacting electron) increases with energy until a few 100 eV. For higher energies up to 10 keV the yield remains roughly constant, once the saturation dose of the ice is reached. This indicates that ongoing irradiation eventually releases the radiolysis products from the water ice even for penetration depths of several micrometers.

Measurement of the 238U neutron-capture cross section and gamma-emission spectra from 10 eV to 100 keV using the DANCE detector at LANSCE

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ullmann, John L; Couture, A J; Keksis, A L

2010-01-01

A careful new measurement of the {sup 238}U(n,{gamma}) cross section from 10 eV to 100 keV has been made using the DANCE detector at LANSCE. DANCE is a 4{pi} calorimetric scintillator array consisting of 160 BaF{sub 2} crystals. Measurements were made on a 48 mg/cm{sup 2} depleted uranium target. The cross sections are in general good agreement with previous measurements. The gamma-ray emission spectra, as a function of gamma multiplicity, were also measured and compared to model calculations.

Optimization of single keV ion implantation for the construction of single P-donor devices

NASA Astrophysics Data System (ADS)

Yang, Changyi; Jamieson, David N.; Hopf, Toby; Andresen, Soren E.; Hearne, Sean M.; Hudson, Fay E.; Pakes, Christopher I.; Mitic, Mladen; Gauja, Eric; Tamanyan, Grigori; Dzurak, Andrew S.; Prawer, Steven; Clark, Robert G.

2005-02-01

We report recent progress in single keV ion implantation and online detection for the controlled implantation of single donors in silicon. When integrated with silicon nanofabrication technology this forms the "top down" strategy for the construction of prototype solid state quantum computer devices based on phosphorus donors in silicon. We have developed a method of single ion implantation and online registration that employs detector electrodes adjacent to the area into which the donors are to be implanted. The implantation sites are positioned with nanometer accuracy using an electron beam lithography patterned PMMA mask. Control of the implantation depth of 20 nm is achieved by tuning the phosphorus ion energy to 14 keV. The counting of single ion implantation in each site is achieved by the detection of e-/h+ pairs produced by the implanted phosphorus ion in the substrate. The system is calibrated by use of Mn K-line x-rays (5.9 and 6.4 keV) and we find the ionization energy of the 14 keV phosphorus ions in silicon to be about 3.5-4.0 keV for implants through a 5 nm SiO2 surface layer. This paper describes the development of an improved PIN detector structure that provides more reliable performance of the earlier MOS structure. With the new structure, the energy noise threshold has been minimized to 1 keV or less. Unambiguous detection/counting of single keV ion implantation events were achieved with a confidence level greater than 98% with a reliable and reproducible fabrication process.

Monolithic CMOS imaging x-ray spectrometers

NASA Astrophysics Data System (ADS)

Kenter, Almus; Kraft, Ralph; Gauron, Thomas; Murray, Stephen S.

2014-07-01

The Smithsonian Astrophysical Observatory (SAO) in collaboration with SRI/Sarnoff is developing monolithic CMOS detectors optimized for x-ray astronomy. The goal of this multi-year program is to produce CMOS x-ray imaging spectrometers that are Fano noise limited over the 0.1-10keV energy band while incorporating the many benefits of CMOS technology. These benefits include: low power consumption, radiation "hardness", high levels of integration, and very high read rates. Small format test devices from a previous wafer fabrication run (2011-2012) have recently been back-thinned and tested for response below 1keV. These devices perform as expected in regards to dark current, read noise, spectral response and Quantum Efficiency (QE). We demonstrate that running these devices at rates ~> 1Mpix/second eliminates the need for cooling as shot noise from any dark current is greatly mitigated. The test devices were fabricated on 15μm, high resistivity custom (~30kΩ-cm) epitaxial silicon and have a 16 by 192 pixel format. They incorporate 16μm pitch, 6 Transistor Pinned Photo Diode (6TPPD) pixels which have ~40μV/electron sensitivity and a highly parallel analog CDS signal chain. Newer, improved, lower noise detectors have just been fabricated (October 2013). These new detectors are fabricated on 9μm epitaxial silicon and have a 1k by 1k format. They incorporate similar 16μm pitch, 6TPPD pixels but have ~ 50% higher sensitivity and much (3×) lower read noise. These new detectors have undergone preliminary testing for functionality in Front Illuminated (FI) form and are presently being prepared for back thinning and packaging. Monolithic CMOS devices such as these, would be ideal candidate detectors for the focal planes of Solar, planetary and other space-borne x-ray astronomy missions. The high through-put, low noise and excellent low energy response, provide high dynamic range and good time resolution; bright, time varying x-ray features could be temporally and

On high-resolution reciprocal-space mapping with a triple-crystal diffractometer for high-energy X-rays.

PubMed

Liss, K D; Royer, A; Tschentscher, T; Suortti, P; Williams, A P

1998-03-01

High-energy X-rav diffraction by means of triple-crystal techniques is a powerful tool for investigating dislocations and strain in bulk materials. Radiation with an energy typically higher than 80 keV combines the advantage of low attenuation with high resolution at large momentum transfers. The triple-crystal diffractometer at the High Energy Beamline of the European Synchrotron Radiation Facility is described. It is shown how the transverse and longitudinal resolution depend on the choice of the crystal reflection, and how the orientation of a reciprocal-lattice distortion in an investigated sample towards the resolution element of the instrument can play an important role. This effect is demonstrated on a single crystal of silicon where a layer of macro pores reveals satellites around the Bragg reflection. The resulting longitudinal distortion can be investigated using the high transverse resolution of the instrument when choosing an appropriate reflection.

X-ray driven channeling acceleration in crystals and carbon nanotubes

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shin, Young-Min; Still, Dean A.; Shiltsev, Vladimir

2013-12-01

Acceleration of particles channeling in a crystal by means of diffracted x-rays via Bormann anomalous transmission was conceived for heavy ions and muons by Tajima and Cavenago [Phys. Rev. Lett. 59, 1440 (1987)], which potentially offers an appreciably high field gradient on the order of GV/cm. The theoretical model of the high gradient acceleration has been studied in two kinds of atomic structure, crystals and carbon nanotubes (CNTs), with analytic calculations and electromagnetic eigenmode simulations. A range of acceleration gradients and cutoffs of the x-ray power (the lowest power limit to overcome the Bremsstrahlung radiation losses) are characterized in termsmore » of the lattice constants, unit cell sizes, and photon energies. The parametric analysis indicates that the required x-ray power can be reduced to an order of megawatt by replacing crystals with CNTs. Eventually, the equivalent dielectric approximation of a multi-wall nanotube shows that 250–810 MeV muons can be synchronously coupled with x-rays of 0.65–1.32 keV in the accelerating structure.« less

Homogeneous alignment of nematic liquid crystals by ion beam etched surfaces

NASA Technical Reports Server (NTRS)

Wintucky, E. G.; Mahmood, R.; Johnson, D. L.

1979-01-01

A wide range of ion beam etch parameters capable of producing uniform homogeneous alignment of nematic liquid crystals on SiO2 films are discussed. The alignment surfaces were generated by obliquely incident (angles of 5 to 25 deg) argon ions with energies in the range of 0.5 to 2.0 KeV, ion current densities of 0.1 to 0.6 mA sq cm and etch times of 1 to 9 min. A smaller range of ion beam parameters (2.0 KeV, 0.2 mA sq cm, 5 to 10 deg and 1 to 5 min.) were also investigated with ZrO2 films and found suitable for homogeneous alignment. Extinction ratios were very high (1000), twist angles were small ( or = 3 deg) and tilt-bias angles very small ( or = 1 deg). Preliminary scanning electron microscopy results indicate a parallel oriented surface structure on the ion beam etched surfaces which may determine alignment.

[Optimum design of imaging spectrometer based on toroidal uniform-line-spaced (TULS) spectrometer].

PubMed

Xue, Qing-Sheng; Wang, Shu-Rong

2013-05-01

Based on the geometrical aberration theory, a optimum-design method for designing an imaging spectrometer based on toroidal uniform grating spectrometer is proposed. To obtain the best optical parameters, twice optimization is carried out using genetic algorithm(GA) and optical design software ZEMAX A far-ultraviolet(FUV) imaging spectrometer is designed using this method. The working waveband is 110-180 nm, the slit size is 50 microm x 5 mm, and the numerical aperture is 0.1. Using ZEMAX software, the design result is analyzed and evaluated. The results indicate that the MTF for different wavelengths is higher than 0.7 at Nyquist frequency 10 lp x mm(-1), and the RMS spot radius is less than 14 microm. The good imaging quality is achieved over the whole working waveband, the design requirements of spatial resolution 0.5 mrad and spectral resolution 0.6 nm are satisfied. It is certificated that the optimum-design method proposed in this paper is feasible. This method can be applied in other waveband, and is an instruction method for designing grating-dispersion imaging spectrometers.

The ASTRO-H X-ray Observatory

NASA Astrophysics Data System (ADS)

Takahashi, Tadayuki; Mitsuda, Kazuhisa; Kelley, Richard; Aarts, Henri; Aharonian, Felix; Akamatsu, Hiroki; Akimoto, Fumie; Allen, Steve; Anabuki, Naohisa; Angelini, Lorella; Arnaud, Keith; Asai, Makoto; Audard, Marc; Awaki, Hisamitsu; Azzarello, Philipp; Baluta, Chris; Bamba, Aya; Bando, Nobutaka; Bautz, Mark; Blandford, Roger; Boyce, Kevin; Brown, Greg; Cackett, Ed; Chernyakova, Mara; Coppi, Paolo; Costantini, Elisa; de Plaa, Jelle; den Herder, Jan-Willem; DiPirro, Michael; Done, Chris; Dotani, Tadayasu; Doty, John; Ebisawa, Ken; Eckart, Megan; Enoto, Teruaki; Ezoe, Yuichiro; Fabian, Andrew; Ferrigno, Carlo; Foster, Adam; Fujimoto, Ryuichi; Fukazawa, Yasushi; Funk, Stefan; Furuzawa, Akihiro; Galeazzi, Massimiliano; Gallo, Luigi; Gandhi, Poshak; Gendreau, Keith; Gilmore, Kirk; Haas, Daniel; Haba, Yoshito; Hamaguchi, Kenji; Hatsukade, Isamu; Hayashi, Takayuki; Hayashida, Kiyoshi; Hiraga, Junko; Hirose, Kazuyuki; Hornschemeier, Ann; Hoshino, Akio; Hughes, John; Hwang, Una; Iizuka, Ryo; Inoue, Yoshiyuki; Ishibashi, Kazunori; Ishida, Manabu; Ishimura, Kosei; Ishisaki, Yoshitaka; Ito, Masayuki; Iwata, Naoko; Iyomoto, Naoko; Kaastra, Jelle; Kallman, Timothy; Kamae, Tuneyoshi; Kataoka, Jun; Katsuda, Satoru; Kawahara, Hajime; Kawaharada, Madoka; Kawai, Nobuyuki; Kawasaki, Shigeo; Khangaluyan, Dmitry; Kilbourne, Caroline; Kimura, Masashi; Kinugasa, Kenzo; Kitamoto, Shunji; Kitayama, Tetsu; Kohmura, Takayoshi; Kokubun, Motohide; Kosaka, Tatsuro; Koujelev, Alex; Koyama, Katsuji; Krimm, Hans; Kubota, Aya; Kunieda, Hideyo; LaMassa, Stephanie; Laurent, Philippe; Lebrun, Francois; Leutenegger, Maurice; Limousin, Olivier; Loewenstein, Michael; Long, Knox; Lumb, David; Madejski, Grzegorz; Maeda, Yoshitomo; Makishima, Kazuo; Marchand, Genevieve; Markevitch, Maxim; Matsumoto, Hironori; Matsushita, Kyoko; McCammon, Dan; McNamara, Brian; Miller, Jon; Miller, Eric; Mineshige, Shin; Minesugi, Kenji; Mitsuishi, Ikuyuki; Miyazawa, Takuya; Mizuno, Tsunefumi; Mori, Hideyuki; Mori, Koji; Mukai, Koji; Murakami, Toshio; Murakami, Hiroshi; Mushotzky, Richard; Nagano, Hosei; Nagino, Ryo; Nakagawa, Takao; Nakajima, Hiroshi; Nakamori, Takeshi; Nakazawa, Kazuhiro; Namba, Yoshiharu; Natsukari, Chikara; Nishioka, Yusuke; Nobukawa, Masayoshi; Nomachi, Masaharu; O'Dell, Steve; Odaka, Hirokazu; Ogawa, Hiroyuki; Ogawa, Mina; Ogi, Keiji; Ohashi, Takaya; Ohno, Masanori; Ohta, Masayuki; Okajima, Takashi; Okamoto, Atsushi; Okazaki, Tsuyoshi; Ota, Naomi; Ozaki, Masanobu; Paerels, Fritzs; Paltani, Stéphane; Parmar, Arvind; Petre, Robert; Pohl, Martin; Porter, F. Scott; Ramsey, Brian; Reis, Rubens; Reynolds, Christopher; Russell, Helen; Safi-Harb, Samar; Sakai, Shin-ichiro; Sameshima, Hiroaki; Sanders, Jeremy; Sato, Goro; Sato, Rie; Sato, Yohichi; Sato, Kosuke; Sawada, Makoto; Serlemitsos, Peter; Seta, Hiromi; Shibano, Yasuko; Shida, Maki; Shimada, Takanobu; Shinozaki, Keisuke; Shirron, Peter; Simionescu, Aurora; Simmons, Cynthia; Smith, Randall; Sneiderman, Gary; Soong, Yang; Stawarz, Lukasz; Sugawara, Yasuharu; Sugita, Hiroyuki; Sugita, Satoshi; Szymkowiak, Andrew; Tajima, Hiroyasu; Takahashi, Hiromitsu; Takeda, Shin-ichiro; Takei, Yoh; Tamagawa, Toru; Tamura, Takayuki; Tamura, Keisuke; Tanaka, Takaaki; Tanaka, Yasuo; Tashiro, Makoto; Tawara, Yuzuru; Terada, Yukikatsu; Terashima, Yuichi; Tombesi, Francesco; Tomida, Hiroshi; Tsuboi, Yohko; Tsujimoto, Masahiro; Tsunemi, Hiroshi; Tsuru, Takeshi; Uchida, Hiroyuki; Uchiyama, Yasunobu; Uchiyama, Hideki; Ueda, Yoshihiro; Ueno, Shiro; Uno, Shinichiro; Urry, Meg; Ursino, Eugenio; de Vries, Cor; Wada, Atsushi; Watanabe, Shin; Werner, Norbert; White, Nicholas; Yamada, Takahiro; Yamada, Shinya; Yamaguchi, Hiroya; Yamasaki, Noriko; Yamauchi, Shigeo; Yamauchi, Makoto; Yatsu, Yoichi; Yonetoku, Daisuke; Yoshida, Atsumasa; Yuasa, Takayuki

2012-09-01

The joint JAXA/NASA ASTRO-H mission is the sixth in a series of highly successful X-ray missions initiated by the Institute of Space and Astronautical Science (ISAS). ASTRO-H will investigate the physics of the highenergy universe via a suite of four instruments, covering a very wide energy range, from 0.3 keV to 600 keV. These instruments include a high-resolution, high-throughput spectrometer sensitive over 0.3-12 keV with high spectral resolution of ΔE ≦ 7 eV, enabled by a micro-calorimeter array located in the focal plane of thin-foil X-ray optics; hard X-ray imaging spectrometers covering 5-80 keV, located in the focal plane of multilayer-coated, focusing hard X-ray mirrors; a wide-field imaging spectrometer sensitive over 0.4-12 keV, with an X-ray CCD camera in the focal plane of a soft X-ray telescope; and a non-focusing Compton-camera type soft gamma-ray detector, sensitive in the 40-600 keV band. The simultaneous broad bandpass, coupled with high spectral resolution, will enable the pursuit of a wide variety of important science themes.

A compact dispersive refocusing Rowland circle X-ray emission spectrometer for laboratory, synchrotron, and XFEL applications

DOE PAGES

Holden, William M.; Hoidn, Oliver R.; Ditter, Alexander S.; ...

2017-07-27

X-ray emission spectroscopy is emerging as an important complement to x-ray absorption fine structure spectroscopy, providing a characterization of the occupied electronic density of states local to the species of interest. Here, we present details of the design and performance of a compact x-ray emission spectrometer that uses a dispersive refocusing Rowland (DRR) circle geometry to achieve excellent performance for the 2-2.5 keV range, i.e., especially for the K-edge emission from sulfur and phosphorous. The DRR approach allows high energy resolution even for unfocused x-ray sources. This property enables high count rates in laboratory studies, approaching those of insertion-device beamlinesmore » at third-generation synchrotrons, despite use of only a low-powered, conventional x-ray tube. The spectrometer, whose overall scale is set by use of a 10-cm diameter Rowland circle and a new small-pixel complementary metal-oxide-semiconductor x-ray camera, is easily portable to synchrotron or x-ray free electron laser beamlines. Photometrics from measurements at the Advanced Light Source show excellent overall instrumental efficiency. In addition, the compact size of this instrument lends itself to future multiplexing to gain large factors in net collection efficiency or its implementation in controlled gas gloveboxes either in the lab or in an endstation.« less

New crystal spectrograph designs and their application to plasma diagnostics (invited)

NASA Astrophysics Data System (ADS)

Förster, E.; Gäbel, K.; Uschmann, I.

1992-10-01

A special crystal monolith was fabricated for absolute measurements of x-ray wavelength. It consists of two flat quartz plates, accurately cut relative to reflecting net planes, with a fixed distance between them. Absolute wavelengths (i.e., without use of reference lines) of L-shell laser produced spectra of Cu, Ge, As, etc. have been measured in the 7.5-8.5 Å with an accuracy of Δλ/λ=10-5. Our Johann type x-ray spectrometer with a cylindrically bent quartz has been used to reveal line coincidences necessary for photopumping processes. In this scheme source-size influences are smaller, therefore, line profiles have been measured at a spectrometer resolution better than 5000. Because of its focusing in the sagittal plane, a von Hámos type x-ray spectrometer has been used to detect the small x-ray emission of subpicosecond laser-produced plasmas (E=2 mJ, t=100 fs). X-ray spectra of Al both Kα, Kβ lines and Heα-resonance line with its satellites. Finally, a multichannel x-ray microscope has been designed and fabricated. It consists of several two-dimensionally bent crystals where each of them images one x-ray line emitted by a laser-produced plasma. The spatial resolution of x-ray line images is about 5 μm, and the width of the spectral ranges is Δλ/λ=10-4 to 10-2. Thus, the spatial distribution of ions radiating in selected x-ray lines have been found being of interest in the study of population inversions.

Thermal gradient crystals as tuneable monochromator for high energy X-rays

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ruett, U.; Schulte-Schrepping, H.; Heuer, J.

2010-06-23

At the high energy synchrotron radiation beamline BW5 at DORIS III at DESY a new monochromator providing broad energy bandwidth and high reflectivity is in use. On a small 10x10x5 mm{sup 3} silicon crystal scattering at the (311) reflection a thermal gradient is applied, which tunes the scattered energy bandwidth. The (311) reflection strongly suppresses the higher harmonics allowing the use of an image plate detector for crystallography. The monochromator can be used at photon energies above 60 keV.

Venus nightside ionosphere - A model with KeV electron impact ionization

NASA Technical Reports Server (NTRS)

Kumar, S.

1982-01-01

The impact of keV electrons is proposed as the strongest source of ionization in a full-up Venus nightside ionosphere model for the equatorial midnight region. The electron impacts lead to a peak ion density of 100,000/cu cm, which was observed by the PV-OIMS experiment on several occasions. In addition, the observed altitude profiles of CO2(+), O(+), O2(+), H(+), and H2(+) can be reproduced by the model on condition that the available keV electron flux is approximated by a reasonable extrapolation from fluxes observed at lower energies.

Spectrometers for compact neutron sources

NASA Astrophysics Data System (ADS)

Voigt, J.; Böhm, S.; Dabruck, J. P.; Rücker, U.; Gutberlet, T.; Brückel, T.

2018-03-01

We discuss the potential for neutron spectrometers at novel accelerator driven compact neutron sources. Such a High Brilliance Source (HBS) relies on low energy nuclear reactions, which enable cryogenic moderators in very close proximity to the target and neutron optics at comparably short distances from the moderator compared to existing sources. While the first effect aims at increasing the phase space density of a moderator, the second allows the extraction of a large phase space volume, which is typically requested for spectrometer applications. We find that competitive spectrometers can be realized if (a) the neutron production rate can be synchronized with the experiment repetition rate and (b) the emission characteristics of the moderator can be matched to the phase space requirements of the experiment. MCNP simulations for protons or deuterons on a Beryllium target with a suitable target/moderator design yield a source brightness, from which we calculate the sample fluxes by phase space considerations for different types of spectrometers. These match closely the figures of todays spectrometers at medium flux sources. Hence we conclude that compact neutron sources might be a viable option for next generation neutron sources.

The Strongest Acceleration of >40 keV Electrons by ICME-driven Shocks at 1 au

NASA Astrophysics Data System (ADS)

Yang, Liu; Wang, Linghua; Li, Gang; Wimmer-Schweingruber, Robert F.; He, Jiansen; Tu, Chuanyi; Tian, Hui; Bale, Stuart D.

2018-01-01

We present two case studies of the in-situ electron acceleration during the 2000 February 11 shock and the 2004 July 22 shock, with the strongest electron flux enhancement at 40 keV across the shock, among all the quasi-perpendicular and quasi-parallel ICME-driven shocks observed by the WIND 3DP instrument from 1995 through 2014 at 1 au. We find that for this quasi-perpendicular (quasi-parallel) shock on 2000 February 11 (2004 July 22), the shocked electron differential fluxes at ∼0.4–50 keV in the downstream generally fit well to a double-power-law spectrum, J ∼ E ‑β , with an index of β ∼ 3.15 (4.0) at energies below a break at ∼3 keV (∼1 keV) and β ∼ 2.65 (2.6) at energies above. For both shock events, the downstream electron spectral indices appear to be similar for all pitch angles, which are significantly larger than the index prediction by diffusive shock acceleration. In addition, the downstream electron pitch-angle distributions show the anisotropic beams in the anti-sunward-traveling direction, while the ratio of the downstream over ambient fluxes appears to peak near 90° pitch angles, at all energies of ∼0.4–50 keV. These results suggest that in both shocks, shock drift acceleration likely plays an important role in accelerating electrons in situ at 1 au. Such ICME-driven shocks could contribute to the formation of solar wind halo electrons at energies ≲2 keV, as well as the production of solar wind superhalo electrons at energies ≳2 keV in interplanetary space.

Far-infrared heterodyne spectrometer

NASA Technical Reports Server (NTRS)

Boreiko, Rita T.; Betz, Al L.

1995-01-01

A far-infrared heterodyne spectrometer was designed and built by our group for observations of atomic and molecular lines from interstellar clouds. Linewidths as narrow as 1 km/s can be expected from such regions, and so the spectrometer is designed with sub-km/s resolution so that observed line profiles will be resolved. Since its debut on the Kuiper Airborne Observatory (KAO) in 1985, the instrument has been used in regular annual flight programs from both Moffett Field, CA and Christchurch, NZ. The basic plan of the spectrometer remains unchanged from the original design presented at the previous airborne science symposium. Numerous improvements and updates to the technical capability have of course been included over the many years of operational service.

Method for calibrating mass spectrometers

DOEpatents

Anderson, Gordon A [Benton City, WA; Brands, Michael D [Richland, WA; Bruce, James E [Schwenksville, PA; Pasa-Tolic, Ljiljana [Richland, WA; Smith, Richard D [Richland, WA

2002-12-24

A method whereby a mass spectra generated by a mass spectrometer is calibrated by shifting the parameters used by the spectrometer to assign masses to the spectra in a manner which reconciles the signal of ions within the spectra having equal mass but differing charge states, or by reconciling ions having known differences in mass to relative values consistent with those known differences. In this manner, the mass spectrometer is calibrated without the need for standards while allowing the generation of a highly accurate mass spectra by the instrument.

Precise Determination of the Intensity of 226Ra Alpha Decay to the 186 keV Excited State

DOE Office of Scientific and Technical Information (OSTI.GOV)

S.P. LaMont; R.J. Gehrke; S.E. Glover

There is a significant discrepancy in the reported values for the emission probability of the 186 keV gamma-ray resulting from the alpha decay of 226 Ra to 186 keV excited state of 222 Rn. Published values fall in the range of 3.28 to 3.59 gamma-rays per 100 alpha-decays. An interesting observation is that the lower value, 3.28, is based on measuring the 186 keV gamma-ray intensity relative to the 226 Ra alpha-branch to the 186 keV level. The higher values, which are close to 3.59, are based on measuring the gamma-ray intensity from mass standards of 226 Ra that aremore » traceable to the mass standards prepared by HÓNIGSCHMID in the early 1930''s. This discrepancy was resolved in this work by carefully measuring the 226 Ra alpha-branch intensities, then applying the theoretical E2 multipolarity internal conversion coefficient of 0.692±0.007 to calculate the 186 keV gamma-ray emission probability. The measured value for the alpha branch to the 186 keV excited state was (6.16±0.03)%, which gives a 186 keV gamma-ray emission probability of (3.64±0.04)%. This value is in excellent agreement with the most recently reported 186 keV gamma-ray emission probabilities determined using 226 Ra mass standards.« less

A space bourne crystal diffraction telescope for the energy range of nuclear transitions

DOE Office of Scientific and Technical Information (OSTI.GOV)

von Ballmoos, P.; Naya, J.E.; Albernhe, F.

1995-10-01

Recent experimental work of the Toulouse-Argonne collaboration has opened for perspective of a focusing gamma-ray telescope operating in the energy range of nuclear transitions, featuring unprecedented sensitivity, angular and energy resolution. The instrument consists of a tunable crystal diffraction lens situated on a stabilized spacecraft, focusing gamma-rays onto a small array of Germanium detectors perched on an extendible boom. While the weight of such an instrument is less than 500 kg, it features an angular resolution of 15 in., an energy resolution of 2 keV and a 3 {sigma} narrow line sensitivity of a few times 10{sup {minus}7} photons s{supmore » {minus}1} cm{sup {minus}2} (10{sup 6} sec observation). This instrumental concept permits observation of any identified source at any selected line-energy in a range of typically 200 keV to 1300 keV. The resulting ``sequential`` operation mode makes sites of explosive nucleosynthesis natural scientific objectives for such a telescope: the nuclear lines of extragalactic supernovae ({sup 56}Ni, {sup 44}Ti, {sup 60}Fe) and galactic novae (p{sup {minus}}p{sup +} line, {sup 7}Be) are accessible to observation, one at a time, due to the erratic appearance and the sequence of half-lifes of these events. Other scientific objectives, include the narrow 511 keV line from galactic broad class annihilators (such as 1E1740-29, nova musca) and possible redshifted annihilation lines from AGN`s.« less

Engine spectrometer probe and method of use

NASA Technical Reports Server (NTRS)

Barkhoudarian, Sarkis (Inventor); Kittinger, Scott A. (Inventor)

2006-01-01

The engine spectrometer probe and method of using the same of the present invention provides a simple engine spectrometer probe which is both lightweight and rugged, allowing an exhaust plume monitoring system to be attached to a vehicle, such as the space shuttle. The engine spectrometer probe can be mounted to limit exposure to the heat and debris of the exhaust plume. The spectrometer probe 50 comprises a housing 52 having an aperture 55 and a fiber optic cable 60 having a fiber optic tip 65. The fiber optic tip 65 has an acceptance angle 87 and is coupled to the aperture 55 so that the acceptance angle 87 intersects the exhaust plume 30. The spectrometer probe can generate a spectrum signal from light in the acceptance angle 506 and the spectrum signal can be provided to a spectrometer 508.

Performance of bent-crystal x-ray microscopes for high energy density physics research

DOE PAGES

Schollmeier, Marius S.; Geissel, Matthias; Shores, Jonathon E.; ...

2015-05-29

We present calculations for the field of view (FOV), image fluence, image monochromaticity, spectral acceptance, and image aberrations for spherical crystal microscopes, which are used as self-emission imaging or backlighter systems at large-scale high energy density physics facilities. Our analytic results are benchmarked with ray-tracing calculations as well as with experimental measurements from the 6.151 keV backlighter system at Sandia National Laboratories. Furthermore, the analytic expressions can be used for x-ray source positions anywhere between the Rowland circle and object plane. We discovered that this enables quick optimization of the performance of proposed but untested, bent-crystal microscope systems to findmore » the best compromise between FOV, image fluence, and spatial resolution for a particular application.« less

MEMS based digital transform spectrometers

NASA Astrophysics Data System (ADS)

Geller, Yariv; Ramani, Mouli

2005-09-01

Earlier this year, a new breed of Spectrometers based on Micro-Electro-Mechanical-System (MEMS) engines has been introduced to the commercial market. The use of these engines combined with transform mathematics, produces powerful spectrometers at unprecedented low cost in various spectral regions.

High spectral resolution of gamma-rays at room temperature by perovskite CsPbBr 3 single crystals

DOE PAGES

He, Yihui; Matei, Liviu; Jung, Hee Joon; ...

2018-04-23

Gamma-ray detection and spectroscopy is the quantitative determination of their energy spectra, and is of critical value and critically important in diverse technological and scientific fields. Here we report an improved melt growth method for cesium lead bromide and a special detector design with asymmetrical metal electrode configuration that leads to a high performance at room temperature. As-grown centimeter-sized crystals possess extremely low impurity levels (below 10 p.p.m. for total 69 elements) and detectors achieve 3.9% energy resolution for 122 keV 57Co gamma-ray and 3.8% for 662 keV 137Cs gamma-ray. Cesium lead bromide is unique among all gamma-ray detection materialsmore » in that its hole transport properties are responsible for the high performance. The superior mobility-lifetime product for holes (1.34 × 10 –3 cm 2 V –1) derives mainly from the record long hole carrier lifetime (over 25 μs). Here, the easily scalable crystal growth and high-energy resolution, highlight cesium lead bromide as an exceptional next generation material for room temperature radiation detection.« less

High spectral resolution of gamma-rays at room temperature by perovskite CsPbBr 3 single crystals

DOE Office of Scientific and Technical Information (OSTI.GOV)

He, Yihui; Matei, Liviu; Jung, Hee Joon

Gamma-ray detection and spectroscopy is the quantitative determination of their energy spectra, and is of critical value and critically important in diverse technological and scientific fields. Here we report an improved melt growth method for cesium lead bromide and a special detector design with asymmetrical metal electrode configuration that leads to a high performance at room temperature. As-grown centimeter-sized crystals possess extremely low impurity levels (below 10 p.p.m. for total 69 elements) and detectors achieve 3.9% energy resolution for 122 keV 57Co gamma-ray and 3.8% for 662 keV 137Cs gamma-ray. Cesium lead bromide is unique among all gamma-ray detection materialsmore » in that its hole transport properties are responsible for the high performance. The superior mobility-lifetime product for holes (1.34 × 10 –3 cm 2 V –1) derives mainly from the record long hole carrier lifetime (over 25 μs). Here, the easily scalable crystal growth and high-energy resolution, highlight cesium lead bromide as an exceptional next generation material for room temperature radiation detection.« less

Determination of glucose concentrations using photonic crystal LEDs

NASA Astrophysics Data System (ADS)

Liao, Yu-Yang; Chen, Yung-Tsan; Chang, Cheng-Yu; Lan, Wen-Yi; Huang, Jian-Jang

2016-09-01

As internet of things (IOT) has become a popular topic in current consumer electronics, there is a demand for cost-effective sensors to monitor bio-signals. Traditional optical sensors employ low-dimensional gratings and high-resolution spectrometers to detect the refractive index changes of the solutions. In this work, we develop an alternative approach to correlate the concentration of molecules to the band diagrams of the photonic crystals. A relatively low-resolution spectrum analyzer can be employed, yet achieves higher sensitivity than traditional approaches.

Sample rotating turntable kit for infrared spectrometers

DOEpatents

Eckels, Joel Del [Livermore, CA; Klunder, Gregory L [Oakland, CA

2008-03-04

An infrared spectrometer sample rotating turntable kit has a rotatable sample cup containing the sample. The infrared spectrometer has an infrared spectrometer probe for analyzing the sample and the rotatable sample cup is adapted to receive the infrared spectrometer probe. A reflectance standard is located in the rotatable sample cup. A sleeve is positioned proximate the sample cup and adapted to receive the probe. A rotator rotates the rotatable sample cup. A battery is connected to the rotator.

A technique for measuring the quality of an elliptically bent pentaerythritol [PET(002)] crystal

DOE PAGES

Haugh, M. J.; Jacoby, K. D.; Barrios, M. A.; ...

2016-08-23

Here, we present a technique for determining the X-ray spectral quality from each region of an elliptically curved PET(002) crystal. The investigative technique utilizes the shape of the crystal rocking curve which changes significantly as the radius of curvature changes. This unique quality information enables the spectroscopist to verify where in the spectral range that the spectrometer performance is satisfactory and where there are regions that would show spectral distortion. A collection of rocking curve measurements for elliptically curved PET(002) has been built up in our X-ray laboratory. The multi-lamellar model from the XOP software has been used as amore » guide and corrections were applied to the model based upon measurements. But, the measurement of RI at small radius of curvature shows an anomalous behavior; the multi-lamellar model fails to show this behavior. The effect of this anomalous RI behavior on an X-ray spectrometer calibration is calculated. It is compared to the multi-lamellar model calculation which is completely inadequate for predicting RI for this range of curvature and spectral energies.« less

A technique for measuring the quality of an elliptically bent pentaerythritol [PET(002)] crystal

NASA Astrophysics Data System (ADS)

Haugh, M. J.; Jacoby, K. D.; Barrios, M. A.; Thorn, D.; Emig, J. A.; Schneider, M. B.

2016-11-01

We present a technique for determining the X-ray spectral quality from each region of an elliptically curved PET(002) crystal. The investigative technique utilizes the shape of the crystal rocking curve which changes significantly as the radius of curvature changes. This unique quality information enables the spectroscopist to verify where in the spectral range that the spectrometer performance is satisfactory and where there are regions that would show spectral distortion. A collection of rocking curve measurements for elliptically curved PET(002) has been built up in our X-ray laboratory. The multi-lamellar model from the XOP software has been used as a guide and corrections were applied to the model based upon measurements. But, the measurement of RI at small radius of curvature shows an anomalous behavior; the multi-lamellar model fails to show this behavior. The effect of this anomalous RI behavior on an X-ray spectrometer calibration is calculated. It is compared to the multi-lamellar model calculation which is completely inadequate for predicting RI for this range of curvature and spectral energies.

Pyroelectric Crystal Accelerator In The Department Of Physics And Nuclear Engineering At West Point

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gillich, Don; Kovanen, Andrew; Anderson, Tom

The Nuclear Science and Engineering Research Center (NSERC), a Defense Threat Reduction Agency (DTRA) office located at the United States Military Academy (USMA), sponsors and manages cadet and faculty research in support of DTRA objectives. The NSERC has created an experimental pyroelectric crystal accelerator program to enhance undergraduate education at USMA in the Department of Physics and Nuclear Engineering. This program provides cadets with hands-on experience in designing their own experiments using an inexpensive tabletop accelerator. This device uses pyroelectric crystals to ionize and accelerate gas ions to energies of {approx}100 keV. Within the next year, cadets and faculty atmore » USMA will use this device to create neutrons through the deuterium-deuterium (D-D) fusion process, effectively creating a compact, portable neutron generator. The double crystal pyroelectric accelerator will also be used by students to investigate neutron, x-ray, and ion spectroscopy.« less

Electro-Optical Imaging Fourier-Transform Spectrometer

NASA Technical Reports Server (NTRS)

Chao, Tien-Hsin; Zhou, Hanying

2006-01-01

An electro-optical (E-O) imaging Fourier-transform spectrometer (IFTS), now under development, is a prototype of improved imaging spectrometers to be used for hyperspectral imaging, especially in the infrared spectral region. Unlike both imaging and non-imaging traditional Fourier-transform spectrometers, the E-O IFTS does not contain any moving parts. Elimination of the moving parts and the associated actuator mechanisms and supporting structures would increase reliability while enabling reductions in size and mass, relative to traditional Fourier-transform spectrometers that offer equivalent capabilities. Elimination of moving parts would also eliminate the vibrations caused by the motions of those parts. Figure 1 schematically depicts a traditional Fourier-transform spectrometer, wherein a critical time delay is varied by translating one the mirrors of a Michelson interferometer. The time-dependent optical output is a periodic representation of the input spectrum. Data characterizing the input spectrum are generated through fast-Fourier-transform (FFT) post-processing of the output in conjunction with the varying time delay.

Diffusive transport of several hundred keV electrons in the Earth's slot region

NASA Astrophysics Data System (ADS)

Ma, Q.; Li, W.; Thorne, R. M.; Bortnik, J.

2017-12-01

We investigate the gradual diffusion of energetic electrons from the inner edge of the outer radiation belt into the slot region. The Van Allen Probes observed slow inward diffusion and decay of 200-600 keV electrons following the intense geomagnetic storm that occurred on 17 March 2013. During the 10-day non-disturbed period following the storm, the peak of electron fluxes gradually moved from L 2.7 to L 2.4, and the flux levels decreased by a factor of 2-4 depending on the electron energy. We simulated the radial intrusion and decay of electrons using a 3-dimentional diffusion code, which reproduced the energy-dependent transport of electrons from 100 keV to 1 MeV in the slot region. At energies of 100-200 keV, the electrons experience fast transport across the slot region due to the dominance of radial diffusion; at energies of 200-600 keV, the electrons gradually diffuse and decay in the slot region due to the comparable radial diffusion rate and pitch angle scattering rate by plasmaspheric hiss; at energies of E > 700 keV, the electrons stopped diffusing near the inner edge of outer radiation belt due to the dominant pitch angle scattering loss. In addition to plasmaspheric hiss, magnetosonic waves and VLF waves can cause the loss of high pitch angle electrons, relaxing the sharp `top-hat' shaped pitch angle distributions created by plasmaspheric hiss. Our simulation indicates the importance of radial diffusion and pitch angle scattering in forming the diffusive intrusion of energetic electrons across the slot region.

Development of a Silicon Drift Detector Array: An X-Ray Fluorescence Spectrometer for Remote Surface Mapping

NASA Technical Reports Server (NTRS)

Gaskin, Jessica A.; Carini, Gabriella A.; Wei, Chen; Elsner, Ronald F.; Kramer, Georgiana; De Geronimo, Gianluigi; Keister, Jeffrey W.; Zheng, Li; Ramsey, Brian D.; Rehak, Pavel;

A sealed titanium window proportional counter for the detection of .5-keV X rays.

NASA Technical Reports Server (NTRS)

Mcclintock, J. E.; Levine, A.; Rappaport, S.

1972-01-01

A sealed Ti window proportional counter sensitive to X radiation in the energy range 0.35-0.45 keV and above 1.5 keV is described. Measurements of the Ti mass absorption coefficients and a graphical summary of the literature values are presented. For a proportional counter with a 930 microgram/sq cm (2.1-micron) Ti window, the peak efficiency at 0.45 keV is found to lie between 4.6% and 7.1%. An application in X-ray astronomy involving a rocket observation of Sco X-1 is discussed.

Scintillation characterization of the pure Tl2LiGdBr6 single crystal

NASA Astrophysics Data System (ADS)

Jang, Jonghun; Rooh, Gul; Kim, Sunghwan; Kim, HongJoo

2018-05-01

A pure Tl2LiGdBr6 (TLGB) single crystal was developed. This scintillator was grown by the two-zone vertical Bridgman technique. Owing to the improvement in the crystal quality of TLGB, excellent scintillation properties were observed. The characterization of this scintillation material was carried out under X- and γ-ray excitations. In the X-ray excitation emission spectrum, the Tl+ ion emission band was observed between 390 and 550 nm and peaked at 435 nm. Under 662 keV γ-ray excitation, the energy resolution and light yield of the grown sample were measured to be 7.2% (FWHM) and 27,000 ± 2,700 ph/MeV, respectively. In addition, under the same γ-ray excitation, scintillation decay time was also measured at room temperature. Three decay time components were found to be 56 ns (24%), 105 ns (53%), and 1.5 µs (23%). Further improvements in scintillation properties are expected with the good quality crystal of this compound.

Impact of Lu/Gd ratio and activator concentration on structure and scintillation properties of LGSO:Ce crystals

NASA Astrophysics Data System (ADS)

Sidletskiy, O.; Bondar, V.; Grinyov, B.; Kurtsev, D.; Baumer, V.; Belikov, K.; Katrunov, K.; Starzhinsky, N.; Tarasenko, O.; Tarasov, V.; Zelenskaya, O.

2010-02-01

We have studied the dependence of structural and scintillation characteristics of Lu 2 xGd 2-2 xSiO 5:Ce (LGSO:Ce) crystals on cation composition. LGSO:Ce crystals at x=0-1 have been obtained by the Czochralski method. We report here a strong correlation between ionic radii of trivalent cations and their distribution between non-equivalent sites in lattice. By choosing the optimal Lu/Gd ratio and Ce concentration we were able to obtain the light output by˜70%, as compared to LSO:Ce crystals, and energy resolution ˜7 at% 662 KeV ( 137Cs); the afterglow level was decreased by 1-3 orders of magnitude as compared to LSO:Ce. We also discuss the possible mechanisms of control on scintillation characteristics of mixed orthosilicates.

Precise rise and decay time measurements of inorganic scintillators by means of X-ray and 511 keV excitation

NASA Astrophysics Data System (ADS)

Gundacker, S.; Turtos, R. M.; Auffray, E.; Lecoq, P.

2018-05-01

The emergence of new solid-state avalanche photodetectors, e.g. SiPMs, with unprecedented timing capabilities opens new ways to profit from ultrafast and prompt photon emission in scintillators. In time of flight positron emission tomography (TOF-PET) and high energy timing detectors based on scintillators the ultimate coincidence time resolution (CTR) achievable is proportional to the square root of the scintillation rise time, decay time and the reciprocal light yield, CTR ∝√{τrτd / LY }. Hence, the precise study of light emission in the very first tens of picoseconds is indispensable to understand time resolution limitations imposed by the scintillator. We developed a time correlated single photon counting setup having a Gaussian impulse response function (IRF) of 63ps sigma, allowing to precisely measure the scintillation rise time of various materials with 511keV excitation. In L(Y)SO:Ce we found two rise time components, the first below the resolution of our setup <10 ps and a second component being ∼380 ps. Co-doping with Ca2+ completely suppresses the slow rise component leading to a very fast initial scintillation emission with a rise time of <10ps. A very similar behavior is observed in LGSO:Ce crystals. The results are further confirmed by complementary measurements using a streak-camera system with pulsed X-ray excitation and additional 511 keV excited measurements of Mg2+ co-doped LuAG:Ce, YAG:Ce and GAGG:Ce samples.

Design, implementation, and performance of the Astro-H soft x-ray spectrometer aperture assembly and blocking filters

NASA Astrophysics Data System (ADS)