Solid Lubrication Fundamentals and Applications: Introduction and Background. Revision 1

NASA Technical Reports Server (NTRS)

Miyoshi, Kazuhisa

1998-01-01

This chapter presents an introduction and historical background to the field of tribology, especially solid lubrication and lubricants and sets them in the perspective of techniques and materials in lubrication. Also, solid and liquid lubrication films are defined and described.

Solid Lubrication Fundamentals and Applications. Chapter 1; Introduction and Background

NASA Technical Reports Server (NTRS)

Miyoshi, Kazuhisa

1996-01-01

This chapter presents an introduction and historical background to the field of tribology, especially solid lubrication and lubricants and sets them in the perspective of techniques and materials in lubrication. Also, solid and liquid lubrication films are defined and described.

A New Type of Self-lubricated Thermal Spray Coatings: Liquid Lubricants Embedded in a Metal Matrix

NASA Astrophysics Data System (ADS)

Espallargas, N.; Armada, S.

2015-01-01

Oils and greases are commonly used for lubricating, rotating and sliding systems such as bearings, gears, connectors, etc. The maintenance of such lubricated systems in some applications where access is difficult (e.g., offshore wind farms and subsea equipment) increases the operational costs. In some cases, it can be thought that the use of solid lubricants (MoS2, PTFE, graphite, etc.) embedded in coatings could be a solution for such applications; however, the mechanical and dynamic conditions of most of the systems are not appropriate for solid lubricants. Despite this, solid lubricants such as PTFE and MoS2 have been largely employed in different industries, especially in those applications where liquid lubricants cannot be used and when the dynamic conditions allow for it. Self-lubricated coatings have been a major topic of interest in thermal spray in the last decades. Although the use of liquid lubricants is desirable whenever it is possible, limited research has been addressed toward the development of self-lubricated coatings containing liquid lubricants. One of the main reasons for this is due to the complexity of embedding liquid lubricant reservoirs inside the coating matrix. In the present work, a new type of liquid-solid self-lubricated coatings is presented, being the matrix a metal alloy. Three thermal spray techniques used were as follows: arc-spray, plasma spray, and HVOAF. The metal matrices were two stainless steel types and liquid lubricant-filled capsules with different liquid contents were used. No degradation of the capsules during spraying was observed and the coatings containing capsules were able to keep a low coefficient of friction. The optimal performance is found for the coatings obtained at the lowest spraying temperature and velocity.

Evaluation of PS 212 Coatings Under Boundary Lubrication Conditions with an Ester-based Oil to 300 C

NASA Technical Reports Server (NTRS)

Sliney, Harold E.; Loomis, William R.; Dellacorte, Christopher

1994-01-01

High friction and wear of turbine engine components occur during high temperature excursions above the oxidation threshold of the liquid lubricant. This paper reports on research to study the use of a high temperature self lubricating coating, PS 212 for back-up lubrication in the event of failure of the liquid lubricant. Pin on disk tests were performed under dry and boundary-lubricated conditions at disk temperatures up to 300 C. The liquid lubricant was a formulated polyol ester qualified under MIL L-23699. At test temperatures above the oil's thermal degradation level, the use of PS 212 reduced wear, providing a back-up lubricant effect.

Automotive gear oil lubricant from soybean oil

USDA-ARS?s Scientific Manuscript database

The use of lubricants that are based on renewable materials is rapidly increasing. Vegetable oils have good lubricity, wear protection and low volatility which are desired properties for automotive gear lubricant applications. Soybean oil is used widely in the lubricant industry due to its properti...

Lubrication Of Nonconformal Contacts

NASA Technical Reports Server (NTRS)

Jeng, Yeau-Ren

1991-01-01

Report discusses advances in knowledge of lubrication of nonconformal contacts in bearings and other machine elements. Reviews previous developments in theory of lubrication, presents advances in theory of lubrication to determine minimum film thickness, and describes experiments designed to investigate one of regimes of lubrication for ball bearings.

Tribological properties and lubrication mechanism of in situ graphene-nickel matrix composite impregnated with lubricating oil

NASA Astrophysics Data System (ADS)

Lei, Yu; Du, Jinfang; Pang, Xianjuan; Wang, Haizhong; Yang, Hua; Jiang, Jinlong

2018-05-01

A solid-liquid synergetic lubricating system has been designed to develop a novel self-lubricating nickel matrix composite. The graphene-nickel (G-Ni) matrix composite with porous structure was fabricated by in situ growing graphene in bulk nickel using a powder metallurgy method. The porous structures of the composite were used to store polyalphaolefin (PAO) oil for self-lubricating. It is found that the G-Ni matrix composite under oil lubrication condition exhibited superior tribological properties as compared to pure nickel and the composite under dry sliding condition. The prestored oil was released from pores to the sliding surface forming a lubricating oil film during friction process. This lubricating oil film can protect the worn surface from severe oxidation, and help the formation and transfer of a carbon-based solid tribofilm derived from graphene and lubricating oil. This solid (graphene)-liquid (oil) synergistic lubricating mechanism is responsible for the reduction of friction coefficient and improvement of wear resistance of the in situ fabricated G-Ni matrix composite.

A Systems Approach to the Solid Lubrication of Foil Air Bearings for Oil-Free Turbomachinery

NASA Technical Reports Server (NTRS)

DellaCorte, Christopher; Zaldana, Antonio R.; Radil, Kevin C.

2002-01-01

Foil air bearings are self-acting hydrodynamic bearings which rely upon solid lubricants to reduce friction and minimize wear during sliding which occurs at start-up and shut-down when surface speeds are too low to allow the formation of a hydrodynamic air film. This solid lubrication is typically accomplished by coating the non-moving foil surface with a thin, soft polymeric film. The following paper introduces a systems approach in which the solid lubrication is provided by a combination of self lubricating shaft coatings coupled with various wear resistant and lubricating foil coatings. The use of multiple materials, each providing different functions is modeled after oil-lubricated hydrodynamic sleeve bearing technology which utilizes various coatings and surface treatments in conjunction with oil lubricants to achieve optimum performance. In this study, room temperature load capacity tests are performed on journal foil air bearings operating at 14,000 rpm. Different shaft and foil coating technologies such as plasma sprayed composites, ceramic, polymer and inorganic lubricant coatings are evaluated as foil bearing lubricants. The results indicate that bearing performance is improved through the individual use of the lubricants and treatments tested. Further, combining several solid lubricants together yielded synergistically better results than any material alone.

Interdisciplinary Approach to Liquid Lubricant Technology

NASA Technical Reports Server (NTRS)

Ku, P. M. (Editor)

1973-01-01

The proceedings of a conference of liquid lubricant technology are presented. The subjects discussed are: (1) requirements and functions of liquid lubricants, (2) mineral oils, (3) greases, (4) theory of rheology, (5) mechanics and thermodynamics in lubrication, (6) environmental capability of liquid lubricants, and (7) wear corrosion and erosion.

Solid lubricant materials for high temperatures: A review

NASA Technical Reports Server (NTRS)

Sliney, Harold E.

1985-01-01

Solid lubricants that can be used above 300 C in air are discussed, including coatings and self-lubricating composite bearing materials. The lubricants considered are representative dichalcogenides, graphite, graphite fluoride, polyimides, soft oxides, oxidatively stable fluorides, and hard coating materials. A few general design considerations revelant to solid lubrication are interspersed.

Method to improve lubricity of low-sulfur diesel and gasoline fuels

DOEpatents

Erdemir, Ali

2004-08-31

A method for providing lubricity in fuels and lubricants includes adding a boron compound to a fuel or lubricant to provide a boron-containing fuel or lubricant. The fuel or lubricant may contain a boron compound at a concentration between about 30 ppm and about 3,000 ppm and a sulfur concentration of less than about 500 ppm. A method of powering an engine to minimize wear, by burning a fuel containing boron compounds. The boron compounds include compound that provide boric acid and/or BO.sub.3 ions or monomers to the fuel or lubricant.

Tribology and energy efficiency: from molecules to lubricated contacts to complete machines.

PubMed

Taylor, Robert Ian

2012-01-01

The impact of lubricants on energy efficiency is considered. Molecular details of base oils used in lubricants can have a great impact on the lubricant's physical properties which will affect the energy efficiency performance of a lubricant. In addition, molecular details of lubricant additives can result in significant differences in measured friction coefficients for machine elements operating in the mixed/boundary lubrication regime. In single machine elements, these differences will result in lower friction losses, and for complete systems (such as cars, trucks, hydraulic circuits, industrial gearboxes etc.) lower fuel consumption or lower electricity consumption can result.

Microfog lubricant application system for advanced turbine engine components, phase 3. [wetting characteristics and deposit forming tendencies of lubricants

NASA Technical Reports Server (NTRS)

Petrucco, R. J.; Leonardi, S. J.

1973-01-01

The wetting characteristics and deposit forming tendencies of a series of lubricants were evaluated using a microfog jet delivery system to wet a flat heated rotating disc. The performances of the nine lubricants are discussed in terms of the various testing parameters which include temperature, disc speed and lubricant gas flow rates. Also discussed are the heat transfer characteristics of two of the lubricants on that same plane disc specimen. The wetting characteristics and heat transfer characteristics of one of the lubricants on a complex disc simulating bearing geometry are also discussed.

Pulsed Plasma Lubrication Device and Method

NASA Technical Reports Server (NTRS)

Hofer, Richard R. (Inventor); Bickler, Donald B. (Inventor); D'Agostino, Saverio A. (Inventor)

2016-01-01

Disclosed herein is a lubrication device comprising a solid lubricant disposed between and in contact with a first electrode and a second electrode dimensioned and arranged such that application of an electric potential between the first electrode and the second electrode sufficient to produce an electric arc between the first electrode and the second electrode to produce a plasma in an ambient atmosphere at an ambient pressure which vaporizes at least a portion of the solid lubricant to produce a vapor stream comprising the solid lubricant. Methods to lubricate a surface utilizing the lubrication device in-situ are also disclosed.

High performance solid and liquid lubricants: An industrial guide

NASA Technical Reports Server (NTRS)

Mcmurtrey, Ernest L.

1987-01-01

This handbook is intended to provide a ready reference for many of the solid and liquid lubricants used in the space industry. Lubricants and lubricant properties are arranged systematically so that designers, engineers, and maintenance personnel can conveniently locate data needed for their work. This handbook is divided into two major parts (A and B). Part A is a compilation of solid lubricant suppliers information on chemical and physical property of data of more than 250 solid lubricants, bonded solid lubricants, dispersions, and composites. Part B is a compilation of chemical and physical property data of more than 250 liquid lubricants, greases, oils, compounds, and fluids. The listed materials cover a broad spectrum from manufacturing and ground support to hardware applications of spacecraft.

Lubrication with solids.

NASA Technical Reports Server (NTRS)

Buckley, D. H.; Johnson, R. L.

1972-01-01

Brief discussion of the historical background, variety range, chemistry, physics, and other properties of solid lubricants, and review of their current uses. The widespread use of solid lubricants did not occur until about 1947. At present, they are the object of such interest that a special international conference on their subject was held in 1971. They are used at temperatures beyond the useful range of conventional lubricating oils and greases. Their low volatility provides them with the capability of functioning effectively in vacuum and invites their use in space applications. Their high load carrying ability makes them useful with heavily loaded components. Solid lubricants, however, do lack some of the desirable properties of conventional lubricants. Unlike oils and greases, which have fluidity and can continuously be carried back into contact with lubricated surfaces, solid lubricants, because of their immobility, have finite lives. Also, oils and greases can carry away frictional heat from contacting surfaces, while solid lubricants cannot.

On the lubrication mechanism of detonation-synthesis nanodiamond additives in lubricant composites

NASA Astrophysics Data System (ADS)

Shepelevskii, A. A.; Esina, A. V.; Voznyakovskii, A. P.; Fadin, Yu. A.

2017-09-01

The lubrication of detonation-synthesis diamond additives in lubricant composites has been discussed. The mechanism of interaction between nanodiamonds and friction surface has been shown to depend on the applied load. Two models of the lubrication of nanodiamonds and the conditions for their validity have also been proposed.

USDOE Top-of-Rail Lubricant Project

DOE Office of Scientific and Technical Information (OSTI.GOV)

Mohumad F. Alzoubi; George R. Fenske; Robert A. Erck

2002-02-01

Lubrication of wheel/rail systems has been recognized for the last two decades as a very important issue for railroads. Energy savings and less friction and wear can be realized if a lubricant can be used at the wheel/rail interface. On the other hand, adverse influences are seen in operating and wear conditions if improper or excessive lubrication is used. Also, inefficiencies in lubrication need to be avoided for economic and environmental reasons. The top-of-rail (TOR) lubricant concept was developed by Texaco Corporation to lubricate wheels and rails effectively and efficiently. Tranergy Corporation has been developing its SENTRAEN 2000{trademark} lubrication systemmore » for the last ten years, and this revolutionary new high-tech on-board rail lubrication system promises to dramatically improve the energy efficiency, performance, safety, and track environment of railroads. The system is fully computer-controlled and ensures that all of the lubricant is consumed as the end of the train passes. Lubricant quantity dispensed is a function of grade, speed, curve, and axle load. Tranergy also has its LA4000{trademark} wheel and rail simulator, a lubrication and traction testing apparatus. The primary task of this project was collecting and analyzing the volatile and semivolatile compounds produced as the lubricant was used. The volatile organic compounds were collected by Carbotrap cartridges and analyzed by adsorption and gas chromatography/mass spectrometry (GC/MS). The semivolatile fraction was obtained by collecting liquid that dripped from the test wheel. The collected material was also analyzed by GC/MS. Both of these analyses were qualitative. The results indicated that in the volatile fraction, the only compounds on the Environmental Protection Agency's (EPA) Superfund List of Analytes detected were contaminants either in the room air or from other potential contamination sources in the laboratory. Similarly, in the semivolatile fraction none of the detected compounds are on the EPA's Superfund List of Analytes. The major compound in the semivolatile fraction is 1,2-propanediol, which was also found as the major component of the TOR lubricant before testing. Other compounds found in trace quantities either were present in the TOR lubricant or were small fragments from the polymeric component of the TOR lubricant. The second task for Argonne in this project was to investigate the effects of axle load, angle of attack, and quantity of lubricant on lateral friction forces, as well as the consumption time of the TOR lubricant. The second task was to collect and qualitatively identify any volatile and semivolatile compounds produced upon use of the TOR lubricant.« less

Lubrication of Space Systems (c)

NASA Technical Reports Server (NTRS)

Fusaro, Robert L.

1995-01-01

This article presents an overview of the current state-of-the-art tribology, some current and future perceived space lubrication problem areas, and some potential new lubrication technologies. It is the author's opinion that tribology technology, in general, has not significantly advanced over the last 20 to 30 years, even though some incremental improvements in the technology have occurred. There is a better understanding of elasto-hydrodynamic lubrication, some new lubricating and wear theories have been developed, and some new liquid and solid lubricants have been formulated. However, the important problems of being able to lubricate reliably at high temperatures or at cryogenic temperatures have not been adequately address.

Self-lubricating polymer composites and polymer transfer film lubrication for space applications

NASA Technical Reports Server (NTRS)

Fusaro, Robert L.

1990-01-01

The use of self-lubricating polymers and polymer composites in space is somewhat limited today. In general, they are only used when other methods are inadequate. There is potential, however, for these materials to make a significant impact on future space missions if properly utilized. Some of the different polymers and fillers used to make self-lubricating composites are surveyed. The mechanisms of composite lubrication and wear, the theory behind transfer film lubricating mechanisms, and some factors which affect polymer composite wear and transfer are examined. In addition, some of the current space tribology application areas for self-lubricating polymer composites and polymer transfer are mentioned.

Water Lubrication of Stainless Steel using Reduced Graphene Oxide Coating

PubMed Central

Kim, Hae-Jin; Kim, Dae-Eun

2015-01-01

Lubrication of mechanical systems using water instead of conventional oil lubricants is extremely attractive from the view of resource conservation and environmental protection. However, insufficient film thickness of water due to low viscosity and chemical reaction of water with metallic materials have been a great obstacle in utilization of water as an effective lubricant. Herein, the friction between a 440 C stainless steel (SS) ball and a 440 C stainless steel (SS) plate in water lubrication could be reduced by as much as 6-times by coating the ball with reduced graphene oxide (rGO). The friction coefficient with rGO coated ball in water lubrication was comparable to the value obtained with the uncoated ball in oil lubrication. Moreover, the wear rate of the SS plate slid against the rGO coated ball in water lubrication was 3-times lower than that of the SS plate slid against the uncoated ball in oil lubrication. These results clearly demonstrated that water can be effectively utilized as a lubricant instead of oil to lower the friction and wear of SS components by coating one side with rGO. Implementation of this technology in mechanical systems is expected to aid in significant reduction of environmental pollution caused by the extensive use of oil lubricants. PMID:26593645

Water Lubrication of Stainless Steel using Reduced Graphene Oxide Coating.

PubMed

Kim, Hae-Jin; Kim, Dae-Eun

2015-11-23

Lubrication of mechanical systems using water instead of conventional oil lubricants is extremely attractive from the view of resource conservation and environmental protection. However, insufficient film thickness of water due to low viscosity and chemical reaction of water with metallic materials have been a great obstacle in utilization of water as an effective lubricant. Herein, the friction between a 440 C stainless steel (SS) ball and a 440 C stainless steel (SS) plate in water lubrication could be reduced by as much as 6-times by coating the ball with reduced graphene oxide (rGO). The friction coefficient with rGO coated ball in water lubrication was comparable to the value obtained with the uncoated ball in oil lubrication. Moreover, the wear rate of the SS plate slid against the rGO coated ball in water lubrication was 3-times lower than that of the SS plate slid against the uncoated ball in oil lubrication. These results clearly demonstrated that water can be effectively utilized as a lubricant instead of oil to lower the friction and wear of SS components by coating one side with rGO. Implementation of this technology in mechanical systems is expected to aid in significant reduction of environmental pollution caused by the extensive use of oil lubricants.

Water Lubrication of Stainless Steel using Reduced Graphene Oxide Coating

NASA Astrophysics Data System (ADS)

Kim, Hae-Jin; Kim, Dae-Eun

2015-11-01

Lubrication of mechanical systems using water instead of conventional oil lubricants is extremely attractive from the view of resource conservation and environmental protection. However, insufficient film thickness of water due to low viscosity and chemical reaction of water with metallic materials have been a great obstacle in utilization of water as an effective lubricant. Herein, the friction between a 440 C stainless steel (SS) ball and a 440 C stainless steel (SS) plate in water lubrication could be reduced by as much as 6-times by coating the ball with reduced graphene oxide (rGO). The friction coefficient with rGO coated ball in water lubrication was comparable to the value obtained with the uncoated ball in oil lubrication. Moreover, the wear rate of the SS plate slid against the rGO coated ball in water lubrication was 3-times lower than that of the SS plate slid against the uncoated ball in oil lubrication. These results clearly demonstrated that water can be effectively utilized as a lubricant instead of oil to lower the friction and wear of SS components by coating one side with rGO. Implementation of this technology in mechanical systems is expected to aid in significant reduction of environmental pollution caused by the extensive use of oil lubricants.

Solid lubrication design methodology, phase 2

NASA Technical Reports Server (NTRS)

Pallini, R. A.; Wedeven, L. D.; Ragen, M. A.; Aggarwal, B. B.

1986-01-01

The high temperature performance of solid lubricated rolling elements was conducted with a specially designed traction (friction) test apparatus. Graphite lubricants containing three additives (silver, phosphate glass, and zinc orthophosphate) were evaluated from room temperature to 540 C. Two hard coats were also evaluated. The evaluation of these lubricants, using a burnishing method of application, shows a reasonable transfer of lubricant and wear protection for short duration testing except in the 200 C temperature range. The graphite lubricants containing silver and zinc orthophosphate additives were more effective than the phosphate glass material over the test conditions examined. Traction coefficients ranged from a low of 0.07 to a high of 0.6. By curve fitting the traction data, empirical equations for slope and maximum traction coefficient as a function of contact pressure (P), rolling speed (U), and temperature (T) can be developed for each lubricant. A solid lubricant traction model was incorporated into an advanced bearing analysis code (SHABERTH). For comparison purposes, preliminary heat generation calculations were made for both oil and solid lubricated bearing operation. A preliminary analysis indicated a significantly higher heat generation for a solid lubricated ball bearing in a deep groove configuration. An analysis of a cylindrical roller bearing configuration showed a potential for a low friction solid lubricated bearing.

41 CFR 101-26.602-1 - Procurement of lubricating oils, greases, and gear lubricants.

Code of Federal Regulations, 2013 CFR

2013-07-01

... (nonaircraft) equipment and of aircraft engine oils on an annual program basis. Estimates of requirements for... program Due on or before Lubricating oils (nonaircraft) 4.1 November 15. Aircraft engine oils 4.2 June 15... lubricating oils, greases, and gear lubricants. 101-26.602-1 Section 101-26.602-1 Public Contracts and...

41 CFR 101-26.602-1 - Procurement of lubricating oils, greases, and gear lubricants.

Code of Federal Regulations, 2014 CFR

2014-07-01

... (nonaircraft) equipment and of aircraft engine oils on an annual program basis. Estimates of requirements for... program Due on or before Lubricating oils (nonaircraft) 4.1 November 15. Aircraft engine oils 4.2 June 15... lubricating oils, greases, and gear lubricants. 101-26.602-1 Section 101-26.602-1 Public Contracts and...

41 CFR 101-26.602-1 - Procurement of lubricating oils, greases, and gear lubricants.

Code of Federal Regulations, 2011 CFR

2011-07-01

... (nonaircraft) equipment and of aircraft engine oils on an annual program basis. Estimates of requirements for... program Due on or before Lubricating oils (nonaircraft) 4.1 November 15. Aircraft engine oils 4.2 June 15... lubricating oils, greases, and gear lubricants. 101-26.602-1 Section 101-26.602-1 Public Contracts and...

41 CFR 101-26.602-1 - Procurement of lubricating oils, greases, and gear lubricants.

Code of Federal Regulations, 2010 CFR

2010-07-01

... (nonaircraft) equipment and of aircraft engine oils on an annual program basis. Estimates of requirements for... program Due on or before Lubricating oils (nonaircraft) 4.1 November 15. Aircraft engine oils 4.2 June 15... lubricating oils, greases, and gear lubricants. 101-26.602-1 Section 101-26.602-1 Public Contracts and...

41 CFR 101-26.602-1 - Procurement of lubricating oils, greases, and gear lubricants.

Code of Federal Regulations, 2012 CFR

2012-07-01

... (nonaircraft) equipment and of aircraft engine oils on an annual program basis. Estimates of requirements for... program Due on or before Lubricating oils (nonaircraft) 4.1 November 15. Aircraft engine oils 4.2 June 15... lubricating oils, greases, and gear lubricants. 101-26.602-1 Section 101-26.602-1 Public Contracts and...

Assurance of lubricant supply in wet-lubricated space bearings

NASA Technical Reports Server (NTRS)

Glassow, F. A.

1976-01-01

Conventional lubrication techniques appear to be satisfactory, but rigorous proof of meeting a ten-year life requirement is lacking. One approach provides additional lubricant only when commanded from ground control, while the other passively augments lubrication at all times. Each technique has specific advantages, and selection should be related to the application to obtain optimum performance.

Lubricant reflow after laser heating in heat assisted magnetic recording

NASA Astrophysics Data System (ADS)

Wu, Haoyu; Mendez, Alejandro Rodriguez; Xiong, Shaomin; Bogy, David B.

2015-05-01

In heat assisted magnetic recording (HAMR) technology for hard disk drives, the media will be heated to about 500 °C during the writing process in order to reduce its magnetic coercivity and thus allow data writing with the magnetic head transducers. The traditional lubricants such as Z-dol and Z-tetraol may not be able to perform in such harsh heating conditions due to evaporation, decomposition and thermal depletion. However, some of the lubricant depletion can be recovered due to reflow after a period of time, which can help to reduce the chance of head disk interface failure. In this study, experiments of lubricant thermal depletion and reflow were performed using a HAMR test stage for a Z-tetraol type lubricant. Various lubricant depletion profiles were generated using different laser heating conditions. The lubricant reflow process after thermal depletion was monitored by use of an optical surface analyzer. In addition, a continuum based lubrication model was developed to simulate the lubricant reflow process. Reasonably good agreement between simulations and experiments was achieved.

Industry Needs Fulfilled by Patented NASA PS300 Solid Lubricant Technology

NASA Technical Reports Server (NTRS)

DellaCorte, Christopher

2003-01-01

In 1999, the NASA Glenn Research Center was awarded a patent (#5866518) for a new high-temperature solid lubricant coating material, PS300. A combination of wear-resistant metals and ceramics with solid lubricant additives, PS300 reduces friction and wear in sliding contacts from below ambient to over 650 C. This lubricant is an outgrowth of over three decades of high-temperature tribological research and was specifically developed as a shaft lubricant to protect foil air bearings used in Oil-Free turbomachinery, like gas turbines. Foil bearings are lubricated by air at high speeds but experience sliding and wear during initial startup and shut down when a lubricating film of air has not yet developed. PS300 shaft coatings have successfully lubricated foil bearings for over 100 000 cycles without wearing out.

Lubricant and additive effects on spur gear fatigue life

NASA Technical Reports Server (NTRS)

Townsend, D. P.; Zaretsky, E. V.; Scibbe, H. W.

1985-01-01

Spur gear endurance tests were conducted with six lubricants using a single lot of consumable-electrode vacuum melted (CVM) AISI 9310 spur gears. The sixth lubricant was divided into four batches each of which had a different additive content. Lubricants tested with a phosphorus-type load carrying additive showed a statistically significant improvement in life over lubricants without this type of additive. The presence of sulfur type antiwear additives in the lubricant did not appear to affect the surface fatigue life of the gears. No statistical difference in life was produced with those lubricants of different base stocks but with similar viscosity, pressure-viscosity coefficients and antiwear additives. Gears tested with a 0.1 wt % sulfur and 0.1 wt % phosphorus EP additives in the lubricant had reactive films that were 200 to 400 (0.8 to 1.6 microns) thick.

Effect of five lubricants on life of AISI 9310 spur gears

NASA Technical Reports Server (NTRS)

Townsend, D. P.; Zaretsky, E. V.

1985-01-01

Spur-gear surface fatigue tests were conducted with five lubricants using a single lot of consumable-electrode vacuum melted (CVM) AISI 9310 spur gears. The lot of gears was divided into five groups, each of which was tested with a different lubricant. The test lubricants are classified as either a synthetic hydrocarbon, mineral oil, or ester-based lubricant. All five lubricants have imilar viscosity and pressure-viscosity coefficients. A pentaerythritol base stock without sufficient antiwear additives produced a surface fatigue life pproximately 22 percent that of the same base stock with chlorine and phosphorus type additives. The presence of sulfur type antiwear additives in the lubricant did not appear to affect the surface fatigue life of the gears tested. No statistical difference in the 10-percent surface fatigue life was produced with four of the five lubricants.

Solid Lubricants for Oil-Free Turbomachinery

NASA Technical Reports Server (NTRS)

DellaCorte, Christopher

2005-01-01

Recent breakthroughs in gas foil bearing solid lubricants and computer based modeling has enabled the development of revolulionary Oil-Free turbomachinery systems. These innovative new and solid lubricants at low speeds (start-up and shut down). Foil bearings are hydrodynamic, self acting fluid film bearings made from thin, flexible sheet metal foils. These thin foils trap a hydrodynamic lubricating air film between their surfaces and moving shaft surface. For low temperature applications, like ainrafl air cycle machines (ACM's), polymer coatings provide important solid lubrication during start-up and shut down prior to the development of the lubricating fluid film. The successful development of Oil-Free gas turbine engines requires bearings which can operate at much higher temperatures (greater than 300 C). To address this extreme solid lubrication need, NASA has invented a new family of compostie solid lubricant coatings, NASA PS300.

Solid Lubricants and Coatings for Extreme Environments: State-of-the-Art Survey

NASA Technical Reports Server (NTRS)

Miyoshi, Kazuhisa

2007-01-01

An investigation was conducted to survey anticipated requirements for solid lubricants in lunar and Martian environments, as well as the effects of these environments on lubricants and their performance and durability. The success of habitats and vehicles on the Moon and Mars, and ultimately, of the human exploration of and permanent human presence on the Moon and Mars, are critically dependent on the correct and reliable operation of many moving mechanical assemblies and tribological components. The coefficient of friction and lifetime of any lubricant generally vary with the environment, and lubricants have very different characteristics under different conditions. It is essential, therefore, to select the right lubrication technique and lubricant for each mechanical and tribological application. Several environmental factors are hazardous to performance integrity on the Moon and Mars. Potential threats common to both the Moon and Mars are low ambient temperatures, wide daily temperature swings (thermal cycling), solar flux, cosmic radiation, and large quantities of dust. The surface of Mars has the additional challenges of dust storms, winds, and a carbon dioxide atmosphere. Solid lubricants and coatings are needed for lunar and Martian applications, where liquid lubricants are ineffective and undesirable, and these lubricants must perform well in the extreme environments of the Moon, Mars, and space, as well as on Earth, where they will be assembled and tested. No solid lubricants and coatings and their systems currently exist or have been validated that meet these requirements, so new solid lubricants must be designed and validated for these applications.

Surface profiles and modulation of ultra-thin perfluoropolyether lubricant in contact sliding

NASA Astrophysics Data System (ADS)

Sinha, S. K.; Kawaguchi, M.; Kato, T.

2004-08-01

Deformation in shear and associated tribological behaviours of ultra-thin lubricants are of significant importance for the lubrication of magnetic hard disks and for other applications such as micro-electromechanical systems, nano-fluidics and nanotechnology. This paper presents the characteristics of the perfluoropolyether ultra-thin lubricant, in terms of its surface profiles when subjected to a contact sliding test. The results indicate that for a several-monolayers thick (~4.0-4.5 nm) lubricant film, sliding produces a considerable amount of surface roughness due to peaks of lubricant that persist during sliding; however, it can flow back or return to a smooth profile after a lapse of time when the sliding is stopped. For a monolayer-thin (~1.4-1.57 nm) film, the lubricant flow is restricted, and the rough profile created due to sliding persists and almost becomes permanent on the wear track. During sliding, due to high shear stress, a characteristic feature of lubricant profile modulation is observed. This modulation, or waviness, is due to the accumulation of lubricant in piles or islands, giving certain amplitudes and frequencies, which themselves depend upon the percentage of lubricant molecules that are chemically bonded to the substrate and the lubricant thickness. The results indicate that ultra-thin lubricants (monolayer and thicker) behave more like a semi-solid (having some sliding characteristics similar to those of rubbers) than a liquid when subjected to a high shear rate during contact sliding.

Solid film lubricants and thermal control coatings flown aboard the EOIM-3 MDA sub-experiment

NASA Technical Reports Server (NTRS)

Murphy, Taylor J.; David, Kaia E.; Babel, Hank W.

1995-01-01

Additional experimental data were desired to support the selection of candidate thermal control coatings and solid film lubricants for the McDonnell Douglas Aerospace (MDA) Space Station hardware. The third Evaluation of Oxygen Interactions With Materials Mission (EOIM-3) flight experiment presented an opportunity to study the effects of the low Earth orbit environment on thermal control coatings and solid film lubricants. MDA provided five solid film lubricants and two anodic thermal control coatings for EOIM-3. The lubricant sample set consisted of three solid film lubricants with organic binders one solid film lubricant with an inorganic binder, and one solid film lubricant with no binder. The anodize coating sample set consisted of undyed sulfuric acid anodize and cobalt sulfide dyed sulfuric acid anodize, each on two different substrate aluminum alloys. The organic and inorganic binders in the solid film lubricants experienced erosion, and the lubricating pigments experienced oxidation. MDA is continuing to assess the effect of exposure to the low Earth orbit environment on the life and friction properties of the lubricants. Results to date support the design practice of shielding solid film lubricants from the low Earth orbit environment. Post-flight optical property analysis of the anodized specimens indicated that there were limited contamination effects and some atomic oxygen and ultraviolet radiation effects. These effects appeared to be within the values predicted by simulated ground testing and analysis of these materials, and they were different for each coating and substrate.

Slippery self-lubricating polymer surfaces

DOE Office of Scientific and Technical Information (OSTI.GOV)

Aizenberg, Joanna; Aizenberg, Michael; Cui, Jiaxi

The present disclosure describes a strategy to create self-healing, slippery self-lubricating polymers. Lubricating liquids with affinities to polymers can be utilized to get absorbed within the polymer and form a lubricant layer (of the lubricating liquid) on the polymer. The lubricant layer can repel a wide range of materials, including simple and complex fluids (water, hydrocarbons, crude oil and bodily fluids), restore liquid-repellency after physical damage, and resist ice, microorganisms and insects adhesion. Some exemplary applications where self-lubricating polymers will be useful include energy-efficient, friction-reduction fluid handling and transportation, medical devices, anti-icing, optical sensing, and as self-cleaning, and anti-fouling materialsmore » operating in extreme environments.« less

Method of removing an immiscible lubricant from a refrigeration system and apparatus for same

DOEpatents

Spauschus, Hans O.; Starr, Thomas L.

1999-01-01

A method of separating an immiscible lubricant from a liquid refrigerant in a refrigerating system including a compressor, a condenser, an expansion device and an evaporator, wherein the expansion device is connected to the condenser by a liquid refrigerant flow line for liquid refrigerant and immiscible lubricant. The method comprising slowing the rate of flow of the liquid refrigerant and immiscible lubricant between the condenser and the expansion device such that the liquid refrigerant and the immiscible lubricant separate based upon differences in density. The method also comprises collecting the separated immiscible lubricant in a collection chamber in fluid communication with the separated immiscible lubricant. Apparatus for performing the method is also disclosed.

HYDROSTATIC PRESSURIZATION AND DEPLETION OF TRAPPED LUBRICANT POOL DURING CREEP CONTACT OF A RIPPLED INDENTER AGAINST A BIPHASIC ARTICULAR CARTILAGE LAYER

PubMed Central

Soltz, Michael A.; Basalo, Ines M.; Ateshian, Gerard A.

2010-01-01

This study presents an analysis of the contact of a rippled rigid impermeable indenter against a cartilage layer, which represents a first simulation of the contact of rough cartilage surfaces with lubricant entrapment. Cartilage was modeled with the biphasic theory for hydrated soft tissues, to account for fluid flow into or out of the lubricant pool. The findings of this study demonstrate that under contact creep, the trapped lubricant pool gets depleted within a time period on the order of seconds or minutes as a result of lubricant flow into the articular cartilage. Prior to depletion, hydrostatic fluid load across the contact interface may be enhanced by the presence of the trapped lubricant pool, depending on the initial geometry of the lubricant pool. According to friction models based on the biphasic nature of the tissue, this enhancement in fluid load support produces a smaller minimum friction coefficient than would otherwise be predicted without a lubricant pool. The results of this study support the hypothesis that trapped lubricant decreases the initial friction coefficient following load application, independently of squeeze-film lubrication effects. PMID:14618917

Liquid-Solid Self-Lubricated Coatings

NASA Astrophysics Data System (ADS)

Armada, S.; Schmid, R.; Equey, S.; Fagoaga, I.; Espallargas, N.

2013-02-01

Self-lubricated coatings have been a major topic of interest in thermal spray in the last decades. Self-lubricated coatings obtained by thermal spray are exclusively based on solid lubricants (PTFE, h-BN, graphite, MoS2, etc.) embedded in the matrix. Production of thermal spray coatings containing liquid lubricants has not yet been achieved because of the complexity of keeping a liquid in a solid matrix during the spraying process. In the present article, the first liquid-solid self-lubricating thermal spray coatings are presented. The coatings are produced by inserting lubricant-filled capsules inside a polymeric matrix. The goal of the coating is to release lubricant to the system when needed. The first produced coatings consisted solely of capsules for confirming the feasibility of the process. For obtaining such a coating, the liquid-filled capsules were injected in the thermal spray flame without any other feedstock material. Once the concept and the idea were proven, a polymer was co-sprayed together with the capsules to obtain a coating containing the lubricant-filled capsules distributed in the solid polymeric matrix. The coatings and the self-lubricated properties have been investigated by means of optical microscopy, Scanning Electron Microscopy, and tribological tests.

Next Generation Refrigeration Lubricants for Low Global Warming Potential/Low Ozone Depleting Refrigeration and Air Conditioning Systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hessell, Edward Thomas

The goal of this project is to develop and test new synthetic lubricants that possess high compatibility with new low ozone depleting (LOD) and low global warming potential (LGWP) refrigerants and offer improved lubricity and wear protection over current lubricant technologies. The improved compatibility of the lubricants with the refrigerants, along with improved lubricating properties, will resulted in lower energy consumption and longer service life of the refrigeration systems used in residential, commercial and industrial heating, ventilating and air-conditioning (HVAC) and refrigeration equipment.

The Stability of Lubricant Oil Acidity of Biogas Fuelled Engine due to Biogas Desulfurization

NASA Astrophysics Data System (ADS)

Gde Tirta Nindhia, Tjokorda; Wayan Surata, I.; Wardana, Ari

2017-05-01

This research is established for the purpose of the understanding the stability of the acidity of lubricant oil in biogas fuelled engine due to the absence of hydrogen sulfide (H2S). As was recognized that other than Methane (CH4), there are also other gas impurities in the biogas such as carbon dioxide (CO2), hydrogen sulfide (H2S), moisture (H2O) and ammonia (NH3). Due to H2S contents in the biogas fuel, the engine was found failure. This is caused by corrosion in the combustion chamber due to increase of lubricant acidity. To overcome this problem in practical, the lubricant is increased the pH to basic level with the hope will be decrease to normal value after several time use. Other method is by installing pH measurement sensor in the engine lubricant so that when lubricant is known turn to be acid, then lubricant replacement should be done. In this research, the effect of biogas desulfurization down to zero level to the acidity of lubricant oil in the four stroke engine was carried out with the hope that neutral lubrication oil to be available during running the engine. The result indicates that by eliminating H2S due desulfurization process, effect on stability and neutrality of pH lubricant. By this method the engine safety can be obtained without often replacement the lubricant oil.

Lubrication from mixture of boric acid with oils and greases

DOEpatents

Erdemir, Ali

1995-01-01

Lubricating compositions including crystalline boric acid and a base lubricant selected from oils, greases and the like. The lubricity of conventional oils and greases can also be improved by adding concentrates of boric acid.

Determination of Lubricants on Ball Bearings by FT-IR using an Integrating Sphere

NASA Technical Reports Server (NTRS)

Street, K. W.; Pepper, S. V.; Wright, A.

2003-01-01

The lifetime determination of space lubricants is done at our facility by accelerated testing. Several micrograms of lubricant are deposited on the surface of a ball by syringing tens of micro liters of dilute lubricant solution. The solvent evaporates and the mass of lubricant is determined by twenty weighings near the balance reliability limit. This process is timely but does not produce a good correlation between the mass of lubricant and the volume of solution applied, as would be expected. The amount of lubricant deposited on a ball can be determined directly by Fourier Transform - Infrared Spectroscopy using an integrating sphere. In this paper, we discuss reasons for choosing this methodology, optimization of quantification conditions and potential applications for the technique. The volume of lubricant solution applied to the ball gives better correlation to the IR intensity than does the weight.

Lubrication System Failure Baseline Testing on an Aerospace Quality Gear Mesh

NASA Technical Reports Server (NTRS)

Handschuh, Robert F.; Morales, Wilfredo

2000-01-01

Aerospace drive systems are required to survive a loss-of-lubrication test for qualification. In many cases emergency lubrication systems need to be designed and utilized to permit the drive system to pass this difficult requirement. The weight of emergency systems can adversely affect the mission capabilities of the aircraft. The possibility to reduce the emergency system weight through the use of mist lubrication will be described. Mist lubrication involves the delivery of a minute amount of an organic liquid as a vapor or fine mist in flowing compressed air to rubbing surfaces. At the rubbing surface, the vapor or mist reacts to form a solid lubricating film. The aim of this study was to establish a baseline for gear behavior under oil depleted conditions. A reactive vapor-mist lubrication method is described and proposed as a candidate emergency lubrication system.

The role of the micro environment on the tribological behavior of materials

NASA Technical Reports Server (NTRS)

Buckley, D. H.

1980-01-01

The properties of the environment which exert an influence upon adhesion, friction, wear, and lubrication of materials in solid state contact are discussed. The effect of the environment upon lubricants and lubricant properties is considered in relation to the interaction of the lubricant with the material surfaces in solid state contact and the ability of lubricants to provide protective surface films.

In situ lubricant degradation in Antarctic marine sediments. 1. Short-term changes.

PubMed

Thompson, Belinda A W; Davies, Noel W; Goldsworthy, Paul M; Riddle, Martin J; Snape, Ian; Stark, Jonathan S

2006-02-01

A large-scale, in situ experiment was set up near the Bailey Peninsula area (Casey Station, East Antarctica) to monitor the natural attenuation of synthetic lubricants in marine sediments over five years. Here, we report the short-term changes after 5 and 56 weeks. The lubricants tested were an unused and used Mobil lubricant (0W/40; Exxon Mobil, Irving, TX, USA) and a biodegradable alternative (0W/20; Fuchs Lubricants, Harvey, IL, USA). Clean sediment was collected, contaminated with the lubricants, and deployed by divers onto the seabed in a randomized block design. The sampled sediments were analyzed by gas chromatography-flame-ionization detector and gas chromatography-mass spectrometry with selective ion monitoring. The base fluid of all lubricant treatments did not decrease significantly after 56 weeks in situ. Alkanoate esters of 1,1,1-tris(hydroxymethyl)propane in the biodegradable and unused lubricants were degraded extensively in situ; however, these esters constituted only a minor proportion of the lubricant volume. The additives, alkylated naphthalenes and substituted diphenylamines, were fairly resistant to degradation, which is of environmental concern because of their toxicity. The biodegradable lubricant did not break down to recognized biodegradable thresholds and, as such, should not be classified as biodegradable under Antarctic marine conditions. A separate experiment was conducted to determine the influence of sediment preparation and deployment on compound ratios within the lubricants, and we found that preparation and deployment of the contaminated sediments had only a minor effect on compound recovery. Further monitoring of this in situ experiment will provide much needed information about the long-term natural attenuation of lubricants.

Hexagonal boron nitride as a tablet lubricant and a comparison with conventional lubricants.

PubMed

Uğurlu, Timuçin; Turkoğlu, Murat

2008-04-02

The objective of this study was to investigate the lubrication properties of hexagonal boron nitride (HBN) as a new tablet lubricant and compare it with conventional lubricants such as magnesium stearate (MGST), stearic acid (STAC), and glyceryl behenate (COMP). Tablets were manufactured on an instrumented single-station tablet press to monitor lower punch ejection force (LPEF) containing varied lubricants in different ratio (0.5, 1, 2%). Tablet crushing strength, disintegration time and thickness were measured. Tensile strength of compacted tablets were measured by applying a diametrical load across the edge of tablets to determine mechanical strength. The deformation mechanism of tablets was studied during compression from the Heckel plots with or without lubricants. MGST was found to be the most effective lubricant based on LPEF-lubrication concentration profile and LPEF of HBN was found very close to that of MGST. HBN was better than both STAC and COMP. A good lubrication was obtained at 0.5% for MGST and HBN (189 and 195N, respectively). Where COMP and STAC showed 20 and 35% more LPEF compare to that of MGST (239 and 288N, respectively). Even at the concentration of 2% COMP and STAC did not decrease LPEF as much as 0.5% of MGST and HBN. Like all conventional lubricants the higher the concentration of HBN the lower the mechanical properties of tablets because of its hydrophobic character. However, this deterioration was not as pronounced as MGST. HBN had no significant effect on tablet properties. Based on the Heckel plots, it was observed that after the addition of 1% lubricant granules showed less plastic deformation.

Method of removing an immiscible lubricant from a refrigeration system and apparatus for same

DOEpatents

Spauschus, H.O.; Starr, T.L.

1999-03-30

A method is described for separating an immiscible lubricant from a liquid refrigerant in a refrigerating system including a compressor, a condenser, an expansion device and an evaporator, wherein the expansion device is connected to the condenser by a liquid refrigerant flow line for liquid refrigerant and immiscible lubricant. The method comprising slowing the rate of flow of the liquid refrigerant and immiscible lubricant between the condenser and the expansion device such that the liquid refrigerant and the immiscible lubricant separate based upon differences in density. The method also comprises collecting the separated immiscible lubricant in a collection chamber in fluid communication with the separated immiscible lubricant. Apparatus for performing the method is also disclosed. 3 figs.

Lubrication from mixture of boric acid with oils and greases

DOEpatents

Erdemir, A.

1995-07-11

Lubricating compositions are disclosed including crystalline boric acid and a base lubricant selected from oils, greases and the like. The lubricity of conventional oils and greases can also be improved by adding concentrates of boric acid.

Research on the Injection Performance of a Novel Lubricating Device Based on Piezoelectric Micro-Jet Technology

NASA Astrophysics Data System (ADS)

Li, Kai; Liu, Jun-kao; Chen, Wei-shan; Ye, Le; Zhang, Lu

2016-08-01

In order to solve the problem of lubrication failure in bearing systems, a novel lubricating device which can achieve drop-on-demand lubrication is proposed based on piezoelectric micro-jet technology. The injection performance of the novel piezoelectric micro-jet lubricating device are analyzed in this paper. The influences of the fluid-structure interaction to the working frequency are studied by comparing the results of tests with simulations. A method used to forecast the working frequency of the micro-jet is proved to be available. A velocity inlet boundary model at the nozzle is derived under the assumption that the lubricating oil cannot be pressed. Combined with this model, the influences of density, dynamic viscosity and surface tension of the lubricating oil on the injection performance are discussed according to the simulation results. An experiment on the injection performance of the micro-jet for ejecting lubricating oil with different dilution ratios is performed. The recommended excitations are given for ejecting lubricating oil with different properties by analyzing the results.

Ionic liquids as lubricant additives: A review

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhou, Yan; Qu, Jun

In pursuit of energy efficiency and durability throughout human history, advances in lubricants have always played important roles. Ionic liquids (ILs) are room-temperature molten salts that possess unique physicochemical properties and have shown great potential in many applications with lubrication as one of the latest. While earlier work (2001–2011) primarily explored the feasibility of using ILs as neat or base lubricants, using ILs as lubricant additives has become the new focal research topic since the breakthrough in ILs’ miscibility in nonpolar hydrocarbon oils in early 2012. This work reviews the recent advances in developing ILs as additives for lubrication withmore » an attempt to correlate among the cationic and anionic structures, oil-solubility, and other relevant physicochemical properties, and lubricating behavior. Effects of the concentration of ILs in lubricants and the compatibility between ILs and other additives in the lubricant formulation on the tribological performance are described followed by a discussion of wear protection mechanism based on tribofilm characterization. As a result, future research directions are suggested at the end.« less

Ionic liquids as lubricant additives: A review

DOE PAGES

Zhou, Yan; Qu, Jun

2016-12-28

In pursuit of energy efficiency and durability throughout human history, advances in lubricants have always played important roles. Ionic liquids (ILs) are room-temperature molten salts that possess unique physicochemical properties and have shown great potential in many applications with lubrication as one of the latest. While earlier work (2001–2011) primarily explored the feasibility of using ILs as neat or base lubricants, using ILs as lubricant additives has become the new focal research topic since the breakthrough in ILs’ miscibility in nonpolar hydrocarbon oils in early 2012. This work reviews the recent advances in developing ILs as additives for lubrication withmore » an attempt to correlate among the cationic and anionic structures, oil-solubility, and other relevant physicochemical properties, and lubricating behavior. Effects of the concentration of ILs in lubricants and the compatibility between ILs and other additives in the lubricant formulation on the tribological performance are described followed by a discussion of wear protection mechanism based on tribofilm characterization. As a result, future research directions are suggested at the end.« less

Lubrication handbook

NASA Technical Reports Server (NTRS)

Campbell, M. E.; Thompson, M. B.

1973-01-01

Information on lubricants from government reports, military specifications, qualified parts lists, and suppliers of commercial lubricants has been consolidated in one source. Handbook includes data on chemical and physical properties of solid, bonded solid, and liquid lubricants; dispersions and composites; and greases, oils, and hydraulic fluids.

Effects of some lubricants and evaluation of compression parameters on directly compressible powders.

PubMed

Uğurlu, Timuçin; Halaçoğlu, Mekin Doğa

2014-05-01

The objective of this study was to investigate the effects of conventional lubricants including a new candidate lubricant "Hexagonal boron nitride (HBN)" on direct compression powders. Lubricants such as magnesium stearate, glyceryl behenate, stearic acid, talc and polyethylene glycol6000 were studied in this article. Tablets were manufactured on an instrumented tablet press with various lubricant concentrations. Bulk and tapped densities, and Carr's index parameters were calculated for powders. Tensile strength, cohesion index, lower punch ejection force and lubricant effectiveness values were investigated for tablets. The deformation mechanisms of tablets were studied during compression from the Heckel plots with or without lubricants. Powders formulated with MGST and HBN showed better flow properties based on Carr's index. MGST was found to be the most effective lubricant based on lubricant effectiveness for tablets. HBN was found very close to MGST with the same concentrations. Other lubricants showed less effectiveness than that of MGST and HBN. It is observed that an increase in the concentration of HBN leads to decreased tensile strength and cohesion index values because of its surface-covering property. Despite covering property, HBN had no significant effect on disintegration time. Based on the Heckel plots at the level of 1%, HBN showed the most pronounced plastic character.

[Acidity and temperature effect on the fluorescence characteristics of hydraulic oils and lubricants].

PubMed

Deng, Hu; Zhou, Xun; Shang, Li-ping; Zhang, Ze-lin; Wang, Shun-li

2014-12-01

By analyzing HyJet V phosphate ester hydraulic oil environmental impacts (oil, etc.) and confounding factors (pH, temperature, etc.), the feasibility was studied for the fluorescence detection of aircraft hydraulic oil leaks. By using the fluorescence spectrophotometer at various acidities and temperatures, the fluorescence properties of HyJet V phosphate ester hydraulic oil, Jet Oil II lubricant and 2197 lubricant were gained. The experimental results are shown as following: The fluorescence peaks of HyJet V phosphate ester hydraulic oil, Jet Oil II lubricant and 2197 lubricant are at 362, 405 and 456 nm, respectively. The impact of temperature on HyJet V phosphate ester hydraulic oil is less effective; Jet Oil II lubricant and 2197 lubricant fluorescence intensity decreases with increasing temperature. When acidity increases, the fluorescence peak of HyJet V phosphate ester hydraulic oil gradient shifts from 370 to 362 nm, and the fluorescence intensity decreases; the fluorescence peak of Jet Oil II lubricant is always 405 nm, while the fluorescence intensity decreases; the fluorescence peak of 2197 lubricant at 456 nm red shifts to 523 nm, and double fluorescence peaks appeare. The results are shown as following: under the influence of the environment and interference factors, the fluorescence characteristics of HyJet V phosphate ester hydraulic oil remain unchanged, and distinguish from Jet Oil II lubricant and 2197 lubricant. Therefore, the experiments indicate that the detection of HyJet V phosphate ester hydraulic oil leak is feasible by using fluorescence method.

Identifying lubricant options for compressor bearing designs

NASA Astrophysics Data System (ADS)

Karnaz, J.; Seeton, C.; Dixon, L.

2017-08-01

Today’s refrigeration and air conditioning market is not only driven by the environmental aspects of the refrigerants, but also by the energy efficiency and reliability of system operation. Numerous types of compressor designs are used in refrigeration and air conditioning applications which means that different bearings are used; and in some cases, multiple bearing types within a single compressor. Since only one lubricant is used, it is important to try to optimize the lubricant to meet the various demands and requirements for operation. This optimization entails investigating different types of lubricant chemistries, viscosities, and various formulation options. What makes evaluating these options more challenging is the refrigerant which changes the properties of the lubricant delivered to the bearing. Once the lubricant and refrigerant interaction are understood, through various test methods, then work can start on collaborating with compressor engineers on identifying the lubricant chemistry and formulation options. These interaction properties are important to the design engineer to make decisions on the adequacy of the lubricant before compressor tests are started. This paper will discuss the process to evaluate lubricants for various types of compressors and bearing design with focus on what’s needed for current refrigerant trends. In addition, the paper will show how the lubricant chemistry choice can be manipulated through understanding of the bearing design and knowledge of interaction with the refrigerant to maximize performance. Emphasis will be placed on evaluation of synthetic lubricants for both natural and synthetic low GWP refrigerants.

MISCIBILITY, SOLUBILITY, AND VISCOSITY MEASUREMENTS FOR R-236EA WITH POTENTIAL LUBRICANTS

EPA Science Inventory

The report gives results of miscibility, solubility, and viscosity measurements of refrigerant R-236ea with three potential lubricants. (NOTE: The data were needed to determine the suitability of refrigerant/lubricant combinations for use in refrigeration systems.) The lubricants...

Microscopic aspects of the effect of friction reducers at the lubrication limit. Ph.D. Thesis

NASA Technical Reports Server (NTRS)

Mansot, J. L.

1984-01-01

An attempt is made to analytically model the physicochemical properties of lubricants and their capacity to reduce friction. A technique of frozen fracturing of the lubricants was employed to study the dispersion of additives throughout a lubricant. Adsorption was observed at the liquid-solid interface, which was the region where the solid and lubricant met, and the molecular dispersion of the additive enhanced the effectiveness of the lubricant. The electrically conductive characteristics of the lubricant at the friction interface indicated the presence of tunneling effects. The Bethe model was used to examine the relationship between the coefficient of friction and the variation of interface thickness. The electron transport permitted an inelastic tunnel electron spectroscopic investigation of the molecular transformations undergone by the additive during friction episodes.

Determination of thin hydrodynamic lubricating film thickness using dichromatic interferometry.

PubMed

Guo, L; Wong, P L; Guo, F; Liu, H C

2014-09-10

This paper introduces the application of dichromatic interferometry for the study of hydrodynamic lubrication. In conventional methods, two beams with different colors are projected consecutively on a static object. By contrast, the current method deals with hydrodynamic lubricated contacts under running conditions and two lasers with different colors are projected simultaneously to form interference images. Dichromatic interferometry incorporates the advantages of monochromatic and chromatic interferometry, which are widely used in lubrication research. This new approach was evaluated statically and dynamically by measuring the inclination of static wedge films and the thickness of the hydrodynamic lubricating film under running conditions, respectively. Results show that dichromatic interferometry can facilitate real-time determination of lubricating film thickness and is well suited for the study of transient or dynamic lubricating problems.

Exposure of natural rubber to personal lubricants--swelling and stress relaxation as potential indicators of reduced seal integrity of non-lubricated male condoms.

PubMed

Sarkar Das, Srilekha; Coburn, James C; Tack, Charles; Schwerin, Matthew R; Richardson, D Coleman

2014-07-01

Male condoms act as mechanical barriers to prevent passage of body fluids. For effective use of condoms the mechanical seal is also expected to remain intact under reasonable use conditions, including with personal lubricants. Absorption of low molecular weight lubricant components into the material of male condoms may initiate material changes leading to swelling and stress relaxation of the polymer network chains that could affect performance of the sealing function of the device. Swelling indicates both a rubber-solvent interaction and stress relaxation, the latter of which may indicate and/or result in a reduced seal pressure in the current context. Swelling and stress relaxation of natural rubber latex condoms were assessed in a laboratory model in the presence of silicone-, glycol-, and water-based lubricants. Within 15 minutes, significant swelling (≥6 %) and stress reduction (≥12 %) of condoms were observed with 2 out of 4 silicone-based lubricants tested, but neither was observed with glycol- or water-based lubricants tested. Under a given strain, reduction in stress was prominent during the swelling processes, but not after the process was complete. Lubricant induced swelling and stress relaxation may loosen the circumferential stress responsible for the mechanical seal. Swelling and stress relaxation behavior of latex condoms in the presence of personal lubricants may be useful tests to identify lubricant-rooted changes in condom-materials. For non-lubricated latex condoms, material characteristics--which are relevant to failure--may change in the presence of a few silicone-based personal lubricants. These changes may in turn induce a loss of condom seal during use, specifically at low strain conditions. Published by Elsevier Inc.

Application of Terahertz Attenuated Total Reflection Spectroscopy to Detect Changes in the Physical Properties of Lactose during the Lubrication Process Required for Drug Formulation.

PubMed

Dohi, Masafumi; Momose, Wataru; Yamashita, Kazunari; Hakomori, Tadashi; Sato, Shusaku; Noguchi, Shuji; Terada, Katsuhide

2017-02-01

Manufacturing the solid dosage form of an orally administered drug requires lubrication to enhance manufacturability, ensuring that critical quality attributes such as disintegration and dissolution of the drug product are maintained during manufacture. Here, to evaluate lubrication performance during manufacture, we used terahertz attenuated total reflection (THz-ATR) spectroscopy to detect differences in the physical characteristics of the lubricated powder. We applied a simple formulation prepared by blending granulated lactose as filler with magnesium stearate as lubricant. A flat tablet was prepared using the lubricated powder to acquire sharp THz-ATR absorption peaks of the samples. First, we investigated the effects of lubricant concentration and compression pressure on preparation of the tablet and then determined the effect of the pressure applied to samples in contact with the ATR prism on sample absorption amplitude. We focused on the differences in the magnitudes of spectra at the lactose-specific frequency. Second, we conducted the dynamic lubrication process using a 120-L mixer to investigate differences in the magnitudes of absorption corresponding to the lactose-specific frequency during lubrication. In both studies, enriching the lubricated powder with a higher concentration of magnesium stearate or prolonging blending time correlated with higher magnitudes of spectra at the lactose-specific frequency. Further, in the dynamic lubrication study, the wettability and disintegration time of the tablets were compared with the absorption spectra amplitudes at the lactose-specific frequency. We conclude that THz-ATR spectroscopy is useful for detecting differences in densities caused by a change in the physical properties of lactose during lubrication.

Spiral Orbit Tribometry. 2; Evaluation of Three Liquid Lubricants in Vacuum

NASA Technical Reports Server (NTRS)

Pepper, Stephen V.; Kingsbury, Edward P.; Kiraly, Louis J. (Technical Monitor)

2002-01-01

The coefficients of friction and relative degradation rates of three lubricants run in the boundary regime in vacuum are evaluated in a Spiral Orbit Tribometer. This tribometer subjected the lubricants to rolling contact conditions similar to those found in angular contact ball bearings. A multiply alkylated cyclopentane (MAC) hydrocarbon lubricant suffered degradation at a rate almost two orders of magnitude less than the degradation rate of two perfluoropolyalkylether (PFPE) lubricants.

Synthetic oils

NASA Technical Reports Server (NTRS)

Hatton, R. E.

1973-01-01

Synthetic lubricants are discussed by chemical class and their general strengths and weaknesses in terms of lubrication properties are analyzed. Comparative ratings are given for 14 chemical classes and are used as a guide for lubricant selection. The effects of chemical structure on the properties of the lubricant are described with special emphasis on thermal stability. The diversity of synthetic lubricants which is provided by the wide range of properties permits many applications, some of which are reported.

Frequency, Patterns and Preferences of Lubricant Use During Anal Intercourse Within Male Sexual Partnerships in Lima, Peru: Implications for a Rectal Microbicide HIV Prevention Intervention

PubMed Central

Clark, J; Salvatierra, Hector Javier; Segura, Eddy Roberto; Salazar, Ximena; Konda, Kelika; Galea, Jerome; Klausner, Jeffrey D; Coates, Thomas; Caceres, Carlos Fernando

2012-01-01

Understanding current practices of lubricant use during anal intercourse can help to assess the contexts for the introduction of topical rectal microbicides as an HIV prevention tool for men who have sex with men (MSM). We used quantitative and qualitative methods to assess: current patterns of lubricant use; preferred characteristics of commercial lubricant formulations; and social and behavioral contexts of lubricant use within male sexual partnerships in Lima, Peru. Between 2007 and 2008, we conducted a quantitative behavioral survey with 547 MSM followed by qualitative individual and group interviews with 36 MSM from Lima, Peru. Approximately half of all participants in the quantitative survey (50.3%) reported using commercial lubricant during intercourse occasionally or consistently during the preceding two months, with lack of availability at the time of intercourse the most commonly reported reason for non-use. No clear preferences regarding the color, smell, taste, or viscosity of commercial lubricants were identified, and all participants who reported using a commercial lubricant used the same product (“Love-Lub”). In the qualitative analysis, participants characterized lubricant use as a sexual practice consistently controlled by the receptive partner, who typically obtained and applied lubricant independently, with or without the consent of the insertive partner. Quantitative findings supported this differential pattern of lubricant use, with men who reported sexual identities or roles consistent with receptive anal intercourse, including unprotected receptive intercourse, more likely to report lubricant use than MSM who claimed an exclusively insertive sexual role. Given the social, behavioral, and biological factors contributing to increased vulnerability for HIV and STI acquisition by the receptive partner in anal intercourse, delivery of a topical rectal microbicide as a lubricant formulation could provide an important HIV prevention resource for at-risk MSM in Lima, Peru. PMID:23082796

FY2013 Progress Report for Fuel & Lubricant Technologies

DOE Office of Scientific and Technical Information (OSTI.GOV)

none,

2014-02-01

Annual progress report for Fuel & Lubricant Technologies. The Fuel & Lubricant Technologies Program supports fuels and lubricants research and development (R&D) to provide vehicle manufacturers and users with cost-competitive options that enable high fuel economy with low emissions, and contribute to petroleum displacement.

FY2014 Fuel & Lubricant Technologies Annual Progress Report

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stork, Kevin

2016-02-01

Annual progress report for Fuel & Lubricant Technologies. The Fuel & Lubricant Technologies Program supports fuels and lubricants research and development (R&D) to provide vehicle manufacturers and users with cost-competitive options that enable high fuel economy with low emissions, and contribute to petroleum displacement.

Women's willingness to experiment with condoms and lubricants: A study of women residing in a high HIV seroprevalence area.

PubMed

Sanders, Stephanie A; Crosby, Richard A; Milhausen, Robin R; Graham, Cynthia A; Tirmizi, Amir; Yarber, William L; Beauchamps, Laura; Mena, Leandro

2018-03-01

The objective of this study was to investigate women's willingness to experiment with new condoms and lubricants, in order to inform condom promotion in a city with high rates of poverty and HIV. One hundred and seventy-three women (85.9% Black) sexually transmitted infection clinic attendees in Jackson, Mississippi, United States completed a questionnaire assessing willingness to experiment with condoms and lubricants and sexual pleasure and lubrication in relation to last condom use. Most women were willing to: (1) experiment with new types of condoms and lubricants to increase their sexual pleasure, (2) touch/handle these products in the absence of a partner, and (3) suggest experimenting with new condoms and lubricants to a sex partner. Previous positive sexual experiences with lubricant during condom use predicted willingness. The role women may play in male condom use should not be underestimated. Clinicians may benefit women by encouraging them to try new types of condoms and lubricants to find products consistent with sexual pleasure.

Elastohydrodynamic Lubrication with Polyolester Lubricants and HFC Refrigerants, Final Report, Volume 2

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gunsel, Selda; Pozebanchuk, Michael

1999-04-01

Lubrication properties of refrigeration lubricants were investigated in high pressure nonconforming contacts under different conditions of temperature, rolling speed, and refrigerant concentration. The program was based upon the recognition that the lubrication regime in refrigeration compressors is generally elastohydrodynamic or hydrodynamic, as determined by the operating conditions of the compressor and the properties of the lubricant. Depending on the compressor design, elastohydrodynamic lubrication conditions exist in many rolling and sliding elements of refrigeration compressors such as roller element bearings, gears, and rotors. The formation of an elastohydrodynamic film separating rubbing surfaces is important in preventing the wear and failure ofmore » compressor elements. It is, therefore, important to predict the elastohydrodynamic (EHD) performance of lubricants under realistic tribocontact renditions. This is, however, difficult as the lubricant properties that control film formation are critically dependent upon pressure and shear, and cannot be evaluated using conventional laboratory instruments. In this study, the elastohydrodynamic behavior of refrigeration lubricants with and without the presence of refrigerants was investigated using the ultrathin film EHD interferometry technique. This technique enables very thin films, down to less than 5 nm, to be measured accurately within an EHD contact under realistic conditions of temperature, shear, and pressure. The technique was adapted to the study of lubricant refrigerant mixtures. Film thickness measurements were obtained on refrigeration lubricants as a function of speed, temperature, and refrigerant concentration. The effects of lubricant viscosity, temperature, rolling speed, and refrigerant concentration on EHD film formation were investigated. From the film thickness measurements, effective pressure-viscosity coefficients were calculated. The lubricants studied in this project included two naphthenic mineral oils (NMO), four polyolesters (POE), and two polyvinyl ether (PVE) fluids. These fluids represented viscosity grades of ISO 32 and ISO 68 and are shown in a table. Refrigerants studied included R-22, R-134a, and R-410A. Film thickness measurements were conducted at 23 C, 45 C, and 65 C with refrigerant concentrations ranging from zero to 60% by weight.« less

Comparison Between Oil-mist and Oil-jet Lubrication of High-speed, Small-bore, Angular-contact Ball Bearings

NASA Technical Reports Server (NTRS)

Pinel, Stanley I.; Signer, Hans R.; Zaretsky, Erwin V.

2001-01-01

Parametric tests were conducted with an optimized 35-mm-bore-angular-contact ball bearing on a high-speed, high-temperature bearing tester. Results from both air-oil mist lubrication and oil-jet lubrication systems used to lubricate the bearing were compared to speeds of 2.5 x 10(exp 6) DN. The maximum obtainable speed with air-oil mist lubrication is 2.5 x 10(exp 6) DN. Lower bearing temperatures and higher power losses are obtained with oil-jet lubrication than with air-oil mist lubrication. Bearing power loss is a direct function of oil flow to the bearing and independent of oil delivery system. For a given oil-flow rate, bearing temperature and power loss increase with increases in speed. Bearing life is an inverse function of temperature, the difference in temperature between the individual bearing ring components, and the resultant elastohydrodynamic (EHD) film thicknesses. Bearing life is independent of the oil delivery system except as it affects temperature. Cage slip increased with increases in speed. Cage slip as high as 7 percent was measured and was generally higher with air-oil mist lubrication than with oil-jet lubrication.

Treatment of Waste Lubricating Oil by Chemical and Adsorption Process Using Butanol and Kaolin

NASA Astrophysics Data System (ADS)

Riyanto; Ramadhan, B.; Wiyanti, D.

2018-04-01

Treatment of waste lubricating oil by chemical and adsorption process using butanol and kaolin has been done. Quality of lubricating oil after treatment was analysis using Atomic Absorption Spectrophotometer (AAS) and Gas Chromatography-Mass Spectrometry (GC-MS). The effects of the treatment of butanol, KOH, and kaolin to metals contain in waste lubricating oil treatment have been evaluated. Treatment of waste lubricating oil has been done using various kaolin weight, butanol, and KOH solution. The result of this research show metal content of Ca, Mg, Pb, Fe and Cr in waste lubricating oil before treatment are 1020.49, 367.02, 16.40, 36.76 and 1,80 ppm, respectively. The metal content of Ca, Mg, Pb, Fe and Cr in the waste lubricating oil after treatment are 0.17, 9.85, 34.07, 78.22 and 1.20 ppm, respectively. The optimum condition for treatment of waste lubricating oil using butanol, KOH, and kaolin is 30 mL, 3.0 g and 1.5 g, respectively. Chemical and adsorption method using butanol and kaolin can be used for decrease of metals contain in waste lubricating oil.

Automotive Fuel Economy - Potential Improvement Through Selected Engine and Differential Gear Lubricants

DOT National Transportation Integrated Search

1981-07-01

This report evaluates the effects of four engine lubricants and three differential gear lubricants on the fuel economy of two 1978 automobiles operated at 20F, 70F, and 100F ambient temperatures. The engine lubricants were evaluated using the 1978 Fe...

Correlation of rheological characteristics of lubricants with transmission efficiency measurements

NASA Technical Reports Server (NTRS)

Jacobson, B. O.; Hamrock, B. J.; Hoeglund, E.

1985-01-01

The power efficiency of a helicopter transmission has been analyzed for 11 lubricants by looking at the Newtonian and non-Newtonian properties of the lubricants. A non-Newtonian property of the lubricants was the limiting shear strength proportionality constant. The tests were performed on a high-pressure, short-time shear strength analyzer. A power efficiency formula that was obtained by analyzing the Newtonian and non-Newtonian properties of the lubricants is presented in detail.

Evaluation of Corrosion Inhibitors as Lubricity Improvers

DTIC Science & Technology

1988-07-01

IF AFWAL-TR-88-2036 I. ov EVALUATION OF CORROSION , INHIBITORS AS LUBRICITY IMPROVERS 0 T.B. Biddle W. H. Edwards United Technologies Corporation...TASK WORK UNIT ELEMENT NO. NO. NO. NO. ITL (include Security C.aulf.cal.on) 6220 F .--- 3048-_ 05 51 valuation of Corrosion Inhibitors as Lubricity...numkr) o GROUP SUB. GR. Bal12nQ ylinder Lubricity)Eva ator, BOCLE, Corrosion Inhibitor , Fuel 01 03 Lubricity, MIL!AI5017, QPL-2 17 Reverse Phase) High

The Role of Nano-TiO2 Lubricating Fluid on the Hot Rolled Surface and Metallographic Structure of SS41 Steel

PubMed Central

Meng, Yanan; Sun, Jianlin; Wu, Ping; Dong, Chang; Yan, Xudong

2018-01-01

In this paper, nano-TiO2lubricating fluid was chosen as an advanced rolling lubricant to investigate its effect on the hot rolled surface and metallographic structure of SS41 steel strips. The tribological performances of nano-TiO2 lubricating fluid were measured by a four-ball tribotester. The hot rolling experiments under different lubrication conditions were carried out by a four-high rolling mill. The surface morphology, oxide scales and metallographic structure after hot rolling were observed using a confocal laser scanning microscope and scanning electron microscope (SEM), respectively. The composition of surface attachments was analyzed with X-ray photoelectron spectroscopy (XPS). The results indicate that the nano-TiO2 lubricating fluid has a better tribological performance. The surface defects on the hot rolled surface could be decreased. The phase composition of the surface still appears as a mixture of ferrite and pearlite. The surface of steel strips is not micro-alloyed with titanium as predicted. Additionally, the grain size of rolled steel strips which were lubricated with the nano-TiO2lubricating fluid decreased by nearly 50%, compared with traditional lubricating fluid. Furthermore, it was found that the thickness of the oxide layers on the surface reduced, whilst the Rockwell hardness of the oxide layers was enhanced as nano-TiO2 lubricating fluid was applied. PMID:29462937

The Role of Nano-TiO2 Lubricating Fluid on the Hot Rolled Surface and Metallographic Structure of SS41 Steel.

PubMed

Meng, Yanan; Sun, Jianlin; Wu, Ping; Dong, Chang; Yan, Xudong

2018-02-16

In this paper, nano-TiO2lubricating fluid was chosen as an advanced rolling lubricant to investigate its effect on the hot rolled surface and metallographic structure of SS41 steel strips. The tribological performances of nano-TiO2 lubricating fluid were measured by a four-ball tribotester. The hot rolling experiments under different lubrication conditions were carried out by a four-high rolling mill. The surface morphology, oxide scales and metallographic structure after hot rolling were observed using a confocal laser scanning microscope and scanning electron microscope (SEM), respectively. The composition of surface attachments was analyzed with X-ray photoelectron spectroscopy (XPS). The results indicate that the nano-TiO2 lubricating fluid has a better tribological performance. The surface defects on the hot rolled surface could be decreased. The phase composition of the surface still appears as a mixture of ferrite and pearlite. The surface of steel strips is not micro-alloyed with titanium as predicted. Additionally, the grain size of rolled steel strips which were lubricated with the nano-TiO2lubricating fluid decreased by nearly 50%, compared with traditional lubricating fluid. Furthermore, it was found that the thickness of the oxide layers on the surface reduced, whilst the Rockwell hardness of the oxide layers was enhanced as nano-TiO2 lubricating fluid was applied.

Effect of handpiece maintenance method on bond strength.

PubMed

Roberts, Howard W; Vandewalle, Kraig S; Charlton, David G; Leonard, Daniel L

2005-01-01

This study evaluated the effect of dental handpiece lubricant on the shear bond strength of three bonding agents to dentin. A lubrication-free handpiece (one that does not require the user to lubricate it) and a handpiece requiring routine lubrication were used in the study. In addition, two different handpiece lubrication methods (automated versus manual application) were also investigated. One hundred and eighty extracted human teeth were ground to expose flat dentin surfaces that were then finished with wet silicon carbide paper. The teeth were randomly divided into 18 groups (n=10). The dentin surface of each specimen was exposed for 30 seconds to water spray from either a lubrication-free handpiece or a lubricated handpiece. Prior to exposure, various lubrication regimens were used on the handpieces that required lubrication. The dentin surfaces were then treated with total-etch, two-step; a self-etch, two-step or a self-etch, one-step bonding agent. Resin composite cylinders were bonded to dentin, the specimens were then thermocycled and tested to failure in shear at seven days. Mean bond strength data were analyzed using Dunnett's multiple comparison test at an 0.05 level of significance. Results indicated that within each of the bonding agents, there were no significant differences in bond strength between the control group and the treatment groups regardless of the type of handpiece or use of routine lubrication.

1 H-NMR with Multivariate Analysis for Automobile Lubricant Comparison.

PubMed

Kim, Siwon; Yoon, Dahye; Lee, Dong-Kye; Yoon, Changshin; Kim, Suhkmann

2017-07-01

Identification of suspected automobile-related lubricants could provide valuable information in forensic cases. We examined that automobile lubricants might exhibit the chemometric characteristics to their individual usages. To compare the degree of clustering in the plots, we co-plotted general industrial oils that were highly dissimilar with automobile lubricants in additive compositions. 1 H-NMR spectroscopy was used with multivariate statistics as a tool for grouping, clustering, and identification of automobile lubricants in laboratory conditions. We analyzed automobile lubricants including automobile engine oils, automobile transmission oils, automobile gear oils, and motorcycle oils. In contrast to the general industrial oils, automobile lubricants showed relatively high tendencies of clustering to their usages. Our pilot study demonstrated that the comparison of known and questioned samples to their usages might be possible in forensic fields. © 2017 American Academy of Forensic Sciences.

Emergency and microfog lubrication and cooling of bearings for Army helicopters

NASA Technical Reports Server (NTRS)

Rosenlieb, J. W.

1978-01-01

An analysis and system study was performed to provide design information regarding lubricant and coolant flow rates and flow paths for effective utilization of the lubricant and coolant in a once-through oil-mist (microfog) and coolant air system. A system was designed, manufactured, coupled with an existing rig and evaluation tests were performed using 46 mm bore split-inner angular-contact ball bearings under 1779N (400 lb.) thrust load. An emergency lubrication aspirator system was also manufactured and tested under lost lubricant conditions. The testing demonstrated the feasibility of using a mist oil and cooling air system to lubricate and cool a high speed helicopter engine mainshaft bearing. The testing also demonstrated the feasibility of using an emergency aspirator lubrication system as a viable survivability concept for helicopter mainshaft engine bearing for periods as long as 30 minutes.

Process for preparing lubricating oil from used waste lubricating oil

DOEpatents

Whisman, Marvin L.; Reynolds, James W.; Goetzinger, John W.; Cotton, Faye O.

1978-01-01

A re-refining process is described by which high-quality finished lubricating oils are prepared from used waste lubricating and crankcase oils. The used oils are stripped of water and low-boiling contaminants by vacuum distillation and then dissolved in a solvent of 1-butanol, 2-propanol and methylethyl ketone, which precipitates a sludge containing most of the solid and liquid contaminants, unspent additives, and oxidation products present in the used oil. After separating the purified oil-solvent mixture from the sludge and recovering the solvent for recycling, the purified oil is preferably fractional vacuum-distilled, forming lubricating oil distillate fractions which are then decolorized and deodorized to prepare blending stocks. The blending stocks are blended to obtain a lubricating oil base of appropriate viscosity before being mixed with an appropriate additive package to form the finished lubricating oil product.

Preparation of microcapsules containing double-component lubricant and self-lubricating performance of polymer composites

NASA Astrophysics Data System (ADS)

Li, Haiyan; Shi, Nanqi; Ji, Jing; Wang, Huaiyuan

2018-05-01

Double-component microcapsules containing lubricant oil and SiO2 nanoparticles were prepared by solvent evaporation method. The synthesized microcapsules have the regular spherical structure with the mean diameter of 105 μm and wall thickness of 15 μm. The synthesized microcapsules have excellent thermal stability, and the lubricant oil content was 71.4 wt%. Self-lubricating polymer composites were fabricated by incorporating double-component microcapsules into epoxy matrix. When the SiO2 nanoparticles content was 3 wt% relative to the lubricant oil, 10 wt% microcapsules brought 60.8% and 93.3% decrease for epoxy composites in the friction coefficient and specific wear rate, respectively. The synergetic effect between lubricant oil and SiO2 nanoparticles play a positive role in improving the triboligical properties of polymer composites.

In situ measurement of the bonded film thickness of Z-Tetraol lubricant on magnetic recording media

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhu Lei; Li Feng

2010-10-15

Currently, the bonded film thickness of perfluoropolyether lubricant on top of magnetic recording media is measured by a two-step process. First, the media disk has to be rinsed thoroughly using a fluorocarbon solvent (for instance, Vetrel) to remove the mobile lubricant. Second, the thickness of the remaining lubricant on the media surface which is regarded as the bonded lubricant thickness is then measured either by Fourier transform infrared spectroscopy (FTIR) or electron spectroscopy for chemical analysis. As the total lubricant thickness approaches single molecular dimension ({approx}10 A), current methods face tremendous challenge on the accuracy and sensitivity of the measurement.more » We studied the spectral characteristics responding to the lubricant bonding with the carbon overcoat by the time-of-flight secondary ion mass spectra and proposed to use the peak area ratio (C{sub 3}H{sub 2}F/C{sub 3}H{sub 5}O and C{sub 4}H{sub 10}O/C{sub 3}H{sub 6}O{sub 2}) to characterize the bonded Z-Tetraol lubricant that produces a direct bonded lubricant thickness measurement without the need to remove the mobile lubricant with a solvent. After taking the background signal of disks prior to bonding by UV irradiation into account, this method becomes independent of the total lubricant thickness as well as shows good correlation linearity (R{sup 2{approx}}87%) with the current FTIR method for the ratio of C{sub 4}H{sub 10}O/C{sub 3}H{sub 6}O{sub 2}.« less

76 FR 49525 - Advisory Circular 20-24C, Approval of Propulsion Fuels and Lubricating Oils

Federal Register 2010, 2011, 2012, 2013, 2014

2011-08-10

... Propulsion Fuels and Lubricating Oils AGENCY: Federal Aviation Administration (FAA), DOT. ACTION: Notice of..., Approval of Propulsion Fuels and Lubricating Oils. This AC provides guidance on regulations and policy... approve aircraft, engines, or APUs to operate with specified propulsion fuels and lubricating oils. DATES...

40 CFR 90.308 - Lubricating oil and test fuels.

Code of Federal Regulations, 2014 CFR

2014-07-01

... 40 Protection of Environment 20 2014-07-01 2013-07-01 true Lubricating oil and test fuels. 90.308... Equipment Provisions § 90.308 Lubricating oil and test fuels. (a) Lubricating oil. Use the engine... manufacturer. (b) Test Fuels—Certification. (1) The manufacturer must use gasoline having the specifications...

40 CFR 90.308 - Lubricating oil and test fuels.

Code of Federal Regulations, 2012 CFR

2012-07-01

... 40 Protection of Environment 21 2012-07-01 2012-07-01 false Lubricating oil and test fuels. 90.308... Equipment Provisions § 90.308 Lubricating oil and test fuels. (a) Lubricating oil. Use the engine... manufacturer. (b) Test Fuels—Certification. (1) The manufacturer must use gasoline having the specifications...

40 CFR 90.308 - Lubricating oil and test fuels.

Code of Federal Regulations, 2013 CFR

2013-07-01

... 40 Protection of Environment 21 2013-07-01 2013-07-01 false Lubricating oil and test fuels. 90.308... Equipment Provisions § 90.308 Lubricating oil and test fuels. (a) Lubricating oil. Use the engine... manufacturer. (b) Test Fuels—Certification. (1) The manufacturer must use gasoline having the specifications...

40 CFR 90.308 - Lubricating oil and test fuels.

Code of Federal Regulations, 2011 CFR

2011-07-01

... 40 Protection of Environment 20 2011-07-01 2011-07-01 false Lubricating oil and test fuels. 90.308... Equipment Provisions § 90.308 Lubricating oil and test fuels. (a) Lubricating oil. Use the engine... manufacturer. (b) Test Fuels—Certification. (1) The manufacturer must use gasoline having the specifications...

40 CFR 90.308 - Lubricating oil and test fuels.

Code of Federal Regulations, 2010 CFR

2010-07-01

... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Lubricating oil and test fuels. 90.308... Equipment Provisions § 90.308 Lubricating oil and test fuels. (a) Lubricating oil. Use the engine... manufacturer. (b) Test Fuels—Certification. (1) The manufacturer must use gasoline having the specifications...

Krytox Lubrication Tape Study. [fluorinated lubricating oil for video tape recorders

NASA Technical Reports Server (NTRS)

Lee, F.

1978-01-01

The use of Krytox, a fluorinated oil, as a tape surface lubricant was studied for a wideband video tape recorder. In spite of the 5 to 1 head wear reduction credited to the surface lubricant, the resultant head life fell short of the 1500 hour goal.

Solid Lubricant For Alumina

NASA Technical Reports Server (NTRS)

Dellacorte, Christopher; Pepper, Stephen V.; Honecy, Frank S.

1993-01-01

Outer layer of silver lubricates, while intermediate layer of titanium ensures adhesion. Lubricating outer films of silver deposited on thin intermediate films of titanium on alumina substrates found to reduce sliding friction and wear. Films provide effective lubrication for ceramic seals, bearings, and other hot sliding components in advanced high-temperature engines.

Reduced Need of Lubricity Additives in Soybean Oil Blends Under Boundary Lubrication Conditions

USDA-ARS?s Scientific Manuscript database

Converging prices of vegetable oils and petroleum, along with increased focus on renewable resources, gave more momentum to vegetable oil lubricants. Boundary lubrication properties of four Extreme Pressure (EP) additive blends in conventional Soy Bean Oil (SBO) and Paraffinic Mineral Oil (PMO) of ...

21 CFR 880.6375 - Patient lubricant.

Code of Federal Regulations, 2010 CFR

2010-04-01

... § 880.6375 Patient lubricant. (a) Identification. A patient lubricant is a device intended for medical... 21 Food and Drugs 8 2010-04-01 2010-04-01 false Patient lubricant. 880.6375 Section 880.6375 Food and Drugs FOOD AND DRUG ADMINISTRATION, DEPARTMENT OF HEALTH AND HUMAN SERVICES (CONTINUED) MEDICAL...

Lubrication system with tolerance for reduced gravity

NASA Technical Reports Server (NTRS)

Portlock, Lawrence E. (Inventor); McCune, Michael E. (Inventor); Dobek, Louis J. (Inventor)

2012-01-01

A lubrication system includes an auxiliary lubricant tank 48, a supply conduit 58 extending from a source of lubricant 26 to the auxiliary lubricant tank. A reduced-G bypass line 108 branches from the conduit and enters the auxiliary tank at a first elevation E.sub.1. The system also includes an auxiliary tank discharge conduit 116, a portion of which resides within the tank. The resident portion has an opening 122 at least partially at a second elevation E.sub.2 higher than the first elevation.

Lubrication System with Tolerance for Reduced Gravity

NASA Technical Reports Server (NTRS)

Portlock, Lawrence E. (Inventor); McCune, Michael E. (Inventor); Dobek, Louis J. (Inventor)

2013-01-01

A lubrication system includes an auxiliary lubricant tank 48, a supply conduit 58 extending from a source of lubricant 26 to the auxiliary lubricant tank. A reduced-G bypass line 108 branches from the conduit and enters the auxiliary tank at a first elevation E.sub.1. The system also includes an auxiliary tank discharge conduit 116, a portion of which resides within the tank. The resident portion has an opening 122 at least partially at a second elevation E.sub.2 higher than the first elevation.

A Rolling Element Tribometer for the Study of Liquid Lubricants in Vacuum

NASA Technical Reports Server (NTRS)

Pepper, Stephen V.; Ebihara, Ben T.; Kingsbury, Edward

1996-01-01

A tribometer for the evaluation of liquid lubricants in vacuum is described. This tribometer is essentially a thrust bearing with three balls and flat races having contact stresses and ball motions similar to those in an angular contact ball bearing operating in the boundary lubrication regime. The friction coefficient, lubrication lifetime, and species evolved from the liquid lubricant by tribodegradation can be determined. A complete analysis of the contact stresses and energy dissipation together with experimental evidence supporting the analysis are presented.

Sporting Good Lubricants

NASA Technical Reports Server (NTRS)

1997-01-01

Sun Coast Chemicals was originally contracted by Lockheed Martin Space Operations to formulate a spray lubricant free of environmental drawbacks for the Mobile Launch Platform used to haul the Space Shuttle from the Kennedy Space Center Vehicle Assembly Building to a launch pad. From this work, Sun Coast introduced Train Track Lubricant, Penetrating Spray Lube, and Biodegradable Hydraulic Fluid. Based on the original lubricant work, two more products have also been introduced. First, the X-1R Super Gun Cleaner and Lubricant protects guns from rust and corrosion caused by environmental conditions. Second, the X-1R Tackle Pack, endorsed by both fresh and saltwater guides and certain reel manufacturers, penetrates, cleans, reduces friction, lubricates, and provides extra protection against rust and corrosion.

Rotary seal with improved film distribution

DOEpatents

Dietle, Lannie Laroy; Schroeder, John Erick

2013-10-08

The present invention is a generally circular rotary seal that establishes sealing between relatively rotatable machine components for lubricant retention and environmental exclusion, and incorporates seal geometry that interacts with the lubricant during relative rotation to distribute a lubricant film within the dynamic sealing interface. The features of a variable inlet size, a variable dynamic lip flank slope, and a reduction in the magnitude and circumferentially oriented portion of the lubricant side interfacial contact pressure zone at the narrowest part of the lip, individually or in combination thereof, serve to maximize interfacial lubrication in severe operating conditions, and also serve to minimize lubricant shear area, seal torque, seal volume, and wear, while ensuring retrofitability into the seal grooves of existing equipment.

Rotary seal with improved film distribution

DOEpatents

Dietle, Lannie Laroy; Schroeder, John Erick

2015-09-01

The present invention is a generally circular rotary seal that establishes sealing between relatively rotatable machine components for lubricant retention and environmental exclusion, and incorporates seal geometry that interacts with the lubricant during relative rotation to distribute a lubricant film within the dynamic sealing interface. The features of a variable inlet size, a variable dynamic lip flank slope, and a reduction in the magnitude and circumferentially oriented portion of the lubricant side interfacial contact pressure zone at the narrowest part of the lip, individually or in combination thereof, serve to maximize interfacial lubrication in severe operating conditions, and also serve to minimize lubricant shear area, seal torque, seal volume, and wear, while ensuring retrofitability into the seal grooves of existing equipment.

Tribological characteristic enhancement effects by polymer thickened oil in lubricated sliding contacts

NASA Astrophysics Data System (ADS)

Pratomo, Ariawan Wahyu; Muchammad, Tauviqirrahman, Mohammad; Jamari, Bayuseno, Athanasius P.

2016-04-01

Polymer thickened oils are the most preferred materials for modern lubrication applications due to their high shear. The present paper explores a lubrication mechanism in sliding contact lubricated with polymer thickened oil considering cavitation. Investigations are carried out by using a numerical method based on commercial CFD (computational fluid dynamic) software ANSYS for fluid flow phenomenon (Fluent) to assess the tribological characteristic (i.e. hydrodynamic pressure distribution) of lubricated sliding contact. The Zwart-Gerber-Belamri model for cavitation is adopted in this simulation to predict the extent of the full film region. The polymer thickened oil is characterized as non-Newtonian power-law fluid. The simulation results show that the cavitation lead lower pressure profile compared to that without cavitation. In addition, it is concluded that the characteristic of the lubrication performance with polymer thickened oil is strongly dependent on the Power-law index of lubricant.

Performance of large-bore tapered-roller bearings under combined radial and thrust load at shaft speeds to 15,000 rpm

NASA Technical Reports Server (NTRS)

Parker, R. J.; Signer, H. R.

1977-01-01

The performance of 120.65-mm bore tapered roller bearings was investigated at shaft speeds up to 15,000 rpm. Temperature distribution and bearing heat generation were determined as a function of shaft speed, radial and thrust loads, lubricant flow rate, and lubricant inlet temperature. Lubricant was supplied by either jets or by a combination of holes through the cone directly to the cone-rib contact and jets at the roller small-end side. Cone-rib lubrication significantly improved high-speed tapered-roller bearing performance, yielding lower cone-face temperatures and lower power loss and allowing lower lubricant flow rates for a given speed condition. Bearing temperatures increased with increased shaft speed and decreased with increased lubricant flow rate. Bearing power loss increased with increased shaft speed and increased lubricant flow rate.

Lubrication of Nitinol 60

NASA Technical Reports Server (NTRS)

Pepper, Stephen V.; DellaCorte, Christopher; Glennon, Glenn

2010-01-01

The mechanical properties of Nitinol 60, 60 wt% Ni, 40 wt% Ti (55 at.% Ni, 45 at.% Ti) are sufficiently attractive to warrant its consideration as a lubricated triboelement. Triboelements are always run lubricated. The ability to lubricate Nitinol 60 by the oils usually used on spacecraft mechanisms--Pennzane 2001A, Krytox 143AC and Castrol 815Z--was experimentally determined. These oils were run in the boundary lubrication regime for Nitinol 60 balls running against Nitinol 60 counterfaces in the vacuum spiral orbit tribometer. Test results consisting of the coefficient of friction versus time (friction traces) and relative degradation rates of the oils are presented. Contrary to the inability to successfully lubricate other metal alloys with high titanium content, it was found that Nitinol 60 is able to be lubricated by these oils. Overall, the results presented here indicate that Nitinol 60 is a credible candidate material for bearing applications.

Lubrication of 35-millimeter-bore ball bearings of several designs to 2.5 million DN

NASA Technical Reports Server (NTRS)

Schuller, F. T.

1983-01-01

Parametric tests were conducted with 35mm bore, angular contact ball bearings with either a single or double outer and guided cage. The bearings were either lubricated by oil jets or employed inner ring lubrication. Outer ring cooling was added in selected tests. Lubricant flow to the bearing ranged from 300 to 1900 cc/min. All bearings were successfully run at speeds to 2.5 million DN. Increasing the lubricant flow decreased bearing ring temperatures but increased bearing power lines. The power loss and race temperatures of a jet lubricated with double outer land guided cage were always higher than those of the single land guided design at similar test conditions. The lowest bearing operating temperatures were achieved when inner ring lubrication and outer ring cooling were combined. It is found that cage slip of a double outer land guided cage is approximately twice that of a single outer land guided cage.

KSC lubricant testing program. [lubrication characteristics and corrosion resistance

NASA Technical Reports Server (NTRS)

Lockhart, B. J.; Bryan, C. J.

1973-01-01

A program was conducted to evaluate the performance of various lubricants in use and considered for use at Kennedy Space Center (KSC). The overall objectives of the program were to: (1) determine the lubrication characteristics and relative corrosion resistance of lubricants in use and proposed for use at KSC; (2) identify materials which may be equivalent to or better than KELF-90 and Krytox 240 AC greases; and (3) identify or develop an improved lubricating oil suitable for use in liquid oxygen (LOX) pumps at KSC. It was concluded that: (1) earth gel thickened greases are very poor corrosion preventive materials in the KSC environment; (2) Halocarbon 25-5S and Braycote 656 were suitable substiutes for KELF-90 and Krytox 240 AC respectively; and (3) none of the oils evaluated possessed the necessary inertness, lubricity, and corrosion prevention characteristics for the KSC LOX pumping systems in their present configuration.

Operating limitations of high speed jet lubricated ball bearings

NASA Technical Reports Server (NTRS)

Zaretsky, E. V.; Signer, H.; Bamberger, E. N.

1975-01-01

A parametric study was performed with 120-mm bore angular-contact ball bearings having a nominal contact angle of 20 degrees. The bearings had either an inner- or an outer-race land riding cage, and lubrication was by recirculating oil jets which had either a single or dual orifice. Thrust load, speed, and lubricant flow rate were varied. Test results were compared with those previously reported and obtained from bearings of the same design which were under-race lubricated but run under the same conditions. Jet lubricated ball bearings were limited to speeds less than 2,500,000 DN, and bearings having inner-race land riding cages produced lower temperatures than bearings with outer-race land riding cages. For a given lubricant flow rate dual orifice jets produced lower bearing temperatures than single orifice jets, but under-race lubrication produced lower bearing temperatures under all conditions of operation with no apparent bearing speed limitation.

Systematic evaluation of common lubricants for optimal use in tablet formulation.

PubMed

Paul, Shubhajit; Sun, Changquan Calvin

2018-05-30

As an essential formulation component for large-scale tablet manufacturing, the lubricant preserves tooling by reducing die-wall friction. Unfortunately, lubrication also often results in adverse effects on tablet characteristics, such as prolonged disintegration, slowed dissolution, and reduced mechanical strength. Therefore, the choice of lubricant and its optimal concentration in a tablet formulation is a critical decision in tablet formulation development to attain low die-wall friction while minimizing negative impact on other tablet properties. Three commercially available tablet lubricants, i.e., magnesium stearate, sodium stearyl fumerate, and stearic acid, were systematically investigated in both plastic and brittle matrices to elucidate their effects on reducing die-wall friction, tablet strength, tablet hardness, tablet friability, and tablet disintegration kinetics. Clear understanding of the lubrication efficiency of commonly used lubricants as well as their impact on tablet characteristics would help future tablet formulation efforts. Copyright © 2018 Elsevier B.V. All rights reserved.

Lubricant depletion under various laser heating conditions in Heat Assisted Magnetic Recording (HAMR)

NASA Astrophysics Data System (ADS)

Xiong, Shaomin; Wu, Haoyu; Bogy, David

2014-09-01

Heat assisted magnetic recording (HAMR) is expected to increase the storage areal density to more than 1 Tb/in2 in hard disk drives (HDDs). In this technology, a laser is used to heat the magnetic media to the Curie point (~400-600 °C) during the writing process. The lubricant on the top of a magnetic disk could evaporate and be depleted under the laser heating. The change of the lubricant can lead to instability of the flying slider and failure of the head-disk interface (HDI). In this study, a HAMR test stage is developed to study the lubricant thermal behavior. Various heating conditions are controlled for the study of the lubricant thermal depletion. The effects of laser heating repetitions and power levels on the lubricant depletion are investigated experimentally. The lubricant reflow behavior is discussed as well.

Inserts Automatically Lubricate Ball Bearings

NASA Technical Reports Server (NTRS)

Hager, J. A.

1983-01-01

Inserts on ball-separator ring of ball bearings provide continuous film of lubricant on ball surfaces. Inserts are machined or molded. Small inserts in ball pockets provide steady supply of lubricant. Technique is utilized on equipment for which maintenance is often poor and lubrication interval is uncertain, such as household appliances, automobiles, and marine engines.

14 CFR 33.39 - Lubrication system.

Code of Federal Regulations, 2014 CFR

2014-01-01

... 14 Aeronautics and Space 1 2014-01-01 2014-01-01 false Lubrication system. 33.39 Section 33.39... system. (a) The lubrication system of the engine must be designed and constructed so that it will... supply is in the engine. (b) The lubrication system of the engine must be designed and constructed to...

40 CFR 89.330 - Lubricating oil and test fuels.

Code of Federal Regulations, 2014 CFR

2014-07-01

... 40 Protection of Environment 20 2014-07-01 2013-07-01 true Lubricating oil and test fuels. 89.330... Equipment Provisions § 89.330 Lubricating oil and test fuels. (a) Lubricating oil. Use the engine... that is conducted by the Administrator shall be performed using test fuels that meet the specifications...

40 CFR 89.330 - Lubricating oil and test fuels.

Code of Federal Regulations, 2011 CFR

2011-07-01

... 40 Protection of Environment 20 2011-07-01 2011-07-01 false Lubricating oil and test fuels. 89.330... Equipment Provisions § 89.330 Lubricating oil and test fuels. (a) Lubricating oil. Use the engine... that is conducted by the Administrator shall be performed using test fuels that meet the specifications...

40 CFR 89.330 - Lubricating oil and test fuels.

Code of Federal Regulations, 2010 CFR

2010-07-01

... 40 Protection of Environment 20 2010-07-01 2010-07-01 false Lubricating oil and test fuels. 89.330... Equipment Provisions § 89.330 Lubricating oil and test fuels. (a) Lubricating oil. Use the engine... that is conducted by the Administrator shall be performed using test fuels that meet the specifications...

40 CFR 89.330 - Lubricating oil and test fuels.

Code of Federal Regulations, 2012 CFR

2012-07-01

... 40 Protection of Environment 21 2012-07-01 2012-07-01 false Lubricating oil and test fuels. 89.330... Equipment Provisions § 89.330 Lubricating oil and test fuels. (a) Lubricating oil. Use the engine... that is conducted by the Administrator shall be performed using test fuels that meet the specifications...

40 CFR 89.330 - Lubricating oil and test fuels.

Code of Federal Regulations, 2013 CFR

2013-07-01

... 40 Protection of Environment 21 2013-07-01 2013-07-01 false Lubricating oil and test fuels. 89.330... Equipment Provisions § 89.330 Lubricating oil and test fuels. (a) Lubricating oil. Use the engine... that is conducted by the Administrator shall be performed using test fuels that meet the specifications...

Selection and Application of Liquid and Semi-Solid Lubricants in Aerospace Vehicles and Supporting Equipment

DTIC Science & Technology

1965-10-01

lubrication method even though the Correct lubricant and method of xubrioation were readily available with a long history of successful operation under...grease has failed. During the discussion of the lubricant failure it is disclosed that the failure is due to corrosion of titani ™ *etal located

Research on Liquid Lubricants for Space Mechanisms

NASA Technical Reports Server (NTRS)

Jones, William R., Jr.; Shogrin, Bradley A.; Jansen, Mark J.

1999-01-01

Four research areas at the NASA Glenn Research Center involving the tribology of space mechanisms are highlighted. These areas include: soluble boundary lubrication additives for perfluoropolyether liquid lubricants, a Pennzane dewetting phenomenon, the effect of ODC-free bearing cleaning processes on bearing lifetimes and the development of a new class of liquid lubricants based on silahydrocarbons.

Research on liquid lubricants for space mechanisms

NASA Technical Reports Server (NTRS)

Jones, William R., Jr.; Shogrin, Bradley A.; Jansen, Mark J.

1998-01-01

Four research areas at the NASA Lewis Research Center involving the tribology of space mechanisms are highlighted. These areas include: soluble boundary lubrication additives for perfluoropolyether liquid lubricants, a Pennzane dewetting phenomenon, the effect of ODC-free bearing cleaning processes on bearing lifetimes, and the development of a new class of liquid lubricants based on silahydrocarbons.

Phosphate Reactions as Mechanisms of High-Temperature Lubrication

NASA Technical Reports Server (NTRS)

Nagarajan, Anitha; Garrido, Carolina; Gatica, Jorge E.; Morales, Wilfredo

2006-01-01

One of the major problems preventing the operation of advanced gas turbine engines at higher temperatures is the inability of currently used liquid lubricants to survive at these higher temperatures under friction and wear conditions. Current state-of-the-art organic liquid lubricants rapidly degrade at temperatures above 300 C; hence some other form of lubrication is necessary. Vapor-phase lubrication is a promising new technology for high-temperature lubrication. This lubrication method employs a liquid phosphate ester that is vaporized and delivered to bearings or gears; the vapor reacts with the metal surfaces, generating a solid lubricious film that has proven very stable at high temperatures. In this study, solid lubricious films were grown on cast-iron foils in order to obtain reaction and diffusion rate data to help characterize the growth mechanism. A phenomenological mathematical model of the film deposition process was derived incorporating transport and kinetic parameters that were coupled to the experimental data. This phenomenological model can now be reliably used as a predictive and scale-up tool for future vapor-phase lubrication studies.

Feasibility Study of Vapor-Mist Phase Reaction Lubrication Using a Thioether Liquid

NASA Technical Reports Server (NTRS)

Morales, Wilfredo; Handschuh, Robert F.; Krantz, Timothy L.

2007-01-01

A primary technology barrier preventing the operation of gas turbine engines and aircraft gearboxes at higher temperatures is the inability of currently used liquid lubricants to survive at the desired operating conditions over an extended time period. Current state-of-the-art organic liquid lubricants rapidly degrade at temperatures above 300 C; hence, another form of lubrication is necessary. Vapor or mist phase reaction lubrication is a unique, alternative technology for high temperature lubrication. The majority of past studies have employed a liquid phosphate ester that was vaporized or misted, and delivered to bearings or gears where the phosphate ester reacted with the metal surfaces generating a solid lubricious film. This method resulted in acceptable operating temperatures suggesting some good lubrication properties, but the continuous reaction between the phosphate ester and the iron surfaces led to wear rates unacceptable for gas turbine engine or aircraft gearbox applications. In this study, an alternative non-phosphate liquid was used to mist phase lubricate a spur gearbox rig operating at 10,000 rpm under highly loaded conditions. After 21 million shaft revolutions of operation the gears exhibited only minor wear.

Double angle seal forming lubricant film

DOEpatents

Ernst, William D.

1984-01-01

A lubricated piston rod seal which inhibits gas leaking from a high pressure chamber on one side of the seal to a low pressure chamber on the other side of the seal. A liquid is supplied to the surface of the piston rod on the low pressure side of the seal. This liquid acts as lubricant for the seal and provides cooling for the rod. The seal, which can be a plastic, elastomer or other material with low elastic modulus, is designed to positively pump lubricant through the piston rod/seal interface in both directions when the piston rod is reciprocating. The capacity of the seal to pump lubricant from the low pressure side to the high pressure side is less than its capacity to pump lubricant from the high pressure side to the low pressure side which ensures that there is zero net flow of lubricant to the high pressure side of the seal. The film of lubricant between the seal and the rod minimizes any sliding contact and prevents the leakage of gas. Under static conditions gas leakage is prevented by direct contact between the seal and the rod.

Development of solid-lubricated ball-screws for use in space

NASA Technical Reports Server (NTRS)

Chiba, Masatoshi; Gyougi, Toru; Nishimura, Makoto; Seki, Katsumi

1991-01-01

Ball-screws lubricated by solid lubricant films containing molybdenum disulphide are developed. The ball-screws (shaft diameter: phi 25 mm, length: 667 mm) were operated under a load of 40 to 120 N at a speed of 1.5 to 200 rpm at 10(exp -5) Pa. First, ball-screws made of stainless steel SUS 440C were studied using test equipment originally designed for this study. To reduce weight, the next step taken was to develop a ball-screw made of 6Al-4V-titanium. Long wear-life of more than 1 x 10(exp 7) revolutions was achieved with solid lubricated ball-screws made of SUS 440C and 6Al-4V-titanium in a hard vacuum. According to the surface profile of the shaft measured after 1 x 10(exp 7) revolutions, more solid lubricant remained on the surface of 6Al-4V-titanium than that of stainless steel. Auger and EPMA analysis confirmed lubrication was maintained by solid lubricant on nuts and screws after the lubricant films on the balls were worn off.

Effect of Applied Load and Sliding Speed on Tribological Behavior of TiAl-Based Self-Lubricating Composites

NASA Astrophysics Data System (ADS)

Liu, Xiyao; Shen, Qiao; Shi, Xiaoliang; Zou, Jialiang; Huang, Yuchun; Zhang, Ao; Yan, Zhao; Deng, Xiaobin; Yang, Kang

2018-01-01

This article was dedicated to explore the combined lubrication of silver, MoS2 and carbon nanotubes (CNTs) based on the changes in applied loads and sliding speeds. The results showed that the formed lubricating films played the major role in undertaking the equivalent stress, as well as effectively reduced friction resistance and material loss. It led to small friction coefficient and less wear rate at 1.2 m/s. At 1.2 m/s-16 N, an integrated lubricating film containing Ag, CNTs and MoS2 was continuously formed, which well provided the excellent lubricating property, resulting in lower friction coefficient (0.19) and less wear rate (1.56 × 10-5 mm3/N m). The formation of Ag and CNTs enriched islands acted as the bearing areas and played the major role in resisting friction resistance. Meanwhile, solid lubricant MoS2 was enriched in the lubricating film and effectively protected lubricating film from being destroyed, resulting in small friction coefficient and less wear rate at 1.2 m/s-16 N.

Nanopolishing by colloidal nanodiamond in elastohydrodynamic lubrication

NASA Astrophysics Data System (ADS)

Shirvani, Khosro A.; Mosleh, Mohsen; Smith, Sonya T.

2016-08-01

In this paper, the feasibility of using explosion synthesized diamond nanoparticles with an average particle size (APS) of 3-5 nm with a concentration of 1 % by weight for improving lubrication and friction in elastohydrodynamic lubrication (EHL) was investigated. Owing to the orders of magnitude increase in the viscosity of the lubricant in the EHL contact zone, diamond nanoparticles in the lubricant polish the surfaces at the nanoscale which decreases the composite roughness of contacting surfaces. The reduced composite roughness results in an increased film thickness ratio which yields lower friction. In the numerical analysis, governing equations of lubricant flow in the full elastohydrodynamic lubrication were solved, and the shear stress distribution over the fluid film was calculated. Using an abrasion model and the shear stress distribution profile, the material removal by the nanofluid containing nanoparticles and the resultant surface roughness were determined. The numerical analysis showed that in full EHL regime, the nanolubricant can reduce the composite roughness of moving surfaces. Experimental results from prior studies which exhibited surface polishing by such nanolubricants in boundary, mixed, and full elastohydrodynamic lubrication were used for comparison to the numerical model.

Lubricant Rheology in Concentrated Contacts

NASA Technical Reports Server (NTRS)

Jacobson, B. O.

1984-01-01

Lubricant behavior in highly stressed situtations shows that a Newtonian model for lubricant rheology is insufficient for explanation of traction behavior. The oil film build up is predicted by using a Newtonian lubricant model except at high slide to roll ratios and at very high loads, where the nonNewtonian behavior starts to be important already outside the Hertzian contact area. Static and dynamic experiments are reported. In static experiments the pressure is applied to the lubricant more than a million times longer than in an EHD contact. Depending on the pressure-temperature history of the experiment the lubricant will become a crystallized or amorphous solid at high pressures. In dynamic experiments, the oil is in an amorphous solid state. Depending on the viscosity, time scale, elasticity of the oil and the bearing surfaces, the oil film pressure, shear strain rate and the type of lubricant, different properties of the oil are important for prediction of shear stresses in the oil. The different proposed models for the lubricant, which describe it to a Newtonian liquid, an elastic liquid, a plastic liquid and an elastic-plastic solid.

Analysis of hazardous organic residues from sodium hydrosulfite industry and utilization as raw materials in a novel solid lubricant production.

PubMed

Shang, Jiwu; Zhang, Yihe; Zhou, Fengshan; Lv, Fengzhu; Han, Feng; Lu, Jinbo; Meng, Xianghai; Chu, Paul K; Ye, Zhengfang; Xing, Jing

2011-12-30

The hazardous organic residual wastes produced by the sodium hydrosulfite industry are demonstrated to be convertible into a novel solid lubricant. Identification and isolation of the organic residues are achieved by Fourier transform infrared (FTIR) spectroscopy, gas chromatography-mass spectrometry (GC-MS), and nuclear magnetic resonance (NMR). FTIR and GC-MS provide important information about the residues and the two main components obtained by column chromatography are further analyzed by NMR. The main organic residues are found to be thiodiglycol and 2,2'-dithiodiethanol which have potential applications in petroleum drilling because of their S-S and/or C-S functional groups. The lubricity of the organic residues is subsequently studied and the influence of different adsorbents on the lubricity is investigated and discussed. This homemade lubricant is observed to have good lubricity and by increasing the concentration of the commercial solid lubricant M, the lubricity diminishes. The process is expected to not only have commercial impact but also help to reduce environmental pollution. Copyright © 2011 Elsevier B.V. All rights reserved.

The roles of contact conformity, temperature and displacement amplitude on the lubricated fretting wear of a steel-on-steel contact

PubMed Central

Warmuth, A. R.; Sun, W.; Shipway, P. H.

2016-01-01

This paper investigates the effect of contact geometry, temperature and displacement amplitude on the fretting behaviour of an aero-turbo oil lubricated cylinder-on-flat contact. To be effective, the lubricant needed both to penetrate the contact and then offer protection. Lubricant penetration into the fretting contact is found to be controlled by two physical parameters, namely (i) the width of the contact that remains covered throughout the fretting test and (ii) the lubricant viscosity. The protection offered by the lubricant (assuming that it has successfully penetrated the contact) is influenced by four physical parameters, namely (i) lubricant viscosity, (ii) traverse velocity, (iii) nominal contact pressure, and (iv) chemical effects. The relationship between the three experimental parameters which were varied in the programme of work (temperature, fretting displacement and cylinder radius) and physical parameters which influence the protection offered by the lubricant film can be competing, and therefore complex wear behaviour is observed. The roles of the various parameters in controlling the wear behaviour are presented in a coherent physical framework. PMID:27853530

Dairy Equipment Lubrication

NASA Technical Reports Server (NTRS)

1978-01-01

Lake To Lake Dairy Cooperative, Manitowoc, Wisconsin, operates four plants in Wisconsin for processing milk, butter and cheese products from its 1,300 member farms. The large co-op was able to realize substantial savings by using NASA information for improved efficiency in plant maintenance. Under contract to Marshall Space Flight Center, Midwest Research Institute compiled a handbook consolidating information about commercially available lubricants. The handbook details chemical and physical properties, applications, specifications, test procedures and test data for liquid and solid lubricants. Lake To Lake's plant engineer used the handbook to effect savings in maintenance labor and materials costs by reducing the number of lubricants used on certain equipment. Strict U.S. Department of Agriculture and Food and Drug Administration regulations preclude lubrication changes n production equipment, but the co-op's maintenance chief was able to eliminate seven types of lubricants for ancillary equipment, such as compressors and high pressure pumps. Handbook data enabled him to select comparable but les expensive lubricants in the materials consolidation process, and simplified lubrication schedules and procedures. The handbook is in continuing use as a reference source when a new item of equipment is purchased.

Lubricant retention in liquid-infused microgrooves exposed to turbulent flow

NASA Astrophysics Data System (ADS)

Fu, Matthew; Chen, Ting-Hsuan; Arnold, Craig; Hultmark, Marcus

2017-11-01

Liquid infused surfaces are a promising method of passive drag reduction for turbulent flows. These surfaces rely on functionalized roughness elements to trap a liquid lubricant that is immiscible with external fluids. The presence of the lubricant creates a collection of fluid-fluid interfaces which can support a finite slip velocity at the effective surface. Generating a streamwise slip at the surface has been demonstrated as an effective mechanism for drag reduction; however, sustained drag reduction is predicated on the retention of the lubricating layer. Here, a turbulent channel-flow facility is used to characterize the robustness of liquid-infused surfaces and evaluate criteria for ensuring retention of the lubricant. Microscale grooved surfaces infused with alkane lubricants are mounted flush in the channel and exposed to turbulent flows. The retention of lubricants and pressure drop are monitored to characterize the effects of surface geometry and lubricant properties. To improve the retention of lubricant within grooved structures, a novel laser patterning technique is used to scribe chemical barriers onto grooved surfaces and evaluated. Supported under ONR Grants N00014-12-1-0875 and N00014-12-1-0962 (program manager Ki-Han Kim) and by the Department of Defense (DoD) through the National Defense Science & Engineering Graduate Fellowship (NDSEG) Program.

In vitro tests of substitute lubricants for wear testing orthopaedic biomaterials.

PubMed

Scholes, Susan C; Joyce, Thomas J

2013-06-01

Bovine serum is the lubricant recommended by several international standards for the wear testing of orthopaedic biomaterials; however, there are issues over its use due to batch variation, degradation, cost and safety. For these reasons, alternative lubricants were investigated. A 50-station Super-CTPOD (circularly translating pin-on-disc) wear test rig was used, which applied multidirectional motion to ultra-high-molecular-weight polyethylene test pins rubbing against cobalt chromium discs. Thirteen possible alternative lubricants were tested. The use of soy protein as a lubricant gave statistically higher wear, while soya oil, olive oil, Channel Island milk, whole milk, whey, wheatgerm oil, 11 mg/mL egg white, albumin/globulin mix and albumin/globulin/chondroitin sulphate mix all gave statistically lower wear than bovine serum. The lubricants giving the closest wear results to bovine serum were 20 and 40 mg/mL egg white solutions. A light absorbance assay found that these egg white solutions suffered from a high degradation rate that increased with increasing protein content. While egg white solutions offer the best alternative lubricant to bovine serum due to the wear volumes produced, cost-effectiveness and safety of handling, protein degradation will still occur, leading to the need for regular lubricant replacement. Of the lubricants tested in this study, none were found to be superior to bovine serum.

Mechanics of a gaseous film barrier to lubricant wetting of elastohydrodynamically lubricated conjunctions

NASA Technical Reports Server (NTRS)

Prahl, J. M.; Hamrock, B. J.

1985-01-01

Two analytical models, one based on simple hydrodynamic lubrication and the other on soft elastohydrodynamic lubrication, are presented and compared to delineate the dominant physical parameters that govern the mechanics of a gaseous film between a small droplet of lubricant and the outer race of a ball bearing. Both models are based on the balance of gravity forces, air drag forces, and air film lubrication forces and incorporate a drag coefficient C sub D and a lubrication coefficient C sub L to be determined from experiment. The soft elastohydrodynamic lubrication (EHL) model considers the effects of droplet deformation and solid-surface geometry; the simpler hydrodynamic lubrication (HL) model assumes that the droplet remains essentially spherical. The droplet's angular position depended primarily on the ratio of gas inertia to droplet gravity forces and on the gas Reynolds number and weakly on the ratio of droplet gravity forces to surface tension forces (Bond number) and geometric ratios for the soft EHL. An experimental configuration in which an oil droplet is supported by an air film on the rotating outer race of a ball bearing within a pressure-controlled chamber produced measurements of droplet angular position as a function of outer-race velocity droplet size and type, and chamber pressure.

Effect of an isotonic lubricant on sperm collection and sperm quality.

PubMed

Agarwal, Ashok; Malvezzi, Helena; Sharma, Rakesh

2013-05-01

To assess the influence of an isotonic lubricant used during sperm sample collection on [1] ease of collection and [2] resultant sperm quality. Paired randomized cross-over design. Tertiary hospital. Healthy men over 18 years old with normal semen analysis as per World Health Organization 2010 guidelines. Collection of semen sample from 22 subjects by masturbation with or without the use of Pre-Seed personal lubricant. Qualitative survey results and quantitative sperm function outcomes were measured to determine resultant sperm quality and collection experience with and without Pre-Seed lubricant. The qualitative questionnaire results showed that 73% of donors prefer the semen collection process with the isotonic lubricant and 55% recommended the use of lubricant in their everyday collection. The motility, viability, membrane integrity, levels of reactive oxygen species, total antioxidant capacity, and percentage of DNA damage in collected semen samples were not affected by the use of the lubricant. More donors prefer, and find it easier, to collect semen samples with the use of the lubricant. The isotonic lubricant Pre-Seed did not compromise sperm quality as evaluated in an array of sperm assays, suggesting its safe use in fertility patients as required during sperm collection. Copyright © 2013 American Society for Reproductive Medicine. Published by Elsevier Inc. All rights reserved.

Effect of lubricant on the reliability of dental implant abutment screw joint: An in vitro laboratory and three-dimension finite element analysis.

PubMed

Wu, Tingting; Fan, Hongyi; Ma, Ruiyang; Chen, Hongyu; Li, Zhi; Yu, Haiyang

2017-06-01

Biomechanical factors play a key role in the success of dental implants. Fracture and loosening of abutment screws are major issues. This study investigated the effect of lubricants on the stability of dental implant-abutment connection. As lubricants, graphite and vaseline were coated on the abutment screw surface, respectively, and a blank without lubricant served as the control. The total friction coefficient (μ tot ), clamping force, fatigue behavior and detorque of the joint combined with dynamic cyclic loading were measured under different lubricating conditions. Further, a three-dimensional finite element analysis was used to investigate stress distribution, in conjunction with experimental images. The results showed that the lubricant reduced μ tot , which in turn led to an increase in clamping force. Decrease in loading increased the fatigue life of the screw. However, use of lubricant at high load reduced the fatigue life. Ductile fracture at the first thread of the screw was the chief failure mode, which was due to maximum von Mises stress. Higher stress levels occurred in the lubricant groups. Lubricated screws resulted in lower detorque which made the joint easier to loosen. In conclusion, the lubricant cannot effectively improve the reliability of dental implant-abutment connection. Keeping the interfaces of implant-screw uncontaminated and strengthening the surface of the screw may be recommend for clinical operation and future design. Copyright © 2016 Elsevier B.V. All rights reserved.

The experimental evaluation and application of high-temperature solid lubricants. Ph.D. Thesis - Case Western Reserve Univ., 1989 Final Report

NASA Technical Reports Server (NTRS)

Dellacorte, Christopher

1990-01-01

A research program is described which developes an understanding of high-temperature solid lubrication and experimental techniques through the development of a composite lubricant coating system. The knowledge gained through this research was then applied to a specific engineering challenge, the tribology of a sliding seal for hypersonic flight vehicles. The solid lubricant coating is a chromium carbide based composite combined with silver, which acts as a low temperature lubricant, and barium fluoride/calcium fluoride eutectic, which acts as a high-temperature lubricant. This composite coating provides good wear resistance and low friction for sliding contacts from room temperature to over 900 C in reducing or oxidative environments. The specific research on this coating included a composition screening using a foil gas bearing test rig and the use of thin silver films to reduce initial wear using a pin-on-disk test rig. The chemical stability of the materials used was also addressed. This research indicated that soft metallic films and materials which become soft at elevated temperatures are potentially good lubricants. The general results from the experiments with the model solid lubricant coating were then applied to a sliding seal design concept. This seal design requires that a braided ceramic fabric slide against a variety of metal counterface materials at temperatures from 25 to 850 C in an oxidative environment. A pin-on-disk tribometer was used to evaluate the tribological properties of these materials and to develop lubrication techniques. The results indicate that these seal materials must be lubricated to prevent wear and reduce friction. Thin films of silver, gold and calcium fluoride provided lubrication to the sliding materials.

An event-level analysis of adding exogenous lubricant to condoms in a sample of men who have vaginal sex with women.

PubMed

Reece, Michael; Mark, Kristen; Herbenick, Debby; Hensel, Devon J; Jawed-Wessel, Sofia; Dodge, Brian

2012-03-01

Little is known about the characteristics of sexual events during which individuals choose to use lubricant with condoms. The aims of this article were to evaluate the determinants of adding lubricant to condoms during baseline and at the event level, to assess the event-level variables' influence on adding lubricants to condoms, and to assess the event-level influence of using condoms with lubricant on event-level condom attitudes. A total of 1,874 men completed a 30-day Internet-based prospective daily diary study of sexual behavior and condom use. Baseline data included demographic variables and information about condom education. Daily diary data included reports of penile-vaginal sex regarding intercourse duration, intercourse intensity, intoxication level, condom application method, partner contraceptive method, and partner and relationship characteristics. Lubricant was added to 24.3% of the study-provided condoms and 26.2% of the condoms selected by study participants. Those with more education and those who were married were more likely to add lubrication to condoms. Adding lubricant to condoms, a female partner putting the condom on with her hands and using contraception, and the event occurring with a wife (vs. girlfriend) was significantly associated with longer intercourse. Event-level lubricant and condom use significantly predicted lower willingness to buy the condom it was used with, as well as to recommend the condom. Adding exogenous lubricant was not related to the participants' confidence in condoms as a method to prevent pregnancy and sexually transmitted infections. The event-level nature of this study provided for a more comprehensive assessment of the situational factors that are associated with applying lubricant to condoms. Findings from this study suggest that men are adding lubricant to condoms for reasons other than to increase condom efficacy. © 2012 International Society for Sexual Medicine.

Vapor/Mist Used to Lubricate Gears After Loss of Primary Lubrication System

NASA Technical Reports Server (NTRS)

Handschuh, Robert F.; Morales, Wilfredo

2001-01-01

Loss of lubrication in rotorcraft drive systems is a demanding requirement placed on drive system manufacturers. The drive system must operate for at least 30 minutes once the primary lubrication system has failed. This test is a military requirement that must be passed prior to certification of the aircraft. As new aircraft engines, operating at higher speeds, are fielded, the requirements for the drive system become increasingly more difficult. Also, the drive system must be lightweight, which minimizes the opportunity to use the gear bodies to absorb the tremendous amount of heating that takes place. In many cases, the amount of heat generated because of the high speed and load requires an emergency lubrication system that negatively impacts the aircraft's weight, complexity, and cost. A single mesh spur gear test rig is being used at the NASA Glenn Research Center to investigate possible emergency lubrication system improvements that will minimize the impact of having these systems onboard rotorcraft. A technique currently being investigated uses a vapor/mist system to lubricate the contacting surfaces after the primary lubrication system has been shut down. A number of tests were conducted in which the vapor/mist used the same lubricant as the primary system, but at a greatly reduced flow rate. Each test was initiated with the primary lubrication system operational and at steady-state conditions for a given speed and load. Then the primary lubrication system was shut down, and the vapor/mist lubrication system was initiated. An example of the tests conducted is shown in the figures. These preliminary tests have uncovered a mechanism that provides a lubricious, carbonaceous solid on the surface that actually reduces the surface temperature of the meshing gear teeth during operation. Surface analysis of the carbonaceous solid revealed it was graphitic. This mechanism is the synthetic lubricant "coking" on the active profile of the gears, which reduces the friction between the contacting gear surfaces. The level of load affects the onset of this mechanism: the higher the load, the sooner coking takes place. Future work will investigate several other factors that could improve the already promising results that have been attained.

Ball Bearings Equipped for In Situ Lubrication on Demand

NASA Technical Reports Server (NTRS)

Marchetti, Mario; Jones, William R., Jr.; Pepper, Stephen V.; Jansen, Mark; Predmore, Roamer

2005-01-01

In situ systems that provide fresh lubricants to ball/race contacts on demand have been developed to prolong the operational lives of ball bearings. These systems were originally intended to be incorporated into ball bearings in mechanisms that are required to operate in outer space for years, in conditions in which lubricants tend to deteriorate and/or evaporate. These systems may also be useful for similarly prolonging bearing lifetimes on Earth. Reservoirs have been among the means used previously to resupply lubricants. Lubricant- resupply reservoirs are bulky and add complexity to bearing assemblies. In addition, such a reservoir cannot be turned on or off as needed: it supplies lubricant continuously, often leading to an excess of lubricant in the bearing. A lubricator of the present type includes a porous ring cartridge attached to the inner or the outer ring of a ball bearing (see Figure 1). Oil is stored in the porous cartridge and is released by heating the cartridge: Because the thermal expansion of the oil exceeds that of the cartridge, heating causes the ejection of some oil. A metal film can be deposited on a face of the cartridge to serve as an electrical-resistance heater. The heater can be activated in response to a measured increase in torque that signals depletion of oil from the bearing/race contacts. Because the oil has low surface tension and readily wets the bearing-ring material, it spreads over the bearing ring and eventually reaches the ball/race contacts. The Marangoni effect (a surface-tension gradient associated with a temperature gradient) is utilized to enhance the desired transfer of lubricant to the ball/race contacts during heating. For a test, a ball bearing designed for use at low speed was assembled without lubricant and equipped with a porous-ring lubricator, the resistance heater of which consumed a power of less than 1 W when triggered on by a torque-measuring device. In the test, a load of 20 lb (.89 N) was applied and the bearing was turned at a rate of 200 RPM. The lubricator control was turned on at the beginning of the test, turned off for about 800 seconds, then turned on again. As shown in Figure 2, the controlled lubricator stabilized the torque in a low range, starting immediately after initial turn-on and immediately after resumption of the lubricator control.

Development and efficiency assessment of process lubrication for hot forging

NASA Astrophysics Data System (ADS)

Kargin, S.; Artyukh, Viktor; Ignatovich, I.; Dikareva, Varvara

2017-10-01

The article considers innovative technologies in testing and production of process lubricants for hot bulk forging. There were developed new compositions of eco-friendly water-graphite process lubricants for hot extrusion and forging. New approaches to efficiency assessment of process lubricants are developed and described in the following article. Laboratory and field results are presented.

Fundamentals of fluid lubrication

NASA Technical Reports Server (NTRS)

Hamrock, Bernard J.

1991-01-01

The aim is to coordinate the topics of design, engineering dynamics, and fluid dynamics in order to aid researchers in the area of fluid film lubrication. The lubrication principles that are covered can serve as a basis for the engineering design of machine elements. The fundamentals of fluid film lubrication are presented clearly so that students that use the book will have confidence in their ability to apply these principles to a wide range of lubrication situations. Some guidance on applying these fundamentals to the solution of engineering problems is also provided.

Vapor-delivered lubrication of steel-steel and steel-ceramic systems

NASA Astrophysics Data System (ADS)

Li, H.; Klaus, E. E.; Duda, J. L.

1993-04-01

Heavy-duty natural gas engines run hot and relatively dry. This provides lubricant and lubrication problems in the piston ring-cylinder and valve areas. A potential materials solution to this problem is the use of ceramic bearing surfaces. The objective of the project was the investigation of the wear characteristics and surface interactions of lubricants on ceramic bearing surfaces and to compare these results with the behavior of the same lubricants on steel surfaces. The temperature range of interest in these comparisons is 200 to 370 C using a four-ball wear tester.

Molecular dynamics study of lubricant depletion by pulsed laser heating

NASA Astrophysics Data System (ADS)

Seo, Young Woo; Rosenkranz, Andreas; Talke, Frank E.

2018-05-01

In this study, molecular dynamics simulations were performed to numerically investigate the effect of pulsed laser heating on lubricant depletion. The maximum temperature, the lubricant depletion width, the number of evaporated lubricant beads and the number of fragmented lubricant chains were studied as a function of laser peak power, pulse duration and repetition rate. A continuous-wave laser and a square pulse laser were simulated and compared to a Gaussian pulse laser. With increasing repetition rate, pulsed laser heating was found to approach continuous-wave laser heating.

Development of high temperature liquid lubricants for low-heat rejection: Heavy duty diesel engines

NASA Technical Reports Server (NTRS)

Wiczynski, P. D.; Marolewski, T. A.

1993-01-01

The objective of this DOE program was to develop a liquid lubricant that will allow advanced diesel engines to operate at top ring reversal temperatures approaching 500 C and sump temperatures approaching 250 C. The lubricants developed demonstrated at marginal increase in sump temperature capability, approximately 15 C, and an increase in top ring reversal temperature. A 15W-40 synthetic lubricant designated HTL-4 was the best lubricant developed in terms of stability, wear control, deposit control dispersancy, and particulate emissions.

Wormgear geometry adopted for implementing hydrostatic lubrication and formulation of the lubrication problem

NASA Technical Reports Server (NTRS)

Sun, D. C.; Yuan, Qin

1995-01-01

The geometrical parameters for a wormgear intended to be used as the transmission in advanced helicopters are finalized. The resulting contact pattern of the meshing tooth surfaces is suitable for the implementation of hydrostatic lubrication Fluid film lubrication of the contact is formulated considering external pressurization as well as hydrodynamic wedge and squeeze actions. The lubrication analysis is aimed at obtaining the oil supply pressure needed to separate the worm and gear surfaces by a prescribed minimum film thickness. The procedure of solving the mathematical problem is outlined.

Effect of surface condition on the formation of solid lubricating films at high temperatures

NASA Technical Reports Server (NTRS)

Hanyaloglu, Bengi; Graham, E. E.

1992-01-01

Solid films were produced on active metal or ceramic surfaces using lubricants (such as tricresyl phosphate) delivered as a vapor at high temperatures, and the lubricity of these deposits under different dynamic wear conditions was investigated. A method is described for chemically activating ceramic surfaces resulting in a surface that could promote the formation of lubricating polymeric derivative of TCP. Experiments were carried out to evaluate the wear characteristics of unlubricated cast iron and of Sialon ceramic at 25 and 280 C, and lubricated with a vapor of TCP at 280 C. It is shown that continuous vapor phase lubrication of chemically treated Sialon reduced its coefficient of friction from 0.7 to less than 0.1.

Evaluation of an In-Situ, Liquid Lubrication System for Space Mechanisms Using a Vacuum Spiral Orbit Tribometer

NASA Technical Reports Server (NTRS)

Jansen, Mark J.; Jones, William R., Jr.; Pepper, Stephen V.

2002-01-01

Many moving mechanical assemblies (MMAs) for space applications rely on a small, initial charge of lubricant for the entire mission lifetime, often in excess of five years. In many cases, the premature failure of a lubricated component can result in mission failure. If lubricant could be resupplied to the contact in-situ, the life of the MMA could be extended. A vacuum spiral orbit tribometer (SOT) was modified to accept a device to supply re-lubrication during testing. It was successfully demonstrated that a liquid lubricant (Pennzane (Registered Trademark)/Nye 2001A) could be evaporated into a contact during operation, lowering the friction coefficient and therefore extending the life of the system.

Transmission Efficiency Measurements and Correlations with Physical Characteristics of the Lubricant

NASA Technical Reports Server (NTRS)

Coy, J. J.; Mitchell, A. M.; Hamrock, B. J.

1984-01-01

Data from helicopter transmission efficiency tests were compared to physical properties of the eleven lubricants used in those tests. The tests were conducted with the OH-58 helicopter main rotor transmission. Efficiencies ranged from 98.3 to 98.8 percent. The data was examined for correlation of physical properties with efficiency. There was a reasonable correlation of efficiency with absolute viscosity if the viscosity was first corrected for temperature and pressure in the lubricated contact. Between lubricants, efficiency did not correlate well with viscosity at atmospheric pressure. Between lubricants, efficiency did not correlate well with calculated lubricant film forming capacity. Bench type sliding friction and wear measurements could not be correlated to transmission efficiency and component wear.

Lubricants or lubricant additives composed of ionic liquids containing ammonium cations

DOEpatents

Qu, Jun [Knoxville, TN; Truhan, Jr; John, J [Cookeville, TN; Dai, Sheng [Knoxville, TN; Luo, Huimin [Knoxville, TN; Blau, Peter J [Knoxville, TN

2010-07-13

A lubricant or lubricant additive is an ionic liquid alkylammonium salt. The alkylammonium salt has the structure R.sub.xNH.sub.(4-x).sup.+,[F.sub.3C(CF.sub.2).sub.yS(O).sub.2].sub.2N.sup- .- where x is 1 to 3, R is independently C.sub.1 to C.sub.12 straight chain alkyl, branched chain alkyl, cycloalkyl, alkyl substituted cycloalkyl, cycloalkyl substituted alkyl, or, optionally, when x is greater than 1, two R groups comprise a cyclic structure including the nitrogen atom and 4 to 12 carbon atoms, and y is independently 0 to 11. The lubricant is effective for the lubrication of many surfaces including aluminum and ceramics surfaces.

Novel nano bearings constructed by physical adsorption

PubMed Central

Zhang, Yongbin

2015-01-01

The paper proposes a novel nano bearing formed by the physical adsorption of the confined fluid to the solid wall. The bearing is formed between two parallel smooth solid plane walls sliding against one another, where conventional hydrodynamic lubrication theory predicted no lubricating effect. In this bearing, the stationary solid wall is divided into two subzones which respectively have different interaction strengths with the lubricating fluid. It leads to different physical adsorption and slip properties of the lubricating fluid at the stationary solid wall respectively in these two subzones. It was found that a significant load-carrying capacity of the bearing can be generated for low lubricating film thicknesses, because of the strong physical adsorption and non-continuum effects of the lubricating film. PMID:26412488

Motion of a rigid sphere through an elastic tube with a lubrication film

NASA Astrophysics Data System (ADS)

Tani, Marie; Cambau, Thomas; Bico, Jose; Reyssat, Etienne

2017-11-01

The motion of large objects through narrow tubes is a common problem in physiology and more generally in the biological world. We built a model experiment where a rigid sphere is moved inside a narrower elastic tube coated with a lubricating fluid. The friction force is generally lower than in a non-lubricated situation. Interestingly, the force increases with the pulling velocity to the power 1/3, and also depends on the viscosity of the lubricant, the geometry and the mechanical properties of the tube. All our experimental data are well described by a scaling law combining lubrication and elasticity equations. We furthermore measured the thickness of the lubricant film. We present all these results.

Comparison of in vivo efficacy of different ocular lubricants in dry eye animal models.

PubMed

Zheng, Xiaodong; Goto, Tomoko; Ohashi, Yuichi

2014-04-29

To compare the efficacy of three types of ocular lubricants in protecting corneal epithelial cells in dry eye animal models. Ocular lubricants containing 0.1% or 0.3% sodium hyaluronate (SH), carboxymethylcellulose (CMC), or hydroxypropyl methylcellulose (HPMC) were tested. First, ocular lubricant containing 0.002% fluorescein was dropped onto the rabbit corneas. The fluorescein intensity as an index of retention was measured. Second, a rabbit dry eye model was made by holding the eye open with a speculum, and 50 μL of each ocular lubricant was dropped onto the cornea. After 3 hours, the corneas were stained with 1% methylene blue (MB), and the absorbance of MB was measured. Third, a rat dry eye model was treated with the ocular lubricants for 4 weeks, and the corneal fluorescein staining was scored. Eyes treated with physiological saline were used as controls. Finally, immunohistochemistry was used to analyze occludin, an epithelial barrier protein, in cultured human corneal epithelial cells pretreated with ocular lubricants and desiccated for 20 or 60 minutes. Our results showed that 0.3% SH had a significantly longer retention time than the other lubricants (all P < 0.01). The absorbance of MB was significantly lower in the 0.3% SH group. The corneas of rats exposed to 0.3% SH had significantly lower fluorescein staining scores. A significantly higher number of occludin-positive cells were found after exposure to 0.3% SH than other lubricants. Ocular lubricant containing 0.3% SH would be preferable to treat patients with dry eye syndrome. Copyright 2014 The Association for Research in Vision and Ophthalmology, Inc.

Identification of lubrication oil in the particulate matter emissions from engine exhaust of in-service commercial aircraft.

PubMed

Yu, Zhenhong; Herndon, Scott C; Ziemba, Luke D; Timko, Michael T; Liscinsky, David S; Anderson, Bruce E; Miake-Lye, Richard C

2012-09-04

Lubrication oil was identified in the organic particulate matter (PM) emissions of engine exhaust plumes from in-service commercial aircraft at Chicago Midway Airport (MDW) and O'Hare International Airport (ORD). This is the first field study focused on aircraft lubrication oil emissions, and all of the observed plumes described in this work were due to near-idle engine operations. The identification was carried out with an Aerodyne high-resolution time-of-flight aerosol mass spectrometer (HR-ToF AMS) via a collaborative laboratory and field investigation. A characteristic mass marker of lubrication oil, I(85)/I(71), the ratio of ion fragment intensity between m/z = 85 and 71, was used to distinguish lubrication oil from jet engine combustion products. This AMS marker was based on ion fragmentation patterns measured using electron impact ionization for two brands of widely used lubrication oil in a laboratory study. The AMS measurements of exhaust plumes from commercial aircraft in this airport field study reveal that lubrication oil is commonly present in organic PM emissions that are associated with emitted soot particles, unlike the purely oil droplets observed at the lubrication system vent. The characteristic oil marker, I(85)/I(71), was applied to quantitatively determine the contribution from lubrication oil in measured aircraft plumes, which ranges from 5% to 100%.

Keeping Your Compressor Healthy: Developing the Right Lubricant Formulation is the Key

NASA Astrophysics Data System (ADS)

Karnaz, Joseph A.; Kultgen, Derek W.

2015-08-01

Selecting the correct compressor lubricant is crucial to the duration of the compressor and the refrigerant systems’ useful life. However, developing an optimized lubricant for a refrigeration system requires a multitude of screenings and tests. The compatibility and stability of the lubricant with the refrigerant and compressor components needs to be examined at various accelerated conditions. The lubricant and refrigerant working viscosity must be determined at various refrigerant concentrations, temperatures and pressures as the diluted refrigerant in the lubricant has a significant effect on the viscosity. The correct lubricant formulation needs to be investigated for optimal performance. A compressor lubricant can provide many benefits to a refrigeration system such as bearing durability, sealing, and increased efficiency. Sometimes it is necessary to formulate the lubricant in order to optimize system performance. Specifically, this study investigated anti-wear properties of different oil additives to create a more robust refrigeration system. Many different additives and concentrations were considered and screened. Pending a successful screen test; these different additives’ anti-wear properties were analyzed using bench top tribology tests. To reduce uncertainty and provide more in-situ results the different additives were operated in a refrigerant compressor on a gas-loop testing apparatus. Oil samples were taken periodically during the test duration for analysis. Lastly, upon test completion the compressors were dismantled and the parts were examined to determine the effectiveness of the anti-wear additives.

Environmental Capability of Liquid Lubricants

NASA Technical Reports Server (NTRS)

Beerbower, A.

1973-01-01

The methods available for predicting the properties of liquid lubricants from their structural formulas are discussed. The methods make it possible to design lubricants by forecasting the results of changing the structure and to determine the limits to which liquid lubricants can cope with environmental extremes. The methods are arranged in order of their thermodynamic properties through empirical physical properties to chemical properties.

Applications of aerospace technology in industry, a technology transfer profile: Lubrication

NASA Technical Reports Server (NTRS)

Kottenstette, J. P.; Freeman, J. E.; Heins, C. R.; Hildred, W. M.; Johnson, F. D.; Staskin, E. R.

1971-01-01

Technology transfer in the lubrication field is discussed in terms of the movement of NASA-generated lubrication technology into the private sector as affected by evolving industrial requirements. An overview of the field is presented, and NASA technical contributions to lubrication technology are described. Specific examples in which these technologies have been used in the private sector are summarized.

Estimation of appropriate lubricating film thickness in ceramic-on-ceramic hip prostheses

NASA Astrophysics Data System (ADS)

Tauviqirrahman, M.; Muchammad, Bayuseno, A. P.; Ismail, R.; Saputra, E.; Jamari, J.

2016-04-01

Artificial hip prostheses, consisting of femoral head and acetabular cup are widely used and have affected the lives of many people.However, the primary issue associated with the long term performance of hip prostheses is loosening induced by excessive wear during daily activity. Therefore, an effective lubrication is necessary to significantly decrease the wear. To help understand the lubricating performance of such typical hip joint prostheses, in the present paper a hydrodynamic lubrication model based on Reynolds equationwas introduced. The material pairs of ceramic acetabular cup against ceramic femoral head was investegated.The main aim of this study is to investigate of the effect of loading on the formation of lubricating film thickness.The model of a ball-in-socket configuration was considered assuming that the cup was stationary while the ball was to rotate at a steady angular velocityvarying loads.Based on simulation result, it was found that to promote fluid film lubrication and prevent the contacting components leading to wear, the film thickness of lubricant should be determined carefully based on the load applied. This finding may have useful implication in predicting the failure of lubricating synovial fluid film and wear generation in hip prostheses.

Robust and Drain Resistant Lubricated Omniphobic Fabrics

NASA Astrophysics Data System (ADS)

Kido, Cassidee; Damle, Viraj; Sun, Xiaoda; Roopesh, Ajay; Doudrick, Kyle; Rykaczewski, Konrad

2014-11-01

The implications of omniphobic fabrics range from stainproof clothing to civilian and military protection from chemical weapons. The challenge comes in developing a product that remains effective in repelling droplets of liquids with a wide range of surface tensions even after being subjected to various stimuli imposed by human use. Omniphobic fabrics can be made by infusing hydrophobic nanoparticle coated fibers with a low surface energy lubricant. These types of lubricant impregnated surfaces can shed large deposited droplets as well as condensed microdroplets of variety of low surface tension liquids. However, here we show that lubricated omniphobic fabrics can easily lose their properties due to degradation of the nanostructure coating or drainage of the lubricant upon contact with a porous surface. We also demonstrate that this issue can be resolved with use of cross-linked polymer coated fibers that are swollen with the lubricant. Use of flexible polymers avoids structure degradation due to fabric deformation, while swelling of the polymer with lubricant minimizes lubricant drainage upon contact maintaining the omniphobic characteristics of the fabric. KR acknowledges startup funding from ASU and collaborative effort with Dr. Tim Burgin and James R. Lee from Naval Surface Warfare Center Dahlgren Division.

Energy efficient reduced graphene oxide additives: Mechanism of effective lubrication and antiwear properties

PubMed Central

Gupta, Bhavana; Kumar, N.; Panda, Kalpataru; Dash, S.; Tyagi, A. K.

2016-01-01

Optimized concentration of reduced graphene oxide (rGO) in the lube is one of the important factors for effective lubrication of solid body contacts. At sufficiently lower concentration, the lubrication is ineffective and friction/wear is dominated by base oil. In contrast, at sufficiently higher concentration, the rGO sheets aggregates in the oil and weak interlayer sliding characteristic of graphene sheets is no more active for providing lubrication. However, at optimized concentration, friction coefficient and wear is remarkably reduced to 70% and 50%, respectively, as compared to neat oil. Traditionally, such lubrication is described by graphene/graphite particle deposited in contact surfaces that provides lower shear strength of boundary tribofilm. In the present investigation, graphene/graphite tribofilm was absent and existing traditional lubrication mechanism for the reduction of friction and wear is ruled out. It is demonstrated that effective lubrication is possible, if rGO is chemically linked with PEG molecules through hydrogen bonding and PEG intercalated graphene sheets provide sufficiently lower shear strength of freely suspended composite tribofilm under the contact pressure. The work revealed that physical deposition and adsorption of the graphene sheets in the metallic contacts is not necessary for the lubrication. PMID:26725334

Friction-induced nano-structural evolution of graphene as a lubrication additive

NASA Astrophysics Data System (ADS)

Zhao, Jun; Mao, Junyuan; Li, Yingru; He, Yongyong; Luo, Jianbin

2018-03-01

Graphene has attracted enormous attention in the field of lubrication based on its excellent physical and chemical properties. Although many studies have obtained thermally or chemically- exfoliated graphene and investigated their wide and important application, few studies have reported their physical nano-structural evolution under friction. In this study, we investigated the lubrication properties of graphene additives with different layer numbers and interlayer spacing by exfoliating. The additives with a higher degrees of exfoliation changed to ordering under friction, and had better lubrication properties, while that with a lower degrees exhibited obvious structural defects and high friction. Therefore, the original degrees of exfoliation plays a key role in the structural evolution of graphene and superior lubrication can be achieved through the physical nano-structure changing to ordering, even graphitization. Furthermore, the ordered tribofilm on the frictional interfaces was parallel to the sliding direction, meaning the highly exfoliated graphene indeed reaching slippage between its layers, which wasn't experimentally discovered in previous studies. This work provides a new understanding of the relationship between friction-induced nano-structural evolution and lubrication properties of graphene as a lubrication additive, and has great potential for the structural design of graphene as a lubrication additive.

Characteristics Study of In-Situ Capacitive Sensor for Monitoring Lubrication Oil Debris.

PubMed

Han, Zhibin; Wang, Yishou; Qing, Xinlin

2017-12-08

As an essential part of engine health monitoring (EHM), online lubrication oil debris monitoring has recently received great attention for the assessment of rotating and reciprocating parts in aero-engines, due to its high integration, low cost and safe characteristics. However, it is be a challenge to find a suitable sensor operating in such a complex environment. We present an unconventional novel approach, in which a cylinder capacitive sensor is designed and integrated with the pipeline of an engine lubrication system, so that the capacitive sensor can effectively detect changes in the lubrication oil condition. In this paper, an attempt to illustrate the performance characteristics of the developed cylinder capacitive sensor is made, through an experiment system that simulates a real scenario of a lubrication oil system. The main aim of the research was to qualitatively describe the relationship between the sensor parameter and the lubrication oil debris. In addition, the effect of the temperature and flow rate of the lubrication oil on capacitance change was performed by several experiments and we figured out a compensation method. The experimental results demonstrated that the cylinder capacitive sensor can potentially be used for lubrication oil debris monitoring of the health condition of an aero-engine.

Correlation between surface topography and lubricant migration in steel sheets for the autobody manufacturing process

NASA Astrophysics Data System (ADS)

Benati, F.; Sacerdotti, F.; Griffiths, B. J.; Butler, C.; Karila, J. M.; Vermeulen, M.; Holtkamp, H.; Gatti, S.

2002-05-01

Material for the production of autobody panels is usually dispatched in the form of coils. Because of their weight, they tend to `compress' the lubricant applied for rust protection and some of it leaks from the coil. Those areas affected by lubricant starvation are known as `dry-spots' and are a cause of a number of product rejections during the subsequent forming operation. A test was deployed with the combined work of Ocas, CORUS IJmuiden and Renault that proved that surface topography controls, amongst other factors, affects lubricant migration. The test consists of compressing a stack of lubricated steel sheets at known pressure for a known time using different lubricants in different amounts. It was observed that, because of the `compression', the lubricant tends to migrate to the side of the sheet, and its migration was quantified using a Fischer Betascope MMS module. Analysis consisted of analysis of variance on several designs of experiments and subsequent correlation with surface topography 3D parameters. These experiments showed the importance of standard amplitude surface parameters and new closed area surface parameters to characterize lubricant migration under pressure.

Liquid Lubricants for Spacecraft Applications

NASA Astrophysics Data System (ADS)

Gill, S.; Rowntree, A.

Liquid lubricants used for spacecraft have advantages over solid lubricants but there are also disadvantages to consider. The challenge is to ensure that the liquid lubricant does not disappear from the mechanism by evaporation or creep. Lubricants can be used as fluids or formulated as greases. The liquids can be highly refined hydrocarbons, PAOs, silicones, polyol esters (POEs), multiply alkylated cycloparaffins, (MACs) or various perfluoropolyethers (PFPEs). Greases are made from these liquids using thickeners such as lithium, calcium or sodium soaps, PTFE, graphite or lead. Operational temperatures range from - 45°C to over 100°C. Low vapour pressures are crucial, below 10-8 mbar at 20°C and total weight loss must be <1% for general applications, <0.1% for optical applications. 'Surface creep rates' must be low, temperature gradients and surface Ra are important factors. The wear rates for standard tests using different lubricants vary over several orders of magnitude for different lubricants, surface coatings and rpm. Unexpected effects, such as PTFE 'plating out' at low rpm, occur. The main issues are to prevent the lubricant escaping from working areas and to protect it from degradation by chemical reactions or radiation.

Oil-air mist lubrication for helicopter gearing

NASA Technical Reports Server (NTRS)

Mcgrogan, F.

1976-01-01

The applicability of a once-through oil mist system to the lubrication of helicopter spur gears was investigated and compared to conventional jet spray lubrication. In the mist lubrication mode, cooling air was supplied at 366K (200 F) to the out of mesh location of the gear sets. The mist air was also supplied at 366K (200 F) to the radial position mist nozzle at a constant rate of 0.0632 mol/s (3 SCFM) per nozzle. The lubricant contained in the mist air varied between 32 - 44 cc/hour. In the recirculating jet spray mode, the flow rate was varied between 1893 - 2650 cc/hour. Visual inspection revealed the jet spray mode produced a superior surface finish on the gear teeth but a thermal energy survey showed a 15 - 20% increase in heat generated. The gear tooth condition in the mist lubrication mode system could be improved if the cooling air and lubricant/air flow ratio were increased. The test gearbox and the procedure used are described.

Scale-Up of Lubricant Mixing Process by Using V-Type Blender Based on Discrete Element Method.

PubMed

Horibe, Masashi; Sonoda, Ryoichi; Watano, Satoru

2018-01-01

A method for scale-up of a lubricant mixing process in a V-type blender was proposed. Magnesium stearate was used for the lubricant, and the lubricant mixing experiment was conducted using three scales of V-type blenders (1.45, 21 and 130 L) under the same fill level and Froude (Fr) number. However, the properties of lubricated mixtures and tablets could not correspond with the mixing time or the total revolution number. To find the optimum scale-up factor, discrete element method (DEM) simulations of three scales of V-type blender mixing were conducted, and the total travel distance of particles under the different scales was calculated. The properties of the lubricated mixture and tablets obtained from the scale-up experiment were well correlated with the mixing time determined by the total travel distance. It was found that a scale-up simulation based on the travel distance of particles is valid for the lubricant mixing scale-up processes.

Evaluation of the lubricating effect of magnesium stearate and glyceryl behenate solid lipid nanoparticles in a direct compression process.

PubMed

Martínez-Acevedo, Lizbeth; Zambrano-Zaragoza, María de la Luz; Vidal-Romero, Gustavo; Mendoza-Elvira, Susana; Quintanar-Guerrero, David

2018-05-02

The aim of this study was to develop solid lipid nanoparticles (SLN) and introduce them into a direct compression process to evaluate their lubricant properties. The study consisted of preparing glyceryl behenate SLN (Compritol® 888 ATO) by hot dispersion, and magnesium stearate SLN by a novel nanoprecipitation/ion exchange method. The ejection force was measured for nanosystems and raw materials in a formulation typically used for direct compression. The smallest particle sizes obtained were 456 nm for Compritol® 888 ATO and 330 nm for magnesium stearate. Results show that the NPs used as lubricants in a direct compression model formulation provided efficient lubrication by maintaining the lubricating properties of the system, thereby decreasing the amount of lubricant used compared to the raw material. The lubricating effect showed an increase of 15-30% for magnesium stearate and Compritol® 888 ATO, compared to the raw material at concentrations above 2%. Copyright © 2018 Elsevier B.V. All rights reserved.

Rotary shaft sealing assembly

DOEpatents

Dietle, Lannie L; Schroeder, John E; Kalsi, Manmohan S; Alvarez, Patricio D

2013-08-13

A rotary shaft sealing assembly in which a first fluid is partitioned from a second fluid in a housing assembly having a rotary shaft located at least partially within. In one embodiment a lip seal is lubricated and flushed with a pressure-generating seal ring preferably having an angled diverting feature. The pressure-generating seal ring and a hydrodynamic seal may be used to define a lubricant-filled region with each of the seals having hydrodynamic inlets facing the lubricant-filled region. Another aspect of the sealing assembly is having a seal to contain pressurized lubricant while withstanding high rotary speeds. Another rotary shaft sealing assembly embodiment includes a lubricant supply providing a lubricant at an elevated pressure to a region between a lip seal and a hydrodynamic seal with a flow control regulating the flow of lubricant past the lip seal. The hydrodynamic seal may include an energizer element having a modulus of elasticity greater than the modulus of elasticity of a sealing lip of the hydrodynamic seal.

Rotary shaft sealing assembly

DOEpatents

Dietle, Lannie L.; Schroeder, John E.; Kalsi, Manmohan S.; Alvarez, Patricio D.

2010-09-21

A rotary shaft sealing assembly in which a first fluid is partitioned from a second fluid in a housing assembly having a rotary shaft located at least partially within. In one embodiment a lip seal is lubricated and flushed with a pressure-generating seal ring preferably having an angled diverting feature. The pressure-generating seal ring and a hydrodynamic seal may be used to define a lubricant-filled region with each of the seals having hydrodynamic inlets facing the lubricant-filled region. Another aspect of the sealing assembly is having a seal to contain pressurized lubricant while withstanding high rotary speeds. Another rotary shaft sealing assembly embodiment includes a lubricant supply providing a lubricant at an elevated pressure to a region between a lip seal and a hydrodynamic seal with a flow control regulating the flow of lubricant past the lip seal. The hydrodynamic seal may include an energizer element having a modulus of elasticity greater than the modulus of elasticity of a sealing lip of the hydrodynamic seal.

Influence of fatty acid methyl esters from hydroxylated vegetable oils on diesel fuel lubricity.

PubMed

Goodrum, John W; Geller, Daniel P

2005-05-01

Current and future regulations on the sulfur content of diesel fuel have led to a decrease in lubricity of these fuels. This decreased lubricity poses a significant problem as it may lead to wear and damage of diesel engines, primarily fuel injection systems. Vegetable oil based diesel fuel substitutes (biodiesel) have been shown to be clean and effective and may increase overall lubricity when added to diesel fuel at nominally low levels. Previous studies on castor oil suggest that its uniquely high level of the hydroxy fatty acid ricinoleic acid may impart increased lubricity to the oil and its derivatives as compared to other vegetable oils. Likewise, the developing oilseed Lesquerella may also increase diesel lubricity through its unique hydroxy fatty acid composition. This study examines the effect of castor and Lesquerella oil esters on the lubricity of diesel fuel using the High-Frequency Reciprocating Rig (HFRR) test and compares these results to those for the commercial vegetable oil derivatives soybean and rapeseed methyl esters.

Development of the water-lubricated thrust bearing of the hydraulic turbine generator

NASA Astrophysics Data System (ADS)

Inoue, K.; Deguchi, K.; Okude, K.; Fujimoto, R.

2012-11-01

In hydropower plant, a large quantities of turbine oil is used as machine control pressure oil and lubricating oil. If the oil leak out from hydropower plant, it flows into a river. And such oil spill has an adverse effect on natural environment because the oil does not degrade easily. Therefore the KANSAI and Hitachi Mitsubishi Hydro developed the water-lubricated thrust bearing for vertical type hydraulic turbine generator. The water-lubricated bearing has advantages in risk avoidance of river pollution because it does not need oil. For proceeding the development of the water-lubricated thrust bearing, we studied following items. The first is the examination of the trial products of water lubricating liquid. The second is the study of bearing structure which can satisfy bearing performance such as temperature characteristic and so on. The third is the mock-up testing for actual application in the future. As a result, it was found that the water-lubricated thrust bearing was technically applicable to actual equipments.

Friction and lubrication modelling in sheet metal forming: Influence of lubrication amount, tool roughness and sheet coating on product quality

NASA Astrophysics Data System (ADS)

Hol, J.; Wiebenga, J. H.; Carleer, B.

2017-09-01

In the stamping of automotive parts, friction and lubrication play a key role in achieving high quality products. In the development process of new automotive parts, it is therefore crucial to accurately account for these effects in sheet metal forming simulations. This paper presents a selection of results considering friction and lubrication modelling in sheet metal forming simulations of a front fender product. For varying lubrication conditions, the front fender can either show wrinkling or fractures. The front fender is modelled using different lubrication amounts, tool roughness’s and sheet coatings to show the strong influence of friction on both part quality and the overall production stability. For this purpose, the TriboForm software is used in combination with the AutoForm software. The results demonstrate that the TriboForm software enables the simulation of friction behaviour for varying lubrication conditions, i.e. resulting in a generally applicable approach for friction characterization under industrial sheet metal forming process conditions.

Film thickness for different regimes of fluid-film lubrication. [elliptical contacts

NASA Technical Reports Server (NTRS)

Hamrock, B. J.; Dowson, D.

1983-01-01

Mathematical formulas are presented which express the dimensionless minimum film thickness for the four lubrication regimes found in elliptical contacts: isoviscous-rigid regime; piezoviscous-rigid regime; isoviscous-elastic regime; and piezoviscous-elastic regime. The relative importance of pressure on elastic distortion and lubricant viscosity is the factor that distinguishes these regimes for a given conjunction geometry. In addition, these equations were used to develop maps of the lubrication regimes by plotting film thickness contours on a log-log grid of the dimensionless viscosity and elasticity parameters for three values of the ellipticity parameter. These results present a complete theoretical film thickness parameter solution for elliptical constants in the four lubrication regimes. The results are particularly useful in initial investigations of many practical lubrication problems involving elliptical conjunctions.

Production of Dense Compact Billet From Ti-Alloy Powder Using Equal Channel Angular Extrusion

DTIC Science & Technology

2007-04-06

dry lubricant 2 175 RT 95.3 dry lubricant 3 262 RT 95.6 dry lubricant 4 21 100 95.4 dry lubricant 5 43 100 96 dry lubricant 6 175 100 96.2 dry...175 98.1 371 3 262 98.2 426 4 350 98.3 412 ECAE compaction with Al tubes 5 350 97.4 415 6 393 97.8 419 7 436 97.6 438 8* 480 98.6 431 ECAE...PRODUCTION OF DENSE COMPACT BILLET FROM Ti-ALLOY POWDER USING EQUAL CHANNEL ANGULAR EXTRUSION Final Report 4 /06/2007

Solid Lubrication Fundamentals and Applications. Chapter 2

NASA Technical Reports Server (NTRS)

Miyoshi, Kazuhisa

1998-01-01

This chapter describes powerful analytical techniques capable of sampling tribological surfaces and solid-film lubricants. Some of these techniques may also be used to determine the locus of failure in a bonded structure or coated substrate; such information is important when seeking improved adhesion between a solid-film lubricant and a substrate and when seeking improved performance and long life expectancy of solid lubricants. Many examples are given here and through-out the book on the nature and character of solid surfaces and their significance in lubrication, friction, and wear. The analytical techniques used include the late spectroscopic methods.

Film thickness for different regimes of fluid-film lubrication

NASA Technical Reports Server (NTRS)

Hamrock, B. J.

1980-01-01

Film thickness equations are provided for four fluid-film lubrication regimes found in elliptical contacts. These regimes are isoviscous-rigid; viscous-rigid; elastohydrodynamic lubrication of low-elastic-modulus materials (soft EHL), or isoviscous-elastic; and elastohydrodynamic lubrication of high-elastic-modulus materials (hard EHL), or viscous-elastic. The influence or lack of influence of elastic and viscous effects is the factor that distinguishes these regimes. The results are presented as a map of the lubrication regimes, with film thickness contours on a log-log grid of the viscosity and elasticity for three values of the ellipticity parameter.

New Lubricant for Pressure Die Casting,

DTIC Science & Technology

synthetic acids, finely dispersed graphite preparations, etc. The new lubricants are not inferior in their properties to the well known foreign lubricants antilov, olea , and emtek used in pressure die casting.

Effect of electrical current on the tribological behavior of the Cu-WS2-G composites in air and vacuum

NASA Astrophysics Data System (ADS)

Qian, Gang; Feng, Yi; Li, Bin; Huang, Shiyin; Liu, Hongjuan; Ding, Kewang

2013-03-01

As the traditional graphite-based composites cannot meet the requirement of rapid developing modern industry, novel sliding electrical contact materials with high self-lubricating performance in multiple environments are eagerly required. Herein a copper-based composite with WS2 and graphite as solid lubricant are fabricated by powder metallurgy hot-pressed method. The friction and wear behaviors of the composites with and without current are investigated under the condition with sliding velocity of 10 m/s and normal load of 2.5 N/cm2 in both air and vacuum. Morphologies of the worn surfaces are observed by optical microscope and compositions of the lubricating films are analyzed by XPS. Surface profile curves and roughness of the worn surfaces are obtained by 2205 surface profiler. The results of wear tests show that the friction coefficient and wear volume loss of the composites with current are greater than that without current in both air and vacuum due to the adverse effects of electrical current which damaged the lubricating film partially and roughed the worn surfaces. XPS results demonstrate that the lubricating film formed in air is composed of oxides of Cu, WS2, elemental S and graphite, while the lubricating film formed in vacuum is composed of Cu, WS2 and graphite. Because of the synergetic lubricating action of oxides of Cu, WS2 and graphite, the composites show low friction coefficient and wear volume loss in air condition. Owing to the fact that graphite loses its lubricity which makes WS2 become the only lubricant, severe adhesive and abrasive wear occur and result in a high value of wear rate in vacuum condition. The formation of the lubricating film on the contact interface between the brush and ring is one of the factors which can greatly affect the wear performance of the brushes. The low contact voltage drop of the composites in vacuum condition is attributed to the high content of Cu in the surface film. This study fabricated a kind of new sliding electrical contact self-lubricating composite with dual-lubricant which can work well in both air and vacuum environments and provides a comprehensive analysis on the lubrication mechanisms of the composite.

Commercial lubricant use among HIV-negative men who have sex with men in Los Angeles: implications for the development of rectal microbicides for HIV prevention.

PubMed

Pines, Heather A; Gorbach, Pamina M; Reback, Cathy J; Landovitz, Raphael J; Mutchler, Matt G; Mitsuyasu, Ronald

2014-01-01

To inform the development and assess potential use of rectal microbicide gels for HIV prevention among men who have sex with men (MSM), we examined the dynamics and contexts of commercial lubricant use during receptive anal intercourse (RAI) within this population. From 2007 to 2010, 168 HIV-negative MSM living in Los Angeles who practice RAI completed computer-assisted self-interviews, which collected information on their last sexual event with ≤3 recent partners, at baseline, three months, and one-year study visits. Logistic generalized linear mixed models were used to identify individual- and sexual event-level characteristics associated with commercial lubricant use during RAI at the last sexual event within 421 partnerships reported by participants over the course of follow-up. During RAI at their last sexual event, 57% of partnerships used a condom and 69% used commercial lubricant. Among partnerships that used commercial lubricant, 56% reported lubricant application by both members of the partnership, 66% first applied lubricant during sex, but before penetration, and 98% applied lubricant at multiple locations. The relationship between substance use and commercial lubricant use varied by condom use (interaction p-value = 0.01). Substance use was positively associated with commercial lubricant use within partnerships that did not use condoms during RAI at their last sexual event (AOR = 4.47, 95% [corrected] [CI]: 1.63-12.28), but no association was observed within partnerships that did use condoms (AOR = 0.66, 95% CI: 0.23-1.85). Commercial lubricant use during RAI was also positively associated with reporting more sexual partners (AOR = 1.18, 95% CI: 1.05-1.31), while older age (units = 5 years; AOR = 0.75, 95% CI: 0.61-0.94), homelessness (past year; AOR = 0.32, 95% CI: 0.13-0.76), and having sex with an older (>10 years) partner (AOR = 0.37, 95% CI: 0.14-0.95) were negatively associated with commercial lubricant use. These factors should be considered in the development of rectal microbicide gels to enhance their acceptability and use among MSM.

Torque vs. induced load of A-286, and MP35N nuts and bolts with cadmium, dry film, and cetyl alcohol lubricants

NASA Technical Reports Server (NTRS)

Crispell, C.

1978-01-01

Data for specific joint design, utilizing various combinations of bolt, nut and lubricants in typical structure of the shuttle booster rocket is obtained. Requirements of the structure performance criteria were to withstand temperatures of 260 C (500 F) and to provide a nut lubricant which would be compatible with sealants used in the joint. Cadmium plating and dry film lubricant meeting the requirements of MIL-L-8937 were the lubricants specified. In a follow up effort, cadmium plating and cetyl alcohol were further specified The materials for the bolt and nut combinations were MP35N and A-286. These materials demand a lubricant to be used to prevent galling of the thread when tightened and also to help reduce the scatter of clamping load in application.

Ionic liquids in tribology.

PubMed

Minami, Ichiro

2009-06-24

Current research on room-temperature ionic liquids as lubricants is described. Ionic liquids possess excellent properties such as non-volatility, non-flammability, and thermo-oxidative stability. The potential use of ionic liquids as lubricants was first proposed in 2001 and approximately 70 articles pertaining to fundamental research on ionic liquids have been published through May 2009. A large majority of the cations examined in this area are derived from 1,3-dialkylimidazolium, with a higher alkyl group on the imidazolium cation being beneficial for good lubrication, while it reduces the thermo-oxidative stability. Hydrophobic anions provide both good lubricity and significant thermo-oxidative stability. The anions decompose through a tribochemical reaction to generate metal fluoride on the rubbed surface. Additive technology to improve lubricity is also explained. An introduction to tribology as an interdisciplinary field of lubrication is also provided.

Tribological performance of nanoparticles as lubricating oil additives

NASA Astrophysics Data System (ADS)

Gulzar, M.; Masjuki, H. H.; Kalam, M. A.; Varman, M.; Zulkifli, N. W. M.; Mufti, R. A.; Zahid, Rehan

2016-08-01

The prospect of modern tribology has been expanded with the advent of nanomaterial-based lubrication systems, whose development was facilitated by the nanotechnology in recent years. In literature, a variety of nanoparticles have been used as lubricant additives with potentially interesting friction and wear properties. To date, although there has been a great deal of experimental research on nanoparticles as lubricating oil additives, many aspects of their tribological behavior are yet to be fully understood. With growing number of possibilities, the key question is: what types of nanoparticles act as a better lubricating oil additive and why? To answer this question, this paper reviews main types of nanoparticles that have been used as lubricants additives and outlines the mechanisms by which they are currently believed to function. Significant aspects of their tribological behavior such as dispersion stability and morphology are also highlighted.

The thermal conductance of solid-lubricated bearings at cryogenic temperatures in vacuum

NASA Technical Reports Server (NTRS)

Anderson, M. J.

1996-01-01

The thermal conductance of Hertzian contacts is of great importance to cryogenic spacecraft mechanisms such as the Infra-Red Space Observatory (ISO) and the Far Infra-Red Space Telescope (FIRST). At cryogenic temperatures, cooling of mechanism shafts and associated components occurs via conduction through the bearings. When fluid lubricants are cooled below their pour points, they no longer lubricate effectively, and it is necessary to use low shear strength solid lubricants. Currently, only very limited low temperature data exists on the thermal conductance of Hertzian contacts in both unlubricated and lubricated conditions. This paper reports on measurements of thermal conductance made on stationary ball bearings under cryo-vacuum conditions. Quantitative data is provided to support the development of computer models predicting the thermal conductance of Hertzian contacts and solid lubricants at cryogenic temperatures.

Ball bearing lubrication: The elastohydrodynamics of elliptical contacts

NASA Technical Reports Server (NTRS)

Hamrock, B. J.; Dowson, D.

1981-01-01

The history of ball bearings is examined, taking into account rollers and the wheel in the early civilizations, the development of early forms of rolling-element bearings in the classical civilizations, the Middle Ages, the Industrial Revolution, the emergence of the precision ball bearing, scientific studies of contact mechanics and rolling friction, and the past fifty years. An introduction to ball bearings is presented, and aspects of ball bearing mechanics are explored. Basic characteristics of lubrication are considered along with lubrication equations, the lubrication of rigid ellipsoidal solids, and elastohydrodynamic lubrication theory. Attention is given to the theoretical results for fully flooded elliptical hydrodynamic contacts, the theoretical results for starved elliptical contacts, experimental investigations, the elastohydrodynamics of elliptical contacts for materials of low elastic modulus, the film thickness for different regimes of fluid-film lubrication, and applications.

Polybasic esters: Novel synthetic lubricants designed for use in HFC compressors

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lilje, K.C.; Sabahi, M.; Hamid, S.

1995-12-31

The replacement of ozone-depleting refrigerants with ozone-friendly hydrofluorocarbons (HFCs) requires the use of lubricants that have not historically been used in refrigeration compressors and systems. Polyalkylene glycol (PAG) and polyol ester (POE) lubricants have been extensively evaluated in various refrigeration applications and are being used commercially. Novel synthetic lubricants have been developed based on polybasic esters (PBEs) resulting from malonate-acrylate Michael adducts. These lubricants were designed to address problems encountered in current HFC systems. PBE-based fluids show desired miscibility with R-134a and other HFC blends, excellent hydrolytic stability, no copper plating (even in wet systems), and excellent lubricity. All ofmore » these properties are obtained without the use of performance-enhancing additives. Key physical property data, bench and compressor test results, and compatibility study results will be presented.« less

High temperature lubricating process

DOEpatents

Taylor, R.W.; Shell, T.E.

1979-10-04

It has been difficult to provide adequate lubrication for load bearing, engine components when such engines are operating in excess of about 475/sup 0/C. The present invention is a process for providing a solid lubricant on a load bearing, solid surface, such as in an engine being operated at temperatures in excess of about 475/sup 0/C. The process comprises contacting and maintaining the following steps: a gas phase is provided which includes at least one component reactable in a temperature dependent reaction to form a solid lubricant; the gas phase is contacted with the load bearing surface; the load bearing surface is maintained at a temperature which causes reaction of the gas phase component and the formation of the solid lubricant; and the solid lubricant is formed directly on the load bearing surface. The method is particularly suitable for use with ceramic engines.

High temperature lubricating process

DOEpatents

Taylor, Robert W.; Shell, Thomas E.

1982-01-01

It has been difficult to provide adaquate lubrication for load bearing, engine components when such engines are operating in excess of about 475.degree. C. The present invention is a process for providing a solid lubricant on a load bearing, solid surface (14), such as in an engine (10) being operated at temperatures in excess of about 475.degree. C. The process comprises contacting and maintaining steps. A gas phase (42) is provided which includes at least one component reactable in a temperature dependent reaction to form a solid lubricant. The gas phase is contacted with the load bearing surface. The load bearing surface is maintained at a temperature which causes reaction of the gas phase component and the formation of the solid lubricant. The solid lubricant is formed directly on the load bearing surface. The method is particularly suitable for use with ceramic engines.

ATM CMG bearing failure analysis

NASA Technical Reports Server (NTRS)

1975-01-01

The cause or causes for the failure of ATM CMG S/N 5 (Skylab 1) and the anomalies associated with ATM CMG S/N 6 (Skylab 2) were investigated. Skylab telemetry data were reviewed and presented in the form of parameter distributions. The theory that the problems were caused by marginal bearing lubrication was studied along with the effects of orbital conditions on lubricants. Bearing tests were performed to investigate the effect of lubricant or lack of lubricant in the ATM CMG bearings and the dispersion and migration of the lubricant. The vacuum and weightless conditions of space were simulated in the bearing tests. Analysis of the results of the tests conducted points to inadequate lubrication as the predominant factor causing the failure of ATM CMG S/N 5 (Skylab 1) and the anomalies associated with ATM CMG S/N 6 (Skylab 2).

Poly(ethylene glycol)/chitosan/sodium glycerophosphate gel replaced the joint capsule with slow-release lubricant after joint surgery.

PubMed

Lu, Hailin; Ren, Shanshan; Li, Xing; Guo, Junde; Dong, Guangneng; Li, Jianhui; Gao, Li

2018-08-01

Body fluid is normally the only lubricant after joint replacement surgery, but wear problems have occurred because body fluid has poor lubrication ability. However, traditional lubricant would be diluted by body fluids and then absorbed by the human body. Therefore, an injectable gel with the ability to slow-release lubricant was designed to replace the joint capsule. The proposed gel, poly(ethylene glycol)/chitosan/sodium glycerophosphate (PEG/CS/GP) composite gel was then tested. The tribology results showed that the PEG/CS/GP gel had excellent slow-release properties, especially under pressure, and the PEG played an important role in improving the gel's rheological and mechanical properties. Moreover, this study revealed that the release solution had a good lubrication effect because the PEG and GP could crosslink via the hydrogen bond effect.

AUTOMOTIVE DIESEL MAINTENANCE 1. UNIT XVII, I--MAINTAINING THE LUBRICATION SYSTEM--CUMMINS DIESEL ENGINE, II--UNIT INSTALLATION AND REMOVAL--DRIVE LINES.

ERIC Educational Resources Information Center

Minnesota State Dept. of Education, St. Paul. Div. of Vocational and Technical Education.

THIS MODULE OF A 30-MODULE COURSE IS DESIGNED TO DEVELOP AN UNDERSTANDING OF THE DIESEL ENGINE LUBRICATION SYSTEM AND THE PROCEDURES FOR REMOVAL AND INSTALLATION OF THE DRIVE LINE USED IN DIESEL ENGINE POWER DISTRIBUTION. TOPICS ARE (1) PROLONGING ENGINE LIFE, (2) FUNCTIONS OF THE LUBRICATING SYSTEM, (3) TRACING THE LUBRICANT FLOW, (4) DETERMINING…

Analytical Approach to the Characterization of Military Lubricants

DTIC Science & Technology

1976-03-01

Continue on reverse side It necessary and Identity by block number) As an integral part of the Army’s overall power train lubrication research! effort...favorable results. Technology has progressed to where it is now possible to qualitatively analyze and quantitate the major base stock components in hybrid...lubricant component to equipment performance, and identify sources of new, used, synthetic and re-refined lubricants, power train and hydraulic

Solid lubricants

NASA Technical Reports Server (NTRS)

Sliney, Harold E.

1991-01-01

The state of knowledge of solid lubricants is reviewed. The results of research on solid lubricants from the 1940's to the present are presented from a historical perspective. Emphasis is placed largely, but not exclusively, on work performed at NASA Lewis Research Center with a natural focus on aerospace applications. However, because of the generic nature of the research, the information presented in this review is applicable to most areas where solid lubricant technology is useful.

Evaluation of the lubrication mechanism at various rotation speeds and granule filling levels in a container mixer using a thermal effusivity sensor.

PubMed

Uchiyama, Jumpei; Aoki, Shigeru

2015-01-01

To research the detailed mechanism of the lubrication process using the thermal effusivity sensor, the relationships of the lubrication progress with the pattern of powder flow, the rotation speed and the filling level were investigated. The thermal effusivity profile was studied as a function of the number of rotations at various rotation speeds. It was observed that at lower rotation speeds, the profiles of the lubrication progress were almost the same, regardless of the rotation speed. In this region, the highest speed was defined as the critical rotation speed (CRS), which was found to be one of the important factors. The CRS had close relations with avalanche flow in the blender. The first and the second phases were observed in the lubrication process. The first phase was influenced by the CRS and the filling level in the blender. The second phase was influenced by the rotation speed. The mechanism of two-phase process was proposed as a macro progression of the dispersion of the lubricant (first phase) and micro progression of the coating of the powder particles with lubricant (second phase). The accurate monitoring by the thermal effusivity sensor was able to help a better understanding in the lubrication process.

Characteristics Study of In-Situ Capacitive Sensor for Monitoring Lubrication Oil Debris

PubMed Central

Han, Zhibin; Wang, Yishou; Qing, Xinlin

2017-01-01

As an essential part of engine health monitoring (EHM), online lubrication oil debris monitoring has recently received great attention for the assessment of rotating and reciprocating parts in aero-engines, due to its high integration, low cost and safe characteristics. However, it is be a challenge to find a suitable sensor operating in such a complex environment. We present an unconventional novel approach, in which a cylinder capacitive sensor is designed and integrated with the pipeline of an engine lubrication system, so that the capacitive sensor can effectively detect changes in the lubrication oil condition. In this paper, an attempt to illustrate the performance characteristics of the developed cylinder capacitive sensor is made, through an experiment system that simulates a real scenario of a lubrication oil system. The main aim of the research was to qualitatively describe the relationship between the sensor parameter and the lubrication oil debris. In addition, the effect of the temperature and flow rate of the lubrication oil on capacitance change was performed by several experiments and we figured out a compensation method. The experimental results demonstrated that the cylinder capacitive sensor can potentially be used for lubrication oil debris monitoring of the health condition of an aero-engine. PMID:29292748

Evaluation of ion-sputtered molybdenum disulfide bearings for spacecraft gimbals

NASA Astrophysics Data System (ADS)

Loewenthal, S. H.; Chou, R. G.; Hopple, G. B.; Wenger, W. L.

1994-07-01

High-density, sputtered molybdenum disulfide films (MoS2) were investigated as lubricants for the next generation of spacecraft gimbal bearings where low torque signatures and long life are required. Low friction in a vacuum environment, virturally no out-gassing, insensitivity to low temperature, and radiation resistance of these lubricant films are valued in such applications. One hundred and twenty five thousand hours of acumulated bearing test time were obtained on 24 pairs of flight-quality bearings ion-sputtered with three types of advanced MoS2 films. Life tests were conducted in a vacuum over a simulated duty cycle for a space payload gimbal. Optimum retainer and ball material composition were investigated. Comparisions were made with test bearings lubricated with liquid space lubricants. Self-lubricating PTFE retainers were required for long life, i.e., greater than 40 million gimbal cycles. Bearings with polyimide retainers, silicon nitride ceramic balls, or steel balls sputtered with MoS2 film suffered early torque failure, irrespective of the type of race-sputtered MoS2 film. Failure generally resulted from excess film or retainer debris deposited in the ball track which tended to jam the bearing. Both grease lubricated and the better MoS2 film lubricated bearings produced long lives, although the torque with liquid lubricants was lower and less irregular.

Relative Lifetimes of Several Space Liquid Lubricants Using a Vacuum Spiral Orbit Tribometer (SOT)

NASA Technical Reports Server (NTRS)

Jansen, Mark J.; Jones, William R., Jr.; Predmore, Roamer E.; Loewenthal, Stuart L.

2001-01-01

A vacuum spiral orbit rolling contact tribometer (SOT) was used to determine the relative lifetimes of several unformulated space liquid lubricants. The lubricants tested included a synthetic hydrocarbon (Pennzane 2001 A), three perfluoropolyethers (Krytox 143AC, Fomblin Z25, and Brayco 815Z), three silahydrocarbons (a tri, a tetra, and a penta) and a polyalphaolefin (Nye PAO-100). The SOT simulates the ball motions in an angular contact bearing and tribochemically degrades microgram quantities of lubricant. Test failure is determined when a preset friction coefficient is exceeded. Relative lifetime (orbits/micro-g) is defined as the number of ball orbits to failure divided by the amount of lubricant on the ball. Conditions included 10 to 200 rpm rotational speed, approximately 50 micro-g lubricant, an initial vacuum < 1.3x10(exp -6) Pa, room temperature (approximately 23 C), a mean Hertzian stress of 1.5 GPa, and 440 C stainless steel specimens. Lubricated lifetimes from longest to shortest were Pennzane 2001 A, the silahydrocarbons and the PAO-100, 143AC, ZI-5, and then 815Z. Relative lifetimes compare favorably to full-scale vacuum gimbal bearing tests. The effect of varying the mean Hertzian stress on the lifetime of some of the lubricants was examined.

Lubricant dynamics under sliding condition in disk drives

NASA Astrophysics Data System (ADS)

Wu, Lin

2006-07-01

In this paper, we develop a two-dimensional flow model for the lubricant flow dynamics under a sliding head in disk drives. Our two-dimensional model includes important physics such as viscous force, external air shearing stress, air bearing pressure, centrifugal force, disjoining pressure, and surface tension. Our analysis shows that the lubricant flow dynamics under the sliding condition is a fully two-dimensional phenomenon and the circumferential lubricant flow is strongly coupled to the radial flow. It is necessary to have a two-dimensional flow model that couples the circumferential and radial flows together and includes all important physics to achieve realistic predictions. Our results show that the external air shearing stress has a dominant effect on the lubricant flow dynamics. Both velocity slippage at wall and Poiseuille flow effects have to be considered in the evaluation of the air shearing stress under the head. The nonuniform air bearing pressure has a non-negligible effect on the lubricant film dynamics mostly through the Poiseuille flow effect on the air shearing stress but not from its direct pushing or sucking effect on the lubricant surface. Prediction of the formation of lubricant depletion tracks under a sliding head using the two-dimensional model agrees reasonably well with the existing experimental measurements.

Evaluation of risk and benefit in thermal effusivity sensor for monitoring lubrication process in pharmaceutical product manufacturing.

PubMed

Uchiyama, Jumpei; Kato, Yoshiteru; Uemoto, Yoshifumi

2014-08-01

In the process design of tablet manufacturing, understanding and control of the lubrication process is important from various viewpoints. A detailed analysis of thermal effusivity data in the lubrication process was conducted in this study. In addition, we evaluated the risk and benefit in the lubrication process by a detailed investigation. It was found that monitoring of thermal effusivity detected mainly the physical change of bulk density, which was changed by dispersal of the lubricant and the coating powder particle by the lubricant. The monitoring of thermal effusivity was almost the monitoring of bulk density, thermal effusivity could have a high correlation with tablet hardness. Moreover, as thermal effusivity sensor could detect not only the change of the conventional bulk density but also the fractional change of thermal conductivity and thermal capacity, two-phase progress of lubrication process could be revealed. However, each contribution of density, thermal conductivity, or heat capacity to thermal effusivity has the risk of fluctuation by formulation. After carefully considering the change factor with the risk to be changed by formulation, thermal effusivity sensor can be a useful tool for monitoring as process analytical technology, estimating tablet hardness and investigating the detailed mechanism of the lubrication process.

Lubricant rheology applied to elastohydrodynamic lubrication

NASA Technical Reports Server (NTRS)

Winer, W. O.; Sanborn, D. M.

1977-01-01

Viscosity measurements in a high pressure rheometer, elastohydrodynamic simulator studies (including the development of a temperature measuring technique), and analytical fluid modeling for elastohydrodynamic contacts are described. The more recent research which is described concerns infrared temperature measurements in elastohydrodynamic contacts and the exploration of the glassy state of lubricants. A correlation, of engineering significance, was made between transient surface temperature measurements and surface roughness profiles. Measurements of glass transitions of lubricants and the study of the effect of rate processes on materials lead to the conclusion that typical lubricants go into the glassy state as they pass through the contact region of typical elastohydrodynamic contacts.

Method For Testing Properties Of Corrosive Lubricants

DOEpatents

Ohi, James; De La Cruz, Jose L.; Lacey, Paul I.

2006-01-03

A method of testing corrosive lubricating media using a wear testing apparatus without a mechanical seal. The wear testing apparatus and methods are effective for testing volatile corrosive lubricating media under pressure and at high temperatures.

The effect of a chlorhexidine-based surgical lubricant during pelvic examination on the detection of group B Streptococcus.

PubMed

Schwope, Ora I; Chen, Katherine T; Mehta, Isha; Re, Margaret; Rand, Larry

2010-03-01

The objective of the study was to estimate whether surgical lubricant used during pelvic examination alters the detection of group B Streptococcus (GBS). We conducted a prospective cohort study of patients undergoing GBS screening at the prenatal clinics of a New York City public hospital. Two specimens were collected from each patient, before and after a pelvic examination with Surgilube (Fougera and Co, Melville, NY), a bacteriostatic surgical lubricant. Test performance indices using GBS status pre-pelvic examination as the reference were calculated. Over 10 months, 168 patients were enrolled in the study. Twenty of 168 patients (11.9%; 95% confidence interval, 7.4-17.8%) tested GBS positive before the pelvic examination. Of the initial 20 GBS-positive patients, 10 tested GBS positive after the pelvic examination with surgical lubricant. The sensitivity of detecting GBS after the examination with surgical lubricant was 50%. Because pelvic examination with surgical lubricant may decrease the detection of GBS, obstetric practitioners should collect GBS screening cultures before the use of surgical lubricant. Copyright 2010 Mosby, Inc. All rights reserved.

Thermo-Rheometric Studies of New Class Ionic Liquid Lubricants

NASA Astrophysics Data System (ADS)

Bakhtiyarov, Sayavur; Street, Kenneth; Scheiman, Daniel; van Dyke, Alan

2010-11-01

Due to their specific properties, such as small volatility, nonflammability, extreme thermal stability, low melting point, wide liquid range, and good miscibility with organic materials, ionic liquids attracted particular interest in various industrial processes. Recently, the unique properties of ionic liquids caught the attention of space tribologists. The traditional lubricating materials used in space have limited lifetimes in vacuum due to the catalytic degradation on metal surfaces, high vaporization at high temperatures, dewetting, and other disadvantages. The lubricants for the space applications must have vacuum stability, high viscosity index, low creep tendency, good elastohydrodynamic and boundary lubrication properties, radiation atomic oxygen resistance, optical or infrared transparency. Unfortunately, the properties such as heat flow, heat capacity, thermogravimetric weight loss, and non-linearity in the rheological behavior of the lubricants are not studied well for newly developed systems. These properties are crucial to analyzing thermodynamic and energy dissipative aspects of the lubrication process. In this paper we will present the rheological and heat and mass transfer measurements for the ionic liquid lubricants, their mixtures with and without additive.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Howell, Caitlin; Vu, Thy L.; Lin, Jennifer J.

Inspired by the long-term effectiveness of living antifouling materials, we have developed a method for the selfreplenishment of synthetic biofouling-release surfaces. These surfaces are created by either molding or directly embedding 3D vascular systems into polydimethylsiloxane (PDMS) and filling them with a silicone oil to generate a nontoxic oil-infused material. When replenished with silicone oil from an outside source, these materials are capable of self-lubrication and continuous renewal of the interfacial fouling-release layer. Under accelerated lubricant loss conditions, fully infused vascularized samples retained significantly more lubricant than equivalent nonvascularized controls. Tests of lubricant-infused PDMS in static cultures of the infectiousmore » bacteria Staphylococcus aureus and Escherichia coli as well as the green microalgae Botryococcus braunii, Chlamydomonas reinhardtii, Dunaliella salina, and Nannochloropsis oculata showed a significant reduction in biofilm adhesion compared to PDMS and glass controls containing no lubricant. Further experiments on vascularized versus nonvascularized samples that had been subjected to accelerated lubricant evaporation conditions for up to 48 h showed significantly less biofilm adherence on the vascularized surfaces. These results demonstrate the ability of an embedded lubricant-filled vascular network to improve the longevity of fouling-release surfaces.« less

Sputtered silver films to improve chromium carbide based solid lubricant coatings for use to 900 C

NASA Technical Reports Server (NTRS)

Dellacorte, Christopher; Sliney, Harold E.; Deadmore, Daniel L.

1988-01-01

Thin silver films, 250 to 3500 A thick, were sputtered onto PS200, a plasma sprayed, chromium carbide based solid lubricant coating, to reduce run-in wear and improve tribological properties. The coating contains bonded chromium carbide as the wear resistant base stock with silver and barium fluoride/calcium fluoride eutectic added as low and high temperature lubricants, respectively. Potential applications for the PS200 coating are cylinder wall/piston ring lubrication for Stirling engines and foil bearing journal lubrication. In this preliminary program, the silver film overlay thickness was optimized based on tests using a pin-on-disk tribometer. The friction and wear studies were performed in a helium atmosphere at temperatures from 25 to 760 C with a sliding velocity of 2.7 m/s under a 4.9 N load. Films between 1000 and 1500 A provide the best lubrication of the counterface material. The films enrich the sliding surface with lubricant and reduce the initial abrasiveness of the as ground, plasma-sprayed coating surface, thus reducing wear.

Sputtered silver films to improve chromium carbide based solid lubricant coatings for use to 900 C

NASA Technical Reports Server (NTRS)

Dellacorte, Christopher; Sliney, Harold E.; Deadmore, Daniel L.

1988-01-01

Thin silver films, 250 to 3500 A thick, were sputtered onto PS200, a plasma sprayed, chromium carbide based solid lubricant coating, to reduce run-in wear and improve tribological properties. The coating contains bonded chromium carbide as the wear resistant base stock with silver and barium fluoride/calcium fluoride eutectic added as low and high temperature lubricants respectively. Potential applications for the PS200 coating are cylinder wall/piston ring lubrication for Stirling engines and foil bearing journal lubrication. In this preliminary program, the silver film overlay thickness was optimized based on tests using a pin-on-disk tribometer. The friction and wear studies were performed in a helium atmosphere at temperatures from 25 to 760 C with a sliding velocity of 2.7 m/s under a 4.9 N load. Films between 1000 and 1500 A provide the best lubrication of the counterface material. The films enrich the sliding surface with lubricant and reduce the initial abrasiveness of the as ground, plasma-sprayed coating surface, thus reducing wear.

Double hollow MoS2 nano-spheres: Synthesis, tribological properties, and functional conversion from lubrication to photocatalysis

NASA Astrophysics Data System (ADS)

Liu, Yueru; Hu, Kunhong; Hu, Enzhu; Guo, Jianhua; Han, Chengliang; Hu, Xianguo

2017-01-01

Molybdenum disulfide (MoS2) has extensive applications in industries as solid lubricants and catalysts. To improve the lubricating performance of MoS2, novel double-hollow-sphere MoS2 (DHSM) nanoparticles with an average diameter of approximately 90 nm were synthesized on sericite mica (SM). When the DHSM/SM composite was used as an additive in polyalphaolefin oil, friction and wear decreased by 22.4% and 63.5% respectively. The low friction and wear were attributed to the easy exfoliation of DHSM. The DHSM/SM composite was then rubbed under 40 MPa for 1 h to investigate the exfoliation and functional conversion behaviors of DHSM. Results showed that DHSM (lubricating structure) on SM could be completely exfoliated into nanosheets (catalytic structure) by rubbing. The nanosheets exfoliated from DHSM presented good photocatalytic activity for the removal of organic compounds from waste water. This work provided both a novel solid lubricant for industrial applications and a possible approach to designing a novel green lubricant for use as a photocatalyst in organic-waste treatment after lubricating service life.

Simulation of lubricating behavior of a thioether liquid lubricant by an electrochemical method

NASA Technical Reports Server (NTRS)

Morales, W.

1984-01-01

An electrochemical cell was constructed to explore the possible radical anion forming behavior of a thioether liquid lubricant. The electrochemical behavior of the thioether was compared with the electrochemical behavior of biphenyl, which is known to form radical anions. Under controlled conditions biphenyl undergoes a reversible reaction to a radical anion, whereas the thioether undergoes an irreversible reduction yielding several products. These results are discussed in relation to boundary lubrication.

Development of a Lubricant Therapy to Prevent Development of Osteoarthritis after Acute Injury of Synovial Joints

DTIC Science & Technology

2015-10-01

AD______________ AWARD NUMBER: W81XWH-14-1-0562 TITLE: Development of a Lubricant Therapy to Prevent Development of Osteoarthritis after Acute...TITLE AND SUBTITLE 5a. CONTRACT NUMBER Development of a Lubricant Therapy to Prevent Development of Osteoarthritis after Acute Injury of Synovial...early-onset osteoarthritis after traumatic joint injury remains a clinical challenge and may be associated with the poor lubricant quality of the

Grease Composition.

DTIC Science & Technology

1975-11-11

acids such as myristic or oleic 12 acid . The maximum amount of these impurities is 3 weight percent. 13 Surface active agents are objectionable in ...lubricants require the lubricant to 21 operate in an environment having high pressure and high shear 22 conditions, a temperature variation from below... in naval rapid firing guns. It is required that lubricants for 4 these guns be effective from -54°C to +150°C. 5 Exi3ting lubricants have had

Repair, Evaluation, Maintenance, and Rehabilitation Research Program. Lubricants for Hydraulic Structures

DTIC Science & Technology

1989-08-01

machinery design , precision machining, proper maintenance, and proper lubrication. Ordinarily, wear is thought of only in terms of abrasive wear occurring in...operate under this principle. However, the design must allow the plates to lift and tilt properly and provide sufficient area to lift the load. 38. Another...friction and wear to a minimum. Boundary Lubrication 42. Lubrication designed to protect against frictional effects when asperities meet is called

Measurements of elastohydrodynamic film thickness, wear and tempering behavior of high pressure oxygen turbopump bearings

NASA Technical Reports Server (NTRS)

Dufrane, K. F.; Merriman, T. L.; Kannel, J. W.; Stockwell, R. D.; Hauser, D.; Vanecho, J. A.

1984-01-01

The reusable design of the Space Shuttle requires a target life of 7.5 hours for the turbopumps of the Space Shuttle main engine (SSME). This large increase from the few hundred seconds required in single-use rockets has caused various problems with the bearings of the turbopumps. The berings of the high pressure oxygen turbopump (HPOTP) were of particular concern because of wear, spalling, and cage failures at service time well below the required 7.5 hours. Lubrication and wear data were developed for the bearings. Since the HPOTP bearings operate in liquid oxygen, conventional liquid lubricants cannot be applied. Therefore, solid lubricant coatings and lubricant transfer from the polytetrafluorethylene (FTFE) cage were the primary lubrication approaches for the bearings. Measurements were made using liquid nitrogen in a rolling disk machine to determine whether usable elastohydrodynamic films could be generated to assist in the bearing lubrication.

Friction losses in a lubricated thrust-loaded cageless angular-contract bearing

NASA Technical Reports Server (NTRS)

Townsend, D. P.; Allen, C. W.; Zaretsky, E. V.

1973-01-01

The NASA spinning torque apparatus was modified to measure the spinning torque on a cageless ball thrust bearing. Friction torque was measured for thrust loads varying from 44.5 to 403 newtons (10 to 90 lb) at speeds of 1000, 2000, and 3000 rpm. Tests were conducted with di-2-ethylhexyl sebacate and a synthetic paraffinic oil. These tests were run with either oil jet lubrication or with a thin surface film of lubricant only. An analytical model which included rolling resistance was developed and extended from previous models for spinning torque and lubricant rheology. The model was extended by the inclusion of rolling resistance. The computed values were in fair agreement with the experimental results and confirmed previous hypotheses that a thin lubricant film gives minimum bearing torque and an oil jet flow of a viscous lubricant will result in considerable rolling torque in addition to the torque due to ball spin.

The relationship between fuel lubricity and diesel injection system wear

NASA Astrophysics Data System (ADS)

Lacy, Paul I.

1992-01-01

Use of low-lubricity fuel may have contributed to increased failure rates associated with critical fuel injection equipment during the 1991 Operation Desert Storm. However, accurate quantitative analysis of failed components from the field is almost impossible due to the unique service history of each pump. This report details the results of pump stand tests with fuels of equal viscosity, but widely different lubricity. Baseline tests were also performed using reference no. 2 diesel fuel. Use of poor lubricity fuel under these controlled conditions was found to greatly reduce both pump durability and engine performance. However, both improved metallurgy and fuel lubricity additives significantly reduced wear. Good correlation was obtained between standard bench tests and lightly loaded pump components. However, high contact loads on isolated components produced a more severe wear mechanism that is not well reflected by the Ball-on-Cylinder Lubricity Evaluator.

Triple-layer configuration for stable high-speed lubricated pipeline transport

NASA Astrophysics Data System (ADS)

Sarmadi, Parisa; Hormozi, Sarah; Frigaard, Ian A.

2017-04-01

Lubricated transport of heavy viscous oils is a popular technology in the pipelining industry, where pumping pressures can be reduced significantly by concentrating the strain rate in a lubricating layer. However, the interface between the lubricating layer and heavy oil is vulnerable to any perturbations in the system as well as transients due to start up, shut down, temperature change, etc. We present a method in which we purposefully position an unyielded skin of a viscoplastic fluid between the oil and the lubricating fluid. The objective is to reduce the frictional pressure gradient while avoiding interfacial instability. We study this methodology in both concentric and eccentric configurations and show its feasibility for a wide range of geometric and flow parameters found in oil pipelining. The eccentric configuration benefits the transport process via generating lift forces to balance the density differences among the layers. We use classical lubrication theory to estimate the leading order pressure distribution in the lubricating layer and calculate the net force on the skin. We explore the effects of skin shape, viscosity ratio, and geometry on the pressure drop, the flow rates of skin and lubricant fluids, and the net force on the skin. We show that the viscosity ratio and the radius of the core fluid are the main parameters that control the pressure drop and consumptions of outer fluids, respectively. The shape of the skin and the eccentricity mainly affect the lubrication pressure. These predictions are essential in designing a stable transport process. Finally, we estimate the yield stress required in order that the skin remain unyielded and ensure interfacial stability.

Thermal and frictional performance evaluation of nano lubricant with multi wall carbon nano tubes (MWCNTs) as nano-additive

NASA Astrophysics Data System (ADS)

Lijesh K., P.; Kumar, Deepak; Muzakkir S., M.; Hirani, Harish

2018-05-01

A Fluid Film Bearings (FFBs) operating in hydrodynamic boundary regime can provide moderate load carrying capacity, negligible wear and friction. However in extreme operating conditions i.e. at high load and low speed, asperities of journal and bearing surfaces come in contact with each other resulting in high wear and friction. During the contact of the asperities, the temperature of the lubricant increases due to frictional heating, resulting in reduction of the viscosity of lubricant. Variation of lubricant viscosity results in low load carrying capacity of the FFB and therefore resulting in detoriation of FFB performance. In the present work it is hypothesized that, by adding multi-functional Multi Wall Carbon Nano-Tubes (MWCNT) (having high thermal conductivity and anti-friction properties) as nano-additive in the base mineral oil, the aforementioned problems can be overcome. To validate the proposed hypothesis, five different samples of lubricant is considered: Sample 1: Base oil, Sample 2: Base oil +0.05% MWCNT, Sample 3: Base oil +0.05% MWCNT +0.5%surfactant, Sample 4: Base oil +0.1% MWCNT +0.5% surfactant, and Sample 5: Base oil +0.15% MWCNT +0.5%surfactant. To evaluate the performance of the developed lubricants, experiments were performed on the reduced scale conformal block on disc test setup. The experimental condition and dimension of the block and disc were decide for the Sommerfeld number equal to 0.0025, which indicates mixed lubrication regime. The performance of lubricant is evaluated by measuring the frictional force and temperature rise of the lubricant during the experiment.

Biobased, environmentally friendly lubricants for processing plants

USDA-ARS?s Scientific Manuscript database

Vegetable oil based lubricants have excellent lubricity, biodegradability, good viscosity temperature characteristics and low evaporation loss, but poor thermos-oxidative stability and cold flow properties. This paper presents a systematic approach to improve the oxidative and cold flow behavior of...

The Synergistic Effects of MoS2 and Liquid Lubrication

NASA Astrophysics Data System (ADS)

Buttery, M.; Roberts, E.; Stanley, S.; Murer, J.

2015-09-01

We present an overview of a three-stage program on the potential for hybrid lubrication of MoS2 and PFPE fluids (Fomblin Z25 & Braycote 601EF) performed at the European Space Tribology Laboratory (ESTL).Tests were performed using a spiral orbit tribometer (SOT) and a pin-on-disc tribometer (POD), demonstrating encouraging results. Hybrid lubrication allows for extended periods of in-air running of MoS2 with no detrimental effect to the subsequent in-vacuum lifetime. In addition, hybrid lubrication was shown to be synergistic, with the lifetime of the hybrid fluid/MoS2 lubrication extended in comparison to the individual constituents, with no detriment to the friction.

Pressure Distribution in a Porous Squeeze Film Bearing Lubricated with a Herschel-Bulkley Fluid

NASA Astrophysics Data System (ADS)

Walicka, A.; Jurczak, P.

2016-12-01

The influence of a wall porosity on the pressure distribution in a curvilinear squeeze film bearing lubricated with a lubricant being a viscoplastic fluid of a Herschel-Bulkley type is considered. After general considerations on the flow of the viscoplastic fluid (lubricant) in a bearing clearance and in a porous layer the modified Reynolds equation for the curvilinear squeeze film bearing with a Herschel-Bulkley lubricant is given. The solution of this equation is obtained by a method of successive approximation. As a result one obtains a formula expressing the pressure distribution. The example of squeeze films in a step bearing (modeled by two parallel disks) is discussed in detail.

The role of the micro environment on the tribological behavior of materials

NASA Technical Reports Server (NTRS)

Buckley, D. H.

1980-01-01

The paper reviews studies of the role of the microenvironment in the adhesion, friction, and wear behavior of materials in solid-state contact. The microenvironment is defined as the environment on the surface of solids in solid-state contact. Properties of the environment are discussed which exert an influence on the adhesion, friction, wear, and lubrication of materials in contact. The effect of the environment on lubricants and their properties is considered with respect to the interaction of lubricants with material surfaces in contact; the effect on the ability of lubricants to provide protective surface films is also considered. It is concluded that naturally occurring oxides are probably the best available natural solid-film lubricants.

Liquid lubrication in space

NASA Technical Reports Server (NTRS)

Zaretsky, Erwin V.

1990-01-01

The requirement for long-term, reliable operation of aerospace mechanisms has, with a few exceptions, pushed the state of the art in tribology. Space mission life requirements in the early 1960s were generally 6 months to a year. The proposed U.S. space station schedule to be launched in the 1990s must be continuously usable for 10 to 20 years. Liquid lubrication systems are generally used for mission life requirements longer than a year. Although most spacecraft or satellites have reached their required lifetimes without a lubrication-related failure, the application of liquid lubricants in the space environment presents unique challenges. The state of the art of liquid lubrication in space as well as the problems and their solutions are reviewed.

Determination of physical and chemical states of lubricants in concentrated contacts, part 2

NASA Technical Reports Server (NTRS)

Lauer, J. L.

1981-01-01

Infrared emission spectroscopy through a window in an operating bearing continued to provide most of the information gathered on the state of lubricants subjected to elastohydrodynamic (EHD) conditions. Other measurements were traction, scanning electron microscopy and elemental surface analysis X-rays. A very significant finding was the decomposition of a naphthenic oil lubricant in the presence of small concentrations of an organic chloride. Olefins and aromatics were formed in ever increasing amounts prior to total lubricant failure. An aromatic fluid also failed in the presence of chloride. A correlation was found between changes of the alignment of lubricant molecules evidence by infrared polarization and changes of traction under varying EHD stresses.

Antibacterial properties of root canal lubricants: a comparison with commonly used irrigants.

PubMed

Wong, Samantha; Mundy, Lance; Chandler, Nicholas; Upritchard, Jenine; Purton, David; Tompkins, Geoffrey

2014-12-01

The aim was to assess in vitro the antibacterial activity of 10 root canal lubricants. K-Y Jelly personal lubricant, RC-Prep, File-Eze, File-Rite, EndoPrep Gel, Endosure Prep Crème 15%, Prep-Rite, Glyde, SlickGel ES and Alpha Glide were selected and compared in their antimicrobial properties to seven irrigants. Serial dilutions of each agent in tryptic soy broth were inoculated with either Enterococcus faecalis or Pseudomonas aeruginosa and incubated at 37C for 24 h. During incubation bacterial growth was measured by optical density (A(600)), and samples removed for cultivation on tryptic soy broth agar. Against both test bacteria after 1 h incubation, six lubricants recorded minimum bactericidal concentrations ranging from 1/10 to 1/80, whereas the inhibitory activity of the irrigants ranged from 1/20 to 1/640. Under these conditions, several lubricants exhibited antimicrobial activity comparable with some irrigants. Three irrigants, Consepsis (containing chlorhexidine), Endosure EDTA/C (containing cetrimide) and EndoPrep Solution (containing cetrimide), showed superior antibacterial action to lubricants against both species. The irrigants containing ethylenediamine tetraacetic acid and cetrimide were the most effective against both bacterial species at all time intervals. Antimicrobial activity of the lubricants did not correlate to pH values, which ranged from 2.9 to 10.3. Root canal lubricants have antibacterial properties that may help to disinfect canals. © 2014 Australian Society of Endodontology.

One of possible variants of the organization for recycling lubricate cooling of technological means for small businesses

NASA Astrophysics Data System (ADS)

Rusica, I.; Toca, A.; Stingaci, I.; Scaticailov, S.; Scaticailov, I.; Marinescu, O.; Kosenko, P.

2016-11-01

In the paper we analyze the application lubricate cooling technological environment in the processing of various materials in the past century greatly have increased cutting speed and respectively, has increased productivity [1]. Today, none of production in which anyway is used metal cutting machines of all types (milling, turning, grinding, drilling, etc.) is not without lubricant cooling technological liquid which in turn are designed to reduce cutting force and the load on metal cutting machine tools and machined parts in order to increase durability machine tools and reduce errors of processing details and also in resource energy saving. When using lubricate cooling technological environment reduces the temperature in the cutting zone resulting in higher tool life and the preservation of the surface structure being treated reducing wear of metal parts of the machine. Typically, lubricant cooling process fluids is used without replacing as long as possible not yet beginning to negatively affect the quality of process. However life expectancy lubricate cooling technological environment is limited. According to existing normative acts every kind of lubricate cooling technological environment through certain time must be deleted by from the system and subjected to a recycling. Lubricate cooling technological environment must be disposed of for the following reasons: occurs the microbial and the mechanical pollution cutting fluid, free oil impairs operational characteristics cutting fluid and increases consumption.

An evaluation of dry film lubricants and substrate materials for use on SSME gimbal bearings

NASA Technical Reports Server (NTRS)

Harp, J. A.

1976-01-01

Failure of the spherical bearing shaft of the Space Shuttle Main Engine (SSME) gimbal bearing assembly was encountered during Design Verification Specification testing of the full scale engine. Investigation revealed that the failure was caused by a deficiency in the lubrication system. Based upon the materials and gimbal operating conditions, a lubricant of MoS2 and graphite with a ceramic binder was the best lubricant candidate for this particular application; however, the decision to implement the change was not made without verification testing. Scaled down simulation testing was performed. Four different substrate materials and eight different dry film lubricants were subjected to tests under simulated SSME environmental and stress load conditions. The test specimens were evaluated for friction and operating life. Each test specimen was subjected to cyclic operation under load until failure. The force required to move the bearing surfaces relative to each other was monitored throughout the test, thus providing analytical data for derivation of the coefficient of friction. Results indicate that the MoS2/graphite lubricant with ceramic binder proved to be superior from the standpoint of endurance and also from the standpoint of friction reducing capabilities when applied to the titanium substrate material used on SSME. Endurance of this lubricant was approximately 16 times that of the lubricant which was being used when the SSME gimbal failed.

Influence of lubrication forces in direct numerical simulations of particle-laden flows

NASA Astrophysics Data System (ADS)

Maitri, Rohit; Peters, Frank; Padding, Johan; Kuipers, Hans

2016-11-01

Accurate numerical representation of particle-laden flows is important for fundamental understanding and optimizing the complex processes such as proppant transport in fracking. Liquid-solid flows are fundamentally different from gas-solid flows because of lower density ratios (solid to fluid) and non-negligible lubrication forces. In this interface resolved model, fluid-solid coupling is achieved by incorporating the no-slip boundary condition implicitly at particle's surfaces by means of an efficient second order ghost-cell immersed boundary method. A fixed Eulerian grid is used for solving the Navier-Stokes equations and the particle-particle interactions are implemented using the soft sphere collision and sub-grid scale lubrication model. Due to the range of influence of lubrication force on a smaller scale than the grid size, it is important to implement the lubrication model accurately. In this work, different implementations of the lubrication model on particle dynamics are studied for various flow conditions. The effect of a particle surface roughness on lubrication force and the particle transport is also investigated. This study is aimed at developing a validated methodology to incorporate lubrication models in direct numerical simulation of particle laden flows. This research is supported from Grant 13CSER014 of the Foundation for Fundamental Research on Matter (FOM), which is part of the Netherlands Organisation for Scientific Research (NWO).

14 CFR 33.39 - Lubrication system.

Code of Federal Regulations, 2011 CFR

2011-01-01

... 14 Aeronautics and Space 1 2011-01-01 2011-01-01 false Lubrication system. 33.39 Section 33.39 Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION AIRCRAFT AIRWORTHINESS STANDARDS: AIRCRAFT ENGINES Design and Construction; Reciprocating Aircraft Engines § 33.39 Lubrication...

14 CFR 33.39 - Lubrication system.

Code of Federal Regulations, 2010 CFR

2010-01-01

... 14 Aeronautics and Space 1 2010-01-01 2010-01-01 false Lubrication system. 33.39 Section 33.39 Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION AIRCRAFT AIRWORTHINESS STANDARDS: AIRCRAFT ENGINES Design and Construction; Reciprocating Aircraft Engines § 33.39 Lubrication...

Pressure-viscosity coefficient of biobased lubricants

USDA-ARS?s Scientific Manuscript database

Film thickness is an important tribological property that is dependent on the combined effect of lubricant properties, material property of friction surfaces, and the operating conditions of the tribological process. Pressure-viscosity coefficient (PVC) is one of the lubricant properties that influe...

The effect of instrument lubricant on the diametral tensile strength and water uptake of posterior composite restorative material.

PubMed

Patel, J; Granger, C; Parker, S; Patel, M

2017-01-01

This in-vitro study investigated the effect of 'instrument lubricants' used during placement of composite restorative material, on the diametral tensile strength (DTS) and water uptake of composite specimens. 300 posterior composite cylindrical specimens were manufactured: 60 with each instrument lubricant (ethanol, 3-step, 2-step and 1-step 'bonding agent') and 60 with no lubricant (controls). Each set of 60 specimens was evenly allocated to one of the following test groups (n=100/group): Group 1 - tested for DTS immediately after manufacture; Groups 2 and 3 - tested for DTS after immersion in phosphate-buffered saline (PBS) for 1 and 12-weeks respectively, using a Universal Instron machine. Water uptake was assessed gravimetrically. Data were statistically analysed with two-way ANOVA and Tukey's post hoc test (α=0.05). The mean DTS and percentage weight change of composite specimens ranged between 32.49-53.14MPa and 0.51-1.36% and varied with lubricant used and time incubated in PBS. All control groups exhibited significantly higher DTS (MPa) (groups 1-3: 53.17±1.78; 50.64±1.85; 45.17±1.77) and lower percentage weight change (groups 2-3: 0.51±0.03; 0.61±0.01) than specimens placed with an instrument lubricant, with significant differences between certain lubricant groups. Data from the present study suggest that the use of instrument lubricant may adversely effect the DTS and water uptake of composite restorative material. The use of instrument lubricants to aid composite placement is widespread however based on the data obtained it is suggested that discontinuing or limiting the use of instrument lubricants, and if necessary using the 'bonding agent' from a 3-step adhesive system is recommended as results suggest this has the least deleterious effect upon material properties.​. Copyright © 2016 Elsevier Ltd. All rights reserved.

Wear of human enamel: a quantitative in vitro assessment.

PubMed

Kaidonis, J A; Richards, L C; Townsend, G C; Tansley, G D

1998-12-01

Many factors influence the extent and rate at which enamel wears. Clinical studies in humans are limited by difficulties in the accurate quantification of intra-oral wear and by a lack of control over the oral environment. The purpose of this study was to determine the wear characteristics of human dental enamel under controlled experimental conditions. An electro-mechanical tooth wear machine, in which opposing enamel surfaces of sectioned, extracted teeth were worn under various conditions, was used to simulate tooth grinding or bruxism. Enamel surface wear was quantified by weight to an accuracy of 0.1 mg, with water uptake and loss controlled. The variables considered included the structure and hardness of enamel, facet area, duration of tooth contact, relative speed of opposing surfaces, temperature, load, pH, and the nature of the lubricant. Enamel wear under non-lubricated conditions increased with increasing load over the range of 1.7 to 16.2 kg. The addition of a liquid lubricant (pH = 7) reduced enamel wear up to 6.7 kg, but when the load increased above this threshold, the rate of wear increased dramatically. With the viscosity of the lubricant constant and pH = 3, the rate of wear was further reduced to less than 10% of the non-lubricated rate at 9.95 kg, after which the rate again increased substantially. Under more extreme conditions (pH = 1.2, simulating gastric acids), the wear was excessive under all experimental loads. When saliva was used as a lubricant, the amount of wear was relatively low at 9.95 kg, but rapid wear occurred at 14.2 kg and above. These results indicate that under non-lubricated conditions, enamel wear remains low at high loads due to the dry-lubricating capabilities of fine enamel powder. Under lubricated conditions, low loads with an acidic lubricant lead to little enamel wear, whereas very low pH results in a high rate of wear under all loads.

A Review to the Laser Cladding of Self-Lubricating Composite Coatings

NASA Astrophysics Data System (ADS)

Quazi, M. M.; Fazal, M. A.; Haseeb, A. S. M. A.; Yusof, Farazila; Masjuki, H. H.; Arslan, A.

2016-06-01

Liquid lubricants are extremely viable in reducing wear damage and friction of mating components. However, due to the relentless pressure and the recent trend towards higher operating environments in advanced automotive and aerospace turbo-machineries, these lubricants cease to perform and hence, an alternate system is required for maintaining the self-lubricating environment. From the viewpoint of tribologist, wear is related to near-surface regions and hence, surface coatings are considered suitable for improving the functioning of tribo-pairs. Wear resistant coatings can be fabricated with the addition of various solid lubricants so as to reduce friction drag. In order to protect bulk substrates, self-lubricating wear resistant composite coatings have been fabricated by employing various surface coating techniques such as electrochemical process, physical and chemical vapor depositions, thermal and plasma spraying, laser cladding etc. Studies related to laser-based surface engineering approaches have remained vibrant and are recognized in altering the near surface regions. In this work, the latest developments in laser based self-lubricating composite coatings are highlighted. Furthermore, the effect of additives, laser processing parameters and their corresponding influence on mechanical and tribological performance is briefly reviewed.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Howell, C; Vu, TL; Lin, JJ

Inspired by the long-term effectiveness of living antifouling materials, we have developed a method for the self-replenishment of synthetic biofouling-release surfaces. These surfaces are created by either molding or directly embedding 3D vascular systems into polydimethylsiloxane (PDMS) and filling them with a silicone oil to generate a nontoxic oil-infused material. When replenished with silicone oil from an outside source, these materials are capable of self-lubrication and continuous renewal of the interfacial fouling-release layer. Under accelerated lubricant loss conditions, fully infused vascularized samples retained significantly more lubricant than equivalent nonvascularized controls. Tests of lubricant-infused PDMS in static cultures of the infectiousmore » bacteria Staphylococcus aureus and Escherichia coli as well as the green microalgae Botryococcus braunii, Chlamydomonas reinhardtii, Dunaliella sauna, and Nannochloropsis oculata showed a significant reduction in biofilm adhesion compared to PDMS and glass controls containing no lubricant. Further experiments on vascularized versus nonvascularized samples that had been subjected to accelerated lubricant evaporation conditions for up to 48 h showed significantly less biofilm adherence on the vascularized surfaces. These results demonstrate the ability of an embedded lubricant-filled vascular network to improve the longevity of fouling-release surfaces.« less

Role of lubricants on friction between self-ligating brackets and archwires.

PubMed

Leal, Renata C; Amaral, Flávia L B; França, Fabiana M G; Basting, Roberta T; Turssi, Cecilia P

2014-11-01

To evaluate the effect of different lubricants on friction between orthodontic brackets and archwires. Active (Quick, Forestadent) and passive (Damon 3MX, Ormco) self-ligating brackets underwent friction tests in the presence of mucin- and carboxymethylcellulose (CMC)-based artificial saliva, distilled water, and whole human saliva (positive control). Dry friction (no lubricant) was used as the negative control. Bracket/wire samples (0.014 × 0.025 inch, CuNiTi, SDS Ormco) underwent friction tests eight times in a universal testing machine. Two-way analysis of variance showed no significant interaction between bracket type and lubricant (P  =  .324). Friction force obtained with passive self-ligating brackets was lower than that for active brackets (P < .001). Friction observed in the presence of artificial saliva did not differ from that generated under lubrication with natural human saliva, as shown by Tukey test. Higher friction forces were found with the use of distilled water or when the test was performed under dry condition (ie, with no lubricant). Lubrication plays a role in friction forces between self-ligating brackets and CuNiTi wires, with mucin- and CMC-based artificial saliva providing a reliable alternative to human natural saliva.

Tribological Behavior of Aqueous Copolymer Lubricant in Mixed Lubrication Regime.

PubMed

Ta, Thi D; Tieu, A Kiet; Zhu, Hongtao; Zhu, Qiang; Kosasih, Prabouno B; Zhang, Jie; Deng, Guanyu

2016-03-02

Although a number of experiments have been attempted to investigate the lubrication of aqueous copolymer lubricant, which is applied widely in metalworking operations, a comprehensive theoretical investigation at atomistic level is still lacking. This study addresses the influence of loading pressure and copolymer concentration on the structural properties and tribological performance of aqueous copolymer solution of poly(propylene oxide)-poly(ethylene oxide)-poly(propylene oxide) (PPO-PEO-PPO) at mixed lubrication using a molecular dynamic (MD) simulation. An effective interfacial potential, which has been derived from density functional theory (DFT) calculations, was employed for the interactions between the fluid's molecules and iron surface. The simulation results have indicated that the triblock copolymer is physisorption on iron surface. Under confinement by iron surfaces, the copolymer molecules form lamellar structure in aqueous solution and behave differently from its bulk state. The lubrication performance of aqueous copolymer lubricant increases with concentration, but the friction reduction is insignificant at high loading pressure. Additionally, the plastic deformation of asperity is dependent on both copolymer concentration and loading pressure, and the wear behavior shows a linear dependence of friction force on the number of transferred atoms between contacting asperities.

Electrokinetic remediation of contaminated soil with waste-lubricant oils and zinc.

PubMed

Park, Sung-Woo; Lee, Jae-Young; Yang, Jung-Seok; Kim, Kyoung-Jo; Baek, Kitae

2009-09-30

The feasibility of electrokinetic technology on the remediation of mixed-waste-contaminated railroad soil, contaminated by lubricant oil and zinc, was investigated. To enhance the removal efficiency, catholyte purging with 0.1M HNO(3) and a supply of non-ionic surfactant, secondary alcohol ethoxylate, was applied to the anode to remove Zn and to solubilize the lubricant oil. The catholyte purging maintained the soil pH as acidic and enhanced desorption of zinc from the soil, where the zeta potential of the acidic soil became positive. Thereafter, the direction of electro-osmotic flow was changed from the cathode to anode and the flow rate was reduced. The lesser in magnitude reverse electro-osmotic flow inhibited the migration of zinc and the lubricant oil was removed by the electro-osmotic flow. The removal of zinc and lubricant oil was enhanced with an increase in voltage gradient; however, a higher voltage gradient resulted in higher energy expenditure. After electrokinetic operation over 17 days, the removal efficiency of zinc was 22.1-24.3%, and that of lubricant oil was 45.1-55.0%. Although the removal of lubricant oil was quite high, the residual concentration did not meet Korean regulation levels.

Analysis of chain saw lubricating oils commonly used in Thailand's southern border provinces for forensic science purpose.

PubMed

Choodum, Aree; Tripuwanard, Kijja; Daeid, Niamh Nic

2014-08-01

In recent years, Thailand's southern border provinces (Malay-Muslim-majority border provinces) have become the scene of violence and insurgency. One of the attack patterns is the blocking of roads with perennial plants followed by planned attacks using improvised explosive devices (IEDs) or weapons on first responders. Containers of viscous dark lubricating oil and traces of lubricants on the felled trees were usually found at the scene. These were suspected to be chain oil lubricant from the chainsaws used to cut down the trees used for the roadblock. This work aimed to differentiate the chromatographic patterns of used lubricating oils available in automobile repair shops from various locations across Thailand's southern border provinces. Lubricating oils were analyzed using gas chromatography/flame ionization detector (GC/FID) every two weeks to study their variation in chemical compositions over time. The results obtained from GC/FID were normalized for differentiation. This included four two-stroke, six four-stroke, and three recycled oils. Two lubricating oils found at an incident scene were also analyzed and the results compared with the chain oil from five seized chainsaws. Copyright © 2014 Elsevier Ireland Ltd. All rights reserved.

Self-Replenishing Vascularized Fouling-Release Surfaces

DOE PAGES

Howell, Caitlin; Vu, Thy L.; Lin, Jennifer J.; ...

2014-08-13

Inspired by the long-term effectiveness of living antifouling materials, we have developed a method for the selfreplenishment of synthetic biofouling-release surfaces. These surfaces are created by either molding or directly embedding 3D vascular systems into polydimethylsiloxane (PDMS) and filling them with a silicone oil to generate a nontoxic oil-infused material. When replenished with silicone oil from an outside source, these materials are capable of self-lubrication and continuous renewal of the interfacial fouling-release layer. Under accelerated lubricant loss conditions, fully infused vascularized samples retained significantly more lubricant than equivalent nonvascularized controls. Tests of lubricant-infused PDMS in static cultures of the infectiousmore » bacteria Staphylococcus aureus and Escherichia coli as well as the green microalgae Botryococcus braunii, Chlamydomonas reinhardtii, Dunaliella salina, and Nannochloropsis oculata showed a significant reduction in biofilm adhesion compared to PDMS and glass controls containing no lubricant. Further experiments on vascularized versus nonvascularized samples that had been subjected to accelerated lubricant evaporation conditions for up to 48 h showed significantly less biofilm adherence on the vascularized surfaces. These results demonstrate the ability of an embedded lubricant-filled vascular network to improve the longevity of fouling-release surfaces.« less

A newly developed lubricant, chitosan laurate, in the manufacture of acetaminophen tablets.

PubMed

Bani-Jaber, Ahmad; Kobayashi, Asuka; Yamada, Kyohei; Haj-Ali, Dana; Uchimoto, Takeaki; Iwao, Yasunori; Noguchi, Shuji; Itai, Shigeru

2015-04-10

To study the usefulness of chitosan laurate (CS-LA), a newly developed chitosan salt, as a lubricant, lubrication properties such as the pressure transmission ratio and ejection force were determined at different concentrations of CS-LA in tableting. In addition, tablet properties such as the tensile strength, disintegration time, and dissolution behavior, were also determined. When CS-LA was mixed at concentrations of 0.1%-3.0%, the pressure transmission ratio was increased in a concentration-dependent manner, and the value at a CS-LA concentration of 3% was equal to that of magnesium stearate (Mg-St), a widely used lubricant. Additionally, a reduction in the ejection force was observed at a concentration from 1%, proving that CS-LA has good lubrication performance. A prolonged disintegration time and decreased tensile strength, which are known disadvantages of Mg-St, were not observed with CS-LA. Furthermore, with CS-LA, retardation of dissolution of the drug from the tablets was not observed. Conjugation of CS with LA was found to be quite important for both lubricant and tablet properties. In conclusion, CS-LA should be useful as an alternative lubricant to Mg-St. Copyright © 2015 Elsevier B.V. All rights reserved.

40 CFR 1065.740 - Lubricants.

Code of Federal Regulations, 2011 CFR

2011-07-01

... 40 Protection of Environment 33 2011-07-01 2011-07-01 false Lubricants. 1065.740 Section 1065.740 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR POLLUTION CONTROLS ENGINE-TESTING PROCEDURES Engine Fluids, Test Fuels, Analytical Gases and Other Calibration Standards § 1065.740 Lubricants...

40 CFR 1065.740 - Lubricants.

Code of Federal Regulations, 2010 CFR

2010-07-01

... 40 Protection of Environment 32 2010-07-01 2010-07-01 false Lubricants. 1065.740 Section 1065.740 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR POLLUTION CONTROLS ENGINE-TESTING PROCEDURES Engine Fluids, Test Fuels, Analytical Gases and Other Calibration Standards § 1065.740 Lubricants...

40 CFR 1065.740 - Lubricants.

Code of Federal Regulations, 2012 CFR

2012-07-01

... 40 Protection of Environment 34 2012-07-01 2012-07-01 false Lubricants. 1065.740 Section 1065.740 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR POLLUTION CONTROLS ENGINE-TESTING PROCEDURES Engine Fluids, Test Fuels, Analytical Gases and Other Calibration Standards § 1065.740 Lubricants...

40 CFR 1065.740 - Lubricants.

Code of Federal Regulations, 2013 CFR

2013-07-01

... 40 Protection of Environment 34 2013-07-01 2013-07-01 false Lubricants. 1065.740 Section 1065.740 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR POLLUTION CONTROLS ENGINE-TESTING PROCEDURES Engine Fluids, Test Fuels, Analytical Gases and Other Calibration Standards § 1065.740 Lubricants...

40 CFR 1065.740 - Lubricants.

Code of Federal Regulations, 2014 CFR

2014-07-01

... 40 Protection of Environment 33 2014-07-01 2014-07-01 false Lubricants. 1065.740 Section 1065.740 Protection of Environment ENVIRONMENTAL PROTECTION AGENCY (CONTINUED) AIR POLLUTION CONTROLS ENGINE-TESTING PROCEDURES Engine Fluids, Test Fuels, Analytical Gases and Other Calibration Standards § 1065.740 Lubricants...

14 CFR 33.71 - Lubrication system.

Code of Federal Regulations, 2013 CFR

2013-01-01

... 14 Aeronautics and Space 1 2013-01-01 2013-01-01 false Lubrication system. 33.71 Section 33.71 Aeronautics and Space FEDERAL AVIATION ADMINISTRATION, DEPARTMENT OF TRANSPORTATION AIRCRAFT AIRWORTHINESS STANDARDS: AIRCRAFT ENGINES Design and Construction; Turbine Aircraft Engines § 33.71 Lubrication system. (a...

Advances in biobased lubricant additive development

USDA-ARS?s Scientific Manuscript database

Lubricant formulations comprise two categories of ingredients: base oils and additives. Depending on its application, a formulation may contain one or more from each category. Additives are the most expensive ingredients of lubricant formulations and, for some applications, can comprise 25 to 40% w/...

The use of perfluoroether lubricants in unprotected space environments

NASA Technical Reports Server (NTRS)

Baxter, B. H.; Hall, B. P.

1985-01-01

A series of ball bearing tests in simulated space environment are described which determine durability of perfluoroether lubricants. The results of the examination of the test bearings for each stage are described and experimental techniques designed to overcome lubricant degradation are outlined.

7 CFR 2902.41 - Metalworking fluids.

Code of Federal Regulations, 2011 CFR

2011-01-01

..., lubrication, corrosion prevention, and reduced wear on the contact parts of machinery used for metalworking... for use in a re-circulating fluid system to provide cooling, lubrication, and corrosion prevention... fluid system to provide cooling, lubrication, and corrosion prevention when applied to metal feedstock...

7 CFR 2902.41 - Metalworking fluids.

Code of Federal Regulations, 2010 CFR

2010-01-01

..., lubrication, corrosion prevention, and reduced wear on the contact parts of machinery used for metalworking... for use in a re-circulating fluid system to provide cooling, lubrication, and corrosion prevention... fluid system to provide cooling, lubrication, and corrosion prevention when applied to metal feedstock...

Synthesis of chloro alkoxy and alkoxy derivatives of methyl oleate

USDA-ARS?s Scientific Manuscript database

Vegetable oil based lubricants typically have improved lubricity and biodegradability over their mineral oil based counterparts. However, vegetable oil lubricants often fail to meet the performance standards of mineral based oils with respect to cold temperature and resistance to oxidation. Olefins ...

Analysis of Lubricant Films in Bearings Under Incipient Failure Conditions.

DTIC Science & Technology

1981-01-01

AFOSUR. 8 2 -34 0 1 ACEjSN NO. lEN’ CATALOG NUMBERFO"R8 0-0010 4 4. TITLE (and Subtitio) S. TYPE OFf REPORT a PERIOD COVERED "Analysis of Lubricant...spectroscopy of the lubricant in operating heavily loaded bearings under so-called elasto- hydrodynamic lubricating conditions. In this type of...Chopper and Blackbody Reference Both interferometers are equipped with choppers of the tuning fork type shown in Fig. 6. The tines are located in front of

On-line surveillance of lubricants in bearings by means of surface acoustic waves.

PubMed

Lindner, Gerhard; Schmitt, Martin; Schubert, Josephine; Krempel, Sandro; Faustmann, Hendrik

2010-01-01

The acoustic wave propagation in bearings filled with lubricants and driven by pulsed excitation of surface acoustic waves has been investigated with respect to the presence and the distribution of different lubricants. Experimental setups, which are based on the mode conversion between surface acoustic waves and compression waves at the interface between a solid substrate of the bearing and a lubricant are described. The results of preliminary measurements at linear friction bearings, rotation ball bearings and axial cylinder roller bearings are presented.

Environmental Assessment for the Army Aviation Support Facility and Administrative Support Facility and the Joint Forces Headquarters, Readiness Center, and Field Maintenance Shop at Francis E. Warren Air Force Base, Cheyenne, Wyoming

DTIC Science & Technology

2006-08-01

helicopter aircraft (zinc chromate), and oil and lubricants. Oil and lubricant waste will be recycled. However. hazardous wastes are not expected to...byproducts used in painting touch-up parts on helicopter aircraft (zinc Final EA v chromate), and oil and lubricants. Oil and lubricant waste would be...79 4-8. Electrical, Heat, and Gas ................................................................................................... 81 4

Use of high pressure liquid chromatography in the study of liquid lubricant oxidation

NASA Technical Reports Server (NTRS)

Morales, W.

1982-01-01

The general principles of classical liquid chromatography and high-pressure liquid chromatography (HPLC) are reviewed, and their advantages and disadvantages are compared. Several chromatographic techniques are reviewed, and the analysis of a C-ether liquid lubricant by each technique is illustrated. An analysis by size exclusion chromatography of an ester lubricant, which had been degraded using a micro-oxidation apparatus, is illustrated to show how HPLC can be used in the study of high-temperature lubricant degradation.

Optimizing power cylinder lubrication on a large bore natural gas engine

NASA Astrophysics Data System (ADS)

Luedeman, Matthew R.

More than 6000 integral compressors, located along America's natural gas pipelines, pump natural gas across the United States. These compressors are powered by 2-stroke, large bore natural gas burning engines. Lowering the operating costs, reducing the emissions, and ensuring that these engines remain compliant with future emission regulations are the drivers for this study. Substantial research has focused on optimizing efficiency and reducing the fuel derived emissions on this class of engine. However, significantly less research has focused on the effect and reduction of lubricating oil derived emissions. This study evaluates the impact of power cylinder lubricating oil on overall engine emissions with an emphasis on reducing oxidation catalyst poisoning. A traditional power cylinder lubricator was analyzed; power cylinder lubricating oil was found to significantly impact exhaust emissions. Lubricating oil was identified as the primary contributor of particulate matter production in a large bore natural gas engine. The particulate matter was determined to be primarily organic carbon, and most likely direct oil carryover of small oil droplets. The particulate matter production equated to 25% of the injected oil at a nominal power cylinder lubrication rate. In addition, power cylinder friction is considered the primary contributor to friction loss in the internal combustion engine. This study investigates the potential for optimizing power cylinder lubrication by controlling power cylinder injection to occur at the optimal time in the piston cycle. By injecting oil directly into the ring pack, it is believed that emissions, catalyst poisoning, friction, and wear can all be reduced. This report outlines the design and theory of two electronically controlled lubrication systems. Experimental results and evaluation of one of the systems is included.

The effects of water lubrication of tracheal tubes on post-intubation airway complications: study protocol for a randomized controlled trial.

PubMed

Kim, Eugene; Yang, Seong Mi; Yoon, So Jeong; Bahk, Jae-Hyon; Seo, Jeong-Hwa

2016-11-25

Water is known to have lubricating properties, thus it is used for lubrication of tracheal tubes to reduce airway injuries caused by intubation. However, there is no definite evidence to substantiate the beneficial effects of lubricating tracheal tubes using water for attenuating airway injuries. Moreover, the lubrication pretreatment may cause contamination of the tube, leading to respiratory infections. Therefore, this trial aims to assess whether no pretreatment of tracheal tubes does not increase post-intubation airway complications as compared with water lubrication of tubes. This is a prospective, double-blind, single-center, parallel-arm, noninferiority, randomized controlled trial to be conducted in participants aged 20-80 years who are undergoing elective surgery under general anesthesia with orotracheal intubation. Participants are randomly assigned into one of two groups depending on whether intubation is performed using a tracheal tube lubricated with water (n = 150) or without any pretreatment (n = 150). The primary outcome is the incidence of sore throat at 0, 2, 4, and 24 h after surgery, which is analyzed with a noninferiority test. The secondary outcomes are the incidence and severity of postoperative hoarseness, oropharyngeal injuries, and respiratory infections. Because we hypothesized that lubricating tracheal tubes using water has no advantage in reducing airway injuries associated with intubation, we will compare the incidence of sore throat, which is the most common complaint after intubation, in a noninferiority manner. This is the first randomized controlled trial to investigate the possibly beneficial or harmful effects of lubricating tracheal tubes using water before intubation. We expect that this trial will provide useful evidence to formulate a protocol for preparing tracheal tubes before intubation. This trial is registered at ClinicalTrials.gov on 1 July 2015 ( NCT02492646 ).

The quantitative surface analysis of an antioxidant additive in a lubricant oil matrix by desorption electrospray ionization mass spectrometry

PubMed Central

Da Costa, Caitlyn; Reynolds, James C; Whitmarsh, Samuel; Lynch, Tom; Creaser, Colin S

2013-01-01

RATIONALE Chemical additives are incorporated into commercial lubricant oils to modify the physical and chemical properties of the lubricant. The quantitative analysis of additives in oil-based lubricants deposited on a surface without extraction of the sample from the surface presents a challenge. The potential of desorption electrospray ionization mass spectrometry (DESI-MS) for the quantitative surface analysis of an oil additive in a complex oil lubricant matrix without sample extraction has been evaluated. METHODS The quantitative surface analysis of the antioxidant additive octyl (4-hydroxy-3,5-di-tert-butylphenyl)propionate in an oil lubricant matrix was carried out by DESI-MS in the presence of 2-(pentyloxy)ethyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate as an internal standard. A quadrupole/time-of-flight mass spectrometer fitted with an in-house modified ion source enabling non-proximal DESI-MS was used for the analyses. RESULTS An eight-point calibration curve ranging from 1 to 80 µg/spot of octyl (4-hydroxy-3,5-di-tert-butylphenyl)propionate in an oil lubricant matrix and in the presence of the internal standard was used to determine the quantitative response of the DESI-MS method. The sensitivity and repeatability of the technique were assessed by conducting replicate analyses at each concentration. The limit of detection was determined to be 11 ng/mm2 additive on spot with relative standard deviations in the range 3–14%. CONCLUSIONS The application of DESI-MS to the direct, quantitative surface analysis of a commercial lubricant additive in a native oil lubricant matrix is demonstrated. © 2013 The Authors. Rapid Communications in Mass Spectrometry published by John Wiley & Sons, Ltd. PMID:24097398

New Lubricants Protect Machines and the Environment

NASA Technical Reports Server (NTRS)

2007-01-01

In 1994, NASA and Lockheed Martin Space Operations commissioned Sun Coast Chemicals of Daytona Inc to develop a new type of lubricant that would be safe for the environment and help "grease the wheels" of the shuttle-bearing launcher platform. Founded in 1989, Sun Coast Chemicals is known amongst the racing circuit for effective lubricants that help overcome engine and transmission problems related to heat and wear damage. In a matter of weeks, Sun Coast Chemical produced the biodegradable, high-performance X-1R Crawler Track Lube. In 1996, Sun Coast Chemical determined there was a market for this new development, and introduced three derivative products, Train Track Lubricant, Penetrating Spray Lubricant, and Biodegradable Hydraulic Fluid, and then quickly followed with a gun lubricant/cleaner and a fishing rod and reel lubricant. Just recently, Sun Coast introduced the X-1R Corporation, which folds the high-performance, environmentally safe benefits into a full line of standard automotive and specially formulated racing products. The entire X-1R automotive product line has stood up to rigorous testing by groups such as the American Society of Mechanical Engineers, the Swedish National Testing and Research Institute, the Department of Mechanical Engineering at Oakland University (Rochester, Michigan), and Morgan-McClure Motorsports (Abingdon, Virginia). The X-1R Corporation also markets "handy packs" for simple jobs around the house, consisting of a multi-purpose, multi-use lubricant and grease. In 2003, The X-1R Corporation teamed up with Philadelphia-based Penn Tackle Manufacturing Co., a leading manufacturer of fishing tackle since 1932, to jointly develop and market a line of advanced lubrication products for saltwater and freshwater anglers

In Situ, On-Demand Lubrication System Developed for Space Mechanisms

NASA Technical Reports Server (NTRS)

Marchetti, Mario; Pepper, Stephen V.; Jansen, Mark J.; Predmore, Roamer E.

2003-01-01

Many moving mechanical assemblies (MMA) for space mechanisms rely on liquid lubricants to provide reliable, long-term performance. The proper performance of the MMA is critical in assuring a successful mission. Historically, mission lifetimes were short and MMA duty cycles were minimal. As mission lifetimes were extended, other components, such as batteries and computers, failed before lubricated systems. However, improvements in these ancillary systems over the last decade have left the tribological systems of the MMAs as the limiting factor in determining spacecraft reliability. Typically, MMAs are initially lubricated with a very small charge that is supposed to last the entire mission lifetime, often well in excess of 5 years. In many cases, the premature failure of a lubricated component can result in mission failure.

Effect of lubricant environment on saw damage in silicon wafers

NASA Technical Reports Server (NTRS)

Kuan, T. S.; Shih, K. K.; Vanvechten, J. A.; Westdorp, W. A.

1982-01-01

The chemomechanical effect of lubricant environments on the inner diameter (ID) sawing induced surface damage in Si wafers was tested for four different lubricants: water, dielectric oil, and two commercial cutting solutions. The effects of applying different potential on Si crystals during the sawing were also tested. It is indicated that the number and depth of surface damage are sensitive to the chemical nature of the saw lubricant. It is determined that the lubricants that are good catalysts for breaking Si bonds can dampen the out of plane blade vibration more effectively and produce less surface damage. Correlations between the applied potential and the depth of damage in the dielectric oil and one of the commercial cutting solutions and possible mechanisms involved are discussed.

Lubricant-impregnated surfaces for electrochemical applications, and devices and systems using same

DOE Office of Scientific and Technical Information (OSTI.GOV)

Solomon, Brian Richmond; Chen, Xinwei; Chiang, Yet-Ming

In certain embodiments, the invention relates to an electrochemical device having a liquid lubricant impregnated surface. At least a portion of the interior surface of the electrochemical device includes a portion that includes a plurality of solid features disposed therein. The plurality of solid features define a plurality of regions therebetween. A lubricant is disposed in the plurality of regions which retain the liquid lubricant in the plurality of regions during operation of the device. An electroactive phase comes in contact with at least the portion of the interior surface. The liquid lubricant impregnated surface introduces a slip at themore » surface when the electroactive phase flows along the surface. The electroactive phase may be a yield stress fluid.« less

Determination of properties of PVE lubricants with HFC refrigerants[PolyVinylEther

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kaneko, Masato; Sakanoue, Shuichi; Tazaki, Toshihiro

1999-07-01

Polyalkyleneglycol (PAG) and polyol ester (POE) have been developed as refrigeration lubricants, used with HFC134a. PAG is used for automotive air conditioning systems and POE is used for domestic reciprocating refrigerators and for A/C systems. Although PAG exhibits good lubricity performance, it is difficult to use for domestic reciprocating refrigerators due to its low dielectric property. POE is difficult to use for automotive A/C systems, due to hydrolysis and poor lubricity performance. Polyvinylether (PVE) can be used in place of PAG and POE with HFC refrigerants. PVE is used for A/C systems as well as refrigerator and freezer applications. PVEmore » is an ideal lubricant for use with HFCs.« less

Overview of liquid lubricants for advanced aircraft

NASA Technical Reports Server (NTRS)

Loomis, W. R.

1982-01-01

An overall status report on liquid lubricants for use in high-performance turbojet engines is presented. Emphasis is placed on the oxidation and thermal stability requirements imposed upon the lubrication system. A brief history is iven of the development of turbine engine lubricants which led to synthetic oils with their inherent modification advantages. The status and state of development of some nine candidate classes of fluids for use in advanced turbine engines are discussed. Published examples of fundamental studies to obtain a better understanding of the chemistry involved in fluid degradation are reviewed. Also, alternatives to high temperature fluid development are described. The importance of of continuing work on improving high temperature lubricant candidates and encouraging development of fluid base stocks is discussed.

MISCIBILITY, SOLUBILITY, VISCOSITY, AND DENSITY MEASUREMENTS FOR R-236FA WITH POTENTIAL LUBRICANTS

EPA Science Inventory

The report gives results of miscibility, solubility, viscosity, and density measurements for refrigerant R-236fa and two potential lubricants . (The data are needed to determine the suitability of refrigerant/lubricant combinations for use in refrigeration systems.) The tested oi...

14 CFR 27.1027 - Transmissions and gearboxes: General.

Code of Federal Regulations, 2013 CFR

2013-01-01

... 14 Aeronautics and Space 1 2013-01-01 2013-01-01 false Transmissions and gearboxes: General. 27... Transmissions and gearboxes: General. (a) The lubrication system for components of the rotor drive system that...) to ensure lubrication during autorotation. (b) Pressure lubrication systems for transmissions and...

14 CFR 27.1027 - Transmissions and gearboxes: General.

Code of Federal Regulations, 2012 CFR

2012-01-01

... 14 Aeronautics and Space 1 2012-01-01 2012-01-01 false Transmissions and gearboxes: General. 27... Transmissions and gearboxes: General. (a) The lubrication system for components of the rotor drive system that...) to ensure lubrication during autorotation. (b) Pressure lubrication systems for transmissions and...

14 CFR 27.1027 - Transmissions and gearboxes: General.

Code of Federal Regulations, 2011 CFR

2011-01-01

... 14 Aeronautics and Space 1 2011-01-01 2011-01-01 false Transmissions and gearboxes: General. 27... Transmissions and gearboxes: General. (a) The lubrication system for components of the rotor drive system that...) to ensure lubrication during autorotation. (b) Pressure lubrication systems for transmissions and...

14 CFR 27.1027 - Transmissions and gearboxes: General.

Code of Federal Regulations, 2014 CFR

2014-01-01

... 14 Aeronautics and Space 1 2014-01-01 2014-01-01 false Transmissions and gearboxes: General. 27... Transmissions and gearboxes: General. (a) The lubrication system for components of the rotor drive system that...) to ensure lubrication during autorotation. (b) Pressure lubrication systems for transmissions and...

Lubrication studies of some type III deep eutectic solvents (DESs)

NASA Astrophysics Data System (ADS)

Ahmed, Essa. I.; Abbott, Andrew. P.; Ryder, Karl S.

2017-09-01

It has previously been shown that eutectic mixtures of quaternary ammonium salts and hydrogen bond donors form liquids with properties similar to ionic liquids [1; 2]. These so-called deep eutectic solvents (DESs) have been shown to have physical properties which would make them useful as base lubricants. The base lubricant needs to show specific properties, including high viscosity index (VI), low friction coefficient (μ), low pour point and corrosivity. To determine the applicability of DESs as base lubricants, physical properties, corrosion and lubrication properties for four type III DESs have been studied and the results have been compared with mineral base oil. The data show that the lubrication properties of DESs are superior to mineral base oil for short distances. All DESs assessed here have higher VI (191, 147, 121 for Ethaline, Glyceline and Reline respectively compared with 100 for mineral base oil), lower pour points than mineral base oil and most of the liquids studied have shown very low corrosion rates (< 3 µm year-1 for mild steel).

Lubricant Effects on Efficiency of a Helicopter Transmission

NASA Technical Reports Server (NTRS)

Mitchell, A. M.; Coy, J. J.

1982-01-01

Eleven different lubricants were used in efficiency tests conducted on the OH-58A helicopter main transmission using the NASA Lewis Research Center's 500 hp torque regenerative helicopter transmission test stand. Tests were run at oil-in temperatures of 355 K and 372 K. The efficiency was calculated from a heat balance on the water running through an oil to water heat exchanger which the transmission was heavily insulated. Results show an efficiency range from 98.3% to 98.8% which is a 50% variation relative to the losses associated with the maximum efficiency measured. For a given lubricant, the efficiency increased as temperature increased and viscosity decreased. There were two exceptions which could not be explained. Between lubricants, efficiency was not correlated with viscosity. There were relatively large variations in efficiency with the different lubricants whose viscosity generally fell in the 5 to 7 centistoke range. The lubricants had no significant effect on the vibration signature of the transmission.

Bio-lubricants derived from waste cooking oil with improved oxidation stability and low-temperature properties.

PubMed

Li, Weimin; Wang, Xiaobo

2015-01-01

Waste cooking oil (WCO) was chemically modified via epoxidation using H2O2 followed by transesterification with methanol and branched alcohols (isooctanol, isotridecanol and isooctadecanol) to produce bio-lubricants with improved oxidative stability and low temperature properties. Physicochemical properties of synthesized bio-lubricants such as pour point (PP), cloud point (CP), viscosity, viscosity index (VI), oxidative stability, and corrosion resistant property were determined according to standard methods. The synthesized bio-lubricants showed improved low temperature flow performances compared with WCO, which can be attributing to the introduction of branched chains in their molecular structures. What's more, the oxidation stability of the WCO showed more than 10 folds improvement due to the elimination of -C=C-bonds in the WCO molecule. Tribological performances of these bio-lubricants were also investigated using four-ball friction and wear tester. Experimental results showed that derivatives of WCO exhibited favorable physicochemical properties and tribological performances which making them good candidates in formulating eco-friendly lubricants.

Ionic Liquids as Novel Lubricants and /or Lubricant Additives

DOE Office of Scientific and Technical Information (OSTI.GOV)

Qu, J.; Viola, M. B.

2013-10-31

This ORNL-GM CRADA developed ionic liquids (ILs) as novel lubricants or oil additives for engine lubrication. A new group of oil-miscible ILs have been designed and synthesized with high thermal stability, non-corrosiveness, excellent wettability, and most importantly effective anti-scuffing/anti-wear and friction reduction characteristics. Mechanistic analysis attributes the superior lubricating performance of IL additives to their physical and chemical interactions with metallic surfaces. Working with a leading lubricant formulation company, the team has successfully developed a prototype low-viscosity engine oil using a phosphonium-phosphate IL as an anti-wear additive. Tribological bench tests of the IL-additized formulated oil showed 20-33% lower friction inmore » mixed and elastohydrodynamic lubrication and 38-92% lower wear in boundary lubrication when compared with commercial Mobil 1 and Mobil Clean 5W-30 engine oils. High-temperature, high load (HTHL) full-size engine tests confirmed the excellent anti-wear performance for the IL-additized engine oil. Sequence VID engine dynamometer tests demonstrated an improved fuel economy by >2% for this IL-additized engine oil benchmarked against the Mobil 1 5W-30 oil. In addition, accelerated catalyst aging tests suggest that the IL additive may potentially have less adverse impact on three-way catalysts compared to the conventional ZDDP. Follow-on research is needed for further development and optimization of IL chemistry and oil formulation to fully meet ILSAC GF-5 specifications and further enhance the automotive engine efficiency and durability.« less

"Insensitive" to touch: fabric-supported lubricant-swollen polymeric films for omniphobic personal protective gear.

PubMed

Damle, Viraj G; Tummala, Abhishiktha; Chandrashekar, Sriram; Kido, Cassidee; Roopesh, Ajay; Sun, Xiaoda; Doudrick, Kyle; Chinn, Jeff; Lee, James R; Burgin, Timothy P; Rykaczewski, Konrad

2015-02-25

The use of personal protective gear made from omniphobic materials that easily shed drops of all sizes could provide enhanced protection from direct exposure to most liquid-phase biological and chemical hazards and facilitate the postexposure decontamination of the gear. In recent literature, lubricated nanostructured fabrics are seen as attractive candidates for personal protective gear due to their omniphobic and self-healing characteristics. However, the ability of these lubricated fabrics to shed low surface tension liquids after physical contact with other objects in the surrounding, which is critical in demanding healthcare and military field operations, has not been investigated. In this work, we investigate the depletion of oil from lubricated fabrics in contact with highly absorbing porous media and the resulting changes in the wetting characteristics of the fabrics by representative low and high surface tension liquids. In particular, we quantify the loss of the lubricant and the dynamic contact angles of water and ethanol on lubricated fabrics upon repeated pressurized contact with highly absorbent cellulose-fiber wipes at different time intervals. We demonstrate that, in contrast to hydrophobic nanoparticle coated microfibers, fabrics encapsulated within a polymer that swells with the lubricant retain the majority of the oil and are capable of repelling high as well as low surface tension liquids even upon multiple contacts with the highly absorbing wipes. The fabric supported lubricant-swollen polymeric films introduced here, therefore, could provide durable and easy to decontaminate protection against hazardous biological and chemical liquids.

Mechanism of lubrication by tricresylphosphate (TCP)

NASA Technical Reports Server (NTRS)

Faut, O. D.; Wheeler, D. R.

1983-01-01

A pin-on-disk tribometer equipped with an induction heater was used to study the coefficient of friction as a function of temperature for tricresylphosphate (TCP) on continuous vacuum melted (CVM) M-50 tool steel when the TCP was present in a liquid reservoir (bulk lubrication), and when it was applied as a liquid layer directly to the disk (limited lubrication). Under limited lubrication conditions, experiments were performed in dry ( 100 ppm H2O) air, dry ( 20 ppm H2O) nitrogen, dry nitrogen with the disks heated to 700 C then cooled to room temperature before the TCP was applied and the measurements made (preheated disks), and moist nitrogen using preheated disks. When the coefficient of friction was plotted as a function of the disk temperature, the friction decreased at a characteristic temperature, T sub r whose observed values were 265 C for bulk lubrication conditions in dry air, 225 C for limited lubrication conditions in dry air, and 215 C for limited lubrication conditions in dry nitrogen. No decrease in friction was observed with preheated disks; instead a sharp failure temperature was observed at 218 C, which was taken as the temperature about which the behavior of TCP should be judged, X-ray photoelectron spectroscopy confirmed the presence of phosphate on the surface of the iron pins used in the tribometer under TCP lubrication. Depth profile studies support the idea that a chemical reaction occurs between the TCP and the metal surface at T sub r.

Origins of extreme boundary lubrication by phosphatidylcholine liposomes.

PubMed

Sorkin, Raya; Kampf, Nir; Dror, Yael; Shimoni, Eyal; Klein, Jacob

2013-07-01

Phosphatidylcholine (PC) vesicles have been shown to have remarkable boundary lubricating properties under physiologically-high pressures. Here we carry out a systematic study, using a surface force balance, of the normal and shear (frictional) forces between two opposing surfaces bearing different PC vesicles across water, to elucidate the origin of these properties. Small unilamellar vesicles (SUVs, diameters < 100 nm) of the symmetric saturated diacyl PCs DMPC (C(14)), DPPC (C(16)) and DSPC (C(18)) attached to mica surfaces were studied in their solid-ordered (SO) phase on the surface. Overall liposome lubrication ability improves markedly with increasing acyl chain length, and correlates strongly with the liposomes' structural integrity on the substrate surface: DSPC-SUVs were stable on the surface, and provided extremely efficient lubrication (friction coefficient μ ≈ 10(-4)) at room temperature at pressures up to at least 18 MPa. DMPC-SUVs ruptured following adsorption, providing poor high-pressure lubrication, while DPPC-SUVs behavior was intermediate between the two. These results can be well understood in terms of the hydration-lubrication paradigm, but suggest that an earlier conjecture, that highly-efficient lubrication by PC-SUVs depended simply on their being in the SO rather than in the liquid-disordered phase, should be more nuanced. Our results indicate that the resistance of the SUVs to mechanical deformation and rupture is the dominant factor in determining their overall boundary lubrication efficiency in our system. Copyright © 2013 Elsevier Ltd. All rights reserved.

Lubrication background

NASA Technical Reports Server (NTRS)

Hamrock, B. J.; Dowson, D.

1981-01-01

Surface topography, including the various physical methods of measuring surfaces, and the various lubrication regimes (hydrodynamic, elastohydrodynamic, boundary, and mixed) are discussed. The historical development of elastohydrodynamic lubrication is outlined. The major accomplishments in four periods, the pre-1950's, the 1950's, the 1960's, and the 1970's are presented.

Lubricity of biobased diesel fuels and additives

USDA-ARS?s Scientific Manuscript database

Modern diesel engines rely on the fuel itself to lubricate moving parts in the fuel and engine systems. Prior to the late 1990s, diesel fuel from petroleum provided sufficient lubricity to effectively reduce wear in injectors and fuel pumps. Increasingly stringent limitations on the sulfur content o...

Lubricating Holes for Corroded Nuts and Bolts

NASA Technical Reports Server (NTRS)

Penn, B. G.; Clemons, J. M.; Ledbetter, Frank E., III

1986-01-01

Corroded fasteners taken apart more easily. Lubricating holes bored to thread from three of flats. Holes facilitate application of penetrating oil to help loosen nut when rusted onto bolt. Holes make it possible to apply lubricants and rust removers directly to more of thread than otherwise reachable.

21 CFR 178.3570 - Lubricants with incidental food contact.

Code of Federal Regulations, 2014 CFR

2014-04-01

... 21 Food and Drugs 3 2014-04-01 2014-04-01 false Lubricants with incidental food contact. 178.3570... approval. (3) Substances identified in this paragraph (a)(3). Substances Limitations Aluminum stearoyl... the lubricant. BHA BHT α-Butyl-omega-hydroxypoly(oxyethylene) poly(oxypropylene) produced by random...

MISCIBILITY, SOLUBILITY, VISCOSITY, AND DENSITY MEASUREMENTS FOR R-236EA WITH FOUR DIFFERENT EXXON LUBRICANTS

EPA Science Inventory

The report discusses miscibility, solubility, viscosity, and density data for the refrigerant hydrofluorocarbon (HFC)-236ea (or R-236ea) and four lubricants supplied by Exxon Corporation. Such data are needed to determine the suitability of refrigerant/lubricant combinations for ...

Rotating plug bearing and seal

DOEpatents

Wade, Elman E.

1977-01-01

A bearing and seal structure for nuclear reactors utilizing rotating plugs above the nuclear reactor vessel. The structure permits lubrication of bearings and seals of the rotating plugs without risk of the lubricant draining into the reactor vessel below. The structure permits lubrication by utilizing a rotating outer race bearing.

Contribution of Lubricating Oil to Particulate Matter Emissions from Light-Duty Gasoline Vehicles in Kansas City

EPA Science Inventory

The contribution of lubricating oil to particulate matter (PM) emissions representative of the in-use 2004 light-duty gasoline vehicles fleet is estimated from the Kansas City Light-Duty Vehicle Emissions Study (KCVES). PM emissions are apportioned to lubricating oil and gasoline...

Air-Lubricated Lead Screw

NASA Technical Reports Server (NTRS)

Perkins, G. S.

1983-01-01

Air lubricated lead screw and nut carefully machined to have closely matched closely fitting threads. Compressed air injected into two plenums encircle nut and flow through orifices to lubricate mating threads. Originally developed to position precisely interferometer retroreflector for airborne measurement of solar infrared radiation, device now has positioning accuracy of 0.25 micron.

Tribological performance of ultra-low viscosity composite base fluid with bio-derived fluid

USDA-ARS?s Scientific Manuscript database

One obvious approach to increase efficiencies in many lubricated systems such as ICE and gearbox is the reduction in viscosity of oil lubricant. Indeed, ultra-low viscosity engine oils are now commercially available. One approach to the development of ultra-low viscosity lubricants without compromis...

21 CFR 178.3570 - Lubricants with incidental food contact.

Code of Federal Regulations, 2011 CFR

2011-04-01

... 21 Food and Drugs 3 2011-04-01 2011-04-01 false Lubricants with incidental food contact. 178.3570... provisions of a prior sanction or approval. (3) Substances identified in this paragraph (a)(3). Substances....1 percent by weight of the lubricant. BHA BHT α-Butyl-omega-hydroxypoly(oxyethylene) poly...

21 CFR 178.3570 - Lubricants with incidental food contact.

Code of Federal Regulations, 2010 CFR

2010-04-01

... 21 Food and Drugs 3 2010-04-01 2009-04-01 true Lubricants with incidental food contact. 178.3570... provisions of a prior sanction or approval. (3) Substances identified in this paragraph (a)(3). Substances....1 percent by weight of the lubricant. BHA BHT α-Butyl-omega-hydroxypoly(oxyethylene) poly...

21 CFR 178.3570 - Lubricants with incidental food contact.

Code of Federal Regulations, 2012 CFR

2012-04-01

... 21 Food and Drugs 3 2012-04-01 2012-04-01 false Lubricants with incidental food contact. 178.3570... provisions of a prior sanction or approval. (3) Substances identified in this paragraph (a)(3). Substances....1 percent by weight of the lubricant. BHA BHT α-Butyl-omega-hydroxypoly(oxyethylene) poly...

21 CFR 178.3570 - Lubricants with incidental food contact.

Code of Federal Regulations, 2013 CFR

2013-04-01

... 21 Food and Drugs 3 2013-04-01 2013-04-01 false Lubricants with incidental food contact. 178.3570... provisions of a prior sanction or approval. (3) Substances identified in this paragraph (a)(3). Substances....1 percent by weight of the lubricant. BHA BHT α-Butyl-omega-hydroxypoly(oxyethylene) poly...

Corrosion protection of steel by thin coatings of starch-oil dry lubricants

USDA-ARS?s Scientific Manuscript database

Corrosion of materials is one of the most serious and challenging problems faced worldwide by industry. Dry lubricants reduce friction between two metal surfaces. This research investigated the inhibition of corrosive behavior a dry lubricant formulation consisting of jet-cooked corn starch and soyb...

Comparison of Extreme Pressure Additive Treat Rates in Soybean and Mineral Oils Under Boundary Lubrication Conditions

USDA-ARS?s Scientific Manuscript database

Traditionally, it is considered that, under boundary lubrication conditions, the reduction in friction and wear is mostly dependent on Extreme Pressure (EP) additives, rather than the basestock. However, several studies indicate that vegetable oils also contribute to the lubricity under this regime...

Ocean Spray Lubricates Winds

ERIC Educational Resources Information Center

Journal of College Science Teaching, 2005

2005-01-01

According to a new study by two University of California, Berkeley, mathematicians and their Russian colleague, the water droplets kicked up by rough seas serve to lubricate the swirling winds of hurricanes and cyclones, letting them build to speeds approaching 200 miles per hour. Without the lubricating effect of the spray, the mathematicians…

Lubricant Evaluation and Performance 2

DTIC Science & Technology

1994-02-01

Damasco 1 1 used the four- ball test to study PPE using MI0 tool steel balls. Figure 105 reveals a reduction of wear after reaching a critical temperature... Damasco , F., "High-Temperature Fluid Lubrication," ASLE Trans., 7, pp. 211-217 (1964). 12. Wills, J.G., Lubrication Fundamentals, Marcel Dekker, Inc., New

Contribution of Lubricating Oil to Particulate Matter Emissions from Light-duty Gasoline Vehicles in Kansas City

EPA Science Inventory

The contribution of lubricating oil to particulate matter (PM) emissions representative of the in-use 2004 light-duty gasoline vehicles fleet is estimated from the Kansas City Light-Duty Vehicle Emissions Study (KCVES). PM emissions are apportioned to lubricating oil and gasoline...

Positive lubrication system

NASA Technical Reports Server (NTRS)

Smith, Dennis W.; Hooper, Fred L.

1990-01-01

As part of the development of an autonomous lubrication system for spin bearings, a system was developed to deliver oil to grease-lubricated bearings upon demand. This positive oil delivery system (PLUS) consists of a pressurized reservoir with a built-in solenoid valve that delivers a predictable quantity of oil to the spin bearing through a system of stainless steel tubes. Considerable testing was performed on the PLUS to characterize its performance and verify its effectiveness, along with qualifying it for flight. Additional development is underway that will lead to the fully autonomous active lubrication system.

CVD method of forming self-lubricating composites

DOEpatents

Besmann, T.M.; Blau, P.J.; Lee, W.Y.; Bae, Y.W.

1998-12-01

An article having a multiphase composite lubricant coating of a hard refractory matrix phase of titanium nitride dispersed with particles of a solid lubricating phase of molybdenum disulfide is prepared by heating the article to temperatures between 350 and 850 C in a reaction vessel at a reduced pressure and passing a gaseous mixture of Ti((CH{sub 3}){sub 2}N){sub 4}, MoF{sub 6}, H{sub 2}S and NH{sub 3} over the heated article forming a multiphase composite lubricant coating on the article. 1 fig.

Influence of Total Inertia Effects in a Thrust Curvilinear Bearing Lubricated with Newtonian Lubricants

NASA Astrophysics Data System (ADS)

Walicka, A.; Jurczak, P.

2017-12-01

In the paper, the flow of a Newtonian type of lubricant in the clearance of a curvilinear bearing is considered. It is assumed that the bearing walls are modelled as smooth and impermeable. In analytical considerations, full inertia of the longitudinal flow and partial inertia of the circumferential flow are taken into account. The equation of motion of the lubricant is solved by the modified method of averaged inertia. A thrust bearing and spherical bearing are considered, for which dimensionless pressure distributions and the bearing capacity are given.

Evaluation for Loss of Lubrication Performance of Black Oxide, Superfinished, and As-Ground Surfaces for Use in Rotorcraft Transmissions

DTIC Science & Technology

2016-09-01

2.3.2 Loss -of-Lubrication Protocol 5 2.3.3 Friction Mapping Protocol 7 2.4 Test Matrices 9 3. Results and Discussion 10 3.1 Load Capacity 10...protocols used to simulate relevant contact conditions are the load capacity (LC), loss -of-lubrication (LoL), and mapping protocols. 2.3.1 Load ...Entrainment velocity (m/s) Slip (%) Skew (°) Load (N) Contact stress (GPa) LoL 16 –100 0 100 1.29 2.3.2.2 Low-Speed Loss -of-Lubrication

New directions in lubrication, materials, wear, and surface interactions - Tribology in the 80's

NASA Technical Reports Server (NTRS)

Loomis, W. R. (Editor)

1985-01-01

New directions in tribology are described. A range of topics is addressed, extending from fundamental research on tribological materials of all kinds and their surface effects, to final technological applications in mechanical components such as bearings, gears, and seals. The general topics addressed include: importance and definition of materials in tribology; future directions of research in adhesion and friction, wear and wear-resistant materials, and liquid lubricants and additives; status and new directions in elastohydrodynamic lubrication and solid lubricants; and tribological materials for mechanical components of the future.

Measurement and Assessment of Bearing Degradation in Ester-Based Lubricant Systems

DTIC Science & Technology

2009-02-01

Co Ni Fe M50 -- 4 1 4.25 0.3 0.3 0.8 -- -- Bal. P675 ~2% 13 0.6 1.8 0.4 0.65 0.07 5.4 2.6 Bal. Compositions in wt% Bearing Steels Lubricant-Water...Measurement and Assessment of Bearing Degradation in Ester- Based Lubricant Systems Darryl P. Butt Department of Materials Science and Engineering...to 00-00-2009 4. TITLE AND SUBTITLE Measurement and Assessment of Bearing Degradation in Ester-Based Lubricant Systems 5a. CONTRACT NUMBER 5b

Oil-air mist lubrication as an emergency system and as a primary lubrication system. [for helicopter engines

NASA Technical Reports Server (NTRS)

Loomis, W. R.

1976-01-01

The feasibility of an emergency aspirator once-through lubrication system was demonstrated as a viable survivability concept for Army helicopter mainshaft engine bearings for periods as long as 30 minutes. It was also shown in an experimental study using a 46-mm bore bearing test machine that an oil-air mist once-through system with auxiliary air cooling is an effective primary lubrication system at speeds up to 2,500,000 DN for extended operating periods of at least 50 hours.

Torquing preload in a lubricated bolt

NASA Technical Reports Server (NTRS)

Seegmiller, H. L.

1978-01-01

The tension preload obtained by torquing a 7/8 in. diam UNC high strength bolt was determined for lubricated and dry conditions. Consistent preload with a variation of + or - 3% was obtained when the bolt head area was lubricated prior to each torque application. Preload tensions nearly 70% greater than the value predicted with the commonly used formula occurred with the lubricated bolt. A reduction to 39% of the initial preload was observed during 50 torque applications without relubrication. Little evidence of wear was noted after 203 cycles of tightening.

CVD method of forming self-lubricating composites

DOEpatents

Besmann, Theodore M.; Blau, Peter J.; Lee, Woo Y.; Bae, Yong W.

1998-01-01

An article having a multiphase composite lubricant coating of a hard refractory matrix phase of titanium nitride dispersed with particles of a solid lubricating phase of molybdenum disulfide is prepared by heating the article to temperatures between 350.degree. and 850.degree. C. in a reaction vessel at a reduced pressure and passing a gaseous mixture of Ti((CH.sub.3).sub.2 N).sub.4, MoF.sub.6, H.sub.2 S and NH.sub.3 over the heated article forming a multiphase composite lubricant coating on the article.

Automotive Lubricant Specification and Testing

NASA Astrophysics Data System (ADS)

Fox, M. F.

This chapter concerns commercial lubricant specification and testing, drawing together the many themes of previous chapters. Military lubricant standards were a very strong initial influence during World War II and led to the separate historical development of the North American and European specification systems. The wide range of functions that a successful lubricant must satisfy is discussed, together with issues of balancing special or universal applications, single or multiple engine tests, the philosophy of accelerated testing and the question of 'who sets the standards?' The role of engine tests and testing organisations is examined.

Dynamic characterization of viscoelastic polymer solutions in a lubricated cylinder - Plate apparatus

NASA Technical Reports Server (NTRS)

Doremus, P.; Piau, J. M.; Altman, R. L.

1987-01-01

The characterization of several viscoelastic lubricants which are oil or water based has been studied in an apparatus consisting of a lubricated cylinder-plate contact. The friction loads were measured as a function of speed. The experimental results show the influence of the molecular weight and of the concentration of the polymeric additive as well as the influence of the viscosity of the oil-base on the load and friction coefficient. Also a test for mechanical degradation was performed on the polymer solutions. Several additives can favor a viscoelastic lubrication.

Investigation of Potential Thermal Processing Techniques for the Enhancement of PS300 High Temperature Solid Lubricant Coatings

NASA Technical Reports Server (NTRS)

Benoy, Patricia A.

2000-01-01

Contemporary trends in rotating machinery development have produced a continuous evolution towards ever increasing speeds and higher operating temperatures. This process has been particularly evident in aerospace and automotive applications such as turbochargers. The combination of high temperature and high speed has exceeded the capacity of mainstream liquid lubrication technology. The NASA Glenn Research Center has been at the forefront in developing innovative solid lubricants for the oil free protection of rotating machinery under these extreme environmental conditions. The most recent of these is the PS 300 series of plasma sprayed solid lubricant coatings. St Louis University and NASA Glenn Research Center entered into this cooperative agreement to investigate potential thermal processing techniques for the enhancement of the PS 304 solid lubricant.

Compaction of AWBA fuel pellets without binders (AWBA Development Program)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Johnson, R.G.R.

1982-08-01

Highly active oxide fuel powders, composed of UO/sub 2/, UO/sub 2/-ThO/sub 2/, or ThO/sub 2/, were compacted into ultra-high density pellets without the use of binders. The objective of the study was to select the optimum die lubricant for compacting these powders into pellets in preparation for sintering to densities in excess of 97% Theoretical Density. The results showed that sintered density was a function of both the lubricant bulk density and concentration with the lowest bulk density lubricant giving the highest sintered densities with a lubricant concentration of 0.1 weight percent. Five calcium and zinc stearates were evaluated withmore » a calcium stearate with a 15 lb/ft/sup 3/ bulk density being the best lubricant.« less

Liquid lubricants for advanced aircraft engines

NASA Technical Reports Server (NTRS)

Loomis, William R.; Fusaro, Robert L.

1993-01-01

An overview of liquid lubricants for use in current and projected high performance turbojet engines is discussed. Chemical and physical properties are reviewed with special emphasis placed on the oxidation and thermal stability requirements imposed upon the lubrication system. A brief history is given of the development of turbine engine lubricants which led to the present day synthetic oils with their inherent modification advantages. The status and state of development of some eleven candidate classes of fluids for use in advanced turbine engines are discussed. Published examples of fundamental studies to obtain a better understanding of the chemistry involved in fluid degradation are reviewed. Alternatives to high temperature fluid development are described. The importance of continuing work on improving current high temperature lubricant candidates and encouraging development of new and improved fluid base stocks are discussed.

High-Performing, Low-Temperature-Operating, Long-Lifetime Aerospace Lubricants

NASA Technical Reports Server (NTRS)

Joshi, Prakash

2015-01-01

Long-duration space exploration will require spacecraft systems that can operate effectively over several years with minimal or no maintenance. Aerospace lubricants are key components of spacecraft systems. Physical Sciences Inc., has synthesized and characterized novel ionic liquids for use in aerospace lubricants that contribute to decreased viscosity, friction, and wear in aerospace systems. The resulting formulations offer low vapor pressure and outgassing properties and thermal stability up to 250 C. They are effective for use at temperatures as low as -70 C and provide long-term operational stability in aerospace systems. In Phase II, the company scaled several new ionic liquids and evaluated a novel formulation in a NASA testbed. The resulting lubricant compounds will offer lower volatility, decreased corrosion, and better tribological characteristics than standard liquid lubricants, particularly at lower temperatures.

Lubrication and cooling for high speed gears

NASA Technical Reports Server (NTRS)

Townsend, D. P.

1985-01-01

The problems and failures occurring with the operation of high speed gears are discussed. The gearing losses associated with high speed gearing such as tooth mesh friction, bearing friction, churning, and windage are discussed with various ways shown to help reduce these losses and thereby improve efficiency. Several different methods of oil jet lubrication for high speed gearing are given such as into mesh, out of mesh, and radial jet lubrication. The experiments and analytical results for the various methods of oil jet lubrication are shown with the strengths and weaknesses of each method discussed. The analytical and experimental results of gear lubrication and cooling at various test conditions are presented. These results show the very definite need of improved methods of gear cooling at high speed and high load conditions.

A Preliminary Study on the Vapor/Mist Phase Lubrication of a Spur Gearbox

NASA Technical Reports Server (NTRS)

Morales, Wilfredo; Handschuh, Robert F.

1999-01-01

Organophosphates have been the primary compounds used in vapor/mist phase lubrication studies involving ferrous bearing material. Experimental results have indicated that the initial formation of an iron phosphate film on a rubbing ferrous surface, followed by the growth (by cationic diffusion) of a lubricious pyrophosphate-type coating over the iron phosphate, is the reason organophosphates work well as vapor/mist phase lubricants. Recent work, however, has shown that this mechanism leads to the depletion of surface iron atoms and to eventual lubrication failure. A new organophosphate formulation was developed which circumvents surface iron depletion. This formulation was tested by generating an iron phosphate coating on an aluminum surface. The new formulation was then used to vapor/mist phase lubricate a spur gearbox in a preliminary study.

Microfog lubrication for aircraft engine bearings

NASA Technical Reports Server (NTRS)

Rosenlieb, J. W.

1976-01-01

An analysis and system study was performed to provide design information regarding lubricant and coolant flow rates and flow paths for effective utilization of the lubricant and coolant in a once through bearing oil mist (microfog) and coolant air system. Both static and dynamic tests were performed. Static tests were executed to evaluate and calibrate the mist supply system. A total of thirteen dynamic step speed bearing tests were performed using four different lubricants and several different mist and air supply configurations. The most effective configuration consisted of supplying the mist and the major portion of the cooling air axially through the bearing. The results of these tests have shown the feasibility of using a once through oil mist and cooling air system to lubricate and cool a high speed, high temperature aircraft engine mainshaft bearing.

Spectroscopic Analysis of Perfluoropolyether Lubricant Degradation During Boundary Lubrication

NASA Technical Reports Server (NTRS)

Herrera-Fierro, Pilar; Shogrin, Bradley A.; Jones, William R., Jr.

1996-01-01

The degradation of a branched perfluoropolyether (PFPE) under boundary lubrication conditions was studied using mu-FTIR and mu-Raman spectroscopies. Stainless steel (440C) discs coated with thin (600A), uniform films of the PFPE were tested in a ball-on-disc apparatus until various levels of friction coefficient were attained. Discs were then examined using the above techniques. When the friction coefficient surpassed the value obtained with an un-lubricated control, the lubricant film had either been physically displaced or partially transformed in to a 'friction polymer'. Infrared analysis of this 'friction polymer' indicated the presence of a polymeric fluorinated acid species (R(sub f)COOH). Raman spectroscopy indicated the presence of amorphous carbon in the wear track and in the friction polymer. Some reaction mechanisms are suggested to explain the results.

Liquid lubricants for advanced aircraft engines

NASA Technical Reports Server (NTRS)

Loomis, William R.; Fusaro, Robert L.

1992-01-01

An overview of liquid lubricants for use in current and projected high performance turbojet engines is discussed. Chemical and physical properties are reviewed with special emphasis placed on the oxidation and thermal stability requirements imposed upon the lubrication system. A brief history is given of the development of turbine engine lubricants which led to the present day synthetic oils with their inherent modification advantages. The status and state of development of some eleven candidate classes of fluids for use in advanced turbine engines are discussed. Published examples of fundamental studies to obtain a better understanding of the chemistry involved in fluid degradation are reviewed. Alternatives to high temperature fluid development are described. The importance of continuing work on improving current high temperature lubricant candidates and encouraging development of new and improved fluid base stocks are discussed.

Galectin-3 Binds to Lubricin and Reinforces the Lubricating Boundary Layer of Articular Cartilage.

PubMed

Reesink, Heidi L; Bonnevie, Edward D; Liu, Sherry; Shurer, Carolyn R; Hollander, Michael J; Bonassar, Lawrence J; Nixon, Alan J

2016-05-09

Lubricin is a mucinous, synovial fluid glycoprotein that enables near frictionless joint motion via adsorption to the surface of articular cartilage and its lubricating properties in solution. Extensive O-linked glycosylation within lubricin's mucin-rich domain is critical for its boundary lubricating function; however, it is unknown exactly how glycosylation facilitates cartilage lubrication. Here, we find that the lubricin glycome is enriched with terminal β-galactosides, known binding partners for a family of multivalent lectins called galectins. Of the galectin family members present in synovial fluid, we find that galectin-3 is a specific, high-affinity binding partner for lubricin. Considering the known ability of galectin-3 to crosslink glycoproteins, we hypothesized that galectins could augment lubrication via biomechanical stabilization of the lubricin boundary layer. We find that competitive inhibition of galectin binding results in lubricin loss from the cartilage surface, and addition of multimeric galectin-3 enhances cartilage lubrication. We also find that galectin-3 has low affinity for the surface layer of osteoarthritic cartilage and has reduced affinity for sialylated O-glycans, a glycophenotype associated with inflammatory conditions. Together, our results suggest that galectin-3 reinforces the lubricin boundary layer; which, in turn, enhances cartilage lubrication and may delay the onset and progression of arthritis.

Galectin-3 Binds to Lubricin and Reinforces the Lubricating Boundary Layer of Articular Cartilage

PubMed Central

Reesink, Heidi L.; Bonnevie, Edward D.; Liu, Sherry; Shurer, Carolyn R.; Hollander, Michael J.; Bonassar, Lawrence J.; Nixon, Alan J.

2016-01-01

Lubricin is a mucinous, synovial fluid glycoprotein that enables near frictionless joint motion via adsorption to the surface of articular cartilage and its lubricating properties in solution. Extensive O-linked glycosylation within lubricin’s mucin-rich domain is critical for its boundary lubricating function; however, it is unknown exactly how glycosylation facilitates cartilage lubrication. Here, we find that the lubricin glycome is enriched with terminal β-galactosides, known binding partners for a family of multivalent lectins called galectins. Of the galectin family members present in synovial fluid, we find that galectin-3 is a specific, high-affinity binding partner for lubricin. Considering the known ability of galectin-3 to crosslink glycoproteins, we hypothesized that galectins could augment lubrication via biomechanical stabilization of the lubricin boundary layer. We find that competitive inhibition of galectin binding results in lubricin loss from the cartilage surface, and addition of multimeric galectin-3 enhances cartilage lubrication. We also find that galectin-3 has low affinity for the surface layer of osteoarthritic cartilage and has reduced affinity for sialylated O-glycans, a glycophenotype associated with inflammatory conditions. Together, our results suggest that galectin-3 reinforces the lubricin boundary layer; which, in turn, enhances cartilage lubrication and may delay the onset and progression of arthritis. PMID:27157803

Method and apparatus for forming flues on tubular stock

DOEpatents

Beck, D.E.; Carson, C.

1979-12-21

The present invention is directed to a die mechanism utilized for forming flues on long, relatively narrow tubular stock. These flues are formed by displacing a die from within the tubular stock through perforations previously drilled through the tubular stock at selected locations. The drawing of the die upsets the material to form the flue of the desired configuration. The die is provided with a lubricating system which enables the lubricant to be dispensed uniformly about the entire periphery of the die in contact with the material being upset so as to assure the formation of the flues. Further, the lubricant is dispensed from within the die onto the peripheral surface of the latter at pressures in the range of about 2000 to 10,000 psi so as to assure the adequate lubrication of the die during the drawing operation. By injecting the lubricant at such high pressures, low viscosity liquid, such as water and/or alcohol, may be efficiently used as a lubricant and also provides a mechanism by which the lubricant may be evaporated from the surface of the flues at ambient conditions so as to negate the cleansing operations previously required prior to joining the flues to other conduit mechanisms by fusion welding and the like.

Compression parameters of hexagonal boron nitride on direct compression mixture of microcrystalline cellulose and modified starch.

PubMed

Halaçoğlu, Mekin Doğa; Uğurlu, Timuçin

2015-01-01

The objective of this study was to investigate the effects of conventional lubricants including a new candidate lubricant "hexagonal boron nitride (HBN)" on direct compression powders. Lubricants such as magnesium stearate (MGST), glyceryl behenate, stearic acid, talc and polyethylene glycol6000 were studied and tablets were manufactured on a single station instrumented tablet press. This study comprised the continuation of our previous one, so mixture of microcrystalline cellulose and modified starch was used as a master formula to evaluate effects of lubricants on pharmaceutical excipients that undergo complete plastic deformation without any fragmentation under compression pressure. Bulk and tapped densities, and Carr's index parameters were calculated for powders. Tensile strength, cohesion index, lower punch ejection force and lubricant effectiveness values were investigated for tablets. The deformation mechanisms of tablets were studied during compression from the Heckel plots with or without lubricant. MGST was found to be the most effective lubricant and HBN was found very close to it. HBN did not show a significant negative effect on the crushing strength and disintegration time of the tablets when we compared with MGST. Based on the Heckel plots at the level of 1%, formulation prepared with HBN showed the most pronounced plastic character.

High-Temperature Solid Lubricants Developed by NASA Lewis Offer Virtually "Unlimited Life" for Oil-Free Turbomachinery

NASA Technical Reports Server (NTRS)

DellaCorte, Christopher; Valco, Mark J.

1999-01-01

The NASA Lewis Research Center is capitalizing on breakthroughs in foil air bearing performance, tribological coatings, and computer analyses to formulate the Oil-free Turbomachinery Program. The program s long-term goal is to develop an innovative, yet practical, oil-free aeropropulsion gas turbine engine that floats on advanced air bearings. This type of engine would operate at higher speeds and temperatures with lower weight and friction than conventional oil-lubricated engines. During startup and shutdown, solid lubricant coatings are required to prevent wear in such engines before the self-generating air-lubrication film develops. NASA s Tribology Branch has created PS304, a chrome-oxide-based plasma spray coating specifically tailored for shafts run against foil bearings. PS304 contains silver and barium fluoride/calcium fluoride eutectic (BaF2/CaF2) lubricant additives that, together, provide lubrication from cold start temperatures to over 650 C, the maximum use temperature for foil bearings. Recent lab tests show that bearings lubricated with PS304 survive over 100 000 start-stop cycles without experiencing any degradation in performance due to wear. The accompanying photograph shows a test bearing after it was run at 650 C. The rubbing process created a "polished" surface that enhances bearing load capacity.

Solubility modeling of refrigerant/lubricant mixtures

DOE Office of Scientific and Technical Information (OSTI.GOV)

Michels, H.H.; Sienel, T.H.

1996-12-31

A general model for predicting the solubility properties of refrigerant/lubricant mixtures has been developed based on applicable theory for the excess Gibbs energy of non-ideal solutions. In our approach, flexible thermodynamic forms are chosen to describe the properties of both the gas and liquid phases of refrigerant/lubricant mixtures. After an extensive study of models for describing non-ideal liquid effects, the Wohl-suffix equations, which have been extensively utilized in the analysis of hydrocarbon mixtures, have been developed into a general form applicable to mixtures where one component is a POE lubricant. In the present study we have analyzed several POEs wheremore » structural and thermophysical property data were available. Data were also collected from several sources on the solubility of refrigerant/lubricant binary pairs. We have developed a computer code (NISC), based on the Wohl model, that predicts dew point or bubble point conditions over a wide range of composition and temperature. Our present analysis covers mixtures containing up to three refrigerant molecules and one lubricant. The present code can be used to analyze the properties of R-410a and R-407c in mixtures with a POE lubricant. Comparisons with other models, such as the Wilson or modified Wilson equations, indicate that the Wohl-suffix equations yield more reliable predictions for HFC/POE mixtures.« less

Biodynamic Performance of Hyaluronic Acid versus Synovial fluid of the Knee for Osteoarthritic Therapy

PubMed Central

Corvelli, Michael; Che, Bernadette; Saeui, Christopher; Singh, Anirudha; Elisseeff, Jennifer

2015-01-01

Hyaluronic acid (HA), a natural biomaterial present in healthy joints but depleted in osteoarthritis (OA), has been employed clinically to provide symptomatic relief of joint pain. Joint movement combined with a reduced joint lubrication in osteoarthritic knees can result in increased wear and tear, chondrocyte apoptosis, and inflammation, leading to cascading cartilage deterioration. Therefore, development of an appropriate cartilage model and evaluation for its friction properties with potential lubricants in different conditions is necessary, which can closely resemble a mechanically induced OA cartilage. Additionally, the comparison of different models with and without endogenous lubricating surface zone proteins, such as PRG4 promotes a well-rounded understanding of cartilage lubrication. In this study, we present our findings on the lubricating effects of HA on different articular cartilage model surfaces in comparison to synovial fluid, a physiological lubricating biomaterial. The mechanical testings data demonstrated that HA reduced average static and kinetic friction coefficient values of the cartilage samples by 75% and 70%, respectively. Furthermore, HA mimicked the friction characteristics of freshly harvested natural synovial fluid throughout all tested and modeled OA conditions with no statistically significant difference. These characteristics led us to exclusively identify HA as an effective boundary layer lubricant in the technology that we develop to treat OA [Singh et al. 2104]. PMID:25858258

A study of the properties of compacts from silicified microcrystalline celluloses.

PubMed

Muzíková, Jitka; Nováková, Petra

2007-07-01

The paper deals with a study of tensile strength and disintegration time of compacts made from silicified microcrystalline celluloses, Prosolv SMCC 90, and Prosolv HD 90, in dependence on compression force, addition of two types of lubricants, and two active ingredients. The lubricants were magnesium stearate and sodium stearyl fumarate in a concentration of 0.5%, the active ingredients being ascorbic acid and acetylsalicylic acid in a concentration of 50%. Prosolv SMCC 90 proved to be better compatible than Prosolv HD 90; the compacts were of higher strength, which was markedly increased with increasing compression force. Prosolv HD 90 was more sensitive to additions of lubricants, and a greater decrease in strength was recorded due to the influence of sodium stearyl fumarate. The effect of lubricants on the strength of compacts in the presence of active ingredients was not identical. The disintegration time of compacts from Prosolv HD 90 without as well as with lubricants was shorter than from Prosolv SMCC 90 and was increasing with increasing compression force. Disintegration time was increased with added lubricants, and it was markedly shortened by addition of active ingredients. Compacts containing ascorbic acid possessed a shorter disintegration time than those containing acetylsalicylic acid, and it was not markedly influenced by the presence of lubricants.

Lubricant distribution and its effect on slider air bearing performance over bit patterned media disk of disk drives

NASA Astrophysics Data System (ADS)

Wu, Lin

2011-04-01

The distribution dynamics of a thin lubricant film on a bit-patterned media disk and its effect on the performance of the ultralow flying air bearing slider of disk drives are studied by direct numerical simulations. Our analysis shows that the physics governing lubricant distribution dynamics changes when deep enough sub-100-nm nanostructures are patterned on the disk surface. Air shearing under the slider that dominates lubricant flow on a flat disk may become negligible on a bit-patterned media disk. Surface tension and disjoining pressure become dominant factors instead. Our results show that disks with nanoscale patterns/roughness may no longer be treated as flat, and the air bearing load may strongly depend not only on the geometric detail of disk patterns but also on how lubricants are distributed on the patterns when slider-disk clearance is reduced to sub-10-nm. Air bearing load and consequently the slider's flying attitude are affected by disk pattern geometry, average lubricant thickness, and material properties of lubricant such as the surface tension coefficient and Hamaker constant. The significantly expanded parameter space, upon which ultralow flying slider's dynamics depends, has to be seriously considered in evaluating the head/disk interface tribology performance of next generation patterned media magnetic recording systems.

Galectin-3 Binds to Lubricin and Reinforces the Lubricating Boundary Layer of Articular Cartilage

NASA Astrophysics Data System (ADS)

Reesink, Heidi L.; Bonnevie, Edward D.; Liu, Sherry; Shurer, Carolyn R.; Hollander, Michael J.; Bonassar, Lawrence J.; Nixon, Alan J.

2016-05-01

Lubricin is a mucinous, synovial fluid glycoprotein that enables near frictionless joint motion via adsorption to the surface of articular cartilage and its lubricating properties in solution. Extensive O-linked glycosylation within lubricin’s mucin-rich domain is critical for its boundary lubricating function; however, it is unknown exactly how glycosylation facilitates cartilage lubrication. Here, we find that the lubricin glycome is enriched with terminal β-galactosides, known binding partners for a family of multivalent lectins called galectins. Of the galectin family members present in synovial fluid, we find that galectin-3 is a specific, high-affinity binding partner for lubricin. Considering the known ability of galectin-3 to crosslink glycoproteins, we hypothesized that galectins could augment lubrication via biomechanical stabilization of the lubricin boundary layer. We find that competitive inhibition of galectin binding results in lubricin loss from the cartilage surface, and addition of multimeric galectin-3 enhances cartilage lubrication. We also find that galectin-3 has low affinity for the surface layer of osteoarthritic cartilage and has reduced affinity for sialylated O-glycans, a glycophenotype associated with inflammatory conditions. Together, our results suggest that galectin-3 reinforces the lubricin boundary layer; which, in turn, enhances cartilage lubrication and may delay the onset and progression of arthritis.

Test Facility Simulation Results for Aerospace Loss-of-Lubrication of Spur Gears

NASA Technical Reports Server (NTRS)

Handschuh, Robert F.; Gargano, Lucas J.

2014-01-01

Prior to receiving airworthiness certification, extensive testing is required during the development of rotary wing aircraft drive systems. Many of these tests are conducted to demonstrate the drive system's ability to operate at extreme conditions, beyond that called for in the normal to maximum power operating range. One of the most extreme tests is referred to as the loss-of-lubrication or run dry test. During this test, the drive system is expected to last at least 30 min without failure while the primary lubrication system is disabled for predetermined, scripted flight conditions. Failure of this test can lead to a partial redesign of the drive system or the addition of an emergency lubrication system. Either of these solutions can greatly increase the aircraft drive system cost and weight and extend the schedule for obtaining airworthiness certification. Recent work at NASA Glenn Research Center focused on performing tests, in a relevant aerospace environment, to simulate the behavior of spur gears under loss-of-lubrication conditions. Tests were conducted using a test facility that was used in the past for spur gear contact fatigue testing. A loss-oflubrication test is initiated by shutting off the single into mesh lubricating jet. The test proceeds until the gears fail and can no longer deliver the applied torque. The observed failures are typically plastically deformed gear teeth, due to the high tooth temperatures, that are no longer in mesh. The effect of several different variables to gear tooth condition during loss-of-lubrication have been tested such as gear pitch, materials, shrouding, lubrication condition, and emergency supplied mist lubrication in earlier testing at NASA. Recent testing has focused on newer aerospace gear steels and imbedding thermocouples in the shrouding to measure the air-oil temperatures flung off the gear teeth. Along with the instrumented shrouding, an instrumented spur gear was also tested. The instrumented spur gear had five thermocouples installed at different locations on the gear tooth and web. The data from these two types of measurements provided important information as to the thermal environment during the loss-of-lubrication event. This data is necessary to validate on-going modeling efforts.

Reduction of friction by recombinant human proteoglycan 4 in IL-1α stimulated bovine cartilage explants.

PubMed

Larson, Katherine M; Zhang, Ling; Elsaid, Khaled A; Schmidt, Tannin A; Fleming, Braden C; Badger, Gary J; Jay, Gregory D

2017-03-01

A boundary lubricant attaches and protects sliding bearing surfaces by preventing interlocking asperity-asperity contact. Proteoglycan-4 (PRG4) is a boundary lubricant found in the synovial fluid that provides chondroprotection to articular surfaces. Inflammation of the diarthrodial joint modulates local PRG4 concentration. Thus, we measured the effects of inflammation, with Interleukin-1α (IL-1α) incubation, upon boundary lubrication and PRG4 expression in bovine cartilage explants. We further aimed to determine whether the addition of exogenous human recombinant PRG4 (rhPRG4) could mitigate the effects of inflammation on boundary lubrication and PRG4 expression in vitro. Cartilage explants, following a 7 day incubation with IL-1α, were tested in a disc-on-disc configuration using either rhPRG4 or saline (PBS control) as a lubricant. Following mechanical testing, explants were studied immunohistochemically or underwent RNA extraction for real-time polymerase chain reaction (RT-PCR). We found that static coefficient of friction (COF) significantly decreased to 0.14 ± 0.065 from 0.21 ± 0.059 (p = 0.014) in IL-1α stimulated explants lubricated with rhPRG4, as compared to PBS. PRG4 expression was significantly up regulated from 30.8 ± 19 copies in control explants lubricated with PBS to 3330 ± 1760 copies in control explants lubricated with rhPRG4 (p < 0.001). Explants stimulated with IL-1α displayed no increase in PRG4 expression upon lubrication with rhPRG4, but with PBS as the lubricant, IL-1α stimulation significantly increased PRG4 expression compared to the control condition from 30.8 ± 19 copies to 401 ± 340 copies (p = 0.015). Overall, these data suggest that exogenous rhPRG4 may provide a therapeutic option for reducing friction in transient inflammatory conditions and increasing PRG4 expression. © 2017 Orthopaedic Research Society. Published by Wiley Periodicals, Inc. J Orthop Res 35:580-589, 2017. © 2017 Orthopaedic Research Society. Published by Wiley Periodicals, Inc.

Enhanced lubricant film formation through micro-dimpled hard-on-hard artificial hip joint: An in-situ observation of dimple shape effects.

PubMed

Choudhury, Dipankar; Rebenda, David; Sasaki, Shinya; Hekrle, Pavel; Vrbka, Martin; Zou, Min

2018-05-01

This study evaluates the impact of dimple shapes on lubricant film formation in artificial hip joints. Micro-dimples with 20-50 µm lateral size and 1 ± 0.2 µm depths were fabricated on CrCoMo hip joint femoral heads using a picosecond laser. Tribological studies were performed using a pendulum hip joint simulator to apply continuous swing flexion-extension motions. The results revealed a significantly enhanced lubricant film thickness (≥ 500 nm) with micro-dimpled prosthesis heads at equilibrium position after the lubricant film has fully developed. The average lubricant film thickness of dimpled prostheses with square- and triangular-shaped dimple arrays over time is about 3.5 that of the non-dimpled prosthesis (204 nm). Remarkably, the prosthesis with square-shaped dimple arrays showed a very fast lubricant film formation reaching their peak values within 0.5 s of pendulum movement, followed by prosthesis with triangular-shaped dimple arrays with a transition period of 42.4 s. The fully developed lubricant film thicknesses (≥ 700 nm) are significantly higher than the surface roughness (≈ 25 nm) demonstrating a hydrodynamic lubrication. Hardly any scratches appeared on the post-experimental prosthesis with square-shaped dimple array and only a few scratches were found on the post-experimental prosthesis with triangular-shaped dimple arrays. Thus, prostheses with square-shaped dimple arrays could be a potential solution for durable artificial hip joints. Copyright © 2018 Elsevier Ltd. All rights reserved.

Rotary seal with enhanced lubrication and contaminant flushing

DOEpatents

Dietle, Lannie L.

2000-01-01

A resilient, ring shaped interference-type hydrodynamic rotary seal having waves on the lubricant side which provide increased film thickness and flushing action by creating contact pressure induced angulated restrictions formed by abrupt restrictive diverters. The angulated restrictions are defined by projecting ridges, corners at the trailing edge of the waves, or simply by use of a converging shape at the trailing edge of the waves which is more abrupt than the gently converging hydrodynamic inlet shape at the leading edge of the waves. The abrupt restrictive diverter performs two functions; a restricting function and a diverting function. The angulated restrictions cause a local film thickness restriction which produces a damming effect preventing a portion of the lubricant from leaking out of the dynamic sealing interface at the trailing edge of the wave, and results in a much thicker lubricant film thickness under the waves. This contributes to more film thickness in the remainder of the dynamic sealing interface toward the environment because film thickness tends to decay gradually rather than abruptly due to the relative stiffness of the seal material. Because of the angle of the abrupt restrictive diverter relative to the relative rotation direction, in conjunction with the restriction or damming effect, a strong diverting action is produced which pumps lubricant across the dynamic sealing interface toward the environment. The lubricant diversion is caused by the component of the rotational velocity tangent to the abrupt restrictive diverter. The component of rotational velocity normal to the abrupt restrictive diverter causes a portion of the lubricant film to be pumped past the abrupt restrictive diverter, thereby assuring adequate lubrication thereof.

Experiments on Ultrasonic Lubrication Using a Piezoelectrically-assisted Tribometer and Optical Profilometer

PubMed Central

Dong, Sheng; Dapino, Marcelo

2015-01-01

Friction and wear are detrimental to engineered systems. Ultrasonic lubrication is achieved when the interface between two sliding surfaces is vibrated at a frequency above the acoustic range (20 kHz). As a solid-state technology, ultrasonic lubrication can be used where conventional lubricants are unfeasible or undesirable. Further, ultrasonic lubrication allows for electrical modulation of the effective friction coefficient between two sliding surfaces. This property enables adaptive systems that modify their frictional state and associated dynamic response as the operating conditions change. Surface wear can also be reduced through ultrasonic lubrication. We developed a protocol to investigate the dependence of friction force reduction and wear reduction on the linear sliding velocity between ultrasonically lubricated surfaces. A pin-on-disc tribometer was built which differs from commercial units in that a piezoelectric stack is used to vibrate the pin at 22 kHz normal to the rotating disc surface. Friction and wear metrics including effective friction force, volume loss, and surface roughness are measured without and with ultrasonic vibrations at a constant pressure of 1 to 4 MPa and three different sliding velocities: 20.3, 40.6, and 87 mm/sec. An optical profilometer is utilized to characterize the wear surfaces. The effective friction force is reduced by 62% at 20.3 mm/sec. Consistently with existing theories for ultrasonic lubrication, the percent reduction in friction force diminishes with increasing speed, down to 29% friction force reduction at 87 mm/sec. Wear reduction remains essentially constant (49%) at the three speeds considered. PMID:26436691

Influence of fluid viscosity and wetting on multiscale viscoelastic lubrication in soft tribological contacts.

PubMed

Selway, Nichola; Chan, Vincent; Stokes, Jason R

2017-02-22

Friction (and lubrication) between soft contacts is prevalent in many natural and engineered systems and plays a crucial role in determining their functionality. The contribution of viscoelastic hysteresis losses to friction in these systems has been well-established and defined for dry contacts; however, the influence of fluid viscosity and wetting on these components of friction has largely been overlooked. We provide systematic experimental evidence of the influence of lubricant viscosity and wetting on lubrication across multiple regimes within a viscoelastic contact. These effects are investigated for comparatively smooth and rough elastomeric contacts (PTFE-PDMS and PDMS-PDMS) lubricated by a series of Newtonian fluids with systematically controlled viscosity and static wetting properties, using a ball-on-disc tribometer. The distinct tribological behaviour, characterised generally by a decrease in the friction coefficient with increasing fluid viscosity and wettability, is explained in terms of lubricant dewetting and squeeze-out dynamics and their impact on multi-scale viscoelastic dissipation mechanisms at the bulk-, asperity-, sub-asperity- and molecular-scale. It is proposed that lubrication within the (non-molecularly) smooth contact is governed by localised fluid entrapment and molecular-scale (interfacial) viscoelastic effects, while additional rubber hysteresis stimulated by fluid-asperity interactions, combined with rapid fluid drainage at low speeds within the rough contact, alter the general shape of the Stribeck curve. This fluid viscosity effect is in some agreement with theoretical predictions. Conventional methods for analysing and interpreting tribological data, which typically involve scaling sliding velocity with lubricant viscosity, need to be revised for viscoelastic contacts with consideration of these indirect viscosity effects.

Copper-acrylic enamel serves as lubricant for cold drawing of refractory metals

NASA Technical Reports Server (NTRS)

Beane, C.; Karasek, F.

1966-01-01

Acrylic enamel spray containing metallic copper pigment lubricates refractory metal tubing during cold drawing operations so that the tubing surface remains free from scratches and nicks and does not seize in the die. Zirconium alloys, zirconium, tantalum alloys, niobium alloys, vanandium alloys and titanium alloys have been drawn using this lubricant.

49 CFR 1242.59 - Train inspection and lubrication (account XX-51-62).

Code of Federal Regulations, 2010 CFR

2010-10-01

... 49 Transportation 9 2010-10-01 2010-10-01 false Train inspection and lubrication (account XX-51-62). 1242.59 Section 1242.59 Transportation Other Regulations Relating to Transportation (Continued) SURFACE...-Transportation § 1242.59 Train inspection and lubrication (account XX-51-62). Separate common expenses on basis...

AUTOMOTIVE DIESEL MAINTENANCE, UNIT V, MAINTAINING THE LUBRICATION SYSTEM--DETROIT DIESEL ENGINE.

ERIC Educational Resources Information Center

Human Engineering Inst., Cleveland, OH.

THIS MODULE OF A 30-MODULE COURSE IS DESIGNED TO DEVELOP AN UNDERSTANDING OF THE OPERATION AND MAINTENANCE OF THE DIESEL ENGINE LUBRICATION SYSTEM. TOPICS ARE LUBE OILS USED, MAINTENANCE OF THE LUBRICATION SYSTEM, AND CRANKCASE VENTILATION COMPONENTS. THE MODULE CONSISTS OF A SELF-INSTRUCTIONAL BRANCH PROGRAMED TRAINING FILM "BASIC ENGINE…

Pretreatment of lubricated surfaces with sputtered cadmium oxide

NASA Technical Reports Server (NTRS)

Fusaro, Robert L. (Inventor)

1991-01-01

Cadmium oxide is used with a dry solid lubricant on a surface to improve wear resistance. The surface topography is first altered by photochemical etching to a predetermined pattern. The cadmium oxide is then sputtered onto the altered surface to form an intermediate layer to more tightly hold the dry lubricant, such as graphite.

Investigation of Phosphate-Containing Salt Melts as High-Temperature Inorganic Lubricants for Metallurgical Processes,

DTIC Science & Technology

The data obtained from the results of oscillographic investigations of the use of saline inorganic lubricants in the pilger mill rolling of steel...for experimental testing as lubricants in pilger mill pipe rolling. It is shown that with the use of the above developed compositions as high

Investigation of some characteristics of polyhydroxy milkweed triglycerides and their acylated derivatives in relation to lubricity

USDA-ARS?s Scientific Manuscript database

Most industrial lubricants are derived from non-renewable petroleum-based sources. As useful as these lubricants are, their unintended consequences are the pollution of our environment as a result of the very slow degradation of the spent materials. Native seed oils, on the other hand, are renewa...

Annual Report - Compatibility of ZDDP and ionic liquid anti-wear additives with hard coatings for engine lubrications

DOE Office of Scientific and Technical Information (OSTI.GOV)

Qu, Jun; Zhou, Yan; Leonard, Donovan N

The objectives for this considerations described here are to; investigate the compatibility of engine lubricant antiwear (AW) additives, specifically conventional zinc dialkyldithiophosphate (ZDDP) and newly developed ionic liquids (ILs), with selected commercial hard coatings, and provide fundamental understanding to guide future development of engine lubricants.

Journal bearing

DOEpatents

Menke, John R.; Boeker, Gilbert F.

1976-05-11

1. An improved journal bearing comprising in combination a non-rotatable cylindrical bearing member having a first bearing surface, a rotatable cylindrical bearing member having a confronting second bearing surface having a plurality of bearing elements, a source of lubricant adjacent said bearing elements for supplying lubricant thereto, each bearing element consisting of a pair of elongated relatively shallowly depressed surfaces lying in a cylindrical surface co-axial with the non-depressed surface and diverging from one another in the direction of rotation and obliquely arranged with respect to the axis of rotation of said rotatable member to cause a flow of lubricant longitudinally along said depressed surfaces from their distal ends toward their proximal ends as said bearing members are rotated relative to one another, each depressed surface subtending a radial angle of less than 360.degree., and means for rotating said rotatable bearing member to cause the lubricant to flow across and along said depressed surfaces, the flow of lubricant being impeded by the non-depressed portions of said second bearing surface to cause an increase in the lubricant pressure.

Fluid lubricated bearing assembly

DOEpatents

Boorse, Henry A.; Boeker, Gilbert F.; Menke, John R.

1976-01-01

1. A support for a loaded rotatable shaft comprising in combination on a housing having a fluid-tight cavity encasing an end portion of said shaft, a thrust bearing near the open end of said cavity for supporting the axial thrust of said shaft, said thrust bearing comprising a thrust plate mounted in said housing and a thrust collar mounted on said shaft, said thrust plate having a central opening the peripheral portion of which is hermetically sealed to said housing at the open end of said cavity, and means for supplying a fluid lubricant to said thrust bearing, said thrust bearing having a lubricant-conducting path connecting said lubricant supplying means with the space between said thrust plate and collar intermediate the peripheries thereof, the surfaces of said plate and collar being constructed and arranged to inhibit radial flow of lubricant and, on rotation of said thrust collar, to draw lubricant through said path between the bearing surfaces and to increase the pressure therebetween and in said cavity and thereby exert a supporting force on said end portion of said shaft.

Ciliary propulsion of objects in tubes: wall drag on swimming Tetrahymena (Ciliata) in the presence of mucin and other long-chain polymers.

PubMed

Winet, H

1976-04-01

The lubrication effect of three long-chain polymers - mucin, methylcellulose and Ficoll - on ciliary propulsion in tubes is measured by plotting the relative velocities of swimming cilitates as a function of the tube bore diameter. Mucin shows the most unequivocal lubrication, which is found at concentrations between 0% and 9.1% (w/v). This observation, coupled with viscometric measurements which show that ciliary tip shear rates are sufficient to solate mucin, serve as the groundwork for a model of mucin lubrication which explains the optimized lubrication behaviour of thixotropic gelating polymers as an expression of the response to shear by the various stages of polymer clustering during the gelatin process. In addition to the lubricative effect, another wall drag reduction effect by mucin was measured in the clearance region beyond the lubrication layer. This apparent viscosity reduction is optimized in the concentration range between I.7% and 4.I% mucin and may also be explained in terms of the properties of gel clustering.

Solid Lubrication Fundamentals and Applications. Chapter 6

NASA Technical Reports Server (NTRS)

Miyoshi, Kazuhisa

2000-01-01

This chapter focuses attention on the friction and wear properties of selected solid lubricating films to aid users in choosing the best lubricant, deposition conditions, and operational variables. For simplicity, discussion of the tribological properties of concern is separated into two parts. The first part of the chapter discusses the different solid lubricating films selected for study including commercially developed solid film lubricants: (1) bonded molybdenum disulfide (MoS2), (2) magnetron-sputtered MoS2, (3) ion-plated silver, (4) ion-plated lead, (5) magnetron-sputtered diamondlike carbon (MS DLC), and (6) plasma-assisted, chemical-vapor-deposited diamondlike carbon (PACVD DEC) films. Marked differences in the friction and wear properties of the different films resulted from the different environmental conditions (ultrahigh vacuum, humid air, and dry nitrogen) and the solid film lubricant materials. The second part of the chapter discusses the physical and chemical characteristics, friction behavior, and endurance life of the magnetron-sputtered MoS2 films. The role of interface species and the effects of applied load, film thickness, oxygen pressure, environment, and temperature on the friction and wear properties are considered.

Lubrication and wear mechanisms of polyimide-bonded graphite fluoride films subjected to low contact stress

NASA Technical Reports Server (NTRS)

Fusaro, R. L.

1980-01-01

The tribological properties of polyimide-bonded graphite fluoride films were studied with a pin-on-disk friction apparatus. A 440 C HT stainless steel rider with a 0.95 millimeter diameter flat area was slid against the film in order to achieve a light, closely controlled contact stress. A 1 kilogram load was applied to this flat to give a projected contact stress of 14 megapascals. Two stages of lubrication were operating. In the first stage, the film supported the load and the lubricating mechanism appeared to be the shear of a thin surface layer of the film between the rider and the bulk of the film. The second stage began after the original film was worn away, and the lubricating mechanism appeared to be the shear of very thin lubricant layers between the flat area on the rider and flat plateaus generated on the sandblasted asperities of the metallic substrate. The major difference between the lubricating mechanisms of the hemispherical and flat riders was that the flat wore through the film much more slowly than did the hemisphere.

An Electrochemical Processing Strategy for Improving Tribological Performance of Aisi 316 Stainless Steel Under Grease Lubrication

NASA Astrophysics Data System (ADS)

Zou, Jiaojuan; Li, Maolin; Lin, Naiming; Zhang, Xiangyu; Qin, Lin; Tang, Bin

2014-12-01

In order to improve the tribological performance of AISI 316 stainless steel (316 SS) under grease lubrication, electrochemical processing was conducted on it to obtain a rough (surface texturing-like) surface by making use of the high sensitivity of austenitic stainless steel to pitting corrosion in Cl--rich environment. Numerous corrosion pits or micro-ditches acted as micro-reservoirs on the obtained surface. While the grease could offer consistent lubrication, and then improve the tribological performance of 316 SS. Tribological behaviors of raw 316 SS and the treated sample were measured using a reciprocating type tribometer sliding against GCr15 steel counterpart under dry and grease lubrication conditions. The results showed that the mass losses of the two samples were in the same order of magnitude, and the raw sample exhibited lower friction coefficient in dry sliding. When the tests were conducted under grease lubrication condition, the friction coefficients and mass losses of the treated sample were far lower than those of the raw 316 SS. The tribological performance of 316 SS under grease lubrication was drastically improved after electrochemical processing.

Investigation of tribological properties of graphene oxide reinforced ultrahigh molecular weight polyethylene under artificial seawater lubricating condition

NASA Astrophysics Data System (ADS)

Pang, Wenchao; Ni, Zifeng; Wu, JiaLiang; Zhao, Yongwu

2018-03-01

A range of ultrahigh molecular weight polyethylene (UHMWPE)/graphene oxide (GO) nanocomposites were fabricated using liquid-phase ultrasonication mixing followed by hot-pressing. The wettability, water absorption and corrosion resistance of composites were studied to prove the composites were suitable for application in liquid environment. The tribological properties of composites under dry, deionized water and seawater lubricating condition were investigated. The results showed that the incorporation of GO decreased the wear rate of UHMWPE under different lubricating conditions and with the increase of GO addition, the wear rate of UHMWPE/GO composites decreased. UHMWPE/GO composites exhibited better tribological behaviors under seawater lubricating condition than other conditions, because good corrosion resistance and excellent wear resistance of UHMWPE/GO composites, and the lubricating effect of seawater is also indispensable.

A New Antiwear Additive/Surface Pretreatment for PFPE Liquid Lubricants

NASA Technical Reports Server (NTRS)

Morales, Wilfredo; Fusaro, Robert L.; Siebert, Mark; Keith, Theo; Jansen, Ralph; Herrera-Fierro, Pilar

1995-01-01

Pin-on-disk tribology experiments were conducted on a perfluoroalkylelher (PFPE) liquid lubricant with and without a new PFPE lubricant antiwear additive material, a silane. It was found that the silane provided moderate improvement in the antiwear performance of the PFPE lubricant when applied to the metallic surface as a surface coating or when added to the PFPE as a dispersion (emulsion). Slightly better results were obtained by using the combination of a surface coating and an emulsion of the silane. The silane emulsions or coatings did not affect the friction properties of the lubricant. Micro-Fourier transformation infrared (muFTIR) spectroscopy analysis was performed to study silane transfer films and the degradation of the PFPE. The silane was found to mitigate degradation of the PFPE which may have been the major reason for the improved antiwear performance observed.

Excellent lubricating behavior of Brasenia schreberi mucilage.

PubMed

Li, Jinjin; Liu, Yuhong; Luo, Jianbin; Liu, Pengxiao; Zhang, Chenhui

2012-05-22

The present work reports an excellent lubrication property of an aquatic plant called Brasenia schreberi (BS). To investigate the lubrication characteristics of the BS mucilage, a novel measuring system is designed, and an ultralow friction coefficient about 0.005 between the mucilage and glass surface has been obtained. It is found that the ultralow friction is closely related to the structure of mucilage and water molecules in the mucilage. The microstructure analysis indicates that the mucilage surrounding BS forms a kind of polysaccharide gel with many nanosheets. A possible lubrication mechanism is proposed that the formation of hydration layers among these polymer nanosheets with plenty of bonded water molecules causes the ultralow friction. The excellent lubrication property has a potential application for reducing the friction between a glossy pill coated with such layer of mucilage and people's throats.

Low torque hydrodynamic lip geometry for bi-directional rotation seals

DOEpatents

Dietle, Lannie L [Houston, TX; Schroeder, John E [Richmond, TX

2009-07-21

A hydrodynamically lubricating geometry for the generally circular dynamic sealing lip of rotary seals that are employed to partition a lubricant from an environment. The dynamic sealing lip is provided for establishing compressed sealing engagement with a relatively rotatable surface, and for wedging a film of lubricating fluid into the interface between the dynamic sealing lip and the relatively rotatable surface in response to relative rotation that may occur in the clockwise or the counter-clockwise direction. A wave form incorporating an elongated dimple provides the gradual convergence, efficient impingement angle, and gradual interfacial contact pressure rise that are conducive to efficient hydrodynamic wedging. Skewed elevated contact pressure zones produced by compression edge effects provide for controlled lubricant movement within the dynamic sealing interface between the seal and the relatively rotatable surface, producing enhanced lubrication and low running torque.

Low torque hydrodynamic lip geometry for rotary seals

DOEpatents

Dietle, Lannie L.; Schroeder, John E.

2015-07-21

A hydrodynamically lubricating geometry for the generally circular dynamic sealing lip of rotary seals that are employed to partition a lubricant from an environment. The dynamic sealing lip is provided for establishing compressed sealing engagement with a relatively rotatable surface, and for wedging a film of lubricating fluid into the interface between the dynamic sealing lip and the relatively rotatable surface in response to relative rotation that may occur in the clockwise or the counter-clockwise direction. A wave form incorporating an elongated dimple provides the gradual convergence, efficient impingement angle, and gradual interfacial contact pressure rise that are conducive to efficient hydrodynamic wedging. Skewed elevated contact pressure zones produced by compression edge effects provide for controlled lubricant movement within the dynamic sealing interface between the seal and the relatively rotatable surface, producing enhanced lubrication and low running torque.

Low torque hydrodynamic lip geometry for bi-directional rotation seals

DOEpatents

Dietle, Lannie L [Houston, TX; Schroeder, John E [Richmond, TX

2011-11-15

A hydrodynamically lubricating geometry for the generally circular dynamic sealing lip of rotary seals that are employed to partition a lubricant from an environment. The dynamic sealing lip is provided for establishing compressed sealing engagement with a relatively rotatable surface, and for wedging a film of lubricating fluid into the interface between the dynamic sealing lip and the relatively rotatable surface in response to relative rotation that may occur in the clockwise or the counter-clockwise direction. A wave form incorporating an elongated dimple provides the gradual convergence, efficient impingement angle, and gradual interfacial contact pressure rise that are conducive to efficient hydrodynamic wedging. Skewed elevated contact pressure zones produced by compression edge effects provide for controlled lubricant movement within the dynamic sealing interface between the seal and the relatively rotatable surface, producing enhanced lubrication and low running torque.

Minimum film thickness in elliptical contacts for different regimes of fluid-film lubrication

NASA Technical Reports Server (NTRS)

Hamrock, B. J.; Dowson, D.

1978-01-01

The film-parameter equations are provided for four fluid-film lubrication regimes found in elliptical contacts. These regimes are isoviscous-rigid; viscous-rigid; elastohydrodynamic of low-elastic-modulus materials, or isoviscous-elastic; and elastohydrodynamic, or viscous-elastic. The influence or lack of influence of elastic and viscous effects is the factor that distinguishes these regimes. The film-parameter equations for the respective regimes come from earlier theoretical studies by the authors on elastohydrodynamic and hydrodynamic lubrication of elliptical conjunctions. These equations are restated and the results are presented as a map of the lubrication regimes, with film-thickness contours on a log-log grid of the viscosity and elasticity parameters for five values of the ellipticity parameter. The results present a complete theoretical film-parameter solution for elliptical contacts in the four lubrication regimes.

Oleoplaning droplets on lubricated surfaces

NASA Astrophysics Data System (ADS)

Daniel, Dan; Timonen, Jaakko V. I.; Li, Ruoping; Velling, Seneca J.; Aizenberg, Joanna

2017-10-01

Recently, there has been much interest in using lubricated surfaces to achieve extreme liquid repellency: a foreign droplet immiscible with the underlying lubricant layer was shown to slide off at a small tilt angle <5°. This behaviour was hypothesized to arise from a thin lubricant overlayer film sandwiched between the droplet and solid substrate, but this has not been observed experimentally. Here, using thin-film interference, we are able to visualize the intercalated film under both static and dynamic conditions. We further demonstrate that for a moving droplet, the film thickness follows the Landau-Levich-Derjaguin law. The droplet is therefore oleoplaning--akin to tyres hydroplaning on a wet road--with minimal dissipative force and no contact line pinning. The techniques and insights presented in this study will inform future work on the fundamentals of wetting for lubricated surfaces and enable their rational design.

Solid lubrication design methodology

NASA Technical Reports Server (NTRS)

Aggarwal, B. B.; Yonushonis, T. M.; Bovenkerk, R. L.

1984-01-01

A single element traction rig was used to measure the traction forces at the contact of a ball against a flat disc at room temperature under combined rolling and sliding. The load and speed conditions were selected to match those anticipated for bearing applications in adiabatic diesel engines. The test program showed that the magnitude of traction forces were almost the same for all the lubricants tested; a lubricant should, therefore, be selected on the basis of its ability to prevent wear of the contact surfaces. Traction vs. slide/roll ratio curves were similar to those for liquid lubricants but the traction forces were an order of magnitude higher. The test data was used to derive equations to predict traction force as a function of contact stress and rolling speed. Qualitative design guidelines for solid lubricated concentrated contacts are proposed.

Compatibility of refrigerants and lubricants with elastomers. Final report

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hamed, G.R.; Seiple, R.H.; Taikum, Orawan

1994-01-01

The information contained in this report is designed to assist the air-conditioning and refrigeration industry in the selection of suitable elastomeric gasket and seal materials that will prove useful in various refrigerant and refrigeration lubricant environments. In part I of the program the swell behavior in the test fluids has been determined using weight and in situ diameter measurements for the refrigerants and weight, diameter and thickness measurements for the lubricants. Weight and diameter measurements are repeated after 2 and 24 hours for samples removed fro the refrigerant test fluids and 24 hours after removal from the lubricants. Part IImore » of the testing program includes the evaluation of tensile strength, hardness, weight, and dimensional changes after immersion aging in refrigerant/lubricant mixtures of selected elastomer formulations at elevated temperature and pressure.« less

The filling of powdered herbs into two-piece hard capsules using hydrogenated cotton seed oil as lubricant.

PubMed

Aling, Joanna; Podczeck, Fridrun

2012-11-20

The aim of this work was to investigate the plug formation and filling properties of powdered herbal leaves using hydrogenated cotton seed oil as an alternative lubricant. In a first step, unlubricated and lubricated herbal powders were studied on a small scale using a plug simulator, and low-force compression physics and parameterization techniques were used to narrow down the range in which the optimum amount of lubricant required would be found. In a second step these results were complemented with investigations into the flow properties of the powders based on packing (tapping) experiments to establish the final optimum lubricant concentration. Finally, capsule filling of the optimum formulations was undertaken using an instrumented tamp filling machine. This work has shown that hydrogenated cotton seed oil can be used advantageously for the lubrication of herbal leaf powders. Stickiness as observed with magnesium stearate did not occur, and the optimum lubricant concentration was found to be less than that required for magnesium stearate. In this work, lubricant concentrations of 1% or less hydrogenated cotton seed oil were required to fill herbal powders into capsules on the instrumented tamp-filling machine. It was found that in principle all powders could be filled successfully, but that for some powders the use of higher compression settings was disadvantageous. Relationships between the particle size distributions of the powders, their flow and consolidation as well as their filling properties could be identified by multivariate statistical analysis. The work has demonstrated that a combination of the identification of plug formation and powder flow properties is helpful in establishing the optimum lubricant concentration required using a small quantity of powder and a powder plug simulator. On an automated tamp-filling machine, these optimum formulations produced satisfactory capsules in terms of coefficient of fill weight variability and capsule weight. Copyright © 2012 Elsevier B.V. All rights reserved.

Effect of viscosity on rolling-element fatigue life at cryogenic temperature with fluorinated ether lubricants

NASA Technical Reports Server (NTRS)

Dietrich, M. W.; Zaretsky, E. V.

1975-01-01

Rolling-element fatigue tests were conducted with 12.7-mm-(1/2-in.-) diameter AISI 52100 steel balls in the NASA five-ball fatigue tester, with a maximum hertz stress of 5500 mN/m2 (800 000 psi), a shaft speed of 4750 rpm, lubricant temperature of 200 K (360 R), a contact angle of 20 deg, using four fluorinated ether lubricants of varying viscosities. No statistically significant differences in rolling-element fatigue life occurred using the four viscosity levels. Elastohydrodynamic calculations indicate that values of the lubricant film parameter were approximately 2 or greater.

Fluorescence excitation-emission matrix spectroscopy for degradation monitoring of machinery lubricants

NASA Astrophysics Data System (ADS)

Sosnovski, Oleg; Suresh, Pooja; Dudelzak, Alexander E.; Green, Benjamin

2018-02-01

Lubrication oil is a vital component of heavy rotating machinery defining the machine's health, operational safety and effectiveness. Recently, the focus has been on developing sensors that provide real-time/online monitoring of oil condition/lubricity. Industrial practices and standards for assessing oil condition involve various analytical methods. Most these techniques are unsuitable for online applications. The paper presents the results of studying degradation of antioxidant additives in machinery lubricants using Fluorescence Excitation-Emission Matrix (EEM) Spectroscopy and Machine Learning techniques. EEM Spectroscopy is capable of rapid and even standoff sensing; it is potentially applicable to real-time online monitoring.

GRAPHITE EXTRUSIONS

DOEpatents

Benziger, T.M.

1959-01-20

A new lubricant for graphite extrusion is described. In the past, graphite extrusion mixtures have bcen composed of coke or carbon black, together with a carbonaceous binder such as coal tar pitch, and a lubricant such as petrolatum or a colloidal suspension of graphite in glycerin or oil. Sinee sueh a lubricant is not soluble in, or compatible with the biiider liquid, such mixtures were difficult to extrude, and thc formed pieees lacked strength. This patent teaches tbe use of fatty acids as graphite extrusion lubricants and definite improvemcnts are realized thereby since the fatty acids are soluble in the binder liquid.

The effect of load in a contact with boundary lubrication. [reduction of coefficient of friction

NASA Technical Reports Server (NTRS)

Georges, J. M.; Lamy, B.; Daronnat, M.; Moro, S.

1978-01-01

The effect of the transition load on the wear in a contact with boundary lubrication was investigated. An experimental method was developed for this purpose, and parameters affecting the boundary lubrication under industrial operating conditions were identified. These parameters are the adsorbed boundary film, the contact microgeometry (surface roughness), macrogeometry, and hardness of materials used. It was found that the curve of the tops of the surface protrustion affect the transition load, and thus the boundary lubrication. The transition load also depends on the chemical nature of the contact and its geometrical and mechanical aspects.

Tribometer for Lubrication Studies in Vacuum

NASA Technical Reports Server (NTRS)

Pepper, Stephen V.

1998-01-01

The NASA Lewis Research Center has developed a new way to evaluate the liquid lubricants used in ball bearings in space mechanisms. For this evaluation, a liquid lubricant is exercised in the rolling contact vacuum tribometer shown in the photo. This tribometer, which is essentially a thrust bearing with three balls and flat races, has contact stresses similar to those in a typical preloaded, angular contact ball bearing. The rotating top plate drives the balls in an outward-winding spiral orbit instead of a circular path. Upon contact with the "guide plate," the balls are forced back to their initial smaller orbit radius; they then repeat this spiral orbit thousands of times. The orbit rate of the balls is low enough, 2 to 5 rpm, to allow the system to operate in the boundary lubrication regime that is most stressful to the liquid lubricant. This system can determine the friction coefficient, lubricant lifetime, and species evolved from the liquid lubricant by tribodegradation. The lifetime of the lubricant charge is only few micrograms, which is "used up" by degradation during rolling. The friction increases when the lubricant is exhausted. The species evolved by the degrading lubricant are determined by a quadrupole residual gas analyzer that directly views the rotating elements. The flat races (plates) and 0.5-in.-diameter balls are of a configuration and size that permit easy post-test examination by optical and electron microscopy and the full suite of modern surface and thin-film chemical analytical techniques, including infrared and Raman microspectroscopy and x-ray photoelectron spectroscopy. In addition, the simple sphere-on-a-flat-plate geometry allows an easy analysis of the contact stresses at all parts of the ball orbit and an understanding of the frictional energy losses to the lubricant. The analysis showed that when the ball contacts the guide plate, gross sliding occurs between the ball and rotating upper plate as the ball forced back to a smaller orbit radius. The friction force due to gross sliding is sensed by the piezoelectric force transducer behind the guide plate and furnishes the coefficient of friction for the system. This tribometer has been used to determine the relative lifetimes of Fomblin Z-25, a lubricant often used in space mechanisms, as a function of the material of the plates against which it was run. The balls were 440C steel in all cases; the plate materials were aluminum, chromium (Cr), 440C steel (17 wt % Cr), and 4150 steel (1 wt % Cr). As shown in the bar graph, the lifetime is greatest for the plate material with least chromium, thus implicating chromium as a tribochemically active element attacking Fomblin Z-25.

Comparison of life cycle emissions and energy consumption for environmentally adapted metalworking fluid systems.

PubMed

Clarens, Andres F; Zimmerman, Julie B; Keoleian, Greg A; Hayes, Kim F; Skerlos, Steven J

2008-11-15

A number of environmentally adapted lubricants have been proposed in response to the environmental and health impacts of metalworking fluids (MWFs). The alternatives typically substitute petroleum with vegetable-based components and/or deliver minimum quantities of lubricant in gas rather than water, with the former strategy being more prevalent than the latter. A comparative life cycle assessment of water- and gas-based systems has shown that delivery of lubricants in air rather than water can reduce solid waste by 60%, water use by 90%, and aquatic toxicity by 80%, while virtually eliminating occupational health concerns. However, air-delivery of lubricants cannot be used for severe machining operations due to limitations of cooling and lubricant delivery. For such operations, lubricants delivered in supercritical carbon dioxide (scCO2) are effective while maintaining the health and environmental advantages of air-based systems. Although delivery conditions were found to significantly influence the environmental burdens of all fluids, energy consumption was relatively constant under expected operating conditions. Global warming potential (GWP) increased when delivering lubricants in gas rather than water though all classes of MWFs have low GWP compared with other factory operations. It is therefore concluded that the possibility of increased GWP when switching to gas-based MWFs is a reasonable tradeoff for definite and large reductions in aquatic toxicity, water use, solid waste, and occupational health risks.

Ion Implantation of Perfluoropolyether-Lubricated Surfaces for Improved Tribological Performance

NASA Technical Reports Server (NTRS)

Shogrin, Brad

1998-01-01

For over 30 years, perfluoropolyethers (PFPE's) have been the liquid lubricants of choice for space applications because of their proven tribological performance and desirable properties, such as low vapor pressure and a wide liquid temperature range. These oils are used in such space mechanisms as gyroscopes, scanning mirrors, actuators, and filter wheels. In the past few years, there have been several incidents during which PFPE-lubricated space mechanisms have shown anomalous behavior. These anomalies are thought to be the result of PFPE degradation. Investigative research focused on understanding and modeling the degradation of PFPE lubricants has shown that PFPE's degrade and lose their desirable properties while under boundary-lubricated, sliding/rolling contacts and at elevated temperatures. These performance deficiencies are strongly dependent on the surface chemistry and reactivity of the lubricated contacts, which dictate the formation of harmful catalytic by-products. One way to inhibit tribo-induced degradation may be to use passivated surfaces that do not promote the formation of harmful by-products. Such a passivated surface would inhibit PFPE degradation and increase the lifetime of the lubricated mechanism. Ion implantation is one such passivation technique. This surface-treatment technique can modify the surface properties of materials without affecting either the properties or dimensions of the bulk material beneath the treated layer. By introducing a foreign species into a submicron surface layer, ion implantation can induce unique surface microstructures.

In-situ, On-demand Lubrication System for Space Mechanisms

NASA Technical Reports Server (NTRS)

Marchetti, Mario; Jones, William R., Jr.; Pepper, Stephen V.; Jansen, Mark J.; Predmore, Roamer E.

2002-01-01

Many of today's spacecraft have long mission lifetimes. Whatever the lubrication method selected, the initial lubricant charge is required to last the entire mission. Fluid lubricant losses are mainly due to evaporation, tribo-degradation, and oil creep out of the tribological regions. In the past, several techniques were developed to maintain the appropriate amount of oil in the system. They were based on oil reservoirs (cartridges, impregnated porous parts), barrier films, and labyrinth seals. Nevertheless, all these systems have had limited success or have not established a proven record for space missions. The system reported here provides to the ball-race contact fresh lubricant in-situ and on demand. The lubricant is stored in a porous cartridge attached to the inner or the outer ring of a ball bearing. The oil is released by heating the cartridge to eject oil, taking advantage of the greater thermal expansion of the oil compared to the porous network. The heating may be activated by torque increases that signal the depletion of oil in the contact. The low surface tension of the oil compared to the ball bearing material is utilized and the close proximity of the cartridge to the moving balls allows the lubricant to reach the ball-race contacts. This oil resupply system can be used to avoid a mechanism failure or reduce torque to an acceptable level and extend the life of the component.

Tooth wear prevention: a quantitative and qualitative in vitro study.

PubMed

Kaidonis, J A; Gratiaen, J; Bhatia, N; Richards, L C; Townsend, G C

2003-03-01

Management of tooth wear from grinding presents a significant clinical challenge. Acrylic nightguards are often used to protect the teeth, but many patients still grind with these appliances. This study aimed to test the effectiveness of three lubricants in reducing enamel wear by using an electro-mechanical machine under controlled conditions, with a view to undertaking a subsequent longitudinal clinical study. Sectioned tooth specimens were worn against each other under different loads and with the addition of three different lubricants: calcium fluoride (CaF) powder, olive-oil, and a combination of calcium fluoride with olive-oil in the form of a slurry. Wear rates of enamel only were quantified by weighing the specimens, and resin replicas of the worn tooth surfaces were made for examination under a scanning electron microscope. All three lubricants reduced the amount of enamel wear significantly compared with wearing specimens without adding lubricants. Wear rate was influenced by the type of lubricant and the load applied. Wear rates were significantly less for olive-oil and the olive-oil/CaF slurry compared with CaF alone. The microwear detail differed between the three lubricants. This study has shown that enamel wear can be reduced using dry or wet lubricants between opposing teeth that are worn under controlled conditions. Further research is required to clarify their possible clinical applications.

49 CFR 230.55 - Tubular type water and lubricator glasses and shields.

Code of Federal Regulations, 2010 CFR

2010-10-01

... 49 Transportation 4 2010-10-01 2010-10-01 false Tubular type water and lubricator glasses and... STANDARDS Boilers and Appurtenances Water Glasses and Gauge Cocks § 230.55 Tubular type water and lubricator glasses and shields. (a) Water glasses. Tubular type water glasses shall be renewed at each 92 service day...

A review of liquid lubricant thermal/oxidative degradation

NASA Technical Reports Server (NTRS)

Jones, W. R., Jr.

1983-01-01

The fundamental processes occurring during the thermal and oxidative degradation of hydrocarbons are reviewed. Particular emphasis is given to various classes of liquid lubricants such as mineral oils, esters, polyphenyl ethers, C-ethers, and fluorinated polyethers. Experimental techniques for determining thermal and oxidative stabilities of lubricants are discussed. The role of inhibitors and catalysis is also covered.

Evaluation of Future Fuels in a High Pressure Common Rail System. Part 3. John Deere 4.5L Powertech Plus

DTIC Science & Technology

2013-01-01

within the fuel injectors regardless of viscosity or lubricity levels. 15. SUBJECT TERMS Fuel Lubricity, Viscosity, HPCR, Synthetic Jet Fuel, Denso... injectors regardless of viscosity or lubricity levels. UNCLASSIFIED v UNCLASSIFIED FOREWORD/ACKNOWLEDGMENTS The U.S. Army TARDEC...40 3.10 UPPER INJECTOR CONNECTING PIN

Experimental Investigations to Enhance the Tribological Performance of Engine Oil by Using Nano-Boric Acid and Functionalized Multiwalled Carbon Nanotubes: A Comparative Study to Assess Wear in Bronze Alloy

NASA Astrophysics Data System (ADS)

Ajay Vardhaman, B. S.; Amarnath, M.; Ramkumar, J.; Rai, Prabhat K.

2018-04-01

In various mechanical systems, lubricants are generally used to reduce friction and wear; thus, the total energy loss in the mechanical systems can be minimized by the proper enhancement of lubrication properties. In general, friction modifiers and antiwear additives are used to improve the tribological properties of the lubricant. However, the use of these additives has to be phased out due to their fast chemical degradation in their applications and other environmental issues. In recent years, the use of nanoparticles as a potential lubricant additive has received considerable attention because of its excellent mechanical and tribological characteristics. The present work describes the tribological behavior of nano-boric acid, multiwalled carbon nanotubes (MWCNTs), and functionalized multiwalled carbon nanotubes (FMWCNTs) modified with carboxylic acid. These nanoparticles were used to enhance the tribological properties of engine oil (SAE20W40) used to lubricate bronze alloy samples. The performance of these nano-coolants was assessed on a linear reciprocating ball-on-flat tribometer. Results highlight the friction and wear behavior of the nano-boric acid, MWCNTs, and FMWCNTs under three varying parameters such as the effect of nanoparticles concentration, load-carrying capacity, and sliding speed. The addition of nano-boric acid, MWCNTs, and FMWCNTs has significantly improved the tribological properties of the base lubricant. The addition of 0.5 wt.% of nano-boric acid, MWCNTs, and FMWCNTs to the base lubricant has decreased the coefficient of friction by 19.76, 30.55, and 35.65%, respectively, and a significant reduction in wear volume by 55.17, 71.42, and 88.97% was obtained in comparison with base lubricant.

Observations of Spacecraft Bearing Lubricant Redistribution Based on Thermal Conductance Measurements

NASA Technical Reports Server (NTRS)

Takeuchi, Yoshimi R.; Frantz, Peter P.; Hilton, Michael R.

2014-01-01

The performance and life of precision ball bearings are critically dependent on maintaining a quantity of oil at the ball/race interface that is sufficient to support a robust protective film. In space applications, where parched conditions are intentionally the norm, harsh operating conditions can displace the small reserves of oil, resulting in reduced film thickness and premature wear. In the past, these effects have proven difficult to model or to measure experimentally. This paper describes a study addressing this challenge, where bearing thermal conductance measurements are employed to infer changes in lubricant quantity at the critical rolling interfaces. In the first part of the paper, we explain how the lubricant's presence and its quantity impacts bearing thermal conductance measurements. For a stationary bearing, we show that conductance is directly related to the lubricant quantity in the ball/race contacts. Hence, aspects of bearing performance related to oil quantity can be understood and insights improved with thermal conductance data. For a moving bearing, a different mechanism of heat transfer dominates and is dependent on lubricant film thickness on the ball. In the second part of the report, we discuss lubricant quantity observations based on bearing thermal conductance measurements. Lubricant quantity, and thus bearing thermal conductance, depends on various initial and operating conditions and is impacted further by the run-in process. A significant effect of maximum run-in speed was also observed, with less oil remaining after obtaining higher speeds. Finally, we show that some of the lubricant that is displaced between the ball and race during run-in operation can be recovered during rest, and we measure the rate of recovery for one example.

Mechanism of Antiwear Property Under High Pressure of Synthetic Oil-Soluble Ultrathin MoS2 Sheets as Lubricant Additives.

PubMed

Chen, Zhe; Liu, Yuhong; Gunsel, Selda; Luo, Jianbin

2018-01-30

Wear occurs between two rubbing surfaces. Severe wear due to seizure under high pressure leads to catastrophic failures of mechanical systems and raises wide concerns. In this paper, a kind of synthetic oil-soluble ultrathin MoS 2 sheets is synthesized and investigated as lubricant additives between steel surfaces. It is found that, with the ultrathin MoS 2 sheets, the wear can be controlled under the nominal pressure of about 1 GPa, whereas the bearable nominal pressure for traditional lubricants is only a few hundred megapascals. It is found that when wear is under control, the real pressure between the asperities agrees with the breaking strength of ultrathin MoS 2 . Therefore, it is believed that, because of the good oil solubility and ultrasmall thickness, the ultrathin MoS 2 sheets can easily enter the contact area between the contacting asperities. Then, the localized seizure and further wear are prevented because there will be no metal-to-metal contact as long as the real pressure between the asperities is below the breaking strength of ultrathin MoS 2 . In this way, the upper limit pressure the lubricant can work is dependent on the mechanical properties of the containing ultrathin two-dimensional (2D) sheets. Additionally, ultrathin MoS 2 sheets with various lateral sizes are compared, and it is found that sheets with a larger size show better lubrication performance. This work discovers the lubrication mechanism of ultrathin MoS 2 sheets as lubricant additives and provides an inspiration to develop a novel generation of lubricant additives with high-strength ultrathin 2D materials.

Synthesis of monodispersed ZnAl{sub 2}O{sub 4} nanoparticles and their tribology properties as lubricant additives

DOE Office of Scientific and Technical Information (OSTI.GOV)

Song, Xiaoyun; Zheng, Shaohua; Zhang, Jun

Graphical abstract: Display Omitted Highlights: ► The preparation of ZnAl{sub 2}O{sub 4} nanoparticles was realized by hydrothermal method. ► After surface modification, ZnAl{sub 2}O{sub 4} nanoparticles of narrow size distribution can disperse in lubricating oil stably. ► The modified ZnAl{sub 2}O{sub 4} nanoparticles as lubricating oil additives exhibit good tribology properties. -- Abstract: Monodispersed spherical zinc aluminate spinel (ZnAl{sub 2}O{sub 4}) nanoparticles were synthesized via a solvothermal method and modified by oleic acid in cyclohexanol solution. The nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and infrared spectrum (IR). The dispersion ability of nanoparticles in lubricant oilmore » was measured with optical absorbance spectrum. The results show that the modified nanoparticles are nearly monodispersed and can stably disperse in lubricant oil. The tribological properties of the ZnAl{sub 2}O{sub 4} nanoparticles as an additive in lubricant oil were evaluated with four-ball test and thrust-ring test. For comparison, ZnO and Al{sub 2}O{sub 3} nanoparticles as additive in lubricant oil were also tested respectively. The results show that ZnAl{sub 2}O{sub 4} nanoparticles exhibit better tribology properties in terms of anti-wear and anti-friction than ZnO or Al{sub 2}O{sub 3} nanoparticles. The anti-friction and anti-wear mechanisms were discussed and the lubricating effect of ZnAl{sub 2}O{sub 4} nanoparticles can be attributed to nano-bearings effect and tribo-sintering mechanism.« less

High Temperature Solid Lubricant Materials for Heavy Duty and Advanced Heat Engines

NASA Technical Reports Server (NTRS)

Dellacorte, C.; Wood, J. C.

1994-01-01

Advanced engine designs incorporate higher mechanical and thermal loading to achieve efficiency improvements. This approach often leads to higher operating temperatures of critical sliding elements (e.g. piston ring/cylinder wall contacts and valve guides) which compromise the use of conventional and even advanced synthetic liquid lubricants. For these applications solid lubricants must be considered. Several novel solid lubricant composites and coatings designated PS/PM200 have been employed to dry and marginally oil lubricated contacts in advanced heat engines. These applications include cylinder kits of heavy duty diesels, and high temperature Stirling engines, sidewall seals of rotary engines, and various exhaust valve and exhaust component applications. This paper describes the tribological and thermophysical properties of these tribomaterials and reviews the results of applying them to engine applications. Other potential tribological materials and applications are also discussed with particular emphasis on heavy duty and advanced heat engines.

Thermal Behavior of Aerospace Spur Gears in Normal and Loss-of-Lubrication Conditions

NASA Technical Reports Server (NTRS)

Handschuh, Robert F.

2015-01-01

Testing of instrumented spur gears operating at aerospace rotorcraft conditions was conducted. The instrumented gears were operated in a normal and in a loss-of-lubrication environment. Thermocouples were utilized to measure the temperature at various locations on the test gears and a test utilized a full-field, high-speed infrared thermal imaging system. Data from thermocouples was recorded during all testing at 1 hertz. One test had the gears shrouded and a second test was run without the shrouds to permit the infrared thermal imaging system to take data during loss-of-lubrication operation. Both tests using instrumented spur gears were run in normal and loss-of-lubrication conditions. Also the result from four other loss-of-lubrication tests will be presented. In these tests two different torque levels were used while operating at the same rotational speed (10000 revolutions per minute).

Thermal Behavior of Aerospace Spur Gears in Normal and Loss-of-Lubrication Conditions

NASA Technical Reports Server (NTRS)

Handschuh, Robert F.

2015-01-01

Testing of instrumented spur gears operating at aerospace rotorcraft conditions was conducted. The instrumented gears were operated in a normal and in a loss-of-lubrication environment. Thermocouples were utilized to measure the temperature at various locations on the test gears and a test utilized a full-field, high-speed infrared thermal imaging system. Data from thermocouples was recorded during all testing at 1 Hz. One test had the gears shrouded and a second test was run without the shrouds to permit the infrared thermal imaging system to take date during loss-of-lubrication operation. Both tests using instrumented spur gears were run in normal and loss-of-lubrication conditions. Also the result from four other loss-of-lubrication tests will be presented. In these tests two different torque levels were used while operating at the same rotational speed (10000 rpm).

A shear localization mechanism for lubricity of amorphous carbon materials

PubMed Central

Ma, Tian-Bao; Wang, Lin-Feng; Hu, Yuan-Zhong; Li, Xin; Wang, Hui

2014-01-01

Amorphous carbon is one of the most lubricious materials known, but the mechanism is not well understood. It is counterintuitive that such a strong covalent solid could exhibit exceptional lubricity. A prevailing view is that lubricity of amorphous carbon results from chemical passivation of dangling bonds on surfaces. Here we show instead that lubricity arises from shear induced strain localization, which, instead of homogeneous deformation, dominates the shearing process. Shear localization is characterized by covalent bond reorientation, phase transformation and structural ordering preferentially in a localized region, namely tribolayer, resulting in shear weakening. We further demonstrate an anomalous pressure induced transition from stick-slip friction to continuous sliding with ultralow friction, due to gradual clustering and layering of graphitic sheets in the tribolayer. The proposed shear localization mechanism sheds light on the mechanism of superlubricity, and would enrich our understanding of lubrication mechanism of a wide variety of amorphous materials. PMID:24412998

Liquid crystals in tribology.

PubMed

Carrión, Francisco-José; Martínez-Nicolás, Ginés; Iglesias, Patricia; Sanes, José; Bermúdez, María-Dolores

2009-09-18

Two decades ago, the literature dealing with the possible applications of low molar mass liquid crystals, also called monomer liquid crystals (MLCs), only included about 50 references. Today, thousands of papers, conference reports, books or book chapters and patents refer to the study and applications of MLCs as lubricants and lubricant additives and efforts are made to develop new commercial applications. The development of more efficient lubricants is of paramount technological and economic relevance as it is estimated that half the energy consumption is dissipated as friction. MLCs have shown their ability to form ordered boundary layers with good load-carrying capacity and to lower the friction coefficients, wear rates and contact temperature of sliding surfaces, thus contributing to increase the components service life and to save energy. This review includes the use of MLCs in lubrication, and dispersions of MLCs in conventional polymers (PDMLCs). Finally, new lubricating system composed of MLC blends with surfactants, ionic liquids or nanophases are considered.

Nitinol 60 as a Material For Spacecraft Triboelements

NASA Technical Reports Server (NTRS)

Pepper, Stephen V.; DellaCorte, Christopher; Noebe, Ronald D.; Hall, David R.; Glennon, Glenn

2009-01-01

The mechanical properties of Nitinol 60, 60 w/o Ni, 40 w/oTi (55 a/o Ni, 45 a/o Ti) are sufficiently attractive to warrant its consideration as a lubricated spacecraft triboelement. The ability to lubricate Nitinol 60 by the oils usually used on spacecraft mechanisms--Pennzane 2001A, Krytox 143AC and Castrol 815Z - was experimentally determined. These oils were run in the boundary lubrication regime for Nitinol 60 balls running against a 440C steel counterface in the vacuum spiral orbit tribometer. Test results consisting of the coefficient of friction versus time (friction traces) and relative degradation rates are presented. Contrary to the inability to successfully lubricate other metal alloys with high titanium content, it was found that Nitinol 60 is able to be lubricated by these oils. Overall, the results presented here indicate that Nitinol 60 is a credible candidate material for spacecraft bearing applications.

Liquid Crystals in Tribology

PubMed Central

Carrión, Francisco-José; Martínez-Nicolás, Ginés; Iglesias, Patricia; Sanes, José; Bermúdez, María-Dolores

2009-01-01

Two decades ago, the literature dealing with the possible applications of low molar mass liquid crystals, also called monomer liquid crystals (MLCs), only included about 50 references. Today, thousands of papers, conference reports, books or book chapters and patents refer to the study and applications of MLCs as lubricants and lubricant additives and efforts are made to develop new commercial applications. The development of more efficient lubricants is of paramount technological and economic relevance as it is estimated that half the energy consumption is dissipated as friction. MLCs have shown their ability to form ordered boundary layers with good load-carrying capacity and to lower the friction coefficients, wear rates and contact temperature of sliding surfaces, thus contributing to increase the components service life and to save energy. This review includes the use of MLCs in lubrication, and dispersions of MLCs in conventional polymers (PDMLCs). Finally, new lubricating system composed of MLC blends with surfactants, ionic liquids or nanophases are considered. PMID:19865534

Aviation-fuel lubricity evaluation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Not Available

1988-07-01

Fuel-system components have experienced problems with the slipperiness or lubricity of the fuel back to the early 1960's. As a consequence of the level of refinement necessary for the PWA 523 fuel (now designated MIL-T-38219 grade JP-7) to obtain its high-temperature stability, many of the polar compounds contributing to lubricity had been removed, resulting in abnormal hydraulic fuel-pump wear. A lubricity-enhancing compound was developed (PWA 536) to eliminate the wear problem. High-pressure piston-type fuel pumps were one of the first parts of the engine fuel system to exhibit problems related to fuel properties. One early problem manifested itself as corrosionmore » of silver-plated slipper pads and was related to carryover of residual-chlorides fuel. Fuel controls were another part of the engine fuel system susceptible to fuel properties. Lack of lubricity agents caused fuel control sliding servo valves to stick.« less

Pressure-dependent surface viscosity and its surprising consequences in interfacial lubrication flows

NASA Astrophysics Data System (ADS)

Manikantan, Harishankar; Squires, Todd M.

2017-02-01

The surface shear rheology of many insoluble surfactants depends strongly on the surface pressure (or concentration) of that surfactant. Here we highlight the dramatic consequences that surface-pressure-dependent surface viscosities have on interfacially dominant flows, by considering lubrication-style geometries within high Boussinesq (Bo) number flows. As with three-dimensional lubrication, high-Bo surfactant flows through thin gaps give high surface pressures, which in turn increase the local surface viscosity, further amplifying lubrication stresses and surface pressures. Despite their strong nonlinearity, the governing equations are separable, so that results from two-dimensional Newtonian lubrication analyses may be immediately adapted to treat surfactant monolayers with a general functional form of ηs(Π ) . Three paradigmatic systems are analyzed to reveal qualitatively new features: a maximum, self-limiting value for surfactant fluxes and particle migration velocities appears for Π -thickening surfactants, and kinematic reversibility is broken for the journal bearing and for suspensions more generally.

Vapor-liquid equilibria for an R134a/lubricant mixture: Measurements and equation-of-state modeling

DOE Office of Scientific and Technical Information (OSTI.GOV)

Huber, M.L.; Holcomb, C.D.; Outcalt, S.L.

2000-07-01

The authors measured bubble point pressures and coexisting liquid densities for two mixtures of R-134a and a polyolester (POE) lubricant. The mass fraction of the lubricant was approximately 9% and 12%, and the temperature ranged from 280 K to 355 K. The authors used the Elliott, Suresh, and Donohue (ESD) equation of state to model the bubble point pressure data. The bubble point pressures were represented with an average absolute deviation of 2.5%. A binary interaction parameter reduced the deviation to 1.4%. The authors also applied the ESD model to other R-134a/POE lubricant data in the literature. As the concentrationmore » of the lubricant increased, the performance of the model deteriorated markedly. However, the use of a single binary interaction parameter reduced the deviations significantly.« less

An Experimental Investigation of the Influence of the Lubricant Viscosity and Additives on Gear Wear

NASA Technical Reports Server (NTRS)

Krantz, Timothy L.; Kahraman, Ahmet

2005-01-01

The influence of lubricant viscosity and additives on the average wear rate of spur gear pairs was investigated experimentally. The gear specimens of a comprehensive gear durability test program that made use of seven lubricants covering a range of viscosities were examined to measure gear tooth wear. The measured wear was related to the as-manufactured surface roughness, the elastohydrodynamic film thickness, and the experimentally determined contact fatigue lives of the same specimens. In general, the wear rate was found to be inversely proportional to the viscosity of the lubricant and to the lambda ratio (also sometimes called the specific film thickness). The data also show an exponential trend between the average wear rates and the surface fatigue lives. Lubricants with similar viscosities but differing additives and compositions had somewhat differing gear surface fatigue lives and wear rates.

Analysis of fluid film lubrication in artificial hip joint replacements with surfaces of high elastic modulus.

PubMed

Jin, Z M; Dowson, D; Fisher, J

1997-01-01

Lubrication mechanisms and contact mechanics have been analysed for total hip joint replacements made from hard bearing surfaces such as metal-on-metal and ceramic-on-ceramic. A similar analysis for ultra-high molecular weight polyethylene (UHMWPE) against a hard bearing surface has also been carried out and used as a reference. The most important factor influencing the predicted lubrication film thickness has been found to be the radial clearance between the ball and the socket. Full fluid film lubrication may be achieved in these hard/hard bearings provided that the surface finish of the bearing surface and the radial clearance are chosen correctly and maintained. Furthermore, there is a close relation between the predicted contact half width and the predicted lubrication film thickness. Therefore, it is important to analyse the contact mechanics in artificial hip joint replacements. Practical considerations of manufacturing these bearing surfaces have also been discussed.

Impact of lubricant parameters on rotary instrument torque and force.

PubMed

Boessler, Claudia; Peters, Ove A; Zehnder, Matthias

2007-03-01

In the current study, the impact of lubricant parameters on simulated root canal instrumentation was investigated. Using size 30 ProFile .06 instruments in milled artificial root canals in human dentin, the effects of sodium hypochlorite (1% NaOCl) and a chelator (18% etidronic acid) in aqueous irrigants on maximum torque, full torsional load, and maximum force values were gauged using a torque testing platform. Furthermore, the impact of the time a chelating lubricant was exposed to dentin as well as its galenic form (aqueous vs. gel-type) on the above outcome variables was evaluated. Aqueous lubricants significantly (p < 0.05, ANOVA, Newman-Keuls) reduced all outcome variables compared to dry conditions. The incorporation of a chelator further reduced these values (p < 0.05), whereas hypochlorite behaved similar to water. The chelator effect was immediate and did not increase with time. An aqueous lubricant was more beneficial than a gel-type counterpart.

Method for lubricating contacting surfaces

DOEpatents

Dugger, Michael T [Tijeras, NM; Ohlhausen, James A [Albuquerque, NM; Asay, David B [Boalsburg, PA; Kim, Seong H [State College, PA

2011-12-06

A method is provided for tribological lubrication of sliding contact surfaces, where two surfaces are in contact and in motion relative to each other, operating in a vapor-phase environment containing at least one alcohol compound at a concentration sufficiently high to provide one monolayer of coverage on at least one of the surfaces, where the alcohol compound continuously reacts at the surface to provide lubrication.

Wear characteristics of bonded solid film lubricant under high load condition

NASA Technical Reports Server (NTRS)

Hiraoka, Naofumi; Sasaki, Akira; Kawashima, Noritsugu; Honda, Toshio

1991-01-01

Wear properties of phenolic resin bonded molybdenum disulfide film lubricant were studied. In-vacuo journal bearing tests were performed to evaluate the wear-life of this film lubricant. The wear-life depends on substrate materials and on sliding velocity. Pretreated substrate surfaces were examined to reveal the reasons for these results. Additionally, investigations on film wear mechanisms were made.

New Method to Produce an Industrial Lubrication Fluid from Vegetable Oil-based Materials

USDA-ARS?s Scientific Manuscript database

The projected demand for industrial and automotive lubricants in the U.S. is ~2.6 billion gallons by 2017, where bio-based lubricants will play an increasing role, from a share of 0.6% today to a possible 1.2% by 2017. This is accompanied by the expected price increase to >$7.00/gallon which will g...

Definition and effect of chemical properties of surfaces in friction, wear, and lubrication

NASA Technical Reports Server (NTRS)

Buckley, D. H.

1978-01-01

Chemical properties relative to their role in adhesion, friction, wear and lubrication discussed in this paper will include: (1) adsorption, both physical and chemical; (2) orientation of the solid as well as the lubricant; (3) surface energy; (4) surface segregation; (5) surface versus bulk metallurgical effects; (6) electronic nature of the surface; and (7) bonding mechanisms.

High Temperature Solid Lubricant Coating for High Temperature Wear Applications

NASA Technical Reports Server (NTRS)

DellaCorte, Christopher (Inventor); Edmonds, Brian J (Inventor)

2014-01-01

A self-lubricating, friction and wear reducing composite useful over a wide temperature range is described herein. The composite includes metal bonded chromium oxide dispersed in a metal binder having a substantial amount of nickel. The composite contains a fluoride of at least one Group I, Group II, or rare earth metal, and optionally a low temperature lubricant metal.

Additives

NASA Technical Reports Server (NTRS)

Smalheer, C. V.

1973-01-01

The chemistry of lubricant additives is discussed to show what the additives are chemically and what functions they perform in the lubrication of various kinds of equipment. Current theories regarding the mode of action of lubricant additives are presented. The additive groups discussed include the following: (1) detergents and dispersants, (2) corrosion inhibitors, (3) antioxidants, (4) viscosity index improvers, (5) pour point depressants, and (6) antifouling agents.

Highly Branched Polyethylenes as Lubricant Viscosity and Friction Modifiers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Robinson, Joshua W.; Zhou, Yan; Qu, Jun

2016-10-08

A series of highly branched polyethylenes (BPE) were prepared and used in a Group I base oil as potential viscosity and friction modifiers. The lubricating performance of these BPEs supports the expected dual functionality. Changes in polarity, topology, and molecular weight of the BPEs showed significant effects on the lubricants’ performance, which provide scientific insights for polymer design in future lubricant development.

Spacecraft materials guide. [including: encapsulants and conformal coatings; optical materials; lubrication; and, bonding and joining processes

NASA Technical Reports Server (NTRS)

Staugaitis, C. L. (Editor)

1975-01-01

Materials which have demonstrated their suitability for space application are summarized. Common, recurring problems in encapsulants and conformal coatings, optical materials, lubrication, and bonding and joining are noted. The subjects discussed include: low density and syntactic foams, electrical encapsulants; optical glasses, interference filter, mirrors; oils, greases, lamillar lubricants; and, soldering and brazing processes.

Lubricant effects on bearing life

NASA Technical Reports Server (NTRS)

Zaretsky, Erwin V.

1986-01-01

Lubricant considerations for rolling-element bearings have within the last two decades taken on added importance in the design and operation of mechanical systems. The phenomenon which limits the useful life of bearings is rolling-element or surface pitting fatigue. The elastohydrodynamic (EHD) film thickness which separates the ball or roller surface from those of the raceways of the bearing directly affects bearing life. Chemical additives added to the lubricant can also significantly affect bearings life and reliability. The interaction of these physical and chemical effects is important to the design engineer and user of these systems. Design methods and lubricant selection for rolling-element bearings are presented and discussed.

Confirmation of heavy metal ions in used lubricating oil from a passenger car using chelating self-assembled monolayer.

PubMed

Ko, Young Gun; Kim, Choong Hyun

2006-09-01

In order to prevent engine failure, the oil must be changed before it loses its protective properties. It is necessary to monitor the actual physical and chemical condition of the oil to reliably determine the optimum oil-change interval. Our study focuses on the condition of the lubricating oil in an operated car engine. Shear stress curves and viscosity curves as a function of the shear rate for fresh and used lubricating oil were examined. Metal nitrate was detected in the lubricating oil from the operated car engine through the use of a chelating self-assembled monolayer.

A New Apparatus to Evaluate Lubricants for Space Applications: The Spiral Orbit Tribometer (SOT)

NASA Technical Reports Server (NTRS)

Jones, William R., Jr.; Pepper, Stephen V.; Jansen, Mark J.; Nguyen, QuynhGiao N.; Kingsbury, Edward P.; Loewenthal, Stuart H.; Predmore, Roamer E.

2000-01-01

Lubricants used in space mechanisms must be thoroughly tested prior to their selection for critical applications. Traditionally, two types of tests have been used: accelerated and full-scale. Accelerated tests are rapid, economical, and provide useful information for gross screening of candidate lubricants. Although full-scale tests are more believable, because they mimic actual spacecraft conditions, they are expensive and time consuming. The spiral orbit tribometer compromises between the two extremes. It rapidly determines the rate of tribochemically induced lubricant consumption, which leads to finite test times, under realistic rolling/pivoting conditions that occur in angular contact bearings.

Experience of Application of Liquid Lubricating Materials during Wide Strip Hot Rolling

NASA Astrophysics Data System (ADS)

Platov, S. I.; Dema, R. R.; Kharchenko, M. V.; Amirov, R. N.

2017-12-01

The paper presents the results of the scientific and practical research of roller systems operation at feed of liquid lubricating materials through the example of the wide strip hot rolling Mill-2000 at PAO MMK. The experiments proved that application of lubricating materials leads to decrease of energy-power parameters of the process by 12 to 15 %, and reduction of work roll wear by 10 to 12%. The practical results of the study are developed recommendations on determination of consumption-volumetric parameters of the supplied lubricating material depending on rheological and geometrical parameters of the rolled strip and current wear of work rolls.

Effects of lubrication on the performance of high speed spur gears

NASA Technical Reports Server (NTRS)

Mizutani, Hachiro; Isikawa, Yuuichi; Townsend, Dennis P.

1989-01-01

An experimental analysis was conducted to determine power loss and gear noise of high speed spur gears with long addendum under various conditions of load, speed, and oil jet pressure for into mesh lubrication. Power losses were calculated from temperature measurements of lubricating oil, gears, gear box, and oil flow rate. Furthermore, power loss was divided into windage loss, friction loss and churning loss. The results show that windage loss and churning loss were the main components of gear power loss of high gear speed. In addition, lubricating conditions had some influences on gear noise especially under low oil temperature or high viscosity.

Preparation and Tribological Study of Biodegradable Lubrication Films on Si Substrate

PubMed Central

Shi, Shih-Chen; Huang, Teng-Feng; Wu, Jhen-Yu

2015-01-01

A novel method for preparing eco-biodegradable lubricant based on hydroxypropyl methylcellulose (HPMC) via hydration process is demonstrated. The smooth and homogeneous HPMC coating has a uniform thickness (~35 μm). It has been demonstrated that the preparation parameters play a critical role in controlling the lubricating behavior of the coating; in addition, excess HPMC and water concentration suppress the tribology properties. Nevertheless, a remarkable friction-reduction and anti-wear performance has been obtained. Impressively, the preparation parameter of 5% HPMC + 30 mL water significantly improves lubricant performance and durability. A simple approach for the water-degradability evaluation of HPMC is proposed. PMID:28788029

Auto-ignition of lubricating oil working at high pressures in a compressor for an air conditioner.

PubMed

Kim, Chul Jin; Choi, Hyo Hyun; Sohn, Chae Hoon

2011-01-15

Auto-ignition of lubricating oil working in a compressor for an air conditioner is studied experimentally. The adopted lubricating oil is an unknown mixture with multi-components and known to have flash point temperature of 170 °C. First, its auto-ignition temperature is measured 365 °C at atmospheric pressure. The lubricating oil works under high-pressure condition up to 30 atm and it is heated and cooled down repeatedly. Accordingly, auto-ignition temperatures or flammable limits of lubricating oil are required at high pressures with respect to fire safety. Because there is not a standard test method for the purpose, a new ignition-test method is proposed in this study and thereby, auto-ignition temperatures are measured over the pressure range below 30 atm. The measured temperatures range from 215 °C to 255 °C and they strongly depend on pressure of gas mixture consisting of oil vapor, nitrogen, and oxygen. They are close to flash point temperature and the lubricating oil can be hazardous when it works for high-pressure operating condition and abundant air flows into a compressor. Copyright © 2010 Elsevier B.V. All rights reserved.

Enhancement of perfluoropolyether boundary lubrication performance: I. Preliminary results

NASA Technical Reports Server (NTRS)

Jones, W. R., Jr.; Ajayi, O. O.; Goodell, A. J.; Wedeven, L. D.; Devine, E.; Premore, R. E.

1995-01-01

A ball bearing simulator operating under starved conditions was used to evaluate the boundary lubrication performance of a perfluoropolyether (PFPE) Krytox 143 AB. Several approaches to enhance boundary lubrication were studied. These included: (1) soluble boundary additives, (2) bearing surface modifications, (3) 'run-in' surface films, and (4) ceramic bearing components. In addition, results were compared with two non-perfluorinated liquid lubricant formulations. Based on these preliminary tests, the following tentative conclusions can be made: (1) substantial improvements in boundary lubrication performance were observed with a beta-diketone boundary additive and a tricresyl phosphate (TCP) liquid surface pretreatment; (2) the use of rough Si3N4 balls (Ra = 40 micro-in) also provided substantial improvement but with concomitant abrasive wear; (3) marginal improvements were seen with two boundary additives (a phosphine and a phosphatriazine) and a neat (100%) fluid (a carboxylic acid terminated PFPE); and surface pretreatments with a synthetic hydrocarbon, a PTFE coating, and TiC coated 440C and smooth Si3N4 balls (R(sub a) less than 1 micro-in); and (4) two non-PFPE lubricant formulations (a PAO and a synthetic hydrocarbon) yielded substantial improvements.

Gear Mesh Loss-of-Lubrication Experiments and Analytical Simulation

NASA Technical Reports Server (NTRS)

Handschuh, Robert F.; Polly, Joseph; Morales, Wilfredo

2011-01-01

An experimental program to determine the loss-of-lubrication (LOL) characteristics of spur gears in an aerospace simulation test facility has been completed. Tests were conducted using two different emergency lubricant types: (1) an oil mist system (two different misted lubricants) and (2) a grease injection system (two different grease types). Tests were conducted using a NASA Glenn test facility normally used for conducting contact fatigue. Tests were run at rotational speeds up to 10000 rpm using two different gear designs and two different gear materials. For the tests conducted using an air-oil misting system, a minimum lubricant injection rate was determined to permit the gear mesh to operate without failure for at least 1 hr. The tests allowed an elevated steady state temperature to be established. A basic 2-D heat transfer simulation has been developed to investigate temperatures of a simulated gear as a function of frictional behavior. The friction (heat generation source) between the meshing surfaces is related to the position in the meshing cycle, the load applied, and the amount of lubricant in the contact. Experimental conditions will be compared to those from the 2-D simulation.

Effect of stress nonhomogeneity on the shear melting of a thin boundary lubrication layer.

PubMed

Lyashenko, Iakov A; Filippov, Alexander E; Popov, Mikhail; Popov, Valentin L

2016-11-01

We consider the dynamical properties of boundary lubrication in contact between two atomically smooth solid surfaces separated by an ultrathin layer of lubricant. In contrast to previous works on this topic, we explicitly consider the heterogeneity of tangential stresses, which arises in a contact of elastic bodies that are moved tangentially relative to each other. To describe phase transitions between structural states of the lubricant we use an approach based on the field theory of phase transitions. It is assumed that the lubricant layer, when stressed, can undergo a shear-melting transition of first or second order. While solutions for the homogeneous system can be easily obtained analytically, the kinetics of the phase transitions in the spatially heterogeneous system can only be studied numerically. In our numerical experiments melting of the lubricant layer starts from the outer boundary of contact and propagates to its center. The melting wave is followed by a wave of solidification. This process repeats itself periodically, following the stick-slip pattern that is characteristic of such systems. Depending on the thermodynamic and kinetic parameters of the model, different modes of sliding with almost complete or only partial intermediate solidification are possible.

A three-dimensional model for lubricant depletion under sliding condition on bit patterned media of hard disk drives

NASA Astrophysics Data System (ADS)

Wu, Lin

2018-05-01

In this paper, we model the depletion dynamics of the molecularly thin layer of lubricants on a bit patterned media disk of hard disk drives under a sliding air bearing head. The dominant physics and consequently, the lubricant depletion dynamics on a patterned disk are shown to be significantly different from the well-studied cases of a smooth disk. Our results indicate that the surface tension effect, which is negligible on a flat disk, apparently suppresses depletion by enforcing a bottleneck effect around the disk pattern peak regions to thwart the migration of lubricants. When the disjoining pressure is relatively small, it assists the depletion. But, when the disjoining pressure becomes dominant, the disjoining pressure resists depletion. Disk pattern orientation plays a critical role in the depletion process. The effect of disk pattern orientation on depletion originates from its complex interaction with other intermingled factors of external air shearing stress distribution and lubricant particle trajectory. Patterning a disk surface with nanostructures of high density, large height/pitch ratio, and particular orientation is demonstrated to be one efficient way to alleviate the formation of lubricant depletion tracks.

Analysis of lubricating oils in shear friction tests using infrared thermography

NASA Astrophysics Data System (ADS)

Da Silva, José Jorge; Maribondo, Juscelino de Farias

2018-03-01

The aim of this work is to analyze the ability of Thermography to monitor the behavior of SAE 20 W50 API SJ and ISO VG 10 lubricating oils from the thermal point of view until the moment of the lubricant film rupture, characterized by the sudden increase in friction, noise, vibration and Temperature in a shear friction test. The methodology used is based on the analysis of thermograms that indicate temperature profiles during the friction tests and at the moment of mechanical failure, comparing these results with those obtained by a thermocouple. The specimens, consisting of SAE 1045 steel cylindrical pins, are rubbed against a wear ring consisting of a weld-locked bearing under the condition of a boundary lubrication regime. Tests were performed by increasing load conditions up to 180 N at 10, 15 and 20 Hz rotations (600, 900 and 1200 rpm). The results show the qualitative and quantitative capacity of the Thermography in the detection of scuffing considering the emissivity of the lubricating oil film equal to 0,82. It is concluded that the Thermography can be used for the detection of the breaking of the lubricating film in pin-on-ring friction tests.

Enhancement of Perfluoropolyether Boundary Lubrication Performance

NASA Technical Reports Server (NTRS)

Jones, W. R., Jr.; Ajayi, O. O.; Wedeven, L. D.

1996-01-01

A ball bearing simulator operating under starved conditions was used to perform screening tests to evaluate the boundary lubrication performance of a branched perfluoropolyether (PFPE), K-143 AB. Several approaches to enhance boundary lubrication were studied. These included: (1) soluble boundary additives, (2) bearing surface modifications, (3) 'run-in' surface films, and (4) ceramic bearing components. In addition, results were compared with two non-perfluorinated liquid lubricant formulations. Based on these tests, the following tentative conclusions can be made: (1) Substantial improvements in boundary lubrication performance were observed with a beta-diketone boundary additive and a tricresyl phosphate (TCP) liquid surface pretreatment, (2) the use of rough Si3N4 balls (R(sub a) = 40 micro-inch) also provided increases in test duration, but with concomitant abrasive wear, (3) moderate improvements were seen with two boundary additives (a phosphine and a phosphatriazine) and a neat (100%) fluid (a carboxylic acid terminated PFPE); and small improvements with surface pretreatments with synthetic hydrocarbons, a polytetrafluoroethylene (PTFE) coating, and TiC coated 440 C and smooth Si3N4 balls (R(sub a) = 1 micro-inch), and (4) two non-PFPE lubricant formulations (a polyalphaolefin (PAO) and synthetic hydrocarbon) yielded substantial improvements.

Breakage is the norm: use of condoms and lubrication in anal sex among Black South African men who have sex with men.

PubMed

Lee, Matthew; Sandfort, Theo; Collier, Kate; Lane, Tim; Reddy, Vasu

2017-04-01

This paper explores condom use and lubrication practices among Black men who have sex with men in South African townships. Results are from 81 in-depth individual interviews conducted among a purposive sample from four townships surrounding Pretoria as part of a larger qualitative study. Awareness that condoms should be used to have safer anal sex was ubiquitous. Fewer men reported that lubricants should be used to facilitate anal intercourse. Partner pressure and partner distrust were the most common barriers cited for not using condoms and lubricants. Knowledge about condom-lubricant compatibility was rare. Condom problems were a norm, with widespread expectations of condom failure. Men's subjectivities - their perceptions of and preferences for specific brands, types and flavours of condoms and lubricants - influenced engagement with such safer-sex technologies. However, what was available in these settings was often neither what men needed nor preferred. Findings show the need to enhance access to appropriate and comprehensive: safer-sex supplies, health services and health education, and underline the importance of efforts to develop targeted programmes relevant to experiences of men who have sex with men in the South African context.

The use of surface layer with boron in friction pairs lubricated by engine oils

NASA Astrophysics Data System (ADS)

Szczypiński-Sala, W.; Lubas, J.

2016-09-01

The aim of the present work is to determine the influence of surface layers with boron and engine oil on the processes of friction and wear in friction pairs. The ring samples with borided surface layer cooperated under test conditions with counterparts made with CuPb30 and AlSn20 bearing alloys. During the tests, the friction pairs were lubricated with 15W/40 Lotos mineral oil and 5W/40 Lotos synthetic oil. The lubrication of friction area with Lotos mineral oil causes the reduction of the friction force, the temperature in the friction area and the wear of the bearing alloys under study, whereas the lubrication with Lotos synthetic oil reduces the changes in the geometrical structure of the cooperating friction pair elements. Lubrication of the friction area in the start-up phase of the friction pair by mineral oil causes faster stabilization of the friction conditions in the contact area than in the cause of lubrication of the friction pair by synthetic oil. The intensity of wear of the AlSn20 bearing alloy cooperating with the borided surface layer is three times smaller than the intensity of use of the CuPb30 alloy bearing.

Tribology of the lubricant quantized sliding state.

PubMed

Castelli, Ivano Eligio; Capozza, Rosario; Vanossi, Andrea; Santoro, Giuseppe E; Manini, Nicola; Tosatti, Erio

2009-11-07

In the framework of Langevin dynamics, we demonstrate clear evidence of the peculiar quantized sliding state, previously found in a simple one-dimensional boundary lubricated model [A. Vanossi et al., Phys. Rev. Lett. 97, 056101 (2006)], for a substantially less idealized two-dimensional description of a confined multilayer solid lubricant under shear. This dynamical state, marked by a nontrivial "quantized" ratio of the averaged lubricant center-of-mass velocity to the externally imposed sliding speed, is recovered, and shown to be robust against the effects of thermal fluctuations, quenched disorder in the confining substrates, and over a wide range of loading forces. The lubricant softness, setting the width of the propagating solitonic structures, is found to play a major role in promoting in-registry commensurate regions beneficial to this quantized sliding. By evaluating the force instantaneously exerted on the top plate, we find that this quantized sliding represents a dynamical "pinned" state, characterized by significantly low values of the kinetic friction. While the quantized sliding occurs due to solitons being driven gently, the transition to ordinary unpinned sliding regimes can involve lubricant melting due to large shear-induced Joule heating, for example at large speed.

Computational Chemistry and Lubrication

NASA Technical Reports Server (NTRS)

Zehe, Michael J.

1998-01-01

Members of NASA Lewis Research Center's Tribology and Surface Science Branch are applying high-level computational chemistry techniques to the development of new lubrication systems for space applications and for future advanced aircraft engines. The next generation of gas turbine engines will require a liquid lubricant to function at temperatures in excess of 350 C in oxidizing environments. Conventional hydrocarbon-based lubricants are incapable of operating in these extreme environments, but a class of compounds known as the perfluoropolyether (PFAE) liquids (see the preceding illustration) shows promise for such applications. These commercially available products are already being used as lubricants in conditions where low vapor pressure and chemical stability are crucial, such as in satellite bearings and composite disk platters. At higher temperatures, however, these compounds undergo a decomposition process that is assisted (catalyzed) by metal and metal oxide bearing surfaces. This decomposition process severely limits the applicability of PFAE's at higher temperatures. A great deal of laboratory experimentation has revealed that the extent of fluid degradation depends on the chemical properties of the bearing surface materials. Lubrication engineers would like to understand the chemical breakdown mechanism to design a less vulnerable PFAE or to develop a chemical additive to block this degradation.

Experimental validation of Critical Temperature-Pressure theory of scuffing

NASA Astrophysics Data System (ADS)

Lee, Si C.; Chen, Huanliang

1995-07-01

A series of experiments was conducted for validating a newly developed theory of scuffing. The Critical temperature-Pressure (CTP) theory is based on the physisorption behavior of lubricants and is capable of predicting the onset of scuffing failures over a wide range of operating conditions, including the contacts operating in the boundary lubrication and in the partial elastohydrodynamic lubrication (EHL) regimes. According to the CTP theory, failures occur when the contact temperature exceeds a certain critical value which is a function of the lubricant pressure generated by the hydrodynamic action of the EHL contact. A special device capable of simulating the ambient conditions of the partial EHL conjunctions (of contact temperature, pressure, and the lubricant pressure) was constructed. A ball-on-flat type wear tester was put inside a pressure vessel, completely immersed in a highly pressurized bath of mineral oil. The temperature on the flat specimen was gradually increased while the ball was slowly traversed. At a certain critical temmperature, the friction force abruptly jumped indicating the incipiency of the lubrication breakdown. This experiment was repeated for several levels of hydrostatic pressure and the corresponding critical temperatures were obtained. The test results showed an excellent correlation with the newly developed CTP theory.

XPS analysis of 440C steel surfaces lubricated with perfluoropolyethers under sliding conditions in high vacuum

NASA Technical Reports Server (NTRS)

Herrera-Fierro, Pilar; Masuko, Masabumi; Jones, William R., Jr.; Pepper, Stephen V.

1994-01-01

This work presents the results of the X-Ray Photoelectron Spectroscopy (XPS) analysis of AISI 440C ball surfaces lubricated with perfluoropolyether (PFPE) oils after friction experiments under sliding conditions at high load in air and vacuum environments. The PFPE lubricants tested were Demnum S100, Fomblin Z-25, and Krytox 143AB. It was found that all the PFPE lubricants were degraded by sliding contact causing the formation of inorganic fluorides on the metallic surfaces and a layer of organic decomposition products. KRYTOX 143AB was the least reactive of the three lubricants tested. It was also found that metal fluoride formed at off-scar areas. This suggests the formation of reactive species, such as COF2 or R(sub f)COF, during sliding experiments, which can diffuse through the lubricant film and react with the metallic surfaces away from the contact region. Comparison of reference specimens before sliding with those that had undergone the sliding tests showed that the amount of non-degraded PFPE remaining on the surface of the balls after the sliding experiments was greater than that of the balls without sliding.

Evaluation of Advanced Solid Lubricant Coatings for Foil Air Bearings Operating at 25 and 500 C

NASA Technical Reports Server (NTRS)

DellaCorte, Christopher; Fellenstein, James A.; Benoy, Patricia A.

1998-01-01

The tribological properties of one chrome oxide and one chrome carbide based solid lubricant coating were evaluated in a partial-arc foil bearing at 25 and 500 C. Start/stop bearing operation up to 20,000 cycles were run under 10 kPa (1.5 psi) static deadweight load. Bearing friction (torque) was measured during the test. Specimen wear and SEM/EDS surface analyses were conducted after testing to understand and elucidate the tribological characteristics observed. The chrome oxide coating which contains both (Ag) and (BaF2/CaF2) for low and high temperature lubrication, exhibited low friction in sliding against Al2O3 coated foils at 25 and 500 C. The chrome carbide coating, which lacked a low temperature lubricant but contained BaF2/CaF2 as a high temperature lubricant, exhibited high friction at 25 C and low friction at 500 C against both bare and Al2O3 coated superalloy foil surfaces. Post test surface analyses suggest that improved tribological performance is exhibited when a lubricant film from the coating transfers to the foil surface.

Performance of two-lobe hole-entry hybrid journal bearing system under the combined influence of textured surface and couple stress lubricant

NASA Astrophysics Data System (ADS)

Khatri, Chandra B.; Sharma, Satish C.

2018-02-01

Textured surface in journal bearings is becoming an important area of investigation during the last few years. Surface textures have the shapes of micro-dimple with a small diameter and depth having order of magnitude of bearing clearance. This paper presents the influence of couple stress lubricant on the circular and non-circular hole-entry hybrid journal bearing system and reports the comparative study between the textured and non-textured circular/non-circular hybrid journal bearing system. The governing Reynolds equation has been modified for the couple stress lubricant flow in the clearance of bearing and journal. The FEM technique has been applied to solve the modified Reynolds equation together with restrictor flow equation. The numerically simulated results indicate that the influence of couple stress lubricant is significantly more in textured journal bearing than that of non-textured journal bearing. Further, it has been observed that the textured two-lobe (δ = 1.1) hybrid journal bearing lubricated with couple stress lubricant provides larger values of fluid film stiffness coefficients and stability threshold speed against other bearings studied in the present paper.

Dissipative Properties of EHD Lubricant Film

NASA Astrophysics Data System (ADS)

Fedorov, S. V.

2018-01-01

For the case of the failure of the lubricant film at hydrodynamic lubrication a common thermodynamic theory of strength is considered. According to this theory the failure occurs when the internal energy density (potential and thermal components) in the volume of material reaches a constant for a given material. A special case of this theory is considered when only the density of heat (kinetic) component of internal energy is taken into account. Temperature condition determines the limit state for liquid lubricants - mineral oils. When analyzing the regularities of friction at EHD lubrication the state and properties of the oil film at the condition of irregular and hydrostatic compression. The original structural model of oil film at EHD lubrication in the form of the rotary oscillating cells with elastic interactions to each other is proposed. It is similar to the Rayleigh-Benard cells and corresponds to the cellular hypothesis of J. Gibbs for the case of equilibrium and reversible process. It is quite possible that the size of the cells have an order of about nano level. The oil film dissipates energy in the direction of relative motion of bodies. This oil film has the highest dissipative properties.

3D Imaging of Water-Drop Condensation on Hydrophobic and Hydrophilic Lubricant-Impregnated Surfaces

NASA Astrophysics Data System (ADS)

Kajiya, Tadashi; Schellenberger, Frank; Papadopoulos, Periklis; Vollmer, Doris; Butt, Hans-Jürgen

2016-04-01

Condensation of water from the atmosphere on a solid surface is an ubiquitous phenomenon in nature and has diverse technological applications, e.g. in heat and mass transfer. We investigated the condensation kinetics of water drops on a lubricant-impregnated surface, i.e., a micropillar array impregnated with a non-volatile ionic liquid. Growing and coalescing drops were imaged in 3D using a laser scanning confocal microscope equipped with a temperature and humidity control. Different stages of condensation can be discriminated. On a lubricant-impregnated hydrophobic micropillar array these are: (1) Nucleation on the lubricant surface. (2) Regular alignment of water drops between micropillars and formation of a three-phase contact line on a bottom of the substrate. (3) Deformation and bridging by coalescence which eventually leads to a detachment of the drops from the bottom substrate. The drop-substrate contact does not result in breakdown of the slippery behaviour. Contrary, on a lubricant-impregnated hydrophilic micropillar array, the condensed water drops replace the lubricant. Consequently, the surface loses its slippery property. Our results demonstrate that a Wenzel-like to Cassie transition, required to maintain the facile removal of condensed water drops, can be induced by well-chosen surface hydrophobicity.

3D Imaging of Water-Drop Condensation on Hydrophobic and Hydrophilic Lubricant-Impregnated Surfaces.

PubMed

Kajiya, Tadashi; Schellenberger, Frank; Papadopoulos, Periklis; Vollmer, Doris; Butt, Hans-Jürgen

2016-04-04

Condensation of water from the atmosphere on a solid surface is an ubiquitous phenomenon in nature and has diverse technological applications, e.g. in heat and mass transfer. We investigated the condensation kinetics of water drops on a lubricant-impregnated surface, i.e., a micropillar array impregnated with a non-volatile ionic liquid. Growing and coalescing drops were imaged in 3D using a laser scanning confocal microscope equipped with a temperature and humidity control. Different stages of condensation can be discriminated. On a lubricant-impregnated hydrophobic micropillar array these are: (1) Nucleation on the lubricant surface. (2) Regular alignment of water drops between micropillars and formation of a three-phase contact line on a bottom of the substrate. (3) Deformation and bridging by coalescence which eventually leads to a detachment of the drops from the bottom substrate. The drop-substrate contact does not result in breakdown of the slippery behaviour. Contrary, on a lubricant-impregnated hydrophilic micropillar array, the condensed water drops replace the lubricant. Consequently, the surface loses its slippery property. Our results demonstrate that a Wenzel-like to Cassie transition, required to maintain the facile removal of condensed water drops, can be induced by well-chosen surface hydrophobicity.

Enhanced basal lubrication and the contribution of the Greenland ice sheet to future sea-level rise

PubMed Central

Shannon, Sarah R.; Payne, Antony J.; Bartholomew, Ian D.; van den Broeke, Michiel R.; Edwards, Tamsin L.; Fettweis, Xavier; Gagliardini, Olivier; Gillet-Chaulet, Fabien; Goelzer, Heiko; Hoffman, Matthew J.; Huybrechts, Philippe; Mair, Douglas W. F.; Nienow, Peter W.; Perego, Mauro; Price, Stephen F.; Smeets, C. J. P. Paul; Sole, Andrew J.; van de Wal, Roderik S. W.; Zwinger, Thomas

2013-01-01

We assess the effect of enhanced basal sliding on the flow and mass budget of the Greenland ice sheet, using a newly developed parameterization of the relation between meltwater runoff and ice flow. A wide range of observations suggest that water generated by melt at the surface of the ice sheet reaches its bed by both fracture and drainage through moulins. Once at the bed, this water is likely to affect lubrication, although current observations are insufficient to determine whether changes in subglacial hydraulics will limit the potential for the speedup of flow. An uncertainty analysis based on our best-fit parameterization admits both possibilities: continuously increasing or bounded lubrication. We apply the parameterization to four higher-order ice-sheet models in a series of experiments forced by changes in both lubrication and surface mass budget and determine the additional mass loss brought about by lubrication in comparison with experiments forced only by changes in surface mass balance. We use forcing from a regional climate model, itself forced by output from the European Centre Hamburg Model (ECHAM5) global climate model run under scenario A1B. Although changes in lubrication generate widespread effects on the flow and form of the ice sheet, they do not affect substantial net mass loss; increase in the ice sheet’s contribution to sea-level rise from basal lubrication is projected by all models to be no more than 5% of the contribution from surface mass budget forcing alone. PMID:23940337

Modification of Bushing Test Rig and Research of Variable Inlet Guide Vane Bushings For Further Development of PM304 Bushings

NASA Technical Reports Server (NTRS)

Yanke, Anne

2004-01-01

PS304 is a high temperature solid lubricant coating comprised of a nickel-chrome binder, chrome oxide hardener, barium-calcium fluoride high temperature lubricant, and silver as the low temperature lubricant. This coating is used to lubricate Oil-Free Foil Air Bearings as they experience friction and wear during start up and shut down. The coating deposition process begins with undercutting the shaft. This area is then sandblasted to provide a rough surface for the coating to adhere to. The coating powder is then sent through the plasma spray gun and a reasonably thick layer is applied to the undercut area of the shaft. The coating is then ground down even with the surface of the shaft and gets a nice polished finish. The foil air bearings use the solid lubricant, as mentioned above, during start up and shut down. During normal operating conditions, generally above 2000RPM, the bearings utilize air as their lubricant. Foil air bearings are comprised of a thin top foil and a corrugated bump foil. They have an interference fit with the shaft before operation. As the air gets "trapped" between the top foil and the shaft, it presses the top foil against the bump foil, in turn compressing the bumps. As the bumps compress, it allows for the air to separate the top foil from the shaft, therefore, utilizing the trapped air as its lubricant.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Olofinjana, Bolutife; Lorenzo-Martin, Cinta; Ajayi, Oyelayo O.

Surface texturing or topographical design is one of the primary techniques to control friction and wear performance of surfaces in tribological contact. Laser surface texturing (LST), whereby a laser beam is used to produce regular arrays of dimples on a surface, has been demonstrated to reduce friction in conformal lubricated contacts. Friction and wear behavior under boundary lubrication is also known to be dependent on the formation and durability of the tribochemical film formed from lubricant additives. In this paper, the effects of LST on the formation and durability of tribochemical films and its consequent impacts on friction and wearmore » behavior in various lubrication regimes were evaluated. Friction and wear tests that cycled through different lubrication regimes were conducted with both polished and LST treated surfaces using a synthetic lubricant with and without model additives of ZDDP and MoDTC mixture. In the base oil without additives, LST produced noticeable reduction in friction in all lubrication regimes. However, with low-friction model additives, friction was higher in tests with LST due to significant differences in the tribochemical film formation in the polished and LST surfaces, as well as the sliding counterface. Continuous tribo-films were formed on ball conterface rubbed against polished surfaces while the films were streaky and discontinuous in ball rubbed against LST surfaces. LST produced more wear on the ball counterface in both base and additized oils. Lastly, no measurable wear was observed in both the polished and LST flat specimens.« less

Development and validation of an environmentally friendly attenuated total reflectance in the mid-infrared region method for the determination of ethanol content in used engine lubrication oil.

PubMed

Hatanaka, Rafael Rodrigues; Sequinel, Rodrigo; Gualtieri, Carlos Eduardo; Tercini, Antônio Carlos Bergamaschi; Flumignan, Danilo Luiz; de Oliveira, José Eduardo

2013-05-15

Lubricating oils are crucial in the operation of automotive engines because they both reduce friction between moving parts and protect against corrosion. However, the performance of lubricant oil may be affected by contaminants, such as gasoline, diesel, ethanol, water and ethylene glycol. Although there are many standard methods and studies related to the quantification of contaminants in lubricant oil, such as gasoline and diesel oil, to the best of our knowledge, no methods have been reported for the quantification of ethanol in used Otto cycle engine lubrication oils. Therefore, this work aimed at the development and validation of a routine method based on partial least-squares multivariate analysis combined with attenuated total reflectance in the mid-infrared region to quantify ethanol content in used lubrication oil. The method was validated based on its figures of merit (using the net analyte signal) as follows: limit of detection (0.049%), limit of quantification (0.16%), accuracy (root mean square error of prediction=0.089% w/w), repeatability (0.05% w/w), fit (R(2)=0.9997), mean selectivity (0.047), sensitivity (0.011), inverse analytical sensitivity (0.016% w/w(-1)) and signal-to-noise ratio (max: 812.4 and min: 200.9). The results show that the proposed method can be routinely implemented for the quality control of lubricant oils. Copyright © 2013 Elsevier B.V. All rights reserved.

The Effect of Composition on the Surface Finish of PS400: A New High Temperature Solid Lubricant Coating

NASA Technical Reports Server (NTRS)

DellaCorte, Christopher; Stanford, malcolm K.; Thomas, Fransua; Edmonds, Brian J.

2010-01-01

A new composite, multi-constituent, solid lubricant coating, NASA PS400, developed for high temperature tribological applications, exhibits a smoother surface finish after grinding and polishing than its predecessors PS200 and PS300. In this paper, the baseline composition of PS400 is modified to investigate each individual constituent s role on the achievable surface finish through a series of coating deposition, grinding, and polishing experiments. Furthermore, to explore the limits of compositional tailoring for improved tribological performance, several PS400 coatings were doped with additional solid lubricants (graphite, MoS2 and BN) and tribologically tested. The test results clearly showed that, compared to PS300 coatings, PS400 achieves a smoother surface finish via a reduced lubricant content. Coatings prepared with higher than the baseline level (10 wt%) of lubricants exhibited higher final surface roughness than the earlier generation PS300 coatings. Reducing or eliminating the one or both lubricants (fluorides or silver) did not further improve the surface finish suggesting that the current composition of PS400 is near optimal with respect to surface finish. Lastly, attempts to improve the poor initial room temperature tribological behavior of PS400 via the addition of traditional solid lubricants were unsuccessful. Based upon this work and earlier results it is expected that future research will concentrate on developing methods to produce a lubricious glaze on the rubbing surface during break in to ensure that low friction and wear are rapidly achieved.

Enhanced basal lubrication and the contribution of the Greenland ice sheet to future sea-level rise.

PubMed

Shannon, Sarah R; Payne, Antony J; Bartholomew, Ian D; van den Broeke, Michiel R; Edwards, Tamsin L; Fettweis, Xavier; Gagliardini, Olivier; Gillet-Chaulet, Fabien; Goelzer, Heiko; Hoffman, Matthew J; Huybrechts, Philippe; Mair, Douglas W F; Nienow, Peter W; Perego, Mauro; Price, Stephen F; Smeets, C J P Paul; Sole, Andrew J; van de Wal, Roderik S W; Zwinger, Thomas

2013-08-27

We assess the effect of enhanced basal sliding on the flow and mass budget of the Greenland ice sheet, using a newly developed parameterization of the relation between meltwater runoff and ice flow. A wide range of observations suggest that water generated by melt at the surface of the ice sheet reaches its bed by both fracture and drainage through moulins. Once at the bed, this water is likely to affect lubrication, although current observations are insufficient to determine whether changes in subglacial hydraulics will limit the potential for the speedup of flow. An uncertainty analysis based on our best-fit parameterization admits both possibilities: continuously increasing or bounded lubrication. We apply the parameterization to four higher-order ice-sheet models in a series of experiments forced by changes in both lubrication and surface mass budget and determine the additional mass loss brought about by lubrication in comparison with experiments forced only by changes in surface mass balance. We use forcing from a regional climate model, itself forced by output from the European Centre Hamburg Model (ECHAM5) global climate model run under scenario A1B. Although changes in lubrication generate widespread effects on the flow and form of the ice sheet, they do not affect substantial net mass loss; increase in the ice sheet's contribution to sea-level rise from basal lubrication is projected by all models to be no more than 5% of the contribution from surface mass budget forcing alone.

Effectiveness of Low Temperature Additives for Biodiesel Blends

DTIC Science & Technology

2012-06-30

Westbrook U.S. Army TARDEC Fuels and Lubricants Research Facility Southwest Research Institute® (SwRI®) San Antonio, TX for U.S. Army TARDEC...INTERIM REPORT TFLRF No. 428 by Steven R. Westbrook U.S. Army TARDEC Fuels and Lubricants Research Facility Southwest Research Institute...Director U.S. Army TARDEC Fuels and Lubricants Research Facility (SwRI®) UNCLASSIFIED UNCLASSIFIED REPORT DOCUMENTATION PAGE Form Approved

SYNTHETIC LUBRICANTS

DTIC Science & Technology

azelaic , and sebacic acids are the most readily available dibasic acids suitable for ester lubricant production, while the petroleum derived Oxo alcohols...of synthetic lubricants for use at low and high temperatures. The diesters of straight-chain dibasic acids lead the field of esters mutable as...dibasic acid esters in all the characteristics studied so far, and this type of ester therefore represents a promising source of synthetic oil. Mono

Thiophenyl ether disiloxanes and trisiloxanes useful as lubricant fluids

NASA Technical Reports Server (NTRS)

Bilow, N.; Akawie, R. I. (Inventor)

1974-01-01

The characteristics of organosilicon compounds for lubrication under extreme conditions are discussed. The substances considered are thiophenyl ether disiloxanes and trisiloxanes. These substances have low pour points and a high degree of radiation resistance. Substitution of sulfur for the phenoxy group oxygen of either siloxane compounds has been found to result in a marked improvement in lubricity. The chemical formulas of the organic compounds are presented.

Scintillation Method of Analysis for Determination of Properties of Wear Particles in Lubricating Oils,

DTIC Science & Technology

1998-01-01

Scintillation Method of Analysis for Determination of Properties of Wear Particles in Lubricating Oils Andrey B. Alkhimov Applied Physics Insitute...lubricating oils; metrological properties ; scintillation spectral analysis; spectrometer; unit-to-unit diagnostics; wear particles. Introduction: In...filter. The use of air reduces the metrological properties of the method, but it saves the operators the trouble and expense of using argon and

Investigation of lubricants under boundary friction

NASA Technical Reports Server (NTRS)

Heidebroek, E; Pietsch, E

1942-01-01

Numerous observations of such lubrication processes within range of boundary friction on journal bearings and gear tooth profiles have strengthened the supposition that it should be possible to study the attendant phenomena with engineering methods and equipment. These considerations formed the basis of the present studies, which have led to the discovery of relations governing the suitability of bearing surfaces and the concept of "lubricating quality."

Development of a Fuel Lubricity Haze Test (FLHT) for Naval Applications

DTIC Science & Technology

2009-03-16

Protection Agency FLHT Fuel Lubricity Haze Tester FOA Fuel Oil Additive FSII Fuel System Icing Inhibitor (additive) FT Fisher Tropsch FY...Light Cycle Oil LSDF Low Sulfur Diesel Fuel MDFI Middle Distillate Flow Improver (additive) MIL-DTL Military Detail MSC Military Sealift...a chemical test for diesel fuel lubricity that included a base extraction, acidification, a back extraction, and analysis with gas chromatography

High temperature lubricants. (Latest citations from the US Patent bibliographic file with exemplary claims). Published Search

DOE Office of Scientific and Technical Information (OSTI.GOV)

NONE

1996-01-01

The bibliography contains citations of selected patents concerning high temperature synthetic and natural lubricating compositions. Thickening agents, thermal stabilizers, polymeric additives, antioxidants, and preservatives are included relative to such lubricants as greases, oils, and soaps. Manufacturing methods and various applications are included. (Contains 50-250 citations and includes a subject term index and title list.) (Copyright NERAC, Inc. 1995)

AUTOMOTIVE DIESEL MAINTENANCE 1. UNIT XXVI, I--CATERPILLAR LUBRICATION SYSTEMS AND COMPONENTS, II--LEARNING ABOUT BRAKES (PART I).

ERIC Educational Resources Information Center

Minnesota State Dept. of Education, St. Paul. Div. of Vocational and Technical Education.

THIS MODULE OF A 30-MODULE COURSE IS DESIGNED TO DEVELOP AN UNDERSTANDING OF THE FUNCTIONS OF DIESEL ENGINE LUBRICATION SYSTEMS AND COMPONENTS AND THE PRINCIPLES OF OPERATION OF BRAKE SYSTEMS USED ON DIESEL POWERED VEHICLES. TOPICS ARE (1) THE NEED FOR OIL, (2) SERVICE CLASSIFICATION OF OILS, (3) CATERPILLAR LUBRICATION SYSTEM COMPONENTS (4)…

ORNL-GM: Development of Ionic Liquid-Additized, GF-5/6 Compatible Low-Viscosity Oils for Automotive Engine and Rear Axle Lubrication for 4% Improved Fuel Economy

DOE Office of Scientific and Technical Information (OSTI.GOV)

Qu, Jun; Zhou, Yan; Luo, Huimin

The overall objective of this project are as follows: Further develop ionic liquid (IL)-additized lowviscosity engine oils meeting the GF-5/6 specifications and possessing superior lubricating characteristics; Expand the IL additive technology to rear axle lubricants; and Seek a combined improvement in the vehicle fuel economy

Evaluation of minimum quantity lubrication grinding with nano-particles and recent related patents.

PubMed

Li, Changhe; Wang, Sheng; Zhang, Qiang; Jia, Dongzhou

2013-06-01

In recent years, a large number of patents have been devoted to developing minimum quantity lubrication (MQL) grinding techniques that can significantly improve both environmentally conscious and energy saving and costeffective sustainable grinding fluid alternatives. Among them, one patent is about a supply system for the grinding fluid in nano-particle jet MQL, which produced MQL lubricant by adding solid nano-particles in degradable grinding fluid. The MQL supply device turns the lubricant to the pulse drops with fixed pressure, unchanged pulse frequency and the same drop diameter. The drops will be produced and injected in the grinding zone in the form of jet flow under high pressure gas and air seal. As people become increasingly demanding on our environment, minimum quantity lubrication has been widely used in the grinding and processing. Yet, it presents the defect of insufficient cooling performance, which confines its development. To improve the heat transfer efficiency of MQL, nano-particles of a certain mass fraction can be added in the minimum quantity of lubricant oil, which concomitantly will improve the lubrication effects in the processing. In this study, the grinding experiment corroborated the effect of nano-particles in surface grinding. In addition, compared with other forms of lubrication, the results presented that the grinding force, the friction coefficient and specific grinding energy of MQL grinding have been significantly weakened, while G ratio greatly rose. These are attributed to the friction oil-film with excellent anti-friction and anti-wear performance, which is generated nano-particles at the wheel/workpiece interface. In this research, the cooling performance of nano-particle jet MQL was analyzed. Based on tests and experiments, the surface temperature was assayed from different methods, including flood lubricating oil, dry grinding, MQL grinding and nano-particle jet MQL grinding. Because of the outstanding heat transfer performance of nano-particles, the ratio of heat delivered by grinding media was increased, leading to lower temperature in the grinding zone. Results demonstrate that nano-particle jet MQL has satisfactory cooling performance as well as a promising future of extensive application.

Experimental verification of nanoparticle jet minimum quantity lubrication effectiveness in grinding

NASA Astrophysics Data System (ADS)

Jia, Dongzhou; Li, Changhe; Zhang, Dongkun; Zhang, Yanbin; Zhang, Xiaowei

2014-12-01

In our experiment, K-P36 precision numerical control surface grinder was used for dry grinding, minimum quantity lubrication (MQL) grinding, nanoparticle jet MQL grinding, and traditional flood grinding of hardened 45 steel. A three-dimensional dynamometer was used to measure grinding force in the experiment. In this research, experiments were conducted to measure and calculate specific tangential grinding force, frictional coefficient, and specific grinding energy, thus verifying the lubrication performance of nanoparticles in surface grinding. Findings present that compared with dry grinding, the specific tangential grinding force of MQL grinding, nanoparticle jet MQL grinding, and flood grinding decreased by 45.88, 62.34, and 69.33 %, respectively. Their frictional coefficient was reduced by 11.22, 29.21, and 32.18 %, and the specific grinding energy declined by 45.89, 62.34, and 69.45 %, respectively. Nanoparticle jet MQL presented ideal lubrication effectiveness, which was attributed to the friction oil film with strong antifriction and anti-wear features formed by nanoparticles on the grinding wheel/workpiece interface. Moreover, lubricating properties of nanoparticles of the same size (50 nm) but different types were verified through experimentation. In our experiment, ZrO2 nanoparticles, polycrystal diamond (PCD) nanoparticles, and MoS2 nanoparticles were used in the comparison of nanoparticle jet MQL grinding. The experimental results manifest that MoS2 nanoparticles exhibited the optimal lubricating effectiveness, followed by PCD nanoparticles. Our research also integrated the properties of different nanoparticles to analyze the lubrication mechanisms of different nanoparticles. The experiment further verified the impact of nanoparticle concentration on the effectiveness of nanoparticle jet MQL in grinding. The experimental results demonstrate that when the nanoparticle mass fraction was 6 %, the minimum specific tangential grinding force, frictional coefficient, and specific grinding energy were 1.285 N/mm, 0.382, and 57.825 J/mm3, respectively. When nanoparticle mass fraction was smaller than 6 %, lubrication effects of nanoparticle jet MQL increased with the rising nanoparticle mass fraction. When nanoparticle mass fraction was larger than 6 %, lubrication effects of nanoparticle jet MQL decreased with the rising nanoparticle mass fraction.

Synthesis of new high performance lubricants and solid lubricants

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lagow, Richard J.

1993-04-08

In our second year of funding we began the testing phase of a number of new classes of lubricants. Three different testing collaborations have already begun and a fourth one is In the works with Dr. Stephen Hsu of the National Institute of Standards and Technology. Dr. Hsu also plans to test some of the same materials for us that Shell Development is studying. With Dr. Bill Jones of NASA, we are studying the effects of branching an high temperature lubricant properties in perfluoropolyethers, Initially Bill Jones is comparing the lubrication and physical properties of perfluorotetraglyme and the following twomore » spherical perfluoropolyethers, Note that one contains a fluorocarbon chain and the other one contains a fluorocarbon ether chain. The synthesis of these was reported in the last progress report. With Professor Patricia Thiel of Iowa State University, we are working on studies of perfluoromethylene oxide ethers and have prepared a series of four of these polyethers to study in collaboration with her research group. These perfluoromethylene oxide ethers have the best low temperature properties of any known lubricants. Thiel's group is studying their interactions with metals under extreme conditions. Thirdly, we have also begun an Interaction with W. August Birke of Shell Development Company in Houston for whom we have already prepared samples of the chlorine-substituted fluorocarbon polyether lubricants whose structures appear on page 54 of our research proposal. Each of these four structures is thought to have potential as lubricant additives to motor oils. We also have underway syntheses of other fluorine-containing branched ether lubricants. These new materials which are also promising as antifriction additives for motor oils appear ahead of the perfluoro additives as Appendix I to the progress report. Additionally for Birke and Shell Development we have at their request prepared the novel compound perfluoro salicylic acid. This synthesis was suggested by the Shell staff who thought that esters of perfluoro salicylic acid might be an excellent antifriction additive for motor oil fuels. One of the best additives currently used in motor oils is the hydrocarbon ester of salicylic acid.« less

Effect of wear of bearing surfaces on elastohydrodynamic lubrication of metal-on-metal hip implants.

PubMed

Liu, F; Jin, Z M; Hirt, F; Rieker, C; Roberts, P; Grigoris, P

2005-09-01

The effect of geometry change of the bearing surfaces owing to wear on the elastohydrodynamic lubrication (EHL) of metal-on-metal (MOM) hip bearings has been investigated theoretically in the present study. A particular MOM Metasul bearing (Zimmer GmbH) was considered, and was tested in a hip simulator using diluted bovine serum. The geometry of the worn bearing surface was measured using a coordinate measuring machine (CMM) and was modelled theoretically on the assumption of spherical geometries determined from the maximum linear wear depth and the angle of the worn region. Both the CMM measurement and the theoretical calculation were directly incorporated into the elastohydrodynamic lubrication analysis. It was found that the geometry of the original machined bearing surfaces, particularly of the femoral head with its out-of-roundness, could lead to a large reduction in the predicted lubricant film thickness and an increase in pressure. However, these non-spherical deviations can be expected to be smoothed out quickly during the initial running-in period. For a given worn bearing surface, the predicted lubricant film thickness and pressure distribution, based on CMM measurement, were found to be in good overall agreement with those obtained with the theoretical model based on the maximum linear wear depth and the angle of the worn region. The gradual increase in linear wear during the running-in period resulted in an improvement in the conformity and consequently an increase in the predicted lubricant film thickness and a decrease in the pressure. For the Metasul bearing tested in an AMTI hip simulator, a maximum total linear wear depth of approximately 13 microm was measured after 1 million cycles and remained unchanged up to 5 million cycles. This resulted in a threefold increase in the predicted average lubricant film thickness. Consequently, it was possible for the Metasul bearing to achieve a fluid film lubrication regime during this period, and this was consistent with the minimal wear observed between 1 and 5 million cycles. However, under adverse in vivo conditions associated with start-up and stopping and depleted lubrication, wear of the bearing surfaces can still occur. An increase in the wear depth beyond a certain limit was shown to lead to the constriction of the lubricant film around the edge of the contact conjunction and consequently to a decrease in the lubricant film thickness. Continuous cycles of a running-in wear period followed by a steady state wear period may be inevitable in MOM hip implants. This highlights the importance of minimizing the wear in these devices during the initial running-in period, particularly from design and manufacturing points of view.

Thermal modelling of a dry revolving vane compressor

NASA Astrophysics Data System (ADS)

Ooi, K. T.; Aw, K. T.

2017-08-01

The lubricant used in compressors serves to lubricate, to seal the gaps to reduce internal leakage and to a certain extent, to cool. However, a lubricant free compressor is attractive if lubricants become a source of contaminant, or in areas where the compressor needs be placed under any orientation, such as those in military or portable computing. In this paper, a thermal model for a dry revolving vane compressor is presented. This thermal model sets out to predict the steady-state operating temperatures of the compressor components. The lumped thermal conductance method was employed. The results of the components temperature will be presented and discussed. A high potential for overheating is observed at the shaft bearings.

Flight-vehicle materials, structures, and dynamics - Assessment and future directions. Vol. 4 - Tribological materials and NDE

NASA Technical Reports Server (NTRS)

Fusaro, Robert L. (Editor); Achenbach, J. D. (Editor)

1993-01-01

The present volume on tribological materials and NDE discusses liquid lubricants for advanced aircraft engines, a liquid lubricant for space applications, solid lubricants for aeronautics, and thin solid-lubricant films in space. Attention is given to the science and technology of NDE, tools for an NDE engineering base, experimental techniques in ultrasonics for NDE and material characterization, and laser ultrasonics. Topics addressed include thermal methods of NDE and quality control, digital radiography in the aerospace industry, materials characterization by ultrasonic methods, and NDE of ceramics and ceramic composites. Also discussed are smart materials and structures, intelligent processing of materials, implementation of NDE technology on flight structures, and solid-state weld evaluation.

Additives for high-temperature liquid lubricants

NASA Technical Reports Server (NTRS)

Lawton, Emil A.; Yavrouian, Andre H.; Repar, John

1988-01-01

A preliminary research program was conducted to demonstrate a new concept for additives to liquid lubricants. It was demonstrated that suspensions of o-phthalonitrile and a substituted 1,2-maleonitrile in mineral oil and dilute solutions of o-phthalonitrile and tetrafluoro-o-phthalonitrile extended the lifetime of bearings under boundary lubricating conditions. The solutions exhibited coefficients of friction under high loads of 0.02-0.03. These results were consistent with the hypothesis that these compounds react with the hot metal surface to form a planar lubricating film by means of a metal or metal oxide template reaction. Also, the adherence was very strong due to the chelating action of the planar macrocycles postulated to form under the experimental conditions.

Characterization of Lubricants on Ball Bearings by FT-IR Using an Integrating Sphere

NASA Technical Reports Server (NTRS)

Street, K. W.; Pepper, S. V.; Wright, A. A.; Grady, B.

2007-01-01

Fourier Transform-Infrared reflectance microspectroscopy has been used extensively for the examination of coatings on nonplanar surfaces such as ball bearings. While this technique offers considerable advantages, practical application has many drawbacks, some of which are easily overcome by the use of integrating sphere technology. This paper describes the use of an integrating sphere for the quantification of thin layers of lubricant on the surface of ball bearings and the parameters which require optimization in order to obtain reliable data. Several applications of the technique are discussed including determination of lubricant load on 12.7 mm steel ball bearings and the examination of degraded lubricant on post mortem specimens.

Analysis of variation in oil pressure in lubricating system

NASA Astrophysics Data System (ADS)

Sharma, Sumit; Upreti, Mritunjay; Sharma, Bharat; Poddar, Keshav

2018-05-01

Automotive Maintenance for an engine contributes to its reliability, energy efficiency and repair cost reduction. Modeling of engine performance and fault detection require large amount of data, which are usually obtained on test benches. This report presents a methodical study on analysis of variation in lubrication system of various medium speed engines. Further this study is limited to the influence of Engine Oil Pressure on frictional losses, Torque analysis for various Oil Pressures and an analytical analysis of engine Lubrication System. The data collected from various Engines under diagnostics is represented graphically. Finally the illustrated results were used as a viable source for detection and troubleshooting of faults in Lubrication System of regular passenger vehicle.

Dynamic analysis of liquid-lubricated hydrostatic journal bearings

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kocur, J.A. Jr.

1990-01-01

A hybrid bearing reduces the dependency of its behavior on the lubricant viscosity, bearing clearance, bearing surface area by combining the hydrostatic and hydrodynamic effects. The combination permits the hybrid bearing to be incorporated into rotor designs, where the working fluids of the rotor may be used in place of externally supplied lubricants. An effective and practical method to predict the static and dynamic behavior of hybrid bearings is developed. The model includes the three major fluid effects in the bearing; the orifice restriction, inertia losses at the pocket edges, and hydrodynamic effects on the bearing land regions. Lubrication ismore » modeled and calculated using a finite element solution of Reynolds equation with turbulence corrections.« less

Development and characterization of lubricants for use near nuclear reactors in space vehicles

NASA Technical Reports Server (NTRS)

Robinson, G. L.; Akawie, R. I.; Gardos, M. N.; Krening, K. C.

1972-01-01

The synthesis and evaluation program was conducted to develop wide-temperature range lubricants suitable for use in space vehicles particularly in the vicinity of nuclear reactors. Synthetic approaches resulted in nonpolymeric, large molecular weight materials, all based on some combination of siloxane and aromatic groups. Evaluation of these materials indicated that certain tetramethyl and hexamethyl disiloxanes containing phenyl thiophenyl substituents are extremely promising with respect to radiation stability, wide temperature range, good lubricity, oxidation resistance and additive acceptance. The synthesis of fluids is discussed, and the equipment and methods used in evaluation are described, some of which were designed to evaluate micro-quantities of the synthesized lubricants.

Investigation of the influence of coolant-lubricant modification on selected effects of pull broaching

NASA Astrophysics Data System (ADS)

Adamczuk, Krzysztof; Legutko, Stanisław; Laber, Alicja; Serwa, Wojciech

2017-10-01

The paper presents the results of testing the wear of the tool (pull broach) and a gear wheel splineway surface roughness after the friction node of pull broach/gear wheel (CuSn12Ni2) had been lubricated with metal machining oil and the same oil modified with chemically active exploitation additive. To designate the influence of modifying metal machining oil by the exploitation additive on the lubricating properties, anti-wear and antiseizure indicators have been appointed. Exploitation tests have proved purposefulness of modifying metal machining oil. Modification of the lubricant has contributed to reduction of the wear of the tools - pull broaches and to reduction of roughness of the splineway surfaces.

A study of energy consumption in turning process using lubrication of nanoparticles enhanced coconut oil (NECO)

NASA Astrophysics Data System (ADS)

Mansor, A. F.; Zakaria, M. S.; Azmi, A. I.; Khalil, A. N. M.; Musa, N. A.

2017-10-01

Cutting fluids play very important role in machining application in order to increase tool life, surface finish and reduce energy consumption. Instead of using petrochemical and synthetic based cutting fluids, vegetable oil based lubricants is safety for operators, environmental friendly and become more popular in the industrial applications. This research paper aims to find the advantage of using vegetable oils (coconut oil) with additional of nano particles (CuO) as lubricant to the energy consumption during machining process. The energy was measured for each run from 2 level factorial experimental layout. Obtained results illustrate that lubricant with enhancement of nanoparticles has capability to improve the energy consumption during the machining process.

Self-Healing Materials for Ecotribology

PubMed Central

Shi, Shih-Chen; Huang, Teng-Feng

2017-01-01

Hydroxypropyl methylcellulose (HPMC) is a biopolymer that is biodegradable, environmentally friendly, and bio-friendly. Owing to its unique chemical structure, HPMC can reduce the coefficient of friction (COF) and frictional wear and thus possesses excellent lubrication properties. HPMC has good dissolvability in specific solvents. The present research focuses on the reversible dissolution reaction subsequent to the film formation of HPMC, with a view to the healing and lubrication properties of thin films. Raman spectroscopy was used to test the film-forming properties of HPMC and the dissolution characteristics of various solvents. In this study, the solvents were water, methanol, ethanol, and acetone. The results showed that the HPMC film had the highest dissolvability in water. The ball-on-disk wear test was used to analyze the lubrication properties of HPMC, and the results showed that HPMC had the same COF and lubrication properties as the original film after being subjected to the water healing treatment. The HPMC film can be reused, recycled, and refilled, making it an ideal lubricant for next-generation ecotribology. PMID:28772449

Studies on tribology

PubMed Central

Hori, Yukio; Kato, Koji

2008-01-01

In high speed rotating machines such as turbines and generators, vibrations of a rotating shaft often hinder the smooth operation of the machine or even cause failure. Oil whip is one of such vibrations due to oil film action of journal bearing. Its mechanism and preventive method is explained and proposed in this paper. Further theoretical and experimental analyses are made for considering heat generation and temperature rise in hydrodynamic lubrication. The usefulness of the lubrication theory based on the k–ε model is also shown for bearings with high eccentricity ratios. In the latter half of this paper, water lubrication, nitrogen gas lubrication and tribo-coated indium lubrication are shown as new promising methods, and their mechanisms are discussed and the importance of tribo-layer is explained. Some mechanisms of wear are introduced for better understanding of tribo-layer. In the last part of this paper, the mechanisms of generating static friction are shown for the cases of plastic contact and elastic contact, which is the base for understanding the mechanism of initiation of macroscopic sliding. PMID:18941304

Lubricant Selection Manual, Phase 3

NASA Technical Reports Server (NTRS)

Kannel, J. W.; Lowry, J. A.; Dufrane, K. F.

1991-01-01

Future spacecraft must be designated to operate for very long time periods in space. For example, a target goal for the Space Station is 30 years of operation. Although the actual life may be significantly less than this optimistic goal, the life will certainly be a critical issue in design. The bearings on primary components such as the alpha and beta joints must obviously be designed and lubricated with the objective of optimum performance life. In addition to these joints, there will be numerous other tribological (rubbing or rolling) interfaced that will be required to function for the life of the spacecraft. A major key to adequate performance of tribological interface is proper lubrication. Lubricants can be divided into two basic classes: solid films and liquids. Both types have been used extensively in space applications. Both have advantages and disadvantages that must be carefully considered in their selection. The purpose here is to summarize selection criteria for liquid and solid lubricants applied to long-life spacecraft.

Studies on tribology.

PubMed

Hori, Yukio; Kato, Koji

2008-01-01

In high speed rotating machines such as turbines and generators, vibrations of a rotating shaft often hinder the smooth operation of the machine or even cause failure. Oil whip is one of such vibrations due to oil film action of journal bearing. Its mechanism and preventive method is explained and proposed in this paper. Further theoretical and experimental analyses are made for considering heat generation and temperature rise in hydrodynamic lubrication. The usefulness of the lubrication theory based on the k-epsilon model is also shown for bearings with high eccentricity ratios. In the latter half of this paper, water lubrication, nitrogen gas lubrication and tribo-coated indium lubrication are shown as new promising methods, and their mechanisms are discussed and the importance of tribo-layer is explained. Some mechanisms of wear are introduced for better understanding of tribo-layer. In the last part of this paper, the mechanisms of generating static friction are shown for the cases of plastic contact and elastic contact, which is the base for understanding the mechanism of initiation of macroscopic sliding.

Radiofrequency-sputtered coatings for lubrication system components and other complex surfaces

NASA Technical Reports Server (NTRS)

Spalvins, T.

1972-01-01

Irregularly shaped surfaces, such as lubrication system components (ball bearings, seals, gears, etc.), can be coated on all surfaces, including irregular shapes, when radiofrequency sputtering is used. When the specimen is properly located with respect to the sputtering target, the sputtered material covers the entire surface of the object irrespective of its geometrical configuration. An adherent, dense film is formed. The film thickness varies from 20 to 50 percent on, for example, a hearing cage or race depending on its geometry. When sputtered solid film lubricants such as molybdenum disulfide are used, a film thickness only of the order of 10 to the minus 7th power m (thousands of angstroms) is required at the contacting areas. It is only essential to determine the required film thickness at the critical areas in need of lubrication. The sections outside the areas to be lubricated fall within the thickness deviation range of 20 to 50 percent, which still constitutes a negligible change respect to tolerance requirements.

Supramolecular ionogel lubricants with imidazolium-based ionic liquids bearing the urea group as gelator.

PubMed

Yu, Qiangliang; Wu, Yang; Li, DongMei; Cai, Meirong; Zhou, Feng; Liu, Weimin

2017-02-01

A new class of ionic liquid gels (ionogels) is prepared through the supramolecular self-assembly of imidazolium-based ionic liquids (ILs) bearing the urea group as gelators in normal ILs. The ILs gelator can self-assemble through hydrogen bonding and hydrophobic interaction to form analogous lamellar structures and solidify base ILs. The obtained ionogels exhibit superior anticorrosion and conductivity characteristics. Moreover, ionogels show fully thermoreversible and favorable thixotropic characteristics, such that they can be used as high-performance semisolid conductive lubricants. The tribological tests reveal that these ionogels lubricants can effectively reduce the friction of sliding pairs effectively and have better tribological performance than the pure ILs under harsh conditions. Ionogel lubricants not only maintain the excellent tribological properties and conductivity of ILs, but also prevent base liquids from creeping and leakage. Therefore, ionogel lubricants can be potentially used in the conductive parts of electrical equipments. Copyright © 2016 Elsevier Inc. All rights reserved.

Bonded Lubricants

NASA Technical Reports Server (NTRS)

1977-01-01

Another spinoff to the food processing industry involves a dry lubricant developed by General Magnaplate Corp. of Linden, N.J. Used in such spacecraft as Apollo, Skylab and Viking, the lubricant is a coating bonded to metal surfaces providing permanent lubrication and corrosion resistance. The coating lengthens equipment life and permits machinery to be operated at greater speed, thus increasing productivity and reducing costs. Bonded lubricants are used in scores of commercia1 applications. They have proved particularly valuable to food processing firms because, while increasing production efficiency, they also help meet the stringent USDA sanitation codes for food-handling equipment. For example, a cookie manufacturer plagued production interruptions because sticky batter was clogging the cookie molds had the brass molds coated to solve the problem. Similarly, a pasta producer faced USDA action on a sanitation violation because dough was clinging to an automatic ravioli-forming machine; use of the anti-stick coating on the steel forming plates solved the dual problem of sanitation deficiency and production line downtime.

Liquid Space Lubricants Examined by Vibrational Micro-Spectroscopy

NASA Technical Reports Server (NTRS)

Street, Kenneth W., Jr.

2008-01-01

Considerable effort has been expended to develop liquid lubricants for satellites and space exploration vehicles. These lubricants must often perform under a range of harsh conditions such as vacuum, radiation, and temperature extremes while in orbit or in transit and in extremely dusty environments at destinations such as the Moon and Mars. Historically, oil development was guided by terrestrial application, which did not provide adequate space lubricants. Novel fluids such as the perfluorinated polyethers provided some relief but are far from ideal. With each new fluid proposed to solve one problem, other problems have arisen. Much of the work performed at the National Aeronautics and Space Administration (NASA) Glenn Research Center (GRC) in elucidating the mechanisms by which chemical degradation of space oils occur has been done by vibrational micro-spectroscopic techniques such as infrared and Raman, which this review details. Presented are fundamental lubrication studies as well as actual case studies in which vibrational spectroscopy has led to millions of dollars in savings and potentially prevented loss of mission.

Experimental and Theoretical Investigations on the Nanoscale Kinetic Friction in Ambient Environmental Conditions.

PubMed

Gueye, Birahima; Zhang, Yan; Wang, Yujuan; Chen, Yunfei

2015-07-08

The liquid lubrication, thermolubricity and dynamic lubricity due to mechanical oscillations are investigated with an atomic force microscope in ambient environmental conditions with different relative humidity (RH) levels. Experimental results demonstrate that high humidity at low-temperature regime enhances the liquid lubricity while at high-temperature regime it hinders the effect of the thermolubricity due to the formation of liquid bridges. Friction response to the dynamic lubricity in both high- and low-temperature regimes keeps the same trends, namely the friction force decreases with increasing the amplitude of the applied vibration on the tip regardless of the RH levels. An interesting finding is that for the dynamic lubricity at high temperature, high-humidity condition leads to the friction forces higher than that at low-humidity condition while at low temperature the opposite trend is observed. An extended two-dimensional dynamic model accounting for the RH is proposed to interpret the frictional mechanism in ambient conditions.

Isolation and characterization of novel strains of Pseudomonas aeruginosa and Serratia marcescens possessing high efficiency to degrade gasoline, kerosene, diesel oil, and lubricating oil.

PubMed

Wongsa, Patcharaporn; Tanaka, Makiko; Ueno, Akio; Hasanuzzaman, Mohammad; Yumoto, Isao; Okuyama, Hidetoshi

2004-12-01

Bacteria possessing high capacity to degrade gasoline, kerosene, diesel oil, and lubricating oil were screened from several areas of Hokkaido, Japan. Among isolates, two strains, WatG and HokM, which were identified as new strains of Pseudomonas aeruginosa and Serratia marcescens species, respectively, showed relatively high capacity and wide spectrum to degrade the hydrocarbons in gasoline, kerosene, diesel, and lubricating oil. About 90-95% of excess amount of total diesel oil and kerosene added to mineral salts media as a sole carbon source could be degraded by WatG within 2 and 3 weeks, respectively. The same amount of lubricating oil was 60% degraded within 2 weeks. Strain HokM was more capable than WatG in degrading aromatic compounds in gasoline. This strain could also degrade kerosene, diesel, and lubricating oil with a capacity of 50-60%. Thus, these two isolates have potential to be useful for bioremediation of sites highly contaminated with petroleum hydrocarbons.

Soft matter dynamics: Accelerated fluid squeeze-out during slip

NASA Astrophysics Data System (ADS)

Hutt, W.; Persson, B. N. J.

2016-03-01

Using a Leonardo da Vinci experimental setup (constant driving force), we study the dependency of lubricated rubber friction on the time of stationary contact and on the sliding distance. We slide rectangular rubber blocks on smooth polymer surfaces lubricated by glycerol or by a grease. We observe a remarkable effect: during stationary contact the lubricant is only very slowly removed from the rubber-polymer interface, while during slip it is very rapidly removed resulting (for the grease lubricated surface) in complete stop of motion after a short time period, corresponding to a slip distance typically of order only a few times the length of the rubber block in the sliding direction. For an elastically stiff material, poly(methyl methacrylate), we observe the opposite effect: the sliding speed increases with time (acceleration), and the lubricant film thickness appears to increase. We propose an explanation for the observed effect based on transient elastohydrodynamics, which may be relevant also for other soft contacts.

Full-scale transmission testing to evaluate advanced lubricants

NASA Technical Reports Server (NTRS)

Lewicki, David G.; Decker, Harry J.; Shimski, John T.

1992-01-01

Experimental tests were performed on the OH-58A helicopter main rotor transmission in the NASA Lewis 500 hp helicopter transmission test stand. The testing was part of a lubrication program. The objectives are to develop and show a separate lubricant for gearboxes with improved performance in life and load carrying capacity. The goal was to develop a testing procedure to fail certain transmission components using a MIL-L-23699 based reference oil and then to run identical tests with improved lubricants and show improved performance. The tests were directed at parts that failed due to marginal lubrication from Navy field experience. These failures included mast shaft bearing micropitting, sun gear and planet bearing fatigue, and spiral bevel gear scoring. A variety of tests were performed and over 900 hrs of total run time accumulated for these tests. Some success was achieved in developing a testing procedure to produce sun gear and planet bearing fatigue failures. Only marginal success was achieved in producing mast shaft bearing micropitting and spiral bevel gear scoring.

Evaluation of replacement thread lubricants for red lead and graphite in mineral oil

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jungling, T.L.; Rauth, D.R.; Goldberg, D.

1998-04-30

Eight commercially available thread lubricants were evaluated to determine the best replacement for Red Lead and Graphite in Mineral Oil (RLGMO). The evaluation included coefficient of friction testing, high temperature anti-seizing testing, room temperature anti-galling testing, chemical analysis for detrimental impurities, corrosion testing, off-gas testing, and a review of health and environmental factors. The coefficient of friction testing covered a wide variety of factors including stud, nut, and washer materials, sizes, manufacturing methods, surface coatings, surface finishes, applied loads, run-in cycles, and relubrication. Only one lubricant, Dow Corning Molykote P37, met all the criteria established for a replacement lubricant. Itmore » has a coefficient of friction range similar to RLGMO. Therefore, it can be substituted directly for RLGMO without changing the currently specified fastener torque values for the sizes, materials and conditions evaluated. Other lubricants did not perform as well as Molykote P37 in one or more test or evaluation categories.« less

Testing the ecotoxicology of vegetable versus mineral based lubricating oils: 1. Degradation rates using tropical marine microbes.

PubMed

Mercurio, Philip; Burns, Kathryn A; Negri, Andrew

2004-05-01

Vegetable-derived lubricants (VDL) might be more biodegradable than mineral-derived lubricants (MDL) due to the absence of high molecular weight aromatics, but this remains largely untested in tropical conditions. In this laboratory study, the degradation rates of 2-stroke, 4-stroke and hydraulic VDLs were compared with their MDL counterparts in the presence of mangrove and coral reef microbial communities. While MDLs were comprised largely of unresolved saturated and some aromatic hydrocarbons, their VDL counterparts contained, potentially more degradable, fatty acid methyl esters. Degradation of some VDL was observed by day 7, with the 2-stroke VDL markedly consumed by mangrove microorganisms and the hydraulic VDL degraded by both microorganism communities after this short period. All of the VDL groups were significantly more degraded than the comparable MDLs mineral oil lubricants over 14 days in the presence of either mangrove or coral reef microbial communities. In general the mangrove-sourced microorganisms more efficiently degraded the lubricants than reef-sourced microorganisms.

Carbon nanotubes/fluorinated polymers nanocomposite thin films for electrical contacts lubrication

NASA Astrophysics Data System (ADS)

Benedetto, A.; Viel, P.; Noël, S.; Izard, N.; Chenevier, P.; Palacin, S.

2007-09-01

The need to operate in extreme environmental conditions (ultra high vacuum, high temperatures, aerospatial environment, …) and the miniaturization toward micro electromechanical systems is demanding new materials in the field of low-level electrical contacts lubrication. Dry and chemically immobilized lubrication is expected to be an alternative to the traditional wet lubricants oils. With the goal to conciliate electrical conductivity and lubricant properties we designed nanocomposite thin films composed of a 2D carbon nanotubes network embedded in an organic matrix. The nanotubes networks were deposited on gold surfaces modified by electrochemical cathodic grafting of poly(acrylonitrile). The same substrate served for covalently bonding the low-friction organic matrix. Three different matrixes were tested: a perfluorinated oligomer chemically grafted and two different polyfluorinated acrylates electrochemically grafted. The nanocomposite thin films have been characterized by ATR FT-IR, XPS and Raman spectroscopy. We measured the effects of the different matrixes and the nanotubes addition on the tribological properties and on the contact resistances of the films.

Assessment of lubricated contacts: Mechanisms of scuffing and scoring

NASA Technical Reports Server (NTRS)

Dyson, A.; Wedeven, L. D.

1983-01-01

Scoring and scuffing are defined as two distinct but related forms of failure of hardened ferrous components lubricated by liquids. Experimental observations of these phenomena are described, and criteria for scoring and scuffing are discussed. The mechanisms proposed by various authors to explain these observations are enumerated. The view presented here is that, under conditions yet to be defined, scoring is a gradual breakdown of the lubrication of interacting asperities, such lubrication being boundary or microelastohydrodynamic in nature, or a mixture of the two. The final scuffing stage represents a breakdown of the main elastohydrodynamic system, but this may be triggered by the deterioration in surface topography as a result of scoring. An extension of published theoretical treatment of elastohydrodynamic breakdown is proposed, and a critical experiment to assess the importance of edge effects in band contacts is suggested. The practical implications of the proposed mechanism are reviewed, and recommendations for further work are made. A possible thermal instability mechanism for the breakdown of boundary lubrication is outlined.

LUBRICATING AND SIZING AGENT FOR GLASS FIBER,

DTIC Science & Technology

GLASS TEXTILES, SURFACE PROPERTIES), (*LUBRICANTS, GLASS TEXTILES), FIBERS , POLYVINYL ALCOHOL, STEARATES, CHROMIUM COMPOUNDS, ALUMINUM COMPOUNDS, MIXTURES, LACTATES, TITANIUM COMPOUNDS, MECHANICAL PROPERTIES, USSR

Dynamic stability and slider-lubricant interactions in hard disk drives

NASA Astrophysics Data System (ADS)

Ambekar, Rohit Pradeep

2007-12-01

Hard disk drives (HDD) have played a significant role in the current information age and have become the backbone of storage. The soaring demand for mass data storage drives the necessity for increasing capacity of the drives and hence the areal density on the disks as well as the reliability of the HDD. To achieve greater areal density in hard disk drives, the flying height of the airbearing slider continually decreases. Different proximity forces and interactions influence the air bearing slider resulting in fly height modulation and instability. This poses several challenges to increasing the areal density (current goal is 2Tb/in.2) as well as making the head-disk interface (HDI) more reliable. Identifying and characterizing these forces or interactions has become important for achieving a stable fly height at proximity and realizing the goals of areal density and reliability. Several proximity forces or interactions influencing the slider are identified through the study of touchdown-takeoff hysteresis. Slider-lubricant interaction which causes meniscus force between the slider and disk as well as airbearing surface contamination seems to be the most important factor affecting stability and reliability at proximity. In addition, intermolecular forces and disk topography are identified as important factors. Disk-to-slider lubricant transfer leads to lubricant pickup on the slider and also causes depletion of lubricant on the disk, affecting stability and reliability of the HDI. Experimental and numerical investigation as well as a parametric study of the process of lubricant transfer has been done using a half-delubed disk. In the first part of this parametric study, dependence on the disk lubricant thickness, lubricant type and slider ABS design has been investigated. It is concluded that the lubricant transfer can occur without slider-disk contact and there can be more than one timescale associated with the transfer. Further, the transfer increases non-linearly with increasing disk lubricant thickness. Also, the transfer depends on the type of lubricant used, and is less for Ztetraol than for Zdol. The slider ABS design also plays an important role, and a few suggestions are made to improve the ABS design for better lubricant performance. In the second part of the parametric study, the effect of carbon overcoat, lubricant molecular weight and inclusion of X-1P and A20H on the slider-lubricant interactions is investigated using a half-delubed disk approach. Based on the results, it is concluded that there exists a critical head-disk clearance above which there is negligible slider-lubricant interaction. The interaction starts at this critical clearance and increases in intensity as the head-disk clearance is further decreased below the critical clearance. Using shear stress simulations and previously published work a theory is developed to support the experimental observations. The critical clearance depends on various HDI parameters and hence can be reduced through proper design of the interface. Comparison of critical clearance on CHx and CHxNy media indicates that presence of nitrogen is better for HDI as it reduces the critical clearance, which is found to increase with increasing lubricant molecular weight and in presence of additives X-1P and A20H. Further experiments maintaining a fixed slider-disk clearance suggest that two different mechanisms dominate the disk-to-slider and slider-to-disk lubricant transfer. One of the key factors influencing the slider stability at proximity is the disk topography, since it provides dynamic excitation to the low-flying sliders and strongly influences its dynamics. The effect of circumferential as well as radial disk topography is investigated using a new method to measure the 2-D (true) disk topography. Simulations using CMLAir dynamic simulator indicate a strong dependence on the circumferential roughness and waviness features as well as radial features, which have not been studied intensively till now. The simulations with 2-D disk topography are viewed as more realistic than the 1-D simulations. Further, it is also seen that the effect of the radial features can be reduced through effective ABS design. Finally, an attempt has been made to establish correlations between some of the proximity interactions as well as others which may affect the HDI reliability by creating a relational chart. Such an organization serves to give a bigger picture of the various efforts being made in the field of HDI reliability and link them together. From this chart, a causal relationship is suggested between the electrostatic, intermolecular and meniscus forces.

High-Temperature Lubricant Analyses Using the System for Thermal Diagnostic Studies (STDS). A Feasibility Study

DTIC Science & Technology

1990-07-01

permeation chromatography (GPC) have been applied to lubricant type samples. 8 Most recently the newly introduced supercritical fluid chromatography (SFC... fluids , such as lubricants and hydraulic fluids can also be examined using various inverse chromatography procedures. Another mode, known as reaction...introduction of new gaseous extraction techniques, e.g., supercritical fluid extraction, procedures such as IGC will probably be developed for vastly

Tribology needs for future space and aeronautical systems

NASA Technical Reports Server (NTRS)

Fusaro, Robert L.

1991-01-01

Future aeronautical and space missions will push tribology technology beyond its current capability. The objective is to discuss the current state of the art of tribology as it is applied to advanced aircraft and spacecraft. Areas of discussion include materials lubrication mechanisms, factors affecting lubrication, current and future tribological problem areas, potential new lubrication techniques, and perceived technology requirements that need to be met in order to solve these tribology problems.

Dry Lubrication of High Temperature Silicon Nitride Rolling Contacts.

DTIC Science & Technology

1980-11-01

comparable to M50 bearing steel [2]. Quality control measures were implemented in the areas of raw material inspection as well as non-destructive evaluation...to oil lubricated bearing steels . Due to the apparent success of graphite at high tem- perature, three vendors were selected that manufacture graph...hybrid bearings ( steel rings and silicon nitride balls) to establish solid lubricant/cage design practices. High temperature bearing tests with silicon

High-temperature lubricants. January 1970-January 1989 (Citations from the US Patent data base). Report for January 1970-January 1989

DOE Office of Scientific and Technical Information (OSTI.GOV)

Not Available

1989-02-01

This bibliography contains citations of selected patents concerning high-temperature synthetic and natural lubricating compositions. Thickening agents, thermal stabilizers, polymeric additives, antioxidants, and preservatives are included relative to such lubricants as greases, oils, and soaps. Methods of manufacturing and various applications are included. (This updated bibliography contains 80 citations, 12 of which are new entries to the previous edition.)

Materials as additives for advanced lubrication

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pol, Vilas G.; Thackeray, Michael M.; Mistry, Kuldeep

This invention relates to carbon-based materials as anti-friction and anti-wear additives for advanced lubrication purposes. The materials comprise carbon nanotubes suspended in a liquid hydrocarbon carrier. Optionally, the compositions further comprise a surfactant (e.g., to aid in dispersion of the carbon particles). Specifically, the novel lubricants have the ability to significantly lower friction and wear, which translates into improved fuel economies and longer durability of mechanical devices and engines.

Lubrication pressure and fractional viscous damping effects on the spring-block model of earthquakes

NASA Astrophysics Data System (ADS)

Tanekou, G. B.; Fogang, C. F.; Kengne, R.; Pelap, F. B.

2018-04-01

We examine the dynamical behaviours of the "single mass-spring" model for earthquakes considering lubrication pressure effects on pre-existing faults and viscous fractional damping. The lubrication pressure supports a part of the load, thereby reducing the normal stress and the associated friction across the gap. During the co-seismic phase, all of the strain accumulated during the inter-seismic duration does not recover; a fraction of this strain remains as a result of viscous relaxation. Viscous damping friction makes it possible to study rocks at depth possessing visco-elastic behaviours. At increasing depths, rock deformation gradually transitions from brittle to ductile. The fractional derivative is based on the properties of rocks, including information about previous deformation events ( i.e., the so-called memory effect). Increasing the fractional derivative can extend or delay the transition from stick-slip oscillation to a stable equilibrium state and even suppress it. For the single block model, the interactions of the introduced lubrication pressure and viscous damping are found to give rise to oscillation death, which corresponds to aseismic fault behaviour. Our result shows that the earthquake occurrence increases with increases in both the damping coefficient and the lubrication pressure. We have also revealed that the accumulation of large stresses can be controlled via artificial lubrication.

Investigating critical effects of variegated lubricants, glidants and hydrophilic additives on lag time of press coated ethylcellulose tablets.

PubMed

Patadia, Riddhish; Vora, Chintan; Mittal, Karan; Mashru, Rajashree

2016-01-01

The research envisaged focuses on vital impacts of variegated lubricants, glidants and hydrophilic additives on lag time of press coated ethylcellulose (EC) tablets using prednisone as a model drug. Several lubricants and glidants such as magnesium stearate, colloidal SiO2, sodium stearyl fumarate, talc, stearic acid, polyethylene glycol (6000) and glyceryl behenate were investigated to understand their effects on lag time by changing their concentrations in outer coat. Further, the effects of hydrophilic additives on lag time were examined for hydroxypropylmethylcellulose (E5), hydroxypropylcellulose (EF and SSL), povidone (K30), copovidone, polyethylene glycol (4000), lactose and mannitol. In vitro drug release testing revealed that each selected lubricant/glidant, if present even at concentration of 0.25% w/w, significantly reduced the lag time of press coated tablets. Specifically, colloidal SiO2 and/or magnesium stearate were detrimental while other lubricants/glidants were relatively less injurious. Among hydrophilic additives, freely water soluble fillers had utmost influence in lag time, whereas, comparatively less impact was observed with polymeric binders. Concisely, glidant and lubricant should be chosen to have minimal impact on lag time and further judicious selection of hydrophilic additives should be exercised for modulating lag time of pulsatile release formulations.

3D Imaging of Water-Drop Condensation on Hydrophobic and Hydrophilic Lubricant-Impregnated Surfaces

PubMed Central

Kajiya, Tadashi; Schellenberger, Frank; Papadopoulos, Periklis; Vollmer, Doris; Butt, Hans-Jürgen

2016-01-01

Condensation of water from the atmosphere on a solid surface is an ubiquitous phenomenon in nature and has diverse technological applications, e.g. in heat and mass transfer. We investigated the condensation kinetics of water drops on a lubricant-impregnated surface, i.e., a micropillar array impregnated with a non-volatile ionic liquid. Growing and coalescing drops were imaged in 3D using a laser scanning confocal microscope equipped with a temperature and humidity control. Different stages of condensation can be discriminated. On a lubricant-impregnated hydrophobic micropillar array these are: (1) Nucleation on the lubricant surface. (2) Regular alignment of water drops between micropillars and formation of a three-phase contact line on a bottom of the substrate. (3) Deformation and bridging by coalescence which eventually leads to a detachment of the drops from the bottom substrate. The drop-substrate contact does not result in breakdown of the slippery behaviour. Contrary, on a lubricant-impregnated hydrophilic micropillar array, the condensed water drops replace the lubricant. Consequently, the surface loses its slippery property. Our results demonstrate that a Wenzel-like to Cassie transition, required to maintain the facile removal of condensed water drops, can be induced by well-chosen surface hydrophobicity. PMID:27040483

Candidate Coatings and Dry Traction Drives for Planetary Vehicles

NASA Technical Reports Server (NTRS)

Fusaro, Robert; Oswald, Fred B.

2002-01-01

Robert Fusaro and Fred Oswald of the Mechanical Components Branch discussed 'Candidate Coatings and Dry Traction Drives for Planetary Vehicles'. Vehicles to be designed for exploration of planets and moons of the solar system will require reliable mechanical drives to operate efficiently. Long-term operation of these drives will be challenging because of extreme operating conditions. These extreme conditions include: very high and/or very cold temperatures, wide temperature ranges, dust, vacuum or low-pressure atmospheres, and corrosive environments. Most drives used on Earth involve oil-lubricated gears. However, due to the extreme conditions on planetary surfaces, it may not be advisable or even possible to use oil lubrication. Unfortunately, solid lubricants do not work well when applied to gears because of the high contact stress conditions and large sliding motion between the teeth, which cause wear and limit life. We believe traction drives will provide an attractive alternative to gear drives. Traction drives are composed of rollers that provide geometry more conducive to solid lubrication. Minimal slip occurs in this contact geometry and thus there is very low wear to the solid lubricant. The challenge for these solid-lubricated drives is finding materials or coatings that provide the required long-life while also providing high traction. We seek materials that provide low wear with high friction.

The effect of casein phosphopeptide-amorphous calcium phosphate on erosive dentine wear.

PubMed

Ranjitkar, S; Narayana, T; Kaidonis, J A; Hughes, T E; Richards, L C; Townsend, G C

2009-06-01

Erosive tooth wear is a growing concern in clinical dentistry. Our aims were to assess the effect of Tooth Mousse (TM) in managing erosive dentine wear in vitro. Opposing enamel and dentine specimens from 36 third molar teeth were worn under a load of 100 N for 75 000 cycles in electromechanical tooth wear machines. In experiment 1, TM was applied continuously at the wear interface and the mean dentine wear rate was compared with those of specimens subjected to continuous application of hydrochloric acid (HCl, pH 3.0) and deionized water (DW, pH 6.1) as lubricants. In experiment 2, specimens were subjected to TM application every 1600 cycles at both pH 3.0 and 6.1, and the mean dentine wear rates were compared with those of specimens worn with continuous application of HCl and DW lubricants. Dentine wear was reduced significantly with continuous application of TM compared with HCl and DW lubricants. Specimens prepared with continuous TM application displayed smooth wear facets, whereas more pronounced microwear details were observed with HCl and DW lubricants. Both remineralization and lubrication seem to contribute to reduction in dentine wear associated with TM application, although lubrication appears to have a more pronounced effect.

Lubrication of Space Shuttle Main Engine Turbopump Bearings

NASA Technical Reports Server (NTRS)

Gibson, Howard; Munafo, Paul (Technical Monitor)

2001-01-01

The Space Shuttle has three main engines that are used for propulsion into orbit. These engines are fed propellants by four turbopumps on each engine. A main element in the turbopump is the bearings supporting the rotor that spins the turbine blades and the pump impeller. These bearings are required to spin at very high speeds, support radial and thrust loads, and have high wear resistance without the benefit of lubrication. The liquid hydrogen and oxygen propellants flow through the bearings to cool the surfaces. The volatile nature of the propellants excludes any conventional means of lubrication. Lubrication for these bearings is provided by the ball separator inside the bearing. The separator is a composite material that supplies a transfer film of lubrication to the rings and balls. New separator materials and lubrication schemes have been investigated at Marshall Space Flight Center in a bearing test rig with promising results. Hybrid bearings with silicon nitride balls have also been evaluated. The use of hybrid, silicon nitride ball bearings in conjunction -with better separator materials has shown excellent results. The work that Marshall has done is being utilized in turbopumps flying on the space shuttle fleet and will be utilized in future space travel. This result of this work is valuable for all aerospace and commercial applications where high-speed bearings are used.

Tribological performance of quaternary CrSiCN coatings under dry and lubricated conditions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lorenzo-Martin, C.; Ajayi, O.; Erdemir, A.

This paper presents an experimental study of friction and wear performance of quaternary CrSiCN coatings deposited on a hardened H-13 steel substrate by a plasma enhanced magnetron sputtering (PEMS) technique. Friction and wear tests were conducted with a reciprocating line contact between a hardened 4370 steel roller and coated and uncoated flat specimens under dry and lubricated conditions. The effects of coating thickness (1, 3.5 and 7.5 μm) on the mechanical properties, friction and wear performance were also assessed. In dry sliding, the friction of coated surfaces was about the same as for uncoated surfaces, except for the 1-μm coating,more » which had higher friction. Friction for coated surfaces under lubricated contact was in general higher than for uncoated surfaces. There was no measurable wear on any of the coated surfaces, under either dry or lubricated conditions. However, wear was higher on the steel roller counterface sliding against the coated surfaces, with the amount of wear proportional to the mating coating thickness. The effectiveness of formulated lubricant additives was also modified by the coating, resulting in major effects on friction and wear behavior. Finally, this reduction in lubricant additive efficacy is due to the fact that the additives were designed and optimized for ferrous surfaces.« less

Determination of Actual Friction Factors in Metal Forming under Heavy Loaded Regimes Combining Experimental and Numerical Analysis.

PubMed

Camacho, Ana María; Veganzones, Mariano; Claver, Juan; Martín, Francisco; Sevilla, Lorenzo; Sebastián, Miguel Ángel

2016-09-01

Tribological conditions can change drastically during heavy loaded regimes as experienced in metal forming; this is especially critical when lubrication can only be applied at the early stage of the process because the homogeneous lubricant layer can break along the die-workpiece interface. In these cases, adopting a constant friction factor for the lubricant-surface pair may not be a valid assumption. This paper presents a procedure based on the use of dual friction factor maps to determine friction factors employed in heavy loaded regimes. A finite element (FE) simulation is used to obtain the friction factor map for the alloy UNS A96082. Experiments were conducted using four lubricants (aluminum anti-size, MoS₂ grease, silicone oil, and copper paste) to determine the actual friction curves. The experimental procedure is based on the application of lubricant only at the beginning of the first stage of ring compression, and not at intermediate stages as is usual in typical ring compression tests (RCTs). The results show that for small reductions ( r h < 20%), the conventional RCT can be applied because the tribological conditions remain similar. For large reductions ( r h > 20%), it is recommended to obtain an average value of the friction factor for every lubricant-surface pair in the range of deformation considered.

Layered Double Hydroxide Nanoplatelets with Excellent Tribological Properties under High Contact Pressure as Water-Based Lubricant Additives

PubMed Central

Wang, Hongdong; Liu, Yuhong; Chen, Zhe; Wu, Bibo; Xu, Sailong; Luo, Jianbin

2016-01-01

High efficient and sustainable utilization of water-based lubricant is essential for saving energy. In this paper, a kind of layered double hydroxide (LDH) nanoplatelets is synthesized and well dispersed in water due to the surface modification with oleylamine. The excellent tribological properties of the oleylamine-modified Ni-Al LDH (NiAl-LDH/OAm) nanoplatelets as water-based lubricant additives are evaluated by the tribological tests in an aqueous environment. The modified LDH nanoplatelets are found to not only reduce the friction but also enhance the wear resistance, compared with the water-based cutting fluid and lubricants containing other particle additives. By adding 0.5 wt% LDH nanoplatelets, under 1.5 GPa initial contact pressure, the friction coefficient, scar diameter, depth and width of the wear track dramatically decrease by 83.1%, 43.2%, 88.5% and 59.5%, respectively. It is considered that the sufficiently small size and the excellent dispersion of NiAl-LDH/OAm nanoplatelets in water are the key factors, so as to make them enter the contact area, form a lubricating film and prevent direct collision of asperity peaks. Our investigations demonstrate that the LDH nanoplatelet as a water-based lubricant additive has a great potential value in industrial application. PMID:26951794

Layered Double Hydroxide Nanoplatelets with Excellent Tribological Properties under High Contact Pressure as Water-Based Lubricant Additives.

PubMed

Wang, Hongdong; Liu, Yuhong; Chen, Zhe; Wu, Bibo; Xu, Sailong; Luo, Jianbin

2016-03-08

High efficient and sustainable utilization of water-based lubricant is essential for saving energy. In this paper, a kind of layered double hydroxide (LDH) nanoplatelets is synthesized and well dispersed in water due to the surface modification with oleylamine. The excellent tribological properties of the oleylamine-modified Ni-Al LDH (NiAl-LDH/OAm) nanoplatelets as water-based lubricant additives are evaluated by the tribological tests in an aqueous environment. The modified LDH nanoplatelets are found to not only reduce the friction but also enhance the wear resistance, compared with the water-based cutting fluid and lubricants containing other particle additives. By adding 0.5 wt% LDH nanoplatelets, under 1.5 GPa initial contact pressure, the friction coefficient, scar diameter, depth and width of the wear track dramatically decrease by 83.1%, 43.2%, 88.5% and 59.5%, respectively. It is considered that the sufficiently small size and the excellent dispersion of NiAl-LDH/OAm nanoplatelets in water are the key factors, so as to make them enter the contact area, form a lubricating film and prevent direct collision of asperity peaks. Our investigations demonstrate that the LDH nanoplatelet as a water-based lubricant additive has a great potential value in industrial application.

Cost-Cutting Powdered Lubricant

NASA Technical Reports Server (NTRS)

2005-01-01

Scientists at NASA's Glenn Research Center developed a high-temperature, solid lubricant coating material that is saving the manufacturing industry millions of dollars. The material came out of 3 decades of tribological research, work studying high-temperature friction, lubrication, and the wearing of interacting surfaces that are in relative motion. It was developed as a shaft coating deposited by thermal spraying to protect foil air bearings used in oil-free turbomachinery, like gas turbines, and is meant to be part of a larger project: an oil-free aircraft engine capable of operating at high temperatures with increased reliability, lowered weight, reduced maintenance requirements, and increased power. This advanced coating, PS300, is a self-lubricating bearing material containing chromium oxide, with additions of a low-temperature start up lubricant (silver) and a high-temperature lubricant, making it remarkably stable at high temperatures, and better suited than previously available materials for high-stress conditions. It improves efficiency, lowers friction, reduces emissions, and has been used by NASA in advanced aeropropulsion engines, refrigeration compressors, turbochargers, and hybrid electrical turbogenerators. PS300 is ideal in any application where lowered weight and reduced maintenance are desired, and high-temperature uses and heavy operating speeds are expected. It has notable uses for the Space Agency, but it has even further-reaching potential for the industrial realm.

A Systems Biology Approach to Synovial Joint Lubrication in Health, Injury, and Disease

PubMed Central

Hui, Alexander Y.; McCarty, William J.; Masuda, Koichi; Firestein, Gary S.; Sah, Robert L.

2013-01-01

The synovial joint contains synovial fluid (SF) within a cavity bounded by articular cartilage and synovium. SF is a viscous fluid that has lubrication, metabolic, and regulatory functions within synovial joints. SF contains lubricant molecules, including proteoglycan-4 and hyaluronan. SF is an ultrafiltrate of plasma with secreted contributions from cell populations lining and within the synovial joint space, including chondrocytes and synoviocytes. Maintenance of normal SF lubricant composition and function are important for joint homeostasis. In osteoarthritis, rheumatoid arthritis, and joint injury, changes in lubricant composition and function accompany alterations in the cytokine and growth factor environment and increased fluid and molecular transport through joint tissues. Thus, understanding the synovial joint lubrication system requires a multi-faceted study of the various parts of the synovial joint and their interactions. Systems biology approaches at multiple scales are being used to describe the molecular, cellular, and tissue components and their interactions that comprise the functioning synovial joint. Analyses of the transcriptome and proteome of SF, cartilage, and synovium suggest that particular molecules and pathways play important roles in joint homeostasis and disease. Such information may be integrated with physicochemical tissue descriptions to construct integrative models of the synovial joint that ultimately may explain maintenance of health, recovery from injury, or development and progression of arthritis. PMID:21826801

Determination of Actual Friction Factors in Metal Forming under Heavy Loaded Regimes Combining Experimental and Numerical Analysis

PubMed Central

Camacho, Ana María; Veganzones, Mariano; Claver, Juan; Martín, Francisco; Sevilla, Lorenzo; Sebastián, Miguel Ángel

2016-01-01

Tribological conditions can change drastically during heavy loaded regimes as experienced in metal forming; this is especially critical when lubrication can only be applied at the early stage of the process because the homogeneous lubricant layer can break along the die-workpiece interface. In these cases, adopting a constant friction factor for the lubricant-surface pair may not be a valid assumption. This paper presents a procedure based on the use of dual friction factor maps to determine friction factors employed in heavy loaded regimes. A finite element (FE) simulation is used to obtain the friction factor map for the alloy UNS A96082. Experiments were conducted using four lubricants (aluminum anti-size, MoS2 grease, silicone oil, and copper paste) to determine the actual friction curves. The experimental procedure is based on the application of lubricant only at the beginning of the first stage of ring compression, and not at intermediate stages as is usual in typical ring compression tests (RCTs). The results show that for small reductions (rh < 20%), the conventional RCT can be applied because the tribological conditions remain similar. For large reductions (rh > 20%), it is recommended to obtain an average value of the friction factor for every lubricant-surface pair in the range of deformation considered. PMID:28773868

Tribological performance of quaternary CrSiCN coatings under dry and lubricated conditions

DOE PAGES

Lorenzo-Martin, C.; Ajayi, O.; Erdemir, A.; ...

2017-06-15

This paper presents an experimental study of friction and wear performance of quaternary CrSiCN coatings deposited on a hardened H-13 steel substrate by a plasma enhanced magnetron sputtering (PEMS) technique. Friction and wear tests were conducted with a reciprocating line contact between a hardened 4370 steel roller and coated and uncoated flat specimens under dry and lubricated conditions. The effects of coating thickness (1, 3.5 and 7.5 μm) on the mechanical properties, friction and wear performance were also assessed. In dry sliding, the friction of coated surfaces was about the same as for uncoated surfaces, except for the 1-μm coating,more » which had higher friction. Friction for coated surfaces under lubricated contact was in general higher than for uncoated surfaces. There was no measurable wear on any of the coated surfaces, under either dry or lubricated conditions. However, wear was higher on the steel roller counterface sliding against the coated surfaces, with the amount of wear proportional to the mating coating thickness. The effectiveness of formulated lubricant additives was also modified by the coating, resulting in major effects on friction and wear behavior. Finally, this reduction in lubricant additive efficacy is due to the fact that the additives were designed and optimized for ferrous surfaces.« less

Methods of Measuring Vapor Pressures of Lubricants With Their Additives Using TGA and/or Microbalances

NASA Technical Reports Server (NTRS)

Scialdone, John J.; Miller, Michael K.; Montoya, Alex F.

1996-01-01

The life of a space system may be critically dependent on the lubrication of some of its moving parts. The vapor pressure, the quantity of the available lubricant, the temperature and the exhaust venting conductance passage are important considerations in the selection and application of a lubricant. In addition, the oil additives employed to provide certain properties of low friction, surface tension, antioxidant and load bearing characteristics, are also very important and need to be known with regard to their amounts and vapor pressures. This paper reports on the measurements and analyses carried out to obtain those parameters for two often employed lubricants, the Apiezon(TM)-C and the Krytox(TM) AB. The measurements were made employing an electronic microbalance and a thermogravimetric analyzer (TGA) modified to operate in a vacuum. The results have been compared to other data on these oils when available. The identification of the mass fractions of the additives in the oil and their vapor pressures as a function of the temperature were carried out. These may be used to estimate the lubricant life given its quantity and the system vent exhaust conductance. It was found that the Apiezon(TM)-C has three main components with different rates of evaporation while the Krytox(TM) did not indicate any measurable additive.

Model-based diagnostics of gas turbine engine lubrication systems

DOE Office of Scientific and Technical Information (OSTI.GOV)

Byington, C.S.

1998-09-01

The objective of the current research was to develop improved methodology for diagnosing anomalies and maintaining oil lubrication systems for gas turbine engines. The effort focused on the development of reasoning modules that utilize the existing, inexpensive sensors and are applicable to on-line monitoring within the full-authority digital engine controller (FADEC) of the engine. The target application is the Enhanced TF-40B gas turbine engine that powers the Landing Craft Air Cushion (LCAC) platform. To accomplish the development of the requisite data fusion algorithms and automated reasoning for the diagnostic modules, Penn State ARL produced a generic Turbine Engine Lubrication Systemmore » Simulator (TELSS) and Data Fusion Workbench (DFW). TELSS is a portable simulator code that calculates lubrication system parameters based upon one-dimensional fluid flow resistance network equations. Validation of the TF- 40B modules was performed using engineering and limited test data. The simulation model was used to analyze operational data from the LCAC fleet. The TELSS, as an integral portion of the DFW, provides the capability to experiment with combinations of variables and feature vectors that characterize normal and abnormal operation of the engine lubrication system. The model-based diagnostics approach is applicable to all gas turbine engines and mechanical transmissions with similar pressure-fed lubrication systems.« less

Direct numerical simulation of turbulent channel flow over a liquid-infused micro-grooved surface

NASA Astrophysics Data System (ADS)

Chang, Jaehee; Jung, Taeyong; Choi, Haecheon; Kim, John

2016-11-01

Recently a superhydrophobic surface has drawn much attention as a passive device to achieve high drag reduction. Despite the high performance promised at ideal conditions, maintaining the interface in real flow conditions is an intractable problem. A non-wetting surface, known as the slippery liquid-infused porous surface (SLIPS) or the lubricant-impregnated surface (LIS), has shown a potential for drag reduction, as the working fluid slips at the interface but cannot penetrate into the lubricant layer. In the present study, we perform direct numerical simulation of turbulent channel flow over a liquid-infused micro-grooved surface to investigate the effects of this surface on the interfacial slip and drag reduction. The flow rate of water is maintained constant corresponding to Reτ 180 in a fully developed turbulent channel flow, and the lubricant layer is shear-driven by the turbulent water flow. The lubricant layer is also simulated with the assumption that the interface is flat (i.e. the surface tension effect is neglected). The solid substrate in which the lubricant is infused is modelled as straight ridges using an immersed boundary method. DNS results show that drag reduction by the liquid-infused surface is highly dependent on the viscosity of the lubricant.

MIL-L-87177 and CLT:X-10 Lubricants Improve Electrical Connector Fretting Corrosion Behavior

DOE Office of Scientific and Technical Information (OSTI.GOV)

AUKLAND,NEIL R.; HANLON,JAMES T.

1999-10-12

We have conducted a fretting research project using MIL-L-87177 and CLT: X-10 lubricants on Nano-miniature connectors. When they were fretted without lubricant, individual connectors first exceeded our 0.5 ohm failure criteria from 2,341 to 45,238 fretting cycles. With additional fretting, their contact resistance increased to more than 100,000 ohms. Unmodified MIL-L-87177 lubricant delayed the onset of first failure to between 430,000 and over 20,000,000 fretting cycles. MIL-L-87177 modified by addition of Teflon powder delayed first failure to beyond 5 million fretting cycles. Best results were obtained when Teflon was used and also when both the straight and modified lubricants weremore » poured into and then out of the connector. CLT: X-10 lubricant delayed the onset of first failure to beyond 55 million cycles in one test where a failure was actually observed and to beyond 20 million cycles in another that was terminated without failure. CLT: X-10 recovered an unlubricated connector driven deeply into failure, with six failed pins recovering immediately and four more recovering during an additional 420 thousand fretting cycles. MIL-L-87177 was not able to recover a connector under similar conditions.« less

Effect of laser surface texturing (LST) on tribochemical films dynamics and friction and wear performance

DOE PAGES

Olofinjana, Bolutife; Lorenzo-Martin, Cinta; Ajayi, Oyelayo O.; ...

2015-06-06

Surface texturing or topographical design is one of the primary techniques to control friction and wear performance of surfaces in tribological contact. Laser surface texturing (LST), whereby a laser beam is used to produce regular arrays of dimples on a surface, has been demonstrated to reduce friction in conformal lubricated contacts. Friction and wear behavior under boundary lubrication is also known to be dependent on the formation and durability of the tribochemical film formed from lubricant additives. In this paper, the effects of LST on the formation and durability of tribochemical films and its consequent impacts on friction and wearmore » behavior in various lubrication regimes were evaluated. Friction and wear tests that cycled through different lubrication regimes were conducted with both polished and LST treated surfaces using a synthetic lubricant with and without model additives of ZDDP and MoDTC mixture. In the base oil without additives, LST produced noticeable reduction in friction in all lubrication regimes. However, with low-friction model additives, friction was higher in tests with LST due to significant differences in the tribochemical film formation in the polished and LST surfaces, as well as the sliding counterface. Continuous tribo-films were formed on ball conterface rubbed against polished surfaces while the films were streaky and discontinuous in ball rubbed against LST surfaces. LST produced more wear on the ball counterface in both base and additized oils. Lastly, no measurable wear was observed in both the polished and LST flat specimens.« less