Review of current neutron detection systems for emergency response

NASA Astrophysics Data System (ADS)

Mukhopadhyay, Sanjoy; Maurer, Richard; Guss, Paul; Kruschwitz, Craig

2014-09-01

Neutron detectors are used in a myriad of applications—from safeguarding special nuclear materials (SNM) to determining lattice spacing in soft materials. The transformational changes taking place in neutron detection and imaging techniques in the last few years are largely being driven by the global shortage of helium-3 (3He). This article reviews the status of neutron sensors used specifically for SNM detection in radiological emergency response. These neutron detectors must be highly efficient, be rugged, have fast electronics to measure neutron multiplicity, and be capable of measuring direction of the neutron sources and possibly image them with high spatial resolution. Neutron detection is an indirect physical process: neutrons react with nuclei in materials to initiate the release of one or more charged particles that produce electric signals that can be processed by the detection system. Therefore, neutron detection requires conversion materials as active elements of the detection system; these materials may include boron-10 (10B), lithium-6 (6Li), and gadollinium-157 (157Gd), to name a few, but the number of materials available for neutron detection is limited. However, in recent years, pulse-shape-discriminating plastic scintillators, scintillators made of helium-4 (4He) under high pressure, pillar and trench semiconductor diodes, and exotic semiconductor neutron detectors made from uranium oxide and other materials have widely expanded the parameter space in neutron detection methodology. In this article we will pay special attention to semiconductor-based neutron sensors. Modern microfabricated nanotubes covered inside with neutron converter materials and with very high aspect ratios for better charge transport will be discussed.

Remote laser drilling and sampling system for the detection of concealed explosives

NASA Astrophysics Data System (ADS)

Wild, D.; Pschyklenk, L.; Theiß, C.; Holl, G.

2017-05-01

The detection of hazardous materials like explosives is a central issue in national security in the field of counterterrorism. One major task includes the development of new methods and sensor systems for the detection. Many existing remote or standoff methods like infrared or raman spectroscopy find their limits, if the hazardous material is concealed in an object. Imaging technologies using x-ray or terahertz radiation usually yield no information about the chemical content itself. However, the exact knowledge of the real threat potential of a suspicious object is crucial for disarming the device. A new approach deals with a laser drilling and sampling system for the use as verification detector for suspicious objects. Central part of the system is a miniaturised, diode pumped Nd:YAG laser oscillator-amplifier. The system allows drilling into most materials like metals, synthetics or textiles with bore hole diameters in the micron scale. During the drilling process, the hazardous material can be sampled for further investigation with suitable detection methods. In the reported work, laser induced breakdown spectroscopy (LIBS) is used to monitor the drilling process and to classify the drilled material. Also experiments were carried out to show the system's ability to not ignite even sensitive explosives like triacetone triperoxide (TATP). The detection of concealed hazardous material is shown for different explosives using liquid chromatography and ion mobility spectrometry.

Double-pulse standoff laser-induced breakdown spectroscopy for versatile hazardous materials detection

NASA Astrophysics Data System (ADS)

Gottfried, Jennifer L.; De Lucia, Frank C.; Munson, Chase A.; Miziolek, Andrzej W.

2007-12-01

We have developed a double-pulse standoff laser-induced breakdown spectroscopy (ST-LIBS) system capable of detecting a variety of hazardous materials at tens of meters. The use of a double-pulse laser improves the sensitivity and selectivity of ST-LIBS, especially for the detection of energetic materials. In addition to various metallic and plastic materials, the system has been used to detect bulk explosives RDX and Composition-B, explosive residues, biological species such as the anthrax surrogate Bacillus subtilis, and chemical warfare simulants at 20 m. We have also demonstrated the discrimination of explosive residues from various interferents on an aluminum substrate.

Development of Measurement Methods for Detection of Special Nuclear Materials using D-D Pulsed Neutron Source

NASA Astrophysics Data System (ADS)

Misawa, Tsuyoshi; Takahashi, Yoshiyuki; Yagi, Takahiro; Pyeon, Cheol Ho; Kimura, Masaharu; Masuda, Kai; Ohgaki, Hideaki

2015-10-01

For detection of hidden special nuclear materials (SNMs), we have developed an active neutron-based interrogation system combined with a D-D fusion pulsed neutron source and a neutron detection system. In the detection scheme, we have adopted new measurement techniques simultaneously; neutron noise analysis and neutron energy spectrum analysis. The validity of neutron noise analysis method has been experimentally studied in the Kyoto University Critical Assembly (KUCA), and was applied to a cargo container inspection system by simulation.

Development of a Dual-Particle Imaging System for Nonproliferation Applications

NASA Astrophysics Data System (ADS)

Poitrasson-Riviere, Alexis Pierre Valere

A rising concern in our society is preventing the proliferation of nuclear weapons and fissionable material. This prevention can be incorporated at multiple levels, from the use of nuclear safeguards in nuclear facilities to the detection of threat objects in the field. At any level, systems used for such tasks need to be specially designed for use with Special Nuclear Material (SNM) which is defined by the NRC as plutonium and uranium enriched in U-233 or U-235 isotopes. These radioactive materials have the particularity of emitting both fast neutrons and gamma rays; thus, systems able to detect both particles simultaneously are particularly desirable. In the field of nuclear nonproliferation and safeguards, detection systems capable of accurately imaging various sources of radiation can greatly simplify any monitoring or detection task. The localization of the radiation sources can allow users of the system to focus their efforts on the areas of interest, whether it be for radiation detection or radiation characterization. This thesis describes the development of a dual-particle imaging system at the University of Michigan to address these technical challenges. The imaging system relies on the use of organic liquid scintillators that can detect both fast neutrons and gamma rays, and inorganic NaI(Tl) scintillators that are not very sensitive to neutrons yet yield photoelectric absorptions from gamma rays. A prototype of the imaging system has been constructed and operated. The system will aid the remote monitoring of nuclear materials within facilities, and it has the scalability for standoff detection in the field. A software suite has been developed to analyze measured data in real time, in an effort to obtain a system as close to field-ready as possible. The system's performance has been tested with various materials of interest, such as MOX and plutonium metal, measured at the PERLA facility of the Joint Research Center in Ispra, Italy. The robust and versatile imaging system is an attractive alternative to the current imaging systems.

Lightning Protection and Detection System

NASA Technical Reports Server (NTRS)

Mielnik, John J. (Inventor); Woodard, Marie (Inventor); Smith, Laura J. (Inventor); Wang, Chuantong (Inventor); Koppen, Sandra V. (Inventor); Dudley, Kenneth L. (Inventor); Szatkowski, George N. (Inventor); Nguyen, Truong X. (Inventor); Ely, Jay J. (Inventor)

2017-01-01

A lightning protection and detection system includes a non-conductive substrate material of an apparatus; a sensor formed of a conductive material and deposited on the non-conductive substrate material of the apparatus. The sensor includes a conductive trace formed in a continuous spiral winding starting at a first end at a center region of the sensor and ending at a second end at an outer corner region of the sensor, the first and second ends being open and unconnected. An electrical measurement system is in communication with the sensor and receives a resonant response from the sensor, to perform detection, in real-time, of lightning strike occurrences and damage therefrom to the sensor and the non-conductive substrate material.

Active Neutron-Based Interrogation System with D-D Neutron Source for Detection of Special Nuclear Materials

NASA Astrophysics Data System (ADS)

Takahashi, Y.; Misawa, T.; Yagi, T.; Pyeon, C. H.; Kimura, M.; Masuda, K.; Ohgaki, H.

2015-10-01

The detection of special nuclear materials (SNM) is an important issue for nuclear security. The interrogation systems used in a sea port and an airport are developed in the world. The active neutron-based interrogation system is the one of the candidates. We are developing the active neutron-based interrogation system with a D-D fusion neutron source for the nuclear security application. The D-D neutron source is a compact discharge-type fusion neutron source called IEC (Inertial-Electrostatic Confinement fusion) device which provides 2.45 MeV neutrons. The nuclear materials emit the highenergy neutrons by fission reaction. High-energy neutrons with energies over 2.45 MeV amount to 30% of all the fission neutrons. By using the D-D neutron source, the detection of SNMs is considered to be possible with the attention of fast neutrons if there is over 2.45 MeV. Ideally, neutrons at En>2.45 MeV do not exist if there is no nuclear materials. The detection of fission neutrons over 2.45 MeV are hopeful prospect for the detection of SNM with a high S/N ratio. In the future, the experiments combined with nuclear materials and a D-D neutron source will be conducted. Furthermore, the interrogation system will be numerically investigated by using nuclear materials, a D-D neutron source, and a steel container.

Early distinction system of mine fire in underground by using a neural-network system

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ohga, Kotaro; Higuchi, Kiyoshi

1996-12-31

In our laboratory, a new detection system using smell detectors was developed to detect the spontaneous combustion of coal and the combustion of other materials used underground. The results of experiments clearly the combustion of materials can be detected earlier by this detection system than by conventional detectors for gas and smoke, and there were significant differences between output data from each smell detector for coal, rubber, oil and wood. In order to discern the source of combustion gases, we have been developing a distinction system using a neural-network system. It has shown successful results in laboratory tests. This papermore » describes our detection system using smell detectors and our distinction system which uses a neural-network system, and presents results of experiments using both systems.« less

46 CFR 161.002-15 - Sample extraction smoke detection systems.

Code of Federal Regulations, 2010 CFR

2010-10-01

... 46 Shipping 6 2010-10-01 2010-10-01 false Sample extraction smoke detection systems. 161.002-15..., CONSTRUCTION, AND MATERIALS: SPECIFICATIONS AND APPROVAL ELECTRICAL EQUIPMENT Fire-Protective Systems § 161.002-15 Sample extraction smoke detection systems. The smoke detecting system must consist of a means for...

Systems and methods for neutron detection using scintillator nano-materials

DOEpatents

Letant, Sonia Edith; Wang, Tzu-Fang

2016-03-08

In one embodiment, a neutron detector includes a three dimensional matrix, having nanocomposite materials and a substantially transparent film material for suspending the nanocomposite materials, a detector coupled to the three dimensional matrix adapted for detecting a change in the nanocomposite materials, and an analyzer coupled to the detector adapted for analyzing the change detected by the detector. In another embodiment, a method for detecting neutrons includes receiving radiation from a source, converting neutrons in the radiation into alpha particles using converter material, converting the alpha particles into photons using quantum dot emitters, detecting the photons, and analyzing the photons to determine neutrons in the radiation.

10 CFR 73.25 - Performance capabilities for physical protection of strategic special nuclear material in transit.

Code of Federal Regulations, 2013 CFR

2013-01-01

... as conditions warrant. (2) Detect and delay any unauthorized attempt to gain access or introduce... of § 73.20(a). (3) Detect attempts to gain unauthorized access or introduce unauthorized materials... system shall: (1) Detect attempts to gain unauthorized entry or introduce unauthorized materials into...

10 CFR 73.25 - Performance capabilities for physical protection of strategic special nuclear material in transit.

Code of Federal Regulations, 2010 CFR

2010-01-01

... as conditions warrant. (2) Detect and delay any unauthorized attempt to gain access or introduce... of § 73.20(a). (3) Detect attempts to gain unauthorized access or introduce unauthorized materials... system shall: (1) Detect attempts to gain unauthorized entry or introduce unauthorized materials into...

10 CFR 73.25 - Performance capabilities for physical protection of strategic special nuclear material in transit.

Code of Federal Regulations, 2014 CFR

2014-01-01

... as conditions warrant. (2) Detect and delay any unauthorized attempt to gain access or introduce... of § 73.20(a). (3) Detect attempts to gain unauthorized access or introduce unauthorized materials... system shall: (1) Detect attempts to gain unauthorized entry or introduce unauthorized materials into...

Apparatus and method for transient thermal infrared spectrometry of flowable enclosed materials

DOEpatents

McClelland, John F.; Jones, Roger W.

1993-03-02

A method and apparatus for enabling analysis of a flowable material enclosed in a transport system having an infrared transparent wall portion. A temperature differential is transiently generated between a thin surface layer portion of the material and a lower or deeper portion of the material sufficient to alter the thermal infrared emission spectrum of the material from the black-body thermal infrared emission spectrum of the material, and the altered thermal infrared emission spectrum is detected through the infrared transparent portion of the transport system while the altered thermal infrared emission spectrum is sufficiently free of self-absorption by the material of emitted infrared radiation. The detection is effected prior to the temperature differential propagating into the lower or deeper portion of the material to an extent such that the altered thermal infrared emission spectrum is no longer sufficiently free of self-absorption by the material of emitted infrared radiation. By such detection, the detected altered thermal infrared emission spectrum is indicative of characteristics relating to molecular composition of the material.

The image enhancement and region of interest extraction of lobster-eye X-ray dangerous material inspection system

NASA Astrophysics Data System (ADS)

Zhan, Qi; Wang, Xin; Mu, Baozhong; Xu, Jie; Xie, Qing; Li, Yaran; Chen, Yifan; He, Yanan

2016-10-01

Dangerous materials inspection is an important technique to confirm dangerous materials crimes. It has significant impact on the prohibition of dangerous materials-related crimes and the spread of dangerous materials. Lobster-Eye Optical Imaging System is a kind of dangerous materials detection device which mainly takes advantage of backscatter X-ray. The strength of the system is its applicability to access only one side of an object, and to detect dangerous materials without disturbing the surroundings of the target material. The device uses Compton scattered x-rays to create computerized outlines of suspected objects during security detection process. Due to the grid structure of the bionic object glass, which imitate the eye of a lobster, grids contribute to the main image noise during the imaging process. At the same time, when used to inspect structured or dense materials, the image is plagued by superposition artifacts and limited by attenuation and noise. With the goal of achieving high quality images which could be used for dangerous materials detection and further analysis, we developed effective image process methods applied to the system. The first aspect of the image process is the denoising and enhancing edge contrast process, during the process, we apply deconvolution algorithm to remove the grids and other noises. After image processing, we achieve high signal-to-noise ratio image. The second part is to reconstruct image from low dose X-ray exposure condition. We developed a kind of interpolation method to achieve the goal. The last aspect is the region of interest (ROI) extraction process, which could be used to help identifying dangerous materials mixed with complex backgrounds. The methods demonstrated in the paper have the potential to improve the sensitivity and quality of x-ray backscatter system imaging.

Method of Fault Detection and Rerouting

NASA Technical Reports Server (NTRS)

Gibson, Tracy L. (Inventor); Medelius, Pedro J. (Inventor); Lewis, Mark E. (Inventor)

2013-01-01

A system and method for detecting damage in an electrical wire, including delivering at least one test electrical signal to an outer electrically conductive material in a continuous or non-continuous layer covering an electrically insulative material layer that covers an electrically conductive wire core. Detecting the test electrical signals in the outer conductive material layer to obtain data that is processed to identify damage in the outer electrically conductive material layer.

Fission meter and neutron detection using poisson distribution comparison

DOEpatents

Rowland, Mark S; Snyderman, Neal J

2014-11-18

A neutron detector system and method for discriminating fissile material from non-fissile material wherein a digital data acquisition unit collects data at high rate, and in real-time processes large volumes of data directly into information that a first responder can use to discriminate materials. The system comprises counting neutrons from the unknown source and detecting excess grouped neutrons to identify fission in the unknown source. Comparison of the observed neutron count distribution with a Poisson distribution is performed to distinguish fissile material from non-fissile material.

Optical methods and systems for detecting a constituent in a gas containing oxygen in harsh environments

DOEpatents

Carpenter, Michael A [Scotia, NY; Sirinakis, George [Bronx, NY

2011-01-04

A method for detecting a gas phase constituent such as carbon monoxide, nitrogen dioxide, hydrogen, or hydrocarbons in a gas comprising oxygen such as air, includes providing a sensing material or film having a metal embedded in a catalytically active matrix such as gold embedded in a yttria stabilized zirconia (YSZ) matrix. The method may include annealing the sensing material at about 900.degree. C., exposing the sensing material and gas to a temperature above 400.degree. C., projecting light onto the sensing material, and detecting a change in the absorption spectrum of the sensing material due to the exposure of the sensing material to the gas in air at the temperature which causes a chemical reaction in the sensing material compared to the absorption spectrum of the sensing material in the absence of the gas. Systems employing such a method are also disclosed.

Time encoded radiation imaging

DOEpatents

Marleau, Peter; Brubaker, Erik; Kiff, Scott

2014-10-21

The various technologies presented herein relate to detecting nuclear material at a large stand-off distance. An imaging system is presented which can detect nuclear material by utilizing time encoded imaging relating to maximum and minimum radiation particle counts rates. The imaging system is integrated with a data acquisition system that can utilize variations in photon pulse shape to discriminate between neutron and gamma-ray interactions. Modulation in the detected neutron count rates as a function of the angular orientation of the detector due to attenuation of neighboring detectors is utilized to reconstruct the neutron source distribution over 360 degrees around the imaging system. Neutrons (e.g., fast neutrons) and/or gamma-rays are incident upon scintillation material in the imager, the photons generated by the scintillation material are converted to electrical energy from which the respective neutrons/gamma rays can be determined and, accordingly, a direction to, and the location of, a radiation source identified.

Material-specific detection and classification of single nanoparticles

PubMed Central

Person, Steven; Deutsch, Bradley; Mitra, Anirban; Novotny, Lukas

2010-01-01

Detection and classification of nanoparticles is important for environmental monitoring, contamination mitigation, biological label tracking, and bio-defense. Detection techniques involve a trade-off between sensitivity, discrimination, and speed. This paper presents a material-specific dual-color common-path interferometric detection system. Two wavelengths are simultaneously used to discriminate between 60 nm silver and 80 nm diameter gold particles in solution with a detection time of τ ≈ 1 ms. The detection technique is applicable to situations where both particle size and material are of interest. PMID:21142033

Trace material detection of surfaces via single-beam femtosecond MCARS

NASA Astrophysics Data System (ADS)

Bowman Pilkington, Sherrie S.; Roberson, Stephen D.; Pellegrino, Paul M.

2016-05-01

There is a significant need for the development of optical diagnostics for rapid and accurate detection of chemical species in convoluted systems. In particular, chemical warfare agents and explosive materials are of interest, however, identification of these species is difficult for a wide variety of reasons. Low vapor pressures, for example, cause traditional Raman scattering to be ineffective due to the incredibly long signal collection times that are required. Multiplex Coherent Anti-Stokes Raman Scattering (MCARS) spectroscopy generates a complete Raman spectrum from the material of interest using a combination of a broadband pulse which drives multiple molecular vibrations simultaneously and a narrow band probe pulse. For most species, the complete Raman spectrum can be detected in milliseconds; this makes MCARS an excellent technique for trace material detection in complex systems. In this paper, we present experimental MCARS results on solid state chemical species in complex systems. The 40fs Ti:Sapphire laser used in this study has sufficient output power to produce both the broadband continuum pulse and narrow band probe pulse simultaneously. A series of explosive materials of interest have been identified and compared with spontaneous Raman spectra, showing the specificity and stability of this system.

Performance estimation for threat detection in CT systems

NASA Astrophysics Data System (ADS)

Montgomery, Trent; Karl, W. Clem; Castañón, David A.

2017-05-01

Detecting the presence of hazardous materials in suitcases and carry-on luggage is an important problem in aviation security. As the set of threats is expanding, there is a corresponding need to increase the capabilities of explosive detection systems to address these threats. However, there is a lack of principled tools for predicting the performance of alternative designs for detection systems. In this paper, we describe an approach for computing bounds on the achievable classification performance of material discrimination systems based on empirical statistics that estimate the f-divergence of the underlying features. Our approach can be used to examine alternative physical observation modalities and measurement configurations, as well as variations in reconstruction and feature extraction algorithms.

Characterization of polymorphic states in energetic samples of 1,3,5-trinitro-1,3,5-triazine (RDX) fabricated using drop-on-demand inkjet technology.

PubMed

Emmons, Erik D; Farrell, Mikella E; Holthoff, Ellen L; Tripathi, Ashish; Green, Norman; Moon, Raphael P; Guicheteau, Jason A; Christesen, Steven D; Pellegrino, Paul M; Fountain, Augustus W

2012-06-01

The United States Army and the first responder community are evaluating optical detection systems for the trace detection of hazardous energetic materials. Fielded detection systems must be evaluated with the appropriate material concentrations to accurately identify the residue in theater. Trace levels of energetic materials have been observed in mutable polymorphic phases and, therefore, the systems being evaluated must be able to detect and accurately identify variant sample phases observed in spectral data. In this work, we report on the novel application of drop-on-demand technology for the fabrication of standardized trace 1,3,5-trinitro-1,3,5-triazine (RDX) samples. The drop-on-demand sample fabrication technique is compared both visually and spectrally to the more commonly used drop-and-dry technique. As the drop-on-demand technique allows for the fabrication of trace level hazard materials, concerted efforts focused on characterization of the polymorphic phase changes observed with low concentrations of RDX commonly used in drop-on-demand processing. This information is important when evaluating optical detection technologies using samples prepared with a drop-on-demand inkjet system, as the technology may be "trained" to detect the common bulk α phase of the explosive based on its spectral features but fall short in positively detecting a trace quantity of RDX (β-phase). We report the polymorphic shifts observed between α- and β-phases of this energetic material and discuss the conditions leading to the favoring of one phase over the other.

Insider Threat - Material Control and Accountability Mitigation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Powell, Danny H; Elwood Jr, Robert H; Roche, Charles T

2011-01-01

The technical objectives of nuclear safeguards are (1) the timely detection of diversion of significant quantities of nuclear material from peaceful uses to the manufacture of nuclear weapons or other nuclear explosive devices or for purposes unknown and (2) the deterrence of such diversion by the risk of early detection. The safeguards and security program must address both outsider threats and insider threats. Outsider threats are primarily addressed by the physical protection system. Insider threats can be any level of personnel at the site including passive or active insiders that could attempt protracted or abrupt diversion. This could occur bymore » an individual acting alone or by collusion between an individual with material control and accountability (MC&A) responsibilities and another individual who has responsibility or control within both the physical protection and the MC&A systems. The insider threat is one that must be understood and incorporated into the safeguards posture. There have been more than 18 documented cases of theft or loss of plutonium or highly enriched uranium. The insider has access, authority, and knowledge, as well as a set of attributes, that make him/her difficult to detect. An integrated safeguards program is designed as a defense-in-depth system that seeks to prevent the unauthorized removal of nuclear material, to provide early detection of any unauthorized attempt to remove nuclear material, and to rapidly respond to any attempted removal of nuclear material. The program is also designed to support protection against sabotage, espionage, unauthorized access, compromise, and other hostile acts that may cause unacceptable adverse impacts on national security, program continuity, the health and safety of employees, the public, or the environment. Nuclear MC&A play an essential role in the capabilities of an integrated safeguards system to deter and detect theft or diversion of nuclear material. An integrated safeguards system with compensating mitigation can decrease the risk of an insider performing a malicious act without detection.« less

A novel material detection algorithm based on 2D GMM-based power density function and image detail addition scheme in dual energy X-ray images.

PubMed

Pourghassem, Hossein

2012-01-01

Material detection is a vital need in dual energy X-ray luggage inspection systems at security of airport and strategic places. In this paper, a novel material detection algorithm based on statistical trainable models using 2-Dimensional power density function (PDF) of three material categories in dual energy X-ray images is proposed. In this algorithm, the PDF of each material category as a statistical model is estimated from transmission measurement values of low and high energy X-ray images by Gaussian Mixture Models (GMM). Material label of each pixel of object is determined based on dependency probability of its transmission measurement values in the low and high energy to PDF of three material categories (metallic, organic and mixed materials). The performance of material detection algorithm is improved by a maximum voting scheme in a neighborhood of image as a post-processing stage. Using two background removing and denoising stages, high and low energy X-ray images are enhanced as a pre-processing procedure. For improving the discrimination capability of the proposed material detection algorithm, the details of the low and high energy X-ray images are added to constructed color image which includes three colors (orange, blue and green) for representing the organic, metallic and mixed materials. The proposed algorithm is evaluated on real images that had been captured from a commercial dual energy X-ray luggage inspection system. The obtained results show that the proposed algorithm is effective and operative in detection of the metallic, organic and mixed materials with acceptable accuracy.

Commissioning and field tests of a van-mounted system for the detection of radioactive sources and Special Nuclear Material

DOE Office of Scientific and Technical Information (OSTI.GOV)

Cester, D.; Lunardon, M.; Stevanato, L.

2015-07-01

MODES SNM project aimed to carry out technical research in order to develop a prototype for a mobile, modular detection system for radioactive sources and Special Nuclear Materials (SNM). Its main goal was to deliver a tested prototype of a modular mobile system capable of passively detecting weak or shielded radioactive sources with accuracy higher than that of currently available systems. By the end of the project all the objectives have been successfully achieved. Results from the laboratory commissioning and the field tests will be presented. (authors)

Thermal imaging measurement of lateral diffusivity and non-invasive material defect detection

DOEpatents

Sun, Jiangang; Deemer, Chris

2003-01-01

A system and method for determining lateral thermal diffusivity of a material sample using a heat pulse; a sample oriented within an orthogonal coordinate system; an infrared camera; and a computer that has a digital frame grabber, and data acquisition and processing software. The mathematical model used within the data processing software is capable of determining the lateral thermal diffusivity of a sample of finite boundaries. The system and method may also be used as a nondestructive method for detecting and locating cracks within the material sample.

System for detecting special nuclear materials

DOEpatents

Jandel, Marian; Rusev, Gencho Yordanov; Taddeucci, Terry Nicholas

2015-07-14

The present disclosure includes a radiological material detector having a convertor material that emits one or more photons in response to a capture of a neutron emitted by a radiological material; a photon detector arranged around the convertor material and that produces an electrical signal in response to a receipt of a photon; and a processor connected to the photon detector, the processor configured to determine the presence of a radiological material in response to a predetermined signature of the electrical signal produced at the photon detector. One or more detectors described herein can be integrated into a detection system that is suited for use in port monitoring, treaty compliance, and radiological material management activities.

The Use of Electronic Book Theft Detection Systems in Libraries.

ERIC Educational Resources Information Center

Witt, Thomas B.

1996-01-01

Although electronic book theft detection systems can be a deterrent to library material theft, no electronic system is foolproof, and a total security program is necessary to ensure collection security. Describes how book theft detection systems work, their effectiveness, and the problems inherent in technology. A total security program considers…

Principle, system, and applications of tip-enhanced Raman spectroscopy

NASA Astrophysics Data System (ADS)

Zhang, MingQian; Wang, Rui; Wu, XiaoBin; Wang, Jia

2012-08-01

Raman spectroscopy is a powerful technique in chemical information characterization. However, this spectral method is subject to two obstacles in nano-material detection. One is diffraction limited spatial resolution, and the other is its inherent small Raman cross section and weak signaling. To resolve these problems, a new approach has been developed, denoted as tip-enhanced Raman spectroscopy (TERS). TERS is capable of high-resolution and high-sensitivity detection and demonstrated to be a promising spectroscopic and micro-topographic method to characterize nano-materials and nanostructures. In this paper, the principle and experimental system of TERS are discussed. The latest application of TERS in molecule detection, biological specimen identification, nanao-material characterization, and semi-conductor material determination with some specific experimental examples are presented.

Detection of special nuclear materials using prompt gamma-rays from fast and slow neutron-induced fission

NASA Astrophysics Data System (ADS)

Kane, Steven Ze

A complete system has been simulated using experimentally obtained input parameters for the detection of special nuclear materials (SNM). A variation of the associated particle imaging (API) technique, referred to as reverse associated particle imaging detection (RAPID), has been developed in the context of detecting 5-kg spherical samples of U-235 in cargo containers uniformly filled with wood (low-Z) or iron (high-Z) at densities ranging from 0.1 g/cm3 to 0.4 g/cm3, the maximal density for a uniformly fully loaded 40-ft standard cargo container. In addition, samples were located at the center of a given container to study worst-case scenarios. The RAPID technique allows for the interrogation of containers at neutron production rates between 1x108 neutrons/s and 4x108 neutrons/s, depending on cargo material and density. These rates are low enough to prevent transmutation of materials in cargo and radiation safety hazards are limited. The merit of performance for the system is the time to detect the threat material with 95% probability of detection and 10-4 false positive rate per interrogated voxel of cargo. The detection of 5-kg of U-235 was chosen because this quantity of material is near the lower limit of the amount of special nuclear material that might be used in a nuclear weapon. This is in contrast to the 25-kg suggested sensitivity proposed by the International Atomic Energy Agency (IAEA).

Inspection applications with higher electron beam energies

NASA Astrophysics Data System (ADS)

Norman, D. R.; Jones, J. L.; Yoon, W. Y.; Haskell, K. J.; Sterbentz, J. W.; Zabriskie, J. M.; Hunt, A. W.; Harmon, F.; Kinlaw, M. T.

2005-12-01

The Idaho National Laboratory has developed prototype shielded nuclear material detection systems based on pulsed photonuclear assessment (PPA) techniques for the inspection of cargo containers. During this work, increased nuclear material detection capabilities have been demonstrated at higher electron beam energies than those allowed by federal regulations for cargo inspection. This paper gives a general overview of a nuclear material detection system, the PPA technique and discusses the benefits of using these higher energies. This paper also includes a summary of the numerical and test results from LINAC operations up to 24 MeV and discusses some of the federal energy limitations associated with cargo inspection.

40 CFR 63.11583 - What are my monitoring requirements?

Code of Federal Regulations, 2010 CFR

2010-07-01

... preparation operation are in target HAP service: (a) Operate a bag leak detection system with alarm that will alert operators of a leak in the control device filter material. If a bag leak detection system with... install, calibrate, operate, and maintain each bag leak detection system and alarm according to...

Chemical Fingerprinting of Materials Developed Due to Environmental Issues

NASA Technical Reports Server (NTRS)

Smith, Doris A.; McCool, A. (Technical Monitor)

2000-01-01

Instrumental chemical analysis methods are developed and used to chemically fingerprint new and modified External Tank materials made necessary by changing environmental requirements. Chemical fingerprinting can detect and diagnose variations in material composition. To chemically characterize each material, fingerprint methods are selected from an extensive toolbox based on the material's chemistry and the ability of the specific methods to detect the material's critical ingredients. Fingerprint methods have been developed for a variety of materials including Thermal Protection System foams, adhesives, primers, and composites.

Fluorescence based explosive detection: from mechanisms to sensory materials.

PubMed

Sun, Xiangcheng; Wang, Ying; Lei, Yu

2015-11-21

The detection of explosives is one of the current pressing concerns in global security. In the past few decades, a large number of emissive sensing materials have been developed for the detection of explosives in vapor, solution, and solid states through fluorescence methods. In recent years, great efforts have been devoted to develop new fluorescent materials with various sensing mechanisms for detecting explosives in order to achieve super-sensitivity, ultra-selectivity, as well as fast response time. This review article starts with a brief introduction on various sensing mechanisms for fluorescence based explosive detection, and then summarizes in an exhaustive and systematic way the state-of-the-art of fluorescent materials for explosive detection with a focus on the research in the recent 5 years. A wide range of fluorescent materials, such as conjugated polymers, small fluorophores, supramolecular systems, bio-inspired materials and aggregation induced emission-active materials, and their sensing performance and sensing mechanism are the centerpiece of this review. Finally, conclusions and future outlook are presented and discussed.

Automatic on-line detection system design research on internal defects of metal materials based on optical fiber F-P sensing technology

NASA Astrophysics Data System (ADS)

Xia, Liu; Shan, Ning; Chao, Ban; Caoshan, Wang

2016-10-01

Metal materials have been used in aerospace and other industrial fields widely because of its excellent characteristics, so its internal defects detection is very important. Ultrasound technology is used widely in the fields of nondestructive detection because of its excellent characteristic. But the conventional detection instrument for ultrasound, which has shortcomings such as low intelligent level and long development cycles, limits its development. In this paper, the theory of ultrasound detection is analyzed. A computational method of the defects distributional position is given. The non-contact type optical fiber F-P interference cavity structure is designed and the length of origin cavity is given. The real-time on-line ultrasound detecting experiment devices for internal defects of metal materials is established based on the optical fiber F-P sensing system. The virtual instrument of automation ultrasound detection internal defects is developed based on LabVIEW software and the experimental study is carried out. The results show that this system can be used in internal defect real-time on-line locating of engineering structures effectively. This system has higher measurement precision. Relative error is 6.7%. It can be met the requirement of engineering practice. The system is characterized by simple operation, easy realization. The software has a friendly interface, good expansibility, and high intelligent level.

Seal system with integral detector

DOEpatents

Fiarman, S.

1982-08-12

A seal system is disclosed for materials where security is of the essence, such as nuclear materials. The seal is tamper-indicating, indicates changes in environmental conditions that evidence attempts to bypass the seal, is unique and cost effective. The seal system is comprised of a seal where an optical signal is transmitted through a loop, with a detector to read said signal, and one or more additional detectors designed to detect environmental changes, these detectors being operatively associated with the seal so that detection of a break in the optical signal or detection of environmental changes will cause an observable change in the seal.

Universal explosive detection system for homeland security applications

NASA Astrophysics Data System (ADS)

Lee, Vincent Y.; Bromberg, Edward E. A.

2010-04-01

L-3 Communications CyTerra Corporation has developed a high throughput universal explosive detection system (PassPort) to automatically screen the passengers in airports without requiring them to remove their shoes. The technical approach is based on the patented energetic material detection (EMD) technology. By analyzing the results of sample heating with an infrared camera, one can distinguish the deflagration or decomposition of an energetic material from other clutters such as flammables and general background substances. This becomes the basis of a universal explosive detection system that does not require a library and is capable of detecting trace levels of explosives with a low false alarm rate. The PassPort is a simple turnstile type device and integrates a non-intrusive aerodynamic sampling scheme that has been shown capable of detecting trace levels of explosives on shoes. A detailed description of the detection theory and the automated sampling techniques, as well as the field test results, will be presented.

Homeland Security and Contraband Detection

NASA Astrophysics Data System (ADS)

Lanza, R. C.

Detection of contraband and illicit materials has become increasingly important, especially since the terrorist attacks in the United States on September 11, 2001. The nature of the detection problem embodies both physics issues and a set of operational constraints that limit the practical application of neutrons. The issue under consideration is detection of materials that are considered serious threats; these may include explosives; radioactive materials, fissile materials, and other materials associated with nuclear weapons, often referred to as special nuclear material (SNM). The overriding constraint is in the physics: systems must be based on clean physics; but unlike physics experiments, detection systems work under the limitation that materials must be identified nonintrusively, without interrupting the normal flow of commerce and with a high probability of detection and a low probability of false alarms. A great deal of work has been reported in the literature on neutron-based techniques for detecting explosives and drugs. The largest impetus by far for detecting explosives comes from aviation industry requirements for inspecting luggage and, to a lesser extent, cargo. The major alternative techniques are either X-ray-based or chemical trace detection methods that look for small traces of explosive residues. The limitations of the X-ray and trace methods in detecting explosives are well known, but currently (2008) it is safe to say that no neutron- or nuclear-based technique is being used routinely for security inspection, despite extensive development of these methods. Smuggling of nuclear materials has become a concern, and neutron techniques are particularly attractive for detecting them. Given the limitations of X-ray techniques and the need for SNM detection, it is now useful to reexamine neutron methodologies, particularly imaging. A significant number of neutron-based techniques have been proposed and are under development for security applications, especially SNM detection, but describing how they work is beyond the scope of the chapter. Instead, one particular approach to neutron imaging, neutron resonance radiography (NRR), is discussed in detail as it illustrates many of the issues connected with imaging and detection.

Eddy Current System for Material Inspection and Flaw Visualization

NASA Technical Reports Server (NTRS)

Bachnak, R.; King, S.; Maeger, W.; Nguyen, T.

2007-01-01

Eddy current methods have been successfully used in a variety of non-destructive evaluation applications including detection of cracks, measurements of material thickness, determining metal thinning due to corrosion, measurements of coating thickness, determining electrical conductivity, identification of materials, and detection of corrosion in heat exchanger tubes. This paper describes the development of an eddy current prototype that combines positional and eddy-current data to produce a C-scan of tested material. The preliminary system consists of an eddy current probe, a position tracking mechanism, and basic data visualization capability. Initial test results of the prototype are presented in this paper.

Measurement of metallic contaminants in food with a high-Tc SQUID

NASA Astrophysics Data System (ADS)

Tanaka, Saburo; Natsume, Miyuki; Uchida, Masashi; Hotta, Naoki; Matsuda, Takemasa; Spanut, Zarina A.; Hatsukade, Yoshimi

2004-04-01

We have proposed and demonstrated a high-Tc SQUID system for detecting metallic contaminants in foodstuffs. There is a demand for the development of systems for detecting not only magnetic materials but also non-magnetic materials such as Cu and aluminium in foodstuffs to ensure food safety. The system consists of a SQUID magnetometer, an excitation coil and a permanent magnet. For a non-magnetic sample, an AC magnetic field is applied during detection to induce an eddy current in the sample. For a magnetizable sample, a strong magnetic field is applied to the sample prior to the detection attempt. We were able to detect a stainless steel ball with a diameter of 0.1 mm and a Cu ball less than 1 mm in diameter, for example.

Detecting nuclear materials smuggling: performance evaluation of container inspection policies.

PubMed

Gaukler, Gary M; Li, Chenhua; Ding, Yu; Chirayath, Sunil S

2012-03-01

In recent years, the United States, along with many other countries, has significantly increased its detection and defense mechanisms against terrorist attacks. A potential attack with a nuclear weapon, using nuclear materials smuggled into the country, has been identified as a particularly grave threat. The system for detecting illicit nuclear materials that is currently in place at U.S. ports of entry relies heavily on passive radiation detectors and a risk-scoring approach using the automated targeting system (ATS). In this article we analyze this existing inspection system and demonstrate its performance for several smuggling scenarios. We provide evidence that the current inspection system is inherently incapable of reliably detecting sophisticated smuggling attempts that use small quantities of well-shielded nuclear material. To counter the weaknesses of the current ATS-based inspection system, we propose two new inspection systems: the hardness control system (HCS) and the hybrid inspection system (HYB). The HCS uses radiography information to classify incoming containers based on their cargo content into "hard" or "soft" containers, which then go through different inspection treatment. The HYB combines the radiography information with the intelligence information from the ATS. We compare and contrast the relative performance of these two new inspection systems with the existing ATS-based system. Our studies indicate that the HCS and HYB policies outperform the ATS-based policy for a wide range of realistic smuggling scenarios. We also examine the impact of changes in adversary behavior on the new inspection systems and find that they effectively preclude strategic gaming behavior of the adversary. © 2011 Society for Risk Analysis.

Status of the Prototype Pulsed Photonuclear Assessment (PPA) Inspection System

DOE Office of Scientific and Technical Information (OSTI.GOV)

Prototype Photonuclear Inspection Technoloby - An

Prototype Photonuclear Inspection Technology – An Integrated Systems Approach* James L. Jonesa, Daren R. Normana, Kevin J. Haskella, James W. Sterbentza, Woo Y. Yoona, Scott M. Watsona, James T. Johnsona, John M. Zabriskiea, Calvin E. Mossb, Frank Harmonc a – Idaho National Laboratory, P.O. Box 1625-2802, Idaho Falls, Idaho 83415-2802 b – Los Alamos National Laboratory, P.O. Box 1663, MS B228, Los Alamos, New Mexico, 87585 c – Idaho State University, 1500 Alvin Ricken Dr., Pocatello, Idaho 83201 Active interrogation technologies are being pursued in order to address many of today’s challenging inspection requirements related to both nuclear and non-nuclearmore » material detection. The Idaho National Laboratory, along with the Los Alamos National Laboratory and the Idaho State University’s Idaho Accelerator Center, continue to develop electron accelerator-based, photonuclear inspection technologies for the detection of shielded nuclear material within air-, rail-, and especially, maritime-cargo containers. This paper presents an overview and status of the prototype Pulsed Photonuclear Assessment (PPA) inspection system and its ability to detect shielded nuclear material by focusing on the integration of three major detection system components: delayed neutron measurement, delayed gamma-ray measurements, and a transmission, gray-scale mapping for shield material detection. Areas of future development and advancement within each detection component will be presented. *Supported in part by the Department of Homeland Security under DOE-ID Contract Number DE-AC07-99ID13727. POC: James L. Jones, 208-526-1730« less

Functional Polymers in Protein Detection Platforms: Optical, Electrochemical, Electrical, Mass-Sensitive, and Magnetic Biosensors

PubMed Central

Hahm, Jong-in

2011-01-01

The rapidly growing field of proteomics and related applied sectors in the life sciences demands convenient methodologies for detecting and measuring the levels of specific proteins as well as for screening and analyzing for interacting protein systems. Materials utilized for such protein detection and measurement platforms should meet particular specifications which include ease-of-mass manufacture, biological stability, chemical functionality, cost effectiveness, and portability. Polymers can satisfy many of these requirements and are often considered as choice materials in various biological detection platforms. Therefore, tremendous research efforts have been made for developing new polymers both in macroscopic and nanoscopic length scales as well as applying existing polymeric materials for protein measurements. In this review article, both conventional and alternative techniques for protein detection are overviewed while focusing on the use of various polymeric materials in different protein sensing technologies. Among many available detection mechanisms, most common approaches such as optical, electrochemical, electrical, mass-sensitive, and magnetic methods are comprehensively discussed in this article. Desired properties of polymers exploited for each type of protein detection approach are summarized. Current challenges associated with the application of polymeric materials are examined in each protein detection category. Difficulties facing both quantitative and qualitative protein measurements are also identified. The latest efforts on the development and evaluation of nanoscale polymeric systems for improved protein detection are also discussed from the standpoint of quantitative and qualitative measurements. Finally, future research directions towards further advancements in the field are considered. PMID:21691441

Enhanced multifunctional paint for detection of radiation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Farmer, Joseph C.; Moses, Edward Ira; Rubenchik, Alexander M.

An enhanced multifunctional paint apparatus, systems, and methods for detecting radiation on a surface include providing scintillation particles; providing an enhance neutron absorptive material; providing a binder; combining the scintillation particles, the enhance neutron absorptive material, and the binder creating a multifunctional paint; applying the multifunctional paint to the surface; and monitoring the surface for detecting radiation.

Raman detection of improvised explosive device (IED) material fabricated using drop-on-demand inkjet technology on several real world surfaces

NASA Astrophysics Data System (ADS)

Farrell, Mikella E.; Holthoff, Ellen L.; Pellegrino, Paul M.

2015-05-01

The requirement to detect hazardous materials (i.e., chemical, biological, and explosive) on a host of materials has led to the development of hazard detection systems. These new technologies and their capabilities could have immediate uses for the US military, national security agencies, and environmental response teams in efforts to keep people secure and safe. In particular, due to the increasing use by terrorists, the detection of common explosives and improvised explosive device (IED) materials have motivated research efforts toward detecting trace (i.e., particle level) quantities on multiple commonly encountered surfaces (e.g., textiles, metals, plastics, natural products, and even people). Non-destructive detection techniques can detect trace quantities of explosive materials; however, it can be challenging in the presence of a complex chemical background. One spectroscopic technique gaining increased attention for detection is Raman. One popular explosive precursor material is ammonium nitrate (AN). The material AN has many agricultural applications, however it can also be used in the fabrication of IEDs or homemade explosives (HMEs). In this paper, known amounts of AN will be deposited using an inkjet printer into several different common material surfaces (e.g., wood, human hair, textiles, metals, plastics). The materials are characterized with microscope images and by collecting Raman spectral data. In this report the detection and identification of AN will be demonstrated.

Methods and systems for detection of radionuclides

DOEpatents

Coates, Jr., John T.; DeVol, Timothy A.

2010-05-25

Disclosed are materials and systems useful in determining the existence of radionuclides in an aqueous sample. The materials provide the dual function of both extraction and scintillation to the systems. The systems can be both portable and simple to use, and as such can beneficially be utilized to determine presence and optionally concentration of radionuclide contamination in an aqueous sample at any desired location and according to a relatively simple process without the necessity of complicated sample handling techniques. The disclosed systems include a one-step process, providing simultaneous extraction and detection capability, and a two-step process, providing a first extraction step that can be carried out in a remote field location, followed by a second detection step that can be carried out in a different location.

Detection of shielded nuclear material in a cargo container

NASA Astrophysics Data System (ADS)

Jones, James L.; Norman, Daren R.; Haskell, Kevin J.; Sterbentz, James W.; Yoon, Woo Y.; Watson, Scott M.; Johnson, James T.; Zabriskie, John M.; Bennett, Brion D.; Watson, Richard W.; Moss, Cavin E.; Frank Harmon, J.

2006-06-01

The Idaho National Laboratory, along with Los Alamos National Laboratory and the Idaho State University's Idaho Accelerator Center, are developing electron accelerator-based, photonuclear inspection technologies for the detection of shielded nuclear material within air-, rail-, and especially, maritime-cargo transportation containers. This paper describes a developing prototypical cargo container inspection system utilizing the Pulsed Photonuclear Assessment (PPA) technology, incorporates interchangeable, well-defined, contraband shielding structures (i.e., "calibration" pallets) providing realistic detection data for induced radiation signatures from smuggled nuclear material, and provides various shielded nuclear material detection results. Using a 4.8-kg quantity of depleted uranium, neutron and gamma-ray detection responses are presented for well-defined shielded and unshielded configurations evaluated in a selected cargo container inspection configuration.

Detection of circumstellar material in a normal type Ia supernova.

PubMed

Patat, F; Chandra, P; Chevalier, R; Justham, S; Podsiadlowski, Ph; Wolf, C; Gal-Yam, A; Pasquini, L; Crawford, I A; Mazzali, P A; Pauldrach, A W A; Nomoto, K; Benetti, S; Cappellaro, E; Elias-Rosa, N; Hillebrandt, W; Leonard, D C; Pastorello, A; Renzini, A; Sabbadin, F; Simon, J D; Turatto, M

2007-08-17

Type Ia supernovae are important cosmological distance indicators. Each of these bright supernovae supposedly results from the thermonuclear explosion of a white dwarf star that, after accreting material from a companion star, exceeds some mass limit, but the true nature of the progenitor star system remains controversial. Here we report the spectroscopic detection of circumstellar material in a normal type Ia supernova explosion. The expansion velocities, densities, and dimensions of the circumstellar envelope indicate that this material was ejected from the progenitor system. In particular, the relatively low expansion velocities suggest that the white dwarf was accreting material from a companion star that was in the red-giant phase at the time of the explosion.

A new miniature hand-held solar-blind reagentless standoff chemical, biological, and explosives (CBE) sensor

NASA Astrophysics Data System (ADS)

Hug, W. F.; Reid, R. D.; Bhartia, R.; Lane, A. L.

2008-04-01

Improvised explosive devices (IEDs), vehicle-borne improvised explosive devices (VBIEDs), and suicide bombers are a major threat to many countries and their citizenry. The ability to detect trace levels of these threats with a miniature, hand-held, reagentless, standoff sensor represents a major improvement in the state of the art of CBE surface sensors. Photon Systems, Inc., in collaboration with Jet Propulsion Laboratory, recently demonstrated a new technology hand-held sensor for reagentless, close-range, standoff detection and identification of trace levels CBE materials on surfaces. This targeted ultraviolet CBE (TUCBE) sensor is the result of an Army Phase I STTR program. The resulting 5lb, 5W, flashlight-sized sensor can discriminate CBE from background materials using a combination of deep UV excited resonance Raman (RR) and laser induced native fluorescence (LINF) emissions resulting from excitation by a new technology deep UV laser. Detection and identification is accomplished in less than 1ms. Standoff excitation of suspicious packages, vehicles, persons, and other objects that may contain hazardous materials is accomplished using wavelengths below 250nm where Raman and native fluorescence emissions occupy distinctly different wavelength regions. This enables simultaneous detection of RR and LINF emissions with no interferences. The sensor employs fused RR/LINF chemometric methods to extract the identity of targeted materials from background clutter. Photon Systems has demonstrated detection and identification of 100ng/cm2 of explosives materials at a distance of 1 meter using a sensor with 3.8 cm optical aperture. Expansion of the optical aperture to 38 cm in a lantern-sized sensor will enable similar detection and identification of CBE materials at standoff distances of 10 meters. As a result of excitation and detection in the deep UV and the use of a gated detection system, the sensor is solar blind and can operate in full daylight conditions.

Detection of explosives, shielded nuclear materials and other hazardous substances in cargo containers

NASA Astrophysics Data System (ADS)

Kuznetsov, Andrey; Evsenin, Alexey; Vakhtin, Dmitry; Gorshkov, Igor; Osetrov, Oleg; Kalinin, Valery

2006-05-01

Nanosecond Neutron Analysis / Associated Particles Technique (NNA/APT) has been used to create devices for detection of explosives, radioactive and heavily shielded nuclear materials in cargo containers. Explosives and other hazardous materials are detected by analyzing secondary high-energy gamma-rays form reactions of fast neutrons with the materials inside the container. Depending on the dimensions of the inspected containers, the detecting system consists of one or several detection modules, each of which contains a small neutron generator with built-in position sensitive detector of associated alpha-particles and several scintillator-based gamma-ray detectors. The same gamma-ray detectors are used to detect unshielded radioactive and nuclear materials. Array of several detectors of fast neutrons is used to detect neutrons from spontaneous and induced fission of nuclear materials. These neutrons can penetrate thick layers of lead shielding, which can be used to conceal gamma-radioactivity from nuclear materials. Coincidence and timing analysis allows one to discriminate between fission neutrons and scattered probing neutrons. Mathematical modeling by MCNP5 code was used to estimate the sensitivity of the device and its optimal configuration. Capability of the device to detect 1 kg of explosive imitator inside container filled with suitcases and other baggage items has been confirmed experimentally. First experiments with heavily shielded nuclear materials have been carried out.

Probe for contamination detection in recyclable materials

DOEpatents

Taleyarkhan, Rusi

2003-08-05

A neutron detection system for detection of contaminants contained within a bulk material during recycling includes at least one neutron generator for neutron bombardment of the bulk material, and at least one gamma ray detector for detection of gamma rays emitted by contaminants within the bulk material. A structure for analyzing gamma ray data is communicably connected to the gamma ray detector, the structure for analyzing gamma ray data adapted. The identity and concentration of contaminants in a bulk material can also be determined. By scanning the neutron beam, discrete locations within the bulk material having contaminants can be identified. A method for recycling bulk material having unknown levels of contaminants includes the steps of providing at least one neutron generator, at least one gamma ray detector, and structure for analyzing gamma ray data, irradiating the bulk material with neutrons, and then determining the presence of at least one contaminant in the bulk material from gamma rays emitted from the bulk material.

Detecting errors and anomalies in computerized materials control and accountability databases

DOE Office of Scientific and Technical Information (OSTI.GOV)

Whiteson, R.; Hench, K.; Yarbro, T.

The Automated MC and A Database Assessment project is aimed at improving anomaly and error detection in materials control and accountability (MC and A) databases and increasing confidence in the data that they contain. Anomalous data resulting in poor categorization of nuclear material inventories greatly reduces the value of the database information to users. Therefore it is essential that MC and A data be assessed periodically for anomalies or errors. Anomaly detection can identify errors in databases and thus provide assurance of the integrity of data. An expert system has been developed at Los Alamos National Laboratory that examines thesemore » large databases for anomalous or erroneous data. For several years, MC and A subject matter experts at Los Alamos have been using this automated system to examine the large amounts of accountability data that the Los Alamos Plutonium Facility generates. These data are collected and managed by the Material Accountability and Safeguards System, a near-real-time computerized nuclear material accountability and safeguards system. This year they have expanded the user base, customizing the anomaly detector for the varying requirements of different groups of users. This paper describes the progress in customizing the expert systems to the needs of the users of the data and reports on their results.« less

Seal system with integral detector

DOEpatents

Fiarman, Sidney

1985-01-01

There is disclosed a seal system for materials where security is of the essence, such as nuclear materials, which is tamper-indicating, which indicates changes in environmental conditions that evidence attempts to by-pass the seal, which is unique and cost effective, said seal system comprised of a seal where an optical signal is transmitted through a loop, with a detector to read said signal, and one or more additional detectors designed to detect environmental changes, these detectors being operatively associated with the seal so that detection of a break in the optical signal or detection of environmental changes will cause an observable change in the seal.

An embedded fibre optic sensor for impact damage detection in composite materials

NASA Astrophysics Data System (ADS)

Glossop, Neil David William

1989-09-01

A structurally embedded fiber optic damage detection sensor for composite materials is described. The system is designed specifically for the detection of barely visible damage resulting from low velocity impacts in Kevlar-epoxy laminates. By monitoring the light transmission properties of optical fiber embedded in the composite, it was shown that the integrity of the material can be accurately determined. The effect of several parameters on the sensitivity of the system was investigated, including the effect of the optical fiber orientation and depth of embedding within the composite. A novel surface was also developed for the optical fibers to ensure they will fracture at the requisite damage level. The influence of the optical fiber sensors on the tensile and compressive material properties and on the impact resistance of the laminate was also studied. Extensive experimental results from impact tests are reported and a numerical model of the impact event is presented which is able to predict and model the damage mechanism and sensor system. A new and powerful method of nondestructive evaluation for translucent composite materials based on image enhanced backlighting is also described.

The probability of flaw detection and the probability of false calls in nondestructive evaluation equipment

NASA Technical Reports Server (NTRS)

Temple, Enoch C.

1994-01-01

The space industry has developed many composite materials that have high durability in proportion to their weights. Many of these materials have a likelihood for flaws that is higher than in traditional metals. There are also coverings (such as paint) that develop flaws that may adversely affect the performance of the system in which they are used. Therefore there is a need to monitor the soundness of composite structures. To meet this monitoring need, many nondestructive evaluation (NDE) systems have been developed. An NDE system is designed to detect material flaws and make flaw measurements without destroying the inspected item. Also, the detection operation is expected to be performed in a rapid manner in a field or production environment. Some of the most recent video-based NDE methodologies are shearography, holography, thermography, and video image correlation.

Detecting fission from special nuclear material sources

DOEpatents

Rowland, Mark S [Alamo, CA; Snyderman, Neal J [Berkeley, CA

2012-06-05

A neutron detector system for discriminating fissile material from non-fissile material wherein a digital data acquisition unit collects data at high rate, and in real-time processes large volumes of data directly into information that a first responder can use to discriminate materials. The system comprises counting neutrons from the unknown source and detecting excess grouped neutrons to identify fission in the unknown source. The system includes a graphing component that displays the plot of the neutron distribution from the unknown source over a Poisson distribution and a plot of neutrons due to background or environmental sources. The system further includes a known neutron source placed in proximity to the unknown source to actively interrogate the unknown source in order to accentuate differences in neutron emission from the unknown source from Poisson distributions and/or environmental sources.

Damage Detection Response Characteristics of Open Circuit Resonant (SansEC) Sensors

NASA Technical Reports Server (NTRS)

Dudley, Kenneth L.; Szatkowski, George N.; Smith, Laura J.; Koppen, Sandra V.; Ely, Jay J.; Nguyen, Truong X.; Wang, Chuantong; Ticatch, Larry A.; Mielnik, John J.

2013-01-01

The capability to assess the current or future state of the health of an aircraft to improve safety, availability, and reliability while reducing maintenance costs has been a continuous goal for decades. Many companies, commercial entities, and academic institutions have become interested in Integrated Vehicle Health Management (IVHM) and a growing effort of research into "smart" vehicle sensing systems has emerged. Methods to detect damage to aircraft materials and structures have historically relied on visual inspection during pre-flight or post-flight operations by flight and ground crews. More quantitative non-destructive investigations with various instruments and sensors have traditionally been performed when the aircraft is out of operational service during major scheduled maintenance. Through the use of reliable sensors coupled with data monitoring, data mining, and data analysis techniques, the health state of a vehicle can be detected in-situ. NASA Langley Research Center (LaRC) is developing a composite aircraft skin damage detection method and system based on open circuit SansEC (Sans Electric Connection) sensor technology. Composite materials are increasingly used in modern aircraft for reducing weight, improving fuel efficiency, and enhancing the overall design, performance, and manufacturability of airborne vehicles. Materials such as fiberglass reinforced composites (FRC) and carbon-fiber-reinforced polymers (CFRP) are being used to great advantage in airframes, wings, engine nacelles, turbine blades, fairings, fuselage structures, empennage structures, control surfaces and aircraft skins. SansEC sensor technology is a new technical framework for designing, powering, and interrogating sensors to detect various types of damage in composite materials. The source cause of the in-service damage (lightning strike, impact damage, material fatigue, etc.) to the aircraft composite is not relevant. The sensor will detect damage independent of the cause. Damage in composite material is generally associated with a localized change in material permittivity and/or conductivity. These changes are sensed using SansEC. The unique electrical signatures (amplitude, frequency, bandwidth, and phase) are used for damage detection and diagnosis. An operational system and method would incorporate a SansEC sensor array on select areas of the aircraft exterior surfaces to form a "Smart skin" sensing surface. In this paper a new method and system for aircraft in-situ damage detection and diagnosis is presented. Experimental test results on seeded fault damage coupons and computational modeling simulation results are presented. NASA LaRC has demonstrated with individual sensors that SansEC sensors can be effectively used for in-situ composite damage detection of delamination, voids, fractures, and rips. Keywords: Damage Detection, Composites, Integrated Vehicle Health Monitoring (IVHM), Aviation Safety, SansEC Sensors

Detection of Illicit Drugs with the EURITRACK System

NASA Astrophysics Data System (ADS)

Perot, B.; Carasco, C.; Valkovic, V.; Sudac, D.; Franulovic, A.

2009-03-01

The EURopean Illicit TRAfficking Countermeasures Kit (EURITRACK) inspection system has been developed within the 6th EU Framework Program to complement X-ray scanners in the detection of explosives and other illicit materials hidden in cargo containers. Gamma rays are produced inside the cargo materials by 14 MeV tagged neutron beams, which yields information about the chemical composition of the transported goods. In the beginning of year 2007, the EURITRACK system was implemented in the Seaport of Rijeka, Croatia, primarily to carry out a demonstration using real containers to conduct a series of detection tests. This article reports tests performed with real samples of illicit drugs hidden in a metallic cargo with an average density of 0.2 g/cm3. Heroin and cocaine have been distinguished from benign substances based on their chemical composition. Marijuana, which chemical composition is similar to benign materials, cannot be distinguished from common organic goods. However, the detection of an unexpected organic substance inside the metallic cargo indicates that a suspicious object has been hidden in the container.

Sensor arrays for detecting microorganisms

NASA Technical Reports Server (NTRS)

Lewis, Nathan S. (Inventor); Freund, Michael S. (Inventor)

2000-01-01

A sensor array for detecting a microorganism comprising first and second sensors electrically connected to an electrical measuring apparatus, wherein the sensors comprise a region of nonconducting organic material and a region of conducting material compositionally that is different than the nonconducting organic material and an electrical path through the regions of nonconducting organic material and the conducting material. A system for identifying microorganisms using the sensor array, a computer and a pattern recognition algorithm, such as a neural net are also disclosed.

Advances in neutron based bulk explosive detection

NASA Astrophysics Data System (ADS)

Gozani, Tsahi; Strellis, Dan

2007-08-01

Neutron based explosive inspection systems can detect a wide variety of national security threats. The inspection is founded on the detection of characteristic gamma rays emitted as the result of neutron interactions with materials. Generally these are gamma rays resulting from thermal neutron capture and inelastic scattering reactions in most materials and fast and thermal neutron fission in fissile (e.g.235U and 239Pu) and fertile (e.g.238U) materials. Cars or trucks laden with explosives, drugs, chemical agents and hazardous materials can be detected. Cargo material classification via its main elements and nuclear materials detection can also be accomplished with such neutron based platforms, when appropriate neutron sources, gamma ray spectroscopy, neutron detectors and suitable decision algorithms are employed. Neutron based techniques can be used in a variety of scenarios and operational modes. They can be used as stand alones for complete scan of objects such as vehicles, or for spot-checks to clear (or validate) alarms indicated by another inspection system such as X-ray radiography. The technologies developed over the last two decades are now being implemented with good results. Further advances have been made over the last few years that increase the sensitivity, applicability and robustness of these systems. The advances range from the synchronous inspection of two sides of vehicles, increasing throughput and sensitivity and reducing imparted dose to the inspected object and its occupants (if any), to taking advantage of the neutron kinetic behavior of cargo to remove systematic errors, reducing background effects and improving fast neutron signals.

Self-diagnostic thermal protection systems for future spacecraft

NASA Astrophysics Data System (ADS)

Hanlon, Alaina B.

The thermal protection system (TPS) represents the greatest risk factor after propulsion for any transatmospheric mission (Dr. Charles Smith, NASA ARC). Any damage to the TPS leaves the space vehicle vulnerable and could result in the loss of human life as happened in the Columbia accident. Aboard the current Space Shuttle Orbiters no system exists to notify the astronauts or ground control if the thermal protection system has been damaged. Through this research, a proof-of-concept monitoring system was developed. The system has two specific applications for thermal protection systems: (1) Improving models used to predict thermal and mechanical response of TPS materials, and (2) Self-diagnosing damage within regions of the TPS and communicating the damage to the appropriate personnel over a potentially unstable network. Mechanical damage is among the most important things to protect the TPS against. Methods to detect the primary types of mechanical damage suffered by thermal protection systems have been developed. Lightweight, low-power sensors were developed to detect any cracks in small regions of a TPS. Implementation of a network of these sensors within 10's to 1000's of regions will eventually provide high spatial resolution of damage detection; allowing for detection of holes in the TPS. Also important in thermal protection material development is to know the ablation rates and time/temperature response of the materials. A new type of sensor has been developed to monitor temperature at different depths within thermal protection materials. The signals being transmitted through the sensors can be multiplexed to allow for mechanical damage and temperature to be monitored using the same sensor.

Early detection of mine fire in underground by using smell detectors

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ohga, Kotaro; Higuchi, Kiyoshi

1995-12-31

In our laboratory, a new detection system using smell detectors was developed to detect the spontaneous combustion of coal and the combustion of other materials used underground. Laboratory experiments were carried out on several kinds of coals, including South African coals, and machine oil, wood and rubber used in belt conveyers. The following results were obtained: (1) Spontaneous combustion of coal can be detected earlier by smell detectors than by conventional CO detection methods. (2) There were no differences in the results using different kinds of coal. (3) Combustion d other materials can also be detected earlier by this systemmore » than by conventional detectors for gas and smoke. (4) Use of this detection system enables one to discern the source of the combustion gases, whether it be coal, wood, oil or rubber.« less

Automated Guided-Wave Scanning Developed to Characterize Materials and Detect Defects

NASA Technical Reports Server (NTRS)

Martin, Richard E.; Gyekenyeski, Andrew L.; Roth, Don J.

2004-01-01

The Nondestructive Evaluation (NDE) Group of the Optical Instrumentation Technology Branch at the NASA Glenn Research Center has developed a scanning system that uses guided waves to characterize materials and detect defects. The technique uses two ultrasonic transducers to interrogate the condition of a material. The sending transducer introduces an ultrasonic pulse at a point on the surface of the specimen, and the receiving transducer detects the signal after it has passed through the material. The aim of the method is to correlate certain parameters in both the time and frequency domains of the detected waveform to characteristics of the material between the two transducers. The scanning system is shown. The waveform parameters of interest include the attenuation due to internal damping, waveform shape parameters, and frequency shifts due to material changes. For the most part, guided waves are used to gauge the damage state and defect growth of materials subjected to various mechanical or environmental loads. The technique has been applied to polymer matrix composites, ceramic matrix composites, and metal matrix composites as well as metallic alloys. Historically, guided wave analysis has been a point-by-point, manual technique with waveforms collected at discrete locations and postprocessed. Data collection and analysis of this type limits the amount of detail that can be obtained. Also, the manual movement of the sensors is prone to user error and is time consuming. The development of an automated guided-wave scanning system has allowed the method to be applied to a wide variety of materials in a consistent, repeatable manner. Experimental studies have been conducted to determine the repeatability of the system as well as compare the results obtained using more traditional NDE methods. The following screen capture shows guided-wave scan results for a ceramic matrix composite plate, including images for each of nine calculated parameters. The system can display up to 18 different wave parameters. Multiple scans of the test specimen demonstrated excellent repeatability in the measurement of all the guided-wave parameters, far exceeding the traditional point-by-point technique. In addition, the scan was able to detect a subsurface defect that was confirmed using flash thermography This technology is being further refined to provide a more robust and efficient software environment. Future hardware upgrades will allow for multiple receiving transducers and the ability to scan more complex surfaces. This work supports composite materials development and testing under the Ultra-Efficient Engine Technology (UEET) Project, but it also will be applied to other material systems under development for a wide range of applications.

Mobile Pit verification system design based on passive special nuclear material verification in weapons storage facilities

DOE Office of Scientific and Technical Information (OSTI.GOV)

Paul, J. N.; Chin, M. R.; Sjoden, G. E.

2013-07-01

A mobile 'drive by' passive radiation detection system to be applied in special nuclear materials (SNM) storage facilities for validation and compliance purposes has been designed through the use of computational modeling and new radiation detection methods. This project was the result of work over a 1 year period to create optimal design specifications to include creation of 3D models using both Monte Carlo and deterministic codes to characterize the gamma and neutron leakage out each surface of SNM-bearing canisters. Results were compared and agreement was demonstrated between both models. Container leakages were then used to determine the expected reactionmore » rates using transport theory in the detectors when placed at varying distances from the can. A 'typical' background signature was incorporated to determine the minimum signatures versus the probability of detection to evaluate moving source protocols with collimation. This established the criteria for verification of source presence and time gating at a given vehicle speed. New methods for the passive detection of SNM were employed and shown to give reliable identification of age and material for highly enriched uranium (HEU) and weapons grade plutonium (WGPu). The finalized 'Mobile Pit Verification System' (MPVS) design demonstrated that a 'drive-by' detection system, collimated and operating at nominally 2 mph, is capable of rapidly verifying each and every weapon pit stored in regularly spaced, shelved storage containers, using completely passive gamma and neutron signatures for HEU and WGPu. This system is ready for real evaluation to demonstrate passive total material accountability in storage facilities. (authors)« less

Radiological Health Protection Issues Associated with Use of Active Detection Technology Systems for Detection of Radioactive Threat Materials

DTIC Science & Technology

2013-07-01

detection system available will simply register events resulting from natural background radiation if a suitable source emission is not employed. The...random fluctuations in the natural background radiation level. Noise within the detection system can result from any of the various components that...Uritani et al., 1994). Nothing can generally be done to reduce or stabilize the amount of natural background radiation present for nonstationary

Seeing Eye Drones: How The DOD Can Transform CBM And Disaster Response In The Homeland

DTIC Science & Technology

2016-12-01

thesis explores the possibility of integrating small unmanned aircraft systems (sUAS) with video capability and CBRN detection and identification sensors...small, unmanned aircraft systems (sUAS) with video capability and CBRN detection and identification sensors for use by National Guard civil support...CBRN) and hazardous material (HAZMAT) materials, as well as providing video to the incident commander. One of the primary benefits of providing

Current trends in gamma radiation detection for radiological emergency response

NASA Astrophysics Data System (ADS)

Mukhopadhyay, Sanjoy; Guss, Paul; Maurer, Richard

2011-09-01

Passive and active detection of gamma rays from shielded radioactive materials, including special nuclear materials, is an important task for any radiological emergency response organization. This article reports on the current trends and status of gamma radiation detection objectives and measurement techniques as applied to nonproliferation and radiological emergencies. In recent years, since the establishment of the Domestic Nuclear Detection Office by the Department of Homeland Security, a tremendous amount of progress has been made in detection materials (scintillators, semiconductors), imaging techniques (Compton imaging, use of active masking and hybrid imaging), data acquisition systems with digital signal processing, field programmable gate arrays and embedded isotopic analysis software (viz. gamma detector response and analysis software [GADRAS]1), fast template matching, and data fusion (merging radiological data with geo-referenced maps, digital imagery to provide better situational awareness). In this stride to progress, a significant amount of inter-disciplinary research and development has taken place-techniques and spin-offs from medical science (such as x-ray radiography and tomography), materials engineering (systematic planned studies on scintillators to optimize several qualities of a good scintillator, nanoparticle applications, quantum dots, and photonic crystals, just to name a few). No trend analysis of radiation detection systems would be complete without mentioning the unprecedented strategic position taken by the National Nuclear Security Administration (NNSA) to deter, detect, and interdict illicit trafficking in nuclear and other radioactive materials across international borders and through the global maritime transportation-the so-called second line of defense.

Biologically inspired autonomous structural materials with controlled toughening and healing

NASA Astrophysics Data System (ADS)

Garcia, Michael E.; Sodano, Henry A.

2010-04-01

The field of structural health monitoring (SHM) has made significant contributions in the field of prognosis and damage detection in the past decade. The advantageous use of this technology has not been integrated into operational structures to prevent damage from propagating or to heal injured regions under real time loading conditions. Rather, current systems relay this information to a central processor or human operator, who then determines a course of action such as altering the mission or scheduling repair maintenance. Biological systems exhibit advanced sensory and healing traits that can be applied to the design of material systems. For instance, bone is the major structural component in vertebrates; however, unlike modern structural materials, bone has many properties that make it effective for arresting the propagation of cracks and subsequent healing of the fractured area. The foremost goal for the development of future adaptive structures is to mimic biological systems, similar to bone, such that the material system can detect damage and deploy defensive traits to impede damage from propagating, thus preventing catastrophic failure while in operation. After sensing and stalling the propagation of damage, the structure must then be repaired autonomously using self healing mechanisms motivated by biological systems. Here a novel autonomous system is developed using shape memory polymers (SMPs), that employs an optical fiber network as both a damage detection sensor and a network to deliver stimulus to the damage site initiating adaptation and healing. In the presence of damage the fiber optic fractures allowing a high power laser diode to deposit a controlled level of thermal energy at the fractured sight locally reducing the modulus and blunting the crack tip, which significantly slows the crack growth rate. By applying a pre-induced strain field and utilizing the shape memory recovery effect, thermal energy can be deployed to close the crack and return the system to its original operating state. The entire system will effectively detect, self toughen, and subsequently heal damage as biological materials such as bone does.

Graphene Oxide/Silver Nanohybrid as Multi-functional Material for Highly Efficient Bacterial Disinfection and Detection of Organic Dye

NASA Astrophysics Data System (ADS)

Tam, Le Thi; Dinh, Ngo Xuan; Van Cuong, Nguyen; Van Quy, Nguyen; Huy, Tran Quang; Ngo, Duc-The; Mølhave, Kristian; Le, Anh-Tuan

2016-10-01

In this work, a multi-functional hybrid system consisting of graphene oxide and silver nanoparticles (GO-Ag NPs) was successfully synthesized by using a two-step chemical process. We firstly demonstrated noticeable bactericidal ability of the GO-Ag hybrid system. We provide more chemo-physical evidence explaining the antibacterial behavior of GO-Ag nanohybrid against Gram-negative Escherichia Coli and Gram-positive Staphylococcus aureus in light of ultrastructural damage analyses and Ag1+ ions release rate onto the cells/medium. A further understanding of the mode of antimicrobial action is very important for designing and developing advanced antimicrobial systems. Secondly, we have also demonstrated that the GO-Ag nanohybrid material could be used as a potential surface enhanced Raman scattering (SERS) substrate to detect and quantify organic dyes, e.g., methylene blue (MB), in aqueous media. Our findings revealed that the GO-Ag hybrid system showed better SERS performance of MB detection than that of pure Ag-NPs. MB could be detected at a concentration as low as 1 ppm. The GO-Ag-based SERS platform can be effectively used to detect trace concentrations of various types of organic dyes in aqueous media. With the aforementioned properties, the GO-Ag hybrid system is found to be very promising as a multi-functional material for advanced biomedicine and environmental monitoring applications.

In-Situ Wire Damage Detection System

NASA Technical Reports Server (NTRS)

Jolley, Scott T. (Inventor); Gibson, Tracy L. (Inventor); Medelius, Pedro J. (Inventor); Roberson, Luke B. (Inventor); Tate, Lanetra C. (Inventor); Smith, Trent M. (Inventor); Williams, Martha K. (Inventor)

2014-01-01

An in-situ system for detecting damage in an electrically conductive wire. The system includes a substrate at least partially covered by a layer of electrically conductive material forming a continuous or non-continuous electrically conductive layer connected to an electrical signal generator adapted to delivering electrical signals to the electrically conductive layer. Data is received and processed to identify damage to the substrate or electrically conductive layer. The electrically conductive material may include metalized carbon fibers, a thin metal coating, a conductive polymer, carbon nanotubes, metal nanoparticles or a combination thereof.

Methods of use for sensor based fluid detection devices

NASA Technical Reports Server (NTRS)

Lewis, Nathan S. (Inventor)

2001-01-01

Methods of use and devices for detecting analyte in fluid. A system for detecting an analyte in a fluid is described comprising a substrate having a sensor comprising a first organic material and a second organic material where the sensor has a response to permeation by an analyte. A detector is operatively associated with the sensor. Further, a fluid delivery appliance is operatively associated with the sensor. The sensor device has information storage and processing equipment, which is operably connected with the device. This device compares a response from the detector with a stored ideal response to detect the presence of analyte. An integrated system for detecting an analyte in a fluid is also described where the sensing device, detector, information storage and processing device, and fluid delivery device are incorporated in a substrate. Methods for use for the above system are also described where the first organic material and a second organic material are sensed and the analyte is detected with a detector operatively associated with the sensor. The method provides for a device, which delivers fluid to the sensor and measures the response of the sensor with the detector. Further, the response is compared to a stored ideal response for the analyte to determine the presence of the analyte. In different embodiments, the fluid measured may be a gaseous fluid, a liquid, or a fluid extracted from a solid. Methods of fluid delivery for each embodiment are accordingly provided.

46 CFR 161.002-9 - Automatic fire detecting system, power supply.

Code of Federal Regulations, 2013 CFR

2013-10-01

... system must meet the requirements of § 113.10-9 of subchapter J (Electrical Engineering Regulations) of... 46 Shipping 6 2013-10-01 2013-10-01 false Automatic fire detecting system, power supply. 161.002-9..., CONSTRUCTION, AND MATERIALS: SPECIFICATIONS AND APPROVAL ELECTRICAL EQUIPMENT Fire-Protective Systems § 161.002...

46 CFR 161.002-9 - Automatic fire detecting system, power supply.

Code of Federal Regulations, 2014 CFR

2014-10-01

... system must meet the requirements of § 113.10-9 of subchapter J (Electrical Engineering Regulations) of... 46 Shipping 6 2014-10-01 2014-10-01 false Automatic fire detecting system, power supply. 161.002-9..., CONSTRUCTION, AND MATERIALS: SPECIFICATIONS AND APPROVAL ELECTRICAL EQUIPMENT Fire-Protective Systems § 161.002...

46 CFR 161.002-9 - Automatic fire detecting system, power supply.

Code of Federal Regulations, 2012 CFR

2012-10-01

... system must meet the requirements of § 113.10-9 of subchapter J (Electrical Engineering Regulations) of... 46 Shipping 6 2012-10-01 2012-10-01 false Automatic fire detecting system, power supply. 161.002-9..., CONSTRUCTION, AND MATERIALS: SPECIFICATIONS AND APPROVAL ELECTRICAL EQUIPMENT Fire-Protective Systems § 161.002...

A Neutron Based Interrogation System For SNM In Cargo

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kane, Steven Z.; Koltick, David S.

A complete system has been simulated using experimentally obtained input parameters for the detection of special nuclear materials (SNM). A variation of the associated particle imaging (API) technique, referred to as reverse associated particle imaging detection (RAPID), has been developed in the context of detecting 5-kg spherical samples of U-235 in cargo. The RAPID technique allows for the interrogation of containers at neutron production rates between {approx}1x10{sup 8} neutrons/s and {approx}3x10{sup 8} neutrons/s. The merit of performance for the system is the time to detect the threat material with 95% probability of detection and 10{sup -4} false positive rate permore » interrogated voxel of cargo. Detection times of 5 minutes were found for a maximally loaded cargo container uniformly filled with iron and as low as 1 second in containers loaded to 1/4 of full capacity with either iron or wood. The worse case system performance, 30 minutes interrogation time, occurs for a maximally loaded container containing wood at 0.4 g/cm{sup 3}.« less

Detection of Shielded Nuclear Material in a Cargo Container

DOE Office of Scientific and Technical Information (OSTI.GOV)

J. L. Jones; D. R. Norman; K. J. Haskell

The Idaho National Laboratory, along with Los Alamos National Laboratory and the Idaho State University’s Idaho Accelerator Center, are developing electron accelerator-based, photonuclear inspection technologies for the detection of shielded nuclear material within air-, rail-, and especially, maritime-cargo transportation containers. This paper describes a developing prototypical cargo container inspection system utilizing the Pulsed Photonuclear Assessment (PPA) technology, incorporates interchangeable, well-defined, contraband shielding structures (i.e., "calibration" pallets) providing realistic detection data for induced radiation signatures from smuggled nuclear material, and provides various shielded nuclear material detection results. Using a 4.8-kg quantity of depleted uranium, neutron and gamma-ray detection responses are presentedmore » for well-defined shielded and unshielded configurations evaluated in a selected cargo container inspection configuration. © 2001 Elsevier Science. All rights reserved« less

Illicit drug detection using energy dispersive x-ray diffraction

NASA Astrophysics Data System (ADS)

Cook, E. J.; Griffiths, J. A.; Koutalonis, M.; Gent, C.; Pani, S.; Horrocks, J. A.; George, L.; Hardwick, S.; Speller, R.

2009-05-01

Illicit drugs are imported into countries in myriad ways, including via the postal system and courier services. An automated system is required to detect drugs in parcels for which X-ray diffraction is a suitable technique as it is non-destructive, material specific and uses X-rays of sufficiently high energy to penetrate parcels containing a range of attenuating materials. A database has been constructed containing the measured powder diffraction profiles of several thousand materials likely to be found in parcels. These include drugs, cutting agents, packaging and other innocuous materials. A software model has been developed using these data to predict the diffraction profiles which would be obtained by X-ray diffraction systems with a range of suggested detector (high purity germanium, CZT and scintillation), source and collimation options. The aim of the model was to identify the most promising system geometries, which was done with the aid of multivariate analysis (MVA). The most promising systems were constructed and tested. The diffraction profiles of a range of materials have been measured and used to both validate the model and to identify the presence of drugs in sample packages.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chiaro, P.J.

A series of tests were performed at Oak Ridge National Laboratory (ORNL) to evaluate and characterize the radiological response of a ''Cricket'' radiation detection system. The ''Cricket'' is manufactured by RAD/COMM Systems Corp., which is located in Ontario, Canada. The system is designed to detect radioactive material that may be contained in scrap metal. The Cricket's detection unit is mounted to the base of a grappler and monitors material, while the grappler's tines hold the material. It can also be used to scan material in an attempt to isolate radioactive material if an alarm occurs. Testing was performed at themore » Environmental Effects Laboratory located at ORNL and operated by the Engineering Science and Technology Division. Tests performed included the following: (1) Background stability, (2) Energy response using {sup 241}Am, {sup 137}Cs, and {sup 60}Co, (3) Surface uniformity, (4) Angular dependence, (5) Alarm actuation, (6) Alarm threshold vs. background, (7) Shielding, (8) Response to {sup 235}U, (9) Response to neutrons using unmoderated {sup 252}Cf, and (10) Response to transient radiation. This report presents a summary of the test results. Background measurements were obtained prior to the performance of each individual test.« less

Surface-enhanced Raman scattering detection of ammonium nitrate samples fabricated using drop-on-demand inkjet technology.

PubMed

Farrell, Mikella E; Holthoff, Ellen L; Pellegrino, Paul M

2014-01-01

The United States Army and the first responder community are increasingly focusing efforts on energetic materials detection and identification. Main hazards encountered in theater include homemade explosives and improvised explosive devices, in part fabricated from simple components like ammonium nitrate (AN). In order to accurately detect and identify these unknowns (energetic or benign), fielded detection systems must be accurately trained using well-understood universal testing substrates. These training substrates must contain target species at known concentrations and recognized polymorphic phases. Ammonium nitrate is an explosive precursor material that demonstrates several different polymorphic phases dependent upon how the material is deposited onto testing substrates. In this paper, known concentrations of AN were uniformly deposited onto commercially available surface-enhanced Raman scattering (SERS) substrates using a drop-on-demand inkjet printing system. The phase changes observed after the deposition of AN under several solvent conditions are investigated. Characteristics of the collected SERS spectra of AN are discussed, and it is demonstrated that an understanding of the exact nature of the AN samples deposited will result in an increased ability to accurately and reliably "train" hazard detection systems.

Adaptable radiation monitoring system and method

DOEpatents

Archer, Daniel E [Livermore, CA; Beauchamp, Brock R [San Ramon, CA; Mauger, G Joseph [Livermore, CA; Nelson, Karl E [Livermore, CA; Mercer, Michael B [Manteca, CA; Pletcher, David C [Sacramento, CA; Riot, Vincent J [Berkeley, CA; Schek, James L [Tracy, CA; Knapp, David A [Livermore, CA

2006-06-20

A portable radioactive-material detection system capable of detecting radioactive sources moving at high speeds. The system has at least one radiation detector capable of detecting gamma-radiation and coupled to an MCA capable of collecting spectral data in very small time bins of less than about 150 msec. A computer processor is connected to the MCA for determining from the spectral data if a triggering event has occurred. Spectral data is stored on a data storage device, and a power source supplies power to the detection system. Various configurations of the detection system may be adaptably arranged for various radiation detection scenarios. In a preferred embodiment, the computer processor operates as a server which receives spectral data from other networked detection systems, and communicates the collected data to a central data reporting system.

Intelligent Extruder

DOE Office of Scientific and Technical Information (OSTI.GOV)

AlperEker; Mark Giammattia; Paul Houpt

''Intelligent Extruder'' described in this report is a software system and associated support services for monitoring and control of compounding extruders to improve material quality, reduce waste and energy use, with minimal addition of new sensors or changes to the factory floor system components. Emphasis is on process improvements to the mixing, melting and de-volatilization of base resins, fillers, pigments, fire retardants and other additives in the :finishing'' stage of high value added engineering polymer materials. While GE Plastics materials were used for experimental studies throughout the program, the concepts and principles are broadly applicable to other manufacturers materials. Themore » project involved a joint collaboration among GE Global Research, GE Industrial Systems and Coperion Werner & Pleiderer, USA, a major manufacturer of compounding equipment. Scope of the program included development of a algorithms for monitoring process material viscosity without rheological sensors or generating waste streams, a novel detection scheme for rapid detection of process upsets and an adaptive feedback control system to compensate for process upsets where at line adjustments are feasible. Software algorithms were implemented and tested on a laboratory scale extruder (50 lb/hr) at GE Global Research and data from a production scale system (2000 lb/hr) at GE Plastics was used to validate the monitoring and detection software. Although not evaluated experimentally, a new concept for extruder process monitoring through estimation of high frequency drive torque without strain gauges is developed and demonstrated in simulation. A plan to commercialize the software system is outlined, but commercialization has not been completed.« less

MCNP Simulation Benchmarks for a Portable Inspection System for Narcotics, Explosives, and Nuclear Material Detection

NASA Astrophysics Data System (ADS)

Alfonso, Krystal; Elsalim, Mashal; King, Michael; Strellis, Dan; Gozani, Tsahi

2013-04-01

MCNPX simulations have been used to guide the development of a portable inspection system for narcotics, explosives, and special nuclear material (SNM) detection. The system seeks to address these threats to national security by utilizing a high-yield, compact neutron source to actively interrogate the threats and produce characteristic signatures that can then be detected by radiation detectors. The portability of the system enables rapid deployment and proximity to threats concealed in small spaces. Both dD and dT electronic neutron generators (ENG) were used to interrogate ammonium nitrate fuel oil (ANFO) and cocaine hydrochloride, and the detector response of NaI, CsI, and LaBr3 were compared. The effect of tungsten shielding on the neutron flux in the gamma ray detectors was investigated, while carbon, beryllium, and polyethylene ENG moderator materials were optimized by determining the reaction rate density in the threats. In order to benchmark the modeling results, experimental measurements are compared with MCNPX simulations. In addition, the efficiency and die-away time of a portable differential die-away analysis (DDAA) detector using 3He proportional counters for SNM detection has been determined.

Computational Electromagnetic Modeling of SansEC(Trade Mark) Sensors

NASA Technical Reports Server (NTRS)

Smith, Laura J.; Dudley, Kenneth L.; Szatkowski, George N.

2011-01-01

This paper describes the preliminary effort to apply computational design tools to aid in the development of an electromagnetic SansEC resonant sensor composite materials damage detection system. The computational methods and models employed on this research problem will evolve in complexity over time and will lead to the development of new computational methods and experimental sensor systems that demonstrate the capability to detect, diagnose, and monitor the damage of composite materials and structures on aerospace vehicles.

Integrated material state awareness system with self-learning symbiotic diagnostic algorithms and models

NASA Astrophysics Data System (ADS)

Banerjee, Sourav; Liu, Lie; Liu, S. T.; Yuan, Fuh-Gwo; Beard, Shawn

2011-04-01

Materials State Awareness (MSA) goes beyond traditional NDE and SHM in its challenge to characterize the current state of material damage before the onset of macro-damage such as cracks. A highly reliable, minimally invasive system for MSA of Aerospace Structures, Naval structures as well as next generation space systems is critically needed. Development of such a system will require a reliable SHM system that can detect the onset of damage well before the flaw grows to a critical size. Therefore, it is important to develop an integrated SHM system that not only detects macroscale damages in the structures but also provides an early indication of flaw precursors and microdamages. The early warning for flaw precursors and their evolution provided by an SHM system can then be used to define remedial strategies before the structural damage leads to failure, and significantly improve the safety and reliability of the structures. Thus, in this article a preliminary concept of developing the Hybrid Distributed Sensor Network Integrated with Self-learning Symbiotic Diagnostic Algorithms and Models to accurately and reliably detect the precursors to damages that occur to the structure are discussed. Experiments conducted in a laboratory environment shows potential of the proposed technique.

Free-radical sensing by using naphthalimide based mesoporous silica (MCM-41) nanoparticles: A combined fluorescence and cellular imaging study

NASA Astrophysics Data System (ADS)

Jha, Gaurav; Roy, Subhasis; Sahu, Prabhat Kumar; Banerjee, Somnath; Anoop, N.; Rahaman, Abdur; Sarkar, Moloy

2018-01-01

Keeping in mind the advantages of material-based systems over simple molecule-based systems, we have designed and developed three inorganic-organic hybrid systems by anchoring 1,8-naphthalimide derivatives to mesoporous silica nanoparticles for detection of free radicals. Prior to photophysical study, systems are characterized by spectroscopic, microscopic and thermo-gravimetric techniques. Steady state and time-resolved fluorescence studies demonstrate that the hydrazine based system is senstive towards detection of various free radicals. Cellular imaging study reveals cell permeability and toxicity study demonstrates the non-toxic nature of the material. These studies have suggested that present system has the potential to be used in various biological applications.

A Robust Damage-Reporting Strategy for Polymeric Materials Enabled by Aggregation-Induced Emission.

PubMed

Robb, Maxwell J; Li, Wenle; Gergely, Ryan C R; Matthews, Christopher C; White, Scott R; Sottos, Nancy R; Moore, Jeffrey S

2016-09-28

Microscopic damage inevitably leads to failure in polymers and composite materials, but it is difficult to detect without the aid of specialized equipment. The ability to enhance the detection of small-scale damage prior to catastrophic material failure is important for improving the safety and reliability of critical engineering components, while simultaneously reducing life cycle costs associated with regular maintenance and inspection. Here, we demonstrate a simple, robust, and sensitive fluorescence-based approach for autonomous detection of damage in polymeric materials and composites enabled by aggregation-induced emission (AIE). This simple, yet powerful system relies on a single active component, and the general mechanism delivers outstanding performance in a wide variety of materials with diverse chemical and mechanical properties.

Fiber optic thermal/fast neutron and gamma ray scintillation detector

DOEpatents

Neal, John S.; Mihalczo, John T

2007-10-30

A system for detecting fissile and fissionable material originating external to the system includes: a .sup.6Li loaded glass fiber scintillator for detecting thermal neutrons, x-rays and gamma rays; a fast scintillator for detecting fast neutrons, x-rays and gamma rays, the fast scintillator conjoined with the glass fiber scintillator such that the fast scintillator moderates fast neutrons prior to their detection as thermal neutrons by the glass fiber scintillator; and a coincidence detection system for processing the time distributions of arriving signals from the scintillators.

Systems and methods of detecting force and stress using tetrapod nanocrystal

DOEpatents

Choi, Charina L.; Koski, Kristie J.; Sivasankar, Sanjeevi; Alivisatos, A. Paul

2013-08-20

Systems and methods of detecting force on the nanoscale including methods for detecting force using a tetrapod nanocrystal by exposing the tetrapod nanocrystal to light, which produces a luminescent response by the tetrapod nanocrystal. The method continues with detecting a difference in the luminescent response by the tetrapod nanocrystal relative to a base luminescent response that indicates a force between a first and second medium or stresses or strains experienced within a material. Such systems and methods find use with biological systems to measure forces in biological events or interactions.

Anomaly detection applied to a materials control and accounting database

DOE Office of Scientific and Technical Information (OSTI.GOV)

Whiteson, R.; Spanks, L.; Yarbro, T.

An important component of the national mission of reducing the nuclear danger includes accurate recording of the processing and transportation of nuclear materials. Nuclear material storage facilities, nuclear chemical processing plants, and nuclear fuel fabrication facilities collect and store large amounts of data describing transactions that involve nuclear materials. To maintain confidence in the integrity of these data, it is essential to identify anomalies in the databases. Anomalous data could indicate error, theft, or diversion of material. Yet, because of the complex and diverse nature of the data, analysis and evaluation are extremely tedious. This paper describes the authors workmore » in the development of analysis tools to automate the anomaly detection process for the Material Accountability and Safeguards System (MASS) that tracks and records the activities associated with accountable quantities of nuclear material at Los Alamos National Laboratory. Using existing guidelines that describe valid transactions, the authors have created an expert system that identifies transactions that do not conform to the guidelines. Thus, this expert system can be used to focus the attention of the expert or inspector directly on significant phenomena.« less

Aptamer-incorporated hydrogels for visual detection, controlled drug release, and targeted cancer therapy

PubMed Central

Liu, Jun; Kang, Huaizhi; Donovan, Michael; Zhu, Zhi

2017-01-01

Hydrogels are water-retainable materials, made from cross-linked polymers, that can be tailored to applications in bioanalysis and biomedicine. As technology advances, an increasing number of molecules have been used as the components of hydrogel systems. However, the shortcomings of these systems have prompted researchers to find new materials that can be incorporated into them. Among all of these emerging materials, aptamers have recently attracted substantial attention because of their unique properties, for example biocompatibility, selective binding, and molecular recognition, all of which make them promising candidates for target-responsive hydrogel engineering. In this work, we will review how aptamers have been incorporated into hydrogel systems to enable colorimetric detection, controlled drug release, and targeted cancer therapy. PMID:22052153

Vision-Based Sensor for Early Detection of Periodical Defects in Web Materials

PubMed Central

Bulnes, Francisco G.; Usamentiaga, Rubén; García, Daniel F.; Molleda, Julio

2012-01-01

During the production of web materials such as plastic, textiles or metal, where there are rolls involved in the production process, periodically generated defects may occur. If one of these rolls has some kind of flaw, it can generate a defect on the material surface each time it completes a full turn. This can cause the generation of a large number of surface defects, greatly degrading the product quality. For this reason, it is necessary to have a system that can detect these situations as soon as possible. This paper presents a vision-based sensor for the early detection of this kind of defects. It can be adapted to be used in the inspection of any web material, even when the input data are very noisy. To assess its performance, the sensor system was used to detect periodical defects in hot steel strips. A total of 36 strips produced in ArcelorMittal Avilés factory were used for this purpose, 18 to determine the optimal configuration of the proposed sensor using a full-factorial experimental design and the other 18 to verify the validity of the results. Next, they were compared with those provided by a commercial system used worldwide, showing a clear improvement. PMID:23112629

Fission meter

DOEpatents

Rowland, Mark S [Alamo, CA; Snyderman, Neal J [Berkeley, CA

2012-04-10

A neutron detector system for discriminating fissile material from non-fissile material wherein a digital data acquisition unit collects data at high rate, and in real-time processes large volumes of data directly into information that a first responder can use to discriminate materials. The system comprises counting neutrons from the unknown source and detecting excess grouped neutrons to identify fission in the unknown source.

A Multiple Sensor Machine Vision System for Automatic Hardwood Feature Detection

Treesearch

D. Earl Kline; Richard W. Conners; Daniel L. Schmoldt; Philip A. Araman; Robert L. Brisbin

1993-01-01

A multiple sensor machine vision prototype is being developed to scan full size hardwood lumber at industrial speeds for automatically detecting features such as knots holes, wane, stain, splits, checks, and color. The prototype integrates a multiple sensor imaging system, a materials handling system, a computer system, and application software. The prototype provides...

A mobile ferromagnetic shape detection sensor using a Hall sensor array and magnetic imaging.

PubMed

Misron, Norhisam; Shin, Ng Wei; Shafie, Suhaidi; Marhaban, Mohd Hamiruce; Mailah, Nashiren Farzilah

2011-01-01

This paper presents a mobile Hall sensor array system for the shape detection of ferromagnetic materials that are embedded in walls or floors. The operation of the mobile Hall sensor array system is based on the principle of magnetic flux leakage to describe the shape of the ferromagnetic material. Two permanent magnets are used to generate the magnetic flux flow. The distribution of magnetic flux is perturbed as the ferromagnetic material is brought near the permanent magnets and the changes in magnetic flux distribution are detected by the 1-D array of the Hall sensor array setup. The process for magnetic imaging of the magnetic flux distribution is done by a signal processing unit before it displays the real time images using a netbook. A signal processing application software is developed for the 1-D Hall sensor array signal acquisition and processing to construct a 2-D array matrix. The processed 1-D Hall sensor array signals are later used to construct the magnetic image of ferromagnetic material based on the voltage signal and the magnetic flux distribution. The experimental results illustrate how the shape of specimens such as square, round and triangle shapes is determined through magnetic images based on the voltage signal and magnetic flux distribution of the specimen. In addition, the magnetic images of actual ferromagnetic objects are also illustrated to prove the functionality of mobile Hall sensor array system for actual shape detection. The results prove that the mobile Hall sensor array system is able to perform magnetic imaging in identifying various ferromagnetic materials.

A Mobile Ferromagnetic Shape Detection Sensor Using a Hall Sensor Array and Magnetic Imaging

PubMed Central

Misron, Norhisam; Shin, Ng Wei; Shafie, Suhaidi; Marhaban, Mohd Hamiruce; Mailah, Nashiren Farzilah

2011-01-01

This paper presents a Mobile Hall Sensor Array system for the shape detection of ferromagnetic materials that are embedded in walls or floors. The operation of the Mobile Hall Sensor Array system is based on the principle of magnetic flux leakage to describe the shape of the ferromagnetic material. Two permanent magnets are used to generate the magnetic flux flow. The distribution of magnetic flux is perturbed as the ferromagnetic material is brought near the permanent magnets and the changes in magnetic flux distribution are detected by the 1-D array of the Hall sensor array setup. The process for magnetic imaging of the magnetic flux distribution is done by a signal processing unit before it displays the real time images using a netbook. A signal processing application software is developed for the 1-D Hall sensor array signal acquisition and processing to construct a 2-D array matrix. The processed 1-D Hall sensor array signals are later used to construct the magnetic image of ferromagnetic material based on the voltage signal and the magnetic flux distribution. The experimental results illustrate how the shape of specimens such as square, round and triangle shapes is determined through magnetic images based on the voltage signal and magnetic flux distribution of the specimen. In addition, the magnetic images of actual ferromagnetic objects are also illustrated to prove the functionality of Mobile Hall Sensor Array system for actual shape detection. The results prove that the Mobile Hall Sensor Array system is able to perform magnetic imaging in identifying various ferromagnetic materials. PMID:22346653

Evanescent field Sensors Based on Tantalum Pentoxide Waveguides – A Review

PubMed Central

Schmitt, Katrin; Oehse, Kerstin; Sulz, Gerd; Hoffmann, Christian

2008-01-01

Evanescent field sensors based on waveguide surfaces play an important role where high sensitivity is required. Particularly tantalum pentoxide (Ta2O5) is a suitable material for thin-film waveguides due to its high refractive index and low attenuation. Many label-free biosensor systems such as grating couplers and interferometric sensors as well as fluorescence-based systems benefit from this waveguide material leading to extremely high sensitivity. Some biosensor systems based on Ta2O5 waveguides already took the step into commercialization. This report reviews the various detection systems in terms of limit of detection, the applications, and the suitable surface chemistry. PMID:27879731

Development Of Ultrasonic Testing Based On Delphi Program As A Learning Media In The Welding Material Study Of Detection And Welding Disables In The Environment Of Vocational Education

NASA Astrophysics Data System (ADS)

Dwi Cahyono, Bagus; Ainur, Chandra

2018-04-01

The development of science and technology has a direct impact on the preparation of qualified workers, including the preparation of vocational high school graduates. Law Number 20 the Year 2003 on National Education System explains that the purpose of vocational education is to prepare learners to be ready to work in certain fields. One of the learning materials in Vocational High School is welding and detecting welding defects. Introduction of welding and detecting welding defects, one way that can be done is by ultrasonic testing will be very difficult if only capitalize the book only. Therefore this study aims to adopt ultrasonic testing in a computer system. This system is called Delphi Program-based Ultrasonic Testing Expert System. This system is used to determine the classification and type of welding defects of the welded defect indicator knew. In addition to the system, there is a brief explanation of the notion of ultrasonic testing, calibration procedures and inspection procedures ultrasonic testing. In this system, ultrasonic input data testing that shows defects entered into the computer manually. This system is built using Delphi 7 software and Into Set Up Compiler as an installer. The method used in this research is Research and Development (R & D), with the following stages: (1) preliminary research; (2) manufacture of software design; (3) materials collection; (4) early product development; (5) validation of instructional media experts; (6) product analysis and revision; (8) media trials in learning; And (9) result of end product of instructional media. The result of the research shows that: (1) the result of feasibility test according to ultrasonic material testing expert that the system is feasible to be used as instructional media in welding material subject and welding defect detection in vocational education environment, because it contains an explanation about detection method of welding defect using method Ultrasonic testing in detail; (2) feasibility test results according to media experts, that this system has a very attractive visual, user friendly, compatible with windows and Linux and media size that is not too large; And (3) result of test by using data of indication of welding defect in PT PAL Surabaya, obtained classification data of welding defect in accordance with calculation of welding defect classification.

ORNL actinide materials and a new detection system for superheavy nuclei

NASA Astrophysics Data System (ADS)

Rykaczewski, Krzysztof P.; Roberto, James B.; Brewer, Nathan T.; Utyonkov, Vladimir K.

2016-12-01

The actinide resources and production capabilities at Oak Ridge National Laboratory (ORNL) are reviewed, including potential electromagnetic separation of rare radioactive materials. The first experiments at the Dubna Gas Filled Recoil Separator (DGFRS) with a new digital detection system developed at ORNL and University of Tennessee Knoxville (UTK) are presented. These studies used 240Pu material provided by ORNL and mixed-Cf targets made at ORNL. The proposal to use an enriched 251Cf target and a large dose of 58Fe beam to reach the N = 184 shell closure and to observe new elements with Z = 124, 122 and 120 is discussed.

Systems and methods for detecting neutrons

DOEpatents

Bross, Alan D.; Mellott, Kerry L.; Pla-Dalmau, Anna

2005-08-09

Systems and methods for detecting neutrons. One or more neutron-sensitive scintillators can be configured from a plurality of nano-sized particles, dopants and an extruded plastic material, such as polystyrene. The nano-sized particles can be compounded into the extruded plastic material with at least one dopant that permits the plastic material to scintillate. One or more plastic light collectors can be associated with a neutron-sensitive scintillator, such that the plastic light collector includes a central hole thereof. A wavelength-shifting fiber can then be located within the hole. The wavelength shifting (WLS) fiber absorbs scintillation light having a wavelength thereof and re-emits the light at a longer wavelength.

Systems and methods for detecting x-rays

DOEpatents

Bross, Alan D.; Mellott, Kerry L.; Pla-Dalmau, Anna

2006-05-02

Systems and methods for detecting x-rays are disclosed herein. One or more x-ray-sensitive scintillators can be configured from a plurality of heavy element nano-sized particles and a plastic material, such as polystyrene. As will be explained in greater detail herein, the heavy element nano-sized particles (e.g., PbWO₄) can be compounded into the plastic material with at least one dopant that permits the plastic material to scintillate. X-rays interact with the heavy element nano-sized particles to produce electrons that can deposit energy in the x-ray sensitive scintillator, which in turn can produce light.

Method and apparatus for continuous fluid leak monitoring and detection in analytical instruments and instrument systems

DOEpatents

Weitz, Karl K [Pasco, WA; Moore, Ronald J [West Richland, WA

2010-07-13

A method and device are disclosed that provide for detection of fluid leaks in analytical instruments and instrument systems. The leak detection device includes a collection tube, a fluid absorbing material, and a circuit that electrically couples to an indicator device. When assembled, the leak detection device detects and monitors for fluid leaks, providing a preselected response in conjunction with the indicator device when contacted by a fluid.

Methods and Apparatus for Detecting Defects in an Object of Interest

NASA Technical Reports Server (NTRS)

Hartman, John K. (Inventor); Pearson, Lee H (Inventor)

2017-01-01

A method for detecting defects in an object of interest comprises applying an ultrasonic signal including a tone burst having a predetermined frequency and number of cycles into an object of interest, receiving a return signal reflected from the object of interest, and processing the return signal to detect defects in at least one inner material. The object may have an outer material and the at least one inner material that have different acoustic impedances. An ultrasonic sensor system includes an ultrasonic sensor configured to generate an ultrasonic signal having a tone burst at a predetermined frequency corresponding to a resonant frequency of an outer material of an object of interest.

Monte Carlo Simulations for the Detection of Buried Objects Using Single Sided Backscattered Radiation.

PubMed

Yip, Mary; Saripan, M Iqbal; Wells, Kevin; Bradley, David A

2015-01-01

Detection of buried improvised explosive devices (IEDs) is a delicate task, leading to a need to develop sensitive stand-off detection technology. The shape, composition and size of the IEDs can be expected to be revised over time in an effort to overcome increasingly sophisticated detection methods. As an example, for the most part, landmines are found through metal detection which has led to increasing use of non-ferrous materials such as wood or plastic containers for chemical based explosives being developed. Monte Carlo simulations have been undertaken considering three different commercially available detector materials (hyperpure-Ge (HPGe), lanthanum(III) bromide (LaBr) and thallium activated sodium iodide (NaI(Tl)), applied at a stand-off distance of 50 cm from the surface and burial depths of 0, 5 and 10 cm, with sand as the obfuscating medium. Target materials representing medium density wood and mild steel have been considered. Each detector has been modelled as a 10 cm thick cylinder with a 20 cm diameter. It appears that HPGe represents the most promising detector for this application. Although it was not the highest density material studied, its excellent energy resolving capability leads to the highest quality spectra from which detection decisions can be inferred. The simulation work undertaken here suggests that a vehicle-born threat detection system could be envisaged using a single betatron and a series of detectors operating in parallel observing the space directly in front of the vehicle path. Furthermore, results show that non-ferrous materials such as wood can be effectively discerned in such remote-operated detection system, with the potential to apply a signature analysis template matching technique for real-time analysis of such data.

Open Circuit Resonant Sensors for Composite Damage Detection and Diagnosis

NASA Technical Reports Server (NTRS)

Mielnik, John J., Jr.

2011-01-01

Under the Integrated Vehicle Health Management (IVHM) program work was begun to investigate the feasibility of sensor systems for detecting and diagnosing damage to aircraft composite structures and materials. Specific interest for this study was in damage initiated by environmental storm hazards and the direct effect of lightning strikes on the material structures of a composite aircraft in flight. A series of open circuit resonant sensors was designed, fabricated, characterized, and determined to be a potentially viable means for damage detection and diagnosis of composite materials. The results of this research and development effort are documented in this report.

The Architecture Design of Detection and Calibration System for High-voltage Electrical Equipment

NASA Astrophysics Data System (ADS)

Ma, Y.; Lin, Y.; Yang, Y.; Gu, Ch; Yang, F.; Zou, L. D.

2018-01-01

With the construction of Material Quality Inspection Center of Shandong electric power company, Electric Power Research Institute takes on more jobs on quality analysis and laboratory calibration for high-voltage electrical equipment, and informationization construction becomes urgent. In the paper we design a consolidated system, which implements the electronic management and online automation process for material sampling, test apparatus detection and field test. In the three jobs we use QR code scanning, online Word editing and electronic signature. These techniques simplify the complex process of warehouse management and testing report transferring, and largely reduce the manual procedure. The construction of the standardized detection information platform realizes the integrated management of high-voltage electrical equipment from their networking, running to periodic detection. According to system operation evaluation, the speed of transferring report is doubled, and querying data is also easier and faster.

Biosensors and their applications in detection of organophosphorus pesticides in the environment.

PubMed

Hassani, Shokoufeh; Momtaz, Saeideh; Vakhshiteh, Faezeh; Maghsoudi, Armin Salek; Ganjali, Mohammad Reza; Norouzi, Parviz; Abdollahi, Mohammad

2017-01-01

This review discusses the past and recent advancements of biosensors focusing on detection of organophosphorus pesticides (OPs) due to their exceptional use during the last decades. Apart from agricultural benefits, OPs also impose adverse toxicological effects on animal and human population. Conventional approaches such as chromatographic techniques used for pesticide detection are associated with several limitations. A biosensor technology is unique due to the detection sensitivity, selectivity, remarkable performance capabilities, simplicity and on-site operation, fabrication and incorporation with nanomaterials. This study also provided specifications of the most OPs biosensors reported until today based on their transducer system. In addition, we highlighted the application of advanced complementary materials and analysis techniques in OPs detection systems. The availability of these new materials associated with new sensing techniques has led to introduction of easy-to-use analytical tools of high sensitivity and specificity in the design and construction of OPs biosensors. In this review, we elaborated the achievements in sensing systems concerning innovative nanomaterials and analytical techniques with emphasis on OPs.

Plasma reactor waste management systems

NASA Technical Reports Server (NTRS)

Ness, Robert O., Jr.; Rindt, John R.; Ness, Sumitra R.

1992-01-01

The University of North Dakota is developing a plasma reactor system for use in closed-loop processing that includes biological, materials, manufacturing, and waste processing. Direct-current, high-frequency, or microwave discharges will be used to produce plasmas for the treatment of materials. The plasma reactors offer several advantages over other systems, including low operating temperatures, low operating pressures, mechanical simplicity, and relatively safe operation. Human fecal material, sunflowers, oats, soybeans, and plastic were oxidized in a batch plasma reactor. Over 98 percent of the organic material was converted to gaseous products. The solids were then analyzed and a large amount of water and acid-soluble materials were detected. These materials could possibly be used as nutrients for biological systems.

Thermographic imaging for high-temperature composite materials: A defect detection study

NASA Technical Reports Server (NTRS)

Roth, Don J.; Bodis, James R.; Bishop, Chip

1995-01-01

The ability of a thermographic imaging technique for detecting flat-bottom hole defects of various diameters and depths was evaluated in four composite systems (two types of ceramic matrix composites, one metal matrix composite, and one polymer matrix composite) of interest as high-temperature structural materials. The holes ranged from 1 to 13 mm in diameter and 0.1 to 2.5 mm in depth in samples approximately 2-3 mm thick. The thermographic imaging system utilized a scanning mirror optical system and infrared (IR) focusing lens in conjunction with a mercury cadmium telluride infrared detector element to obtain high resolution infrared images. High intensity flash lamps located on the same side as the infrared camera were used to heat the samples. After heating, up to 30 images were sequentially acquired at 70-150 msec intervals. Limits of detectability based on depth and diameter of the flat-bottom holes were defined for each composite material. Ultrasonic and radiographic images of the samples were obtained and compared with the thermographic images.

Applications of a Fast Neutron Detector System to Verification of Special Nuclear Materials

NASA Astrophysics Data System (ADS)

Mayo, Douglas R.; Byrd, Roger C.; Ensslin, Norbert; Krick, Merlyn S.; Mercer, David J.; Miller, Michael C.; Prettyman, Thomas H.; Russo, Phyllis A.

1998-04-01

An array of boron-loaded plastic optically coupled to bismuth germanate scintillators has been developed to detect neutrons for measurement of special nuclear materials. The phoswiched detection system has the advantage of a high neutron detection efficiency and short die-away time. This is achieved by mixing the moderator (plastic) and the detector (^10B) at the molecular level. Simulations indicate that the neutron capture probabilities equal or exceed those of the current thermal neutron multiplicity techniques which have the moderator (polyethylene) and detectors (^3He gas proportional tubes) macroscopically separate. Experiments have been performed to characterize the response of these detectors and validate computer simulations. The fast neutron detection system may be applied to the quantitative assay of plutonium in high (α,n) backgrounds, with emphasis on safeguards and enviromental scenarios. Additional applications of the insturment, in a non-quantative mode, has been tested for possible verification activities involving dismantlement of nuclear weapons. A description of the detector system, simulations and preliminary data will be presented.

Detection of chemical warfare simulants using Raman excitation at 1064 nm

NASA Astrophysics Data System (ADS)

Dentinger, Claire; Mabry, Mark W.; Roy, Eric G.

2014-05-01

Raman spectroscopy is a powerful technique for material identification. The technique is sensitive to primary and higher ordered molecular structure and can be used to identify unknown materials by comparison with spectral reference libraries. Additionally, miniaturization of opto-electronic components has permitted development of portable Raman analyzers that are field deployable. Raman scattering is a relatively weak effect compared to a competing phenomenon, fluorescence. Even a moderate amount of fluorescence background interference can easily prevent identification of unknown materials. A long wavelength Raman system is less likely to induce fluorescence from a wider variety of materials than a higher energy visible laser system. Compounds such as methyl salicylate (MS), diethyl malonate (DEM), and dimethyl methylphosphonate (DMMP) are used as chemical warfare agent (CWA) simulants for development of analytical detection strategies. Field detection of these simulants however poses unique challenges because threat identification must be made quickly without the turnaround time usually required for a laboratory based analysis. Fortunately, these CWA simulants are good Raman scatterers, and field based detection using portable Raman instruments is promising. Measurements of the CWA simulants were done using a 1064 nm based portable Raman spectrometer. The longer wavelength excitation laser was chosen relative to a visible based laser systems because the 1064 nm based spectrometer is less likely to induce fluorescence and more suitable to a wider range of materials. To more closely mimic real world measurement situations, different sample presentations were investigated.

Millimeter wave detection of nuclear radiation: an alternative detection mechanism.

PubMed

Gopalsami, N; Chien, H T; Heifetz, A; Koehl, E R; Raptis, A C

2009-08-01

We present a nuclear radiation detection mechanism using millimeter waves as an alternative to conventional detection. It is based on the concept that nuclear radiation causes ionization of air and that if we place a dielectric material near the radiation source, it acts as a charge accumulator of the air ions. We have found that millimeter waves can interrogate the charge cloud on the dielectric material remotely. This concept was tested with a standoff millimeter wave system by monitoring the charge levels on a cardboard tube placed in an x-ray beam.

10 CFR 73.45 - Performance capabilities for fixed site physical protection systems.

Code of Federal Regulations, 2010 CFR

2010-01-01

... authorization schedules and entry criteria before permitting entry and to initiate response measures to deny... movement of strategic special nuclear material within material access areas. To achieve this capability the physical protection system shall: (1) Detect unauthorized placement and movement of strategic special...

Development of a handheld widefield hyperspectral imaging (HSI) sensor for standoff detection of explosive, chemical, and narcotic residues

NASA Astrophysics Data System (ADS)

Nelson, Matthew P.; Basta, Andrew; Patil, Raju; Klueva, Oksana; Treado, Patrick J.

2013-05-01

The utility of Hyper Spectral Imaging (HSI) passive chemical detection employing wide field, standoff imaging continues to be advanced in detection applications. With a drive for reduced SWaP (Size, Weight, and Power), increased speed of detection and sensitivity, developing a handheld platform that is robust and user-friendly increases the detection capabilities of the end user. In addition, easy to use handheld detectors could improve the effectiveness of locating and identifying threats while reducing risks to the individual. ChemImage Sensor Systems (CISS) has developed the HSI Aperio™ sensor for real time, wide area surveillance and standoff detection of explosives, chemical threats, and narcotics for use in both government and commercial contexts. Employing liquid crystal tunable filter technology, the HSI system has an intuitive user interface that produces automated detections and real-time display of threats with an end user created library of threat signatures that is easily updated allowing for new hazardous materials. Unlike existing detection technologies that often require close proximity for sensing and so endanger operators and costly equipment, the handheld sensor allows the individual operator to detect threats from a safe distance. Uses of the sensor include locating production facilities of illegal drugs or IEDs by identification of materials on surfaces such as walls, floors, doors, deposits on production tools and residue on individuals. In addition, the sensor can be used for longer-range standoff applications such as hasty checkpoint or vehicle inspection of residue materials on surfaces or bulk material identification. The CISS Aperio™ sensor has faster data collection, faster image processing, and increased detection capability compared to previous sensors.

Radiation Detection and Dual-Energy X-Ray Imaging for Port Security

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pashby, J.; Glenn, S.; Divin, C.

Millions of cargo containers are transported across the United States border annually and are inspected for illicit radioactive material and contraband using a combination of passive radiation portal monitors (RPM) and high energy X-ray non-intrusive inspection (NII) systems. As detection performance is expected to vary with the material composition of cargo, characterizing the types of material present in cargo is important to national security. This work analyzes the passive radiation and dual energy radiography signatures from on RPM and two NII system, respectively. First, the cargos were analyzed to determine their ability to attenuate emissions from an embedded radioactive source.more » Secondly, dual-energy X-ray discrimination was used to determine the material composition and density of the cargos.« less

Locating Sensors for Detecting Source-to-Target Patterns of Special Nuclear Material Smuggling: A Spatial Information Theoretic Approach

PubMed Central

Przybyla, Jay; Taylor, Jeffrey; Zhou, Xuesong

2010-01-01

In this paper, a spatial information-theoretic model is proposed to locate sensors for detecting source-to-target patterns of special nuclear material (SNM) smuggling. In order to ship the nuclear materials from a source location with SNM production to a target city, the smugglers must employ global and domestic logistics systems. This paper focuses on locating a limited set of fixed and mobile radiation sensors in a transportation network, with the intent to maximize the expected information gain and minimize the estimation error for the subsequent nuclear material detection stage. A Kalman filtering-based framework is adapted to assist the decision-maker in quantifying the network-wide information gain and SNM flow estimation accuracy. PMID:22163641

Locating sensors for detecting source-to-target patterns of special nuclear material smuggling: a spatial information theoretic approach.

PubMed

Przybyla, Jay; Taylor, Jeffrey; Zhou, Xuesong

2010-01-01

In this paper, a spatial information-theoretic model is proposed to locate sensors for detecting source-to-target patterns of special nuclear material (SNM) smuggling. In order to ship the nuclear materials from a source location with SNM production to a target city, the smugglers must employ global and domestic logistics systems. This paper focuses on locating a limited set of fixed and mobile radiation sensors in a transportation network, with the intent to maximize the expected information gain and minimize the estimation error for the subsequent nuclear material detection stage. A Kalman filtering-based framework is adapted to assist the decision-maker in quantifying the network-wide information gain and SNM flow estimation accuracy.

Terahertz Computed Tomography of NASA Thermal Protection System Materials

NASA Technical Reports Server (NTRS)

Roth, D. J.; Reyes-Rodriguez, S.; Zimdars, D. A.; Rauser, R. W.; Ussery, W. W.

2011-01-01

A terahertz axial computed tomography system has been developed that uses time domain measurements in order to form cross-sectional image slices and three-dimensional volume renderings of terahertz-transparent materials. The system can inspect samples as large as 0.0283 cubic meters (1 cubic foot) with no safety concerns as for x-ray computed tomography. In this study, the system is evaluated for its ability to detect and characterize flat bottom holes, drilled holes, and embedded voids in foam materials utilized as thermal protection on the external fuel tanks for the Space Shuttle. X-ray micro-computed tomography was also performed on the samples to compare against the terahertz computed tomography results and better define embedded voids. Limits of detectability based on depth and size for the samples used in this study are loosely defined. Image sharpness and morphology characterization ability for terahertz computed tomography are qualitatively described.

Active interrogation using low-energy nuclear reactions

NASA Astrophysics Data System (ADS)

Antolak, Arlyn; Doyle, Barney; Leung, Ka-Ngo; Morse, Daniel; Provencio, Paula

2005-09-01

High-energy photons and neutrons can be used to interrogate for heavily shielded fissile materials inside sealed cargo containers by detecting their prompt and/or delayed fission signatures. The FIND (Fissmat Inspection for Nuclear Detection) active interrogation system is based on a dual neutron+gamma source that uses low-energy (< 500 keV) proton- or deuteron-induced nuclear reactions to produce high intensities of mono-energetic gamma rays and/or neutrons. The source can be operated in either pulsed (e.g., to detect delayed photofission neutrons and gammas) or continuous (e.g., detecting prompt fission signatures) modes. For the gamma-rays, the source target can be segmented to incorporate different (p,γ) isotopes for producing gamma-rays at selective energies, thereby improving the probability of detection. The design parameters for the FIND system are discussed and preliminary accelerator-based measurements of gamma and neutron yields, background levels, and fission signals for several target materials under consideration are presented.

RadMAP: The Radiological Multi-sensor Analysis Platform

NASA Astrophysics Data System (ADS)

Bandstra, Mark S.; Aucott, Timothy J.; Brubaker, Erik; Chivers, Daniel H.; Cooper, Reynold J.; Curtis, Joseph C.; Davis, John R.; Joshi, Tenzing H.; Kua, John; Meyer, Ross; Negut, Victor; Quinlan, Michael; Quiter, Brian J.; Srinivasan, Shreyas; Zakhor, Avideh; Zhang, Richard; Vetter, Kai

2016-12-01

The variability of gamma-ray and neutron background during the operation of a mobile detector system greatly limits the ability of the system to detect weak radiological and nuclear threats. The natural radiation background measured by a mobile detector system is the result of many factors, including the radioactivity of nearby materials, the geometric configuration of those materials and the system, the presence of absorbing materials, and atmospheric conditions. Background variations tend to be highly non-Poissonian, making it difficult to set robust detection thresholds using knowledge of the mean background rate alone. The Radiological Multi-sensor Analysis Platform (RadMAP) system is designed to allow the systematic study of natural radiological background variations and to serve as a development platform for emerging concepts in mobile radiation detection and imaging. To do this, RadMAP has been used to acquire extensive, systematic background measurements and correlated contextual data that can be used to test algorithms and detector modalities at low false alarm rates. By combining gamma-ray and neutron detector systems with data from contextual sensors, the system enables the fusion of data from multiple sensors into novel data products. The data are curated in a common format that allows for rapid querying across all sensors, creating detailed multi-sensor datasets that are used to study correlations between radiological and contextual data, and develop and test novel techniques in mobile detection and imaging. In this paper we will describe the instruments that comprise the RadMAP system, the effort to curate and provide access to multi-sensor data, and some initial results on the fusion of contextual and radiological data.

Life detection systems.

NASA Technical Reports Server (NTRS)

Mitz, M. A.

1972-01-01

Some promising newer approaches for detecting microorganisms are discussed, giving particular attention to the integration of different methods into a single instrument. Life detection methods may be divided into biological, chemical, and cytological methods. Biological methods are based on the biological properties of assimilation, metabolism, and growth. Devices for the detection of organic materials are considered, taking into account an instrument which volatilizes, separates, and analyzes a sample sequentially. Other instrumental systems described make use of a microscope and the cytochemical staining principle.

Physical security and cyber security issues and human error prevention for 3D printed objects: detecting the use of an incorrect printing material

NASA Astrophysics Data System (ADS)

Straub, Jeremy

2017-06-01

A wide variety of characteristics of 3D printed objects have been linked to impaired structural integrity and use-efficacy. The printing material can also have a significant impact on the quality, utility and safety characteristics of a 3D printed object. Material issues can be created by vendor issues, physical security issues and human error. This paper presents and evaluates a system that can be used to detect incorrect material use in a 3D printer, using visible light imaging. Specifically, it assesses the ability to ascertain the difference between materials of different color and different types of material with similar coloration.

Open Circuit Resonant (SansEC) Sensor for Composite Damage Detection and Diagnosis in Aircraft Lightning Environments

NASA Technical Reports Server (NTRS)

Wang, Chuantong; Dudley, Kenneth L.; Szatkowski, George N.

2012-01-01

Composite materials are increasingly used in modern aircraft for reducing weight, improving fuel efficiency, and enhancing the overall design, performance, and manufacturability of airborne vehicles. Materials such as fiberglass reinforced composites (FRC) and carbon-fiber-reinforced polymers (CFRP) are being used to great advantage in airframes, wings, engine nacelles, turbine blades, fairings, fuselage and empennage structures, control surfaces and coverings. However, the potential damage from the direct and indirect effects of lightning strikes is of increased concern to aircraft designers and operators. When a lightning strike occurs, the points of attachment and detachment on the aircraft surface must be found by visual inspection, and then assessed for damage by maintenance personnel to ensure continued safe flight operations. In this paper, a new method and system for aircraft in-situ damage detection and diagnosis are presented. The method and system are based on open circuit (SansEC) sensor technology developed at NASA Langley Research Center. SansEC (Sans Electric Connection) sensor technology is a new technical framework for designing, powering, and interrogating sensors to detect damage in composite materials. Damage in composite material is generally associated with a localized change in material permittivity and/or conductivity. These changes are sensed using SansEC. Unique electrical signatures are used for damage detection and diagnosis. NASA LaRC has both experimentally and theoretically demonstrated that SansEC sensors can be effectively used for in-situ composite damage detection.

Nondestructive Inspection System for Special Nuclear Material Using Inertial Electrostatic Confinement Fusion Neutrons and Laser Compton Scattering Gamma-Rays

NASA Astrophysics Data System (ADS)

Ohgaki, H.; Daito, I.; Zen, H.; Kii, T.; Masuda, K.; Misawa, T.; Hajima, R.; Hayakawa, T.; Shizuma, T.; Kando, M.; Fujimoto, S.

2017-07-01

A Neutron/Gamma-ray combined inspection system for hidden special nuclear materials (SNMs) in cargo containers has been developed under a program of Japan Science and Technology Agency in Japan. This inspection system consists of an active neutron-detection system for fast screening and a laser Compton backscattering gamma-ray source in coupling with nuclear resonance fluorescence (NRF) method for precise inspection. The inertial electrostatic confinement fusion device has been adopted as a neutron source and two neutron-detection methods, delayed neutron noise analysis method and high-energy neutron-detection method, have been developed to realize the fast screening system. The prototype system has been constructed and tested in the Reactor Research Institute, Kyoto University. For the generation of the laser Compton backscattering gamma-ray beam, a race track microtron accelerator has been used to reduce the size of the system. For the NRF measurement, an array of LaBr3(Ce) scintillation detectors has been adopted to realize a low-cost detection system. The prototype of the gamma-ray system has been demonstrated in the Kansai Photon Science Institute, National Institutes for Quantum and Radiological Science and Technology. By using numerical simulations based on the data taken from these prototype systems and the inspection-flow, the system designed by this program can detect 1 kg of highly enriched 235U (HEU) hidden in an empty 20-ft container within several minutes.

Detection Of Special Nuclear Materials Tagged Neutrons

DOE Office of Scientific and Technical Information (OSTI.GOV)

Deyglun, Clement; Perot, Bertrand; Carasco, Cedric

In order to detect Special Nuclear Materials (SNM) in unattended luggage or cargo containers in the field of homeland security, fissions are induced by 14 MeV neutrons produced by an associated particle DT neutron generator, and prompt fission particles correlated with tagged neutron are detected by plastic scintillators. SMN produce high multiplicity events due to induced fissions, whereas nonnuclear materials produce low multiplicity events due to cross-talk, (n,2n) or (n,n'γ) reactions. The data acquisition electronics is made of compact FPGA boards. The coincidence window is triggered by the alpha particle detection, allowing to tag the emission date and direction ofmore » the 14 MeV interrogating neutron. The first part of the paper presents experiment vs. calculation comparisons to validate MCNP-PoliMi simulations and the post-processing tools developed with the data analysis framework ROOT. Measurements have been performed using different targets (iron, lead, graphite), first with small plastic scintillators (10 x 10 x 10 cm{sup 3}) and then with large detectors (10 x 10 x 100 cm{sup 3}) to demonstrate that nuclear materials can be differentiated from nonnuclear dense materials (iron, lead) in iron and wood matrixes. A special attention is paid on SNM detection in abandoned luggage. In the second part of the paper, the performances of a cargo container inspection system are studied by numerical simulation, following previous work reported in. Detectors dimensions and shielding against the neutron generator background are optimized for container inspection. Events not correlated to an alpha particle (uncorrelated background), counting statistics, time and energy resolutions of the data acquisition system are all taken into account in a realistic numerical model. The impact of the container matrix (iron, ceramic, wood) has been investigated by studying the system capability to detect a few kilograms of SNM in different positions in the cargo container, within 10 min acquisitions. (authors)« less

Nuclear Security in the 21^st Century

NASA Astrophysics Data System (ADS)

Archer, Daniel E.

2006-10-01

Nuclear security has been a priority for the United States, starting in the 1940s with the secret cities of the Manhattan Project. In the 1970s, the United States placed radiation monitoring equipment at nuclear facilities to detect nuclear material diversion. Following the breakup of the Soviet Union, cooperative Russian/U.S. programs were launched in Russia to secure the estimated 600+ metric tons of fissionable materials against diversion (Materials Protection, Control, and Accountability -- MPC&A). Furthermore, separate programs were initiated to detect nuclear materials at the country's borders in the event that these materials had been stolen (Second Line of Defense - SLD). In the 2000s, new programs have been put in place in the United States for radiation detection, and research is being funded for more advanced systems. This talk will briefly touch on the history of nuclear security and then focus on some recent research efforts in radiation detection. Specifically, a new breed of radiation monitors will be examined along with the concept of sensor networks.

Improved explosive collection and detection with rationally assembled surface sampling materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chouyyok, Wilaiwan; Bays, J. Timothy; Gerasimenko, Aleksandr A.

Sampling and detection of trace explosives is a key analytical process in modern transportation safety. In this work we have explored some of the fundamental analytical processes for collection and detection of trace level explosive on surfaces with the most widely utilized system, thermal desorption IMS. The performance of the standard muslin swipe material was compared with chemically modified fiberglass cloth. The fiberglass surface was modified to include phenyl functional groups. When compared to standard muslin, the phenyl functionalized fiberglass sampling material showed better analyte release from the sampling material as well as improved response and repeatability from multiple usesmore » of the same swipe. The improved sample release of the functionalized fiberglass swipes resulted in a significant increase in sensitivity. Various physical and chemical properties were systematically explored to determine optimal performance. The results herein have relevance to improving the detection of other explosive compounds and potentially to a wide range of other chemical sampling and field detection challenges.« less

Design and validation of inert homemade explosive simulants for X-ray-based inspection systems

NASA Astrophysics Data System (ADS)

Faust, Anthony A.; Nacson, Sabatino; Koffler, Bruce; Bourbeau, Éric; Gagne, Louis; Laing, Robin; Anderson, C. J.

2014-05-01

Transport Canada (TC), the Canadian Armed Forces, and other public security agencies have an interest in the assessment of the potential utility of advanced explosives detection technologies to aid in the detection and interdiction of commercial grade, military grade, and homemade or improvised explosives (HME or IE). The availability of suitable, non-hazardous, non-toxic, explosive simulants is of concern when assessing the potential utility of such detection systems. Lack of simulants limits the training opportunities, and ultimately the detection probability, of security personnel using these systems. While simulants for commercial and military grade explosives are available for a wide variety of detection technologies, the design and production of materials to simulate improvised explosives has not kept pace with this emerging threat. Funded by TC and the Canadian Safety and Security Program, Defence Research and Development Canada (DRDC), Visiontec Systems, and Optosecurity engaged in an effort to develop inert, non-toxic Xray interrogation simulants for IE materials such as ammonium nitrate, potassium chlorate, and triacetone triperoxide. These simulants were designed to mimic key X-ray interrogation-relevant material properties of real improvised explosives, principally their bulk density and effective atomic number. Different forms of the simulants were produced and tested, simulating the different explosive threat formulations that could be encountered by front line security workers. These simulants comply with safety and stability requirements, and as best as possible match form and homogeneity. This paper outlines the research program, simulant design, and validation.

Gas cluster ion beam for the characterization of organic materials in submarine basalts as Mars analogs

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sano, Naoko, E-mail: naoko.sano@ncl.ac.uk; Barlow, Anders J.; Cumpson, Peter J.

The solar system contains large quantities of organic compounds that can form complex molecular structures. The processing of organic compounds by biological systems leads to molecules with distinctive structural characteristics; thus, the detection and characterization of organic materials could lead to a high degree of confidence in the existence of extra-terrestrial life. Given the nature of the surface of most planetary bodies in the solar system, evidence of life is more likely to be found in the subsurface where conditions are more hospitable. Basalt is a common rock throughout the solar system and the primary rock type on Mars andmore » Earth. Basalt is therefore a rock type that subsurface life might exploit and as such a suitable material for the study of methods required to detect and analyze organic material in rock. Telluric basalts from Earth represent an analog for extra-terrestrial rocks where the indigenous organic matter could be analyzed for molecular biosignatures. This study focuses on organic matter in the basalt with the use of surface analysis techniques utilizing Ar gas cluster ion beams (GCIB); time of flight secondary ion mass spectrometry (ToF-SIMS), and x-ray photoelectron spectroscopy (XPS), to characterize organic molecules. Tetramethylammonium hydroxide (TMAH) thermochemolysis was also used to support the data obtained using the surface analysis techniques. The authors demonstrate that organic molecules were found to be heterogeneously distributed within rock textures. A positive correlation was observed to exist between the presence of microtubule textures in the basalt and the organic compounds detected. From the results herein, the authors propose that ToF-SIMS with an Ar GCIB is effective at detecting organic materials in such geological samples, and ToF-SIMS combined with XPS and TMAH thermochemolysis may be a useful approach in the study of extra-terrestrial organic material and life.« less

N-SCAN: new vibromodulation system for detection and monitoring of cracks and other contact-type defects

NASA Astrophysics Data System (ADS)

Donskoy, Dmitri; Ekimov, Alexander; Luzzato, Emile; Lottiaux, Jean-Louis; Stoupin, Stanislav; Zagrai, Andrei

2003-08-01

In recent years, innovative vibro-modulation technique has been introduced for detection of contact-type interfaces such as cracks, debondings, and delaminations. The technique utilizes the effect of nonlinear interaction of ultrasound and vibrations at the interface of the defect. Vibration varies on the contact area of the interface modulating passing through ultrasonic wave. The modulation manifests itself as additional side-band spectral components with the combination frequencies in the spectrum of the received signal. The presence of these components allows for detection and differentiation of the contact-type defects from other structural and material inhomogeneities. Vibro-modulation technique has been implemented in N-SCAN damage detection system. The system consists of a digital synthesizer, high and low frequency amplifiers, a magnetostrictive shaker, ultrasonic transducers and a PC-based data acquisition/processing station with N-SCAN software. The ability of the system to detect contact-type defects was experimentally verified using specimens of simple and complex geometries made of steel, aluminum, composites and other structural materials. N-SCAN proved to be very effective for nondestructive testing of full-scale structures ranging from 24 foot-long gun barrels to stainless steel pipes used in nuclear power plants. Among advantages of the system are applicability for the wide range of structural materials and for structures with complex geometries, real time data processing, convenient interface for system operation, simplicity of interpretation of results, no need for sensor scanning along structure, onsite inspection of large structures at a fraction of time as compared with conventional techniques. This paper describes the basic principles of nonlinear vibro-modulation NDE technique, some theoretical background for nonlinear interaction and justification of signal processing algorithm. It is also presents examples of practical implementation and application of the technique.

Damage Assessment of Creep Tested and Thermally Aged Metallic Alloys Using Acousto-Ultrasonics

NASA Technical Reports Server (NTRS)

Gyekenyesi, Andrew L.; Kautz, Harold E.; Baaklini, George Y.

2001-01-01

In recent years emphasis has been placed on the early detection of material changes experienced in turbine powerplant components. During the scheduled overhaul of a turbine, the current techniques of examination of various hot section components aim to find flaws such as cracks, wear, and erosion, as well as excessive deformations. Thus far, these localized damage modes have been detected with satisfactory results. However, the techniques used to find these flaws provide no information on life until the flaws are actually detected. Major improvements in damage assessment, safety, as well as more accurate life prediction could be achieved if nondestructive evaluation (NDE) techniques could be utilized to sense material changes that occur prior to the localized defects mentioned. Because of elevated temperatures and excessive stresses, turbine components may experience creep behavior. As a result, it is desirable to monitor and access the current condition of such components. Research at the NASA Glenn Research Center involves developing and utilizing an NDE technique that discloses distributed material changes that occur prior to the localized damage detected by the current methods of inspection. In a recent study, creep processes in a nickel-base alloy were the life-limiting condition of interest, and the NDE technique was acousto-ultrasonics (AU). AU is an NDE technique that utilizes two ultrasonic transducers to interrogate the condition of a test specimen. The sending transducer introduces an ultrasonic pulse at a point on the surface of the specimen while a receiving transducer detects the signal after it has passed through the material. The goal of the method is to correlate certain parameters of the detected waveform to characteristics of the material between the two transducers. Here, the waveform parameter of interest is the attenuation due to internal damping for which information is being garnered from the frequency domain. The parameters utilized to indirectly quantify the attenuation are the ultrasonic decay rate as well as various moments of the frequency power spectrum. A new, user-friendly, graphical interface AU system was developed at NASA Glenn. This system is an all-inclusive, multifunction system that controls the sending and receiving ultrasonic transducers as well as all posttest signal analysis. The system's postprocessing software calculates the multiple parameters used to study the material of interest.

Application of gas-coupled laser acoustic detection to gelatins and underwater sensing

DOE Office of Scientific and Technical Information (OSTI.GOV)

Caron, James N.; Kunapareddy, Pratima

2014-02-18

Gas-coupled Laser Acoustic Detection (GCLAD) has been used as a method to sense ultrasound waves in materials without contact of the material surface. To sense the waveform, a laser beam is directed parallel to the material surface and displaced or deflected when the radiated waveform traverses the beam. We present recent tests that demonstrate the potential of using this technique for detecting ultrasound in gelatin phantoms and in water. As opposed to interferometric detection, GCLAD operates independently of the optical surface properties of the material. This allows the technique to be used in cases where the material is transparent ormore » semi-transparent. We present results on sensing ultrasound in gelatin phantoms that are used to mimic biological materials. As with air-coupled transducers, the frequency response of GCLAD at high frequencies is limited by the high attenuation of ultrasound in air. In contrast, water has a much lower attenuation. Here we demonstrate the use of a GCLAD-like system in water, measuring the directivity response at 1 MHz and sensing waveforms with higher frequency content.« less

Performance of coincidence-based PSD on LiF/ZnS Detectors for Multiplicity Counting

DOE Office of Scientific and Technical Information (OSTI.GOV)

Robinson, Sean M.; Stave, Sean C.; Lintereur, Azaree

Abstract: Mass accountancy measurement is a nuclear nonproliferation application which utilizes coincidence and multiplicity counters to verify special nuclear material declarations. With a well-designed and efficient detector system, several relevant parameters of the material can be verified simultaneously. 6LiF/ZnS scintillating sheets may be used for this purpose due to a combination of high efficiency and short die-away times in systems designed with this material, but involve choices of detector geometry and exact material composition (e.g., the addition of Ni-quenching in the material) that must be optimized for the application. Multiplicity counting for verification of declared nuclear fuel mass involves neutronmore » detection in conditions where several neutrons arrive in a short time window, with confounding gamma rays. This paper considers coincidence-based Pulse-Shape Discrimination (PSD) techniques developed to work under conditions of high pileup, and the performance of these algorithms with different detection materials. Simulated and real data from modern LiF/ZnS scintillator systems are evaluated with these techniques and the relationship between the performance under pileup and material characteristics (e.g., neutron peak width and total light collection efficiency) are determined, to allow for an optimal choice of detector and material.« less

Infrared detector device inspection system

DOEpatents

Soehnel, Grant; Bender, Daniel A.

2016-08-09

Methods and apparatuses for identifying carrier lifetimes are disclosed herein. In a general embodiment, a beam of light is sent to a group of locations on a material for an optical device. Photons emitted from the material are detected at each of the group of locations. A carrier lifetime is identified for each of the group of locations based on the photons detected from each of the group of locations.

Turbomachine monitoring system and method

DOEpatents

Delvaux, John McConnell

2016-02-23

In an embodiment, a system includes a turbomachine having a first turbomachine component including a first mechanoluminescent material. The first turbomachine component is configured to produce a first light emission upon exposure to a mechanical stimulus sufficient to cause mechanoluminescence by the first mechanoluminescent material. The system also includes a turbomachine monitoring system configured to monitor the structural health of the first component based on detection of the first light emission.

Method of Generating X-Ray Diffraction Data for Integral Detection of Twin Defects in Super-Hetero-Epitaxial Materials

NASA Technical Reports Server (NTRS)

Park, Yeonjoon (Inventor); Choi, Sang Hyouk (Inventor); King, Glen C. (Inventor); Elliott, James R. (Inventor)

2009-01-01

A method provides X-ray diffraction (XRD) data suitable for integral detection of a twin defect in a strained or lattice-matched epitaxial material made from components having crystal structures having symme try belonging to different space groups. The material is mounted in a n X-ray diffraction (XRD) system. In one embodiment, the XRD system's goniometer angle Omega is set equal to (Theta(sub B)-Beta) where The ta(sub B) is a Bragg angle for a designated crystal plane of the allo y that is disposed at a non-perpendicular orientation with respect to the {111) crystal plane, and Beta is the angle between the designate d crystal plane and a { 111 } crystal plane of one of the epitaxial components. The XRD system's detector angle is set equal to (Theta(su b B)+Beta). The material can be rotated through an angle of azimuthal rotation Phi about the axis aligned with the material. Using the det ector, the intensity of the X-ray diffraction is recorded at least at the angle at which the twin defect occurs.

Acoustic Emission Detection of Impact Damage on Space Shuttle Structures

NASA Technical Reports Server (NTRS)

Prosser, William H.; Gorman, Michael R.; Madaras, Eric I.

2004-01-01

The loss of the Space Shuttle Columbia as a result of impact damage from foam debris during ascent has led NASA to investigate the feasibility of on-board impact detection technologies. AE sensing has been utilized to monitor a wide variety of impact conditions on Space Shuttle components ranging from insulating foam and ablator materials, and ice at ascent velocities to simulated hypervelocity micrometeoroid and orbital debris impacts. Impact testing has been performed on both reinforced carbon composite leading edge materials as well as Shuttle tile materials on representative aluminum wing structures. Results of these impact tests will be presented with a focus on the acoustic emission sensor responses to these impact conditions. These tests have demonstrated the potential of employing an on-board Shuttle impact detection system. We will describe the present plans for implementation of an initial, very low frequency acoustic impact sensing system using pre-existing flight qualified hardware. The details of an accompanying flight measurement system to assess the Shuttle s acoustic background noise environment as a function of frequency will be described. The background noise assessment is being performed to optimize the frequency range of sensing for a planned future upgrade to the initial impact sensing system.

Handheld dual thermal neutron detector and gamma-ray spectrometer

DOE Office of Scientific and Technical Information (OSTI.GOV)

Stowe, Ashley C.; Burger, Arnold; Bhattacharya, Pijush

2017-05-02

A combined thermal neutron detector and gamma-ray spectrometer system, including: a first detection medium including a lithium chalcopyrite crystal operable for detecting neutrons; a gamma ray shielding material disposed adjacent to the first detection medium; a second detection medium including one of a doped metal halide, an elpasolite, and a high Z semiconductor scintillator crystal operable for detecting gamma rays; a neutron shielding material disposed adjacent to the second detection medium; and a photodetector coupled to the second detection medium also operable for detecting the gamma rays; wherein the first detection medium and the second detection medium do not overlapmore » in an orthogonal plane to a radiation flux. Optionally, the first detection medium includes a .sup.6LiInSe.sub.2 crystal. Optionally, the second detection medium includes a SrI.sub.2(Eu) scintillation crystal.« less

Performance characterization of material identification systems

NASA Astrophysics Data System (ADS)

Brown, Christopher D.; Green, Robert L.

2006-10-01

In recent years a number of analytical devices have been proposed and marketed specifically to enable field-based material identification. Technologies reliant on mass, near- and mid-infrared, and Raman spectroscopies are available today, and other platforms are imminent. These systems tend to perform material recognition based on an on-board library of material signatures. While figures of merit for traditional quantitative analytical sensors are broadly established (e.g., SNR, selectivity, sensitivity, limit of detection/decision), measures of performance for material identification systems have not been systematically discussed. In this paper we present an approach to performance characterization similar in spirit to ROC curves, but including elements of precision-recall curves and specialized for the intended-use of material identification systems. Important experimental considerations are discussed, including study design, sources of bias, uncertainty estimation, and cross-validation and the approach as a whole is illustrated using a commercially available handheld Raman material identification system.

77 FR 6857 - Pipeline Safety: Notice of Public Meetings on Improving Pipeline Leak Detection System...

Federal Register 2010, 2011, 2012, 2013, 2014

2012-02-09

... DEPARTMENT OF TRANSPORTATION Pipeline and Hazardous Materials Safety Administration [Docket ID... installed to lessen the volume of natural gas and hazardous liquid released during catastrophic pipeline... p.m. Panel 3: Considerations for Natural Gas Pipeline Leak Detection Systems 3:30 p.m. Break 3:45 p...

Research on metallic material defect detection based on bionic sensing of human visual properties

NASA Astrophysics Data System (ADS)

Zhang, Pei Jiang; Cheng, Tao

2018-05-01

Due to the fact that human visual system can quickly lock the areas of interest in complex natural environment and focus on it, this paper proposes an eye-based visual attention mechanism by simulating human visual imaging features based on human visual attention mechanism Bionic Sensing Visual Inspection Model Method to Detect Defects of Metallic Materials in the Mechanical Field. First of all, according to the biologically visually significant low-level features, the mark of defect experience marking is used as the intermediate feature of simulated visual perception. Afterwards, SVM method was used to train the advanced features of visual defects of metal material. According to the weight of each party, the biometrics detection model of metal material defect, which simulates human visual characteristics, is obtained.

Network of wireless gamma ray sensors for radiological detection and identification

NASA Astrophysics Data System (ADS)

Barzilov, A.; Womble, P.; Novikov, I.; Paschal, J.; Board, J.; Moss, K.

2007-04-01

The paper describes the design and development of a network of wireless gamma-ray sensors based on cell phone or WiFi technology. The system is intended for gamma-ray detection and automatic identification of radioactive isotopes and nuclear materials. The sensor is a gamma-ray spectrometer that uses wireless technology to distribute the results. A small-size sensor module contains a scintillation detector along with a small size data acquisition system, PDA, battery, and WiFi radio or a cell phone modem. The PDA with data acquisition and analysis software analyzes the accumulated spectrum on real-time basis and returns results to the screen reporting the isotopic composition and intensity of detected radiation source. The system has been programmed to mitigate false alarms from medical isotopes and naturally occurring radioactive materials. The decision-making software can be "trained" to indicate specific signatures of radiation sources like special nuclear materials. The sensor is supplied with GPS tracker coupling radiological information with geographical coordinates. The sensor is designed for easy use and rapid deployment in common wireless networks.

Fluorescence emission spectral measurements for the detection of oil on shore

DOE Office of Scientific and Technical Information (OSTI.GOV)

Balick, L.K.; Di Benedetto, J.A.; Lutz, S.S.

1997-06-01

The US DOE Special Technologies Laboratory is developing an airborne Laser-Induced Fluorescence Imaging (LIFI) system to support environmental management of government Utilities. This system, or a system to be derived from it, is being evaluated for its potential to detect spilled oils on shore, in wetlands, and on ice. To more fully understand the detectivity of oil spills, emphasis has been placed on the spectral contrast between the oil signatures and signatures associated with the natural backgrounds (sand, vegetation, etc.). To support this evaluation, two series of controlled measurements have been performed to provide rigorous characterization of the excitation-emission propertiesmore » of some oils and background materials, and to look at the effects of weathering of oil on terrestrial background materials. Oil targets included a heavy crude oil, diesel, kerosene, and aviation fuel and backgrounds included beach sand, straw, mud, tar and kelp. Fluorescence of oil on background materials decreases rapidly over the first few days of exposure to the environment and is more rapid than for neat oil samples.« less

Fluorescence emission spectral measurements for the detection of oil on shore

DOE Office of Scientific and Technical Information (OSTI.GOV)

Balick, L.K.; Di Benedetto, J.A.; Lutz, S.S.

1996-12-31

The U.S. DOE Special Technologies Laboratory is developing an airborne Laser-Induced Fluorescence Imaging (LIFI) system to support environmental management of government facilities. This system, or a system to be derived from it, is being evaluated for its potential to detect spilled oils oN shore, in wetlands, and on ice. To more fully understand the detectivity of oil spills, emphasis has been placed on the spectral contrast between the oil signatures and signatures associated with the natural backgrounds (sand, vegetation, etc.). To support this evaluation, two series of controlled measurements have been performed to provide rigorous characterization of the excitation-emission propertiesmore » of some oils and background materials, and to look at the effects of weathering of oil on terrestrial background materials. Oil targets included a heavy crude oil, diesel, kerosene, and aviation fuel and backgrounds included beach sand, straw, mud, tar and kelp. Fluorescence of oil on background materials decreases rapidly over the first few days of exposure to the environment and is more rapid than for neat oil samples.« less

Coherent scattering noise reduction method with wavelength diversity detection for holographic data storage system

NASA Astrophysics Data System (ADS)

Nakamura, Yusuke; Hoshizawa, Taku; Takashima, Yuzuru

2017-09-01

A new method, wavelength diversity detection (WDD), for improving signal quality is proposed and its effectiveness is numerically confirmed. We consider that WDD is especially effective for high-capacity systems having low hologram diffraction efficiencies. In such systems, the signal quality is primarily limited by coherent scattering noise; thus, effective improvement of the signal quality under a scattering-limited system is of great interest. WDD utilizes a new degree of freedom, the spectrum width, and scattering by molecules to improve the signal quality of the system. We found that WDD improves the quality by counterbalancing the degradation of the quality due to Bragg mismatch. With WDD, a higher-scattering-coefficient medium can improve the quality. The result provides an interesting insight into the requirements for material characteristics, especially for a large-M/# material. In general, a larger-M/# material contains more molecules; thus, the system is subject to more scattering, which actually improves the quality with WDD. We propose a pathway for a future holographic data storage system (HDSS) using WDD, which can record a larger amount of data than a conventional HDSS.

APSTNG: neutron interrogation for detection of explosives, drugs, and nuclear and chemical warfare materials

NASA Astrophysics Data System (ADS)

Rhodes, Edgar A.; Peters, Charles W.

1993-02-01

A recently developed neutron diagnostic probe system has the potential to satisfy a significant number of van-mobile and fixed-portal requirements for nondestructive detection, including monitoring of contraband explosives, drugs, and weapon materials, and treaty verification of sealed munitions. The probe is based on a unique associated-particle sealed-tube neutron generator (APSTNG) that interrogates the object of interest with a low-intensity beam of 14- MeV neutrons generated from the deuterium-tritium reaction and that detects the alpha-particle associated with each neutron. Gamma-ray spectra of resulting neutron reactions identify nuclides associated with all major chemicals in explosives, drugs, and chemical warfare agents, as well as many pollutants and fissile and fertile special nuclear material. Flight times determined from detection times of the gamma-rays and alpha-particles yield a separate coarse tomographic image of each identified nuclide. The APSTNG also forms the basis for a compact fast-neutron transmission imaging system that can be used along with or instead of the emission imaging system. Proof-of-concept experiments have been performed under laboratory conditions for simulated nuclear and chemical warfare munitions and for explosives and drugs. The small and relatively inexpensive APSTNG exhibits high reliability and can be quickly replaced. Surveillance systems based on APSTNG technology can avoid the large physical size, high capital and operating expenses, and reliability problems associated with complex accelerators.

Source imaging of drums in the APNEA system

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hensley, D.

1995-12-31

The APNea System is a neutron assay device utilizing both a passive mode and a differential-dieaway active mode. The total detection efficiency is not spatially uniform, even for an empty chamber, and a drum matrix in the chamber can severely distort this response. In order to achieve a response which is independent of the way the source material is distributed in a drum, an imaging procedure has been developed which treats the drum as a number of virtual (sub)volumes. Since each virtual volume of source material is weighted with the appropriate instrument parameters (detection efficiency and thermal flux), the finalmore » assay result is essentially independent of the actual distribution of the source material throughout the drum and its matrix.« less

Accelerating fissile material detection with a neutron source

DOEpatents

Rowland, Mark S.; Snyderman, Neal J.

2018-01-30

A neutron detector system for discriminating fissile material from non-fissile material wherein a digital data acquisition unit collects data at high rate, and in real-time processes large volumes of data directly to count neutrons from the unknown source and detecting excess grouped neutrons to identify fission in the unknown source. The system includes a Poisson neutron generator for in-beam interrogation of a possible fissile neutron source and a DC power supply that exhibits electrical ripple on the order of less than one part per million. Certain voltage multiplier circuits, such as Cockroft-Walton voltage multipliers, are used to enhance the effective of series resistor-inductor circuits components to reduce the ripple associated with traditional AC rectified, high voltage DC power supplies.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Chiaro, PJ

The Environmental Effects Laboratory of the Engineering Science and Technology Division of Oak Ridge National Laboratory performed a series of tests to further evaluate and characterize the radiological response of a ''Cricket'' radiation detection system. The Cricket, manufactured by Rad/Comm Systems Corporation of Ontario, Canada, is designed to detect radioactive material that may be contained in scrap metal. The Cricket's detection unit is designed to be mounted to the base of a grappler, allowing it to monitor material while the material is being held by the grappler tines. The Cricket was tested for background stability, energy response, spherical response, surfacemore » uniformity, angular dependence, and alarm actuation. Some of these tests were repeated from a prior test of a Cricket at the Environmental Effects Laboratory as reported in ORNL/TM-2002/94. Routine environmental tests--normal temperature and relatively humidity--were also performed as part of this testing process. Overall, the Cricket performed well during the testing process. The design of the instrument and the inherent photon energy of the radionuclides had some affect on portions of the tests but do not detract from the value-added benefits of the Cricket's detection capabilities.« less

Biosignature Preservation and Detection in Mars Analog Environments.

PubMed

Hays, Lindsay E; Graham, Heather V; Des Marais, David J; Hausrath, Elisabeth M; Horgan, Briony; McCollom, Thomas M; Parenteau, M Niki; Potter-McIntyre, Sally L; Williams, Amy J; Lynch, Kennda L

2017-04-01

This review of material relevant to the Conference on Biosignature Preservation and Detection in Mars Analog Environments summarizes the meeting materials and discussions and is further expanded upon by detailed references to the published literature. From this diverse source material, there is a detailed discussion on the habitability and biosignature preservation potential of five primary analog environments: hydrothermal spring systems, subaqueous environments, subaerial environments, subsurface environments, and iron-rich systems. Within the context of exploring past habitable environments on Mars, challenges common to all of these key environments are laid out, followed by a focused discussion for each environment regarding challenges to orbital and ground-based observations and sample selection. This leads into a short section on how these challenges could influence our strategies and priorities for the astrobiological exploration of Mars. Finally, a listing of urgent needs and future research highlights key elements such as development of instrumentation as well as continued exploration into how Mars may have evolved differently from Earth and what that might mean for biosignature preservation and detection. Key Words: Biosignature preservation-Biosignature detection-Mars analog environments-Conference report-Astrobiological exploration. Astrobiology 17, 363-400.

Highly Sensitive and Selective Uranium Detection in Natural Water Systems Using a Luminescent Mesoporous Metal-Organic Framework Equipped with Abundant Lewis Basic Sites: A Combined Batch, X-ray Absorption Spectroscopy, and First Principles Simulation Investigation.

PubMed

Liu, Wei; Dai, Xing; Bai, Zhuanling; Wang, Yanlong; Yang, Zaixing; Zhang, Linjuan; Xu, Lin; Chen, Lanhua; Li, Yuxiang; Gui, Daxiang; Diwu, Juan; Wang, Jianqiang; Zhou, Ruhong; Chai, Zhifang; Wang, Shuao

2017-04-04

Uranium is not only a strategic resource for the nuclear industry but also a global contaminant with high toxicity. Although several strategies have been established for detecting uranyl ions in water, searching for new uranium sensor material with great sensitivity, selectivity, and stability remains a challenge. We introduce here a hydrolytically stable mesoporous terbium(III)-based MOF material compound 1, whose channels are as large as 27 Å × 23 Å and are equipped with abundant exposed Lewis basic sites, the luminescence intensity of which can be efficiently and selectively quenched by uranyl ions. The detection limit in deionized water reaches 0.9 μg/L, far below the maximum contamination standard of 30 μg/L in drinking water defined by the United States Environmental Protection Agency, making compound 1 currently the only MOF material that can achieve this goal. More importantly, this material exhibits great capability in detecting uranyl ions in natural water systems such as lake water and seawater with pH being adjusted to 4, where huge excesses of competing ions are present. The uranyl detection limits in Dushu Lake water and in seawater were calculated to be 14.0 and 3.5 μg/L, respectively. This great detection capability originates from the selective binding of uranyl ions onto the Lewis basic sites of the MOF material, as demonstrated by synchrotron radiation extended X-ray adsorption fine structure, X-ray adsorption near edge structure, and first principles calculations, further leading to an effective energy transfer between the uranyl ions and the MOF skeleton.

Advances in Nuclear Monitoring Technologies

NASA Astrophysics Data System (ADS)

Park, Brent

2006-03-01

Homeland security requires low-cost, large-area detectors for locating and identifying weapons-usable nuclear materials and monitors for radiological isotopes that are more robust than current systems. Recent advances in electronics materials and nanotechnology, specifically organic semiconductors and inorganic quantum dots, offer potential improvements. We provide an overview of the physical processes involved in radiation detection using these new materials in the design of new device structures. Examples include recent efforts on quantum dots, as well as more traditional radiation-detecting materials such as CdZnTe and high-pressure xenon. Detector improvements demand not only new materials but also enhanced data-analysis tools that reduce false alarms and thus increase the quality of decisions. Additional computing power on hand-held platforms should enable the application of advanced algorithms to radiation-detection problems in the field, reducing the need to transmit data and thus delay analysis.

Application of thermoluminescence for detection of cascade shower 1: Hardware and software of reader system

NASA Technical Reports Server (NTRS)

Akashi, M.; Kawaguchi, S.; Watanabe, Z.; Misaki, A.; Niwa, M.; Okamoto, Y.; Fujinaga, T.; Ichimura, M.; Shibata, T.; Dake, S.

1985-01-01

A reader system for the detection of cascade showers via luminescence induced by heating sensitive material (BaSO4:Eu) is developed. The reader system is composed of following six instruments: (1) heater, (2) light guide, (3) image intensifier, (4) CCD camera, (5) image processor, (6) microcomputer. The efficiency of these apparatuses and software application for image analysis is reported.

Rattling Nucleons: New Developments in Active Interrogation of Special Nuclear Material

DOE Office of Scientific and Technical Information (OSTI.GOV)

Robert C. Runkle; David L. Chichester; Scott J. Thompson

2012-01-01

Active interrogation is a vigorous area of research and development due to its promise of offering detection and characterization capabilities of special nuclear material in environments where passive detection fails. The primary value added by active methods is the capability to penetrate shielding - special nuclear material itself, incidental materials, or intentional shielding - and advocates hope that active interrogation will provide a solution to the problem of detecting shielded uranium, which is at present the greatest obstacle to interdiction efforts. The technique also provides a unique benefit for quantifying nuclear material in high background-radiation environments, an area important formore » nuclear material safeguards and material accountancy. Progress has been made in the field of active interrogation on several fronts, most notably in the arenas of source development, systems integration, and the integration and exploitation of multiple fission and non-fission signatures. But penetration of interrogating radiation often comes at a cost, not only in terms of finance and dose but also in terms of induced backgrounds, system complexity, and extended measurement times (including set up and acquisition). These costs make the calculus for deciding to implement active interrogation more subtle than may be apparent. The purpose of this review is thus to examine existing interrogation methods, compare and contrast their attributes and limitations, and identify missions where active interrogation may hold the most promise.« less

Rattling nucleons: New developments in active interrogation of special nuclear material

NASA Astrophysics Data System (ADS)

Runkle, Robert C.; Chichester, David L.; Thompson, Scott J.

2012-01-01

Active interrogation is a vigorous area of research and development due to its promise of offering detection and characterization capabilities of special nuclear material in environments where passive detection fails. The primary value added by active methods is the capability to penetrate shielding—special nuclear material itself, incidental materials, or intentional shielding—and advocates hope that active interrogation will provide a solution to the problem of detecting shielded uranium, which is at present the greatest obstacle to interdiction efforts. The technique also provides a unique benefit for quantifying nuclear material in high background-radiation environments, an area important for nuclear material safeguards and material accountancy. Progress has been made in the field of active interrogation on several fronts, most notably in the arenas of source development, systems integration, and the integration and exploitation of multiple fission and non-fission signatures. But penetration of interrogating radiation often comes at a cost, not only in terms of finance and dose but also in terms of induced backgrounds, system complexity, and extended measurement times (including set up and acquisition). These costs make the calculus for deciding to implement active interrogation more subtle than may be apparent. The purpose of this review is thus to examine existing interrogation methods, compare and contrast their attributes and limitations, and identify missions where active interrogation may hold the most promise.

Visible-light system for detecting doxorubicin contamination on skin and surfaces.

PubMed

Van Raalte, J; Rice, C; Moss, C E

1990-05-01

A portable system that uses fluorescence stimulated by visible light to identify doxorubicin contamination on skin and surfaces was studied. When activated by violet-blue light in the 465-nm range, doxorubicin fluoresces, emitting orange-red light in the 580-nm range. The light source to stimulate fluorescence was a slide projector with a filter to selectively pass short-wave (blue) visible light. Fluorescence was both observed visually with viewing spectacles and photographed. Solutions of doxorubicin in sterile 0.9% sodium chloride injection were prepared in nine standard concentrations ranging from 2 to 0.001 mg/mL. Droplets of each admixture were placed on stainless steel, laboratory coat cloth, pieces of latex examination glove, bench-top absorbent padding, and other materials on which antineoplastics might spill or leak. These materials then were stored for up to eight weeks and photographed weekly. The relative ability of water, household bleach, hydrogen peroxide solution, and soap solution to deactivate doxorubicin was also measured. Finally, this system was used to inspect the antineoplastic-drug preparation and administration areas of three outpatient cancer clinics for doxorubicin contamination. Doxorubicin fluorescence was easily detectable with viewing spectacles when a slide projector was used as the light source. The photographic method was sensitive for doxorubicin concentrations from 2.0 to 0.001 mg/mL. Immersion of study materials in bleach for one minute eliminated detectable fluorescence. Doxorubicin contamination is detectable for at least eight weeks in the ambient environment. Probable doxorubicin contamination was detected in two of the three clinics surveyed. A safe, portable system that uses fluorescence stimulated by visible light is a sensitive method for detecting doxorubicin on skin and surfaces.

Infrared-Proximity-Sensor Modules For Robot

NASA Technical Reports Server (NTRS)

Parton, William; Wegerif, Daniel; Rosinski, Douglas

1995-01-01

Collision-avoidance system for articulated robot manipulators uses infrared proximity sensors grouped together in array of sensor modules. Sensor modules, called "sensorCells," distributed processing board-level products for acquiring data from proximity-sensors strategically mounted on robot manipulators. Each sensorCell self-contained and consists of multiple sensing elements, discrete electronics, microcontroller and communications components. Modules connected to central control computer by redundant serial digital communication subsystem including both serial and a multi-drop bus. Detects objects made of various materials at distance of up to 50 cm. For some materials, such as thermal protection system tiles, detection range reduced to approximately 20 cm.

Nanoplatforms for Detection, Remediation and Protection Against Chem-Bio Warfare

NASA Astrophysics Data System (ADS)

Denkbaş, E. B.; Bayram, C.; Kavaz, D.; Çirak, T.; Demirbilek, M.

Chemical and biological substances have been used as warfare agents by terrorists by varying degree of sophistication. It is critical that these agents be detected in real-time with high level of sensitively, specificity, and accuracy. Many different types of techniques and systems have been developed to detect these agents. But there are some limitations in these conventional techniques and systems. Limitations include the collection, handling and sampling procedures, detection limits, sample transfer, expensive equipment, personnel training, and detection materials. Due to the unique properties such as quantum effect, very high surface/volume ratio, enhanced surface reactivity, conductivity, electrical and magnetic properties of the nanomaterials offer great opportunity to develop very fast, sensitive, accurate and cost effective detection techniques and systems to detect chemical and biological (chem.-bio) warfare agents. Furthermore, surface modification of the materials is very easy and effective way to get functional or smart surfaces to be used as nano-biosensor platform. In that respect many different types of nanomaterials have been developed and used for the detection, remediation and protection, such as gold and silver nanoparticles, quantum dots, Nano chips and arrays, fluorescent polymeric and magnetic nanoparticles, fiber optic and cantilever based nanobiosensors, nanofibrillar nanostructures etc. This study summarizes preparation and characterization of nanotechnology based approaches for the detection of and remediation and protection against chem.-bio warfare agents.

Backscatter X-Ray Development for Space Vehicle Thermal Protection Systems

NASA Astrophysics Data System (ADS)

Bartha, Bence B.; Hope, Dale; Vona, Paul; Born, Martin; Corak, Tony

2011-06-01

The Backscatter X-Ray (BSX) imaging technique is used for various single sided inspection purposes. Previously developed BSX techniques for spray-on-foam insulation (SOFI) have been used for detecting defects in Space Shuttle External Tank foam insulation. The developed BSX hardware and techniques are currently being enhanced to advance Non-Destructive Evaluation (NDE) methods for future space vehicle applications. Various Thermal Protection System (TPS) materials were inspected using the enhanced BSX imaging techniques, investigating the capability of the method to detect voids and other discontinuities at various locations within each material. Calibration standards were developed for the TPS materials in order to characterize and develop enhanced BSX inspection capabilities. The ability of the BSX technique to detect both manufactured and natural defects was also studied and compared to through-transmission x-ray techniques. The energy of the x-ray, source to object distance, angle of x-ray, focal spot size and x-ray detector configurations were parameters playing a significant role in the sensitivity of the BSX technique to image various materials and defects. The image processing of the results also showed significant increase in the sensitivity of the technique. The experimental results showed BSX to be a viable inspection technique for space vehicle TPS systems.

Wireless Metal Detection and Surface Coverage Sensing for All-Surface Induction Heating

PubMed Central

Kilic, Veli Tayfun; Unal, Emre; Demir, Hilmi Volkan

2016-01-01

All-surface induction heating systems, typically comprising small-area coils, face a major challenge in detecting the presence of a metallic vessel and identifying its partial surface coverage over the coils to determine which of the coils to power up. The difficulty arises due to the fact that the user can heat vessels made of a wide variety of metals (and their alloys). To address this problem, we propose and demonstrate a new wireless detection methodology that allows for detecting the presence of metallic vessels together with uniquely sensing their surface coverages while also identifying their effective material type in all-surface induction heating systems. The proposed method is based on telemetrically measuring simultaneously inductance and resistance of the induction coil coupled with the vessel in the heating system. Here, variations in the inductance and resistance values for an all-surface heating coil loaded by vessels (made of stainless steel and aluminum) at different positions were systematically investigated at different frequencies. Results show that, independent of the metal material type, unique identification of the surface coverage is possible at all freqeuncies. Additionally, using the magnitude and phase information extracted from the coupled coil impedance, unique identification of the vessel effective material is also achievable, this time independent of its surface coverage. PMID:26978367

Electrochemical detection for microscale analytical systems: a review.

PubMed

Wang, Joseph

2002-02-11

As the field of chip-based microscale systems continues its rapid growth, there are urgent needs for developing compatible detection modes. Electrochemistry detection offers considerable promise for such microfluidic systems, with features that include remarkable sensitivity, inherent miniaturization and portability, independence of optical path length or sample turbidity, low cost, low-power requirements and high compatibility with advanced micromachining and microfabrication technologies. This paper highlights recent advances, directions and key strategies in controlled-potential electrochemical detectors for miniaturized analytical systems. Subjects covered include the design and integration of the electrochemical detection system, its requirements and operational principles, common electrode materials, derivatization reactions, electrical-field decouplers, typical applications and future prospects. It is expected that electrochemical detection will become a powerful tool for microscale analytical systems and will facilitate the creation of truly portable (and possibly disposable) devices.

Photonuclear-based Detection of Nuclear Smuggling in Cargo Containers

NASA Astrophysics Data System (ADS)

Jones, J. L.; Haskell, K. J.; Hoggan, J. M.; Norman, D. R.; Yoon, W. Y.

2003-08-01

The Idaho National Engineering and Environmental Laboratory (INEEL) and the Los Alamos National Laboratory (LANL) have performed experiments in La Honda, California and at the Idaho Accelerator Center in Pocatello, Idaho to assess and develop a photonuclear-based detection system for shielded nuclear materials in cargo containers. The detection system, measuring photonuclear-related neutron emissions, is planned for integration with the ARACOR Eagle Cargo Container Inspection System (Sunnyvale, CA). The Eagle Inspection system uses a nominal 6-MeV electron accelerator and operates with safe radiation exposure limits to both container stowaways and to its operators. The INEEL has fabricated custom-built, helium-3-based, neutron detectors for this inspection application and is performing an experimental application assessment. Because the Eagle Inspection system could not be moved to LANL where special nuclear material was available, the response of the Eagle had to be determined indirectly so as to support the development and testing of the detection system. Experiments in California have successfully matched the delayed neutron emission performance of the ARACOR Eagle with that of the transportable INEEL electron accelerator (i.e., the Varitron) and are reported here. A demonstration test is planned at LANL using the Varitron and shielded special nuclear materials within a cargo container. Detector results are providing very useful information regarding the challenges of delayed neutron counting near the photofission threshold energy of 5.5 - 6.0 MeV, are identifying the possible utilization of prompt neutron emissions to allow enhanced signal-to-noise measurements, and are showing the overall benefits of using higher electron beam energies.

Development of Decision Making Algorithm for Control of Sea Cargo Containers by ``TAGGED'' Neutron Method

NASA Astrophysics Data System (ADS)

Anan'ev, A. A.; Belichenko, S. G.; Bogolyubov, E. P.; Bochkarev, O. V.; Petrov, E. V.; Polishchuk, A. M.; Udaltsov, A. Yu.

2009-12-01

Nowadays in Russia and abroad there are several groups of scientists, engaged in development of systems based on "tagged" neutron method (API method) and intended for detection of dangerous materials, including high explosives (HE). Particular attention is paid to possibility of detection of dangerous objects inside a sea cargo container. Energy gamma-spectrum, registered from object under inspection is used for determination of oxygen/carbon and nitrogen/carbon chemical ratios, according to which dangerous object is distinguished from not dangerous one. Material of filled container, however, gives rise to additional effects of rescattering and moderation of 14 MeV primary neutrons of generator, attenuation of secondary gamma-radiation from reactions of inelastic neutron scattering on objects under inspection. These effects lead to distortion of energy gamma-response from examined object and therefore prevent correct recognition of chemical ratios. These difficulties are taken into account in analytical method, presented in the paper. Method has been validated against experimental data, obtained by the system for HE detection in sea cargo, based on API method and developed in VNIIA. Influence of shielding materials on results of HE detection and identification is considered. Wood and iron were used as shielding materials. Results of method application for analysis of experimental data on HE simulator measurement (tetryl, trotyl, hexogen) are presented.

Development of force-detected THz-ESR measurement system and its application to metal porphyrin complexes

NASA Astrophysics Data System (ADS)

Takahashi, Hideyuki; Okamoto, Tsubasa; Ohmichi, Eiji; Ohta, Hitoshi

Electron spin resonance spectroscopy in the terahertz region (THz-ESR) is a promising technique to study biological materials such as metalloproteins because it directly probes the metal ion sites that play an important role in the emergence of functionality. By combining THz-ESR with force detection, the samples mass is reduced to the order of ng. This feature is of great advantage because the sample preparation process of biological materials is time-consuming. We developed a force-detected THz-ESR system utilizing optical interferometry for precise cantilever displacement measurement. In order to suppress the sensitivity fluctuation and instability of cantilever dynamics under high magnetic field, the tuning of interferometer is feedback-controlled during a measurement. By using this system, we successfully observed the ESR signal of hemin, which is a model substance of hemoglobin and myoglobin, in THz region.

Smart materials: strain sensing and stress determination by means of nanotube sensing systems, composites, and devices

NASA Technical Reports Server (NTRS)

Kim, Jong Dae (Inventor); Nagarajaiah, Satish (Inventor); Barrera, Enrique V. (Inventor); Dharap, Prasad (Inventor); Zhiling, Li (Inventor)

2010-01-01

The present invention is directed toward devices comprising carbon nanotubes that are capable of detecting displacement, impact, stress, and/or strain in materials, methods of making such devices, methods for sensing/detecting/monitoring displacement, impact, stress, and/or strain via carbon nanotubes, and various applications for such methods and devices. The devices and methods of the present invention all rely on mechanically-induced electronic perturbations within the carbon nanotubes to detect and quantify such stress/strain. Such detection and quantification can rely on techniques which include, but are not limited to, electrical conductivity/conductance and/or resistivity/resistance detection/measurements, thermal conductivity detection/measurements, electroluminescence detection/measurements, photoluminescence detection/measurements, and combinations thereof. All such techniques rely on an understanding of how such properties change in response to mechanical stress and/or strain.

Data Fusion for a Vision-Radiological System for Source Tracking and Discovery

DOE Office of Scientific and Technical Information (OSTI.GOV)

Enqvist, Andreas; Koppal, Sanjeev

2015-07-01

A multidisciplinary approach to allow the tracking of the movement of radioactive sources by fusing data from multiple radiological and visual sensors is under development. The goal is to improve the ability to detect, locate, track and identify nuclear/radiological threats. The key concept is that such widely available visual and depth sensors can impact radiological detection, since the intensity fall-off in the count rate can be correlated to movement in three dimensions. To enable this, we pose an important question; what is the right combination of sensing modalities and vision algorithms that can best compliment a radiological sensor, for themore » purpose of detection and tracking of radioactive material? Similarly what is the best radiation detection methods and unfolding algorithms suited for data fusion with tracking data? Data fusion of multi-sensor data for radiation detection have seen some interesting developments lately. Significant examples include intelligent radiation sensor systems (IRSS), which are based on larger numbers of distributed similar or identical radiation sensors coupled with position data for network capable to detect and locate radiation source. Other developments are gamma-ray imaging systems based on Compton scatter in segmented detector arrays. Similar developments using coded apertures or scatter cameras for neutrons have recently occurred. The main limitation of such systems is not so much in their capability but rather in their complexity and cost which is prohibitive for large scale deployment. Presented here is a fusion system based on simple, low-cost computer vision and radiological sensors for tracking of multiple objects and identifying potential radiological materials being transported or shipped. The main focus of this work is the development on two separate calibration algorithms for characterizing the fused sensor system. The deviation from a simple inverse square-root fall-off of radiation intensity is explored and accounted for. In particular, the computer vision system enables a map of distance-dependence of the sources being tracked. Infrared, laser or stereoscopic vision sensors are all options for computer-vision implementation depending on interior vs exterior deployment, resolution desired and other factors. Similarly the radiation sensors will be focused on gamma-ray or neutron detection due to the long travel length and ability to penetrate even moderate shielding. There is a significant difference between the vision sensors and radiation sensors in the way the 'source' or signals are generated. A vision sensor needs an external light-source to illuminate the object and then detects the re-emitted illumination (or lack thereof). However, for a radiation detector, the radioactive material is the source itself. The only exception to this is the field of active interrogations where radiation is beamed into a material to entice new/additional radiation emission beyond what the material would emit spontaneously. The aspect of the nuclear material being the source itself means that all other objects in the environment are 'illuminated' or irradiated by the source. Most radiation will readily penetrate regular material, scatter in new directions or be absorbed. Thus if a radiation source is located near a larger object that object will in turn scatter some radiation that was initially emitted in a direction other than the direction of the radiation detector, this can add to the count rate that is observed. The effect of these scatter is a deviation from the traditional distance dependence of the radiation signal and is a key challenge that needs a combined system calibration solution and algorithms. Thus both an algebraic approach as well as a statistical approach have been developed and independently evaluated to investigate the sensitivity to this deviation from the simplified radiation fall-off as a function of distance. The resulting calibrated system algorithms are used and demonstrated in various laboratory scenarios, and later in realistic tracking scenarios. The selection and testing of radiological and computer-vision sensors for the additional specific scenarios will be the subject of ongoing and future work. (authors)« less

Perimeter intrusion detection and assessment system

DOE Office of Scientific and Technical Information (OSTI.GOV)

Eaton, M.J.; Jacobs, J.; McGovern, D.E.

1977-01-01

The key elements of the system considered at a materials storage site are intrusion sensors, alarm assessment, and system control and display. Three papers discussing each of these topics are compiled. They are abstracted individually. (JSR)

Nondestructive testing based on scanning-from-heating approach: application to nonthrough defect detection and fiber orientation assessment

NASA Astrophysics Data System (ADS)

Belkacemi, Mohamed; Stolz, Christophe; Mathieu, Alexandre; Lemaitre, Guillaume; Massich, Joan; Aubreton, Olivier

2015-11-01

Today, industries ensure the quality of their manufactured products through computer vision techniques and nonconventional imaging. Three-dimensional (3-D) scanners and nondestructive testing (NDT) systems are commonly used independently for such applications. Furthermore, these approaches combined constitute hybrid systems, providing a 3-D reconstruction and NDT analysis. These systems, however, suffer from drawbacks such as errors during the data fusion and higher cost for manufacturers. In an attempt to solve these problems, a single active thermography system based on scanning-from-heating is proposed in this paper. In addition to 3-D digitization of the object, our contributions are twofold: (1) the nonthrough defect detection for a homogeneous metallic object and (2) fiber orientation assessment for a long fiber composite material. The experiments on steel and aluminum plates show that our method achieves the detection of nonthrough defects. Additionally, the estimation of the fiber orientation is evaluated on carbon-fiber composite material.

Particle detection systems and methods

DOEpatents

Morris, Christopher L.; Makela, Mark F.

2010-05-11

Techniques, apparatus and systems for detecting particles such as muons and neutrons. In one implementation, a particle detection system employs a plurality of drift cells, which can be for example sealed gas-filled drift tubes, arranged on sides of a volume to be scanned to track incoming and outgoing charged particles, such as cosmic ray-produced muons. The drift cells can include a neutron sensitive medium to enable concurrent counting of neutrons. The system can selectively detect devices or materials, such as iron, lead, gold, uranium, plutonium, and/or tungsten, occupying the volume from multiple scattering of the charged particles passing through the volume and can concurrently detect any unshielded neutron sources occupying the volume from neutrons emitted therefrom. If necessary, the drift cells can be used to also detect gamma rays. The system can be employed to inspect occupied vehicles at border crossings for nuclear threat objects.

Method and apparatus for testing surface characteristics of a material

NASA Technical Reports Server (NTRS)

Johnson, David L. (Inventor); Kersker, Karl D. (Inventor); Stratton, Troy C. (Inventor); Richardson, David E. (Inventor)

2006-01-01

A method, apparatus and system for testing characteristics of a material sample is provided. The system includes an apparatus configured to house the material test sample while defining a sealed volume against a surface of the material test sample. A source of pressurized fluid is in communication with, and configured to pressurize, the sealed volume. A load applying apparatus is configured to apply a defined load to the material sample while the sealed volume is monitored for leakage of the pressurized fluid. Thus, the inducement of surface defects such as microcracking and crazing may be detected and their effects analyzed for a given material. The material test samples may include laminar structures formed of, for example, carbon cloth phenolic, glass cloth phenolic, silica cloth phenolic materials or carbon-carbon materials. In one embodiment the system may be configured to analyze the material test sample while an across-ply loading is applied thereto.

Applicability of the ParaDNA(®) Screening System to Seminal Samples.

PubMed

Tribble, Nicholas D; Miller, Jamie A D; Dawnay, Nick; Duxbury, Nicola J

2015-05-01

Seminal fluid represents a common biological material recovered from sexual assault crime scenes. Such samples can be prescreened using different techniques to determine cell type and relative amount before submitting for full STR profiling. The ParaDNA(®) Screening System is a novel forensic test which identifies the presence of DNA through amplification and detection of two common STR loci (D16S539 and TH01) and the Amelogenin marker. The detection of the Y allele in samples could provide a useful tool in the triage and submission of sexual assault samples by enforcement authorities. Male template material was detected on a range of common sexual assault evidence items including cotton pillow cases, condoms, swab heads and glass surfaces and shows a detection limit of 1 in 1000 dilution of neat semen. These data indicate this technology has the potential to be a useful tool for the detection of male donor DNA in sexual assault casework. © 2015 American Academy of Forensic Sciences.

In field application of differential Die-Away time technique for detecting gram quantities of fissile materials

NASA Astrophysics Data System (ADS)

Remetti, Romolo; Gandolfo, Giada; Lepore, Luigi; Cherubini, Nadia

2017-10-01

In the frame of Chemical, Biological, Radiological, and Nuclear defense European activities, the ENEA, the Italian National Agency for New Technologies, Energy and Sustainable Economic Development, is proposing the Neutron Active Interrogation system (NAI), a device designed to find transuranic-based Radioactive Dispersal Devices hidden inside suspected packages. It is based on Differential Die-Away time Analysis, an active neutron technique targeted in revealing the presence of fissile material through detection of induced fission neutrons. Several Monte Carlo simulations, carried out by MCNPX code, and the development of ad-hoc design methods, have led to the realization of a first prototype based on a 14 MeV d-t neutron generator coupled with a tailored moderating structure, and an array of helium-3 neutron detectors. The complete system is characterized by easy transportability, light weight, and real-time response. First results have shown device's capability to detect gram quantities of fissile materials.

Simulation Of A Photofission-Based Cargo Interrogation System

DOE Office of Scientific and Technical Information (OSTI.GOV)

King, Michael; Gozani, Tsahi; Stevenson, John

A comprehensive model has been developed to characterize and optimize the detection of Bremsstrahlung x-ray induced fission signatures from nuclear materials hidden in cargo containers. An effective active interrogation system should not only induce a large number of fission events but also efficiently detect their signatures. The proposed scanning system utilizes a 9-MV commercially available linear accelerator and the detection of strong fission signals i.e. delayed gamma rays and prompt neutrons. Because the scanning system is complex and the cargo containers are large and often highly attenuating, the simulation method segments the model into several physical steps, representing each changemore » of radiation particle. Each approximation is carried-out separately, resulting in a major reduction in computational time and a significant improvement in tally statistics. The model investigates the effect on the fission rate and detection rate by various cargo types, densities and distributions. Hydrogenous and metallic cargos, homogeneous and heterogeneous, as well as various locations of the nuclear material inside the cargo container were studied. We will show that for the photofission-based interrogation system simulation, the final results are not only in good agreement with a full, single-step simulation but also with experimental results, further validating the full-system simulation.« less

System for use with solid state dosimeter

DOEpatents

Miller, Steven D.; McDonald, Joseph C.; Eichner, Fred N.; Tomeraasen, Paul L.

1990-01-01

The present invention constitutes a system for determining the amounts of ionizing radiation to which dosimeters using thermoluminescent materials have been exposed. In accordance with this system, the thermoluminescent materials which comprise the dosimeters are first cooled by contact with a cryogenic substance such as liquified nitrogen. The thermoluminescent materials are then optically stimulated by exposure to ultraviolet light. Thereafter, the amounts of visible light emitted by the thermoluminescent materials are detected and counted as the materials are allowed to warm up to room temperature. The amounts of luminescence exhibited by the materials are related to radiation exposure and provide a sensitive measure of radiation dosage. It has been discovered that the above procedure is most effective when heavily doped thermoluminescent materials are used and that the procedure allows many useful plastic materials to now be employed in dosimeter constructions.

System for use with solid state dosimeter

DOEpatents

Miller, S.D.; McDonald, J.C.; Eichner, F.N.; Tomeraasen, P.L.

1990-09-04

The present invention constitutes a system for determining the amounts of ionizing radiation to which dosimeters using thermoluminescent materials have been exposed. In accordance with this system, the thermoluminescent materials which comprise the dosimeters are first cooled by contact with a cryogenic substance such as liquefied nitrogen. The thermoluminescent materials are then optically stimulated by exposure to ultraviolet light. Thereafter, the amounts of visible light emitted by the thermoluminescent materials are detected and counted as the materials are allowed to warm up to room temperature. The amounts of luminescence exhibited by the materials are related to radiation exposure and provide a sensitive measure of radiation dosage. It has been discovered that the above procedure is most effective when heavily doped thermoluminescent materials are used and that the procedure allows many useful plastic materials to now be employed in dosimeter constructions. 3 figs.

Research on the system scheme and experiment for the active laser polarization imaging

NASA Astrophysics Data System (ADS)

Fu, Qiang; Duan, Jin; Zhao, Rui; Li, Zheng; Zhang, Su; Zhan, Juntong; Zhu, Yong; Jiang, Hui-Lin

2015-10-01

The polarization imaging detection technology increased the polarization information on the basis of the intensity imaging, which is extensive application in the military and civil and other fields. The research present and development trend of polarization imaging detection technology was introduce, the system scheme of the active polarization imaging detection was put forward, and the key technologies such as the polarization information detection, optical system design, polarization radiation calibration and image fusion approach was analyzed. On this basis, detection system by existing equipment of laboratory was set up, and on the different materials such as wood, metal, plastic and goal was detected by polarization imaging to realize the active polarization imaging detection. The results show that image contrast of the metal and man-made objects is higher, the polarization effect is better, which provided the basis on the better performance of the polarization imaging instruments.

Detection of small metal particles by a quasi-optical system at sub-millimeter wavelength

NASA Astrophysics Data System (ADS)

Kitahara, Yasuyuki; Domier, C. W.; Ikeda, Makoto; Pham, Anh-Vu; Luhmann, Neville C.

2016-04-01

Inspection of alien metal particles in electronic materials such as glass fibers and resins is a critical issue to control the quality and guarantee the safety of products. In this paper, we present a new detection technique using sub-millimeter wave for films as electric materials in product lines. The advantage of using sub-millimeter wave frequency is that it is easy to distinguish conductive particles from a nonconductive material such as plastic films. Scattering of a submillimeter wave by a metal particle is used as the detection principle. By simulation, it is observed that the scattering pattern varies intricately as the diameter varies from 10 to 700 μm at 300 GHz. The demonstration system is composed of a Keysight performance network analyzer (N5247A PNA-X) with 150-330 GHz VDI extension modules, transmitting and receiving antennas, and focusing dielectric lens. An output signal is radiated via an antenna and focused onto a metal particle on a film. The wave scattered by the metal particle is detected by an identical antenna through a lens. The signal scattered from a metal particle is evaluated from the insertion loss between antennas (S21). The result shows that a particle of diameter 300 μm is detectable at 150-330 GHz through S21 in the experimental system that we prepared. Peaks calculated in simulation were detected in experimental data as well as in the curves of the particle diameter versus S21. It was shown that using this peak frequency could improve S21 level without higher frequency.

A novel cell line generated using the CRISPR/Cas9 technology as universal quality control material for KRAS G12V mutation testing.

PubMed

Jia, Shiyu; Zhang, Rui; Lin, Guigao; Peng, Rongxue; Gao, Peng; Han, Yanxi; Fu, Yu; Ding, Jiansheng; Wu, Qisheng; Zhang, Kuo; Xie, Jiehong; Li, Jinming

2018-06-01

KRAS mutations are the key indicator for EGFR monoclonal antibody-targeted therapy and acquired drug resistance, and their accurate detection is critical to the clinical decision-making of colorectal cancer. However, no proper quality control material is available for the current detection methods, particularly next-generation sequencing (NGS). The ideal quality control material for NGS needs to provide both the tumor mutation gene and the matched background genomic DNA, which is uncataloged in public databases, to accurately distinguish germline polymorphisms and somatic mutations. We developed a novel KRAS G12V mutant cell line using the clustered regularly interspaced short palindromic repeat (CRISPR)/CRISPR-associated protein 9 (Cas9) technique to make up for the deficiencies in existing quality control material and further validated the feasibility of the cell line as quality control material by amplification refractory mutation system (ARMS), Sanger sequencing, digital PCR (dPCR), and NGS. We verified that the edited cell line specifically had the G12V mutation, and the validation results presented a high consistency among the four methods of detection. The three cell lines screened contained the G12V mutation and the mutation allele fractions of G12V-1, G12V-2, and G12V-3 were 52.01%, 82.06%, and 17.29%, respectively. The novel KRAS G12V cell line generated using the CRISPR/Cas9 gene editing system is suitable as a quality control material for all current detection methods and provides a new direction in the development of quality control material. © 2018 Wiley Periodicals, Inc.

Detection and traceability of genetically modified organisms in the food production chain.

PubMed

Miraglia, M; Berdal, K G; Brera, C; Corbisier, P; Holst-Jensen, A; Kok, E J; Marvin, H J P; Schimmel, H; Rentsch, J; van Rie, J P P F; Zagon, J

2004-07-01

Both labelling and traceability of genetically modified organisms are current issues that are considered in trade and regulation. Currently, labelling of genetically modified foods containing detectable transgenic material is required by EU legislation. A proposed package of legislation would extend this labelling to foods without any traces of transgenics. These new legislations would also impose labelling and a traceability system based on documentation throughout the food and feed manufacture system. The regulatory issues of risk analysis and labelling are currently harmonised by Codex Alimentarius. The implementation and maintenance of the regulations necessitates sampling protocols and analytical methodologies that allow for accurate determination of the content of genetically modified organisms within a food and feed sample. Current methodologies for the analysis of genetically modified organisms are focused on either one of two targets, the transgenic DNA inserted- or the novel protein(s) expressed- in a genetically modified product. For most DNA-based detection methods, the polymerase chain reaction is employed. Items that need consideration in the use of DNA-based detection methods include the specificity, sensitivity, matrix effects, internal reference DNA, availability of external reference materials, hemizygosity versus homozygosity, extrachromosomal DNA, and international harmonisation. For most protein-based methods, enzyme-linked immunosorbent assays with antibodies binding the novel protein are employed. Consideration should be given to the selection of the antigen bound by the antibody, accuracy, validation, and matrix effects. Currently, validation of detection methods for analysis of genetically modified organisms is taking place. In addition, new methodologies are developed, including the use of microarrays, mass spectrometry, and surface plasmon resonance. Challenges for GMO detection include the detection of transgenic material in materials with varying chromosome numbers. The existing and proposed regulatory EU requirements for traceability of genetically modified products fit within a broader tendency towards traceability of foods in general and, commercially, towards products that can be distinguished from each other. Traceability systems document the history of a product and may serve the purpose of both marketing and health protection. In this framework, segregation and identity preservation systems allow for the separation of genetically modified and non-modified products from "farm to fork". Implementation of these systems comes with specific technical requirements for each particular step of the food processing chain. In addition, the feasibility of traceability systems depends on a number of factors, including unique identifiers for each genetically modified product, detection methods, permissible levels of contamination, and financial costs. In conclusion, progress has been achieved in the field of sampling, detection, and traceability of genetically modified products, while some issues remain to be solved. For success, much will depend on the threshold level for adventitious contamination set by legislation. Copryright 2004 Elsevier Ltd.

Enhanced optical coupling and Raman scattering via microscopic interface engineering

NASA Astrophysics Data System (ADS)

Thompson, Jonathan V.; Hokr, Brett H.; Kim, Wihan; Ballmann, Charles W.; Applegate, Brian E.; Jo, Javier A.; Yamilov, Alexey; Cao, Hui; Scully, Marlan O.; Yakovlev, Vladislav V.

2017-11-01

Spontaneous Raman scattering is an extremely powerful tool for the remote detection and identification of various chemical materials. However, when those materials are contained within strongly scattering or turbid media, as is the case in many biological and security related systems, the sensitivity and range of Raman signal generation and detection is severely limited. Here, we demonstrate that through microscopic engineering of the optical interface, the optical coupling of light into a turbid material can be substantially enhanced. This improved coupling facilitates the enhancement of the Raman scattering signal generated by molecules within the medium. In particular, we detect at least two-orders of magnitude more spontaneous Raman scattering from a sample when the pump laser light is focused into a microscopic hole in the surface of the sample. Because this approach enhances both the interaction time and interaction region of the laser light within the material, its use will greatly improve the range and sensitivity of many spectroscopic techniques, including Raman scattering and fluorescence emission detection, inside highly scattering environments.

Colorimetric detection of uranium in water

DOEpatents

DeVol, Timothy A [Clemson, SC; Hixon, Amy E [Piedmont, SC; DiPrete, David P [Evans, GA

2012-03-13

Disclosed are methods, materials and systems that can be used to determine qualitatively or quantitatively the level of uranium contamination in water samples. Beneficially, disclosed systems are relatively simple and cost-effective. For example, disclosed systems can be utilized by consumers having little or no training in chemical analysis techniques. Methods generally include a concentration step and a complexation step. Uranium concentration can be carried out according to an extraction chromatographic process and complexation can chemically bind uranium with a detectable substance such that the formed substance is visually detectable. Methods can detect uranium contamination down to levels even below the MCL as established by the EPA.

High throughput liquid absorption preconcentrator sampling instrument

DOEpatents

Zaromb, Solomon; Bozen, Ralph M.

1992-01-01

A system for detecting trace concentrations of an analyte in air includes a preconcentrator for the analyte and an analyte detector. The preconcentrator includes an elongated tubular container comprising a wettable material. The wettable material is continuously wetted with an analyte-sorbing liquid which flows from one part of the container to a lower end. Sampled air flows through the container in contact with the wetted material with a swirling motion which results in efficient transfer of analyte vapors or aerosol particles to the sorbing liquid and preconcentration of traces of analyte in the liquid. The preconcentrated traces of analyte may be either detected within the container or removed therefrom for injection into a separate detection means or for subsequent analysis.

High-throughput liquid-absorption preconcentrator sampling methods

DOEpatents

Zaromb, Solomon

1994-01-01

A system for detecting trace concentrations of an analyte in air includes a preconcentrator for the analyte and an analyte detector. The preconcentrator includes an elongated tubular container comprising a wettable material. The wettable material is continuously wetted with an analyte-sorbing liquid which flows from one part of the container to a lower end. Sampled air flows through the container in contact with the wetted material with a swirling motion which results in efficient transfer of analyte vapors or aerosol particles to the sorbing liquid and preconcentration of traces of analyte in the liquid. The preconcentrated traces of analyte may be either detected within the container or removed therefrom for injection into a separate detection means or for subsequent analysis.

High throughput liquid absorption preconcentrator sampling instrument

DOEpatents

Zaromb, S.; Bozen, R.M.

1992-12-22

A system for detecting trace concentrations of an analyte in air includes a preconcentrator for the analyte and an analyte detector. The preconcentrator includes an elongated tubular container comprising a wettable material. The wettable material is continuously wetted with an analyte-sorbing liquid which flows from one part of the container to a lower end. Sampled air flows through the container in contact with the wetted material with a swirling motion which results in efficient transfer of analyte vapors or aerosol particles to the sorbing liquid and preconcentration of traces of analyte in the liquid. The preconcentrated traces of analyte may be either detected within the container or removed therefrom for injection into a separate detection means or for subsequent analysis. 12 figs.

High-throughput liquid-absorption preconcentrator sampling methods

DOEpatents

Zaromb, S.

1994-07-12

A system for detecting trace concentrations of an analyte in air includes a preconcentrator for the analyte and an analyte detector. The preconcentrator includes an elongated tubular container comprising a wettable material. The wettable material is continuously wetted with an analyte-sorbing liquid which flows from one part of the container to a lower end. Sampled air flows through the container in contact with the wetted material with a swirling motion which results in efficient transfer of analyte vapors or aerosol particles to the sorbing liquid and preconcentration of traces of analyte in the liquid. The preconcentrated traces of analyte may be either detected within the container or removed therefrom for injection into a separate detection means or for subsequent analysis. 12 figs.

Systems for detecting charged particles in object inspection

DOEpatents

Morris, Christopher L.; Makela, Mark F.

2013-08-20

Techniques, apparatus and systems for detecting particles such as muons. In one implementation, a monitoring system has a cosmic ray-produced charged particle tracker with a plurality of drift cells. The drift cells, which can be for example aluminum drift tubes, can be arranged at least above and below a volume to be scanned to thereby track incoming and outgoing charged particles, such as cosmic ray-produced muons, while also detecting gamma rays. The system can selectively detect devices or materials, such as iron, lead, gold and/or tungsten, occupying the volume from multiple scattering of the charged particles passing through the volume and can also detect any radioactive sources occupying the volume from gamma rays emitted therefrom. If necessary, the drift tubes can be sealed to eliminate the need for a gas handling system. The system can be employed to inspect occupied vehicles at border crossings for nuclear threat objects.

Optical Detection Of Cryogenic Leaks

NASA Technical Reports Server (NTRS)

Wyett, Lynn M.

1988-01-01

Conceptual system identifies leakage without requiring shutdown for testing. Proposed device detects and indicates leaks of cryogenic liquids automatically. Detector makes it unnecessary to shut equipment down so it can be checked for leakage by soap-bubble or helium-detection methods. Not necessary to mix special gases or other materials with cryogenic liquid flowing through equipment.

Turnitoff: Identifying and Fixing a Hole in Current Plagiarism Detection Software

ERIC Educational Resources Information Center

Heather, James

2010-01-01

In recent times, "plagiarism detection software" has become popular in universities and colleges, in an attempt to stem the tide of plagiarised student coursework. Such software attempts to detect any copied material and identify its source. The most popular such software is Turnitin, a commercial system used by thousands of institutions…

Nucleic acid-coupled colorimetric analyte detectors

DOEpatents

Charych, Deborah H.; Jonas, Ulrich

2001-01-01

The present invention relates to methods and compositions for the direct detection of analytes and membrane conformational changes through the detection of color changes in biopolymeric materials. In particular, the present invention provide for the direct colorimetric detection of analytes using nucleic acid ligands at surfaces of polydiacetylene liposomes and related molecular layer systems.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Achey, R.; Rivera, O.; Wellons, M.

Microporous zeolite adsorbent materials are widely used as a medium for separating gases. Adsorbent gas separation systems can run at ambient temperature and require minimal pressure to flow the input gas stream across the adsorbent bed. This allows for low energy consumption relative to other types of separation systems. Specific zeolites also have a high capacity and selectivity for the gases of interest, leading to compact and efficient separation systems. These characteristics are particularly advantageous for the application of signatures detection for non-proliferation, which often requires portable systems with low power draw. Savannah River National Laboratory currently is the leadermore » in using zeolites for noble gas sampling for non-proliferation detection platforms. However, there is a constant customer need for improved sampling capabilities. Development of improved zeolite materials will lead to improved sampling technology. Microwave-assisted and conventional hydrothermal synthesis have been used to make a variety of zeolites tailored for noble gas separation. Materials characterization data collected in this project has been used to help guide the synthesis of improved zeolite materials. Candidate materials have been down-selected based on highest available surface area, maximum overall capacity for gas adsorption and highest selectivity. The creation of improved adsorbent materials initiated in this project will lead to development of more compact, efficient and effective noble gas collectors and concentrators. The work performed in this project will be used as a foundation for funding proposals for further material development as well as possible industrial applications.« less

Impact source localisation in aerospace composite structures

NASA Astrophysics Data System (ADS)

De Simone, Mario Emanuele; Ciampa, Francesco; Boccardi, Salvatore; Meo, Michele

2017-12-01

The most commonly encountered type of damage in aircraft composite structures is caused by low-velocity impacts due to foreign objects such as hail stones, tool drops and bird strikes. Often these events can cause severe internal material damage that is difficult to detect and may lead to a significant reduction of the structure’s strength and fatigue life. For this reason there is an urgent need to develop structural health monitoring systems able to localise low-velocity impacts in both metallic and composite components as they occur. This article proposes a novel monitoring system for impact localisation in aluminium and composite structures, which is able to determine the impact location in real-time without a-priori knowledge of the mechanical properties of the material. This method relies on an optimal configuration of receiving sensors, which allows linearization of well-known nonlinear systems of equations for the estimation of the impact location. The proposed algorithm is based on the time of arrival identification of the elastic waves generated by the impact source using the Akaike Information Criterion. The proposed approach was demonstrated successfully on both isotropic and orthotropic materials by using a network of closely spaced surface-bonded piezoelectric transducers. The results obtained show the validity of the proposed algorithm, since the impact sources were detected with a high level of accuracy. The proposed impact detection system overcomes current limitations of other methods and can be retrofitted easily on existing aerospace structures allowing timely detection of an impact event.

Combined, solid-state molecular property and gamma spectrometers for CBRNE detection

NASA Astrophysics Data System (ADS)

Rogers, Ben; Grate, Jay; Pearson, Brett; Gallagher, Neal; Wise, Barry; Whitten, Ralph; Adams, Jesse

2013-05-01

Nevada Nanotech Systems, Inc. (Nevada Nano) has developed a multi-sensor solution to Chemical, Biological, Radiological, Nuclear and Explosives (CBRNE) detection that combines the Molecular Property Spectrometer™ (MPS™)—a micro-electro-mechanical chip-based technology capable of measuring a variety of thermodynamic and electrostatic molecular properties of sampled vapors and particles—and a compact, high-resolution, solid-state gamma spectrometer module for identifying radioactive materials, including isotopes used in dirty bombs and nuclear weapons. By conducting multiple measurements, the system can provide a more complete characterization of an unknown sample, leading to a more accurate identification. Positive identifications of threats are communicated using an integrated wireless module. Currently, system development is focused on detection of commercial, military and improvised explosives, radioactive materials, and chemical threats. The system can be configured for a variety of CBRNE applications, including handheld wands and swab-type threat detectors requiring short sample times, and ultra-high sensitivity detectors in which longer sampling times are used. Here we provide an overview of the system design and operation and present results from preliminary testing.

Thermal Infrared Spectral Band Detection Limits for Unidentified Surface Materials

NASA Technical Reports Server (NTRS)

Kirkland, Laurel E.; Herr, Kenneth C.; Salisbury, John W.

2001-01-01

Infrared emission spectra recorded by airborne or satellite spectrometers can be searched for spectral features to determine the composition of rocks on planetary surfaces. Surface materials are identified by detections of characteristic spectral bands. We show how to define whether to accept an observed spectral feature as a detection when the target material is unknown. We also use remotely sensed spectra measured by the Thermal Emission Spectrometer (TES) and the Spatially Enhanced Broadband Array Spectrograph System to illustrate the importance of instrument parameters and surface properties on band detection limits and how the variation in signal-to-noise ratio with wavelength affects the bands that are most detectable for a given instrument. The spectrometer's sampling interval, spectral resolution, signal-to-noise ratio as a function of wavelength, and the sample's surface properties influence whether the instrument can detect a spectral feature exhibited by a material. As an example, in the 6-13 micrometer wavelength region, massive carbonates exhibit two bands: a very strong, broad feature at approximately 6.5 micrometers and a less intense, sharper band at approximately 11.25 micrometers. Although the 6.5-micrometer band is stronger and broader in laboratory-measured spectra, the 11.25-micrometer band will cause a more detectable feature in TES spectra.

Method and system for determining depth distribution of radiation-emitting material located in a source medium and radiation detector system for use therein

DOEpatents

Benke, Roland R.; Kearfott, Kimberlee J.; McGregor, Douglas S.

2003-03-04

A method, system and a radiation detector system for use therein are provided for determining the depth distribution of radiation-emitting material distributed in a source medium, such as a contaminated field, without the need to take samples, such as extensive soil samples, to determine the depth distribution. The system includes a portable detector assembly with an x-ray or gamma-ray detector having a detector axis for detecting the emitted radiation. The radiation may be naturally-emitted by the material, such as gamma-ray-emitting radionuclides, or emitted when the material is struck by other radiation. The assembly also includes a hollow collimator in which the detector is positioned. The collimator causes the emitted radiation to bend toward the detector as rays parallel to the detector axis of the detector. The collimator may be a hollow cylinder positioned so that its central axis is perpendicular to the upper surface of the large area source when positioned thereon. The collimator allows the detector to angularly sample the emitted radiation over many ranges of polar angles. This is done by forming the collimator as a single adjustable collimator or a set of collimator pieces having various possible configurations when connected together. In any one configuration, the collimator allows the detector to detect only the radiation emitted from a selected range of polar angles measured from the detector axis. Adjustment of the collimator or the detector therein enables the detector to detect radiation emitted from a different range of polar angles. The system further includes a signal processor for processing the signals from the detector wherein signals obtained from different ranges of polar angles are processed together to obtain a reconstruction of the radiation-emitting material as a function of depth, assuming, but not limited to, a spatially-uniform depth distribution of the material within each layer. The detector system includes detectors having different properties (sensitivity, energy resolution) which are combined so that excellent spectral information may be obtained along with good determinations of the radiation field as a function of position.

Tagged Neutron Source for API Inspection Systems with Greatly Enhanced Spatial Resolution

DOE Office of Scientific and Technical Information (OSTI.GOV)

None

2012-06-04

We recently developed induced fission and transmission imaging methods with time- and directionally-tagged neutrons offer new capabilities for characterization of fissile material configurations and enhanced detection of special nuclear materials (SNM). An Advanced Associated Particle Imaging (API) generator with higher angular resolution and neutron yield than existing systems is needed to fully exploit these methods.

On-line, continuous monitoring in solar cell and fuel cell manufacturing using spectral reflectance imaging

DOEpatents

Sopori, Bhushan; Rupnowski, Przemyslaw; Ulsh, Michael

2016-01-12

A monitoring system 100 comprising a material transport system 104 providing for the transportation of a substantially planar material 102, 107 through the monitoring zone 103 of the monitoring system 100. The system 100 also includes a line camera 106 positioned to obtain multiple line images across a width of the material 102, 107 as it is transported through the monitoring zone 103. The system 100 further includes an illumination source 108 providing for the illumination of the material 102, 107 transported through the monitoring zone 103 such that light reflected in a direction normal to the substantially planar surface of the material 102, 107 is detected by the line camera 106. A data processing system 110 is also provided in digital communication with the line camera 106. The data processing system 110 is configured to receive data output from the line camera 106 and further configured to calculate and provide substantially contemporaneous information relating to a quality parameter of the material 102, 107. Also disclosed are methods of monitoring a quality parameter of a material.

Remote detection of stress corrosion cracking: Surface composition and crack detection

NASA Astrophysics Data System (ADS)

Lissenden, Cliff J.; Jovanovic, Igor; Motta, Arthur T.; Xiao, Xuan; Le Berre, Samuel; Fobar, David; Cho, Hwanjeong; Choi, Sungho

2018-04-01

Chloride induced stress corrosion cracking (SCC) of austenitic stainless steel is a potential issue in long term dry storage of spent nuclear fuel canisters. In order for SCC to occur there must be a corrosive environment, a susceptible material, and a driving force. Because it is likely that the material in the heat affected zone (HAZ) of welded stainless steel structures has been sensitized as a result of chromium depletion at the grain boundaries and a thermal residual stress driving force is likely present if solution annealing is not performed, two issues are critical. Is the environment corrosive, i.e., are chlorides present in solution on the surface? And then, are there cracks that could propagate? Remote detection of chlorides on the surface can be accomplished by laser induced breakdown spectroscopy (LIBS), while cracks can be detected by shear horizontal guided waves generated by electromagnetic acoustic transducers (EMATs). Both are noncontact methods that are amenable to robotic delivery systems and harsh environments. The sensitivity to chlorine on stainless steel of a LIBS system that employs optical fiber for pulse delivery is demonstrated. Likewise, the ability of the EMAT system to detect cracks of a prescribed size and orientation is shown. These results show the potential for remote detection of Cl and cracks in dry storage spent fuel canisters.

Encapsulated microenergetic material

DOEpatents

Roberts, Jeffery James; Aines, Roger D.; Duoss, Eric B.; Spadaccini, Christopher M.; Vandersall, Kevin S.

2018-02-20

Providing high energy materials that can be placed in previously created fractures and activating them in place to extend or change an existing fracture system. Also detecting the location of fractures or permeable pathways and a means to assess the extent and efficiency of proppant emplacement.

Encapsulated microenergetic material

DOEpatents

Roberts, Jeffery James; Aines, Roger D.; Duoss, Eric B.; Spadaccini, Christopher M.; Vandersall, Kevin S.

2017-02-07

Providing high energy materials that can be placed in previously created fractures and activating them in place to extend or change an existing fracture system. Also detecting the location of fractures or permeable pathways and a means to assess the extent and efficiency of proppant emplacement.

Antimicrobial Materials for Advanced Microbial Control in Spacecraft Water Systems

NASA Technical Reports Server (NTRS)

Birmele, Michele; Caro, Janicce; Newsham, Gerard; Roberts, Michael; Morford, Megan; Wheeler, Ray

2012-01-01

Microbial detection, identification, and control are essential for the maintenance and preservation of spacecraft water systems. Requirements set by NASA put limitations on the energy, mass, materials, noise, cost, and crew time that can be devoted to microbial control. Efforts are being made to attain real-time detection and identification of microbial contamination in microgravity environments. Research for evaluating technologies for capability enhancement on-orbit is currently focused on the use of adenosine triphosphate (ATP) analysis for detection purposes and polymerase chain reaction (peR) for microbial identification. Additional research is being conducted on how to control for microbial contamination on a continual basis. Existing microbial control methods in spacecraft utilize iodine or ionic silver biocides, physical disinfection, and point-of-use sterilization filters. Although these methods are effective, they require re-dosing due to loss of efficacy, have low human toxicity thresholds, produce poor taste, and consume valuable mass and crew time. Thus, alternative methods for microbial control are needed. This project also explores ultraviolet light-emitting diodes (UV-LEDs), surface passivation methods for maintaining residual biocide levels, and several antimicrobial materials aimed at improving current microbial control techniques, as well as addressing other materials presently under analysis and future directions to be pursued.

Optochemical sensor based on screenprinted fluorescent sensorspots surrounded by organic photodiodes for multianalyte detection

NASA Astrophysics Data System (ADS)

Kraker, E.; Lamprecht, B.; Haase, A.; Jakopic, G.; Abel, T.; Konrad, C.; Köstler, S.; Tscherner, M.; Stadlober, B.; Mayr, T.

2010-08-01

A compact, integrated photoluminescence based oxygen sensor, utilizing an organic light emitting device (OLED) as the light source and an organic photodiode (OPD) as the detection unit, is described. The detection system of the sensor array consists of an array of circular screen-printed fluorescent sensor spots surrounded by organic photodiodes as integrated fluorescence detectors. The OPD originates from the well-known Tang photodiode, consisting of a stacked layer of copper phthalocyanine (CuPc, p-type material) and perylene tetracarboxylic bisbenzimidazole (PTCBi, n-type material). An additional layer of tris-8-hydroxyquinolinatoaluminium (Alq3, n-type material) was inserted between the PTCBi layer and cathode. An ORMOCERR layer was used as encapsulation layer. For excitation an organic light emitting diode is used. The sensor spot and the detector are processed on the same flexible substrate. This approach not only simplifies the detection system by minimizing the numbers of required optical components - no optical filters have to be used for separating the excitation light and the luminescent emission-, but also has a large potential for low-cost sensor applications. The feasibility of the concept is demonstrated by an integrated oxygen sensor, indicating good performance. Sensor schemes for other chemical parameters are proposed.

Evaluation of detection and response times of fire sensors using an atmospheric monitoring system

PubMed Central

Rowland, J.H.; Litton, C.D.; Thomas, R.A.

2017-01-01

Atmospheric monitoring systems (AMS) are required when using air from conveyor belt entries to ventilate working sections in U.S. underground coal mines. AMS technology has the potential to increase fire safety mine-wide, but research is needed to determine the detection and response times for fires of a variety of combustible materials. To evaluate the potential of an AMS for fire detection in other areas of a coal mine, a series of full-scale fire experiments were conducted to determine detection and response times from fires of different combustible materials that are found in U.S. underground coal mines, including high- and low-volatility coals, conveyor belts, brattice materials, different types of wood, diesel fuel, and a foam sealant. These experiments were conducted in the Safety Research Coal Mine (SRCM) of the U.S. National Institute for Occupational Safety and Health (NIOSH) located in Pittsburgh, PA, using a commercially available AMS that is typical of current technology. The results showed that through proper selection of sensors and their locations, a mine-wide AMS can provide sufficient early fire warning times and improve the health and safety of miners. PMID:28529442

Evaluation of detection and response times of fire sensors using an atmospheric monitoring system.

PubMed

Rowland, J H; Litton, C D; Thomas, R A

2016-01-01

Atmospheric monitoring systems (AMS) are required when using air from conveyor belt entries to ventilate working sections in U.S. underground coal mines. AMS technology has the potential to increase fire safety mine-wide, but research is needed to determine the detection and response times for fires of a variety of combustible materials. To evaluate the potential of an AMS for fire detection in other areas of a coal mine, a series of full-scale fire experiments were conducted to determine detection and response times from fires of different combustible materials that are found in U.S. underground coal mines, including high- and low-volatility coals, conveyor belts, brattice materials, different types of wood, diesel fuel, and a foam sealant. These experiments were conducted in the Safety Research Coal Mine (SRCM) of the U.S. National Institute for Occupational Safety and Health (NIOSH) located in Pittsburgh, PA, using a commercially available AMS that is typical of current technology. The results showed that through proper selection of sensors and their locations, a mine-wide AMS can provide sufficient early fire warning times and improve the health and safety of miners.

Final Report on the Detection of Green Monopropellants

NASA Technical Reports Server (NTRS)

Gibson, Tracy L.; DeVor, Robert W.; Bauer, Brint M.; Captain, James; Coutts, Janelle L.; Surma, Jan M.

2015-01-01

In 2014, National Aeronautics and Space Administration (NASA) Kennedy Space Center (KSC) funded a project titled "Familiarization and Detection of Green Monopropellants" utilizing Independent Research and Technology Development (IR&TD) and Center Innovation Fund (CIF) funding. The purpose of the project was to evaluate methods of detection for ammonium dinitramide (ADN) and hydroxylammonium nitrate (HAN). An Engineering Services Contract (ESC) task order was created with the scope of evaluation of several methods of detecting ADN- and HAN-based propellants, as well as development of methods for detection. Detection methods include developed methods such as colorimetric indicating absorbent socks, and commercial-off-the- shelf (COTS) units for ammonia detection. An additional goal of the task order was for ESC to become familiar with ADN's and HAN's material properties and material compatibility. Two approaches were initially investigated as possible methods for the detection of HAN (or AFM315E) and ADN (or LMP-103S). These approaches were colorimetric analysis and instrumentation-based COTS vapor sensors utilization. Initial testing showed that the relatively non-existent vapor pressure of the AF-M315E (of which HAN is a major component) propellant would make the use of COTS sensors difficult for real-time area monitoring of HAN; a small response was detected through the use of active COTS sensors, including the RAE Systems MultiRAE Lite and Drager X-act (registered) 5000, but the levels detected were below the threshold limit value for the toxic gas ammonia. Therefore, a detection system ased upon a colorimetric indicator impregnated into an absorbent material was developed. Preliminary analysis (ESC-245-FDG-001) identified a particularly outstanding candidate as a colorimetric indicator for the detection of the presence of AF-M315E in the form of a Methyl Red (Basic) indicator. Materials impregnated with this indicator exhibit significant color change and the materials are not susceptible to interference from exposure to water or carbon dioxide. The completed detection system for HAN/AF-M315E consists of absorbent socks packed with Fisher Universal Spill Absorbent capable of absorbing and containing any propellant spills that they come into contact with along with indicating wipes. The absorbent socks are also chemically treated with a Methyl Red (Basic) indicator solution to provide the end user with a visual indication that a leak has occurred and proper protective precautions must be undertaken. An added benefit of this detection system is that the absorbent socks should neutralize/absorb any commodity that it comes into contact with (until saturation is reached). Additional adsorbent socks can be deployed until a color change is not seen, indicating that the HAN/AF-M315E contamination has been contained. The indicating wipes provide the user the opportunity to wipe surfaces to determine if there is any HAN/AF-M315E or HAN/AFM315E residue present. The wipes should allow the detection of fuel levels that may be too small to detect with the absorbent socks. The development of a detection system for the ADN/LMP-103S focused on the use of various COTS sensors used as real-time area monitoring devices and personal dosimeters. These COTS based sensor systems were of several different types, including both actively pumped and diffusion-based passive systems, as well as a "rope"-type chemical sensing cable. The results highlighted some of the major differences between the two monopropellants undergoing evaluation. Unlike HAN, ADN (which is the major constituent of LMP-103S) exhibits a much more volatile nature in comparison to AF-M315E. In fact, testing showed that a large percentage of the fuel was lost during the sampling measurement (greater than 10 percent by mass); although this testing cannot tell if the volatile component is the ADN itself or another component of the monopropellant solution. Not surprisingly, all four of the procured vapor-based COTS sensors showed positive results when exposed to solutions of the LMP-103S (ESC-245-FDG-002). The completed detection system for ADN/LMP-103S consists of a combination of two of the tested COTS sensor systems, the RAE Systems MultiRAE Lite and the BW Technologies GasAlert Extreme. These systems are meant to be used in conjunction with one another, which allows for the end-user to have both real-time area monitoring (MultiRAE Lite) as well as a personal dosimeter device (GasAlert Extreme) which can be worn as additional personal protective equipment. An stainless steel extension wand was fabricated and included in the detection system for the MultiRAE Lite to allow for more remote sensing, and connects via the active pumping inlet of the sensor. As stated, the final results of this testing resulted in the production of two "kits" which can be used for the detection of HAN/AF-M315E and ADN/LMP-103s (ESC-245-FDG-003).

Fabrication and testing of a standoff trace explosives detection system

NASA Astrophysics Data System (ADS)

Waterbury, Robert; Rose, Jeremy; Vunck, Darius; Blank, Thomas; Pohl, Ken; Ford, Alan; McVay, Troy; Dottery, Ed

2011-05-01

In order to stop the transportation of materials used for IED manufacture, a standoff checkpoint explosives detection system (CPEDS) has recently been fabricated. The system incorporates multi-wavelength Raman spectroscopy and laser induced breakdown spectroscopy (LIBS) modalities with a LIBS enhancement technique called TEPS to be added later into a single unit for trace detection of explosives at military checkpoints. Newly developed spectrometers and other required sensors all integrated with a custom graphical user interface for producing simplified, real-time detection results are also included in the system. All equipment is housed in a military ruggedized shelter for potential deployment intheater for signature collection. Laboratory and performance data, as well as the construction of the CPEDS system and its potential deployment capabilities, will be presented in the current work.

Fluid leak indicator

NASA Technical Reports Server (NTRS)

Anderson, G. E.; Loo, S. (Inventor)

1985-01-01

A fluid leak indicator for detecting and indicating leaks in visually inaccessible fluid tubing joints, such as those obstructed by insulation includes a bag system and a wicking system surrounding or wrapping the joints under the visual obstructing material. Leaking fluid is collected in the bag or on the wicking material where it is conducted along the wicking material to a visily accessible capturing transparent indicator bulb for providing a visual indication of the leak without requiring a chemical change in the capturing indicator bulb.

Active detection of shielded SNM with 60-keV neutrons

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hagmann, C; Dietrich, D; Hall, J

2008-07-08

Fissile materials, e.g. {sup 235}U and {sup 239}Pu, can be detected non-invasively by active neutron interrogation. A unique characteristic of fissile material exposed to neutrons is the prompt emission of high-energy (fast) fission neutrons. One promising mode of operation subjects the object to a beam of medium-energy (epithermal) neutrons, generated by a proton beam impinging on a Li target. The emergence of fast secondary neutrons then clearly indicates the presence of fissile material. Our interrogation system comprises a low-dose 60-keV neutron generator (5 x 10{sup 6}/s), and a 1 m{sup 2} array of scintillators for fast neutron detection. Preliminary experimentalmore » results demonstrate the detectability of small quantities (370 g) of HEU shielded by steel (200 g/cm{sup 2}) or plywood (30 g/cm{sup 2}), with a typical measurement time of 1 min.« less

DOD Financial Management: The Defense Finance and Accounting Service Needs to Fully Implement Financial Improvements for Contract Pay

DTIC Science & Technology

2014-06-01

effectiveness of controls that would prevent, or detect and correct, potential misstatements in the financial statements. cMisstatements are the result...reporting. For example, a system edit used to prevent or detect a duplicate entry is an application control. gA material weakness is a deficiency, or...combination of deficiencies, in internal control, such that there is a reasonable possibility that a material misstatement of the entity’s financial

DEVELOPMENT OF DECISION MAKING ALGORITHM FOR CONTROL OF SEA CARGO CONTAINERS BY 'TAGGED' NEUTRON METHOD

DOE Office of Scientific and Technical Information (OSTI.GOV)

Anan'ev, A. A.; Belichenko, S. G.; Bogolyubov, E. P.

Nowadays in Russia and abroad there are several groups of scientists, engaged in development of systems based on 'tagged' neutron method (API method) and intended for detection of dangerous materials, including high explosives (HE). Particular attention is paid to possibility of detection of dangerous objects inside a sea cargo container. Energy gamma-spectrum, registered from object under inspection is used for determination of oxygen/carbon and nitrogen/carbon chemical ratios, according to which dangerous object is distinguished from not dangerous one. Material of filled container, however, gives rise to additional effects of rescattering and moderation of 14 MeV primary neutrons of generator, attenuationmore » of secondary gamma-radiation from reactions of inelastic neutron scattering on objects under inspection. These effects lead to distortion of energy gamma-response from examined object and therefore prevent correct recognition of chemical ratios. These difficulties are taken into account in analytical method, presented in the paper. Method has been validated against experimental data, obtained by the system for HE detection in sea cargo, based on API method and developed in VNIIA. Influence of shielding materials on results of HE detection and identification is considered. Wood and iron were used as shielding materials. Results of method application for analysis of experimental data on HE simulator measurement (tetryl, trotyl, hexogen) are presented.« less

Study of gamma detection capabilities of the REWARD mobile spectroscopic system

NASA Astrophysics Data System (ADS)

Balbuena, J. P.; Baptista, M.; Barros, S.; Dambacher, M.; Disch, C.; Fiederle, M.; Kuehn, S.; Parzefall, U.

2017-07-01

REWARD is a novel mobile spectroscopic radiation detector system for Homeland Security applications. The system integrates gamma and neutron detection equipped with wireless communication. A comprehensive simulation study on its gamma detection capabilities in different radioactive scenarios is presented in this work. The gamma detection unit consists of a precise energy resolution system based on two stacked (Cd,Zn)Te sensors working in coincidence sum mode. The volume of each of these CZT sensors is 1 cm3. The investigated energy windows used to determine the detection capabilities of the detector correspond to the gamma emissions from 137Cs and 60Co radioactive sources (662 keV and 1173/1333 keV respectively). Monte Carlo and Technology Computer-Aided Design (TCAD) simulations are combined to determine its sensing capabilities for different radiation sources and estimate the limits of detection of the sensing unit as a function of source activity for several shielding materials.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Samanta, C.; Yasasvi Gangavarapu, P. R.; Naik, A. K.

Atomically thin two dimensional (2D) layered materials have emerged as a new class of material for nanoelectromechanical systems (NEMS) due to their extraordinary mechanical properties and ultralow mass density. Among them, graphene has been the material of choice for nanomechanical resonator. However, recent interest in 2D chalcogenide compounds has also spurred research in using materials such as MoS{sub 2} for the NEMS applications. As the dimensions of devices fabricated using these materials shrink down to atomically thin membrane, strain and nonlinear effects have become important. A clear understanding of the nonlinear effects and the ability to manipulate them is essentialmore » for next generation sensors. Here, we report on all electrical actuation and detection of few-layer MoS{sub 2} resonator. The ability to electrically detect multiple modes and actuate the modes deep into the nonlinear regime enables us to probe the nonlinear coupling between various vibrational modes. The modal coupling in our device is strong enough to detect three distinct internal resonances.« less

Experimental demonstration of multiple monoenergetic gamma radiography for effective atomic number identification in cargo inspection

NASA Astrophysics Data System (ADS)

Henderson, Brian S.; Lee, Hin Y.; MacDonald, Thomas D.; Nelson, Roberts G.; Danagoulian, Areg

2018-04-01

The smuggling of special nuclear materials (SNMs) through international borders could enable nuclear terrorism and constitutes a significant threat to global security. This paper presents the experimental demonstration of a novel radiographic technique for quantitatively reconstructing the density and type of material present in commercial cargo containers, as a means of detecting such threats. Unlike traditional techniques which use sources of bremsstrahlung photons with a continuous distribution of energies, multiple monoenergetic gamma radiography utilizes monoenergetic photons from nuclear reactions, specifically the 4.4 and 15.1 MeV photons from the 11B(d,nγ)12C reaction. By exploiting the Z-dependence of the photon interaction cross sections at these two specific energies, it is possible to simultaneously determine the areal density and the effective atomic number as a function of location for a 2D projection of a scanned object. The additional information gleaned from using and detecting photons of specific energies for radiography substantially increases the resolving power between different materials. This paper presents results from the imaging of mock cargo materials ranging from Z ≈5 -92 , demonstrating accurate reconstruction of the effective atomic number and areal density of the materials over the full range. In particular, the system is capable of distinguishing pure materials with Z ≳ 70 , such as lead and uranium—a critical requirement of a system designed to detect SNM. This methodology could be used to screen commercial cargoes with high material specificity, to distinguish most benign materials from SNM, such as uranium and plutonium.

[The development and implementation of polymerase chain reaction to detect in real-time operation mode yersinia pestis in field material].

PubMed

Afanas'ev, M V; Chipanin, E V; Shestakov, V E; Denisov, A V; Fomina, L A; Ostiak, A S; Balakhonov, S V

2013-03-01

The article presents the results of development and practical implementation of system of polymerase chain reaction testing in real-time operation mode to detect agent of plague infield material. In laboratory conditions the system demonstrated good results and hence it was applied in conditions of field laboratory of epidemiologic team during planned epizootologic examination of Gorno-Altaisk hot spot of plague. The sampling consisted of more than 1400 objects. It was demonstrated that high sensitivity and specificity is immanent to proposed system. The adaptation of the system to the real time amplifier "Smart Cycler" (Cephid, USA) having some specific technical characteristics makes it possible to consider the proposed test-system as an effective sensitive and precise instrument for screening studies in the process of regular epizootologic examinations of hot spots of plague.

Applied Nuclear Accountability Systems: A Case Study in the System Architecture and Development of NuMAC

DOE Office of Scientific and Technical Information (OSTI.GOV)

Campbell, Andrea Beth

2004-07-01

This is a case study of the NuMAC nuclear accountability system developed at a private fuel fabrication facility. This paper investigates nuclear material accountability and safeguards by researching expert knowledge applied in the system design and development. Presented is a system developed to detect and deter the theft of weapons grade nuclear material. Examined is the system architecture that includes: issues for the design and development of the system; stakeholder issues; how the system was built and evolved; software design, database design, and development tool considerations; security and computing ethics. (author)

Surface-geophysical techniques used to detect existing and infilled scour holes near bridge piers

USGS Publications Warehouse

Placzek, Gary; Haeni, F.P.

1995-01-01

Surface-geophysical techniques were used with a position-recording system to study riverbed scour near bridge piers. From May 1989 to May 1993. Fathometers, fixed- and swept-frequency con- tinuous seismic-reflection profiling (CSP) systems, and a ground-penetrating radar (GPR) system were used with a laser-positioning system to measure the depth and extent of existing and infilled scour holes near bridge piers. Equipment was purchased commercially and modified when necessary to interface the components and (or) to improve their performance. Three 200-kHz black-and-white chart- recording Fathometers produced profiles of the riverbed that included existing scour holes and exposed pier footings. The Fathometers were used in conjunction with other geophysical techniques to help interpret the geophysical data. A 20-kHz color Fathometer delineated scour-hole geometry and, in some cases, the thickness of fill material in the hole. The signal provided subbottom information as deep as 10 ft in fine-grained materials and resolved layers of fill material as thin as 1 foot thick. Fixed-frequency and swept-frequency CSP systems were evaluated. The fixed-frequency system used a 3.5-, 7.0-, or 14-kHz signal. The 3.5-kHz signal pene- trated up to 50 ft of fine-grained material and resolved layers as thin as 2.5-ft thick. The 14-kHz signal penetrated up to 20 ft of fine-grained material and resolved layers as thin as 1-ft thick. The swept-frequency systems used a signal that swept from 2- to 16-kHz. With this system, up to 50 ft of penetration was achieved, and fill material as thin as 1 ft was resolved. Scour-hole geometry, exposed pier footings, and fill thickness in scour holes were detected with both CSP systems. The GPR system used an 80-, 100-, or 300-megahertz signal. The technique produced records in water up to 15 ft deep that had a specific conductance less than 200x11ms/cm. The 100-MHz signal penetrated up to 40 ft of resistive granular material and resolved layers as thin as 2-ft thick. Scour-hole geometry, the thickness of fill material in scour holes, and riverbed deposition were detected using this technique. Processing techniques were applied after data collection to assist with the interpretation of the data. Data were transferred from the color Fathometer, CSP, and GPR systems to a personal computer, and a commercially available software package designed to process GPR data was used to process the GPR and CSP data. Digital filtering, predictive-deconvolution, and migration algorithms were applied to some of the data. The processed data were displayed and printed as color amplitude or wiggle-trace plots. These processing methods eased and improved the interpretation of some of the data, but some interference from side echoes from bridge piers and multiple reflections remained in the data. The surface-geophysical techniques were applied at six bridge sites in Connecticut. Each site had different water depths, specific conductance, and riverbed materials. Existing and infilled scour holes, exposed pier footings, and riverbed deposition were detected by the surveys. The interpretations of the geophysical data were confirmed by comparing the data with lithologic and (or) probing data.

30 CFR 75.301 - Definitions.

Code of Federal Regulations, 2011 CFR

2011-07-01

...-warning fire detection systems using newer technology that provides equal or greater protection, as... be purchased from the American Society for Testing Materials (ASTM), 1916 Race Street, Philadelphia..., copies of the document can be purchased from the American Society for Testing Materials (ASTM), 100 Barr...

Recognized Leader in Electrochemical Purification

ScienceCinema

Hoppe, Eric

2018-01-16

PNNL scientists developed an electrochemical method for purifying copper, a key material that makes possible radiation detection systems of unprecedented sensitivity. The method begins with the purest copper materials available, and results in the lowest-background copper in the world. Chemist Eric Hoppe explains the process.

Homogenization optics to improve detectability of a fluorescence response to a single laser pulse: Detection of feces on apples

USDA-ARS?s Scientific Manuscript database

Fecal contamination of produce is a known food safety risk. Measuring fluorescence responses to UV excitation is an established method for detecting such contamination. One measurement system utilizes a pulsed UV laser to induce a fluorescence response from fecal material and a gated intensified cam...

The Fundamentals of Thermal Imaging Systems.

DTIC Science & Technology

1979-05-10

detection , recognition, or identification, of real ’coene objects aire discussed. It is hoped that the text will be useful to FLIR designers, evaluators...AND ANDERSON EXPERIMENT ........................ 205 Appendix F - BASIC SNR AND DETECTIVITY RELATIONS ................................... 209 Appendix... detection , recognition, or identification, of real scene objects are discussed. I• It is hoped that the material in the text will be useful to

X-ray radiography for container inspection

DOEpatents

Katz, Jonathan I [Clayton, MO; Morris, Christopher L [Los Alamos, NM

2011-06-07

Arrangements of X-ray inspection systems are described for inspecting high-z materials in voluminous objects such as containers. Inspection methods may involve generating a radiographic image based on detected attenuation corresponding to a pulsed beams of radiation transmitted through a voluminous object. The pulsed beams of radiation are generated by a high-energy source and transmitted substantially downward along an incident angle, of approximately 1.degree. to 30.degree., to a vertical axis extending through the voluminous object. The generated radiographic image may be analyzed to detect on localized high attenuation representative of high-z materials and to discriminate high-z materials from lower and intermediate-z materials on the basis of the high density and greater attenuation of high-z material for higher energy (3-10 MeV) X-rays, and the compact nature of threatening masses of fissionable materials.

Real space mapping of ionic diffusion and electrochemical activity in energy storage and conversion materials

DOEpatents

Kalinin, Sergei V; Balke, Nina; Kumar, Amit; Dudney, Nancy J; Jesse, Stephen

2014-05-06

A method and system for probing mobile ion diffusivity and electrochemical reactivity on a nanometer length scale of a free electrochemically active surface includes a control module that biases the surface of the material. An electrical excitation signal is applied to the material and induces the movement of mobile ions. An SPM probe in contact with the surface of the material detects the displacement of mobile ions at the surface of the material. A detector measures an electromechanical strain response at the surface of the material based on the movement and reactions of the mobile ions. The use of an SPM tip to detect local deformations allows highly reproducible measurements in an ambient environment without visible changes in surface structure. The measurements illustrate effective spatial resolution comparable with defect spacing and well below characteristic grain sizes of the material.

FT-IR standoff detection of thermally excited emissions of trinitrotoluene (TNT) deposited on aluminum substrates.

PubMed

Castro-Suarez, John R; Pacheco-Londoño, Leonardo C; Vélez-Reyes, Miguel; Diem, Max; Tague, Thomas J; Hernandez-Rivera, Samuel P

2013-02-01

A standoff detection system was assembled by coupling a reflecting telescope to a Fourier transform infrared spectrometer equipped with a cryo-cooled mercury cadmium telluride detector and used for detection of solid-phase samples deposited on substrates. Samples of highly energetic materials were deposited on aluminum substrates and detected at several collector-target distances by performing passive-mode, remote, infrared detection measurements on the heated analytes. Aluminum plates were used as support material, and 2,4,6-Trinitrotoluene (TNT) was used as the target. For standoff detection experiments, the samples were placed at different distances (4 to 55 m). Several target surface temperatures were investigated. Partial least squares regression analysis was applied to the analysis of the intensities of the spectra obtained. Overall, standoff detection in passive mode was useful for quantifying TNT deposited on the aluminum plates with high confidence up to target-collector distances of 55 m.

Damage detection in sandwich composite materials using laser vibrometry in conjunction with nonlinear system identification

NASA Astrophysics Data System (ADS)

Underwood, Sara; Koester, David; Adams, Douglas E.

2009-03-01

Fiberglass sandwich panels are tested to study a vibration-based method for locating damage in composite materials. This method does not rely on a direct comparison of the natural frequencies, mode shapes, or residues in the forced vibration response data. Specifically, a nonlinear system identification based method for damage detection is sought that reduces the sensitivity of damage detection results to changes in vibration measurements due to variations in boundary conditions, environmental conditions, and material properties of the panel. Damage mechanisms considered include a disbond between the core and face sheet and a crack within the core. A panel is excited by a skewed piezoelectric actuator over a broad frequency range while a three-dimensional scanning laser vibrometer measures the surface velocity of the panel along three orthogonal axes. The forced frequency response data measured using the scanning laser vibrometer at multiple excitation amplitudes is processed to identify areas of the panel that exhibit significant nonlinear response characteristics. It is demonstrated that these localized nonlinearities in the panel coincide with the damaged areas of the composite material. Because changes in the measured frequency response functions due to nonlinear distortions associated with the damage can be identified without comparing the vibration data to a reference (baseline) signature of the undamaged material, this vibration technique for damage detection in composite materials exhibits less sensitivity to variations in the underlying linear characteristics than traditional methods. It is also demonstrated that the damage at a given location can be classified as either due to a disbond or core crack because these two types of damage produce difference signatures when comparing the multi-amplitude frequency response functions.

Damage assessment of composite plate structures with material and measurement uncertainty

NASA Astrophysics Data System (ADS)

Chandrashekhar, M.; Ganguli, Ranjan

2016-06-01

Composite materials are very useful in structural engineering particularly in weight sensitive applications. Two different test models of the same structure made from composite materials can display very different dynamic behavior due to large uncertainties associated with composite material properties. Also, composite structures can suffer from pre-existing imperfections like delaminations, voids or cracks during fabrication. In this paper, we show that modeling and material uncertainties in composite structures can cause considerable problem in damage assessment. A recently developed C0 shear deformable locking free refined composite plate element is employed in the numerical simulations to alleviate modeling uncertainty. A qualitative estimate of the impact of modeling uncertainty on the damage detection problem is made. A robust Fuzzy Logic System (FLS) with sliding window defuzzifier is used for delamination damage detection in composite plate type structures. The FLS is designed using variations in modal frequencies due to randomness in material properties. Probabilistic analysis is performed using Monte Carlo Simulation (MCS) on a composite plate finite element model. It is demonstrated that the FLS shows excellent robustness in delamination detection at very high levels of randomness in input data.

Improved Fission Neutron Data Base for Active Interrogation of Actinides

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pozzi, Sara; Czirr, J. Bart; Haight, Robert

2013-11-06

This project will develop an innovative neutron detection system for active interrogation measurements. Many active interrogation methods to detect fissionable material are based on the detection of neutrons from fission induced by fast neutrons or high-energy gamma rays. The energy spectrum of the fission neutrons provides data to identify the fissionable isotopes and materials such as shielding between the fissionable material and the detector. The proposed path for the project is as follows. First, the team will develop new neutron detection systems and algorithms by Monte Carlo simulations and bench-top experiments. Next, They will characterize and calibrate detection systems bothmore » with monoenergetic and white neutron sources. Finally, high-fidelity measurements of neutron emission from fissions induced by fast neutrons will be performed. Several existing fission chambers containing U-235, Pu-239, U-238, or Th-232 will be used to measure the neutron-induced fission neutron emission spectra. The challenge for making confident measurements is the detection of neutrons in the energy ranges of 0.01 – 1 MeV and above 8 MeV, regions where the basic data on the neutron energy spectrum emitted from fission is least well known. In addition, improvements in the specificity of neutron detectors are required throughout the complete energy range: they must be able to clearly distinguish neutrons from other radiations, in particular gamma rays and cosmic rays. The team believes that all of these challenges can be addressed successfully with emerging technologies under development by this collaboration. In particular, the collaboration will address the area of fission neutron emission spectra for isotopes of interest in the advanced fuel cycle initiative (AFCI).« less

Evaluation of eddy current and magnetic techniques for inspecting rebars in bridge barrier rails

NASA Astrophysics Data System (ADS)

Lo, C. C. H.; Nakagawa, N.

2013-01-01

This paper reports on a feasibility study of using eddy current (EC) and magnetic flux leakage (MFL) methods to detect corrosion damage in rebars that anchor concrete barrier rails to the road deck of bridge structures. EC and MFL measurements were carried out on standalone rebars with and without artificial defects of 25% and 50% material loss, using a commercial EC-based rebar locator and a MFL system that was developed using giant magnetoresistance sensors to detect leakage fluxes from the defects. Both techniques can readily detect the defects at a distance of 2.5″ (63.5 mm). The amplitudes of the EC and MFL signals vary monotonically with the amount of material loss, indicating the potential of using the techniques to quantify material loss of standalone rebars.

Search for Superconductivity in Micrometeorites

PubMed Central

Guénon, S.; Ramírez, J. G.; Basaran, Ali C.; Wampler, J.; Thiemens, M.; Taylor, S.; Schuller, Ivan K.

2014-01-01

We have developed a very sensitive, highly selective, non-destructive technique for screening inhomogeneous materials for the presence of superconductivity. This technique, based on phase sensitive detection of microwave absorption is capable of detecting 10−12 cc of a superconductor embedded in a non-superconducting, non-magnetic matrix. For the first time, we apply this technique to the search for superconductivity in extraterrestrial samples. We tested approximately 65 micrometeorites collected from the water well at the Amundsen-Scott South pole station and compared their spectra with those of eight reference materials. None of these micrometeorites contained superconducting compounds, but we saw the Verwey transition of magnetite in our microwave system. This demonstrates that we are able to detect electro-magnetic phase transitions in extraterrestrial materials at cryogenic temperatures. PMID:25476841

Characterization of dielectric materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

King, Danny J.; Babinec, Susan; Hagans, Patrick L.

2017-06-27

A system and a method for characterizing a dielectric material are provided. The system and method generally include applying an excitation signal to electrodes on opposing sides of the dielectric material to evaluate a property of the dielectric material. The method can further include measuring the capacitive impedance across the dielectric material, and determining a variation in the capacitive impedance with respect to either or both of a time domain and a frequency domain. The measured property can include pore size and surface imperfections. The method can still further include modifying a processing parameter as the dielectric material is formedmore » in response to the detected variations in the capacitive impedance, which can correspond to a non-uniformity in the dielectric material.« less

Enhancing nuclear quadrupole resonance (NQR) signature detection leveraging interference suppression algorithms

NASA Astrophysics Data System (ADS)

DeBardelaben, James A.; Miller, Jeremy K.; Myrick, Wilbur L.; Miller, Joel B.; Gilbreath, G. Charmaine; Bajramaj, Blerta

2012-06-01

Nuclear quadrupole resonance (NQR) is a radio frequency (RF) magnetic spectroscopic technique that has been shown to detect and identify a wide range of explosive materials containing quadrupolar nuclei. The NQR response signal provides a unique signature of the material of interest. The signal is, however, very weak and can be masked by non-stationary RF interference (RFI) and thermal noise, limiting detection distance. In this paper, we investigate the bounds on the NQR detection range for ammonium nitrate. We leverage a low-cost RFI data acquisition system composed of inexpensive B-field sensing and commercial-off-the-shelf (COTS) software-defined radios (SDR). Using collected data as RFI reference signals, we apply adaptive filtering algorithms to mitigate RFI and enable NQR detection techniques to approach theoretical range bounds in tactical environments.

A Fluorescent Tile DNA Diagnocode System for In Situ Rapid and Selective Diagnosis of Cytosolic RNA Cancer Markers

PubMed Central

Park, Kyung Soo; Shin, Seung Won; Jang, Min Su; Shin, Woojung; Yang, Kisuk; Min, Junhong; Cho, Seung-Woo; Oh, Byung-Keun; Bae, Jong Wook; Jung, Sunghwan; Choi, Jeong-Woo; Um, Soong Ho

2015-01-01

Accurate cancer diagnosis often requires extraction and purification of genetic materials from cells, and sophisticated instrumentations that follow. Otherwise in order to directly treat the diagnostic materials to cells, multiple steps to optimize dose concentration and treatment time are necessary due to diversity in cellular behaviors. These processes may offer high precision but hinder fast analysis of cancer, especially in clinical situations that need rapid detection and characterization of cancer. Here we present a novel fluorescent tile DNA nanostructure delivered to cancer cytosol by employing nanoparticle technology. Its structural anisotropicity offers easy manipulation for multifunctionalities, enabling the novel DNA nanostructure to detect intracellular cancer RNA markers with high specificity within 30 minutes post treatment, while the nanoparticle property bypasses the requirement of treatment optimization, effectively reducing the complexity of applying the system for cancer diagnosis. Altogether, the system offers a precise and rapid detection of cancer, suggesting the future use in the clinical fields. PMID:26678430

Two techniques for eliminating luminol interference material and flow system configurations for luminol and firefly luciferase systems

NASA Technical Reports Server (NTRS)

Thomas, R. R.

1976-01-01

Two methods for eliminating luminol interference materials are described. One method eliminates interference from organic material by pre-reacting a sample with dilute hydrogen peroxide. The reaction rate resolution method for eliminating inorganic forms of interference is also described. The combination of the two methods makes the luminol system more specific for bacteria. Flow system designs for both the firefly luciferase and luminol bacteria detection systems are described. The firefly luciferase flow system incorporating nitric acid extraction and optimal dilutions has a functional sensitivity of 3 x 100,000 E. coli/ml. The luminol flow system incorporates the hydrogen peroxide pretreatment and the reaction rate resolution techniques for eliminating interference. The functional sensitivity of the luminol flow system is 1 x 10,000 E. coli/ml.

Fast Photo-detection in Phototransistors based on Group III-VI Layered Materials.

NASA Astrophysics Data System (ADS)

Patil, Prasanna; Ghosh, Sujoy; Wasala, Milinda; Lei, Sidong; Vajtai, Robert; Ajayan, Pulickel; Talapatra, Saikat

Response time of a photo detector is one of the crucial aspect of photo-detection. Recently it has been shown that direct band gap of few layered group III-VI materials helps in increased absorption of light thereby enhancing the photo responsive properties of these materials. Ternary system of Copper Indium Selenide has been extensively used in optoelectronics industry and it is expected that 2D layered structure of Copper Indium Selenide will be a key component of future optoelectronics devices based on 2D materials. Here we report fast photo detection in few layers of Copper Indium Selenide (CuIn7Se11) phototransistor. Few-layers of CuIn7Se11 flakes were exfoliated from crystals grown using chemical vapor transport technique. Our photo response characterization indicates responsivity of 104 mA/W with external quantum efficiency exceeding 103. We have found response time of few μs which is one of the fastest response among photodetectors based on 2D materials. We also found specific detectivity of 1012 Jones which is an order higher than conventional photodetectors. A comparison between response times of various layered group III-VI materials will be presented and discussed. This work is supported by the U.S. Army Research Office through a MURI Grant # W911NF-11-1-0362.

Raman spectroscopy method for subsurface detection of food powders through plastic layers

NASA Astrophysics Data System (ADS)

Dhakal, Sagar; Chao, Kuanglin; Qin, Jianwei; Schmidt, Walter F.; Kim, Moon S.; Chan, Diane E.; Bae, Abigail

2017-05-01

Proper chemical analyses of materials in sealed containers are important for quality control purpose. Although it is feasible to detect chemicals at top surface layer, it is relatively challenging to detect objects beneath obscuring surface. This study used spatially offset Raman spectroscopy (SORS) method to detect urea, ibuprofen and acetaminophen powders contained within one or more (up to eight) layers of gelatin capsules to demonstrate subsurface chemical detection and identification. A 785 nm point-scan Raman spectroscopy system was used to acquire spatially offset Raman spectra for an offset range of 0 to 10 mm from the surfaces of 24 encapsulated samples, using a step size of 0.1 mm to obtain 101 spectral measurements per sample. With increasing offset distance, the fraction of information from the deeper subsurface material increased compared to that from the top surface material. The series of measurements was analyzed to differentiate and identify the top surface and subsurface materials. Containing mixed contributions from the powder and capsule, the SORS of each sample was decomposed using self modeling mixture analysis (SMA) to obtain pure component spectra of each component and corresponding components were identified using spectral information divergence values. Results show that SORS technique together with SMA method has a potential for non-invasive detection of chemicals at deep subsurface layer.

Radiation Detection at Borders for Homeland Security

NASA Astrophysics Data System (ADS)

Kouzes, Richard

2004-05-01

Countries around the world are deploying radiation detection instrumentation to interdict the illegal shipment of radioactive material crossing international borders at land, rail, air, and sea ports of entry. These efforts include deployments in the US and a number of European and Asian countries by governments and international agencies. Items of concern include radiation dispersal devices (RDD), nuclear warheads, and special nuclear material (SNM). Radiation portal monitors (RPMs) are used as the main screening tool for vehicles and cargo at borders, supplemented by handheld detectors, personal radiation detectors, and x-ray imaging systems. Some cargo contains naturally occurring radioactive material (NORM) that triggers "nuisance" alarms in RPMs at these border crossings. Individuals treated with medical radiopharmaceuticals also produce nuisance alarms and can produce cross-talk between adjacent lanes of a multi-lane deployment. The operational impact of nuisance alarms can be significant at border crossings. Methods have been developed for reducing this impact without negatively affecting the requirements for interdiction of radioactive materials of interest. Plastic scintillator material is commonly used in RPMs for the detection of gamma rays from radioactive material, primarily due to the efficiency per unit cost compared to other detection materials. The resolution and lack of full-energy peaks in the plastic scintillator material prohibits detailed spectroscopy. However, the limited spectroscopic information from plastic scintillator can be exploited to provide some discrimination. Energy-based algorithms used in RPMs can effectively exploit the crude energy information available from a plastic scintillator to distinguish some NORM. Whenever NORM cargo limits the level of the alarm threshold, energy-based algorithms produce significantly better detection probabilities for small SNM sources than gross-count algorithms. This presentation discusses experience with RPMs for interdiction of radioactive materials at borders.

Analyses via automated mass spectrometry (MS/DS)

NASA Technical Reports Server (NTRS)

Koenig, T.

1985-01-01

New or improved uses of the Finnigan 4000 quadrupole mass spectrometer (MS) with its associated INCOS data system (DS) were investigated. The first phase involved an evaluative activity in which specific problems with miscalibration and gas chromatographic column conditioning were identified. This also revealed one solution to the problem of detection of substances not visible in the gas chromatography detection mode. A second phase was to seek useful applications of the direct inlet systems. This mode of sample introduction has not been previously utilized on the existing equipment and was successfully applied to the analysis of the components of TONOX 60/40 and in the thermal degradation products of some polymeric materials. Suggestions are made for improving and expanding the use of the MS/DS system in materials development and testing.

21 CFR 862.1660 - Quality control material (assayed and unassayed).

Code of Federal Regulations, 2013 CFR

2013-04-01

... SERVICES (CONTINUED) MEDICAL DEVICES CLINICAL CHEMISTRY AND CLINICAL TOXICOLOGY DEVICES Clinical Chemistry... control material (assayed and unassayed) for clinical chemistry is a device intended for medical purposes for use in a test system to estimate test precision and to detect systematic analytical deviations...

21 CFR 862.1660 - Quality control material (assayed and unassayed).

Code of Federal Regulations, 2014 CFR

2014-04-01

... SERVICES (CONTINUED) MEDICAL DEVICES CLINICAL CHEMISTRY AND CLINICAL TOXICOLOGY DEVICES Clinical Chemistry... control material (assayed and unassayed) for clinical chemistry is a device intended for medical purposes for use in a test system to estimate test precision and to detect systematic analytical deviations...

21 CFR 862.1660 - Quality control material (assayed and unassayed).

Code of Federal Regulations, 2012 CFR

2012-04-01

... SERVICES (CONTINUED) MEDICAL DEVICES CLINICAL CHEMISTRY AND CLINICAL TOXICOLOGY DEVICES Clinical Chemistry... control material (assayed and unassayed) for clinical chemistry is a device intended for medical purposes for use in a test system to estimate test precision and to detect systematic analytical deviations...

75 FR 53855 - Airworthiness Directives; BAE Systems (Operations) Limited Model BAe 146 and Avro 146-RJ Airplanes

Federal Register 2010, 2011, 2012, 2013, 2014

2010-09-02

.... This puncture tends to result in a tear, which, if detected in time, can be repaired with tape; however... bag also tends to cause tears in the material, making the insulation material sag, thereby causing...

75 FR 27959 - Airworthiness Directives; BAE Systems (Operations) Limited Model BAe 146 and Avro 146-RJ Airplanes

Federal Register 2010, 2011, 2012, 2013, 2014

2010-05-19

.... This puncture tends to result in a tear, which, if detected in time, can be repaired with tape; however... bag also tends to cause tears in the material, making the insulation material sag, thereby causing...

Detecting and identifying DNA via the THz backbone frequency using a metamaterial-based label-free biosensor

NASA Astrophysics Data System (ADS)

Mirzaei, Sahar; Green, Nicolas G.; Rotaru, Mihai; Pu, Suan Hui

2017-02-01

In genetic diagnostics, laboratory-based equipment generally uses analytical techniques requiring complicated and expensive fluorescent labelling of target DNA molecules. Intense research effort into, and commercial development of, Point-of-Care diagnostics and Personalized Healthcare are driving the development of simple, fast and cost-effective detection methods. One potential label-free DNA detection method uses Terahertz (THz) spectroscopy of the natural responses of DNA in metamaterial structures, which are engineered to have properties that are impossible to obtain in natural materials. This paper presents a study of the development of metamaterials based on asymmetric X-shaped resonator inclusions as a functional sensor for DNA. Gold X-shaped resonator structures with dimensions of 90/85 μm were demonstrated to produce trapped mode resonant frequency in the correct range for DNA detection. Realistic substrate materials in the form of 375 μm thick quartz were investigated, demonstrating that the non-transparent nature of the material resulted in the production of standing waves, affecting the system response, as well as requiring a reduction in scale of the resonator of 85%. As a result, the effect of introducing etched windows in the substrate material were investigated, demonstrating that increased window size significantly reduces the effect of the substrate on the system response. The device design showed a good selectivity when RNA samples were introduced to the model, demonstrating the potential for this design of device in the development of sensors capable of performing cheap and simple genetic analysis of DNA, giving label-free detection at high sensitivity.

Surface Cleaning Techniques: Ultra-Trace ICP-MS Sample Preparation and Assay of HDPE

DOE Office of Scientific and Technical Information (OSTI.GOV)

Overman, Nicole R.; Hoppe, Eric W.; Addleman, Raymond S.

2013-06-01

The world’s most sensitive radiation detection and assay systems depend upon ultra-low background (ULB) materials to reduce unwanted radiological backgrounds. Herein, we evaluate methods to clean HDPE, a material of interest to ULB systems and the means to provide rapid assay of surface and bulk contamination. ULB level material and ultra-trace level detection of actinide elements is difficult to attain, due to the introduction of contamination from sample preparation equipment such as pipette tips, sample vials, forceps, etc. and airborne particulate. To date, literature available on the cleaning of such polymeric materials and equipment for ULB applications and ultra-trace analysesmore » is limited. For these reasons, a study has been performed to identify an effective way to remove surface contamination from polymers in an effort to provide improved instrumental detection limits. Inductively Coupled Plasma Mass Spectroscopy (ICP-MS) was utilized to assess the effectiveness of a variety of leachate solutions for removal of inorganic uranium and thorium surface contamination from polymers, specifically high density polyethylene (HDPE). HDPE leaching procedures were tested to optimize contaminant removal of thorium and uranium. Calibration curves for thorium and uranium ranged from 15 ppq (fg/mL) to 1 ppt (pg/mL). Detection limits were calculated at 6 ppq for uranium and 7 ppq for thorium. Results showed the most effective leaching reagent to be clean 6 M nitric acid for 72 hour exposures. Contamination levels for uranium and thorium found in the leachate solutions were significant for ultralow level radiation detection applications.« less

Radiation-Responsive Esculin-Derived Molecular Gels as Signal Enhancers for Optical Imaging.

PubMed

Silverman, Julian R; Zhang, Qize; Pramanik, Nabendu B; Samateh, Malick; Shaffer, Travis M; Sagiri, Sai Sateesh; Grimm, Jan; John, George

2017-12-13

Recent interest in detecting visible photons that emanate from interactions of ionizing radiation (IR) with matter has spurred the development of multifunctional materials that amplify the optical signal from radiotracers. Tailored stimuli-responsive systems may be paired with diagnostic radionuclides to improve surgical guidance and aid in detecting therapeutic radionuclides otherwise difficult to image with conventional nuclear medicine approaches. Because light emanating from these interactions is typically low in intensity and blue-weighted (i.e., greatly scattered and absorbed in vivo), it is imperative to increase or shift the photon flux for improved detection. To address this challenge, a gel that is both scintillating and fluorescent is used to enhance the optical photon output in image mapping for cancer imaging. Tailoring biobased materials to synthesize thixotropic thermoreversible hydrogels (a minimum gelation concentration of 0.12 wt %) offers image-aiding systems which are not only functional but also potentially economical, safe, and environmentally friendly. These robust gels (0.66 wt %, ∼900 Pa) respond predictably to different types of IRs including β- and γ-emitters, resulting in a doubling of the detectable photon flux from these emitters. The synthesis and formulation of such a gel are explored with a focus on its physicochemical and mechanical properties, before being utilized to enhance the visible photon flux from a panel of radionuclides as detected. The possibility of developing a topical cream of this gel makes this system an attractive potential alternative to current techniques, and the multifunctionality of the gelator may serve to inspire future next-generation materials.

Associated-particle sealed-tube neutron probe for characterization of materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rhodes, E.; Dickerman, C.E.; Peters, C.W.

1993-10-01

A neutron diagnostic probe system has been developed that can identify and image most elements having a larger atomic number than boron. It can satisfy van-mobile and fixed-portal requirements for nondestructive detection of contraband drugs, explosives, and nuclear and chemical warfare weapon materials, and for treaty verification of sealed munitions and remediation of radioactive waste. The probe is based on a nonpulsed associated-particle sealed-tube neutron generator (APSTNG) that interrogates the object with a 14-MeV neutrons and detects alpha-particle associated with each neutron. Gamma-ray spectra of resulting neutron reactions (primarily inelastic scattering) identify nuclides associated with drugs, explosives, and other contraband.more » Flight times determined from detection times of gamma-rays and alpha-particles yield a separate coarse tomographic image of each identified nuclide. Chemical substances are identified and imaged by comparing relative spectra fine intensities with ratios of elements in reference compounds. The High-energy neutrons in gamma-rays will penetrate large objects and dense materials. The source and emission detection systems can be on the same side, allowing measurements with access to one side only. A high signal-to-background ratio is obtained and maximum information is extracted from each detected gamma-ray, yet high-bandwidth data acquisition is not required. The APSTNG also forms the basis for a compact fast-neutron transmission imaging system. No collimators are required, and only minimal shielding is needed. The small and relatively inexpensive neutron generator tube exhibits high reliability and can be quickly replaced. The detector arrays and associated electronics can be made reliable with low maintenance cost.« less

Smart materials and structures

NASA Technical Reports Server (NTRS)

Rogowski, Robert S.; Heyman, Joseph S.

1993-01-01

Embedded optical fibers allow not only the cure-monitoring and in-service lifetime measurements of composite materials, but the NDE of material damage and degradation with aging. The capabilities of such damage-detection systems have been extended to allow the quantitative determination of 2D strain in materials by several different methods, including the interferometric and the numerical. It remains to be seen, what effect the embedded fibers have on the strength of the 'smart' materials created through their incorporation.

Piezoelectric Materials Under Natural and Man-Made Radiation: The Potential for Direct Radiation Detection

NASA Astrophysics Data System (ADS)

Wart, Megan; Simpson, Evan; Flaska, Marek

2018-01-01

Radiation detection systems used for monitoring long term waste storage need to be compact, rugged, and have low or no power requirements. By using piezoelectric materials it may be possible to create a reliable self-powered radiation detection system. To determine the feasibility of this approach, the electrical signal response of the piezoelectric materials to radiation must be characterized. To do so, an experimental geometry has been designed and a neutron source has been chosen as described in this paper, which will be used to irradiate a uranium foil for producing fission fragments. These future experiments will be aimed at finding the threshold of exposure of lead zirconate titanate (PZT) plates needed to produce and electrical signal. Based on the proposed experimental geometry the thermal neutron beam-line at the Breazeale Reactor at The Pennsylvania State University will be used as the neutron source. The uranium foil and neutron source will be able to supply a maximum flux of 1.5e5 fission fragments/second*cm2 to each of the PZT plates.

Fluorescent x-ray computed tomography to visualize specific material distribution

NASA Astrophysics Data System (ADS)

Takeda, Tohoru; Yuasa, Tetsuya; Hoshino, Atsunori; Akiba, Masahiro; Uchida, Akira; Kazama, Masahiro; Hyodo, Kazuyuki; Dilmanian, F. Avraham; Akatsuka, Takao; Itai, Yuji

1997-10-01

Fluorescent x-ray computed tomography (FXCT) is being developed to detect non-radioactive contrast materials in living specimens. The FXCT systems consists of a silicon channel cut monochromator, an x-ray slit and a collimator for detection, a scanning table for the target organ and an x-ray detector for fluorescent x-ray and transmission x-ray. To reduce Compton scattering overlapped on the K(alpha) line, incident monochromatic x-ray was set at 37 keV. At 37 keV Monte Carlo simulation showed almost complete separation between Compton scattering and the K(alpha) line. Actual experiments revealed small contamination of Compton scattering on the K(alpha) line. A clear FXCT image of a phantom was obtained. Using this system the minimal detectable dose of iodine was 30 ng in a volume of 1 mm3, and a linear relationship was demonstrated between photon counts of fluorescent x-rays and the concentration of iodine contrast material. The use of high incident x-ray energy allows an increase in the signal to noise ratio by reducing the Compton scattering on the K(alpha) line.

Explosives (and other threats) detection using pulsed neutron interrogation and optimized detectors

NASA Astrophysics Data System (ADS)

Strellis, Dan A.; Elsalim, Mashal; Gozani, Tsahi

2011-06-01

We have previously reported results from a human-portable system using neutron interrogation to detect contraband and explosives. We summarized our methodology for distinguishing threat materials such as narcotics, C4, and mustard gas in the myriad of backgrounds present in the maritime environment. We are expanding our mission for the Domestic Nuclear Detection Office (DNDO) to detect Special Nuclear Material (SNM) through the detection of multiple fission signatures without compromising the conventional threat detection performance. This paper covers our initial investigations into using neutrons from compact pulsed neutron generators via the d(D,n)3He or d(T,n)α reactions with energies of ~2.5 and 14 MeV, respectively, for explosives (and other threats) detection along with a variety of gamma-ray detectors. Fast neutrons and thermal neutrons (after successive collisions) can stimulate the emission of various threat detection signatures. For explosives detection, element-specific gamma-ray signatures via the (n,n'γ) inelastic scattering reaction and the (n,'γ) thermal capture reaction are detected. For SNM, delayed gamma-rays following fission can be measured with the same detector. Our initial trade-off investigations of several gamma-ray detectors types (NaI, CsI, LaBr3, HPGe) for measuring gamma-ray signatures in a pulsed neutron environment for potential application in a human-portable active interrogation system are covered in this paper.

Subsurface damage detection in non-ferrous systems using 3D synchronous magnetic inspection

NASA Astrophysics Data System (ADS)

Gray, David; Berry, David

2018-04-01

Prime Photonics is developing a non-destructive inspection (NDI) technology, 3-D synchronous magnetic imaging system (3-D SMIS), that uses synchronous detection of magnetic signatures resulting from ultrasonic excitation to measure both surface and subsurface flaws in conductive structures. 3-D SMIS is showing promise in a wide range of NDI/NDE uses including characterizing surface-breaking cracks in ferrous and non-ferrous materials, locating and characterizing subsurface cracks within nonferrous conductive materials (Ti 6-4 and carbon fiber composites), and characterization of subsurface residual stresses. The technology offers a non-contact, high resolution inspection technique that does not require austere environments, and can accommodate non-planar specimen geometries.

Enhanced coupling of light into a turbid medium through microscopic interface engineering

PubMed Central

Thompson, Jonathan V.; Hokr, Brett H.; Kim, Wihan; Ballmann, Charles W.; Applegate, Brian E.; Jo, Javier; Yamilov, Alexey; Cao, Hui; Scully, Marlan O.; Yakovlev, Vladislav V.

2017-01-01

There are many optical detection and sensing methods used today that provide powerful ways to diagnose, characterize, and study materials. For example, the measurement of spontaneous Raman scattering allows for remote detection and identification of chemicals. Many other optical techniques provide unique solutions to learn about biological, chemical, and even structural systems. However, when these systems exist in a highly scattering or turbid medium, the optical scattering effects reduce the effectiveness of these methods. In this article, we demonstrate a method to engineer the geometry of the optical interface of a turbid medium, thereby drastically enhancing the coupling efficiency of light into the material. This enhanced optical coupling means that light incident on the material will penetrate deeper into (and through) the medium. It also means that light thus injected into the material will have an enhanced interaction time with particles contained within the material. These results show that, by using the multiple scattering of light in a turbid medium, enhanced light–matter interaction can be achieved; this has a direct impact on spectroscopic methods such as Raman scattering and fluorescence detection in highly scattering regimes. Furthermore, the enhanced penetration depth achieved by this method will directly impact optical techniques that have previously been limited by the inability to deposit sufficient amounts of optical energy below or through highly scattering layers. PMID:28701381

Acoustic Emission Beamforming for Detection and Localization of Damage

NASA Astrophysics Data System (ADS)

Rivey, Joshua Callen

The aerospace industry is a constantly evolving field with corporate manufacturers continually utilizing innovative processes and materials. These materials include advanced metallics and composite systems. The exploration and implementation of new materials and structures has prompted the development of numerous structural health monitoring and nondestructive evaluation techniques for quality assurance purposes and pre- and in-service damage detection. Exploitation of acoustic emission sensors coupled with a beamforming technique provides the potential for creating an effective non-contact and non-invasive monitoring capability for assessing structural integrity. This investigation used an acoustic emission detection device that employs helical arrays of MEMS-based microphones around a high-definition optical camera to provide real-time non-contact monitoring of inspection specimens during testing. The study assessed the feasibility of the sound camera for use in structural health monitoring of composite specimens during tensile testing for detecting onset of damage in addition to nondestructive evaluation of aluminum inspection plates for visualizing stress wave propagation in structures. During composite material monitoring, the sound camera was able to accurately identify the onset and location of damage resulting from large amplitude acoustic feedback mechanisms such as fiber breakage. Damage resulting from smaller acoustic feedback events such as matrix failure was detected but not localized to the degree of accuracy of larger feedback events. Findings suggest that beamforming technology can provide effective non-contact and non-invasive inspection of composite materials, characterizing the onset and the location of damage in an efficient manner. With regards to the nondestructive evaluation of metallic plates, this remote sensing system allows us to record wave propagation events in situ via a single-shot measurement. This is a significant improvement over the conventional wave propagation tracking technique based on laser doppler vibrometry that requires synchronization of data acquired from numerous excitations and measurements. The proposed technique can be used to characterize and localize damage by detecting the scattering, attenuation, and reflections of stress waves resulting from damage and defects. These studies lend credence to the potential development of new SHM/NDE techniques based on acoustic emission beamforming for characterizing a wide spectrum of damage modes in next-generation materials and structures without the need for mounted contact sensors.

Detection of gamma-neutron radiation by solid-state scintillation detectors. Detection of gamma-neutron radiation by novel solid-state scintillation detectors

DOE Office of Scientific and Technical Information (OSTI.GOV)

Ryzhikov, V.; Grinyov, B.; Piven, L.

It is known that solid-state scintillators can be used for detection of both gamma radiation and neutron flux. In the past, neutron detection efficiencies of such solid-state scintillators did not exceed 5-7%. At the same time it is known that the detection efficiency of the gamma-neutron radiation characteristic of nuclear fissionable materials is by an order of magnitude higher than the efficiency of detection of neutron fluxes alone. Thus, an important objective is the creation of detection systems that are both highly efficient in gamma-neutron detection and also capable of exhibiting high gamma suppression for use in the role ofmore » detection of neutron radiation. In this work, we present the results of our experimental and theoretical studies on the detection efficiency of fast neutrons from a {sup 239}Pu-Be source by the heavy oxide scintillators BGO, GSO, CWO and ZWO, as well as ZnSe(Te, O). The most probable mechanism of fast neutron interaction with nuclei of heavy oxide scintillators is the inelastic scattering (n, n'γ) reaction. In our work, fast neutron detection efficiencies were determined by the method of internal counting of gamma-quanta that emerge in the scintillator from (n, n''γ) reactions on scintillator nuclei with the resulting gamma energies of ∼20-300 keV. The measured efficiency of neutron detection for the scintillation crystals we considered was ∼40-50 %. The present work included a detailed analysis of detection efficiency as a function of detector and area of the working surface, as well as a search for new ways to create larger-sized detectors of lower cost. As a result of our studies, we have found an unusual dependence of fast neutron detection efficiency upon thickness of the oxide scintillators. An explanation for this anomaly may involve the competition of two factors that accompany inelastic scattering on the heavy atomic nuclei. The transformation of the energy spectrum of neutrons involved in the (n, n'γ) reactions towards lower energies and the isotropic character of scattering of the secondary neutrons may lead to the observed limitation of the length of effective interaction, since a fraction of the secondary neutrons that propagate in the forward direction are not subject to further inelastic scattering because of their substantially lower energy. At these reduced energies, it is the capture cross-section (n, γ) that becomes predominant, resulting in lower detection efficiency. Based on these results, several types of detectors have been envisioned for application in detection systems for nuclear materials. The testing results for one such detector are presented in this work. We have studied the possibility of creation of a composite detector with scintillator granules placed inside a transparent polymer material. Because of the low transparency of such a dispersed scintillator, better light collection conditions are ensured by incorporation of a light guide between the scintillator layers. This guide is made of highly transparent polymer material. The use of a high-transparency hydrogen-containing polymer material for light guides not only ensures optimum conditions of light collection in the detector, but also allows certain deceleration of neutron radiation, increasing its interaction efficiency with the composite scintillation panels; accordingly, the detector signal is increased by 5-8%. When fast neutrons interact with the scintillator material, the resulting inelastic scattering gamma-quanta emerge, having different energies and different delay times with respect to the moment of the neutron interaction with the nucleus of the scintillator material (delay times ranging from 1x10{sup -9} to 1.3x10{sup -6} s). These internally generated gamma-quanta interact with the scintillator, and the resulting scintillation light is recorded by the photo-receiver. Since neutron sources are also strong sources of low-energy gamma-radiation, the use of dispersed ZnSe(Te) scintillator material provides high gamma-radiation detection efficiency in that energy range. This new type of gamma-neutron detector is based on a 'sandwich' structure using a ZnSe composite film and light guide with a fast neutron detection efficiency of about 6%. Its high detection efficiency of low-energy gamma-radiation allows a substantial increase (by an order of magnitude) in the efficiency of detection of neutron sources and transuranic materials by means of simultaneous detection of accompanying gamma-radiation. The design and fabrication technology of this detector allows the creation of gamma-neutron detectors characterized by high sensitivity at relatively low costs (as compared with analogs using oxide scintillators) for portable inspection systems. The sandwich structure can be comprised of any number of plates, with no limitations on thickness or area.« less

Portable multispectral fluorescence imaging system for food safety applications

NASA Astrophysics Data System (ADS)

Lefcourt, Alan M.; Kim, Moon S.; Chen, Yud-Ren

2004-03-01

Fluorescence can be a sensitive method for detecting food contaminants. Of particular interest is detection of fecal contamination as feces is the source of many pathogenic organisms. Feces generally contain chlorophyll a and related compounds due to ingestion of plant materials, and these compounds can readily be detected using fluorescence techniques. Described is a fluorescence-imaging system consisting primarily of a UV light source, an intensified camera with a six-position filter wheel, and software for controlling the system and automatically analyzing the resulting images. To validate the system, orchard apples artificially contaminated with dairy feces were used in a "hands-on" public demonstration. The contamination sites were easily identified using automated edge detection and threshold detection algorithms. In addition, by applying feces to apples and then washing sets of apples at hourly intervals, it was determined that five h was the minimum contact time that allowed identification of the contamination site after the apples were washed. There are many potential uses for this system, including studying the efficacy of apple washing systems.

Standoff detection of explosive molecules using nanosecond gated Raman spectroscopy

NASA Astrophysics Data System (ADS)

Chung, Jin Hyuk; Cho, Soo Gyeong

2013-06-01

Recently, improvised explosive device (IED) has been a serious threat for many countries. One of the approaches to alleviate this threat is standoff detection of explosive molecules used in IEDs. Raman spectroscopy is a prospective method among many technologies under research to achieve this goal. It provides unique information of the target materials, through which the ingredients used in IEDs can be analyzed and identified. The main problem of standoff Raman spectroscopic detection is the large background noise hindering weak Raman signals from the target samples. Typical background noise comes from both ambient fluorescent lights indoor and sunlight outdoor whose intensities are usually much larger than that of Raman scattering from the sample. Under the proper condition using pulse laser and ICCD camera with nanosecond pulse width and gating technology, we succeed to separate and remove these background noises from Raman signals. For this experiment, we build an optical system for standoff detection of explosive molecules. We use 532 nm, 10 Hz, Q-switching Nd:YAG laser as light source, and ICCD camera triggered by laser Qswitching time with proper gate delay regarding the flight time of Raman from target materials. Our detection system is successfully applied to detect and identify more than 20 ingredients of IEDs including TNT, RDX, and HMX which are located 10 to 54 meters away from the system.

Detection of microbial biofilms on food processing surfaces: Hyperspectral fluorescence imaging study

USDA-ARS?s Scientific Manuscript database

We used a portable hyperspectral fluorescence imaging system to evaluate biofilm formations on four types of food processing surface materials including stainless steel, polypropylene used for cutting boards, and household counter top materials such as formica and granite. The objective of this inve...

10 CFR 73.46 - Fixed site physical protection systems, subsystems, components, and procedures.

Code of Federal Regulations, 2014 CFR

2014-01-01

..., components, and procedures. 73.46 Section 73.46 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) PHYSICAL... Energy couriers engaged in the transport of special nuclear material. The search function for detection... of Energy vehicles engaged in transporting special nuclear material and emergency vehicles under...

10 CFR 73.46 - Fixed site physical protection systems, subsystems, components, and procedures.

Code of Federal Regulations, 2012 CFR

2012-01-01

..., components, and procedures. 73.46 Section 73.46 Energy NUCLEAR REGULATORY COMMISSION (CONTINUED) PHYSICAL... Energy couriers engaged in the transport of special nuclear material. The search function for detection... of Energy vehicles engaged in transporting special nuclear material and emergency vehicles under...

Defense Departmental Reporting System-Budgetary Was Not Effectively Implemented for the Army General Fund

DTIC Science & Technology

2012-05-31

or events. Unsupported journal vouchers increase the risk of materially misstated balances reported on the AGF financial statements. DFAS...with U.S. generally accepted accounting principles and that the Army automated systems did not support material amounts on the financial statements...files, abnormal balance detection , journal vouchers, and reconciliations between Army and OMB SF 133s and the Statements of Budgetary Resources

Portable Microleak-Detection System

NASA Technical Reports Server (NTRS)

Rivers, H. Kevin; Sikora, Joseph G.; Sankaran, Sankara N.

2007-01-01

The figure schematically depicts a portable microleak-detection system that has been built especially for use in testing hydrogen tanks made of polymer-matrix composite materials. (As used here, microleak signifies a leak that is too small to be detectable by the simple soap-bubble technique.) The system can also be used to test for microleaks in tanks that are made of other materials and that contain gases other than hydrogen. Results of calibration tests have shown that measurement errors are less than 10 percent for leak rates ranging from 0.3 to 200 cm3/min. Like some other microleak-detection systems, this system includes a vacuum pump and associated plumbing for sampling the leaking gas, and a mass spectrometer for analyzing the molecular constituents of the gas. The system includes a flexible vacuum chamber that can be attached to the outer surface of a tank or other object of interest that is to be tested for leakage (hereafter denoted, simply, the test object). The gas used in a test can be the gas or vapor (e.g., hydrogen in the original application) to be contained by the test object. Alternatively, following common practice in leak testing, helium can be used as a test gas. In either case, the mass spectrometer can be used to verify that the gas measured by the system is the test gas rather than a different gas and, hence, that the leak is indeed from the test object.

High contrast computed tomography with synchrotron radiation

NASA Astrophysics Data System (ADS)

Itai, Yuji; Takeda, Tohoru; Akatsuka, Takao; Maeda, Tomokazu; Hyodo, Kazuyuki; Uchida, Akira; Yuasa, Tetsuya; Kazama, Masahiro; Wu, Jin; Ando, Masami

1995-02-01

This article describes a new monochromatic x-ray CT system using synchrotron radiation with applications in biomedical diagnosis which is currently under development. The system is designed to provide clear images and to detect contrast materials at low concentration for the quantitative functional evaluation of organs in correspondence with their anatomical structures. In this system, with x-ray energy changing from 30 to 52 keV, images can be obtained to detect various contrast materials (iodine, barium, and gadolinium), and K-edge energy subtraction is applied. Herein, the features of the new system designed to enhance the advantages of SR are reported. With the introduction of a double-crystal monochromator, the high-order x-ray contamination is eliminated. The newly designed CCD detector with a wide dynamic range of 60 000:1 has a spatial resolution of 200 μm. The resulting image quality, which is expected to show improved contrast and spatial resolution, is currently under investigation.

Monitoring of human populations for early markers of cadmium toxicity: A review

DOE Office of Scientific and Technical Information (OSTI.GOV)

Fowler, Bruce A.

2009-08-01

Exposure of human populations to cadmium (Cd) from air, food and water may produce effects in organs such as the kidneys, liver, lungs, cardiovascular, immune and reproductive systems. Since Cd has been identified as a human carcinogen, biomarkers for early detection of susceptibility to cancer are of an importance to public health. The ability to document Cd exposure and uptake of this element through biological monitoring is a first step towards understanding its health effects. Interpretation and application of biological monitoring data for predicting human health outcomes require correlation with biological measures of organ system responses to the documented exposure.more » Essential to this understanding is the detection and linkage of early biological responses toxic effects in target cell populations. Fortunately, advances in cell biology have resulted in the development of pre-clinical biological markers (biomarkers) that demonstrate measurable and characteristic molecular changes in organ systems following chemical exposures that occur prior to the onset of overt clinical disease or development of cancer. Technical advances have rendered a number of these biomarkers practical for monitoring Cd-exposed human populations. Biomarkers will be increasingly important in relation to monitoring effects from the exposure to new Cd-based high technology materials. For example, cadmium-selenium (CdSe), nano-materials made from combinations of these elements have greatly altered cellular uptake characteristics due to particle size. These differences may greatly alter effects at the target cell level and hence risks for organ toxicities from such exposures. The value of validated biomarkers for early detection of systemic Cd-induced effects in humans cannot be underestimated due to the rapid expansion of nano-material technologies. This review will attempt to briefly summarize the applications, to date, of biomarker endpoints for assessing target organ system effects in humans and experimental systems from Cd exposure. Further, it will attempt to provide a prospective look at the possible future of biomarkers. The emphasis will be on the detection of early toxic effects from exposure to Cd in new products such as nano-materials and identification of populations at special risk for Cd toxicity.« less

Monitoring of human populations for early markers of cadmium toxicity: a review.

PubMed

Fowler, Bruce A

2009-08-01

Exposure of human populations to cadmium (Cd) from air, food and water may produce effects in organs such as the kidneys, liver, lungs, cardiovascular, immune and reproductive systems. Since Cd has been identified as a human carcinogen, biomarkers for early detection of susceptibility to cancer are of an importance to public health. The ability to document Cd exposure and uptake of this element through biological monitoring is a first step towards understanding its health effects. Interpretation and application of biological monitoring data for predicting human health outcomes require correlation with biological measures of organ system responses to the documented exposure. Essential to this understanding is the detection and linkage of early biological responses toxic effects in target cell populations. Fortunately, advances in cell biology have resulted in the development of pre-clinical biological markers (biomarkers) that demonstrate measurable and characteristic molecular changes in organ systems following chemical exposures that occur prior to the onset of overt clinical disease or development of cancer. Technical advances have rendered a number of these biomarkers practical for monitoring Cd-exposed human populations. Biomarkers will be increasingly important in relation to monitoring effects from the exposure to new Cd-based high technology materials. For example, cadmium-selenium (CdSe), nano-materials made from combinations of these elements have greatly altered cellular uptake characteristics due to particle size. These differences may greatly alter effects at the target cell level and hence risks for organ toxicities from such exposures. The value of validated biomarkers for early detection of systemic Cd-induced effects in humans cannot be underestimated due to the rapid expansion of nano-material technologies. This review will attempt to briefly summarize the applications, to date, of biomarker endpoints for assessing target organ system effects in humans and experimental systems from Cd exposure. Further, it will attempt to provide a prospective look at the possible future of biomarkers. The emphasis will be on the detection of early toxic effects from exposure to Cd in new products such as nano-materials and identification of populations at special risk for Cd toxicity.

New radiological material detection technologies for nuclear forensics: Remote optical imaging and graphene-based sensors.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Harrison, Richard Karl; Martin, Jeffrey B.; Wiemann, Dora K.

We developed new detector technologies to identify the presence of radioactive materials for nuclear forensics applications. First, we investigated an optical radiation detection technique based on imaging nitrogen fluorescence excited by ionizing radiation. We demonstrated optical detection in air under indoor and outdoor conditions for alpha particles and gamma radiation at distances up to 75 meters. We also contributed to the development of next generation systems and concepts that could enable remote detection at distances greater than 1 km, and originated a concept that could enable daytime operation of the technique. A second area of research was the development ofmore » room-temperature graphene-based sensors for radiation detection and measurement. In this project, we observed tunable optical and charged particle detection, and developed improved devices. With further development, the advancements described in this report could enable new capabilities for nuclear forensics applications.« less

Fluid leak indicator

NASA Technical Reports Server (NTRS)

Anderson, George E. (Inventor); Loo, Shu (Inventor)

1989-01-01

A fluid leak indicator (30) for detecting and indicating leaks in visually inaccessible fluid tubing joints (20, 21), such as those obstructed by insulation (24), includes a bag system (25) and a wicking system (30) surrounding or wrapping the joints (20, 21) under the visual obstructing material (24). Leaking fluid is collected in the bag (25) or on the wicking material (34) where it is conducted along the wicking material (34) to a visibly accessible capturing transparent indicator bulb (35) for providing a visual indication of the leak without requiring a chemical change in the capturing indicator bulb (35).

Detection of solid C(triple bond)N bearing materials on solar system bodies

NASA Technical Reports Server (NTRS)

Cruikshank, Dale P.; Hartmann, W. K.; Tholen, David J.; Allamandola, L. J.; Brown, R. H.; Matthews, C. N.; Bell, J. F.

1991-01-01

We found observational evidence for the presence of C(triple bond)N-bearing solid materials on four classes of Solar System bodies: comets, asteroids, the rings of Uranus, and Saturn's satellite Iapetus. Gaseous CN was known in comet spectra, and the IR spectra of Comet P/Halley show emission of the CN fundamental at 4.5 microns interpreted as solids containing CN- group in the grains of the inner coma. The presented data offer the first evidence for chemically related material on the other objects.

Ejection of rocky and icy material from binary star systems: implications for the origin and composition of 1I/`Oumuamua

NASA Astrophysics Data System (ADS)

Jackson, Alan P.; Tamayo, Daniel; Hammond, Noah; Ali-Dib, Mohamad; Rein, Hanno

2018-06-01

In single-star systems like our own Solar system, comets dominate the mass budget of bodies ejected into interstellar space, since they form further away and are less tightly bound. However, 1I/`Oumuamua, the first interstellar object detected, appears asteroidal in its spectra and lack of detectable activity. We argue that the galactic budget of interstellar objects like 1I/`Oumuamua should be dominated by planetesimal material ejected during planet formation in circumbinary systems, rather than in single-star systems or widely separated binaries. We further show that in circumbinary systems, rocky bodies should be ejected in comparable numbers to icy ones. This suggests that a substantial fraction of interstellar objects discovered in future should display an active coma. We find that the rocky population, of which 1I/`Oumuamua seems to be a member, should be predominantly sourced from A-type and late B-star binaries.

Chemical Sensors Based on Metal Oxide Nanostructures

NASA Technical Reports Server (NTRS)

Hunter, Gary W.; Xu, Jennifer C.; Evans, Laura J.; VanderWal, Randy L.; Berger, Gordon M.; Kulis, Mike J.; Liu, Chung-Chiun

2006-01-01

This paper is an overview of sensor development based on metal oxide nanostructures. While nanostructures such as nanorods show significan t potential as enabling materials for chemical sensors, a number of s ignificant technical challenges remain. The major issues addressed in this work revolve around the ability to make workable sensors. This paper discusses efforts to address three technical barriers related t o the application of nanostructures into sensor systems: 1) Improving contact of the nanostructured materials with electrodes in a microse nsor structure; 2) Controling nanostructure crystallinity to allow co ntrol of the detection mechanism; and 3) Widening the range of gases that can be detected by using different nanostructured materials. It is concluded that while this work demonstrates useful tools for furt her development, these are just the beginning steps towards realizati on of repeatable, controlled sensor systems using oxide based nanostr uctures.

Detection of errant laser beams

NASA Astrophysics Data System (ADS)

Taylor, Arthur F. D. S.; Edwards, Stanley A.; Barrett, J. A.; Bandle, Anthony M.

1990-10-01

The new generation of automated laser machine tools poses problems for those responsible for setting safety standards. While traditional safeguarding will frustrate full exploitation of this hybrid technology, wholesale abandonment of effective containment in favour of safety monitoring and control systems is unlikely to be acceptable. Long term, quantitative risk assessment will resolve this dilemma. Short term, guide lines will have to be derived from practical considerations of the laser facility design, materials, primary safety devices and procedures. Earlier risk assessments are reviewed relative to the emerging perspective of high average power laser installations. Aspects of extended beam delivery systems and equipment utilization and maintenance are examined to assess possible interaction with operational safety and in particular the potential to adversely influence errant laser beam occurrances (ELBO). To satisfy international safety standards for a laser enclosure which offers flexibility and is cost effective a detection system is described which continuously surveys the inside of the enclosure. Extensive trials have been carried out with high average power lasers (up to 10kW) where a range of engineering materials has been exposed to a laser beam. It is shown that the ratio of detection and shut down time to the burn through time can be an acceptable risk and thus indicate which materials will prove adequate.

Standoff detection: distinction of bacteria by hyperspectral laser induced fluorescence

NASA Astrophysics Data System (ADS)

Walter, Arne; Duschek, Frank; Fellner, Lea; Grünewald, Karin M.; Hausmann, Anita; Julich, Sandra; Pargmann, Carsten; Tomaso, Herbert; Handke, Jürgen

2016-05-01

Sensitive detection and rapid identification of hazardous bioorganic material with high sensitivity and specificity are essential topics for defense and security. A single method can hardly cover these requirements. While point sensors allow a highly specific identification, they only provide localized information and are comparatively slow. Laser based standoff systems allow almost real-time detection and classification of potentially hazardous material in a wide area and can provide information on how the aerosol may spread. The coupling of both methods may be a promising solution to optimize the acquisition and identification of hazardous substances. The capability of the outdoor LIF system at DLR Lampoldshausen test facility as an online classification tool has already been demonstrated. Here, we present promising data for further differentiation among bacteria. Bacteria species can express unique fluorescence spectra after excitation at 280 nm and 355 nm. Upon deactivation, the spectral features change depending on the deactivation method.

Anomaly Detection Techniques with Real Test Data from a Spinning Turbine Engine-Like Rotor

NASA Technical Reports Server (NTRS)

Abdul-Aziz, Ali; Woike, Mark R.; Oza, Nikunj C.; Matthews, Bryan L.

2012-01-01

Online detection techniques to monitor the health of rotating engine components are becoming increasingly attractive to aircraft engine manufacturers in order to increase safety of operation and lower maintenance costs. Health monitoring remains a challenge to easily implement, especially in the presence of scattered loading conditions, crack size, component geometry, and materials properties. The current trend, however, is to utilize noninvasive types of health monitoring or nondestructive techniques to detect hidden flaws and mini-cracks before any catastrophic event occurs. These techniques go further to evaluate material discontinuities and other anomalies that have grown to the level of critical defects that can lead to failure. Generally, health monitoring is highly dependent on sensor systems capable of performing in various engine environmental conditions and able to transmit a signal upon a predetermined crack length, while acting in a neutral form upon the overall performance of the engine system.

Intriguing differences and similarities in the surface compositions of the icy Saturnian and Galilean satellites

NASA Astrophysics Data System (ADS)

Hibbitts, C.

2006-12-01

Many materials in addition to water ice have been discovered in the surfaces of the icy Galilean and Saturnian satellites. Spacecraft infrared spectroscopy show intriguing differences and similarities suggestive of variations in primordial compositions and subsequent alteration. However, within the diverse compositions in their surfaces are similarities that cross between the systems. For instance, when nonice material is detected on these satellites, it is always hydrated. CO2 is detected in both systems where it is trapped in a host material except possibly for Enceladus where it may be deposited as ice from plumes [1-7]. Satellites in both systems contain aromatic hydrocarbons [8] and possibly CN-bearing materials [9]. The surfaces of Callisto, Ganymede, Europa, Iapetus, Phoebe, Hyperion, and Dione each contain some low albedo non-ice materials. The spectra have a broad 3-micron absorption feature due to structural OH or adsorbed water. However, the band is not sharp like a well-ordered clay mineral but broad, similar in some regards to less well-structured palagonite, goethite, or Murchison meteorite. The hydration of Jovian satellite nonice materials is greater for surfaces that have experienced more tectonism and alteration (i.e. increases from Callisto inward to Europa). The nonice material on Callisto appears to be a single composition (though itself possibly a mixture) that is slightly hydrated [10]. The nonice material on Europa is also of uniform composition everywhere observed, a very heavily hydrated material, perhaps a salt, hydrated SO4 (i.e. sulfuric acid), or both, that either originates from the subsurface ocean, radiolytically altered surface material, or both [11-13]. Ganymede appears to contain two types nonice materials; one an unidentified heavily hydrated material spectrally distinct from the Europa hydrate [11] and a second much less-abundant, less hydrated material spectrally similar to the Callisto nonice material that is largely associated with dark ray craters, possibly impactor contamination or desiccated Ganymede hydrate. The nonice materials on Phoebe and Iapetus is redder (from 1-2.5 microns) than the reddest material on the Galilean satellites (on Callisto) and compositionally different from each other. Iapetus appears to contain some (more) tholin material than Phoebe [14]. The CO2 on both satellites is similar to the CO2 detected in the nonice materials on Callisto and Ganymede with a reflectance minimum ~ 4.258 microns. The spectrum of the CO2 detected on Hyperion and Dione is distinct from that on Iapetus and Phoebe, having a reflectance minimum 10nm shorter at ~ 4.246 microns. This suggests a different bonding energy and possibly a different host material. In summary, the compositions of the icy Galilean satellites reflect the evolutionary state of their surfaces. The compositions of the icy Saturnian satellites are also complex, but with the exception of Enceladus, do not yet show any obvious dependencies on surface structure. There may some commonality in primordial compositions between the satellites of the two systems. References: [1]1Carlson et al., (1996) Science; [2] McCord et al., (1998) J. Geophys. Res.;[3] Hibbitts et al., (2000), J. Geophys. Res; [4] Hibbitts et al., (2003) J. Geophys. Res; [5] Clark et al., (2005) Nature; [6] Buratti et al., (2005) Astrophys. J.; [7] Brown et al., (2006) , Icarus; [8] Clark et al., (2005), Fall AGU; [9] Cruikshank et al., (2005), DPS [10] Calvin et al., (1991), Icarus; [11] McCord et al., 2000; [12]Carlson et al., 1999; [13]Orlando et al., (2005) Icarus; [14] Owens et al., (2001) Icarus;.

Simulations of Multi-Gamma Coincidences From Neutron-Induced Fission in Special Nuclear Materials

NASA Astrophysics Data System (ADS)

Kane, Steven; Gozani, Tsahi; King, Michael J.; Kwong, John; Brown, Craig; Gary, Charles; Firestone, Murray I.; Nikkel, James A.; McKinsey, Daniel N.

2013-04-01

A study is presented on the detection of illicit special nuclear materials (SNM) in cargo containers using a conceptual neutron-based inspection system with xenon-doped liquefied argon (LAr(Xe)) scintillation detectors for coincidence gamma-ray detection. For robustness, the system is envisioned to exploit all fission signatures, namely both prompt and delayed neutron and gamma emissions from fission reactions induced in SNM. However, this paper focuses exclusively on the analysis of the prompt gamma ray emissions. The inspection system probes a container using neutrons produced either by (d, D) or (d, T) in pulsed form or from an associated particle neutron generator to exploit the associated particle imaging (API) technique, thereby achieving background reduction and imaging. Simulated signal and background estimates were obtained in MCNPX (2.7) for a 2 kg sphere of enriched uranium positioned at the center of a 1m × 1m × 1m container, which is filled uniformly with wood or iron cargos at 0.1 g/cc or 0.4 g/cc. Detection time estimates are reported assuming probabilities of detection of 95% and false alarm of 0.5%.

Chemicapacitive microsensors for detection of explosives and TICs

NASA Astrophysics Data System (ADS)

Patel, Sanjay V.; Hobson, Stephen T.; Cemalovic, Sabina; Mlsna, Todd E.

2005-10-01

Seacoast Science develops chemical sensors that use polymer-coated micromachined capacitors to measure the dielectric permittivity of an array of selectively absorbing materials. We present recent results demonstrating the sensor technology's capability to detect components in explosives and toxic industrial chemicals. These target chemicals are detected with functionalized polymers or network materials, chosen for their ability to adsorb chemicals. When exposed to vapors or gases, the permittivity of these sorbent materials changes depending on the strength of the vapor-sorbent interaction. Sensor arrays made of ten microcapacitors on a single chip have been previously shown to detect vapors of organic compounds (chemical warfare agents, industrial solvents, fuels) and inorganic gases (SO2, CO2, NO2). Two silicon microcapacitor structures were used, one with parallel electrode plates and the other with interdigitated "finger-like" electrodes. The parallel-plates were approximately 300 μm wide and separated by 750 nm. The interdigitated electrodes were approximately 400 μm long and were elevated above the substrate to provide faster vapor access. Eight to sixteen of these capacitors are fabricated on chips that are 5 x 2 mm and are packaged in less than 50 cm3 with supporting electronics and batteries, all weighing less than 500 grams. The capacitors can be individually coated with different materials creating a small electronic nose that produces different selectivity patterns in response to different chemicals. The resulting system's compact size, low-power consumption and low manufacturing costs make the technology ideal for integration into various systems for numerous applications.

Small threat and contraband detection with TNA-based systems.

PubMed

Shaw, T J; Brown, D; D'Arcy, J; Liu, F; Shea, P; Sivakumar, M; Gozani, T

2005-01-01

The detection of small threats, such as explosives, drugs, and chemical weapons, concealed or encased in surrounding material, is a major concern in areas from security checkpoints to UneXploded Ordnance (UXO) clearance. Techniques such as X-ray and trace detection are often ineffectual in these applications. Thermal neutron analysis (TNA) provides an effective method for detecting concealed threats. This paper shows the effectiveness of Ancore's SPEDS, based on TNA, in detecting concealed liquid threats and differentiating live from inert mortar shells.

Nanowire-based detector

DOEpatents

Berggren, Karl K; Hu, Xiaolong; Masciarelli, Daniele

2014-06-24

Systems, articles, and methods are provided related to nanowire-based detectors, which can be used for light detection in, for example, single-photon detectors. In one aspect, a variety of detectors are provided, for example one including an electrically superconductive nanowire or nanowires constructed and arranged to interact with photons to produce a detectable signal. In another aspect, fabrication methods are provided, including techniques to precisely reproduce patterns in subsequently formed layers of material using a relatively small number of fabrication steps. By precisely reproducing patterns in multiple material layers, one can form electrically insulating materials and electrically conductive materials in shapes such that incoming photons are redirected toward a nearby electrically superconductive materials (e.g., electrically superconductive nanowire(s)). For example, one or more resonance structures (e.g., comprising an electrically insulating material), which can trap electromagnetic radiation within its boundaries, can be positioned proximate the nanowire(s). The resonance structure can include, at its boundaries, electrically conductive material positioned proximate the electrically superconductive nanowire such that light that would otherwise be transmitted through the sensor is redirected toward the nanowire(s) and detected. In addition, electrically conductive material can be positioned proximate the electrically superconductive nanowire (e.g. at the aperture of the resonant structure), such that light is directed by scattering from this structure into the nanowire.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shourbaji, AA

Oak Ridge National Laboratory conducted field radiological measurements at two port locations at the request of the Environmental Protection Agency (EPA). The radiological measurements were performed on five radiation detection systems at the port of Darrow, Louisiana and three systems at the port of Charleston, South Carolina. Darrow was visited on January 20-23, 2004 and Charleston on May 25, 2004. All tested systems are designed to detect radioactive material that might be present in scrap metals as the scrap is being unloaded from ships. All eight systems are commercially known as the Cricket and manufactured by RAD/COMM Systems. Each radiationmore » detection system consists of a detector with two channels and a wireless transmitter, both mounted on the grapple, and a controller located in the crane cab. The cranes at both locations are operated by the Cooper T. Smith Company. The purpose of the radiological measurements was to evaluate the performance of the radiation detection systems in terms of their ability to detect elevated radiation levels, and to develop a routine testing method for all EPA Cricket systems.« less

Combined Photoneutron And X Ray Interrogation Of Containers For Nuclear Materials

NASA Astrophysics Data System (ADS)

Gozani, Tsahi; Shaw, Timothy; King, Michael J.; Stevenson, John; Elsalim, Mashal; Brown, Craig; Condron, Cathie

2011-06-01

Effective cargo inspection systems for nuclear material detection require good penetration by the interrogating radiation, generation of a sufficient number of fissions, and strong and penetrating detection signatures. Inspection systems need also to be sensitive over a wide range of cargo types and densities encountered in daily commerce. Thus they need to be effective with highly hydrogenous cargo, where neutron attenuation is a major limitation, as well as with dense metallic cargo, where x-ray penetration is low. A system that interrogates cargo with both neutrons and x-rays can, in principle, achieve high performance over the widest range of cargos. Moreover, utilizing strong prompt-neutron (˜3 per fission) and delayed-gamma ray (˜7 per fission) signatures further strengthens the detection sensitivity across all cargo types. The complementary nature of x-rays and neutrons, used as both probing radiation and detection signatures, alleviates the need to employ exceedingly strong sources, which would otherwise be required to achieve adequate performance across all cargo types, if only one type of radiation probe were employed. A system based on the above principles, employing a commercially-available 9 MV linac was developed and designed. Neutrons are produced simultaneously with x-rays by the photonuclear interaction of the x-ray beam with a suitable converter. A total neutron yield on the order of 1011 n/s is achieved with an average electron beam current of 100 μA. If fissionable material is present, fissions are produced both by the high-energy x-ray beam and by the photoneutrons. Photofission and neutron fission dominate in hydrogenous and metallic cargos, respectively. Neutron-capture gamma rays provide information on the cargo composition. The prompt neutrons resulting from fission are detected by two independent detector systems: by very efficient Differential Die Away Analysis (DDAA) detectors, and by direct detection of neutrons with energies higher than 3 MeV using a recently developed fluorine-based threshold activation detector (TAD). The delayed gamma-ray signals are measured with high efficiency with the same TAD and with additional lower-cost plastic scintillators.

Characterizing the Atomic Structure in Low Concentrations of Weakly Ordered, Weakly Scattering Materials Using the Pair Distribution Function

NASA Astrophysics Data System (ADS)

Terban, Maxwell W.

Nanoscale structural characterization is critical to understanding the physical underpinnings of properties and behavior in materials with technological applications. The work herein shows how the pair distribution function technique can be applied to x-ray total scattering data for material systems which weakly scatter x-rays, a typically difficult task due to the poor signal-to-noise obtained from the structures of interest. Characterization and structural modeling are demonstrated for a variety of molecular and porous systems, along with the detection and characterization of disordered, minority phases and components. In particular, reliable detection and quantitative analysis are demonstrated for nanocrystals of an active pharmaceutical ingredient suspended in dilute solution down to a concentration of 0.25 wt. %, giving a practical limit of detection for ordered nanoscale phases within a disordered matrix. Further work shows that minority nanocrystalline phases can be detected, fingerprinted, and modeled for mixed crystalline and amorphous systems of small molecules and polymers. The crystallization of amorphous lactose is followed under accelerated aging conditions. Melt quenching is shown to produce a different local structure than spray drying or freeze drying, along with increased resistance to crystallization. The initial phases which form in the spray dried formulation are identified as a mixture of polymorphs different from the final alpha-lactose monohydrate form. Hard domain formation in thermoplastic polyurethanes is also characterized as a function of methylene diphenyl diisocyanate and butanediol component ratio, showing that distinct and different hard phase structures can form and are solved by indexing with structures derived from molecular dynamics relaxation. In both cases, phase fractions can be quantified in the mixed crystalline and amorphous systems by fitting with both standards or structure models. Later chapters, demonstrate pair distribution characterization of particle incorporation, structure, and synthesis of nanoporous materials. Nanoparticle size distributions are extracted from platinum nanoparticles nucleating within a zeolite matrix through structural modeling, and validated by transmission electron microscope studies. The structure of zirconium phosphonate-phosphate unconventional metal organic framework is determined to consist of turbostratically disordered nanocrystalline layers of Zr-phenylphosphonate, and the local environment of terbium intercalated between the layers is found to resemble the local environment in scheelite-type terbium phosphate. Finally, the early stages of reaction between aqueous zinc dinitrate hexahydrate and methanolic 2-methylimidazole are characterized using in situ total scattering measurements, showing that secondary building units of tetrahedrally coordinated by 2-methylimidazole initially form upon reaction. Overall, the methodologies are developed and applied toward phase detection, identification, solution, and behavior in pharmaceuticals, polymers, and nanoporous materials along with advice for carrying out experiments and analysis on such materials such that they can be extended to other similar systems.

Detecting Symptoms of Low Performance Using Production Rules

ERIC Educational Resources Information Center

Bravo, Javier; Ortigosa, Alvaro

2009-01-01

E-Learning systems offer students innovative and attractive ways of learning through augmentation or substitution of traditional lectures and exercises with online learning material. Such material can be accessed at any time from anywhere using different devices, and can be personalized according to the individual student's needs, goals and…

Field-deployable sniffer for 2,4-dinitrotoluene detection.

PubMed

Albert, K J; Myrick, M L; Brown, S B; James, D L; Milanovich, F P; Walt, D R

2001-08-01

A field-deployable instrument has been developed to detect low-level 2,4-dinitrotoluene (2,4-DNT) vapors. The system is based on previously developed artificial nose technology and employs an array of sensory materials attached to the distal tips of an optical fiber bundle. Both semiselective and nonspecific, cross-reactive sensors were employed. Each sensor within the array responds differentially to vapor exposure so the array's fluorescence response patterns are unique for each analyte. The instrument is computationally "trained" to discriminate target response patterns from nontarget and background environments. This detection system has been applied to detect 2,4-DNT, an analyte commonly detected on the soil surface above buried 2,4,6-trinitrotoluene (TNT) land mines, in spiked soil and aqueous and ground samples. The system has been characterized and demonstrated the ability to detect 120 ppb 2,4-DNT vapor in blind (unknown) humidified samples during a supervised field test.

Device and nondestructive method to determine subsurface micro-structure in dense materials

DOEpatents

Sun, Jiangang [Westmont, IL

2006-05-09

A method and a device to detect subsurface three-dimensional micro-structure in a sample by illuminating the sample with light of a given polarization and detecting light emanating from the sample that has a different direction of polarization by means of a confocal optical system.

Advances in developing rapid, reliable and portable detection systems for alcohol.

PubMed

Thungon, Phurpa Dema; Kakoti, Ankana; Ngashangva, Lightson; Goswami, Pranab

2017-11-15

Development of portable, reliable, sensitive, simple, and inexpensive detection system for alcohol has been an instinctive demand not only in traditional brewing, pharmaceutical, food and clinical industries but also in rapidly growing alcohol based fuel industries. Highly sensitive, selective, and reliable alcohol detections are currently amenable typically through the sophisticated instrument based analyses confined mostly to the state-of-art analytical laboratory facilities. With the growing demand of rapid and reliable alcohol detection systems, an all-round attempt has been made over the past decade encompassing various disciplines from basic and engineering sciences. Of late, the research for developing small-scale portable alcohol detection system has been accelerated with the advent of emerging miniaturization techniques, advanced materials and sensing platforms such as lab-on-chip, lab-on-CD, lab-on-paper etc. With these new inter-disciplinary approaches along with the support from the parallel knowledge growth on rapid detection systems being pursued for various targets, the progress on translating the proof-of-concepts to commercially viable and environment friendly portable alcohol detection systems is gaining pace. Here, we summarize the progress made over the years on the alcohol detection systems, with a focus on recent advancement towards developing portable, simple and efficient alcohol sensors. Copyright © 2017 Elsevier B.V. All rights reserved.

Defect mapping system

DOEpatents

Sopori, Bhushan L.

1995-01-01

Apparatus for detecting and mapping defects in the surfaces of polycrystalline materials in a manner that distinguishes dislocation pits from grain boundaries includes a laser for illuminating a wide spot on the surface of the material, a light integrating sphere with apertures for capturing light scattered by etched dislocation pits in an intermediate range away from specular reflection while allowing light scattered by etched grain boundaries in a near range from specular reflection to pass through, and optical detection devices for detecting and measuring intensities of the respective intermediate scattered light and near specular scattered light. A center blocking aperture or filter can be used to screen out specular reflected light, which would be reflected by nondefect portions of the polycrystalline material surface. An X-Y translation stage for mounting the polycrystalline material and signal processing and computer equipment accommodate rastor mapping, recording, and displaying of respective dislocation and grain boundary defect densities. A special etch procedure is included, which prepares the polycrystalline material surface to produce distinguishable intermediate and near specular light scattering in patterns that have statistical relevance to the dislocation and grain boundary defect densities.

Defect mapping system

DOEpatents

Sopori, B.L.

1995-04-11

Apparatus for detecting and mapping defects in the surfaces of polycrystalline materials in a manner that distinguishes dislocation pits from grain boundaries includes a laser for illuminating a wide spot on the surface of the material, a light integrating sphere with apertures for capturing light scattered by etched dislocation pits in an intermediate range away from specular reflection while allowing light scattered by etched grain boundaries in a near range from specular reflection to pass through, and optical detection devices for detecting and measuring intensities of the respective intermediate scattered light and near specular scattered light. A center blocking aperture or filter can be used to screen out specular reflected light, which would be reflected by nondefect portions of the polycrystalline material surface. An X-Y translation stage for mounting the polycrystalline material and signal processing and computer equipment accommodate rastor mapping, recording, and displaying of respective dislocation and grain boundary defect densities. A special etch procedure is included, which prepares the polycrystalline material surface to produce distinguishable intermediate and near specular light scattering in patterns that have statistical relevance to the dislocation and grain boundary defect densities. 20 figures.

A sensitive, selective, and portable detector for contraband: The compact integrated narcotics detection instrument

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tuemer, T.O.; Doan, L.; Su, C.W.

2000-07-01

A Compact Integrated Narcotics Detection Instrument (CINDI) has been developed at NOVA R and D, Inc., in cooperation with the US Coast Guard. This detector utilizes neutrons emitted from {sup 252}Cf. Neutrons emitted from the front face of CINDI penetrate dense compartment barrier materials with little change in energy but are backscattered by hydrogen-rich materials such as drugs. The backscattered neutrons are detected, and the rate is displayed by a microprocessor-controller integrated into CINDI. The operator guides the detector along a suspected area and receives immediate feedback from the state-of-the-art electronics. For user safety, the device incorporates a highly sensitivemore » detection scheme to permit the use of a very weak radioactive source, without compromising detectability. CINDI is capable of detecting narcotics effectively behind panels made of steel, wood, fiberglass, or even lead-lined materials. This makes it useful for inspecting marine vessels, ship bulkheads, automobiles, structure walls, or small sealed containers. Figure 2 shows three views of the CINDI instrument. CINDI responds strongly to hydrogen-rich materials such as narcotics. It has been tested at NOVA, the US Coast Guard, and Brewt Power Systems. The results of the tests show excellent response and specificity to narcotics. CINDI has led to a new technology that shows promise for identifying the concealed contraband. The new technique uses a fusion of two independent but complementary signals for detecting and possibly identifying concealed drugs in a variety of carriers such as vehicles, marine vessels, airplanes, containers, cargo, and luggage. The carriers will be scanned using both neutron and gamma-ray sources. The signal from both the neutron and gamma-ray backscattering and/or transmission can be used simultaneously to detect and possibly identify the contrabands it has been trained for. A system that can produce three-dimensional images for both signals may also be developed. The two images may be combined and analyzed by a fast host computer to detect concealed contraband. The two independent signatures when analyzed simultaneously may help determine the type of concealed contraband.« less

Technical approaches to reducing the threat of nuclear terrorism

NASA Astrophysics Data System (ADS)

Priedhorsky, William C.

2005-04-01

The threat of a nuclear attack on the United States by terrorists using a smuggled weapon is now considered more likely than an attack by a nuclear-armed ballistic missle. Consequently it is important to understand what can be done to detect and intercept a nuclear weapon being smuggled into the United States. A significant quantity of smuggled nuclear material has been intercepted already, but science and technology have so far contributed little to its interception. The critical special nuclear materials, plutonium and highly enriched uranium, are only weakly radioactive and detection of their radioactivity is limited both by atmospheric attenuation and by competition with natural backgrounds. Although many schemes for long-range detection of radioactivity have been proposed, none so far appears feasible. Detection of nuclear radiation can be improved using new technologies and sensing systems, but it will still be possible only at relatively small distances. Consequently the best approach to containing dangerous nuclear materials is at their sources; containment within lengthy borders and large areas is extremely difficult.

Spectroscopy from Space

NASA Astrophysics Data System (ADS)

Clark, R. N.; Swayze, G. A.; Carlson, R.; Grundy, W.; Noll, K.

2014-01-01

This chapter reviews detection of materials on solid and liquid (lakes and ocean) surfaces in the solar system using ultraviolet to infrared spectroscopy from space, or near space (high altitude aircraft on the Earth), or in the case of remote objects, earth-based and earth-orbiting telescopes. Point spectrometers and imaging spectrometers have been probing the surfaces of our solar system for decades. Spacecraft carrying imaging spectrometers are currently in orbit around Mercury, Venus, Earth, Mars, and Saturn, and systems have recently visited Jupiter, comets, asteroids, and one spectrometer-carrying spacecraft is on its way to Pluto. Together these systems are providing a wealth of data that will enable a better understanding of the composition of condensed matter bodies in the solar system. Minerals, ices, liquids, and other materials have been detected and mapped on the Earth and all planets and/or their satellites where the surface can be observed from space, with the exception of Venus whose thick atmosphere limits surface observation. Basaltic minerals (e.g., pyroxene and olivine) have been detected with spectroscopy on the Earth, Moon, Mars and some asteroids. The greatest mineralogic diversity seen from space is observed on the Earth and Mars. The Earth, with oceans, active tectonic and hydrologic cycles, and biological processes, displays the greatest material diversity including the detection of amorphous and crystalline inorganic materials, organic compounds, water and water ice. Water ice is a very common mineral throughout the Solar System and has been unambiguously detected or inferred in every planet and/or their moon(s) where good spectroscopic data has been obtained. In addition to water ice, other molecular solids have been observed in the solar system using spectroscopic methods. Solid carbon dioxide is found on all systems beyond the Earth except Pluto, although CO2 sometimes appears to be trapped in other solids rather than as an ice on some objects. The largest deposits of carbon dioxide ice are found on Mars. Sulfur dioxide ice is found in the Jupiter system. Nitrogen and methane ices are common beyond the Uranian system. Saturn's moon Titan probably has the most complex active extra-terrestrial surface chemistry involving organic compounds. Some of the observed or inferred compounds include ices of benzene (C6H6), cyanoacetylene (HC3N), toluene (C7H8), cyanogen (C2N2), acetonitrile (CH3CN), water (H2O), carbon dioxide (CO2), and ammonia (NH3). Confirming compounds on Titan is hampered by its thick smoggy atmosphere, where in relative terms the atmospheric interferences that hamper surface characterization lie between that of Venus and Earth. In this chapter we exclude discussion of the planets Jupiter, Saturn, Uranus, and Neptune because their thick atmospheres preclude observing the surface, even if surfaces exist. However, we do discuss spectroscopic observations on a number of the extra-terrestrial satellite bodies. Ammonia was predicted on many icy moons but is notably absent among the definitively detected ices with possible exceptions on Charon and possible trace amounts on some of the Saturnian satellites. Comets, storehouses of many compounds that could exist as ices in their nuclei, have only had small amounts of water ice definitively detected on their surfaces from spectroscopy. Only two asteroids have had a direct detection of surface water ice, although its presence can be inferred in others.

SNM detection with an optimized water Cherenkov neutron detector

NASA Astrophysics Data System (ADS)

Dazeley, S.; Sweany, M.; Bernstein, A.

2012-11-01

Special Nuclear Material (SNM) can either spontaneously fission or be induced to do so: either case results in neutron emission. For this reason, neutron detection performs a crucial role in the functionality of Radiation Portal Monitoring (RPM) devices. Since neutrons are highly penetrating and difficult to shield, they could potentially be detected escaping even a well-shielded cargo container. If the shielding were sophisticated, detecting escaping neutrons would require a highly efficient detector with close to full solid angle coverage. In 2008, we reported the successful detection of neutrons with a 250 liter (l) gadolinium doped water Cherenkov prototype [1]—a technology that could potentially be employed cost effectively with full solid angle coverage. More recently we have built and tested both 1-kl and 3.5-kl versions [2], demonstrating that very large, cost effective, non-flammable and environmentally benign neutron detectors can be operated efficiently without being overwhelmed by background. In this paper, we present a new design for a modular system of water-based neutron detectors that could be deployed as a real RPM. The modules contain a number of optimizations that have not previously been combined within a single system. We present simulations of the new system, based on the performance of our previous detectors. Our simulations indicate that an optimized system such as is presented here could achieve SNM sensitivity competitive with a large 3He-based system. Moreover, the realization of large, cost effective neutron detectors could, for the first time, enable the detection of multiple neutrons per fission from within a large object such as a cargo container. Such a signal would provide a robust indication of the presence of fissioning material, reducing the frequency of false alarms while increasing sensitivity.

SNM Detection with an Optimized Water Cherenkov Neutron Detector

DOE PAGES

Dazeley, S.; Sweany, M.; Bernstein, A.

2012-07-23

Special Nuclear Material (SNM) can either spontaneously fission or be induced to do so: either case results in neutron emission. For this reason, neutron detection performs a crucial role in the functionality of Radiation Portal Monitoring (RPM) devices. Since neutrons are highly penetrating and difficult to shield, they could potentially be detected escaping even a well-shielded cargo container. If the shielding were sophisticated, detecting escaping neutrons would require a highly efficient detector with close to full solid angle coverage. In 2008, we reported the successful detection of neutrons with a 250 liter (l) gadolinium doped water Cherenkov prototype—a technology thatmore » could potentially be employed cost effectively with full solid angle coverage. More recently we have built and tested both 1-kl and 3.5-kl versions, demonstrating that very large, cost effective, non-flammable and environmentally benign neutron detectors can be operated efficiently without being overwhelmed by background. In our paper, we present a new design for a modular system of water-based neutron detectors that could be deployed as a real RPM. The modules contain a number of optimizations that have not previously been combined within a single system. We present simulations of the new system, based on the performance of our previous detectors. These simulations indicate that an optimized system such as is presented here could achieve SNM sensitivity competitive with a large 3He-based system. Moreover, the realization of large, cost effective neutron detectors could, for the first time, enable the detection of multiple neutrons per fission from within a large object such as a cargo container. Such a signal would provide a robust indication of the presence of fissioning material, reducing the frequency of false alarms while increasing sensitivity.« less

Optical demodulation system for digitally encoded suspension array in fluoroimmunoassay

NASA Astrophysics Data System (ADS)

He, Qinghua; Li, Dongmei; He, Yonghong; Guan, Tian; Zhang, Yilong; Shen, Zhiyuan; Chen, Xuejing; Liu, Siyu; Lu, Bangrong; Ji, Yanhong

2017-09-01

A laser-induced breakdown spectroscopy and fluorescence spectroscopy-coupled optical system is reported to demodulate digitally encoded suspension array in fluoroimmunoassay. It takes advantage of the plasma emissions of assembled elemental materials to digitally decode the suspension array, providing a more stable and accurate recognition to target biomolecules. By separating the decoding procedure of suspension array and adsorption quantity calculation of biomolecules into two independent channels, the cross talk between decoding and label signals in traditional methods had been successfully avoided, which promoted the accuracy of both processes and realized more sensitive quantitative detection of target biomolecules. We carried a multiplexed detection of several types of anti-IgG to verify the quantitative analysis performance of the system. A limit of detection of 1.48×10-10 M was achieved, demonstrating the detection sensitivity of the optical demodulation system.

Cargo Container Imaging with Gaseous Detectors

NASA Astrophysics Data System (ADS)

Forest, Tony

2006-10-01

The gas electron multiplier (GEM) , developed at CERN by Fabio Sauli, represents the latest innovation in micropattern gaseous detectors and has been utilized as a preamplification stage in applications ranging from fundamental physics experiments to medical imaging. Although cargo container inspection systems are currently in place using gamma-rays or X-rays, they are predominantly designed with a resolution to detect contraband. Current imaging systems also suffer from false alarms due to naturally radioactive cargo when radiation portal monitors are used for passive detection of nuclear materials. Detection of small shielded radioactive elements is even more problematic. Idaho State University has been developing a system to image cargo containers in order to detect small shielded radioactive cargo. The possible application of an imaging system with gas electron multiplication will be shown along with preliminary images using gaseous detectors instead of the scintillators currently in use.

Superconductivity up to 114 K in the Bi-Al-Ca-Sr-Cu-O compound system without rare-earth elements

NASA Technical Reports Server (NTRS)

Chu, C. W.; Bechtold, J.; Gao, L.; Hor, P. H.; Huang, Z. J.

1988-01-01

Stable superconductivity up to 114 K has been reproducibly detected in Bi-Al-Ca-Sr-Cu-O multiphase systems without any rare-earth elements. Pressure has only a slight positive effect on T(c). These observations provide an extra material base for the study of the mechanism of high-temperature superconductivity and also the prospect of reduced material cost for future applications of superconductivity.

Analysis of cured carbon-phenolic decomposition products to investigate the thermal decomposition of nozzle materials

NASA Technical Reports Server (NTRS)

Thompson, James M.; Daniel, Janice D.

1989-01-01

The development of a mass spectrometer/thermal analyzer/computer (MS/TA/Computer) system capable of providing simultaneous thermogravimetry (TG), differential thermal analysis (DTA), derivative thermogravimetry (DTG) and evolved gas detection and analysis (EGD and EGA) under both atmospheric and high pressure conditions is described. The combined system was used to study the thermal decomposition of the nozzle material that constitutes the throat of the solid rocket boosters (SRB).

Search for Extralunar Materials in Apollo Soil Samples

NASA Astrophysics Data System (ADS)

Lucey, P. G.; Honniball, C.; Crites, S.; Taylor, G. J.; Martel, L.

2017-12-01

It has long been proposed that the lunar surface is a pristine collector of material from across the solar system. The Moon is exposed to the same meteorite flux as the Earth, but because its surface is unaltered by processes such as plate tectonics, aqueous alteration, or recent volcanism, the Moon may have recorded a much longer meteoritic history than the chemically and physically active Earth. By studying lunar soils at the individual grain level, we have the potential to identify and study material from across the inner solar system. We have developed three hyperspectral imaging microscopes to search a large quantity of lunar soil grains for rare lunar, and extra-lunar minerals. We are using lunar-exotic mineralogy as a tracer to detect extralunar candidates. One hyperspectral microscope covers the 1-2.5 micron region for detection of water and hydroxyl overtones in alteration minerals such as phyllosilicates. The second instrument covers the 2.5 to 5 micron region to characterize the 3 micron water region, and for detection of organics and carbonates. The third covers the thermal infrared for detection of phosphates and zeolites as well as the major lunar silicates. We are examining 1 million grains of varying sizes from Apollo 11 ,12, 14 and 16 landing sites. Using the USGS spectral library and the Tetracorder mineral mapping algorithm, we are matching library mineral spectra with the grain spectra we acquire. To validate our ability to detect and match mineral spectra, we are conducting scans of relevent mineral seperates and mixtures at the individual grain level. Results of this mineral inventory will provide contraints on various models and estimates for material transfer between the terrestrial planets.

Liquefied Noble Gas (LNG) detectors for detection of nuclear materials

NASA Astrophysics Data System (ADS)

Nikkel, J. A.; Gozani, T.; Brown, C.; Kwong, J.; McKinsey, D. N.; Shin, Y.; Kane, S.; Gary, C.; Firestone, M.

2012-03-01

Liquefied-noble-gas (LNG) detectors offer, in principle, very good energy resolution for both neutrons and gamma rays, fast response time (hence high-count-rate capabilities), excellent discrimination between neutrons and gamma rays, and scalability to large volumes. They do, however, need cryogenics. LNG detectors in sizes of interest for fissionable material detection in cargo are reaching a certain level of maturity because of the ongoing extensive R&}D effort in high-energy physics regarding their use in the search for dark matter and neutrinoless double beta decay. The unique properties of LNG detectors, especially those using Liquid Argon (LAr) and Liquid Xenon (LXe), call for a study to determine their suitability for Non-Intrusive Inspection (NII) for Special Nuclear Materials (SNM) and possibly for other threats in cargo. Rapiscan Systems Laboratory, Yale University Physics Department, and Adelphi Technology are collaborating in the investigation of the suitability of LAr as a scintillation material for large size inspection systems for air and maritime containers and trucks. This program studies their suitability for NII, determines their potential uses, determines what improvements in performance they offer and recommends changes to their design to further enhance their suitability. An existing 3.1 liter LAr detector (microCLEAN) at Yale University, developed for R&}D on the detection of weakly interacting massive particles (WIMPs) was employed for testing. A larger version of this detector (15 liters), more suitable for the detection of higher energy gamma rays and neutrons is being built for experimental evaluation. Results of measurements and simulations of gamma ray and neutron detection in microCLEAN and a larger detector (326 liter CL38) are presented.

Entanglement of remote material qubits through nonexciting interaction with single photons

NASA Astrophysics Data System (ADS)

Li, Gang; Zhang, Pengfei; Zhang, Tiancai

2018-05-01

We propose a scheme to entangle multiple material qubits through interaction with single photons via nonexciting processes associated with strongly coupling systems. The basic idea is based on the material state dependent reflection and transmission for the input photons. Thus, the material qubits in several systems can be entangled when one photon interacts with each system in cascade and the photon paths are mixed by the photon detection. The character of nonexciting of material qubits does not change the state of the material qubit and thus ensures the possibility of purifying entangled states by using more photons under realistic imperfect parameters. It also guarantees directly scaling up the scheme to entangle more qubits. Detailed analysis of fidelity and success probability of the scheme in the frame of an optical Fabry-Pérot cavity based strongly coupling system is presented. It is shown that a two-qubit entangled state with fidelity above 0.99 is promised with only two photons by using currently feasible experimental parameters. Our scheme can also be directly implemented on other strongly coupled system.

Actuation of chitosan-aptamer nanobrush borders for pathogen sensing.

PubMed

Hills, Katherine D; Oliveira, Daniela A; Cavallaro, Nicholas D; Gomes, Carmen L; McLamore, Eric S

2018-03-26

We demonstrate a sensing mechanism for rapid detection of Listeria monocytogenes in food samples using the actuation of chitosan-aptamer nanobrush borders. The bio-inspired soft material and sensing strategy mimic natural symbiotic systems, where low levels of bacteria are selectively captured from complex matrices. To engineer this biomimetic system, we first develop reduced graphene oxide/nanoplatinum (rGO-nPt) electrodes, and characterize the fundamental electrochemical behavior in the presence and absence of chitosan nanobrushes during actuation (pH-stimulated osmotic swelling). We then characterize the electrochemical behavior of the nanobrush when receptors (antibodies or DNA aptamers) are conjugated to the surface. Finally, we test various techniques to determine the most efficient capture strategy based on nanobrush actuation, and then apply the biosensors in a food product. Maximum cell capture occurs when aptamers conjugated to the nanobrush bind cells in the extended conformation (pH < 6), followed by impedance measurement in the collapsed nanobrush conformation (pH > 6). The aptamer-nanobrush hybrid material was more efficient than the antibody-nanobrush material, which was likely due to the relatively high adsorption capacity for aptamers. The biomimetic material was used to develop a rapid test (17 min) for selectively detecting L. monocytogenes at concentrations ranging from 9 to 107 CFU mL-1 with no pre-concentration, and in the presence of other Gram-positive cells (Listeria innocua and Staphylococcus aureus). Use of this bio-inspired material is among the most efficient for L. monocytogenes sensing to date, and does not require sample pretreatment, making nanobrush borders a promising new material for rapid pathogen detection in food.

Fluorescent scanning x-ray tomography with synchrotron radiation

NASA Astrophysics Data System (ADS)

Takeda, Tohoru; Maeda, Toshikazu; Yuasa, Tetsuya; Akatsuka, Takao; Ito, Tatsuo; Kishi, Kenichi; Wu, Jin; Kazama, Masahiro; Hyodo, Kazuyuki; Itai, Yuji

1995-02-01

Fluorescent scanning (FS) x-ray tomography was developed to detect nonradioactive tracer materials (iodine and gadolinium) in a living object. FS x-ray tomography consists of a silicon (111) channel cut monochromator, an x-ray shutter, an x-ray slit system and a collimator for detection, a scanning table for the target organ, and an x-ray detector with pure germanium. The minimal detectable dose of iodine in this experiment was 100 ng in a volume of 2 mm3 and a linear relationship was shown between the photon counts of a fluorescent x ray and the concentration of iodine contrast material. A FS x-ray tomographic image was clearly obtained with a phantom.

Error Detection in Mechanized Classification Systems

ERIC Educational Resources Information Center

Hoyle, W. G.

1976-01-01

When documentary material is indexed by a mechanized classification system, and the results judged by trained professionals, the number of documents in disagreement, after suitable adjustment, defines the error rate of the system. In a test case disagreement was 22 percent and, of this 22 percent, the computer correctly identified two-thirds of…

DOE Office of Scientific and Technical Information (OSTI.GOV)

Shedlock, Daniel; Dugan, Edward T.; Jacobs, Alan M.

X-ray backscatter radiography by selective detection (RSD) is a field tested and innovative approach to non-destructive evaluation (NDE). RSD is an enhanced single-side x-ray Compton backscatter imaging (CBI) technique which selectively detects scatter components to improve image contrast and quality. Scatter component selection is accomplished through a set of specially designed detectors with fixed and movable collimators. Experimental results have shown that this NDE technique can be used to detect boric acid deposition on a metallic plate through steel foil reflective insulation commonly covering reactor pressure vessels. The current system is capable of detecting boric acid deposits with sub-millimeter resolution,more » through such insulating materials. Industrial systems have been built for Lockheed Martin Space Co. and NASA. Currently the x-ray backscatter RSD scanning systems developed by the University of Florida are being used to inspect the spray-on foam insulation (SOFI) used on the external tank of the space shuttle. RSD inspection techniques have found subsurface cracking in the SOFI thought to be responsible for the foam debris which separated from the external tank during the last shuttle launch. These industrial scanning systems can be customized for many applications, and a smaller, lighter, more compact unit design is being developed. The smaller design is approximately four inches wide, three inches high, and about 12 inches in length. This smaller RSD system can be used for NDE of areas that cannot be reached with larger equipment. X-ray backscatter RSD is a proven technology that has been tested on a wide variety of materials and applications. Currently the system has been used to inspect materials such as aluminum, plastics, honeycomb laminates, reinforced carbon composites, steel, and titanium. The focus of RSD is for one-sided detection for applications where conventional non-destructive examination methods either will not work or give poor results. Acquired images have clearly shown, for a variety of conditions, that proper selection of x-ray field scatter components leads to a significant improvement in image quality and contrast. Improvements are significant enough in some cases that objects not visible to conventional CBI or transmission radiography become readily discernable with RSD. (authors)« less

The Use of Fast Neutron Detection for Materials Accountability

NASA Astrophysics Data System (ADS)

Nakae, L. F.; Chapline, G. F.; Glenn, A. M.; Kerr, P. L.; Kim, K. S.; Ouedraogo, S. A.; Prasad, M. K.; Sheets, S. A.; Snyderman, N. J.; Verbeke, J. M.; Wurtz, R. E.

2014-02-01

For many years at LLNL, we have been developing time-correlated neutron detection techniques and algorithms for applications such as Arms Control, Threat Detection and Nuclear Material Assay. Many of our techniques have been developed specifically for the relatively low efficiency (a few percent) inherent in man-portable systems. Historically, thermal neutron detectors (mainly 3He) were used, taking advantage of the high thermal neutron interaction cross-sections, but more recently we have been investigating the use of fast neutron detection with liquid scintillators, inorganic crystals, and in the near future, pulse-shape discriminating plastics that respond over 1000 times faster (nanoseconds versus tens of microseconds) than thermal neutron detectors. Fast neutron detection offers considerable advantages, since the inherent nanosecond production timescales of fission and neutron-induced fission are preserved and measured instead of being lost in the thermalization of thermal neutron detectors. We are now applying fast neutron technology to the safeguards regime in the form of high efficiency counters. Faster detector response times and sensitivity to neutron momentum show promise in measuring, differentiating, and assaying samples that have modest to very high count rates, as well as mixed neutron sources (e.g., Pu oxide or Mixed Cm and Pu). Here we report on measured results with our existing liquid scintillator array and promote the design of a nuclear material assay system that incorporates fast neutron detection, including the surprising result that fast liquid scintillator becomes competitive and even surpasses the precision of 3He counters measuring correlated pairs in modest (kg) samples of plutonium.

Detection of rabbit and hare processed material in compound feeds by TaqMan real-time PCR.

PubMed

Pegels, N; López-Calleja, I; García, T; Martín, R; González, I

2013-01-01

Food and feed traceability has become a priority for governments due to consumer demand for comprehensive and integrated safety policies. In the present work, a TaqMan real-time PCR assay targeting the mitochondrial 12S rRNA gene was developed for specific detection of rabbit and hare material in animal feeds and pet foods. The technique is based on the use of three species-specific primer/probe detection systems targeting three 12S rRNA gene fragments: one from rabbit species, another one from hare species and a third fragment common to rabbit and hare (62, 102 and 75 bp length, respectively). A nuclear 18S rRNA PCR system, detecting a 77-bp amplicon, was used as positive amplification control. Assay performance and sensitivity were assessed through the analysis of a batch of laboratory-scale feeds treated at 133°C at 3 bar for 20 min to reproduce feed processing conditions dictated by European regulations. Successful detection of highly degraded rabbit and hare material was achieved at the lowest target concentration assayed (0.1%). Furthermore, the method was applied to 96 processed commercial pet food products to determine whether correct labelling had been used at the market level. The reported real-time PCR technique detected the presence of rabbit tissues in 80 of the 96 samples analysed (83.3%), indicating a possible labelling fraud in some pet foods. The real-time PCR method reported may be a useful tool for traceability purposes within the framework of feed control.

Calibration and testing of a Raman hyperspectral imaging system to reveal powdered food adulteration

PubMed Central

Lohumi, Santosh; Lee, Hoonsoo; Kim, Moon S.; Qin, Jianwei; Kandpal, Lalit Mohan; Bae, Hyungjin; Rahman, Anisur

2018-01-01

The potential adulteration of foodstuffs has led to increasing concern regarding food safety and security, in particular for powdered food products where cheap ground materials or hazardous chemicals can be added to increase the quantity of powder or to obtain the desired aesthetic quality. Due to the resulting potential health threat to consumers, the development of a fast, label-free, and non-invasive technique for the detection of adulteration over a wide range of food products is necessary. We therefore report the development of a rapid Raman hyperspectral imaging technique for the detection of food adulteration and for authenticity analysis. The Raman hyperspectral imaging system comprises of a custom designed laser illumination system, sensing module, and a software interface. Laser illumination system generates a 785 nm laser line of high power, and the Gaussian like intensity distribution of laser beam is shaped by incorporating an engineered diffuser. The sensing module utilize Rayleigh filters, imaging spectrometer, and detector for collection of the Raman scattering signals along the laser line. A custom-built software to acquire Raman hyperspectral images which also facilitate the real time visualization of Raman chemical images of scanned samples. The developed system was employed for the simultaneous detection of Sudan dye and Congo red dye adulteration in paprika powder, and benzoyl peroxide and alloxan monohydrate adulteration in wheat flour at six different concentrations (w/w) from 0.05 to 1%. The collected Raman imaging data of the adulterated samples were analyzed to visualize and detect the adulterant concentrations by generating a binary image for each individual adulterant material. The results obtained based on the Raman chemical images of adulterants showed a strong correlation (R>0.98) between added and pixel based calculated concentration of adulterant materials. This developed Raman imaging system thus, can be considered as a powerful analytical technique for the quality and authenticity analysis of food products. PMID:29708973

Calibration and testing of a Raman hyperspectral imaging system to reveal powdered food adulteration.

PubMed

Lohumi, Santosh; Lee, Hoonsoo; Kim, Moon S; Qin, Jianwei; Kandpal, Lalit Mohan; Bae, Hyungjin; Rahman, Anisur; Cho, Byoung-Kwan

2018-01-01

The potential adulteration of foodstuffs has led to increasing concern regarding food safety and security, in particular for powdered food products where cheap ground materials or hazardous chemicals can be added to increase the quantity of powder or to obtain the desired aesthetic quality. Due to the resulting potential health threat to consumers, the development of a fast, label-free, and non-invasive technique for the detection of adulteration over a wide range of food products is necessary. We therefore report the development of a rapid Raman hyperspectral imaging technique for the detection of food adulteration and for authenticity analysis. The Raman hyperspectral imaging system comprises of a custom designed laser illumination system, sensing module, and a software interface. Laser illumination system generates a 785 nm laser line of high power, and the Gaussian like intensity distribution of laser beam is shaped by incorporating an engineered diffuser. The sensing module utilize Rayleigh filters, imaging spectrometer, and detector for collection of the Raman scattering signals along the laser line. A custom-built software to acquire Raman hyperspectral images which also facilitate the real time visualization of Raman chemical images of scanned samples. The developed system was employed for the simultaneous detection of Sudan dye and Congo red dye adulteration in paprika powder, and benzoyl peroxide and alloxan monohydrate adulteration in wheat flour at six different concentrations (w/w) from 0.05 to 1%. The collected Raman imaging data of the adulterated samples were analyzed to visualize and detect the adulterant concentrations by generating a binary image for each individual adulterant material. The results obtained based on the Raman chemical images of adulterants showed a strong correlation (R>0.98) between added and pixel based calculated concentration of adulterant materials. This developed Raman imaging system thus, can be considered as a powerful analytical technique for the quality and authenticity analysis of food products.

Performance status of a small robot-mounted or hand-held, solar-blind, standoff chemical, biological, and explosives (CBE) sensor

NASA Astrophysics Data System (ADS)

Hug, W. F.; Reid, R. D.; Bhartia, R.; Lane, A. L.

2009-05-01

Photon Systems and JPL are continuing development of a new technology robot-mounted or hand-held sensor for reagentless, short-range, standoff detection and identification of trace levels CBE materials on surfaces. This deep ultraviolet CBE sensor is the result of ongoing Army STTR and DTRA programs. The evolving 6 lb, 15W, lantern-size sensor can discriminate CBE from background clutter materials using a combination of deep UV excited resonance Raman (RR) and laser induced native fluorescence (LINF) emissions resulting from excitation by a new technology deep UV laser. Standoff excitation of suspicious packages, vehicles, persons, and other objects that may contain hazardous materials is accomplished using wavelengths below 250nm where RR and LINF emissions occupy distinctly different wavelength regions. This enables simultaneous detection of RR and LINF emissions with no spectral overlap or interference of LINF over RR or RR over LINF. The new eye-safe targeted ultraviolet chemical, biological, and explosives (TUCBE) sensor can detect and identify less than 1 μg/cm2 of explosives or 104 bacterial spores at 10 meters standoff, or 10 ng/cm2 of explosives or 102 bacterial spores/cm2 at 1 meter standoff. Detection and identification requires less than 1 ms and has a sample rate up to 20 Hz. Lower concentrations of contamination can be detected and identified as closer ranges and higher concentrations at longer ranges. The sensor is solar blind and can be operated in full daylight conditions as a result of excitation and detection in the deep UV and the use of a gated detection system.

Performance of Integrated Fiber Optic, Piezoelectric, and Shape Memory Alloy Actuators/Sensors in Thermoset Composites

NASA Technical Reports Server (NTRS)

Trottier, C. Michael

1996-01-01

Recently, scientists and engineers have investigated the advantages of smart materials and structures by including actuators in material systems for controlling and altering the response of structural environments. Applications of these materials systems include vibration suppression/isolation, precision positioning, damage detection and tunable devices. Some of the embedded materials being investigated for accomplishing these tasks include piezoelectric ceramics, shape memory alloys, and fiber optics. These materials have some benefits and some shortcomings; each is being studied for use in active material design in the SPICES (Synthesis and Processing of Intelligent Cost Effective Structures) Consortium. The focus of this paper concerns the manufacturing aspects of smart structures by incorporating piezoelectric ceramics, shape memory alloys and fiber optics in a reinforced thermoset matrix via resin transfer molding (RTM).

Terahertz computed tomography of NASA thermal protection system materials

NASA Astrophysics Data System (ADS)

Roth, D. J.; Reyes-Rodriguez, S.; Zimdars, D. A.; Rauser, R. W.; Ussery, W. W.

2012-05-01

A terahertz (THz) axial computed tomography system has been developed that uses time domain measurements in order to form cross-sectional image slices and three dimensional volume renderings of terahertz-transparent materials. The system can inspect samples as large as 0.0283 m3 (1 ft3) with no safety concerns as for x-ray computed tomography. In this study, the THz-CT system was evaluated for its ability to detect and characterize 1) an embedded void in Space Shuttle external fuel tank thermal protection system (TPS) foam material and 2) impact damage in a TPS configuration under consideration for use in NASA's multi-purpose Orion crew module (CM). Micro-focus X-ray CT is utilized to characterize the flaws and provide a baseline for which to compare the THz CT results.

Immobilized lipid-bilayer materials

DOEpatents

Sasaki, Darryl Y.; Loy, Douglas A.; Yamanaka, Stacey A.

2000-01-01

A method for preparing encapsulated lipid-bilayer materials in a silica matrix comprising preparing a silica sol, mixing a lipid-bilayer material in the silica sol and allowing the mixture to gel to form the encapsulated lipid-bilayer material. The mild processing conditions allow quantitative entrapment of pre-formed lipid-bilayer materials without modification to the material's spectral characteristics. The method allows for the immobilization of lipid membranes to surfaces. The encapsulated lipid-bilayer materials perform as sensitive optical sensors for the detection of analytes such as heavy metal ions and can be used as drug delivery systems and as separation devices.

Radiation portal monitor system and method

DOEpatents

Morris, Christopher [Los Alamos, NM; Borozdin, Konstantin N [Los Alamos, NM; Green, J Andrew [Los Alamos, NM; Hogan, Gary E [Los Alamos, NM; Makela, Mark F [Los Alamos, NM; Priedhorsky, William C [Los Alamos, NM; Saunders, Alexander [Los Alamos, NM; Schultz, Larry J [Los Alamos, NM; Sossong, Michael J [Los Alamos, NM

2009-12-15

A portal monitoring system has a cosmic ray charged particle tracker with a plurality of drift cells. The drift cells, which can be for example aluminum drift tubes, can be arranged at least above and below a volume to be scanned to thereby track incoming and outgoing charged particles, such as cosmic ray muons, whilst also detecting gamma rays. The system can selectively detect devices or materials, such as iron, lead, gold and/or tungsten, occupying the volume from multiple scattering of the charged particles passing through the volume and can also detect any radioactive sources occupying the volume from gamma rays emitted therefrom. If necessary, the drift tubes can be sealed to eliminate the need for a gas handling system. The system can be employed to inspect occupied vehicles at border crossings for nuclear threat objects.

Task-oriented situation recognition

NASA Astrophysics Data System (ADS)

Bauer, Alexander; Fischer, Yvonne

2010-04-01

From the advances in computer vision methods for the detection, tracking and recognition of objects in video streams, new opportunities for video surveillance arise: In the future, automated video surveillance systems will be able to detect critical situations early enough to enable an operator to take preventive actions, instead of using video material merely for forensic investigations. However, problems such as limited computational resources, privacy regulations and a constant change in potential threads have to be addressed by a practical automated video surveillance system. In this paper, we show how these problems can be addressed using a task-oriented approach. The system architecture of the task-oriented video surveillance system NEST and an algorithm for the detection of abnormal behavior as part of the system are presented and illustrated for the surveillance of guests inside a video-monitored building.

Linac based photofission inspection system employing novel detection concepts

NASA Astrophysics Data System (ADS)

Stevenson, John; Gozani, Tsahi; Elsalim, Mashal; Condron, Cathie; Brown, Craig

2011-10-01

Rapiscan Systems is developing a LINAC based cargo inspection system for detection of special nuclear material (SNM) in cargo containers. The system, called Photofission Based Alarm Resolution (PBAR) is being developed under a DHD/DNDO Advanced Technology Demonstration (ATD) program. The PBAR system is based on the Rapiscan Eagle P9000 X-ray system, which is a portal system with a commercial 9 MeV LINAC X-ray source. For the purposes of the DNDO ATD program, a conveyor system was installed in the portal to allow scanning and precise positioning of 20 ft ISO cargo containers. The system uses a two step inspection process. In the first step, the basic scan, the container is quickly and completely inspected using two independent radiography arrays: the conventional primary array with high spatial resolution and a lower resolution spectroscopic array employing the novel Z-Spec method. The primary array uses cadmium tungstate (CdWO 4) detectors with conventional current mode readouts using photodiodes. The Z-Spec array uses small plastic scintillators capable of performing very fast (up to 10 8 cps) gamma-ray spectroscopy. The two radiography arrays are used to locate high-Z objects in the image such as lead, tungsten, uranium, which could be potential shielding materials as well as SNM itself. In the current system, the Z-Spec works by measuring the energy spectrum of transmitted X-rays. For high-Z materials the higher end of the energy spectrum is more attenuated than for low-Z materials and thus has a lower mean energy and a narrower width than low- and medium-Z materials. The second step in the inspection process is the direct scan or alarm clearing scan. In this step, areas of the container image, which were identified as high Z, are re-inspected. This is done by precisely repositioning the container to the location of the high-Z object and performing a stationary irradiation of the area with X-ray beam. Since there are a large number of photons in the 9 MV Bremsstrahlung spectrum above the photofission "threshold" of about 6 MeV, the X-ray beam induces numerous fissions if nuclear material is present. The PBAR system looks for the two most prolific fission signatures to confirm the presence of special nuclear materials (SNM). These are prompt neutrons and delayed gamma rays. The PBAR system uses arrays of two types of fast and highly efficient gamma ray detectors: plastic and fluorocarbon scintillators. The latter serves as a detector of fission prompt neutrons using the novel threshold activation detector (TAD) concept as well as a very efficient delayed gamma ray detector. The major advantage of TAD for detecting the prompt neutrons is its insensitivity to the intense source related backgrounds. The current status of the system and experimental results will be shown and discussed.

Development of a Highly Sensitive Nested-PCR Procedure Using a Single Closed Tube for Detection of Erwinia amylovora in Asymptomatic Plant Material

PubMed Central

Llop, Pablo; Bonaterra, Anna; Peñalver, Javier; López, María M.

2000-01-01

A novel method, which involves a nested PCR in a single closed tube, was developed for the sensitive detection of Erwinia amylovora in plant material. The external and internal primer pairs used had different annealing temperatures and directed the amplification of a specific DNA fragment from plasmid pEA29. The procedure involved two consecutive PCRs, the first of which was performed at a higher annealing temperature that allowed amplification only by the external primer pair. Using pure cultures of E. amylovora, the sensitivity of the nested PCR in one tube was similar to that of a standard nested PCR in two tubes. The specificity and sensitivity were greater than those of standard PCR procedures that used a single primer pair. The presence of inhibitors in plant material, very common in E. amylovora hosts, is overcome with this system in combination with a simple DNA extraction protocol because it eliminates many of the inhibitory compounds. In addition, it needs a very small sample volume (1 μl of DNA extracted). With 83 samples of naturally infected material, this method achieved better results than any other PCR technique: standard PCR detected 55% of positive samples, two-tube nested PCR detected 71% of positive samples, and nested PCR in a single closed tube detected 78% of positive samples. When analyzing asymptomatic plant material, the number of positive samples detected by the developed nested PCR was also the highest, compared with the PCR protocols indicated previously (17, 20, and 25% of 251 samples analyzed, respectively). This method is proposed for the detection of endophytic and epiphytic populations of E. amylovora in epidemiological studies and for routine use in quarantine surveys, due to its high sensitivity, specificity, speed, and simplicity. PMID:10788384

Hyperspectral imaging for differentiation of foreign materials from pinto beans

NASA Astrophysics Data System (ADS)

Mehrubeoglu, Mehrube; Zemlan, Michael; Henry, Sam

2015-09-01

Food safety and quality in packaged products are paramount in the food processing industry. To ensure that packaged products are free of foreign materials, such as debris and pests, unwanted materials mixed with the targeted products must be detected before packaging. A portable hyperspectral imaging system in the visible-to-NIR range has been used to acquire hyperspectral data cubes from pinto beans that have been mixed with foreign matter. Bands and band ratios have been identified as effective features to develop a classification scheme for detection of foreign materials in pinto beans. A support vector machine has been implemented with a quadratic kernel to separate pinto beans and background (Class 1) from all other materials (Class 2) in each scene. After creating a binary classification map for the scene, further analysis of these binary images allows separation of false positives from true positives for proper removal action during packaging.

2D metal profile detector using a polymeric fiber optic sensor

NASA Astrophysics Data System (ADS)

Hua, Wei-Shu; Hooks, Joshua R.; Erwin, Nicholas A.; Wu, Wen-Jong; Wang, Wei-Chih

2012-04-01

As sensors become integrated in more applications, interest in magnetostrictive sensor technology has blossomed. Magnetostrictive materials have many advantages and useful applications in daily life, such as high efficient coupling between elastic and polymer material, large displacement, magnetic field sensors, micro actuator and motion motor, etc. The purpose of this paper is to develop a metal sensor which is capable of detecting different geometries and shapes of metal objects. The main configuration is using a Mach-Zehnder fiber-optic interferometer coated with magnetostrictive material. The metal detector system is a novel design of metal detector, easy to fabricate and capable of high sensitivity. In our design, metal detection is made possible by disrupting the magnetic flux density that encompasses the magnetostriction sensor. In this paper, experimental setups are described and metal sensing results are presented. The results of detecting complex metal's geometry and metal's mapping results are discussed.

A triphenylamine-functionalized luminescent sensor for efficient p-nitroaniline detection.

PubMed

Ji, Ning-Ning; Shi, Zhi-Qiang; Hu, Hai-Liang; Zheng, He-Gen

2018-05-14

The combination of π-conjugated fluorophores within a hybrid system gives rise to a triphenylamine-functionalized material [Zn(bpba)(NO3)] (1) (Hbpba = 4-(bis(4-(pyridin-4-yl)phenyl)amino)benzoic acid). Compound 1 features a 2D + 2D → 2D parallel polycatenation structure with 63-hcb net. Photophysical studies revealed that the title phase showed superior sensitivity towards p-nitroaniline (p-NA) with a low detection limit (down to ∼0.10 ppm). Specifically, following a new detection route, vapor-sensing experiments using a saturated ethanol solution of nitroaromatic isomers have been established for the first time. Highly sensitive and selective detection of p-NA by the proposed material with a rapid response time (t = 30 s, QE > 90.0%) as compared to that via the control isomers (t = 60s, QE < 6.0%) demonstrates an attractive feasible route and a promising luminescent sensor for nitroaromatic detection.

Sensor and methods of detecting target materials and situations in closed systems

DOEpatents

Mee, David K.; Ripley, Edward B.; Nienstedt, Zachary C.; Nienstedt, Alex W.; Howell, Jr., Layton N.

2018-03-13

Disclosed is a passive, in-situ pressure sensor. The sensor includes a sensing element having a ferromagnetic metal and a tension inducing mechanism coupled to the ferromagnetic metal. The tension inducing mechanism is operable to change a tensile stress upon the ferromagnetic metal based on a change in pressure in the sensing element. Changes in pressure are detected based on changes in the magnetic switching characteristics of the ferromagnetic metal when subjected to an alternating magnetic field caused by the change in the tensile stress. The sensing element is embeddable in a closed system for detecting pressure changes without the need for any penetrations of the system for power or data acquisition by detecting changes in the magnetic switching characteristics of the ferromagnetic metal caused by the tensile stress.

An Ice Protection and Detection Systems Manufacturer's Perspective

NASA Technical Reports Server (NTRS)

Sweet, Dave

2009-01-01

Accomplishments include: World Class Aircraft Icing Research Center and Facility. Primary Sponsor/Partner - Aircraft Icing Consortia/Meetings. Icing Research Tunnel. Icing Test Aircraft. Icing Codes - LEWICE/Scaling, et al. Development of New Technologies (SBIR, STTR, et al). Example: Look Ahead Ice Detection. Pilot Training Materials. Full Cooperation with Academia, Government and Industry.

Novel method of detecting movement of the interference fringes using one-dimensional PSD.

PubMed

Wang, Qi; Xia, Ji; Liu, Xu; Zhao, Yong

2015-06-02

In this paper, a method of using a one-dimensional position-sensitive detector (PSD) by replacing charge-coupled device (CCD) to measure the movement of the interference fringes is presented first, and its feasibility is demonstrated through an experimental setup based on the principle of centroid detection. Firstly, the centroid position of the interference fringes in a fiber Mach-Zehnder (M-Z) interferometer is solved in theory, showing it has a higher resolution and sensitivity. According to the physical characteristics and principles of PSD, a simulation of the interference fringe's phase difference in fiber M-Z interferometers and PSD output is carried out. Comparing the simulation results with the relationship between phase differences and centroid positions in fiber M-Z interferometers, the conclusion that the output of interference fringes by PSD is still the centroid position is obtained. Based on massive measurements, the best resolution of the system is achieved with 5.15, 625 μm. Finally, the detection system is evaluated through setup error analysis and an ultra-narrow-band filter structure. The filter structure is configured with a one-dimensional photonic crystal containing positive and negative refraction material, which can eliminate background light in the PSD detection experiment. This detection system has a simple structure, good stability, high precision and easily performs remote measurements, which makes it potentially useful in material small deformation tests, refractivity measurements of optical media and optical wave front detection.

A dynamical study on extrasolar comets

NASA Astrophysics Data System (ADS)

Loibnegger, B.; Dvorak, R.

2017-09-01

Since the detection of absorption features in spectra of beta Pictoris varying on short time scales it is known that comets exist in other stellar systems. We investigate the dynamics of comets in two differently build systems (HD 10180 and HIP 14810). The outcomes of the scattering process, as there are collisions with the planets, captures and ejections from the systems are analysed statistically. Collisions and close encounters with the planets are investigated in more detail in order to conclude about transport of water and organic material. We will also investigate the possibility of detection of comets in other planetary systems.

A single-shot nanosecond neutron pulsed technique for the detection of fissile materials

NASA Astrophysics Data System (ADS)

Gribkov, V.; Miklaszewski, R. A.; Chernyshova, M.; Scholz, M.; Prokopovicz, R.; Tomaszewski, K.; Drozdowicz, K.; Wiacek, U.; Gabanska, B.; Dworak, D.; Pytel, K.; Zawadka, A.

2012-07-01

A novel technique with the potential of detecting hidden fissile materials is presented utilizing the interaction of a single powerful and nanosecond wide neutron pulse with matter. The experimental system is based on a Dense Plasma Focus (DPF) device as a neutron source generating pulses of almost mono-energetic 2.45 MeV and/or 14.0 MeV neutrons, a few nanoseconds in width. Fissile materials, consisting of heavy nuclei, are detected utilizing two signatures: firstly by measuring those secondary fission neutrons which are faster than the elastically scattered 2.45 MeV neutrons of the D-D reaction in the DPF; secondly by measuring the pulses of the slower secondary fission neutrons following the pulse of the fast 14 MeV neutrons from the D-T reaction. In both cases it is important to compare the measured spectrum of the fission neutrons induced by the 2.45 MeV or 14 MeV neutron pulse of the DPF with theoretical spectra obtained by mathematical simulation. Therefore, results of numerical modelling of the proposed system, using the MCNP5 and the FLUKA codes are presented and compared with experimental data.

Biosignature Preservation and Detection in Mars Analog Environments

PubMed Central

Graham, Heather V.; Des Marais, David J.; Hausrath, Elisabeth M.; Horgan, Briony; McCollom, Thomas M.; Parenteau, M. Niki; Potter-McIntyre, Sally L.; Williams, Amy J.; Lynch, Kennda L.

2017-01-01

Abstract This review of material relevant to the Conference on Biosignature Preservation and Detection in Mars Analog Environments summarizes the meeting materials and discussions and is further expanded upon by detailed references to the published literature. From this diverse source material, there is a detailed discussion on the habitability and biosignature preservation potential of five primary analog environments: hydrothermal spring systems, subaqueous environments, subaerial environments, subsurface environments, and iron-rich systems. Within the context of exploring past habitable environments on Mars, challenges common to all of these key environments are laid out, followed by a focused discussion for each environment regarding challenges to orbital and ground-based observations and sample selection. This leads into a short section on how these challenges could influence our strategies and priorities for the astrobiological exploration of Mars. Finally, a listing of urgent needs and future research highlights key elements such as development of instrumentation as well as continued exploration into how Mars may have evolved differently from Earth and what that might mean for biosignature preservation and detection. Key Words: Biosignature preservation—Biosignature detection—Mars analog environments—Conference report—Astrobiological exploration. Astrobiology 17, 363–400. PMID:28177270

A 10,000-Pen Nanoplotter with Integrated Ink Delivery System

DTIC Science & Technology

2007-03-03

and Chemically Encoded Nanoparticle Materials in Biomolecule Detection,” MRS Bulletin, 2005, 30, 376-380. 35. Vega, R.A.; Maspoch, D.; Salaita, K...Burgenstock Conference, Burgenstock, Switzerland; “Nanostructures in Chemistry and Biodiagnostics,” (Mirkin, C.A.; 2006). 16. Center for Nanoscale Materials ...SEMI NanoForum, Chicago, IL; “A Vision for Nanoscience and Nanotechnology,” (Mirkin, C.A.; 2005). 21. MIT Materials Seminar Series, Cambridge, MA

Electrical detection of microwave assisted magnetization reversal by spin pumping

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rao, Siddharth; Subhra Mukherjee, Sankha; Elyasi, Mehrdad

2014-03-24

Microwave assisted magnetization reversal has been investigated in a bilayer system of Pt/ferromagnet by detecting a change in the polarity of the spin pumping signal. The reversal process is studied in two material systems, Pt/CoFeB and Pt/NiFe, for different aspect ratios. The onset of the switching behavior is indicated by a sharp transition in the spin pumping voltage. At a threshold value of the external field, the switching process changes from partial to full reversal with increasing microwave power. The proposed method provides a simple way to detect microwave assisted magnetization reversal.

Paint for detection of corrosion and warning of chemical and radiological attack

DOEpatents

Farmer, Joseph C [Tracy, CA

2010-08-24

A system for warning of corrosion, chemical, or radiological substances. The system comprises painting a surface with a paint or coating that includes an indicator material and monitoring the surface for indications of the corrosion, chemical, or radiological substances.

Biocontrol and Rapid Detection of Food-Borne Pathogens Using Bacteriophages and Endolysins

PubMed Central

Bai, Jaewoo; Kim, You-Tae; Ryu, Sangryeol; Lee, Ju-Hoon

2016-01-01

Bacteriophages have been suggested as natural food preservatives as well as rapid detection materials for food-borne pathogens in various foods. Since Listeria monocytogenes-targeting phage cocktail (ListShield) was approved for applications in foods, numerous phages have been screened and experimentally characterized for phage applications in foods. A single phage and phage cocktail treatments to various foods contaminated with food-borne pathogens including E. coli O157:H7, Salmonella enterica, Campylobacter jejuni, Listeria monocytogenes, Staphylococcus aureus, Cronobacter sakazakii, and Vibrio spp. revealed that they have great potential to control various food-borne pathogens and may be alternative for conventional food preservatives. In addition, phage-derived endolysins with high host specificity and host lysis activities may be preferred to food applications rather than phages. For rapid detection of food-borne pathogens, cell-wall binding domains (CBDs) from endolysins have been suggested due to their high host-specific binding. Fluorescence-tagged CBDs have been successfully evaluated and suggested to be alternative materials of expensive antibodies for various detection applications. Most recently, reporter phage systems have been developed and tested to confirm their usability and accuracy for specific detection. These systems revealed some advantages like rapid detection of only viable pathogenic cells without interference by food components in a very short reaction time, suggesting that these systems may be suitable for monitoring of pathogens in foods. Consequently, phage is the next-generation biocontrol agent as well as rapid detection tool to confirm and even identify the food-borne pathogens present in various foods. PMID:27092128

Inductance and resistance measurement method for vessel detection and coil powering in all-surface inductive heating systems composed of outer squircle coils

NASA Astrophysics Data System (ADS)

Kilic, Veli Tayfun; Unal, Emre; Demir, Hilmi Volkan

2017-05-01

In this work, we investigate a method proposed for vessel detection and coil powering in an all-surface inductive heating system composed of outer squircle coils. Besides conventional circular coils, coils with different shapes such as outer squircle coils are used for and enable efficient all-surface inductive heating. Validity of the method, which relies on measuring inductance and resistance values of a loaded coil at different frequencies, is experimentally demonstrated for a coil with shape different from conventional circular coil. Simple setup was constructed with a small coil to model an all-surface inductive heating system. Inductance and resistance maps were generated by measuring coil's inductance and resistance values at different frequencies loaded by a plate made of different materials and located at various positions. Results show that in an induction hob for various coil geometries it is possible to detect a vessel's presence, to identify its material type and to specify its position on the hob surface by considering inductance and resistance of the coil measured on at least two different frequencies. The studied method is important in terms of enabling safe, efficient and user flexible heating in an all-surface inductive heating system by automatically detecting the vessel's presence and powering on only the coils that are loaded by the vessel with predetermined current levels.

Monte Carlo parametric studies of neutron interrogation with the Associated Particle Technique for cargo container inspections

NASA Astrophysics Data System (ADS)

Deyglun, Clément; Carasco, Cédric; Pérot, Bertrand

2014-06-01

The detection of Special Nuclear Materials (SNM) by neutron interrogation is extensively studied by Monte Carlo simulation at the Nuclear Measurement Laboratory of CEA Cadarache (French Alternative Energies and Atomic Energy Commission). The active inspection system is based on the Associated Particle Technique (APT). Fissions induced by tagged neutrons (i.e. correlated to an alpha particle in the DT neutron generator) in SNM produce high multiplicity coincidences which are detected with fast plastic scintillators. At least three particles are detected in a short time window following the alpha detection, whereas nonnuclear materials mainly produce single events, or pairs due to (n,2n) and (n,n'γ) reactions. To study the performances of an industrial cargo container inspection system, Monte Carlo simulations are performed with the MCNP-PoliMi transport code, which records for each neutron history the relevant information: reaction types, position and time of interactions, energy deposits, secondary particles, etc. The output files are post-processed with a specific tool developed with ROOT data analysis software. Particles not correlated with an alpha particle (random background), counting statistics, and time-energy resolutions of the data acquisition system are taken into account in the numerical model. Various matrix compositions, suspicious items, SNM shielding and positions inside the container, are simulated to assess the performances and limitations of an industrial system.

Space Station Freedom Toxic and Reactive Materials Handling

NASA Technical Reports Server (NTRS)

Baugher, Charles R. (Editor)

1990-01-01

Viable research in materials processing in space requires the utilization of a wide variety of chemicals and materials, many of which are considered toxic and/or highly reactive with other substances. A realistic view of the experiments which are most likely to be accomplished in the early Space Station phases are examined and design issues addressed which are related to their safe implementation. Included are discussions of materials research on Skylab, Spacelab, and the Shuttle mid-deck; overviews of early concepts for specialized Space Station systems designed to help contain potential problems; descriptions of industrial experience with ground-based research; and an overview of the state-of-the-art in contamination detection systems.

Method of reducing chlorofluorocarbon refrigerant emissons to the atmosphere

DOEpatents

DeVault, Robert C.; Fairchild, Phillip D.; Biermann, Wendell J.

1990-01-01

A method is disclosed for reducing chloroflurocarbon (CFC) refrigerant emissions during removal or transfer or refrigerants from a vapor compression cooling system or heat pump which comprises contacting the refrigerant with a suitable sorbent material. The sorbent material allows for the storage and retention or the chlorofluorocarbon in non-gaseous form so that it does not tend to escape to the atmosphere where it would cause harm by contributing to ozone depletion. In other aspects of the invention, contacting of CFC refrigerants with sorbent material allows for purification and recycling of used refrigerant, and a device containing stored sorbent material can be employed in the detection of refrigerant leakage in a cooling system or heat pump.

Detecting strain in birefringent materials using spectral polarimetry

NASA Technical Reports Server (NTRS)

Garner, Harold R. (Inventor); Ragucci, Anthony J. (Inventor); Cisar, Alan J. (Inventor); Huebschman, Michael L. (Inventor)

2010-01-01

A method, computer program product and system for analyzing multispectral images from a plurality of regions of birefringent material, such as a polymer film, using polarized light and a corresponding polar analyzer to identify differential strain in the birefringent material. For example, the birefringement material may be low-density polyethylene (LDPE), high-density polyethylene (HDPE), polypropylene, polyethylene terephthalate (PET), polyvinyl chloride (PVC), polyvinylidene chloride, polyester, nylon, or cellophane film. Optionally, the method includes generating a real-time quantitative strain map.

Effects of antenna length and material on output power and detection of miniature radio transmitters

USGS Publications Warehouse

Beeman, J.W.; Bower, N.; Juhnke, S.; Dingmon, L.; Van Den, Tillaart; Thomas, T.

2007-01-01

The optimal antenna of transmitters used in small aquatic animals is often a compromise between efficient radio wave propagation and effects on animal behavior. Radio transmission efficiency generally increases with diameter and length of the conductor, but increased antenna length or weight can adversely affect animal behavior. We evaluated the effects of changing antenna length and material on the subsequent tag output power, reception, and detection of tagged fish. In a laboratory, we compared the relative signal strengths in water of 150 MHz transmitters over a range of antenna lengths (from 6 to 30 cm) and materials (one weighing about half of the other). The peak relative signal strengths were at 20 and 22 cm, which are approximately one wavelength underwater at the test frequency. The peak relative signal strengths at these lengths were approximately 50% greater than those of 30 cm antennas, a length commonly used in fisheries research. Few significant differences were present in distances for the operator to hear or the telemetry receiver to decode transmitters from a boat-mounted receiving system based on antenna length, but the percent of tagged fish detected passing a hydroelectric dam fitted with an array of receiving systems was significantly greater at the antenna length with peak output power in laboratory tests. This study indicates careful choice of antenna length and material of small transmitters can be used to reduce weight and possible antenna effects on animal behavior, to maximize tag output power and detection, or to balance these factors based on the needs of the application. ?? 2007 Springer Science+Business Media B.V.

Detection and quantification of beef and pork materials in meat products by duplex droplet digital PCR.

PubMed

Cai, Yicun; He, Yuping; Lv, Rong; Chen, Hongchao; Wang, Qiang; Pan, Liangwen

2017-01-01

Meat products often consist of meat from multiple animal species, and inaccurate food product adulteration and mislabeling can negatively affect consumers. Therefore, a cost-effective and reliable method for identification and quantification of animal species in meat products is required. In this study, we developed a duplex droplet digital PCR (dddPCR) detection and quantification system to simultaneously identify and quantify the source of meat in samples containing a mixture of beef (Bos taurus) and pork (Sus scrofa) in a single digital PCR reaction tube. Mixed meat samples of known composition were used to test the accuracy and applicability of this method. The limit of detection (LOD) and the limit of quantification (LOQ) of this detection and quantification system were also identified. We conclude that our dddPCR detection and quantification system is suitable for quality control and routine analyses of meat products.

System for characterizing semiconductor materials and photovoltaic device

DOEpatents

Sopori, B.L.

1996-12-03

Apparatus for detecting and mapping defects in the surfaces of polycrystalline material in a manner that distinguishes dislocation pits from grain boundaries includes a first laser of a first wavelength for illuminating a wide spot on the surface of the material, a second laser of a second relatively shorter wavelength for illuminating a relatively narrower spot on the surface of the material, a light integrating sphere with apertures for capturing light scattered by etched dislocation pits in an intermediate range away from specular reflection while allowing light scattered by etched grain boundaries in a near range from specular reflection to pass through, and optical detection devices for detecting and measuring intensities of the respective intermediate scattered light and near specular scattered light. A center blocking aperture or filter can be used to screen out specular reflected light, which would be reflected by nondefect portions of the polycrystalline material surface. An X-Y translation stage for mounting the polycrystalline material and signal processing and computer equipment accommodate raster mapping, recording, and displaying of respective dislocation and grain boundary defect densities. A special etch procedure is included, which prepares the polycrystalline material surface to produce distinguishable intermediate and near specular light scattering in patterns that have statistical relevance to the dislocation and grain boundary defect densities. A reflectance measurement of the piece of material is obtained by adding together the signals from the optical detection devices. In the case where the piece of material includes a photovoltaic device, the current induced in the device by the illuminating light can be measured with a current sensing amplifier after the light integrating sphere is moved away from the device. 22 figs.

System for characterizing semiconductor materials and photovoltaic device

DOEpatents

Sopori, Bhushan L.

1996-01-01

Apparatus for detecting and mapping defects in the surfaces of polycrystalline material in a manner that distinguishes dislocation pits from grain boundaries includes a first laser of a first wavelength for illuminating a wide spot on the surface of the material, a second laser of a second relatively shorter wavelength for illuminating a relatively narrower spot on the surface of the material, a light integrating sphere with apertures for capturing light scattered by etched dislocation pits in an intermediate range away from specular reflection while allowing light scattered by etched grain boundaries in a near range from specular reflection to pass through, and optical detection devices for detecting and measuring intensities of the respective intermediate scattered light and near specular scattered light. A center blocking aperture or filter can be used to screen out specular reflected light, which would be reflected by nondefect portions of the polycrystalline material surface. An X-Y translation stage for mounting the polycrystalline material and signal processing and computer equipment accommodate raster mapping, recording, and displaying of respective dislocation and grain boundary defect densities. A special etch procedure is included, which prepares the polycrystalline material surface to produce distinguishable intermediate and near specular light scattering in patterns that have statistical relevance to the dislocation and grain boundary defect densities. A reflectance measurement of the piece of material is obtained by adding together the signals from the optical detection devices. In the case where the piece of material includes a photovoltaic device, the current induced in the device by the illuminating light can be measured with a current sensing amplifier after the light integrating sphere is moved away from the device.

Structurally integrated fiber optic damage assessment system for composite materials.

PubMed

Measures, R M; Glossop, N D; Lymer, J; Leblanc, M; West, J; Dubois, S; Tsaw, W; Tennyson, R C

1989-07-01

Progress toward the development of a fiber optic damage assessment system for composite materials is reported. This system, based on the fracture of embedded optical fibers, has been characterized with respect to the orientation and location of the optical fibers in the composite. Together with a special treatment, these parameters have been tailored to yield a system capable of detecting the threshold of damage for various impacted Kevlar/epoxy panels. The technique has been extended to measure the growth of a damage region which could arise from either impact, manufacturing flaws, or static overloading. The mechanism of optical fiber fracture has also been investigated. In addition, the influence of embedded optical fibers on the tensile and compressive strength of the composite material has been studied. Image enhanced backlighting has been shown to be a powerful and convenient method of assessing internal damage to translucent composite materials.

Biological cell as a soft magnetoelectric material: Elucidating the physical mechanisms underpinning the detection of magnetic fields by animals

NASA Astrophysics Data System (ADS)

Krichen, S.; Liu, L.; Sharma, P.

2017-10-01

Sharks, birds, bats, turtles, and many other animals can detect magnetic fields. Aside from using this remarkable ability to exploit the terrestrial magnetic field map to sense direction, a subset is also able to implement a version of the so-called geophysical positioning system. How do these animals detect magnetic fields? The answer to this rather deceptively simple question has proven to be quite elusive. The currently prevalent theories, while providing interesting insights, fall short of explaining several aspects of magnetoreception. For example, minute magnetic particles have been detected in magnetically sensitive animals. However, how is the detected magnetic field converted into electrical signals given any lack of experimental evidence for relevant electroreceptors? In principle, a magnetoelectric material is capable of converting magnetic signals into electricity (and vice versa). This property, however, is rare and restricted to a rather small set of exotic hard crystalline materials. Indeed, such elements have never been detected in the animals studied so far. In this work we quantitatively outline the conditions under which a biological cell may detect a magnetic field and convert it into electrical signals detectable by biological cells. Specifically, we prove the existence of an overlooked strain-mediated mechanism and show that most biological cells can act as nontrivial magnetoelectric materials provided that the magnetic permeability constant is only slightly more than that of a vacuum. The enhanced magnetic permeability is easily achieved by small amounts of magnetic particles that have been experimentally detected in magnetosensitive animals. Our proposed mechanism appears to explain most of the experimental observations related to the physical basis of magnetoreception.

A multisensor system for airborne surveillance of oil pollution

NASA Technical Reports Server (NTRS)

Edgerton, A. T.; Ketchal, R.; Catoe, C.

1973-01-01

The U.S. Coast Guard is developing a prototype airborne oil surveillance system for use in its Marine Environmental Protection Program. The prototype system utilizes an X-band side-looking radar, a 37-GHz imaging microwave radiometer, a multichannel line scanner, and a multispectral low light level system. The system is geared to detecting and mapping oil spills and potential pollution violators anywhere within a 25 nmi range of the aircraft flight track under all but extreme weather conditions. The system provides for false target discrimination and maximum identification of spilled materials. The system also provides an automated detection alarm, as well as a color display to achieve maximum coupling between the sensor data and the equipment operator.

Detection of special nuclear materials with the associate particle technique

NASA Astrophysics Data System (ADS)

Carasco, Cédric; Deyglun, Clément; Pérot, Bertrand; Eléon, Cyrille; Normand, Stéphane; Sannié, Guillaume; Boudergui, Karim; Corre, Gwenolé; Konzdrasovs, Vladimir; Pras, Philippe

2013-04-01

In the frame of the French trans-governmental R&D program against chemical, biological, radiological, nuclear and explosives (CBRN-E) threats, CEA is studying the detection of Special Nuclear Materials (SNM) by neutron interrogation with fast neutrons produced by an associated particle sealed tube neutron generator. The deuterium-tritium fusion reaction produces an alpha particle and a 14 MeV neutron almost back to back, allowing tagging neutron emission both in time and direction with an alpha particle position-sensitive sensor embedded in the generator. Fission prompt neutrons and gamma rays induced by tagged neutrons which are tagged by an alpha particle are detected in coincidence with plastic scintillators. This paper presents numerical simulations performed with the MCNP-PoliMi Monte Carlo computer code and with post processing software developed with the ROOT data analysis package. False coincidences due to neutron and photon scattering between adjacent detectors (cross talk) are filtered out to increase the selectivity between nuclear and benign materials. Accidental coincidences, which are not correlated to an alpha particle, are also taken into account in the numerical model, as well as counting statistics, and the time-energy resolution of the data acquisition system. Such realistic calculations show that relevant quantities of SNM (few kg) can be distinguished from cargo and shielding materials in 10 min acquisitions. First laboratory tests of the system under development in CEA laboratories are also presented.

Characterization and detection of acceleration-induced cavitation in soft materials using a drop-tower-based integrated system

NASA Astrophysics Data System (ADS)

Kang, Wonmo; Chen, YungChia; Bagchi, Amit; O'Shaughnessy, Thomas J.

2017-12-01

The material response of biologically relevant soft materials, e.g., extracellular matrix or cell cytoplasm, at high rate loading conditions is becoming increasingly important for emerging medical implications including the potential of cavitation-induced brain injury or cavitation created by medical devices, whether intentional or not. However, accurately probing soft samples remains challenging due to their delicate nature, which often excludes the use of conventional techniques requiring direct contact with a sample-loading frame. We present a drop-tower-based method, integrated with a unique sample holder and a series of effective springs and dampers, for testing soft samples with an emphasis on high-rate loading conditions. Our theoretical studies on the transient dynamics of the system show that well-controlled impacts between a movable mass and sample holder can be used as a means to rapidly load soft samples. For demonstrating the integrated system, we experimentally quantify the critical acceleration that corresponds to the onset of cavitation nucleation for pure water and 7.5% gelatin samples. This study reveals that 7.5% gelatin has a significantly higher, approximately double, critical acceleration as compared to pure water. Finally, we have also demonstrated a non-optical method of detecting cavitation in soft materials by correlating cavitation collapse with structural resonance of the sample container.

Terahertz imaging devices and systems, and related methods, for detection of materials

DOEpatents

Kotter, Dale K.

2016-11-15

Terahertz imaging devices may comprise a focal plane array including a substrate and a plurality of resonance elements. The plurality of resonance elements may comprise a conductive material coupled to the substrate. Each resonance element of the plurality of resonance elements may be configured to resonate and produce an output signal responsive to incident radiation having a frequency between about a 0.1 THz and 4 THz range. A method of detecting a hazardous material may comprise receiving incident radiation by a focal plane array having a plurality of discrete pixels including a resonance element configured to absorb the incident radiation at a resonant frequency in the THz, generating an output signal from each of the discrete pixels, and determining a presence of a hazardous material by interpreting spectral information from the output signal.

Responsive hybrid inorganic-organic system derived from lanthanide luminescence

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhou, Zhan; Zheng, Yuhui, E-mail: yhzheng78@scnu.edu.cn; Jiang, Lasheng

2016-05-15

Highlights: • A novel covalent hybrid material was used to detect hemoglobin. • All the recognition experiments were performed in buffer solution. • Porous nano-structures was extensively studied for the recognition. - Abstract: Terbium ions were incorporated into new organic-inorganic matrices to achieve intense green emissions. Hemoglobin (HB) interactions lead to dramatic changes in the luminescence emission intensities. Infrared spectra, morphological studies and photoluminescence give information for the speciation and process of hemoglobin additions. The porous material has a large specific surface area of 351 cm{sup 2}/g and the detection limit for HB (0.7 μM) was much lower than itsmore » physical doped material (8 μM). This promising hybrid material will lead to the design of versatile optical probes that are efficiently responding to the external targets.« less

Multispectral image fusion for detecting land mines

DOE Office of Scientific and Technical Information (OSTI.GOV)

Clark, G.A.; Sengupta, S.K.; Aimonetti, W.D.

1995-04-01

This report details a system which fuses information contained in registered images from multiple sensors to reduce the effects of clutter and improve the ability to detect surface and buried land mines. The sensor suite currently consists of a camera that acquires images in six bands (400nm, 500nm, 600nm, 700nm, 800nm and 900nm). Past research has shown that it is extremely difficult to distinguish land mines from background clutter in images obtained from a single sensor. It is hypothesized, however, that information fused from a suite of various sensors is likely to provide better detection reliability, because the suite ofmore » sensors detects a variety of physical properties that are more separable in feature space. The materials surrounding the mines can include natural materials (soil, rocks, foliage, water, etc.) and some artifacts.« less

Development of a simple-material discrimination method with three plastic scintillator strips for visualizing nuclear reactors

NASA Astrophysics Data System (ADS)

Takamatsu, k.; Tanaka, h.; Shoji, d.

2012-04-01

The Fukushima Daiichi nuclear disaster is a series of equipment failures and nuclear meltdowns, following the T¯o hoku earthquake and tsunami on 11 March 2011. We present a new method for visualizing nuclear reactors. Muon radiography based on the multiple Coulomb scattering of cosmic-ray muons has been performed. In this work, we discuss experimental results obtained with a cost-effective simple detection system assembled with three plastic scintillator strips. Actually, we counted the number of muons that were not largely deflected by restricting the zenith angle in one direction to 0.8o. The system could discriminate Fe, Pb and C. Materials lighter than Pb can be also discriminated with this system. This method only resolves the average material distribution along the muon path. Therefore the user must make assumptions or interpretations about the structure, or must use more than one detector to resolve the three dimensional material distribution. By applying this method to time-dependent muon radiography, we can detect changes with time, rendering the method suitable for real-time monitoring applications, possibly providing useful information about the reaction process in a nuclear reactor such as burnup of fuels. In nuclear power technology, burnup (also known as fuel utilization) is a measure of how much energy is extracted from a primary nuclear fuel source. Monitoring the burnup of fuels as a nondestructive inspection technique can contribute to safer operation. In nuclear reactor, the total mass is conserved so that the system cannot be monitored by conventional muon radiography. A plastic scintillator is relatively small and easy to setup compared to a gas or layered scintillation system. Thus, we think this simple radiographic method has the potential to visualize a core directly in cases of normal operations or meltdown accidents. Finally, we considered only three materials as a first step in this work. Further research is required to improve the ability of imaging the material distribution in a mass-conserved system.

A PROBABILISTIC METHOD FOR ESTIMATING MONITORING POINT DENSITY FOR CONTAINMENT SYSTEM LEAK DETECTION

EPA Science Inventory

The use of physical and hydraulic containment systems for the isolation of contaminated ground water and aquifer materials ssociated with hazardous waste sites has increased during the last decade. The existing methodologies for monitoring and evaluating leakage from hazardous w...

Oil defect detection of electrowetting display

NASA Astrophysics Data System (ADS)

Chiang, Hou-Chi; Tsai, Yu-Hsiang; Yan, Yung-Jhe; Huang, Ting-Wei; Mang, Ou-Yang

2015-08-01

In recent years, transparent display is an emerging topic in display technologies. Apply in many fields just like mobile device, shopping or advertising window, and etc. Electrowetting Display (EWD) is one kind of potential transparent display technology advantages of high transmittance, fast response time, high contrast and rich color with pigment based oil system. In mass production process of Electrowetting Display, oil defects should be found by Automated Optical Inspection (AOI) detection system. It is useful in determination of panel defects for quality control. According to the research of our group, we proposed a mechanism of AOI detection system detecting the different kinds of oil defects. This mechanism can detect different kinds of oil defect caused by oil overflow or material deteriorated after oil coating or driving. We had experiment our mechanism with a 6-inch Electrowetting Display panel from ITRI, using an Epson V750 scanner with 1200 dpi resolution. Two AOI algorithms were developed, which were high speed method and high precision method. In high precision method, oil jumping or non-recovered can be detected successfully. This mechanism of AOI detection system can be used to evaluate the oil uniformity in EWD panel process. In the future, our AOI detection system can be used in quality control of panel manufacturing for mass production.

Indirect Estimation of Radioactivity in Containerized Cargo

DOE Office of Scientific and Technical Information (OSTI.GOV)

Jarman, Kenneth D.; Scherrer, Chad; Smith, Eric L.

Detecting illicit nuclear and radiological material in containerized cargo challenges the state of the art in detection systems. Current systems are being evaluated and new systems envisioned to address the need for the high probability of detection and extremely low false alarm rates necessary to thwart potential threats and extremely low nuisance and false alarm rates while maintaining necessary to maintain the flow of commerce impacted by the enormous volume of commodities imported in shipping containers. Maintaining flow of commerce also means that primary inspection must be rapid, requiring relatively indirect measurements of cargo from outside the containers. With increasingmore » information content in such indirect measurements, it is natural to ask how the information might be combined to improved detection. Toward this end, we present an approach to estimating isotopic activity of naturally occurring radioactive material in cargo grouped by commodity type, combining container manifest data with radiography and gamma spectroscopy aligned to location along the container. The heart of this approach is our statistical model of gamma counts within peak regions of interest, which captures the effects of background suppression, counting noise, convolution of neighboring cargo contributions, and down-scattered photons to provide physically constrained estimates of counts due to decay of specific radioisotopes in cargo alone. Coupled to that model, we use a mechanistic model of self-attenuated radiation flux to estimate the isotopic activity within cargo, segmented by location within each container, that produces those counts. We demonstrate our approach by applying it to a set of measurements taken at the Port of Seattle in 2006. This approach to synthesizing disparate available data streams and extraction of cargo characteristics holds the potential to improve primary inspection using current detection capabilities and to enable simulation-based evaluation of new candidate detection systems.« less

Efficient material decomposition method for dual-energy X-ray cargo inspection system

NASA Astrophysics Data System (ADS)

Lee, Donghyeon; Lee, Jiseoc; Min, Jonghwan; Lee, Byungcheol; Lee, Byeongno; Oh, Kyungmin; Kim, Jaehyun; Cho, Seungryong

2018-03-01

Dual-energy X-ray inspection systems are widely used today for it provides X-ray attenuation contrast of the imaged object and also its material information. Material decomposition capability allows a higher detection sensitivity of potential targets including purposely loaded impurities in agricultural product inspections and threats in security scans for example. Dual-energy X-ray transmission data can be transformed into two basis material thickness data, and its transformation accuracy heavily relies on a calibration of material decomposition process. The calibration process in general can be laborious and time consuming. Moreover, a conventional calibration method is often challenged by the nonuniform spectral characteristics of the X-ray beam in the entire field-of-view (FOV). In this work, we developed an efficient material decomposition calibration process for a linear accelerator (LINAC) based high-energy X-ray cargo inspection system. We also proposed a multi-spot calibration method to improve the decomposition performance throughout the entire FOV. Experimental validation of the proposed method has been demonstrated by use of a cargo inspection system that supports 6 MV and 9 MV dual-energy imaging.

Photovoltaic-Pyroelectric Coupled Effect Induced Electricity for Self-Powered Photodetector System.

PubMed

Ma, Nan; Zhang, Kewei; Yang, Ya

2017-12-01

Ferroelectric materials have demonstrated novel photovoltaic effect to scavenge solar energy. However, most of the ferroelectric materials with wide bandgaps (2.7-4 eV) suffer from low power conversion efficiency of less than 0.5% due to absorbing only 8-20% of solar spectrum. Instead of harvesting solar energy, these ferroelectric materials can be well suited for photodetector applications, especially for sensing near-UV irradiations. Here, a ferroelectric BaTiO 3 film-based photodetector is demonstrated that can be operated without using any external power source and a fast sensing of 405 nm light illumination is enabled. As compared with photovoltaic effect, both the responsivity and the specific detectivity of the photodetector can be dramatically enhanced by larger than 260% due to the light-induced photovoltaic-pyroelectric coupled effect. A self-powered photodetector array system can be utilized to achieve spatially resolved light intensity detection by recording the output voltage signals as a mapping figure. © 2017 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

High operation temperature of HgCdTe photodiodes by bulk defect passivation

NASA Astrophysics Data System (ADS)

Boieriu, Paul; Velicu, S.; Bommena, R.; Buurma, C.; Blisset, C.; Grein, C.; Sivananthan, S.; Hagler, P.

2013-01-01

Spatial noise and the loss of photogenerated current due material non-uniformities limit the performance of long wavelength infrared (LWIR) HgCdTe detector arrays. Reducing the electrical activity of defects is equivalent to lowering their density, thereby allowing detection and discrimination over longer ranges. Infrared focal plane arrays (IRFPAs) in other spectral bands will also benefit from detectivity and uniformity improvements. Larger signal-to-noise ratios permit either improved accuracy of detection/discrimination when an IRFPA is employed under current operating conditions, or provide similar performance with the IRFPA operating under less stringent conditions such as higher system temperature, increased system jitter or damaged read out integrated circuit (ROIC) wells. The bulk passivation of semiconductors with hydrogen continues to be investigated for its potential to become a tool for the fabrication of high performance devices. Inductively coupled plasmas have been shown to improve the quality and uniformity of semiconductor materials and devices. The retention of the benefits following various aging conditions is discussed here.

Regional Detection of Decoupled Explosions, Yield Estimation from Surface Waves, Two-Dimensional Source Effects, Three-Dimensional Earthquake Modeling and Automated Magnitude Measures

DTIC Science & Technology

1980-07-01

41 3.2 EXPERIMENTAL DETERMINATION OF THE DEPENDENCE OF RAYLEIGH WAVE AMPLITUDE ON PROPERTIES OF THE SOURCE MATERIAL ...Surface Wave Observations ...... ................ 48 3.3.3 Surface Wave Dependence on Source Material Properties ..... ................ .. 51 SYSTEMS...with various aspects of the problem of estimating yield from single station recordings of surface waves. The material in these four summaries has been

Dual-Phase Lock-In Amplifier Based on FPGA for Low-Frequencies Experiments

PubMed Central

Macias-Bobadilla, Gonzalo; Rodríguez-Reséndiz, Juvenal; Mota-Valtierra, Georgina; Soto-Zarazúa, Genaro; Méndez-Loyola, Maurino; Garduño-Aparicio, Mariano

2016-01-01

Photothermal techniques allow the detection of characteristics of material without invading it. Researchers have developed hardware for some specific Phase and Amplitude detection (Lock-In Function) applications, eliminating space and unnecessary electronic functions, among others. This work shows the development of a Digital Lock-In Amplifier based on a Field Programmable Gate Array (FPGA) for low-frequency applications. This system allows selecting and generating the appropriated frequency depending on the kind of experiment or material studied. The results show good frequency stability in the order of 1.0 × 10−9 Hz, which is considered good linearity and repeatability response for the most common Laboratory Amplitude and Phase Shift detection devices, with a low error and standard deviation. PMID:26999138

Dual-Phase Lock-In Amplifier Based on FPGA for Low-Frequencies Experiments.

PubMed

Macias-Bobadilla, Gonzalo; Rodríguez-Reséndiz, Juvenal; Mota-Valtierra, Georgina; Soto-Zarazúa, Genaro; Méndez-Loyola, Maurino; Garduño-Aparicio, Mariano

2016-03-16

Photothermal techniques allow the detection of characteristics of material without invading it. Researchers have developed hardware for some specific Phase and Amplitude detection (Lock-In Function) applications, eliminating space and unnecessary electronic functions, among others. This work shows the development of a Digital Lock-In Amplifier based on a Field Programmable Gate Array (FPGA) for low-frequency applications. This system allows selecting and generating the appropriated frequency depending on the kind of experiment or material studied. The results show good frequency stability in the order of 1.0 × 10(-9) Hz, which is considered good linearity and repeatability response for the most common Laboratory Amplitude and Phase Shift detection devices, with a low error and standard deviation.

Development of a Miniature Mass Spectrometer and an Automated Detector for Sampling Explosive Materials

PubMed Central

Hashimoto, Yuichiro

2017-01-01

The development of a robust ionization source using the counter-flow APCI, miniature mass spectrometer, and an automated sampling system for detecting explosives are described. These development efforts using mass spectrometry were made in order to improve the efficiencies of on-site detection in areas such as security, environmental, and industrial applications. A development team, including the author, has struggled for nearly 20 years to enhance the robustness and reduce the size of mass spectrometers to meet the requirements needed for on-site applications. This article focuses on the recent results related to the detection of explosive materials where automated particle sampling using a cyclone concentrator permitted the inspection time to be successfully reduced to 3 s. PMID:28337396

Response of the REWARD detection system to the presence of a Radiological Dispersal Device

DOE Office of Scientific and Technical Information (OSTI.GOV)

Luis, R.; Baptista, M.; Barros, S.

2015-07-01

In recent years an increased international concern has emerged about the radiological and nuclear (RN) threats associated with the illicit trafficking of nuclear and radioactive materials that could be potentially used for terrorist attacks. The objective of the REWARD (Real Time Wide Area Radiation Surveillance System) project, co-funded by the European Union 7. Framework Programme Security, consisted in building a mobile system for real time, wide area radiation surveillance, using a CdZnTe detector for gamma radiation and a neutron detector based on novel silicon technologies. The sensing unit includes a GPS system and a wireless communication interface to send themore » data remotely to a monitoring base station, where it will be analyzed in real time and correlated with historical data from the tag location, in order to generate an alarm when an abnormal situation is detected. Due to its portability and accuracy, the system will be extremely useful in many different scenarios such as nuclear terrorism, lost radioactive sources, radioactive contamination or nuclear accidents. This paper shortly introduces the REWARD detection system, depicts some terrorist threat scenarios involving radioactive sources and special nuclear materials and summarizes the simulation work undertaken during the past three years in the framework of the REWARD project. The main objective consisted in making predictions regarding the behavior of the REWARD system in the presence of a Radiological Dispersion Device (RDD), one of the reference scenarios foreseen for REWARD, using the Monte Carlo simulation program MCNP6. The reference scenario is characterized in detail, from the i) radiological protection, ii) radiation detection requirements and iii) communications points of view. Experimental tests were performed at the Fire Brigades Facilities in Rome and at the Naples Fire Brigades, and the results, which validate the simulation work, are presented and analyzed. The response of the REWARD detection system to the presence of an RDD is predicted and discussed. (authors)« less

Line-scanning Raman imaging spectroscopy for detection of fingerprints.

PubMed

Deng, Sunan; Liu, Le; Liu, Zhiyi; Shen, Zhiyuan; Li, Guohua; He, Yonghong

2012-06-10

Fingerprints are the best form of personal identification for criminal investigation purposes. We present a line-scanning Raman imaging system and use it to detect fingerprints composed of β-carotene and fish oil on different substrates. Although the line-scanning Raman system has been used to map the distribution of materials such as polystyrene spheres and minerals within geological samples, this is the first time to our knowledge that the method is used in imaging fingerprints. Two Raman peaks of β-carotene (501.2, 510.3 nm) are detected and the results demonstrate that both peaks can generate excellent images with little difference between them. The system operates at a spectra resolution of about 0.4 nm and can detect β-carotene signals in petroleum ether solution with the limit of detection of 3.4×10(-9) mol/L. The results show that the line-scanning Raman imaging spectroscopy we have built has a high accuracy and can be used in the detection of latent fingerprints in the future.

Natural frequency identification of smart washer by using adaptive observer

NASA Astrophysics Data System (ADS)

Ito, Hitoshi; Okugawa, Masayuki

2014-04-01

Bolted joints are used in many machines/structures and some of them have been loosened during long time use, and unluckily these bolt loosening may cause a great accident of machines/structures system. These bolted joint, especially in important places, are main object of maintenance inspection. Maintenance inspection with human- involvement is desired to be improved owing to time-consuming, labor-intensive and high-cost. By remote and full automation monitoring of the bolt loosening, constantly monitoring of bolted joint is achieved. In order to detect loosening of bolted joints without human-involvement, applying a structural health monitoring technique and smart structures/materials concept is the key objective. In this study, a new method of bolt loosening detection by adopting a smart washer has been proposed, and the basic detection principle was discussed with numerical analysis about frequency equation of the system, was confirmed experimentally. The smart washer used in this study is in cantilever type with piezoelectric material, which adds the washer the self-sensing and actuation function. The principle used to detect the loosening of the bolts is a method of a bolt loosening detection noted that the natural frequency of a smart washer system is decreasing by the change of the bolt tightening axial tension. The feature of this proposed method is achieving to identify the natural frequency at current condition on demand by adopting the self-sensing and actuation function and system identification algorithm for varying the natural frequency depending the bolt tightening axial tension. A novel bolt loosening detection method by adopting adaptive observer is proposed in this paper. The numerical simulations are performed to verify the possibility of the adaptive observer-based loosening detection. Improvement of the detection accuracy for a bolt loosening is confirmed by adopting initial parameter and variable adaptive gain by numerical simulation.

The effects of different restorative materials on the detection of approximal caries in cone-beam computed tomography scans with and without metal artifact reduction mode.

PubMed

Cebe, Fatma; Aktan, Ali Murat; Ozsevik, Abdul Semih; Ciftci, Mehmet Ertugrul; Surmelioglu, Hatice Derya

2017-03-01

The aim of this study was to investigate the influence of artifacts produced by different restorative materials on the detection of approximal caries in cone-beam computed tomography (CBCT) scans with and without the application of an artifact-reduction (AR) option. Ninety-eight noncavitated premolar and molar teeth were placed with approximal contacts consisting of 2 sound or carious teeth and 1 mesial-occlusal-distal restored tooth with resin-modified glass-ionomer cement (RMGIC), amalgam, composite, ceramic-based composite (CBC), or computer-aided design-computer-aided manufacturing (CAD-CAM) zirconia materials in between. The teeth were scanned with a CBCT system with and without the AR option. Images were evaluated by 2 observers. The teeth were histologically evaluated, and sensitivity, specificity, and areas under the receiver operating characteristic (ROC) curve were calculated according to the appropriate threshold. Specificity and sensitivity values for contact surfaces ranged from 0-48.39 and 82.93-98.40, respectively. The AR option affected (P < .05) approximal caries detection of the amalgam, composite, CAD-CAM, and CBC groups in contact surfaces and composite and RMGIC groups in noncontact surfaces. Artifacts produced by different restorative materials could affect approximal caries detection in CBCT scans. Use of the AR option with CBCT scans increases the accuracy of approximal caries detection. Copyright © 2016 Elsevier Inc. All rights reserved.

Vision inspection system and method

NASA Technical Reports Server (NTRS)

Huber, Edward D. (Inventor); Williams, Rick A. (Inventor)

1997-01-01

An optical vision inspection system (4) and method for multiplexed illuminating, viewing, analyzing and recording a range of characteristically different kinds of defects, depressions, and ridges in a selected material surface (7) with first and second alternating optical subsystems (20, 21) illuminating and sensing successive frames of the same material surface patch. To detect the different kinds of surface features including abrupt as well as gradual surface variations, correspondingly different kinds of lighting are applied in time-multiplexed fashion to the common surface area patches under observation.

Ampoule Failure System

NASA Technical Reports Server (NTRS)

Watring, Dale A. (Inventor); Johnson, Martin L. (Inventor)

1996-01-01

An ampoule failure system for use in material processing furnaces comprising a containment cartridge and an ampoule failure sensor. The containment cartridge contains an ampoule of toxic material therein and is positioned within a furnace for processing. An ampoule failure probe is positioned in the containment cartridge adjacent the ampoule for detecting a potential harmful release of toxic material therefrom during processing. The failure probe is spaced a predetermined distance from the ampoule and is chemically chosen so as to undergo a timely chemical reaction with the toxic material upon the harmful release thereof. The ampoule failure system further comprises a data acquisition system which is positioned externally of the furnace and is electrically connected to the ampoule failure probe so as to form a communicating electrical circuit. The data acquisition system includes an automatic shutdown device for shutting down the furnace upon the harmful release of toxic material. It also includes a resistance measuring device for measuring the resistance of the failure probe during processing. The chemical reaction causes a step increase in resistance of the failure probe whereupon the automatic shutdown device will responsively shut down the furnace.

A binned clustering algorithm to detect high-Z material using cosmic muons

NASA Astrophysics Data System (ADS)

Thomay, C.; Velthuis, J. J.; Baesso, P.; Cussans, D.; Morris, P. A. W.; Steer, C.; Burns, J.; Quillin, S.; Stapleton, M.

2013-10-01

We present a novel approach to the detection of special nuclear material using cosmic rays. Muon Scattering Tomography (MST) is a method for using cosmic muons to scan cargo containers and vehicles for special nuclear material. Cosmic muons are abundant, highly penetrating, not harmful for organic tissue, cannot be screened against, and can easily be detected, which makes them highly suited to the use of cargo scanning. Muons undergo multiple Coulomb scattering when passing through material, and the amount of scattering is roughly proportional to the square of the atomic number Z of the material. By reconstructing incoming and outgoing tracks, we can obtain variables to identify high-Z material. In a real life application, this has to happen on a timescale of 1 min and thus with small numbers of muons. We have built a detector system using resistive plate chambers (RPCs): 12 layers of RPCs allow for the readout of 6 x and 6 y positions, by which we can reconstruct incoming and outgoing tracks. In this work we detail the performance of an algorithm by which we separate high-Z targets from low-Z background, both for real data from our prototype setup and for MC simulation of a cargo container-sized setup. (c) British Crown Owned Copyright 2013/AWE

Spectral feature variations in x-ray diffraction imaging systems

NASA Astrophysics Data System (ADS)

Wolter, Scott D.; Greenberg, Joel A.

2016-05-01

Materials with different atomic or molecular structures give rise to unique scatter spectra when measured by X-ray diffraction. The details of these spectra, though, can vary based on both intrinsic (e.g., degree of crystallinity or doping) and extrinsic (e.g., pressure or temperature) conditions. While this sensitivity is useful for detailed characterizations of the material properties, these dependences make it difficult to perform more general classification tasks, such as explosives threat detection in aviation security. A number of challenges, therefore, currently exist for reliable substance detection including the similarity in spectral features among some categories of materials combined with spectral feature variations from materials processing and environmental factors. These factors complicate the creation of a material dictionary and the implementation of conventional classification and detection algorithms. Herein, we report on two prominent factors that lead to variations in spectral features: crystalline texture and temperature variations. Spectral feature comparisons between materials categories will be described for solid metallic sheet, aqueous liquids, polymer sheet, and metallic, organic, and inorganic powder specimens. While liquids are largely immune to texture effects, they are susceptible to temperature changes that can modify their density or produce phase changes. We will describe in situ temperature-dependent measurement of aqueous-based commercial goods in the temperature range of -20°C to 35°C.

International Conference on Control and Estimation of Distributed Parameter Systems: Nonlinear Phenomena Held in Vorau, Austria on July 18-24, 1993

DTIC Science & Technology

1993-07-24

detection anit charact(erization in smart material structures 21 NI. BER;OUNIoUX, T. N’IANNIKK6) AN) D. TmIA: Optimnality conditions for non-qumalified...UISA DAMAGE DETECTION AND CHARACTERIZATION IN SMART MATERIAL STRUCTURES HI. TF. BANKS AND) Y, WAN(, C~enter for Rtsvarchliti Scientific Cumpiptatioii...111,u’, + +pt,’, ,x 123 22 (3.3) 0~’ ={( othi’i-wist’. Wie iitmt sought to dlemnonstrat~e tiht capabliity of1 pieoll"t~tItrit m~aterialds inl smart

Combination neutron-gamma ray detector

DOEpatents

Stuart, Travis P.; Tipton, Wilbur J.

1976-10-26

A radiation detection system capable of detecting neutron and gamma events and distinguishing therebetween. The system includes a detector for a photomultiplier which utilizes a combination of two phosphor materials, the first of which is in the form of small glass beads which scintillate primarily in response to neutrons and the second of which is a plastic matrix which scintillates in response to gammas. A combination of pulse shape and pulse height discrimination techniques is utilized to provide an essentially complete separation of the neutron and gamma events.

Uncooled infrared photon detector and multicolor infrared detection using microoptomechanical sensors

DOEpatents

Datskos, Panagiotis G.; Rajic, Solobodan; Datskou, Irene C.

1999-01-01

Systems and methods for infrared detection are described. An optomechanical photon detector includes a semiconductor material and is based on measurement of a photoinduced lattice strain. A multicolor infrared sensor includes a stack of frequency specific optomechanical detectors. The stack can include one, or more, of the optomechanical photon detectors that function based on the measurement of photoinduced lattice strain. The systems and methods provide advantages in that rapid, sensitive multicolor infrared imaging can be performed without the need for a cooling subsystem.

Surface-enhanced Raman detection of CW agents in water using gold sol gel substrates

NASA Astrophysics Data System (ADS)

Premasiri, W. Ranjith; Clarke, Richard H.; Womble, M. Edward

2002-02-01

The development of a water analysis system capable of detecting both inanimate trace chemical contaminants and viable microbial contaminants has long been a project of interest to our group. The capability of detecting both chemical and biological agent sources in a single device configuration would clearly add to the value of such a product. In the present work, we describe results with chemical warfare agents from our efforts to produce a Raman system for the detection of both chemical and biological warfare agents in water. We utilize laser Raman light scattering and employ Surface Enhanced Raman Spectroscopy (SERS)on solid state gold sol-gel detectors combined with fiber optic collection of the enhanced light signal in the sampling system to augment the normally low intensity Raman Scattering signal from trace materials.

Guided Wave Sensing In a Carbon Steel Pipe Using a Laser Vibrometer System

NASA Astrophysics Data System (ADS)

Ruíz Toledo, Abelardo; Salazar Soler, Jordi; Chávez Domínguez, Juan Antonio; García Hernández, Miguel Jesús; Turó Peroy, Antoni

2010-05-01

Non-Destructive Evaluation (NDE) techniques have achieved a great development during the last decades as a valuable tool for material characterization, manufacturing control and structural integrity tests. Among these tools, the guided wave technology has been rapidly extended because it reduces inspection time and costs compared to the ordinary point by point testing in large structures, as well as because of the possibility of inspecting under insulation and coating conditions. This fast development has motivated the creation of several inspection and material characterization systems including different technologies which can be combined with this technique. Different measurements systems based on laser techniques have been presented in order to inspect pipes, plates and diverse structures. Many of them are experimental systems of high cost and complexity which combine the employment of a laser for generation of waves in the structure and an interferometer for detection. Some of them employ air-coupled ultrasound generation transducers, with high losses in air and which demand high energy for exciting waves in materials of high stiffness. The combined employment of a commercial vibrometer system for Lamb wave sensing in plates has been successfully shown in the literature. In this paper we present a measurement system based on the combined employment of a piezoelectric wedge transducer and a laser vibrometer to sense guided acoustic waves in carbon steel pipes. The measurement system here presented is mainly compounded of an angular wedge transducer, employed to generate the guided wave and a commercial laser vibrometer used in the detection process. The wedge transducer is excited by means of a signal function generator whose output signal has been amplified with a power signal amplifier. A high precision positioning system is employed to place the laser beam at different points through the pipe surface. The signal detected by the laser vibrometer system is amplified with a signal amplifier and then it is displayed in a digital storage oscilloscope. This set-up offers the possibility of analyzing in a simpler way the wave propagation and the material evaluation in pipes of certain wall thickness. The material characterization considering distinct wave propagation modes can be easily achieved, changing the different incident angles of the wedge piezoelectric probe and their combined employment with several driving signals. Moreover, this experimental sensing system offers other possibilities of inspecting and analyzing the wave propagation in some features (bends, flange joints, welds,…) of the pipe surface which cause very large reflections and mode conversions and which in practice limits the inspection range when are inspected with conventional receiving transducer arrangements.

Miniature Laboratory for Detecting Sparse Biomolecules

NASA Technical Reports Server (NTRS)

Lin, Ying; Yu, Nan

2005-01-01

A miniature laboratory system has been proposed for use in the field to detect sparsely distributed biomolecules. By emphasizing concentration and sorting of specimens prior to detection, the underlying system concept would make it possible to attain high detection sensitivities without the need to develop ever more sensitive biosensors. The original purpose of the proposal is to aid the search for signs of life on a remote planet by enabling the detection of specimens as sparse as a few molecules or microbes in a large amount of soil, dust, rocks, water/ice, or other raw sample material. Some version of the system could prove useful on Earth for remote sensing of biological contamination, including agents of biological warfare. Processing in this system would begin with dissolution of the raw sample material in a sample-separation vessel. The solution in the vessel would contain floating microscopic magnetic beads coated with substances that could engage in chemical reactions with various target functional groups that are parts of target molecules. The chemical reactions would cause the targeted molecules to be captured on the surfaces of the beads. By use of a controlled magnetic field, the beads would be concentrated in a specified location in the vessel. Once the beads were thus concentrated, the rest of the solution would be discarded. This procedure would obviate the filtration steps and thereby also eliminate the filter-clogging difficulties of typical prior sample-concentration schemes. For ferrous dust/soil samples, the dissolution would be done first in a separate vessel before the solution is transferred to the microbead-containing vessel.

PubMed

Miranda, Geraldo Elias; Melani, Rodolfo Francisco Haltenhoff; Francisquini, Luiz; Daruge, Eduardo

2017-01-01

The aim of this study was to identify the combination of wavelength and filter that best detects tooth and bone, and to determine which biological materials (enamel, dental root or bone) have highest fluorescence intensity when exposed to an alternate light source (ALS). Tooth and bone samples were lighted with ALS and photographed. Adobe Photoshop™ and ImageJ™ softwares were used for image analysis. Data obtained by measuring the photograph pixels were subjected to analysis of variance. The mean values of significant effects were compared by the Tukey test. In all tests, the significance level was set at p≤0.05 and the values calculated by the SAS system. The results showed that the best combination for detecting tooth and bone is an illumination wavelength of 455 nm with an orange filter. The fluorescence of dental root is greater than that of enamel, which in turn is greater than that of bone. The biological material had markedly higher fluorescence than the inert material. This knowledge can help the forensic expert to screen and detect biological materials, for example in situations where there are fragmented teeth and small bones, both at the scene and in the laboratory.

The design and performance of a scintillating-fibre tracker for the cosmic-ray muon tomography of legacy nuclear waste containers

NASA Astrophysics Data System (ADS)

Clarkson, A.; Hamilton, D. J.; Hoek, M.; Ireland, D. G.; Johnstone, J. R.; Kaiser, R.; Keri, T.; Lumsden, S.; Mahon, D. F.; McKinnon, B.; Murray, M.; Nutbeam-Tuffs, S.; Shearer, C.; Staines, C.; Yang, G.; Zimmerman, C.

2014-05-01

Tomographic imaging techniques using the Coulomb scattering of cosmic-ray muons are increasingly being exploited for the non-destructive assay of shielded containers in a wide range of applications. One such application is the characterisation of legacy nuclear waste materials stored within industrial containers. The design, assembly and performance of a prototype muon tomography system developed for this purpose are detailed in this work. This muon tracker comprises four detection modules, each containing orthogonal layers of Saint-Gobain BCF-10 2 mm-pitch plastic scintillating fibres. Identification of the two struck fibres per module allows the reconstruction of a space point, and subsequently, the incoming and Coulomb-scattered muon trajectories. These allow the container content, with respect to the atomic number Z of the scattering material, to be determined through reconstruction of the scattering location and magnitude. On each detection layer, the light emitted by the fibre is detected by a single Hamamatsu H8500 MAPMT with two fibres coupled to each pixel via dedicated pairing schemes developed to ensure the identification of the struck fibre. The PMT signals are read out to standard charge-to-digital converters and interpreted via custom data acquisition and analysis software. The design and assembly of the detector system are detailed and presented alongside results from performance studies with data collected after construction. These results reveal high stability during extended collection periods with detection efficiencies in the region of 80% per layer. Minor misalignments of millimetre order have been identified and corrected in software. A first image reconstructed from a test configuration of materials has been obtained using software based on the Maximum Likelihood Expectation Maximisation algorithm. The results highlight the high spatial resolution provided by the detector system. Clear discrimination between the low, medium and high-Z materials assayed is also observed.

Methods and approaches of utilizing ionic liquids as gas sensing materials

PubMed Central

Rehman, Abdul

2017-01-01

Gas monitoring is of increasing significance for a broad range of applications in the fields of environmental and civil infrastructures, climate and energy, health and safety, industry and commerce. Even though there are many gas detection devices and systems available, the increasing needs for better detection technologies that not only satisfy the high analytical standards but also meet additional device requirements (e.g., being robust to survive under field conditions, low cost, small, smart, more mobile), demand continuous efforts in developing new methods and approaches for gas detection. Ionic Liquids (ILs) have attracted a tremendous interest as potential sensing materials for the gas sensor development. Being composed entirely of ions and with a broad structural and functional diversity, i.e., bifunctional (organic/inorganic), biphasic (solid/liquid) and dual-property (solvent/electrolyte), they have the complementing attributes and the required variability to allow a systematic design process across many sensing components to enhance sensing capability especially for miniaturized sensor system implementation. The emphasis of this review is to describe molecular design and control of IL interface materials to provide selective and reproducible response and to synergistically integrate IL sensing materials with low cost and low power electrochemical, piezoelectric/QCM and optical transducers to address many gas detection challenges (e.g., sensitivity, selectivity, reproducibility, speed, stability, cost, sensor miniaturization, and robustness). We further show examples to justify the importance of understanding the mechanisms and principles of physicochemical and electrochemical reactions in ILs and then link those concepts to developing new sensing methods and approaches. By doing this, we hope to stimulate further research towards the fundamental understanding of the sensing mechanisms and new sensor system development and integration, using simple sensing designs and flexible sensor structures both in terms of scientific operation and user interface that can be miniaturized and interfaced with modern wireless monitoring technologies to achieve specifications heretofore unavailable on current markets for the next generation of gas sensor applications. PMID:29142738

Improved sensing using simultaneous deep-UV Raman and fluorescence detection-II

NASA Astrophysics Data System (ADS)

Hug, W. F.; Bhartia, R.; Sijapati, K.; Beegle, L. W.; Reid, R. D.

2014-05-01

Photon Systems in collaboration with JPL is continuing development of a new technology robot-mounted or hand-held sensor for reagentless, short-range, standoff detection and identification of trace levels chemical, biological, and explosive (CBE) materials on surfaces. This deep ultraviolet CBE sensor is the result of Army STTR and DTRA programs. The evolving 10 to 15 lb, 20 W, sensor can discriminate CBE from background clutter materials using a fusion of deep UV excited resonance Raman (RR) and laser induced native fluorescence (LINF) emissions collected is less than 1 ms. RR is a method that provides information about molecular bonds, while LINF spectroscopy is a much more sensitive method that provides information regarding the electronic configuration of target molecules. Standoff excitation of suspicious packages, vehicles, persons, and other objects that may contain hazardous materials is accomplished using excitation in the deep UV where there are four main advantages compared to near-UV, visible or near-IR counterparts. 1) Excited between 220 and 250 nm, Raman emission occur within a fluorescence-free region of the spectrum, eliminating obscuration of weak Raman signals by fluorescence from target or surrounding materials. 2) Because Raman and fluorescence occupy separate spectral regions, detection can be done simultaneously, providing an orthogonal set of information to improve both sensitivity and lower false alarm rates. 3) Rayleigh law and resonance effects increase Raman signal strength and sensitivity of detection. 4) Penetration depth into target in the deep UV is short, providing spatial/spectral separation of a target material from its background or substrate. 5) Detection in the deep UV eliminates ambient light background and enable daylight detection.

Chemically-functionalized microcantilevers for detection of chemical, biological and explosive material

DOEpatents

Pinnaduwage, Lal A [Knoxville, TN; Thundat, Thomas G [Knoxville, TN; Brown, Gilbert M [Knoxville, TN; Hawk, John Eric [Olive Branch, MS; Boiadjiev, Vassil I [Knoxville, TN

2007-04-24

A chemically functionalized cantilever system has a cantilever coated on one side thereof with a reagent or biological species which binds to an analyte. The system is of particular value when the analyte is a toxic chemical biological warfare agent or an explosive.

Method for warning of radiological and chemical substances using detection paints on a vehicle surface

DOEpatents

Farmer, Joseph C [Tracy, CA

2012-03-13

A system for warning of corrosion, chemical, or radiological substances. The system comprises painting a surface with a paint or coating that includes an indicator material and monitoring the surface for indications of the corrosion, chemical, or radiological substances.

Surface with two paint strips for detection and warning of chemical warfare and radiological agents

DOEpatents

Farmer, Joseph C.

2013-04-02

A system for warning of corrosion, chemical, or radiological substances. The system comprises painting a surface with a paint or coating that includes an indicator material and monitoring the surface for indications of the corrosion, chemical, or radiological substances.

Implications for Planetary System Formation from Interstellar Object 1I/2017 U1 (‘Oumuamua)

NASA Astrophysics Data System (ADS)

Trilling, David E.; Robinson, Tyler; Roegge, Alissa; Chandler, Colin Orion; Smith, Nathan; Loeffler, Mark; Trujillo, Chad; Navarro-Meza, Samuel; Glaspie, Lori M.

2017-12-01

The recently discovered minor body 1I/2017 U1 (‘Oumuamua) is the first known object in our solar system that is not bound by the Sun’s gravity. Its hyperbolic orbit (eccentricity greater than unity) strongly suggests that it originated outside our solar system; its red color is consistent with substantial space weathering experienced over a long interstellar journey. We carry out a simple calculation of the probability of detecting such an object. We find that the observed detection rate of 1I-like objects can be satisfied if the average mass of ejected material from nearby stars during the process of planetary formation is ˜20 Earth masses, similar to the expected value for our solar system. The current detection rate of such interstellar interlopers is estimated to be 0.2 yr-1, and the expected number of detections over the past few years is almost exactly one. When the Large Synoptic Survey Telescope begins its wide, fast, deep all-sky survey, the detection rate will increase to 1 yr-1. Those expected detections will provide further constraints on nearby planetary system formation through a better estimate of the number and properties of interstellar objects.

Systems and methods for detecting nuclear radiation in the presence of backgrounds

DOEpatents

Bross, Alan D.; Mellott, Kerry L.; Pla-Dalmau, Anna

2005-06-21

Systems and methods for the simultaneous detection and identification of radiation species, including neutrons, gammas/x-rays and minimum ionizing particles (MIPs). A plurality of rectangular and/or triangularly shaped radiation sensitive scintillators can be configured from a plurality of nano-sized particles, dopants and an extruded plastic material. A wavelength-shifting fiber can then be located within a central hole of each extruded scintillator, wherein the wavelength-shifting fiber absorbs scintillation light and re-emits the light at a longer wavelength, thereby piping the light to a photodetector whose response to the light indicates the presence of radiation The resulting method and system can simultaneously detect neutrons, gamma rays, x-rays and cosmic rays (MIPs) and identify each.

Compositional mapping of Saturn's satellite Dione with Cassini VIMS and implications of dark material in the Saturn system

USGS Publications Warehouse

Clark, R.N.; Curchin, J.M.; Jaumann, R.; Cruikshank, D.P.; Brown, R.H.; Hoefen, T.M.; Stephan, K.; Moore, Johnnie N.; Buratti, B.J.; Baines, K.H.; Nicholson, P.D.; Nelson, R.M.

2008-01-01

Cassini VIMS has obtained spatially resolved imaging spectroscopy data on numerous satellites of Saturn. A very close fly-by of Dione provided key information for solving the riddle of the origin of the dark material in the Saturn system. The Dione VIMS data show a pattern of bombardment of fine, sub-0.5-??m diameter particles impacting the satellite from the trailing side direction. Multiple lines of evidence point to an external origin for the dark material on Dione, including the global spatial pattern of dark material, local patterns including crater and cliff walls shielding implantation on slopes facing away from the trailing side, exposing clean ice, and slopes facing the trailing direction which show higher abundances of dark material. Multiple spectral features of the dark material match those seen on Phoebe, Iapetus, Hyperion, Epimetheus and the F-ring, implying the material has a common composition throughout the Saturn system. However, the exact composition of the dark material remains a mystery, except that bound water and, tentatively, ammonia are detected, and there is evidence both for and against cyanide compounds. Exact identification of composition requires additional laboratory work. A blue scattering peak with a strong UV-visible absorption is observed in spectra of all satellites which contain dark material, and the cause is Rayleigh scattering, again pointing to a common origin. The Rayleigh scattering effect is confirmed with laboratory experiments using ice and 0.2-??m diameter carbon grains when the carbon abundance is less than about 2% by weight. Rayleigh scattering in solids is also confirmed in naturally occurring terrestrial rocks, and in previously published reflectance studies. The spatial pattern, Rayleigh scattering effect, and spectral properties argue that the dark material is only a thin coating on Dione's surface, and by extension is only a thin coating on Phoebe, Hyperion, and Iapetus, although the dark material abundance appears higher on Iapetus, and may be locally thick. As previously concluded for Phoebe, the dark material appears to be external to the Saturn system and may be cometary in origin. We also report a possible detection of material around Dione which may indicate Dione is active and contributes material to the E-ring, but this observation must be confirmed.

THz computed tomography system with zero-order Bessel beam

NASA Astrophysics Data System (ADS)

Niu, Liting; Wu, Qiao; Wang, Kejia; Liu, Jinsong; Yang, Zhengang

2018-01-01

Terahertz (THz) waves can penetrate many optically opaque dielectric materials such as plastics, ceramics and colorants. It is effective to reveal the internal structures of these materials. We have built a THz Computed Tomography (CT) system with 0.3 THz zero-order Bessel beam to improve the depth of focus of this imaging system for the non-diffraction property of Bessel beam. The THz CT system has been used to detect a paper cup with a metal rod inside. Finally, the acquired projection data have been processed by the filtered back-projection algorithm and the reconstructed image of the sample has been obtained.

A macroscopic non-destructive testing system based on the cantilever-sample contact resonance

NASA Astrophysics Data System (ADS)

Fu, Ji; Lin, Lizhi; Zhou, Xilong; Li, Yingwei; Li, Faxin

2012-12-01

Detecting the inside or buried defects in materials and structures is always a challenge in the field of nondestructive testing (NDT). In this paper, enlightened by the operation principle of the contact resonance force microscopy or atomic force acoustic microscopy (AFAM), we proposed a macroscopic NDT system based on contact resonance of the cantilever-sample surface to detect the local stiffness variations in materials or structures. We fabricated a piezoelectric unimorph with the dimension typically of 150 mm × 8 mm × 2 mm to act as a macroscopic cantilever, whose flexural mode vibration was driven by a wideband power amplifier together with a signal generator. The vibration signal of the macroscopic cantilever is detected by a high sensitive strain gauge bonded on the cantilever surface which is much more stable than the laser diode sensor in AFAM, thus making it very suitable for outdoor operations. Scanning is realized by a three-dimensional motorized stage with the Z axis for pressing force setting. The whole system is controlled by a LabVIEW-based homemade software. Like the AFAM, this NDT system can also work in two modes, i.e., the single-frequency mode and the resonance-tracking mode. In the latter mode, the contact stiffness at each pixel of the sample can be obtained by using the measured contact resonance frequency and a beam dynamics model. Testing results of this NDT system on a grid structure with an opaque panel show that in both modes the prefabricated defect beneath the panel can be detected and the grid structures can be clearly "seen," which indicates the validity of this NDT system. The sensitivity of this NDT system was also examined.

High reliability - low noise radionuclide signature identification algorithms for border security applications

NASA Astrophysics Data System (ADS)

Lee, Sangkyu

Illicit trafficking and smuggling of radioactive materials and special nuclear materials (SNM) are considered as one of the most important recent global nuclear threats. Monitoring the transport and safety of radioisotopes and SNM are challenging due to their weak signals and easy shielding. Great efforts worldwide are focused at developing and improving the detection technologies and algorithms, for accurate and reliable detection of radioisotopes of interest in thus better securing the borders against nuclear threats. In general, radiation portal monitors enable detection of gamma and neutron emitting radioisotopes. Passive or active interrogation techniques, present and/or under the development, are all aimed at increasing accuracy, reliability, and in shortening the time of interrogation as well as the cost of the equipment. Equally important efforts are aimed at advancing algorithms to process the imaging data in an efficient manner providing reliable "readings" of the interiors of the examined volumes of various sizes, ranging from cargos to suitcases. The main objective of this thesis is to develop two synergistic algorithms with the goal to provide highly reliable - low noise identification of radioisotope signatures. These algorithms combine analysis of passive radioactive detection technique with active interrogation imaging techniques such as gamma radiography or muon tomography. One algorithm consists of gamma spectroscopy and cosmic muon tomography, and the other algorithm is based on gamma spectroscopy and gamma radiography. The purpose of fusing two detection methodologies per algorithm is to find both heavy-Z radioisotopes and shielding materials, since radionuclides can be identified with gamma spectroscopy, and shielding materials can be detected using muon tomography or gamma radiography. These combined algorithms are created and analyzed based on numerically generated images of various cargo sizes and materials. In summary, the three detection methodologies are fused into two algorithms with mathematical functions providing: reliable identification of radioisotopes in gamma spectroscopy; noise reduction and precision enhancement in muon tomography; and the atomic number and density estimation in gamma radiography. It is expected that these new algorithms maybe implemented at portal scanning systems with the goal to enhance the accuracy and reliability in detecting nuclear materials inside the cargo containers.

Inspection of defects of composite materials in inner cylindrical surfaces using endoscopic shearography

NASA Astrophysics Data System (ADS)

Macedo, Fabiano Jorge; Benedet, Mauro Eduardo; Fantin, Analucia Vieira; Willemann, Daniel Pedro; da Silva, Fábio Aparecido Alves; Albertazzi, Armando

2018-05-01

This work presents the development of a special shearography system with radial sensitivity and explores its applicability for detecting adhesion flaws on internal surfaces of flanged joints of composite material pipes. The inspection is performed from the inner surface of the tube where the flange is adhered. The system uses two conical mirrors to achieve radial sensitivity. A primary 45° conical mirror is responsible for promoting the inspection of the internal tubular surface on its 360° A special Michelson interferometer is formed replacing one of the plane mirrors by a conical mirror. The image reflected by this conical mirror is shifted away from the image center in a radial way and a radial shear is produced on the images. The concept was developed and a prototype built and tested. First, two tubular steel specimens internally coated with composite material and having known artificial defects were analyzed to test the ability of the system to detect the flaws. After the principle validation, two flanged joints were then analyzed: (a) a reference one, without any artificial defects and (b) a test one with known artificial defects, simulating adhesion failures with different dimensions and locations. In all cases, thermal loading was applied through a hot air blower on the outer surface of the joint. The system presented very good results on all inspected specimens, being able to detect adhesion flaws present in the flanged joints. The experimental results obtained in this work are promising and open a new front for inspections of inner surfaces of pipes with shearography.

Wet Oxidation as a Waste Treatment Method in Closed Systems

NASA Technical Reports Server (NTRS)

Onisko, B. L.; Wydeven, T.

1982-01-01

The chemistry of the wet oxidation process was investigated in relation to production of plant nutrients from plant and human waste materials as required for a closed life support system. Hydroponically grown lettuce plants were used as a model plant waste, and oxygen gas was used as an oxidant. Organic nitrogen content was decreased 88-100%, depending on feed material. Production of ammonia and nitrogen gas accounted for all of the observed decrease in organic nitrogen content. No nitrous oxide (N2O) was detected. The implications of these results for closed life support systems are discussed.

Wet oxidation as a waste treatment in closed systems

NASA Technical Reports Server (NTRS)

Onisko, B. L.; Wydeven, T.

1981-01-01

The chemistry of the wet oxidation process has been investigated in relation to production of plant nutrients from plant and human waste materials as required for a closed life-support system. Hydroponically grown lettuce plants were used as a model plant waste and oxygen gas was used as oxidant. Organic nitrogen content was decreased 88-100% depending on feed material. Production of ammonia and nitrogen gas account for all of the observed decrease in organic nitrogen content. No nitrous oxide (N2O) was detected. The implications of these results for closed life-support systems are discussed.

In-field tests of the EURITRACK tagged neutron inspection system

NASA Astrophysics Data System (ADS)

Carasco, C.; Perot, B.; Bernard, S.; Mariani, A.; Szabo, J.-L.; Sannie, G.; Roll, Th.; Valkovic, V.; Sudac, D.; Viesti, G.; Lunardon, M.; Bottosso, C.; Fabris, D.; Nebbia, G.; Pesente, S.; Moretto, S.; Zenoni, A.; Donzella, A.; Moszynski, M.; Gierlik, M.; Batsch, T.; Wolski, D.; Klamra, W.; Le Tourneur, P.; Lhuissier, M.; Colonna, A.; Tintori, C.; Peerani, P.; Sequeira, V.; Salvato, M.

2008-04-01

The EURopean Illicit TRAfficking Countermeasures Kit (EURITRACK) inspection system has been designed to complement X-ray scanners in the detection of explosives and other illicit materials hidden in cargo containers. The containers are interrogated by a 14-MeV tagged neutron beam at any suspect position in the X-ray image. Interrogation of a specific volume element with tagged neutrons yields information about the chemical composition of the material. Implementation and performance tests of the EURITRACK system in the Port of Rijeka in Croatia are described. Cargo container inspection results are reported and discussed.

Integrated Optoelectronics for Parallel Microbioanalysis

NASA Technical Reports Server (NTRS)

Stirbl, Robert; Moynihan, Philip; Bearman, Gregory; Lane, Arthur

2003-01-01

Miniature, relatively inexpensive microbioanalytical systems ("laboratory-on-achip" devices) have been proposed for the detection of hazardous microbes and toxic chemicals. Each system of this type would include optoelectronic sensors and sensor-output-processing circuitry that would simultaneously look for the optical change, fluorescence, delayed fluorescence, or phosphorescence signatures from multiple redundant sites that have interacted with the test biomolecules in order to detect which one(s) was present in a given situation. These systems could be used in a variety of settings that could include doctors offices, hospitals, hazardous-material laboratories, biological-research laboratories, military operations, and chemical-processing plants.

Design of an automated cart and mount for a hyperspectral imaging system to be used in produce fields

USDA-ARS?s Scientific Manuscript database

The goal of this project was to construct a cart and a mounting system that would allow a hyperspectral laser-induced fluorescence imaging system (HLIFIS) to be used to detect fecal material in produce fields. Fecal contaminated produce is a recognized food safety risk. Previous research demonstrate...

Systems to Detect Bacterial Contamination of Banked Blood in a Rapid, Non-Invasive Low Technology Manner. Phase 1.

DTIC Science & Technology

1994-08-25

Department of the Army position, policy or decision unless so designated by other documentation. 94-30800 IIV III !111 IiI I ’ I foron Appr •vedREPORT...copyrighted material is quoted, permission has been obtained to use such material. Where material from documents designated for limited distribution is...Laser Scanning Densitometry for quantitation of the color changes. (6) Narrative: a. Eperimental Methods: 1. Bacteria: Ten bacterial species

Stand-off spectroscopy for the detection of chemical warfare agents

NASA Astrophysics Data System (ADS)

Clewes, Rhea J.; Howle, Chris R.; Stothard, David J. M.; Dunn, Malcolm H.; Robertson, Gordon; Miller, William; Malcolm, Graeme; Maker, Gareth; Cox, Rick; Williams, Brad; Russell, Matt

2012-10-01

The most desirable configuration for detection of toxic chemicals utilises the maximum distance between detector and hazard. This approach minimises the contamination of equipment or personnel. Where the target chemical is an involatile liquid, indirect detection of the liquid contamination is made difficult by inherently low vapour pressure. In this instance, direct detection of the chemical hazard is the best approach. Recent technology developments have allowed spectroscopic systems to provide multiple options for the stand-off detection of involatile chemical warfare agents (CWAs). Two different stand-off spectroscopic systems, based upon IR absorption and Raman spectroscopic techniques are described here. The Negative Contrast Imager (NCI) is based upon an optical parametric oscillator (OPO) source comprising a Q-switched intracavity MgO:PPLN crystal. This crystal has a fanned grating design and wavelength tuning is achieved by translating the PPLN crystal within the 1064 nm pump beam. This approach enables the production of shortwave and midwave IR radiation (1.5 - 1.8 μm and 2.6 - 3.8 μm, respectively), which is scanned across the scene of interest. Target materials that have an absorption feature commensurate with the wavelength of incoming radiation reduce the intensity of returned signal, resulting in dark pixels in the acquired image. This method enables location and classification of the target material. Stand-off Raman spectroscopy allows target chemicals to be identified at range through comparison of the acquired signature relative to a spectral database. In this work, we used a Raman system based upon a 1047 nm Nd:YLF laser source and a proprietary InGaAsP camera system. Utilisation of a longer excitation wavelength than most conventional stand-off detection systems (e.g. 532 or 785 nm) enables reduction of fluorescence from both the surface and the deposited chemicals, thereby revealing the Raman spectrum. NCI and Raman spectroscopy are able to detect CWAs on surfaces at distances of 2 - 10 metres and have potential to detect over longer ranges. We report the successful identification of at least 60 μl of nitrogen mustard at a distance of a 2 m and 10 m using NCI and Raman spectroscopy.

ICP-MS as a novel detection system for quantitative element-tagged immunoassay of hidden peanut allergens in foods.

PubMed

Careri, Maria; Elviri, Lisa; Mangia, Alessandro; Mucchino, Claudio

2007-03-01

A novel ICP-MS-based ELISA immunoassay via element-tagged determination was devised for quantitative analysis of hidden allergens in food. The method was able to detect low amounts of peanuts (down to approximately 2 mg peanuts kg(-1) cereal-based matrix) by using a europium-tagged antibody. Selectivity was proved by the lack of detectable cross-reaction with a number of protein-rich raw materials.

Advanced Laser-Compton Gamma-Ray Sources for Nuclear Materials Detection, Assay and Imaging

NASA Astrophysics Data System (ADS)

Barty, C. P. J.

2015-10-01

Highly-collimated, polarized, mono-energetic beams of tunable gamma-rays may be created via the optimized Compton scattering of pulsed lasers off of ultra-bright, relativistic electron beams. Above 2 MeV, the peak brilliance of such sources can exceed that of the world's largest synchrotrons by more than 15 orders of magnitude and can enable for the first time the efficient pursuit of nuclear science and applications with photon beams, i.e. Nuclear Photonics. Potential applications are numerous and include isotope-specific nuclear materials management, element-specific medical radiography and radiology, non-destructive, isotope-specific, material assay and imaging, precision spectroscopy of nuclear resonances and photon-induced fission. This review covers activities at the Lawrence Livermore National Laboratory related to the design and optimization of mono-energetic, laser-Compton gamma-ray systems and introduces isotope-specific nuclear materials detection and assay applications enabled by them.

Optical pH detector based on LTCC and sol-gel technologies

NASA Astrophysics Data System (ADS)

Tadaszak, R. J.; Łukowiak, A.; Golonka, L. J.

2013-01-01

This paper presents an investigation on using sol-gel thin film as a material for sensors application in LTCC (Low Temperature Co-fired Ceramics) technology. This material gives the opportunity to make new, low-cost highly integrated optoelectronic devices. Sensors with optical detection are a significant part of these applications. They can be used for quick and safe diagnostics of some parameters. Authors present a pH detector with the optical detection system made of the LTCC material. The main part of the device is a flow channel with the chamber and sol-gel active material. The silica sol-gel with bromocresol green indicator was used. As the absorbance of sol-gel layer changes with the pH value of a measured medium, the transmitted light power was measured. The pH detector was integrated with the electronic components on the LTCC substrate.

Synthesis of InSb Nanowire Architectures - Building Blocks for Majorana Devices

NASA Astrophysics Data System (ADS)

Car, Diana

Breakthroughs in material development are playing a major role in the emerging field of topological quantum computation with Majorana Zero Modes (MZMs). Due to the strong spin-orbit interaction and large Landé g-factor InSb nanowires are one of the most promising one dimensional material systems in which to detect MZMs. The next generation of Majorana experiments should move beyond zero-mode detection and demonstrate the non-Abelian nature of MZMs by braiding. To achieve this goal advanced material platforms are needed: low-disorder, single-crystalline, planar networks of nanowires with high spin-orbit energy. In this talk I will discuss the formation and electronic properties of InSb nanowire networks. The bottom-up synthesis method we have developed is generic and can be employed to synthesize interconnected nanowire architectures of group III-V, II-VI and IV materials as long as they grow along a <111>direction.

[Monolithic column-gold composite substrate preparation and application to SERS detection of pigment].

PubMed

Xie, Yun-Fei; Li, Yan; Yu, Hui; Qian, He; Yao, Wei-Rong

2014-03-01

In the present study, we developed a novel SERS substrate with the porous monolith material combined with classic gold nanoparticles, and erythrosine as the research object, by adjusting the different experimental conditions for optimal SERS enhancements, including system pH and mixing time, and ultimately selected the optimum pH value 5.06 and mixing time 25 min. Compared with the traditional gold plastic substrate enhancement effect, the experimental conditions were applied to the monolith substrate SERS detection of dye erythrosine, different concentrations of samples were used for erythrosine SERS detection, and the detection limit reached 0.1 g x mL(-1). The method uses the payload of gold nanoparticles in mesoporous materials to effectively enhance the SERS signal. And this method has the advantages of simpleness and good stability, which provides a favorable theoretical basis for the rapid prohibited colorings screening.

Department of Defense Chemical and Biological Defense Programs. Annual Report to Congress 2007

DTIC Science & Technology

2007-04-01

Bio aerosol Detection GREEN CB.37 CB agent Water monitor AMBER CB.42 environmental Fate of agents GREEN CB.45 Self -Detoxifying materials AMBER CB.46...nano-Closure Systems • Self -Detoxifying Surfaces/materials 32 C h a P t e r 2 C he m ic al a nd B io lo gi ca l D ef en se r eq ui re m en ts...resistant, selective permeable materials, and aerosol and vapor-resistant breathable materials. The addition of a self -detoxification component is

Rocky Planetary Debris Around Young WDs

NASA Astrophysics Data System (ADS)

Gaensicke, B.

2014-04-01

The vast majority of all known planet host stars, including the Sun, will eventually evolve into red giants and finally end their lives as white dwarfs: extremely dense Earth-sized stellar embers. Only close-in planets will be devoured during the red-giant phase. In the solar system, Mars, the asteroid belt, and all the giant planets will escape evaporation, and the same is true for many of the known exo-planets. It is hence certain that a significant fraction of the known white dwarfs were once host stars to planets, and it is very likely that many of them still have remnants of planetary systems. The detection of metals in the atmospheres of white dwarfs is the unmistakable signpost of such evolved planetary systems. The strong surface gravity of white dwarfs causes metals to sink out of the atmosphere on time-scales much shorter than their cooling ages, leading unavoidably to pristine H/He atmospheres. Therefore any metals detected in the atmosphere of a white dwarf imply recent or ongoing accretion of planetary debris. In fact, planetary debris is also detected as circumstellar dust and gas around a number of white dwarfs. These debris disks are formed from the tidal disruption of asteroids or Kuiper belt-like objects, stirred up by left-over planets, and are subsequently accreted onto the white dwarf, imprinting their abundance pattern into its atmosphere. Determining the photospheric abundances of debris-polluted white dwarfs is hence entirely analogue to the use of meteorites, "rocks that fell from the sky", for measuring the abundances of planetary material in the solar system. I will briefly review this new field of exo-planet science, and then focus on the results of a large, unbiased COS snapshot survey of relatively young ( 20-100Myr) white dwarfs that we carried out in Cycle 18/19. * At least 30% of all white dwarfs in our sample are accreting planetary debris, and that fraction may be as high as 50%. * In most cases where debris pollution is detected, the low C/Si ratio demonstrates that the planetary material is of rocky nature. * None of the 9 systems where we measure the C/O ratio shows evidence for carbon-dominated chemistry, implying that "carbon planets" are not common. * In the most polluted white dwarfs, we measure the debris abundances of up to 11 elements, enabling a detailed comparison between the chemistry of exo-planetary material with that of solar system meteorites. We find that the exo-planetary debris shares many characteristics of solar-system material, i.e. a wide spread in the relative abundances of Mg, Fe, Si, and O, a constant Al/Ca ratio, and evidence for differentiation in the form of Fe over-abundances All of the above is suggestive that thermal and collisional processing of planetary material in those systems might have been similar to that in the solar system.

Using eDNA to estimate distribution of fish species in a complex river system (presentation)

EPA Science Inventory

Environmental DNA (eDNA) analysis of biological material shed by aquatic organisms is a noninvasive genetic tool that can improve efficiency and reduce costs associated with species detection in aquatic systems. eDNA methods are widely used to assess presence/absence of a target ...

A novel method for NDT applications using NXCT system at the Missouri University of Science & Technology

NASA Astrophysics Data System (ADS)

Sinha, Vaibhav; Srivastava, Anjali; Koo Lee, Hyoung

2014-06-01

A novel method for non-destructive analysis has been developed using a neutron/X-ray combined computed tomography (NXCT) system at the Missouri University of Science and Technology Reactor (MSTR). This imaging system takes advantage of the fact that neutrons and X-rays have characteristically different interactions with same materials. NXCT fuses the imaging capabilities of both systems at one location and allows instant evaluation for nondestructive testing (NDT) applications. This technique promises viable advances in the field of NDT. In this paper, the complete design criteria and procedures are provided. The described design criteria and procedures can effectively be utilized to design and develop advanced combined computed tomography system. The successful operation of the high resolution X-ray and neutron computed tomography has been demonstrated in this paper. The utility and importance of the NXCT system has been shown by nondestructive evaluation of various phantoms constituting different materials, geometrical, structural and compositional information. The concept of NXCT can be useful for concealed material detection, material characterization, investigation of complex geometries involving different atomic number materials and real time imaging for in-situ studies.

Scatter in Cargo Radiography

DOE Office of Scientific and Technical Information (OSTI.GOV)

Miller, Erin A.; Caggiano, Joseph A.; Runkle, Robert C.

As a complement to passive detection systems, radiographic inspection of cargo is an increasingly important tool for homeland security because it has the potential to detect highly attenuating objects associated with special nuclear material or surrounding shielding. Detecting such objects relies on high image contrast between regions of different density and atomic number (Z). Threat detection is affected by scatter of the interrogating beam, both in the cargo and surrounding objects, which degrades image contrast. Here, we work to determine the extent to which scatter plays a role in radiographic imaging of cargo containers.

Energy Resolution and Temperature Dependence of Ce:GAGG Coupled to 3mm × 3mm Silicon Photomultipliers

NASA Astrophysics Data System (ADS)

Seitz, B.; Rivera, N. Campos; Stewart, A. G.

2016-04-01

Scintillators are a critical component of sensor systems for the detection of ionizing radiation. Such systems have a diverse portfolio of applications from medical imaging, well logging in oil exploration, and detection systems for the prevention of the illicit movement of nuclear materials. The rare earth element cerium is an ideal dopant for a variety of host scintillating materials due to the fast 5d1 → 4f radiative transition of Ce3+. Cerium-doped gadolinium aluminium gallium garnet (Ce:GAGG) is a relatively new single crystal scintillator with several interesting properties. These include high light yield, an emission peak well-matched to silicon sensors, and low intrinsic energy resolution. Moreover, the material has high density and is nonhygroscopic. In this paper, we review the properties of cerium-doped GAGG and report energy-resolution (ER) measurements over the temperature range -10°C to +50°C for 3 × 3 × 30 mm3 Ce:GAGG crystals optically coupled to a silicon photomultipler (SiPM) sensor with a 3 mm × 3 mm active area. In addition, the linearity of the scintillator-SiPM response as a function of gamma energy is reported.

Sensor-enabled chem/bio contamination detection system dedicated to situational awareness of water distribution security status

NASA Astrophysics Data System (ADS)

Ginsberg, Mark D.; Smith, Eddy D.; VanBlaricum, Vicki; Hock, Vincent F.; Kroll, Dan; Russell, Kevin J.

2010-04-01

Both real events and models have proven that drinking water systems are vulnerable to deliberate and/or accidental contamination. Additionally, homeland security initiatives and modeling efforts have determined that it is relatively easy to orchestrate the contamination of potable water supplies. Such contamination can be accomplished with classic and non-traditional chemical agents, toxic industrial chemicals (TICs), and/or toxic industrial materials (TIMs). Subsequent research and testing has developed a proven network for detection and response to these threats. The method uses offthe- shelf, broad-spectrum analytical instruments coupled with advanced interpretive algorithms. The system detects and characterizes any backflow events involving toxic contaminants by employing unique chemical signature (fingerprint) response data. This instrumentation has been certified by the Office of Homeland Security for detecting deliberate and/or accidental contamination of critical water infrastructure. The system involves integration of several mature technologies (sensors, SCADA, dynamic models, and the HACH HST Guardian Blue instrumentation) into a complete, real-time, management system that also can be used to address other water distribution concerns, such as corrosion. This paper summarizes the reasons and results for installing such a distribution-based detection and protection system.

Method of noncontacting ultrasonic process monitoring

DOEpatents

Garcia, Gabriel V.; Walter, John B.; Telschow, Kenneth L.

1992-01-01

A method of monitoring a material during processing comprising the steps of (a) shining a detection light on the surface of a material; (b) generating ultrasonic waves at the surface of the material to cause a change in frequency of the detection light; (c) detecting a change in the frequency of the detection light at the surface of the material; (d) detecting said ultrasonic waves at the surface point of detection of the material; (e) measuring a change in the time elapsed from generating the ultrasonic waves at the surface of the material and return to the surface point of detection of the material, to determine the transit time; and (f) comparing the transit time to predetermined values to determine properties such as, density and the elastic quality of the material.

New software to model energy dispersive X-ray diffraction in polycrystalline materials

NASA Astrophysics Data System (ADS)

Ghammraoui, B.; Tabary, J.; Pouget, S.; Paulus, C.; Moulin, V.; Verger, L.; Duvauchelle, Ph.

2012-02-01

Detection of illicit materials, such as explosives or drugs, within mixed samples is a major issue, both for general security and as part of forensic analyses. In this paper, we describe a new code simulating energy dispersive X-ray diffraction patterns in polycrystalline materials. This program, SinFullscat, models diffraction of any object in any diffractometer system taking all physical phenomena, including amorphous background, into account. Many system parameters can be tuned: geometry, collimators (slit and cylindrical), sample properties, X-ray source and detector energy resolution. Good agreement between simulations and experimental data was obtained. Simulations using explosive materials indicated that parameters such as the diffraction angle or the energy resolution of the detector have a significant impact on the diffraction signature of the material inspected. This software will be a convenient tool to test many diffractometer configurations, providing information on the one that best restores the spectral diffraction signature of the materials of interest.

Hybrid Integrated Label-Free Chemical and Biological Sensors

PubMed Central

Mehrabani, Simin; Maker, Ashley J.; Armani, Andrea M.

2014-01-01

Label-free sensors based on electrical, mechanical and optical transduction methods have potential applications in numerous areas of society, ranging from healthcare to environmental monitoring. Initial research in the field focused on the development and optimization of various sensor platforms fabricated from a single material system, such as fiber-based optical sensors and silicon nanowire-based electrical sensors. However, more recent research efforts have explored designing sensors fabricated from multiple materials. For example, synthetic materials and/or biomaterials can also be added to the sensor to improve its response toward analytes of interest. By leveraging the properties of the different material systems, these hybrid sensing devices can have significantly improved performance over their single-material counterparts (better sensitivity, specificity, signal to noise, and/or detection limits). This review will briefly discuss some of the methods for creating these multi-material sensor platforms and the advances enabled by this design approach. PMID:24675757

Hybrid integrated label-free chemical and biological sensors.

PubMed

Mehrabani, Simin; Maker, Ashley J; Armani, Andrea M

2014-03-26

Label-free sensors based on electrical, mechanical and optical transduction methods have potential applications in numerous areas of society, ranging from healthcare to environmental monitoring. Initial research in the field focused on the development and optimization of various sensor platforms fabricated from a single material system, such as fiber-based optical sensors and silicon nanowire-based electrical sensors. However, more recent research efforts have explored designing sensors fabricated from multiple materials. For example, synthetic materials and/or biomaterials can also be added to the sensor to improve its response toward analytes of interest. By leveraging the properties of the different material systems, these hybrid sensing devices can have significantly improved performance over their single-material counterparts (better sensitivity, specificity, signal to noise, and/or detection limits). This review will briefly discuss some of the methods for creating these multi-material sensor platforms and the advances enabled by this design approach.

Trends and comparison of water quality and bottom material of northeastern Arkansas streams, 1974-85, and effects of planned diversions

DOE Office of Scientific and Technical Information (OSTI.GOV)

Petersen, J.C.

1990-01-01

Water quality of several rivers in Arkansas was compared using median values at individual water quality stations. Differences were detected in several properties, including common dissolved constituents, alkalinity, nutrients, fecal coliform bacteria, trace metals, pesticides, and sediment. In bottom material, organochlorine pesticides were detected much more frequently than organophosphorus pesticides and were higher in rivers with beds of fine-gradient particles. Time trends were examined using the Seasonal Kendall test. Trends in conductance, sodium adsorption ratio, chloride, phosphorus, and ammonia were usually not detectable. Sulfate concentrations were increasing at approximately one-half of the stations studied while fecal-coliform bacteria concentrations decreased atmore » approximately one-half of the stations. The most potentially detrimental effects upon water quality resulting from surface water diversions were related to increases of common dissolved constituents. From available data, the largest of these increases would be caused by diversion from the Arkansas River. Potential effects not specifically examined include resuspension of bottom materials resulting from construction and operation of the diversion system. Use of some surface waters for artificial recharge of the alluvial aquifer may adversely affect the recharge systems or the aquifer. Possible effects include plugging of the injection well and the aquifer.« less

Real-Time Model-Based Leak-Through Detection within Cryogenic Flow Systems

NASA Technical Reports Server (NTRS)

Walker, M.; Figueroa, F.

2015-01-01

The timely detection of leaks within cryogenic fuel replenishment systems is of significant importance to operators on account of the safety and economic impacts associated with material loss and operational inefficiencies. Associated loss in control of pressure also effects the stability and ability to control the phase of cryogenic fluids during replenishment operations. Current research dedicated to providing Prognostics and Health Management (PHM) coverage of such cryogenic replenishment systems has focused on the detection of leaks to atmosphere involving relatively simple model-based diagnostic approaches that, while effective, are unable to isolate the fault to specific piping system components. The authors have extended this research to focus on the detection of leaks through closed valves that are intended to isolate sections of the piping system from the flow and pressurization of cryogenic fluids. The described approach employs model-based detection of leak-through conditions based on correlations of pressure changes across isolation valves and attempts to isolate the faults to specific valves. Implementation of this capability is enabled by knowledge and information embedded in the domain model of the system. The approach has been used effectively to detect such leak-through faults during cryogenic operational testing at the Cryogenic Testbed at NASA's Kennedy Space Center.

Automatic Emboli Detection System for the Artificial Heart

NASA Astrophysics Data System (ADS)

Steifer, T.; Lewandowski, M.; Karwat, P.; Gawlikowski, M.

In spite of the progress in material engineering and ventricular assist devices construction, thromboembolism remains the most crucial problem in mechanical heart supporting systems. Therefore, the ability to monitor the patient's blood for clot formation should be considered an important factor in development of heart supporting systems. The well-known methods for automatic embolus detection are based on the monitoring of the ultrasound Doppler signal. A working system utilizing ultrasound Doppler is being developed for the purpose of flow estimation and emboli detection in the clinical artificial heart ReligaHeart EXT. Thesystem will be based on the existing dual channel multi-gate Doppler device with RF digital processing. A specially developed clamp-on cannula probe, equipped with 2 - 4 MHz piezoceramic transducers, enables easy system setup. We present the issuesrelated to the development of automatic emboli detection via Doppler measurements. We consider several algorithms for the flow estimation and emboli detection. We discuss their efficiency and confront them with the requirements of our experimental setup. Theoretical considerations are then met with preliminary experimental findings from a) flow studies with blood mimicking fluid and b) in-vitro flow studies with animal blood. Finally, we discuss some more methodological issues - we consider several possible approaches to the problem of verification of the accuracy of the detection system.

Explosive simulants for testing explosive detection systems

DOEpatents

Kury, John W.; Anderson, Brian L.

1999-09-28

Explosives simulants that include non-explosive components are disclosed that facilitate testing of equipment designed to remotely detect explosives. The simulants are non-explosive, non-hazardous materials that can be safely handled without any significant precautions. The simulants imitate real explosives in terms of mass density, effective atomic number, x-ray transmission properties, and physical form, including moldable plastics and emulsions/gels.

Optimized acoustic biochip integrated with microfluidics for biomarkers detection in molecular diagnostics.

PubMed

Papadakis, G; Friedt, J M; Eck, M; Rabus, D; Jobst, G; Gizeli, E

2017-09-01

The development of integrated platforms incorporating an acoustic device as the detection element requires addressing simultaneously several challenges of technological and scientific nature. The present work was focused on the design of a microfluidic module, which, combined with a dual or array type Love wave acoustic chip could be applied to biomedical applications and molecular diagnostics. Based on a systematic study we optimized the mechanics of the flow cell attachment and the sealing material so that fluidic interfacing/encapsulation would impose minimal losses to the acoustic wave. We have also investigated combinations of operating frequencies with waveguide materials and thicknesses for maximum sensitivity during the detection of protein and DNA biomarkers. Within our investigations neutravidin was used as a model protein biomarker and unpurified PCR amplified Salmonella DNA as the model genetic target. Our results clearly indicate the need for experimental verification of the optimum engineering and analytical parameters, in order to develop commercially viable systems for integrated analysis. The good reproducibility of the signal together with the ability of the array biochip to detect multiple samples hold promise for the future use of the integrated system in a Lab-on-a-Chip platform for application to molecular diagnostics.

Method and apparatus for determining the physical properties of materials using dynamic light scattering techniques

NASA Technical Reports Server (NTRS)

Dhadwal, Harbans S. (Inventor)

1992-01-01

A system for determining the physical properties of materials through the use of dynamic light scattering is disclosed. The system includes a probe, a laser source for directing a laser beam into the probe, and a photodetector for converting scattered light detected by the probe into electrical signals. The probe includes at least one optical fiber connected to the laser source and a second optical fiber connected to the photodetector. Each of the fibers may adjoin a gradient index microlens which is capable of providing a collimated laser beam into a scattering medium. The position of the second optical fiber with respect to the optical axis of the probe determines whether homodyne or self-beating detection is provided. Self-beating detection may be provided without a gradient index microlens. This allows a very small probe to be constructed which is insertable through a hypodermic needle or the like into a droplet extending from such a needle. A method of detecting scattered light through the use of a collimated, Gaussian laser beam is also provided. A method for controlling the waist and divergence of the optical field emanating from the free end of an optical fiber is also provided.

A novel method for detecting neutralizing antibodies against therapeutic proteins by measuring gene expression.

PubMed

Yu, Yanbin; Piddington, Christopher; Fitzpatrick, Dan; Twomey, Brian; Xu, Ren; Swanson, Steven J; Jing, Shuqian

2006-10-20

The presence of neutralizing antibodies against protein therapeutics is a concern in the biomedical field. Such antibodies not only reduce the efficacy of protein therapeutics, but also impose potential dangers to the patients receiving them. To date, a small number of in vitro cell-based bioassays for detecting neutralizing antibodies against therapeutic proteins have been developed. Most of the existing assays, however, either involve the use of radioactive materials or have limited sensitivities and/or poor specificities. With advances in mRNA profiling and detection techniques, we have established a novel and non-radioactive bioassay system using branched DNA (bDNA) technology for detecting protein-therapeutic neutralizing antibodies in patient serum. Our assay measures the variations of target gene expression that reflect the biologic effect of the therapeutic agent and the capability of the antibodies, if present, to neutralize the therapeutics. Compared with most existing assays, the new assay is more sensitive and specific, and completely eliminates the use of radioactive materials. Application of the new assay system can be widely expanded if new target genes and responding cell lines for other therapeutics are identified or engineered.

Fast photoresponse and high detectivity in copper indium selenide (CuIn7Se11) phototransistors

NASA Astrophysics Data System (ADS)

Ghosh, Sujoy; Patil, Prasanna D.; Wasala, Milinda; Lei, Sidong; Nolander, Andrew; Sivakumar, Pooplasingam; Vajtai, Robert; Ajayan, Pulickel; Talapatra, Saikat

2018-03-01

The fast and sensitive detection of light can lead to a variety of optoelectronics and/or photonic-based applications in fields ranging from fast optical switching devices to health and environmental monitoring systems. Although several systems based on organic and inorganic materials show high sensitivity to visible light, in general they suffer from slow response times. Here we show that phototransistors fabricated using multilayers of CuIn7Se11 exhibit response times of ~ tens of µs with responsivity (R) values  >  10 AW-1 and with external quantum efficiencies reaching beyond 103 % when excited with a 658 nm wavelength laser. These devices also show high specific detectivity (D *) values of ~1012 Jones. The responsivity and detectivity exhibited by these phototransistors are at least an order of magnitude better than commercially available conventional Si-based photodetectors, coupled with response times that are orders of magnitude better than several other families of layered materials investigated so far. The properties of the CuIn7Se11 phototransistor can be further tuned and enhanced by applying a back-gate voltage. Our investigations indicate that such layered ternary compounds can potentially be used as components in opto-electronics-related applications.

Molecular Thermometry

PubMed Central

McCabe, Kevin M.; Hernandez, Mark

2010-01-01

Conventional temperature measurements rely on material responses to heat, which can be detected visually. When Galileo developed an air expansion based device to detect temperature changes, Santorio, a contemporary physician, added a scale to create the first thermometer. With this instrument, patients’ temperatures could be measured, recorded and related to changing health conditions. Today, advances in materials science and bioengineering provide new ways to report temperature at the molecular level in real time. In this review the scientific foundations and history of thermometry underpin a discussion of the discoveries emerging from the field of molecular thermometry. Intracellular nanogels and heat sensing biomolecules have been shown to accurately report temperature changes at the nano-scale. Various systems will soon provide the ability to accurately measure temperature changes at the tissue, cellular, and even sub-cellular level, allowing for detection and monitoring of very small changes in local temperature. In the clinic this will lead to enhanced detection of tumors and localized infection, and accurate and precise monitoring of hyperthermia based therapies. Some nanomaterial systems have even demonstrated a theranostic capacity for heat-sensitive, local delivery of chemotherapeutics. Just as early thermometry moved into the clinic, so too will these molecular thermometers. PMID:20139796

Computer Vision and Machine Learning for Autonomous Characterization of AM Powder Feedstocks

NASA Astrophysics Data System (ADS)

DeCost, Brian L.; Jain, Harshvardhan; Rollett, Anthony D.; Holm, Elizabeth A.

2017-03-01

By applying computer vision and machine learning methods, we develop a system to characterize powder feedstock materials for metal additive manufacturing (AM). Feature detection and description algorithms are applied to create a microstructural scale image representation that can be used to cluster, compare, and analyze powder micrographs. When applied to eight commercial feedstock powders, the system classifies powder images into the correct material systems with greater than 95% accuracy. The system also identifies both representative and atypical powder images. These results suggest the possibility of measuring variations in powders as a function of processing history, relating microstructural features of powders to properties relevant to their performance in AM processes, and defining objective material standards based on visual images. A significant advantage of the computer vision approach is that it is autonomous, objective, and repeatable.

Detection of TNT using a sensitive two-photon organic dendrimer for remote sensing

NASA Astrophysics Data System (ADS)

Narayanan, Aditya; Varnavski, Oleg; Mongin, Oliver; Majoral, Jean-Pierre; Blanchard-Desce, Mireille; Goodson, Theodore, III

2008-03-01

There is currently a need for superior stand-off detection schemes for protection against explosive weapons of mass destruction. Fluorescence detection at small distances from the target has proven to be attractive. A novel unexplored route in fluorescence chemical sensing that utilizes the exceptional spectroscopic capabilities of nonlinear optical methods is two-photon excited fluorescence. This approach utilizes infra-red light for excitation of remote sensors. Infra-red light suffers less scattering in porous materials which is beneficial for vapor sensing and has greater depth of penetration through the atmosphere, and there are fewer concerns regarding eye safety in remote detection schemes. We demonstrate this method using a novel dendritic system which possesses both excellent fluorescence sensitivity to the presence of TNT with infra-red pulses of light and high two-photon absorption (TPA) response. This illustrates the use of TPA for potential stand-off detection of energetic materials in the infra-red spectral regions in a highly two-photon responsive dendrimer.

Towards advanced biological detection using surface enhanced raman scattering (SERS)-based sensors

NASA Astrophysics Data System (ADS)

Hankus, Mikella E.; Stratis-Cullum, Dimitra N.; Pellegrino, Paul M.

2010-08-01

The Army has a need for an accurate, fast, reliable and robust means to identify and quantify defense related materials. Raman spectroscopy is a form of vibrational spectroscopy that is rapidly becoming a valuable tool for homeland defense applications, as it is well suited for the molecular identification of a variety of compounds, including explosives and chemical and biological hazards. To measure trace levels of these types of materials, surface enhanced Raman scattering (SERS), a specialized form of Raman scattering, can be employed. The SERS enhancements are produced on, or in close proximity to, a nanoscale roughened metal surface and are typically associated with increased local electromagnetic field strengths. However, before application of SERS in the field and in particular to biological and other hazard sensing applications, significant improvements in substrate performance are needed. In this work, we will report the use of several SERS substrate architectures (colloids, film-over-nanospheres (FONs) and commercially available substrates) for detecting and differentiating numerous endospore samples. The variance in spectra as obtained using different sensing architectures will also be discussed. Additionally, the feasibility of using a modified substrate architecture that is tailored with molecular recognition probe system for detecting biological samples will be explored. We will discuss the progress towards an advanced, hybrid molecular recognition with a SERS/Fluorescence nanoprobe system including the optimization, fabrication, and spectroscopic analysis of samples on a commercially available substrate. Additionally, the feasibility of using this single-step switching architecture for hazard material detection will also be explored.

Wireless sensing system for non-invasive monitoring of attributes of contents in a container

NASA Technical Reports Server (NTRS)

Woodard, Stanley E. (Inventor)

2010-01-01

A wireless sensing system monitors the level, temperature, magnetic permeability and electrical dielectric constant of a non-gaseous material in a container. An open-circuit electrical conductor is shaped to form a two-dimensional geometric pattern that can store and transfer electrical and magnetic energy. The conductor resonates in the presence of a time-varying magnetic field to generate a harmonic response. The conductor is mounted in an environmentally-sealed housing. A magnetic field response recorder wirelessly transmits the time-varying magnetic field to power the conductor, and wirelessly detects the harmonic response that is an indication of at least one of level of the material in the container, temperature of the material in the container, magnetic permeability of the material in the container, and dielectric constant of the material in the container.

Terahertz detection and identification of defects in layered polymer composites and composite coatings

NASA Astrophysics Data System (ADS)

Lopato, Przemyslaw; Chady, Tomasz

2013-03-01

Modern industry makes more and more extensive use of various composite materials. In this paper, for the purposes of various composite materials evaluation, the terahertz imaging method is presented. Basalt fibre-reinforced composites and polymeric anticorrosion coatings are considered. Basalt fibre composites are the innovative materials that are being increasingly used in modern industry. The paper also briefly introduces a specific type of complex coating of steel applied in the industry (e.g. oil or chemical). Two methods of defects detection in the mentioned structures are presented. The first method is based on a system identification, whereas the second one is on the estimation of time-domain signal parameters. Finally, the results achieved during terahertz inspection of coatings are compared with those obtained using active thermography.

Nondestructive detection and measurement of hydrogen embrittlement

DOEpatents

Alex, Franklin; Byrne, Joseph Gerald

1977-01-01

A nondestructive system and method for the determination of the presence and extent of hydrogen embrittlement in metals, alloys, and other crystalline structures subject thereto. Positron annihilation characteristics of the positron-electron annihilation within the tested material provide unique energy distribution curves for each type of material tested at each respective stage of hydrogen embrittlement. Gamma radiation resulting from such annihilation events is detected and statistically summarized by appropriate instrumentation to reveal the variations of electron activity within the tested material caused by hydrogen embrittlement therein. Such data from controlled tests provides a direct indication of the relative stages of hydrogen embrittlement in the form of unique energy distribution curves which may be utilized as calibration curves for future comparison with field tests to give on-site indication of progressive stages of hydrogen embrittlement.

Detection of pulsed neutrons with solid-state electronics

NASA Astrophysics Data System (ADS)

Chatzakis, J.; Rigakis, I.; Hassan, S. M.; Clark, E. L.; Lee, P.

2016-09-01

Measurements of the spatial and time-resolved characteristics of pulsed neutron sources require large area detection materials and fast circuitry that can process the electronic pulses readout from the active region of the detector. In this paper, we present a solid-state detector based on the nuclear activation of materials by neutrons, and the detection of the secondary particle emission of the generated radionuclides’ decay. The detector utilizes a microcontroller that communicates using a modified SPI protocol. A solid-state, pulse shaping filter follows a charge amplifier, and it is designed as an inexpensive, low-noise solution for measuring pulses measured by a digital counter. An imaging detector can also be made by using an array of these detectors. The system can communicate with an interface unit and pass an image to a personal computer.

"Smoke": Characterization Of Smoke Particulate For Spacecraft Fire Detection

NASA Technical Reports Server (NTRS)

Urban, David L.; Mulholland, George W.; Yang, Jiann; Cleary, Thomas G.; Yuan, Zeng-Guang

2003-01-01

The "Smoke" experiment is a flight definition investigation that seeks to increase our understanding of spacecraft fire detection through measurements of particulate size distributions of preignition smokes from typical spacecraft materials. Owing to the catastrophic risk posed by even a very small fire in a spacecraft, the design goal for spacecraft fire detection is to detect the fire as quickly as possible, preferably in the preignition phase before a real flaming fire has developed. Consequently the target smoke for detection is typically not soot (typical of established hydrocarbon fires) but instead, pyrolysis products, and recondensed polymer particles. At the same time, false alarms are extremely costly as the crew and the ground team must respond quickly to every alarm. The U.S. Space Shuttle (STS: Space Transportation System) and the International Space Station (ISS) both use smoke detection as the primary means of fire detection. These two systems were designed in the absence of any data concerning low-gravity smoke particle (and background dust) size distributions. The STS system uses an ionization detector coupled with a sampling pump and the ISS system is a forward light scattering detector operating in the near IR. These two systems have significantly different sensitivities with the ionization detector being most sensitive (on a mass concentration basis) to smaller particulate and the light scattering detector being most sensitive to particulate that is larger than 1 micron. Since any smoke detection system has inherent size sensitivity characteristics, proper design of future smoke detection systems will require an understanding of the background and alarm particle size distributions that can be expected in a space environment.

Progress In Developing Laser Based Post Irradiation Examination Infrastructure

DOE Office of Scientific and Technical Information (OSTI.GOV)

Smith, James A.; Scott, Clark L.; Benefiel, Brad C.

To be able to understand the performance of reactor fuels and materials, irradiated materials must be characterized effectively and efficiently in a high rad environment. The characterization work must be performed remotely and in an environment hostile to instrumentation. Laser based characterization techniques provide the ability to be remote and robust in a hot-cell environment. Laser based instrumentation also can provide high spatial resolution suitable for scanning and imaging large areas. The INL is currently developing three laser based Post Irradiation Examination (PIE) stations for the Hot Fuel Examination Facility at the INL. These laser based systems will characterize irradiatedmore » materials and fuels. The characterization systems are the following: Laser Shock Laser based ultrasonic C-scan system Gas Assay, Sample, and Recharge system (GASR, up-grade to an existing system). The laser shock technique will characterize material properties and failure loads/mechanisms in various materials such as LWR fuel, plate fuel, and next generation fuel forms, for PIE in high radiation areas. The laser shock-technique induces large amplitude shock waves to mechanically characterize interfaces such as the fuel-clad bond. The shock wave travels as a compression wave through the material to the free (unconfined) back surface and reflects back through the material under test as a rarefaction (tensile) wave. This rarefaction wave is the physical mechanism that produces internal de-lamination failure. As part of the laser shock system, a laser-based ultrasonic C-scan system will be used to detect and characterize debonding caused by the laser shock technique. The laser ultrasonic system will be fully capable of performing classical non-destructive evaluation testing and imaging functions such as microstructure characterization, flaw detection and dimensional metrology in complex components. The purpose of the GASR is to measure the pressure/volume of the plenum of an irradiated fuel element and obtain fission gas samples for analysis. The study of pressure and volume in the plenum of an irradiated fuel element and the analysis of fission gases released from the fuel is important to understanding the performance of reactor fuels and materials. This system may also be used to measure the pressure/volume of other components (such as control blades) and obtain gas samples from these components for analysis. The main function of the laser in this application is to puncture the fuel element to allow the fission gas to escape and if necessary to weld the spot close. The GASR station will have the inherent capability to perform cutting welding and joining functions within a hot-cell.« less

Non-destructive testing method and apparatus

DOEpatents

Akers, Douglas W [Idaho Falls, ID

2011-10-04

Non-destructive testing apparatus may comprise a photon source and a source material that emits positrons in response to bombardment of the source material with photons. The source material is positionable adjacent the photon source and a specimen so that when the source material is positioned adjacent the photon source it is exposed to photons produced thereby. When the source material is positioned adjacent the specimen, the specimen is exposed to at least some of the positrons emitted by the source material. A detector system positioned adjacent the specimen detects annihilation gamma rays emitted by the specimen. Another embodiment comprises a neutron source and a source material that emits positrons in response to neutron bombardment.

Pseudo-Random Modulation of a Laser Diode for Generating Ultrasonic Longitudinal Waves

NASA Technical Reports Server (NTRS)

Madaras, Eric I.; Anatasi, Robert F.

2004-01-01

Laser generated ultrasound systems have historically been more complicated and expensive than conventional piezoelectric based systems, and this fact has relegated the acceptance of laser based systems to niche applications for which piezoelectric based systems are less suitable. Lowering system costs, while improving throughput, increasing ultrasound signal levels, and improving signal-to-noise are goals which will help increase the general acceptance of laser based ultrasound. One current limitation with conventional laser generated ultrasound is a material s damage threshold limit. Increasing the optical power to generate more signal eventually damages the material being tested due to rapid, high heating. Generation limitations for laser based ultrasound suggests the use of pulse modulation techniques as an alternate generation method. Pulse modulation techniques can spread the laser energy over time or space, thus reducing laser power densities and minimizing damage. Previous experiments by various organizations using spatial or temporal pulse modulation have been shown to generate detectable surface, plate, and bulk ultrasonic waves with narrow frequency bandwidths . Using narrow frequency bandwidths improved signal detectability, but required the use of expensive and powerful lasers and opto-electronic systems. The use of a laser diode to generate ultrasound is attractive because of its low cost, small size, light weight, simple optics and modulation capability. The use of pulse compression techniques should allow certain types of laser diodes to produce usable ultrasonic signals. The method also does not need to be limited to narrow frequency bandwidths. The method demonstrated here uses a low power laser diode (approximately 150 mW) that is modulated by controlling the diode s drive current and the resulting signal is recovered by cross correlation. A potential application for this system which is briefly demonstrated is in detecting signals in thick composite materials where attenuation is high and signal amplitude and bandwidth are at a premium.

Thermal protection system (TPS) monitoring using acoustic emission

NASA Astrophysics Data System (ADS)

Hurley, D. A.; Huston, D. R.; Fletcher, D. G.; Owens, W. P.

2011-04-01

This project investigates acoustic emission (AE) as a tool for monitoring the degradation of thermal protection systems (TPS). The AE sensors are part of an array of instrumentation on an inductively coupled plasma (ICP) torch designed for testing advanced thermal protection aerospace materials used for hypervelocity vehicles. AE are generated by stresses within the material, propagate as elastic stress waves, and can be detected with sensitive instrumentation. Graphite (POCO DFP-2) is used to study gas-surface interaction during degradation of thermal protection materials. The plasma is produced by a RF magnetic field driven by a 30kW power supply at 3.5 MHz, which creates a noisy environment with large spikes when powered on or off. AE are waveguided from source to sensor by a liquid-cooled copper probe used to position the graphite sample in the plasma stream. Preliminary testing was used to set filters and thresholds on the AE detection system (Physical Acoustics PCI-2) to minimize the impact of considerable operating noise. Testing results show good correlation between AE data and testing environment, which dictates the physics and chemistry of the thermal breakdown of the sample. Current efforts for the project are expanding the dataset and developing statistical analysis tools. This study shows the potential of AE as a powerful tool for analysis of thermal protection material thermal degradations with the unique capability of real-time, in-situ monitoring.

Material discrimination using scattering and stopping of cosmic ray muons and electrons: Differentiating heavier from lighter metals as well as low-atomic weight materials

NASA Astrophysics Data System (ADS)

Blanpied, Gary; Kumar, Sankaran; Dorroh, Dustin; Morgan, Craig; Blanpied, Isabelle; Sossong, Michael; McKenney, Shawn; Nelson, Beth

2015-06-01

Reported is a new method to apply cosmic-ray tomography in a manner that can detect and characterize not only dense assemblages of heavy nuclei (like Special Nuclear Materials, SNM) but also assemblages of medium- and light-atomic-mass materials (such as metal parts, conventional explosives, and organic materials). Characterization may enable discrimination between permitted contents in commerce and contraband (explosives, illegal drugs, and the like). Our Multi-Mode Passive Detection System (MMPDS) relies primarily on the muon component of cosmic rays to interrogate Volumes of Interest (VOI). Muons, highly energetic and massive, pass essentially un-scattered through materials of light atomic mass and are only weakly scattered by conventional metals used in industry. Substantial scattering and absorption only occur when muons encounter sufficient thicknesses of heavy elements characteristic of lead and SNM. Electrons are appreciably scattered by light elements and stopped by sufficient thicknesses of materials containing medium-atomic-mass elements (mostly metals). Data include simulations based upon GEANT and measurements in the HMT (Half Muon Tracker) detector in Poway, CA and a package scanner in both Poway and Socorro NM. A key aspect of the present work is development of a useful parameter, designated the "stopping power" of a sample. The low-density regime, comprising organic materials up to aluminum, is characterized using very little scattering but a strong variation in stopping power. The medium-to-high density regime shows a larger variation in scattering than in stopping power. The detection of emitted gamma rays is another useful signature of some materials.

Monitoring of Thermal Protection Systems Using Robust Self-Organizing Optical Fiber Sensing Networks

NASA Technical Reports Server (NTRS)

Richards, Lance

2013-01-01

The general aim of this work is to develop and demonstrate a prototype structural health monitoring system for thermal protection systems that incorporates piezoelectric acoustic emission (AE) sensors to detect the occurrence and location of damaging impacts, and an optical fiber Bragg grating (FBG) sensor network to evaluate the effect of detected damage on the thermal conductivity of the TPS material. Following detection of an impact, the TPS would be exposed to a heat source, possibly the sun, and the temperature distribution on the inner surface in the vicinity of the impact measured by the FBG network. A similar procedure could also be carried out as a screening test immediately prior to re-entry. The implications of any detected anomalies in the measured temperature distribution will be evaluated for their significance in relation to the performance of the TPS during re-entry. Such a robust TPS health monitoring system would ensure overall crew safety throughout the mission, especially during reentry

Nuclear Resonance Fluorescence Response of U-235

NASA Astrophysics Data System (ADS)

Warren, Glen

2008-05-01

Nuclear resonance fluorescence (NRF) is a physical process that provides an isotopic-specific signature that could be used for the identification and characterization of materials. The technique involves the detection of prompt discrete-energy photons emitted from a sample, which is exposed to photons in the MeV energy range. Potential applications of the technique range from detection of high explosives to characterization of special nuclear materials. Pacific Northwest National Laboratory and Passport Systems have collaboratively conducted a set of measurements to search for an NRF response of U-235 in the 1.5 to 9 MeV energy range. Results from these measurements will be presented.

Convenient, Sensitive and High-Throughput Method for Screening Botanic Origin

NASA Astrophysics Data System (ADS)

Yuan, Yuan; Jiang, Chao; Liu, Libing; Yu, Shulin; Cui, Zhanhu; Chen, Min; Lin, Shufang; Wang, Shu; Huang, Luqi

2014-06-01

In this work, a rapid (within 4-5 h), sensitive and visible new method for assessing botanic origin is developed by combining loop-mediated isothermal amplification with cationic conjugated polymers. The two Chinese medicinal materials (Jin-Yin-Hua and Shan-Yin-Hua) with similar morphology and chemical composition were clearly distinguished by gene SNP genotyping assays. The identification of plant species in Patented Chinese drugs containing Lonicera buds is successfully performed using this detection system. The method is also robust enough to be used in high-throughput screening. This new method is very helpful to identify herbal materials, and is beneficial for detecting safety and quality of botanic products.

III-V strain layer superlattice based band engineered avalanche photodiodes (Presentation Recording)

NASA Astrophysics Data System (ADS)

Ghosh, Sid

2015-08-01

Laser detection and ranging (LADAR)-based systems operating in the Near Infrared (NIR) and Short Wave Infrared (SWIR) have become popular optical sensors for remote sensing, medical, and environmental applications. Sophisticated laser-based radar and weapon systems used for long-range military and astronomical applications need to detect, recognize, and track a variety of targets under a wide spectrum of atmospheric conditions. Infrared APDs play an important role in LADAR systems by integrating the detection and gain stages in a single device. Robust silicon-APDs are limited to visible and very near infrared region (< 1 um), while InGaAs works well up to wavelengths of about 1.5um. Si APDs have low multiplication or excess noise but are limited to below 1um due very poor quantum efficiency above 0.8um. InGaAs and Ge APDs operate up to wavelengths of 1.5um but have poor multiplication or excess noise due to a low impact ionization coefficient ratio between electrons and holes. For the past several decades HgCdTe has been traditionally used in longer wavelength (> 3um) infrared photon detection applications. Recently, various research groups (including Ghosh et. al.) have reported SWIR and MWIR HgCdTe APDs on CdZnTe and Si substrates. However, HgCdTe APDs suffer from low breakdown fields due to material defects, and excess noise increases significantly at high electric fields. During the past decade, InAs/GaSb Strain Layer Superlattice (SLS) material system has emerged as a potential material for the entire infrared spectrum because of relatively easier growth, comparable absorption coefficients, lower tunneling currents and longer Auger lifetimes resulting in enhanced detectivities (D*). Band engineering in type II SLS allows us to engineer avalanche properties of electrons and holes. This is a great advantage over bulk InGaAs and HgCdTe APDs where engineering avalanche properties is not possible. The talk will discuss the evolution of superlattice based avalanche photodiodes and some of the recent results on the work being done at Raytheon on SWIR avalanche photodiodes.

Identification of carbohydrates by matrix-free material-enhanced laser desorption/ionisation mass spectrometry.

PubMed

Hashir, Muhammad Ahsan; Stecher, Guenther; Bakry, Rania; Kasemsook, Saowapak; Blassnig, Bernhard; Feuerstein, Isabel; Abel, Gudrun; Popp, Michael; Bobleter, Ortwin; Bonn, Guenther K

2007-01-01

Matrix-assisted laser desorption/ionisation time-of-flight mass spectrometry (MALDI-TOF-MS) is a sensitive mass spectrometric technique which utilises acidic materials as matrices for laser energy absorption, desorption and ionisation of analytes. These matrix materials produce background signals particularly in the low-mass range and make the detection and identification of small molecules difficult and nearly impossible. To overcome this problem this paper introduces matrix-free material-enhanced laser desorption/ionisation mass spectrometry (mf-MELDI-MS) for the screening and analysis of small molecules such as carbohydrates. For this purpose, 4,4'-azo-dianiline was immobilised on silica gel enabling the absorption of laser energy sufficient for successful desorption and ionisation of low molecular weight compounds. The particle and pore sizes, the solvent system for suspension and the sample preparation procedures have been optimised. The newly synthesised MELDI material delivered excellent spectra with regard to signal-to-noise ratio and detection sensitivity. Finally, wheat straw degradation products and Salix alba L. plant extracts were analysed proving the high performance and excellent behaviour of the introduced material. Copyright (c) 2007 John Wiley & Sons, Ltd.

Development of E-Learning Materials for Machining Safety Education

NASA Astrophysics Data System (ADS)

Nakazawa, Tsuyoshi; Mita, Sumiyoshi; Matsubara, Masaaki; Takashima, Takeo; Tanaka, Koichi; Izawa, Satoru; Kawamura, Takashi

We developed two e-learning materials for Manufacturing Practice safety education: movie learning materials and hazard-detection learning materials. Using these video and sound media, students can learn how to operate machines safely with movie learning materials, which raise the effectiveness of preparation and review for manufacturing practice. Using these materials, students can realize safety operation well. Students can apply knowledge learned in lectures to the detection of hazards and use study methods for hazard detection during machine operation using the hazard-detection learning materials. Particularly, the hazard-detection learning materials raise students‧ safety consciousness and increase students‧ comprehension of knowledge from lectures and comprehension of operations during Manufacturing Practice.

CuAAC-Based Click Chemistry in Self-Healing Polymers.

PubMed

Döhler, Diana; Michael, Philipp; Binder, Wolfgang H

2017-10-17

Click chemistry has emerged as a significant tool for materials science, organic chemistry, and bioscience. Based on the initial concept of Barry Sharpless in 2001, the copper(I)-catalyzed azide/alkyne cycloaddition (CuAAC) reaction has triggered a plethora of chemical concepts for linking molecules and building blocks under ambient conditions, forming the basis for applications in autonomous cross-linking materials. Self-healing systems on the other hand are often based on mild cross-linking chemistries that are able to react either autonomously or upon an external trigger. In the ideal case, self-healing takes place efficiently at low temperatures, independent of the substrate(s) used, by forming strong and stable networks, binding to the newly generated (cracked) interfaces to restore the original material properties. The use of the CuAAC in self-healing systems, most of all the careful design of copper-based catalysts linked to additives as well as the chemical diversity of substrates, has led to an enormous potential of applications of this singular reaction. The implementation of click-based strategies in self-healing systems therefore is highly attractive, as here chemical (and physical) concepts of molecular reactivity, molecular design, and even metal catalysis are connected to aspects of materials science. In this Account, we will show how CuAAC reactions of multivalent components can be used as a tool for self-healing materials, achieving cross-linking at low temperatures (exploiting concepts of autocatalysis or internal chelation within the bulk CuAAC and systematic optimization of the efficiency of the used Cu(I) catalysts). Encapsulation strategies to separate the click components by micro- and nanoencapsulation are required in this context. Consequently, the examples reported here describe chemical concepts to realize more efficient and faster click reactions in self-healing polymeric materials. Thus, enhanced chain diffusion in (hyper)branched polymers, autocatalysis, or internal chelation concepts enable efficient click cross-linking already at 5 °C with a simultaneously reduced amount of Cu(I) catalyst and increased reaction rates, culminating in the first reported self-healing system based on click cycloaddition reactions. Via tailor-made nanocarbon/Cu(I) catalysts we can further improve the click cross-linking reaction in view of efficiency and kinetics, leading to the generation of self-healing graphene-based epoxy nanocomposites. Additionally, we have designed special CuAAC click methods for chemical reporting and visualization systems based on the detection of ruptured capsules via a fluorogenic click reaction, which can be combined with CuAAC cross-linking reactions to obtain simultaneous stress detection and self-healing within polymeric materials. In a similar concept, we have prepared polymeric Cu(I)-biscarbene complexes to detect (mechanical) stress within self-healing polymeric materials via a triggered fluorogenic reaction, thus using a destructive force for a constructive chemical response.

Nondestructive evaluation of structural ceramics by photoacoustic microscopy

NASA Technical Reports Server (NTRS)

Khandelwal, Pramod K.

1987-01-01

A photoacoustic microscopy (PAM) digital imaging system was developed and utilized to characterize silicon nitride material at the various stages of the ceramic fabrication process. Correlation studies revealed that photoacoustic microscopy detected failure initiating defects in substantially more specimens than microradiography and ultrasonic techniques. Photoacoustic microscopy detected 10 to 100 micron size surface and subsurface pores and inclusions, respectively, up to 80 microns below the interrogating surface in machined sintered silicon nitride. Microradiography detected 50 micron diameter fracture controlling pores and inclusions. Subsurface holes were detected up to a depth of 570 microns and 1.00 mm in sintered silicon nitride and silicon carbide, respectively. Seeded voids of 20 to 30 micron diameters at the surface and 50 microns below the interrogating surface were detected by photoacoustic microscopy and microradiography with 1 percent X-ray thickness sensitivity. Tight surface cracks of 96 micron length x 48 micron depth were detected by photoacoustic microscopy. PAM volatilized and removed material in the green state which resulted in linear shallow microcracks after sintering. This significantly limits the use of PAM as an in-process NDE technique.

Finger-attachment device for the feedback of gripping and pulling force in a manipulating system for brain tumor resection.

PubMed

Chinbe, Hiroyuki; Yoneyama, Takeshi; Watanabe, Tetsuyou; Miyashita, Katsuyoshi; Nakada, Mitsutoshi

2018-01-01

Development and evaluation of an effective attachment device for a bilateral brain tumor resection robotic surgery system based on the sensory performance of the human index finger in order to precisely detect gripping- and pulling-force feedback. First, a basic test was conducted to investigate the performance of the human index finger in the gripping- and pulling-force feedback system. Based on the test result, a new finger-attachment device was designed and constructed. Then, discrimination tests were conducted to assess the pulling force and the feedback on the hardness of the gripped material. The results of the basic test show the application of pulling force on the side surface of the finger has an advantage to distinguish the pulling force when the gripping force is applied on the finger-touching surface. Based on this result, a finger-attachment device that applies a gripping force on the finger surface and pulling force on the side surface of the finger was developed. By conducting a discrimination test to assess the hardness of the gripped material, an operator can distinguish whether the gripped material is harder or softer than a normal brain tissue. This will help in confirming whether the gripped material is a tumor. By conducting a discrimination test to assess the pulling force, an operator can distinguish the pulling-force resistance when attempting to pull off the soft material. Pulling-force feedback may help avoid the breaking of blood pipes when they are trapped in the gripper or attached to the gripped tissue. The finger-attachment device that was developed for detecting gripping- and pulling-force feedback may play an important role in the development of future neurosurgery robotic systems for precise and safe resection of brain tumors.

System and method for non-destructive evaluation of surface characteristics of a magnetic material

DOEpatents

Jiles, David C.; Sipahi, Levent B.

1994-05-17

A system and a related method for non-destructive evaluation of the surface characteristics of a magnetic material. The sample is excited by an alternating magnetic field. The field frequency, amplitude and offset are controlled according to a predetermined protocol. The Barkhausen response of the sample is detected for the various fields and offsets and is analyzed. The system produces information relating to the frequency content, the amplitude content, the average or RMS energy content, as well as count rate information, for each of the Barkhausen responses at each of the excitation levels applied during the protocol. That information provides a contiguous body of data, heretofore unavailable, which can be analyzed to deduce information about the surface characteristics of the material at various depths below the surface.

A Decision Theoretic Approach to Evaluate Radiation Detection Algorithms

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nobles, Mallory A.; Sego, Landon H.; Cooley, Scott K.

2013-07-01

There are a variety of sensor systems deployed at U.S. border crossings and ports of entry that scan for illicit nuclear material. In this work, we develop a framework for comparing the performance of detection algorithms that interpret the output of these scans and determine when secondary screening is needed. We optimize each algorithm to minimize its risk, or expected loss. We measure an algorithm’s risk by considering its performance over a sample, the probability distribution of threat sources, and the consequence of detection errors. While it is common to optimize algorithms by fixing one error rate and minimizing another,more » our framework allows one to simultaneously consider multiple types of detection errors. Our framework is flexible and easily adapted to many different assumptions regarding the probability of a vehicle containing illicit material, and the relative consequences of a false positive and false negative errors. Our methods can therefore inform decision makers of the algorithm family and parameter values which best reduce the threat from illicit nuclear material, given their understanding of the environment at any point in time. To illustrate the applicability of our methods, in this paper, we compare the risk from two families of detection algorithms and discuss the policy implications of our results.« less

A novel approach to simulate chest wall micro-motion for bio-radar life detection purpose

NASA Astrophysics Data System (ADS)

An, Qiang; Li, Zhao; Liang, Fulai; Chen, Fuming; Wang, Jianqi

2016-10-01

Volunteers are often recruited to serve as the detection targets during the research process of bio-radar life detection technology, in which the experiment results are highly susceptible to the physical status of different individuals (shape, posture, etc.). In order to objectively evaluate the radar system performance and life detection algorithms, a standard detection target is urgently needed. The paper first proposed a parameter quantitatively controllable system to simulate the chest wall micro-motion caused mainly by breathing and heart beating. Then, the paper continued to analyze the material and size selection of the scattering body mounted on the simulation system from the perspective of back scattering energy. The computational electromagnetic method was employed to determine the exact scattering body. Finally, on-site experiments were carried out to verify the reliability of the simulation platform utilizing an IR UWB bioradar. Experimental result shows that the proposed system can simulate a real human target from three aspects: respiration frequency, amplitude and body surface scattering energy. Thus, it can be utilized as a substitute for a human target in radar based non-contact life detection research in various scenarios.

Influence of incident angle on the decoding in laser polarization encoding guidance

NASA Astrophysics Data System (ADS)

Zhou, Muchun; Chen, Yanru; Zhao, Qi; Xin, Yu; Wen, Hongyuan

2009-07-01

Dynamic detection of polarization states is very important for laser polarization coding guidance systems. In this paper, a set of dynamic polarization decoding and detection system used in laser polarization coding guidance was designed. Detection process of the normal incident polarized light is analyzed with Jones Matrix; the system can effectively detect changes in polarization. Influence of non-normal incident light on performance of polarization decoding and detection system is studied; analysis showed that changes in incident angle will have a negative impact on measure results, the non-normal incident influence is mainly caused by second-order birefringence and polarization sensitivity effect generated in the phase delay and beam splitter prism. Combined with Fresnel formula, decoding errors of linearly polarized light, elliptically polarized light and circularly polarized light with different incident angles into the detector are calculated respectively, the results show that the decoding errors increase with increase of incident angle. Decoding errors have relations with geometry parameters, material refractive index of wave plate, polarization beam splitting prism. Decoding error can be reduced by using thin low-order wave-plate. Simulation of detection of polarized light with different incident angle confirmed the corresponding conclusions.

A new tool for the rapid remote detection of leaks from subsea pipelines during remotely operated vehicle inspections

NASA Astrophysics Data System (ADS)

McStay, D.; McIlroy, J.; Forte, A.; Lunney, F.; Greenway, T.; Thabeth, K.; Dean, G.

2005-06-01

A new 2000 m depth rated subsea sensor that can effectively, rapidly and remotely detect leaks of fluorescein dye, leak detection chemicals and hydraulic fluids from underwater structures is reported. The system utilizes ultra-bright LED technology to project a structured beam of light, at a wavelength suitable to excite the fluorescence of the target material, into the water column. The resultant fluorescence is collected and digital signal processing used to extract the intensity. The system is capable of detecting ppm concentrations of fluorescein at a range of 2.5 m in water in real time. The ability to stand-off from subsea structures, while rapidly detecting the chemicals makes the system highly suited to subsea leak inspections with remotely operated vehicles or autonomous underwater vehicles, as it allows the vehicles to be flown quickly and safely over the structure to be inspected. This increases both the speed and effectiveness of the inspection. The remote detection capability is also highly effective for probing complex underwater structures. The system has been successfully used in real subsea survey applications and has been found to be effective, user friendly and to dramatically reduce inspection times and hence costs.

Numerical analysis of PZT rebar active sensing system for structural health monitoring of RC structure

NASA Astrophysics Data System (ADS)

Wu, F.; Yi, J.; Li, W. J.

2014-03-01

An active sensing diagnostic system for reinforced concrete SHM has been under investigation. Test results show that the system can detect the damage of the structure. To fundamentally understand the damage algorithm and therefore to establish a robust diagnostic method, accurate Finite Element Analysis (FEA) for the system becomes essential. For the system, a rebar with surface bonded PZT under a transient wave load was simulated and analyzed using commercial FEA software. A detailed 2D axi-symmetric model for a rebar attaching PZT was first established. The model simulates the rebar with wedges, an epoxy adhesive layer, as well as a PZT layer. PZT material parameter transformation with high order tensors was discussed due to the format differences between IEEE Standard and ANSYS. The selection of material properties such as Raleigh damping coefficients was discussed. The direct coupled-field analysis type was selected during simulation. The results from simulation matched well with the experimental data. Further simulation for debonding damage detection for concrete beam with the PZT rebar has been performed. And the numerical results have been validated with test results too. The good consistency between two proves that the numerical models were reasonably accurate. Further system optimization has been performed based on these models. By changing PZT layout and size, the output signals could be increased with magnitudes. And the damage detection signals have been found to be increased exponentially with the debonding size of the rebar.

A three-stage treatment system for highly polluted urban road runoff.

PubMed

Hilliges, Rita; Schriewer, Alexander; Helmreich, Brigitte

2013-10-15

A three-stage treatment device for polluted urban road runoff was installed and tested at a highly trafficked urban road over a period of one year. In the first stage coarse material and particles from the runoff are removed by a special gutter system. The second stage eliminates particles using a hydrodynamic separator. In the third stage dissolved pollutants are adsorbed in a filter unit with lignite as filter material. Twenty-four rain events were sampled over the one year period and analyzed for dissolved and particulate copper (Cu), zinc (Zn), lead (Pb), suspended solids (SS), total organic carbon (TOC), sodium (Na), and pH value. The treatment system was able to safely retain all relevant pollutants during the investigated period, except Na. In the effluent of the treatment device Pb could never be detected, values measured for Zn were in the range of the detection limit. Cu, the element most frequently detected in the effluent, never exceeded the critical value of 50 μg/L set by the German Federal Soil Protection Act and Ordinance. The median Cu concentration in the effluent of the treatment system was 8.13 μg/L. The treatment system proved to be very effective. Highly polluted road runoff can be purified by the system to an extent that no contamination risk for soil and groundwater remains when infiltrated into the soil. Copyright © 2013 Elsevier Ltd. All rights reserved.

An improved NSGA - II algorithm for mixed model assembly line balancing

NASA Astrophysics Data System (ADS)

Wu, Yongming; Xu, Yanxia; Luo, Lifei; Zhang, Han; Zhao, Xudong

2018-05-01

Aiming at the problems of assembly line balancing and path optimization for material vehicles in mixed model manufacturing system, a multi-objective mixed model assembly line (MMAL), which is based on optimization objectives, influencing factors and constraints, is established. According to the specific situation, an improved NSGA-II algorithm based on ecological evolution strategy is designed. An environment self-detecting operator, which is used to detect whether the environment changes, is adopted in the algorithm. Finally, the effectiveness of proposed model and algorithm is verified by examples in a concrete mixing system.

Development of a written music-recognition system using Java and open source technologies

NASA Astrophysics Data System (ADS)

Loibner, Gernot; Schwarzl, Andreas; Kovač, Matthias; Paulus, Dietmar; Pölzleitner, Wolfgang

2005-10-01

We report on the development of a software system to recognize and interpret printed music. The overall goal is to scan printed music sheets, analyze and recognize the notes, timing, and written text, and derive the all necessary information to use the computers MIDI sound system to play the music. This function is primarily useful for musicians who want to digitize printed music for editing purposes. There exist a number of commercial systems that offer such a functionality. However, on testing these systems, we were astonished on how weak they behave in their pattern recognition parts. Although we submitted very clear and rather flawless scanning input, none of these systems was able to e.g. recognize all notes, staff lines, and systems. They all require a high degree of interaction, post-processing, and editing to get a decent digital version of the hard copy material. In this paper we focus on the pattern recognition area. In a first approach we tested more or less standard methods of adaptive thresholding, blob detection, line detection, and corner detection to find the notes, staff lines, and candidate objects subject to OCR. Many of the objects on this type of material can be learned in a training phase. None of the commercial systems we saw offers the option to train special characters or unusual signatures. A second goal in this project is to use a modern software engineering platform. We were interested in how well Java and open source technologies are suitable for pattern recognition and machine vision. The scanning of music served as a case-study.

Imaging spectroscopy: Earth and planetary remote sensing with the USGS Tetracorder and expert systems

USGS Publications Warehouse

Clark, Roger N.; Swayze, Gregg A.; Livo, K. Eric; Kokaly, Raymond F.; Sutley, Steve J.; Dalton, J. Brad; McDougal, Robert R.; Gent, Carol A.

2003-01-01

Imaging spectroscopy is a tool that can be used to spectrally identify and spatially map materials based on their specific chemical bonds. Spectroscopic analysis requires significantly more sophistication than has been employed in conventional broadband remote sensing analysis. We describe a new system that is effective at material identification and mapping: a set of algorithms within an expert system decision‐making framework that we call Tetracorder. The expertise in the system has been derived from scientific knowledge of spectral identification. The expert system rules are implemented in a decision tree where multiple algorithms are applied to spectral analysis, additional expert rules and algorithms can be applied based on initial results, and more decisions are made until spectral analysis is complete. Because certain spectral features are indicative of specific chemical bonds in materials, the system can accurately identify and map those materials. In this paper we describe the framework of the decision making process used for spectral identification, describe specific spectral feature analysis algorithms, and give examples of what analyses and types of maps are possible with imaging spectroscopy data. We also present the expert system rules that describe which diagnostic spectral features are used in the decision making process for a set of spectra of minerals and other common materials. We demonstrate the applications of Tetracorder to identify and map surface minerals, to detect sources of acid rock drainage, and to map vegetation species, ice, melting snow, water, and water pollution, all with one set of expert system rules. Mineral mapping can aid in geologic mapping and fault detection and can provide a better understanding of weathering, mineralization, hydrothermal alteration, and other geologic processes. Environmental site assessment, such as mapping source areas of acid mine drainage, has resulted in the acceleration of site cleanup, saving millions of dollars and years in cleanup time. Imaging spectroscopy data and Tetracorder analysis can be used to study both terrestrial and planetary science problems. Imaging spectroscopy can be used to probe planetary systems, including their atmospheres, oceans, and land surfaces.

Electrical network method for the thermal or structural characterization of a conducting material sample or structure

DOEpatents

Ortiz, Marco G.

1993-01-01

A method for modeling a conducting material sample or structure system, as an electrical network of resistances in which each resistance of the network is representative of a specific physical region of the system. The method encompasses measuring a resistance between two external leads and using this measurement in a series of equations describing the network to solve for the network resistances for a specified region and temperature. A calibration system is then developed using the calculated resistances at specified temperatures. This allows for the translation of the calculated resistances to a region temperature. The method can also be used to detect and quantify structural defects in the system.

Electrical network method for the thermal or structural characterization of a conducting material sample or structure

DOEpatents

Ortiz, M.G.

1993-06-08

A method for modeling a conducting material sample or structure system, as an electrical network of resistances in which each resistance of the network is representative of a specific physical region of the system. The method encompasses measuring a resistance between two external leads and using this measurement in a series of equations describing the network to solve for the network resistances for a specified region and temperature. A calibration system is then developed using the calculated resistances at specified temperatures. This allows for the translation of the calculated resistances to a region temperature. The method can also be used to detect and quantify structural defects in the system.

Optimizing spectral CT parameters for material classification tasks

NASA Astrophysics Data System (ADS)

Rigie, D. S.; La Rivière, P. J.

2016-06-01

In this work, we propose a framework for optimizing spectral CT imaging parameters and hardware design with regard to material classification tasks. Compared with conventional CT, many more parameters must be considered when designing spectral CT systems and protocols. These choices will impact material classification performance in a non-obvious, task-dependent way with direct implications for radiation dose reduction. In light of this, we adapt Hotelling Observer formalisms typically applied to signal detection tasks to the spectral CT, material-classification problem. The result is a rapidly computable metric that makes it possible to sweep out many system configurations, generating parameter optimization curves (POC’s) that can be used to select optimal settings. The proposed model avoids restrictive assumptions about the basis-material decomposition (e.g. linearity) and incorporates signal uncertainty with a stochastic object model. This technique is demonstrated on dual-kVp and photon-counting systems for two different, clinically motivated material classification tasks (kidney stone classification and plaque removal). We show that the POC’s predicted with the proposed analytic model agree well with those derived from computationally intensive numerical simulation studies.

Optimizing Spectral CT Parameters for Material Classification Tasks

PubMed Central

Rigie, D. S.; La Rivière, P. J.

2017-01-01

In this work, we propose a framework for optimizing spectral CT imaging parameters and hardware design with regard to material classification tasks. Compared with conventional CT, many more parameters must be considered when designing spectral CT systems and protocols. These choices will impact material classification performance in a non-obvious, task-dependent way with direct implications for radiation dose reduction. In light of this, we adapt Hotelling Observer formalisms typically applied to signal detection tasks to the spectral CT, material-classification problem. The result is a rapidly computable metric that makes it possible to sweep out many system configurations, generating parameter optimization curves (POC’s) that can be used to select optimal settings. The proposed model avoids restrictive assumptions about the basis-material decomposition (e.g. linearity) and incorporates signal uncertainty with a stochastic object model. This technique is demonstrated on dual-kVp and photon-counting systems for two different, clinically motivated material classification tasks (kidney stone classification and plaque removal). We show that the POC’s predicted with the proposed analytic model agree well with those derived from computationally intensive numerical simulation studies. PMID:27227430

Radiograph and passive data analysis using mixed variable optimization

DOEpatents

Temple, Brian A.; Armstrong, Jerawan C.; Buescher, Kevin L.; Favorite, Jeffrey A.

2015-06-02

Disclosed herein are representative embodiments of methods, apparatus, and systems for performing radiography analysis. For example, certain embodiments perform radiographic analysis using mixed variable computation techniques. One exemplary system comprises a radiation source, a two-dimensional detector for detecting radiation transmitted through a object between the radiation source and detector, and a computer. In this embodiment, the computer is configured to input the radiographic image data from the two-dimensional detector and to determine one or more materials that form the object by using an iterative analysis technique that selects the one or more materials from hierarchically arranged solution spaces of discrete material possibilities and selects the layer interfaces from the optimization of the continuous interface data.

Efficacy of reciprocating and rotary NiTi instruments for retreatment of curved root canals assessed by micro-CT.

PubMed

Rödig, T; Reicherts, P; Konietschke, F; Dullin, C; Hahn, W; Hülsmann, M

2014-10-01

To compare the efficacy of reciprocating and rotary NiTi-instruments in removing filling material from curved root canals using micro-computed tomography. Sixty curved root canals were prepared and filled with gutta-percha and sealer. After determination of root canal curvatures and radii in two directions as well as volumes of filling material, the teeth were assigned to three comparable groups (n = 20). Retreatment was performed using Reciproc, ProTaper Universal Retreatment or Hedström files. Percentages of residual filling material and dentine removal were assessed using micro-CT imaging. Working time and procedural errors were recorded. Statistical analysis was performed by variance procedures. No significant differences amongst the three retreatment techniques concerning residual filling material were detected (P > 0.05). Hedström files removed significantly more dentine than ProTaper Universal Retreatment (P < 0.05), but the difference concerning dentine removal between both NiTi systems was not significant (P > 0.05). Reciproc and ProTaper Universal Retreatment were significantly faster than Hedström files (P = 0.0001). No procedural errors such as instrument fracture, blockage, ledging or perforation were detected for Hedström files. Three perforations were recorded for ProTaper Universal Retreatment, and in both NiTi groups, one instrument fracture occured. Remnants of filling material were observed in all samples with no significant differences between the three techniques. Hedström files removed significantly more dentine than ProTaper Universal Retreatment, but no significant differences between both NiTi systems were detected. Procedural errors were observed with ProTaper Universal Retreatment and Reciproc. © 2014 International Endodontic Journal. Published by John Wiley & Sons Ltd.

Radiation detector based on a matrix of crossed wavelength-shifting fibers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Kross, Brian J.; Weisenberger, Andrew; Zorn, Carl

A radiation detection system comprising a detection grid of wavelength shifting fibers with a volume of scintillating material at the intersecting points of the fibers. Light detectors, preferably Silicon Photomultipliers, are positioned at the ends of the fibers. The position of radiation is determined from data obtained from the detection grid. The system is easily scalable, customizable, and also suitable for use in soil and underground applications. An alternate embodiment employs a fiber grid sheet or layer which is comprised of multiple fibers secured to one another within the same plane. This embodiment further includes shielding in order to preventmore » radiation cross-talk within the grid layer.« less

Deploying Nuclear Detection Systems: A Proposed Strategy for Combating Nuclear Terrorism

DTIC Science & Technology

2007-07-01

lower cost than other gamma radiation detectors (if increased count rate is all one is looking for). Low cost makes plastic scintillation detectors...material, particularly enriched uranium and plutonium, the basic fuel for nuclear bombs. • Measures to strengthen international institutions to... uranium to specifications required for a nuclear weapon.1 This illicit shipment of centrifuges was part of an international nuclear materials

Anisotropic determination and correction for ultrasonic flaw detection by spectral analysis

DOEpatents

Adler, Laszlo; Von Cook, K.; Simpson, Jr., William A.; Lewis, D. Kent

1978-01-01

The anisotropic nature of a material is determined by measuring the velocity of an ultrasonic longitudinal wave and a pair of perpendicular ultrasonic shear waves through a sample of the material each at a plurality of different angles in three planes orthogonal to each other. The determined anisotropic nature is used as a correction factor in a spectral analyzing system of flaw determination.

Permeation absorption sampler with multiple detection

DOEpatents

Zaromb, Solomon

1990-01-01

A system for detecting analytes in air or aqueous systems includes a permeation absorption preconcentrator sampler for the analytes and analyte detectors. The preconcentrator has an inner fluid-permeable container into which a charge of analyte-sorbing liquid is intermittently injected, and a fluid-impermeable outer container. The sample is passed through the outer container and around the inner container for trapping and preconcentrating the analyte in the sorbing liquid. The analyte can be detected photometrically by injecting with the sorbing material a reagent which reacts with the analyte to produce a characteristic color or fluorescence which is detected by illuminating the contents of the inner container with a light source and measuring the absorbed or emitted light, or by producing a characteristic chemiluminescence which can be detected by a suitable light sensor. The analyte can also be detected amperometrically. Multiple inner containers may be provided into which a plurality of sorbing liquids are respectively introduced for simultaneously detecting different analytes. Baffles may be provided in the outer container. A calibration technique is disclosed.

Safe gas handling and system design for the large scale production of amorphous silicon based solar cells

NASA Astrophysics Data System (ADS)

Fortmann, C. M.; Farley, M. V.; Smoot, M. A.; Fieselmann, B. F.

1988-07-01

Solarex is one of the leaders in amorphous silicon based photovoltaic production and research. The large scale production environment presents unique safety concerns related to the quantity of dangerous materials as well as the number of personnel handling these materials. The safety measures explored by this work include gas detection systems, training, and failure resistant gas handling systems. Our experiences with flow restricting orifices in the CGA connections and the use of steel cylinders is reviewed. The hazards and efficiency of wet scrubbers for silane exhausts are examined. We have found it to be useful to provide the scrubbler with temperature alarms.

Identification and Imaging of Special Nuclear Materials and Contraband using Active x-ray Interrogation

NASA Astrophysics Data System (ADS)

Van Liew, Seth; Bertozzi, William; D'Olympia, Nathan; Franklin, Wilbur A.; Korbly, Stephen E.; Ledoux, Robert J.; Wilson, Cody M.

A x-ray inspection system utilizing a continuous-wave 9 MeV rhodotron x-ray source for scanning cargo containers is presented. This system scans for contraband, anomalies, stowaway passengers, and nuclear threats for trucks and towed cargo containers. A transmission image is generated concurrently with a 3D image of the cargo, the latter presenting material information in the form of atomic number and density. Neutrons from photofission are also detected during each scan. In addition, nuclear resonance fluorescence detectors are capable of identifying specific isotopes. This system has recently been deployed at the Port of Boston.

The study of excited oxygen molecule gas species production and quenching on thermal protection system materials

NASA Technical Reports Server (NTRS)

Nordine, Paul C.; Fujimoto, Gordon T.; Greene, Frank T.

1987-01-01

The detection of excited oxygen and ozone molecules formed by surface catalyzed oxygen atom recombination and reaction was investigated by laser induced fluorescence (LIF), molecular beam mass spectrometric (MBMS), and field ionization (FI) techniques. The experiment used partially dissociated oxygen flows from a microwave discharge at pressures in the range from 60 to 400 Pa or from an inductively coupled RF discharge at atmospheric pressure. The catalyst materials investigated were nickel and the reaction cured glass coating used for Space Shuttle reusable surface insulation tiles. Nonradiative loss processes for the laser excited states makes LIF detection of O2 difficult such that formation of excited oxygen molecules could not be detected in the flow from the microwave discharge or in the gaseous products of atom loss on nickel. MBMS experiments showed that ozone was a product of heterogeneous O atom loss on nickel and tile surfaces at low temperatures and that ozone is lost on these materials at elevated temperatures. FI was separately investigated as a method by which excited oxygen molecules may be conveniently detected. Partial O2 dissociation decreases the current produced by FI of the gas.

Magnetoresistive flux focusing eddy current flaw detection

NASA Technical Reports Server (NTRS)

Wincheski, Russell A. (Inventor); Simpson, John W. (Inventor); Namkung, Min (Inventor)

2005-01-01

A giant magnetoresistive flux focusing eddy current device effectively detects deep flaws in thick multilayer conductive materials. The probe uses an excitation coil to induce eddy currents in conducting material perpendicularly oriented to the coil's longitudinal axis. A giant magnetoresistive (GMR) sensor, surrounded by the excitation coil, is used to detect generated fields. Between the excitation coil and GMR sensor is a highly permeable flux focusing lens which magnetically separates the GMR sensor and excitation coil and produces high flux density at the outer edge of the GMR sensor. The use of feedback inside the flux focusing lens enables complete cancellation of the leakage fields at the GMR sensor location and biasing of the GMR sensor to a location of high magnetic field sensitivity. In an alternate embodiment, a permanent magnet is positioned adjacent to the GMR sensor to accomplish the biasing. Experimental results have demonstrated identification of flaws up to 1 cm deep in aluminum alloy structures. To detect deep flaws about circular fasteners or inhomogeneities in thick multilayer conductive materials, the device is mounted in a hand-held rotating probe assembly that is connected to a computer for system control, data acquisition, processing and storage.

Hyperspectral target detection using manifold learning and multiple target spectra

DOE PAGES

Ziemann, Amanda K.; Theiler, James; Messinger, David W.

2016-03-31

Imagery collected from satellites and airborne platforms provides an important tool for remotely analyzing the content of a scene. In particular, the ability to remotely detect a specific material within a scene is of critical importance in nonproliferation and other applications. The sensor systems that process hyperspectral images collect the high-dimensional spectral information necessary to perform these detection analyses. For a d-dimensional hyperspectral image, however, where d is the number of spectral bands, it is common for the data to inherently occupy an m-dimensional space with m << d. In the remote sensing community, this has led to recent interestmore » in the use of manifold learning, which seeks to characterize the embedded lower-dimensional, nonlinear manifold that the data discretely approximate. The research presented in this paper focuses on a graph theory and manifold learning approach to target detection, using an adaptive version of locally linear embedding that is biased to separate target pixels from background pixels. Finally, this approach incorporates multiple target signatures for a particular material, accounting for the spectral variability that is often present within a solid material of interest.« less

Magnetoresistive Flux Focusing Eddy Current Flaw Detection

NASA Technical Reports Server (NTRS)

Wincheski, Russell A. (Inventor); Namkung, Min (Inventor); Simpson, John W. (Inventor)

2005-01-01

A giant magnetoresistive flux focusing eddy current device effectively detects deep flaws in thick multilayer conductive materials. The probe uses an excitation coil to induce eddy currents in conducting material perpendicularly oriented to the coil s longitudinal axis. A giant magnetoresistive (GMR) sensor, surrounded by the excitation coil, is used to detect generated fields. Between the excitation coil and GMR sensor is a highly permeable flux focusing lens which magnetically separates the GMR sensor and excitation coil and produces high flux density at the outer edge of the GMR sensor. The use of feedback inside the flux focusing lens enables complete cancellation of the leakage fields at the GMR sensor location and biasing of the GMR sensor to a location of high magnetic field sensitivity. In an alternate embodiment, a permanent magnet is positioned adjacent to the GMR sensor to accomplish the biasing. Experimental results have demonstrated identification of flaws up to 1 cm deep in aluminum alloy structures. To detect deep flaws about circular fasteners or inhomogeneities in thick multi-layer conductive materials, the device is mounted in a hand-held rotating probe assembly that is connected to a computer for system control, data acquisition, processing and storage.

Preparation of TNT, RDX and Ammonium Nitrate Standards on Gold-on-Silicon Surfaces by Thermal Inkjet Technology

NASA Astrophysics Data System (ADS)

Wrable-Rose, Madeline; Primera-Pedrozo, Oliva M.; Pacheco-Londoño, Leonardo C.; Hernandez-Rivera, Samuel P.

2010-12-01

This research examines the surface contamination properties, trace sample preparation methodologies, detection systems response and generation of explosive contamination standards for trace detection systems. Homogeneous and reproducible sample preparation is relevant for trace detection of chemical threats, such as warfare agents, highly energetic materials (HEM) and toxic industrial chemicals. The objective of this research was to develop a technology capable of producing samples and standards of HEM with controlled size and distribution on a substrate to generate specimens that would reproduce real contamination conditions. The research activities included (1) a study of the properties of particles generated by two deposition techniques: sample smearing deposition and inkjet deposition, on gold-coated silicon, glass and stainless steel substrates; (2) characterization of composition, distribution and adhesion characteristics of deposits; (3) evaluation of accuracy and reproducibility for depositing neat highly energetic materials such as TNT, RDX and ammonium nitrate; (4) a study of HEM-surface interactions using FTIR-RAIRS; and (5) establishment of protocols for validation of surface concentration using destructive methods such as HPLC.

Investigations of surface coatings to reduce memory effect in plastic scintillator detectors used for radioxenon detection

NASA Astrophysics Data System (ADS)

Bläckberg, L.; Fay, A.; Jõgi, I.; Biegalski, S.; Boman, M.; Elmgren, K.; Fritioff, T.; Johansson, A.; Mårtensson, L.; Nielsen, F.; Ringbom, A.; Rooth, M.; Sjöstrand, H.; Klintenberg, M.

2011-11-01

In this work Al2O3 and SiO2 coatings are tested as Xe diffusion barriers on plastic scintillator substrates. The motivation is improved beta-gamma coincidence detection systems, used to measure atmospheric radioxenon within the verification regime of the Comprehensive Nuclear-Test-Ban Treaty. One major drawback with the current setup of these systems is that the radioxenon tends to diffuse into the plastic scintillator material responsible for the beta detection, resulting in an unwanted memory effect. Here, coatings with thicknesses between 20 and 900 nm have been deposited onto plastic scintillators, and investigated using two different experimental techniques. The results show that all tested coatings reduce the Xe diffusion into the plastic. The reduction is observed to increase with coating thickness for both coating materials. The 425 nm Al2O3 coating is the most successful one, presenting a diffusion reduction of a factor 100, compared to uncoated plastic. In terms of memory effect reduction this coating is thus a viable solution to the problem in question.

Chromato-fluorographic drug detector. [device for detecting and recording fluorescent properties of materials

NASA Technical Reports Server (NTRS)

Parker, J. A.; Dimeff, J.; Heimbuch, A. H. (Inventor)

1974-01-01

A drug detecting apparatus which includes a chromatographic system for separating particular substances from a sample solution passed through it is described. A source of radiation causes the substance to emit fluorescent radiation as it moves through the chromatographic system. An optical system spectrally separates the fluorescent radiation according to wavelength and for focusing particular portions of the separated spectrum through an exit aperture. A photodetector which is responsive to the radiation passing through the exit aperture develops an electrical signal commensurate with the intensity of the radiation. The electrical signal is recorded to provide an indication of certain characteristics of the substance.

Vibrational spectroscopy standoff detection of threat chemicals

NASA Astrophysics Data System (ADS)

Ortiz-Rivera, William; Pacheco-Londoño, Leonardo C.; Castro-Suarez, John R.; Felix-Rivera, Hilsamar; Hernandez-Rivera, Samuel P.

2011-06-01

Spectroscopy based standoff detection systems: Raman and FTIR have been tested for detection of threat chemicals, including highly energetic materials, homemade explosives, explosives formulations and high explosives mixtures. Other threat chemicals studied included toxic industrial compounds (TIC) and chemical agent simulants. Microorganisms and biological threat agent simulants have also been detected at standoff distances. Open Path FTIR has been used to detect vapors and chemicals deposited on metal surfaces at μg/cm2 levels at distances as far as 30 m in active mode and 60 m in passive mode. In the case of Raman telescope, standoff distances for acetonitrile and ammonium nitrate were 140 m.

Raman scattering spectroscopy for explosives identification

NASA Astrophysics Data System (ADS)

Nagli, L.; Gaft, M.

2007-04-01

Real time detection and identification of explosives at a standoff distance is a major issue in efforts to develop defense against so-called Improvised Explosive Devices (IED). It is recognized that the only technique, which is potentially capable to standoff detection of minimal amounts of explosives is laser-based spectroscopy. LDS technique belongs to trace detection, namely to its micro-particles variety. We applied gated Raman and time-resolved luminescence spectroscopy for detection of main explosive materials, both factory and homemade. Raman system was developed and tested by LDS for field remote detection and identification of minimal amounts of explosives on relevant surfaces at a distance of up to 30 meters.

Application of High-Throughput Seebeck Microprobe Measurements on Thermoelectric Half-Heusler Thin Film Combinatorial Material Libraries.

PubMed

Ziolkowski, Pawel; Wambach, Matthias; Ludwig, Alfred; Mueller, Eckhard

2018-01-08

In view of the variety and complexity of thermoelectric (TE) material systems, combinatorial approaches to materials development come to the fore for identifying new promising compounds. The success of this approach is related to the availability and reliability of high-throughput characterization methods for identifying interrelations between materials structures and properties within the composition spread libraries. A meaningful characterization starts with determination of the Seebeck coefficient as a major feature of TE materials. Its measurement, and hence the accuracy and detectability of promising material compositions, may be strongly affected by thermal and electrical measurement conditions. This work illustrates the interrelated effects of the substrate material, the layer thickness, and spatial property distributions of thin film composition spread libraries, which are studied experimentally by local thermopower scans by means of the Potential and Seebeck Microprobe (PSM). The study is complemented by numerical evaluation. Material libraries of the half-Heusler compound system Ti-Ni-Sn were deposited on selected substrates (Si, AlN, Al 2 O 3 ) by magnetron sputtering. Assuming homogeneous properties of a film, significant decrease of the detected thermopower S m can be expected on substrates with higher thermal conductivity, yielding an underestimation of materials thermopower between 15% and 50%, according to FEM (finite element methods) simulations. Thermally poor conducting substrates provide a better accuracy with thermopower underestimates lower than 8%, but suffer from a lower spatial resolution. According to FEM simulations, local scanning of sharp thermopower peaks on lowly conductive substrates is linked to an additional deviation of the measured thermopower of up to 70% compared to homogeneous films, which is 66% higher than for corresponding cases on substrates with higher thermal conductivity of this study.

Trace vapor detection of hydrogen peroxide: An effective approach to identification of improvised explosive devices

NASA Astrophysics Data System (ADS)

Xu, Miao

Vapor detection has been proven as one of the practical, noninvasive methods suitable for explosives detection among current explosive detection technologies. Optical methods (especially colorimetric and fluorescence spectral methods) are low in cost, provide simple instrumentation alignment, while still maintaining high sensitivity and selectivity, these factors combined facilitate broad field applications. Trace vapor detection of hydrogen peroxide (H2O2) represents an effective approach to noninvasive detection of peroxide-based explosives, though development of such a sensor system with high reliability and sufficient sensitivity (reactivity) still remains challenging. Three vapor sensor systems for H2O2 were proposed and developed in this study, which exploited specific chemical reaction towards H2O2 to ensure the selectivity, and materials surface engineering to afford efficient air sampling. The combination of these features enables expedient, cost effective, reliable detection of peroxide explosives. First, an expedient colorimetric sensor for H2O2 vapor was developed, which utilized the specific interaction between Ti(oxo) and H2O2 to offer a yellow color development. The Ti(oxo) salt can be blended into a cellulose microfibril network to produce tunable interface that can react with H2O2. The vapor detection limit can reach 400 ppb. To further improve the detection sensitivity, a naphthalimide based fluorescence turn-on sensor was designed and developed. The sensor mechanism was based on H2O2-mediated oxidation of a boronate fluorophore, which is nonfluorescent in ICT band, but becomes strongly fluorescent upon conversion into the phenol state. The detection limit of this sensory material was improved to be below 10 ppb. However, some technical factors such as sensor concentration, local environment, and excitation intensity were found difficult to control to make the sensor system sufficiently reproducible. To solve the problem, we developed a ratiometric fluorescence sensor, which allows for dual-band emission monitoring and thus enhances the detection reliability. Moreover, the significant spectral overlap between the fluorescence of the pristine sensor and the absorption of the reacted state enables effective Foster Resonance Energy Transfer (FRET). This FRET process can significantly enhance the fluorescence sensing efficiency in comparison to the normal single-band sensor system, for which the sensing efficiency is solely determined by the stoichiometric conversion of sensor molecules.

Adaptive algorithm of selecting optimal variant of errors detection system for digital means of automation facility of oil and gas complex

NASA Astrophysics Data System (ADS)

Poluyan, A. Y.; Fugarov, D. D.; Purchina, O. A.; Nesterchuk, V. V.; Smirnova, O. V.; Petrenkova, S. B.

2018-05-01

To date, the problems associated with the detection of errors in digital equipment (DE) systems for the automation of explosive objects of the oil and gas complex are extremely actual. Especially this problem is actual for facilities where a violation of the accuracy of the DE will inevitably lead to man-made disasters and essential material damage, at such facilities, the diagnostics of the accuracy of the DE operation is one of the main elements of the industrial safety management system. In the work, the solution of the problem of selecting the optimal variant of the errors detection system of errors detection by a validation criterion. Known methods for solving these problems have an exponential valuation of labor intensity. Thus, with a view to reduce time for solving the problem, a validation criterion is compiled as an adaptive bionic algorithm. Bionic algorithms (BA) have proven effective in solving optimization problems. The advantages of bionic search include adaptability, learning ability, parallelism, the ability to build hybrid systems based on combining. [1].

Activation and evaluation of GaN photocathodes

NASA Astrophysics Data System (ADS)

Qian, Yunsheng; Chang, Benkang; Qiao, Jiangliang; Zhang, Yijun; Fu, Rongguo; Qiu, Yafeng

2009-09-01

Gallium Nitride (GaN) photocathodes are potentially attractive as UV detective materials and electron sources. Based on the activation and evaluation system for GaAs photocathode, which consists of ultra-high vacuum (UHV) activation chamber, multi-information measurement system, X-ray photoelectron spectroscopy (XPS), and ultraviolet ray photoelectron spectroscopy (UPS), the control and measurement system for the activation of UV photocathodes was developed. The developed system, which consists of Xenon lamp, monochromator with scanner, signal-processing module, power control unit of Cs and O source, A/D adapter, digital I/O card, computer and software, can control the activation of GaN photocathodes and measure on-line the spectral response curves of GaN photocathodes. GaN materials on sapphire substrate were grown by Metal-Organic Chemical Vapor Deposition (MOCVD) with p-type Mg doping. The GaN materials were activated by Cs-O. The spectral response and quantum efficiency (QE) were measured and calculated. The experiment results are discussed.

Methods and systems for detection of ice formation on surfaces

NASA Technical Reports Server (NTRS)

Alfano, Robert R. (Inventor); Wang, Wubao (Inventor); Sztul, Henry (Inventor); Budansky, Yury (Inventor)

2007-01-01

A system for detecting ice formation on metal, painted metal and other material surfaces can include a transparent window having an exterior surface upon which ice can form; a light source and optics configured and arranged to illuminate the exterior surface of the window from behind the exterior surface; and a detector and optics configured and arranged to receive light backscattered by the exterior surface and any ice disposed on the exterior surface and determine the thickness of the ice layer. For example, the system can be used with aircraft by placing one or more windows in the wings of the aircraft. The system is used for a novel optical method for real-time on-board detection and warning of ice formation on surfaces of airplanes, unmanned aerial vehicles (UAVs), and other vehicles and stationary structures to improve their safety and operation.

Developments on a SEM-based X-ray tomography system: Stabilization scheme and performance evaluation

NASA Astrophysics Data System (ADS)

Gomes Perini, L. A.; Bleuet, P.; Filevich, J.; Parker, W.; Buijsse, B.; Kwakman, L. F. Tz.

2017-06-01

Recent improvements in a SEM-based X-ray tomography system are described. In this type of equipment, X-rays are generated through the interaction between a highly focused electron-beam and a geometrically confined anode target. Unwanted long-term drifts of the e-beam can lead to loss of X-ray flux or decrease of spatial resolution in images. To circumvent this issue, a closed-loop control using FFT-based image correlation is integrated to the acquisition routine, in order to provide an in-line drift correction. The X-ray detection system consists of a state-of-the-art scientific CMOS camera (indirect detection), featuring high quantum efficiency (˜60%) and low read-out noise (˜1.2 electrons). The system performance is evaluated in terms of resolution, detectability, and scanning times for applications covering three different scientific fields: microelectronics, technical textile, and material science.

Development of the new generation of glass-based neutron detection materials

NASA Astrophysics Data System (ADS)

Dosovitskiy, Alexey E.; Dosovitskiy, Georgy A.; Korjik, Mikhail V.

2012-10-01

Approach to obtaining of neutron detector material alternative to 3He containing ionization gas detectors is proposed. Recently, a severe deficit of the 3He has pushed its price up strongly, so alternative cheaper detecting materials are demanded. Possible alternatives to 3He are materials containing 10B and 6Li isotopes. These two elements form many inorganic materials, either crystalline or amorphous. Glass scintillators look very advantageous as detector materials, especially for large area detectors, as their manufacturing could be cheaper and easier-to-scale, compared to single crystals and ceramics. A poor exciton transport, which is a fundamental feature of glass scintillators, limits their light yield and, therefore, practical use. Here we discuss a possibility to improve energy transfer to luminescent centers by creation of high concentration of crystalline luminophore particles in the glass matrix. This could be achieved through the controlled crystallization of the glass. We demonstrate how this approach works in well known Li-Al-Si (LAS) glass system. Partially crystallized Ce3+-doped glass with nanocrystalline inclusions is obtained, which shows the superior scintillation properties compared to amorphous glass. The material is characterized by an emission spectrum shift towards shorter wavelengths, which provides low light self-absorption.

A simulation study of detection of weapon of mass destruction based on radar

NASA Astrophysics Data System (ADS)

Sharifahmadian, E.; Choi, Y.; Latifi, S.

2013-05-01

Typical systems used for detection of Weapon of Mass Destruction (WMD) are based on sensing objects using gamma rays or neutrons. Nonetheless, depending on environmental conditions, current methods for detecting fissile materials have limited distance of effectiveness. Moreover, radiation related to gamma- rays can be easily shielded. Here, detecting concealed WMD from a distance is simulated and studied based on radar, especially WideBand (WB) technology. The WB-based method capitalizes on the fact that electromagnetic waves penetrate through different materials at different rates. While low-frequency waves can pass through objects more easily, high-frequency waves have a higher rate of absorption by objects, making the object recognition easier. Measuring the penetration depth allows one to identify the sensed material. During simulation, radar waves and propagation area including free space, and objects in the scene are modeled. In fact, each material is modeled as a layer with a certain thickness. At start of simulation, a modeled radar wave is radiated toward the layers. At the receiver side, based on the received signals from every layer, each layer can be identified. When an electromagnetic wave passes through an object, the wave's power will be subject to a certain level of attenuation depending of the object's characteristics. Simulation is performed using radar signals with different frequencies (ranges MHz-GHz) and powers to identify different layers.

SWIR hyperspectral imaging detector for surface residues

NASA Astrophysics Data System (ADS)

Nelson, Matthew P.; Mangold, Paul; Gomer, Nathaniel; Klueva, Oksana; Treado, Patrick

2013-05-01

ChemImage has developed a SWIR Hyperspectral Imaging (HSI) sensor which uses hyperspectral imaging for wide area surveillance and standoff detection of surface residues. Existing detection technologies often require close proximity for sensing or detecting, endangering operators and costly equipment. Furthermore, most of the existing sensors do not support autonomous, real-time, mobile platform based detection of threats. The SWIR HSI sensor provides real-time standoff detection of surface residues. The SWIR HSI sensor provides wide area surveillance and HSI capability enabled by liquid crystal tunable filter technology. Easy-to-use detection software with a simple, intuitive user interface produces automated alarms and real-time display of threat and type. The system has potential to be used for the detection of variety of threats including chemicals and illicit drug substances and allows for easy updates in the field for detection of new hazardous materials. SWIR HSI technology could be used by law enforcement for standoff screening of suspicious locations and vehicles in pursuit of illegal labs or combat engineers to support route-clearance applications- ultimately to save the lives of soldiers and civilians. In this paper, results from a SWIR HSI sensor, which include detection of various materials in bulk form, as well as residue amounts on vehicles, people and other surfaces, will be discussed.

Subsurface sounders

NASA Technical Reports Server (NTRS)

1975-01-01

Airborne or spaceborne electromagnetic systems used to detect subsurface features are discussed. Data are given as a function of resistivity of ground material, magnetic permeability of free space, and angular frequency. It was noted that resistivities vary with the water content and temperature.

Thin-Layer and Paper Chromatography.

ERIC Educational Resources Information Center

Sherma, Joseph; Fried, Bernard

1984-01-01

Reviews literature on chromatography examining: books, reviews, student experiments; chromatographic systems, techniques, apparatus; detecting and identification of separated zones; preparative chromatography and radiochromatography; and applications related to specific materials (such as acids, alcohols, amino acids, antibiotics, enzymes, dyes,…

Design of a piezoelectric-based structural health monitoring system for damage detection in composite materials

NASA Astrophysics Data System (ADS)

Kessler, Seth S.; Spearing, S. Mark

2002-07-01

Cost-effective and reliable damage detection is critical for the utilization of composite materials. This paper presents the conclusions of an experimental and analytical survey of candidate methods for in-situ damage detection in composite structures. Experimental results are presented for the application of modal analysis and Lamb wave techniques to quasi-isotropic graphite/epoxy test specimens containing representative damage. Piezoelectric patches were used as actuators and sensors for both sets of experiments. Modal analysis methods were reliable for detecting small amounts of global damage in a simple composite structure. By comparison, Lamb wave methods were sensitive to all types of local damage present between the sensor and actuator, provided useful information about damage presence and severity, and present the possibility of estimating damage type and location. Analogous experiments were also performed for more complex built-up structures. These techniques are suitable for structural health monitoring applications since they can be applied with low power conformable sensors and can provide useful information about the state of a structure during operation. Piezoelectric patches could also be used as multipurpose sensors to detect damage by a variety of methods such as modal analysis, Lamb wave, acoustic emission and strain based methods simultaneously, by altering driving frequencies and sampling rates. This paper present guidelines and recommendations drawn from this research to assist in the design of a structural health monitoring system for a vehicle. These systems will be an important component in future designs of air and spacecraft to increase the feasibility of their missions.

A Portable Wireless Communication Platform Based on a Multi-Material Fiber Sensor for Real-Time Breath Detection

PubMed Central

Bellemare-Rousseau, Simon; Khalil, Mazen; Messaddeq, Younes

2018-01-01

In this paper, we present a new mobile wireless communication platform for real-time monitoring of an individual’s breathing rate. The platform takes the form of a wearable stretching T-shirt featuring a sensor and a detection base station. The sensor is formed by a spiral-shaped antenna made from a multi-material fiber connected to a compact transmitter. Based on the resonance frequency of the antenna at approximately 2.4 GHz, the breathing sensor relies on its Bluetooth transmitter. The contactless and non-invasive sensor is designed without compromising the user’s comfort. The sensing mechanism of the system is based on the detection of the signal amplitude transmitted wirelessly by the sensor, which is found to be sensitive to strain. We demonstrate the capability of the platform to detect the breathing rates of four male volunteers who are not in movement. The breathing pattern is obtained through the received signal strength indicator (RSSI) which is filtered and analyzed with home-made algorithms in the portable system. Numerical simulations of human breath are performed to support the experimental detection, and both results are in a good agreement. Slow, fast, regular, irregular, and shallow breathing types are successfully recorded within a frequency interval of 0.16–1.2 Hz, leading to a breathing rate varying from 10 to 72 breaths per minute. PMID:29587396

A Portable Wireless Communication Platform Based on a Multi-Material Fiber Sensor for Real-Time Breath Detection.

PubMed

Roudjane, Mourad; Bellemare-Rousseau, Simon; Khalil, Mazen; Gorgutsa, Stepan; Miled, Amine; Messaddeq, Younes

2018-03-25

In this paper, we present a new mobile wireless communication platform for real-time monitoring of an individual's breathing rate. The platform takes the form of a wearable stretching T-shirt featuring a sensor and a detection base station. The sensor is formed by a spiral-shaped antenna made from a multi-material fiber connected to a compact transmitter. Based on the resonance frequency of the antenna at approximately 2.4 GHz, the breathing sensor relies on its Bluetooth transmitter. The contactless and non-invasive sensor is designed without compromising the user's comfort. The sensing mechanism of the system is based on the detection of the signal amplitude transmitted wirelessly by the sensor, which is found to be sensitive to strain. We demonstrate the capability of the platform to detect the breathing rates of four male volunteers who are not in movement. The breathing pattern is obtained through the received signal strength indicator (RSSI) which is filtered and analyzed with home-made algorithms in the portable system. Numerical simulations of human breath are performed to support the experimental detection, and both results are in a good agreement. Slow, fast, regular, irregular, and shallow breathing types are successfully recorded within a frequency interval of 0.16-1.2 Hz, leading to a breathing rate varying from 10 to 72 breaths per minute.