Science.gov

Sample records for medium energy x-rays

  1. The energy dependence of lithium formate and alanine EPR dosimeters for medium energy x rays

    SciTech Connect

    Waldeland, Einar; Hole, Eli Olaug; Sagstuen, Einar; Malinen, Eirik

    2010-07-15

    Purpose: To perform a systematic investigation of the energy dependence of alanine and lilthium formate EPR dosimeters for medium energy x rays. Methods: Lithium formate and alanine EPR dosimeters were exposed to eight different x-ray beam qualities, with nominal potentials ranging from 50 to 200 kV. Following ionometry based on standards of absorbed dose to water, the dosimeters were given two different doses of approximately 3 and 6 Gy for each radiation quality, with three dosimeters for each dose. A reference series was also irradiated to three different dose levels at a {sup 60}Co unit. The dose to water energy response, that is, the dosimeter reading per absorbed dose to water relative to that for {sup 60}Co {gamma}-rays, was estimated for each beam quality. In addition, the energy response was calculated by Monte Carlo simulations and compared to the experimental energy response. Results: The experimental energy response estimates ranged from 0.89 to 0.94 and from 0.68 to 0.90 for lithium formate and alanine, respectively. The uncertainties in the experimental energy response estimates were typically 3%. The relative effectiveness, that is, the ratio of the experimental energy response to that following Monte Carlo simulations was, on average, 0.96 and 0.94 for lithium formate and alanine, respectively. Conclusions: This work shows that lithium formate dosimeters are less dependent on x-ray energy than alanine. Furthermore, as the relative effectiveness for both lithium formate and alanine were systematically less than unity, the yield of radiation-induced radicals is decreased following x-irradiation compared to irradiation with {sup 60}Co {gamma}-rays.

  2. Relative response of the alanine dosimeter to medium energy x-rays.

    PubMed

    Anton, M; Büermann, L

    2015-08-01

    The response of the alanine dosimeter to kilovoltage x-rays with respect to the dose to water was measured, relative to the response to Co-60 radiation.Two series of x-ray qualities were investigated, one ranging from 30 kV to 100 kV tube voltage (TW series), the other one ranging from 70 kV to 280 kV (TH series). Due to the use of the water calorimeter as a primary standard, the uncertainty of the delivered dose is significantly lower than for other published data. The alanine response was measured as described in a previous publication (Anton et al 2013 Phys. Med. Biol. 58 3259-82). The uncertainty component due to the alanine measurement and analysis is ⩽0.4%, the major part of the combined uncertainty of the relative response originates from the uncertainty of the delivered dose. The relative uncertainties of the relative response vary from ⩽2% for the TW series to ⩽1.1% for the TH series.Different from the behaviour of the alanine dosimeter for megavoltage x-rays or electrons, the relative response drops significantly from unity for Co-60 radiation to less than 64% for the TW quality with a tube voltage of 30 kV. In order to reproduce this behaviour through Monte Carlo simulations, not only the ratio of the absorbed dose to alanine to the absorbed dose to water has to be known, but also the intrinsic efficiency, i.e. the dependence of the number of free radicals generated per unit of absorbed dose on the photon energy. This quantity is not yet accessible for the TW series.For a possible use of the alanine dosimeter for kilovoltage x-rays, for example in electronic brachytherapy, users should rely on the measured data for the relative response which have become available with this publication. PMID:26216572

  3. Relative response of the alanine dosimeter to medium energy x-rays

    NASA Astrophysics Data System (ADS)

    Anton, M.; Büermann, L.

    2015-08-01

    The response of the alanine dosimeter to kilovoltage x-rays with respect to the dose to water was measured, relative to the response to Co-60 radiation. Two series of x-ray qualities were investigated, one ranging from 30 kV to 100 kV tube voltage (TW series), the other one ranging from 70 kV to 280 kV (TH series). Due to the use of the water calorimeter as a primary standard, the uncertainty of the delivered dose is significantly lower than for other published data. The alanine response was measured as described in a previous publication (Anton et al 2013 Phys. Med. Biol. 58 3259-82). The uncertainty component due to the alanine measurement and analysis is ⩽0.4%, the major part of the combined uncertainty of the relative response originates from the uncertainty of the delivered dose. The relative uncertainties of the relative response vary from ⩽2% for the TW series to ⩽1.1% for the TH series. Different from the behaviour of the alanine dosimeter for megavoltage x-rays or electrons, the relative response drops significantly from unity for Co-60 radiation to less than 64% for the TW quality with a tube voltage of 30 kV. In order to reproduce this behaviour through Monte Carlo simulations, not only the ratio of the absorbed dose to alanine to the absorbed dose to water has to be known, but also the intrinsic efficiency, i.e. the dependence of the number of free radicals generated per unit of absorbed dose on the photon energy. This quantity is not yet accessible for the TW series. For a possible use of the alanine dosimeter for kilovoltage x-rays, for example in electronic brachytherapy, users should rely on the measured data for the relative response which have become available with this publication.

  4. Relative response of the alanine dosimeter to medium energy x-rays.

    PubMed

    Anton, M; Büermann, L

    2015-08-01

    The response of the alanine dosimeter to kilovoltage x-rays with respect to the dose to water was measured, relative to the response to Co-60 radiation.Two series of x-ray qualities were investigated, one ranging from 30 kV to 100 kV tube voltage (TW series), the other one ranging from 70 kV to 280 kV (TH series). Due to the use of the water calorimeter as a primary standard, the uncertainty of the delivered dose is significantly lower than for other published data. The alanine response was measured as described in a previous publication (Anton et al 2013 Phys. Med. Biol. 58 3259-82). The uncertainty component due to the alanine measurement and analysis is ⩽0.4%, the major part of the combined uncertainty of the relative response originates from the uncertainty of the delivered dose. The relative uncertainties of the relative response vary from ⩽2% for the TW series to ⩽1.1% for the TH series.Different from the behaviour of the alanine dosimeter for megavoltage x-rays or electrons, the relative response drops significantly from unity for Co-60 radiation to less than 64% for the TW quality with a tube voltage of 30 kV. In order to reproduce this behaviour through Monte Carlo simulations, not only the ratio of the absorbed dose to alanine to the absorbed dose to water has to be known, but also the intrinsic efficiency, i.e. the dependence of the number of free radicals generated per unit of absorbed dose on the photon energy. This quantity is not yet accessible for the TW series.For a possible use of the alanine dosimeter for kilovoltage x-rays, for example in electronic brachytherapy, users should rely on the measured data for the relative response which have become available with this publication.

  5. Quality indexes based on water measurements for low and medium energy x-ray beams: A theoretical study with PENELOPE

    SciTech Connect

    Chica, U.; Anguiano, M.; Lallena, A. M.; Vilches, M.

    2014-01-15

    Purpose : To study the use of quality indexes based on ratios of absorbed doses in water at two different depths to characterize x-ray beams of low and medium energies. Methods : A total of 55 x-ray beam spectra were generated with the codes XCOMP5R and SPEKCALC and used as input of a series of Monte Carlo simulations performed with PENELOPE, in which the percentage depth doses in water and thek{sub Q,Q{sub 0}} factors, defined in the TRS-398 protocol, were determined for each beam. Some of these calculations were performed by simulating the ionization chamber PTW 30010. Results : The authors found that the relation betweenk{sub Q,Q{sub 0}} and the ratios of absorbed doses at two depths is almost linear. A set of ratios statistically compatible with that showing the best fit has been determined. Conclusions : The results of this study point out which of these ratios of absorbed doses in water could be used to better characterize x-ray beams of low and medium energies.

  6. An alternative scheme of angular-dispersion analyzers for high-resolution medium-energy inelastic X-ray scattering.

    PubMed

    Huang, Xian Rong

    2011-11-01

    The development of medium-energy inelastic X-ray scattering optics with meV and sub-meV resolution has attracted considerable efforts in recent years. Meanwhile, there are also concerns or debates about the fundamental and feasibility of the involved schemes. Here the central optical component, the back-reflection angular-dispersion monochromator or analyzer, is analyzed. The results show that the multiple-beam diffraction effect together with transmission-induced absorption can noticeably reduce the diffraction efficiency, although it may not be a fatal threat. In order to improve the efficiency, a simple four-bounce analyzer is proposed that completely avoids these two adverse effects. The new scheme is illustrated to be a feasible alternative approach for developing meV- to sub-meV-resolution inelastic X-ray scattering spectroscopy.

  7. Development of observational and instrumental techniques in hard X-ray and medium energy gamma-ray astronomy

    NASA Technical Reports Server (NTRS)

    Pelling, M.

    1985-01-01

    The technical activities, scientific results, related space hardware projects and personnel of the high energy astrophysics program are reported. The development of observational and instrumental techniques in hard X-ray (0.001 to 100 keV) and medium energy gamma-ray (0.1 to 10 MeV) astronomy are examined. Many of these techniques were developed explicitly for use on high altitude balloons where most of the scientific results were obtained. The extensive observational activity using balloons are tabulated. Virtually every research activity will eventually result in a major space hardware development effort.

  8. ART-XC: A Medium-energy X-ray Telescope System for the Spectrum-R-Gamma Mission

    NASA Technical Reports Server (NTRS)

    Arefiev, V.; Pavlinsky, M.; Lapshov, I.; Thachenko, A.; Sazonov, S.; Revnivtsev, M.; Semena, N.; Buntov,M.; Vikhlinin, A.; Gubarev, M.; ODell, S.; Ramsey, B.; Romaine, S.; Swartz. D/; Weisskopf, M.; Hasinger, G.; Predehl, P.; Grigorovich, S.; Litvin, D.; Meidinger, N.; Strueder, L. W.

    2008-01-01

    The ART-XC instrument is an X-ray grazing-incidence telescope system in an ABRIXAS-type optical configuration optimized for the survey observational mode of the Spectrum-RG astrophysical mission which is scheduled to be launched in 2011. ART-XC has two units, each equipped with four identical X-ray multi-shell mirror modules. The optical axes of the individual mirror modules are not parallel but are separated by several degrees to permit the four modules to share a single CCD focal plane detector, 1/4 of the area each. The 450-micron-thick pnCCD (similar to the adjacent eROSITA telescope detector) will allow detection of X-ray photons up to 15 keV. The field of view of the individual mirror module is about 18 x 18 arcminutes(exp 2) and the sensitivity of the ART-XC system for 4 years of survey will be better than 10(exp -12) erg s(exp -1) cm(exp -2) over the 4-12 keV energy band. This will allow the ART-XC instrument to discover several thousand new AGNs.

  9. Observing soft X-ray line emission from the interstellar medium with X-ray calorimeter on a sounding rocket

    NASA Technical Reports Server (NTRS)

    Zhang, J.; Edwards, B.; Juda, M.; Mccammon, D.; Skinner, M.; Kelley, R.; Moseley, H.; Schoelkopf, R.; Szymkowiak, A.

    1990-01-01

    For an X-ray calorimeter working at 0.1 K, the energy resolution ideally can be as good as one eV for a practical detector. A detector with a resolution of 17 eV FWHM at 6 keV has been constructed. It is expected that this can be improved by a factor of two or more. With X-ray calorimeters flown on a sounding rocket, it should be possible to observe soft X-ray line emission from the interstellar medium over the energy range 0.07 to 1 keV. Here, a preliminary design for an X-ray calorimeter rocket experiment and the spectrum which might be observed from an equilibrium plasma are presented. For later X-ray calorimeter sounding rocket experiments, it is planned to add an aluminum foil mirror with collecting area of about 400 sq cm to observe line features from bright supernova remnants.

  10. First international comparison of primary absorbed dose to water standards in the medium-energy X-ray range

    NASA Astrophysics Data System (ADS)

    Büermann, Ludwig; Guerra, Antonio Stefano; Pimpinella, Maria; Pinto, Massimo; de Pooter, Jacco; de Prez, Leon; Jansen, Bartel; Denoziere, Marc; Rapp, Benjamin

    2016-01-01

    This report presents the results of the first international comparison of primary measurement standards of absorbed dose to water for the medium-energy X-ray range. Three of the participants (VSL, PTB, LNE-LNHB) used their existing water calorimeter based standards and one participant (ENEA) recently developed a new standard based on a water-graphite calorimeter. The participants calibrated three transfer chambers of the same type in terms of absorbed dose to water (NDw) and in addition in terms of air kerma (NK) using the CCRI radiation qualities in the range 100 kV to 250 kV. The additional NK values were intended to be used for a physical analysis of the ratios NDw/NK. All participants had previously participated in the BIPM.RI(I)-K3 key comparison of air kerma standards. Ratios of pairs of NMI's NK results of the current comparison were found to be consistent with the corresponding key comparison results within the expanded uncertainties of 0.6 % - 1 %. The NDw results were analysed in terms of the degrees of equivalence with the comparison reference values which were calculated for each beam quality as the weighted means of all results. The participant's results were consistent with the reference value within the expanded uncertainties. However, these expanded uncertainties varied significantly and ranged between about 1-1.8 % for the water calorimeter based standards and were estimated at 3.7 % for the water-graphite calorimeter. It was shown previously that the ratios NDw/NK for the type of ionization chamber used as transfer chamber in this comparison were very close (within less than 1 %) to the calculated values of (bar muen/ρ)w,ad, the mean values of the water-to-air ratio of the mass-energy-absorption coefficients at the depth d in water. Some of the participant's results deviated significantly from the expected behavior. Main text To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of

  11. KEY COMPARISON: APMP/TCRI key comparison report of measurement of air kerma for medium-energy x-rays (APMP.RI(I)-K3)

    NASA Astrophysics Data System (ADS)

    Lee, J. H.; Hwang, W. S.; Kotler, L. H.; Webb, D. V.; Büermann, L.; Burns, D. T.; Takeyeddin, M.; Shaha, V. V.; Srimanoroth, S.; Meghzifene, A.; Hah, S. H.; Chun, K. J.; Kadni, T. B.; Takata, N.; Msimang, Z.

    2008-01-01

    The APMP/TCRI Dosimetry Working Group performed the APMP.RI(I)-K3 key comparison of measurement of air kerma for medium-energy x-rays (100 kV to 250 kV) between 2000 and 2003. In total, 11 institutes took part in the comparison, among which 8 were APMP member laboratories. Two commercial cavity ionization chambers were used as transfer instruments and circulated among the participants. All the participants established the 100 kV, 135 kV, 180 kV and 250 kV x-ray beam qualities equivalent to those of the BIPM. The results showed that the maximum difference between the participants and the BIPM in the medium-energy x ray range, evaluated using the comparison data of the linking laboratories ARPANSA and PTB, is less than 1.4%. The degrees of equivalence between the participants are presented and this comparison confirms the calibration capabilities of the participating laboratories. Main text. To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/. The final report has been peer-reviewed and approved for publication by the CCRI Section I, according to the provisions of the CIPM Mutual Recognition Arrangement (MRA).

  12. X-ray diffraction study of stress relaxation in cubic boron nitride films grown with simultaneous medium-energy ion bombardment

    SciTech Connect

    Abendroth, B.; Gago, R.; Eichhorn, F.; Moeller, W.

    2004-12-13

    Relaxation of the intrinsic stress of cubic boron nitride (cBN) thin films has been studied by x-ray diffraction (XRD) using synchrotron light. The stress relaxation has been attained by simultaneous medium-energy ion bombardment (2-10 keV) during magnetron sputter deposition, and was confirmed macroscopically by substrate curvature measurements. In order to investigate the stress-release mechanisms, XRD measurements were performed in in-plane and out-of-plane geometry. The analysis shows a pronounced biaxial state of compressive stress in the cBN films grown without medium-energy ion bombardment. This stress is partially released during the medium-energy ion bombardment. It is suggested that the main path for stress relaxation is the elimination of strain within the cBN grains due to annealing of interstitials.

  13. A graphite calorimeter for absolute measurements of absorbed dose to water: application in medium-energy x-ray filtered beams

    NASA Astrophysics Data System (ADS)

    Pinto, M.; Pimpinella, M.; Quini, M.; D'Arienzo, M.; Astefanoaei, I.; Loreti, S.; Guerra, A. S.

    2016-02-01

    The Italian National Institute of Ionizing Radiation Metrology (ENEA-INMRI) has designed and built a graphite calorimeter that, in a water phantom, has allowed the determination of the absorbed dose to water in medium-energy x-rays with generating voltages from 180 to 250 kV. The new standard is a miniaturized three-bodies calorimeter, with a disc-shaped core of 21 mm diameter and 2 mm thickness weighing 1.134 g, sealed in a PMMA waterproof envelope with air-evacuated gaps. The measured absorbed dose to graphite is converted into absorbed dose to water by means of an energy-dependent conversion factor obtained from Monte Carlo simulations. Heat-transfer correction factors were determined by FEM calculations. At a source-to-detector distance of 100 cm, a depth in water of 2 g cm-2, and at a dose rate of about 0.15 Gy min-1, results of calorimetric measurements of absorbed dose to water, D w, were compared to experimental determinations, D wK, obtained via an ionization chamber calibrated in terms of air kerma, according to established dosimetry protocols. The combined standard uncertainty of D w and D wK were estimated as 1.9% and 1.7%, respectively. The two absorbed dose to water determinations were in agreement within 1%, well below the stated measurement uncertainties. Advancements are in progress to extend the measurement capability of the new in-water-phantom graphite calorimeter to other filtered medium-energy x-ray qualities and to reduce the D w uncertainty to around 1%. The new calorimeter represents the first implementation of in-water-phantom graphite calorimetry in the kilovoltage range and, allowing independent determinations of D w, it will contribute to establish a robust system of absorbed dose to water primary standards for medium-energy x-ray beams.

  14. A graphite calorimeter for absolute measurements of absorbed dose to water: application in medium-energy x-ray filtered beams.

    PubMed

    Pinto, M; Pimpinella, M; Quini, M; D'Arienzo, M; Astefanoaei, I; Loreti, S; Guerra, A S

    2016-02-21

    The Italian National Institute of Ionizing Radiation Metrology (ENEA-INMRI) has designed and built a graphite calorimeter that, in a water phantom, has allowed the determination of the absorbed dose to water in medium-energy x-rays with generating voltages from 180 to 250 kV. The new standard is a miniaturized three-bodies calorimeter, with a disc-shaped core of 21 mm diameter and 2 mm thickness weighing 1.134 g, sealed in a PMMA waterproof envelope with air-evacuated gaps. The measured absorbed dose to graphite is converted into absorbed dose to water by means of an energy-dependent conversion factor obtained from Monte Carlo simulations. Heat-transfer correction factors were determined by FEM calculations. At a source-to-detector distance of 100 cm, a depth in water of 2 g cm(-2), and at a dose rate of about 0.15 Gy min(-1), results of calorimetric measurements of absorbed dose to water, D(w), were compared to experimental determinations, D wK, obtained via an ionization chamber calibrated in terms of air kerma, according to established dosimetry protocols. The combined standard uncertainty of D(w) and D(wK) were estimated as 1.9% and 1.7%, respectively. The two absorbed dose to water determinations were in agreement within 1%, well below the stated measurement uncertainties. Advancements are in progress to extend the measurement capability of the new in-water-phantom graphite calorimeter to other filtered medium-energy x-ray qualities and to reduce the D(w) uncertainty to around 1%. The new calorimeter represents the first implementation of in-water-phantom graphite calorimetry in the kilovoltage range and, allowing independent determinations of D(w), it will contribute to establish a robust system of absorbed dose to water primary standards for medium-energy x-ray beams. PMID:26841127

  15. Key comparison BIPM.RI(I)-K3 of the air-kerma standards of the NRC, Canada and the BIPM in medium-energy x-rays

    NASA Astrophysics Data System (ADS)

    Burns, D. T.; Kessler, C.; Mainegra-Hing, E.; Shen, H.; McEwen, M. R.

    2016-01-01

    A key comparison has been made between the air-kerma standards of the NRC, Canada and the BIPM in the medium-energy x-ray range. The results show the standards to be in agreement at the level of the standard uncertainty of the comparison of 3.3 parts in 103. The results are analysed and presented in terms of degrees of equivalence, suitable for entry in the BIPM key comparison database. Main text To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/. The final report has been peer-reviewed and approved for publication by the CCRI, according to the provisions of the CIPM Mutual Recognition Arrangement (CIPM MRA).

  16. Key comparison BIPM.RI(I)-K3 of the air-kerma standards of the NMIJ, Japan and the BIPM in medium-energy x-rays

    NASA Astrophysics Data System (ADS)

    Burns, D. T.; Kessler, C.; Tanaka, T.; Kurosawa, T.; Saito, N.

    2016-01-01

    A key comparison has been made between the air-kerma standards of the NMIJ, Japan and the BIPM in the medium-energy x-ray range. The results show the standards to be in agreement at the level of the standard uncertainty of the comparison of 3.1 parts in 103. A trend is evident in the results for the different radiation qualities. The results are analysed and presented in terms of degrees of equivalence, suitable for entry in the BIPM key comparison database. Main text To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/. The final report has been peer-reviewed and approved for publication by the CCRI, according to the provisions of the CIPM Mutual Recognition Arrangement (CIPM MRA).

  17. X-Ray Transition Energies Database

    National Institute of Standards and Technology Data Gateway

    SRD 128 X-Ray Transition Energies Database (Web, free access)   This X-ray transition table provides the energies and wavelengths for the K and L transitions connecting energy levels having principal quantum numbers n = 1, 2, 3, and 4. The elements covered include Z = 10, neon to Z = 100, fermium. There are two unique features of this data base: (1) a serious attempt to have all experimental values on a scale consistent with the International System of measurement (the SI) and (2) inclusion of accurate theoretical estimates for all transitions.

  18. Energy Scales in X-Ray Microcalorimeters

    NASA Technical Reports Server (NTRS)

    Tillotson, W. A.; Boyce, K. R.; Brown, G. V.; Cottam, J.; Figueroa, E.; Kelley, R. L.; Porter, F. S.; Stahle, C. K.

    2003-01-01

    Microcalorimeter pulse shape characteristics, such as pulse height, decay time and rise time, are dependent on the detector temperature and bias as well as the photon energy and flux. We examine the nature of the temperature dependency by illuminating the ASTRO-E2 X-ray Spectrometer (XRS) microcalorimeter array with X-rays generated by electron impact on a range of foil targets. The resulting pulses are collected for a range of detector temperatures. We observe and model the temperature dependence of the pulse shape characteristics by fitting the data with non-linear pulse models. Our aim is to determine a robust method for correcting the energy scale obtained in ground calibration for slight differences in the operating conditions while in orbit.

  19. ISMabs: A Comprehensive X-Ray Absorption Model for the Interstellar Medium

    NASA Astrophysics Data System (ADS)

    Gatuzz, E.; García, J.; Kallman, T. R.; Mendoza, C.; Gorczyca, T. W.

    2015-02-01

    We present an X-ray absorption model for the interstellar medium, to be referred to as ISMabs, that takes into account both neutral and ionized species of cosmically abundant elements, and includes the most accurate atomic data available. Using high-resolution spectra from eight X-ray binaries obtained with the Chandra High Energy Transmission Grating Spectrometer, we proceed to benchmark the atomic data in the model particularly in the neon K-edge region. Compared with previous photoabsorption models, which solely rely on neutral species, the inclusion of ions leads to improved spectral fits. Fit parameters comprise the column densities of abundant contributors that allow direct estimates of the ionization states. ISMabs is provided in the appropriate format to be implemented in widely used X-ray spectral fitting packages such as XSPEC, ISIS, and SHERPA.

  20. Oxygen, neon, and iron X-ray absorption in the local interstellar medium

    NASA Astrophysics Data System (ADS)

    Gatuzz, Efraín; García, Javier A.; Kallman, Timothy R.; Mendoza, Claudio

    2016-04-01

    Aims: We present a detailed study of X-ray absorption in the local interstellar medium by analyzing the X-ray spectra of 24 galactic sources obtained with the Chandra High Energy Transmission Grating Spectrometer and the XMM-Newton Reflection Grating Spectrometer. Methods: By modeling the continuum with a simple broken power-law and by implementing the new ISMabs X-ray absorption model, we have estimated the total H, O, Ne, and Fe column densities towards the observed sources. Results: We have determined the absorbing material distribution as a function of source distance and galactic latitude-longitude. Conclusions: Direct estimates of the fractions of neutrally, singly, and doubly ionized species of O, Ne, and Fe reveal the dominance of the cold component, thus indicating an overall low degree of ionization. Our results are expected to be sensitive to the model used to describe the continuum in all sources.

  1. ISMabs: A COMPREHENSIVE X-RAY ABSORPTION MODEL FOR THE INTERSTELLAR MEDIUM

    SciTech Connect

    Gatuzz, E.; Mendoza, C.; García, J.; Kallman, T. R.; Gorczyca, T. W. E-mail: claudio@ivic.gob.ve E-mail: timothy.r.kallman@nasa.gov

    2015-02-10

    We present an X-ray absorption model for the interstellar medium, to be referred to as ISMabs, that takes into account both neutral and ionized species of cosmically abundant elements, and includes the most accurate atomic data available. Using high-resolution spectra from eight X-ray binaries obtained with the Chandra High Energy Transmission Grating Spectrometer, we proceed to benchmark the atomic data in the model particularly in the neon K-edge region. Compared with previous photoabsorption models, which solely rely on neutral species, the inclusion of ions leads to improved spectral fits. Fit parameters comprise the column densities of abundant contributors that allow direct estimates of the ionization states. ISMabs is provided in the appropriate format to be implemented in widely used X-ray spectral fitting packages such as XSPEC, ISIS, and SHERPA.

  2. The high energy X-ray universe

    PubMed Central

    Giacconi, Riccardo

    2010-01-01

    Since its beginning in the early 1960s, the field of X-ray astronomy has exploded, experiencing a ten-billion-fold increase in sensitivity, which brought it on par with the most advanced facilities at all wavelengths. I will briefly describe the revolutionary first discoveries prior to the launch of the Chandra and XMM-Newton X-ray observatories, present some of the current achievements, and offer some thoughts about the future of this field. PMID:20404148

  3. The Einstein Observatory Extended Medium-Sensitivity Survey. I - X-ray data and analysis

    NASA Technical Reports Server (NTRS)

    Gioia, I. M.; Maccacaro, T.; Schild, R. E.; Wolter, A.; Stocke, J. T.

    1990-01-01

    This paper presents the results of the analysis of the X-ray data and the optical identification for the Einstein Observatory Extended Medium-Sensitivity Survey (EMSS). The survey consists of 835 serendipitous sources detected at or above 4 times the rms level in 1435 imaging proportional counter fields with centers located away from the Galactic plane. Their limiting sensitivities are about (5-300) x 10 to the -14th ergs/sq cm sec in the 0.3-3.5-keV energy band. A total area of 778 square deg of the high-Galactic-latitude sky has been covered. The data have been analyzed using the REV1 processing system, which takes into account the nonuniformities of the detector. The resulting EMSS catalog of X-ray sources is a flux-limited and homogeneous sample of astronomical objects that can be used for statistical studies.

  4. X-ray characterization by energy-resolved powder diffraction

    NASA Astrophysics Data System (ADS)

    Cheung, G.; Hooker, S. M.

    2016-08-01

    A method for single-shot, nondestructive characterization of broadband x-ray beams, based on energy-resolved powder diffraction, is described. Monte-Carlo simulations are used to simulate data for x-ray beams in the keV range with parameters similar to those generated by betatron oscillations in a laser-driven plasma accelerator. The retrieved x-ray spectra are found to be in excellent agreement with those of the input beams for realistic numbers of incident photons. It is demonstrated that the angular divergence of the x rays can be deduced from the deviation of the detected photons from the Debye-Scherrer rings which would be produced by a parallel beam. It is shown that the angular divergence can be measured as a function of the photon energy, yielding the angularly resolved spectrum of the input x-ray beam.

  5. Polarimeter for Low Energy X-ray Astrophysical Sources (PLEXAS)

    NASA Technical Reports Server (NTRS)

    Murray, Stephen S.; Pierce, David L. (Technical Monitor)

    2002-01-01

    The Polarimeter for Low Energy X-ray Astrophysical Sources (PLEXAS) is an astrophysics mission concept for measuring the polarization of X-ray sources at low energies below the C-K band (less than 277 eV). PLEXAS uses the concept of variations in the reflectivity of a multilayered X-ray telescope as a function of the orientation of an X-rays polarization vector with respect to the reflecting surface of the optic. By selecting an appropriate multilayer, and rotating the X-ray telescope while pointing to a source, there will be a modulation in the source intensity, as measured at the focus of the telescope, which is proportional to the degree of polarization in the source.

  6. EFFECT OF METALLICITY ON X-RAY EMISSION FROM THE WARM-HOT INTERGALACTIC MEDIUM

    SciTech Connect

    Ursino, E.; Galeazzi, M.; Roncarelli, M.

    2010-09-20

    Hydrodynamic simulations predict that a significant fraction of the gas in the current universe is in the form of high temperature, highly ionized plasma emitting and absorbing primarily in the soft X-ray and UV bands, dubbed the warm-hot intergalactic medium (WHIM). Its signature should be observable in redshifted emission and absorption lines from highly ionized elements. To determine the expected WHIM emission in the soft X-ray band we used the output of a large scale smoothed particle hydrodynamic simulation to generate images and spectra with angular resolution of 14'' and energy resolution of 1 eV. The current biggest limit of any hydrodynamic simulation in predicting the X-ray emission comes from metal diffusion. In our investigation, by using four different models for the WHIM metallicity we have found a strong dependence of the emission on the model used, with differences up to almost an order of magnitude. For each model, we have investigated the redshift distribution and angular scale of the emission, confirming that most photons come from redshift z < 1.2 and that the emission has a typical angular scale of less than a few arcminutes. We also compared our simulations with the few currently available observations and found that, within the variation of the metallicity models, our predictions are in good agreement with current constraints on the WHIM emission, and at this time the weak experimental constraints on the WHIM emission are not sufficient to exclude any of the models used.

  7. The X-Ray Zurich Environmental Study (X-ZENS). II. X-Ray Observations of the Diffuse Intragroup Medium in Galaxy Groups

    NASA Astrophysics Data System (ADS)

    Miniati, Francesco; Finoguenov, Alexis; Silverman, John D.; Carollo, Marcella; Cibinel, Anna; Lilly, Simon J.; Schawinski, Kevin

    2016-03-01

    We present the results of a pilot XMM-Newton and Chandra program aimed at studying the diffuse intragroup medium (IGM) of optically selected nearby groups from the Zurich ENvironmental Study (ZENS) catalog. The groups are in a narrow mass range about {10}13 {M}⊙ , a mass scale at which the interplay between the IGM and the group member galaxies is still largely unprobed. X-ray emission from the IGM is detected in the energy band 0.5-2 keV with flux ≤slant {10}-13 erg s-1 cm-2, which is one order of magnitude fainter than for typical ROSAT groups (RASS). For many groups, we set upper limits on the X-ray luminosity, indicating that the detections are likely probing the upper envelope of the X-ray emitting groups. We find that weighting the group halo mass by the fraction of the total stellar mass locked in the bulge galaxy components might reduce the bias of mass estimates based on the total optical luminosity with respect to the X-ray mass estimates, (consistent with Andreon, at larger mass scales). We measure a stellar mass fraction with a median value of about 1%, with a contribution from the most massive galaxies between 30% and 50%. Optical and X-ray data often give complementary answers concerning the dynamical state of the groups, and are essential for a complete picture of the group system. Extending this pilot program to a larger sample of groups is necessary to unveil any imprint of interaction between member galaxies and IGM in halo potentials of key importance for environmentally driven galactic evolution.

  8. Heating the intergalactic medium by X-rays from population III binaries in high-redshift galaxies

    SciTech Connect

    Xu, Hao; Norman, Michael L.; Ahn, Kyungjin; Wise, John H.; O'Shea, Brian W. E-mail: mlnorman@ucsd.edu E-mail: jwise@gatech.edu

    2014-08-20

    Due to their long mean free path, X-rays are expected to have an important impact on cosmic reionization by heating and ionizing the intergalactic medium (IGM) on large scales, especially after simulations have suggested that Population III (Pop III) stars may form in pairs at redshifts as high as 20-30. We use the Pop III distribution and evolution from a self-consistent cosmological radiation hydrodynamic simulation of the formation of the first galaxies and a simple Pop III X-ray binary model to estimate their X-ray output in a high-density region larger than 100 comoving (Mpc){sup 3}. We then combine three different methods—ray tracing, a one-zone model, and X-ray background modeling—to investigate the X-ray propagation, intensity distribution, and long-term effects on the IGM thermal and ionization state. The efficiency and morphology of photoheating and photoionization are dependent on the photon energies. The sub-kiloelectronvolt X-rays only impact the IGM near the sources, while the kiloelectronvolt photons contribute significantly to the X-ray background and heat and ionize the IGM smoothly. The X-rays just below 1 keV are most efficient in heating and ionizing the IGM. We find that the IGM might be heated to over 100 K by z = 10 and the high-density source region might reach 10{sup 4} K, limited by atomic hydrogen cooling. This may be important for predicting the 21 cm neutral hydrogen signals. On the other hand, the free electrons from X-ray ionizations are not enough to contribute significantly to the optical depth of the cosmic microwave background to the Thomson scattering.

  9. Development of a low debris x-ray backlighter source via laser irradiation of a cluster gas medium

    NASA Astrophysics Data System (ADS)

    Lowe, Hazel; Patankar, Siddarth; Giltrap, Samuel; Stuart, Nicholas; Robinson, Timothy; Gumbrell, Edward; Smith, Roland; Imperial College Team; AWE Collaboration

    2015-11-01

    X-ray backlighter sources, typically based on laser irradiated solid targets, are of great importance for radiography of transient plasmas produced in high power laser-target interactions. Here we report on the development of an atomic cluster gas based x-ray source and assess its viability for x-ray point projection imaging motivated by the debris free, high repetition rate nature of laser-cluster gas interactions. The dependence on cluster size and atomic number of the anisotropic radial x-ray distribution, 100 μm x-ray source size and multi-keV free electron temperatures produced by the interaction of a 1TW short pulse (500fs), high contrast laser system operating at 1054nm with high density Ar, Kr and Xe cluster gas media have been investigated. Previously, when propagated through a large (10mm) volume cluster gas medium at 1017 atoms/cc, >95% of the laser energy contained in a short pulse was absorbed launching a strong, radiative cylindrical blast wave. At 1019 atoms/cc, the absorption of the laser energy by the cluster gas medium was high (>85%). However, optical probing at 2 ω showed that the laser energy was predominantly absorbed at the edge of the gas volume where the energy absorbed per unit length rapidly changed over a scale length of 2mm launching a radiative, elliptical blast wave.

  10. Treatment of foods with high-energy X rays

    NASA Astrophysics Data System (ADS)

    Cleland, M. R.; Meissner, J.; Herer, A. S.; Beers, E. W.

    2001-07-01

    The treatment of foods with ionizing energy in the form of gamma rays, accelerated electrons, and X rays can produce beneficial effects, such as inhibiting the sprouting in potatoes, onions, and garlic, controlling insects in fruits, vegetables, and grains, inhibiting the growth of fungi, pasteurizing fresh meat, poultry, and seafood, and sterilizing spices and food additives. After many years of research, these processes have been approved by regulatory authorities in many countries and commercial applications have been increasing. High-energy X rays are especially useful for treating large packages of food. The most attractive features are product penetration, absorbed dose uniformity, high utilization efficiency and short processing time. The ability to energize the X-ray source only when needed enhances the safety and convenience of this technique. The availability of high-energy, high-power electron accelerators, which can be used as X-ray generators, makes it feasible to process large quantities of food economically. Several industrial accelerator facilities already have X-ray conversion equipment and several more will soon be built with product conveying systems designed to take advantage of the unique characteristics of high-energy X rays. These concepts will be reviewed briefly in this paper.

  11. Dosimetric properties of high energy current (HEC) detector in keV x-ray beams

    NASA Astrophysics Data System (ADS)

    Zygmanski, Piotr; Shrestha, Suman; Elshahat, Bassem; Karellas, Andrew; Sajo, Erno

    2015-04-01

    We introduce a new x-ray radiation detector. The detector employs high-energy current (HEC) formed by secondary electrons consisting predominantly of photoelectrons and Auger electrons, to directly convert x-ray energy to detector signal without externally applied power and without amplification. The HEC detector is a multilayer structure composed of thin conducting layers separated by dielectric layers with an overall thickness of less than a millimeter. It can be cut to any size and shape, formed into curvilinear surfaces, and thus can be designed for a variety of QA applications. We present basic dosimetric properties of the detector as function of x-ray energy, depth in the medium, area and aspect ratio of the detector, as well as other parameters. The prototype detectors show similar dosimetric properties to those of a thimble ionization chamber, which operates at high voltage. The initial results obtained for kilovoltage x-rays merit further research and development towards specific medical applications.

  12. Portable energy dispersive X-ray fluorescence and X-ray diffraction and radiography system for archaeometry

    NASA Astrophysics Data System (ADS)

    Mendoza Cuevas, Ariadna; Perez Gravie, Homero

    2011-03-01

    Starting on a laboratory developed portable X-ray fluorescence (PXRF) spectrometer; three different analytical results can be performed: analysis of chemical elements, analysis of major chemical crystalline phase and structural analysis, which represents a contribution to a new, low cost development of portable X-ray analyzer; since these results are respectively obtained with independent equipments for X-ray fluorescence, X-ray diffraction and radiography. Detection limits of PXRF were characterized using standard reference materials for ceramics, glass, bronze and bones, which are the main materials requiring quantitative analysis in art and archeological objects. A setup for simultaneous energy dispersive X-ray fluorescence and diffraction (ED (XRF-XRD)) in the reflection mode has been tested for in situ and non-destructive analysis according to the requirements of art objects inspection. The system uses a single low power X-ray tube and an X-ray energy dispersive detector to measure X-ray diffraction spectrum at a fixed angle. Application to the identification of jadeite-jade mineral in archeological objects by XRD is presented. A local high resolution radiography image obtained with the same low power X-ray tube allows for studies in painting and archeological bones.

  13. Deeply X-raying the high-energy sky

    NASA Astrophysics Data System (ADS)

    Bottacini, Eugenio; Ajello, Marco

    2016-05-01

    All-sky explorations by Fermi-LAT have revolutionized our view of the gamma-ray Universe. While its ongoing all-sky survey counts thousands of sources, essential issues related to the nature of unassociated sources call for more sensitive all-sky surveys at hard X-ray energies that allow for their identification. This latter energy band encodes the hard-tail of the thermal emission and the soft-tail of non-thermal emission thereby bridging the non-thermal and thermal emission mechanisms of gamma-ray sources. All-sky surveys at hard X-rays are best performed by current coded-mask telescopes Swift/BAT and INTEGRAL/IBIS. To boost the hard X-ray all-sky sensitivity, we have developed an ad hoc technique by combining photons from independent observations of BAT and IBIS. The resulting Swift-INTEGRAL X-ray (SIX) survey has an improved source-number density. This improvement is essential to enhance the positive hard X-ray - gamma-ray source matches. We present the results from the scientific link between the neighboring gamma-ray and hard X-ray bands in the context of galactic and extragalactic source classes of the second catalog Fermi Gamma-ray LAT (2FGL).

  14. Exotic X-ray Sources from Intermediate Energy Electron Beams

    SciTech Connect

    Chouffani, K.; Wells, D.; Harmon, F.; Jones, J.L.; Lancaster, G.

    2003-08-26

    High intensity x-ray beams are used in a wide variety of applications in solid-state physics, medicine, biology and material sciences. Synchrotron radiation (SR) is currently the primary, high-quality x-ray source that satisfies both brilliance and tunability. The high cost, large size and low x-ray energies of SR facilities, however, are serious limitations. Alternatively, 'novel' x-ray sources are now possible due to new small linear accelerator (LINAC) technology, such as improved beam emittance, low background, sub-Picosecond beam pulses, high beam stability and higher repetition rate. These sources all stem from processes that produce Radiation from relativistic Electron beams in (crystalline) Periodic Structures (REPS), or the periodic 'structure' of laser light. REPS x-ray sources are serious candidates for bright, compact, portable, monochromatic, and tunable x-ray sources with varying degrees of polarization and coherence. Despite the discovery and early research into these sources over the past 25 years, these sources are still in their infancy. Experimental and theoretical research are still urgently needed to answer fundamental questions about the practical and ultimate limits of their brightness, mono-chromaticity etc. We present experimental results and theoretical comparisons for three exotic REPS sources. These are Laser-Compton Scattering (LCS), Channeling Radiation (CR) and Parametric X-Radiation (PXR)

  15. Focal construct geometry for high intensity energy dispersive x-ray diffraction based on x-ray capillary optics.

    PubMed

    Li, Fangzuo; Liu, Zhiguo; Sun, Tianxi; Jiang, Bowen; Zhu, Yu

    2016-03-14

    We presented a focal construct geometry (FCG) method for high intensity energy dispersive X-ray diffraction by utilizing a home-made ellipsoidal single-bounce capillary (ESBC) and a polycapillary parallel X-ray lens (PPXRL). The ESBC was employed to focus the X-rays from a conventional laboratory source into a small focal spot and to produce an annular X-ray beam in the far-field. Additionally, diffracted polychromatic X-rays were confocally collected by the PPXRL attached to a stationary energy-resolved detector. Our FCG method based on ESBC and PPXRL had achieved relatively high intensity diffraction peaks and effectively narrowed the diffraction peak width which was helpful in improving the potential d-spacing resolution for material phase analysis.

  16. High-resolution X-ray spectroscopy of four active galaxies - Probing the intercloud medium

    NASA Astrophysics Data System (ADS)

    Lum, Kenneth S. K.; Canizares, Claude R.; Markert, Thomas H.; Arnaud, Keith A.

    1990-07-01

    The focal plane crystal spectrometer (FPCS) on the Einstein Observatory has been used to perform a high-resolution spectroscopic search for oxygen X-ray line emission from four active galaxies: Fairall 9, Mrk 421, Mrk 501, and PKS 0548 - 322. Specifically, O VIII Ly-alpha and Ly-beta, whose unredshifted energies are 653 and 775 eV, respectively, were sought. No narrow-line emission was detected within the energy bands searched. Upper limits are calculated on the line flux from these sources of 30 eV equivalent width and use a photoionization model to place corresponding upper limits on the densities of diffuse gas surrounding the active nuclei. The upper limits on gas density range from about 0.02-50/cu cm and probe various radial distances from the central source. This is the first time high-resolution X-ray spectroscopy has been used to place constraints on the intercloud medium in active galaxies.

  17. Single atom identification by energy dispersive x-ray spectroscopy

    SciTech Connect

    Lovejoy, T. C.; Dellby, N.; Krivanek, O. L.; Ramasse, Q. M.; Falke, M.; Kaeppel, A.; Terborg, R.; Zan, R.

    2012-04-09

    Using aberration-corrected scanning transmission electron microscope and energy dispersive x-ray spectroscopy, single, isolated impurity atoms of silicon and platinum in monolayer and multilayer graphene are identified. Simultaneously acquired electron energy loss spectra confirm the elemental identification. Contamination difficulties are overcome by employing near-UHV sample conditions. Signal intensities agree within a factor of two with standardless estimates.

  18. High resolution, low energy avalanche photodiode X-ray detectors

    NASA Technical Reports Server (NTRS)

    Farrell, R.; Vanderpuye, K.; Entine, G.; Squillante, M. R.

    1991-01-01

    Silicon avalanche photodiodes have been fabricated, and their performance as X-ray detectors has been measured. Photon sensitivity and energy resolution were measured as a function of size and operating parameters. Noise thresholds as low as 212 eV were obtained at room temperature, and backscatter X-ray fluorescence data were obtained for aluminum and other light elements. It is concluded that the results with the X-ray detector are extremely encouraging, and the performance is challenging the best available proportional counters. While not at the performance level of either cryogenic silicon or HgI2, these device operate at room temperature and can be reproduced in large numbers and with much larger areas than typically achieved with HgI2. In addition, they are rugged and appear to be indefinitely stable.

  19. High energy transmission annular beam X-ray diffraction.

    PubMed

    Dicken, Anthony; Shevchuk, Alex; Rogers, Keith; Godber, Simon; Evans, Paul

    2015-03-01

    We demonstrate material phase retrieval by linearly translating extended polycrystalline samples along the symmetry axis of an annular beam of high-energy X-rays. A series of pseudo-monochromatic diffraction images are recorded from the dark region encompassed by the beam. We measure Bragg maxima from different annular gauge volumes in the form of bright spots in the X-ray diffraction intensity. We present the experiment data from three materials with different crystallographic structural properties i.e. near ideal, large grain size and preferred orientation. This technique shows great promise for analytical inspection tasks requiring highly penetrating radiation such as security screening, medicine and non-destructive testing.

  20. Systematic survey of the dose enhancement in tissue-equivalent materials facing medium- and high-Z backscatterers exposed to X-rays with energies from 5 to 250 keV.

    PubMed

    Seidenbusch, M; Harder, D; Regulla, D

    2014-05-01

    The present study has been inspired by the results of earlier dose measurements in tissue-equivalent materials adjacent to thin foils of aluminum, copper, tin, gold, and lead. Large dose enhancements have been observed in low-Z materials near the interface when this ensemble was irradiated with X-rays of qualities known from diagnostic radiology. The excess doses have been attributed to photo-, Compton, and Auger electrons released from the metal surfaces. Correspondingly, high enhancements of biological effects have been observed in single cell layers arranged close to gold surfaces. The objective of the present work is to systematically survey, by calculation, the values of the dose enhancement in low-Z media facing backscattering materials with a variety of atomic numbers and over a large range of photon energies. Further parameters to be varied are the distance of the point of interest from the interface and the kind of the low-Z material. The voluminous calculations have been performed using the PHOTCOEF algorithm, a proven set of interpolation functions fitted to long-established Monte Carlo results, for primary photon energies between 5 and 250 keV and for atomic numbers varying over the periodic system up to Z = 100. The calculated results correlate well with our previous experimental results. It is shown that the values of the dose enhancement (a) vary strongly in dependence upon Z and photon energy; (b) have maxima in the energy region from 40 to 60 keV, determined by the K and L edges of the backscattering materials; and (c) are valued up to about 130 for "International Commission on Radiological Protection (ICRP) soft tissue" (soft tissue composition recommended by the ICRP) as the adjacent low-Z material. Maximum dose enhancement associated with the L edge occurs for materials with atomic numbers between 50 and 60, e.g., barium (Z = 56) and iodine (Z = 53). Such materials typically serve as contrast media in medical X-ray diagnostics. The gradual

  1. X-ray and Sunyaev-Zel'Dovich properties of the warm-hot intergalactic medium

    SciTech Connect

    Ursino, E.; Galeazzi, M.; Huffenberger, K.

    2014-07-01

    We use numerical simulations to predict the soft X-ray ([0.4-0.6] keV) and Sunyaev-Zel'dovich (SZ) signal (at 150 GHz) from a large-scale structure in the universe and then compute two-point statistics to study the spatial distribution and time evolution of the signals. The average X-ray signal predicted for the warm-hot intergalactic medium (WHIM) is in good agreement with observational constraints that set it at about 10% of the total diffuse X-ray background. The characteristic angle computed with the autocorrelation function is of the order of some arcminutes and becomes smaller at higher redshift. The power spectrum peak of the SZ due to the WHIM is at l ∼ 10,000 and has an amplitude of ∼0.2 μK{sup 2}, about one order of magnitude below the signal measured with telescopes like Planck, Atacama Cosmology Telescope, and South Pole Telescope. Even if the high-redshift WHIM signal is too weak to be detected using X-rays only, the small-scale correlation between X-ray and SZ maps is dominated by the high-redshift WHIM. This makes the analysis of the SZ signal in support of X-rays a promising tool to study the early time WHIM.

  2. A newly developed multilayer semiconductor x-ray detector for the observations of wide energy-range x rays

    NASA Astrophysics Data System (ADS)

    Hirata, M.; Cho, T.; Kohagura, J.; Yatsu, K.; Tamano, T.; Miyoshi, S.; Kondoh, T.; Saitoh, Y.; Sato, K.; Miyahara, S.; Hirano, K.; Maezawa, H.

    1995-02-01

    For the purpose of the developments of wide-energy-range-sensitive x-ray detectors, we have designed and fabricated a new-type multilayer semiconductor x-ray detector. This new-type detector has been characterized using synchrotron radiation from a 2.5-GeV positron storage ring at the Photon Factory of the National Laboratory for High Energy Physics (KEK). This new detector is essentially composed of four layers of commercially available photodiodes. Each photodiode is made from a 300-μm thick, and a 10×10-mm square-shaped wafer. For the common affiliation of these individual photodiodes, the quantum efficiency normalized by the photon energy η/E begins to decrease at 8 keV, and then η/E decreases down to 26% at 20 keV. On the other hand, for our newly designed detector a flat response even in the 10-20-keV energy regime (beam line 15C at the Photon Factory) is observed, and even at 100 keV η/E<30% is still anticipated. This new x-ray detector has various advantages: (i) A compact, and (ii) outgas-free detector for a high-vacuum use, along with (iii) a high degree of immunity to ambient magnetic fields. Furthermore, (iv) the combination of the x-ray signal outputs from each detector layer provides information on the x-ray emitting electron energies. These properties are quite suitable for the use of the fusion-oriented plasma x-ray diagnostics under intense-magnetic field and high-vacuum conditions so as to interpret wide-band x-ray emitting electron-velocity distribution functions from the x-ray data.

  3. X-ray amplifier energy deposition scaling with channeled propagation

    SciTech Connect

    Boyer, K.; Luk, T.S.; McPherson, A.

    1991-12-31

    The spatial control of the energy deposited for excitation of an x-ray amplifier plays an important role in the fundamental scaling relationship between the required energy, the gain and the wavelength. New results concerning the ability to establish confined modes of propagation of sort pulse radiation of sufficiently high intensity in plasmas lead to a sharply reduced need for the total energy deposited, since the concentration of deposited power can be very efficiently organized.

  4. High-energy X-ray spectra of five sources.

    NASA Technical Reports Server (NTRS)

    Ricker, G. R.; Mcclintock, J. E.; Gerassimenko, M.; Lewin , W. H. G.

    1973-01-01

    On October 15-16, 1970, we carried out balloon X-ray observations from Australia at energies above 15 keV. We present the high-energy X-ray spectra of three sources discovered by us, GX 301-2, GX 304-1, and GX 1 + 4. The data suggest that these high-energy sources correspond to the sources 2U 1223-62, 2U 1258-61, and 2U 1728-24 respectively. We also present the spectra for two additional sources, GX 5-1 (2U 1757-25) and GX 3 + 1 (2U 1744-26). The average intensity of the highly variable source GX 301-2 was observed to be as great as Tau X-1 in the energy range 15-50 keV.

  5. Flywheel energy storage for x-ray machines.

    PubMed

    Siedband, M P; Showers, D K

    1984-01-01

    X-ray image quality for stop-motion exposures is greatly affected by the system power capability. High power levels are required for adequate resolution, which often precludes the use of mobile x-ray systems for stop-motion exposures. Currently available mobile systems use (1) 90-V nickel-cadmium batteries capable of 120 A, (2) a power line of 220 V ac, 60 Hz capable of about 100 A, or (3) a capacitor discharge unit using 1.0-microF capacitors and limited to 17-mAs equivalent output (compared to three-phase systems at 100 kVp). In each case, instantaneous power is usually limited to 10 kW. An alternative means which now appears to be a practical power source for mobile x-ray systems is the flywheel energy storage system. A 5-kg flywheel has been constructed which runs at 10 000 rpm and stores 25 000 J while drawing only a few hundred watts to bring the system up to speed. When coupled to an aircraft alternator, pulsed power levels of 25 kW have been achieved. The aircraft alternator also has the advantage of high-frequency output which has permitted the use of smaller high-voltage transformers. This system permits the generation of powerful x rays using low-power sources, such as single automobile batteries, common 115-V outlets, or electrical sources of poor regulation such as found in Third World countries.

  6. Phase contrast imaging with coherent high energy X-rays

    SciTech Connect

    Snigireva, I.

    1997-02-01

    X-ray imaging concern high energy domain (>6 keV) like a contact radiography, projection microscopy and tomography is used for many years to discern the features of the internal structure non destructively in material science, medicine and biology. In so doing the main contrast formation is absorption that makes some limitations for imaging of the light density materials and what is more the resolution of these techniques is not better than 10-100 {mu}m. It was turned out that there is now way in which to overcome 1{mu}m or even sub-{mu}m resolution limit except phase contrast imaging. It is well known in optics that the phase contrast is realised when interference between reference wave front and transmitted through the sample take place. Examples of this imaging are: phase contrast microscopy suggested by Zernike and Gabor (in-line) holography. Both of this techniques: phase contrast x-ray microscopy and holography are successfully progressing now in soft x-ray region. For imaging in the hard X-rays to enhance the contrast and to be able to resolve phase variations across the beam the high degree of the time and more importantly spatial coherence is needed. Because of this it was reasonable that the perfect crystal optics was involved like Bonse-Hart interferometry, double-crystal and even triple-crystal set-up using Laue and Bragg geometry with asymmetrically cut crystals.

  7. High energy, high resolution X-ray optics

    NASA Technical Reports Server (NTRS)

    Weisskopf, Martin C.; Joy, Marshall; Kahn, Steven

    1990-01-01

    The scientific goals of X-ray astronomy are considered to evaluate the relative advantages of using classical Wolter-1 optics or using a different approach. The portion of the X-ray band over 10 keV is unexploited in the present X-ray optics technology, and focussing in this portion of the band is crucial because nonfocussed experiments are background limited. The basic design of 'hard' X-ray optics is described theoretically emphasizing the very small angles of incidence in the grazing-incidence optics. Optimization of the signal-to-noise ratio is found to occur at a finite angular resolution. In real applications, the effective area reduced by the efficiency of the two reflections is 80 percent at energies up to 40 keV, and the quality of the reflecting surface can be monitored to minimize scattering. Focussing optics are found to offer improvements in signal-to-noise as well as more effective scientific return because microelectronic focal-plane technology is employed.

  8. Bone age assessment by dual-energy X-ray absorptiometry in children: an alternative for X-ray?

    PubMed Central

    Heppe, D H M; Taal, H R; Ernst, G D S; Van Den Akker, E L T; Lequin, M M H; Hokken-Koelega, A C S; Geelhoed, J J M; Jaddoe, V W V

    2012-01-01

    Objective The aim of the study was to validate dual-energy X-ray absorptiometry (DXA) as a method to assess bone age in children. Methods Paired dual-energy X-ray absorptiometry (DXA) scans and X-rays of the left hand were performed in 95 children who attended the paediatric endocrinology outpatient clinic of University Hospital Rotterdam, the Netherlands. We compared bone age assessments by DXA scan with those performed by X-ray. Bone age assessment was performed by two blinded observers according to the reference method of Greulich and Pyle. Intra-observer and interobserver reproducibility were investigated using the intraclass correlation coefficient (ICC), and agreement was tested using Bland and Altman plots. Results The intra-observer ICCs for both observers were 0.997 and 0.991 for X-ray and 0.993 and 0.987 for DXA assessments. The interobserver ICC was 0.993 and 0.991 for X-ray and DXA assessments, respectively. The mean difference between bone age assessed by X-ray and DXA was 0.11 years. The limits of agreement ranged from −0.82 to 1.05 years, which means that 95% of all differences between the methods were covered by this range. Conclusions Results of bone age assessment by DXA scan are similar to those obtained by X-ray. The DXA method seems to be an alternative for assessing bone age in a paediatric hospital-based population. PMID:21586503

  9. Hot bubbles in a magnetic interstellar medium - Another look at the soft X-ray background

    NASA Technical Reports Server (NTRS)

    Edgar, Richard J.; Cox, Donald P.

    1993-01-01

    An attempt is made to understand the origin and properties of an isolated local bubble of hot gas using models of explosive events in a magnetic interstellar medium which mimic the local bubble in terms of the C band X-ray surface brightness and radius. The residual bubble of hot gas reaches a maximum size with an internal pressure below ambient, and then shrinks to smaller volume and a pressure nearly equal to ambient. The X-ray brightness reaches its minimum at the time of maximum radius and rises thereafter. It is found that the bubble growth must have been confined by a probably unacceptably large external pressure in order for the hot gas in the maximally extended cavity to radiate at a rate like that observed in the soft X-ray background.

  10. Phase-resolved X-ray spectroscopy and spectral energy distribution of the X-ray soft polar RS Caeli

    NASA Astrophysics Data System (ADS)

    Traulsen, I.; Reinsch, K.; Schwope, A. D.; Schwarz, R.; Walter, F. M.; Burwitz, V.

    2014-02-01

    Context. RS Cae is the third target in our series of XMM-Newton observations of soft X-ray-dominated polars. Aims: Our observational campaign aims to better understand and describe the multiwavelength data, the physical properties of the system components, and the short- and long-term behavior of the component fluxes in RS Cae. Methods: We employ stellar atmosphere, stratified accretion-column, and widely used X-ray spectral models. We fit the XMM-Newton spectra, model the multiband light curves, and opt for a mostly consistent description of the spectral energy distribution. Results: Our XMM-Newton data of RS Cae are clearly dominated by soft X-ray emission. The X-ray light curves are shaped by emission from the main accretion region, which is visible over the whole orbital cycle, interrupted only by a stream eclipse. The optical light curves are formed by cyclotron and stream emission. The XMM-Newton X-ray spectra comprise a black-body-like and a plasma component at mean temperatures of 36 eV and 7 keV. The spectral fits give evidence of a partially absorbing and a reflection component. Multitemperature models, covering a broader temperature range in the X-ray emitting accretion regions, reproduce the spectra appropriately well. Including archival data, we describe the spectral energy distribution with a combination of models based on a consistent set of parameters and derive a lower limit estimate of the distance d ≳ 750 pc. Conclusions: The high bolometric soft-to-hard flux ratios and short-term variability of the (X-ray) light curves are characteristic of inhomogeneous accretion. RS Cae clearly belongs in the group of polars that show a very strong soft X-ray flux compared to their hard X-ray flux. The different black-body fluxes and similar hard X-ray and optical fluxes during the XMM-Newton and ROSAT observations show that soft and hard X-ray emission are not directly correlated. Based on observations obtained with XMM-Newton, an ESA science mission with

  11. Energy Feedback from X-ray Binaries in the Early Universe

    NASA Technical Reports Server (NTRS)

    Fragos, T.; Lehmer, B..; Naoz, S.; Zezas, A.; Basu-Zych, A.

    2013-01-01

    X-ray photons, because of their long mean-free paths, can easily escape the galactic environments where they are produced, and interact at long distances with the intergalactic medium, potentially having a significant contribution to the heating and reionization of the early universe. The two most important sources of X-ray photons in the universe are active galactic nuclei (AGNs) and X-ray binaries (XRBs). In this Letter we use results from detailed, large scale population synthesis simulations to study the energy feedback of XRBs, from the first galaxies (z (redshift) approximately equal to 20) until today.We estimate that X-ray emission from XRBs dominates over AGN at z (redshift) greater than or approximately equal to 6-8. The shape of the spectral energy distribution of the emission from XRBs shows little change with redshift, in contrast to its normalization which evolves by approximately 4 orders of magnitude, primarily due to the evolution of the cosmic star-formation rate. However, the metallicity and the mean stellar age of a given XRB population affect significantly its X-ray output. Specifically, the X-ray luminosity from high-mass XRBs per unit of star-formation rate varies an order of magnitude going from solar metallicity to less than 10% solar, and the X-ray luminosity from low-mass XRBs per unit of stellar mass peaks at an age of approximately 300 Myr (million years) and then decreases gradually at later times, showing little variation for mean stellar ages 3 Gyr (Giga years, or billion years). Finally, we provide analytical and tabulated prescriptions for the energy output of XRBs, that can be directly incorporated in cosmological simulations.

  12. Energy Feedback from X-Ray Binaries in the Early Universe

    NASA Astrophysics Data System (ADS)

    Fragos, T.; Lehmer, B. D.; Naoz, S.; Zezas, A.; Basu-Zych, A.

    2013-10-01

    X-ray photons, because of their long mean-free paths, can easily escape the galactic environments where they are produced, and interact at long distances with the intergalactic medium, potentially having a significant contribution to the heating and reionization of the early universe. The two most important sources of X-ray photons in the universe are active galactic nuclei (AGNs) and X-ray binaries (XRBs). In this Letter we use results from detailed, large scale population synthesis simulations to study the energy feedback of XRBs, from the first galaxies (z ~ 20) until today. We estimate that X-ray emission from XRBs dominates over AGN at z >~ 6-8. The shape of the spectral energy distribution of the emission from XRBs shows little change with redshift, in contrast to its normalization which evolves by ~4 orders of magnitude, primarily due to the evolution of the cosmic star-formation rate. However, the metallicity and the mean stellar age of a given XRB population affect significantly its X-ray output. Specifically, the X-ray luminosity from high-mass XRBs per unit of star-formation rate varies an order of magnitude going from solar metallicity to less than 10% solar, and the X-ray luminosity from low-mass XRBs per unit of stellar mass peaks at an age of ~300 Myr and then decreases gradually at later times, showing little variation for mean stellar ages >~ 3 Gyr. Finally, we provide analytical and tabulated prescriptions for the energy output of XRBs, that can be directly incorporated in cosmological simulations.

  13. X-ray energy optimisation in computed microtomography.

    PubMed

    Spanne, P

    1989-06-01

    Expressions describing the absorbed dose and the number of incident photons necessary for the detection of a contrasting detail in x-ray transmission CT imaging of a circular phantom are derived as functions of the linear attenuation coefficients of the materials comprising the object and the detail. A shell of a different material can be included to allow simulation of CT imaging of the skulls of small laboratory animals. The equations are used to estimate the optimum photon energy in x-ray transmission computed microtomography. The optimum energy depends on whether the number of incident photons or the absorbed dose at a point in the object is minimised. For a water object of 300 mm diameter the two optimisation criteria yield optimum photon energies differing by an order of magnitude.

  14. Spectacular X-ray Jet Points Toward Cosmic Energy Booster

    NASA Astrophysics Data System (ADS)

    2000-06-01

    NASA's Chandra X-ray Observatory has revealed a spectacular luminous spike of X rays that emanates from the vicinity of a giant black hole in the center of the radio galaxy Pictor A. The spike, or jet, is due to a beam of particles that streaks across hundreds of thousands of light years of intergalactic space toward a brilliant X-ray hot spot that marks its end point. Pictor A Image Press Image and Caption The hot spot is at least 800 thousand light years (8 times the diameter of our Milky Way galaxy) away from where the jet originates. It is thought to represent the advancing head of the jet, which brightens conspicuously where it plows into the tenuous gas of intergalactic space. The jet, powered by the giant black hole, originates from a region of space no bigger than the solar system. "Both the brightness and the spectrum of the X rays are very different from what theory predicts," Professor Andrew Wilson reported today at the 196th national meeting of the American Astronomical Society in Rochester, New York. Wilson, of the University of Maryland, College Park, along with Dr. Patrick Shopbell and Dr. Andrew Young, also of the University of Maryland, are submitting an article on this research to the Astrophysical Journal. "The Chandra observations are telling us that something out there is producing many more high-energy particles than we expected," said Wilson. One possible explanation for the X rays is that shock waves along the side and head of the X-ray jet are accelerating electrons and possibly protons to speeds close to that of light. In the process the electrons are boosted to energies as high as 100 million times their own rest mass energy. These electrons lose their energy rapidly as they produce X rays, so this could be the first direct evidence of this process so far outside a galaxy. The hot spot has been seen with optical and radio telescopes. Radio telescopes have also observed a faint jet. Jets are thought to be produced by the extreme

  15. X-Ray Constraints on the Warm-Hot Intergalactic Medium

    NASA Technical Reports Server (NTRS)

    Kuntz, K. D.; Snowden, S. I.; Mushotzky, R. F.; White, Nicholas E. (Technical Monitor)

    2000-01-01

    Three observational constraints can be placed on a warm-hot intergalactic medium (WHIM) using ROSAT Position Sensitive Proportional Counter (PSPC) pointed and survey data, the emission strength, the energy spectrum, and the fluctuation spectrum. The upper limit to the emission strength of the WHIM is 7.5 +/- 1.0 keV/(s*sq cm*sr*keV) in the 3/4 keV band, an unknown portion of which value may be due to our own Galactic halo. The spectral stape of the WHIM emission can be described as thermal emission with logT = 6.42, although the true spectrum is more likely to come from a range of temperatures. The values of emission strength and spectral shape are in reasonable agreement with hydrodynamical cosmological models. The autocorrelation function in the 0.44 keV < E < 1.21 keV band range, w(theta), for the extragalactic soft X-ray background (SXRB) which includes both the WHIM and contributions due to point sources, is approx. < 0.002 for 10 min < 0 < 20 min in the 3/4 keV band. This value is lower than the Croft et al. (2000) cosmological model by a factor of approx. 5, but is still not inconsistent with cosmological models. It is also found that the normalization of the extragalactic power law component of the soft X-ray background spectrum must be 9.5 +/- 0.9 keV/(s*sq cm*sr*keV) to be consistent with the ROSAT All-Sky Survey.

  16. Bursting SN 1996cr's bubble: hydrodynamic and X-ray modelling of its circumstellar medium

    NASA Astrophysics Data System (ADS)

    Dwarkadas, V. V.; Dewey, D.; Bauer, F.

    2010-09-01

    SN1996cr is one of the five closest supernovae (SNe) to explode in the past 30 yr. Due to its fortuitous location in the Circinus galaxy at ~3.7 Mpc, there is a wealth of recently acquired and serendipitous archival data available to piece together its evolution over the past decade, including a recent 485-ks Chandra high-energy transmission grating spectrum. In order to interpret these data, we have explored hydrodynamic simulations, followed by computations of simulated spectra and light curves under non-equilibrium ionization conditions, and directly compared them to the observations. Our simulated spectra manage to fit both the X-ray continuum and lines at four epochs satisfactorily, while our computed light curves are in good agreement with additional flux-monitoring data sets. These calculations allow us to infer the nature and structure of the circumstellar medium (CSM), the evolution of the SN shock wave, and the abundances of the ejecta and surrounding medium. The data imply that SN 1996cr exploded in a low-density medium before interacting with a dense shell of material about 0.03 pc away from the progenitor star. We speculate that the shell could be due to the interaction of a blue supergiant or Wolf-Rayet wind with a previously existing red supergiant (RSG) wind. The shock wave has now exited the shell and is expanding in the medium exterior to it, possibly the undisturbed continuation of the dense RSG wind. The narrow lines that earned SN 1996cr its IIn designation possibly arise from dense, shocked clumps in the CSM. Although the possibility for a luminous blue variable progenitor for this Type IIn SN cannot be completely excluded, it is inconsistent with much of the data. These calculations allow us to probe the stellar mass-loss in the very last phases (<104 yr) of a massive star's life (>106 yr), and provide another means to deducing the progenitor of the SN.

  17. Refractive optical elements and optical system for high energy x-ray microscopy

    SciTech Connect

    Simon, M.; Altapova, V.; Baumbach, T.; Kluge, M.; Last, A.; Marschall, F.; Mohr, J.; Nazmov, V.; Vogt, H.

    2012-05-17

    In material science, X-ray radiation with photon energies above 25 keV is used because of its penetration into high density materials. Research of the inner structure of novel materials, such as electrodes in high power batteries for engines, require X-ray microscopes operating in the hard X-ray energy range. A flexible X-ray microscope for hard X-rays with photon energies higher than 25 keV will be realized at the synchrotron source ANKA in Karlsruhe, Germany. The device will use refractive X-ray lenses as condenser as well as objective lenses.

  18. Studies of dark energy with X-ray observatories.

    PubMed

    Vikhlinin, Alexey

    2010-04-20

    I review the contribution of Chandra X-ray Observatory to studies of dark energy. There are two broad classes of observable effects of dark energy: evolution of the expansion rate of the Universe, and slow down in the rate of growth of cosmic structures. Chandra has detected and measured both of these effects through observations of galaxy clusters. A combination of the Chandra results with other cosmological datasets leads to 5% constraints on the dark energy equation-of-state parameter, and limits possible deviations of gravity on large scales from general relativity. PMID:20404207

  19. Studies of dark energy with x-ray observatories

    PubMed Central

    Vikhlinin, Alexey

    2010-01-01

    I review the contribution of Chandra X-ray Observatory to studies of dark energy. There are two broad classes of observable effects of dark energy: evolution of the expansion rate of the Universe, and slow down in the rate of growth of cosmic structures. Chandra has detected and measured both of these effects through observations of galaxy clusters. A combination of the Chandra results with other cosmological datasets leads to 5% constraints on the dark energy equation-of-state parameter, and limits possible deviations of gravity on large scales from general relativity. PMID:20404207

  20. Investigating Microphysics of Intracluster Medium with Advanced Hydrodynamic Simulations and X-Ray Observations

    NASA Astrophysics Data System (ADS)

    Markevitch, Maxim

    Clusters of galaxies are the largest virialized mass concentrations in the Universe, and have long been recognized as sensitive cosmological probes. It is becoming increasingly clear that to realize their full potential for cosmology, we need to drastically reduce uncertainties in the cluster mass estimates and their relation to various cluster observables that arise from our lack of knowledge of the microphysics of the intracluster medium (ICM). Such ICM properties as thermal conductivity, viscosity, strength and structure of the magnetic fields, the energy in the cosmic ray components and electron-ion equilibration rates are very uncertain. Each of these can have a significant impact on the cluster thermal balance and the quantities that we observe in the X-ray, SZ, and radio bands. Theoretical estimates of thermal conductivity and viscosity are particularly uncertain -- by orders of magnitude. The heat can be conducted only along the magnetic field lines, but by some estimates, even along the lines it can be effectively suppressed by small- scale field fluctuations. Even less understood is the physical nature and the magnitude of viscosity, which bears directly on the ICM heating and mixing processes and the damping of turbulence. We have identified a method to constrain these quantities by contrasting high-quality X-ray observations of merging clusters with our high-resolution magnetohydrodynamic simulations that would follow the evolution of the magnetic field and include various levels of anisotropic conduction and viscosity. Thermal conduction can best be constrained by comparing X-ray temperature maps for several well-observed merging clusters with the maps for their simulated analogs. The conduction at interesting levels is expected to erase any small-scale temperature nonuniformities on timescales comparable to that of the merger. Currently, the most readily observable effect of viscosity is the suppression of instabilities in the cluster `cold fronts

  1. On the detectability of CO molecules in the interstellar medium via X-ray spectroscopy

    NASA Astrophysics Data System (ADS)

    Joachimi, Katerine; Gatuzz, Efraín; García, Javier A.; Kallman, Timothy R.

    2016-09-01

    We present a study of the detectability of CO molecules in the Galactic interstellar medium using high-resolution X-ray spectra obtained with the XMM-Newton Reflection Grating Spectrometer. We analysed 10 bright low mass X-ray binaries (LMXBs) to study the CO contribution in their line of sights. A total of 25 observations were fitted with the ISMabs X-ray absorption model which includes photoabsorption cross-sections for O I, O II, O III and CO. We performed a Monte Carlo (MC) simulation analysis of the goodness of fit in order to estimate the significance of the CO detection. We determine that the statistical analysis prevents a significant detection of CO molecular X-ray absorption features, except for the lines of sight towards XTE J1718-330 and 4U 1636-53. In the case of XTE J1817-330, this is the first report of the presence of CO along its line of sight. Our results reinforce the conclusion that molecules have a minor contribution to the absorption features in the O K-edge spectral region. We estimate a CO column density lower limit to perform a significant detection with XMM-Newton of N(CO) > 6 × 1016 cm-2 for typical exposure times.

  2. X-ray scatter correction for dual-energy x-ray absorptiometry: compensation of patient's lean/fat composition

    NASA Astrophysics Data System (ADS)

    Dinten, Jean-Marc; Darboux, Michel; Bordy, Thomas; Robert-Coutant, Christine; Gonon, Georges

    2004-05-01

    At CEA-LETI, a DEXA approach for systems using a digital 2D radiographic detector has been developed. It relies on an original X-rays scatter management method, based on a combined use of an analytical model and of scatter calibration data acquired through different thicknesses of Lucite slabs. Since Lucite X-rays interaction properties are equivalent to fat, the approach leads to a scatter flux map representative of a 100% fat region. However, patients" soft tissues are composed of lean and fat. Therefore, the obtained scatter map has to be refined in order to take into account the various fat ratios that can present patients. This refinement consists in establishing a formula relating the fat ratio to the thicknesses of Low and High Energy Lucite slabs leading to same signal level. This proportion is then used to compute, on the basis of X-rays/matter interaction equations, correction factors to apply to Lucite equivalent X-rays scatter map. Influence of fat ratio correction has been evaluated, on a digital 2D bone densitometer, with phantoms composed of a PVC step (simulating bone) and different Lucite/water thicknesses as well as on patients. The results show that our X-rays scatter determination approach can take into account variations of body composition.

  3. High Resolution Spectroscopy of X-ray Quasars: Searching for the X-ray Absorption from the Warm-Hot Intergalactic Medium

    NASA Technical Reports Server (NTRS)

    Fang, Taotao; Canizares, Claude R.; Marshall, Herman L.

    2004-01-01

    We present a survey of six low to moderate redshift quasars with Chandra and XMM-Newton. The primary goal is to search for the narrow X-ray absorption lines produced by highly ionized metals in the Warm-Hot Intergalactic Medium. All the X-ray spectra can be well fitted by a power law with neutral hydrogen absorption. Only one feature is detected at above 3-sigma level in all the spectra, which is consistent with statistic fluctuation. We discuss the implications in our understanding of the baryon content of the universe. We also discuss the implication of the non-detection of the local (z approx. 0) X-ray absorption.

  4. High resolution, multiple-energy linear sweep detector for x-ray imaging

    DOEpatents

    Perez-Mendez, Victor; Goodman, Claude A.

    1996-01-01

    Apparatus for generating plural electrical signals in a single scan in response to incident X-rays received from an object. Each electrical signal represents an image of the object at a different range of energies of the incident X-rays. The apparatus comprises a first X-ray detector, a second X-ray detector stacked upstream of the first X-ray detector, and an X-ray absorber stacked upstream of the first X-ray detector. The X-ray absorber provides an energy-dependent absorption of the incident X-rays before they are incident at the first X-ray detector, but provides no absorption of the incident X-rays before they are incident at the second X-ray detector. The first X-ray detector includes a linear array of first pixels, each of which produces an electrical output in response to the incident X-rays in a first range of energies. The first X-ray detector also includes a circuit that generates a first electrical signal in response to the electrical output of each of the first pixels. The second X-ray detector includes a linear array of second pixels, each of which produces an electrical output in response to the incident X-rays in a second range of energies, broader than the first range of energies. The second X-ray detector also includes a circuit that generates a second electrical signal in response to the electrical output of each of the second pixels.

  5. High resolution, multiple-energy linear sweep detector for x-ray imaging

    DOEpatents

    Perez-Mendez, V.; Goodman, C.A.

    1996-08-20

    Apparatus is disclosed for generating plural electrical signals in a single scan in response to incident X-rays received from an object. Each electrical signal represents an image of the object at a different range of energies of the incident X-rays. The apparatus comprises a first X-ray detector, a second X-ray detector stacked upstream of the first X-ray detector, and an X-ray absorber stacked upstream of the first X-ray detector. The X-ray absorber provides an energy-dependent absorption of the incident X-rays before they are incident at the first X-ray detector, but provides no absorption of the incident X-rays before they are incident at the second X-ray detector. The first X-ray detector includes a linear array of first pixels, each of which produces an electrical output in response to the incident X-rays in a first range of energies. The first X-ray detector also includes a circuit that generates a first electrical signal in response to the electrical output of each of the first pixels. The second X-ray detector includes a linear array of second pixels, each of which produces an electrical output in response to the incident X-rays in a second range of energies, broader than the first range of energies. The second X-ray detector also includes a circuit that generates a second electrical signal in response to the electrical output of each of the second pixels. 12 figs.

  6. Radiosensitization of high-Z compounds by medium-energy 160 kV vs. high-energy 6 MV X-rays for radiation therapy: Theoretical, in vitro and in vivo studies of platinum compounds activating glioma F98 cancer cells

    NASA Astrophysics Data System (ADS)

    Lim, S.; Pradhan, A.; Nahar, S.; Montenegro, M.; Barth, R.; Nakkula, R.; Turro, C.

    2013-03-01

    Energy dependence of X-ray irradiation of high-Z compounds for enhanced radiosensitization is explored thoeretically and via in vitro and in vivo experiments. The cell killing ability of medium-energy X-rays from 160 kV source are found to be more effective than 6 MV X-rays in activating high-Z contrast agents. Results are presented for a newly synthesized Pt compound, Pyridine Terpyridine Pt(II) Nitrate ([Pt(typ)(py)]) and carboplatin in treating F98 rat glioma. In-vitro results show considerable reduction in cell viability for radiosensitized cells irradiated with a 160 kV irradiator. Cells treated with 6 MV LINAC radiation find little variation with radiation dose. Maximum dose enhancement factors (DEFs) and minimum cancer cell survival fractions correspond to 50-200 keV range, and fall rapidly at higher energies. Theoretical calculations of photoelectric absorption vis-a-vis total scattering demonstrates this energy dependence. However, in vivo studies of rats treated with [Pt(tpy)(py)] had a severe negative neurotoxic response, confirmed by histopathological analysis. But subsequent in vivo studies using carboplatin showed very positive results in the treatment of F98 glioma bearing rats and potential clinical radiation therapy.

  7. Evolution of X-Ray Clusters of Galaxies and Shock Heating of the Intracluster Medium

    NASA Astrophysics Data System (ADS)

    Takizawa, Motokazu; Mineshige, Shin

    1998-05-01

    Evolutions of spherical X-ray clusters of galaxies are studied by using an N-body+total variation diminishing (TVD) mesh code. We consider a growth of density perturbation of 1015 M⊙ composed of dark matter and gas in a cold dark matter-dominated universe with Ω0 = 1 or 0.2. When the perturbation collapsed at z ~ 1, a shock front appears at r ~ 0.1 Mpc, moving outward as ambient gas accretes toward cluster center. The shock front separates the inner X-ray-emitting, hot region from the outer cool region. In the former, gas is almost in hydrostatic equilibrium but with small radial infall (~100 km s-1) being left, while in the latter, gas falls almost freely and emits no X-rays. Gas inside the shock is strongly compressed and heated by shock so that X-ray luminosity rapidly rises in the early stage (until temperature reaches about virial). In the late stage, on the other hand, the X-ray luminosity rises only gradually due partly to the expansion of the inner high-temperature region and partly to the increase of X-ray emissivity of gas as the result of continuous adiabatic compression inside the shock. We also find that the density distribution is generally less concentrated in a lower density universe and, hence, X-ray luminosity rises more slowly than in a higher density universe. The shock front structure, which was not clearly resolved in the previous SPH simulations, is clearly captured by the present simulations. Our results confirm that shock heating plays an important role in the heating process of the intracluster medium. In addition, we find that a sound wave propagates outward, thereby producing modulations with amplitudes of ~10% in the radial temperature and density profiles which, in turn, cause time variations in the strength of the shock. Such modulations, if observed, could be used as a probe to investigate the internal structure of clusters and the initial temperature of gas.

  8. Suspension criteria for dual energy X ray absorptiometry.

    PubMed

    McLean, I D

    2013-02-01

    The use of dual-energy X-ray absorptiometry (DXA) units primarily for the assessment of fracture risk and in the diagnosis of osteoporosis is ubiquitous in Europe and ever-expanding in its implementation worldwide. DXA is known for its reported low radiation dose and precision in the determination of bone mineral density. However, the use of simple suspension criteria, as proposed in the new EC report RP-162, will identify units that are unfit for useful and safe diagnosis. Such suspension levels, however, are not a substitute for regular maintenance, quality control testing and optimisation of clinical outcomes.

  9. A high-resolution X-ray image of Puppis A - Inhomogeneities in the interstellar medium

    NASA Technical Reports Server (NTRS)

    Petre, R.; Kriss, G. A.; Winkler, P. F.; Canizares, C. R.

    1982-01-01

    Eleven HRI exposures from the Einstein Observatory are assembled into an 0.1-4 keV image of the Puppis A supernova remnant which displays a complex morphology that may reflect the structure of the shocked interstellar medium. In addition to showing a density gradient of a factor greater than four across the approximately 30 pc diameter of the remnant perpendicular to the galactic plane, a shell of X-ray emission is seen surrounding the northern half of Puppis A, coincident with the radio shell, whose edge brightness profile indicates direct hot plasma heating by the blast wave rather than evaporation from clouds. The interior structure of the supernova remnant suggests inhomogeneities whose sizes range over 0.1-5 pc, but with moderate density contrast. Although isolated clouds of 10-30/cu cm density are responsible for the two brightest X-ray features, they represent only a small fraction of the Puppis A mass.

  10. Energy-dispersive small-angle X-ray scattering with cone collimation using X-ray capillary optics

    NASA Astrophysics Data System (ADS)

    Li, Fangzuo; Liu, Zhiguo; Sun, Tianxi

    2016-09-01

    Energy-dispersive small-angle X-ray scattering (ED-SAXS) with an innovative design of cone collimation based on an ellipsoidal single-bounce capillary (ESBC) and a polycapillary parallel X-ray lens (PPXRL) had been explored. Using this new cone collimation system, scattering angle 2θ has a theoretical minimum angle related to the mean half-opening angle of the hollow cone beam of 1.42 mrad, and with the usable X-ray energy ranging from 4 to 30 keV, the resulting observable scattering vector q is down to a minimum value of about 0.003 Å-1 (or a Bragg spacing of about 2100 Å). However, the absorption of lower energies by X-ray capillary optics, sample transmission, and detector response function limits the application range to lower energy. Cone collimation ED-SAXS experiments carried out on pure water, Lupolen, and in situ temperature-dependent measurement of diacetylenic acid/melamine micelle solid were presented at three different scattering angles 2θ of 0.18°, 0.70° and 1.18° to illustrate the new opportunities offered by this technique as well as its limitations. Also, a comparison has been made by replacing the PPXRL with a pinhole, and the result shows that cone collimation ED-SAXS based on ESBC with PPXRL was helpful in improving the signal-to-noise ratio (i.e., reducing the parasitic background scattering) than ESBC with a pinhole. The cone collimation instrument based on X-ray capillary optics could be considered as a promising tool to perform SAXS experiments, especially cone collimation ED-SAXS has potential application for the in situ temperature-dependent studying on the kinetics of phase transitions.

  11. Dimensionality and noise in energy selective x-ray imaging

    SciTech Connect

    Alvarez, Robert E.

    2013-11-15

    Purpose: To develop and test a method to quantify the effect of dimensionality on the noise in energy selective x-ray imaging.Methods: The Cramèr-Rao lower bound (CRLB), a universal lower limit of the covariance of any unbiased estimator, is used to quantify the noise. It is shown that increasing dimensionality always increases, or at best leaves the same, the variance. An analytic formula for the increase in variance in an energy selective x-ray system is derived. The formula is used to gain insight into the dependence of the increase in variance on the properties of the additional basis functions, the measurement noise covariance, and the source spectrum. The formula is also used with computer simulations to quantify the dependence of the additional variance on these factors. Simulated images of an object with three materials are used to demonstrate the trade-off of increased information with dimensionality and noise. The images are computed from energy selective data with a maximum likelihood estimator.Results: The increase in variance depends most importantly on the dimension and on the properties of the additional basis functions. With the attenuation coefficients of cortical bone, soft tissue, and adipose tissue as the basis functions, the increase in variance of the bone component from two to three dimensions is 1.4 × 10{sup 3}. With the soft tissue component, it is 2.7 × 10{sup 4}. If the attenuation coefficient of a high atomic number contrast agent is used as the third basis function, there is only a slight increase in the variance from two to three basis functions, 1.03 and 7.4 for the bone and soft tissue components, respectively. The changes in spectrum shape with beam hardening also have a substantial effect. They increase the variance by a factor of approximately 200 for the bone component and 220 for the soft tissue component as the soft tissue object thickness increases from 1 to 30 cm. Decreasing the energy resolution of the detectors increases

  12. PHERMEX: Pulsed High-Energy Radiographic Machine Emitting X rays

    SciTech Connect

    Dick, R.D.

    1981-01-01

    The PHERMEX facility used to provide flash radiographs of explosives and explosive-driven metal systems is described. With this facility, precision radiographs of large objects containing materials with high atomic number and high density are attainable. PHERMEX encompasses the high-current, three-cavity, 30-MeV linear electron accelerator; the 50-MHz-radiofrequency power source to drive the cavities; timing, firing, and signal detection system; and a data-acquisition system. Some unique features of PHERMEX are reliability; very intensive submicrosecond bremsstrahlung source rich in 4- to 8-MeV x rays; less than 1.0-mm-diam spot size; precision determination of edges, discontinuities, and areal-mass distribution; and flash radiographs of large explosive systems close to the x-ray target. Some aspects of the PHERMEX-upgrading program are discussed. The program will result (1) in an increased electron-beam energy to about 50 MeV, (2) the use of an electron-gun pulser that is capable of producing three time-adjustable pulses for obtaining three radiographic pictures of a single explosive event, (3) an increased electron injection energy of 1.25 MeV, (4) the capability for recording high-speed signals, and (5) the use of computers to assist the monitoring and control of the data-acquisition system and the PHERMEX accelerator.

  13. A versatile medium-resolution x-ray emission spectrometer for diamond anvil cell applications

    SciTech Connect

    Mortensen, D. R.; Seidler, G. T.; Bradley, J. A.; Lipp, M. J.; Evans, W. J.; Chow, P.; Xiao, Y.-M.; Boman, G.; Bowden, M. E.

    2013-08-15

    We present design and performance details for a polycapillary-coupled x-ray spectrometer that provides very high collection efficiency at a moderate energy resolution suitable for many studies of nonresonant x-ray emission spectroscopy, especially for samples of heavy elements under high pressures. Using a single Bragg analyzer operating close to backscattering geometry so as to minimize the effect of the weak divergence of the quasicollimated exit beam from the polycapillary optic, this instrument can maintain a typical energy resolution of 5 eV over photon energies from 5 keV to 10 keV. We find dramatically improved count rates as compared to a traditional higher-resolution instrument based on a single spherically bent crystal analyzer.

  14. A Versatile Medium-Resolution X-ray Emission Spectrometer for Diamond Anvil Cell Applications

    SciTech Connect

    Mortensen, Devon R.; Seidler, G. T.; Bradley, J. A.; Lipp, M. J.; Evans, W. J.; Chow, P.; Xiao, Y. M.; Boman, G.; Bowden, Mark E.

    2013-08-28

    We present design and performance details for a polycapillary-coupled x-ray spectrometer that provides very high collection efficiency at a moderate energy resolution suitable for many studies of nonresonant x-ray emission spectroscopy, especially for samples of heavy elements under high pressures. Using a single Bragg analyzer operating close to a backscattering so as to minimize the effect of the weak divergence of the quasicollimated exit beam from the polycapillary optic, this instrument can maintain a typical energy resolution of 5 eV over photon energies from 5 keV to 10 keV. We find dramatically improved count rates as compared to a traditional higher-resolution instrument based on a single spherically-bent crystal analyzer.

  15. A versatile medium-resolution x-ray emission spectrometer for diamond anvil cell applications.

    PubMed

    Mortensen, D R; Seidler, G T; Bradley, J A; Lipp, M J; Evans, W J; Chow, P; Xiao, Y-M; Boman, G; Bowden, M E

    2013-08-01

    We present design and performance details for a polycapillary-coupled x-ray spectrometer that provides very high collection efficiency at a moderate energy resolution suitable for many studies of nonresonant x-ray emission spectroscopy, especially for samples of heavy elements under high pressures. Using a single Bragg analyzer operating close to backscattering geometry so as to minimize the effect of the weak divergence of the quasicollimated exit beam from the polycapillary optic, this instrument can maintain a typical energy resolution of 5 eV over photon energies from 5 keV to 10 keV. We find dramatically improved count rates as compared to a traditional higher-resolution instrument based on a single spherically bent crystal analyzer.

  16. Energy dispersive X-ray analyses of organelles of NaCI-treated maize root cells

    NASA Astrophysics Data System (ADS)

    Stelzer, Ralf

    1984-04-01

    NaCl sensitive plants of Zea mays cv. ADOUR were grown in nutrient solutions with or without NaCl. Frozen, hydrated root-tip tissues were investigated by means of an ETEC scanning electron microscope fitted with a KEVEX energy dispersive X-ray analyser. Morphological details of the gently etched but non-coated surface of the cross fractured specimen were easy to identify and to analyse using an electron beam with a low intensity at 10 kV. X-ray data obtained from cell compartments and organelles as nuclei, nucleoli and mitochondria within individual cells establish typical X-ray spectra. Comparisons of these spectra support the hypothesis that Na + ions are predominantly localized in vacuoles and also to a lesser extent in the cytoplasm, e.g. in small vesicles, but not in other cell organelles. Furthermore the analysed cell compartments show differences in the distribution of Mg, P, S, Cl, K and Ca effected by the addition of NaCl to the growth medium. The X-ray data are discussed in relation to the physiological meaning of a NaCl induced redistribution of elements within individual maize root cells.

  17. Characterization of Japanese color sticks by energy dispersive X-ray fluorescence, X-ray diffraction and Fourier transform infrared analysis

    NASA Astrophysics Data System (ADS)

    Manso, M.; Valadas, S.; Pessanha, S.; Guilherme, A.; Queralt, I.; Candeias, A. E.; Carvalho, M. L.

    2010-04-01

    This work comprises the use of energy dispersive X-ray fluorescence (EDXRF), X-ray diffraction (XRD) and Fourier transformed infrared (FTIR) techniques for the study of the composition of twentieth century traditional Japanese color sticks. By using the combination of analytical techniques it was possible to obtain information on inorganic and organic pigments, binders and fillers present in the sticks. The colorant materials identified in the sticks were zinc and titanium white, chrome yellow, yellow and red ochre, vermillion, alizarin, indigo, Prussian and synthetic ultramarine blue. The results also showed that calcite and barite were used as inorganic mineral fillers while Arabic gum was the medium used. EDXRF offered great potential for such investigations since it allowed the identification of the elements present in the sample preserving its integrity. However, this information alone was not enough to clearly identify some of the materials in study and therefore it was necessary to use XRD and FTIR techniques.

  18. Carbon and oxygen X-ray line emission from the interstellar medium

    NASA Technical Reports Server (NTRS)

    Schnopper, H. W.; Delvaille, J. P.; Rocchia, R.; Blondel, C.; Cheron, C.; Christy, J. C.; Ducros, R.; Koch, L.; Rothenflug, R.

    1982-01-01

    A soft X-ray, 0.3-1.0 keV spectrum from a 1 sr region which includes a portion of the North Polar Spur, obtained by three rocketborne lithium-drifted silicon detectors, shows the C V, C VI, O VII and O VIII emission lines. The spectrum is well fitted by a two-component, modified Kato (1976) model, where the coronal emission is in collisional equilibrium, with interstellar medium and North Polar Spur temperatures of 1.1 and 3.8 million K, respectively.

  19. Methods for calculating X-ray diffuse scattering from a crystalline medium with spheroidal quantum dots

    SciTech Connect

    Punegov, V. I. Sivkov, D. V.

    2015-03-15

    Two independent approaches to calculate the angular distribution of X-ray diffusion scattering from a crystalline medium with spheroidal quantum dots (QDs) have been proposed. The first method is based on the analytical solution involving the multipole expansion of elastic strain fields beyond QDs. The second approach is based on calculations of atomic displacements near QDs by the Green’s function method. An analysis of the diffuse scattering intensity distribution in the reciprocal space within these two approaches shows that both methods yield similar results for the chosen models of QD spatial distribution.

  20. High energy X-ray phase and dark-field imaging using a random absorption mask

    NASA Astrophysics Data System (ADS)

    Wang, Hongchang; Kashyap, Yogesh; Cai, Biao; Sawhney, Kawal

    2016-07-01

    High energy X-ray imaging has unique advantage over conventional X-ray imaging, since it enables higher penetration into materials with significantly reduced radiation damage. However, the absorption contrast in high energy region is considerably low due to the reduced X-ray absorption cross section for most materials. Even though the X-ray phase and dark-field imaging techniques can provide substantially increased contrast and complementary information, fabricating dedicated optics for high energies still remain a challenge. To address this issue, we present an alternative X-ray imaging approach to produce transmission, phase and scattering signals at high X-ray energies by using a random absorption mask. Importantly, in addition to the synchrotron radiation source, this approach has been demonstrated for practical imaging application with a laboratory-based microfocus X-ray source. This new imaging method could be potentially useful for studying thick samples or heavy materials for advanced research in materials science.

  1. 30-Lens interferometer for high-energy X-rays.

    PubMed

    Lyubomirskiy, Mikhail; Snigireva, Irina; Kohn, Victor; Kuznetsov, Sergey; Yunkin, Vyacheslav; Vaughan, Gavin; Snigirev, Anatoly

    2016-09-01

    A novel high-energy multi-lens interferometer consisting of 30 arrays of planar compound refractive lenses is reported. Under coherent illumination each lens array creates a diffraction-limited secondary source. Overlapping such coherent beams produces an interference pattern demonstrating strong longitudinal functional dependence. The proposed multi-lens interferometer was tested experimentally at the 100 m-long ID11 ESRF beamline in the X-ray energy range from 30 to 65 keV. The interference pattern generated by the interferometer was recorded at fundamental and fractional Talbot distances. An effective source size (FWHM) of the order of 15 µm was determined from the first Talbot image, proving the concept that the multi-lens interferometer can be used as a high-resolution tool for beam diagnostics. PMID:27577763

  2. X-ray diamond detectors with energy resolution

    SciTech Connect

    Conte, G.; Girolami, M.; Salvatori, S.; Ralchenko, V.

    2007-10-29

    Polycrystalline diamond detectors with energy resolving capability of the impinging beam were realized and tested by using a miniature pyroelectric x-ray pulse generator. Microstrip structures were defined by photolithography aimed to reduce parasitic capacitances and to perform characterization measurements in a sandwich configuration. Leakage currents as low as 20 pA at 500 V were measured on a 270 {mu}m thick device. Pulse height distributions were carried out around Ta L{alpha} (8.14 keV) and Cu K{alpha} (8.05 keV) characteristic lines of the source. Energy resolution at 200 V was found equal to 9% with an increase to 11% at 500 V. When the bias was increased to the maximum voltage the sample shows an Ohmic behavior.

  3. 30-Lens interferometer for high-energy X-rays.

    PubMed

    Lyubomirskiy, Mikhail; Snigireva, Irina; Kohn, Victor; Kuznetsov, Sergey; Yunkin, Vyacheslav; Vaughan, Gavin; Snigirev, Anatoly

    2016-09-01

    A novel high-energy multi-lens interferometer consisting of 30 arrays of planar compound refractive lenses is reported. Under coherent illumination each lens array creates a diffraction-limited secondary source. Overlapping such coherent beams produces an interference pattern demonstrating strong longitudinal functional dependence. The proposed multi-lens interferometer was tested experimentally at the 100 m-long ID11 ESRF beamline in the X-ray energy range from 30 to 65 keV. The interference pattern generated by the interferometer was recorded at fundamental and fractional Talbot distances. An effective source size (FWHM) of the order of 15 µm was determined from the first Talbot image, proving the concept that the multi-lens interferometer can be used as a high-resolution tool for beam diagnostics.

  4. Synchrotron energy-dispersive X-ray diffraction tomography

    NASA Astrophysics Data System (ADS)

    Hall, C.; Barnes, P.; Cockcroft, J. K.; Colston, S. L.; Häusermann, D.; Jacques, S. D. M.; Jupe, A. C.; Kunz, M.

    1998-04-01

    Energy-dispersive diffraction tomography using white-beam synchrotron X-rays with energies up to 140 keV yields images of the interior features of solid objects up to 50 mm thick. The volume sampled is determined by the geometry of the diffracting lozenge defined by the incident beam, the detector system collimation and the Bragg angle. Using conventional beam slits to form a highly collimated 50 μm × 50 μm incident beam and a 40 μm collimator aperture, we demonstrate on a PEEK phantom that a lateral resolution (transverse to the beam direction) of a few microns can be achieved. The resolution in the direction of the incident beam is necessarily poorer than this since the diffracting lozenge is elongated in this direction, with length increasing rapidly at small angles. There is no evidence of significant contamination of the diffracted intensity by the effects of multiple scattering from outside the primary lozenge.

  5. A medium sensitivity X-ray survey using the Einstein Observatory - The log N-log S relation for extragalactic X-ray sources

    NASA Technical Reports Server (NTRS)

    Maccacaro, T.; Gioia, I. M.; Zamorani, G.; Feigelson, E. D.; Fener, M.; Giacconi, R.; Griffiths, R. E.; Murray, S. S.; Stocke, J.; Liebert, J.

    1982-01-01

    The paper presents results of an X-ray survey of about 50 sq deg of the high galactic latitude sky at sensitivities in the range of 7 x 10 to the -14 to 5 x 10 to the -12 ergs/sq cm/s. The number-flux relation is derived for the extragalactic population to yield a best-fit power-law slope of 1.53 + or - 0.16, and the content of the sample is analyzed in terms of types of sources, appearing to be significantly different from the content of similar samples selected at higher fluxes. The medium sensitivity sample of extragalactic sources is dominated by active galactic nuclei, while samples selected at higher fluxes and higher energies are dominated by clusters of galaxies. Thus, the number-flux relation for extragalactic sources may be interpreted to a first approximation as the sum of the two different distributions with flatter and steeper slopes describing clusters and AGNs, respectively.

  6. Temporal evolution of an energetic electron population in an inhomogeneous medium: Application to solar hard X-ray bursts

    NASA Technical Reports Server (NTRS)

    Vilmer, N.; Mackinnon, A. L.; Trottet, G.

    1985-01-01

    Energetic electrons accelerated during solar flares can be studied through the hard X-ray emission they produce when interacting with the solar ambient atmosphere. In the case of the non thermal hard X-ray emission, the instanteous X-ray flux emitted at one point of the atmosphere is related to the instantaneous fast electron spectrum at that point. A hard X-ray source model then requires the understanding of the evolution in space and time of the fast particle distribution. The physical processes involved here are energy losses due to Coulomb collisions and pitch angle scattering due to both collisions and magnetic field gradients.

  7. High-Energy X-Ray Diffraction Analysis Tool

    2011-11-29

    The functionality of heRXD includes the following: distance and angular calibration and viewing flat-panel detector images used for X-ray diffraction; image (polar) rebinning or "caking"; line position fitting in powder diffraction images; image segmentation or "blob finding"; crystal orentation indesing; and lattice vector refinement. These functionalities encompass a critical set analyzing teh data for high-energy diffraction measurements that are currently performed at synchrotron sources such as the Advanced Photon Source (APS). The software design modularmore » and open source under LGPL. The intent is to provide a common framework and graphical user interface that has the ability to utillize internal as well as external subroutines to provide various optins for performing the fuctionalities listed above. The software will initially be deployed at several national user facilities--including APS, ALS, and CHESS--and then made available for download using a hosting service such as sourceforge.« less

  8. High-Energy X-Ray Diffraction Analysis Tool

    SciTech Connect

    2011-11-29

    The functionality of heRXD includes the following: distance and angular calibration and viewing flat-panel detector images used for X-ray diffraction; image (polar) rebinning or "caking"; line position fitting in powder diffraction images; image segmentation or "blob finding"; crystal orentation indesing; and lattice vector refinement. These functionalities encompass a critical set analyzing teh data for high-energy diffraction measurements that are currently performed at synchrotron sources such as the Advanced Photon Source (APS). The software design modular and open source under LGPL. The intent is to provide a common framework and graphical user interface that has the ability to utillize internal as well as external subroutines to provide various optins for performing the fuctionalities listed above. The software will initially be deployed at several national user facilities--including APS, ALS, and CHESS--and then made available for download using a hosting service such as sourceforge.

  9. Development of Compton X-ray spectrometer for high energy resolution single-shot high-flux hard X-ray spectroscopy.

    PubMed

    Kojima, Sadaoki; Ikenouchi, Takahito; Arikawa, Yasunobu; Sakata, Shohei; Zhang, Zhe; Abe, Yuki; Nakai, Mitsuo; Nishimura, Hiroaki; Shiraga, Hiroyuki; Ozaki, Tetsuo; Miyamoto, Shuji; Yamaguchi, Masashi; Takemoto, Akinori; Fujioka, Shinsuke; Azechi, Hiroshi

    2016-04-01

    Hard X-ray spectroscopy is an essential diagnostics used to understand physical processes that take place in high energy density plasmas produced by intense laser-plasma interactions. A bundle of hard X-ray detectors, of which the responses have different energy thresholds, is used as a conventional single-shot spectrometer for high-flux (>10(13) photons/shot) hard X-rays. However, high energy resolution (Δhv/hv < 0.1) is not achievable with a differential energy threshold (DET) X-ray spectrometer because its energy resolution is limited by energy differences between the response thresholds. Experimental demonstration of a Compton X-ray spectrometer has already been performed for obtaining higher energy resolution than that of DET spectrometers. In this paper, we describe design details of the Compton X-ray spectrometer, especially dependence of energy resolution and absolute response on photon-electron converter design and its background reduction scheme, and also its application to the laser-plasma interaction experiment. The developed spectrometer was used for spectroscopy of bremsstrahlung X-rays generated by intense laser-plasma interactions using a 200 μm thickness SiO2 converter. The X-ray spectrum obtained with the Compton X-ray spectrometer is consistent with that obtained with a DET X-ray spectrometer, furthermore higher certainly of a spectral intensity is obtained with the Compton X-ray spectrometer than that with the DET X-ray spectrometer in the photon energy range above 5 MeV. PMID:27131669

  10. Development of Compton X-ray spectrometer for high energy resolution single-shot high-flux hard X-ray spectroscopy.

    PubMed

    Kojima, Sadaoki; Ikenouchi, Takahito; Arikawa, Yasunobu; Sakata, Shohei; Zhang, Zhe; Abe, Yuki; Nakai, Mitsuo; Nishimura, Hiroaki; Shiraga, Hiroyuki; Ozaki, Tetsuo; Miyamoto, Shuji; Yamaguchi, Masashi; Takemoto, Akinori; Fujioka, Shinsuke; Azechi, Hiroshi

    2016-04-01

    Hard X-ray spectroscopy is an essential diagnostics used to understand physical processes that take place in high energy density plasmas produced by intense laser-plasma interactions. A bundle of hard X-ray detectors, of which the responses have different energy thresholds, is used as a conventional single-shot spectrometer for high-flux (>10(13) photons/shot) hard X-rays. However, high energy resolution (Δhv/hv < 0.1) is not achievable with a differential energy threshold (DET) X-ray spectrometer because its energy resolution is limited by energy differences between the response thresholds. Experimental demonstration of a Compton X-ray spectrometer has already been performed for obtaining higher energy resolution than that of DET spectrometers. In this paper, we describe design details of the Compton X-ray spectrometer, especially dependence of energy resolution and absolute response on photon-electron converter design and its background reduction scheme, and also its application to the laser-plasma interaction experiment. The developed spectrometer was used for spectroscopy of bremsstrahlung X-rays generated by intense laser-plasma interactions using a 200 μm thickness SiO2 converter. The X-ray spectrum obtained with the Compton X-ray spectrometer is consistent with that obtained with a DET X-ray spectrometer, furthermore higher certainly of a spectral intensity is obtained with the Compton X-ray spectrometer than that with the DET X-ray spectrometer in the photon energy range above 5 MeV.

  11. Improved energy coupling into the gain region of the Ni-like Pd transient collisional x-ray laser

    SciTech Connect

    Smith, R; Dunn, J; Filevich, J; Moon, S; Nilsen, J; Keenan, R; Shlyaptsev, V; Rocca, J; Hunter, J; Shepherd, R; Booth, R; Marconi, M

    2004-10-05

    We present within this paper a series of experiments, which yield new observations to further our understanding of the transient collisional x-ray laser medium. We use the recently developed technique of picosecond x-ray laser interferometry to probe the plasma conditions in which the x-ray laser is generated and propagates. This yields two dimensional electron density maps of the plasma taken at different times relative to the peak of the 600ps plasma-forming beam. In another experimental campaign, the output of the x-ray laser plasma column is imaged with a spherical multilayer mirror onto a CCD camera to give a two-dimensional intensity map of the x-ray laser output. Near-field imaging gives insights into refraction, output intensity and spatial mode structure. Combining these images with the density maps gives an indication of the electron density at which the x-ray laser is being emitted at (yielding insights into the effect of density gradients on beam propagation). Experimental observations coupled with simulations predict that most effective coupling of laser pump energy occurs when the duration of the main heating pulse is comparable to the gain lifetime ({approx}10ps for Ni-like schemes). This can increase the output intensity by more than an order of magnitude relative to the case were the same pumping energy is delivered within a shorter heating pulse duration (< 3ps). We have also conducted an experiment in which the output of the x-ray laser was imaged onto the entrance slit of a high temporal resolution streak camera. This effectively takes a one-dimensional slice of the x-ray laser spatial profile and sweeps it in time. Under some conditions we observe rapid movement of the x-ray laser ({approx} 3 {micro}m/ps) towards the target surface.

  12. High resolution energy-sensitive digital X-ray

    DOEpatents

    Nygren, David R.

    1995-01-01

    An apparatus and method for detecting an x-ray and for determining the depth of penetration of an x-ray into a semiconductor strip detector. In one embodiment, a semiconductor strip detector formed of semiconductor material is disposed in an edge-on orientation towards an x-ray source such that x-rays From the x-ray source are incident upon and substantially perpendicular to the front edge of the semiconductor strip detector. The semiconductor strip detector is formed of a plurality of segments. The segments are coupled together in a collinear arrangement such that the semiconductor strip detector has a length great enough such that substantially all of the x-rays incident on the front edge of the semiconductor strip detector interact with the semiconductor material which forms the semiconductor strip detector. A plurality of electrodes are connected to the semiconductor strip detect or such that each one of the of semiconductor strip detector segments has at least one of the of electrodes coupled thereto. A signal processor is also coupled to each one of the electrodes. The present detector detects an interaction within the semiconductor strip detector, between an x-ray and the semiconductor material, and also indicates the depth of penetration of the x-ray into the semiconductor strip detector at the time of the interaction.

  13. High resolution energy-sensitive digital X-ray

    DOEpatents

    Nygren, D.R.

    1995-07-18

    An apparatus and method for detecting an x-ray and for determining the depth of penetration of an x-ray into a semiconductor strip detector. In one embodiment, a semiconductor strip detector formed of semiconductor material is disposed in an edge-on orientation towards an x-ray source such that x-rays from the x-ray source are incident upon and substantially perpendicular to the front edge of the semiconductor strip detector. The semiconductor strip detector is formed of a plurality of segments. The segments are coupled together in a collinear arrangement such that the semiconductor strip detector has a length great enough such that substantially all of the x-rays incident on the front edge of the semiconductor strip detector interact with the semiconductor material which forms the semiconductor strip detector. A plurality of electrodes are connected to the semiconductor strip detector such that each one of the semiconductor strip detector segments has at least one of the of electrodes coupled thereto. A signal processor is also coupled to each one of the electrodes. The present detector detects an interaction within the semiconductor strip detector, between an x-ray and the semiconductor material, and also indicates the depth of penetration of the x-ray into the semiconductor strip detector at the time of the interaction. 5 figs.

  14. Dual energy iodine contrast CT with monochromatic x-rays

    SciTech Connect

    Dilmanian, F.A.; Wu, X.Y.; Kress, J.

    1995-12-31

    Computed tomography (CT) with monochromatic x-ray beams was used to image phantoms and a live rabbit using the preclinical Multiple Energy Computed Tomography (MECT) system at the National Synchrotron Light Source. MECT has a horizontal fan beam with a subject apparatus rotating about a vertical axis. Images were obtained at 43 keV for single-energy studies, and at energies immediately below and above the 33.17 keV iodine K-edge for dual-energy subtraction CT. Two CdWO{sub 4}-photodiode array detectors were used. The high-resolution detector (0.5 mm pitch, uncollimated) provided 14 line pair/cm in-plane spatial resolution, with lower image noise than conventional CT. Images with the low-resolution detector (1.844-mm pitch, collimated to 0.922 mm detector elements) had a sensitivity for iodine of {approx} 60 {micro}g/cc in 11-mm channels inside a 135 mm-diameter acrylic cylindrical phantom for a slice height of 2.5 mm and a surface does of {approx} 4 cGy. The image noise was {approx} 1 Hounsfield Unit (HU); it was {approx} 3 HU for the same phantom imaged with conventional CT at approximately the same dose, slice height, and spatial resolution ({approx} 7 lp/cm). These results show the potential advantage of MECT, despite present technical limitations.

  15. Superiority of Low Energy 160 KV X-Rays Compared to High Energy 6 MV X-Rays in Heavy Element Radiosensitization for Cancer Treatment

    NASA Astrophysics Data System (ADS)

    Lim, Sara N.; Pradhan, Anil K.; Nahar, Sultana N.; Barth, Rolf F.; Yang, Weilian; Nakkula, Robin J.; Palmer, Alycia; Turro, Claudia

    2013-06-01

    High energy X-rays in the MeV range are generally employed in conventional radiation therapy from linear accelerators (LINAC) to ensure sufficient penetration depths. However, lower energy X-rays in the keV range may be more effective when coupled with heavy element (high-Z or HZ) radiosensitizers. Numerical simulations of X-ray energy deposition for tumor phantoms sensitized with HZ radiosensitizers were performed using the Monte Carlo code Geant4. The results showed enhancement in energy deposition to radiosensitized phantoms relative to unsensitized phantoms for low energy X-rays in the keV range. In contrast, minimal enhancement was seen using high energy X-rays in the MeV range. Dose enhancement factors (DEFs) were computed and showed radiosensitization only in the low energy range < 200 keV, far lower than the energy of the majority of photons in the LINAC energy range. In vitro studies were carried to demonstrate the tumoricidal effects of HZ sensitized F98 rat glioma cells following irradiation with both low energy 160 kV and high energy 6 MV X-ray sources. The platinum compound, pyridine terpyridine Pt(II) nitrate, was initially used because it was 7x less toxic that an equivalent amount of carboplatin in vitro studies. This would allow us to separate the radiotoxic and the chemotoxic effects of HZ sensitizers. Results from this study showed a 10-fold dose dependent reduction in surviving fractions (SF) of radiosensitized cells treated with low energy 160 kV X-rays compared to those treated with 6 MV X-rays. This is in agreement with our simulations that show an increase in dose deposition in radiosensitized tumors for low energy X-rays. Due to unforeen in vivo toxicity, however, another in vitro study was performed using the commonly used, Pt-based chemotherapeutic drug carboplatin which confirmed earlier results. This lays the ground work for a planned in vivo study using F98 glioma bearing rats. This study demonstrates that while high energy X-rays are

  16. An edge-on charge-transfer design for energy-resolved x-ray detection.

    PubMed

    Shi, Zaifeng; Yang, Haoyu; Cong, Wenxiang; Wang, Ge

    2016-06-01

    As an x-ray beam goes through the human body, it will collect important information via interaction with tissues. Since this interaction is energy-sensitive, the state-of-the-art spectral CT technologies provide higher quality images of biological tissues with x-ray energy information (or spectral information). With existing energy-integrating technologies, a large fraction of energy information is ignored in the x-ray detection process. Although the recently proposed photon-counting technology promises to achieve higher image quality at a lower radiation dose, it suffers from limitations in counting rate, performance uniformity, and fabrication cost. In this paper, we focus on an alternative approach to resolve the energy distribution of transmitted x-ray photons. First, we analyze the x-ray attenuation in a silicon substrate and describe a linear approximation model for x-ray detection. Then, we design an edge-on architecture based on the proposed energy-resolving model. In our design, the x-ray-photon-induced charges are transferred sequentially resembling the working process of a CCD camera. Finally, we numerically evaluate the linear approximation of x-ray attenuation and derive the energy distribution of x-ray photons. Our simulation results show that the proposed energy-sensing approach is feasible and has the potential to complement the photon-counting technology.

  17. An edge-on charge-transfer design for energy-resolved x-ray detection.

    PubMed

    Shi, Zaifeng; Yang, Haoyu; Cong, Wenxiang; Wang, Ge

    2016-06-01

    As an x-ray beam goes through the human body, it will collect important information via interaction with tissues. Since this interaction is energy-sensitive, the state-of-the-art spectral CT technologies provide higher quality images of biological tissues with x-ray energy information (or spectral information). With existing energy-integrating technologies, a large fraction of energy information is ignored in the x-ray detection process. Although the recently proposed photon-counting technology promises to achieve higher image quality at a lower radiation dose, it suffers from limitations in counting rate, performance uniformity, and fabrication cost. In this paper, we focus on an alternative approach to resolve the energy distribution of transmitted x-ray photons. First, we analyze the x-ray attenuation in a silicon substrate and describe a linear approximation model for x-ray detection. Then, we design an edge-on architecture based on the proposed energy-resolving model. In our design, the x-ray-photon-induced charges are transferred sequentially resembling the working process of a CCD camera. Finally, we numerically evaluate the linear approximation of x-ray attenuation and derive the energy distribution of x-ray photons. Our simulation results show that the proposed energy-sensing approach is feasible and has the potential to complement the photon-counting technology. PMID:27192190

  18. An edge-on charge-transfer design for energy-resolved x-ray detection

    NASA Astrophysics Data System (ADS)

    Shi, Zaifeng; Yang, Haoyu; Cong, Wenxiang; Wang, Ge

    2016-06-01

    As an x-ray beam goes through the human body, it will collect important information via interaction with tissues. Since this interaction is energy-sensitive, the state-of-the-art spectral CT technologies provide higher quality images of biological tissues with x-ray energy information (or spectral information). With existing energy-integrating technologies, a large fraction of energy information is ignored in the x-ray detection process. Although the recently proposed photon-counting technology promises to achieve higher image quality at a lower radiation dose, it suffers from limitations in counting rate, performance uniformity, and fabrication cost. In this paper, we focus on an alternative approach to resolve the energy distribution of transmitted x-ray photons. First, we analyze the x-ray attenuation in a silicon substrate and describe a linear approximation model for x-ray detection. Then, we design an edge-on architecture based on the proposed energy-resolving model. In our design, the x-ray-photon-induced charges are transferred sequentially resembling the working process of a CCD camera. Finally, we numerically evaluate the linear approximation of x-ray attenuation and derive the energy distribution of x-ray photons. Our simulation results show that the proposed energy-sensing approach is feasible and has the potential to complement the photon-counting technology.

  19. Detection of high energy X-rays from the galactic center region

    NASA Technical Reports Server (NTRS)

    Dennis, B. R.; Beall, J. H.; Cutler, E. P.; Crannell, C. J.; Dolan, J. G.; Frost, K. J.; Orwig, L. E.

    1979-01-01

    Observations of the galactic center region made with the high energy X-ray detector on OSO-8 are discussed. A strong hard X-ray which was detected during these observations from the vicinity of the galactic center are examined. The counting rate spectrum and the photon number spectrum of the flux are determined. Comparisons with the high energy X-ray fluxes observed from sources in the region by others are discussed.

  20. The Diffuse EUV and X-Ray Background as a Probe of the Interstellar Medium

    NASA Technical Reports Server (NTRS)

    Lieu, Richard

    2001-01-01

    We have used the Deep Survey telescope of the Extreme Ultraviolet Explorer to investigate shadows in the diffuse EUV/soft X-ray background that are cast by clouds in the interstellar medium. We confirm the existence of a shadow previously reported and provide evidence for two new shadows. We used IRAS data to identify the clouds producing these shadows and to determine their optical depth to EUV radiation. The EUV-absorbing clouds are optically thick in the EUV, and all EUV emission detected in the direction of these shadows must be produced from material in front of the clouds. We obtained new optical data to determine the distance to these clouds. We use a new differential cloud technique to obtain the pressure of the interstellar medium. These results do not depend on any zero-level calibration of the data. Our results provide evidence that the pressure of the hot interstellar gas is the same in three different directions in the local interstellar medium and is at least 8 times higher than that derived for the Local Cloud surrounding our Sun. This provides new evidence for large thermal pressure imbalances in the local ISM and directly contradicts the basic assumption of thermal pressure equilibrium used in almost all present models of the interstellar medium.

  1. Quasi-stellar objects in the intergalactic medium: Source for the cosmic X-ray background

    SciTech Connect

    Sherman, R.D.

    1980-06-15

    QSOs are regarded as sources of both electromagnetic radiation and ejected matter that heat and ionize a dense intergalactic medium (IGM). Using current estimates of QSO luminosity, number density, evolution, and spectral index, we study three viable models: the diffuse cosmic X-ray background is (1) due entirely to thermal Bremsstrahlung of the IGM, (2) completely supplied by QSO X-radiation, (3) or a combination of both. The upper limits on an IGM fractional density with respect to closure are ..cap omega..=0.26, 0.24, and 0.21 for pure collisional, photo/collisional mixture, and pure photoionization, respectively. These calculations give emission spectra, Compton distortion of the cosmic microwave background, and optical depths to distant OSOs for comparison with relevant data.

  2. Stacked Fresnel Zone Plates for High Energy X-rays

    SciTech Connect

    Snigireva, Irina; Snigirev, Anatoly; Vaughan, Gavin; Di Michiel, Marco; Kohn, Viktor; Yunkin, Vyacheslav; Grigoriev, Maxim

    2007-01-19

    A stacking technique was developed in order to increase focusing efficiency of Fresnel zone plates (FZP) at high energies. Two identical Si chips each of which containing 9 FZPs were used for stacking. Alignment of the chips was achieved by on-line observation of the moire pattern. The formation of moire patterns was studied theoretically and experimentally at different experimental conditions. To provide the desired stability Si-chips were bonded together with slow solidification speed epoxy glue. A technique of angular alignment in order to compensate a linear displacement in the process of gluing was proposed. Two sets of stacked FZPs were experimentally tested to focus 15 and 50 keV x rays. The gain in the efficiency by factor 2.5 was demonstrated at 15 keV. The focal spot of 1.8 {mu}m vertically and 14 {mu}m horizontally with 35% efficiency was measured at 50 keV. Forecast for the stacking of nanofocusing FZPs was discussed.

  3. Automatic detection of bone fragments in poultry using multi-energy x-rays

    DOEpatents

    Gleason, Shaun S [Knoxville, TN; Paulus, Michael J [Knoxville, TN; Mullens, James A [Knoxville, TN

    2002-04-09

    At least two linear arrays of x-ray detectors are placed below a conveyor belt in a poultry processing plant. Multiple-energy x-ray sources illuminate the poultry and are detected by the detectors. Laser profilometry is used to measure the poultry thickness as the x-ray data is acquired. The detector readout is processed in real time to detect the presence of small highly attenuating fragments in the poultry, i.e., bone, metal, and cartilage.

  4. Energy dispersive X-ray reflectivity characterization of semiconductor heterostructures and interfaces

    SciTech Connect

    Chason, E.; Mayer, T.M.; Krstelj, Z.M.

    1995-07-01

    Energy dispersive X-ray reflectivity is a versatile tool for analyzing thin film structures. Layer thickness, interface roughness and composition can be determined with a single non-destructive measurement. Use of energy dispersive detection enables spectra to be acquired in less than 500 s with a rotating anode X-ray generator, making the study of kinetics possible.

  5. A Review of X-ray Diagnostic Calibrations in the 2 to 100 keV Region Using the High Energy X-ray Calibration Facility (HEX)

    SciTech Connect

    Ali, Zaheer; Pond, T; Buckles, R A; Maddox, B R; Chen, C D; DeWald, E L; Izumi, N; Stewart, R

    2010-05-19

    The precise and accurate measurement of X-rays in the 2 keV to 100 keV region is crucial to the understanding of HED plasmas and warm dense matter in general. With the emergence of inertially confined plasma facilities as the premier platforms for ICF, laboratory astrophysics, and national security related plasma experiments, the need to calibrate diagnostics in the high energy X-ray regime has grown. At National Security Technologies High Energy X-ray Calibration Facility (HEX) in Livermore, California, X-ray imagers, filter-fluorescer spectrometers, crystal spectrometers, image plates, and nuclear diagnostics are calibrated. The HEX can provide measurements of atomic line radiation, X-ray flux (accuracy within 10%), and X-ray energy (accuracy within 1%). The HEX source is comprised of a commercial 160 kV X-ray tube, a fluorescer wheel, a filter wheel, and a lead encasement. The X-ray tube produces a Tungsten bremsstrahlung spectrum which causes a foil to fluoresce line radiation. To minimize bremsstrahlung in the radiation for calibration we also provide various foils as filters. For experimental purposes, a vacuum box capable of 10{sup -7} Torr, as well as HPGe and CdTe radiation detectors, are provided on an optical table. Most geometries and arrangements can be changed to meet experimental needs.

  6. Diffuse Hard X-Ray Emission in Starburst Galaxies as Synchrotron from Very High Energy Electrons

    NASA Astrophysics Data System (ADS)

    Lacki, Brian C.; Thompson, Todd A.

    2013-01-01

    The origin of the diffuse hard X-ray (2-10 keV) emission from starburst galaxies is a long-standing problem. We suggest that synchrotron emission of 10-100 TeV electrons and positrons (e ±) can contribute to this emission, because starbursts have strong magnetic fields. We consider three sources of e ± at these energies: (1) primary electrons directly accelerated by supernova remnants, (2) pionic secondary e ± created by inelastic collisions between cosmic ray (CR) protons and gas nuclei in the dense interstellar medium of starbursts, and (3) pair e ± produced between the interactions between 10 and 100 TeV γ-rays and the intense far-infrared (FIR) radiation fields of starbursts. We create one-zone steady-state models of the CR population in the Galactic center (R <= 112 pc), NGC 253, M82, and Arp 220's nuclei, assuming a power-law injection spectrum for electrons and protons. We consider different injection spectral slopes, magnetic field strengths, CR acceleration efficiencies, and diffusive escape times, and include advective escape, radiative cooling processes, and secondary and pair e ±. We compare these models to extant radio and GeV and TeV γ-ray data for these starbursts, and calculate the diffuse synchrotron X-ray and inverse Compton (IC) luminosities of these starbursts in the models which satisfy multiwavelength constraints. If the primary electron spectrum extends to ~PeV energies and has a proton/electron injection ratio similar to the Galactic value, we find that synchrotron emission contributes 2%-20% of their unresolved, diffuse hard X-ray emission. However, there is great uncertainty in this conclusion because of the limited information on the CR electron spectrum at these high energies. IC emission is likewise a minority of the unresolved X-ray emission in these starbursts, from 0.1% in the Galactic center to 10% in Arp 220's nuclei, with the main uncertainty being the starbursts' magnetic field. We also model generic starbursts, including

  7. Measurements of High Energy X-Ray Dose Distributions Using Multi-Dimensional Fiber-Optic Radiation Detectors

    NASA Astrophysics Data System (ADS)

    Jang, Kyoung Won; Cho, Dong Hyun; Shin, Sang Hun; Lee, Bongsoo; Chung, Soon-Cheol; Tack, Gye-Rae; Yi, Jeong Han; Kim, Sin; Cho, Hyosung

    In this study, we have fabricated multi-dimensional fiber-optic radiation detectors with organic scintillators, plastic optical fibers and photo-detectors such as photodiode array and a charge-coupled device. To measure the X-ray dose distributions of the clinical linear accelerator in the tissue-equivalent medium, we have fabricated polymethylmethacrylate phantoms which have one-dimensional and two-dimensional fiber-optic detector arrays inside. The one-dimensional and two-dimensional detector arrays can be used to measure percent depth doses and surface dose distributions of high energy X-ray in the phantom respectively.

  8. Studying X-Ray Binaries with High Energy Frequency Quasi-Periodic Oscillations

    NASA Technical Reports Server (NTRS)

    Kaaret, P.; West, Donald K. (Technical Monitor)

    2002-01-01

    The goal of this investigation is to further our understanding of the dynamics of secreting neutron stars and black holes in the hope of using these systems as probes of the physics of strong gravitational fetus. The main focus of this work has been a multi-year program of simultaneous millisecond X-ray timing and spectral observations carried out with the Rossi X-Ray Timing Explorer (RXTE) to perform the X-ray timing and one of the satellites Asca, BeppoSAX, or Chandra to perform X-ray spectral measurements. With the advent of Chandra, we have extended our work to incLude extragalactic X-ray binaries. We conducted a comprehensive study of the X-ray and radio behavior of the Black Hole Candidate (BHC) X-ray transient XTE J1550-564 using RXTE, Chandra, and the Australian Telescope Compact Array (ATCA). We showed that strong radio emission is associated with major X-ray outbursts involving an X-ray state transition, while a compact radio jet is seen in the low/hard X-ray state found in the outburst decay. Interesting, the total energy required to produce the compact jet may be a substantial fraction of the total accretion energy of the system in that state. We also performed a detailed study of the spectral and timing properties of the decay. In joint RXTE/BeppoSAX observations of the neutron-star X-ray binary Cyg X-2, we discovered a correlation between the timing properties (the frequency of the horizontal branch oscillations) and the properties of a soft, thermal component of the X-ray spectrum. d e showed that more detX- ray from accreting neutron stars. We have completed analysis of RXTE observations of the X-ray transient SAX J1750.8-2900 made after detection of X-ray bursts from the source with the BeppoSAX Wide-Field Camera. We discovered millisecond oscillations in both the persistent emission and in the X-ray bursts.

  9. Energy dependence measurement of small-type optically stimulated luminescence (OSL) dosimeter by means of characteristic X-rays induced with general diagnostic X-ray equipment.

    PubMed

    Takegami, Kazuki; Hayashi, Hiroaki; Okino, Hiroki; Kimoto, Natsumi; Maehata, Itsumi; Kanazawa, Yuki; Okazaki, Tohru; Hashizume, Takuya; Kobayashi, Ikuo

    2016-01-01

    For X-ray inspections by way of general X-ray equipment, it is important to measure an entrance-skin dose. Recently, a small optically stimulated luminescence (OSL) dosimeter was made commercially available by Landauer, Inc. The dosimeter does not interfere with the medical images; therefore, it is expected to be a convenient detector for measuring personal exposure doses. In an actual clinical situation, it is assumed that X-rays of different energies will be detected by a dosimeter. For evaluation of the exposure dose measured by a dosimeter, it is necessary to know the energy dependence of the dosimeter. Our aim in this study was to measure the energy dependence of the OSL dosimeter experimentally in the diagnostic X-ray region. Metal samples weighing several grams were irradiated and, in this way, characteristic X-rays having energies ranging from 8 to 85 keV were generated. Using these mono-energetic X-rays, the dosimeter was irradiated. Simultaneously, the fluence of the X-rays was determined with a CdTe detector. The energy-dependent efficiency of the dosimeter was derived from the measured value of the dosimeter and the fluence. Moreover, the energy-dependent efficiency was calculated by Monte-Carlo simulation. The efficiency obtained in the experiment was in good agreement with that of the simulation. In conclusion, our proposed method, in which characteristic X-rays are used, is valuable for measurement of the energy dependence of a small OSL dosimeter in the diagnostic X-ray region. PMID:26589210

  10. Energy dependence measurement of small-type optically stimulated luminescence (OSL) dosimeter by means of characteristic X-rays induced with general diagnostic X-ray equipment.

    PubMed

    Takegami, Kazuki; Hayashi, Hiroaki; Okino, Hiroki; Kimoto, Natsumi; Maehata, Itsumi; Kanazawa, Yuki; Okazaki, Tohru; Hashizume, Takuya; Kobayashi, Ikuo

    2016-01-01

    For X-ray inspections by way of general X-ray equipment, it is important to measure an entrance-skin dose. Recently, a small optically stimulated luminescence (OSL) dosimeter was made commercially available by Landauer, Inc. The dosimeter does not interfere with the medical images; therefore, it is expected to be a convenient detector for measuring personal exposure doses. In an actual clinical situation, it is assumed that X-rays of different energies will be detected by a dosimeter. For evaluation of the exposure dose measured by a dosimeter, it is necessary to know the energy dependence of the dosimeter. Our aim in this study was to measure the energy dependence of the OSL dosimeter experimentally in the diagnostic X-ray region. Metal samples weighing several grams were irradiated and, in this way, characteristic X-rays having energies ranging from 8 to 85 keV were generated. Using these mono-energetic X-rays, the dosimeter was irradiated. Simultaneously, the fluence of the X-rays was determined with a CdTe detector. The energy-dependent efficiency of the dosimeter was derived from the measured value of the dosimeter and the fluence. Moreover, the energy-dependent efficiency was calculated by Monte-Carlo simulation. The efficiency obtained in the experiment was in good agreement with that of the simulation. In conclusion, our proposed method, in which characteristic X-rays are used, is valuable for measurement of the energy dependence of a small OSL dosimeter in the diagnostic X-ray region.

  11. The high energy X-ray spectrum of the Crab Nebula observed from OSO 8

    NASA Technical Reports Server (NTRS)

    Dolan, J. F.; Crannell, L. J.; Dennis, B. R.; Orwig, L. E.; Maurer, G. S.; Frost, K. J.

    1977-01-01

    The X-ray spectrum of the Crab Nebula was measured with the scintillation spectrometer on board the OSO-8 satellite. The total emission of the X-ray source shows no long term variability. The spectrum itself can be described by a single power law out to energies of at least 500 keV.

  12. Compact pnCCD-based X-ray camera with high spatial and energy resolution: a color X-ray camera.

    PubMed

    Scharf, O; Ihle, S; Ordavo, I; Arkadiev, V; Bjeoumikhov, A; Bjeoumikhova, S; Buzanich, G; Gubzhokov, R; Günther, A; Hartmann, R; Kühbacher, M; Lang, M; Langhoff, N; Liebel, A; Radtke, M; Reinholz, U; Riesemeier, H; Soltau, H; Strüder, L; Thünemann, A F; Wedell, R

    2011-04-01

    For many applications there is a requirement for nondestructive analytical investigation of the elemental distribution in a sample. With the improvement of X-ray optics and spectroscopic X-ray imagers, full field X-ray fluorescence (FF-XRF) methods are feasible. A new device for high-resolution X-ray imaging, an energy and spatial resolving X-ray camera, is presented. The basic idea behind this so-called "color X-ray camera" (CXC) is to combine an energy dispersive array detector for X-rays, in this case a pnCCD, with polycapillary optics. Imaging is achieved using multiframe recording of the energy and the point of impact of single photons. The camera was tested using a laboratory 30 μm microfocus X-ray tube and synchrotron radiation from BESSY II at the BAMline facility. These experiments demonstrate the suitability of the camera for X-ray fluorescence analytics. The camera simultaneously records 69,696 spectra with an energy resolution of 152 eV for manganese K(α) with a spatial resolution of 50 μm over an imaging area of 12.7 × 12.7 mm(2). It is sensitive to photons in the energy region between 3 and 40 keV, limited by a 50 μm beryllium window, and the sensitive thickness of 450 μm of the chip. Online preview of the sample is possible as the software updates the sums of the counts for certain energy channel ranges during the measurement and displays 2-D false-color maps as well as spectra of selected regions. The complete data cube of 264 × 264 spectra is saved for further qualitative and quantitative processing.

  13. An X-ray image of the violent interstellar medium in 30 Doradus

    NASA Astrophysics Data System (ADS)

    Wang, Q.; Helfand, D. J.

    1991-04-01

    A detailed analysis of the X-ray emission from the largest H II region complex in the Local Group, 30 Dor, is presented. Applying a new maximum entropy deconvolution algorithm to the Einstein Observatory data, reveals striking correlations among the X-ray, radio, and optical morphologies of the region, with X-ray-emitting bubbles filling cavities surrounded by H-alpha shells and coextensive diffuse X-ray and radio continuum emission from throughout the region. The total X-ray luminosity in the 0.16-3.5 keV band from an area within 160 pc of the central cluster R136 is about 2 x 10 to the 37th ergs/sec.

  14. Single photon energy dispersive x-ray diffraction.

    PubMed

    Higginbotham, Andrew; Patel, Shamim; Hawreliak, James A; Ciricosta, Orlando; Collins, Gilbert W; Coppari, Federica; Eggert, Jon H; Suggit, Matthew J; Tang, Henry; Wark, Justin S

    2014-03-01

    With the pressure range accessible to laser driven compression experiments on solid material rising rapidly, new challenges in the diagnosis of samples in harsh laser environments are emerging. When driving to TPa pressures (conditions highly relevant to planetary interiors), traditional x-ray diffraction techniques are plagued by increased sources of background and noise, as well as a potential reduction in signal. In this paper we present a new diffraction diagnostic designed to record x-ray diffraction in low signal-to-noise environments. By utilising single photon counting techniques we demonstrate the ability to record diffraction patterns on nanosecond timescales, and subsequently separate, photon-by-photon, signal from background. In doing this, we mitigate many of the issues surrounding the use of high intensity lasers to drive samples to extremes of pressure, allowing for structural information to be obtained in a regime which is currently largely unexplored.

  15. Single photon energy dispersive x-ray diffraction

    SciTech Connect

    Higginbotham, Andrew; Patel, Shamim; Ciricosta, Orlando; Suggit, Matthew J.; Wark, Justin S.; Hawreliak, James A.; Collins, Gilbert W.; Coppari, Federica; Eggert, Jon H.; Tang, Henry

    2014-03-15

    With the pressure range accessible to laser driven compression experiments on solid material rising rapidly, new challenges in the diagnosis of samples in harsh laser environments are emerging. When driving to TPa pressures (conditions highly relevant to planetary interiors), traditional x-ray diffraction techniques are plagued by increased sources of background and noise, as well as a potential reduction in signal. In this paper we present a new diffraction diagnostic designed to record x-ray diffraction in low signal-to-noise environments. By utilising single photon counting techniques we demonstrate the ability to record diffraction patterns on nanosecond timescales, and subsequently separate, photon-by-photon, signal from background. In doing this, we mitigate many of the issues surrounding the use of high intensity lasers to drive samples to extremes of pressure, allowing for structural information to be obtained in a regime which is currently largely unexplored.

  16. X-RAY ABSORPTION BY THE WARM-HOT INTERGALACTIC MEDIUM IN THE HERCULES SUPERCLUSTER

    SciTech Connect

    Ren, Bin; Fang, Taotao; Buote, David A.

    2014-02-10

    ''Missing baryons'', in the form of warm-hot intergalactic medium (WHIM), are expected to reside in cosmic filamentary structures that can be traced by signposts such as large-scale galaxy superstructures. The clear detection of an X-ray absorption line in the Sculptor Wall demonstrated the success of using galaxy superstructures as a signpost to search for the WHIM. Here we present an XMM -Newton Reflection Grating Spectrometer observation of the blazar Mkn 501, located in the Hercules Supercluster. We detected an O VII Kα absorption line at the 98.7% level (2.5σ) at the redshift of the foreground Hercules Supercluster. The derived properties of the absorber are consistent with theoretical expectations of the WHIM. We discuss the implication of our detection for the search for the ''missing baryons''. While this detection shows again that using signposts is a very effective strategy to search for the WHIM, follow-up observations are crucial both to strengthen the statistical significance of the detection and to rule out other interpretations. A local, z ∼ 0 O VII Kα absorption line was also clearly detected at the 4σ level, and we discuss its implications for our understanding of the hot gas content of our Galaxy.

  17. High-energy x-ray diffraction study of pure amorphous silicon

    SciTech Connect

    Laaziri, K.; Kycia, S.; Roorda, S.; Chicoine, M.; Robertson, J.L.; Wang, J.; Moss, S.C.

    1999-11-01

    Medium and high-energy x-ray diffraction has been used to study the atomic structure of pure amorphous Si prepared by MeV Si implantation into crystalline silicon. Both as-implanted and annealed samples were studied. The inelastically scattered x rays were removed by fitting the energy spectrum for the scattered x rays. The atomic scattering factor of silicon, previously known reliably up to 20 {Angstrom}{sup {minus}1}, has been extended to 55 {Angstrom}{sup {minus}1}. The radial distribution function of amorphous Si, before and after annealing, has been determined through an unbiased Fourier transformation of the normalized scattering data. Gaussian fits to the first neighbor peak in these functions shows that scattering data out to at least 40 {Angstrom}{sup {minus}1} is required to reliably determine the radial distribution function. The first-shell coordination number increases from 3.79 to 3.88 upon thermal annealing at 600{degree}C, whereas that of crystalline Si determined from similar measurements on a Si powder analyzed using the same technique is 4.0. Amorphous Si is therefore under coordinated relative to crystalline Si. Noise in the distribution function, caused by statistical variations in the scattering data at high-momentum transfer, has been reduced without affecting the experimental resolution through filtering of the interference function after subtracting the contribution of the first-neighbor peak. The difference induced by thermal annealing in the remainder of the radial distribution functions, thus revealed, is much smaller than previously believed. {copyright} {ital 1999} {ital The American Physical Society}

  18. A Chandra X-Ray Investigation of the Violent Interstellar Medium: From Dwarf Starbursts to Ultraluminous Infrared Galaxies

    NASA Astrophysics Data System (ADS)

    Grimes, J. P.; Heckman, T.; Strickland, D.; Ptak, A.

    2005-07-01

    We have analyzed observations with the Chandra X-Ray Observatory of the diffuse emission by hot gas in seven dwarf starburst galaxies, six edge-on starburst galaxies, and nine ultraluminous infrared galaxies. These systems cover ranges of ~104 in X-ray luminosity, and several thousand in star formation rate and K-band luminosity (a proxy for stellar mass). Despite this range in fundamental parameters, we find that the properties of the diffuse X-ray emission are very similar in all three classes of starburst galaxies. The spectrum of the diffuse emission is well fitted by thermal emission from gas with kT~0.25-0.8 keV and with several times solar abundance ratios of α-elements to Fe. The ratio of the thermal X-ray to far-infrared luminosity is roughly constant, as is the characteristic surface brightness of the diffuse X-ray emission. The size of the diffuse X-ray source increases systematically with both far-infrared and K-band luminosity. All three classes show strong morphological relationships between the regions of hot gas probed by the diffuse X-ray emission and the warm gas probed by optical line emission. These findings suggest that the same physical mechanism is producing the diffuse X-ray emission in the three types of starbursts. These results are consistent with that mechanism being shocks driven by a galactic ``superwind,'' which is powered by the kinetic energy collectively supplied by stellar winds and supernovae in the starburst.

  19. The Einstein Observatory Medium Sensitivity Survey - Optical identifications for a complete sample of X-ray sources

    NASA Technical Reports Server (NTRS)

    Stocke, J. T.; Liebert, J.; Gioia, I. M.; Maccacaro, T.; Griffiths, R. E.; Danziger, I. J.; Kunth, D.; Lub, J.

    1983-01-01

    It is suggested that virtually all the X-ray sources in the Einstein Observatory's Medium Sensitivity Survey flux range can be identified with objects visible on the POSS, on the basis of the complete identification of all sources north of -25 deg declination. There is no evidence for a significant population of 'blank field' X-ray sources at this flux level, and therefore no evidence for any new X-ray source class with very high L(x)/L(v). Most of the quasars detected in the present survey are spectroscopically similar to optical or radio-selected quasars. About 25 percent of the quasar sample, however, had reddish colors, and permitted lines dominated by a narrow-line component. These objects form a second sequence of active galactic nuclei, distinct in their optical properties from the broad line objects.

  20. High-energy x-ray backlighter spectrum measurements using calibrated image plates

    NASA Astrophysics Data System (ADS)

    Maddox, B. R.; Park, H. S.; Remington, B. A.; Izumi, N.; Chen, S.; Chen, C.; Kimminau, G.; Ali, Z.; Haugh, M. J.; Ma, Q.

    2011-02-01

    The x-ray spectrum between 18 and 88 keV generated by a petawatt laser driven x-ray backlighter target was measured using a 12-channel differential filter pair spectrometer. The spectrometer consists of a series of filter pairs on a Ta mask coupled with an x-ray sensitive image plate. A calibration of Fuji™ MS and SR image plates was conducted using a tungsten anode x-ray source and the resulting calibration applied to the design of the Ross pair spectrometer. Additionally, the fade rate and resolution of the image plate system were measured for quantitative radiographic applications. The conversion efficiency of laser energy into silver Kα x rays from a petawatt laser target was measured using the differential filter pair spectrometer and compared to measurements using a single photon counting charge coupled device.

  1. High-energy x-ray backlighter spectrum measurements using calibrated image plates

    SciTech Connect

    Maddox, B.R.; Park, H.S.; Remington, B.A.; Izumi, N.; Chen, S.; Chen, C.; Kimminau, G.; Ali, Z.; Haugh, M.J.; Ma, Q.

    2012-10-10

    The x-ray spectrum between 18 and 88 keV generated by a petawatt laser driven x-ray backlighter target was measured using a 12-channel differential filter pair spectrometer. The spectrometer consists of a series of filter pairs on a Ta mask coupled with an x-ray sensitive image plate. A calibration of Fuji{trademark} MS and SR image plates was conducted using a tungsten anode x-ray source and the resulting calibration applied to the design of the Ross pair spectrometer. Additionally, the fade rate and resolution of the image plate system were measured for quantitative radiographic applications. The conversion efficiency of laser energy into silver K{alpha} x rays from a petawatt laser target was measured using the differential filter pair spectrometer and compared to measurements using a single photon counting charge coupled device.

  2. High Energy Astronomy Observatory (HEAO)-2 in the X-Ray Calibration Facility

    NASA Technical Reports Server (NTRS)

    1977-01-01

    This photograph is of the High Energy Astronomy Observatory (HEAO)-2 telescope being evaluated by engineers in the clean room of the X-Ray Calibration Facility at the Marshall Space Flight Center (MSFC). The MSFC was heavily engaged in the technical and scientific aspects, testing and calibration, of the HEAO-2 telescope The HEAO-2 was the first imaging and largest x-ray telescope built to date. The X-Ray Calibration Facility was built in 1976 for testing MSFC's HEAO-2. The facility is the world's largest, most advanced laboratory for simulating x-ray emissions from distant celestial objects. It produced a space-like environment in which components related to x-ray telescope imaging are tested and the quality of their performance in space is predicted. The original facility contained a 1,000-foot long by 3-foot diameter vacuum tube (for the x-ray path) cornecting an x-ray generator and an instrument test chamber. Recently, the facility was upgraded to evaluate the optical elements of NASA's Hubble Space Telescope, Chandra X-Ray Observatory and Compton Gamma-Ray Observatory.

  3. The interstellar medium in the direction of the Crab Nebula - Reconciling soft X-ray and radio observations

    NASA Technical Reports Server (NTRS)

    Ride, S. K.; Walker, A. B. C., Jr.

    1977-01-01

    The total soft X-ray photoabsorption cross section of the interstellar medium (ISM) in the direction of the Crab Nebula is computed on the basis of a two-phase model of the ISM. This cross section is used to reanalyze Copernicus data on the X-ray spectrum of the Crab between 0.7 and 1.5 keV. The total hydrogen column density along the line of sight to that nebula is found to be approximately 2.6 by 10 to the 21st power H atoms/sq cm. This result is evaluated in light of the two-phase model of the ISM, and the predictions based on the X-ray data are compared with results of radio and UV observations. A discrepancy between the radio and X-ray measurements of the hydrogen column density is resolved by noting that 21-cm absorption measurements sample only the neutral hydrogen in clouds while X-ray measurements are sensitive to all forms of hydrogen in both cloud and intercloud regions. It is suggested that roughly 50% of the hydrogen in the direction of the Crab Nebula is in clouds and that 85% of this hydrogen is neutral and atomic.

  4. High energy X-ray phase and dark-field imaging using a random absorption mask.

    PubMed

    Wang, Hongchang; Kashyap, Yogesh; Cai, Biao; Sawhney, Kawal

    2016-01-01

    High energy X-ray imaging has unique advantage over conventional X-ray imaging, since it enables higher penetration into materials with significantly reduced radiation damage. However, the absorption contrast in high energy region is considerably low due to the reduced X-ray absorption cross section for most materials. Even though the X-ray phase and dark-field imaging techniques can provide substantially increased contrast and complementary information, fabricating dedicated optics for high energies still remain a challenge. To address this issue, we present an alternative X-ray imaging approach to produce transmission, phase and scattering signals at high X-ray energies by using a random absorption mask. Importantly, in addition to the synchrotron radiation source, this approach has been demonstrated for practical imaging application with a laboratory-based microfocus X-ray source. This new imaging method could be potentially useful for studying thick samples or heavy materials for advanced research in materials science. PMID:27466217

  5. High energy X-ray phase and dark-field imaging using a random absorption mask

    PubMed Central

    Wang, Hongchang; Kashyap, Yogesh; Cai, Biao; Sawhney, Kawal

    2016-01-01

    High energy X-ray imaging has unique advantage over conventional X-ray imaging, since it enables higher penetration into materials with significantly reduced radiation damage. However, the absorption contrast in high energy region is considerably low due to the reduced X-ray absorption cross section for most materials. Even though the X-ray phase and dark-field imaging techniques can provide substantially increased contrast and complementary information, fabricating dedicated optics for high energies still remain a challenge. To address this issue, we present an alternative X-ray imaging approach to produce transmission, phase and scattering signals at high X-ray energies by using a random absorption mask. Importantly, in addition to the synchrotron radiation source, this approach has been demonstrated for practical imaging application with a laboratory-based microfocus X-ray source. This new imaging method could be potentially useful for studying thick samples or heavy materials for advanced research in materials science. PMID:27466217

  6. Artifacts in energy dispersive x-ray spectrometry in the scanning electron microscope (II).

    PubMed

    Fiori, C E; Newbury, D E

    1980-01-01

    The quality of x-ray spectra obtained with an energy dispersive x-ray spectrometer on an electron beam instrument can be severely compromised by the presence of electromagnetic interference. Sources of electromagnetic interference include ground currents and signals generated by time-varying currents in instrument components such as scan coils. Spectrometer resolution can be degraded by the accumulation of ice and vaccum oil on critical components of the device. Operation at high electron energy can cause artifacts in spectra due to direct entry of electrons and spurious x-rays into the detector. Processing high energy photons (above 40 keV) can lead to detector saturation effects which degrade resolution and affect dead time correction. Transmission of high energy x-rays through the detector accompanied by Compton scattering can lead to a distortion of the low energy portion of the spectrum.

  7. Artifacts in energy dispersive x-ray spectrometry in the scanning electron microscope (II).

    PubMed

    Fiori, C E; Newbury, D E

    1980-01-01

    The quality of x-ray spectra obtained with an energy dispersive x-ray spectrometer on an electron beam instrument can be severely compromised by the presence of electromagnetic interference. Sources of electromagnetic interference include ground currents and signals generated by time-varying currents in instrument components such as scan coils. Spectrometer resolution can be degraded by the accumulation of ice and vaccum oil on critical components of the device. Operation at high electron energy can cause artifacts in spectra due to direct entry of electrons and spurious x-rays into the detector. Processing high energy photons (above 40 keV) can lead to detector saturation effects which degrade resolution and affect dead time correction. Transmission of high energy x-rays through the detector accompanied by Compton scattering can lead to a distortion of the low energy portion of the spectrum. PMID:7423119

  8. X-ray reflectivity measurements of surface roughness using energy dispersive detection

    SciTech Connect

    Chason, E.; Warwick, D.T.

    1990-01-01

    We describe a new technique for measuring x-ray reflectivity using energy dispersive x-ray detection. The benefits of this method are the use of a fixed scattering angle and parallel detection of all energies simultaneously. These advantages make the technique more readily useable with laboratory x-ray sources and more compatible with growth chambers. We find excellent agreement between the calculated Fresnel reflectivity and the reflectivity obtained from a smooth Ge (001) surface. Reflectivities obtained during 500 eV Xe ion bombardment of Ge surfaces demonstrate the sensitivity of the technique to be better than 1 {angstrom}. 9 refs., 4 figs.

  9. Energy-dependent Orbital Modulation of X-rays and Constraints on Emission of the Jet in Cyg X-3

    NASA Technical Reports Server (NTRS)

    Zdziarski, Andrzej A.; Maitra, Chandreyee; Frankowski, Adam; Skinner, Gerald K.; Misra, Ranjeev

    2012-01-01

    We study orbital modulation of X-rays from Cyg X-3, using data from Swift, INTEGRAL and RXTE. Using the wealth of the presently available data and an improved averaging method, we obtain energy-dependent folded and averaged light curves with unprecedented accuracy. We find that above 5 keV, the modulation depth decreases with the increasing energy, which is consistent with the modulation being caused by both bound-free absorption and Compton scattering in the stellar wind of the donor, with minima corresponding to the highest optical depth, which occurs around the superior conjunction. We find a decrease of the depth below 3 keV, which appears to be due to re-emission of the absorbed continuum by the wind in soft X-ray lines. Based on the shape of the folded light curves, any X-ray contribution from the jet in Cyg X-3, which emits ?-rays detected at energies > 0.1 GeV in soft spectral states, is found to be minor up to 100 keV. This implies the presence of a rather sharp low-energy break in the jet MeV-range spectrum.We also calculate phase-resolved RXTE X-ray spectra, and show the difference between the spectra corresponding to phases around the superior and inferior conjunctions can indeed be accounted for by a combined effect of bound-free absorption in an ionized medium and Compton scattering.

  10. X-Ray Photoelectron Spectroscopy and the Role of Relaxation Energy in Understanding Chemical Shifts

    ERIC Educational Resources Information Center

    Ellison, Frank O.; White, Michael G.

    1976-01-01

    Discusses the measurement of electrons ejected from a system which is being irradiated with X-rays or ultraviolet photons, and a theoretical model for calculating core-electron ionization energies. (MLH)

  11. Instantaneous x-ray radiation energy from laser produced polystyrene plasmas for shock ignition conditions

    SciTech Connect

    Shang, Wanli; Wei, Huiyue; Li, Zhichao; Yi, Rongqing; Zhu, Tuo; Song, Tianmin; Huang, Chengwu; Yang, Jiamin

    2013-10-15

    Laser target energy coupling mechanism is crucial in the shock ignition (SI) scheme, and x-ray radiation energy is a non-negligible portion of the laser produced plasma energy. To evaluate the x-ray radiation energy amount at conditions relevant to SI scheme, instantaneous x-ray radiation energy is investigated experimentally with continuum phase plates smoothed lasers irradiating layer polystyrene targets. Comparative laser pulses without and with shock spike are employed. With the measured x-ray angular distribution, full space x-ray radiation energy and conversion efficiency are observed. Instantaneous scaling law of x-ray conversion efficiency is obtained as a function of laser intensity and time. It should be pointed out that the scaling law is available for any laser pulse shape and intensity, with which irradiates polystyrene planar target with intensity from 2 × 10{sup 14} to 1.8 × 10{sup 15} W/cm{sup 2}. Numerical analysis of the laser energy transformation is performed, and the simulation results agree with the experimental data.

  12. Fat to muscle ratio measurements with dual energy x-ray absorbtiometry

    DOE PAGESBeta

    Chen, A.; Luo, J.; Wang, A.; Broadbent, C.; Zhong, J.; Dilmanian, F. A.; Zafonte, F.; Zhong, Z.

    2015-03-14

    Accurate measurement of the fat-to-muscle ratio in animal model is important for obesity research. In addition, an efficient way to measure the fat to muscle ratio in animal model using dual-energy absorptiometry is presented in this paper. A radioactive source exciting x-ray fluorescence from a target material is used to provide the two x-ray energies needed. The x-rays, after transmitting through the sample, are measured with an energy-sensitive Ge detector. Phantoms and specimens were measured. The results showed that the method was sensitive to the fat to muscle ratios with good linearity. A standard deviation of a few percent inmore » the fat to muscle ratio could be observed with the x-ray dose of 0.001 mGy.« less

  13. Fat to muscle ratio measurements with dual energy x-ray absorbtiometry

    SciTech Connect

    Chen, A.; Luo, J.; Wang, A.; Broadbent, C.; Zhong, J.; Dilmanian, F. A.; Zafonte, F.; Zhong, Z.

    2015-03-14

    Accurate measurement of the fat-to-muscle ratio in animal model is important for obesity research. In addition, an efficient way to measure the fat to muscle ratio in animal model using dual-energy absorptiometry is presented in this paper. A radioactive source exciting x-ray fluorescence from a target material is used to provide the two x-ray energies needed. The x-rays, after transmitting through the sample, are measured with an energy-sensitive Ge detector. Phantoms and specimens were measured. The results showed that the method was sensitive to the fat to muscle ratios with good linearity. A standard deviation of a few percent in the fat to muscle ratio could be observed with the x-ray dose of 0.001 mGy.

  14. Fat to muscle ratio measurements with dual energy x-ray absorbtiometry

    NASA Astrophysics Data System (ADS)

    Chen, A.; Luo, J.; Wang, A.; Broadbent, C.; Zhong, J.; Dilmanian, F. A.; Zafonte, F.; Zhong, Z.

    2015-07-01

    Accurate measurement of the fat-to-muscle ratio in animal model is important for obesity research. An efficient way to measure the fat to muscle ratio in animal model using dual-energy absorptiometry is presented in this paper. A radioactive source exciting x-ray fluorescence from a target material is used to provide the two x-ray energies needed. The x-rays, after transmitting through the sample, are measured with an energy-sensitive Ge detector. Phantoms and specimens were measured. The results showed that the method was sensitive to the fat to muscle ratios with good linearity. A standard deviation of a few percent in the fat to muscle ratio could be observed with the x-ray dose of 0.001 mGy.

  15. Energy response calibration of photon-counting detectors using X-ray fluorescence: a feasibility study

    PubMed Central

    Cho, H-M; Ding, H; Ziemer, BP; Molloi, S

    2014-01-01

    Accurate energy calibration is critical for the application of energy-resolved photon-counting detectors in spectral imaging. The aim of this study is to investigate the feasibility of energy response calibration and characterization of a photon-counting detector using X-ray fluorescence. A comprehensive Monte Carlo simulation study was performed using Geant4 Application for Tomographic Emission (GATE) to investigate the optimal technique for X-ray fluorescence calibration. Simulations were conducted using a 100 kVp tungsten-anode spectra with 2.7 mm Al filter for a single pixel cadmium telluride (CdTe) detector with 3 × 3 mm2 in detection area. The angular dependence of X-ray fluorescence and scatter background was investigated by varying the detection angle from 20° to 170° with respect to the beam direction. The effects of the detector material, shape, and size on the recorded X-ray fluorescence were investigated. The fluorescent material size effect was considered with and without the container for the fluorescent material. In order to provide validation for the simulation result, the angular dependence of X-ray fluorescence from five fluorescent materials was experimentally measured using a spectrometer. Finally, eleven of the fluorescent materials were used for energy calibration of a CZT-based photon-counting detector. The optimal detection angle was determined to be approximately at 120° with respect to the beam direction, which showed the highest fluorescence to scatter ratio (FSR) with a weak dependence on the fluorescent material size. The feasibility of X-ray fluorescence for energy calibration of photon-counting detectors in the diagnostic X-ray energy range was verified by successfully calibrating the energy response of a CZT-based photon-counting detector. The results of this study can be used as a guideline to implement the X-ray fluorescence calibration method for photon-counting detectors in a typical imaging laboratory. PMID:25369288

  16. Energy response calibration of photon-counting detectors using x-ray fluorescence: a feasibility study.

    PubMed

    Cho, H-M; Ding, H; Ziemer, B P; Molloi, S

    2014-12-01

    Accurate energy calibration is critical for the application of energy-resolved photon-counting detectors in spectral imaging. The aim of this study is to investigate the feasibility of energy response calibration and characterization of a photon-counting detector using x-ray fluorescence. A comprehensive Monte Carlo simulation study was performed using Geant4 Application for Tomographic Emission (GATE) to investigate the optimal technique for x-ray fluorescence calibration. Simulations were conducted using a 100 kVp tungsten-anode spectra with 2.7 mm Al filter for a single pixel cadmium telluride (CdTe) detector with 3 × 3 mm(2) in detection area. The angular dependence of x-ray fluorescence and scatter background was investigated by varying the detection angle from 20° to 170° with respect to the beam direction. The effects of the detector material, shape, and size on the recorded x-ray fluorescence were investigated. The fluorescent material size effect was considered with and without the container for the fluorescent material. In order to provide validation for the simulation result, the angular dependence of x-ray fluorescence from five fluorescent materials was experimentally measured using a spectrometer. Finally, eleven of the fluorescent materials were used for energy calibration of a CZT-based photon-counting detector. The optimal detection angle was determined to be approximately at 120° with respect to the beam direction, which showed the highest fluorescence to scatter ratio (FSR) with a weak dependence on the fluorescent material size. The feasibility of x-ray fluorescence for energy calibration of photon-counting detectors in the diagnostic x-ray energy range was verified by successfully calibrating the energy response of a CZT-based photon-counting detector. The results of this study can be used as a guideline to implement the x-ray fluorescence calibration method for photon-counting detectors in a typical imaging laboratory.

  17. Energy Dependence of Synchrotron X-Ray Rims in Tycho's Supernova Remnant

    NASA Technical Reports Server (NTRS)

    Tran, Aaron; Williams, Brian J.; Petre, Robert; Ressler, Sean M.; Reynolds, Stephen P.

    2015-01-01

    Several young supernova remnants exhibit thin X-ray bright rims of synchrotron radiation at their forward shocks. Thin rims require strong magnetic field amplification beyond simple shock compression if rim widths are only limited by electron energy losses. But, magnetic field damping behind the shock could produce similarly thin rims with less extreme field amplification. Variation of rim width with energy may thus discriminate between competing influences on rim widths. We measured rim widths around Tycho's supernova remnant in 5 energy bands using an archival 750 ks Chandra observation. Rims narrow with increasing energy and are well described by either loss-limited or damped scenarios, so X-ray rim width-energy dependence does not uniquely specify a model. But, radio counterparts to thin rims are not loss-limited and better reflect magnetic field structure. Joint radio and X-ray modeling favors magnetic damping in Tycho's SNR with damping lengths approximately 1-5% of remnant radius and magnetic field strengths approximately 50-400 micron G assuming Bohm diffusion. X-ray rim widths are approximately 1% of remnant radius, somewhat smaller than inferred damping lengths. Electron energy losses are important in all models of X-ray rims, suggesting that the distinction between loss-limited and damped models is blurred in soft X-rays. All loss-limited and damping models require magnetic fields approximately greater than 20 micron G, arming the necessity of magnetic field amplification beyond simple compression.

  18. ENERGY DEPENDENCE OF SYNCHROTRON X-RAY RIMS IN TYCHO’S SUPERNOVA REMNANT

    SciTech Connect

    Tran, Aaron; Williams, Brian J.; Petre, Robert; Reynolds, Stephen P.

    2015-10-20

    Several young supernova remnants (SNRs) exhibit thin X-ray bright rims of synchrotron radiation at their forward shocks. Thin rims require strong magnetic field amplification beyond simple shock compression if rim widths are only limited by electron energy losses. But, magnetic field damping behind the shock could produce similarly thin rims with less extreme field amplification. Variation of rim width with energy may thus discriminate between competing influences on rim widths. We measured rim widths around Tycho's SNR in five energy bands using an archival 750 ks Chandra observation. Rims narrow with increasing energy and are well described by either loss-limited or damped scenarios, so X-ray rim width-energy dependence does not uniquely specify a model. But, radio counterparts to thin rims are not loss-limited and better reflect magnetic field structure. Joint radio and X-ray modeling favors magnetic damping in Tycho's SNR with damping lengths ∼1%–5% of remnant radius and magnetic field strengths ∼50–400 μG assuming Bohm diffusion. X-ray rim widths are ∼1% of remnant radius, somewhat smaller than inferred damping lengths. Electron energy losses are important in all models of X-ray rims, suggesting that the distinction between loss-limited and damped models is blurred in soft X-rays. All loss-limited and damping models require magnetic fields ≳20 μG, affirming the necessity of magnetic field amplification beyond simple compression.

  19. Calibration of an imaging crystal spectrometer for low x-ray energies

    SciTech Connect

    Lee, S. G.; Bak, J. G.; Bitter, M.

    2008-01-15

    An x-ray imaging crystal spectrometer was designed for the Hanbit magnetic mirror device to observe spectra of heliumlike neon at 13.4474 A. The spectrometer consists of a spherically bent mica crystal and an x-ray sensitive vacuum charge coupled device camera. This spectrometer can provide spatially resolved spectra, making it possible to obtain profiles of the ion charge state distribution from line ratios and profiles of the plasma rotation velocity from Doppler shift measurements. The paper describes measurements of spectral resolution of this instrument for low x-ray energies.

  20. Interferometric phase-contrast X-ray CT imaging of VX2 rabbit cancer at 35keV X-ray energy

    NASA Astrophysics Data System (ADS)

    Takeda, Tohoru; Wu, Jin; Tsuchiya, Yoshinori; Yoneyama, Akio; Lwin, Thet-Thet; Hyodo, Kazuyuki; Itai, Yuji

    2004-05-01

    Imaging of large objects at 17.7-keV low x-ray energy causes huge x-ray exposure to the objects even using interferometric phase-contrast x-ray CT (PCCT). Thus, we tried to obtain PCCT images at high x-ray energy of 35keV and examined the image quality using a formalin-fixed VX2 rabbit cancer specimen with 15-mm in diameter. The PCCT system consisted of an asymmetrically cut silicon (220) crystal, a monolithic x-ray interferometer, a phase-shifter, an object cell and an x-ray CCD camera. The PCCT at 35 keV clearly visualized various inner structures of VX2 rabbit cancer such as necrosis, cancer, the surrounding tumor vessels, and normal liver tissue. Besides, image-contrast was not degraded significantly. These results suggest that the PCCT at 35 KeV is sufficient to clearly depict the histopathological morphology of VX2 rabbit cancer specimen.

  1. Understanding Electrocatalytic Pathways in Low and Medium Temperature Fuel Cells: Synchrotron-based In Situ X-Ray Absorption Spectroscopy

    SciTech Connect

    Mukerjee, S.; Ziegelbauer, J; Arruda, T; Ramaker, D; Shyam, B

    2008-01-01

    Over the last few decades, researchers have made significant developments in producing more advanced electrocatalytic materials for power generation applications. For example, traditional fuel cell catalysts often involve high-priced precious metals such as Pt. However, in order for fuel cells to become commercially viable, there is a need to reduce or completely remove precious metal altogether. As a result, a myriad of novel, unconventional materials have been explored such as chalcogenides, porphyrins, and organic-metal-macrocycles for low/medium temperature fuel cells as well as enzymatic and microbial fuel cells. As these materials increasingly become more complex, researchers often find themselves in search of new characterization methods, especially those which are allow in situ and operando measurements with element specificity. One such method that has received much attention for analysis of electrocatalytic materials is X-ray absorption spectroscopy (XAS). XAS is an element specific, core level absorption technique which yields structural and electronic information. As a core electron method, XAS requires an extremely bright source, hence a synchrotron. The resulting intensity of synchrotron radiation allow for experiments to be conducted in situ, under electrochemically relevant conditions. Although a bulk-averaging technique requiring rigorous mathematical manipulation, XAS has the added benefit that it can probe materials which possess no long range order. This makes it ideal to characterize nano-scale electrocatalysts. XAS experiments are conducted by ramping the X-ray photon energy while measuring absorption of the incident beam the sample or by counting fluorescent photons released from a sample due to subsequent relaxation. Absorption mode XAS follows the Beer-Lambert Law, {mu}x = log(I{sub 0}/I{sub t}) (1) where {mu} is the absorption coefficient, x is the sample thickness and I{sub 0} and I{sub t} are the intensities of the incident and

  2. Low-energy x-ray irradiation for electrophysiological studies

    SciTech Connect

    Schauer, D.A.; Zeman, G.H.; Pellmar, T.C.

    1989-01-01

    High-dose-rate acute whole-body exposures have been the main focus of radiobiology research conducted at the Armed Forces Radiobiology Research Institute (AFRRI) for many years. Extensive quantitative studies have been conducted analyzing behavioral effects, radiation-induced syndromes, and combined injury phenomena. Tolliver and Pellmar initiated a study to evaluate radiation damage to brain neurophysiology. A 50-kVp molybdenum target/filter x-ray tube was installed inside a lead-shielded Faraday cage. High-dose rates of up to 1.54 Gy/min (17.4-keV weighted average photons) were used to conduct local in vitro irradiations of the hippocampal region of guinea pig brains. Electrophysiological recordings of subtle changes in neuronal activity indicate this system is suitable for this application.

  3. Bone mineral measurement using dual energy x ray densitometry

    NASA Technical Reports Server (NTRS)

    Smith, Steven W.

    1989-01-01

    Bone mineral measurements before and after space missions have shown that weightlessness greatly accelerates bone demineralization. Bone mineral losses as high as 1 to 3 percent per month were reported. Highly precise instrumentation is required to monitor this loss and thereby test the efficacy of treatment. During the last year, a significant improvement was made in Dual-Photon Absorptiometry by replacing the radioactive source with an x ray tube. Advantages of this system include: better precision, lower patient dose, better spacial resolution, and shorter scan times. The high precision and low radiation dose of this technique will allow detection of bone mineral changes of less than 1 percent with measurements conducted directly at the sites of interest. This will allow the required bone mineral studies to be completed in a shorter time with greater confidence.

  4. Investigation of TLD-700 energy response to low energy x-ray encountered in diagnostic radiology

    NASA Astrophysics Data System (ADS)

    Herrati, Ammar; Bourouina, Mourad; Khalal-Kouache, Karima

    2016-05-01

    The aim of thiswork is to study the energy dependence of thermoluminescent dosimeter (TLD-700) for low energy X-ray beams encountered in conventional diagnostic radiology. In the first step, we studied some characteristics (reproducibility and linearity) of TLD-700 chips using a 137Cs source, and selected TLD chips with reproducibility better than 2.5%. Then we determined TLD-700 energy response for diagnostic radiology X-ray qualities, and investigated its influence on air kerma estimate. A maximum deviation of 60% can be obtained if TLDs are calibrated for 137Cs radiation source and used in diagnostic radiology fields. However, this deviation became less than 20% if TLDs chips are calibrated for the reference x-ray radiation quality RQR5 (recommended by the IEC 61267 standard). Consequently, we recommend calibrating this kind of TLDdetector with RQR5 diagnostic radiology X-ray quality. This method permits to obtain a good accuracy when assessing the entrance dose in diagnostic radiology procedures.

  5. CdZnTe x-ray detector for 30 {endash} 100 keV energy

    SciTech Connect

    Yoo, S.-S.; Rodricks, B.; Shastri, S.D.; Montano, P.A.

    1996-07-01

    High-pressure-Bridgman (HPB) grown CdZnTe x-ray detectors 1.25-1.7 mm thick were tested using monochromatic x-rays of 30 to 100 keV generated by a high energy x-ray generator. The results were compared with a commercially available 5 cm thick NaI detector. A linear dependence of the counting rate versus the x-ray generator tube current was observed at 58.9 keV. The measured pulse height of the photopeaks shows a linear dependence on energy. Electron and hole mobility-lifetime products ({mu}{tau}) were deduced by fitting bias dependent photopeak channel numbers at 30 keV x-ray energy. Values of 2 x 10{sup -3} cm{sup 2}/V and 2 x 10{sup -4}cm{sup 2}/V were obtained for {mu}{tau}{sub e} and {mu}{tau}{sub p}, respectively. The detector efficiency of CdZnTe at a 100 V bias was as high as, or higher than 90 % compared to a NaI detector. At x-ray energies higher than 70 keV, the detection efficiency becomes a dominant factor and decreases to 75 % at 100 keV.

  6. Thermal expansion in UO2 determined by high-energy X-ray diffraction

    NASA Astrophysics Data System (ADS)

    Guthrie, M.; Benmore, C. J.; Skinner, L. B.; Alderman, O. L. G.; Weber, J. K. R.; Parise, J. B.; Williamson, M.

    2016-10-01

    Here we present crystallographic analyses of high-energy X-ray diffraction data on polycrystalline UO2 up to the melting temperature. The Rietveld refinements of our X-ray data are in agreement with previous measurements, but are systematically located around the upper bound of their uncertainty, indicating a slightly steeper trend of thermal expansion compared to established values. This observation is consistent with recent first principles calculations.

  7. Novel X-ray imaging diagnostics of high energy nanosecond pulse accelerators.

    SciTech Connect

    Smith, Graham W.; Gallegos, Roque Rosauro; Hohlfelder, Robert James; Beutler, David Eric; Dudley, John; Seymour, Calvin L. G.; Bell, John D.

    2004-08-01

    Pioneering x-ray imaging has been undertaken on a number of AWE's and Sandia National Laboratories radiation effects x-ray simulators. These simulators typically yield a single very short (<50ns) pulse of high-energy (MeV endpoint energy bremsstrahlung) x-ray radiation with doses in the kilorad (krad(Si)) region. X-ray source targets vary in size from 2 to 25cm diameter, dependent upon the particular simulator. Electronic imaging of the source x-ray emission under dynamic conditions yields valuable information upon how the simulator is performing. The resultant images are of interest to the simulator designer who may configure new x-ray source converter targets and diode designs. The images can provide quantitative information about machine performance during radiation effects testing of components under active conditions. The effects testing program is a valuable interface for validation of high performance computer codes and models for the radiation effects community. A novel high-energy x-ray imaging spectrometer is described whereby the spectral energy (0.1 to 2.5MeV) profile may be discerned from the digitally recorded and viewable images via a pinhole/scintillator/CCD imaging system and knowledge of the filtration parameters. Unique images, analysis and a preliminary evaluation of the capability of the spectrometer are presented. Further, a novel time resolved imaging system is described that captures a sequence of high spatial resolution temporal images, with zero interframe time, in the nanosecond timeframe, of our source x-rays.

  8. Energy dispersive X-ray analysis on an absolute scale in scanning transmission electron microscopy.

    PubMed

    Chen, Z; D'Alfonso, A J; Weyland, M; Taplin, D J; Allen, L J; Findlay, S D

    2015-10-01

    We demonstrate absolute scale agreement between the number of X-ray counts in energy dispersive X-ray spectroscopy using an atomic-scale coherent electron probe and first-principles simulations. Scan-averaged spectra were collected across a range of thicknesses with precisely determined and controlled microscope parameters. Ionization cross-sections were calculated using the quantum excitation of phonons model, incorporating dynamical (multiple) electron scattering, which is seen to be important even for very thin specimens.

  9. The role of x-ray Swank factor in energy-resolving photon-counting imaging

    SciTech Connect

    Tanguay, Jesse; Kim, Ho Kyung; Cunningham, Ian. A.

    2010-12-15

    Purpose: Energy-resolved x-ray imaging has the potential to improve contrast-to-noise ratio by measuring the energy of each interacting photon and applying optimal weighting factors. The success of energy-resolving photon-counting (EPC) detectors relies on the ability of an x-ray detector to accurately measure the energy of each interacting photon. However, the escape of characteristic emissions and Compton scatter degrades spectral information. This article makes the theoretical connection between accuracy and imprecision in energy measurements with the x-ray Swank factor for a-Se, Si, CdZnTe, and HgI{sub 2}-based detectors. Methods: For a detector that implements adaptive binning to sum all elements in which x-ray energy is deposited for a single interaction, energy imprecision is shown to depend on the Swank factor for a large element with x rays incident at the center. The response function for each converter material is determined using Monte Carlo methods and used to determine energy accuracy, Swank factor, and relative energy imprecision in photon-energy measurements. Results: For each material, at energies below the respective K edges, accuracy is close to unity and imprecision is only a few percent. Above the K-edge energies, characteristic emission results in a drop in accuracy and precision that depends on escape probability. In Si, and to some extent a-Se, Compton-scatter escape also degrades energy precision with increasing energy. The influence of converter thickness on energy accuracy and imprecision is modest for low-Z materials but becomes important when using high-Z materials at energies greater than the K-edge energies. Conclusions: Accuracy and precision in energy measurements by EPC detectors are determined largely by the energy-dependent x-ray Swank factor. Modest decreases in the Swank factor (5%-15%) result in large increases in relative imprecision (30%-40%).

  10. FEEDBACK FROM HIGH-MASS X-RAY BINARIES ON THE HIGH-REDSHIFT INTERGALACTIC MEDIUM: MODEL SPECTRA

    SciTech Connect

    Power, Chris; James, Gillian; Wynn, Graham; Combet, Celine

    2013-02-10

    Massive stars at redshifts z {approx}> 6 are predicted to have played a pivotal role in cosmological reionization as luminous sources of ultraviolet (UV) photons. However, the remnants of these massive stars could be equally important as X-ray-luminous (L{sub X} {approx} 10{sup 38} erg s{sup -1}) high-mass X-ray binaries (HMXBs). Because the absorption cross section of neutral hydrogen decreases sharply with photon energy ({sigma}{proportional_to}E {sup -3}), X-rays can escape more freely than UV photons from the star-forming regions in which they are produced, allowing HMXBs to make a potentially significant contribution to the ionizing X-ray background during reionization. In this paper, we explore the ionizing power of HMXBs at redshifts z {approx}> 6 using a Monte Carlo model for a coeval stellar population of main-sequence stars and HMXBs. Using the archetypal Galactic HMXB Cygnus X-1 as our template, we propose a composite HMXB spectral energy distribution consisting of blackbody and power-law components, whose contributions depend on the accretion state of the system. We determine the time-dependent ionizing power of a combined population of UV-luminous stars and X-ray-luminous HMXBs and deduce fitting formulae for the boost in the population's ionizing power arising from HMXBs; these fits allow for simple implementation of HMXB feedback in numerical simulations. Based on this analysis, we estimate the contribution of high-redshift HMXBs to the present-day soft X-ray background, and we show that it is a factor of {approx}100-1000 smaller than the observed limit. Finally, we discuss the implications of our results for the role of HMXBs in reionization and in high-redshift galaxy formation.

  11. High energy x-ray imager for inertial confinement fusion at the National Ignition Facility

    NASA Astrophysics Data System (ADS)

    Tommasini, Riccardo; Koch, Jeffrey A.; Young, Bruce; Ng, Ed; Phillips, Tom; Dauffy, Lucile

    2006-10-01

    X-ray imaging is a fundamental diagnostic tool for inertial confinement fusion (ICF) research and provides data on the size and the shape of the core in implosions. We report on the feasibility and performance analyses of an ignition x-ray imager to be used on cryogenic deuterium-tritium implosions at the National Ignition Facility. The system is intended to provide time-integrated, broadband, moderate-energy x-ray core images of imploding inertial confinement fusion capsules. It is optimized with respect to spatial-resolution, signal-to-background, and signal-to-noise ratios, taking into account the extreme operating conditions expected at NIF due to high expected neutrons yields, gamma rays, and x rays from laser-plasma interactions.

  12. A High Energy X-ray Imager for Inertial Confinement Fusion at the National Ignition Facility

    SciTech Connect

    Tommasini, R; Koch, J A; Young, B; Ng, E; Phillips, T; Dauffy, L

    2006-05-03

    X-ray imaging is a fundamental diagnostic tool for inertial confinement fusion (ICF) research, and provides data on the size and the shape of the core in implosions. We report on the feasibility and performance analysis of an ignition x-ray imager to be used on cryogenic DT implosions at the National Ignition Facility. The system is intended to provide time-integrated, broadband, moderate-energy x-ray core images of imploding ICF capsules. It is optimized with respect to spatial-resolution, signal-to-background and signal-to-noise ratios, taking into account the extreme operating conditions expected at NIF due to high expected neutrons yields, gamma-rays, and x-rays from laser-plasma interactions.

  13. High-Energy X-ray Absorption Diagnostics as an Experimental Combustion Technique

    NASA Astrophysics Data System (ADS)

    Dunnmon, Jared; Sobhani, Sadaf; Hinshaw, Waldo; Fahrig, Rebecca; Ihme, Matthias

    2015-11-01

    X-ray diagnostics such as X-ray Computed Tomography (XCT) have recently been utilized for measurement of scalar concentration fields in gas-phase flow phenomena. In this study, we apply high-energy X-ray absorption techniques to visualize a laboratory-scale flame via fluoroscopic measurements by using krypton as a radiodense tracer media. Advantages of X-ray absorption diagnostics in a combustion context, including application to optically inaccessible environments and lack of ambient photon interference, are demonstrated. Analysis methods and metrics for extracting physical insights from these data are presented. The accuracy of the diagnostic is assessed via comparison to known results from canonical flame configurations, and the potential for further applications is discussed. Support from the NDSEG fellowship, Bosch, and NASA are gratefully acknolwedged.

  14. Material depth reconstruction method of multi-energy X-ray images using neural network.

    PubMed

    Lee, Woo-Jin; Kim, Dae-Seung; Kang, Sung-Won; Yi, Won-Jin

    2012-01-01

    With the advent of technology, multi-energy X-ray imaging is promising technique that can reduce the patient's dose and provide functional imaging. Two-dimensional photon-counting detector to provide multi-energy imaging is under development. In this work, we present a material decomposition method using multi-energy images. To acquire multi-energy images, Monte Carlo simulation was performed. The X-ray spectrum was modeled and ripple effect was considered. Using the dissimilar characteristics in energy-dependent X-ray attenuation of each material, multiple energy X-ray images were decomposed into material depth images. Feedforward neural network was used to fit multi-energy images to material depth images. In order to use the neural network, step wedge phantom images were used for training neuron. Finally, neural network decomposed multi-energy X-ray images into material depth image. To demonstrate the concept of this method, we applied it to simulated images of a 3D head phantom. The results show that neural network method performed effectively material depth reconstruction.

  15. Calculating the X-Ray Fluorescence from the Planet Mercury Due to High-Energy Electrons

    NASA Technical Reports Server (NTRS)

    Burbine, T. H.; Trombka, J. I.; Bergstrom, P. M., Jr.; Christon, S. P.

    2005-01-01

    The least-studied terrestrial planet is Mercury due to its proximity to the Sun, which makes telescopic observations and spacecraft encounters difficult. Our lack of knowledge about Mercury should change in the near future due to the recent launching of MESSENGER, a Mercury orbiter. Another mission (BepiColombo) is currently being planned. The x-ray spectrometer on MESSENGER (and planned for BepiColombo) can characterize the elemental composition of a planetary surface by measuring emitted fluorescent x-rays. If electrons are ejected from an atom s inner shell by interaction with energetic particles such as photons, electrons, or ions, electrons from an outer shell can transfer to the inner shell. Characteristic x-rays are then emitted with energies that are the difference between the binding energy of the ion in its excited state and that of the ion in its ground state. Because each element has a unique set of energy levels, each element emits x-rays at a unique set of energies. Electrons and ions usually do not have the needed flux at high energies to cause significant x-ray fluorescence on most planetary bodies. This is not the case for Mercury where high-energy particles were detected during the Mariner 10 flybys. Mercury has an intrinsic magnetic field that deflects the solar wind, resulting in a bow shock in the solar wind and a magnetospheric cavity. Electrons and ions accelerated in the magnetosphere tend to follow its magnetic field lines and can impact the surface on Mercury s dark side Modeling has been done to determine if x-ray fluorescence resulting from the impact of high-energy electrons accelerated in Mercury's magnetosphere can be detected by MESSENGER. Our goal is to understand how much bulk chemical information can be obtained from x-ray fluorescence measurements on the dark side of Mercury.

  16. Absolute measurements of x-ray backlighter sources at energies above 10 keV

    SciTech Connect

    Maddox, B. R.; Park, H. S.; Remington, B. A.; Chen, C.; Chen, S.; Prisbrey, S. T.; Comley, A.; Back, C. A.; Szabo, C.; Seely, J. F.; Feldman, U.; Hudson, L. T.; Seltzer, S.; Haugh, M. J.; Ali, Z.

    2011-05-15

    Line emission and broadband x-ray sources with x-ray energies above 10 keV have been investigated using a range of calibrated x-ray detectors for use as x-ray backlighters in high energy density (HED) experiments. The conversion efficiency of short- and long-pulse driven Mo and Ag line-emission backlighters at 17 and 22 keV was measured to investigate the crossover region between short- and long-pulse conversion efficiency. It was found that significant 17 and 22 keV line emissions were observed using a 3 {omega}, 1 ns long-pulse drive for Mo and Ag targets and a comparison between the measured Mo x-ray spectrum and calculations using an atomic physics code suggests that the line emission is due to thermal emission from N-like Mo atoms. Electron temperatures derived from fits to the continuum region of the x-ray spectra agree well with the T{sub hot} scaling as 100x(I{lambda}{sup 2}){sup 1/3}. The continuum emissions from empty and 1 atm Kr-filled imploded CH shell targets were also measured for the use as broadband backlighters.

  17. Red and Dead Supergiants: what X-ray and radio observations of type IIP supernovae reveal about the interaction of shocks with the medium the star explodes in

    NASA Astrophysics Data System (ADS)

    Ray, Alak; Chakraborti, Sayan

    2015-08-01

    X-ray and radio emission from a class of supernovae that forms almost half of all core collapse supernovae, type II Plateau SNe (SNIIP) probe the interaction of the SN shock with the medium the parent star exploded in. We have carried out observations of a number of SN IIP with Chandra, EVLA and GMRT telescopes. Our Chandra observations of SN 2013ej and SN 2004dj measured the separate contributions of thermal emission from the SN shocks and the power-law nonthermal part arising out of accelerated particles undergoing inverse Compton scattering on low energy photons from the SN photosphere. The combination of radio and X-ray properties indicate the (lack of) equipartition between magnetic fields amplified by the shock and the relativistic particles accelerated by it. Since the SN shock travels through the circumstellar wind at a speed much higher than that of the wind set up by the progenitor, the X-ray observations track the long history of mass loss from the progenitor star. An interesting case is that of SN 2011ja, which suggests that a fraction of type IIP supernovae may interact with circumstellar medium set up by episodic or non-steady ejections from the progenitor.

  18. Motion-induced depth effect using a multiple-view dual-energy x-ray camera

    NASA Astrophysics Data System (ADS)

    Evans, J. Paul O.; Hon, Hock W.; Chan, Jer W.

    2002-11-01

    A novel 3D X-ray imaging technique to enhance the visual interpretation of complex X-ray images routinely encountered in aviation security applications has been developed. The 3D information is visualised as a smooth object rotation on a video display monitor. Further work enabled motion parallax to be combined with binocular parallax to produce a dynamic stereoscopic display. This imaging technique is equally applicable to both standard monochrome X-ray imaging and dual-energy X-ray imaging. The latter exploits the difference in magnitude between a high energy X-ray signal and a low energy X-ray signal to compute materials discrimination information made available to the human observer by colour encoding the resultant images. To produce the required image data an integrated dual-energy X-ray camera incorporating a novel castellated dual-energy scintillator arrangement has been developed.

  19. Compensational scintillation detector with a flat energy response for flash X-ray measurements

    SciTech Connect

    Chen Liang; Quan Lin; Zhang Zhongbing; Ouyang Xiaoping; Liu Bin; Liu Jinliang

    2013-01-15

    To measure the intensity of flash X-ray sources directly, a novel scintillation detector with a fast time response and flat energy response is developed by combining film scintillators of doped ZnO crystal and fast organic scintillator together. Through compensation design, the dual-scintillator detector (DSD) achieved a flat energy response to X-rays from tens of keV to several MeV, and sub-nanosecond time response by coupling to ultrafast photo-electronic devices. A prototype detector was fabricated according to the theoretical design; it employed ZnO:In and EJ228 with thicknesses of 0.3 mm and 0.1 mm, respectively. The energy response of this detector was tested on monoenergetic X-ray and {gamma}-ray sources. The detector performs very well with a sensitivity fluctuation below 5% for 8 discrete energy points within the 40-250 keV energy region and for other energies of 662 keV and 1.25 MeV as well, showing good accordance with the theoretical design. Additionally, the detector works properly for the application to the flash X-ray radiation field absolute intensity measurement. This DSD may be very useful for the diagnosis of time-resolved dynamic physical processes of flash X-ray sources without knowing the exact energy spectrum.

  20. Compensational scintillation detector with a flat energy response for flash X-ray measurements.

    PubMed

    Chen, Liang; Ouyang, Xiaoping; Liu, Bin; Liu, Jinliang; Quan, Lin; Zhang, Zhongbing

    2013-01-01

    To measure the intensity of flash X-ray sources directly, a novel scintillation detector with a fast time response and flat energy response is developed by combining film scintillators of doped ZnO crystal and fast organic scintillator together. Through compensation design, the dual-scintillator detector (DSD) achieved a flat energy response to X-rays from tens of keV to several MeV, and sub-nanosecond time response by coupling to ultrafast photo-electronic devices. A prototype detector was fabricated according to the theoretical design; it employed ZnO:In and EJ228 with thicknesses of 0.3 mm and 0.1 mm, respectively. The energy response of this detector was tested on monoenergetic X-ray and γ-ray sources. The detector performs very well with a sensitivity fluctuation below 5% for 8 discrete energy points within the 40-250 keV energy region and for other energies of 662 keV and 1.25 MeV as well, showing good accordance with the theoretical design. Additionally, the detector works properly for the application to the flash X-ray radiation field absolute intensity measurement. This DSD may be very useful for the diagnosis of time-resolved dynamic physical processes of flash X-ray sources without knowing the exact energy spectrum.

  1. Compensational scintillation detector with a flat energy response for flash X-ray measurements

    NASA Astrophysics Data System (ADS)

    Chen, Liang; Ouyang, Xiaoping; Liu, Bin; Liu, Jinliang; Quan, Lin; Zhang, Zhongbing

    2013-01-01

    To measure the intensity of flash X-ray sources directly, a novel scintillation detector with a fast time response and flat energy response is developed by combining film scintillators of doped ZnO crystal and fast organic scintillator together. Through compensation design, the dual-scintillator detector (DSD) achieved a flat energy response to X-rays from tens of keV to several MeV, and sub-nanosecond time response by coupling to ultrafast photo-electronic devices. A prototype detector was fabricated according to the theoretical design; it employed ZnO:In and EJ228 with thicknesses of 0.3 mm and 0.1 mm, respectively. The energy response of this detector was tested on monoenergetic X-ray and γ-ray sources. The detector performs very well with a sensitivity fluctuation below 5% for 8 discrete energy points within the 40-250 keV energy region and for other energies of 662 keV and 1.25 MeV as well, showing good accordance with the theoretical design. Additionally, the detector works properly for the application to the flash X-ray radiation field absolute intensity measurement. This DSD may be very useful for the diagnosis of time-resolved dynamic physical processes of flash X-ray sources without knowing the exact energy spectrum.

  2. Evaluation of Exposure From a Low Energy X-Ray Device Using Thermoluminescent Dosimeters

    NASA Technical Reports Server (NTRS)

    Edwards, David L.; Harris, William S., Jr.

    1997-01-01

    The exposure from an electron beam welding device was evaluated using thermoluminescent dosimeters (TLDs). The device generated low energy X-rays which the current dose equivalent conversion algorithm was not designed to evaluate making it necessary to obtain additional information relating to TLD operation at the photon energies encountered with the device. This was accomplished by performing irradiations at the National Institute of Standards and Technology (NIST) using low energy X-ray techniques. The resulting data was used to determine TLD badge response for low energy X-rays and to establish the relationship between TLD element response and the dose equivalent at specific depths in tissue for these photon energies. The new energy/dose equivalent calibration data was used to calculate the shallow and eye dose equivalent of badges exposed to the device.

  3. ALEXIS (Array of Low-Energy X-Ray Imaging Sensors): A narrow-band survey/monitor of the ultrasoft x-ray sky

    SciTech Connect

    Priedhorsky, W.C.; Bloch, J.J.; Cordova, F.; Smith, B.W.; Ulibarri, M.; Chavez, J.; Evans, E.; Seigmund, O.H.W.; Marshall, H.; Vallerga, J.

    1989-01-01

    Los Alamos and Sandia National Laboratories are building an ultrasoft X-ray monitor experiment. This experiment, called ALEXIS (Array of Low-Energy X-Ray Imaging Sensors), consists of six compact normal-incidence telescopes. ALEXIS will operate in the range 70--110 eV. The ultrasoft X-ray/EUV band is nearly uncharted territory for astrophysics. ALEXIS, with its wide fields-of-view and well-defined wavelength bands, will complement the upcoming NASA Extreme Ultraviolet Explorer and ROSAT EUV Wide Field Camera, which are sensitive broad-band survey experiments. The program objectives of ALEXIS are to (1) demonstrate the feasibility of a wide field-of-view, normal incidence ultrasoft X-ray telescope system and (2) to determine ultrasoft X-ray backgrounds in the space environment. As a dividend, ALEXIS will pursue the following scientific objectives: (1) to map the diffuse background, with unprecedented angular resolution, in several emission-line bands, (2) to perform a narrow-band survey of point sources, (3) to search for transient phenomena in the ultrasoft X-ray band, and (4) to provide synoptic monitoring of variable ultrasoft X-ray sources such as cataclysmic variables and flare stars. ALEXIS is designed to be flown on a small autonomous payload carrier (a minisat) that could be launched from any expendable launch vehicle. The experiment weighs 100 pounds, draws 40 watts, and produces 10 kbps of data. It can be flown in any low earth orbit. Onboard data storage allows operation and tracking from a single ground station at Los Alamos. 57 refs., 12 figs.

  4. X-ray polarimetry: A new window on the high energy sky

    NASA Astrophysics Data System (ADS)

    Bellazzini, R.; Muleri, F.

    2010-11-01

    Polarimetry is widely considered a powerful observational technique in X-ray astronomy, useful to enhance our understanding of the emission mechanisms, geometry and magnetic field arrangement of many compact objects. However, the lack of suitable sensitive instrumentation in the X-ray energy band has been the limiting factor for its development in the last three decades. Up to now, polarization measurements have been made exclusively with Bragg diffraction at 45∘ or Compton scattering at 90∘ and the only unambiguous detection of X-ray polarization has been obtained for one of the brightest object in the X-ray sky, the Crab Nebula. Only recently, with the development of a new class of high sensitivity imaging detectors, the possibility to exploit the photoemission process to measure the photon polarization has become a reality. We will report on the performance of an imaging X-ray polarimeter based on photoelectric effect. The device derives the polarization information from the track of the photoelectrons imaged by a finely subdivided Gas Pixel Detector. It has a great sensitivity even with telescopes of modest area and can perform simultaneously good imaging, moderate spectroscopy and high rate timing. Being truly 2D it is non-dispersive and does not require any rotation. This device is included in the scientific payload of many proposals of satellite mission which have the potential to unveil polarimetry also in X-rays in a few years.

  5. Pulse energy measurement at the hard x-ray laser in Japan

    SciTech Connect

    Kato, M.; Tanaka, T.; Saito, N.; Kurosawa, T.; Richter, M.; Sorokin, A. A.; Tiedtke, K.; Kudo, T.; Yabashi, M.; Tono, K.; Ishikawa, T.

    2012-07-09

    The pulse energies of a free electron laser have accurately been measured in the hard x-ray spectral range. In the photon energy regime from 4.4 keV to 16.8 keV, pulse energies up to 100 {mu}J were obtained at the hard x-ray laser facility SACLA (SPring-8 Angstrom Compact free-electron LAser). Two independent methods, using a cryogenic radiometer and a gas monitor detector, were applied and agreement within 3.3% was achieved. Based on our validated pulse energy measurement, a SACLA online monitor detector could be calibrated for all future experiments.

  6. Volumetric measurement of residual stress using high energy x-ray diffraction

    NASA Astrophysics Data System (ADS)

    Whitesell, R.; McKenna, A.; Wendt, S.; Gray, J.

    2016-02-01

    We present results and recent developments from our laboratory, bench-top high energy x-ray diffraction system (HEXRD), between diffraction energies 50 and 150 KeV, to measure internal strain of moderately sized objects. Traditional x-ray strain measurements are limited to a few microns depth due to the use of Cu Kα1 Mo Kα1 radiation. The use of high energy x-rays for volumetric measurements of strain is typically the domain of synchrotron sources. We discuss the use of industrial 320kVp tube sources to generate a brighter x-ray beam along with a method using the intrinsic 43 eV width of the Kα1 characteristic peak of tungsten to measure volumetric strains in a number of industrially relevant materials. We will present volumetric strain measurements from two examples, first, additive manufacturing (AM) parts with various build configurations and, secondly, residual strain depth profiles from shot peened surface treatments. The spatial resolution of these depth profiles is ˜75 microns. The development of a faster method as compared to energy dispersive or θ-2θ scans is based on the intensity variation measurement of the strain using the aforementioned 43 eV characteristic tungsten kα line. We will present recent results on the development of this new tool and on x-ray diffraction measurements at high energy.

  7. Measurement of the energy dependence of X-ray-induced decomposition of potassium chlorate.

    PubMed

    Pravica, Michael; Bai, Ligang; Sneed, Daniel; Park, Changyong

    2013-03-21

    We report the first measurements of the X-ray induced decomposition of KClO3 as a function of energy in two experiments. KClO3 was pressurized to 3.5 GPa and irradiated with monochromatic synchrotron X-rays ranging in energy from 15 to 35 keV in 5 keV increments. A systematic increase in the decomposition rate as the energy was decreased was observed, which agrees with the 1/E(3) trend for the photoelectric process, except at the lowest energy studied. A second experiment was performed to access lower energies (10 and 12 keV) using a beryllium gasket; suggesting an apparent resonance near 15 keV or 0.83 Ǻ maximizing the chemical decomposition rate. A third experiment was performed using KIO3 to ascertain the anionic dependence of the decomposition rate, which was observed to be far slower than in KClO3, suggesting that the O-O distance is the critical factor in chemical reactions. These results will be important for more efficiently initiating chemical decomposition in materials using selected X-ray wavelengths that maximize decomposition to aid useful hard X-ray-induced chemistry and contribute understanding of the mechanism of X-ray-induced decomposition of the chlorates.

  8. X-ray ionization yields and energy spectra in liquid argon

    NASA Astrophysics Data System (ADS)

    Bondar, A.; Buzulutskov, A.; Dolgov, A.; Shekhtman, L.; Sokolov, A.

    2016-04-01

    The main purpose of this work is to provide reference data on X-ray ionization yields and energy spectra in liquid Ar to the studies in the field of Cryogenic Avalanche Detectors (CRADs) for rare-event and other experiments, based on liquid Ar detectors. We present the results of two related researches. First, the X-ray recombination coefficients in the energy range of 10-1000 keV and ionization yields at different electric fields, between 0.6 and 2.3 kV/cm, are determined in liquid Ar based on the results of a dedicated experiment. Second, the energy spectra of pulsed X-rays in liquid Ar in the energy range of 15-40 keV, obtained in given experiments including that with the two-phase CRAD, are interpreted and compared to those calculated using a computer program, to correctly determine the absorbed X-ray energy. The X-ray recombination coefficients and ionization yields have for the first time been presented for liquid Ar in systematic way.

  9. Hiresmon: A Fast High Resolution Beam Position Monitor for Medium Hard and Hard X-Rays

    SciTech Connect

    Menk, Ralf Hendrik; Giuressi, Dario; Arfelli, Fulvia; Rigon, Luigi

    2007-01-19

    The high-resolution x-ray beam position monitor (XBPM) is based on the principle of a segmented longitudinal ionization chamber with integrated readout and USB2 link. In contrast to traditional transversal ionization chambers here the incident x-rays are parallel to the collecting field which allows absolute intensity measurements with a precision better than 0.3 %. Simultaneously the beam position in vertical and horizontal direction can be measured with a frame rate of one kHz. The precision of position encoding depends only on the SNR of the synchrotron radiation and is in the order of micro meters at one kHz frame rate and 108 photon /sec at 9 KeV.

  10. X-ray grating interferometry at photon energies over 180 keV

    NASA Astrophysics Data System (ADS)

    Ruiz-Yaniz, M.; Koch, F.; Zanette, I.; Rack, A.; Meyer, P.; Kunka, D.; Hipp, A.; Mohr, J.; Pfeiffer, F.

    2015-04-01

    We report on the implementation and characterization of grating interferometry operating at an x-ray energy of 183 keV. With the possibility to use this technique at high x-ray energies, bigger specimens could be studied in a quantitative way. Also, imaging strongly absorbing specimens will benefit from the advantages of the phase and dark-field signals provided by grating interferometry. However, especially at these high photon energies the performance of the absorption grating becomes a key point on the quality of the system, because the grating lines need to keep their small width of a couple of micrometers and exhibit a greater height of hundreds of micrometers. The performance of high aspect ratio absorption gratings fabricated with different techniques is discussed. Further, a dark-field image of an alkaline multicell battery highlights the potential of high energy x-ray grating based imaging.

  11. X-ray grating interferometry at photon energies over 180 keV

    SciTech Connect

    Ruiz-Yaniz, M.; Koch, F.; Meyer, P.; Kunka, D.; Mohr, J.; Zanette, I.; Rack, A.; Hipp, A.; Pfeiffer, F.

    2015-04-13

    We report on the implementation and characterization of grating interferometry operating at an x-ray energy of 183 keV. With the possibility to use this technique at high x-ray energies, bigger specimens could be studied in a quantitative way. Also, imaging strongly absorbing specimens will benefit from the advantages of the phase and dark-field signals provided by grating interferometry. However, especially at these high photon energies the performance of the absorption grating becomes a key point on the quality of the system, because the grating lines need to keep their small width of a couple of micrometers and exhibit a greater height of hundreds of micrometers. The performance of high aspect ratio absorption gratings fabricated with different techniques is discussed. Further, a dark-field image of an alkaline multicell battery highlights the potential of high energy x-ray grating based imaging.

  12. Room-temperature mercuric iodide spectrometry for low-energy X-rays

    NASA Technical Reports Server (NTRS)

    Kusmiss, J. H.; Barton, J. B.; Huth, G. C.; Economou, T. E.; Turkevich, A. L.; Iwanczyk, J. S.; Dabrowski, A. J.

    1982-01-01

    A discussion of the limits of energy resolution in different energy ranges is given. The energy resolution of a spectrometer is analyzed in terms of the parameters characterizing the crystal, the detector, and the amplification electronics. A high-resolution room-temperature HgI2 spectrometry system was used to measure low-energy X-ray fluorescence spectra. For the MgK-alpha X-ray line the measured resolution was 245 eV (fwhm); the electronic noise linewidth of the system was 225 eV. Alpha-particles were used to excite X-ray fluorescence from low-Z elements separately or in combination. The shape of the photopeaks in the spectra is discussed.

  13. Design and Implementation of an Acoustic X-ray Detector to Measure the LCLS Beam Energy

    SciTech Connect

    Loos, Jennifer L.; /San Jose State U. /SLAC

    2010-08-25

    On April 11, 2009, first light was seen from LCLS. The present apparatus being used to measure the x-ray beam energy is the Total Energy Sensor which uses a suite of thermal sensors. Another device is needed to cross-check the energy measurements. This new diagnostic tool utilizes radiation acoustic phenomena to determine the x-ray beam energy. A target is hit by the x-rays from the beam, and a voltage is generated in two piezoelectric sensors attached to the target in response to the consequent deformation. Once the voltage is known, the power can be obtained. Thermal sensors will also be attached to the target for calibration purposes. Material selection and design were based on: durability, ultra-high vacuum compatibility, safety and thermal properties. The target material was also chosen for its acoustic properties which were determined from tests using a frequency generator and laser. Initial tests suggest the device will function as anticipated.

  14. Energy Dispersive X-ray Tomography for 3D Elemental Mapping of Individual Nanoparticles

    PubMed Central

    Slater, Thomas J. A.; Lewis, Edward A.; Haigh, Sarah J.

    2016-01-01

    Energy dispersive X-ray spectroscopy within the scanning transmission electron microscope (STEM) provides accurate elemental analysis with high spatial resolution, and is even capable of providing atomically resolved elemental maps. In this technique, a highly focused electron beam is incident upon a thin sample and the energy of emitted X-rays is measured in order to determine the atomic species of material within the beam path. This elementally sensitive spectroscopy technique can be extended to three dimensional tomographic imaging by acquiring multiple spectrum images with the sample tilted along an axis perpendicular to the electron beam direction. Elemental distributions within single nanoparticles are often important for determining their optical, catalytic and magnetic properties. Techniques such as X-ray tomography and slice and view energy dispersive X-ray mapping in the scanning electron microscope provide elementally sensitive three dimensional imaging but are typically limited to spatial resolutions of > 20 nm. Atom probe tomography provides near atomic resolution but preparing nanoparticle samples for atom probe analysis is often challenging. Thus, elementally sensitive techniques applied within the scanning transmission electron microscope are uniquely placed to study elemental distributions within nanoparticles of dimensions 10-100 nm. Here, energy dispersive X-ray (EDX) spectroscopy within the STEM is applied to investigate the distribution of elements in single AgAu nanoparticles. The surface segregation of both Ag and Au, at different nanoparticle compositions, has been observed. PMID:27403838

  15. Low-energy X-ray detection with an in-vacuum PILATUS detector

    NASA Astrophysics Data System (ADS)

    Marchal, Julien; Luethi, Benjamin; Ursachi, Catalin; Mykhaylyk, Vitaliy; Wagner, Armin

    2011-11-01

    The feasibility of using PILATUS single-X-ray-photon counting detectors for long-wavelength macromolecular crystallography was investigated by carrying out a series of experiments at Diamond Light Source. A water-cooled PILATUS 100k detector was tested in vacuum with monochromatic 3 keV X-rays on the Diamond test beamline B16. Effects of detector cooling on noise performance, energy calibration and threshold trimming were investigated. When detecting 3 keV X-rays, the electronic noise of the analogue output of pixel preamplifiers forces the threshold to be set at a higher level than the 50% energy level recommended to minimize charge-sharing effects. The influence of threshold settings at low X-ray energy was studied by characterizing the detector response to a collimated beam of 3 keV X-rays scanned across several pixels. The relationship between maximum count rate and minimum energy threshold was investigated separately for various detector gain settings.

  16. X-Ray Lines Close to Kll Auger Electron Energies from Iron, Cobalt, Nickel, and Copper Monocrystals

    NASA Astrophysics Data System (ADS)

    Koo, Yeon Deog

    1990-01-01

    By x-ray bombardment of metal monocrystals (Fe, Co, Ni, and Cu), x-rays of KLL radiative Auger electrons (KLL RAE) can be observed on the low energy side of the Kalpha lines. The energies of the x-rays of the KLL RAE of each monocrystal are the same for different lattice planes and when different kinds of x-ray tubes (Mo, W, and Cu) are used. Therefore, the peak energies detected within the KLL Auger electron energy limit are interpreted as KLL RAE x-rays. The measured intensity ratios of KLL/Kalpha are about 0.3%. Additionally, the ratio of I(Kbeta )/I(Kalpha) and I(Si escape peak)/I(Kalpha) are measured. All of these values agree well with theoretical values. The beam shapes of KLL RAE x-rays are studied by taking pictures of x-ray films. The intensity distribution for Ni and Cu are measured by changing the crystal angle with respect to the incident x-ray beam near the Bragg angles of KLL RAE x-rays. It is shown that the KLL RAE x-rays are very sharp and stimulated when the crystal is set at the Bragg angle of the KLL RAE with respect to the incident beam, which contains both the pumping radiation and Bremsstrahlung of the frequencies in the KLL RAE range in which the KLL x-rays stimulation is achieved.

  17. Macro and micro full field x-ray fluorescence with an X-ray pinhole camera presenting high energy and high spatial resolution.

    PubMed

    Romano, Francesco Paolo; Caliri, Claudia; Cosentino, Luigi; Gammino, Santo; Giuntini, Lorenzo; Mascali, David; Neri, Lorenzo; Pappalardo, Lighea; Rizzo, Francesca; Taccetti, Francesco

    2014-11-01

    This work describes a tabletop (50 cm × 25 cm × 25 cm) full field X-ray pinhole camera (FF-XPC) presenting high energy- and high spatial-resolution. The FF-XPC consists of a conventional charge-coupled device (CCD) detector coupled, in a coaxial geometry, to a pinhole collimator of small diameter. The X-ray fluorescence (XRF) is induced on the samples with an external low-power X-ray tube. The use of the CCD as an energy dispersive X-ray detector was obtained by adopting a multi-image acquisition in single photon counting and by developing a processing algorithm to be applied in real-time to each of the acquired image-frames. This approach allowed the measurement of X-ray spectra with an energy resolution down to 133 eV at the reference value of 5.9 keV. The detection of the X-ray fluorescence through the pinhole-collimator allowed the two-dimensional elemental mapping of the irradiated samples. Two magnifications (M), determined by the relative sample-pinhole-CCD distances, are used in the present setup. A low value of M (equal to 0.35×) allows the macro-FF-XRF of large area samples (up to 4 × 4 cm(2)) with a spatial resolution down to 140 μm; a large magnification (M equal to 6×) is used for the micro-FF-XRF of small area samples (2.5 × 2.5 mm(2)) with a spatial resolution down to 30 μm.

  18. Airborne particles in the Miyagi Museum of Art in Sendai, Japan, studied by electron probe X-ray microanalysis and energy dispersive X-ray fluorescence analysis.

    PubMed

    Injuk, Jasna; Osán, Janos; Van Grieken, René; Tsuji, Kouichi

    2002-05-01

    The presented work provides baseline data on the existing airborne conditions in the Miyagi Museum of Art in Sendai, Japan, during the summer of 2000. The chemical composition, size and indoor and outdoor origin of the suspended particulate matter were identified using a number of advanced X-ray techniques, such as Electron Probe X-Ray Microanalysis (EPXMA) and Energy Dispersive X-Ray Fluorescence Analysis (EDXRF). Our results, to the best of our knowledge, represent the first detailed study of the chemical nature of the indoor particulate matter in a Japanese museum and, as such, may contribute to future improvements of the air quality inside museums and to the lasting conservation of works of art.

  19. Application of dual-energy x-ray techniques for automated food container inspection

    NASA Astrophysics Data System (ADS)

    Shashishekhar, N.; Veselitza, D.

    2016-02-01

    Manufacturing for plastic food containers often results in small metal particles getting into the containers during the production process. Metal detectors are usually not sensitive enough to detect these metal particles (0.5 mm or lesser), especially when the containers are stacked in large sealed shipping packages; X-ray inspection of these packages provides a viable alternative. This paper presents the results of an investigation into dual-energy X-ray techniques for automated detection of small metal particles in plastic food container packages. The sample packages consist of sealed cardboard boxes containing stacks of food containers: plastic cups for food, and Styrofoam cups for noodles. The primary goal of the investigation was to automatically identify small metal particles down to 0.5 mm diameter in size or less, randomly located within the containers. The multiple container stacks in each box make it virtually impossible to reliably detect the particles with single-energy X-ray techniques either visually or with image processing. The stacks get overlaid in the X-ray image and create many indications almost identical in contrast and size to real metal particles. Dual-energy X-ray techniques were investigated and found to result in a clear separation of the metal particles from the food container stack-ups. Automated image analysis of the resulting images provides reliable detection of the small metal particles.

  20. X-ray photoemission and energy dispersive spectroscopy of hydroxyapatite-coated titanium

    SciTech Connect

    Drummond, J.L.; Steinberg, A.D.; Krauss, A.R.

    1997-07-01

    The purpose of this study was to determine the chemical composition changes of hydroxyapatite (HA) coated titanium using surface analysis (X-ray photoemission) and bulk analysis (energy dispersive spectroscopy). The specimens examined were controls and specimens aged 30 min and 3 h at room temperature in distilled water and 0.2M sodium phosphate buffer (pH 7.2). Each X-ray photoemission cycle consisted of three scans followed by argon sputtering for 10 min for usually 20 cycles, corresponding to a sampling depth of {approximately}1,500 {angstrom}. The energy dispersive spectroscopy analysis was on a 110 by 90 {micro}m area for 500 s. The X-ray photoemission results indicated the oxidation effect of water on the titanium (as TiO{sub 2}) and the effect of the buffer to increase the surface concentration of phosphorus. No differences in the chemical composition were observed by energy dispersive spectroscopy analysis.

  1. High-energy-resolution X-ray monochromator calibration using the detailed-balance principle

    PubMed Central

    Zhao, J. Y.; Sturhahn, W.

    2012-01-01

    A new method is presented to calibrate an X-ray energy scale with sub-meV relative accuracy by using the detailed-balance principle of the phonon creation and annihilation. This method is conveniently used to define or verify the energy scale of high-energy-resolution monochromators that are used in inelastic X-ray scattering and nuclear resonant inelastic X-ray scattering instruments at synchrotron radiation facilities. This method does not rely on sample properties and its precision only depends on the statistical data quality. Well calibrated instruments are essential for reliable comparison of data sets obtained at different synchrotron radiation beamlines, of data with theoretical predictions, and of data from other techniques such as neutron or light scattering. The principle of the detailed-balance method is described in this paper and demonstrated experimentally. PMID:22713897

  2. The extended medium sensitivity survey distant cluster sample - X-ray data and interpretation of the luminosity evolution

    NASA Technical Reports Server (NTRS)

    Henry, J. P.; Gioia, I. M.; Maccacaro, T.; Morris, S. L.; Stocke, J. T.; Wolter, A.

    1992-01-01

    The X-ray properties of a cluster of galaxies subsample of the Einstein Extended Medium Sensitivity Survey is described. A summary of this sample and its implication has been presented previously; this paper gives the full details. The cluster subsample is 98.4 percent identified and contains 93 X-ray-selected clusters to a redshift of 0.58. The cluster X-ray luminosity function at three cosmic epochs is derived. While the present luminosity function agrees with previous determinations at the lowest redshifts, it is found that the volume density of high-luminosity clusters is greater now than it was in the past. The normalization, shape, and time dependence of the luminosity function can be described by a simple hierarchical formation model with parameters which also describe the temperature function of an independent sample of low-redshift clusters. In this model the comoving hot gas density remains constant with time at least to redshifts of order 0.35.

  3. X-RAY SEARCHES FOR EMISSION FROM THE WHIM IN THE GALACTIC HALO AND THE INTERGALACTIC MEDIUM

    SciTech Connect

    Bregman, Joel N.; Otte, Birgit; Irwin, Jimmy A.; Putman, Mary E.; Lloyd-Davies, Edward J.; Bruens, Christian E-mail: otteb@umich.edu E-mail: mputman@astro.columbia.edu E-mail: cbruens@astro.uni-bonn.de

    2009-07-10

    At least 50% of the baryons in the local universe are undetected and predicted to be in a hot dilute phase (10{sup 5}-10{sup 7} K) in low and moderate overdensity environments. We searched for the predicted diffuse faint emission through shadowing observations whereby cool foreground gas absorbs more distant diffuse emission. Observations were obtained with Chandra and XMM-Newton. Using the cold gas in two galaxies, NGC 891 and NGC 5907, shadows were not detected and a newer observation of NGC 891 fails to confirm a previously reported X-ray shadow. Our upper limits lie above model predictions. For Local Group studies, we used a cloud in the Magellanic Stream and a compact high-velocity cloud to search for a shadow. Instead of a shadow, the X-ray emission was brighter toward the Magellanic Stream cloud and there is a less significant brightness enhancement toward the other cloud also. The brightness enhancement toward the Magellanic Stream cloud is probably due to an interaction with a hot ambient medium that surrounds the Milky Way. We suggest that this interaction drives a shock into the cloud, heating the gas to X-ray emitting temperatures.

  4. Quantitative imaging using high-energy X-ray phase-contrast CT with a 70 kVp polychromatic X-ray spectrum.

    PubMed

    Sarapata, Adrian; Willner, Marian; Walter, Marco; Duttenhofer, Thomas; Kaiser, Konradin; Meyer, Pascal; Braun, Christian; Fingerle, Alexander; Noël, Peter B; Pfeiffer, Franz; Herzen, Julia

    2015-01-12

    Imaging of large and dense objects with grating-based X-ray phase-contrast computed tomography requires high X-ray photon energy and large fields of view. It has become increasingly possible due to the improvements in the grating manufacturing processes. Using a high-energy X-ray phase-contrast CT setup with a large (10 cm in diameter) analyzer grating and operated at an acceleration tube voltage of 70 kVp, we investigate the complementarity of both attenuation and phase contrast modalities with materials of various atomic numbers (Z). We confirm experimentally that for low-Z materials, phase contrast yields no additional information content over attenuation images, yet it provides increased contrast-to-noise ratios (CNRs). The complementarity of both signals can be seen again with increasing Z of the materials and a more comprehensive material characterization is thus possible. Imaging of a part of a human cervical spine with intervertebral discs surrounded by bones and various soft tissue types showcases the benefit of high-energy X-ray phase-contrast system. Phase-contrast reconstruction reveals the internal structure of the discs and makes the boundary between the disc annulus and nucleus pulposus visible. Despite the fact that it still remains challenging to develop a high-energy grating interferometer with a broad polychromatic source with satisfactory optical performance, improved image quality for phase contrast as compared to attenuation contrast can be obtained and new exciting applications foreseen. PMID:25835698

  5. High-energy synchrotron radiation x-ray microscopy: Present status and future prospects

    SciTech Connect

    Jones, K.W.; Gordon, B.M.; Spanne, P. ); Rivers, M.L.; Sutton, S.R. )

    1991-01-01

    High-energy radiation synchrotron x-ray microscopy is used to characterize materials of importance to the chemical and materials sciences and chemical engineering. The x-ray microscope (XRM) forms images of elemental distributions fluorescent x rays or images of mass distributions by measurement of the linear attenuation coefficient of the material. Distributions of sections through materials are obtained non-destructively using the technique of computed microtomography. The energy range of the x rays used for the XRM ranges from a few keV at the minimum value to more than 100 keV, which is sufficient to excite the K-edge of all naturally occurring elements. The work in progress at the Brookhaven NSLS X26 and X17 XRM is described in order to show the current status of the XRM. While there are many possible approaches to the XRM instrumentation, this instrument gives state-of-the-art performance in most respects and serves as a reasonable example of the present status of the instrumentation in terms of the spatial resolution and minimum detection limits obtainable. The examples of applications cited give an idea of the types of research fields that are currently under investigation. They can be used to illustrate how the field of x-ray microscopy will benefit from the use of bending magnets and insertion devices at the Advanced Photon Source. 8 refs., 5 figs.

  6. Catalytic Adventures in Space and Time Using High Energy X-rays

    SciTech Connect

    Newton, Mark A.; Di Michiel, Marco; Ferri, Davide; Fernàndez-Garcia, Marcos; Beale, Andrew M.; Jacques, Simon D. M.; Chupas, Peter J.; Chapman, Karena W.

    2014-09-16

    Very high energy X-rays have long offered great promise in providing great insight into the inner workings of catalysts; insights that may complement the array of techniques available to researchers in catalysis either in the laboratory or at more conventional X-ray wavelengths. This contribution aims to critically assess the diverse possibilities now available in the high energy domain as a result of the maturation of third generation synchrotron facilities and to look forward to the potential that forthcoming developments in synchrotron source technology may offer the world of catalysis in the near future.

  7. Energy calibration of a high-resolution inelastic x-ray scattering spectrometer

    SciTech Connect

    Verbeni, Roberto; D'Astuto, Matteo; Krisch, Michael; Lorenzen, Maren; Mermet, Alain; Monaco, Giulio; Requardt, Herwig; Sette, Francesco

    2008-08-15

    The energy scale of a triple-axis x-ray spectrometer with meV energy resolution based on perfect silicon crystal optics is calibrated, utilizing the most recent determination of the silicon lattice parameter and its thermal expansion coefficient and recording the dispersion of longitudinal acoustic and optical phonons in a diamond single crystal and the molecular vibration mode in liquid nitrogen. Comparison of the x-ray results with previous inelastic neutron and Raman scattering results as well as with ab initio phonon dispersion calculations yields an overall agreement better than 2%.

  8. High pressure XANES and XMCD in the tender X-ray energy range

    NASA Astrophysics Data System (ADS)

    Wilhelm, F.; Garbarino, G.; Jacobs, J.; Vitoux, H.; Steinmann, R.; Guillou, F.; Snigirev, A.; Snigireva, I.; Voisin, P.; Braithwaite, D.; Aoki, D.; Brison, J.-P.; Kantor, I.; Lyatun, I.; Rogalev, A.

    2016-07-01

    We have developed an experimental setup at the ESRF beamline ID12 dedicated to X-ray absorption and magnetic circular dichroism measurements at high pressure adapted for the tender X-ray energy range and compatible with low temperatures and with high magnetic field. The focused incoming X-ray beam passes through a thin diamond disk attached to a fully perforated diamond anvil and X-ray fluorescence photons from the sample are collected in back-scattering geometry through the same diamond disk. The pressure in the cell is measured using the ruby luminescence through a full diamond anvil. The highest pressure attainable with this diamond anvil cell (DAC) depends on the thickness of the diamond disk and it is above 16 GPa for a 80-μm thick plate and exceeds 4.5 GPa in the case of 30-μm diamond disk. Excellent performances of this setup in the tender X-ray range are illustrated with X-ray absorption near-edge structure studies of the phase transitions in KCl at the potassium and chlorine K-edges (3.61 and 2.82 keV, respectively) as well as in CdS at the sulfur K-edge (2.47 keV). This DAC together with a dedicated total fluorescence yield (TFY) detector could be mounted in the main heat exchanger of a cryostat and inserted in a bore of a superconducting magnet, this makes possible to perform X-ray magnetic circular dichroism (XMCD) experiments at low temperature, high magnetic field and high pressure. Feasibility of this approach is shown with the XMCD results obtained at the U M?-edges in ferromagnetic superconductor UGe?.

  9. Validation of a New Skinfold Prediction Equation Based on Dual-Energy X-Ray Absorptiometry

    ERIC Educational Resources Information Center

    Ball, Stephen; Cowan, Celsi; Thyfault, John; LaFontaine, Tom

    2014-01-01

    Skinfold prediction equations recommended by the American College of Sports Medicine underestimate body fat percentage. The purpose of this research was to validate an alternative equation for men created from dual energy x-ray absorptiometry. Two hundred ninety-seven males, aged 18-65, completed a skinfold assessment and dual energy x-ray…

  10. High-energy synchrotron X-ray radiography of shock-compressed materials

    NASA Astrophysics Data System (ADS)

    Rutherford, Michael E.; Chapman, David J.; Collinson, Mark A.; Jones, David R.; Music, Jasmina; Stafford, Samuel J. P.; Tear, Gareth R.; White, Thomas G.; Winters, John B. R.; Drakopoulos, Michael; Eakins, Daniel E.

    2015-06-01

    This presentation will discuss the development and application of a high-energy (50 to 250 keV) synchrotron X-ray imaging method to study shock-compressed, high-Z samples at Beamline I12 at the Diamond Light Source synchrotron (Rutherford-Appleton Laboratory, UK). Shock waves are driven into materials using a portable, single-stage gas gun designed by the Institute of Shock Physics. Following plate impact, material deformation is probed in-situ by white-beam X-ray radiography and complimentary velocimetry diagnostics. The high energies, large beam size (13 x 13 mm), and appreciable sample volumes (~ 1 cm3) viable for study at Beamline I12 compliment existing in-house pulsed X-ray capabilities and studies at the Dynamic Compression Sector. The authors gratefully acknowledge the ongoing support of Imperial College London, EPSRC, STFC and the Diamond Light Source, and AWE Plc.

  11. Time-delayed beam splitting with energy separation of x-ray channels

    SciTech Connect

    Stetsko, Yuri P.; Shvyd'ko, Yuri V.; Brian Stephenson, G.

    2013-10-21

    We introduce a time-delayed beam splitting method based on the energy separation of x-ray photon beams. It is implemented and theoretically substantiated on an example of an x-ray optical scheme similar to that of the classical Michelson interferometer. The splitter/mixer uses Bragg-case diffraction from a thin diamond crystal. Another two diamond crystals are used as back-reflectors. Because of energy separation and a minimal number (three) of optical elements, the split-delay line has high efficiency and is simple to operate. Due to the high transparency of diamond crystal, the split-delay line can be used in a beam sharing mode at x-ray free-electron laser facilities.

  12. Superconducting Detector System for High-Resolution Energy-Dispersive Soft X-Ray Spectroscopy

    SciTech Connect

    Friedrich, S; Niedermayr, T; Drury, O; Funk, T; Frank, M; Labov, S E; Cramer, S

    2001-02-21

    Synchrotron-based soft x-ray spectroscopy is often limited by detector performance. Grating spectrometers have the resolution, but lack the efficiency for the analysis of dilute samples. Semiconducting Si(Li) or Ge detectors are efficient, but often lack the resolution to separate weak signals from strong nearby lines in multi-element samples. Superconducting tunnel junctions (STJs) operated at temperatures below 1 K can be used as high-resolution high-efficiency x-ray detectors. They combine high energy resolution around 10 eV FWHM with the broad band efficiency of energy-dispersive detectors. We have designed a two-stage adiabatic demagnetization refrigerator (ADR) to operate STJ detectors in x-ray fluorescence measurements at beam line 4 of the ALS. We demonstrate the capabilities of such a detector system for fluorescence analysis of dilute metal sites in proteins and inorganic model compounds.

  13. The HERO Program: High-Energy Replicated Optics for a Hard-X-Ray Balloon Payload

    NASA Technical Reports Server (NTRS)

    Ramsey, B. D.; Engelhaupt, D.; Speegle, C. O.; Austin, R. A.; Kolodziejczak, J. J.; ODell, S. L.; Weisskopf, M. C.

    1999-01-01

    We are developing high-energy replicated optics for a balloon-borne hard-x-ray telescope. When completed, the telescope will have around 150 square cm of effective collecting area up to 65 keV, and an angular resolution of around 30 arc seconds, half power diameter. When used in conjunction with an array of focal plane imaging detectors, for which Gas Scintillation Proportional Counters are under development, the payload will provide unprecedented sensitivity for pointed observations in the hard-x-ray band. We will present an overview of the High Energy Replicated Optics (HERO) program together with test data from the first mirror units. The overall sensitivity of the full payload, when flown on long- and ultra-long-duration balloon flights, will be compared with past and planned satellite-borne hard-x-ray missions.

  14. Investigation of high-resolution superconducting tunnel junction detectors for low-energy X-ray fluorescence analysis

    NASA Astrophysics Data System (ADS)

    Beckhoff, B.; Fliegauf, R.; Ulm, G.

    2003-04-01

    The energy resolution of conventional semiconductor detectors is insufficient for simultaneously separating the leading fluorescence lines of low Z and medium Z materials in the soft X-ray regime. It is therefore important to investigate alternative detection instruments offering higher energy resolution and evaluate their applicability to soft X-ray fluorescence (XRF) analysis. In this paper, various results of the characterization and evaluation of a cryogenic superconducting tunnel junction (STJ) detector, which was provided to the Physikalisch-Technische Bundesanstalt (PTB) by the Lawrence Livermore National Laboratory, are given with respect to both detector response functions and XRF. For this investigation, monochromatized undulator radiation of high spectral purity, available to the PTB X-ray radiometry laboratory at the electron storage ring BESSY II, was employed, by which it was possible to record the STJ response functions at various photon energies of interest ranging from 180 to 1600 eV. By scanning the effective detector area and the adjacent substrate and leads, relevant artefacts of the detector response were identified.

  15. Monochromatic x-ray radiography for areal-density measurement of inertial fusion energy fuel in fast ignition experimenta)

    NASA Astrophysics Data System (ADS)

    Fujioka, Shinsuke; Fujiwara, Takashi; Tanabe, Minoru; Nishimura, Hiroaki; Nagatomo, Hideo; Ohira, Shinji; Inubushi, Yuichi; Shiraga, Hiroyuki; Azechi, Hiroshi

    2010-10-01

    Ultrafast, two-dimensional x-ray imaging is an important diagnostics for the inertial fusion energy research, especially in investigating implosion dynamics at the final stage of the fuel compression. Although x-ray radiography was applied to observing the implosion dynamics, intense x-rays emitted from the high temperature and dense fuel core itself are often superimposed on the radiograph. This problem can be solved by coupling the x-ray radiography with monochromatic x-ray imaging technique. In the experiment, 2.8 or 5.2 keV backlight x-rays emitted from laser-irradiated polyvinyl chloride or vanadium foils were selectively imaged by spherically bent quartz crystals with discriminating the out-of-band emission from the fuel core. This x-ray radiography system achieved 24 μm and 100 ps of spatial and temporal resolutions, respectively.

  16. Observation of solar high energy gamma and X-ray emission and solar energetic particles

    NASA Astrophysics Data System (ADS)

    Struminsky, A.; Gan, W.

    2015-08-01

    We considered 18 solar flares observed between June 2010 and July 2012, in which high energy >100 MeV γ-emission was registered by the Large Area Telescope (LAT) aboard FermiGRO. We examined for these γ-events soft X-ray observations by GOES, hard X-ray observations by the Anti-Coincidence Shield of the SPectrometer aboard INTEGRAL (ACS SPI) and the Gamma-Ray burst Monitor (GBM) aboard FermiGRO. Hard X-ray and π0-decay γ-ray emissions are used as tracers of electron and proton acceleration, respectively. Bursts of hard X-ray were observed by ACS SPI during impulsive phase of 13 events. Bursts of hard X- ray >100 keV were not found during time intervals, when prolonged hard y-emission was registered by LAT/FermiGRO. Those events showing prolonged high-energy gamma-ray emission not accompanied by >100 keV hard X-ray emission are interpreted as an indication of either different acceleration processes for protons and electrons or as the presence of a proton population accelerated during the impulsive phase of the flare and subsequently trapped by some magnetic structure. In-situ energetic particle measurements by GOES and STEREO (High Energy Telescope, HET) shows that five of these y-events were not accompanied by SEP events at 1 AU, even when multi-point measurements including STEREO are taken into account. Therefore accelerated protons are not always released into the heliosphere. A longer delay between the maximum temperature and the maximum emission measure characterises flares with prolonged high energy γ-emission and solar proton events.

  17. X-ray measurements at high-power lasers. Relative conversion efficiencies of short pulse laser light into K X-ray radiation in medium to high Z elements

    NASA Astrophysics Data System (ADS)

    Szabo, C. I.; Indelicato, P.; Gumberidze, A.; Holland, G. E.; Seely, J. F.; Hudson, L. T.; Henins, A.; Audebert, P.; Bastiani-Ceccotti, S.; Tabakhoff, E.; Brambrink, E.

    2009-03-01

    Conversion efficiencies of laser light into K x-ray radiation are used to characterize laser-solid interactions e.g. in measurements with back-lighter targets in Inertial Confinement Fusion research or in ultra short x-ray science where ultra short laser pulses are used to create x-rays for investigation of dynamic processes. In our measurements we observed high energy (few tens of keV) K x-ray radiation of element pairs created upon impact of a 1 ps, 100 J laser pulse on the target surface. The high-energy electrons created in this interaction ionise and excite the target material. We have used high purity alloy foils of Pd and Ag, as well as In and Sn and crystals of CsI and rare earth molybdates as target materials. Both constituents of these targets were simultaneously excited in one shot. The K x-ray radiation was dispersed and detected with the LCS (LULI Crystal Spectrometer), a Cauchois-type cylindrically bent transmission-crystal spectrometer. Measuring ratios in the x-ray spectra permits determination of relative conversion efficiencies for pairs of elements under identical laser-target interaction conditions.

  18. The application of thermoluminescence dosimetry in X-ray energy discrimination.

    PubMed

    Nelson, V K; Holloway, L; McLean, I D

    2015-12-01

    Clinical dosimetry requires an understanding of radiation energy to accurately determine the delivered dose. For many situations this is known, however there are also many situations where the radiation energy is not well known, thus limiting dosimetric accuracy. This is the case in personnel dosimetry where thermo luminescent (TL) dosimetry is the method of choice. Traditionally beam energy characteristics in personnel dosimetry are determined through discrimination with the use of various filters fitted within a radiation monitor. The presence of scattered and characteristic radiation produced by these metallic filters, however, can compromise the results. In this study the TL response of five materials TLD100, TLD100H, TLD200, TLD400 and TLD500, was measured at various X-ray energies. The TL sensitivity ratio for various combinations of materials as a function of X-ray energy was calculated. The results indicate that in personal dosimetry a combination of three or more TL detector system has a better accuracy of estimation of effective radiation energy of an X-ray beam than some of the current method of employed for energy estimation and has the potential to improve the accuracy in dose determination in a variety of practical situations. The development of this method also has application in other fields including quality assurance of the orthovoltage therapy machines, dosimetry intercomparisons of kilovoltage X-ray beams, and measurement of the dose to critical organs outside a treatment field of a megavoltage therapy beam. PMID:26330215

  19. The application of thermoluminescence dosimetry in X-ray energy discrimination.

    PubMed

    Nelson, V K; Holloway, L; McLean, I D

    2015-12-01

    Clinical dosimetry requires an understanding of radiation energy to accurately determine the delivered dose. For many situations this is known, however there are also many situations where the radiation energy is not well known, thus limiting dosimetric accuracy. This is the case in personnel dosimetry where thermo luminescent (TL) dosimetry is the method of choice. Traditionally beam energy characteristics in personnel dosimetry are determined through discrimination with the use of various filters fitted within a radiation monitor. The presence of scattered and characteristic radiation produced by these metallic filters, however, can compromise the results. In this study the TL response of five materials TLD100, TLD100H, TLD200, TLD400 and TLD500, was measured at various X-ray energies. The TL sensitivity ratio for various combinations of materials as a function of X-ray energy was calculated. The results indicate that in personal dosimetry a combination of three or more TL detector system has a better accuracy of estimation of effective radiation energy of an X-ray beam than some of the current method of employed for energy estimation and has the potential to improve the accuracy in dose determination in a variety of practical situations. The development of this method also has application in other fields including quality assurance of the orthovoltage therapy machines, dosimetry intercomparisons of kilovoltage X-ray beams, and measurement of the dose to critical organs outside a treatment field of a megavoltage therapy beam.

  20. Bismuth Sulfide Nanoflowers for Detection of X-rays in the Mammographic Energy Range

    PubMed Central

    Nambiar, Shruti; Osei, Ernest K.; Yeow, John T. W.

    2015-01-01

    The increased use of diagnostic x-rays, especially in the field of medical radiology, has necessitated a significant demand for high resolution, real-time radiation detectors. In this regard, the photoresponse of bismuth sulfide (Bi2S3), an n-type semiconducting metal chalcogenide, to low energy x-rays has been investigated in this study. In recent years, several types of nanomaterials of Bi2S3 have been widely studied for optoelectronic and thermoelectric applications. However, photoresponse of Bi2S3 nanomaterials for dosimetric applications has not yet been reported. The photosensitivity of Bi2S3 with nanoscale “flower-like” structures was characterized under x-ray tube-potentials typically used in mammographic procedures. Both dark current and photocurrent were measured under varying x-ray doses, field sizes, and bias voltages for each of the tube potentials – 20, 23, 26 and 30 kV. Results show that the Bi2S3 nanoflowers instantaneously responded to even minor changes in the dose delivered. The photoresponse was found to be relatively high (few nA) at bias voltage as low as +1 V, and fairly repeatable for both short and long exposures to mammographic x-rays with minimal or no loss in sensitivity. The overall dose-sensitivity of the Bi2S3 nanoflowers was found to be similar to that of a micro-ionization chamber. PMID:25801531

  1. Bismuth sulfide nanoflowers for detection of X-rays in the mammographic energy range.

    PubMed

    Nambiar, Shruti; Osei, Ernest K; Yeow, John T W

    2015-03-24

    The increased use of diagnostic x-rays, especially in the field of medical radiology, has necessitated a significant demand for high resolution, real-time radiation detectors. In this regard, the photoresponse of bismuth sulfide (Bi2S3), an n-type semiconducting metal chalcogenide, to low energy x-rays has been investigated in this study. In recent years, several types of nanomaterials of Bi2S3 have been widely studied for optoelectronic and thermoelectric applications. However, photoresponse of Bi2S3 nanomaterials for dosimetric applications has not yet been reported. The photosensitivity of Bi2S3 with nanoscale "flower-like" structures was characterized under x-ray tube-potentials typically used in mammographic procedures. Both dark current and photocurrent were measured under varying x-ray doses, field sizes, and bias voltages for each of the tube potentials - 20, 23, 26 and 30 kV. Results show that the Bi2S3 nanoflowers instantaneously responded to even minor changes in the dose delivered. The photoresponse was found to be relatively high (few nA) at bias voltage as low as +1 V, and fairly repeatable for both short and long exposures to mammographic x-rays with minimal or no loss in sensitivity. The overall dose-sensitivity of the Bi2S3 nanoflowers was found to be similar to that of a micro-ionization chamber.

  2. Diagnosing x-ray power and energy of tungsten wire array z-pinch with a flat spectral response x-ray diode.

    PubMed

    Wang, Kun-lun; Ren, Xiao-dong; Huang, Xian-bin; Zhang, Si-qun; Zhou, Shao-tong; Dan, Jia-kun; Li, Jing; Xu, Qiang; Ouyang, Kai; Cai, Hong-chun; Wei, Bing; Ji, Ce; Feng, Shu-ping; Wang, Meng; Xie, Wei-ping; Deng, Jian-jun

    2015-11-01

    Fast z-pinch is a very efficient way of converting electromagnetic energy to radiation. With an 8-10 MA current on primary test stand facility, about 1 MJ electromagnetic energy is delivered to vacuum chamber, which heats z-pinch plasma to radiate soft x-ray. To develop a pulsed high power x-ray source, we studied the applicability of diagnosing x-ray power from tungsten wire array z-pinch with a flat spectral response x-ray diode (FSR-XRD). The detector was originally developed to diagnose radiation of a hohlraum in SG-III prototype laser facility. It utilized a gold cathode XRD and a specially configured compound gold filter to yield a nearly flat spectral response in photon energy range of 0.1-4 keV. In practice, it was critical to avoid surface contamination of gold cathode. It is illustrated that an exposure of an XRD to multiple shots caused a significant change of response. Thus, in diagnosing x-ray power and energy, we used each XRD in only one shot after calibration. In a shot serial, output of FSR-XRD was compared with output of a nickel bolometer. In these shots, the outputs agreed with each other within their uncertainties which were about 12% for FSR-XRD and about 15% for bolometer. Moreover, the ratios between the FSR-XRD and the bolometer among different shots were explored. In 8 shots, the standard deviation of the ratio was 6%. It is comparable to XRD response change of 7%. PMID:26628136

  3. Diagnosing x-ray power and energy of tungsten wire array z-pinch with a flat spectral response x-ray diode

    SciTech Connect

    Wang, Kun-lun; Ren, Xiao-dong; Huang, Xian-bin Zhang, Si-qun; Zhou, Shao-tong; Dan, Jia-kun; Li, Jing; Xu, Qiang; Ouyang, Kai; Cai, Hong-chun; Wei, Bing; Ji, Ce; Feng, Shu-ping; Wang, Meng; Xie, Wei-ping; Deng, Jian-jun

    2015-11-15

    Fast z-pinch is a very efficient way of converting electromagnetic energy to radiation. With an 8-10 MA current on primary test stand facility, about 1 MJ electromagnetic energy is delivered to vacuum chamber, which heats z-pinch plasma to radiate soft x-ray. To develop a pulsed high power x-ray source, we studied the applicability of diagnosing x-ray power from tungsten wire array z-pinch with a flat spectral response x-ray diode (FSR-XRD). The detector was originally developed to diagnose radiation of a hohlraum in SG-III prototype laser facility. It utilized a gold cathode XRD and a specially configured compound gold filter to yield a nearly flat spectral response in photon energy range of 0.1-4 keV. In practice, it was critical to avoid surface contamination of gold cathode. It is illustrated that an exposure of an XRD to multiple shots caused a significant change of response. Thus, in diagnosing x-ray power and energy, we used each XRD in only one shot after calibration. In a shot serial, output of FSR-XRD was compared with output of a nickel bolometer. In these shots, the outputs agreed with each other within their uncertainties which were about 12% for FSR-XRD and about 15% for bolometer. Moreover, the ratios between the FSR-XRD and the bolometer among different shots were explored. In 8 shots, the standard deviation of the ratio was 6%. It is comparable to XRD response change of 7%.

  4. Inelastic x-ray scattering at modest energy resolution

    SciTech Connect

    Finkelstein, K. D.; Tischler, J. Z.; Larson, B. C.

    1997-07-01

    We report results from the development of an inelastic scattering spectrometer designed to take advantage of high energy synchrotron radiation available at CHESS. The device allows a large increase of the effective scattering volume in the sample by permitting measurements to be made in an energy range up to 25 KeV. The highest useable energy appears limited by the efficiency of the analyzers under consideration. At 20 KeV a novel 4-bounce, sagittal focusing monochromator passes 10e11 photons/second with Darwin width limited energy resolution. In the scattering plane, the monochromator images the electron beam producing a small scattering source for the analyzing optics. Analyzer systems under study include a cooled mosaic crystal in para-focusing geometry, and an adjustable spherically bent silicon crystal respectively for parallel and point-by-point collection of the energy loss spectrum. This paper discusses the optical configurations presents results from our early measurements and suggests directions for improvements.

  5. Energy calibration of superconducting transition edge sensors for x-ray detection using pulse analysis

    SciTech Connect

    Hollerith, C.; Simmnacher, B.; Weiland, R.; Feilitzsch, F. v.; Isaila, C.; Jochum, J.; Potzel, W.; Hoehne, J.; Phelan, K.; Wernicke, D.; May, T.

    2006-05-15

    Transition edge sensors (TESs) have been developed to be used as high-resolution x-ray detectors. They show excellent energy resolution and can be used in many applications. TESs are a special kind of calorimeters that can determine small temperature changes after x-ray absorption. Such a temperature change causes a strong resistance change (superconducting to normal-conducting phase transition) that can be measured. The energy calibration of a TES based spectrometer is problematic due to the nonlinear behavior of the detector response. In this article, a method is introduced to calibrate the energy scale of TES spectra. This is accomplished by calculating the energy dependence of the response of the detector operated in electrothermal feedback mode. Using this method a calibration accuracy of a few eV for an x-ray energy of 6 keV can be achieved. Examples of energy dispersive x-ray spectroscopy (EDS) measurements demonstrate the high quality of this method for everyday use of TES EDS detectors in material analysis. However, because the method relies only on a few very general assumptions, it should also be useful for other kinds of TES detectors.

  6. Energy-discriminating K-edge x-ray computed tomography system

    NASA Astrophysics Data System (ADS)

    Watanabe, Manabu; Sato, Eiichi; Abderyim, Purkhet; Matsukiyo, Hiroshi; Osawa, Akihiro; Enomoto, Toshiyuki; Nagao, Jiro; Nomiya, Seiichiro; Hitomi, Keitaro; Ogawa, Akira; Sato, Shigehiro; Ichimaru, Toshio

    2008-08-01

    An energy-discriminating K-edge x-ray Computed Tomography (CT) system is useful for increasing contrast resolution of a target region and for diagnosing cancers utilizing a drug delivery system. The CT system is of the first generation type and consists of an x-ray generator, a turn table, a translation stage, a two-stage controller, a cadmium telluride (CdTe) detector, a charge amplifier, a shaping amplifier, a multi-channel analyzer (MCA), a counter board (CB), and a personal computer (PC). The K-edge CT is accomplished by repeating translation and rotation of an object. Penetrating x-ray spectra from the object are measured by a spectrometer utilizing the CdTe detector, amplifiers, and MCA. Both the photon energy and the energy width are selected by the MCA for discriminating photon energy. Enhanced iodine K-edge x-ray CT was performed by selecting photons with energies just beyond iodine K-edge energy of 33.2 keV.

  7. A dynamic material discrimination algorithm for dual MV energy X-ray digital radiography.

    PubMed

    Li, Liang; Li, Ruizhe; Zhang, Siyuan; Zhao, Tiao; Chen, Zhiqiang

    2016-08-01

    Dual-energy X-ray radiography has become a well-established technique in medical, industrial, and security applications, because of its material or tissue discrimination capability. The main difficulty of this technique is dealing with the materials overlapping problem. When there are two or more materials along the X-ray beam path, its material discrimination performance will be affected. In order to solve this problem, a new dynamic material discrimination algorithm is proposed for dual-energy X-ray digital radiography, which can also be extended to multi-energy X-ray situations. The algorithm has three steps: α-curve-based pre-classification, decomposition of overlapped materials, and the final material recognition. The key of the algorithm is to establish a dual-energy radiograph database of both pure basis materials and pair combinations of them. After the pre-classification results, original dual-energy projections of overlapped materials can be dynamically decomposed into two sets of dual-energy radiographs of each pure material by the algorithm. Thus, more accurate discrimination results can be provided even with the existence of the overlapping problem. Both numerical and experimental results that prove the validity and effectiveness of the algorithm are presented. PMID:27239987

  8. A dynamic material discrimination algorithm for dual MV energy X-ray digital radiography.

    PubMed

    Li, Liang; Li, Ruizhe; Zhang, Siyuan; Zhao, Tiao; Chen, Zhiqiang

    2016-08-01

    Dual-energy X-ray radiography has become a well-established technique in medical, industrial, and security applications, because of its material or tissue discrimination capability. The main difficulty of this technique is dealing with the materials overlapping problem. When there are two or more materials along the X-ray beam path, its material discrimination performance will be affected. In order to solve this problem, a new dynamic material discrimination algorithm is proposed for dual-energy X-ray digital radiography, which can also be extended to multi-energy X-ray situations. The algorithm has three steps: α-curve-based pre-classification, decomposition of overlapped materials, and the final material recognition. The key of the algorithm is to establish a dual-energy radiograph database of both pure basis materials and pair combinations of them. After the pre-classification results, original dual-energy projections of overlapped materials can be dynamically decomposed into two sets of dual-energy radiographs of each pure material by the algorithm. Thus, more accurate discrimination results can be provided even with the existence of the overlapping problem. Both numerical and experimental results that prove the validity and effectiveness of the algorithm are presented.

  9. Semiconductor detector performance for low-energy x-rays

    SciTech Connect

    Jaklevic, J.M.; Walton, J.T.; McMurray, R.E. Jr.; Madden, N.W.; Goulding, F.S.

    1987-06-01

    Factors that limit the capabilities of semiconductor detectors at photon energies below 5 keV include energy resolution, detector efficiency, and detector-related continuum background. These properties can be controlled to a certain extent by optimal detector design and fabrication techniques. We describe measurements on the low-energy response of Si(Li) detectors obtained using a tunable, low-energy monochromatic source. Window thicknesses have been measured for a number of devices using different materials for the entry contact. The interpretation of these results in terms of existing detector window models is discussed. Results obtained using a new contact structure demonstrate that a dramatic reduction in window-related absorption in Si(Li) detectors can be achieved.

  10. Improvements in the Low Energy Collection Efficiency of Si(Li) X-ray Detectors

    SciTech Connect

    Cox,C.; Fischer, D.; Schwartz, W.; Song, Y.

    2005-01-01

    Soft X-ray beam-line applications are of fundamental importance to material research, and commonly employ high-resolution Si(Li) detectors for energy dispersive spectroscopy. However, the measurement of X-rays below 1 keV is compromised by absorption in the material layers in front of the active crystal and a dead layer at the crystal surface. Various Schottky barrier type contacts were investigated resulting in a 40% reduction of the dead-layer thickness and a factor of two increased sensitivity at carbon K{sub {alpha}} compared to the standard Si(Li) detector. Si(Li) detectors were tested on the U7A soft X-ray beam-line at the National Synchrotron Light Source and on a scanning electron microscope (SEM).

  11. High resolution energy-angle correlation measurement of hard x rays from laser-Thomson backscattering.

    PubMed

    Jochmann, A; Irman, A; Bussmann, M; Couperus, J P; Cowan, T E; Debus, A D; Kuntzsch, M; Ledingham, K W D; Lehnert, U; Sauerbrey, R; Schlenvoigt, H P; Seipt, D; Stöhlker, Th; Thorn, D B; Trotsenko, S; Wagner, A; Schramm, U

    2013-09-13

    Thomson backscattering of intense laser pulses from relativistic electrons not only allows for the generation of bright x-ray pulses but also for the investigation of the complex particle dynamics at the interaction point. For this purpose a complete spectral characterization of a Thomson source powered by a compact linear electron accelerator is performed with unprecedented angular and energy resolution. A rigorous statistical analysis comparing experimental data to 3D simulations enables, e.g., the extraction of the angular distribution of electrons with 1.5% accuracy and, in total, provides predictive capability for the future high brightness hard x-ray source PHOENIX (photon electron collider for narrow bandwidth intense x rays) and potential gamma-ray sources.

  12. Compact 'diode-based' multi-energy soft x-ray diagnostic for NSTX

    SciTech Connect

    Tritz, K.; Clayton, D. J.; Stutman, D.; Finkenthal, M.

    2012-10-15

    A novel and compact, diode-based, multi-energy soft x-ray (ME-SXR) diagnostic has been developed for the National Spherical Tokamak Experiment. The new edge ME-SXR system tested on NSTX consists of a set of vertically stacked diode arrays, each viewing the plasma tangentially through independent pinholes and filters providing an overlapping view of the plasma midplane which allows simultaneous SXR measurements with coarse sub-sampling of the x-ray spectrum. Using computed x-ray spectral emission data, combinations of filters can provide fast (>10 kHz) measurements of changes in the electron temperature and density profiles providing a method to 'fill-in' the gaps of the multi-point Thomson scattering system.

  13. Low energy x-ray response of Ge detectors with amorphous Ge entrance contacts

    SciTech Connect

    Luke, P.N.; Rossington, C.S.; Wesela, M.F.

    1993-10-01

    The low energy x-ray response of GI detectors with amorphous GI entrance contacts has been evaluated. The spectral background due to near contact incomplete charge collection was found to consist of two components: a low level component which is insensitive to applied voltage and a high level step-like component which is voltage dependent. At high operating voltages, the high level component can be completely suppressed, resulting in background levels which are much lower than those previously observed using GI detectors with Pd surface barrier or B ion implanted contacts, and which also compare favorably to those obtained with Si(Li) x-ray detectors. The response of these detectors to {sup 55}Fe and 1.77 keV x-rays is shown. A qualitative explanation of the origins of the observed background components is presented.

  14. The high energy X-ray detector on the Ariel-5 satellite

    NASA Technical Reports Server (NTRS)

    Engel, A. R.; Coe, M. J.

    1977-01-01

    The Imperial College hard X-ray detector which is used to make spectral measurements in the 26 keV to 1.2 MeV energy range on celestial X-ray sources from the Ariel-5 satellite is described. Details are given of the design, calibration and in-orbit performance of the detector. A modulation process is used to detect weak signals against a background and we give details of the spectrum unfolding techniques used to convert the measured spectra into corrected incident spectra.

  15. Compton scattering imaging of a working battery using synchrotron high-energy X-rays.

    PubMed

    Itou, Masayoshi; Orikasa, Yuki; Gogyo, Yuma; Suzuki, Kosuke; Sakurai, Hiroshi; Uchimoto, Yoshiharu; Sakurai, Yoshiharu

    2015-01-01

    Results of studies on Compton scattering imaging using synchrotron high-energy X-rays are reported. The technique is applied to a discharging coin cell, and the intensity of Compton scattered X-rays from the inside of the cell has been measured as a function of position and time. The position-time intensity map captures the migration of lithium ions in the positive electrode and reveals the structural change due to the volume expansion of the electrode. This experiment is a critical step in developing synchrotron-based Compton scattering imaging for electrochemical cells at a product level.

  16. Preliminary research on dual-energy X-ray phase-contrast imaging

    NASA Astrophysics Data System (ADS)

    Han, Hua-Jie; Wang, Sheng-Hao; Gao, Kun; Wang, Zhi-Li; Zhang, Can; Yang, Meng; Zhang, Kai; Zhu, Pei-Ping

    2016-04-01

    Dual-energy X-ray absorptiometry (DEXA) has been widely applied to measure the bone mineral density (BMD) and soft-tissue composition of the human body. However, the use of DEXA is greatly limited for low-Z materials such as soft tissues due to their weak absorption, while X-ray phase-contrast imaging (XPCI) shows significantly improved contrast in comparison with the conventional standard absorption-based X-ray imaging for soft tissues. In this paper, we propose a novel X-ray phase-contrast method to measure the area density of low-Z materials, including a single-energy method and a dual-energy method. The single-energy method is for the area density calculation of one low-Z material, while the dual-energy method aims to calculate the area densities of two low-Z materials simultaneously. Comparing the experimental and simulation results with the theoretical ones, the new method proves to have the potential to replace DEXA in area density measurement. The new method sets the prerequisites for a future precise and low-dose area density calculation method for low-Z materials. Supported by Major State Basic Research Development Program (2012CB825800), Science Fund for Creative Research Groups (11321503) and National Natural Science Foundation of China (11179004, 10979055, 11205189, 11205157)

  17. Thermal Acoustic Sensor for High Pulse Energy X-ray FEL Beams

    SciTech Connect

    Smith, T.J.; Frisch, J.C.; Kraft, E.M.; Loos, J.; Bentsen, G.S.; /Rochester U.

    2011-12-13

    The pulse energy density of X-ray FELs will saturate or destroy conventional X-ray diagnostics, and the use of large beam attenuation will result in a beam that is dominated by harmonics. We present preliminary results at the LCLS from a pulse energy detector based on the thermal acoustic effect. In this type of detector an X-ray resistant material (boron carbide in this system) intercepts the beam. The pulse heating of the target material produces an acoustic pulse that can be detected with high frequency microphones to produce a signal that is linear in the absorbed energy. The thermal acoustic detector is designed to provide first- and second-order calorimetric measurement of X-ray FEL pulse energy. The first-order calorimetry is a direct temperature measurement of a target designed to absorb all or most of the FEL pulse power with minimal heat leak. The second-order measurement detects the vibration caused by the rapid thermoelastic expansion of the target material each time it absorbs a photon pulse. Both the temperature change and the amplitude of the acoustic signal are directly related to the photon pulse energy.

  18. Inelastic x-ray scattering at modest energy resolution

    SciTech Connect

    Finkelstein, K.D.; Larson, B.C.

    1997-07-01

    We report results from the development of an inelastic scattering spectrometer designed to take advantage of high energy synchrotron radiation available at CHESS. The device allows a large increase of the effective scattering volume in the sample by permitting measurements to be made in an energy range up to 25 KeV. The highest useable energy appears limited by the efficiency of the analyzers under consideration. At 20 KeV a novel 4-bounce, sagittal focusing monochromator passes 10e11 photons/second with Darwin width limited energy resolution. In the scattering plane, the monochromator images the electron beam producing a small scattering source for the analyzing optics. Analyzer systems under study include a cooled mosaic crystal in para-focusing geometry, and an adjustable spherically bent silicon crystal respectively for parallel and point-by-point collection of the energy loss spectrum. This paper discusses the optical configurations presents results from our early measurements and suggests directions for improvements. {copyright} {ital 1997 American Institute of Physics.}

  19. Energy-Dispersive X-Ray Fluorescence Spectrometry: A Long Overdue Addition to the Chemistry Curriculum

    ERIC Educational Resources Information Center

    Palmer, Peter T.

    2011-01-01

    Portable Energy-Dispersive X-Ray Fluorescence (XRF) analyzers have undergone significant improvements over the past decade. Salient advantages of XRF for elemental analysis include minimal sample preparation, multielement analysis capabilities, detection limits in the low parts per million (ppm) range, and analysis times on the order of 1 min.…

  20. Investigation of pulsed X-ray radiation of a plasma focus in a broad energy range

    SciTech Connect

    Savelov, A. S. Salakhutdinov, G. Kh.; Koltunov, M. V.; Lemeshko, B. D.; Yurkov, D. I.; Sidorov, P. P.

    2011-12-15

    The results of the experimental investigations of the spectral composition of plasma focus X-ray radiation in the photon energy range of 1.5 keV-400 keV are presented. Three regions in the radiation spectrum where the latter is of a quasi-thermal nature with a corresponding effective temperature are distinguished.

  1. Comparison of Anthropometry to Dual Energy X-Ray Absorptiometry: A New Prediction Equation for Women

    ERIC Educational Resources Information Center

    Ball, Stephen; Swan, Pamela D.; DeSimone, Rosemarie

    2004-01-01

    The purpose of this study was to assess the accuracy of three recommended anthropometric equations for women and then develop an updated prediction equation using dual energy x-ray absorptiometry (DXA). The percentage of body fat (%BF) by anthropometry was significantly correlated (r = .896-. 929; p [is less than] .01) with DXA, but each equation…

  2. Filter-fluorescer measurement of low-voltage simulator x-ray energy spectra

    SciTech Connect

    Baldwin, G.T.; Craven, R.E.

    1986-01-01

    X-ray energy spectra of the Maxwell Laboratories MBS and Physics International Pulserad 737 were measured using an eight-channel filter-fluorescer array. The PHOSCAT computer code was used to calculate channel response functions, and the UFO code to unfold spectrum.

  3. On the calculation of the gauge volume size for energy-dispersive X-ray diffraction.

    PubMed

    Rowles, Matthew R

    2011-11-01

    Equations for the calculation of the dimensions of a gauge volume, also known as the active volume or diffraction lozenge, in an energy-dispersive diffraction experiment where the detector is collimated by two ideal slits have been developed. Equations are given for equatorially divergent and parallel incident X-ray beams, assuming negligible axial divergence. PMID:21997921

  4. Analysis of tincal ore waste by energy dispersive X-ray fluorescence (EDXRF) Technique

    NASA Astrophysics Data System (ADS)

    Kalfa, Orhan Murat; Üstündağ, Zafer; Özkırım, Ilknur; Kagan Kadıoğlu, Yusuf

    2007-01-01

    Etibank Borax Plant is located in Kırka-Eskişehir, Turkey. The borax waste from this plant was analyzed by means of energy dispersive X-ray fluorescence (EDXRF). The standard addition method was used for the determination of the concentration of Al, Fe, Zn, Sn, and Ba. The results are presented and discussed in this paper.

  5. Luminescence imaging of water during irradiation of X-ray photons lower energy than Cerenkov- light threshold

    NASA Astrophysics Data System (ADS)

    Yamamoto, Seiichi; Koyama, Shuji; Komori, Masataka; Toshito, Toshiyuki

    2016-10-01

    Luminescence imaging of water using X-ray photon irradiation at energy lower than maximum energy of ~200 keV is thought to be impossible because the secondary electrons produced in this energy range do not emit Cerenkov- light. Contrary to this consensus assumption, we show that the luminescence imaging of water can be achieved by X-ray irradiation at energy lower than 120 keV. We placed water phantoms on a table with a conventional X-ray imaging system, and luminescence images of these phantoms were measured with a high-sensitivity, cooled charge coupled device (CCD) camera during X-ray photon irradiation at energy below 120 keV. We also carried out such imaging of an acrylic block and plastic scintillator. The luminescence images of water phantoms taken during X-ray photon irradiation clearly showed X-ray photon distribution. The intensity of the X-ray photon images of the phantom increased almost proportionally to the number of X-ray irradiations. Lower-energy X-ray photon irradiation showed lower-intensity luminescence at the deeper parts of the phantom due to the higher X-ray absorption in the water phantom. Furthermore, lower-intensity luminescence also appeared at the deeper parts of the acrylic phantom due to its higher density than water. The intensity of the luminescence for water was 0.005% of that for plastic scintillator. Luminescence imaging of water during X-ray photon irradiation at energy lower than 120 keV was possible. This luminescence imaging method is promising for dose estimation in X-ray imaging systems.

  6. Energy resolution and high count rate performance of superconducting tunnel junction x-ray spectrometers

    NASA Astrophysics Data System (ADS)

    Frank, M.; Hiller, L. J.; le Grand, J. B.; Mears, C. A.; Labov, S. E.; Lindeman, M. A.; Netel, H.; Chow, D.; Barfknecht, A. T.

    1998-01-01

    We present experimental results obtained with a cryogenically cooled, high-resolution x-ray spectrometer based on a 141 μm×141 μm Nb-Al-Al2O3-Al-Nb superconducting tunnel junction (STJ) detector in a demonstration experiment. Using monochromatized synchrotron radiation we studied the energy resolution of this energy-dispersive spectrometer for soft x rays with energies between 70 and 700 eV and investigated its performance at count rates up to nearly 60 000 cps. At count rates of several 100 cps we achieved an energy resolution of 5.9 eV (FWHM) and an electronic noise of 4.5 eV for 277 eV x rays (the energy corresponding to C K). Increasing the count rate, the resolution 277 eV remained below 10 eV for count rates up to ˜10 000 cps and then degraded to 13 eV at 23 000 cps and 20 eV at 50 000 cps. These results were achieved using a commercially available spectroscopy amplifier with a baseline restorer. No pile-up rejection was applied in these measurements. Our results show that STJ detectors can operate at count rates approaching those of semiconductor detectors while still providing a significantly better energy resolution for soft x rays. Thus STJ detectors may prove very useful in microanalysis, synchrotron x-ray fluorescence (XRF) applications, and XRF analysis of light elements (K lines) and transition elements (L lines).

  7. High Miller-index germanium crystals for high-energy x-ray imaging applications.

    PubMed

    Koch, J A; Lee, J J; Haugh, M J

    2015-12-01

    Near-normal-incidence bent crystals are widely used for x-ray imaging applications. Advantages include high collection solid angle and potentially high efficiency for narrow-band sources, while disadvantages include relatively large (several Å) interatomic spacings and a limited number of suitable matches between a crystal 2d value and an integral multiple of useful emission line wavelengths. The disadvantages become more significant at x-ray energies >10  keV. The former disadvantage can be mitigated by using high-order reflections from crystal planes having low Miller indices, but both disadvantages can be mitigated by using low-order reflections from crystal planes having high Miller indices. We report here on integrated reflectivity measurements we performed of Ge (15,7,7) (2d=0.6296  Å), a candidate for imaging Ru He-α (θ(B)=87°). We find good agreement with calculations, and the data show a multitude of closely spaced reflections with slightly different Bragg angles including a fifth-order reflection of Ge (3,1,1) that has comparable reflectivity. This demonstrates that arbitrary choices of Miller indices in Ge crystals can be used to fine-tune Bragg angles for near-normal-incidence x-ray imaging at tens of kiloelectron volt x-ray energies with minimal lower-energy contamination from lower-order reflections, and that existing calculational tools can be used to reliably estimate integrated reflectivity. PMID:26836681

  8. X-ray lasers and methods utilizing two component driving illumination provided by optical laser means of relatively low energy and small physical size

    DOEpatents

    Rosen, Mordecai D.; Matthews, Dennis L.

    1991-01-01

    An X-ray laser (10), and related methodology, are disclosed wherein an X-ray laser target (12) is illuminated with a first pulse of optical laser radiation (14) of relatively long duration having scarcely enough energy to produce a narrow and linear cool plasma of uniform composition (38). A second, relatively short pulse of optical laser radiation (18) is uniformly swept across the length, from end to end, of the plasma (38), at about the speed of light, to consecutively illuminate continuously succeeding portions of the plasma (38) with optical laser radiation having scarcely enough energy to heat, ionize, and invert them into the continuously succeeding portions of an X-ray gain medium. This inventive double pulse technique results in a saving of more than two orders of magnitude in driving optical laser energy, when compared to the conventional single pulse approach.

  9. CT dual-energy decomposition into x-ray signatures ρe and Ze

    NASA Astrophysics Data System (ADS)

    Martz, Harry E.; Seetho, Issac M.; Champley, Kyle E.; Smith, Jerel A.; Azevedo, Stephen G.

    2016-05-01

    In a recent journal article [IEEE Trans. Nuc. Sci., 63(1), 341-350, 2016], we introduced a novel method that decomposes dual-energy X-ray CT (DECT) data into electron density (ρe) and a new effective-atomic-number called Ze in pursuit of system-independent characterization of materials. The Ze of a material, unlike the traditional Zeff, is defined relative to the actual X-ray absorption properties of the constituent atoms in the material, which are based on published X-ray cross sections. Our DECT method, called SIRZ (System-Independent ρe, Ze), uses a set of well-known reference materials and an understanding of the system spectral response to produce accurate and precise estimates of the X-ray-relevant basis variables (ρe, Ze) regardless of scanner or spectra in diagnostic energy ranges (30 to 200 keV). Potentially, SIRZ can account for and correct spectral changes in a scanner over time and, because the system spectral response is included in the technique, additional beam-hardening correction is not needed. Results show accuracy (<3%) and precision (<2%) values that are much better than prior methods on a wide range of spectra. In this paper, we will describe how to convert DECT system output into (ρe, Ze) features and we present our latest SIRZ results compared with ground truth for a set of materials.

  10. High-Energy Density science with an ultra-bright x-ray laser

    NASA Astrophysics Data System (ADS)

    Glenzer, Siegfried

    2015-11-01

    This talk will review recent progress in high-energy density physics using the world's brightest x-ray source, the Linac Coherent Light Source, SLAC's free electron x-ray laser. These experiments investigate laser-driven matter in extreme conditions where powerful x-ray scattering and imaging techniques have been applied to resolve ionic interactions at atomic (Ångstrom) scale lengths and to visualize the formation of dense plasma states. Major research areas include dynamic compression experiments of solid targets to determine structural properties and to discover and characterize phase transitions at mega-bar pressures. A second area studies extreme fields produced by high-intensity radiation where fundamental questions of laboratory plasmas can be related to cosmological phenomena. Each of these areas takes advantage of the unique properties of the LCLS x-ray beam. They include small foci for achieving high intensity or high spatial resolution, high photon flux for dynamic structure factor measurements in single shots, and high spectral bandwidth to resolve plasmon (Langmuir) waves or ion acoustic waves in dense plasmas. We will further describe new developments of ultrafast pump-probe technique at high repetition rates. These include studies on dense cryogenic hydrogen that have begun providing fundamental insights into the physical properties of matter in extreme conditions that are important for astrophysics, fusion experiments and generation of radiation sources. This work was supported by DOE Office of Science, Fusion Energy Science under FWP 100182.

  11. Response of large area avalanche photodiodes to low energy x rays

    SciTech Connect

    Gentile, T. R.; Bales, M.; Arp, U.; Dong, B.; Farrell, R.

    2012-05-15

    For an experiment to study neutron radiative beta-decay, we operated large area avalanche photodiodes (APDs) near liquid nitrogen temperature to detect x rays with energies between 0.2 keV and 20 keV. Whereas there are numerous reports of x ray spectrometry using APDs at energies above 1 keV, operation near liquid nitrogen temperature allowed us to reach a nominal threshold of 0.1 keV. However, due to the short penetration depth of x rays below 1 keV, the pulse height spectrum of the APD become complex. We studied the response using monochromatic x ray beams and employed phenomenological fits of the pulse height spectrum to model the measurement of a continuum spectrum from a synchrotron. In addition, the measured pulse height spectrum was modelled using a profile for the variation in efficiency of collection of photoelectrons with depth into the APD. The best results are obtained with the collection efficiency model.

  12. Absolute pulse energy measurements of soft x-rays at the Linac Coherent Light Source.

    PubMed

    Tiedtke, K; Sorokin, A A; Jastrow, U; Juranić, P; Kreis, S; Gerken, N; Richter, M; Arp, U; Feng, Y; Nordlund, D; Soufli, R; Fernández-Perea, M; Juha, L; Heimann, P; Nagler, B; Lee, H J; Mack, S; Cammarata, M; Krupin, O; Messerschmidt, M; Holmes, M; Rowen, M; Schlotter, W; Moeller, S; Turner, J J

    2014-09-01

    This paper reports novel measurements of x-ray optical radiation on an absolute scale from the intense and ultra-short radiation generated in the soft x-ray regime of a free electron laser. We give a brief description of the detection principle for radiation measurements which was specifically adapted for this photon energy range. We present data characterizing the soft x-ray instrument at the Linac Coherent Light Source (LCLS) with respect to the radiant power output and transmission by using an absolute detector temporarily placed at the downstream end of the instrument. This provides an estimation of the reflectivity of all x-ray optical elements in the beamline and provides the absolute photon number per bandwidth per pulse. This parameter is important for many experiments that need to understand the trade-offs between high energy resolution and high flux, such as experiments focused on studying materials via resonant processes. Furthermore, the results are compared with the LCLS diagnostic gas detectors to test the limits of linearity, and observations are reported on radiation contamination from spontaneous undulator radiation and higher harmonic content. PMID:25321502

  13. Development of optics for x-ray phase-contrast imaging of high energy density plasmas

    SciTech Connect

    Stutman, D.; Finkenthal, M.; Moldovan, N.

    2010-10-15

    Phase-contrast or refraction-enhanced x-ray radiography can be useful for the diagnostic of low-Z high energy density plasmas, such as imploding inertial confinement fusion (ICF) pellets, due to its sensitivity to density gradients. To separate and quantify the absorption and refraction contributions to x-ray images, methods based on microperiodic optics, such as shearing interferometry, can be used. To enable applying such methods with the energetic x rays needed for ICF radiography, we investigate a new type of optics consisting of grazing incidence microperiodic mirrors. Using such mirrors, efficient phase-contrast imaging systems could be built for energies up to {approx}100 keV. In addition, a simple lithographic method is proposed for the production of the microperiodic x-ray mirrors based on the difference in the total reflection between a low-Z substrate and a high-Z film. Prototype mirrors fabricated with this method show promising characteristics in laboratory tests.

  14. Method for obtaining silver nanoparticle concentrations within a porous medium via synchrotron X-ray computed microtomography.

    PubMed

    Molnar, Ian L; Willson, Clinton S; O'Carroll, Denis M; Rivers, Mark L; Gerhard, Jason I

    2014-01-21

    Attempts at understanding nanoparticle fate and transport in the subsurface environment are currently hindered by an inability to quantify nanoparticle behavior at the pore scale (within and between pores) within realistic pore networks. This paper is the first to present a method for high resolution quantification of silver nanoparticle (nAg) concentrations within porous media under controlled experimental conditions. This method makes it possible to extract silver nanoparticle concentrations within individual pores in static and quasi-dynamic (i.e., transport) systems. Quantification is achieved by employing absorption-edge synchrotron X-ray computed microtomography (SXCMT) and an extension of the Beer-Lambert law. Three-dimensional maps of X-ray mass linear attenuation are converted to SXCMT-determined nAg concentration and are found to closely match the concentrations determined by ICP analysis. In addition, factors affecting the quality of the SXCMT-determined results are investigated: 1) The acquisition of an additional above-edge data set reduced the standard deviation of SXCMT-determined concentrations; 2) X-ray refraction at the grain/water interface artificially depresses the SXCMT-determined concentrations within 18.1 μm of a grain surface; 3) By treating the approximately 20 × 10(6) voxels within each data set statistically (i.e., averaging), a high level of confidence in the SXCMT-determined mean concentrations can be obtained. This novel method provides the means to examine a wide range of properties related to nanoparticle transport in controlled laboratory porous medium experiments. PMID:24354304

  15. A new detector system for low energy X-ray fluorescence coupled with soft X-ray microscopy: First tests and characterization

    NASA Astrophysics Data System (ADS)

    Gianoncelli, Alessandra; Bufon, Jernej; Ahangarianabhari, Mahdi; Altissimo, Matteo; Bellutti, Pierluigi; Bertuccio, Giuseppe; Borghes, Roberto; Carrato, Sergio; Cautero, Giuseppe; Fabiani, Sergio; Giacomini, Gabriele; Giuressi, Dario; Kourousias, George; Menk, Ralf Hendrik; Picciotto, Antonino; Piemonte, Claudio; Rachevski, Alexandre; Rashevskaya, Irina; Stolfa, Andrea; Vacchi, Andrea; Zampa, Gianluigi; Zampa, Nicola; Zorzi, Nicola

    2016-04-01

    The last decades have witnessed substantial efforts in the development of several detector technologies for X-ray fluorescence (XRF) applications. In spite of the increasing trend towards performing, cost-effective and reliable XRF systems, detectors for soft X-ray spectroscopy still remain a challenge, requiring further study, engineering and customization in order to yield effective and efficient systems. In this paper we report on the development, first characterization and tests of a novel multielement detector system based on low leakage current silicon drift detectors (SDD) coupled to ultra low noise custom CMOS preamplifiers for synchrotron-based low energy XRF. This new system exhibits the potential for improving the count rate by at least an order of magnitude resulting in ten-fold shorter dwell time at an energy resolution similar to that of single element silicon drift detectors.

  16. The energy spectrum of X-rays from rocket-triggered lightning

    NASA Astrophysics Data System (ADS)

    Arabshahi, S.; Dwyer, J. R.; Cramer, E. S.; Grove, J. E.; Gwon, C.; Hill, J. D.; Jordan, D. M.; Lucia, R. J.; Vodopiyanov, I. B.; Uman, M. A.; Rassoul, H. K.

    2015-10-01

    Although the production of X-rays from natural and rocket-triggered lightning leaders have been studied in detail over the last 10 years, the energy spectrum of the X-rays has never been well measured because the X-rays are emitted in very short but intense bursts that result in pulse pileup in the detectors. The energy spectrum is important because it provides information about the source mechanism for producing the energetic runaway electrons and about the electric fields that they traverse. We have recently developed and operated the first spectrometer for the energetic radiation from lightning. The instrument is part of the Atmospheric Radiation Imagery and Spectroscopy (ARIS) project and will be referred to as ARIS-S (ARIS Spectrometer). It consists of seven 3'' NaI(Tl)/photomultiplier tube scintillation detectors with different thicknesses of attenuators, ranging from no attenuator to more than 1'' of lead placed over the detector (all the detectors are in a 1/8'' thick aluminum box). Using X-ray pulses preceding 48 return strokes in 8 rocket-triggered lightnings, we found that the spectrum of X-rays from leaders is too soft to be consistent with Relativistic Runaway Electron Avalanche. It has a power law dependence on the energies of the photons, and the power index, λ, is between 2.5 and 3.5. We present the details of the design of the instrument and the results of the analysis of the lightning data acquired during the summer of 2012.

  17. High-energy neutrino fluxes from AGN populations inferred from X-ray surveys

    NASA Astrophysics Data System (ADS)

    Jacobsen, Idunn B.; Wu, Kinwah; On, Alvina Y. L.; Saxton, Curtis J.

    2015-08-01

    High-energy neutrinos and photons are complementary messengers, probing violent astrophysical processes and structural evolution of the Universe. X-ray and neutrino observations jointly constrain conditions in active galactic nuclei (AGN) jets: their baryonic and leptonic contents, and particle production efficiency. Testing two standard neutrino production models for local source Cen A (Koers & Tinyakov and Becker & Biermann), we calculate the high-energy neutrino spectra of single AGN sources and derive the flux of high-energy neutrinos expected for the current epoch. Assuming that accretion determines both X-rays and particle creation, our parametric scaling relations predict neutrino yield in various AGN classes. We derive redshift-dependent number densities of each class, from Chandra and Swift/BAT X-ray luminosity functions (Silverman et al. and Ajello et al.). We integrate the neutrino spectrum expected from the cumulative history of AGN (correcting for cosmological and source effects, e.g. jet orientation and beaming). Both emission scenarios yield neutrino fluxes well above limits set by IceCube (by ˜4-106 × at 1 PeV, depending on the assumed jet models for neutrino production). This implies that: (i) Cen A might not be a typical neutrino source as commonly assumed; (ii) both neutrino production models overestimate the efficiency; (iii) neutrino luminosity scales with accretion power differently among AGN classes and hence does not follow X-ray luminosity universally; (iv) some AGN are neutrino-quiet (e.g. below a power threshold for neutrino production); (v) neutrino and X-ray emission have different duty cycles (e.g. jets alternate between baryonic and leptonic flows); or (vi) some combination of the above.

  18. Feasibility of using intermediate x-ray energies for highly conformal extracranial radiotherapy

    SciTech Connect

    Dong, Peng; Yu, Victoria; Nguyen, Dan; Demarco, John; Low, Daniel A.; Sheng, Ke; Woods, Kaley; Boucher, Salime

    2014-04-15

    Purpose: To investigate the feasibility of using intermediate energy 2 MV x-rays for extracranial robotic intensity modulated radiation therapy. Methods: Two megavolts flattening filter free x-rays were simulated using the Monte Carlo code MCNP (v4c). A convolution/superposition dose calculation program was tuned to match the Monte Carlo calculation. The modeled 2 MV x-rays and actual 6 MV flattened x-rays from existing Varian Linacs were used in integrated beam orientation and fluence optimization for a head and neck, a liver, a lung, and a partial breast treatment. A column generation algorithm was used for the intensity modulation and beam orientation optimization. Identical optimization parameters were applied in three different planning modes for each site: 2, 6 MV, and dual energy 2/6 MV. Results: Excellent agreement was observed between the convolution/superposition and the Monte Carlo calculated percent depth dose profiles. For the patient plans, overall, the 2/6 MV x-ray plans had the best dosimetry followed by 2 MV only and 6 MV only plans. Between the two single energy plans, the PTV coverage was equivalent but 2 MV x-rays improved organs-at-risk sparing. For the head and neck case, the 2MV plan reduced lips, mandible, tongue, oral cavity, brain, larynx, left and right parotid gland mean doses by 14%, 8%, 4%, 14%, 24%, 6%, 30% and 16%, respectively. For the liver case, the 2 MV plan reduced the liver and body mean doses by 17% and 18%, respectively. For the lung case, lung V20, V10, and V5 were reduced by 13%, 25%, and 30%, respectively. V10 of heart with 2 MV plan was reduced by 59%. For the partial breast treatment, the 2 MV plan reduced the mean dose to the ipsilateral and contralateral lungs by 27% and 47%, respectively. The mean body dose was reduced by 16%. Conclusions: The authors showed the feasibility of using flattening filter free 2 MV x-rays for extracranial treatments as evidenced by equivalent or superior dosimetry compared to 6 MV plans

  19. Robust x-ray based material identification using multi-energy sinogram decomposition

    NASA Astrophysics Data System (ADS)

    Yuan, Yaoshen; Tracey, Brian; Miller, Eric

    2016-05-01

    There is growing interest in developing X-ray computed tomography (CT) imaging systems with improved ability to discriminate material types, going beyond the attenuation imaging provided by most current systems. Dual- energy CT (DECT) systems can partially address this problem by estimating Compton and photoelectric (PE) coefficients of the materials being imaged, but DECT is greatly degraded by the presence of metal or other materials with high attenuation. Here we explore the advantages of multi-energy CT (MECT) systems based on photon-counting detectors. The utility of MECT has been demonstrated in medical applications where photon- counting detectors allow for the resolution of absorption K-edges. Our primary concern is aviation security applications where K-edges are rare. We simulate phantoms with differing amounts of metal (high, medium and low attenuation), both for switched-source DECT and for MECT systems, and include a realistic model of detector energy 0 resolution. We extend the DECT sinogram decomposition method of Ying et al. to MECT, allowing estimation of separate Compton and photoelectric sinograms. We furthermore introduce a weighting based on a quadratic approximation to the Poisson likelihood function that deemphasizes energy bins with low signal. Simulation results show that the proposed approach succeeds in estimating material properties even in high-attenuation scenarios where the DECT method fails, improving the signal to noise ratio of reconstructions by over 20 dB for the high-attenuation phantom. Our work demonstrates the potential of using photon counting detectors for stably recovering material properties even when high attenuation is present, thus enabling the development of improved scanning systems.

  20. High Energy Neutrino Flash From Far-UV/X-Ray Flares of Gamma-Ray Bursts

    SciTech Connect

    Murase, Kohta; Nagataki, Shigehiro; /Kyoto U., Yukawa Inst., Kyoto /KIPAC, Menlo Park

    2006-04-25

    The recent observations of bright optical and X-ray flares by the Swift satellite suggest these are produced by the late activities of the central engine. We study the neutrino emission from far-UV/X-ray flares under the late internal shock model. Since the efficiency of pion production in the highest energy is higher than that of the prompt bursts, such neutrino flashes from flares can give comparable or larger contributions to a diffuse very high energy neutrino background if the total energy input into flares is comparable to the radiated energy of the prompt bursts. These signals are very important because they have possibility to probe the nature of flares (baryonic or magnetic, the photon field, the magnetic field, and so on).

  1. The nuclear spectroscopic telescope array (NuSTAR) high-energy X-ray mission

    NASA Astrophysics Data System (ADS)

    Madsen, Kristin K.; Harrison, Fiona A.; An, Hongjun; Boggs, Steven E.; Christensen, Finn E.; Cook, Rick; Craig, William W.; Forster, Karl; Fuerst, Felix; Grefenstette, Brian; Hailey, Charles J.; Kitaguchi, Takao; Markwardt, Craig; Mao, Peter; Miyasaka, Hiromasa; Rana, Vikram R.; Stern, Daniel K.; Zhang, William W.; Zoglauer, Andreas; Walton, Dominic; Westergaard, Niels J.

    2014-07-01

    The Nuclear Spectroscopic Telescope Array (NuSTAR) mission was launched on 2012 June 13 and is the first focusing high-energy X-ray telescope in orbit operating above ~10 keV. NuSTAR flies two co-aligned Wolter-I conical approximation X-ray optics, coated with Pt/C and W/Si multilayers, and combined with a focal length of 10.14 meters this enables operation from 3-79 keV. The optics focus onto two focal plane arrays, each consisting of 4 CdZnTe pixel detectors, for a field of view of 12.5 arcminutes. The inherently low background associated with concentrating the X-ray light enables NuSTAR to probe the hard X-ray sky with a more than 100-fold improvement in sensitivity, and with an effective point spread function FWHM of 18 arcseconds (HPD ~1), NuSTAR provides a leap of improvement in resolution over the collimated or coded mask instruments that have operated in this bandpass. We present in-orbit performance details of the observatory and highlight important science results from the first two years of the mission.

  2. The Nuclear Spectroscopic Telescope Array (NuSTAR) High-Energy X-ray Mission

    NASA Technical Reports Server (NTRS)

    Harrison, Fiona A.; Craig, Willliam W.; Christensen, Finn E.; Hailey, Charles J.; Zhang, William W.; Boggs, Steven E.; Stern, Daniel; Cook, W. Rick; Forster, Karl; Giommi, Paolo; Grefenstette, Brian W.; Kim, Yunjin; Kitaguchi, Takao; Koglin, Jason E.; Madsen, Kristin K.; Mao, Peter H.; Miyasaka, Hiromasa; Mori, Kaya; Perri, Matteo; Markwardt, Craig B.; Wik, Daniel R.; Hornschemeier, Anne E.; Ptak, Andrew; Rigby, Jane R.

    2013-01-01

    High-energy X-ray telescope in orbit. NuSTAR operates in the band from 3 to 79 keV, extending the sensitivity of focusing far beyond the 10 keV high-energy cutoff achieved by all previous X-ray satellites. The inherently low background associated with concentrating the X-ray light enables NuSTAR to probe the hard X-ray sky with a more than 100-fold improvement in sensitivity over the collimated or coded mask instruments that have operated in this bandpass. Using its unprecedented combination of sensitivity and spatial and spectral resolution, NuSTAR will pursue five primary scientific objectives: (1) probe obscured active galactic nucleus (AGN) activity out to thepeak epoch of galaxy assembly in the universe (at z 2) by surveying selected regions of the sky; (2) study the population of hard X-ray-emitting compact objects in the Galaxy by mapping the central regions of the Milky Way; (3) study the non-thermal radiation in young supernova remnants, both the hard X-ray continuum and the emission from the radioactive element 44Ti; (4) observe blazars contemporaneously with ground-based radio, optical, and TeV telescopes, as well as with Fermi and Swift, to constrain the structure of AGN jets; and (5) observe line and continuum emission from core-collapse supernovae in the Local Group, and from nearby Type Ia events, to constrain explosion models. During its baseline two-year mission, NuSTAR will also undertake a broad program of targeted observations. The observatory consists of two co-aligned grazing-incidence X-ray telescopes pointed at celestial targets by a three-axis stabilized spacecraft. Deployed into a 600 km, near-circular, 6 inclination orbit, the observatory has now completed commissioning, and is performing consistent with pre-launch expectations. NuSTAR is now executing its primary science mission, and with an expected orbit lifetime of 10 yr, we anticipate proposing a guest investigator program, to begin in late 2014.

  3. THE NUCLEAR SPECTROSCOPIC TELESCOPE ARRAY (NuSTAR) HIGH-ENERGY X-RAY MISSION

    SciTech Connect

    Harrison, Fiona A.; Cook, W. Rick; Forster, Karl; Grefenstette, Brian W.; Madsen, Kristin K.; Mao, Peter H.; Miyasaka, Hiromasa; Craig, William W.; Pivovaroff, Michael J.; Christensen, Finn E.; Hailey, Charles J.; Koglin, Jason E.; Mori, Kaya; Zhang, William W.; Boggs, Steven E.; Stern, Daniel; Kim, Yunjin; Giommi, Paolo; Perri, Matteo; and others

    2013-06-20

    The Nuclear Spectroscopic Telescope Array (NuSTAR) mission, launched on 2012 June 13, is the first focusing high-energy X-ray telescope in orbit. NuSTAR operates in the band from 3 to 79 keV, extending the sensitivity of focusing far beyond the {approx}10 keV high-energy cutoff achieved by all previous X-ray satellites. The inherently low background associated with concentrating the X-ray light enables NuSTAR to probe the hard X-ray sky with a more than 100-fold improvement in sensitivity over the collimated or coded mask instruments that have operated in this bandpass. Using its unprecedented combination of sensitivity and spatial and spectral resolution, NuSTAR will pursue five primary scientific objectives: (1) probe obscured active galactic nucleus (AGN) activity out to the peak epoch of galaxy assembly in the universe (at z {approx}< 2) by surveying selected regions of the sky; (2) study the population of hard X-ray-emitting compact objects in the Galaxy by mapping the central regions of the Milky Way; (3) study the non-thermal radiation in young supernova remnants, both the hard X-ray continuum and the emission from the radioactive element {sup 44}Ti; (4) observe blazars contemporaneously with ground-based radio, optical, and TeV telescopes, as well as with Fermi and Swift, to constrain the structure of AGN jets; and (5) observe line and continuum emission from core-collapse supernovae in the Local Group, and from nearby Type Ia events, to constrain explosion models. During its baseline two-year mission, NuSTAR will also undertake a broad program of targeted observations. The observatory consists of two co-aligned grazing-incidence X-ray telescopes pointed at celestial targets by a three-axis stabilized spacecraft. Deployed into a 600 km, near-circular, 6 Degree-Sign inclination orbit, the observatory has now completed commissioning, and is performing consistent with pre-launch expectations. NuSTAR is now executing its primary science mission, and with an

  4. Novel energy resolving x-ray pinhole camera on Alcator C-Moda)

    NASA Astrophysics Data System (ADS)

    Pablant, N. A.; Delgado-Aparicio, L.; Bitter, M.; Brandstetter, S.; Eikenberry, E.; Ellis, R.; Hill, K. W.; Hofer, P.; Schneebeli, M.

    2012-10-01

    A new energy resolving x-ray pinhole camera has been recently installed on Alcator C-Mod. This diagnostic is capable of 1D or 2D imaging with a spatial resolution of ≈1 cm, an energy resolution of ≈1 keV in the range of 3.5-15 keV and a maximum time resolution of 5 ms. A novel use of a Pilatus 2 hybrid-pixel x-ray detector [P. Kraft et al., J. Synchrotron Rad. 16, 368 (2009), 10.1107/S0909049509009911] is employed in which the lower energy threshold of individual pixels is adjusted, allowing regions of a single detector to be sensitive to different x-ray energy ranges. Development of this new detector calibration technique was done as a collaboration between PPPL and Dectris Ltd. The calibration procedure is described, and the energy resolution of the detector is characterized. Initial data from this installation on Alcator C-Mod is presented. This diagnostic provides line-integrated measurements of impurity emission which can be used to determine impurity concentrations as well as the electron energy distribution.

  5. Novel energy resolving x-ray pinhole camera on Alcator C-Mod.

    PubMed

    Pablant, N A; Delgado-Aparicio, L; Bitter, M; Brandstetter, S; Eikenberry, E; Ellis, R; Hill, K W; Hofer, P; Schneebeli, M

    2012-10-01

    A new energy resolving x-ray pinhole camera has been recently installed on Alcator C-Mod. This diagnostic is capable of 1D or 2D imaging with a spatial resolution of ≈1 cm, an energy resolution of ≈1 keV in the range of 3.5-15 keV and a maximum time resolution of 5 ms. A novel use of a Pilatus 2 hybrid-pixel x-ray detector [P. Kraft et al., J. Synchrotron Rad. 16, 368 (2009)] is employed in which the lower energy threshold of individual pixels is adjusted, allowing regions of a single detector to be sensitive to different x-ray energy ranges. Development of this new detector calibration technique was done as a collaboration between PPPL and Dectris Ltd. The calibration procedure is described, and the energy resolution of the detector is characterized. Initial data from this installation on Alcator C-Mod is presented. This diagnostic provides line-integrated measurements of impurity emission which can be used to determine impurity concentrations as well as the electron energy distribution.

  6. Novel energy resolving x-ray pinhole camera on Alcator C-Mod

    SciTech Connect

    Pablant, N. A.; Delgado-Aparicio, L.; Bitter, M.; Ellis, R.; Hill, K. W.; Brandstetter, S.; Eikenberry, E.; Hofer, P.; Schneebeli, M.

    2012-10-15

    A new energy resolving x-ray pinhole camera has been recently installed on Alcator C-Mod. This diagnostic is capable of 1D or 2D imaging with a spatial resolution of Almost-Equal-To 1 cm, an energy resolution of Almost-Equal-To 1 keV in the range of 3.5-15 keV and a maximum time resolution of 5 ms. A novel use of a Pilatus 2 hybrid-pixel x-ray detector [P. Kraft et al., J. Synchrotron Rad. 16, 368 (2009)] is employed in which the lower energy threshold of individual pixels is adjusted, allowing regions of a single detector to be sensitive to different x-ray energy ranges. Development of this new detector calibration technique was done as a collaboration between PPPL and Dectris Ltd. The calibration procedure is described, and the energy resolution of the detector is characterized. Initial data from this installation on Alcator C-Mod is presented. This diagnostic provides line-integrated measurements of impurity emission which can be used to determine impurity concentrations as well as the electron energy distribution.

  7. Measurements of the spectrum and energy dependence of X-ray transition radiation

    NASA Technical Reports Server (NTRS)

    Cherry, M. L.

    1978-01-01

    The results of experiments designed to test the theory of X-ray transition radiation and to verify the predicted dependence of the characteristic features of the radiation on the radiator dimensions are presented. The X-ray frequency spectrum produced by 5- to 9-GeV electrons over the range 4 to 30 keV was measured with a calibrated single-crystal Bragg spectrometer, and at frequencies up to 100 keV with an NaI scintillator. The interference pattern in the spectrum and the hardening of the radiation with increasing foil thickness are clearly observed. The energy dependence of the total transition-radiation intensity was studied using a radiator with large dimensions designed to yield energy-dependent signals at very high particle energies, up to E/mc-squared approximately equal to 100,000. The results are in good agreement with the theoretical predictions.

  8. MASS AND ENERGY OF ERUPTING SOLAR PLASMA OBSERVED WITH THE X-RAY TELESCOPE ON HINODE

    SciTech Connect

    Lee, Jin-Yi; Moon, Yong-Jae; Kim, Kap-Sung; Raymond, John C.; Reeves, Katharine K.

    2015-01-10

    We investigate seven eruptive plasma observations by Hinode/XRT. Their corresponding EUV and/or white light coronal mass ejection features are visible in some events. Five events are observed in several passbands in X-rays, which allows for the determination of the eruptive plasma temperature using a filter ratio method. We find that the isothermal temperatures vary from 1.6 to 10 MK. These temperatures are an average weighted toward higher temperature plasma. We determine the mass constraints of eruptive plasmas by assuming simplified geometrical structures of the plasma with isothermal plasma temperatures. This method provides an upper limit to the masses of the observed eruptive plasmas in X-ray passbands since any clumping causes the overestimation of the mass. For the other two events, we assume the temperatures are at the maximum temperature of the X-ray Telescope (XRT) temperature response function, which gives a lower limit of the masses. We find that the masses in XRT, ∼3 × 10{sup 13}-5 × 10{sup 14} g, are smaller in their upper limit than the total masses obtained by LASCO, ∼1 × 10{sup 15} g. In addition, we estimate the radiative loss, thermal conduction, thermal, and kinetic energies of the eruptive plasma in X-rays. For four events, we find that the thermal conduction timescales are much shorter than the duration of eruption. This result implies that additional heating during the eruption may be required to explain the plasma observations in X-rays for the four events.

  9. Dual-energy tissue cancellation in mammography with quasi-monochromatic x-rays

    NASA Astrophysics Data System (ADS)

    Marziani, M.; Taibi, A.; Tuffanelli, A.; Gambaccini, M.

    2002-01-01

    Dual-energy radiography has not evolved into a routine clinical examination yet due to intrinsic limitations of both dual-kVp imaging and single-exposure imaging with conventional x-ray sources. The recent introduction of novel quasi-monochromatic x-ray sources and detectors could lead to interesting improvements, especially in mammography where the complex structure of healthy tissues often masks the detectability of lesions. A dual-energy radiography technique based on a tissue cancellation algorithm has been developed for mammography, with the aim of maximizing the low intrinsic contrast of pathologic tissues while being able to minimize or cancel the contrast between glandular and fat tissues. Several images of a plastic test object containing various tissue equivalent inserts were acquired in the energy range 17-36 keV using a quasi-monochromatic x-ray source and a scintillator-coated CCD detector. Images acquired at high and low energies were non-linearly combined to generate two energy-independent basis images. Suitable linear combinations of these two basis images result in the elimination of the contrast of a given material with respect to another. This makes it possible to selectively cancel certain details in the processed image.

  10. Characterization of energy response for photon-counting detectors using x-ray fluorescence

    PubMed Central

    Ding, Huanjun; Cho, Hyo-Min; Barber, William C.; Iwanczyk, Jan S.; Molloi, Sabee

    2014-01-01

    Purpose: To investigate the feasibility of characterizing a Si strip photon-counting detector using x-ray fluorescence. Methods: X-ray fluorescence was generated by using a pencil beam from a tungsten anode x-ray tube with 2 mm Al filtration. Spectra were acquired at 90° from the primary beam direction with an energy-resolved photon-counting detector based on an edge illuminated Si strip detector. The distances from the source to target and the target to detector were approximately 19 and 11 cm, respectively. Four different materials, containing silver (Ag), iodine (I), barium (Ba), and gadolinium (Gd), were placed in small plastic containers with a diameter of approximately 0.7 cm for x-ray fluorescence measurements. Linear regression analysis was performed to derive the gain and offset values for the correlation between the measured fluorescence peak center and the known fluorescence energies. The energy resolutions and charge-sharing fractions were also obtained from analytical fittings of the recorded fluorescence spectra. An analytical model, which employed four parameters that can be determined from the fluorescence calibration, was used to estimate the detector response function. Results: Strong fluorescence signals of all four target materials were recorded with the investigated geometry for the Si strip detector. The average gain and offset of all pixels for detector energy calibration were determined to be 6.95 mV/keV and −66.33 mV, respectively. The detector’s energy resolution remained at approximately 2.7 keV for low energies, and increased slightly at 45 keV. The average charge-sharing fraction was estimated to be 36% within the investigated energy range of 20–45 keV. The simulated detector output based on the proposed response function agreed well with the experimental measurement. Conclusions: The performance of a spectral imaging system using energy-resolved photon-counting detectors is very dependent on the energy calibration of the

  11. Characterization of energy response for photon-counting detectors using x-ray fluorescence

    SciTech Connect

    Ding, Huanjun; Cho, Hyo-Min; Molloi, Sabee; Barber, William C.; Iwanczyk, Jan S.

    2014-12-15

    Purpose: To investigate the feasibility of characterizing a Si strip photon-counting detector using x-ray fluorescence. Methods: X-ray fluorescence was generated by using a pencil beam from a tungsten anode x-ray tube with 2 mm Al filtration. Spectra were acquired at 90° from the primary beam direction with an energy-resolved photon-counting detector based on an edge illuminated Si strip detector. The distances from the source to target and the target to detector were approximately 19 and 11 cm, respectively. Four different materials, containing silver (Ag), iodine (I), barium (Ba), and gadolinium (Gd), were placed in small plastic containers with a diameter of approximately 0.7 cm for x-ray fluorescence measurements. Linear regression analysis was performed to derive the gain and offset values for the correlation between the measured fluorescence peak center and the known fluorescence energies. The energy resolutions and charge-sharing fractions were also obtained from analytical fittings of the recorded fluorescence spectra. An analytical model, which employed four parameters that can be determined from the fluorescence calibration, was used to estimate the detector response function. Results: Strong fluorescence signals of all four target materials were recorded with the investigated geometry for the Si strip detector. The average gain and offset of all pixels for detector energy calibration were determined to be 6.95 mV/keV and −66.33 mV, respectively. The detector’s energy resolution remained at approximately 2.7 keV for low energies, and increased slightly at 45 keV. The average charge-sharing fraction was estimated to be 36% within the investigated energy range of 20–45 keV. The simulated detector output based on the proposed response function agreed well with the experimental measurement. Conclusions: The performance of a spectral imaging system using energy-resolved photon-counting detectors is very dependent on the energy calibration of the

  12. X-ray photo-emission and energy dispersive spectroscopy of HA coated titanium

    SciTech Connect

    Drummond, J.L.; Steinberg, A.D.; Krauss, A.R.

    1997-08-01

    The purpose of this study was to determine the chemical composition changes of hydroxyapatite (HA) coated titanium using surface analysis (x-ray photo-emission) and bulk analysis (energy dispersive spectroscopy). The specimens examined were controls, 30 minutes and 3 hours aged specimens in distilled water or 0.2M sodium phosphate buffer (pH 7.2) at room temperature. Each x-ray photo-emission cycle consisted of 3 scans followed by argon sputtering for 10 minutes for a total of usually 20 cycles, corresponding to a sampling depth of {approximately} 1500 {angstrom}. The energy dispersive spectroscopy analysis was on a 110 by 90 {mu}m area for 500 sec. Scanning electron microscopy examination showed crystal formation (3P{sub 2}O{sub 5}*2CAO*?H{sub 2}O by energy dispersive spectroscopy analysis) on the HA coating for the specimens aged in sodium phosphate buffer. The x-ray photo-emission results indicated the oxidation effect of water on the titanium (as TiO{sub 2}) and the effect of the buffer to increase the surface concentration of phosphorous. No differences in the chemical composition were observed by energy dispersive spectroscopy analysis. The crystal growth was only observed for the sodium phosphate buffer specimens and only on the HA surface.

  13. Techniques for deriving tissue structure from multiple projection dual-energy x-ray absorptiometry

    NASA Technical Reports Server (NTRS)

    Charles, Jr., Harry K. (Inventor); Beck, Thomas J. (Inventor); Feldmesser, Howard S. (Inventor); Magee, Thomas C. (Inventor)

    2004-01-01

    Techniques for deriving bone properties from images generated by a dual-energy x-ray absorptiometry apparatus include receiving first image data having pixels indicating bone mineral density projected at a first angle of a plurality of projection angles. Second image data and third image data are also received. The second image data indicates bone mineral density projected at a different second angle. The third image data indicates bone mineral density projected at a third angle. The third angle is different from the first angle and the second angle. Principal moments of inertia for a bone in the subject are computed based on the first image data, the second image data and the third image data. The techniques allow high-precision, high-resolution dual-energy x-ray attenuation images to be used for computing principal moments of inertia and strength moduli of individual bones, plus risk of injury and changes in risk of injury to a patient.

  14. Structured photocathodes for improved high-energy x-ray efficiency in streak cameras

    NASA Astrophysics Data System (ADS)

    Opachich, Y. P.; Bell, P. M.; Bradley, D. K.; Chen, N.; Feng, J.; Gopal, A.; Hatch, B.; Hilsabeck, T. J.; Huffman, E.; Koch, J. A.; Landen, O. L.; MacPhee, A. G.; Nagel, S. R.; Udin, S.

    2016-11-01

    We have designed and fabricated a structured streak camera photocathode to provide enhanced efficiency for high energy X-rays (1-12 keV). This gold coated photocathode was tested in a streak camera and compared side by side against a conventional flat thin film photocathode. Results show that the measured electron yield enhancement at energies ranging from 1 to 10 keV scales well with predictions, and that the total enhancement can be more than 3×. The spatial resolution of the streak camera does not show degradation in the structured region. We predict that the temporal resolution of the detector will also not be affected as it is currently dominated by the slit width. This demonstration with Au motivates exploration of comparable enhancements with CsI and may revolutionize X-ray streak camera photocathode design.

  15. A high resolution gas scintillation proportional counter for studying low energy cosmic X-ray sources

    NASA Technical Reports Server (NTRS)

    Hamilton, T. T.; Hailey, C. J.; Ku, W. H.-M.; Novick, R.

    1980-01-01

    In recent years much effort has been devoted to the development of large area gas scintillation proportional counters (GSPCs) suitable for use in X-ray astronomy. The paper deals with a low-energy GSPC for use in detecting sub-keV X-rays from cosmic sources. This instrument has a measured energy resolution of 85 eV (FWHM) at 149 eV over a sensitive area of 5 sq cm. The development of imaging capability for this instrument is discussed. Tests are performed on the feasibility of using an arrangement of several phototubes placed adjacent to one another to determine event locations in a large flat counter. A simple prototype has been constructed and successfully operated.

  16. Scanning electron microscope/energy dispersive x ray analysis of impact residues in LDEF tray clamps

    NASA Technical Reports Server (NTRS)

    Bernhard, Ronald P.; Durin, Christian; Zolensky, Michael E.

    1993-01-01

    Detailed optical scanning of tray clamps is being conducted in the Facility for the Optical Inspection of Large Surfaces at JSC to locate and document impacts as small as 40 microns in diameter. Residues from selected impacts are then being characterized by Scanning Electron Microscopy/Energy Dispersive X-ray Analysis at CNES. Results from this analysis will be the initial step to classifying projectile residues into specific sources.

  17. AAS HIGH-ENERGY ASTROPHYSICS DIVISION: X-rays Hit the Spot for Astrophysicists.

    PubMed

    Irion, R

    2000-12-01

    About 500 astronomers flocked to Waikiki Beach from 6 to 10 November for a meeting of the American Astronomical Society's High-Energy Astrophysics Division. Looking splendid in their complimentary aloha shirts, speakers told tales of intense radiation from deep space, including x-rays from baby stars and from quasars, which could help refine estimates of how quickly the universe is expanding. PMID:17742051

  18. The medium sensitivity survey - A new sample of X-ray sources with optical identifications and the revised extragalactic log N-log S

    NASA Technical Reports Server (NTRS)

    Gioia, I. M.; Maccacaro, T.; Schild, R. E.; Stocke, J. T.; Liebert, J. W.; Danziger, I. J.; Kunth, D.; Lub, J.

    1984-01-01

    Maccacaro et al. (1982) surveyed approximately 50 sq deg in different regions of the sky at medium sensitivity flux levels intermediate between the Uhuru/Ariel V limit and the Einstein deep survey limit. This 'first' medium sensitivity survey (MSS 1) was primarily aimed at the analysis of the source-count relation for extragalactic X-ray sources. The present investigation is concerned with an extension of the MSS 1 on the basis of an analysis of new fields obtained with the aid of the Imaging Proportional Counter (IPC) on board the Einstein Observatory. A parallel optical program to identify all the new sources was also undertaken. X-ray and optical data are presented for this 'second' complete sample of medium sensitivity survey X-ray sources (MSS 2). The log N-log S relation is derived and discussed.

  19. COASTING EXTERNAL SHOCK IN WIND MEDIUM: AN ORIGIN FOR THE X-RAY PLATEAU DECAY COMPONENT IN SWIFT GAMMA-RAY BURST AFTERGLOWS

    SciTech Connect

    Shen Rongfeng; Matzner, Christopher D. E-mail: matzner@astro.utoronto.ca

    2012-01-01

    The plateaus observed in about one half of the early X-ray afterglows are the most puzzling feature in gamma-ray bursts (GRBs) detected by Swift. By analyzing the temporal and spectral indices of a large X-ray plateau sample, we find that 55% can be explained by external, forward shock synchrotron emission produced by a relativistic ejecta coasting in a {rho}{proportional_to}r{sup -2}, wind-like medium; no energy injection into the shock is needed. After the ejecta collects enough medium and transitions to the adiabatic, decelerating blast wave phase, it produces the post-plateau decay. For those bursts consistent with this model, we find an upper limit for the initial Lorentz factor of the ejecta, {Gamma}{sub 0} {<=} 46({epsilon}{sub e}/0.1){sup -0.24}({epsilon}{sub B}/0.01){sup 0.17}; the isotropic equivalent total ejecta energy is E{sub iso} {approx} 10{sup 53}({epsilon}{sub e}/0.1){sup -1.3}({epsilon}{sub B}/0.01){sup -0.09}(t{sub b} /10{sup 4} s) erg, where {epsilon}{sub e} and {epsilon}{sub B} are the fractions of the total energy at the shock downstream that are carried by electrons and the magnetic field, respectively, and t{sub b} is the end of the plateau. Our finding supports Wolf-Rayet stars as the progenitor stars of some GRBs. It raises intriguing questions about the origin of an intermediate-{Gamma}{sub 0} ejecta, which we speculate is connected to the GRB jet emergence from its host star. For the remaining 45% of the sample, the post-plateau decline is too rapid to be explained in the coasting-in-wind model, and energy injection appears to be required.

  20. HIGH ENERGY, HIGH BRIGHTNESS X-RAYS PRODUCED BY COMPTON BACKSCATTERING AT THE LIVERMORE PLEIADES FACILITY

    SciTech Connect

    Tremaine, A M; Anderson, S G; Betts, S; Crane, J; Gibson, D J; Hartemann, F V; Jacob, J S; Frigola, P; Lim, J; Rosenzweig, J; Travish, G

    2005-05-19

    PLEIADES (Picosecond Laser Electron Interaction for the Dynamic Evaluation of Structures) produces tunable 30-140 keV x-rays with 0.3-5 ps pulse lengths and up to 10{sup 7} photons/pulse by colliding a high brightness electron beam with a high power laser. The electron beam is created by an rf photo-injector system, accelerated by a 120 MeV linac, and focused to 20 {micro}m with novel permanent magnet quadrupoles. To produce Compton back scattered x-rays, the electron bunch is overlapped with a Ti:Sapphire laser that delivers 500 mJ, 100 fs, pulses to the interaction point. K-edge radiography at 115 keV on Uranium has verified the angle correlated energy spectrum inherent in Compton scattering and high-energy tunability of the Livermore source. Current upgrades to the facility will allow laser pumping of targets synchronized to the x-ray source enabling dynamic diffraction and time-resolved studies of high Z materials. Near future plans include extending the radiation energies to >400 keV, allowing for nuclear fluorescence studies of materials.

  1. Bone calcium/phosphorus ratio determination using dual energy X-ray method.

    PubMed

    Sotiropoulou, P; Fountos, G; Martini, N; Koukou, V; Michail, C; Kandarakis, I; Nikiforidis, G

    2015-05-01

    Non-invasive dual energy methods have been used extensively on osteoporosis diagnosis estimating parameters, such as, Bone Mineral Density (BMD) and Bone Mineral Content (BMC). In this study, an X-ray dual energy method (XRDE) was developed for the estimation of the bone Calcium-to-Phosphorous (Ca/P) mass ratio, as a bone quality index. The optimized irradiation parameters were assessed by performing analytical model simulations. X-ray tube output, filter material and thickness were used as input parameters. A single exposure technique, combined with K-edge filtering, was applied. The optimal X-ray spectra were selected according to the resulted precision and accuracy values. Experimental evaluation was performed on an XRDE system incorporating a Cadmium Telluride (CdTe) photon counting detector and three bone phantoms with different nominal mass Ca/P ratios. Additionally, the phantoms' mass Ca/P ratios were validated with energy-dispersive X-ray spectroscopy (EDX). Simulation results showed that the optimum filter atomic number (Z) ranges between 57 and 70. The optimum spectrum was obtained at 100 kVp, filtered with Cerium (Ce), with a surface density of 0.88 g/cm(2). All Ca/P ratio measurements were found to be accurate to within 1.6% of the nominal values, while the precision ranged between 0.91 and 1.37%. The accuracy and precision values of the proposed non-invasive method contributes to the assessment of the bone quality state through the mass Ca/P ratio determination.

  2. Star Factory Near Galactic Center Bathed In High-Energy X-Rays

    NASA Astrophysics Data System (ADS)

    2001-06-01

    Near the crowded core of the Milky Way galaxy, where stars shine so brightly and plentifully that planets there would never experience nighttime, astronomers have found a new phenomenon: a cauldron of 60-million-degree gas enveloping a cluster of young stars. Professor Farhad Zadeh of Northwestern University and his collaborators used NASA's Chandra X-ray Observatory to trace the gas around the Arches cluster, a well-studied region of star formation that is home to some of our Galaxy's largest and youngest stars. "This is the first time we have seen a young cluster of stars surrounded by such a halo of high-energy X-rays," said Zadeh in a press conference at the American Astronomical Society in Pasadena, CA. "This supports theoretical predictions that stellar winds from massive stars can collide with each other and generate very hot gas." Massive stars, newborn stars, and stellar winds have long been known to emit X-rays. The Chandra results are significant because they identify this new type of mechanism of colliding winds to generate X-rays as energetic as those seen in distant starburst galaxies, which are known for their furious pace of star production. The Arches cluster is about 26,000 light years from Earth and only about 1 to 2 million years old. It is also less than 100 light years from what is thought to be a supermassive black hole in the center of our Galaxy. The cluster contains 150 hot, young stars, known as "O" stars, concentrated within a diameter of one light year, making it the most compact cluster known in the Milky Way galaxy. The density of stars makes the region in and around the Arches cluster a microcosm of what is likely occurring in starburst galaxies. "The Arches cluster is one of the best 'local' analogues of starburst galaxies-- the most prodigious stellar nurseries known," said Casey Law of the Harvard-Smithsonian Center for Astrophysics. "Yet the Arches cluster is in our backyard, not millions of light years away." The Arches Cluster

  3. Nonthermal X-ray Spectral Flattening toward Low Energies in Early Impulsive Flares

    NASA Technical Reports Server (NTRS)

    Holman, Gordon D.

    2007-01-01

    The determination of the low-energy cutoff to nonthermal electron distributions is critical to the calculation of the nonthermal energy in solar flares. The most direct evidence for low-energy cutoffs is flattening of the power-law, nontherma1 X-ray spectra at low energies. However, because of the plasma preheating often seen in flares, the thermal emissions at low energies may hide such spectral flattening of the nonthermal component. We select a category of flares, which we call "early impulsive flares", in which the > 25 keV hard X-ray (HXR) flux increase is delayed by less than 30 s after the flux increase at lower energies. Thus, the plasma preheating in these flares is minimal, so the nonthermal spectrum can be determined to lower energies than in flares with significant preheating. Out of a sample of 33 early impulsive flares observed by the Ramaty High Energy Solar Spectroscopy Imager (RHESSI), 9 showed spectral flattening toward low energies. In these events, the break energy of the double power-law fit to the HXR spectra lies in the range of 10-50 keV, significantly lower than the value we have seen for other flares that do not show such early impulsive emissions. In particular, it correlates with the HXR flux. After correcting the spatially-integrated spectra for albedo from isotropically emitted X-rays and using RHESSI imaging spectroscopy to exclude the extended albedo halo, we find that albedo associated with isotropic or nearly isotropic electrons can only account for the spectral flattening in 3 flares near Sun center. The spectral flattening in the remaining 6 flares is found to be consistent with the existence of a low-energy cutoff in the electron spectrum, falling in the range of 15-50 keV, which also correlates with the HXR flux.

  4. Microstructures for high-energy x-ray and particle-imaging applications

    SciTech Connect

    Ceglio, N.M.; Stone, G.F.; Hawryluk, A.M.

    1981-05-01

    Coded imaging techniques using thick, micro-Fresnel zone plates as coded apertures have been used to image x-ray emissions (2-20 keV) and 3.5 MeV Alpha particle emissions from laser driven micro-implosions. Image resolution in these experiments was 3-8 ..mu..m. Extension of this coded imaging capability to higher energy x-rays (approx. 100 keV) and more penetrating charged particles (e.g. approx. 15 MeV protons) requires the fabrication of very thick (50-200 ..mu..m), high aspect ratio (10:1), gold Fresnel zone plates with narrow linewidths (5-25 ..mu..m) for use as coded aperatures. A reactive ion etch technique in oxygen has been used to produce thick zone plate patterns in polymer films. The polymer patterns serve as electroplating molds for the subsequent fabrication of the free-standing gold zone plate structures.

  5. Gas Scintillation Proportional Counters for High-Energy X-ray Astronomy

    NASA Technical Reports Server (NTRS)

    Gubarev, Mikhail; Ramsey, Brian; Apple, Jeffery

    2003-01-01

    A focal plane array of high-pressure gas scintillation proportional counters (GSPC) for a balloon-borne hard-x-ray telescope is under development at the Marshall Space Flight Center. These detectors have an active area of approx. 20 sq cm, and are filled with a high pressure (10(exp 6) Pa) xenon-helium mixture. Imaging is via crossed-grid position-sensitive phototubes sensitive in the UV region. The performance of the GSPC is well matched to that of the telescopes x-ray optics which have response to 75 keV and a focal spot size of approx. 500 microns. The detector s energy resolution, 4% FWHM at 60 keV, is adequate for resolving the broad spectral lines of astrophysical importance and for accurate continuum measurements. Full details of the instrument and its performance will be provided.

  6. Crystallographic Characterization of Extraterrestrial Materials by Energy-Scanning X-ray Diffraction

    NASA Technical Reports Server (NTRS)

    Hagiya, Kenji; Mikouchi, Takashi; Ohsumi, Kazumasa; Terada, Yasuko; Yagi, Naoto; Komatsu, Mutsumi; Yamaguchi, Shoki; Hirata, Arashi; Kurokawa, Ayaka; Zolensky, Michael E. (Principal Investigator)

    2016-01-01

    We have continued our long-term project using X-ray diffraction to characterize a wide range of extraterrestrial samples. The stationary sample method with polychromatic X-rays is advantageous because the irradiated area of the sample is always same and fixed, meaning that all diffraction spots occur from the same area of the sample, however, unit cell parameters cannot be directly obtained by this method though they are very important for identification of mineral and for determination of crystal structures. In order to obtain the cell parameters even in the case of the sample stationary method, we apply energy scanning of a micro-beam of monochromatic SR at SPring-8.

  7. Fast scattering simulation tool for multi-energy x-ray imaging

    NASA Astrophysics Data System (ADS)

    Sossin, A.; Tabary, J.; Rebuffel, V.; Létang, J. M.; Freud, N.; Verger, L.

    2015-12-01

    A combination of Monte Carlo (MC) and deterministic approaches was employed as a means of creating a simulation tool capable of providing energy resolved x-ray primary and scatter images within a reasonable time interval. Libraries of Sindbad, a previously developed x-ray simulation software, were used in the development. The scatter simulation capabilities of the tool were validated through simulation with the aid of GATE and through experimentation by using a spectrometric CdTe detector. A simple cylindrical phantom with cavities and an aluminum insert was used. Cross-validation with GATE showed good agreement with a global spatial error of 1.5% and a maximum scatter spectrum error of around 6%. Experimental validation also supported the accuracy of the simulations obtained from the developed software with a global spatial error of 1.8% and a maximum error of around 8.5% in the scatter spectra.

  8. High energy X-ray photon counting imaging using linear accelerator and silicon strip detectors

    NASA Astrophysics Data System (ADS)

    Tian, Y.; Shimazoe, K.; Yan, X.; Ueda, O.; Ishikura, T.; Fujiwara, T.; Uesaka, M.; Ohno, M.; Tomita, H.; Yoshihara, Y.; Takahashi, H.

    2016-09-01

    A photon counting imaging detector system for high energy X-rays is developed for on-site non-destructive testing of thick objects. One-dimensional silicon strip (1 mm pitch) detectors are stacked to form a two-dimensional edge-on module. Each detector is connected to a 48-channel application specific integrated circuit (ASIC). The threshold-triggered events are recorded by a field programmable gate array based counter in each channel. The detector prototype is tested using 950 kV linear accelerator X-rays. The fast CR shaper (300 ns pulse width) of the ASIC makes it possible to deal with the high instant count rate during the 2 μs beam pulse. The preliminary imaging results of several metal and concrete samples are demonstrated.

  9. Residual strain gradient determination in metal matrix composites by synchrotron X-ray energy dispersive diffraction

    NASA Technical Reports Server (NTRS)

    Kuntz, Todd A.; Wadley, Haydn N. G.; Black, David R.

    1993-01-01

    An X-ray technique for the measurement of internal residual strain gradients near the continuous reinforcements of metal matrix composites has been investigated. The technique utilizes high intensity white X-ray radiation from a synchrotron radiation source to obtain energy spectra from small (0.001 cu mm) volumes deep within composite samples. The viability of the technique was tested using a model system with 800 micron Al203 fibers and a commercial purity titanium matrix. Good agreement was observed between the measured residual radial and hoop strain gradients and those estimated from a simple elastic concentric cylinders model. The technique was then used to assess the strains near (SCS-6) silicon carbide fibers in a Ti-14Al-21Nb matrix after consolidation processing. Reasonable agreement between measured and calculated strains was seen provided the probe volume was located 50 microns or more from the fiber/matrix interface.

  10. Focal plane transport assembly controls for the High Energy Astronomy Observatory X-ray telescope

    NASA Technical Reports Server (NTRS)

    Carpenter, C.; Strizhak, E.; Brissette, R.

    1979-01-01

    The High Energy Astronomy Observatory - Mission B (HEAO-B) is a satellite observatory for the purpose of performing a detailed X-ray survey of the celestial sphere. Measurements will be made of stellar radiation in the range of 0.2 to 20 keV. The central part of the Observatory is an X-ray telescope, into the focus of which a variety of imaging instruments and spectrographs may be introduced. The telescope has a resolution of about 1 arc second, so that the instruments must be placed with extreme precision. This is obtained by a mechanical system of toggles and stops and a motor drive system controlled by a position sensing potentiometer with a resolution of about 1.5 degrees

  11. Multiple energy computed tomography with monochromatic x rays from the NSLS

    SciTech Connect

    Dilmanian, F.A.; Nachaliel, E.; Garrett, R.F.; Thomlinson, W.C.; Chapman, L.D.; Moulin, H.R.; Oversluizen, T.; Rarback, H.M.; Rivers, M.; Spanne, P.; Thompson, A.C.; Zeman, H.D.

    1991-12-31

    We used monochromatic x rays from the X17 superconducting wiggler beamline at the National Synchrotron Light Source (NSLS), Brookhaven National Laboratory, for dual-energy quantitative computed tomography (CT) of a 27 mm-diameter phantom containing solutions of different KOH concentrations in cylindrical holes of 5-mm diameter. The CT configuration was a fixed horizontal fan-shaped beam of 1.5 mm height and 30 mm width, and a subject rotating around a vertical axis. The transmitted x rays were detected by a linear-array Si(Li) detector with 120 elements of 0.25 mm width each. We used a two-crystal Bragg-Bragg fixed-exit monochromator with Si<220> crystals. Dual photon absorptiometry (DPA) CT data were taken at 20 and 38 keV. The reconstructed phantom images show the potential of the system for quantitative CT.

  12. X-ray Spectrometry.

    ERIC Educational Resources Information Center

    Markowicz, Andrzej A.; Van Grieken, Rene E.

    1984-01-01

    Provided is a selective literature survey of X-ray spectrometry from late 1981 to late 1983. Literature examined focuses on: excitation (photon and electron excitation and particle-induced X-ray emission; detection (wavelength-dispersive and energy-dispersive spectrometry); instrumentation and techniques; and on such quantitative analytical…

  13. Large-aperture prism-array lens for high-energy X-ray focusing.

    PubMed

    Zhang, Weiwei; Liu, Jing; Chang, Guangcai; Shi, Zhan; Li, Ming; Ren, Yuqi; Zhang, Xiaowei; Yi, Futing; Liu, Peng; Sheng, Weifan

    2016-09-01

    A new prism-array lens for high-energy X-ray focusing has been constructed using an array of different prisms obtained from different parabolic structures by removal of passive parts of material leading to a multiple of 2π phase variation. Under the thin-lens approximation the phase changes caused by this lens for a plane wave are exactly the same as those caused by a parabolic lens without any additional corrections when they have the same focal length, which will provide good focusing; at the same time, the total transmission and effective aperture of this lens are both larger than those of a compound kinoform lens with the same focal length, geometrical aperture and feature size. This geometry can have a large aperture that is not limited by the feature size of the lens. Prototype nickel lenses with an aperture of 1.77 mm and focal length of 3 m were fabricated by LIGA technology, and were tested using CCD camera and knife-edge scan method at the X-ray Imaging and Biomedical Application Beamline BL13W1 at Shanghai Synchrotron Radiation Facility, and provided a focal width of 7.7 µm and a photon flux gain of 14 at an X-ray energy of 50 keV. PMID:27577761

  14. Quantitative energy-dispersive x-ray diffraction for identification of counterfeit medicines: a preliminary study

    NASA Astrophysics Data System (ADS)

    Crews, Chiaki C. E.; O'Flynn, Daniel; Sidebottom, Aiden; Speller, Robert D.

    2015-06-01

    The prevalence of counterfeit and substandard medicines has been growing rapidly over the past decade, and fast, nondestructive techniques for their detection are urgently needed to counter this trend. In this study, energy-dispersive X-ray diffraction (EDXRD) combined with chemometrics was assessed for its effectiveness in quantitative analysis of compressed powder mixtures. Although EDXRD produces lower-resolution diffraction patterns than angular-dispersive X-ray diffraction (ADXRD), it is of interest for this application as it carries the advantage of allowing the analysis of tablets within their packaging, due to the higher energy X-rays used. A series of caffeine, paracetamol and microcrystalline cellulose mixtures were prepared with compositions between 0 - 100 weight% in 20 weight% steps (22 samples in total, including a centroid mixture), and were pressed into tablets. EDXRD spectra were collected in triplicate, and a principal component analysis (PCA) separated these into their correct positions in the ternary mixture design. A partial least-squares (PLS) regression model calibrated using this training set was validated using both segmented cross-validation, and with a test set of six samples (mixtures in 8:1:1 and 5⅓:2⅓:2⅓ ratios) - the latter giving a root-mean square error of prediction (RMSEP) of 1.30, 2.25 and 2.03 weight% for caffeine, paracetamol and cellulose respectively. These initial results are promising, with RMSEP values on a par with those reported in the ADXRD literature.

  15. High-energy x-ray grating-based phase-contrast radiography of human anatomy

    NASA Astrophysics Data System (ADS)

    Horn, Florian; Hauke, Christian; Lachner, Sebastian; Ludwig, Veronika; Pelzer, Georg; Rieger, Jens; Schuster, Max; Seifert, Maria; Wandner, Johannes; Wolf, Andreas; Michel, Thilo; Anton, Gisela

    2016-03-01

    X-ray grating-based phase-contrast Talbot-Lau interferometry is a promising imaging technology that has the potential to raise soft tissue contrast in comparison to conventional attenuation-based imaging. Additionally, it is sensitive to attenuation, refraction and scattering of the radiation and thus provides complementary and otherwise inaccessible information due to the dark-field image, which shows the sub-pixel size granularity of the measured object. Until recent progress the method has been mainly limited to photon energies below 40 keV. Scaling the method to photon energies that are sufficient to pass large and spacious objects represents a challenging task. This is caused by increasing demands regarding the fabrication process of the gratings and the broad spectra that come along with the use of polychromatic X-ray sources operated at high acceleration voltages. We designed a setup that is capable to reach high visibilities in the range from 50 to 120 kV. Therefore, spacious and dense parts of the human body with high attenuation can be measured, such as a human knee. The authors will show investigations on the resulting attenuation, differential phase-contrast and dark-field images. The images experimentally show that X-ray grating-based phase-contrast radiography is feasible with highly absorbing parts of the human body containing massive bones.

  16. Usefulness of an energy-binned photon-counting x-ray detector for dental panoramic radiographs

    NASA Astrophysics Data System (ADS)

    Fukui, Tatsumasa; Katsumata, Akitoshi; Ogawa, Koichi; Fujiwara, Shuu

    2015-03-01

    A newly developed dental panoramic radiography system is equipped with a photon-counting semiconductor detector. This photon-counting detector acquires transparent X-ray beams by dividing them into several energy bands. We developed a method to identify dental materials in the patient's teeth by means of the X-ray energy analysis of panoramic radiographs. We tested various dental materials including gold alloy, dental amalgam, dental cement, and titanium. The results of this study suggest that X-ray energy scattergram analysis could be used to identify a range of dental materials in a patient's panoramic radiograph.

  17. Ultrahigh energy resolution focusing monochromator for inelastic x-ray scattering spectrometer.

    PubMed

    Suvorov, Alexey; Cunsolo, Alessandro; Chubar, Oleg; Cai, Yong Q

    2015-11-30

    A further development of a focusing monochromator concept for X-ray energy resolution of 0.1 meV and below is presented. Theoretical analysis of several optical layouts based on this concept was supported by numerical simulations performed in the "Synchrotron Radiation Workshop" software package using the physical-optics approach and careful modeling of partially-coherent synchrotron (undulator) radiation. Along with the energy resolution, the spectral shape of the energy resolution function was investigated. It was shown that under certain conditions the decay of the resolution function tails can be faster than that of the Gaussian function.

  18. X-ray spectroscopy studies of nonradiative energy transfer processes in luminescent lanthanide materials

    NASA Astrophysics Data System (ADS)

    Pacold, Joseph I.

    Luminescent materials play important roles in energy sciences, through solid state lighting and possible applications in solar energy utilization, and in biomedical research and applications, such as in immunoassays and fluorescence microscopy. The initial excitation of a luminescent material leads to a sequence of transitions between excited states, ideally ending with the emission of one or more optical-wavelength photons. It is essential to understand the microscopic physics of this excited state cascade in order to rationally design materials with high quantum efficiencies or with other fine-tuning of materials response. While optical-wavelength spectroscopies have unraveled many details of the energy transfer pathways in luminescent materials, significant questions remain open for many lanthanide-based luminescent materials. For organometallic dyes in particular, quantum yields remain limited in comparison with inorganic phosphors. This dissertation reports on a research program of synchrotron x-ray studies of the excited state electronic structure and energy-relaxation cascade in trivalent lanthanide phosphors and dyes. To this end, one of the primary results presented here is the first time-resolved x-ray absorption near edge spectroscopy studies of the transient 4f excited states in lanthanide-activated luminescent dyes and phosphors. This is a new application of time-resolved x-ray absorption spectroscopy that makes it possible to directly observe and, to some extent, quantify intramolecular nonradiative energy transfer processes. We find a transient increase in 4f spectral weight associated with an excited state confined to the 4f shell of trivalent Eu. This result implies that it is necessary to revise the current theoretical understanding of 4f excitation in trivalent lanthanide activators: either transient 4f-5d mixing effects are much stronger than previously considered, or else the lanthanide 4f excited state has an unexpectedly large contribution

  19. Near optimal energy selective x-ray imaging system performance with simple detectors

    SciTech Connect

    Alvarez, Robert E.

    2010-02-15

    Purpose: This article describes a method to achieve near optimal performance with low energy resolution detectors. Tapiovaara and Wagner [Phys. Med. Biol. 30, 519-529 (1985)] showed that an energy selective x-ray system using a broad spectrum source can produce images with a larger signal to noise ratio (SNR) than conventional systems using energy integrating or photon counting detectors. They showed that there is an upper limit to the SNR and that it can be achieved by measuring full spectrum information and then using an optimal energy dependent weighting. Methods: A performance measure is derived by applying statistical detection theory to an abstract vector space of the line integrals of the basis set coefficients of the two function approximation to the x-ray attenuation coefficient. The approach produces optimal results that utilize all the available energy dependent data. The method can be used with any energy selective detector and is applied not only to detectors using pulse height analysis (PHA) but also to a detector that simultaneously measures the total photon number and integrated energy, as discussed by Roessl et al. [Med. Phys. 34, 959-966 (2007)]. A generalization of this detector that improves the performance is introduced. A method is described to compute images with the optimal SNR using projections in a ''whitened'' vector space transformed so the noise is uncorrelated and has unit variance in both coordinates. Material canceled images with optimal SNR can also be computed by projections in this space. Results: The performance measure is validated by showing that it provides the Tapiovaara-Wagner optimal results for a detector with full energy information and also a conventional detector. The performance with different types of detectors is compared to the ideal SNR as a function of x-ray tube voltage and subject thickness. A detector that combines two bin PHA with a simultaneous measurement of integrated photon energy provides near ideal

  20. X-ray spectroscopy for chemical and energy sciences: the case of heterogeneous catalysis.

    PubMed

    Frenkel, Anatoly I; van Bokhoven, Jeroen A

    2014-09-01

    Heterogeneous catalysis is the enabling technology for much of the current and future processes relevant for energy conversion and chemicals synthesis. The development of new materials and processes is greatly helped by the understanding of the catalytic process at the molecular level on the macro/micro-kinetic time scale and on that of the actual bond breaking and bond making. The performance of heterogeneous catalysts is inherently the average over the ensemble of active sites. Much development aims at unravelling the structure of the active site; however, in general, these methods yield the ensemble-average structure. A benefit of X-ray-based methods is the large penetration depth of the X-rays, enabling in situ and operando measurements. The potential of X-ray absorption and emission spectroscopy methods (XANES, EXAFS, HERFD, RIXS and HEROS) to directly measure the structure of the catalytically active site at the single nanoparticle level using nanometer beams at diffraction-limited storage ring sources is highlighted. The use of pump-probe schemes coupled with single-shot experiments will extend the time range from the micro/macro-kinetic time domain to the time scale of bond breaking and making. PMID:25177997

  1. X-ray Spectroscopy for Chemical and Energy Sciences. the Case of Heterogeneous Catalysis

    SciTech Connect

    Frenkel, A. I.; van Bokhoven, J. A.

    2014-09-01

    Heterogeneous catalysis is the enabling technology for much of the current and future processes relevant for energy conversion and chemicals synthesis. The development of new materials and processes is greatly helped by the understanding of the catalytic process at the molecular level on the macro/micro-kinetic time scale and on that of the actual bond breaking and bond making. The performance of heterogeneous catalysts is inherently the average over the ensemble of active sites. Much development aims at unravelling the structure of the active site; however, in general, these methods yield the ensemble-average structure. A benefit of X-ray-based methods is the large penetration depth of the X-rays, enabling in situ and operando measurements. Furthermore, the potential of X-ray absorption and emission spectroscopy methods (XANES, EXAFS, HERFD, RIXS and HEROS) to directly measure the structure of the catalytically active site at the single nanoparticle level using nanometer beams at diffraction-limited storage ring sources is highlighted. Use of pump-probe schemes coupled with single-shot experiments will extend the time range from the micro/macro-kinetic time domain to the time scale of bond breaking and making.

  2. The UCSD high energy X-ray timing experiment cosmic ray particle anticoincidence detector

    NASA Technical Reports Server (NTRS)

    Hink, P. L.; Rothschild, R. E.; Pelling, M. R.; Macdonald, D. R.; Gruber, D. E.

    1991-01-01

    The HEXTE, part of the X-Ray Timing Explorer (XTE), is designed to make high sensitivity temporal and spectral measurements of X-rays with energies between 15 and 250 keV using NaI/CsI phoswich scintillation counters. To achieve the required sensitivity it is necessary to provide anticoincidence of charged cosmic ray particles incident upon the instrument, some of which interact to produce background X-rays. The proposed cosmic ray particle anticoincidence shield detector for HEXTE uses a novel design based on plastic scintillators and wavelength-shifter bars. It consists of five segments, each with a 7 mm thick plastic scintillator, roughly 50 cm x 50 cm in size, coupled to two wavelength-shifter bars viewed by 1/2 inch photomultiplier tubes. These segments are configured into a five-sided, box-like structure around the main detector system. Results of laboratory testing of a model segment, and calculations of the expected performance of the flight segments and particle anticoincidence detector system are presented to demonstrate that the above anticoincidence detector system satisfies its scientific requirements.

  3. X-ray generator

    DOEpatents

    Dawson, John M.

    1976-01-01

    Apparatus and method for producing coherent secondary x-rays that are controlled as to direction by illuminating a mixture of high z and low z gases with an intense burst of primary x-rays. The primary x-rays are produced with a laser activated plasma, and these x-rays strip off the electrons of the high z atoms in the lasing medium, while the low z atoms retain their electrons. The neutral atoms transfer electrons to highly excited states of the highly striped high z ions giving an inverted population which produces the desired coherent x-rays. In one embodiment, a laser, light beam provides a laser spark that produces the intense burst of coherent x-rays that illuminates the mixture of high z and low z gases, whereby the high z atoms are stripped while the low z ones are not, giving the desired mixture of highly ionized and neutral atoms. To this end, the laser spark is produced by injecting a laser light beam, or a plurality of beams, into a first gas in a cylindrical container having an adjacent second gas layer co-axial therewith, the laser producing a plasma and the intense primary x-rays in the first gas, and the second gas containing the high and low atomic number elements for receiving the primary x-rays, whereupon the secondary x-rays are produced therein by stripping desired ions in a neutral gas and transfer of electrons to highly excited states of the stripped ions from the unionized atoms. Means for magnetically confining and stabilizing the plasma are disclosed for controlling the direction of the x-rays.

  4. Energies of GRB blast waves and prompt efficiencies as implied by modelling of X-ray and GeV afterglows

    NASA Astrophysics Data System (ADS)

    Beniamini, Paz; Nava, Lara; Duran, Rodolfo Barniol; Piran, Tsvi

    2015-11-01

    We consider a sample of 10 gamma-ray bursts with long-lasting ( ≳ 102 s) emission detected by Fermi/Large Area Telescope and for which X-ray data around 1 d are also available. We assume that both the X-rays and the GeV emission are produced by electrons accelerated at the external forward shock, and show that the X-ray and the GeV fluxes lead to very different estimates of the initial kinetic energy of the blast wave. The energy estimated from GeV is on average ˜50 times larger than the one estimated from X-rays. We model the data (accounting also for optical detections around 1 d, if available) to unveil the reason for this discrepancy and find that good modelling within the forward shock model is always possible and leads to two possibilities: (i) either the X-ray emitting electrons (unlike the GeV emitting electrons) are in the slow-cooling regime or (ii) the X-ray synchrotron flux is strongly suppressed by Compton cooling, whereas, due to the Klein-Nishina suppression, this effect is much smaller at GeV energies. In both cases the X-ray flux is no longer a robust proxy for the blast wave kinetic energy. On average, both cases require weak magnetic fields (10-6 ≲ ɛB ≲ 10-3) and relatively large isotropic kinetic blast wave energies 10^{53} erg<{E}_{0,kin}<10^{55} erg corresponding to large lower limits on the collimated energies, in the range 10^{52} erg<{E}_{θ ,kin}<5× 10^{52} erg for an ISM (interstellar medium) environment with n ˜ 1 cm-3 and 10^{52} erg<{E}_{θ ,kin}<10^{53} erg for a wind environment with A* ˜ 1. These energies are larger than those estimated from the X-ray flux alone, and imply smaller inferred values of the prompt efficiency mechanism, reducing the efficiency requirements on the still uncertain mechanism responsible for prompt emission.

  5. Energy calibration of energy-resolved photon-counting pixel detectors using laboratory polychromatic x-ray beams

    NASA Astrophysics Data System (ADS)

    Youn, Hanbean; Han, Jong Chul; Kam, Soohwa; Yun, Seungman; Kim, Ho Kyung

    2014-10-01

    Recently, photon-counting detectors capable of resolving incident x-ray photon energies have been considered for use in spectral x-ray imaging applications. For reliable use of energy-resolved photon-counting detectors (ERPCDs), energy calibration is an essential procedure prior to their use because variations in responses from each pixel of the ERPCD for incident photons, even at the same energy, are inevitable. Energy calibration can be performed using a variety of methods. In all of these methods, the photon spectra with well-defined peak energies are recorded. Every pixel should be calibrated on its own. In this study, we suggest the use of a conventional polychromatic x-ray source (that is typically used in laboratories) for energy calibration. The energy calibration procedure mainly includes the determination of the peak energies in the spectra, flood-field irradiation, determination of peak channels, and determination of calibration curves (i.e., the slopes and intercepts of linear polynomials). We applied a calibration algorithm to a CdTe ERPCD comprised of 128×128 pixels with a pitch of 0.35 mm using highly attenuated polychromatic x-ray beams to reduce the pulse pile-up effect, and to obtain a narrow-shaped spectrum due to beam hardening. The averaged relative error in calibration curves obtained from 16,384 pixels was about 0.56% for 59.6 keV photons from an Americium radioisotope. This pixel-by-pixel energy calibration enhanced the signal- and contrast-to-noise ratios in images, respectively, by a factor of ~5 and 3 due to improvement in image homogeneity, compared to those obtained without energy calibration. One secondary finding of this study was that the x-ray photon spectra obtained using a common algorithm for computing x-ray spectra reasonably described the peaks in the measured spectra, which implies easier peak detection without the direct measurement of spectra using a separate spectrometer. The proposed method will be a useful alternative to

  6. NuSTAR Detection of High-Energy X-Ray Emission and Rapid Variability from Sagittarius A(star) Flares

    NASA Technical Reports Server (NTRS)

    Barriere, Nicolas M.; Tomsick, John A.; Baganoff, Frederick K.; Boggs, Steven E.; Christensen, Finn E.; Craig, William W.; Dexter, Jason; Grefenstette, Brian; Hailey, Charles J.; Zhang, William W.

    2014-01-01

    Sagittarius A(star) harbors the supermassive black hole that lies at the dynamical center of our Galaxy. Sagittarius A(star) spends most of its time in a low luminosity emission state but flares frequently in the infrared and X-ray, increasing up to a few hundred fold in brightness for up to a few hours at a time. The physical processes giving rise to the X-ray flares are uncertain. Here we report the detection with the NuSTAR observatory in Summer and Fall 2012 of four low to medium amplitude X-ray flares to energies up to 79 keV. For the first time, we clearly see that the power-law spectrum of Sagittarius A(star) X-ray flares extends to high energy, with no evidence for a cut off. Although the photon index of the absorbed power-law fits are in agreement with past observations, we find a difference between the photon index of two of the flares (significant at the 95% confidence level). The spectra of the two brightest flares (approx. 55 times quiescence in the 2- 10 keV band) are compared to simple physical models in an attempt to identify the main X-ray emission mechanism, but the data do not allow us to significantly discriminate between them. However, we confirm the previous finding that the parameters obtained with synchrotron models are, for the X-ray emission, physically more reasonable than those obtained with inverse-Compton models. One flare exhibits large and rapid (less than 100 s) variability, which, considering the total energy radiated, constrains the location of the flaring region to be within approx. 10 Schwarzschild radii of the black hole.

  7. NuSTAR detection of high-energy X-ray emission and rapid variability from Sagittarius A{sup *} flares

    SciTech Connect

    Barrière, Nicolas M.; Tomsick, John A.; Boggs, Steven E.; Craig, William W.; Zoglauer, Andreas; Baganoff, Frederick K.; Christensen, Finn E.; Dexter, Jason; Grefenstette, Brian; Harrison, Fiona A.; Madsen, Kristin K.; Hailey, Charles J.; Mori, Kaya; Zhang, Shuo; Stern, Daniel; Zhang, William W.

    2014-05-01

    Sagittarius A{sup *} harbors the supermassive black hole that lies at the dynamical center of our Galaxy. Sagittarius A{sup *} spends most of its time in a low luminosity emission state but flares frequently in the infrared and X-ray, increasing up to a few hundred fold in brightness for up to a few hours at a time. The physical processes giving rise to the X-ray flares are uncertain. Here we report the detection with the NuSTAR observatory in Summer and Fall 2012 of four low to medium amplitude X-ray flares to energies up to 79 keV. For the first time, we clearly see that the power-law spectrum of Sagittarius A{sup *} X-ray flares extends to high energy, with no evidence for a cutoff. Although the photon index of the absorbed power-law fits are in agreement with past observations, we find a difference between the photon index of two of the flares (significant at the 95% confidence level). The spectra of the two brightest flares (∼55 times quiescence in the 2-10 keV band) are compared to simple physical models in an attempt to identify the main X-ray emission mechanism, but the data do not allow us to significantly discriminate between them. However, we confirm the previous finding that the parameters obtained with synchrotron models are, for the X-ray emission, physically more reasonable than those obtained with inverse Compton models. One flare exhibits large and rapid (<100 s) variability, which, considering the total energy radiated, constrains the location of the flaring region to be within ∼10 Schwarzschild radii of the black hole.

  8. Common features of particle beams and x-rays generated in a low energy dense plasma focus device

    NASA Astrophysics Data System (ADS)

    Behbahani, R. A.; Xiao, C.

    2015-02-01

    Features of energetic charged particle beams and x-ray emission in a low energy (1-2 kJ) plasma focus (DPF) device are described and the possible mechanism are explained based on circuit analyses and energy balance in the DPF system. In particular, the resistance and the voltage across the plasma column are estimated to explain the mechanisms of the generation of particle beams and hard x-ray. The analysis shows that the total inductance of a DPF might have played a role for enhancement of the particle beams and x-ray emissions during the phase of anomalous resistance.

  9. Common features of particle beams and x-rays generated in a low energy dense plasma focus device

    SciTech Connect

    Behbahani, R. A.; Xiao, C.

    2015-02-15

    Features of energetic charged particle beams and x-ray emission in a low energy (1–2 kJ) plasma focus (DPF) device are described and the possible mechanism are explained based on circuit analyses and energy balance in the DPF system. In particular, the resistance and the voltage across the plasma column are estimated to explain the mechanisms of the generation of particle beams and hard x-ray. The analysis shows that the total inductance of a DPF might have played a role for enhancement of the particle beams and x-ray emissions during the phase of anomalous resistance.

  10. Multi-energy x-ray detector calibration for Te and impurity density (nZ) measurements of MCF plasmas

    NASA Astrophysics Data System (ADS)

    Maddox, J.; Pablant, N.; Efthimion, P.; Delgado-Aparicio, L.; Hill, K. W.; Bitter, M.; Reinke, M. L.; Rissi, M.; Donath, T.; Luethi, B.; Stratton, B.

    2016-11-01

    Soft x-ray detection with the new "multi-energy" PILATUS3 detector systems holds promise as a magnetically confined fusion (MCF) plasma diagnostic for ITER and beyond. The measured x-ray brightness can be used to determine impurity concentrations, electron temperatures, ne 2 Z eff products, and to probe the electron energy distribution. However, in order to be effective, these detectors which are really large arrays of detectors with photon energy gating capabilities must be precisely calibrated for each pixel. The energy-dependence of the detector response of the multi-energy PILATUS3 system with 100 K pixels has been measured at Dectris Laboratory. X-rays emitted from a tube under high voltage bombard various elements such that they emit x-ray lines from Zr-Lα to Ag-Kα between 1.8 and 22.16 keV. Each pixel on the PILATUS3 can be set to a minimum energy threshold in the range from 1.6 to 25 keV. This feature allows a single detector to be sensitive to a variety of x-ray energies, so that it is possible to sample the energy distribution of the x-ray continuum and line-emission. PILATUS3 can be configured for 1D or 2D imaging of MCF plasmas with typical spatial energy and temporal resolution of 1 cm, 0.6 keV, and 5 ms, respectively.

  11. Multi-energy x-ray detector calibration for Te and impurity density (nZ) measurements of MCF plasmas

    DOE PAGESBeta

    Maddox, J.; Pablant, N.; Efthimion, P.; Delgado-Aparicio, L.; Hill, K. W.; Bitter, M.; Reinke, M. L.; Rissi, M.; Donath, T.; Luethi, B.; et al

    2016-09-07

    Here, soft x-ray detection with the new "multi-energy" PILATUS3 detector systems holds promise as a magnetically confined fusion (MCF) plasma diagnostic for ITER and beyond. The measured x-ray brightness can be used to determine impurity concentrations, electron temperatures, n2eZeff products, and to probe the electron energy distribution. However, in order to be effective, these detectors which are really large arrays of detectors with photon energy gating capabilities must be precisely calibrated for each pixel. The energy-dependence of the detector response of the multi-energy PILATUS3 system with 100 K pixels has been measured at Dectris Laboratory. X-rays emitted from a tubemore » under high voltage bombard various elements such that they emit x-ray lines from Zr-Lα to Ag-Kα between 1.8 and 22.16 keV. Each pixel on the PILATUS3 can be set to a minimum energy threshold in the range from 1.6 to 25 keV. This feature allows a single detector to be sensitive to a variety of x-ray energies, so that it is possible to sample the energy distribution of the x-ray continuum and line-emission. PILATUS3 can be configured for 1D or 2D imaging of MCF plasmas with typical spatial energy and temporal resolution of 1 cm, 0.6 keV, and 5 ms, respectively.« less

  12. Flare onsets in hard and soft X-rays. [magnetic energy conversion in sun

    NASA Technical Reports Server (NTRS)

    Machado, Marcos E.; Orwig, Larry E.; Antonucci, Ester

    1986-01-01

    It is shown that the onset of solar flares, within about 2 min or less before the impulsive peaks, is characterized by an increase in high-energy emission at E less than 100 keV, and strong broadening of soft X-ray lines characteristic of the 10-million-K plasma already present at this stage. The observations are interpreted in terms of the early signature of energy release, during a phase preceding the instability that leads to strong particle acceleration.

  13. Superconducting tunneling-junction detectors of X-ray radiation. Issues concerning the energy resolution

    SciTech Connect

    Andrianov, V. A. Gor'kov, V. P. Koshelets, V. P. Filippenko, L. V.

    2007-02-15

    The effect of the recombination-and edge-related losses of nonequilibrium quasiparticles on the energy resolution of superconducting tunneling detectors is studied. The dependence of the signal on the energy of X-ray photons is measured and the shape of instrument-related lines is studied for the Ti/Nb/Al/AlO{sub x}/Al/Nb/NbN detectors with the Ti/Nb passive electrode. Experimental data are analyzed using the diffusion-based model of tunneling detectors.

  14. Monte Carlo analysis of energy dependent anisotropy of bremsstrahlung x-ray spectra

    SciTech Connect

    Kakonyi, Robert; Erdelyi, Miklos; Szabo, Gabor

    2009-09-15

    The energy resolved emission angle dependence of x-ray spectra was analyzed by MCNPX (Monte Carlo N particle Monte Carlo) simulator. It was shown that the spectral photon flux had a maximum at a well-defined emission angle due to the anisotropy of the bremsstrahlung process. The higher the relative photon energy, the smaller the emission angle belonging to the maximum was. The trends predicted by the Monte Carlo simulations were experimentally verified. The Monte Carlo results were compared to both the Institute of Physics and Engineering in Medicine spectra table and the SPEKCALCV1.0 code.

  15. High energy resolution x-ray spectrometer for high count rate XRF applications

    SciTech Connect

    Rossington, C.S.; Madden, N.W.; Chapman, K.

    1993-08-01

    A new x-ray spectrometer has been constructed which incorporates a novel large area, low capacitance Si(Li) detector and a low noise JFET (junction field effect transistor) pr- eamplifier. The spectrometer operates at high count rates without the conventional compromise in energy resolution. For example, at an amplifier peaking time of 1 {mu}sec and a throughput count rate of 145,000 counts sec{sup {minus}1}, the energy resolution at 5.9 key is 220 eV FWHM. Commercially available spectrometers utilizing conventional geometry Si(Li) detectors with areas equivalent to the new detector have resolutions on the order of 540 eV under the same conditions. Conventional x-ray spectrometers offering high energy resolution must employ detectors with areas one-tenth the size of the new LBL detector (20 mm{sup 2} compared with 200 mm{sup 2}). However, even with the use of the smaller area detectors, the energy resolution of a commercial system is typically limited to approximately 300 eV (again, at 1 {mu}sec and 5.9 keV) due to the noise of the commercially available JFET`S. The new large area detector is useful in high count rate applications, but is also useful in the detection of weak photon signals, in which it is desirable to subtend as large an angle of the available photon flux as possible, while still maintaining excellent energy resolution. X-ray fluorescence data from the new spectrometer is shown in comparison to a commercially available system in the analysis of a dilute multi-element material, and also in conjunction with high count rate synchrotron EXAMS applications.

  16. On filtration for high-energy phase-contrast x-ray imaging

    NASA Astrophysics Data System (ADS)

    Riess, Christian; Mohamed, Ashraf; Hinshaw, Waldo; Fahrig, Rebecca

    2015-03-01

    Phase-sensitive x-ray imaging promises unprecedented soft-tissue contrast and resolution. However, several practical challenges have to be overcome when using the setup in a clinical environment. The system design that is currently closest to clinical use is the grating-based Talbot-Lau interferometer (GBI).1-3 The requirements for patient imaging are low patient dose, fast imaging time, and high image quality. For GBI, these requirements can be met most successfully with a narrow energy width, high- ux spectrum. Additionally, to penetrate a human-sized object, the design energy of the system has to be well above 40 keV. To our knowledge, little research has been done so far to investigate optimal GBI filtration at such high x-ray energies. In this paper, we study different filtration strategies and their impact on high-energy GBI. Specifically, we compare copper filtration at low peak voltage with equal-absorption, equal-imaging time K-edge filtration of spectra with higher peak voltage under clinically realistic boundary conditions. We specifically focus on a design energy of 59 keV and investigate combinations of tube current, peak voltage, and filtration that lead to equal patient absorption. Theoretical considerations suggest that the K edge of tantalum might provide a transmission pocket at around 59 keV, yielding a well-shaped spectrum. Although one can observe a slight visibility benefit when using tungsten or tantalum filtration, experimental results indicate that visibility benefits most from a low x-ray tube peak voltage.

  17. Extended X-Ray Jet in Nearby Galaxy Reveals Energy Source

    NASA Astrophysics Data System (ADS)

    1999-10-01

    NASA's Chandra X-ray Observatory has made an extraordinary image of Centaurus A, a nearby galaxy noted for its explosive activity. The image shows X-ray jets erupting from the center of the galaxy over a distance of 25,000 light years. Also detected are a group of X-ray sources clustered around the nucleus, which is believed to harbor a supermassive black hole. The X-ray jets and the cluster of sources may be a byproduct of a titanic collision between galaxies several hundred million years ago. "This image is great," said Dr. Ethan Schreier of the Space Telescope Science Institute, "For twenty years we have been trying to understand what produced the X rays seen in the Centaurus A jet. Now we at last know that the X-ray emission is produced by extremely high-energy electrons spiraling around a magnetic field." Schreier explained that the length and shape of the X-ray jet pinned down the source of the radiation. The entire length of the X-ray jet is comparable to the diameter of the Milky Way Galaxy. Other features of the image excite scientists. "Besides the jets, one of the first things I noticed about the image was the new population of sources in the center of the galaxy," said Dr. Christine Jones from the Harvard-Smithsonian Center for Astrophysics . "They are grouped in a sphere around the nucleus, which must be telling us something very fundamental about how the galaxy, and the supermassive black hole in the center, were formed." Astronomers have accumulated evidence with optical and infrared telescopes that Centaurus A collided with a small spiral galaxy several hundred million years ago. This collision is believed to have triggered a burst of star formation and supplied gas to fuel the activity of the central black hole. more - According to Dr. Giuseppina Fabbiano, of Harvard-Smithsonian, "The Chandra image is like having a whole new laboratory to work in. Now we can see the main jet, the counter jet, and the extension of the jets beyond the galaxy. It is

  18. Formation, disruption and energy output of Population III X-ray binaries

    NASA Astrophysics Data System (ADS)

    Ryu, Taeho; Tanaka, Takamitsu L.; Perna, Rosalba

    2016-02-01

    The first astrophysical objects shaped the cosmic environment by reionizing and heating the intergalactic medium (IGM). Particularly, X-rays are very efficient at heating the IGM before reionization is complete. High-mass X-ray binaries (HMXBs) in early stellar populations are prime candidates for driving the thermal evolution of the IGM at redshifts z ≳ 20; however, their formation efficiency is not well understood. Using N-body simulations, we estimate the HMXB formation rate via mutual gravitational interactions of nascent, small groups of the Population III stars. We run two sets of calculations: (i) stars formed in small groups of five in nearly Keplerian initial orbits and (ii) collision of two such groups (an expected outcome of mergers of host protogalaxies). We find that HMXBs form at a rate of one per ≳ 104 M⊙ in newly born stars, and that they emit with a power of ˜1041 erg s-1 in the 2-10 keV band per star formation rate. This value is a factor of ˜102 larger than what is observed in star-forming galaxies at lower redshifts; the X-ray production from early HMXBs would have been even more copious, if they also formed in situ or via migration in protostellar discs. Combining our results with earlier studies suggests that early HMXBs were highly effective at heating the IGM and leaving a strong 21-cm signature. We discuss broader implications of our results, such as the rate of long gamma-ray bursts from Population III stars and the direct collapse channel for massive black hole formation.

  19. Streaked spectrometry using multilayer x-ray-interference mirrors to investigate energy transport in laser-plasma applications

    SciTech Connect

    Stradling, G.L.; Barbee, T.W. Jr.; Henke, B.L.; Campbell, E.M.; Mead, W.C.

    1981-08-01

    Transport of energy in laser-produced plasmas is scrutinized by devising spectrally and temporally identifiable characteristics in the x-ray emission history which identify the heat-front position at various times in the heating process. Measurements of the relative turn-on times of these characteristics show the rate of energy transport between various points. These measurements can in turn constrain models of energy transport phenomena. We are time-resolving spectrally distinguishable subkilovolt x-ray emissions from different layers of a disk target to examine the transport rate of energy into the target. A similar technique is used to measure the lateral expansion rate of the plasma spot. A soft x-ray streak camera with 15-psec temporal resolution is used to make the temporal measurements. Spectral discrimination of the incident signal is provided by multilayer x-ray interference mirrors.

  20. X-ray Sources by Energy Recovered Linacs and Their Needed R&D

    SciTech Connect

    Benson, Stephen; Douglas, David; Dowell, David; Hernandez-Garcia, Carlos; Kayran, D; Krafft, Geoffrey; Legg, Robert; Moog, E; Obina, T; Rimmer, Robert; Yakimenko, V

    2011-05-01

    In this paper we review the current state of research on energy recovered linacs as drivers for future X-ray sources. For many types of user experiments, such sources may have substantial advantages compared to the workhorse sources of the present: high energy storage rings. Energy recovered linacs need to be improved beyond present experience in both energy and average current to support this application. To build an energy recovered linac based X-ray user facility presents many interesting challenges. We present summaries on the Research and Development (R&D) topics needed for full development of such a source, including the discussion at the Future Light Sources Workshop held in Gaithersburg, Maryland on September 15- 17, 2009. A rst iteration of an R&D plan is presented that is founded on the notion of building a set of succeedingly larger test accelerators exploring cathode physics, high average current injector physics, and beam recirculation and beam energy recovery at high average current. Our basic conclusion is that a reviewable design of such a source can be developed after an R&D period of ve to ten years.

  1. Electron-Excited X-Ray Microanalysis at Low Beam Energy: Almost Always an Adventure!

    PubMed

    Newbury, Dale E; Ritchie, Nicholas W M

    2016-08-01

    Scanning electron microscopy with energy-dispersive spectrometry has been applied to the analysis of various materials at low-incident beam energies, E 0≤5 keV, using peak fitting and following the measured standards/matrix corrections protocol embedded in the National Institute of Standards and Technology Desktop Spectrum Analyzer-II analytical software engine. Low beam energy analysis provides improved spatial resolution laterally and in-depth. The lower beam energy restricts the atomic shells that can be ionized, reducing the number of X-ray peak families available to the analyst. At E 0=5 keV, all elements of the periodic table except H and He can be measured. As the beam energy is reduced below 5 keV, elements become inaccessible due to lack of excitation of useful characteristic X-ray peaks. The shallow sampling depth of low beam energy microanalysis makes the technique more sensitive to surface compositional modification due to formation of oxides and other reaction layers. Accurate and precise analysis is possible with the use of appropriate standards and by accumulating high count spectra of unknowns and standards (>1 million counts integrated from 0.1 keV to E 0). PMID:27515566

  2. Electron-Excited X-Ray Microanalysis at Low Beam Energy: Almost Always an Adventure!

    PubMed

    Newbury, Dale E; Ritchie, Nicholas W M

    2016-08-01

    Scanning electron microscopy with energy-dispersive spectrometry has been applied to the analysis of various materials at low-incident beam energies, E 0≤5 keV, using peak fitting and following the measured standards/matrix corrections protocol embedded in the National Institute of Standards and Technology Desktop Spectrum Analyzer-II analytical software engine. Low beam energy analysis provides improved spatial resolution laterally and in-depth. The lower beam energy restricts the atomic shells that can be ionized, reducing the number of X-ray peak families available to the analyst. At E 0=5 keV, all elements of the periodic table except H and He can be measured. As the beam energy is reduced below 5 keV, elements become inaccessible due to lack of excitation of useful characteristic X-ray peaks. The shallow sampling depth of low beam energy microanalysis makes the technique more sensitive to surface compositional modification due to formation of oxides and other reaction layers. Accurate and precise analysis is possible with the use of appropriate standards and by accumulating high count spectra of unknowns and standards (>1 million counts integrated from 0.1 keV to E 0).

  3. Ground state potential energy surfaces around selected atoms from resonant inelastic x-ray scattering

    NASA Astrophysics Data System (ADS)

    Schreck, Simon; Pietzsch, Annette; Kennedy, Brian; Såthe, Conny; Miedema, Piter S.; Techert, Simone; Strocov, Vladimir N.; Schmitt, Thorsten; Hennies, Franz; Rubensson, Jan-Erik; Föhlisch, Alexander

    2016-01-01

    Thermally driven chemistry as well as materials’ functionality are determined by the potential energy surface of a systems electronic ground state. This makes the potential energy surface a central and powerful concept in physics, chemistry and materials science. However, direct experimental access to the potential energy surface locally around atomic centers and to its long-range structure are lacking. Here we demonstrate how sub-natural linewidth resonant inelastic soft x-ray scattering at vibrational resolution is utilized to determine ground state potential energy surfaces locally and detect long-range changes of the potentials that are driven by local modifications. We show how the general concept is applicable not only to small isolated molecules such as O2 but also to strongly interacting systems such as the hydrogen bond network in liquid water. The weak perturbation to the potential energy surface through hydrogen bonding is observed as a trend towards softening of the ground state potential around the coordinating atom. The instrumental developments in high resolution resonant inelastic soft x-ray scattering are currently accelerating and will enable broad application of the presented approach. With this multidimensional potential energy surfaces that characterize collective phenomena such as (bio)molecular function or high-temperature superconductivity will become accessible in near future.

  4. Ground state potential energy surfaces around selected atoms from resonant inelastic x-ray scattering

    PubMed Central

    Schreck, Simon; Pietzsch, Annette; Kennedy, Brian; Såthe, Conny; Miedema, Piter S.; Techert, Simone; Strocov, Vladimir N.; Schmitt, Thorsten; Hennies, Franz; Rubensson, Jan-Erik; Föhlisch, Alexander

    2016-01-01

    Thermally driven chemistry as well as materials’ functionality are determined by the potential energy surface of a systems electronic ground state. This makes the potential energy surface a central and powerful concept in physics, chemistry and materials science. However, direct experimental access to the potential energy surface locally around atomic centers and to its long-range structure are lacking. Here we demonstrate how sub-natural linewidth resonant inelastic soft x-ray scattering at vibrational resolution is utilized to determine ground state potential energy surfaces locally and detect long-range changes of the potentials that are driven by local modifications. We show how the general concept is applicable not only to small isolated molecules such as O2 but also to strongly interacting systems such as the hydrogen bond network in liquid water. The weak perturbation to the potential energy surface through hydrogen bonding is observed as a trend towards softening of the ground state potential around the coordinating atom. The instrumental developments in high resolution resonant inelastic soft x-ray scattering are currently accelerating and will enable broad application of the presented approach. With this multidimensional potential energy surfaces that characterize collective phenomena such as (bio)molecular function or high-temperature superconductivity will become accessible in near future. PMID:26821751

  5. Ground state potential energy surfaces around selected atoms from resonant inelastic x-ray scattering.

    PubMed

    Schreck, Simon; Pietzsch, Annette; Kennedy, Brian; Såthe, Conny; Miedema, Piter S; Techert, Simone; Strocov, Vladimir N; Schmitt, Thorsten; Hennies, Franz; Rubensson, Jan-Erik; Föhlisch, Alexander

    2016-01-01

    Thermally driven chemistry as well as materials' functionality are determined by the potential energy surface of a systems electronic ground state. This makes the potential energy surface a central and powerful concept in physics, chemistry and materials science. However, direct experimental access to the potential energy surface locally around atomic centers and to its long-range structure are lacking. Here we demonstrate how sub-natural linewidth resonant inelastic soft x-ray scattering at vibrational resolution is utilized to determine ground state potential energy surfaces locally and detect long-range changes of the potentials that are driven by local modifications. We show how the general concept is applicable not only to small isolated molecules such as O2 but also to strongly interacting systems such as the hydrogen bond network in liquid water. The weak perturbation to the potential energy surface through hydrogen bonding is observed as a trend towards softening of the ground state potential around the coordinating atom. The instrumental developments in high resolution resonant inelastic soft x-ray scattering are currently accelerating and will enable broad application of the presented approach. With this multidimensional potential energy surfaces that characterize collective phenomena such as (bio)molecular function or high-temperature superconductivity will become accessible in near future.

  6. X-ray Sources by Energy Recovered Linacs and Their Needed R&D

    SciTech Connect

    Geoffrey Krafft, Stephen Benson, Michael Borland, David Douglas, David Dowell, Carlos Hernandez-Garcia, Dmitry Kayran, Robert Legg, Elizabeth Moog, Takashi Obina, Robert Rimmer, Vitaly Yakimenko

    2011-05-01

    In this paper we review the current state of research on energy recovered linacs as drivers for future X-ray sources. For many types of user experiments, such sources may have substantial advantages compared to the workhorse sources of the present: high energy storage rings. Energy recovered linacs need to be improved beyond present experience in both energy and average current to support this application. To build an energy recovered linac based X-ray user facility presents many interesting challenges. We present summaries on the Research and Development (R&D) topics needed for full development of such a source, including the discussion at the Future Light Sources Workshop held in Gaithersberg, Maryland on September 15-17, 2009. A first iteration of an R&D plan is presented that is founded on the notion of building a set of succeedingly larger test accelerators exploring cathode physics, high average current injector physics, and beam recirculation and beam energy recovery at high average current. Our basic conclusion is that a reviewable design of such a source can be developed after an R&D period of reasonably short duration.

  7. SU-C-18C-03: Dual-Energy X-Ray Fluoroscopy Imaging System

    SciTech Connect

    Virshup, G; Richmond, M; Mostafavi, H; Ganguly, A; Fu, D

    2014-06-01

    Purpose: This work studies the clinical utility of dual energy (DE) subtraction fluoroscopy for fiducial-free tumor tracking in lung radiation therapy (RT). Improvement in tumor visualization and quantification of tumor shift within a breathing cycle were analyzed. Methods: Twenty subjects who were undergoing RT for lung cancer were recruited following institutional review board approval. The subjects had a range of tumor sizes, locations in the lungs, and body sizes. An x-ray imaging system was setup with the following components: (a) x-ray tube (Varian G-242, Varian Medical Systems (VMS), CA) (b) flat panel detector (4030CB, VMS, CA) and (c) x-ray generator (EPS 50RF, EMD, Canada). Firmware and software modifications were made to the generator to allow 10 x-ray pulse pairs with alternating low/high kV, 100 ms apart for ∼4s (one breathing cycle). Images were obtained at 4 angles: 0°, 45°, 90° and 135°. Weighted subtraction of a kV-pair image set was used to create a “bone-free” image of the lungs. The 2D tumor-shift in each subtracted image and the 3D shift during a breathing cycle was calculated using all views. Results: The subjects enrolled had the following statistics: average age 62.3±7.1 years, 5 female/15 male, 11 had tumors on the right and 9 on the left and the average tumor size was ∼31.4±10.8 mm. X-ray imaging conditions for the pulse pairs were: 70/120 kVp, 280/221 mA and 65/8 ms. For views where these parameters were insufficient 80/130 kVp, 280/221 mA and 60/12 ms was used. Tumor visibility improved for 0°, 45°, 90° and 135° in 100%, 55%, 75% and 80% of the cases respectively. Tumor shift during a breathing cycle was: 2.4±1.0 mm AP, 2.7±1.4 mm LR and 7.6±4.8 mm IS. Conclusion: DE subtraction fluoroscopy allowed improved visualization and quantification of movement of tumors in the lungs during a breathing cycle. This study was entirely funded by Varian Medical Systems.

  8. Synchrotron soft X-ray absorption spectroscopy study of carbon and silicon nanostructures for energy applications.

    PubMed

    Zhong, Jun; Zhang, Hui; Sun, Xuhui; Lee, Shuit-Tong

    2014-12-10

    Carbon and silicon materials are two of the most important materials involved in the history of the science and technology development. In the last two decades, C and Si nanoscale materials, e.g., carbon nanotubes, graphene, and silicon nanowires, and quantum dots, have also emerged as the most interesting nanomaterials in nanoscience and nanotechnology for their myriad promising applications such as for electronics, sensors, biotechnology, etc. In particular, carbon and silicon nanostructures are being utilized in energy-related applications such as catalysis, batteries, solar cells, etc., with significant advances. Understanding of the nature of surface and electronic structures of nanostructures plays a key role in the development and improvement of energy conversion and storage nanosystems. Synchrotron soft X-ray absorption spectroscopy (XAS) and related techniques, such as X-ray emission spectroscopy (XES) and scanning transmission X-ray microscopy (STXM), show unique capability in revealing the surface and electronic structures of C and Si nanomaterials. In this review, XAS is demonstrated as a powerful technique for probing chemical bonding, the electronic structure, and the surface chemistry of carbon and silicon nanomaterials, which can greatly enhance the fundamental understanding and also applicability of these nanomaterials in energy applications. The focus is on the unique advantages of XAS as a complementary tool to conventional microscopy and spectroscopy for effectively providing chemical and structural information about carbon and silicon nanostructures. The employment of XAS for in situ, real-time study of property evolution of C and Si nanostructures to elucidate the mechanisms in energy conversion or storage processes is also discussed.

  9. Energy dependence of the band-limited noise in black hole X-ray binaries★

    NASA Astrophysics Data System (ADS)

    Stiele, H.; Yu, W.

    2015-10-01

    Black hole low-mass X-ray binaries show a variety of variability features, which manifest as narrow peak-like structures superposed on broad noise components in power density spectra in the hard X-ray emission. In this work, we study variability properties of the band-limited noise component during the low-hard state for a sample of black hole X-ray binaries. We investigate the characteristic frequency and amplitude of the band-limited noise component and study covariance spectra. For observations that show a noise component with a characteristic frequency above 1 Hz in the hard energy band (4-8 keV), we found this very same component at a lower frequency in the soft band (1-2 keV). This difference in characteristic frequency is an indication that while both the soft and the hard band photons contribute to the same band-limited noise component, which likely represents the modulation of the mass accretion rate, the origin of the soft photons is actually further away from the black hole than the hard photons. Thus, the soft photons are characterized by larger radii, lower frequencies and softer energies, and are probably associated with a smaller optical depth for Comptonization up-scattering from the outer layer of the corona, or suggest a temperature gradient of the corona. We interpret this energy dependence within the picture of energy-dependent power density states as a hint that the contribution of the up-scattered photons originating in the outskirts of the Comptonizing corona to the overall emission in the soft band is becoming significant.

  10. Tunable X-ray source

    DOEpatents

    Boyce, James R.

    2011-02-08

    A method for the production of X-ray bunches tunable in both time and energy level by generating multiple photon, X-ray, beams through the use of Thomson scattering. The method of the present invention simultaneously produces two X-ray pulses that are tunable in energy and/or time.

  11. Analysis of nuclear materials by energy dispersive x-ray fluorescence and spectral effects of alpha decay

    SciTech Connect

    Worley, Christopher G

    2009-01-01

    Energy dispersive X-ray fluorescence (EDXRF) spectra collected from alpha emitters are complicated by artifacts inherent to the alpha decay process, particularly when using portable instruments. For example, {sup 239}Pu EDXRF spectra exhibit a prominent uranium L X-ray emission peak series due to sample alpha decay rather than source-induced X-ray fluorescence. A portable EDXRF instrument was used to collect spectra from plutonium, americium, and a Pu-contaminated steel sample. The plutonium sample was also analyzed by wavelength dispersive XRF to demonstrate spectral differences observed when using these very different instruments.

  12. A compact source of intense 1-100 keV monochromatic X-rays from low energy protons

    NASA Astrophysics Data System (ADS)

    Arduini, G.; Cicardi, C.; Milazzo, M.; Sangaletti, L.; Silari, M.

    1995-05-01

    The properties and possible applications of a very intense source of monochromatic X-rays, tunable in the 1-100 keV range, obtained by coupling a low energy (2-4 MeV) high current proton accelerator with an irradiation chamber provided with a multiple target system and collimator are discussed. The properties of the source are presented in terms of intensity, monochromaticity, polarizability and time structure. Fields where such a source can be employed are discussed, namely PIXE-induced XRF, X-ray photoemission spectroscopy, generation of soft X-rays, radiographic applications in archeometry and medical radiography with monoenergetic radiation.

  13. Development of a high energy x-ray polarimeter for small satellites

    SciTech Connect

    Gunji, S.; Austin, R.A.; Elsner, R.F.

    1996-12-31

    We are developing a Thomson-scattering-type polarimeter sensitive in the energy range from 10 keV to 20 keV for a small satellite. The polarimeter consists of three beryllium disks as scatterers and a cylindrical position-sensitive proportional counter as a detector of the scattered X rays. Its performance has been investigated through computer simulations. From these, it was concluded that the polarimeter can obtain a modulation factor of 34%, a detection efficiency of {approximately}10%, and a minimum detectable polarization of about 3.0% for Her X-1 in 2 keV bands and a 2 x 10{sup 5} sec observation.

  14. Distinction between entrance and exit wounds by energy dispersive X-ray fluorescence spectrometry.

    PubMed

    Tanaka, Naoko; Kinoshita, Hiroshi; Takakura, Ayaka; Jamal, Mostofa; Ito, Asuka; Kumihashi, Mitsuru; Tsutsui, Kunihiko; Kimura, Shoji; Ameno, Kiyoshi

    2016-09-01

    We investigated gunshot wounds in two autopsy cases using energy dispersive X-ray spectrometry (EDX). Lead and copper were detected in the entrance wound of one case and lead, antimony, and copper were detected in that of the other case. In the exit wounds of both cases, lead, antimony, and copper were below detection limits. These findings indicate that the detection of metallic elements, such as lead, antimony, and copper, which are found in bullets, may be useful for differentiating entrance from exit wounds using EDX. PMID:27591531

  15. Towards hybrid pixel detectors for energy-dispersive or soft X-ray photon science.

    PubMed

    Jungmann-Smith, J H; Bergamaschi, A; Brückner, M; Cartier, S; Dinapoli, R; Greiffenberg, D; Huthwelker, T; Maliakal, D; Mayilyan, D; Medjoubi, K; Mezza, D; Mozzanica, A; Ramilli, M; Ruder, Ch; Schädler, L; Schmitt, B; Shi, X; Tinti, G

    2016-03-01

    JUNGFRAU (adJUstiNg Gain detector FoR the Aramis User station) is a two-dimensional hybrid pixel detector for photon science applications at free-electron lasers and synchrotron light sources. The JUNGFRAU 0.4 prototype presented here is specifically geared towards low-noise performance and hence soft X-ray detection. The design, geometry and readout architecture of JUNGFRAU 0.4 correspond to those of other JUNGFRAU pixel detectors, which are charge-integrating detectors with 75 µm × 75 µm pixels. Main characteristics of JUNGFRAU 0.4 are its fixed gain and r.m.s. noise of as low as 27 e(-) electronic noise charge (<100 eV) with no active cooling. The 48 × 48 pixels JUNGFRAU 0.4 prototype can be combined with a charge-sharing suppression mask directly placed on the sensor, which keeps photons from hitting the charge-sharing regions of the pixels. The mask consists of a 150 µm tungsten sheet, in which 28 µm-diameter holes are laser-drilled. The mask is aligned with the pixels. The noise and gain characterization, and single-photon detection as low as 1.2 keV are shown. The performance of JUNGFRAU 0.4 without the mask and also in the charge-sharing suppression configuration (with the mask, with a `software mask' or a `cluster finding' algorithm) is tested, compared and evaluated, in particular with respect to the removal of the charge-sharing contribution in the spectra, the detection efficiency and the photon rate capability. Energy-dispersive and imaging experiments with fluorescence X-ray irradiation from an X-ray tube and a synchrotron light source are successfully demonstrated with an r.m.s. energy resolution of 20% (no mask) and 14% (with the mask) at 1.2 keV and of 5% at 13.3 keV. The performance evaluation of the JUNGFRAU 0.4 prototype suggests that this detection system could be the starting point for a future detector development effort for either applications in the soft X-ray energy regime or for an energy

  16. Determination of carrier yields for neutron activation analysis using energy dispersive X-ray spectrometry

    USGS Publications Warehouse

    Johnson, R.G.; Wandless, G.A.

    1984-01-01

    A new method is described for determining carrier yield in the radiochemical neutron activation analysis of rare-earth elements in silicate rocks by group separation. The method involves the determination of the rare-earth elements present in the carrier by means of energy-dispersive X-ray fluorescence analysis, eliminating the need to re-irradiate samples in a nuclear reactor after the gamma ray analysis is complete. Results from the analysis of USGS standards AGV-1 and BCR-1 compare favorably with those obtained using the conventional method. ?? 1984 Akade??miai Kiado??.

  17. Extension to Low Energies (<7keV) of High Pressure X-Ray Absorption Spectroscopy

    SciTech Connect

    Itie, J.-P.; Flank, A.-M.; Lagarde, P.; Idir, M.; Polian, A.; Couzinet, B.

    2007-01-19

    High pressure x-ray absorption has been performed down to 3.6 keV, thanks to the new LUCIA beamline (SLS, PSI) and to the use of perforated diamonds or Be gasket. Various experimental geometries are proposed, depending on the energy of the edge and on the concentration of the studied element. A few examples will be presented: BaTiO3 at the titanium K edge, Zn0.95 Mn0.05O at the manganese K edge, KCl at the potassium K edge.

  18. Characterization of a free air ionization chamber for low energy X-rays

    NASA Astrophysics Data System (ADS)

    Silva, N. F.; Xavier, M.; Vivolo, V.; Caldas, L. V. E.

    2016-07-01

    Free air ionization chambers are used by most primary metrology laboratories as primary standards of the quantities air kerma and exposure in X-ray beams. The free air ionization chamber for low energies of the Calibration Laboratory (LCI) of IPEN showed in a characterization test a problem in the set responsible for the variation of its sensitive volume. After a modification in the support of the micrometers used for the movement of the internal cylinder and the establishment of a new alignment system protocol, the tests were redone. The objective of this work was to present the results obtained in the new condition.

  19. Processing and quantification of x-ray energy dispersive spectra in the Analytical Electron Microscope

    SciTech Connect

    Zaluzec, N.J.

    1988-08-01

    Spectral processing in x-ray energy dispersive spectroscopy deals with the extraction of characteristic signals from experimental data. In this text, the four basic procedures for this methodology are reviewed and their limitations outlined. Quantification, on the other hand, deals with the interpretation of the information obtained from spectral processing. Here the limitations are for the most part instrumental in nature. The prospects of higher voltage operation does not, in theory, present any new problems and may in fact prove to be more desirable assuming that electron damage effects do not preclude analysis. 28 refs., 6 figs.

  20. Towards hybrid pixel detectors for energy-dispersive or soft X-ray photon science.

    PubMed

    Jungmann-Smith, J H; Bergamaschi, A; Brückner, M; Cartier, S; Dinapoli, R; Greiffenberg, D; Huthwelker, T; Maliakal, D; Mayilyan, D; Medjoubi, K; Mezza, D; Mozzanica, A; Ramilli, M; Ruder, Ch; Schädler, L; Schmitt, B; Shi, X; Tinti, G

    2016-03-01

    JUNGFRAU (adJUstiNg Gain detector FoR the Aramis User station) is a two-dimensional hybrid pixel detector for photon science applications at free-electron lasers and synchrotron light sources. The JUNGFRAU 0.4 prototype presented here is specifically geared towards low-noise performance and hence soft X-ray detection. The design, geometry and readout architecture of JUNGFRAU 0.4 correspond to those of other JUNGFRAU pixel detectors, which are charge-integrating detectors with 75 µm × 75 µm pixels. Main characteristics of JUNGFRAU 0.4 are its fixed gain and r.m.s. noise of as low as 27 e(-) electronic noise charge (<100 eV) with no active cooling. The 48 × 48 pixels JUNGFRAU 0.4 prototype can be combined with a charge-sharing suppression mask directly placed on the sensor, which keeps photons from hitting the charge-sharing regions of the pixels. The mask consists of a 150 µm tungsten sheet, in which 28 µm-diameter holes are laser-drilled. The mask is aligned with the pixels. The noise and gain characterization, and single-photon detection as low as 1.2 keV are shown. The performance of JUNGFRAU 0.4 without the mask and also in the charge-sharing suppression configuration (with the mask, with a `software mask' or a `cluster finding' algorithm) is tested, compared and evaluated, in particular with respect to the removal of the charge-sharing contribution in the spectra, the detection efficiency and the photon rate capability. Energy-dispersive and imaging experiments with fluorescence X-ray irradiation from an X-ray tube and a synchrotron light source are successfully demonstrated with an r.m.s. energy resolution of 20% (no mask) and 14% (with the mask) at 1.2 keV and of 5% at 13.3 keV. The performance evaluation of the JUNGFRAU 0.4 prototype suggests that this detection system could be the starting point for a future detector development effort for either applications in the soft X-ray energy regime or for an energy

  1. Quantitative analysis of annealed scanning probe tips using energy dispersive x-ray spectroscopy

    SciTech Connect

    Cobley, R. J.; Brown, R. A.; Barnett, C. J.; Maffeis, T. G. G.; Penny, M. W.

    2013-01-14

    A quantitative method to measure the reduction in oxide species on the surface of electrochemically etched tungsten tips during direct current annealing is developed using energy dispersive x-ray spectroscopy. Oxide species are found to decrease with annealing current, with the trend repeatable over many tips and along the length of the tip apex. A linear resistivity approximation finds significant oxide sublimation occurs at 1714 K, but surface melting and tip broadening at 2215 K. This method can be applied to calibrate any similar annealing stage, and to identify the tradeoff regime between required morphological and chemical properties.

  2. A Fabry-Perot interferometer for sub-meV x-ray energy resolution

    SciTech Connect

    Caticha, A.; Aliberti, K.; Caticha-Ellis, S.

    1996-09-01

    The optical theory of Fabry-Perot interferometers (FPIs) for x rays using dynamically diffracting thin perfect crystals as reflectors is developed. Application to a device using high diffraction orders in silicon crystals of thickness of the order of 100 {mu}m or more shows that energy resolutions of the order of a tenth of a meV are achievable. The effect that various features, such as gap and mirror thickness, lattice mismatches, etc., have on the FPI resonances is studied. {copyright} {ital 1996 American Institute of Physics.}

  3. Method and apparatus for multiple-projection, dual-energy x-ray absorptiometry scanning

    NASA Technical Reports Server (NTRS)

    Charles, Jr., Harry K. (Inventor); Beck, Thomas J. (Inventor); Feldmesser, Howard S. (Inventor); Magee, Thomas C. (Inventor)

    2007-01-01

    Methods and apparatuses for advanced, multiple-projection, dual-energy X-ray absorptiometry scanning systems include combinations of a conical collimator; a high-resolution two-dimensional detector; a portable, power-capped, variable-exposure-time power supply; an exposure-time control element; calibration monitoring; a three-dimensional anti-scatter-grid; and a gantry-gantry base assembly that permits up to seven projection angles for overlapping beams. Such systems are capable of high precision bone structure measurements that can support three dimensional bone modeling and derivations of bone strength, risk of injury, and efficacy of countermeasures among other properties.

  4. Analysis of Fast Electron Energy Distribution by Measuring Hard X-ray Bremsstrahlung

    NASA Astrophysics Data System (ADS)

    Daykin, Tyler; Sawada, Hiroshi; Sentoku, Yasuhiko; Bass, Anthony; Griffin, Brandon; Pandit, Rishi; Beg, Farhat; Chen, Hui; McLean, Harry; Link, Anthony; Patel, Prav; Ping, Yuan

    2015-11-01

    Characterization of intense, short-pulse laser-produced fast electrons is important for fundamental understanding and applications. We carried out an experiment to characterize the fast electron energy distribution by measuring angular-dependent high-energy bremsstrahlung x-rays. A 100 μm thick metal foil (Al, Cu, and Ag) mounted on a plastic backing was irradiated by the 0.35 ps, 15 J Leopard Laser at the Nevada Terawatt Facility. The bremsstrahlung x-rays and the escaping electrons from the target were recorded using differential filter stack spectrometers at 22° and 45° off laser axis and a magnet-based electron spectrometer along the laser axis. The electron spectrum inferred from two different diagnostics had single slope temperature of ~ 1.5 MeV for the Cu foil. The results were compared to an analytic calculation and a 2-D Particle-in-cell code, PICLS. The analysis of the electron energy distribution and angular distribution will be presented. This work was supported by the UNR Office of the Provost and by DOE/OFES under Contract No. DE-SC0008827. This collaborative work was partially supported under the auspices of the US Department of Energy by Lawrence Livermore National Laboratory under Con.

  5. Development of a high-energy-resolution x-ray microcalorimeter using Ti/Au TES

    NASA Astrophysics Data System (ADS)

    Kudo, Hiroyuki; Yokoyama, Yuichi; Shoji, Shuichi; Oshima, Tohru; Aruga, Youichi; Maegami, Kana; Fujimoto, Ryuichi; Miyazaki, Toshiyuki; Mitsuda, Kazuhisa

    1999-10-01

    A prototype of an x-ray microcalorimeter using Titanium/Gold transition edge sensor (TES) for detecting cosmic rays is fabricated and tested. This paper reports first experimental result of the prototype. By using silicon bulk micromachining, freestanding microstructure suspended with fine beams are obtained to achieve thermal isolation from the substrate. A superconductor, Ti in this case, can be used as a very sensitive temperature sensor at the narrow temperature range around its transition temperature. At the low temperatures below 1K, the microstructure with very small heat capacity is expected to be thermally detecting single photons. Design consideration to realize radiation detection with extremely good energy resolution has been taken place. Our tentative goal is to obtain the energy resolution of 20eV for 10keV radiation at 0.5K. We have fabricated a test device of the TES. The sensitivity of it is larger than 1000, which is enough for this purpose. The energy resolution of the prototype of the x-ray microcalorimeter was 550eV for 6keV radiation at approximately 0.5K. This value is smaller than that expected. An optimization of the TES features is still necessary for a good energy resolution.

  6. Determination of selenium in biological samples with an energy-dispersive X-ray fluorescence spectrometer.

    PubMed

    Li, Xiaoli; Yu, Zhaoshui

    2016-05-01

    Selenium is both a nutrient and a toxin. Selenium-especially organic selenium-is a core component of human nutrition. Thus, it is very important to measure selenium in biological samples. The limited sensitivity of conventional XRF hampers its widespread use in biological samples. Here, we describe the use of high-energy (100kV, 600W) linearly polarized beam energy-dispersive X-Ray fluorescence spectroscopy (EDXRF) in tandem with a three-dimensional optics design to determine 0.1-5.1μgg(-1) levels of selenium in biological samples. The effects of various experimental parameters such as applied voltage, acquisition time, secondary target and various filters were thoroughly investigated. The detection limit of selenium in biological samples via high-energy (100kV, 600W) linearly polarized beam energy-dispersive X-ray fluorescence spectroscopy was decreased by one order of magnitude versus conventional XRF (Paltridge et al., 2012) and found to be 0.1μg/g. To the best of our knowledge, this is the first report to describe EDXRF measurements of Se in biological samples with important implications for the nutrition and analytical chemistry communities. PMID:26922394

  7. [Application of the racial algorithm in energy dispersive X-ray fluorescence overlapped spectrum analysis].

    PubMed

    Zeng, Guo-Qiang; Luo, Yao-Yao; Ge, Liang-Quan; Zhang, Qing-Xian; Gu, Yi; Cheng, Feng

    2014-02-01

    In the energy dispersive X-ray fluorescence spectrum analysis, scintillation detector such as NaI (Tl) detector usually has a low energy resolution at around 8%. The low energy resolution causes problems in spectral data analysis especially in the high background and low counts condition, it is very limited to strip the overlapped spectrum, and the more overlapping the peaks are, the more difficult to peel the peaks, and the qualitative and quantitative analysis can't be carried out because we can't recognize the peak address and peak area. Based on genetic algorithm and immune algorithm, we build a new racial algorithm which uses the Euclidean distance as the judgment of evolution, the maximum relative error as the iterative criterion to be put into overlapped spectrum analysis, then we use the Gaussian function to simulate different overlapping degrees of the spectrum, and the racial algorithm is used in overlapped peak separation and full spectrum simulation, the peak address deviation is in +/- 3 channels, the peak area deviation is no more than 5%, and it is proven that this method has a good effect in energy dispersive X-ray fluorescence overlapped spectrum analysis.

  8. High energy X-ray observations of Sco-like sources with Ariel V

    NASA Technical Reports Server (NTRS)

    Greenhill, J. G.; Coe, M. J.; Burnell, S. J. B.; Strong, K. T.; Carpenter, G. F.

    1979-01-01

    Results are reported for observations of Sco X-1 and the similar sources 4U 1702-36 (GX 349+2, Sco X-2), 4U 1813-14 (GX 17+2), and 4U 1758-25 (GX 5-1) by several of the X-ray telescopes aboard the Ariel 5 satellite over the energy range from 2 to approximately 100 keV. The results confirm the existence of a high-energy tail in the spectrum of Sco X-1, demonstrate that 4U 1702-36 has a similar spectrum, and provide evidence for a variation of the 26-56-keV flux from 4U 1702-36 by more than a factor of four with no related change in the 2.9-7.6-keV flux. The high-energy emission from Sco X-1 is found to be one to two orders of magnitude above the extrapolated low-energy emission. Observed X-ray, radio, and optical properties of these four sources, as well as two additional Sco-like sources, are summarized.

  9. Optimum filter selection for Dual Energy X-ray Applications through Analytical Modeling

    NASA Astrophysics Data System (ADS)

    Koukou, V.; Martini, N.; Michail, C.; Sotiropoulou, P.; Kalyvas, N.; Kandarakis, I.; Nikiforidis, G.; Fountos, G.

    2015-09-01

    In this simulation study, an analytical model was used in order to determine the optimal acquisition parameters for a dual energy breast imaging system. The modeled detector system, consisted of a 33.91mg/cm2 Gd2O2S:Tb scintillator screen, placed in direct contact with a high resolution CMOS sensor. Tungsten anode X-ray spectra, filtered with various filter materials and filter thicknesses were examined for both the low- and high-energy beams, resulting in 3375 combinations. The selection of these filters was based on their K absorption edge (K-edge filtering). The calcification signal-to-noise ratio (SNRtc) and the mean glandular dose (MGD) were calculated. The total mean glandular dose was constrained to be within acceptable levels. Optimization was based on the maximization of the SNRtc/MGD ratio. The results showed that the optimum spectral combination was 40kVp with added beam filtration of 100 μm Ag and 70kVp Cu filtered spectrum of 1000 μm for the low- and high-energy, respectively. The minimum detectable calcification size was 150 μm. Simulations demonstrate that this dual energy X-ray technique could enhance breast calcification detection.

  10. Dual-source multi-energy CT with triple or quadruple x-ray beams

    NASA Astrophysics Data System (ADS)

    Yu, Lifeng; Li, Zhoubo; Leng, Shuai; McCollough, Cynthia H.

    2016-03-01

    Energy-resolved photon-counting CT (PCCT) is promising for material decomposition with multi-contrast agents. However, corrections for non-idealities of PCCT detectors are required, which are still active research areas. In addition, PCCT is associated with very high cost due to lack of mass production. In this work, we proposed an alternative approach to performing multi-energy CT, which was achieved by acquiring triple or quadruple x-ray beam measurements on a dual-source CT scanner. This strategy was based on a "Twin Beam" design on a single-source scanner for dual-energy CT. Examples of beam filters and spectra for triple and quadruple x-ray beam were provided. Computer simulation studies were performed to evaluate the accuracy of material decomposition for multi-contrast mixtures using both tri-beam and quadruple-beam configurations. The proposed strategy can be readily implemented on a dual-source scanner, which may allow material decomposition of multi-contrast agents to be performed on clinical CT scanners with energy-integrating detector.

  11. Metastable phase diagram of Bi probed by single-energy x-ray absorption detection and angular dispersive x-ray diffraction

    SciTech Connect

    Principi, E.; Minicucci, M.; Di Cicco, A.; Trapananti, A.; De Panfilis, S.; Poloni, R.

    2006-08-01

    In this paper we report the results of a detailed experimental study of samples composed of micrometric Bi droplets providing an insight into the metastable phase diagram of Bi. To this purpose we have used the single-energy x-ray absorption detection technique in combination with angular dispersive x-ray diffraction available at the BM29 beamline of the European Synchrotron Radiation Facility. This unconventional approach has given proof of being a different and reliable tool for detecting subtle structural modifications in condensed matter. The investigation has revealed a large variety of metastable Bi polymorphs in a broad range of pressures and temperatures (25-500 deg. C, 0-6 GPa) and the occurrence of a Bi crystalline structure isomorphic to the {beta}-tin structure. We have shown that the range of undercooling of liquid Bi strongly depends upon pressure and the underlying solid stable and metastable phases. As a final result a Bi-phase diagram including metastable phases is proposed, which takes into account all structural information obtained from this experiment.

  12. Time-resolved soft-x-ray studies of energy transport in layered and planar laser-driven targets

    SciTech Connect

    Stradling, G.L.

    1982-04-19

    New low-energy x-ray diagnostic techniques are used to explore energy-transport processes in laser heated plasmas. Streak cameras are used to provide 15-psec time-resolution measurements of subkeV x-ray emission. A very thin (50 ..mu..g/cm/sup 2/) carbon substrate provides a low-energy x-ray transparent window to the transmission photocathode of this soft x-ray streak camera. Active differential vacuum pumping of the instrument is required. The use of high-sensitivity, low secondary-electron energy-spread CsI photocathodes in x-ray streak cameras is also described. Significant increases in sensitivity with only a small and intermittant decrease in dynamic range were observed. These coherent, complementary advances in subkeV, time-resolved x-ray diagnostic capability are applied to energy-transport investigations of 1.06-..mu..m laser plasmas. Both solid disk targets of a variety of Z's as well as Be-on-Al layered-disk targets were irradiated with 700-psec laser pulses of selected intensity between 3 x 10/sup 14/ W/cm/sup 2/ and 1 x 10/sup 15/ W/cm/sup 2/.

  13. Radiation decay of thaumatin crystals at three X-ray energies

    PubMed Central

    Liebschner, Dorothee; Rosenbaum, Gerold; Dauter, Miroslawa; Dauter, Zbigniew

    2015-01-01

    Radiation damage is an unavoidable obstacle in X-ray crystallographic data collection for macromolecular structure determination, so it is important to know how much radiation a sample can endure before being degraded beyond an acceptable limit. In the literature, the threshold at which the average intensity of all recorded reflections decreases to a certain fraction of the initial value is called the ‘dose limit’. The first estimated D 50 dose-limit value, at which the average diffracted intensity was reduced to 50%, was 20 MGy and was derived from observing sample decay in electron-diffraction experiments. A later X-ray study carried out at 100 K on ferritin protein crystals arrived at a D 50 of 43 MGy, and recommended an intensity reduction of protein reflections to 70%, D 70, corresponding to an absorbed dose of 30 MGy, as a more appropriate limit for macromolecular crystallography. In the macromolecular crystallography community, the rate of intensity decay with dose was then assumed to be similar for all protein crystals. A series of diffraction images of cryocooled (100 K) thaumatin crystals at identical small, 2° rotation intervals were recorded at X-ray energies of 6.33 , 12.66 and 19.00 keV. Five crystals were used for each wavelength. The decay in the average diffraction intensity to 70% of the initial value, for data extending to 2.45 Å resolution, was determined to be about 7.5 MGy at 6.33 keV and about 11 MGy at the two higher energies. PMID:25849388

  14. Dynamic Hohlraums as x-ray sources in high-energy density science

    NASA Astrophysics Data System (ADS)

    Hansen, J. F.; Glendinning, S. G.; Heeter, R. F.; Brockington, S. J. E.

    2008-01-01

    The first demonstration of laser driven dynamic Hohlraums (LDDH) as a spectrally smooth backlighter source for opacity and temperature measurements through absorption spectrometry of materials in local thermodynamic equilibrium at temperatures >150eV has been made. This is a crucial temperature regime for future astrophysics and ignition fusion experiments at the nearly completed National Ignition Facility (NIF) [E. I. Moses and C. R. Wuest, Fusion Sci. Technol. 47, 314 (2005)] at the Lawrence Livermore National Laboratory. The new backlighter consists of a LDDH filled with either krypton or argon that implodes to create an x-ray flash. The properties of this x-ray flash have been measured in experiments at the Omega laser [T. R. Boehly et al., Opt. Commun. 133, 495 (1997)] at the Laboratory for Laser Energetics in Rochester, New York, satisfying all requirements imposed by future experiments: (1) the emission spectrum extends to at least 5.5keV, well above the maximum x-ray energy (˜3.5keV) obtained from the previously "best" opacity backlighters (uranium M-shell emission backlighters); (2) the spectrum is smooth and featureless (intensity variation <6%rms), allowing absorption spectrometry through experimental samples; (3) the emission source size is sufficiently small (<50μm) for projection backlighting through future samples; (4) the emission is bright enough (and twice as bright as imploding hydrogen-filled capsules) for gated spectrometer measurements; (5) the emission duration is optimized (≈100ps) for the current and future generations of spectrometers; and (6) by using only a small number of beams with limited energy and symmetry for the backlighter (10 out of 60 beams in the Omega experiments), the majority of laser beams are left available for heating sample materials to >150eV.

  15. REVEALING THE STRUCTURE OF AN ACCRETION DISK THROUGH ENERGY-DEPENDENT X-RAY MICROLENSING

    SciTech Connect

    Chartas, G.; Moore, D.; Kochanek, C. S.; Mosquera, A. M.; Blackburne, J. A.; Dai, X.

    2012-10-01

    We present results from monitoring observations of the gravitationally lensed quasar RX J1131-1231 performed with the Chandra X-Ray Observatory. The X-ray observations were planned with relatively long exposures that allowed a search for energy-dependent microlensing in the soft (0.2-2 keV) and hard (2-10 keV) light curves of the images of RX J1131-1231. We detect significant microlensing in the X-ray light curves of images A and D, and energy-dependent microlensing of image D. The magnification of the soft band appears to be larger than that in the hard band by a factor of {approx}1.3 when image D becomes more magnified. This can be explained by the difference between a compact, softer-spectrum corona that is producing a more extended, harder spectrum reflection component off the disk. This is supported by the evolution of the fluorescent iron line in image D over three consecutive time-averaged phases of the light curve. In the first period, an Fe line at E = 6.35{sup +0.14}{sub -0.14} keV is detected (at >99% confidence). In the second period, two Fe lines are detected, one at E = 5.50{sup +0.03}{sub -0.08} keV (detected at >99% confidence) and another at E = 6.04{sup +0.10}{sub -0.07} keV (marginally detected at >90% confidence), and in the third period, a broadened Fe line at 6.42{sup +0.16}{sub -0.14} keV is detected (at >99% confidence). This evolution of the Fe line profile during the microlensing event is consistent with the line distortion expected when a caustic passes over the inner disk where the shape of the fluorescent Fe line is distorted by general relativistic and Doppler effects.

  16. Formation and propagation of laser-driven plasma jets in an ambient medium studied with X-ray radiography and optical diagnostics

    SciTech Connect

    Dizière, A.; Pelka, A.; Ravasio, A.; Yurchak, R.; Loupias, B.; Falize, E.; Kuramitsu, Y.; Sakawa, Y.; Morita, T.; Pikuz, S.; Koenig, M.

    2015-01-15

    In this paper, we present experimental results obtained on the LULI2000 laser facility regarding structure and dynamics of astrophysical jets propagating in interstellar medium. The jets, generated by using a cone-shaped target, propagate in a nitrogen gas that mimics the interstellar medium. X-ray radiography as well as optical diagnostics were used to probe both high and low density regions. In this paper, we show how collimation of the jets evolves with the gas density.

  17. YAP imager and its application with high-energy X-ray beams up to 150 keV

    NASA Astrophysics Data System (ADS)

    Hirota, K.; Toyokawa, H.; Suzuki, M.; Kudo, T.; Nomachi, M.; Sugaya, Y.; Yosoi, M.; Gorin, A.; Manuilov, I.; Riazantsev, A.; Kuroda, K.

    2003-09-01

    An X-ray imaging detector called YAP imager has been developed for high-energy X-ray region at the SPring-8 facility. It possesses a [128×128] matrix of YAlO 3:Ce crystals, each element having a volume of 1×1×6 mm 3. A NIM logic module using programmable logic device chip was also developed as a position encoder. The YAP imager has been applied for some applications with a thermal barrier coating material and multi-layer metal sheets targets in the incident X-ray energy region of 70-150 keV. Direct X-ray beam profile at 100 keV was also measured.

  18. X-ray dual energy spectral parameter optimization for bone Calcium/Phosphorus mass ratio estimation

    NASA Astrophysics Data System (ADS)

    Sotiropoulou, P. I.; Fountos, G. P.; Martini, N. D.; Koukou, V. N.; Michail, C. M.; Valais, I. G.; Kandarakis, I. S.; Nikiforidis, G. C.

    2015-09-01

    Calcium (Ca) and Phosphorus (P) bone mass ratio has been identified as an important, yet underutilized, risk factor in osteoporosis diagnosis. The purpose of this simulation study is to investigate the use of effective or mean mass attenuation coefficient in Ca/P mass ratio estimation with the use of a dual-energy method. The investigation was based on the minimization of the accuracy of Ca/P ratio, with respect to the Coefficient of Variation of the ratio. Different set-ups were examined, based on the K-edge filtering technique and single X-ray exposure. The modified X-ray output was attenuated by various Ca/P mass ratios resulting in nine calibration points, while keeping constant the total bone thickness. The simulated data were obtained considering a photon counting energy discriminating detector. The standard deviation of the residuals was used to compare and evaluate the accuracy between the different dual energy set-ups. The optimum mass attenuation coefficient for the Ca/P mass ratio estimation was the effective coefficient in all the examined set-ups. The variation of the residuals between the different set-ups was not significant.

  19. Laboratory x ray lasers

    NASA Astrophysics Data System (ADS)

    Matthews, D. L.

    1989-08-01

    One of the most innovative spinoffs of ICF technology and physics was the development of the x ray wavelength laser. The first incontrovertible demonstration of this type of laser came from LLNL in 1984 using the Novette laser to pump a selenium foil target. The power and energy of Novette were then needed to produce a column of plasma of sufficient length to achieve a sufficient gainlength product (approximately 5.5, this corresponds to an amplification of approximately 250X) that could unquestionably illustrate the lasing effect. LLNL ICF expertise was also required to develop time-resolved spectrometers used to view the lasing transitions at approximately 20 nm, a region of the XUV spectrum normally dominated by high backgrounds. The design of the x ray laser amplifier, which required maintaining nonequilibrium level populations in a tailored plasma having the proper conditions for gain and x ray laser beam propagation, was accomplished with modified versions of ICF kinetics and hydrodynamics codes. Since the first demonstration, progress in the development of the x ray laser was rapid. New achievements include production of megawatt power levels at 20 nm, amplified spontaneous emission levels approaching saturation intensity GL of approximately 17 at 20 nm, efficiency (x ray laser energy/pump energy) approximately 10(exp 6), the demonstration of double and triple pass amplification (hinting at the possibility of producing x ray wavelength resonators), the focusing of x ray lasers to pump other types of lasers and the first demonstration of an x ray hologram produced by an x ray laser. The generation of amplification at ever shorter wavelength is possible using various types of inversion schemes. We depict below this progress benchmarked against production of gain in the water window (2.2 to 4.4 nm,), where applications to biological imaging may be facilitated.

  20. Material separation in x-ray CT with energy resolved photon-counting detectors

    PubMed Central

    Wang, Xiaolan; Meier, Dirk; Taguchi, Katsuyuki; Wagenaar, Douglas J.; Patt, Bradley E.; Frey, Eric C.

    2011-01-01

    Purpose: The objective of the study was to demonstrate that, in x-ray computed tomography (CT), more than two types of materials can be effectively separated with the use of an energy resolved photon-counting detector and classification methodology. Specifically, this applies to the case when contrast agents that contain K-absorption edges in the energy range of interest are present in the object. This separation is enabled via the use of recently developed energy resolved photon-counting detectors with multiple thresholds, which allow simultaneous measurements of the x-ray attenuation at multiple energies. Methods: To demonstrate this capability, we performed simulations and physical experiments using a six-threshold energy resolved photon-counting detector. We imaged mouse-sized cylindrical phantoms filled with several soft-tissue-like and bone-like materials and with iodine-based and gadolinium-based contrast agents. The linear attenuation coefficients were reconstructed for each material in each energy window and were visualized as scatter plots between pairs of energy windows. For comparison, a dual-kVp CT was also simulated using the same phantom materials. In this case, the linear attenuation coefficients at the lower kVp were plotted against those at the higher kVp. Results: In both the simulations and the physical experiments, the contrast agents were easily separable from other soft-tissue-like and bone-like materials, thanks to the availability of the attenuation coefficient measurements at more than two energies provided by the energy resolved photon-counting detector. In the simulations, the amount of separation was observed to be proportional to the concentration of the contrast agents; however, this was not observed in the physical experiments due to limitations of the real detector system. We used the angle between pairs of attenuation coefficient vectors in either the 5-D space (for non-contrast-agent materials using energy resolved photon

  1. Micro energy dispersive X-ray fluorescence analysis of polychrome lead-glazed Portuguese faiences

    NASA Astrophysics Data System (ADS)

    Guilherme, A.; Pessanha, S.; Carvalho, M. L.; dos Santos, J. M. F.; Coroado, J.

    2010-04-01

    Several glazed ceramic pieces, originally produced in Coimbra (Portugal), were submitted to elemental analysis, having as premise the pigment manufacture production recognition. Although having been produced in Coimbra, their location changed as time passed due to historical reasons. A recent exhibition in Coimbra brought together a great number of these pieces and in situ micro Energy Dispersive X-ray Fluorescence (µ-EDXRF) analyses were performed in order to achieve some chemical and physical data on the manufacture of faiences in Coimbra. A non-commercial µ-EDXRF equipment for in situ analysis was employed in this work, carrying some important improvements when compared to the conventional ones, namely, analyzing spot sizes of about 100 µm diameter. The combination of a capillary X-ray lens with a new generation of low power microfocus X-ray tube and a drift chamber detector enabled a portable unit for micro-XRF with a few tens of µm lateral resolution. The advantages in using a portable system emphasized with polycapillary optics enabled to distinguish proximal different pigmented areas, as well as the glaze itself. These first scientific results on the pigment analysis of the collection of faiences seem to point to a unique production center with own techniques and raw materials. This conclusion arose with identification of the blue pigments having in its constitution Mn, Fe Co and As and the yellows as a result of the combination between Pb and Sb. A statistical treatment was used to reveal groups of similarities on the pigments elemental profile.

  2. X-ray lithography masking

    NASA Technical Reports Server (NTRS)

    Smith, Henry I. (Inventor); Lim, Michael (Inventor); Carter, James (Inventor); Schattenburg, Mark (Inventor)

    1998-01-01

    X-ray masking apparatus includes a frame having a supporting rim surrounding an x-ray transparent region, a thin membrane of hard inorganic x-ray transparent material attached at its periphery to the supporting rim covering the x-ray transparent region and a layer of x-ray opaque material on the thin membrane inside the x-ray transparent region arranged in a pattern to selectively transmit x-ray energy entering the x-ray transparent region through the membrane to a predetermined image plane separated from the layer by the thin membrane. A method of making the masking apparatus includes depositing back and front layers of hard inorganic x-ray transparent material on front and back surfaces of a substrate, depositing back and front layers of reinforcing material on the back and front layers, respectively, of the hard inorganic x-ray transparent material, removing the material including at least a portion of the substrate and the back layers of an inside region adjacent to the front layer of hard inorganic x-ray transparent material, removing a portion of the front layer of reinforcing material opposite the inside region to expose the surface of the front layer of hard inorganic x-ray transparent material separated from the inside region by the latter front layer, and depositing a layer of x-ray opaque material on the surface of the latter front layer adjacent to the inside region.

  3. Low-energy d-d excitations in MnO studied by resonant x-ray fluorescence spectroscopy

    SciTech Connect

    Butorin, S.M.; Guo, J.; Magnuson, M.

    1997-04-01

    Resonant soft X-ray emission spectroscopy has been demonstrated to possess interesting abilities for studies of electronic structure in various systems, such as symmetry probing, alignment and polarization dependence, sensitivity to channel interference, etc. In the present abstract the authors focus on the feasibility of resonant soft X-ray emission to probe low energy excitations by means of resonant electronic X-ray Raman scattering. Resonant X-ray emission can be regarded as an inelastic scattering process where a system in the ground state is transferred to a low excited state via a virtual core excitation. The energy closeness to a core excitation of the exciting radiation enhances the (generally) low probability for inelastic scattering at these wavelengths. Therefore soft X-ray emission spectroscopy (in resonant electronic Raman mode) can be used to study low energy d-d excitations in transition metal systems. The involvement of the intermediate core state allows one to use the selection rules of X-ray emission, and the appearance of the elastically scattered line in the spectra provides the reference to the ground state.

  4. The LCLS variable-energy hard X-ray single-shot spectrometer.

    PubMed

    Rich, David; Zhu, Diling; Turner, James; Zhang, Dehong; Hill, Bruce; Feng, Yiping

    2016-01-01

    The engineering design, implementation, operation and performance of the new variable-energy hard X-ray single-shot spectrometer (HXSSS) for the LCLS free-electron laser (FEL) are reported. The HXSSS system is based on a cylindrically bent Si thin crystal for dispersing the incident polychromatic FEL beam. A spatially resolved detector system consisting of a Ce:YAG X-ray scintillator screen, an optical imaging system and a low-noise pixelated optical camera is used to record the spectrograph. The HXSSS provides single-shot spectrum measurements for users whose experiments depend critically on the knowledge of the self-amplified spontaneous emission FEL spectrum. It also helps accelerator physicists for the continuing studies and optimization of self-seeding, various improved mechanisms for lasing mechanisms, and FEL performance improvements. The designed operating energy range of the HXSSS is from 4 to 20 keV, with the spectral range of order larger than 2% and a spectral resolution of 2 × 10(-5) or better. Those performance goals have all been achieved during the commissioning of the HXSSS.

  5. Practical applications of energy dispersive X-ray microanalysis in diagnostic oral pathology

    SciTech Connect

    Daley, T.D.; Gibson, D. )

    1990-03-01

    Energy dispersive X-ray microanalysis is a powerful tool that can reveal the presence and relative quantities of elements in minute particles in biologic materials. Although this technique has been used in some aspects of dental research, it has rarely been applied to diagnostic oral pathology. The purpose of this paper is to inform practicing dentists and oral specialists about the diagnostic potential of this procedure by presenting three case reports. The first case involved the identification of flakes of a metallic material claimed by a 14-year-old girl to appear periodically between her mandibular molars. In the second case, a periodontist was spared a lawsuit when a freely mobile mass in the antrum of his patient was found to be a calcium-phosphorus compound not related to the periodontal packing that had been used. The third case involved the differential diagnosis of amalgam tattoo and graphite tattoo in a pigmented lesion of the hard palate mucosa. The results of the analyses were significant and indicate a role for this technique in the assessment of selected cases. Potential for wider use of energy dispersive X-ray microanalysis in diagnostic oral pathology exists as research progresses.

  6. Performance of Gas Scintillation Proportional Counter Array for High-Energy X-Ray Observatory

    NASA Technical Reports Server (NTRS)

    Gubarev, Mikhail; Ramsey, Brian; Apple, Jeffery

    2004-01-01

    A focal plane array of high-pressure gas scintillation proportional counters (GSPC) for a High Energy X-Ray Observatory (HERO) is developed at the Marshall Space Flight Center. The array is consisted from eight GSPCs and is a part of balloon born payload scheduled to flight in May 2004. These detectors have an active area of approximately 20 square centimeters, and are filled with a high pressure (10(exp 6) Pa) xenon-helium mixture. Imaging is via crossed-grid position-sensitive phototubes sensitive in the UV region. The performance of the GSPC is well matched to that of the telescopes x-ray optics which have response to 75 keV and a focal spot size of approximately 500 microns. The detector's energy resolution, 4% FWHM at 60 keV, is adequate for resolving the broad spectral lines of astrophysical importance and for accurate continuum measurements. Results of the on-earth detector calibration will be presented and in-flight detector performance will be provided, as available.

  7. Low-energy x-ray emission from magnetic-fusion plasmas

    SciTech Connect

    Hill, K.W.; Bitter, M.; Eames, D.; von Goeler, S.; Goldman, M.; Sauthoff, N.R.; Silver, E.

    1982-04-01

    Complex, transient, spatially inhomogeneous tokamak plasmas require careful diagnosis. As the reactor regime is approached, soft x rays become more important as a versatile diagnostic tool and an energy-loss mechanism. Continuum emission provides a measure of electron temperature and light impurity content. Impurity lines serve as a probe for ion and electron temperature, impurity behavior, and radiative cooling. The entire spectrum yields vital information on instabilities and disruptions. The importance of impurities is illustrated by the extensive efforts toward understanding impurity production, effects, and control. Minute heavy impurity concentrations can prevent reactor ignition. Si(Li) - detector arrays give a broad overview of continuum and line x-ray emission (.3 to 50 keV) with moderate energy (200 eV) and time (50 ms) resolution. Bragg crystal and grating spectrometers provide detailed information on impurity lines with moderate to excellent (E/..delta..E = 100 to 23,000) resolving power and 1 to 50 ms time resolution. Imaging detector arrays measure rapid (approx. 10 ..mu..s) fluctuations due to MHD instabilities and probe impurity behavior and radiative cooling. Future tokamaks require more diagnostic channels to avoid spatial scanning, higher throughput for fast, single-shot diagnosis, increased spectral information per sample period via fast scanning or use of multi-element detectors with dispersive elements, and radiation shielding and hardening of detectors.

  8. The LCLS variable-energy hard X-ray single-shot spectrometer

    SciTech Connect

    Rich, David; Zhu, Diling; Turner, James; Zhang, Dehong; Hill, Bruce; Feng, Yiping

    2016-01-01

    The engineering design, implementation, operation and performance of the new variable-energy hard X-ray single-shot spectrometer (HXSSS) for the LCLS free-electron laser (FEL) are reported. The HXSSS system is based on a cylindrically bent Si thin crystal for dispersing the incident polychromatic FEL beam. A spatially resolved detector system consisting of a Ce:YAG X-ray scintillator screen, an optical imaging system and a low-noise pixelated optical camera is used to record the spectrograph. The HXSSS provides single-shot spectrum measurements for users whose experiments depend critically on the knowledge of the self-amplified spontaneous emission FEL spectrum. It also helps accelerator physicists for the continuing studies and optimization of self-seeding, various improved mechanisms for lasing mechanisms, and FEL performance improvements. The designed operating energy range of the HXSSS is from 4 to 20 keV, with the spectral range of order larger than 2% and a spectral resolution of 2 × 10-5or better. Those performance goals have all been achieved during the commissioning of the HXSSS.

  9. The LCLS variable-energy hard X-ray single-shot spectrometer

    SciTech Connect

    Rich, David; Zhu, Diling; Turner, James; Zhang, Dehong; Hill, Bruce; Feng, Yiping

    2016-01-01

    The engineering design, implementation, operation and performance of the new variable-energy hard X-ray single-shot spectrometer (HXSSS) for the LCLS free-electron laser (FEL) are reported. The HXSSS system is based on a cylindrically bent Si thin crystal for dispersing the incident polychromatic FEL beam. A spatially resolved detector system consisting of a Ce:YAG X-ray scintillator screen, an optical imaging system and a low-noise pixelated optical camera is used to record the spectrograph. The HXSSS provides single-shot spectrum measurements for users whose experiments depend critically on the knowledge of the self-amplified spontaneous emission FEL spectrum. It also helps accelerator physicists for the continuing studies and optimization of self-seeding, various improved mechanisms for lasing mechanisms, and FEL performance improvements. The designed operating energy range of the HXSSS is from 4 to 20 keV, with the spectral range of order larger than 2% and a spectral resolution of 2 × 10-5or better. Those performance goals have all been achieved during the commissioning of the HXSSS.

  10. The LCLS variable-energy hard X-ray single-shot spectrometer.

    PubMed

    Rich, David; Zhu, Diling; Turner, James; Zhang, Dehong; Hill, Bruce; Feng, Yiping

    2016-01-01

    The engineering design, implementation, operation and performance of the new variable-energy hard X-ray single-shot spectrometer (HXSSS) for the LCLS free-electron laser (FEL) are reported. The HXSSS system is based on a cylindrically bent Si thin crystal for dispersing the incident polychromatic FEL beam. A spatially resolved detector system consisting of a Ce:YAG X-ray scintillator screen, an optical imaging system and a low-noise pixelated optical camera is used to record the spectrograph. The HXSSS provides single-shot spectrum measurements for users whose experiments depend critically on the knowledge of the self-amplified spontaneous emission FEL spectrum. It also helps accelerator physicists for the continuing studies and optimization of self-seeding, various improved mechanisms for lasing mechanisms, and FEL performance improvements. The designed operating energy range of the HXSSS is from 4 to 20 keV, with the spectral range of order larger than 2% and a spectral resolution of 2 × 10(-5) or better. Those performance goals have all been achieved during the commissioning of the HXSSS. PMID:26698039

  11. Development of a dual MCP framing camera for high energy x-rays

    SciTech Connect

    Izumi, N. Hall, G. N.; Carpenter, A. C.; Allen, F. V.; Cruz, J. G.; Felker, B.; Hargrove, D.; Holder, J.; Lumbard, A.; Montesanti, R.; Palmer, N. E.; Piston, K.; Stone, G.; Thao, M.; Vern, R.; Zacharias, R.; Landen, O. L.; Tommasini, R.; Bradley, D. K.; Bell, P. M.; and others

    2014-11-15

    Recently developed diagnostic techniques at LLNL require recording backlit images of extremely dense imploded plasmas using hard x-rays, and demand the detector to be sensitive to photons with energies higher than 50 keV [R. Tommasini et al., Phys. Phys. Plasmas 18, 056309 (2011); G. N. Hall et al., “AXIS: An instrument for imaging Compton radiographs using ARC on the NIF,” Rev. Sci. Instrum. (these proceedings)]. To increase the sensitivity in the high energy region, we propose to use a combination of two MCPs. The first MCP is operated in a low gain regime and works as a thick photocathode, and the second MCP works as a high gain electron multiplier. We tested the concept of this dual MCP configuration and succeeded in obtaining a detective quantum efficiency of 4.5% for 59 keV x-rays, 3 times larger than with a single plate of the thickness typically used in NIF framing cameras.

  12. Incident-energy-dependent spectral weight of resonant inelastic x-ray scattering in doped cuprates

    NASA Astrophysics Data System (ADS)

    Tsutsui, Kenji; Tohyama, Takami

    2016-08-01

    We theoretically investigate the incident-photon energy ωi dependence of resonant inelastic x-ray scattering (RIXS) tuned for the Cu L edge in cuprate superconductors by using the exact diagonalization technique for a single-band Hubbard model. Depending on the value of core-hole Coulomb interaction in the intermediate state, RIXS for non-spin-flip channel shows either a ωi-dependent fluorescencelike or ωi-independent Raman-like behavior for hole doping. An analysis of x-ray absorption suggests that the core-hole Coulomb interaction is larger than on-site Coulomb interaction in the Hubbard model, resulting in a fluorescencelike behavior in RIXS consistent with recent RIXS experiments. A shift on the high-energy side of the center of spectral distribution is also predicted for electron-doped systems though spectral weight is small. Main structures in the spin-flip channel exhibit a Raman-like behavior as expected, accompanied with a fluorescencelike behavior with small intensity.

  13. High energy white beam x-ray diffraction studies of residual strains in engineering components

    NASA Astrophysics Data System (ADS)

    Zhang, S. Y.; Vorster, W.; Jun, T. S.; Song, X.; Golshan, M.; Laundy, D.; Walsh, M. J.; Korsunsky, A. M.

    2008-09-01

    In order to predict the durability of engineering components and improve performance, it is mandatory to understand residual stresses. The last decade has witnessed a significant increase of residual stress evaluation using diffraction of penetrating radiation, such as neutrons or high energy X-rays. They provide a powerful non-destructive method for determining the level of residual stresses in engineering components through precise characterisation of interplanar crystal lattice spacing. The unique non-destructive nature of these measurement techniques is particularly beneficial in the context of engineering design, since it allows the evaluation of a variety of structural and deformational parameters inside real components without material removal, or at worst with minimal interference. However, while most real engineering components have complex shape and are often large in size, leading to measurement and interpretation difficulties, since experimental facilities usually have limited space for mounting the sample, limited sample travel range, limited loading capacity of the sample positioning system, etc. Consequently, samples often have to be sectioned, requiring appropriate corrections on measured data; or facilities must be improved. Our research group has contributed to the development of engineering applications of high-energy X-ray diffraction methods for residual stress evaluation, both at synchrotron sources and in the lab setting, including multiple detector setup, large engineering component manipulation and measurement at the UK Synchrotron Radiation Source (SRS Daresbury), and in our lab at Oxford. A nickel base superalloy combustion casing and a large MIG welded Al alloy plate were successfully studied.

  14. Si(Li) detectors with thin dead layers for low energy x-ray detection

    SciTech Connect

    Rossington, C.S.; Walton, J.T.; Jaklevic, J.M.

    1990-10-01

    Regions of incomplete charge collection, or dead layers'', are compared for Si(Li) detectors fabricated with Au and Pd entrance window electrodes. The dead layers were measured by characterizing the detector spectral response to x-ray energies above and below the Si K{alpha} absorption edge. It was found that Si(Li) detectors with Pd electrodes exhibit consistently thinner effective Si dead layers than those with Au electrodes. Furthermore, it is demonstrated that the minimum thickness required for low resistivity Pd electrodes is thinner than that required for low resistivity Au electrodes, which further reduces the signal attenuation in Pd/Si(Li) detectors. A model, based on Pd compensation of oxygen vacancies in the SiO{sub 2} at the entrance window Si(Li) surface, is proposed to explain the observed differences in detector dead layer thickness. Electrode structures for optimum Si(Li) detector performance at low x-ray energies are discussed. 18 refs., 8 figs., 1 tab.

  15. X-Ray Background Survey Spectrometer (XBSS)

    NASA Technical Reports Server (NTRS)

    Sanders, W. T. (Principal Investigator); Paulos, R. J.

    1996-01-01

    The objective of this investigation was to perform a spectral survey of the low energy diffuse X-ray background using the X-ray Background Survey Spectrometer (XBSS) on board the Space Station Freedom (SSF). XBSS obtains spectra of the X-ray diffuse background in the 11-24 A and 44-84 A wavelength intervals over the entire sky with 15 deg spatial resolution. These X-rays are almost certainly from a very hot (10(exp 6) K) component of the interstellar medium that is contained in regions occupying a large fraction of the interstellar volume near the Sun. Astrophysical plasmas near 10(exp 6) K are rich in emission lines, and the relative strengths of these lines, besides providing information about the physical conditions of the emitting gas, also provide information about its history and heating mechanisms.

  16. High energy x-ray phase contrast CT using glancing-angle grating interferometers

    SciTech Connect

    Sarapata, A.; Stayman, J. W.; Siewerdsen, J. H.; Finkenthal, M.; Stutman, D.; Pfeiffer, F.

    2014-02-15

    Purpose: The authors present initial progress toward a clinically compatible x-ray phase contrast CT system, using glancing-angle x-ray grating interferometry to provide high contrast soft tissue images at estimated by computer simulation dose levels comparable to conventional absorption based CT. Methods: DPC-CT scans of a joint phantom and of soft tissues were performed in order to answer several important questions from a clinical setup point of view. A comparison between high and low fringe visibility systems is presented. The standard phase stepping method was compared with sliding window interlaced scanning. Using estimated dose values obtained with a Monte-Carlo code the authors studied the dependence of the phase image contrast on exposure time and dose. Results: Using a glancing angle interferometer at high x-ray energy (∼45 keV mean value) in combination with a conventional x-ray tube the authors achieved fringe visibility values of nearly 50%, never reported before. High fringe visibility is shown to be an indispensable parameter for a potential clinical scanner. Sliding window interlaced scanning proved to have higher SNRs and CNRs in a region of interest and to also be a crucial part of a low dose CT system. DPC-CT images of a soft tissue phantom at exposures in the range typical for absorption based CT of musculoskeletal extremities were obtained. Assuming a human knee as the CT target, good soft tissue phase contrast could be obtained at an estimated absorbed dose level around 8 mGy, similar to conventional CT. Conclusions: DPC-CT with glancing-angle interferometers provides improved soft tissue contrast over absorption CT even at clinically compatible dose levels (estimated by a Monte-Carlo computer simulation). Further steps in image processing, data reconstruction, and spectral matching could make the technique fully clinically compatible. Nevertheless, due to its increased scan time and complexity the technique should be thought of not as

  17. X-ray beam design for multi-energy imaging with charge-integrating detector: A simulation study

    NASA Astrophysics Data System (ADS)

    Baek, Cheol-Ha; Kim, Daehong

    2015-11-01

    Multi-energy X-ray imaging systems have been widely used for clinical examinations. In order to enhance the imaging quality of these X-ray systems, a dual-energy system that can obtain specific information has been developed in order to discriminate different materials. Although the dual-energy system shows reliable performance for clinical applications, it is necessary to improve the method in order to minimize radiation dose, reduce projection error, and increase image contrast. The purpose of this study is to develop a triple energy technique that can discriminate three materials for the purpose of enhancing imaging quality and patient safety. The X-ray system tube voltage was varied from 40 to 90 kV, and filters (that can generate three X-ray energies) were installed, consisting of pure elemental materials in foil form (including Al, Cu, I, Ba, Ce, Gd, Er, and W). The X-ray beam was evaluated with respect to mean energy ratio, contrast variation ratio, and exposure efficiency. In order to estimate the performance of the suggested technique, Monte Carlo was conducted, and the results were compared to the photon-counting method. As a result, the density maps of iodine, aluminum, and polymethyl methacrylate (PMMA) using the X-ray beam were more accurate in comparison to that obtained with the photon-counting method. According to the results, the suggested triple energy technique can improve the accuracy of the determination of thickness of density. Moreover, the X-ray beam could reduce unnecessary patient dose.

  18. Energy Dispersive X-Ray and Electrochemical Impedance Spectroscopies for Performance and Corrosion Analysis of PEMWEs

    NASA Astrophysics Data System (ADS)

    Steen, S. M., Iii; Zhang, F.-Y.

    2014-11-01

    Proton exchange membrane water electrolyzers (PEMWEs) are a promising energy storage technology due to their high efficiency, compact design, and ability to be used in a renewable energy system. Before they are able to make a large commercial impact, there are several hurdles facing the technology today. Two powerful techniques for both in-situ and ex- situ characterizations to improve upon their performance and better understand their corrosion are electrochemical impedance spectroscopy and energy dispersive x-ray spectroscopy, respectively. In this paper, the authors use both methods in order to characterize the anode gas diffusion layer (GDL) in a PEMWE cell and better understand the corrosion that occurs in the oxygen electrode during electrolysis.

  19. Shakeup in soft-x-ray emission. I. The low-energy tail

    NASA Astrophysics Data System (ADS)

    Livins, Peteris; Schnatterly, S. E.

    1988-04-01

    The L soft-x-ray emission spectra for Al and Si, and the K emission for graphite and diamond are analyzed, taking into account the effects of multielectron transitions which produce a low-energy tail on the main band. Through an appropriate transformation on the initial states, it is shown that the final-state rule of Von Barth and Grossman is a direct result of exchange. A ``Pauli rigidity'' forces the initial-state wave function to approach that of the final state, except near the Fermi energy. An assumption of random phases allows a formal solution that includes single-particle shakeup events to all orders. It is argued that a low-energy feature of silicon is structure due to the shakeup of single-particle-like excitations rather than a plasmon satellite.

  20. Characterization of a 2D soft x-ray tomography camera with discrimination in energy bands

    SciTech Connect

    Romano, A.; Pacella, D.; Gabellieri, L.; Tilia, B.; Piergotti, V.; Mazon, D.; Malard, P.

    2010-10-15

    A gas detector with a 2D pixel readout is proposed for a future soft x-ray (SXR) tomography with discrimination in energy bands separately per pixel. The detector has three gas electron multiplier foils for the electron amplification and it offers the advantage, compared with the single stage, to be less sensitive to neutrons and gammas. The energy resolution and the detection efficiency of the detector have been accurately studied in the laboratory with continuous SXR spectra produced by an electronic tube and line emissions produced by fluorescence (K, Fe, and Mo) in the range of 3-17 keV. The front-end electronics, working in photon counting mode with a selectable threshold for pulse discrimination, is optimized for high rates. The distribution of the pulse amplitude has been indirectly derived by means of scans of the threshold. Scans in detector gain have also been performed to assess the capability of selecting different energy ranges.

  1. Hard x-ray generation by low energy, tightly focused laser pulses

    NASA Astrophysics Data System (ADS)

    Takano, K.; Nemoto, K.; Nayuki, T.; Oishi, Y.; Fujii, T.; Zhidkov, A.; Hotta, E.; Todoriki, M.; Hasegawa, S.

    2008-06-01

    The interaction of λ2 laser pulses with plasma is studied to scale the high-field physics from high power laser systems to low-energy, high-repetition-rate lasers. For this purpose, 20mJ, 40fs Ti:sapphire laser pulses were focused in a spot of 2.2×2.3μm2 with a maximum intensity of I ˜1019W/cm2. Efficient generations of energetic electrons (˜1MeV) and hard x-rays with energies of over 100keV were obtained by irradiating the low-energy, tightly focused laser pulses on a massive Cu target.

  2. Boundary displacement measurements using multi-energy soft x-rays

    SciTech Connect

    Tritz, K. Stutman, D.; Diallo, A.; LeBlanc, B. P.; Sabbagh, S.

    2014-11-15

    The Multi-Energy Soft X-ray (ME-SXR) system on NSTX provides radial profiles of soft X-ray emission, measured through a set of filters with varying thickness, which have been used to reconstruct the electron temperature on fast time scales (∼10 kHz). In addition to this functionality, here we show that the ME-SXR system can be used to measure the boundary displacement of the NSTX plasma with a few mm spatial resolution during magnetohydrodyamic (MHD) activity. Boundary displacement measurements can serve to inform theoretical predictions of neoclassical toroidal viscosity, and will be used to investigate other edge phenomena on NSTX-U. For example, boundary measurements using filtered SXR measurements can provide information on pedestal steepness and dynamic evolution leading up to and during edge localized modes (ELMs). Future applications include an assessment of a simplified, filtered SXR edge detection system as well as its suitability for real-time non-magnetic boundary feedback for ELMs, MHD, and equilibrium position control.

  3. Material Discrimination for Treaty Verification with Multi-energy, X-ray Radiography

    SciTech Connect

    Gilbert, Andrew J.; McDonald, Benjamin S.; Robinson, Sean M.; White, Timothy A.; Jarman, Kenneth D.; Deinert, Mark

    2013-06-10

    As nuclear warhead stockpiles are reduced under current and future arms treaties, accuracy in accountancy of material stockpiles becomes increasingly important. Image-based active interrogation offers advantages to spectroscopic detection in its ability to measure the location and extent of a material, or materials, of interest from a declaration. However, the detail that imaging provides is often viewed as too intrusive due to its potential to disseminate sensitive information. In this work, we present a method for reducing multi-energy, x-ray radiography data to a few important attributes, based on declarations from behind an information barrier, which can then be used to confirm or deny a declaration. We build on previous work by improving the physics modeling; considering currently attainable, multiple-endpoint x-ray systems; and posing the problem as a nonlinear, inverse problem. Regularization is added to the problem, which smooths the solution and stabilizes an otherwise unstable solution. Here we show the ability to discriminate high-atomic–number materials from others with simulated single-view multiple-endpoint radiography data and present results from initial bench-top measurements.

  4. The Next Generation Atlas of Quasar Spectral Energy Distributions from Radio to X-Rays

    NASA Astrophysics Data System (ADS)

    Shang, Zhaohui; Brotherton, Michael S.; Wills, Beverley J.; Wills, D.; Cales, Sabrina L.; Dale, Daniel A.; Green, Richard F.; Runnoe, Jessie C.; Nemmen, Rodrigo S.; Gallagher, Sarah C.; Ganguly, Rajib; Hines, Dean C.; Kelly, Benjamin J.; Kriss, Gerard A.; Li, Jun; Tang, Baitian; Xie, Yanxia

    2011-09-01

    We have produced the next generation of quasar spectral energy distributions (SEDs), essentially updating the work of Elvis et al. by using high-quality data obtained with several space- and ground-based telescopes, including NASA's Great Observatories. We present an atlas of SEDs of 85 optically bright, non-blazar quasars over the electromagnetic spectrum from radio to X-rays. The heterogeneous sample includes 27 radio-quiet and 58 radio-loud quasars. Most objects have quasi-simultaneous ultraviolet-optical spectroscopic data, supplemented with some far-ultraviolet spectra, and more than half also have Spitzer mid-infrared Infrared Spectrograph spectra. The X-ray spectral parameters are collected from the literature where available. The radio, far-infrared, and near-infrared photometric data are also obtained from either the literature or new observations. We construct composite SEDs for radio-loud and radio-quiet objects and compare these to those of Elvis et al., finding that ours have similar overall shapes, but our improved spectral resolution reveals more detailed features, especially in the mid- and near-infrared.

  5. First TDCR measurements at low energies using a miniature x-ray tube.

    PubMed

    Halter, E; Thiam, C; Bobin, C; Bouchard, J; Chambellan, D; Chauvenet, B; Hamel, M; Rocha, L; Trocmé, M; Woo, R

    2014-11-01

    Developed for radionuclide standardization using liquid scintillation, the Triple to Double Coincidence Ratio (TDCR) method is applied using coincidence counting obtained with a specific three-photomultiplier system. For activity determination, a statistical model of light emission is classically used to establish a relation between the detection efficiency and the experimental TDCR value. At LNE-LNHB, a stochastic approach of the TDCR modeling was developed using the Monte Carlo code Geant4. The interest of this TDCR-Geant4 model is the possibility to simulate the propagation of optical photons from their creation in the scintillation vial to the production of photoelectrons in photomultipliers. As an alternative to the use of radionuclide sources, first TDCR measurements are presented using a miniature x-ray tube closely coupled to the scintillation vial. The objective of this new set-up was to enable low-energy depositions (lower than 20 keV) in liquid scintillator in order to study the influence of both time and geometrical dependence between PMTs already observed with radioactive sources. As for the statistical TDCR model, the non-linearity of light emission is implemented in the TDCR-Geant4 model using the Birks formula which depends on the kB factor and the scintillation yield. Measurements performed with the x-ray tube are extended to the assessment of these parameters and they are tested afterwards in the TDCR-Geant4 model for activity measurements of (3)H. PMID:24685767

  6. THE NEXT GENERATION ATLAS OF QUASAR SPECTRAL ENERGY DISTRIBUTIONS FROM RADIO TO X-RAYS

    SciTech Connect

    Shang Zhaohui; Li Jun; Xie Yanxia; Brotherton, Michael S.; Cales, Sabrina L.; Dale, Daniel A.; Runnoe, Jessie C.; Kelly, Benjamin J.; Wills, Beverley J.; Wills, D.; Green, Richard F.; Nemmen, Rodrigo S.; Ganguly, Rajib; Hines, Dean C.; Kriss, Gerard A.; Tang, Baitian

    2011-09-01

    We have produced the next generation of quasar spectral energy distributions (SEDs), essentially updating the work of Elvis et al. by using high-quality data obtained with several space- and ground-based telescopes, including NASA's Great Observatories. We present an atlas of SEDs of 85 optically bright, non-blazar quasars over the electromagnetic spectrum from radio to X-rays. The heterogeneous sample includes 27 radio-quiet and 58 radio-loud quasars. Most objects have quasi-simultaneous ultraviolet-optical spectroscopic data, supplemented with some far-ultraviolet spectra, and more than half also have Spitzer mid-infrared Infrared Spectrograph spectra. The X-ray spectral parameters are collected from the literature where available. The radio, far-infrared, and near-infrared photometric data are also obtained from either the literature or new observations. We construct composite SEDs for radio-loud and radio-quiet objects and compare these to those of Elvis et al., finding that ours have similar overall shapes, but our improved spectral resolution reveals more detailed features, especially in the mid- and near-infrared.

  7. Biomedical and agricultural applications of energy dispersive X-ray spectroscopy in electron microscopy.

    PubMed

    Wyroba, Elżbieta; Suski, Szymon; Miller, Karolina; Bartosiewicz, Rafał

    2015-09-01

    Energy dispersive X-ray spectroscopy (EDS) in electron microscopy has been widely used in many research areas since it provides precise information on the chemical composition of subcellular structures that may be correlated with their high resolution images. In EDS the characteristic X-rays typical of each element are analyzed and the new detectors - an example of which we describe - allow for setting precisely the area of measurements and acquiring signals as a point analysis, as a linescan or in the image format of the desired area. Mapping of the elements requires stringent methods of sample preparation to prevent redistribution/loss of the elements as well as elimination of the risk of overlapping spectra. Both qualitative and quantitative analyses may be performed at a low probe current suitable for thin biological samples. Descriptions of preparation techniques, drawbacks and precautions necessary to obtain reliable results are provided, including data on standards, effects of specimen roughness and quantification. Data on EPMA application in different fields of biomedical and agricultural studies are reviewed. In this review we refer to recent EDS/EPMA applications in medical diagnostics, studies on air pollution and agrochemicals as well as on plant models used to monitor the environment.

  8. CALIBRATION OF THE NuSTAR HIGH-ENERGY FOCUSING X-RAY TELESCOPE

    SciTech Connect

    Madsen, Kristin K.; Harrison, Fiona A.; Grefenstette, Brian W.; Miyasaka, Hiromasa; Forster, Karl; Fuerst, Felix; Rana, Vikram; Walton, Dominic J.; Markwardt, Craig B.; An, Hongjun; Bachetti, Matteo; Kitaguchi, Takao; Bhalerao, Varun; Boggs, Steve; Craig, William W.; Christensen, Finn E.; Hailey, Charles J.; Perri, Matteo; Puccetti, Simonetta; Stern, Daniel; and others

    2015-09-15

    We present the calibration of the Nuclear Spectroscopic Telescope Array (NuSTAR) X-ray satellite. We used the Crab as the primary effective area calibrator and constructed a piece-wise linear spline function to modify the vignetting response. The achieved residuals for all off-axis angles and energies, compared to the assumed spectrum, are typically better than ±2% up to 40 keV and 5%–10% above due to limited counting statistics. An empirical adjustment to the theoretical two-dimensional point-spread function (PSF) was found using several strong point sources, and no increase of the PSF half-power diameter has been observed since the beginning of the mission. We report on the detector gain calibration, good to 60 eV for all grades, and discuss the timing capabilities of the observatory, which has an absolute timing of ±3 ms. Finally, we present cross-calibration results from two campaigns between all the major concurrent X-ray observatories (Chandra, Swift, Suzaku, and XMM-Newton), conducted in 2012 and 2013 on the sources 3C 273 and PKS 2155-304, and show that the differences in measured flux is within ∼10% for all instruments with respect to NuSTAR.

  9. Solar flares X-ray polarimetry in a wide energy band

    NASA Astrophysics Data System (ADS)

    Fabiani, Sergio; Campana, Riccardo; Costa, Enrico; Muleri, Fabio; Bellazzini, Ronaldo; Soffitta, Paolo; Del Monte, Ettore; Rubini, Alda

    2012-07-01

    Polarimetry of solar flares X-ray emission is an additional tool for investigating particles dynamics within the solar atmosphere. Accelerated electrons by magnetic reconnection in the corona produce bremsstrahlung radiation as primary emission in the footpoints of a solar flare which has moreover the possibility to be Compton backscattered resulting in albedo emission. Non-thermal bremsstrahlung emission is expected to be a significant above 15 keV and highly polarized. The albedo component peaks between 20 and 50 keV, its polarization properties depend on the Compton scattering angle. Such a diffusion modifies the spectrum and the polarization of the primary bremsstrahlung emission. Hard X-ray polarimetry, spectroscopy and imaging are therefore necessary to disentangle and modeling the different components in a solar flare. We present a non imaging Compton polarimeter sensitive from 20 keV designed as a single scattering unit surrounded by absorbers of high atomic number. A photelectric polarimeter based on the Gas Pixel Detector technology sensitive in the 15-35 keV energy band can be coupled for imaging.

  10. HERO: High Energy Replicated Optics for a Hard-X-Ray Balloon Payload

    NASA Technical Reports Server (NTRS)

    Ramsey, B.; Engelhaupt, D.; Speegle, C. O.; ODell, S. L.; Austin, R. A.; Elsner, R. F.; Kolodziejczak, J. J.; Weisskopf, M. C.

    2000-01-01

    We are developing high-energy grazing-incidence replicated optics for a balloon-borne hard-x-ray telescope. When completed, the instrument will have 170 cm2 of effective collecting area at 40 keV and 130 square cm at 60 keV with <= 30 arc seconds half power diameter. This payload will offer unprecedented sensitivity in the hard-x-ray region, with around 250 microCrab sensitivity on long-duration flights and 50-100 microCrab on ultra- long-duration balloon missions The payload consists of 16 mirror modules, each with 14 nested mirrors made from a high-strength nickel alloy, and a corresponding array of 16 focal plane detectors. An engineering demonstration flight is scheduled for the Spring of 2000, using just two mirror modules each with 3 shells, above a pair of gas-scintillation-proportional counters. This flight is intended to test a newly designed gondola pointing and aspect system and the stability of the optical bench design. The first scientific flight of the full payload is scheduled for the Fall of 2002. Full details of the payload and its capabilities will be presented together with data from various mirror-module tests. If available data from the first flight will also be presented.

  11. Efficacy of fixed filtration for rapid kVp-switching dual energy x-ray systems

    SciTech Connect

    Yao, Yuan; Wang, Adam S.; Pelc, Norbert J.

    2014-03-15

    Purpose: Dose efficiency of dual kVp imaging can be improved if the two beams are filtered to remove photons in the common part of their spectra, thereby increasing spectral separation. While there are a number of advantages to rapid kVp-switching for dual energy, it may not be feasible to have two different filters for the two spectra. Therefore, the authors are interested in whether a fixed added filter can improve the dose efficiency of kVp-switching dual energy x-ray systems. Methods: The authors hypothesized that a K-edge filter would provide the energy selectivity needed to remove overlap of the spectra and hence increase the precision of material separation at constant dose. Preliminary simulations were done using calcium and water basis materials and 80 and 140 kVp x-ray spectra. Precision of the decomposition was evaluated based on the propagation of the Poisson noise through the decomposition function. Considering availability and cost, the authors chose a commercial Gd{sub 2}O{sub 2}S screen as the filter for their experimental validation. Experiments were conducted on a table-top system using a phantom with various thicknesses of acrylic and copper and 70 and 125 kVp x-ray spectra. The authors kept the phantom exposure roughly constant with and without filtration by adjusting the tube current. The filtered and unfiltered raw data of both low and high energy were decomposed into basis material and the variance of the decomposition for each thickness pair was calculated. To evaluate the filtration performance, the authors measured the ratio of material decomposition variance with and without filtration. Results: Simulation results show that the ideal filter material depends on the object composition and thickness, and ranges across the lanthanide series, with higher atomic number filters being preferred for more attenuating objects. Variance reduction increases with filter thickness, and substantial reductions (40%) can be achieved with a 2× loss in

  12. Characterization of medium-range order in organic-inorganic hybrid nanomaterials by fluctuation x-ray microscopy.

    SciTech Connect

    Fan, L.; Paterson, D.; McNulty, I.; Treacy, M. M. J.; Kumar, D.; Du, P.; Wiesner, U.; Gibson, J. M.; Experimental Facilities Division; Arizona State Univ.; Cornell Univ.

    2006-01-01

    Medium-range order (MRO) is crucial for understanding the nature of defects, mechanical behaviors, rheology in polymers, order-disorder processes and nucleation, etc. Measuring MRO is a challenging problem. Recently, we have developed fluctuation x-ray microscopy (FXM), which offers quantitative insight into MRO in materials at the micrometer scale. In this paper, we have applied our further-developed technique for characterization of MRO in nanomaterials. The study of mesostructured polymer-inorganic hybrid materials is an exciting, emerging research area offering enormous scientific and technological promise. The ability to control the shape, size and order of hybrid materials is a key requirement for their future development. By choice of the appropriate block copolymer system and inorganic precursors, the shape and size of the hybrid materials can be controlled at the nanometer scale. However, the control of formation and ordering of the nanostructures with medium to long range order remains a challenge that limits advances in many fields of nanotechnology. By using FXM here we examine the influence of sol-gel process variables on medium range order. The FXM method is described elsewhere. Two hybrids of PI-b-PEO/aluminosilicates with {approx}20nm phase separation length scale were prepared using known procedures. The PI-b-PEO amphiphilic block copolymer was synthesized via anionic polymerization techniques. Hybrids were fabricated by dissolving 0.05 g of PI-b-PEO in tetrahydrofuran (THF) (sample A) or a THF/chloroform mixture (28/72 v/v) (sample B) and adding 0.3 g of pre-hydrolyzed sol-gel inorganic precursors (3-glycidyloxypropyl-trimethoxysilane and aluminum-tri-secbutoxide). Samples were spin coated onto Si{sub 3}N{sub 4} windows on Si substrate. Both samples were UV/ozone treated for degrading the isoprene components in order to increase contrast for x-ray scattering experiments. The sample A was further cacinated at 350 C to remove all organic components

  13. Low energy X-ray spectra measured with a mercuric iodide energy dispersive spectrometer in a scanning electron microscope

    NASA Technical Reports Server (NTRS)

    Iwanczyk, J. S.; Dabrowski, A. J.; Huth, G. C.; Bradley, J. G.; Conley, J. M.

    1986-01-01

    A mercuric iodide energy dispersive X-ray spectrometer, with Peltier cooling provided for the detector and input field effect transistor, has been developed and tested in a scanning electron microscope. X-ray spectra were obtained with the 15 keV electron beam. An energy resolution of 225 eV (FWHM) for Mn-K(alpha) at 5.9 keV and 195 eV (FWHM) for the Mg-K line at 1.25 keV has been measured. Overall system noise level was 175 eV (FWHM). The detector system characterization with a carbon target demonstrated good energy sensitivity at low energies and lack of significant spectral artifacts at higher energies.

  14. Sub-second variations of high energy ( 300 keV) hard X-ray emission from solar flares

    NASA Technical Reports Server (NTRS)

    Bai, Taeil

    1986-01-01

    Subsecond variations of hard X-ray emission from solar flares were first observed with a balloon-borne detector. With the launch of the Solar Maximum Mission (SMM), it is now well known that subsecond variations of hard X-ray emission occur quite frequently. Such rapid variations give constraints on the modeling of electron energization. Such rapid variations reported until now, however, were observed at relatively low energies. Fast mode data obtained by the Hard X-ray Burst Spectrometer (HXRBS) has time resolution of approximately 1 ms but has no energy resolution. Therefore, rapid fluctuations observed in the fast-mode HXRBS data are dominated by the low energy hard X-rays. It is of interest to know whether rapid fluctuations are observed in high-energy X-rays. The highest energy band at which subsecond variations were observed is 223 to 1057 keV. Subsecond variations observed with HXRBS at energies greater than 300 keV are reported, and the implications discussed.

  15. Relationship between dual-energy X-ray absorptiometry volumetric assessment and X-ray computed tomography-derived single-slice measurement of visceral fat.

    PubMed

    Xia, Yi; Ergun, David L; Wacker, Wynn K; Wang, Xin; Davis, Cynthia E; Kaul, Sanjiv

    2014-01-01

    To reduce radiation exposure and cost, visceral adipose tissue (VAT) measurement on X-ray computed tomography (CT) has been limited to a single slice. Recently, the US Food and Drug Administration has approved a dual-energy X-ray absorptiometry (DXA) application validated against CT to measure VAT volume. The purpose of this study was to develop an algorithm to compute single-slice area values on DXA at 2 common landmarks, L2/3 and L4/5, from an automated volumetrically derived measurement of VAT. Volumetric CT and total body DXA were measured in 55 males (age: 21-77 yr; body mass index [BMI]: 21.1-37.9) and 60 females (age: 21-85 yr; BMI: 20.0-39.7). Equations were developed by applying the relationship of CT single-slice area and volume measurements of VAT to the DXA VAT volume measure as well as validating these against the CT single-slice measurements. Correlation coefficients between DXA estimate of single-slice area and CT were 0.94 for L2/3 and 0.96 for L4/5. The mean difference between DXA estimate of single-slice area and CT was 5 cm(2) at L2/3 and 3.8 cm(2) at L4/5. Bland-Altman analysis showed a fairly constant difference across the single-slice range in this study, and the 95% limits of agreement for the 2 methods were -44.6 to +54.6 cm(2) for L2/3 and -47.3 to +54.9 cm(2) for L4/5. In conclusion, a volumetric measurement of VAT by DXA can be used to estimate single-slice measurements at the L2/3 and the L4/5 landmarks.

  16. Studying X-Ray Binaries with High Energy Frequency Quasi-Periodic Oscillations

    NASA Technical Reports Server (NTRS)

    Oliversen, Ronald J. (Technical Monitor); Kaaret, P.

    2003-01-01

    The goal of this investigation is to further our understanding of the dynamics of accreting neutron stars and black holes in the hope of using these systems as probes of the physics of strong gravitational fields. The main focus of this work has been a multi-year program of simultaneous millisecond x-ray timing and spectral observations carried out with the Rossi X-Ray Timing Explorer (RXTE) to perform the x-ray timing and one of the satellites Asca, BeppoSAX, or Chandra to perform x-ray spectral measurements. With the advent of Chandra, we have extended our work to include imaging of X-ray jets from binaries and the study of extragalactic X-ray binaries. Significant progress was made over the past year.

  17. Differential Effects of X-Rays and High-Energy {sup 56}Fe Ions on Human Mesenchymal Stem Cells

    SciTech Connect

    Kurpinski, Kyle; Jang, Deok-Jin; Bhattacharya, Sanchita; Rydberg, Bjorn; Chu, Julia; So, Joanna; Wyrobek, Andy; Li Song; Wang Daojing

    2009-03-01

    Purpose: Stem cells hold great potential for regenerative medicine, but they have also been implicated in cancer and aging. How different kinds of ionizing radiation affect stem cell biology remains unexplored. This study was designed to compare the biological effects of X-rays and of high-linear energy transfer (LET) {sup 56}Fe ions on human mesenchymal stem cells (hMSC). Methods and Materials: A multi-functional comparison was carried out to investigate the differential effects of X-rays and {sup 56}Fe ions on hMSC. The end points included modulation of key markers such as p53, cell cycle progression, osteogenic differentiation, and pathway and networks through transcriptomic profiling and bioinformatics analysis. Results: X-rays and {sup 56}Fe ions differentially inhibited the cell cycle progression of hMSC in a p53-dependent manner without impairing their in vitro osteogenic differentiation process. Pathway and network analyses revealed that cytoskeleton and receptor signaling were uniquely enriched for low-dose (0.1 Gy) X-rays. In contrast, DNA/RNA metabolism and cell cycle regulation were enriched for high-dose (1 Gy) X-rays and {sup 56}Fe ions, with more significant effects from {sup 56}Fe ions. Specifically, DNA replication, DNA strand elongation, and DNA binding/transferase activity were perturbed more severely by 1 Gy {sup 56}Fe ions than by 1 Gy X-rays, consistent with the significant G2/M arrest for the former while not for the latter. Conclusions: {sup 56}Fe ions exert more significant effects on hMSC than X-rays. Since hMSC are the progenitors of osteoblasts in vivo, this study provides new mechanistic understandings of the relative health risks associated with low- and high-dose X-rays and high-LET space radiation.

  18. Pixellated Cd(Zn)Te high-energy X-ray instrument

    NASA Astrophysics Data System (ADS)

    Seller, P.; Bell, S.; Cernik, R. J.; Christodoulou, C.; Egan, C. K.; Gaskin, J. A.; Jacques, S.; Pani, S.; Ramsey, B. D.; Reid, C.; Sellin, P. J.; Scuffham, J. W.; Speller, R. D.; Wilson, M. D.; Veale, M. C.

    2011-12-01

    We have developed a pixellated high energy X-ray detector instrument to be used in a variety of imaging applications. The instrument consists of either a Cadmium Zinc Telluride or Cadmium Telluride (Cd(Zn)Te) detector bump-bonded to a large area ASIC and packaged with a high performance data acquisition system. The 80 by 80 pixels each of 250 μm by 250 μm give better than 1 keV FWHM energy resolution at 59.5 keV and 1.5 keV FWHM at 141 keV, at the same time providing a high speed imaging performance. This system uses a relatively simple wire-bonded interconnection scheme but this is being upgraded to allow multiple modules to be used with very small dead space. The readout system and the novel interconnect technology is described and how the system is performing in several target applications.

  19. Pixellated Cd(Zn)Te high-energy X-ray instrument

    PubMed Central

    Seller, P.; Bell, S.; Cernik, R.J.; Christodoulou, C.; Egan, C.K.; Gaskin, J.A.; Jacques, S.; Pani, S.; Ramsey, B.D.; Reid, C.; Sellin, P.J.; Scuffham, J.W.; Speller, R.D.; Wilson, M.D.; Veale, M.C.

    2012-01-01

    We have developed a pixellated high energy X-ray detector instrument to be used in a variety of imaging applications. The instrument consists of either a Cadmium Zinc Telluride or Cadmium Telluride (Cd(Zn)Te) detector bump-bonded to a large area ASIC and packaged with a high performance data acquisition system. The 80 by 80 pixels each of 250 μm by 250 μm give better than 1 keV FWHM energy resolution at 59.5 keV and 1.5 keV FWHM at 141 keV, at the same time providing a high speed imaging performance. This system uses a relatively simple wire-bonded interconnection scheme but this is being upgraded to allow multiple modules to be used with very small dead space. The readout system and the novel interconnect technology is described and how the system is performing in several target applications. PMID:22737179

  20. An ARXPS and ERXPS study of quaternary ammonium and phosphonium ionic liquids: utilising a high energy Ag Lα' X-ray source.

    PubMed

    Blundell, Rebecca K; Delorme, Astrid E; Smith, Emily F; Licence, Peter

    2016-02-17

    A series of ammonium- and phosphonium-based ionic liquids have been probed using X-ray photoelectron spectroscopy (XPS) with a high energy Ag Lα' X-ray source. The capability of the Ag Lα' X-ray source for ionic liquid analysis is confirmed alongside the characterisation of previously undetected high energy core photoelectron emissions. Additionally, the utilisation of the Ag Lα' X-ray source as a depth profiling technique (ERXPS) to investigate the structure of the ionic liquid/vacuum interface has been demonstrated, with comparison made to angle resolved X-ray photoelectron spectroscopy (ARXPS).

  1. [Influence of the Experiment Energy Dispersive X-Ray Fluorescence Measurement of Uranium by Different Excitation Source].

    PubMed

    Xiong, Chao; Ge, Liang-quan; Liu, Duan; Zhang, Qing-xian; Gu, Yi; Luo, Yao-yao; Zhao, Jian-kun

    2016-03-01

    Aiming at the self-excitation effect on the interference of measurements which exist in the process of Energy dispersive X-ray fluorescence method for uranium measurement. To solve the problem of radioactive isotopes only used as excitation source in determination of uranium. Utilizing the micro X-ray tube to test Self-excitation effect to get a comparison of the results obtained by three different uranium ore samples--109 Cd, 241 Am and Mirco X-ray tube. The results showed that self-excitation effect produced the area measure of characteristic X-ray peak is less than 1% of active condition, also the interference of measurements can be negligible. Photoelectric effect cross-section excited by 109 Cd is higher, corresponding fluorescence yield is higher than excited by 241 Am as well due to characteristics X-ray energy of 109 Cd, 22.11 & 24.95 KeV adjacent to absorption edge energy of L(α), 21.75 KeV, based on the above, excitation efficiency by 109 Cd is higher than 241 Am; The fact that measurement error excited by 241 Am is significantly greater than by 109 Cd is mainly due to peak region overlap between L energy peaks of uranium and Scattering peak of 241 Am, 26.35 keV, These factors above caused the background of measured Spectrum higher; The error between the uranium content in ore samples which the X-ray tube as the excitation source and the chemical analysis results is within 10%. Conclusion: This paper come to the conclusion that the technical quality of uranium measurement used X-ray tube as excitation source is superior to that in radioactive source excitation mode. PMID:27400534

  2. [Influence of the Experiment Energy Dispersive X-Ray Fluorescence Measurement of Uranium by Different Excitation Source].

    PubMed

    Xiong, Chao; Ge, Liang-quan; Liu, Duan; Zhang, Qing-xian; Gu, Yi; Luo, Yao-yao; Zhao, Jian-kun

    2016-03-01

    Aiming at the self-excitation effect on the interference of measurements which exist in the process of Energy dispersive X-ray fluorescence method for uranium measurement. To solve the problem of radioactive isotopes only used as excitation source in determination of uranium. Utilizing the micro X-ray tube to test Self-excitation effect to get a comparison of the results obtained by three different uranium ore samples--109 Cd, 241 Am and Mirco X-ray tube. The results showed that self-excitation effect produced the area measure of characteristic X-ray peak is less than 1% of active condition, also the interference of measurements can be negligible. Photoelectric effect cross-section excited by 109 Cd is higher, corresponding fluorescence yield is higher than excited by 241 Am as well due to characteristics X-ray energy of 109 Cd, 22.11 & 24.95 KeV adjacent to absorption edge energy of L(α), 21.75 KeV, based on the above, excitation efficiency by 109 Cd is higher than 241 Am; The fact that measurement error excited by 241 Am is significantly greater than by 109 Cd is mainly due to peak region overlap between L energy peaks of uranium and Scattering peak of 241 Am, 26.35 keV, These factors above caused the background of measured Spectrum higher; The error between the uranium content in ore samples which the X-ray tube as the excitation source and the chemical analysis results is within 10%. Conclusion: This paper come to the conclusion that the technical quality of uranium measurement used X-ray tube as excitation source is superior to that in radioactive source excitation mode.

  3. Enhanced neoplastic transformation by mammography X rays relative to 200 kVp X rays: indication for a strong dependence on photon energy of the RBE(M) for various end points.

    PubMed

    Frankenberg, D; Kelnhofer, K; Bär, K; Frankenberg-Schwager, M

    2002-01-01

    The fundamental assumption implicit in the use of the atomic bomb survivor data to derive risk estimates is that the gamma rays of Hiroshima and Nagasaki are considered to have biological efficiencies equal to those of other low-LET radiations up to 10 keV/microm, including mammography X rays. Microdosimetric and radiobiological data contradict this assumption. It is therefore of scientific and public interest to evaluate the efficiency of mammography X rays (25-30 kVp) to induce cancer. In this study, the efficiency of mammography X rays relative to 200 kVp X rays to induce neoplastic cell transformation was evaluated using cells of a human hybrid cell line (CGL1). For both radiations, a linear-quadratic dose-effect relationship was observed for neoplastic transformation of CGL1 cells; there was a strong linear component for the 29 kVp X rays. The RBE(M) of mammography X rays relative to 200 kVp X rays was determined to be about 4 for doses < or = 0.5 Gy. A comparison of the electron fluences for both X rays provides strong evidence that electrons with energies of < or = 15 keV can induce neoplastic transformation of CGL1 cells. Both the data available in the literature and the results of the present study strongly suggest an increase of RBE(M) for carcinogenesis in animals, neoplastic cell transformation, and clastogenic effects with decreasing photon energy or increasing LET to an RBE(M) approximately 8 for mammography X rays relative to 60Co gamma rays. PMID:11754647

  4. The Prospects for Constraining Dark Energy withFuture X-ray Cluster Gas Mass Fraction Measurements

    SciTech Connect

    Rapetti, David; Allen, Steven W.

    2007-10-15

    We examine the ability of a future X-ray observatory, with capabilities similar to those planned for the Constellation-X mission, to constrain dark energy via measurements of the cluster X-ray gas mass fraction, fgas. We find that fgas measurements for a sample of {approx}500 hot (kT{approx}> 5keV), X-ray bright, dynamically relaxed clusters, to a precision of {approx}5 percent, can be used to constrain dark energy with a Dark Energy Task Force (DETF; Albrecht et al. 2006) figure of merit of 20-50. Such constraints are comparable to those predicted by the DETF for other leading, planned 'Stage IV' dark energy experiments. A future fgas experiment will be preceded by a large X-ray or SZ survey that will find hot, X-ray luminous clusters out to high redshifts. Short 'snapshot' observations with the new X-ray observatory should then be able to identify a sample of {approx}500 suitably relaxed systems. The redshift, temperature and X-ray luminosity range of interest has already been partially probed by existing X-ray cluster surveys which allow reasonable estimates of the fraction of clusters that will be suitably relaxed for fgas work to be made; these surveys also show that X-ray flux contamination from point sources is likely to be small for the majority of the targets of interest. Our analysis uses a Markov Chain Monte Carlo method which fully captures the relevant degeneracies between parameters and facilities the incorporation of priors and systematic uncertainties in the analysis. We explore the effects of such uncertainties, for scenarios ranging from optimistic to pessimistic. We conclude that the fgas experiment offers a competitive and complementary approach to the best other large, planned dark energy experiments. In particular, the fgas experiment will provide tight constraints on the mean matter and dark energy densities, with a peak sensitivity for dark energy work at redshifts midway between those of supernovae and baryon acoustic oscillation

  5. Mesoscale Science with High Energy X-ray Diffraction Microscopy at the Advanced Photon Source

    NASA Astrophysics Data System (ADS)

    Suter, Robert

    2014-03-01

    Spatially resolved diffraction of monochromatic high energy (> 50 keV) x-rays is used to map microstructural quantities inside of bulk polycrystalline materials. The non-destructive nature of High Energy Diffraction Microscopy (HEDM) measurements allows tracking of responses as samples undergo thermo-mechanical or other treatments. Volumes of the order of a cubic millimeter are probed with micron scale spatial resolution. Data sets allow direct comparisons to computational models of responses that frequently involve long-ranged, multi-grain interactions; such direct comparisons have only become possible with the development of HEDM and other high energy x-ray methods. Near-field measurements map the crystallographic orientation field within and between grains using a computational reconstruction method that simulates the experimental geometry and matches orientations in micron sized volume elements to experimental data containing projected grain images in large numbers of Bragg peaks. Far-field measurements yield elastic strain tensors through indexing schemes that sort observed diffraction peaks into sets associated with individual crystals and detect small radial motions in large numbers of such peaks. Combined measurements, facilitated by a new end station hutch at Advanced Photon Source beamline 1-ID, are mutually beneficial and result in accelerated data reduction. Further, absorption tomography yields density contrast that locates secondary phases, void clusters, and cracks, and tracks sample shape during deformation. A collaboration led by the Air Force Research Laboratory and including the Advanced Photon Source, Lawrence Livermore National Laboratory, Carnegie Mellon University, Petra-III, and Cornell University and CHESS is developing software and hardware for combined measurements. Examples of these capabilities include tracking of grain boundary migrations during thermal annealing, tensile deformation of zirconium, and combined measurements of nickel

  6. Statistical reconstruction for x-ray computed tomography using energy-integrating detectors

    NASA Astrophysics Data System (ADS)

    Lasio, Giovanni M.; Whiting, Bruce R.; Williamson, Jeffrey F.

    2007-04-01

    Statistical image reconstruction (SR) algorithms have the potential to significantly reduce x-ray CT image artefacts because they use a more accurate model than conventional filtered backprojection and can incorporate effects such as noise, incomplete data and nonlinear detector response. Most SR algorithms assume that the CT detectors are photon-counting devices and generate Poisson-distributed signals. However, actual CT detectors integrate energy from the x-ray beam and exhibit compound Poisson-distributed signal statistics. This study presents the first assessment of the impact on image quality of the resultant mismatch between the detector and signal statistics models assumed by the sinogram data model and the reconstruction algorithm. A 2D CT projection simulator was created to generate synthetic polyenergetic transmission data assuming (i) photon-counting with simple Poisson-distributed signals and (ii) energy-weighted detection with compound Poisson-distributed signals. An alternating minimization (AM) algorithm was used to reconstruct images from the data models (i) and (ii) for a typical abdominal scan protocol with incident particle fluence levels ranging from 105 to 1.6 × 106 photons/detector. The images reconstructed from data models (i) and (ii) were compared by visual inspection and image-quality figures of merit. The reconstructed image quality degraded significantly when the means were mismatched from the assumed model. However, if the signal means are appropriately modified, images from data models (i) and (ii) did not differ significantly even when SNR is very low. While data-mean mismatches characteristic of the difference between particle-fluence and energy-fluence transmission can cause significant streaking and cupping artefacts, the mismatch between the actual and assumed CT detector signal statistics did not significantly degrade image quality once systematic data means mismatches were corrected.

  7. Soil characterization by energy dispersive X-ray fluorescence: sampling strategy for in situ analysis.

    PubMed

    Custo, Graciela; Boeykens, Susana; Dawidowski, L; Fox, L; Gómez, D; Luna, F; Vázquez, Cristina

    2005-07-01

    This work describes a sampling strategy that will allow the use of portable EDXRF (energy dispersive X-ray fluorescence) instruments for "in situ" soil analysis. The methodology covers a general approach to planning field investigations for any type of environmental studies and it was applied for a soil characterization study in the zone of Campana, Argentina, by evaluating data coming from an EDXRF spectrometer with a radioisotope excitation source. Simulating non-treated sampled as "in situ" samples and a soil characterization for Campana area was intended. "In situ" EDXRF methodology is a powerful analytical modality with the advantage of providing data immediately, allowing a fast general screening of the soil composition. PMID:16038489

  8. Compositional analysis of Ceramic Glaze by Laser Induced Breakdown Spectroscopy and Energy Dispersive X-Ray

    NASA Astrophysics Data System (ADS)

    Khedr, A.; Abdel-kareem, O.; Elnabi, S. H.; Harith, M. A.

    2011-09-01

    Laser induced breakdown spectroscopy (LIBS) has been applied for the analysis of Egyptian Islamic glaze ceramic sample. The sample dating back to Fatimid period (969-1169AD), and collected from Al-Fustat excavation store in Cairo. The analysis of contaminated pottery sample has been performed to draw mapping for the elemental compositions by LIBS technique. LIBS measurements have been done by the fundamental wavelength (1064 nm) of Nd: YAG laser for the elemental analysis and performing the cleaning processes of the pottery sample. In addition, complementary analyses were carried out by scanning electron microscopy linked with energy dispersive X-ray microanalysis (SEM/EDX) to obtain verification of chemical results. The morphological surfaces before and after cleaning has been done by Optical Microscopy (OM).

  9. Evaluation on determination of iodine in coal by energy dispersive X-ray fluorescence

    USGS Publications Warehouse

    Wang, B.; Jackson, J.C.; Palmer, C.; Zheng, B.; Finkelman, R.B.

    2005-01-01

    A quick and inexpensive method of relative high iodine determination from coal samples was evaluated. Energy dispersive X-ray fluorescence (EDXRF) provided a detection limit of about 14 ppm (3 times of standard deviations of the blank sample), without any complex sample preparation. An analytical relative standard deviation of 16% was readily attainable for coal samples. Under optimum conditions, coal samples with iodine concentrations higher than 5 ppm can be determined using this EDXRF method. For the time being, due to the general iodine concentrations of coal samples lower than 5 ppm, except for some high iodine content coal, this method can not effectively been used for iodine determination. More work needed to meet the requirement of determination of iodine from coal samples for this method. Copyright ?? 2005 by The Geochemical Society of Japan.

  10. High transmission Ni compound refractive lens for high energy X-rays.

    PubMed

    Brancewicz, M; Itou, M; Sakurai, Y; Andrejczuk, A; Chiba, S; Kayahara, Y; Inoue, T; Nagamine, M

    2016-08-01

    We present a new planar Ni compound refractive lens for high energy X-rays (116 keV). The lens is composed of identical plano-concave elements with longitudinal parabolic grooves manufactured by a punch technique. In order to increase the lens transmission, the thickness of the single lens at the parabolic groove vertex was reduced to less than 5 μm and the radius of curvature was reduced to about 20 μm. The small radius of curvature allowed us to reduce the number of single elements needed to get the focal length of 3 m to 54 single lenses. The gain parameter has been significantly improved compared to the previous lenses due to higher transmission, but the focused beam size and its gain are not as good as expected, mostly due to the aberrations caused by the lens shape imperfections. PMID:27587159

  11. Note: Characterization of a high-photon-energy X-ray imager

    SciTech Connect

    Storm, M.; Schiebel, P.; Freeman, R. R.; Akli, K. U.; Eichman, B.; Theobald, W.; Mileham, C.; Stoeckl, C.; Begishev, I. A.; Fiksel, G.; Zhong, Z.; Stephens, R. B.

    2013-10-15

    The Bragg angle, rocking curve, and reflection efficiency of a quartz crystal x-ray imager (Miller indices 234) were measured at photon energy of 15.6909 keV, corresponding to the K{sub α2} line of Zr, using the X15A beamline at the National Synchrotron Light Source at Brookhaven National Laboratory. One flat and three spherically curved samples were tested. The peak reflectivity of the best-performing crystal was determined to be (3.6 ± 0.7) × 10{sup −4} with a rocking-curve full width at half maximum of 0.09°. The Zr K{sub α2} emission was imaged from a hot Zr plasma generated by a 10-J multiterawatt laser.

  12. Performance of bent-crystal x-ray microscopes for high energy density physics research.

    PubMed

    Schollmeier, Marius S; Geissel, Matthias; Shores, Jonathon E; Smith, Ian C; Porter, John L

    2015-06-01

    We present calculations for the field of view (FOV), image fluence, image monochromaticity, spectral acceptance, and image aberrations for spherical crystal microscopes, which are used as self-emission imaging or backlighter systems at large-scale high energy density physics facilities. Our analytic results are benchmarked with ray-tracing calculations as well as with experimental measurements from the 6.151 keV backlighter system at Sandia National Laboratories. The analytic expressions can be used for x-ray source positions anywhere between the Rowland circle and object plane. This enables quick optimization of the performance of proposed but untested, bent-crystal microscope systems to find the best compromise between FOV, image fluence, and spatial resolution for a particular application.

  13. High transmission Ni compound refractive lens for high energy X-rays

    NASA Astrophysics Data System (ADS)

    Brancewicz, M.; Itou, M.; Sakurai, Y.; Andrejczuk, A.; Chiba, S.; Kayahara, Y.; Inoue, T.; Nagamine, M.

    2016-08-01

    We present a new planar Ni compound refractive lens for high energy X-rays (116 keV). The lens is composed of identical plano-concave elements with longitudinal parabolic grooves manufactured by a punch technique. In order to increase the lens transmission, the thickness of the single lens at the parabolic groove vertex was reduced to less than 5 μm and the radius of curvature was reduced to about 20 μm. The small radius of curvature allowed us to reduce the number of single elements needed to get the focal length of 3 m to 54 single lenses. The gain parameter has been significantly improved compared to the previous lenses due to higher transmission, but the focused beam size and its gain are not as good as expected, mostly due to the aberrations caused by the lens shape imperfections.

  14. Performance of bent-crystal x-ray microscopes for high energy density physics research

    NASA Astrophysics Data System (ADS)

    Schollmeier, M.; Geissel, M.; Shores, J. E.; Smith, I. C.; Porter, J. L.

    2015-11-01

    We present calculations for the field of view (FOV), image fluence, image monochromaticity, spectral acceptance, and image aberrations for spherical crystal microscopes, which are used as self-emission imaging or backlighter systems at large-scale high energy density physics facilities. Our analytic results are benchmarked with ray-tracing calculations as well as with experimental measurements from the 6.151 keV backlighter system at Sandia National Laboratories. The analytic expressions can be used for x-ray source positions anywhere between the Rowland circle and object plane. This enables quick optimization of the performance of proposed but untested, bent-crystal microscope systems to find the best compromise between FOV, image fluence, and spatial resolution for a particular application.

  15. Investigation of gas generation in regenerative fuel cells by low-energy X-rays

    NASA Astrophysics Data System (ADS)

    Selamet, Omer Faruk; Deevanhxay, Phengxay; Tsushima, Shohji; Hirai, Shuichiro

    2015-11-01

    Gas generation and discharge behaviors in an operating regenerative fuel cell (RFC) are investigated using low-energy X-ray radiography. In situ visualization at high spatial and temporal resolution reveal dynamic and inhomogeneous behaviors of the gas generation in the membrane electrode assembly (MEA) in the RFC. Temporal and spatial variation of the gas thickness in the MEA is quantitatively discussed and shows an intermittent and periodic discharge processes of the gas generated by electrolysis, suggesting that the reaction sites in the catalyst layer and the discharging path of gas bubbles are well established in the MEA for the electrolysis. Larger gas accumulation and discharge in the gas diffusion layer (GDL) under the ribs are identified in comparison with those under the channels, which is attributed to the relatively longer path for accumulated gas under the ribs to be discharged into the flow channels.

  16. Sodium Chloride Diffusion during Muscle Salting Evidenced by Energy-Dispersive X-ray Spectroscopy Imaging.

    PubMed

    Filgueras, Rénata; Peyrin, Frédéric; Vénien, Annie; Hénot, Jean Marc; Astruc, Thierry

    2016-01-27

    To better understand the relationship between the muscle structure and NaCl transfers in meat, we used energy-dispersive X-ray spectroscopy (EDS) coupled with scanning electron microscopy (SEM) to analyze brined and dry-salted rat muscles. The muscles were freeze-dried to avoid the delocalization of soluble ions that happens in regular dehydration through a graded series of ethanol. Na and Cl maps were superimposed on SEM images to combine the muscle structure and NaCl diffusion. Brining causes rapid diffusion of NaCl through the tissue. Most brine diffuses in a linear front from the muscle surface, but a small proportion enters through the perimysium network. The muscle area penetrated by brine shows heterogeneous patterns of NaCl retention, with some connective tissue islets containing more NaCl than other parts of perimysium. NaCl penetration is considerably slower after dry salting than after brining.

  17. Performance of bent-crystal x-ray microscopes for high energy density physics research

    SciTech Connect

    Schollmeier, Marius S.; Geissel, Matthias; Shores, Jonathon E.; Smith, Ian C.; Porter, John L.

    2015-05-29

    We present calculations for the field of view (FOV), image fluence, image monochromaticity, spectral acceptance, and image aberrations for spherical crystal microscopes, which are used as self-emission imaging or backlighter systems at large-scale high energy density physics facilities. Our analytic results are benchmarked with ray-tracing calculations as well as with experimental measurements from the 6.151 keV backlighter system at Sandia National Laboratories. Furthermore, the analytic expressions can be used for x-ray source positions anywhere between the Rowland circle and object plane. We discovered that this enables quick optimization of the performance of proposed but untested, bent-crystal microscope systems to find the best compromise between FOV, image fluence, and spatial resolution for a particular application.

  18. Performance of bent-crystal x-ray microscopes for high energy density physics research

    DOE PAGESBeta

    Schollmeier, Marius S.; Geissel, Matthias; Shores, Jonathon E.; Smith, Ian C.; Porter, John L.

    2015-05-29

    We present calculations for the field of view (FOV), image fluence, image monochromaticity, spectral acceptance, and image aberrations for spherical crystal microscopes, which are used as self-emission imaging or backlighter systems at large-scale high energy density physics facilities. Our analytic results are benchmarked with ray-tracing calculations as well as with experimental measurements from the 6.151 keV backlighter system at Sandia National Laboratories. Furthermore, the analytic expressions can be used for x-ray source positions anywhere between the Rowland circle and object plane. We discovered that this enables quick optimization of the performance of proposed but untested, bent-crystal microscope systems to findmore » the best compromise between FOV, image fluence, and spatial resolution for a particular application.« less

  19. SINISTER CAUSE OF HIGH BONE MINERAL DENSITY ON DUAL ENERGY X-RAY ABSORPTIOMETRY.

    PubMed

    Razi, Mairah; Hassan, Aamna

    2016-01-01

    Dual energy X-ray absorptiometry (DXA) has an established, well standardized role in the measurement of bone mineral density (BMD). In routine clinical practice, the main focus of bone densitometry is to identify low bone mass for the diagnosis and monitoring of osteoporosis particularly in postmenopausal females and in high risk individuals. Less commonly, elevated BMD can also be seen on routine DXA scanning usually due to degenerative disease. However, a range of other skeletal disorders can also lead to high BMD. Careful recognition of various artefacts and pathologic processes that can falsely elevate the BMD is essential for accurate DXA scan analysis and reporting. We present a case of high BMD in a patient of prostate carcinoma with widespread sclerotic metastases. PMID:27323594

  20. Energy-Sensitive Single-Photon X-ray and Particle Imaging

    NASA Astrophysics Data System (ADS)

    Lotto, Christian

    Energy-sensitive detectors perform asynchronous arrival detection of single X-Ray photons and particles. Their ability of measuring the detected particles' energy improves the performance of the particle counting applications and enables spectroscopic applications. In such detectors, either a semiconductor layer for direct conversion or a combination of a scintillator and a semiconductor sensing device for visible photons is used for generation of an electrical charge pulse per absorbed particle. This charge amount, which represents the particle energy, is detected by an asynchronous charge pulse detecting circuit. The noise of such circuits defines the lowest discrimination threshold of counting systems and the energy resolution of spectroscopic applications. Therefore, low noise, low power consumption, and low area are requirements for charge pulse detecting circuits used in segmented energy sensitive particle detectors with a high number of pixels. Choice of a sensing device, definition of the charge pulse detecting circuit's topology, and analysis of interdependences amongst the above performance parameters are covered and a context with employed readout schemes, processing circuits, and target applications is established in this chapter. Energy-sensitive detectors perform asynchronous arrival detection of single X-Ray photons and particles. Their ability of measuring the detected particles' energy improves the performance of the particle counting applications and enables spectroscopic applications. In such detectors, either a semiconductor layer for direct conversion or a combination of a scintillator and a semiconductor sensing device for visible photons is used for generation of an electrical charge pulse per absorbed particle. This charge amount, which represents the particle energy, is detected by an asynchronous charge pulse detecting circuit. The noise of such circuits defines the lowest discrimination threshold of counting systems and the energy

  1. Measurement of the high energy component of the x-ray spectra in the VENUS electron cyclotron resonance ion source.

    PubMed

    Leitner, D; Benitez, J Y; Lyneis, C M; Todd, D S; Ropponen, T; Ropponen, J; Koivisto, H; Gammino, S

    2008-03-01

    High performance electron cyclotron resonance (ECR) ion sources, such as VENUS (Versatile ECR for NUclear Science), produce large amounts of x-rays. By studying their energy spectra, conclusions can be drawn about the electron heating process and the electron confinement. In addition, the bremsstrahlung from the plasma chamber is partly absorbed by the cold mass of the superconducting magnet, adding an extra heat load to the cryostat. Germanium or NaI detectors are generally used for x-ray measurements. Due to the high x-ray flux from the source, the experimental setup to measure bremsstrahlung spectra from ECR ion sources is somewhat different from that for the traditional nuclear physics measurements these detectors are generally used for. In particular, the collimation and background shielding can be problematic. In this paper, we will discuss the experimental setup for such a measurement, the energy calibration and background reduction, the shielding of the detector, and collimation of the x-ray flux. We will present x-ray energy spectra and cryostat heating rates depending on various ion source parameters, such as confinement fields, minimum B-field, rf power, and heating frequency. PMID:18377002

  2. Laboratory-based x-ray reflectometer for multilayer characterization in the 15–150 keV energy band

    SciTech Connect

    Windt, David L.

    2015-04-15

    A laboratory-based X-ray reflectometer has been developed to measure the performance of hard X-ray multilayer coatings at their operational X-ray energies and incidence angles. The instrument uses a sealed-tube X-ray source with a tungsten anode that can operate up to 160 kV to provide usable radiation in the 15–150 keV energy band. Two sets of adjustable tungsten carbide slit assemblies, spaced 4.1 m apart, are used to produce a low-divergence white beam, typically set to 40 μm × 800 μm in size at the sample. Multilayer coatings under test are held flat using a vacuum chuck and are mounted at the center of a high-resolution goniometer used for precise angular positioning of the sample and detector; additionally, motorized linear stages provide both vertical and horizontal adjustments of the sample position relative to the incident beam. A CdTe energy-sensitive detector, located behind a third adjustable slit, is used in conjunction with pulse-shaping electronics and a multi-channel analyzer to capture both the incident and reflected spectra; the absolute reflectance of the coating under test is computed as the ratio of the two spectra. The instrument’s design, construction, and operation are described in detail, and example results are presented obtained with both periodic, narrow-band and depth-graded, wide-band hard X-ray multilayer coatings.

  3. Laboratory-based X-ray reflectometer for multilayer characterization in the 15-150 keV energy band.

    PubMed

    Windt, David L

    2015-04-01

    A laboratory-based X-ray reflectometer has been developed to measure the performance of hard X-ray multilayer coatings at their operational X-ray energies and incidence angles. The instrument uses a sealed-tube X-ray source with a tungsten anode that can operate up to 160 kV to provide usable radiation in the 15-150 keV energy band. Two sets of adjustable tungsten carbide slit assemblies, spaced 4.1 m apart, are used to produce a low-divergence white beam, typically set to 40 μm × 800 μm in size at the sample. Multilayer coatings under test are held flat using a vacuum chuck and are mounted at the center of a high-resolution goniometer used for precise angular positioning of the sample and detector; additionally, motorized linear stages provide both vertical and horizontal adjustments of the sample position relative to the incident beam. A CdTe energy-sensitive detector, located behind a third adjustable slit, is used in conjunction with pulse-shaping electronics and a multi-channel analyzer to capture both the incident and reflected spectra; the absolute reflectance of the coating under test is computed as the ratio of the two spectra. The instrument's design, construction, and operation are described in detail, and example results are presented obtained with both periodic, narrow-band and depth-graded, wide-band hard X-ray multilayer coatings.

  4. MEASUREMENT OF THE HIGH ENERGY COMPONENT OF THE X-RAY SPECTRA INTHE VENUS ECR ION SOURCE

    SciTech Connect

    Leitner, Daniela; Benitez, Janilee Y.; Lyneis, Claude M.; Todd,Damon S.; Ropponen,Tommi; Ropponen,Janne; Koivisto, Hannu; Gammino, Santo

    2007-11-15

    High performance electron cyclotron resonance (ECR) ion sources, such as VENUS (Versatile ECR for Nuclear Science), produce large amounts of x-rays. By studying their energy spectra, conclusions can be drawn about the electron heating process and the electron confinement. In addition, the bremsstrahlung from the plasma chamber is partly absorbed by the cold mass of the superconducting magnet adding an extra heat load to the cryostat. Germanium or NaI detectors are generally used for x-ray measurements. Due to the high x-ray flux from the source, the experimental set-up to measure bremsstrahlung spectra from ECR ion sources is somewhat different than for the traditional nuclear physics measurements these detectors are generally used for. In particular the collimation and background shielding can be problematic. In this paper we will discuss the experimental set-up for such a measurement, the energy calibration and background reduction, the correction for detector efficiency, the shielding of the detector and collimation of the x-ray flux. We will present x-ray energy spectra and cryostat heating rates in dependence of various ion source parameters such as confinement fields, minimum B-field, rf power and heating frequency.

  5. Measurement of the high energy component of the x-ray spectra in the VENUS electron cyclotron resonance ion source

    SciTech Connect

    Leitner, D.; Benitez, J. Y.; Lyneis, C. M.; Todd, D. S.; Ropponen, T.; Ropponen, J.; Koivisto, H.; Gammino, S.

    2008-03-15

    High performance electron cyclotron resonance (ECR) ion sources, such as VENUS (Versatile ECR for NUclear Science), produce large amounts of x-rays. By studying their energy spectra, conclusions can be drawn about the electron heating process and the electron confinement. In addition, the bremsstrahlung from the plasma chamber is partly absorbed by the cold mass of the superconducting magnet, adding an extra heat load to the cryostat. Germanium or NaI detectors are generally used for x-ray measurements. Due to the high x-ray flux from the source, the experimental setup to measure bremsstrahlung spectra from ECR ion sources is somewhat different from that for the traditional nuclear physics measurements these detectors are generally used for. In particular, the collimation and background shielding can be problematic. In this paper, we will discuss the experimental setup for such a measurement, the energy calibration and background reduction, the shielding of the detector, and collimation of the x-ray flux. We will present x-ray energy spectra and cryostat heating rates depending on various ion source parameters, such as confinement fields, minimum B-field, rf power, and heating frequency.

  6. Laboratory-based x-ray reflectometer for multilayer characterization in the 15-150 keV energy band

    NASA Astrophysics Data System (ADS)

    Windt, David L.

    2015-04-01

    A laboratory-based X-ray reflectometer has been developed to measure the performance of hard X-ray multilayer coatings at their operational X-ray energies and incidence angles. The instrument uses a sealed-tube X-ray source with a tungsten anode that can operate up to 160 kV to provide usable radiation in the 15-150 keV energy band. Two sets of adjustable tungsten carbide slit assemblies, spaced 4.1 m apart, are used to produce a low-divergence white beam, typically set to 40 μm × 800 μm in size at the sample. Multilayer coatings under test are held flat using a vacuum chuck and are mounted at the center of a high-resolution goniometer used for precise angular positioning of the sample and detector; additionally, motorized linear stages provide both vertical and horizontal adjustments of the sample position relative to the incident beam. A CdTe energy-sensitive detector, located behind a third adjustable slit, is used in conjunction with pulse-shaping electronics and a multi-channel analyzer to capture both the incident and reflected spectra; the absolute reflectance of the coating under test is computed as the ratio of the two spectra. The instrument's design, construction, and operation are described in detail, and example results are presented obtained with both periodic, narrow-band and depth-graded, wide-band hard X-ray multilayer coatings.

  7. Comparing performances of a CdTe X-ray spectroscopic detector and an X-ray dual-energy sandwich detector

    NASA Astrophysics Data System (ADS)

    Gorecki, A.; Brambilla, A.; Moulin, V.; Gaborieau, E.; Radisson, P.; Verger, L.

    2013-11-01

    Multi-energy (ME) detectors are becoming a serious alternative to classical dual-energy sandwich (DE-S) detectors for X-ray applications such as medical imaging or explosive detection. They can use the full X-ray spectrum of irradiated materials, rather than disposing only of low and high energy measurements, which may be mixed. In this article, we intend to compare both simulated and real industrial detection systems, operating at a high count rate, independently of the dimensions of the measurements and independently of any signal processing methods. Simulations or prototypes of similar detectors have already been compared (see [1] for instance), but never independently of estimation methods and never with real detectors. We have simulated both an ME detector made of CdTe - based on the characteristics of the MultiX ME100 and - a DE-S detector - based on the characteristics of the Detection Technology's X-Card 1.5-64DE model. These detectors were compared to a perfect spectroscopic detector and an optimal DE-S detector. For comparison purposes, two approaches were investigated. The first approach addresses how to distinguise signals, while the second relates to identifying materials. Performance criteria were defined and comparisons were made over a range of material thicknesses and with different photon statistics. Experimental measurements in a specific configuration were acquired to checks simulations. Results showed good agreement between the ME simulation and the ME100 detector. Both criteria seem to be equivalent, and the ME detector performs 3.5 times better than the DE-S detector with same photon statistics based on simulations and experimental measurements. Regardless of the photon statistics ME detectors appeared more efficient than DE-S detectors for all material thicknesses between 1 and 9 cm when measuring plastics with an attenuation signature close that of explosive materials. This translates into an improved false detection rate (FDR): DE

  8. High-energy X-ray diffraction of melts and amorphous solids at extreme conditions

    NASA Astrophysics Data System (ADS)

    Prescher, C.; Yu, T.; Wang, Y.; Eng, P. J.; Skinner, L. B.; Stubbs, J.; Prakapenka, V.

    2015-12-01

    The structural analysis of amorphous materials, glasses and liquids at extreme conditions using X-ray diffraction is a very challenging endeavor. The samples are typically very small and surrounded by pressure vessels, which result in a huge background signal which may be orders of magnitude stronger than the actual sample signal. Furthermore, the background signal changes during compression in diamond anvil cells (DAC), making analysis of the diffraction data impossible at large pressures (>60 GPa). A key factor for obtaining high quality structural data is the maximum obtainable Q of the data collection. While at ambient conditions a maximum Q of more than 20 Å-1 has become standard, at high pressures data have been reported and analyzed with a maximum Q as low as 7 Å-1, which significantly reduces the resolution of the obtained real space data for multicomponent systems. In order to overcome those challenges, we have successfully installed a multichannel collimator (MCC) for the DAC setup at APS/GSECARS 13-IDD and for the Paris Edinburgh Press (PEP) at 13-IDC. The MCC leads to a significant increase in signal to background ratio and the background remains almost constant during compression in a DAC and removes the additional diffraction signal from the pressure media in the PEP. The combination of MCC and the high-energy X-ray optics of the 13ID beamline enables data collection of melts, glasses and amorphous materials up to 10 GPa in the PEP with a maximum Q of about 16 Å-1 and the collection of amorphous materials and glasses up to pressures above 150 GPa with a maximum Q of about 13 Å-1, thus, enabling the structural investigation of amorphous materials at much larger pressures than previously achievable. Further, we have developed several new user-friendly software packages for the analysis of X-ray diffraction data with specific data reduction and optimization algorithms for the analysis of amorphous materials at high-pressure. In order to show the

  9. Capabilities of dual-energy x-ray imaging in medicine and security

    NASA Astrophysics Data System (ADS)

    Ryzhikov, Volodymyr D.; Grinyov, Borys V.; Opolonin, Oleksandr D.; Galkin, Serhiy M.; Lysetska, Olena K.; Voronkin, Yevheniy F.; Kostioukevitch, Serhiy A.

    2012-10-01

    The dual-energy computer tomography compared with its traditional single-energy variant ensures substantially higher contrast sensitivity. The evaluation of the signal ratio from high-energy and low-energy detectors has been carried out using a simplified model of the dual-energy detector array and accounting for the X-ray tube spectrum. We proposed to use of a dual-energy receiving-detecting circuit with a detector pair ZnSe/CsI or ZnSe/CdWO that allows efficient distinction between muscular and bone tissues, which supports our earlier theoretical assumptions that this method could be successfully used for separate detection of materials differing in their effective atomic number Zeff and local density (e.g., calcium contents in bone densitometry), so as can be turn to account for new generation instruments. A possibility of dual energy tomography use for osteoporosis diagnostics was considered. Direct image reconstruction of biological objects has been carried out, demonstrating details of bones with different density. The density of the bone depends on the calcium content, which is not more than 20 % for the narrow part and about 18,5 % in the broad part. This results obtained were in good agreement with the results of the independent chemical analysis.

  10. Structural analysis of polymer thin films using GISAXS in the tender X-ray region: Concept and design of GISAXS experiments using the tender X-ray energy at BL-15A2 at the Photon Factory

    NASA Astrophysics Data System (ADS)

    Takagi, H.; Igarashi, N.; Mori, T.; Saijo, S.; Nagatani, Y.; Ohta, H.; Yamamoto, K.; Shimizu, N.

    2016-10-01

    If small angle X-ray scattering (SAXS) utilizing the soft X-ray region is available, advanced and unique experiments, which differ from traditional SAXS methods, can be realized. For example, grazing-incidence small angle X-ray scattering (GISAXS) using hard X-ray is a powerful tool for understanding the nanostructure in both vertical and lateral directions of thin films, while GISAXS utilizing the tender X-ray region (SX-GISAXS) enables depth-resolved analysis as well as a standard GISAXS analysis in thin films. Thus, at BL-15A2 at the Photon Factory, a dedicated diffractometer for SX-GISAXS (above 2.1 keV) was constructed. This diffractometer is composed of four vacuum chambers and can be converted into the vacuum state from the sample chamber in front of the detector surface. Diffractions are clearly observed until 12th peak when measuring collagen by SAXS with an X-ray energy of 2.40 keV and a camera length of 825 mm. Additionally, we conducted the model experiment using SX-GISAXS with an X-ray energy of 2.40 keV to confirm that a poly(methyl methacrylate)-poly(n-butyl acrylate) block copolymer thin film has a microphase-separated structure in the thin film, which is composed of lamellae aligned both parallel and perpendicular to the substrate surface. Similarly, in a polystyrene-poly(methyl methacrylate) block copolymer thin film, SX-GISAXS with 3.60 keV and 5.73 keV revealed that hexagonally packed cylinders are aligned parallel to the substrate surface. The incident angle dependence of the first order peak position of the qz direction obtained from experiments at various incident X-ray energies agrees very well with the theoretical one calculated from the distorted wave Born approximation.

  11. Metrology for the Development of High Energy X-Ray Optics

    NASA Technical Reports Server (NTRS)

    Gubarev, Mikhail; Ramsey, Brian; Engelhaupt, Darell; Dpeegle, Chet

    2005-01-01

    We are developing grazing incidence x-ray optics for a balloon-borne hard-x-ray telescope (HERO). The instrument will have 200 sq cm effective collecting area at 40 keV and an angular resolution goal of 15 arcsec. The HERO mirror shells are fabricated using electroform-nickel replication off super-polished cylindrical mandrels. The angular resolution goal puts stringent requirements on the quality of x-ray mirrors and, hence, on mandrel quality. We used metrology in an iterative approach to monitor and refine the x- ray mirror fabrication process. Comparison of surface figure and microroughness measurements of the mandrel and the shells will be presented together with results from x-ray tests.

  12. Constraints on energy release in solar flares from RHESSI and GOES X-ray observations. II. Energetics and energy partition

    NASA Astrophysics Data System (ADS)

    Warmuth, A.; Mann, G.

    2016-04-01

    Aims: We derive constraints on energy release, transport and conversion processes in solar flares based on a detailed characterization of the physical parameters of both the thermal plasma and the accelerated nonthermal electrons based on X-ray observations. In particular, we address the questions of whether the energy required to heat the thermal plasma can be supplied by nonthermal particles, and how the energetics derived from X-rays compare to the total bolometric radiated energy. Methods: Time series of spectral fits and images for 24 flares ranging from GOES class C3.4 to X17.2 were obtained using RHESSI hard X-ray observations. This has been supplemented by GOES soft X-ray fluxes. In our companion Paper I, we have used this data set to obtain the basic physical parameters for the thermal plasma (using the isothermal approximation) and the injected energetic electrons (assuming the thick-target model). Here, we used this data set to derive the flare energetics, including thermal energy, radiative and conductive energy loss, gravitational and flow energy of the plasma, and kinetic energy of the injected electrons. We studied how the thermal energies compare to the energy in nonthermal electrons, and how the various energetics and energy partition depend on flare importance. Results: All flare energetics show a good to excellent correlation with the peak GOES flux. The gravitational energy of the evaporated plasma and the kinetic energy of plasma flows can be neglected in the discussion of flare energetics. The radiative energy losses are comparable to the maximum thermal energy, while the conductive losses are considerably higher than the maximum thermal energy, especially in weaker flares. The total heating requirement of the hot plasma amounts to ≈50% of the total bolometric energy loss, with the conductive losses as a major contribution. The nonthermal energy input by energetic electrons is not sufficient to account for the total heating requirements of

  13. Remarkable events from X ray emulsion chambers and multiple production at LHC energy

    NASA Astrophysics Data System (ADS)

    Capdevielle, J. N.; Talai, M. C.; Attallah, R.

    The CORSIKA programme and specific Monte Carlo collision generators are employed in the interpretation of X-ray emulsion chambers data on super gamma ray families at mountain altitude (Chacaltaya, Kanbala, Pamir...) and in the stratosphere (Concorde, balloons). The consequences of measurement conditions(energy thresholds levels...) are detailed to extract common features for the neutral and charged secondaries. The vertex is approached by invariant mass method, geometry, pseudo rapidity distributions , and factors. Sorting the gamma's coupled in the maximum of invariant histograms, we evaluate the multiplicity , , inelasticity behavior up to LHC energy. Attention is given to the penetration power of EAS which levels off one energy decade around the knee and observations related with the fragmentation region (high energy hadron and gamma spectra in EAS, intensity of families with halo's). Hints of new physics are considered around the intriguing alignments registrated in the energy band between colliders and LHC. Several events (stratosphere and mountain) exhibit coplanar emission at similar visible energy, suggesting the valence diquark breaking. Such violent breaking suppressing the leading cluster recombination might come from the rupture of the string under very high tension between the two partners of the diquark.

  14. X-ray lithography source

    DOEpatents

    Piestrup, M.A.; Boyers, D.G.; Pincus, C.

    1991-12-31

    A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits is disclosed. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and eliminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an excellent moderate-priced X-ray source for lithography. 26 figures.

  15. X-ray lithography source

    DOEpatents

    Piestrup, Melvin A.; Boyers, David G.; Pincus, Cary

    1991-01-01

    A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and elminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an exellent moderate-priced X-ray source for lithography.

  16. Analysis of energy dispersive x-ray diffraction profiles for material identification, imaging and system control

    NASA Astrophysics Data System (ADS)

    Cook, Emily Jane

    2008-12-01

    This thesis presents the analysis of low angle X-ray scatter measurements taken with an energy dispersive system for substance identification, imaging and system control. Diffraction measurements were made on illicit drugs, which have pseudo- crystalline structures and thus produce diffraction patterns comprising a se ries of sharp peaks. Though the diffraction profiles of each drug are visually characteristic, automated detection systems require a substance identification algorithm, and multivariate analysis was selected as suitable. The software was trained with measured diffraction data from 60 samples covering 7 illicit drugs and 5 common cutting agents, collected with a range of statistical qual ities and used to predict the content of 7 unknown samples. In all cases the constituents were identified correctly and the contents predicted to within 15%. Soft tissues exhibit broad peaks in their diffraction patterns. Diffraction data were collected from formalin fixed breast tissue samples and used to gen erate images. Maximum contrast between healthy and suspicious regions was achieved using momentum transfer windows 1.04-1.10 and 1.84-1.90 nm_1. The resulting images had an average contrast of 24.6% and 38.9% compared to the corresponding transmission X-ray images (18.3%). The data was used to simulate the feedback for an adaptive imaging system and the ratio of the aforementioned momentum transfer regions found to be an excellent pa rameter. Investigation into the effects of formalin fixation on human breast tissue and animal tissue equivalents indicated that fixation in standard 10% buffered formalin does not alter the diffraction profiles of tissue in the mo mentum transfer regions examined, though 100% unbuffered formalin affects the profile of porcine muscle tissue (a substitute for glandular and tumourous tissue), though fat is unaffected.

  17. Development of a CdTe pixel detector with a window comparator ASIC for high energy X-ray applications

    NASA Astrophysics Data System (ADS)

    Hirono, T.; Toyokawa, H.; Furukawa, Y.; Honma, T.; Ikeda, H.; Kawase, M.; Koganezawa, T.; Ohata, T.; Sato, M.; Sato, G.; Takagaki, M.; Takahashi, T.; Watanabe, S.

    2011-09-01

    We have developed a photon-counting-type CdTe pixel detector (SP8-01). SP8-01 was designed as a prototype of a high-energy X-ray imaging detector for experiments using synchrotron radiation. SP8-01 has a CdTe sensor of 500 μm thickness, which has an absorption efficiency of almost 100% up to 50 keV and 45% even at 100 keV. A full-custom application specific integrated circuit (ASIC) was designed as a readout circuit of SP8-01, which is equipped with a window-type discriminator. The upper discriminator realizes a low-background measurement, because X-ray beams from the monochromator contain higher-order components beside the fundamental X-rays in general. ASIC chips were fabricated with a TSMC 0.25 μm CMOS process, and CdTe sensors were bump-bonded to the ASIC chips by a gold-stud bonding technique. Beam tests were performed at SPring-8. SP8-01 detected X-rays up to 120 keV. The capability of SP8-01 as an imaging detector for high-energy X-ray synchrotron radiation was evaluated with its performance characteristics.

  18. MeV per nucleon ion irradiation of nuclear materials with high energy synchrotron X-ray characterization

    NASA Astrophysics Data System (ADS)

    Pellin, M. J.; Yacout, Abdellatif M.; Mo, Kun; Almer, Jonathan; Bhattacharya, S.; Mohamed, Walid; Seidman, D.; Ye, Bei; Yun, D.; Xu, Ruqing; Zhu, Shaofei

    2016-04-01

    The combination of MeV/Nucleon ion irradiation (e.g. 133 MeV Xe) and high energy synchrotron x-ray characterization (e.g. at the Argonne Advanced Photon Source, APS) provides a powerful characterization method to understand radiation effects and to rapidly screen materials for the nuclear reactor environment. Ions in this energy range penetrate ∼10 μm into materials. Over this range, the physical interactions vary (electronic stopping, nuclear stopping and added interstitials). Spatially specific x-ray (and TEM and nanoindentation) analysis allow individual quantification of these various effects. Hard x-rays provide the penetration depth needed to analyze even nuclear fuels. Here, this combination of synchrotron x-ray and MeV/Nucleon ion irradiation is demonstrated on U-Mo fuels. A preliminary look at HT-9 steels is also presented. We suggest that a hard x-ray facility with in situ MeV/nucleon irradiation capability would substantially accelerate the rate of discovery for extreme materials.

  19. Energy Dispersive Spectrometry and Quantitative Analysis Short Course. Introduction to X-ray Energy Dispersive Spectrometry and Quantitative Analysis

    NASA Technical Reports Server (NTRS)

    Carpenter, Paul; Curreri, Peter A. (Technical Monitor)

    2002-01-01

    This course will cover practical applications of the energy-dispersive spectrometer (EDS) to x-ray microanalysis. Topics covered will include detector technology, advances in pulse processing, resolution and performance monitoring, detector modeling, peak deconvolution and fitting, qualitative and quantitative analysis, compositional mapping, and standards. An emphasis will be placed on use of the EDS for quantitative analysis, with discussion of typical problems encountered in the analysis of a wide range of materials and sample geometries.

  20. Compton scattering for spectroscopic detection of ultra-fast, high flux, broad energy range X-rays

    SciTech Connect

    Cipiccia, S.; Wiggins, S. M.; Brunetti, E.; Vieux, G.; Yang, X.; Welsh, G. H.; Anania, M.; Islam, M. R.; Ersfeld, B.; Jaroszynski, D. A.; Maneuski, D.; Montgomery, R.; Smith, G.; Hoek, M.; Hamilton, D. J.; Shea, V. O.; Issac, R. C.; Lemos, N. R. C.; Dias, J. M.; and others

    2013-11-15

    Compton side-scattering has been used to simultaneously downshift the energy of keV to MeV energy range photons while attenuating their flux to enable single-shot, spectrally resolved, measurements of high flux X-ray sources to be undertaken. To demonstrate the technique a 1 mm thick pixelated cadmium telluride detector has been used to measure spectra of Compton side-scattered radiation from a Cobalt-60 laboratory source and a high flux, high peak brilliance X-ray source of betatron radiation from a laser-plasma wakefield accelerator.

  1. A rotational and axial motion system load frame insert for in situ high energy x-ray studies.

    PubMed

    Shade, Paul A; Blank, Basil; Schuren, Jay C; Turner, Todd J; Kenesei, Peter; Goetze, Kurt; Suter, Robert M; Bernier, Joel V; Li, Shiu Fai; Lind, Jonathan; Lienert, Ulrich; Almer, Jonathan

    2015-09-01

    High energy x-ray characterization methods hold great potential for gaining insight into the behavior of materials and providing comparison datasets for the validation and development of mesoscale modeling tools. A suite of techniques have been developed by the x-ray community for characterizing the 3D structure and micromechanical state of polycrystalline materials; however, combining these techniques with in situ mechanical testing under well characterized and controlled boundary conditions has been challenging due to experimental design requirements, which demand new high-precision hardware as well as access to high-energy x-ray beamlines. We describe the design and performance of a load frame insert with a rotational and axial motion system that has been developed to meet these requirements. An example dataset from a deforming titanium alloy demonstrates the new capability.

  2. A rotational and axial motion system load frame insert for in situ high energy x-ray studies.

    PubMed

    Shade, Paul A; Blank, Basil; Schuren, Jay C; Turner, Todd J; Kenesei, Peter; Goetze, Kurt; Suter, Robert M; Bernier, Joel V; Li, Shiu Fai; Lind, Jonathan; Lienert, Ulrich; Almer, Jonathan

    2015-09-01

    High energy x-ray characterization methods hold great potential for gaining insight into the behavior of materials and providing comparison datasets for the validation and development of mesoscale modeling tools. A suite of techniques have been developed by the x-ray community for characterizing the 3D structure and micromechanical state of polycrystalline materials; however, combining these techniques with in situ mechanical testing under well characterized and controlled boundary conditions has been challenging due to experimental design requirements, which demand new high-precision hardware as well as access to high-energy x-ray beamlines. We describe the design and performance of a load frame insert with a rotational and axial motion system that has been developed to meet these requirements. An example dataset from a deforming titanium alloy demonstrates the new capability. PMID:26429452

  3. A rotational and axial motion system load frame insert for in situ high energy x-ray studies

    SciTech Connect

    Shade, Paul A. Schuren, Jay C.; Turner, Todd J.; Blank, Basil; Kenesei, Peter; Goetze, Kurt; Lienert, Ulrich; Almer, Jonathan; Suter, Robert M.; Bernier, Joel V.; Li, Shiu Fai; Lind, Jonathan

    2015-09-15

    High energy x-ray characterization methods hold great potential for gaining insight into the behavior of materials and providing comparison datasets for the validation and development of mesoscale modeling tools. A suite of techniques have been developed by the x-ray community for characterizing the 3D structure and micromechanical state of polycrystalline materials; however, combining these techniques with in situ mechanical testing under well characterized and controlled boundary conditions has been challenging due to experimental design requirements, which demand new high-precision hardware as well as access to high-energy x-ray beamlines. We describe the design and performance of a load frame insert with a rotational and axial motion system that has been developed to meet these requirements. An example dataset from a deforming titanium alloy demonstrates the new capability.

  4. Characterization of the C-MOS Cd-Te Imager PIXIRAD for energy discriminated X-ray imaging

    NASA Astrophysics Data System (ADS)

    Romano, A.; Pacella, D.; Claps, G.; Causa, F.; Gabellieri, L.

    2015-02-01

    The aim of the present work is to assess the operational characteristics of the PIXIRAD Imaging Counter for use in high-definition energy resolved X-ray imaging for different applications. The PIXIRAD imager was developed by an INFN-Pisa Spin-off. It works in photon counting mode in a wide energy range, soft and hard X-rays (2-100 keV), with pulse discrimination defined by two thresholds. The 650 μ m thick CdTe X-ray sensor is interfaced with a CMOS VLSI chip organized on a 512× 476 matrix of 55 μ m exagonal pixels (total active area of 30.7× 24.8 mm2). The experimental characterization was carried out in the range 3.7-80 keV, to assess the energy discrimination capability and detection efficiency of the PIXIRAD. Energy discrimination in bands was investigated using calibrated monochromatic X-ray sources (fluorescence of Ca, Fe, Cu, Br, Mo, Ag, I, Ta) and a BaCs radioactive source. In addition, two absolutely calibrated X-ray sources (Moxtek 50 kV Bullet and Oxford Instruments SB-80-1M) were utilized. The experimental data show that the PIXIRAD energy response is linear up to about 15 keV, beyond which the cluster size becomes larger than the pixel dimension. It produces multiple counts resulting in a tail at lower energy. Energy resolution was estimated to be about 30%. The effects in term of energy discrimination and a ``smooth energy discrimination'' in bands has been investigated by studying the separation between different energy lines, acquiring combined images with different energy ranges and setting properly the PIXIRAD threshold.

  5. Energy resolved two-dimensional soft x-ray radiography with a micropattern gas detector

    SciTech Connect

    Pacella, Danilo; Bellazzini, Ronaldo; Finkenthal, Michael

    2006-04-15

    This article discusses the use of energy resolved two-dimensional soft x-ray imaging (ERXI), in the range of 2-8 keV, to study and investigate composition and depth of different materials. This technique represents a new approach in which imaging is merged with multienergy analysis, performed with spectral scans in 25 energy subintervals. The detector used is a micropattern gas detector with gas electron multiplier as amplifying structure, pixel readout board with 144 pixels (12x12), and electronics for photon counting for each pixel. As the detector works in a proportional regime, images in adjustable energy windows (independently for each pixel) can be acquired. Energy resolution enhances the contrast and the imaging capability providing more information of the transparencies of the materials under investigations. Contact radiographies have been made with samples of four different materials: CaCl, organic fat matter, aluminum, and thin plastic tape. The resulting data transparency curves for these materials have been derived. These curves demonstrate the value of ERXI at high performances (high efficiency, high dynamics, and high contrast), potentially relevant for many future applications.

  6. Energy-dispersive X-ray emission spectroscopy using an X-ray free-electron laser in a shot-by-shot mode

    DOE PAGESBeta

    Alonso-Mori, Roberto; Kern, Jan; Gildea, Richard J.; Sokaras, Dimosthenis; Weng, Tsu -Chien; Lassalle-Kaiser, Benedikt; Tran, Rosalie; Hattne, Johan; Laksmono, Hartawan; Hellmich, Julia; et al

    2012-11-05

    The ultrabright femtosecond X-ray pulses provided by X-ray free-electron lasers open capabilities for studying the structure and dynamics of a wide variety of systems beyond what is possible with synchrotron sources. Recently, this “probe-before-destroy” approach has been demonstrated for atomic structure determination by serial X-ray diffraction of microcrystals. There has been the question whether a similar approach can be extended to probe the local electronic structure by X-ray spectroscopy. To address this, we have carried out femtosecond X-ray emission spectroscopy (XES) at the Linac Coherent Light Source using redox-active Mn complexes. XES probes the charge and spin states as wellmore » as the ligand environment, critical for understanding the functional role of redox-active metal sites. Kβ1,3 XES spectra of MnII and Mn2III,IV complexes at room temperature were collected using a wavelength dispersive spectrometer and femtosecond X-ray pulses with an individual dose of up to >100 MGy. The spectra were found in agreement with undamaged spectra collected at low dose using synchrotron radiation. Our results demonstrate that the intact electronic structure of redox active transition metal compounds in different oxidation states can be characterized with this shot-by-shot method. This opens the door for studying the chemical dynamics of metal catalytic sites by following reactions under functional conditions. Furthermore, the technique can be combined with X-ray diffraction to simultaneously obtain the geometric structure of the overall protein and the local chemistry of active metal sites and is expected to prove valuable for understanding the mechanism of important metalloproteins, such as photosystem II.« less

  7. Energy-dispersive X-ray emission spectroscopy using an X-ray free-electron laser in a shot-by-shot mode

    SciTech Connect

    Alonso-Mori, Roberto; Kern, Jan; Gildea, Richard J.; Sokaras, Dimosthenis; Weng, Tsu -Chien; Lassalle-Kaiser, Benedikt; Tran, Rosalie; Hattne, Johan; Laksmono, Hartawan; Hellmich, Julia; Glockner, Carina; Echols, Nathaniel; Sierra, Raymond G.; Schafer, Donald W.; Sellberg, Jonas; Kenney, Christopher; Herbst, Ryan; Pines, Jack; Hart, Philip; Herrmann, Sven; Grosse-Kunstleve, Ralf W.; Latimer, Matthew J.; Fry, Alan R.; Messerschmidt, Marc M.; Miahnahri, Alan; Seibert, M. Marvin; Zwart, Petrus H.; White, William E.; Adams, Paul D.; Bogan, Michael J.; Boutet, Sebastien; Williams, Garth J.; Zouni, Athina; Messinger, Johannes; Glatzel, Pieter; Sauter, Nicholas K.; Yachandra, Vittal K.; Yano, Junko; Bergmann, Uwe

    2012-11-05

    The ultrabright femtosecond X-ray pulses provided by X-ray free-electron lasers open capabilities for studying the structure and dynamics of a wide variety of systems beyond what is possible with synchrotron sources. Recently, this “probe-before-destroy” approach has been demonstrated for atomic structure determination by serial X-ray diffraction of microcrystals. There has been the question whether a similar approach can be extended to probe the local electronic structure by X-ray spectroscopy. To address this, we have carried out femtosecond X-ray emission spectroscopy (XES) at the Linac Coherent Light Source using redox-active Mn complexes. XES probes the charge and spin states as well as the ligand environment, critical for understanding the functional role of redox-active metal sites. Kβ1,3 XES spectra of MnII and Mn2III,IV complexes at room temperature were collected using a wavelength dispersive spectrometer and femtosecond X-ray pulses with an individual dose of up to >100 MGy. The spectra were found in agreement with undamaged spectra collected at low dose using synchrotron radiation. Our results demonstrate that the intact electronic structure of redox active transition metal compounds in different oxidation states can be characterized with this shot-by-shot method. This opens the door for studying the chemical dynamics of metal catalytic sites by following reactions under functional conditions. Furthermore, the technique can be combined with X-ray diffraction to simultaneously obtain the geometric structure of the overall protein and the local chemistry of active metal sites and is expected to prove valuable for understanding the mechanism of important metalloproteins, such as photosystem II.

  8. Learning to Apply Metrology Principles to the Measurement of X-ray Intensities in the 500 eV to 110 keV Energy Range

    SciTech Connect

    Haugh, M. J.; Pond, T.; Silbernagel, C.; Torres, P.; Marlett, K.; Goldin, F.; Cyr, S.

    2011-02-08

    National Security Technologies, LLC (NSTec), Livermore Operations, has two optical radiation calibration laboratories accredited by “the National Voluntary Laboratories Accreditation Program (NVLAP) which is the accrediting body of” the National Institute of Standards and Technology (NIST), and is now working towards accreditation for its X-ray laboratories. NSTec operates several laboratories with X-ray sources that generate X-rays in the energy range from 50 eV to 115 keV. These X-ray sources are used to characterize and calibrate diagnostics and diagnostic components used by the various national laboratories, particularly for plasma analysis on the Lawrence Livermore National Laboratory (LLNL) National Ignition Facility (NIF). Because X-ray photon flux measurement methods that can be accredited, i.e., traceable to NIST, have not been developed for sources operating in these energy ranges, NSTec, NIST, and the National Voluntary Accreditation Program (NVLAP) together have defined a path toward the development and validation of accredited metrology methods for X-ray energies. The methodology developed for the high energy X-ray (HEX) Laboratory was NSTec’s starting point for X-ray metrology accreditation and will be the basis for the accredited processes in the other X-ray laboratories. This paper will serve as a teaching tool, by way of this example using the NSTec X-ray sources, for the process and methods used in developing an accredited traceable metrology.

  9. Alignment, Assembly and Testing of High Energy X-Ray Optics

    NASA Technical Reports Server (NTRS)

    Gubarev, Mikhail; Ramsey, Brian

    2005-01-01

    We are developing grazing-incidence x-ray imaging optics for a balloon-borne hard x-ray telescope (HERO). The HERO payload, scheduled for launch in May 2005, currently consists of 8 mirror modules each containing 12 mirror shells fabricated using electroform-nickel replication off super-polished cylindrical mandrels. An optical system developed for aligning and assembling the shells in the modules will be described. Sources for systematic errors associated with this process will be discussed and results from on-ground x-ray testing of each module will be presented.

  10. Athermal Energy Loss from X-rays Deposited in Thin Superconducting Films on Solid Substrates

    NASA Technical Reports Server (NTRS)

    Kozorezov, Alexander G.; Lambert, Colin J.; Bandler, Simon R.; Balvin, Manuel A.; Busch, Sarah E.; Sagler, Peter N.; Porst, Jan-Patrick; Smith, Stephen J.; Stevenson, Thomas R.; Sadleir, John E.

    2013-01-01

    When energy is deposited in a thin-film cryogenic detector, such as from the absorption of an X-ray, an important feature that determines the energy resolution is the amount of athermal energy that can be lost to the heat bath prior to the elementary excitation systems coming into thermal equilibrium. This form of energy loss will be position-dependent and therefore can limit the detector energy resolution. An understanding of the physical processes that occur when elementary excitations are generated in metal films on dielectric substrates is important for the design and optimization of a number of different types of low temperature detector. We have measured the total energy loss in one relatively simple geometry that allows us to study these processes and compare measurements with calculation based upon a model for the various di.erent processes. We have modeled the athermal phonon energy loss in this device by finding an evolving phonon distribution function that solves the system of kinetic equations for the interacting system of electrons and phonons. Using measurements of device parameters such as the Debye energy and the thermal di.usivity we have calculated the expected energy loss from this detector geometry, and also the position-dependent variation of this loss. We have also calculated the predicted impact on measured spectral line-shapes, and shown that they agree well with measurements. In addition, we have tested this model by using it to predict the performance of a number of other types of detector with di.erent geometries, where good agreement is also found.

  11. Optimizing the operation of a high resolution vertical Johann spectrometer using a high energy fluorescer x-ray source

    SciTech Connect

    Haugh, Michael; Stewart, Richard

    2010-10-15

    This paper describes the operation and testing for a vertical Johann spectrometer (VJS) operating in the 13 keV range. The spectrometer is designed to use thin curved mica crystals or thick germanium crystals. The VJS must have a resolution of E/{Delta}E=3000 or better to measure the Doppler broadening of highly ionized krypton and operate at a small x-ray angle in order to be used as a diagnostic in a laser plasma target chamber. The VJS was aligned, tested, and optimized using a fluorescer type high energy x-ray (HEX) source located at National Security Technologies (NSTec), LLC, in Livermore, CA. The HEX uses a 160 kV x-ray tube to excite fluorescence from various targets. Both rubidium and bismuth fluorescers were used for this effort. This presentation describes the NSTec HEX system and the methods used to optimize and characterize the VJS performance.

  12. Optimizing the Operation of a Vertical Johann Spectrometer Using a High Energy Fluorescer X-ray Source

    SciTech Connect

    Haugh, Michael; Stewart, Richard

    2010-10-01

    This paper describes the operation and testing for a Vertical Johann Spectrometer (VJS) operating in the 13 keV range. The spectrometer is designed to use thin curved mica crystals or thick germanium crystals. The VJS must have a resolution E/ΔE=3000 or better to measure Doppler broadening of highly ionized krypton and operate at a small X-ray angle in order to be used as a diagnostic in a laser plasma target chamber. The VJS was aligned, tested, and optimized using a fluorescer type high energy X-ray (HEX) source located at National Security Technologies, LLC (NSTec), in Livermore, California. The HEX uses a 160 kV X-ray tube to excite fluorescence from various targets. Both rubidium and bismuth fluorescers were used for this effort. This presentation describes the NSTec HEX system and the methods used to optimize and characterize the VJS performance.

  13. A proposal for an x-ray free-electron laser oscillator with an energy-recovery linac.

    SciTech Connect

    Kim, K. J.; Shvyd'ko, Y.; Reiche, S.; Accelerator Systems Division; UCLA

    2008-06-01

    We show that a free-electron laser oscillator generating x rays with wavelengths of about 1 {angstrom} is feasible using ultralow emittance electron beams of a multi-GeV energy-recovery linac, combined with a low-loss crystal cavity. The device will produce x-ray pulses with 10{sup 9} photons at a repetition rate of 1-100 MHz. The pulses are temporarily and transversely coherent, with a rms bandwidth of about 2 meV, and rms pulse length of about 1 ps.

  14. Characterization of spatially resolved high resolution x-ray spectrometers for high energy density physics and light source experiments

    SciTech Connect

    Hill, K. W. Bitter, M.; Delgado-Aparacio, L.; Efthimion, P.; Pablant, N. A.; Lu, J.; Beiersdorfer, P.; Chen, H.; Magee, E.

    2014-11-15

    A high resolution 1D imaging x-ray spectrometer concept comprising a spherically bent crystal and a 2D pixelated detector is being optimized for diagnostics of small sources such as high energy density physics (HEDP) and synchrotron radiation or x-ray free electron laser experiments. This instrument is used on tokamak experiments for Doppler measurements of ion temperature and plasma flow velocity profiles. Laboratory measurements demonstrate a resolving power, E/ΔE of order 10 000 and spatial resolution better than 10 μm. Initial tests of the high resolution instrument on HEDP plasmas are being performed.

  15. Silicon saw-tooth refractive lens for high-energy x-rays made using a diamond saw.

    SciTech Connect

    Said, A. H.; Shastri, S. D.; X-Ray Science Division

    2010-01-01

    Silicon is a material well suited for refractive lenses operating at high X-ray energies (>50 keV), particularly if implemented in a single-crystal form to minimize small-angle scattering. A single-crystal silicon saw-tooth refractive lens, fabricated by a dicing process using a thin diamond wheel, was tested with 115 keV X-rays, giving an ideal 17 {mu}m line focus width in a long focal length, 2:1 ratio demagnification geometry, with a source-to-focus distance of 58.5 m. The fabrication is simple, using resources typically available at any synchrotron facility's optics shop.

  16. A Proposal for an X-Ray Free-Electron Laser Oscillator with an Energy-Recovery Linac

    SciTech Connect

    Kim, Kwang-Je; Shvydko, Yuri; Reiche, Sven

    2008-06-20

    We show that a free-electron laser oscillator generating x rays with wavelengths of about 1 A is feasible using ultralow emittance electron beams of a multi-GeV energy-recovery linac, combined with a low-loss crystal cavity. The device will produce x-ray pulses with 10{sup 9} photons at a repetition rate of 1-100 MHz. The pulses are temporarily and transversely coherent, with a rms bandwidth of about 2 meV, and rms pulse length of about 1 ps.

  17. A Giant Lyα Nebula in the Core of an X-Ray Cluster at Z = 1.99: Implications for Early Energy Injection

    NASA Astrophysics Data System (ADS)

    Valentino, Francesco; Daddi, Emanuele; Finoguenov, Alexis; Strazzullo, Veronica; Le Brun, Amandine; Vignali, Cristian; Bournaud, Frédéric; Dickinson, Mark; Renzini, Alvio; Béthermin, Matthieu; Zanella, Anita; Gobat, Raphaël; Cimatti, Andrea; Elbaz, David; Onodera, Masato; Pannella, Maurilio; Sargent, Mark; Arimoto, Nobuo; Carollo, Marcella; Starck, Jean-Luc

    2016-09-01

    We present the discovery of a giant ≳100 kpc Lyα nebula detected in the core of the X-ray emitting cluster CL J1449+0856 at z = 1.99 through Keck/LRIS narrow-band imaging. This detection extends the known relation between Lyα nebulae and overdense regions of the universe to the dense core of a 5-7 × 1013 M ⊙ cluster. The most plausible candidates to power the nebula are two Chandra-detected AGN host cluster members, while cooling from the X-ray phase and cosmological cold flows are disfavored primarily because of the high Lyα to X-ray luminosity ratio ({L}{Lyα }/{L}{{X}}≈ 0.3, ≳10-1000 times higher than in local cool-core clusters) and by current modeling. Given the physical conditions of the Lyα-emitting gas and the possible interplay with the X-ray phase, we argue that the Lyα nebula would be short-lived (≲10 Myr) if not continuously replenished with cold gas at a rate of ≳1000 M ⊙ yr-1. We investigate the possibility that cluster galaxies supply the required gas through outflows and we show that their total mass outflow rate matches the replenishment necessary to sustain the nebula. This scenario directly implies the extraction of energy from galaxies and its deposition in the surrounding intracluster medium (ICM), as required to explain the thermodynamic properties of local clusters. We estimate an energy injection of the order of ≈ 2 {{keV}} per particle in the ICM over a 2 Gyr interval. In our baseline calculation, AGNs provide up to 85% of the injected energy and two-thirds of the mass, while the rest is supplied by supernovae-driven winds.

  18. Deterministic Computer-Controlled Polishing Process for High-Energy X-Ray Optics

    NASA Technical Reports Server (NTRS)

    Khan, Gufran S.; Gubarev, Mikhail; Speegle, Chet; Ramsey, Brian

    2010-01-01

    A deterministic computer-controlled polishing process for large X-ray mirror mandrels is presented. Using tool s influence function and material removal rate extracted from polishing experiments, design considerations of polishing laps and optimized operating parameters are discussed

  19. Mammalian cell killing by ultrasoft X rays and high-energy radiation: an extension of the MK model.

    PubMed

    Hawkins, Roland B

    2006-08-01

    An alternate formulation of the microdosimetric-kinetic (MK) model is presented that applies to irradiation of mammalian cells with ultrasoft X rays as well as high-energy radiations of variable linear energy transfer (LET). Survival and DNA double-strand break measurements for V79 cells from the literature are examined to illustrate application of the model. It is demonstrated that the linear component of the linear-quadratic survival relationship (alpha) is enhanced because repairable potentially lethal lesions formed from a single ultrasoft X-ray energy deposition event, when closer on average than for a single high-energy radiation event, are more likely to combine to form a lethal lesion. The quadratic component (beta) of the linear-quadratic survival relationship is increased because the potentially lethal lesions formed by ultrasoft X rays are created with greater efficiency than those of high-energy radiation. In addition, potentially lethal lesions from very low-energy carbon K-shell X rays may be enriched in structural forms that favor combination to form lethal lesions instead of repair. These features account for the increased effectiveness of killing of V79 cells by ultrasoft X rays compared to cobalt-60 gamma radiation. The importance of pairwise combination of potentially lethal lesions to form exchange chromosome aberrations that become lethal lesions is discussed. The extended MK model explains and reconciles differences between the MK model and the theory of dual radiation action on the one hand, and on the other, the view that variation in the RBE with radiation quality is explained by differences in energy deposition in nanometer- rather than micrometer-size volumes.

  20. Body Composition Comparison: Bioelectric Impedance Analysis with Dual-Energy X-Ray Absorptiometry in Adult Athletes

    ERIC Educational Resources Information Center

    Company, Joe; Ball, Stephen

    2010-01-01

    The primary purpose of this study was to investigate the accuracy of the DF50 (ImpediMed Ltd, Eight Mile Plains, Queensland, Australia) bioelectrical impedance analysis device using dual-energy x-ray absorptiometry as the criterion in two groups: endurance athletes and power athletes. The secondary purpose was to develop accurate body fat…

  1. Assessing Body Composition of Children and Adolescents Using Dual-Energy X-Ray Absorptiometry, Skinfolds, and Electrical Impedance

    ERIC Educational Resources Information Center

    Mooney, Angela; Kelsey, Laurel; Fellingham, Gilbert W.; George, James D.; Hager, Ron L.; Myrer, J. William; Vehrs, Pat R.

    2011-01-01

    To determine the validity and reliability of percent body fat estimates in 177 boys and 154 girls between 12-17 years of age, percent body fat was assessed once using dual-energy X-ray absorptiometry and twice using the sum of two skinfolds and three bioelectrical impedance analysis devices. The assessments were repeated on 79 participants on a…

  2. Measurements of electron temperature profiles on Alcator C-Mod using a novel energy-resolving x-ray camera

    NASA Astrophysics Data System (ADS)

    Maddox, J.; Delgado, L.; Pablant, N.; Hill, K. W.; Bitter, M.; Efthimion, P.; Rice, J.

    2015-11-01

    The most common electron temperature diagnostics, Thomson Scattering (TS) and Electron Cyclotron Emission (ECE), both require large diagnostic footprints and expensive optics. Another electron temperature diagnostic is the Pulse-Height-Analysis (PHA) system, which derives the electron temperature from the x-ray bremsstrahlung continuum. However, the main disadvantage of the PHA method is poor temporal resolution of the Si(Li) diode detectors. This paper presents a novel x-ray pinhole camera, which uses a pixilated Pilatus detector that allows single photon counting at a rate 2MHz per pixel and the setting of energy thresholds. The detector configuration is optimized by Shannon-sampling theory, such that spatial profiles of the x-ray continuum intensity can be obtained simultaneously for different energies, in the range from 4 to 16 keV. The exponential-like dependence of the x-ray intensity with photon energies is compared with a model describing the Be filter, attenuation in air, and detector efficiency, as well as different sets of energy thresholds. Electron temperature measurements are compared with TS and ECE measurements. This work was supported by the US DOE Contract No.DE-AC02-09CH11466 and the DoE Summer Undergraduate Laboratory Internship (SULI) program.

  3. A hybrid Monte Carlo model for the energy response functions of X-ray photon counting detectors

    NASA Astrophysics Data System (ADS)

    Wu, Dufan; Xu, Xiaofei; Zhang, Li; Wang, Sen

    2016-09-01

    In photon counting computed tomography (CT), it is vital to know the energy response functions of the detector for noise estimation and system optimization. Empirical methods lack flexibility and Monte Carlo simulations require too much knowledge of the detector. In this paper, we proposed a hybrid Monte Carlo model for the energy response functions of photon counting detectors in X-ray medical applications. GEANT4 was used to model the energy deposition of X-rays in the detector. Then numerical models were used to describe the process of charge sharing, anti-charge sharing and spectral broadening, which were too complicated to be included in the Monte Carlo model. Several free parameters were introduced in the numerical models, and they could be calibrated from experimental measurements such as X-ray fluorescence from metal elements. The method was used to model the energy response function of an XCounter Flite X1 photon counting detector. The parameters of the model were calibrated with fluorescence measurements. The model was further tested against measured spectrums of a VJ X-ray source to validate its feasibility and accuracy.

  4. DISCOVERY OF ENERGY-DEPENDENT X-RAY MICROLENSING IN Q2237+0305

    SciTech Connect

    Chen Bin; Dai Xinyu; Kochanek, C. S.; Blackburne, Jeffrey A.; Chartas, George; Kozlowski, Szymon

    2011-10-20

    We present our long-term Chandra X-ray monitoring data for the gravitationally lensed quasar Q2237+0305 with 20 epochs spanning 10 years. We easily detect microlensing variability between the images in the full (0.2-8 keV), soft (0.2-2 keV), and hard (2-8 keV) bands at very high confidence. We also detect, for the first time, chromatic microlensing differences between the soft and hard X-ray bands. The hard X-ray band is more strongly microlensed than the soft band, suggesting that the corona above the accretion disk thought to generate the X-rays has a non-uniform electron distribution, in which the hotter and more energetic electrons occupy more compact regions surrounding the black holes. Both the hard and soft X-ray bands are more strongly microlensed than the optical (rest-frame UV) emission, indicating that the X-ray emission is more compact than the optical, confirming the microlensing results from other lenses.

  5. Correlation of Thermally Induced Pores with Microstructural Features Using High Energy X-rays

    NASA Astrophysics Data System (ADS)

    Menasche, David B.; Shade, Paul A.; Lind, Jonathan; Li, Shiu Fai; Bernier, Joel V.; Kenesei, Peter; Schuren, Jay C.; Suter, Robert M.

    2016-11-01

    Combined application of a near-field High Energy Diffraction Microscopy measurement of crystal lattice orientation fields and a tomographic measurement of pore distributions in a sintered nickel-based superalloy sample allows pore locations to be correlated with microstructural features. Measurements were carried out at the Advanced Photon Source beamline 1-ID using an X-ray energy of 65 keV for each of the measurement modes. The nickel superalloy sample was prepared in such a way as to generate significant thermally induced porosity. A three-dimensionally resolved orientation map is directly overlaid with the tomographically determined pore map through a careful registration procedure. The data are shown to reliably reproduce the expected correlations between specific microstructural features (triple lines and quadruple nodes) and pore positions. With the statistics afforded by the 3D data set, we conclude that within statistical limits, pore formation does not depend on the relative orientations of the grains. The experimental procedures and analysis tools illustrated are being applied to a variety of materials problems in which local heterogeneities can affect materials properties.

  6. A novel scatter separation method for multi-energy x-ray imaging

    NASA Astrophysics Data System (ADS)

    Sossin, A.; Rebuffel, V.; Tabary, J.; Létang, J. M.; Freud, N.; Verger, L.

    2016-06-01

    X-ray imaging coupled with recently emerged energy-resolved photon counting detectors provides the ability to differentiate material components and to estimate their respective thicknesses. However, such techniques require highly accurate images. The presence of scattered radiation leads to a loss of spatial contrast and, more importantly, a bias in radiographic material imaging and artefacts in computed tomography (CT). The aim of the present study was to introduce and evaluate a partial attenuation spectral scatter separation approach (PASSSA) adapted for multi-energy imaging. This evaluation was carried out with the aid of numerical simulations provided by an internal simulation tool, Sindbad-SFFD. A simplified numerical thorax phantom placed in a CT geometry was used. The attenuation images and CT slices obtained from corrected data showed a remarkable increase in local contrast and internal structure detectability when compared to uncorrected images. Scatter induced bias was also substantially decreased. In terms of quantitative performance, the developed approach proved to be quite accurate as well. The average normalized root-mean-square error between the uncorrected projections and the reference primary projections was around 23%. The application of PASSSA reduced this error to around 5%. Finally, in terms of voxel value accuracy, an increase by a factor  >10 was observed for most inspected volumes-of-interest, when comparing the corrected and uncorrected total volumes.

  7. X-ray optics of gold nanoparticles.

    PubMed

    Letfullin, Renat R; Rice, Colin E W; George, Thomas F

    2014-11-01

    Gold nanoparticles have been investigated as contrast agents for traditional x-ray medical procedures, utilizing the strong absorption characteristics of the nanoparticles to enhance the contrast of the detected x-ray image. Here we use the Kramers-Kronig relation for complex atomic scattering factors to find the real and imaginary parts of the index of refraction for the medium composed of single-element materials or compounds in the x-ray range of the spectrum. These complex index of refraction values are then plugged into a Lorenz-Mie theory to calculate the absorption efficiency of various size gold nanoparticles for photon energies in the 1-100 keV range. Since the output from most medical diagnostic x-ray devices follows a wide and filtered spectrum of photon energies, we introduce and compute the effective intensity-absorption-efficiency values for gold nanoparticles of radii varying from 5 to 50 nm, where we use the TASMIP model to integrate over all spectral energies generated by typical tungsten anode x-ray tubes with kilovolt potentials ranging from 50 to 150 kVp.

  8. ELECTRON ENERGY PARTITION IN THE ABOVE-THE-LOOPTOP SOLAR HARD X-RAY SOURCES

    SciTech Connect

    Oka, Mitsuo; Krucker, Säm; Hudson, Hugh S.; Saint-Hilaire, Pascal

    2015-02-01

    Solar flares produce non-thermal electrons with energies up to tens of MeVs. To understand the origin of energetic electrons, coronal hard X-ray (HXR) sources, in particular above-the-looptop sources, have been studied extensively. However, it still remains unclear how energies are partitioned between thermal and non-thermal electrons within the above-the-looptop source. Here we show that the kappa distribution, when compared to conventional spectral models, can better characterize the above-the-looptop HXRs (≳15 keV) observed in four different cases. The widely used conventional model (i.e., the combined thermal plus power-law distribution) can also fit the data, but it returns unreasonable parameter values due to a non-physical sharp lower-energy cutoff E{sub c}. In two cases, extreme-ultraviolet data were available from SDO/AIA and the kappa distribution was still consistent with the analysis of differential emission measure. Based on the kappa distribution model, we found that the 2012 July 19 flare showed the largest non-thermal fraction of electron energies about 50%, suggesting equipartition of energies. Considering the results of particle-in-cell simulations, as well as density estimates of the four cases studied, we propose a scenario in which electron acceleration is achieved primarily by collisionless magnetic reconnection, but the electron energy partition in the above-the-looptop source depends on the source density. In low-density above-the-looptop regions (few times 10{sup 9} cm{sup –3}), the enhanced non-thermal tail can remain and a prominent HXR source is created, whereas in higher-densities (>10{sup 10} cm{sup –3}), the non-thermal tail is suppressed or thermalized by Coulomb collisions.

  9. SN 2005ip: A luminous type IIn supernova emerging from a dense circumstellar medium as revealed by X-ray observations

    SciTech Connect

    Katsuda, Satoru; Maeda, Keiichi; Nozawa, Takaya; Pooley, David; Immler, Stefan

    2014-01-10

    We report on the X-ray spectral evolution of the nearby Type IIn supernova (SN) 2005ip based on Chandra and Swift observations covering ∼1-6 yr after explosion. X-ray spectra in all epochs are well fitted by a thermal emission model with kT ≳ 7 keV. The somewhat high temperature suggests that the X-ray emission mainly arises from the circumstellar medium (CSM) heated by the forward shock. We find that the spectra taken two to three years after the explosion are heavily absorbed (N {sub H} ∼ 5 × 10{sup 22} cm{sup –2}), but the absorption gradually decreases to the level of the Galactic absorption (N {sub H} ∼ 4 × 10{sup 20} cm{sup –2}) at the final epoch. This indicates that the SN went off in a dense CSM and that the forward shock has overtaken it. The intrinsic X-ray luminosity stays constant until the final epoch, when it drops by a factor of ∼2. The intrinsic 0.2-10 keV luminosity during the plateau phase is measured to be ∼1.5 × 10{sup 41} erg s{sup –1}, ranking SN 2005ip as one of the brightest X-ray SNe. Based on the column density, we derive a lower limit of a mass-loss rate to be M-dot ∼1.5×10{sup −2} (V{sub w} /100 km s{sup –1}) M {sub ☉} yr{sup –1}, which roughly agrees with that inferred from the X-ray luminosity, M-dot ∼2×10{sup −2} (V{sub w} /100 km s{sup –1}) M {sub ☉} yr{sup –1}, where V{sub w} is the circumstellar wind speed. Such a high mass-loss rate suggests that the progenitor star had eruptive mass ejections similar to a luminous blue variable star. The total mass ejected in the eruptive period is estimated to be ∼15 M {sub ☉}, indicating that the progenitor mass is ≳ 25 M {sub ☉}.

  10. CORRELATED X-RAY AND VERY HIGH ENERGY EMISSION IN THE GAMMA-RAY BINARY LS I +61 303

    SciTech Connect

    Anderhub, H.; Biland, A.; Antonelli, L. A.; Antoranz, P.; Balestra, S.; Barrio, J. A.; Backes, M.; Becker, J. K.; Baixeras, C.; Bastieri, D.; Bock, R. K.; Gonzalez, J. Becerra; Bednarek, W.; Berger, K.; Bernardini, E.; Bigas, O. Blanch; Bonnoli, G.; Bordas, P.; Bosch-Ramon, V.; Tridon, D. Borla E-mail: jogler@mppmu.mpg.d

    2009-11-20

    The discovery of very high energy (VHE) gamma-ray emitting X-ray binaries has triggered an intense effort to better understand the particle acceleration, absorption, and emission mechanisms in compact binary systems, which provide variable conditions along eccentric orbits. Despite this, the nature of some of these systems, and of the accelerated particles producing the VHE emission, is unclear. To answer some of these open questions, we conducted a multiwavelength campaign of the VHE gamma-ray emitting X-ray binary LS I +61 303 including the MAGIC telescope, XMM-Newton, and Swift during 60% of an orbit in 2007 September. We detect a simultaneous outburst at X-ray and VHE bands, with the peak at phase 0.62 and a similar shape at both wavelengths. A linear fit to the simultaneous X-ray/VHE pairs obtained during the outburst yields a correlation coefficient of r = 0.97, while a linear fit to all simultaneous pairs provides r = 0.81. Since a variable absorption of the VHE emission towards the observer is not expected for the data reported here, the correlation found indicates a simultaneity in the emission processes. Assuming that they are dominated by a single particle population, either hadronic or leptonic, the X-ray/VHE flux ratio favors leptonic models. This fact, together with the detected photon indices, suggests that in LS I +61 303 the X-rays are the result of synchrotron radiation of the same electrons that produce VHE emission as a result of inverse Compton scattering of stellar photons.

  11. Prediction and Measurement of X-Ray Spectral and Intensity Distributions from Low Energy Electron Impact Sources

    NASA Technical Reports Server (NTRS)

    Edwards, David L.

    1999-01-01

    In-vacuum electron beam welding is a technology that NASA considered as a joining technique for manufacture of space structures. The interaction of energetic electrons with metal produces x-rays. The radiation exposure to astronauts performing the in-vacuum electron beam welding must be characterized and minimized to insure safe operating conditions. This investigation characterized the x-ray environment due to operation of an in-vacuum electron beam welding tool. NASA, in a joint venture with the Russian Space Agency, was scheduled to perform a series of welding in space experiments on board the United States Space Shuttle. This series of experiments was named the International Space Welding Experiment (ISWE). The hardware associated with the ISWE was leased to NASA, by the Paton Welding Institute (PWI) in Ukraine, for ground based welding experiments in preparation for flight. Two tests were scheduled, using the ISWE electron beam welding tool, to characterize the radiation exposure to an astronaut during the operation of the ISWE. These radiation exposure tests consisted of Thermoluminescence Dosimeters (TLD's) shielded with material currently used by astronauts during Extra Vehicular Activities (EVA) and exposed to x-ray radiation generated by operation of an in-vacuum electron beam welding tool. This investigation was the first known application of TLD's to measure absorbed dose from x-rays of energy less than 10 KeV. The ISWE hardware was returned to Ukraine before the issue of adequate shielding for the astronauts was verified. Therefore, alternate experimental and analytical methods were developed to measure and predict the x-ray spectral and intensity distribution generated by electron impact with metal. These x-ray spectra were used to calculate the absorbed radiation dose to astronauts. These absorbed dose values were compared to TLD measurements obtained during actual operation of the in-vacuum electron beam welding tool. The calculated absorbed dose

  12. Correlated X-Ray and Very High Energy Emission in the Gamma-Ray Binary LS I +61 303

    NASA Astrophysics Data System (ADS)

    Anderhub, H.; Antonelli, L. A.; Antoranz, P.; Backes, M.; Baixeras, C.; Balestra, S.; Barrio, J. A.; Bastieri, D.; Becerra González, J.; Becker, J. K.; Bednarek, W.; Berger, K.; Bernardini, E.; Biland, A.; Blanch Bigas, O.; Bock, R. K.; Bonnoli, G.; Bordas, P.; Borla Tridon, D.; Bosch-Ramon, V.; Bose, D.; Braun, I.; Bretz, T.; Britzger, D.; Camara, M.; Carmona, E.; Carosi, A.; Colin, P.; Commichau, S.; Contreras, J. L.; Cortina, J.; Costado, M. T.; Covino, S.; Dazzi, F.; De Angelis, A.; de Cea del Pozo, E.; De los Reyes, R.; De Lotto, B.; De Maria, M.; De Sabata, F.; Delgado Mendez, C.; Domínguez, A.; Dominis Prester, D.; Dorner, D.; Doro, M.; Elsaesser, D.; Errando, M.; Ferenc, D.; Fernández, E.; Firpo, R.; Fonseca, M. V.; Font, L.; Galante, N.; García López, R. J.; Garczarczyk, M.; Gaug, M.; Godinovic, N.; Goebel, F.; Hadasch, D.; Herrero, A.; Hildebrand, D.; Höhne-Mönch, D.; Hose, J.; Hrupec, D.; Hsu, C. C.; Jogler, T.; Klepser, S.; Kranich, D.; La Barbera, A.; Laille, A.; Leonardo, E.; Lindfors, E.; Lombardi, S.; Longo, F.; López, M.; Lorenz, E.; Majumdar, P.; Maneva, G.; Mankuzhiyil, N.; Mannheim, K.; Maraschi, L.; Mariotti, M.; Martínez, M.; Mazin, D.; Meucci, M.; Miranda, J. M.; Mirzoyan, R.; Miyamoto, H.; Moldón, J.; Moles, M.; Moralejo, A.; Nieto, D.; Nilsson, K.; Ninkovic, J.; Orito, R.; Oya, I.; Paoletti, R.; Paredes, J. M.; Pasanen, M.; Pascoli, D.; Pauss, F.; Pegna, R. G.; Perez-Torres, M. A.; Persic, M.; Peruzzo, L.; Prada, F.; Prandini, E.; Puchades, N.; Puljak, I.; Reichardt, I.; Rhode, W.; Ribó, M.; Rico, J.; Rissi, M.; Robert, A.; Rügamer, S.; Saggion, A.; Saito, T. Y.; Salvati, M.; Sánchez-Conde, M.; Satalecka, K.; Scalzotto, V.; Scapin, V.; Schweizer, T.; Shayduk, M.; Shore, S. N.; Sidro, N.; Sierpowska-Bartosik, A.; Sillanpää, A.; Sitarek, J.; Sobczynska, D.; Spanier, F.; Spiro, S.; Stamerra, A.; Stark, L. S.; Suric, T.; Takalo, L.; Tavecchio, F.; Temnikov, P.; Tescaro, D.; Teshima, M.; Torres, D. F.; Turini, N.; Vankov, H.; Wagner, R. M.; Zabalza, V.; Zandanel, F.; Zanin, R.; Zapatero, J.; MAGIC Collaboration; Falcone, A.; Vetere, L.; Gehrels, N.; Trushkin, S.; Dhawan, V.; Reig, P.

    2009-11-01

    The discovery of very high energy (VHE) gamma-ray emitting X-ray binaries has triggered an intense effort to better understand the particle acceleration, absorption, and emission mechanisms in compact binary systems, which provide variable conditions along eccentric orbits. Despite this, the nature of some of these systems, and of the accelerated particles producing the VHE emission, is unclear. To answer some of these open questions, we conducted a multiwavelength campaign of the VHE gamma-ray emitting X-ray binary LS I +61 303 including the MAGIC telescope, XMM-Newton, and Swift during 60% of an orbit in 2007 September. We detect a simultaneous outburst at X-ray and VHE bands, with the peak at phase 0.62 and a similar shape at both wavelengths. A linear fit to the simultaneous X-ray/VHE pairs obtained during the outburst yields a correlation coefficient of r = 0.97, while a linear fit to all simultaneous pairs provides r = 0.81. Since a variable absorption of the VHE emission towards the observer is not expected for the data reported here, the correlation found indicates a simultaneity in the emission processes. Assuming that they are dominated by a single particle population, either hadronic or leptonic, the X-ray/VHE flux ratio favors leptonic models. This fact, together with the detected photon indices, suggests that in LS I +61 303 the X-rays are the result of synchrotron radiation of the same electrons that produce VHE emission as a result of inverse Compton scattering of stellar photons.

  13. Experimental measurement of radiological penumbra associated with intermediate energy x-rays (1 MV) and small radiosurgery field sizes

    SciTech Connect

    Keller, Brian M.; Beachey, David J.; Pignol, Jean-Philippe

    2007-10-15

    Stereotactic radiosurgery is used to treat intracranial lesions with a high degree of accuracy. At the present time, x-ray energies at or above Co-60 gamma rays are used. Previous Monte Carlo simulations have demonstrated that intermediate energy x-ray photons or IEPs (defined to be photons in the energy range of 0.2-1.2 MeV), combined with small field sizes, produce a reduced radiological penumbra leading to a sharper dose gradient, improved dose homogeneity and sparing of critical anatomy adjacent to the target volume. This hypothesis is based on the fact that, for small x-ray fields, a dose outside the treatment volume is dictated mainly by the range of electrons set into motion by x-ray photons. The purpose of this work is: (1) to produce intermediate energy x rays using a detuned medical linear accelerator (2) to characterize the energy of this beam (3) to measure the radiological penumbra for IEPs and small fields to compare with that produced by 6 MV x rays or Co-60, and (4) to compare these experimental measurements with Monte Carlo computer simulations. The maximum photon energy of our IEP x-ray spectrum was measured to be 1.2 MeV. Gafchromic EBT films (ISP Technologies, Wayne, NJ) were irradiated and read using a novel digital microscopy imaging system with high spatial resolution. Under identical irradiation conditions the measured radiological penumbra widths (80%-20% distance), for field sizes ranging from 0.3x0.3 to 4.0x4.0 cm{sup 2}, varied from 0.3-0.77 mm (1.2 MV) and from 1.1-2.1 mm (6 MV). Even more dramatic were the differences found when comparing the 90%-10% or the 95%-5% widths, which are in fact more significant in radiotherapy. Monte Carlo simulations agreed well with the experimental findings. The reduction in radiological penumbra could be substantial for specific clinical situations such as in the treatment of an ocular melanoma abutting the macula or for the treatment of functional disorders such as trigeminal neuralgia (a nonlethal

  14. Probing the micro-mechanical behavior of bone via high-energy x-rays.

    SciTech Connect

    Almer, J.; Stock, S. R.; X-Ray Science Division; Northwestern Univ.

    2006-01-01

    the sample. While under load, high-energy x-rays (80.7 keV) of transverse size 0.05(x) x 0.05(y) mm{sup 2} were used to sample through the entire thickness (z) of the sample. Wide-angle scattering patterns at multiple x-positions (y=0) were collected using a large area detector, with each 2D pattern containing data in a plane approximately parallel to the sample x-y plane. Internal strains along the longitudinal/loading direction ({var_epsilon}{sub yy}) are shown for the apatite (002) reflection in Fig. 1. Values for five different lateral positions are shown, with x = -1 mm near the convex side of the sample and x = +1 near the concave side. Also shown are value from the strain gage located on the concave side of the specimen. All internal strains are non-zero before unloading and {var_epsilon}{sub yy} {approx} -700 {mu}{var_epsilon}. When stress is applied, strain response varies substantially across the sample, with {var_epsilon}{sub yy} (x = 1) showing the highest compression while {var_epsilon}{sub yy} (x = -1) slightly more tensile values. The macroscopic strain increases similar to, but at a higher degree than, {var_epsilon}{sub yy} (x = -1). At the maximum applied stress of {approx}33 MPa the sample experienced multiple cracks, as verified via post-mortem analysis. Upon unloading the macroscopic strain was primarily elastic, as values (nearly) returned to those seen upon loading.

  15. High Energy Laboratory Astrophysics using an X-Ray Microcalorimeter with an Electron Beam Ion Trap

    NASA Astrophysics Data System (ADS)

    Porter, Frederick

    Since the summer of 2000 we have successfully deployed a high-resolution x-ray microcalorimeter spectrometer, based on the spaceflight XRS instrument, at the Electron Beam Ion Trap (EBIT) facility at the Lawrence Livermore National Laboratory. Over the last 15 years, this highly successful partnership has made fundamental measurements in laboratory astrophysics including the measurements of the absolute cross sections of all the Fe L shell transitions from Fe XVII to Fe XXIV, line ratios in Fe and Ni L shell transitions, measurements of Fe K shell emission over a wide range of electron energies, and direct measurements of charge exchange emission from highly ionized Fe, O, N, and most recently L shell S, using a variety of donor gases. This work has resulted in the publication of over 40 peer-reviewed articles with many more either submitted or in preparation. The newest addition to the facility, the ECS microcalorimeter spectrometer, developed under this program, has performed flawlessly as a facility-class instrument since 2007. We propose here to continue our highly successful partnership and deploy new technology to resolve lines in the important 1/4 keV band that encompasses the M-shell iron emission and the L shell emission, including charge exchange, of many of the lower-Z elements, such as Si, S, Mg, Ne, Ca, and Ar. This work is highly relevant to NASA objectives as it allows for the unambiguous connection between spectroscopic observations with Chandra, XMM, Astro-H, and future spectrometers aboard missions like Athena, and the physics occurring in the cosmological source. Our program aids these measurements by benchmarking the spectroscopic synthesis models used to interpret all x-ray observations. Without laboratory measurements to support these models, it is not a priori certain that the models are correct, and the observational data correctly interpreted. This is especially true for charge exchange measurements, where there are substantially

  16. Plasma conditions for improved energy coupling into the gain region of the Ni-like Pd transient collisional x-ray laser

    SciTech Connect

    Smith, R F; Dunn, J; Filevich, J; Moon, S; Nilsen, J; Keenan, R; Shlyaptsev, V N; Rocca, J J; Hunter, J R; Marconi, M C

    2004-10-04

    We have directly probed the plasma conditions in which the Ni-like Pd transient collisional x-ray laser is generated and propagates by measuring the near-field image and by utilizing picosecond resolution soft x-ray laser interferometry of the preformed Pd plasma gain medium. The electron density and gain region of the plasma have been determined experimentally and are found to be in good agreement with simulations. We observe a strong dependence of the laser pump-gain medium coupling on the laser pump parameters. The most efficient coupling of laser pump energy into the gain region occurs with the formation of lower density gradients in the pre-formed plasma and when the duration of the main heating pulse is comparable to the gain lifetime ({approx}10ps for mid-Z Ni-like schemes). This increases the output intensity by more than an order of magnitude relative to the commonly utilized case where the same pumping energy is delivered within a shorter heating pulse duration (< 3ps). In contrast, the higher intensity heating pulses are observed to be absorbed at higher electron densities and in regions where steep density gradients limit the effective length of the gain medium.

  17. Hard X-Ray Emission of X-Ray Bursters

    NASA Technical Reports Server (NTRS)

    Kaaret, P.

    1999-01-01

    The primary goal of this proposal was to perform an accurate measurement of the broadband x-ray spectrum of a neutron-star low-mass x-ray binary found in a hard x-ray state. This goal was accomplished using data obtained under another proposal, which has provided exciting new information on the hard x-ray emission of neutron-star low-mass x-ray binaries. In "BeppoSAX Observations of the Atoll X-Ray Binary 4U0614+091", we present our analysis of the spectrum of 4U0614+091 over the energy band from 0.3-150 keV. Our data confirm the presence of a hard x-ray tail that can be modeled as thermal Comptonization of low-energy photons on electrons having a very high temperature, greater than 220 keV, or as a non-thermal powerlaw. Such a very hard x-ray spectrum has not been previously seen from neutron-star low-mass x-ray binaries. We also detected a spectral feature that can be interpreted as reprocessing, via Compton reflection, of the direct emission by an optically-thick disk and found a correlation between the photon index of the power-law tail and the fraction of radiation reflected which is similar to the correlation found for black hole candidate x-ray binaries and Seyfert galaxies. A secondary goal was to measure the timing properties of the x-ray emission from neutronstar low-mass x-ray binaries in their low/hard states.

  18. Chemical versus dual energy x-ray absorptiometry for detecting age-associated body compositional changes in male rats☆

    PubMed Central

    Feely, Rebecca. S.; Larkin, Lisa M.; Halter, Jeffrey B.; Dengel, Donald R.

    2009-01-01

    Aging is associated with increases in body mass and fat mass (FM), whereas fat-free mass (FFM) either decreases or remains unchanged. The purpose of this study was to determine whether dual-energy X-ray absorptiometry (DXA) accurately detects age-associated changes in male Fischer 344 × Brown–Norway rats ages 8, 18, and 28 months. Eviscerated animal carcasses were first examined via the Lunar DPX-IQ DXA (small animal software version 1.0; HiRes (0.6 × 1.2 mm) medium mode). Eviscerated carcasses were then weighed, autoclaved, homogenized, and fat isolated from aliquots of homogenate via methanol/chloroform extraction. In both chemical (CHEM) and DXA analysis, carcass mass (CM), FM, and % fat were significantly higher (P < 0.0001) in the 18 and 28 versus 8-month-old rats. CHEM showed greater FFM in the 18 versus 8 months-old rats but not the 28 months-old animals. DXA was unable to detect the age-associated changes in FFM. Regression analysis showed a strong correlation between CHEM and DXA methods for CM (r = 0.98, P < 0.0001) and FM (r = 0.97, P < 0.0001), but less strong for FFM (r = 0.59, P = 0.0002). In conclusion, compared to CHEM, DXA consistently overestimated CM and FM across the age groups by 9% and 77%, respectively, and underestimated FFM by 5%. PMID:10832061

  19. An energy dispersive x-ray scattering and molecular dynamics study of liquid dimethyl carbonate

    NASA Astrophysics Data System (ADS)

    Gontrani, Lorenzo; Russina, Olga; Marincola, Flaminia Cesare; Caminiti, Ruggero

    2009-12-01

    In this work, we report on the first x-ray diffraction study on liquid dimethyl carbonate. Diffraction spectra were collected with an energy-dispersive instrument, whose wide Q-range allows the structure determination of weakly ordered systems (such as liquids). The structural correlation in this liquid ranges up to about 20 Å. The observed patterns are interpreted with a structural model derived from classical molecular dynamics simulations. The simulations were run using OPLS force field, only slightly modified to restrain bond distances to the experimental values. The model structure function and radial distribution functions, averaged among the productive trajectory frames, are in very good agreement with the corresponding experimental ones. Molecular dynamics results show that the deviations from C2v cis-cis structure, predicted by ab initio calculations and observed by electron diffraction in the gas phase, are small. By analyzing the intra- and intermolecular pair distribution functions, it was possible to assign the peaks of the experimental radial distribution function to specific structural correlations, and to compute the different average intermolecular coordination numbers. The intermolecular methyl-carbonyl oxygen distance is thoroughly discussed to assess the presence of weak C-H⋯ṡO hydrogen bonds.

  20. High temperature monitoring of silicon carbide ceramics by confocal energy dispersive X-ray fluorescence spectrometry

    NASA Astrophysics Data System (ADS)

    Li, Fangzuo; Liu, Zhiguo; Sun, Tianxi

    2016-04-01

    In the present work, we presented an alternative method for monitoring of the oxidation situation of silicon carbide (SiC) ceramics at various high temperatures in air by measuring the Compton-to-Rayleigh intensity ratios (ICo/IRa) and effective atomic numbers (Zeff) of SiC ceramics with the confocal energy dispersive X-ray fluorescence (EDXRF) spectrometer. A calibration curve of the relationship between ICo/IRa and Zeff was established by using a set of 8 SiC calibration samples. The sensitivity of this approach is so high that it can be easily distinguished samples of Zeff differing from each other by only 0.01. The linear relationship between the variation of Zeff and the variations of contents of C, Si and O of SiC ceramics were found, and the corresponding calculation model of the relationship between the ΔZ and the ΔCC, ΔCSi, and ΔCO were established. The variation of contents of components of the tested SiC ceramics after oxidation at high temperature was quantitatively calculated based on the model. It was shown that the results of contents of carbon, silicon and oxygen obtained by this method were in good agreement with the results obtained by XPS, giving values of relative deviation less than 1%. It was concluded that the practicality of this proposed method for monitoring of the oxidation situation of SiC ceramics at high temperatures was acceptable.

  1. Edge multi-energy soft x-ray diagnostic in Experimental Advanced Superconducting Tokamak

    SciTech Connect

    Li, Y. L.; Xu, G. S.; Wan, B. N.; Lan, H.; Liu, Y. L.; Wei, J.; Zhang, W.; Hu, G. H.; Wang, H. Q.; Duan, Y. M.; Zhao, J. L.; Wang, L.; Liu, S. C.; Ye, Y.; Li, J.; Lin, X.; Li, X. L.; Tritz, K.; Zhu, Y. B.

    2015-12-15

    A multi-energy soft x-ray (ME-SXR) diagnostic has been built for electron temperature profile in the edge plasma region in Experimental Advanced Superconducting Tokamak (EAST) after two rounds of campaigns. Originally, five preamplifiers were mounted inside the EAST vacuum vessel chamber attached to five vertically stacked compact diode arrays. A custom mechanical structure was designed to protect the detectors and electronics under constraints of the tangential field of view for plasma edge and the allocation of space. In the next experiment, the mechanical structure was redesigned with a barrel structure to absolutely isolate it from the vacuum vessel. Multiple shielding structures were mounted at the pinhole head to protect the metal foils from lithium coating. The pre-amplifiers were moved to the outside of the vacuum chamber to avoid introducing interference. Twisted copper cooling tube was embedded into the back-shell near the diode to limit the temperature of the preamplifiers and diode arrays during vacuum vessel baking when the temperature reached 150 °C. Electron temperature profiles were reconstructed from ME-SXR measurements using neural networks.

  2. Comparison of the Bod Pod and dual energy x-ray absorptiometry in men.

    PubMed

    Ball, Stephen D; Altena, Thomas S

    2004-06-01

    The majority of studies investigating the accuracy of the Bod Pod have compared it to hydrostatic weighing (HW), the long held, and perhaps outdated 'gold standard' method of body composition analysis. Much less research has compared the Bod Pod to dual energy x-ray absorptiometry (DXA), a technique that is becoming popular as an alternative reference method. The purpose of this study was to compare per cent fat estimates by the Bod Pod to those of DXA in a large number of men. Participants were 160 men (32 +/- 11 years). Per cent body fat was estimated to be 19.4 +/- 6.8 and 21.6 +/- 8.4 for DXA and the Bod Pod, respectively. Although the two methods were highly correlated (0.94), the mean difference of 2.2% was significant (p < 0.01). The amount of difference increased as body fatness increased (p < 0.0001). The results of this study indicate that a difference between methods existed for our sample of men. It is uncertain exactly where the difference lies. Practitioners should be aware that even with the use of technologically sophisticated methods (i.e., Bod Pod, DXA), differences between methods exist and the determination of body composition is at best, an estimation.

  3. Micro energy-dispersive x-ray fluorescence spectrometry study of dentin coating with nanobiomaterials

    NASA Astrophysics Data System (ADS)

    Soares, Luís. Eduardo Silva; Nahorny, Sídnei; Marciano, Fernanda Roberta; Zanin, Hudson; Lobo, Anderson de Oliveira

    2015-06-01

    New biomaterials such as multi-walled carbon nanotubes oxide/graphene oxide (MWCNTO/GO), nanohydroxyapatite (nHAp) and combination of them together or not to acidulated phosphate fluoride gel (F) have been tested as protective coating before root dentin erosion. Fourteen bovine teeth were cleaned, polished, divided into two parts (n=28) and assigned to seven groups: (Control) - without previous surface treatment; F treatment; nHAp; MWCNTO/GO; F+nHAp; F+MWCNTO/GO and F+MWCNTO/GO/nHAp composites. Each sample had two sites of pre-treatments: acid etched area and an area without treatment. After the biomaterials application, the samples were submitted to six cycles (demineralization: orange juice, 10 min; remineralization: artificial saliva, 1 h). Micro energy-dispersive X-ray fluorescence spectrometry (μ-EDXRF) mapping area analyses were performed after erosive cycling on both sites (n=84). μ-EDXRF mappings showed that artificial saliva and MWCNTO/GO/nHAp/F composite treatments produced lower dentin demineralization than in the other groups. Exposed dentin tubules allowed better interaction of nanobiomaterials than in smear layer covered dentin. Association of fluoride with other biomaterials had a positive influence on acid etched dentin. MWCNTO/GO/nHAp/F composite treatment resulted in levels of demineralization similar to the control group.

  4. Determination of actinide speciation in solution using high-energy X-ray scattering.

    PubMed

    Soderholm, L; Skanthakumar, S; Neuefeind, J

    2005-09-01

    High-energy X-ray scattering (HEXS) has been used to understand the coordination environment of the uranyl ion in a perchlorate solution. Assuming the two coordinating oxo ligands bound to U(VI) are represented in a peak in the pair distribution function (PDF) at 1.766(1) A, integration of the peak intensity is used to quantify the charge located on the oxygens. The dioxo ligands are essentially neutral, as predicted by numerous published calculations, with a charge of -16.4(8) electrons. The peak in the PDF at 2.420(1) A is consistent with equatorial ligating waters. The intensity of this peak is inconsistent with an integral coordination number and is used to propose a solution equilibrium of five and four waters coordinating to the uranyl(VI) ion favoring the five-coordinate species. This equilibrium is then used to experimentally determine that five-coordinate uranyl is 1.19+/-0.42 kcal/mol more stable than its four-coordinate counterpart under the conditions of the experiment. Further peaks in the Fourier transform of the scattering data at 4.50, 7, and 8.7 A are attributed to uranium-solvent correlations.

  5. Edge multi-energy soft x-ray diagnostic in Experimental Advanced Superconducting Tokamak

    NASA Astrophysics Data System (ADS)

    Li, Y. L.; Xu, G. S.; Tritz, K.; Zhu, Y. B.; Wan, B. N.; Lan, H.; Liu, Y. L.; Wei, J.; Zhang, W.; Hu, G. H.; Wang, H. Q.; Duan, Y. M.; Zhao, J. L.; Wang, L.; Liu, S. C.; Ye, Y.; Li, J.; Lin, X.; Li, X. L.

    2015-12-01

    A multi-energy soft x-ray (ME-SXR) diagnostic has been built for electron temperature profile in the edge plasma region in Experimental Advanced Superconducting Tokamak (EAST) after two rounds of campaigns. Originally, five preamplifiers were mounted inside the EAST vacuum vessel chamber attached to five vertically stacked compact diode arrays. A custom mechanical structure was designed to protect the detectors and electronics under constraints of the tangential field of view for plasma edge and the allocation of space. In the next experiment, the mechanical structure was redesigned with a barrel structure to absolutely isolate it from the vacuum vessel. Multiple shielding structures were mounted at the pinhole head to protect the metal foils from lithium coating. The pre-amplifiers were moved to the outside of the vacuum chamber to avoid introducing interference. Twisted copper cooling tube was embedded into the back-shell near the diode to limit the temperature of the preamplifiers and diode arrays during vacuum vessel baking when the temperature reached 150 °C. Electron temperature profiles were reconstructed from ME-SXR measurements using neural networks.

  6. On the variation of solar flare coronal X-ray source sizes with energy

    SciTech Connect

    Jeffrey, Natasha L. S.; Kontar, Eduard P.; Bian, Nicolas H.; Emslie, A. Gordon

    2014-05-20

    Observations with RHESSI have enabled the detailed study of the structure of dense hard X-ray coronal sources in solar flares. The variation of source extent with electron energy has been discussed in the context of streaming of non-thermal particles in a one-dimensional cold target model and the results used to constrain both the physical extent of, and density within, the electron acceleration region. Here, we extend this investigation to a more physically realistic model of electron transport that takes into account the finite temperature of the ambient plasma, the initial pitch angle distribution of the accelerated electrons, and the effects of collisional pitch angle scattering. The finite temperature results in the thermal diffusion of electrons, which leads to the observationally inferred value of the acceleration region volume being an overestimate of its true value. The different directions of the electron trajectories, a consequence of both the non-zero injection pitch angle and scattering within the target, cause the projected propagation distance parallel to the guiding magnetic field to be reduced, so that a one-dimensional interpretation can overestimate the actual density by a factor of up to ∼6. The implications of these results for the determination of acceleration region properties (specific acceleration rate, filling factor, etc.) are discussed.

  7. Elemental analysis of mining wastes by energy dispersive X-ray fluorescence (EDXRF)

    NASA Astrophysics Data System (ADS)

    Gonzalez-Fernandez, O.; Queralt, I.; Carvalho, M. L.; Garcia, G.

    2007-08-01

    An energy dispersive X-ray fluorescence (EDXRF) tri-axial geometry experimental spectrometer has been employed to determine the concentrations of 13 different elements (K, Ca, Ti, Cr, Mn, Fe, Co, Ni, Cu, Zn, Rb, Sr and Pb) in mine wastes from different depths of two mine tailings from the Cartagena-La Union (Spain) mining district. The elements were determined and quantified using the fundamental parameters method. The concentrations of Cr, Ni, Cu, Zn and Pb were compared to the values from the European and Spanish legislation to evaluate the environmental risk and to classify the wastes as inert wastes or as wastes that have to be control land-filled. The results obtained demonstrate that these wastes can be considered as inert for the considered elements, apart from the concentration levels of Zn and Pb. Whilst Zn slightly overpasses the regulatory levels, Pb mean value exceeds three to six times the value to be considered as Class I potential land-filling material.

  8. Edge multi-energy soft x-ray diagnostic in Experimental Advanced Superconducting Tokamak.

    PubMed

    Li, Y L; Xu, G S; Tritz, K; Zhu, Y B; Wan, B N; Lan, H; Liu, Y L; Wei, J; Zhang, W; Hu, G H; Wang, H Q; Duan, Y M; Zhao, J L; Wang, L; Liu, S C; Ye, Y; Li, J; Lin, X; Li, X L

    2015-12-01

    A multi-energy soft x-ray (ME-SXR) diagnostic has been built for electron temperature profile in the edge plasma region in Experimental Advanced Superconducting Tokamak (EAST) after two rounds of campaigns. Originally, five preamplifiers were mounted inside the EAST vacuum vessel chamber attached to five vertically stacked compact diode arrays. A custom mechanical structure was designed to protect the detectors and electronics under constraints of the tangential field of view for plasma edge and the allocation of space. In the next experiment, the mechanical structure was redesigned with a barrel structure to absolutely isolate it from the vacuum vessel. Multiple shielding structures were mounted at the pinhole head to protect the metal foils from lithium coating. The pre-amplifiers were moved to the outside of the vacuum chamber to avoid introducing interference. Twisted copper cooling tube was embedded into the back-shell near the diode to limit the temperature of the preamplifiers and diode arrays during vacuum vessel baking when the temperature reached 150 °C. Electron temperature profiles were reconstructed from ME-SXR measurements using neural networks.

  9. Low-energy X-ray fluorescence microscopy opening new opportunities for bio-related research

    PubMed Central

    Kaulich, Burkhard; Gianoncelli, Alessandra; Beran, Alfred; Eichert, Diane; Kreft, Ivan; Pongrac, Paula; Regvar, Marjana; Vogel-Mikuš, Katarina; Kiskinova, Maya

    2009-01-01

    Biological systems are unique matter with very complex morphology and highly heterogeneous chemical composition dominated by light elements. Discriminating qualitatively at the sub-micrometer level the lateral distribution of constituent elements, and correlating it to the sub-cellular biological structure, continues to be a challenge. The low-energy X-ray fluorescence microspectroscopy, recently implemented in TwinMic scanning transmission mode, has opened up new opportunities for mapping the distribution of the light elements, complemented by morphology information provided by simultaneous acquisition of absorption and phase contrast images. The important new information that can be obtained in bio-related research domains is demonstrated by two pilot experiments with specimens of interest for marine biology and food science. They demonstrate the potential to yield important insights into the structural and compositional enrichment, distribution and correlation of essential trace elements in the lorica of Tintinnopsis radix, and the lateral distribution of trace nutrients in the seeds of wheat Triticum aestivum. PMID:19570794

  10. X-ray energy flow and radiography measurements of evolving density perturbations

    NASA Astrophysics Data System (ADS)

    Moore, A. S.; Graham, P.; Taylor, M. J.; Foster, J. M.; Sorce, C.; Reighard, A.; MacLaren, S.; Young, P.; Glendinning, G.; Blue, B. E.; Back, C. A.; Hund, J.

    2008-11-01

    X-radiation transport through plasma density gradients, such as N-waves, form a closely coupled system that is challenging to simulate. Such situations are a key component of the physics of laser-heated hohlraums occurring in the laser-heated cavity and also in the laser-entry and any diagnostic holes. In addition the similarity to some astrophysical conditions may mean that such experiments can be used as a laboratory-scale analogue for their investigation. To better understand these phenomena, we present results from a series of experiments performed at the Omega laser facility. Using a laser-heated hohlraum drive, a tantalum aerogel with an initial seed perturbation is heated, and x-rays initially free-stream through the perturbation before they fill with plasma and radiation transport becomes diffuse. We present energy flux measurements diagnosed using two different methods, and complementary radiography results that achieve sufficient contrast, despite the high background of the hohlraum, to enable the complex shock interactions and stagnation to be directly observed. These results are compared with simulations performed using a 2-D Eulerian hydrocode, which are able to reproduce the overall energetics, and much of the details of the deceleration shock and axial stagnation region at the centre of the slit.

  11. Advances in the detection of as in environmental samples using low energy X-ray fluorescence in a scanning transmission X-ray microscope: arsenic immobilization by an Fe(II)-oxidizing freshwater bacteria.

    PubMed

    Hitchcock, A P; Obst, M; Wang, J; Lu, Y S; Tyliszczak, T

    2012-03-01

    Speciation and quantitative mapping of elements, organic and inorganic compounds, and mineral phases in environmental samples at high spatial resolution is needed in many areas of geobiochemistry and environmental science. Scanning transmission X-ray microscopes (STXMs) provide a focused beam which can interrogate samples at a fine spatial scale. Quantitative chemical information can be extracted using the transmitted and energy-resolved X-ray fluorescence channels simultaneously. Here we compare the relative merits of transmission and low-energy X-ray fluorescence detection of X-ray absorption for speciation and quantitative analysis of the spatial distribution of arsenic(V) within cell-mineral aggregates formed by Acidovorax sp. strain BoFeN1, an anaerobic nitrate-reducing Fe(II)-oxidizing β-proteobacteria isolated from the sediments of Lake Constance. This species is noted to be highly tolerant to high levels of As(V). Related, As-tolerant Acidovorax-strains have been found in As-contaminated groundwater wells in Bangladesh and Cambodia wherein they might influence the mobility of As by providing sorption sites which might have different properties as compared to chemically formed Fe-minerals. In addition to demonstrating the lower detection limits that are achieved with X-ray fluorescence relative to transmission detection in STXM, this study helps to gain insights into the mechanisms of As immobilization by biogenic Fe-mineral formation and to further the understanding of As-resistance of anaerobic Fe(II)-oxidizing bacteria.

  12. Polycrystalline lead iodide films produced by solution evaporation and tested in the mammography X-ray energy range

    NASA Astrophysics Data System (ADS)

    Condeles, J. F.; Mulato, M.

    2016-02-01

    Lead iodide polycrystalline films have been deposited on corning glass substrates using solution evaporation in oven. Films 6 μm-thick were obtained with full coverage of the substrates as verified by scanning electron microscopy. Some pin-holes were observable. X-ray diffraction revealed a crystalline structure corresponding to the 4 H-PbI2 polytype formation. Polarized Raman scattering experiments indicated a lamellar structure. Anisotropy was also investigated using depolarization ratio calculations. The optical and electrical properties of the samples were investigated using photoluminescence and dark conductivity as a function of temperature, respectively. Activation energies of 0.10 up to 0.89 eV were related to two main electrical transport mechanisms. Films were also exposed to X-ray irradiation in the mammography X-ray energy range. The detector produced was also exposed to X-ray from 5 mR up to 1450 mR. A linear response was observed as a function of dose with a slope of 0.52 nA/mm2 per mR.

  13. Synchrotron x-ray high energy PDF and tomography studies for gallium melts under high-pressure conditions

    NASA Astrophysics Data System (ADS)

    Liu, H.; Liu, L. L.; Li, R.; Li, L.

    2015-12-01

    Liquid gallium exhibits unusual and unique physical properties. A rich polymorphism and metastable modifications of solid Ga have been discovered and a number of studies of liquid gallium under high pressure conditions were reported. However, some fundamental properties, such as the equation of state (EoS) of Ga melt under extreme conditions remain unclear. To compare to the previous reports, we performed the pair distribution function (PDF) study using diamond anvil cell, in which synchrotron high-energy x-ray total scattering data, combined with reverse Monte Carlo simulation, was used to study the microstructure and EoS of liquid gallium under high pressure at room temperature conditions. The EoS of Ga melt, which was measured from synchrotron x-ray tomography method at room temperature, was used to avoid the potential relatively big errors for the density estimation from the reverse Monte Carlo simulation with the mathematical fit to the measured structure factor data. The volume change of liquid gallium have been studied as a function of pressure and temperature up to 5 GPa at 370 K using synchrotron x-ray microtomography combined with energy dispersive x-ray diffraction (EDXRD) techniques using Drickamer press. The directly measured P-V-T curves were obtained from 3D tomography reconstruction data. The existence of possible liquid-liquid phase transition regions is proposed based on the abnormal compressibility and local structure change in Ga melts.

  14. AN EXPLANATION FOR THE DIFFERENT X-RAY TO OPTICAL COLUMN DENSITIES IN THE ENVIRONMENTS OF GAMMA RAY BURSTS: A PROGENITOR EMBEDDED IN A DENSE MEDIUM

    SciTech Connect

    Krongold, Yair; Prochaska, J. Xavier

    2013-09-10

    We study the {approx}> 10 ratios in the X-ray to optical column densities inferred from afterglow spectra of gamma ray bursts (GRBs) due to gas surrounding their progenitors. We present time-evolving photoionization calculations for these afterglows and explore different conditions of their environment. We find that homogenous models of the environment (constant density) predict X-ray columns similar to those found in the optical spectra, with the bulk of the opacity being produced by neutral material at large distances from the burst. This result is independent of gas density or metallicity. Only models assuming a progenitor immersed in a dense ({approx}10{sup 2-4} cm{sup -3}) cloud of gas (with radius {approx}10 pc), with a strong, declining gradient of density for the surrounding interstellar medium (ISM) are able to account for the large X-ray to optical column density ratios. However, to avoid an unphysical correlation between the size of this cloud and the size of the ionization front produced by the GRB, the models also require that the circumburst medium is already ionized prior to the burst. The inferred cloud masses are {approx}< 10{sup 6} M{sub Sun }, even if low metallicities in the medium are assumed (Z {approx} 0.1 Z{sub Sun }). These cloud properties are consistent with those found in giant molecular clouds and our results support a scenario in which the progenitors reside within intense star formation regions of galaxies. Finally, we show that modeling over large samples of GRB afterglows may offer strong constraints on the range of properties in these clouds, and the host galaxy ISM.

  15. Solar X-ray physics

    SciTech Connect

    Bornmann, P.L. )

    1991-01-01

    Research on solar X-ray phenomena performed by American scientists during 1987-1990 is reviewed. Major topics discussed include solar images observed during quiescent times, the processes observed during solar flares, and the coronal, interplanetary, and terrestrial phenomena associated with solar X-ray flares. Particular attention is given to the hard X-ray emission observed at the start of the flare, the energy transfer to the soft X-ray emitting plasma, the late resolution of the flare as observed in soft X-ray, and the rate of occurrence of solar flares as a function of time and latitude. Pertinent aspects of nonflaring, coronal X-ray emission and stellar flares are also discussed. 175 refs.

  16. Miniature x-ray source

    DOEpatents

    Trebes, James E.; Stone, Gary F.; Bell, Perry M.; Robinson, Ronald B.; Chornenky, Victor I.

    2002-01-01

    A miniature x-ray source capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature x-ray source comprises a compact vacuum tube assembly containing a cathode, an anode, a high voltage feedthru for delivering high voltage to the anode, a getter for maintaining high vacuum, a connection for an initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is highly x-ray transparent and made, for example, from boron nitride. The compact size and potential for remote operation allows the x-ray source, for example, to be placed adjacent to a material sample undergoing analysis or in proximity to the region to be treated for medical applications.

  17. YIELDS OF IONS AND EXCITED STATES IN NONPOLAR LIQUIDS EXPOSED TO X-RAYS OF 1 TO 30 KEV ENERGY

    SciTech Connect

    HOLROYD,R.A.

    1999-08-18

    When x-rays from a synchrotron source are absorbed in a liquid, the x-ray energy (E{sub x}) is converted by the photoelectric effect into the kinetic energy of the electrons released. For hydrocarbons, absorption by the K-electrons of carbon dominates. Thus the energy of the photoelectron (E{sub pe}) is E{sub x}-E{sub b}, where E{sub b} is the K-shell binding energy of carbon. Additional electrons with energy equal to E{sub b} is released in the Auger process that fills the hole in the K-shell. These energetic electrons will produce many ionizations, excitations and products. The consequences of the high density of ionizations and excitations along the track of the photoelectron and special effects near the K-edge are examined here.

  18. DETERMINING NEUTRON STAR MASSES AND RADII USING ENERGY-RESOLVED WAVEFORMS OF X-RAY BURST OSCILLATIONS

    SciTech Connect

    Lo, Ka Ho; Lamb, Frederick K.; Miller, M. Coleman; Bhattacharyya, Sudip

    2013-10-10

    Simultaneous, precise measurements of the mass M and radius R of neutron stars can yield uniquely valuable information about the still uncertain properties of cold matter at several times the density of nuclear matter. One method that could be used to measure M and R is to analyze the energy-dependent waveforms of the X-ray flux oscillations seen during some thermonuclear bursts from some neutron stars. These oscillations are thought to be produced by X-ray emission from hotter regions on the surface of the star that are rotating at or near the spin frequency of the star. Here we explore how well M and R could be determined by generating and analyzing, using Bayesian techniques, synthetic energy-resolved X-ray data that we produce assuming a future space mission having 2-30 keV energy coverage and an effective area of 10 m{sup 2}, such as the proposed Large Observatory for X-Ray Timing or Advanced X-Ray Timing Array missions. We find that waveforms from hot spots within 10° of the rotation equator usually constrain both M and R with an uncertainty of about 10%, if there are 10{sup 6} total counts from the spot, whereas waveforms from spots within 20° of the rotation pole provide no useful constraints. The constraints we report can usually be achieved even if the burst oscillations vary with time and data from multiple bursts must be used to obtain 10{sup 6} counts from the hot spot. This is therefore a promising method to constrain M and R tightly enough to discriminate strongly between competing models of cold, high-density matter.

  19. An experimental investigation on reduced radiological penumbra for intermediate energy x-rays: Implications for small field radiosurgery

    NASA Astrophysics Data System (ADS)

    Keller, Brian Michael

    Current day external beam radiation therapy typically uses x-ray energies in the megavoltage (6--18 MV) or in the superficial/orthovoltage (80--350 kVp) energy ranges. It has been found that intermediate energy x-rays (those greater than orthovoltage but sub-megavoltage) may offer an advantage in the field of high precision radiation therapy such as in radiosurgery. This advantage is a reduction in the radiological penumbra associated with small (less than about 3 cm) radiation dose fields. A consequence of reduced radiological penumbra is a more homogenous, conformal dose distribution in the patient with dose escalation and organ sparing made more feasible. The objectives of this thesis were as follows: to produce and to characterize an intermediate energy x-ray beam, to establish a method of accurate penumbra measurement at the micron level for millimeter size fields, to measure the radiological penumbra of single small intermediate energy x-ray fields, and to show the clinical consequences of a multiple beam irradiation in a stereotactic head phantom. A maximum photon energy of 1.2 +/- 0.1 MeV was determined for the intermediate energy x-ray spectrum at the expense of a low dose rate. A digital microscope with a computer controlled translation stage was investigated for its ability to resolve steep dose gradients in Gafchromic EBT film for field sizes as small as 1 mm and for photon energies as low as 100 kVp. The microscope-film system resolved gradients to within about 30 mum, limited by the inherent spatial resolution of the film, the noise of the system, and the uncertainties of measurement. Penumbra widths were compared for 1.2 MV versus 6 MV for identical irradiation conditions. In some instances, there was a five-fold reduction in the radiological penumbra of single 1.2 MV x-ray beams. A multiple beam arc irradiation demonstrated that the advantages seen with single beams carry over to multiple beams. The benefits of reduced radiological penumbra for

  20. Use of oily contrast medium for selective drug targeting to tumor: enhanced therapeutic effect and X-ray image

    SciTech Connect

    Iwai, K.; Maeda, H.; Konno, T.

    1984-05-01

    Highly malignant rabbit tumor (VX-2) was implanted in the liver in 63 rabbits. Selective delivery of the anticancer agent copoly(styrenemaleic acid) conjugated to neocarzinostatin (SMANCS) was performed by injection via the proper hepatic artery. By using low-kVp X-ray examination of the resected liver, Lipiodol was found to distribute through the entire liver arterial lumina and was retained for about 24 hr, but disappeared gradually. However, Lipiodol was retained in the tumor tissue and vessels for at least 7 days. A radioactive analogue of Lipiodol, was prepared by using (/sup 14/C)linoleic acid. This analogue was used in the study of the distribution by low-kVp X-ray examination, Sudan III staining, and autoradiography. Lipiodol remained in the tumor vessels as well as the tumor cells. The use of the radioisotope yielded a quantitative profile of Lipiodol accumulation in tumor tissues. Its major excretion route appeared to be through the bile. The biological activity of SMANCS was also determined in both tumor and liver, no activity was found in other organs. The relatively high biological activity of SMANCS in the nontumorous liver adjacent to the tumor may be the result of continuous drug release from SMANCS-Lipiodol in the tumor tissue.

  1. A Variable-Energy Soft X-Ray Microprobe to Investigate Mechanisms of the Radiation-Induced Bystander Effect.

    SciTech Connect

    Folkard, Melvyn; Vojnovic, Borivoj; Schettino, Giuseppe; Atkinson, Kirk; Prise, Kevin, M.; Michael, Barry, D.

    2007-01-23

    The Gray Cancer Institute has pioneered the use of X ray focussing techniques to develop systems for micro irradiating individual cells and sub cellular targets in vitro. Cellular micro irradiation is now recognised as a highly versatile technique for understanding how ionising radiation interacts with living cells and tissues. The strength of the technique lies in its ability to deliver precise doses of radiation to selected individual cells (or sub cellular targets). The application of this technique in the field of radiation biology continues to be of great interest for investigating a number of phenomena currently of concern to the radiobiological community. One important phenomenon is the so called ‘bystander effect’ where it is observed that unirradiated cells can also respond to signals transmitted by irradiated neighbours. Clearly, the ability of a microbeam to irradiate just a single cell or selected cells within a population is well suited to studying this effect. Our prototype ‘tabletop’ X-ray microprobe was optimised for focusing 278 eV C-K X rays and has been used successfully for a number of years. However, we have sought to develop a new variable energy soft X-ray microprobe capable of delivering focused CK (0.28 keV), Al-K (1.48 keV) and notably, Ti-K (4.5 keV) X rays. Ti-K X rays are capable of penetrating several cell layers and are therefore much better suited to studies involving tissues and multi cellular layers. In our new design, X-rays are generated by the focussed electron bombardment of a material whose characteristic-K radiation is required. The source is mounted on a 1.5 x 1.0 metre optical table. Electrons are generated by a custom built gun, designed to operate up to 15 kV. The electrons are focused using a permanent neodymium iron boron magnet assembly. Focusing is achieved by adjusting the accelerating voltage and by fine tuning the target position via a vacuum position feedthrough. To analyze the electron beam properties, a

  2. A dual-energy medical instrument for measurement of x-ray source voltage and dose rate

    NASA Astrophysics Data System (ADS)

    Ryzhikov, V. D.; Naydenov, S. V.; Volkov, V. G.; Opolonin, O. D.; Makhota, S.; Pochet, T.; Smith, C. F.

    2016-03-01

    An original dual-energy detector and medical instrument have been developed to measure the output voltages and dose rates of X-ray sources. Theoretical and experimental studies were carried out to characterize the parameters of a new scintillator-photodiode sandwich-detector based on specially-prepared zinc selenide crystals in which the low-energy detector (LED) works both as the detector of the low-energy radiation and as an absorption filter allowing the highenergy fraction of the radiation to pass through to the high-energy detector (HED). The use of the LED as a low-energy filter in combination with a separate HED opens broad possibilities for such sandwich structures. In particular, it becomes possible to analyze and process the sum, difference and ratio of signals coming from these detectors, ensuring a broad (up to 106) measurement range of X-ray intensity from the source and a leveling of the energy dependence. We have chosen an optimum design of the detector and the geometry of the component LED and HED parts that allow energy-dependence leveling to within specified limits. The deviation in energy dependence of the detector does not exceed about 5% in the energy range from 30 to 120 keV. The developed detector and instrument allow contactless measurement of the anode voltage of an X-ray emitter from 40 to 140 kV with an error no greater than 3%. The dose rate measurement range is from 1 to 200 R/min. An original medical instrument has passed clinical testing and was recommended for use in medical institutions for X-ray diagnostics.

  3. Soft X-Ray Emission in the Water Window Region with Nitrogen Filling in a Low Energy Plasma Focus

    NASA Astrophysics Data System (ADS)

    Akel, M.; Lee, S.

    2013-02-01

    For operation of the plasma focus in nitrogen, a focus pinch compression temperature range of 74-173 eV (0.86 × 106-2 × 106 K) is found to be suitable for good yield of nitrogen soft X-rays in the water window region. Using this temperature window, numerical experiments using five phase Lee model have been investigated on UNU/ICTP PFF and APF plasma focus devices with nitrogen filling gas. The Lee model was applied to characterize and optimize these two plasma focus devices. The optimum nitrogen soft X-ray yield was found to be Ysxr = 2.73 J, with the corresponding efficiency of 0.13 % for UNU/ICTP PFF device, while for APF device it was Ysxr = 4.84 J, with the corresponding efficiency of 0.19 % without changing the capacitor bank, merely by changing the electrode configuration and operating pressure. The Lee model code was also used to run numerical experiments for optimizing soft X-ray yield with reducing L0, varying z0 and `a'. From these numerical experiments we expect to increase the nitrogen soft X-ray yield of low energy plasma focus devices to maximum value of near 8 J, with the corresponding efficiency of 0.4 %, at an achievable L0 = 10 nH.

  4. Spectral response calibrations of x-ray diode photocathodes in the 50-5900 eV photon energy region

    NASA Astrophysics Data System (ADS)

    Bentley, C. D.; Simmons, A. C.

    2001-01-01

    X-ray diode photocathodes are employed in diagnostic instruments on the Helen laser at the Atomic Weapons Establishment (AWE) Aldermaston, UK. The photocathodes are mainly used in the Dante fast diode array and flat response diodes. These diagnostics enable the soft x-ray spectral emissions of laser irradiated targets to be determined. To derive quantitative spectral information, the quantum efficiency of the photocathodes must be known over the range of x-ray energies of interest. The photocathodes were manufactured in 1982, and were initially calibrated at that time. Since then further measurements have been performed in 1988 and 1999. The photocathodes have been exposed to a wide range of conditions during their lives, ranging from use in experiments to storage in a dry nitrogen environment. Reported here are the results of calibrations performed in 1999 at the soft x-ray calibration facility EXCALIBUR at AWE, Aldermaston, and at the National Synchrotron Light Source in Brookhaven NY. An assessment of their current condition and an evaluation of the change in their response over time, and the possible reasons for these changes, are made.

  5. Hard X-Ray Flare Source Sizes Measured with the Ramaty High Energy Solar Spectroscopic Imager

    NASA Technical Reports Server (NTRS)

    Dennis, Brian R.; Pernak, Rick L.

    2009-01-01

    Ramaty High Energy Solar Spectroscopic Imager (RHESSI) observations of 18 double hard X-ray sources seen at energies above 25 keV are analyzed to determine the spatial extent of the most compact structures evident in each case. The following four image reconstruction algorithms were used: Clean, Pixon, and two routines using visibilities maximum entropy and forward fit (VFF). All have been adapted for this study to optimize their ability to provide reliable estimates of the sizes of the more compact sources. The source fluxes, sizes, and morphologies obtained with each method are cross-correlated and the similarities and disagreements are discussed. The full width at half-maximum (FWHM) of the major axes of the sources with assumed elliptical Gaussian shapes are generally well correlated between the four image reconstruction routines and vary between the RHESSI resolution limit of approximately 2" up to approximately 20" with most below 10". The FWHM of the minor axes are generally at or just above the RHESSI limit and hence should be considered as unresolved in most cases. The orientation angles of the elliptical sources are also well correlated. These results suggest that the elongated sources are generally aligned along a flare ribbon with the minor axis perpendicular to the ribbon. This is verified for the one flare in our list with coincident Transition Region and Coronal Explorer (TRACE) images. There is evidence for significant extra flux in many of the flares in addition to the two identified compact sources, thus rendering the VFF assumption of just two Gaussians inadequate. A more realistic approximation in many cases would be of two line sources with unresolved widths. Recommendations are given for optimizing the RHESSI imaging reconstruction process to ensure that the finest possible details of the source morphology become evident and that reliable estimates can be made of the source dimensions.

  6. X-Ray Microanalysis and Electron Energy Loss Spectrometry in the Analytical Electron Microscope: Review and Future Directions

    NASA Technical Reports Server (NTRS)

    Goldstein, J. I.; Williams, D. B.

    1992-01-01

    This paper reviews and discusses future directions in analytical electron microscopy for microchemical analysis using X-ray and Electron Energy Loss Spectroscopy (EELS). The technique of X-ray microanalysis, using the ratio method and k(sub AB) factors, is outlined. The X-ray absorption correction is the major barrier to the objective of obtaining I% accuracy and precision in analysis. Spatial resolution and Minimum Detectability Limits (MDL) are considered with present limitations of spatial resolution in the 2 to 3 microns range and of MDL in the 0.1 to 0.2 wt. % range when a Field Emission Gun (FEG) system is used. Future directions of X-ray analysis include improvement in X-ray spatial resolution to the I to 2 microns range and MDL as low as 0.01 wt. %. With these improvements the detection of single atoms in the analysis volume will be possible. Other future improvements include the use of clean room techniques for thin specimen preparation, quantification available at the I% accuracy and precision level with light element analysis quantification available at better than the 10% accuracy and precision level, the incorporation of a compact wavelength dispersive spectrometer to improve X-ray spectral resolution, light element analysis and MDL, and instrument improvements including source stability, on-line probe current measurements, stage stability, and computerized stage control. The paper reviews the EELS technique, recognizing that it has been slow to develop and still remains firmly in research laboratories rather than in applications laboratories. Consideration of microanalysis with core-loss edges is given along with a discussion of the limitations such as specimen thickness. Spatial resolution and MDL are considered, recognizing that single atom detection is already possible. Plasmon loss analysis is discussed as well as fine structure analysis. New techniques for energy-loss imaging are also summarized. Future directions in the EELS technique will be

  7. Determination of trace elements in Syrian medicinal plants and their infusions by energy dispersive X-ray fluorescence and total reflection X-ray fluorescence spectrometry

    NASA Astrophysics Data System (ADS)

    Khuder, A.; Sawan, M. Kh.; Karjou, J.; Razouk, A. K.

    2009-07-01

    X-ray fluorescence (XRF) and total-reflection X-ray fluorescence (TXRF) techniques suited well for a multi-element determination of K, Ca, Mn, Fe, Cu, Zn, Rb, and Sr in some Syrian medicinal plant species. The accuracy and the precision of both techniques were verified by analyzing the Standard Reference Materials (SRM) peach-1547 and apple leaves-1515. A good agreement between the measured concentrations of the previously mentioned elements and the certified values were obtained with errors less than 10.7% for TXRF and 15.8% for XRF. The determination of Br was acceptable only by XRF with an error less than 24%. Furthermore, the XRF method showed a very good applicability for the determination of K, Ca, Mn, Fe, Cu, Zn, Rb, Sr, and Br in infusions of different Syrian medicinal plant species, namely anise ( Anisum vulgare), licorice root ( Glycyrrhiza glabra), and white wormwood ( Artemisia herba-alba).

  8. Crystal Engineering on Industrial Diaryl Pigments Using Lattice Energy Minimizations and X-ray Powder Diffraction

    SciTech Connect

    Schmidt,M.; Dinnebier, R.; Kalkhof, H.

    2007-01-01

    Diaryl azo pigments play an important role as yellow pigments for printing inks, with an annual pigment production of more than 50,000 t. The crystal structures of Pigment Yellow 12 (PY12), Pigment Yellow 13 (PY13), Pigment Yellow 14 (PY14), and Pigment Yellow 83 (PY83) were determined from X-ray powder data using lattice energy minimizations and subsequent Rietveld refinements. Details of the lattice energy minimization procedure and of the development of a torsion potential for the biphenyl fragment are given. The Rietveld refinements were carried out using rigid bodies, or constraints. It was also possible to refine all atomic positions individually without any constraint or restraint, even for PY12 having 44 independent non-hydrogen atoms per asymmetric unit. For PY14 (23 independent non-hydrogen atoms), additionally all atomic isotropic temperature factors could be refined individually. PY12 crystallized in a herringbone arrangement with twisted biaryl fragments. PY13 and PY14 formed a layer structure of planar molecules. PY83 showed a herringbone structure with planar molecules. According to quantum mechanical calculations, the twisting of the biaryl fragment results in a lower color strength of the pigments, whereas changes in the substitution pattern have almost no influence on the color strength of a single molecule. Hence, the experimentally observed lower color strength of PY12 in comparison with that of PY13 and PY83 can be explained as a pure packing effect. Further lattice energy calculations explained that the four investigated pigments crystallize in three different structures because these structures are the energetically most favorable ones for each compound. For example, for PY13, PY14, or PY83, a PY12-analogous crystal structure would lead to considerably poorer lattice energies and lower densities. In contrast, lattice energy calculations revealed that PY12 could adopt a PY13-type structure with only slightly poorer energy. This structure was

  9. Design and Performance of a TES X-ray Microcalorimeter Array for Energy Dispersive Spectroscopy on Scanning Transmission Electron Microscope

    NASA Astrophysics Data System (ADS)

    Muramatsu, Haruka; Nagayoshi, K.; Hayashi, T.; Sakai, K.; Yamamoto, R.; Mitsuda, K.; Yamasaki, N. Y.; Maehata, K.; Hara, T.

    2016-07-01

    We discuss the design and performance of a transition edge sensor (TES) X-ray microcalorimeter array for scanning transmission electron microscope (STEM)-energy dispersive X-ray spectroscopy (EDS). The TES X-ray microcalorimeter has better energy resolution compared to conventional silicon drift detector and STEM-EDS utilizing a TES detector makes it possible to map the distribution of elements on a specimen in addition to analyze the composition. The requirement for a TES detector is a high counting rate (>20 kcps), wide energy band (0.5-15 keV) and good energy resolution (<10 eV) full width at half maximum. The major improvement of this development is to increase the maximum counting rate. In order to accommodate the high counting rate, we adopted an 8 × 8 format, 64-pixel array and common biasing scheme for the readout method. We did all design and fabrication of the device in house. With the device we have fabricated most recently, the pulse decay time is 40 \\upmu s which is expected to achieve 50 kcps. For a single pixel, the measured energy resolution was 7.8 eV at 5.9 keV. This device satisfies the requirements of counting rate and energy resolution, although several issues remain where the performance must be confirmed.

  10. Interstellar dust as generator of x ray radiation

    NASA Technical Reports Server (NTRS)

    Ibadov, Subhon

    1989-01-01

    The x ray generation due to arising of hot dense plasma balls at high-velocity (greater than or equal to 70 km/s) collisions of dust grains in the interstellar medium is considered. Analytical expressions for efficiency of conversions of colliding dust particle kinetic energy into x ray radiation are presented. The observed intensity distribution of the diffuse component of soft cosmic x rays (0.1 to 1 keV) may be partly caused by collisions between the dusty components of high velocity clouds and of the disk of the Galaxy.

  11. Double-energy X-ray absorptiometry in the diagnosis of osteopenia in ancient skeletal remains.

    PubMed

    González-Reimers, E; Velasco-Vázquez, J; Arnay-de-la-Rosa, M; Santolaria-Fernández, F; Gómez-Rodríguez, M A; Machado-Calvo, M

    2002-06-01

    Bone mineral density (BMD) assessed by double-energy X-ray absorptiometry (DEXA) accurately estimates the bone mass in living individuals, and is thus the method usually employed in the diagnosis and follow-up of osteopenia. It is preferred, in clinical settings, to the more invasive and destructive histomorphometrical assessment of trabecular bone mass in undecalcified bone samples. This study was performed in order to examine the value of DEXA-assessed BMD at the proximal end of the right tibia, either alone or in combination with the cortico-medullary index at the midshaft point of the right tibia (CMI), in the diagnosis of osteopenia in a prehistoric sample composed of 95 pre-Hispanic individuals from Gran Canaria. Age at death could be estimated in 34 cases. Diagnosis of osteopenia was performed by histomorphometrical assessment of trabecular bone mass (TBM) in an undecalcified bone section of a small portion of the proximal epiphysis of the right tibia. A high prevalence of osteopenia was found among the population of Gran Canaria. Both TBM and BMD were significantly lower in the older individuals than in younger ones, and BMD was also significantly lower in female individuals. BMD was moderately correlated with TBM (r = +0.51); the correlation was higher if CMI was included (multiple r = +0.615). BMD values lower than 0.7 g/cm2 showed a high specificity (>93%) at excluding normal TBM values. These methods were prospectively applied in a further sample of 21 right tibiae from Gran Canaria, Tenerife, and El Hierro. The results were similar to those obtained in the larger sample. Thus, DEXA-assessed BMD combined with CMI (noninvasive procedures) may be useful in detecting osteopenia in ancient populations.

  12. THE SAP3 COMPUTER PROGRAM FOR QUANTITATIVE MULTIELEMENT ANALYSIS BY ENERGY DISPERSIVE X-RAY FLUORESCENCE

    SciTech Connect

    Nielson, K. K.; Sanders, R. W.

    1982-04-01

    SAP3 is a dual-function FORTRAN computer program which performs peak analysis of energy-dispersive x-ray fluorescence spectra and then quantitatively interprets the results of the multielement analysis. It was written for mono- or bi-chromatic excitation as from an isotopic or secondary excitation source, and uses the separate incoherent and coherent backscatter intensities to define the bulk sample matrix composition. This composition is used in performing fundamental-parameter matrix corrections for self-absorption, enhancement, and particle-size effects, obviating the need for specific calibrations for a given sample matrix. The generalized calibration is based on a set of thin-film sensitivities, which are stored in a library disk file and used for all sample matrices and thicknesses. Peak overlap factors are also determined from the thin-film standards, and are stored in the library for calculating peak overlap corrections. A detailed description is given of the algorithms and program logic, and the program listing and flow charts are also provided. An auxiliary program, SPCAL, is also given for use in calibrating the backscatter intensities. SAP3 provides numerous analysis options via seventeen control switches which give flexibility in performing the calculations best suited to the sample and the user needs. User input may be limited to the name of the library, the analysis livetime, and the spectrum filename and location. Output includes all peak analysis information, matrix correction factors, and element concentrations, uncertainties and detection limits. Twenty-four elements are typically determined from a 1024-channel spectrum in one-to-two minutes using a PDP-11/34 computer operating under RSX-11M.

  13. Dual-energy X-ray absorptiometry body composition in patients with secondary osteoporosis.

    PubMed

    Messina, Carmelo; Monaco, Cristian Giuseppe; Ulivieri, Fabio Massimo; Sardanelli, Francesco; Sconfienza, Luca Maria

    2016-08-01

    Due to the tight relationship between bone and soft tissues, there has been an increased interest in body composition assessment in patients with secondary osteoporosis as well as other pathological conditions. Dual-energy X-ray absorptiometry (DXA) is primarily devoted to the evaluation of bone mineral status, but continuous scientific advances of body composition software made DXA a rapid and easily available technique to assess body composition in terms of fat mass and lean mass. As a result, the International Society for Clinical Densitometry (ISCD) recently developed Official Positions regarding the use of this technique for body composition analysis. According to ISCD paper, indications are mainly limited to three conditions: HIV patients treated with antiretroviral agents associated with a risk of lipoatrophy; obese patients undergoing treatment for high weight loss; patients with sarcopenia or muscle weakness. Nevertheless, there are several other interesting clinical applications that were not included in the ISCD position paper, such as body composition assessment in patients undergoing organ transplantation, pulmonary disease as well as all those chronic condition that may lead to malnutrition. In conclusion, DXA body composition offers new diagnostic and research possibilities for a variety of diseases; due to its high reproducibility, DXA has also the potential to monitor body composition changes with pharmacological, nutritional or physic therapeutic interventions. ISCD addressed and recommended a list of clinical condition, but the crescent availability of DXA scans and software improvements may open the use of DXA to other indication in the next future. This article provides an overview of DXA body composition indications in the management of secondary osteoporosis and other clinical indications in adults. PMID:27048946

  14. Dual-Energy X-Ray Absorptiometry Prediction of Adipose Tissue Depots in Children and Adolescents

    PubMed Central

    Bauer, Jacqueline; Thornton, John; Heymsfield, Steven; Kelly, Kim; Ramirez, Alexander; Gidwani, Sonia; Gallagher, Dympna

    2013-01-01

    Background The measurement of adipose tissue depots in-vivo requires expensive imaging methods not accessible to most clinicians and researchers. The study aim was to derive mathematical models to predict total adipose tissue (TAT) and sub-depots from total body fat derived from a dual energy x-ray absorptiometry (DXA) scan. Methods Models were developed to predict magnetic resonance imaging derived TAT and sub-depots subcutaneous (SAT), visceral (VAT), and intermuscular (IMAT) from DXA total body fat using cross-sectional data (T0) and validated results using 1 (T1) and 2 (T2) year follow-up data. Subjects were 176 multi-ethnic healthy children ages 5 to 17 years at T0. 22 were measured at T1 and T2. TAT was compared to fat. Results At T0, TAT was greater than fat (12.5 ± 8.4 vs.12.0 ± 9.4 kg; p< 0.0001), with a quadratic relationship between TAT and fat which varied by sex. Predicted mean TAT’s were not different from measured TAT’s: T1: (9.84±4.45 kg vs. 9.50±4.37 kg; p=0.11) T2: (12.94±6.75 kg vs. 12.89±7.09 kg; p=0.76). The quadratic relationship was not influenced by race or age. Conclusions In general, the prediction equations for TAT and sub-depots were consistent with the measured values using T1 and T2 data. PMID:22821057

  15. A review of the use of dual-energy X-ray absorptiometry (DXA) in rheumatology

    PubMed Central

    Tanner, S Bobo; Moore, Charles F

    2012-01-01

    The principal use of dual-energy X-ray absorptiometry (DXA) is to diagnose and monitor osteoporosis and therefore reduce fracture risk, associated morbidity, and mortality. In the field of rheumatology, DXA is an essential component of patient care because of both rheumatologists’ prescription of glucocorticoid treatment as well as the effects of rheumatological diseases on bone health. This review will summarize the use of DXA in the field of rheumatology, including the concern for glucocorticoid-induced osteoporosis, as well as the association of osteoporosis with a sampling of such rheumatologic conditions as rheumatoid arthritis (RA), systemic lupus erythematosus, ankylosing spondylitis, juvenile idiopathic arthritis, and scleroderma or systemic sclerosis. Medicare guidelines recognize the need to perform DXA studies in patients treated with glucocorticoids, and the World Health Organization FRAX tool uses data from DXA as well as the independent risk factors of RA and glucocorticoid use to predict fracture risk. However, patient access to DXA measurement in the US is in jeopardy as a result of reimbursement restrictions. DXA technology can simultaneously be used to discover vertebral fractures with vertebral fracture assessment and provide patients with a rapid, convenient, and low-radiation opportunity to clarify future fracture and comorbidity risks. An emerging use of DXA technology is the analysis of body composition of RA patients and thus the recognition of “rheumatoid cachexia,” in which patients are noted to have a worse prognosis even when the RA appears well controlled. Therefore, the use of DXA in rheumatology is an important tool for detecting osteoporosis, reducing fracture risk and unfavorable outcomes in rheumatological conditions. The widespread use of glucocorticoids and the underlying inflammatory conditions create a need for assessment with DXA. There are complications of conditions found in rheumatology that could be prevented with

  16. Block-copolymer of polyethylene glycol and polylysine as a carrier of organic iodine: design of long-circulating particulate contrast medium for X-ray computed tomography.

    PubMed

    Trubetskoy, V S; Gazelle, G S; Wolf, G L; Torchilin, V P

    1997-01-01

    In order to obtain small, polymer-stabilized particulate carriers for organic iodine to serve as a contrast agent for X-ray computed tomography (CT) an attempt was made to design a carrier based on polymeric micelles. Here we describe the synthesis of an iodine-containing amphiphilic block-copolymer which can micellize in aqueous solutions. The two blocks of the copolymer consisted of methoxypoly(ethyleneglycol) and poly[epsilon,N-(triiodobenzoyl)-L-lysine]. Upon dispersion in water, the block copolymer formed particles with average diameter 80 nm and iodine content up to 44.7%. The particles start to dissociate to the individual polymeric chains in the concentration range of 0.05-0.5 microM in water at 23 degrees C. Upon intravenous injection at 250 mg of iodine/kg (570 mg of the agent/kg) in rabbits the medium demonstrated exceptional 24 hr half-life in the blood substantiating corona/core structure of the particles with PEG chains protecting the iodine-containing core. The possible use of these particulates as contrast medium for X-ray computed tomography is discussed.

  17. Energy of microwave-emitting electrons and hard x-ray/microwave source model in solar flares

    NASA Technical Reports Server (NTRS)

    Nitta, N.; Kosugi, T.

    1986-01-01

    Based on the rate of increse of the microwave flux relative to the hard X-ray flux at various energies from the onset to the peak of a flare, the mean energy of microwave-emitting electrons is estimated for 22 flares observed simultaneously in hard X-rays and microwaves. The energy of electrons varying in proportion to the 17 GHz emission is found to concentrate below 100 keV, and the mean energy or eletrons emitting 70 keV x-rays is less than about 130 keV for thin-target and less than about 180 keV for thick-target emission models, suggesting that the 17 GHz emission derives from electrons with energy of less than a few hundred keV. The magnetic field strength in the microwave source is found to be 500-1000 G for the thick-target and 1000-2000 G for the thin-target case, and 16 of the 22 events examined can be successfully explained by the thick-target model. Of the six events which cannot be explained by the thick-target model, two events give L of less than about 300 km.

  18. Investigating the Liquid Distribution in a Reactive Distillation Packing Using High Energy X-Ray Tomography

    NASA Astrophysics Data System (ADS)

    Abdullah, J.; Aferka, S.; Crine, M.; Saroha, A. K.; Toye, D.; Marchot, Pierre

    2007-06-01

    Liquid distribution in a 0.1 m diameter column packed with Katapak-SP12 is investigated with a 420 kV X-ray tomograph. The distribution of the various liquid hold up between baskets and corrugated sheets is quantified.

  19. High Energy X-Ray System Specification for the Device Assembly Facility (DAF) at the NNSS

    SciTech Connect

    Fry, David A.

    2012-08-10

    This specification establishes requirements for an X-Ray System to be used at the Device Assembly Facility (DAF) at the Nevada National Security Site (NNSS) to support radiography of experimental assemblies for Laboratory (LANL, LLNL, SNL) programs conducting work at the NNSS.

  20. Planetary X-ray studies: past, present and future

    NASA Astrophysics Data System (ADS)

    Branduardi-Raymont, Graziella

    2016-07-01

    Our solar system is a fascinating physics laboratory and X-ray observations are now firmly established as a powerful diagnostic tool of the multiple processes taking place in it. The science that X-rays reveal encompasses solar, space plasma and planetary physics, and the response of bodies in the solar system to the impact of the Sun's activity. This talk will review what we know from past observations and what we expect to learn in the short, medium and long term. Observations with Chandra and XMM-Newton have demonstrated that the origin of Jupiter's bright soft X-ray aurorae lies in the Charge eXchange (CX) process, likely to involve the interaction with atmospheric neutrals of local magnetospheric ions, as well as those carried in the solar wind. At higher energies electron bremsstrahlung is thought to be the X-ray emitting mechanism, while the whole planetary disk acts as a mirror for the solar X-ray flux via Thomson and fluorescent scattering. This 'X-ray mirror' phenomenon is all that is observed from Saturn's disk, which otherwise lacks X-ray auroral features. The Earth's X-ray aurora is bright and variable and mostly due to electron bremsstrahlung and line emission from atmospheric species. Un-magnetised planets, Venus and Mars, do not show X-ray aurorae but display the interesting combination of mirroring the solar X-ray flux and producing X-rays by Solar Wind Charge eXchange (SWCX) in their exospheres. These processes respond to different solar stimulation (photons and solar wind plasma respectively) hence their relative contributions are seen to vary according to the Sun's output. Present and future of planetary X-ray studies are very bright. We are preparing for the arrival of the Juno mission at Jupiter this summer and for coordinated observations with Chandra and XMM-Newton on the approach and later during Juno's orbital phase. These will allow direct correlation of the local plasma conditions with the X-ray emissions and the establishment of the