Laboratory measurements of microwave and millimeter-wave properties of planetary atmospheric constituents

NASA Technical Reports Server (NTRS)

Steffes, Paul G.

1989-01-01

Accurate data on microwave and millimeter-wave properties of potential planetary atmospheric constituents is critical for the proper interpretation of radio occultation measurements, and of radio astronomical observations of both continuum and spectral line emissions. Such data is also needed to correct for atmospheric effects on radar studies of surface reflectivity. Since the refractive and absorptive properties of atmospheric constituents often vary drastically from theoretically-predicted profiles, especially under the extreme conditions characteristic of the planetary atmosphere, laboratory measurements under simulated planetary conditions are required. This paper reviews the instrumentation and techniques used for laboratory measurement of the refractivity and absorptivity of atmospheric constituents at wavelengths longward of 1 mm, under simulated planetary conditions (temperature, pressure, and broadening gases). Techniques for measuring both gases and condensates are considered. Also reviewed are the relative accuracies of the various techniques. Laboratory measurements are reviewed which have already been made, and additional measurements which are needed for interpretation of data from Venus and the outer planets, are highlighted.

Electric microwave absorption for the study of GaAs/AlGaAs heterostructure systems

NASA Astrophysics Data System (ADS)

Zappe, Hans P.; Jantz, Wolfgang

1990-12-01

The use of magnetic-field-dependent microwave absorption as a nondestructive and contact-free means to study transport behavior in GaAs/AlGaAs devices is explored. This technique allows quick measurement of resistance, mobility, and carrier concentration in bulk substrates as well as in the two-dimensional electron gas of heterostructure quantum wells. The two- and three-dimensional conductivities may be separably evaluated, allowing detailed study of conduction in the active layer of high-electron-mobility devices. A brief theoretical foundation is provided, followed by application of the approach to examination of device structural dependencies, carrier-density conduction behavior, and the effects of etch processing on quantum-well integrity.

Method and apparatus for selectively annealing heterostructures using microwave

NASA Technical Reports Server (NTRS)

Atwater, Harry A. (Inventor); Brain, Ruth A. (Inventor); Barmatz, Martin B. (Inventor)

1998-01-01

The present invention discloses a process for selectively annealing heterostructures using microwaves. A heterostructure, comprised of a material having higher microwave absorption and a material having lower microwave absorption, is exposed to microwaves in the cavity. The higher microwave absorbing material absorbs the microwaves and selectively heats while the lower microwave absorbing material absorbs small amounts of microwaves and minimally heats. The higher microwave absorbing material is thereby annealed onto the less absorbing material which is thermally isolated.

Method and apparatus for selectively annealing heterostructures using microwaves

NASA Technical Reports Server (NTRS)

Atwater, Harry A. (Inventor); Brain, Ruth A. (Inventor); Barmatz, Martin B. (Inventor)

1998-01-01

The present invention discloses a process for selectively annealing heterostructures using microwaves. A heterostructure, comprised of a material having higher microwave absorption and a material having lower microwave absorption, is exposed to microwaves in the cavity. The higher microwave absorbing material absorbs the microwaves and selectively heats while the lower microwave absorbing material absorbs small amounts of microwaves and minimally heats. The higher microwave absorbing material is thereby annealed onto the less absorbing material which is thermally isolated.

Efficient finite element simulation of slot spirals, slot radomes and microwave structures

NASA Technical Reports Server (NTRS)

Gong, J.; Volakis, J. L.

1995-01-01

This progress report contains the following two documents: (1) 'Efficient Finite Element Simulation of Slot Antennas using Prismatic Elements' - A hybrid finite element-boundary integral (FE-BI) simulation technique is discussed to treat narrow slot antennas etched on a planar platform. Specifically, the prismatic elements are used to reduce the redundant sampling rates and ease the mesh generation process. Numerical results for an antenna slot and frequency selective surfaces are presented to demonstrate the validity and capability of the technique; and (2) 'Application and Design Guidelines of the PML Absorber for Finite Element Simulations of Microwave Packages' - The recently introduced perfectly matched layer (PML) uniaxial absorber for frequency domain finite element simulations has several advantages. In this paper we present the application of PML for microwave circuit simulations along with design guidelines to obtain a desired level of absorption. Different feeding techniques are also investigated for improved accuracy.

Large-scale synthesis and microwave absorption enhancement of actinomorphic tubular ZnO/CoFe2O4 nanocomposites.

PubMed

Cao, Jing; Fu, Wuyou; Yang, Haibin; Yu, Qingjiang; Zhang, Yanyan; Liu, Shikai; Sun, Peng; Zhou, Xiaoming; Leng, Yan; Wang, Shuangming; Liu, Bingbing; Zou, Guangtian

2009-04-09

Actinomorphic tubular ZnO/CoFe(2)O(4) nanocomposites were fabricated in large scale via a simple solution method at low temperature. The phase structures, morphologies, particle size, shell thickness, chemical compositions of the composites have been characterized by X-ray diffraction (XRD), field emission scanning electron microscope (FESEM), energy dispersive X-ray spectroscopy (EDS), and transmission electron microscopy (TEM). The as-synthesized nanocomposites were uniformly dispersed into the phenolic resin then the mixture was pasted on metal plate with the area of 200 mm x 200 mm as the microwave absorption test plate. The test of microwave absorption was carried out by the radar-absorbing materials (RAM) reflectivity far field radar cross-section (RCS) method. The range of microwave absorption is from 2 to 18 Hz and the best microwave absorption reach to 28.2 dB at 8.5 Hz. The results indicate that the composites are of excellence with respect to microwave absorption.

Ultralight Fe@C Nanocapsules/Sponge Composite with Reversibly Tunable Microwave Absorption Performances.

PubMed

Li, Yixing; Mao, Zhe; Liu, Rongge; Zhao, Xiaoning; Zhang, Yanhui; Qin, Gaowu; Zhang, Xuefeng

2017-08-11

Microwave absorbers are usually designed to solve electromagnetic interferences at a specific frequency, while the requirements may be dynamic during service life. Therefore, a recoverable tuning for microwave absorption properties in response to an external stimulus would be highly desirable. We herein present a micro/nano-scale hybrid absorber, in which high-performance Fe@C nanocapsule absorbents are integrated with a porous melamine sponge skeleton, exhibiting multiple merits of light weight, strong absorption and high elasticity. By mechanically compressing and decompressing the absorber, microwave absorption performances can be effectively shifted between 18 GHz and 26.5 GHz. The present study thus provides a new strategy for the design of a 'dynamic' microwave absorber.

Ultralight Fe@C Nanocapsules/Sponge Composite with Reversibly Tunable Microwave Absorption Performances

NASA Astrophysics Data System (ADS)

Li, Yixing; Mao, Zhe; Liu, Rongge; Zhao, Xiaoning; Zhang, Yanhui; Qin, Gaowu; Zhang, Xuefeng

2017-08-01

Microwave absorbers are usually designed to solve electromagnetic interferences at a specific frequency, while the requirements may be dynamic during service life. Therefore, a recoverable tuning for microwave absorption properties in response to an external stimulus would be highly desirable. We herein present a micro/nano-scale hybrid absorber, in which high-performance Fe@C nanocapsule absorbents are integrated with a porous melamine sponge skeleton, exhibiting multiple merits of light weight, strong absorption and high elasticity. By mechanically compressing and decompressing the absorber, microwave absorption performances can be effectively shifted between 18 GHz and 26.5 GHz. The present study thus provides a new strategy for the design of a ‘dynamic’ microwave absorber.

Improved solvent-free microwave extraction of essential oil from dried Cuminum cyminum L. and Zanthoxylum bungeanum Maxim.

PubMed

Wang, Ziming; Ding, Lan; Li, Tiechun; Zhou, Xin; Wang, Lu; Zhang, Hanqi; Liu, Li; Li, Ying; Liu, Zhihong; Wang, Hongju; Zeng, Hong; He, Hui

2006-01-13

Solvent-free microwave extraction (SFME) is a recently developed green technique which is performed in atmospheric conditions without adding any solvent or water. SFME has already been applied to extraction of essential oil from fresh plant materials or dried materials prior moistened. The essential oil is evaporated by the in situ water in the plant materials. In this paper, it was observed that an improved SFME, in which a kind of microwave absorption solid medium, such as carbonyl iron powders (CIP), was added and mixed with the sample, can be applied to extraction of essential oil from the dried plant materials without any pretreatment. Because the microwave absorption capacity of CIP is much better than that of water, the extraction time while using the improved SFME is no more than 30 min using a microwave power of 85 W. Compared to the conventional SFME, the advantages of improved SFME were to speed up the extraction rate and need no pretreatment. Improved SFME has been compared with conventional SFME, microwave-assisted hydrodistillation (MAHD) and conventional hydrodistillation (HD) for the extraction of essential oil from dried Cuminum cyminum L. and Zanthoxylum bungeanum Maxim. By using GC-MS system the compositions of essential oil extracted by applying four kinds of extraction methods were identified. There was no obvious difference in the quality of essential oils obtained by the four kinds of extraction methods.

Discrimination of the earthquake-origin microwave emission from the data of the spaceborne radiometer

NASA Astrophysics Data System (ADS)

Maeda, T.; Takano, T.

2007-12-01

Formerly, we found the microwave emission during rock crash in a laboratory for the first time in the world, and calibrated the emitted power. The detected signal is a sequence of pulses which include microwaves at the selected frequency bands of 300MHz, 2GHz and 22GHz. This fact suggested another means to detect an earthquake which is associated with rock crash or plate slip. For this purpose, we have analyzed the data obtained by the microwave radiometer, AMSR-E loaded on the satellite Aqua. Generally, since a microwave emission observed by AMSR-E is affected by various factors (e.g., emission of the earth's surface and emission, absorption and scattering of the atmosphere), we developed some analysis techniques first. Then, we have successfully extracted features observed only at the earthquake occurrence by these techniques. This earthquake was occurred at Morocco in 2004. Since the depth of the seismic center was shallower and the magnitude was larger, we have specifically focused on analysis of this earthquake. This presentation first presents the estimation of the received power by a receiver aboard a satellite. Then, the data obtained by AMSR-E are described including the disturbances or ambiguity of the data. The techniques to extract microwave signatures out of disturbances are given. Finally, an example of the data analysis is explained in the case of Morocco earthquake to show distinct emission of microwaves in relation with geological features.

Easily Dispersible NiFe2O4/RGO Composite for Microwave Absorption Properties in the X-Band

NASA Astrophysics Data System (ADS)

Bateer, Buhe; Zhang, Jianjao; Zhang, Hongchen; Zhang, Xiaochen; Wang, Chunyan; Qi, Haiqun

2018-01-01

Composites with good dispersion and excellent microwave absorption properties have important applications. Therefore, an easily dispersible NiFe2O4/reduced graphene oxide (RGO) composite has been prepared conveniently through a simple hydrothermal method. Highly crystalline, small size (about 7 nm) monodispersed NiFe2O4 nanoparticles (NPs) are evenly distributed on the surface of RGO. The microwave absorbability revealed that the NiFe2O4/RGO composite exhibits excellent microwave absorption properties in the X-band (8-12 GHz), and the minimum reflection loss of the NiFe2O4/RGO composite is -27.7 dB at 9.2 GHz. The NiFe2O4/RGO composite has good dispersibility in nonpolar solvent, which facilitates the preparation of stable commercial microwave absorbing coatings. It can be a promising candidate for lightweight microwave absorption materials in many application fields.

Microporous Co@C Nanoparticles Prepared by Dealloying CoAl@C Precursors: Achieving Strong Wideband Microwave Absorption via Controlling Carbon Shell Thickness.

PubMed

Li, Da; Liao, Haoyan; Kikuchi, Hiroaki; Liu, Tong

2017-12-27

Excellent magnetic features make Co-based materials promising candidates as high-performance microwave absorbers. However, it is still a significant challenge for Co-based absorbers to possess high-intensity and broadband absorption simultaneously, owing to the lack of dielectric loss and impedance matching. Herein, microporous Co@C nanoparticles (NPs) with carbon shell thicknesses ranging from 1.8-4.9 nm have been successfully synthesized by dealloying CoAl@C precursors. All of the samples exhibit high microwave absorption performance. The microporous Co@C sample possessing a carbon shell of 1.8 nm exhibits the highest absorption intensity among these samples with a minimum reflection loss (RL) of -141.1 dB, whose absorption bandwidth for RL ≤ -10 dB is 7.3 GHz. As the thickness of the carbon shell increases, the absorption bandwidth of the NPs becomes wider. For the sample with the carbon shell thickness of 4.9 nm, the absorption bandwidth for RL ≤ -10 dB reaches a record high of 13.2 GHz. The outstanding microwave attenuation properties are attributed to the dielectric loss of the carbon shell, the magnetic loss of the Co core, and the cooperation of the core-shell structure and microporous morphology. The strong wideband microwave absorption of the carbon-coated microporous Co NPs highlights their potential applications in microwave absorbing systems.

Skull and cerebrospinal fluid effects on microwave radiation propagation in human brain

NASA Astrophysics Data System (ADS)

Ansari, M. A.; Zarei, M.; Akhlaghipour, N.; Niknam, A. R.

2017-12-01

The determination of microwave absorption distribution in the human brain is necessary for the detection of brain tumors using thermo-acoustic imaging and for removing them using hyperthermia treatment. In contrast to ionizing radiation, hyperthermia treatment can be applied to remove tumors inside the brain without the concern of including secondary malignancies, which typically form from the neuronal cells of the septum pellucidum. The aim of this study is to determine the microwave absorption distribution in an adult human brain and to study the effects of skull and cerebrospinal fluid on the propagation of microwave radiation inside the brain. To this end, we simulate the microwave absorption distribution in a realistic adult brain model (Colin 27) using the mesh-based Monte Carlo (MMC) method. This is because in spite of there being other numerical methods, the MMC does not require a large memory, even for complicated geometries, and its algorithm is simple and easy to implement with low computational cost. The brain model is constructed using high-resolution (1 mm isotropic voxel) and low noise magnetic resonance imaging (MRI) scans and its volume contains 181×217×181 voxels, covering the brain completely. Using the MMC method, the radiative transport equation is solved and the absorbed microwave energy distribution in different brain regions is obtained without any fracture or anomaly. The simulation results show that the skull and cerebrospinal fluid guide the microwave radiation and suppress its penetration through deep brain compartments as a shielding factor. These results reveal that the MMC can be used to predict the amount of required energy to increase the temperature inside the tumour during hyperthermia treatment. Our results also show why a deep tumour inside an adult human brain cannot be efficiently treated using hyperthermia treatment. Finally, the accuracy of the presented numerical method is verified using the signal flow graph technique.

Influence of MnO2 decorated Fe nano cauliflowers on microwave absorption and impedance matching of polyvinylbutyral (PVB) matrix

NASA Astrophysics Data System (ADS)

Bora, Pritom J.; Porwal, Mayuri; Vinoy, K. J.; Ramamurthy, Praveen C.; Madras, Giridhar

2016-09-01

In this work, a promising, polyvinyl butryl (PVB)-MnO2 decorated Fe composite was synthesised and microwave absorption properties were studied for the most important frequency ranges i.e., X-band (8.2-12.4 GHz) and Ku-band (12.4-18 GHz). The microwave absorption of Fe nano cauliflower structure can be enhanced by MnO2 nanofiber coating. 10 wt% Fe-MnO2 nano cauliflower loaded PVB composite films (2 mm thick) shows an appreciable increase in microwave absorption properties. In X-band, the reflection loss (RL) of this composite decreases almost linearly to -7.5 dB, whereas in the Ku-band the minimum RL was found to be -15.7 dB at 14.7 GHz. Here it was observed that impedance matching is the primarily important factor responsible for enhanced microwave absorption. Further, enhancement of EM attenuation constant (α), dielectrics, scattering attenuation also bolsters the obtained results. This polymer composite can be considered as a novel microwave absorbing coating material.

Microwave absorption through the martensitic and Curie transitions in Ni45Cr5Mn37In13

NASA Astrophysics Data System (ADS)

Pandey, Sudip; Vyzulin, Sergey; Quetz, Abdiel; Aryal, Anil; Dubenko, Igor; Granovsky, Alexander; Stadler, Shane; Ali, Naushad

2018-05-01

We have investigated the electron spin resonance (ESR) of the Ni45Cr5Mn37In13 Heusler alloy near the structural and magnetic phase transition temperatures. Ni45Cr5Mn37In13 is characterized by a first order magnetostructural (martensitic) transition (MST) with magneto-responsive properties such as magnetoresistance, Hall and magnetocaloric effects, etc., in the vicinity of the MST. Since the details and origins of these behaviors are not well understood, we used a technique beyond magnetometry, i.e., "microwave absorption", to reveal new information. ESR studies of Ni45Cr5Mn37In13 shows that this compound is characterized by wide absorption spectra at temperatures greater than 250 K that depend on the angle of the magnetic field relative to the normal to the sample plate (α) and temperature (T). Two local maxima at about 5 and 6 kOe were detected for α close to zero degrees near the martensitic transition and Curie temperatures. The absorption spectra are discussed along with the results of the structural and magnetic studies.

Search for Superconductivity in Micrometeorites

PubMed Central

Guénon, S.; Ramírez, J. G.; Basaran, Ali C.; Wampler, J.; Thiemens, M.; Taylor, S.; Schuller, Ivan K.

2014-01-01

We have developed a very sensitive, highly selective, non-destructive technique for screening inhomogeneous materials for the presence of superconductivity. This technique, based on phase sensitive detection of microwave absorption is capable of detecting 10−12 cc of a superconductor embedded in a non-superconducting, non-magnetic matrix. For the first time, we apply this technique to the search for superconductivity in extraterrestrial samples. We tested approximately 65 micrometeorites collected from the water well at the Amundsen-Scott South pole station and compared their spectra with those of eight reference materials. None of these micrometeorites contained superconducting compounds, but we saw the Verwey transition of magnetite in our microwave system. This demonstrates that we are able to detect electro-magnetic phase transitions in extraterrestrial materials at cryogenic temperatures. PMID:25476841

Enhancing the microwave absorption properties of amorphous CoO nanosheet-coated Co (hexagonal and cubic phases) through interfacial polarizations.

PubMed

Deng, Jiushuai; Li, Shimei; Zhou, Yuanyuan; Liang, Luyang; Zhao, Biao; Zhang, Xi; Zhang, Rui

2018-01-01

Core-shell flower-like composites were successfully prepared by a simple polyol method. These composites were formed by coating dual-phased (face-centered cubic [fcc] and hexagonal close-packed [hcp]) Co with amorphous CoO nanosheets. The microwave absorption properties of the flower-like Co@CoO paraffin composites with various Co@CoO amounts were then investigated. Results showed that the paraffin-based composite containing 70wt% flower-like Co@CoO displayed excellent microwave absorption properties (R E =24.74dB·GHz/mm). The minimum reflection loss of -30.4dB was obtained at 16.1GHz with a small thickness of 1.5mm, and 1.5mm bandwidth reached 4.6GHz (13.4-18GHz) below -10dB (90% microwave absorption). The excellent microwave absorption properties of flower-like Co@CoO are attributed to the synergetic effect between magnetic loss and dielectric loss, and the magnetic loss makes a main contribution to absorption. The core-shell flower-like structures with dual Co phases also contributed to microwave absorption. The amorphous CoO nanosheets were able to generate multiple reflections and exhibit scattering. In addition, the novel absorption mechanism that enhanced interfacial polarization was proposed. This enhancement resulted from the presence of interfaces between the hcp and fcc phases and between the core-shell Co@CoO composites. Copyright © 2017 Elsevier Inc. All rights reserved.

The impact of different multi-walled carbon nanotubes on the X-band microwave absorption of their epoxy nanocomposites.

PubMed

Che, Bien Dong; Nguyen, Bao Quoc; Nguyen, Le-Thu T; Nguyen, Ha Tran; Nguyen, Viet Quoc; Van Le, Thang; Nguyen, Nieu Huu

2015-01-01

Carbon nanotube (CNT) characteristics, besides the processing conditions, can change significantly the microwave absorption behavior of CNT/polymer composites. In this study, we investigated the influence of three commercial multi-walled CNT materials with various diameters and length-to-diameter aspect ratios on the X-band microwave absorption of epoxy nanocomposites with CNT contents from 0.125 to 2 wt%, prepared by two dispersion methods, i.e. in solution with surfactant-aiding and via ball-milling. The laser diffraction particle size and TEM analysis showed that both methods produced good dispersions at the microscopic level of CNTs. Both a high aspect ratio resulting in nanotube alignment trend and good infiltration of the matrix in the individual nanotubes, which was indicated by high Brookfield viscosities at low CNT contents of CNT/epoxy dispersions, are important factors to achieve composites with high microwave absorption characteristics. The multi-walled carbon nanotube (MWCNT) with the largest aspect ratio resulted in composites with the best X-band microwave absorption performance, which is considerably better than that of reported pristine CNT/polymer composites with similar or lower thicknesses and CNT loadings below 4 wt%. A high aspect ratio of CNTs resulting in microscopic alignment trend of nanotubes as well as a good level of micro-scale CNT dispersion resulting from good CNT-matrix interactions are crucial to obtain effective microwave absorption performance. This study demonstrated that effective radar absorbing MWCNT/epoxy nanocomposites having small matching thicknesses of 2-3 mm and very low filler contents of 0.25-0.5 wt%, with microwave energy absorption in the X-band region above 90% and maximum absorption peak values above 97%, could be obtained via simple processing methods, which is promising for mass production in industrial applications. Graphical AbstractComparison of the X-band microwave reflection loss of epoxy composites of various commercial multi-walled carbon nanotube materials.

Laboratory evaluation and application of microwave absorption properties under simulated conditions for planetary atmospheres

NASA Technical Reports Server (NTRS)

Steffes, Paul G.

1987-01-01

Radio absorptivity data for planetary atmospheres obtained from spacecraft radio occultation experiments and Earth-based radio astronomical observations can be used to infer abundances of microwave absorbing atmospheric constituents in those atmospheres, as long as reliable information regarding the microwave absorping properties of potential constituents is available. The use of theoretically derived microwave absorption properties for such atmospheric constituents, or laboratory measurements of such properties under environmental conditions which are significantly different than those of the planetary atmosphere being studied, often leads to significant misinterpretation of available opacity data. Laboratory measurement of the microwave properties of atmospheric gases under simulated conditions for the outer planets were conducted. Results of these measurements are discussed.

Estimation of Rainfall Rates from Passive Microwave Remote Sensing.

NASA Astrophysics Data System (ADS)

Sharma, Awdhesh Kumar

Rainfall rates have been estimated using the passive microwave and visible/infrared remote sensing techniques. Data of September 14, 1978 from the Scanning Multichannel Microwave Radiometer (SMMR) on board SEA SAT-A and the Visible and Infrared Spin Scan Radiometer (VISSR) on board GOES-W (Geostationary Operational Environmental Satellite - West) was obtained and analyzed for rainfall rate retrieval. Microwave brightness temperatures (MBT) are simulated, using the microwave radiative transfer model (MRTM) and atmospheric scattering models. These MBT were computed as a function of rates of rainfall from precipitating clouds which are in a combined phase of ice and water. Microwave extinction due to ice and liquid water are calculated using Mie-theory and Gamma drop size distributions. Microwave absorption due to oxygen and water vapor are based on the schemes given by Rosenkranz, and Barret and Chung. The scattering phase matrix involved in the MRTM is found using Eddington's two stream approximation. The surface effects due to winds and foam are included through the ocean surface emissivity model. Rainfall rates are then inverted from MBT using the optimization technique "Leaps and Bounds" and multiple linear regression leading to a relationship between the rainfall rates and MBT. This relationship has been used to infer the oceanic rainfall rates from SMMR data. The VISSR data has been inverted for the rainfall rates using Griffith's scheme. This scheme provides an independent means of estimating rainfall rates for cross checking SMMR estimates. The inferred rainfall rates from both techniques have been plotted on a world map for comparison. A reasonably good correlation has been obtained between the two estimates.

Effects of natural zeolite and ferric oxide to electromagnetic and reflection loss properties of polyurethane nanocomposite

NASA Astrophysics Data System (ADS)

Gultom, G.; Wirjosentono, B.; Ginting, M.; Sebayang, K.

2017-07-01

Microwave-absorptive polymeric composite materials are becoming important to protect interference of any communication systems due to increasing use of microwave-inducing devices. In this work, the microwave-absorptive polyurethane nanocomposites were prepared using natural zeolites of Sarulla North Sumatra and commercial ferric oxide as fillers. Weight ratios of the polyurethane to natural zeolite and ferric oxide were varied (90%:6%:4%; 80%:12%:8%; 70%:24%:6%) by weight. The fillers were prepared using ball milling technique and characterized for their particle size distributions using Particle Size Analyzer. The nanocomposites, prepared using in-situ reaction of polyethylene glycol, toluene diisocyanate and fillers. The complex permittivity (ε’and ε”) and complex permeability (μ’ and μ”) as electromagnetic properties were calculated using NRW method after collecting real and imaginary S parameter using Vector Network Analyzer measurement at X band frequency. Results show ratio of the fillers will affect the permeability, permittivity and reflection loss of the materials. The best reflection loss was shown -40.588 dB (>99 % absorption) at ratio for polyurethane : nanozeolite : ferric oxide (80%:12%:8%) by weight observed at 10.92 GHz. According to the measurement and calculation was shown the polyurethane filled with natural nanozeolite and ferric oxide is a good electromagnetic wave attenuation material.

Unusual continuous dual absorption peaks in Ca-doped BiFeO3 nanostructures for broadened microwave absorption

NASA Astrophysics Data System (ADS)

Li, Zhong-Jun; Hou, Zhi-Ling; Song, Wei-Li; Liu, Xing-Da; Cao, Wen-Qiang; Shao, Xiao-Hong; Cao, Mao-Sheng

2016-05-01

Electromagnetic absorption materials have received increasing attention owing to their wide applications in aerospace, communication and the electronics industry, and multiferroic materials with both polarization and magnetic properties are considered promising ceramics for microwave absorption application. However, the insufficient absorption intensity coupled with the narrow effective absorption bandwidth has limited the development of high-performance multiferroic materials for practical microwave absorption. To address such issues, in the present work, we utilize interfacial engineering in BiFeO3 nanoparticles via Ca doping, with the purpose of tailoring the phase boundary. Upon Ca-substitution, the co-existence of both R3c and P4mm phases has been confirmed to massively enhance both dielectric and magnetic properties via manipulating the phase boundary and the destruction of the spiral spin structure. Unlike the commonly reported magnetic/dielectric hybrid microwave absorption composites, Bi0.95Ca0.05FeO3 has been found to deliver unusual continuous dual absorption peaks at a small thickness (1.56 mm), which has remarkably broadened the effective absorption bandwidth (8.7-12.1 GHz). The fundamental mechanisms based on the phase boundary engineering have been discussed, suggesting a novel platform for designing advanced multiferroic materials with wide applications.Electromagnetic absorption materials have received increasing attention owing to their wide applications in aerospace, communication and the electronics industry, and multiferroic materials with both polarization and magnetic properties are considered promising ceramics for microwave absorption application. However, the insufficient absorption intensity coupled with the narrow effective absorption bandwidth has limited the development of high-performance multiferroic materials for practical microwave absorption. To address such issues, in the present work, we utilize interfacial engineering in BiFeO3 nanoparticles via Ca doping, with the purpose of tailoring the phase boundary. Upon Ca-substitution, the co-existence of both R3c and P4mm phases has been confirmed to massively enhance both dielectric and magnetic properties via manipulating the phase boundary and the destruction of the spiral spin structure. Unlike the commonly reported magnetic/dielectric hybrid microwave absorption composites, Bi0.95Ca0.05FeO3 has been found to deliver unusual continuous dual absorption peaks at a small thickness (1.56 mm), which has remarkably broadened the effective absorption bandwidth (8.7-12.1 GHz). The fundamental mechanisms based on the phase boundary engineering have been discussed, suggesting a novel platform for designing advanced multiferroic materials with wide applications. Electronic supplementary information (ESI) available. See DOI: 10.1039/c6nr00223d

Lightweight and efficient microwave absorbing materials based on walnut shell-derived nano-porous carbon.

PubMed

Qiu, Xu; Wang, Lixi; Zhu, Hongli; Guan, Yongkang; Zhang, Qitu

2017-06-08

Lightweight microwave absorbing materials have drawn tremendous attention. Herein, nano-porous biomass carbon materials have been prepared by carbonization with a subsequent potassium hydroxide activation of walnut shells and the microwave absorption properties have also been investigated. The obtained samples have large specific surface areas with numerous micropores and nanopores. The sample activated at 600 °C with a specific surface area of 736.2 m 2 g -1 exhibits the most enhanced microwave absorption performance. It has the maximum reflection loss of -42.4 dB at 8.88 GHz and the effective absorption bandwidth (reflection loss below -10 dB) is 1.76 GHz (from 8.08 GHz to 9.84 GHz), corresponding to a thickness of 2 mm. Additionally, the effective absorption bandwidth can reach 2.24 GHz (from 10.48 GHz to 12.72 GHz) when the absorber thickness is 1.5 mm. Three-dimensional porous architecture, interfacial polarization relaxation loss, and the dipolar relaxation loss make a great contribution to the excellent microwave absorption performance. In contrast, the non-activated sample with lower specific surface area (435.3 m 2 g -1 ) has poor microwave absorption performance due to a poor dielectric loss capacity. This comparison highlights the role of micropores and nanopores in improving the dielectric loss property of porous carbon materials. To sum up, porous biomass carbon has great potential to become lightweight microwave absorbers. Moreover, KOH is an efficient activation agent in the fabrication of carbonaceous materials.

Influence of external magnetic field on the microwave absorption properties of carbonyl iron and polychloroprene composites film

NASA Astrophysics Data System (ADS)

Wang, Haiyan; Li, Mingjie; Li, Xueai

2016-12-01

The carbonyl iron particles were dispersed in a polychloroprene rubber (CR) matrix under a magnetic field for a practical application as microwave absorption composites film. In comparison with the carbonyl iron particles (CIP)/CR composites film prepared by general route, such films made with external magnetic field exhibit excellent microwave absorption properties, strongly depending on the increment of anisotropy and rearrangement of magnetic particles. The film made under external magnetic field with a thickness of only 0.54 mm shows least reflection loss of -15.98 dB and the reflection loss value less than -10.0 dB over the frequency range of 11.4˜14.8 GHz. The results indicated the composite film made under external magnetic field have excellent microwave absorption properties, which suggest that the composites thin film could be used as a thinner and lighter microwave absorber.

Resonance lamp absorption measurement of OH number density and temperature in expansion tube scramjet engine tests

NASA Technical Reports Server (NTRS)

Lempert, Walter R.; Trucco, Richard E.; Bittner, Robert D.

1992-01-01

In this paper, we report results of hydroxyl radical and static temperature measurements performed in the General Applied Science Laboratories-NASA HYPULSE expansion tube facility using the microwave resonance lamp absorption technique. Data were obtained as part of a series of hydrogen/air and hydrogen/oxygen combustion tests at stagnation enthalpies corresponding to Mach 17 flight speeds. Data from a representative injector configuration is compared to a full Navier-Stokes CFD solution.

Microwave absorption in powders of small conducting particles for heating applications.

PubMed

Porch, Adrian; Slocombe, Daniel; Edwards, Peter P

2013-02-28

In microwave chemistry there is a common misconception that small, highly conducting particles heat profusely when placed in a large microwave electric field. However, this is not the case; with the simple physical explanation that the electric field (which drives the heating) within a highly conducting particle is highly screened. Instead, it is the magnetic absorption associated with induction that accounts for the large experimental heating rates observed for small metal particles. We present simple principles for the effective heating of particles in microwave fields from calculations of electric and magnetic dipole absorptions for a range of practical values of particle size and conductivity. For highly conducting particles, magnetic absorption dominates electric absorption over a wide range of particle radii, with an optimum absorption set by the ratio of mean particle radius a to the skin depth δ (specifically, by the condition a = 2.41δ). This means that for particles of any conductivity, optimized magnetic absorption (and hence microwave heating by magnetic induction) can be achieved by simple selection of the mean particle size. For weakly conducting samples, electric dipole absorption dominates, and is maximized when the conductivity is approximately σ ≈ 3ωε(0) ≈ 0.4 S m(-1), independent of particle radius. Therefore, although electric dipole heating can be as effective as magnetic dipole heating for a powder sample of the same volume, it is harder to obtain optimized conditions at a fixed frequency of microwave field. The absorption of sub-micron particles is ineffective in both magnetic and electric fields. However, if the particles are magnetic, with a lossy part to their complex permeability, then magnetic dipole losses are dramatically enhanced compared to their values for non-magnetic particles. An interesting application of this is the use of very small magnetic particles for the selective microwave heating of biological samples.

Effect of Zn doping on the microwave absorption of BFO multiferroic materials

NASA Astrophysics Data System (ADS)

Bi, S.; Li, J.; Mei, B.; Su, X. J.; Ying, C. Z.; Li, P. H.

2018-01-01

The microwave absorbing materials were firstly used in the Second World War. And the BiFeO3 (BFO) based microwave absorbers have been widely applied into the microwave absorbing area due to its possession of excellent electromagnetic properties. Various methods have been conducted to improve the microwave absorption performance of the BFO based materials. In the work, the sol-gel method were used to prepare the BFO, and the Zn were doped into the BFO to prepare the Bi1-xZnxFeO3 nanoparticles. The X-ray diffraction, scanning electron microscope, and vector network analysis (VNA) were conducted to characterize the microstructure and electromagnetic properties of the as-prepared samples. The results indicate that the Bi1-xZnxFeO3 nanoparticles were successfully gained and the as-prepared samples possess excellent microwave absorption properties.

Flux flow induced microwave absorption in high temperature superconductor Bi 2-XPb XSr 2Ca N-1Cu NO 4+2N

NASA Astrophysics Data System (ADS)

Owens, F. J.

1990-12-01

Direct measurements of microwave absorption without use of rf H field modulation in granular composites of the 115 K superconductor Bi 2-XPb XSr 2Ca N-1Cu NO 4+2N as a function of magnetic field above 0.1 T reveal a continuing increase of absorption of microwave energy increasing magnetic field. The temperature and magnetic field dependence of the absorption are very different from the low magnetic field (<0.01 T) absorption arising from weak links in the material. The magnetic field and temperature dependence are consistent with the behavior of thermally activated flux flow resistance suggesting the absorption is due to flux creep.

On the application of cw external cavity quantum cascade infrared lasers for plasma diagnostics

NASA Astrophysics Data System (ADS)

Lopatik, D.; Lang, N.; Macherius, U.; Zimmermann, H.; Röpcke, J.

2012-11-01

Three continuous wave external cavity quantum cascade lasers (EC-QCLs) operating between 1305 and 2260 cm-1 (4.42-7.66 µm) have been tested as radiation sources for an absorption spectrometer focused on the analysis of physical and chemical phenomena in molecular plasmas. Based on the wide spectral tunability of EC-QCLs, multiple species detection has become feasible and is demonstrated in a study of low-pressure Ar/N2 microwave plasmas containing methane as a hydrocarbon precursor. Using the direct absorption technique, the evolution of the concentrations of CH4, C2H2, HCN and H2O has been monitored depending on the discharge conditions at a pressure of p = 0.5 mbar and at a frequency of f = 2.45 GHz in a planar microwave plasma reactor. The concentrations were found to be in the range of 1011-1014 molecules cm-3. In addition, based on the analysis of the line profile of selected absorption lines, the gas temperature Tg has been calculated in dependence on the discharge power. Tg increased with the power values and was in the range between 400 and 700 K. Further, in a pure He/Ar microwave plasma, the wavelength modulation spectroscopy technique has been applied for the sensitive detection of transient plasma species with absorbencies down to 10-5. The typical spectral line width of an EC-QCL under the study was found to be in the range 24 to 38 MHz depending (i) on the chopping technique used and (ii) on a single or averaged measurement approach. Further, different methods for the modulation and tuning of the laser radiation have been tested. Varying the power values of an EC-QCL between 0.1 and 154 mW for direct absorption measurements under low pressure conditions, no saturation effects in determining the concentrations of methane, acetylene and carbon monoxide could be found under the experimental conditions used, i.e. for lines with line strengths between 10-19 and 10-22 cm molecule-1.

A theoretical study of microwave beam absorption by a rectenna

NASA Technical Reports Server (NTRS)

Ott, J. H.; Rice, J. S.; Thorn, D. C.

1980-01-01

The rectenna's microwave power beam absorption limit was theoretically confirmed by two mathematical models descriptive of the microwave absorption process; first one model was based on the current sheet equivalency of a large planar array above a reflector and the second model, which was based on the properties of a waveguide with special imaging characteristics, quantified the electromagnetic modes (field configurations) in the immediate vicinity of a Rectenna element spacing which permit total power beam absorption by preventing unwanted modes from propagating (scattering) were derived using these models. Several factors causing unwanted scattering are discussed.

A selective review of ground based passive microwave radiometric probing of the atmosphere

NASA Technical Reports Server (NTRS)

Welch, W. J.

1969-01-01

The absorption of the various atmospheric constituents with significant microwave spectra is reviewed. Based on the available data, an estimate is made of the uncertainty in the microwave absorption coefficients of the major constituents, water vapor and oxygen. Then there is an examination of the integral equations which describe the three basic types of observations: measurement of the spectrum of absorption of the sun's radiation by an atmospheric constituent, measurement of the emission spectrum of a constituent, and measurement at one frequency of the zenith angle dependence of the absorption or emission of the atmosphere.

Magnetoabsorption and magnetic hysteresis in Ni ferrite nanoparticles

NASA Astrophysics Data System (ADS)

Hernández-Gómez, P.; Muñoz, J. M.; Valente, M. A.; Torres, C.; de Francisco, C.

2013-01-01

Nickel ferrite nanoparticles were prepared by a modified sol-gel technique employing coconut oil, and then annealed at different temperatures in 400-1200 °C range. This route of preparation has revealed to be one efficient and cheap technique to obtain high quality nickel ferrite nanosized powder. Sample particles sizes obtained with XRD data and Scherrer's formula lie in 13 nm to 138 nm, with increased size with annealing temperature. Hysteresis loops have been obtained at room temperature with an inductive method. Magnetic field induced microwave absorption in nanoscale ferrites is a recent an active area of research, in order to characterize and explore potential novel applications. In the present work microwave magnetoabsorption data of the annealed nickel ferrite nanoparticles are presented. These data have been obtained with a system based on a network analyzer that operates in the frequency range 0 - 8.5 GHz. At fields up to 400 mT we can observe a peak according to ferromagnetic resonance theory. Sample annealed at higher temperature exhibits different absorption, coercivity and saturation magnetization figures, revealing its multidomain character.

Unusual continuous dual absorption peaks in Ca-doped BiFeO3 nanostructures for broadened microwave absorption.

PubMed

Li, Zhong-Jun; Hou, Zhi-Ling; Song, Wei-Li; Liu, Xing-Da; Cao, Wen-Qiang; Shao, Xiao-Hong; Cao, Mao-Sheng

2016-05-21

Electromagnetic absorption materials have received increasing attention owing to their wide applications in aerospace, communication and the electronics industry, and multiferroic materials with both polarization and magnetic properties are considered promising ceramics for microwave absorption application. However, the insufficient absorption intensity coupled with the narrow effective absorption bandwidth has limited the development of high-performance multiferroic materials for practical microwave absorption. To address such issues, in the present work, we utilize interfacial engineering in BiFeO3 nanoparticles via Ca doping, with the purpose of tailoring the phase boundary. Upon Ca-substitution, the co-existence of both R3c and P4mm phases has been confirmed to massively enhance both dielectric and magnetic properties via manipulating the phase boundary and the destruction of the spiral spin structure. Unlike the commonly reported magnetic/dielectric hybrid microwave absorption composites, Bi0.95Ca0.05FeO3 has been found to deliver unusual continuous dual absorption peaks at a small thickness (1.56 mm), which has remarkably broadened the effective absorption bandwidth (8.7-12.1 GHz). The fundamental mechanisms based on the phase boundary engineering have been discussed, suggesting a novel platform for designing advanced multiferroic materials with wide applications.

Thermal effects of X-band microwaves on skin tissues

NASA Astrophysics Data System (ADS)

Song, Kyo D.; Yoon, Hargsoon; Lee, Kunik; Kim, Jaehwan; Choi, Sang H.

2012-04-01

Microwave can be used as a power carrier to implanted medical devices wirelessly, which is regarded as one of the attractive features for medical applications. The loss mechanism of microwave transmission through lossy media often appears as a thermal effect due to the absorption of microwave. Such a thermal effect on human tissue has not rigorously studied yet. The thermal effect on living tissues was experimentally tested with animal skins to understand the absorption characteristics of microwave. In this paper, the frequency range of microwave used for the tests was from 6 GHz to 13 GHz.

Microwave absorption in substances that form hydration layers with water

NASA Astrophysics Data System (ADS)

Garner, H. R.; Ohkawa, T.; Tuason, O.; Lee, R. L.

1990-12-01

The microwave absorption of certain water soluble polymers (polyethylene glycol, polyvinyl pyrrolidone, proteins, and DNA) in solution is composed of three parts: absorption in the free water, absorption in the substance, and absorption in the hydration layer. Ethanol, sucrose, glycerol, and sodium acetate, which form weak hydrogen bonds or have an ionic nature in aqueous solutions, also have microwave absorption signatures similar to polymers that form hydration layers. The frequency-dependent absorption of the free water and of the hydration layer water is described by a simple Debye relaxation model. The absorption per unit sample volume attributable to the hydration layer is solute concentration dependent, and a simple model is used to describe the dependence. The hydration-layer relaxation time was found to vary from substance to substance and with solute concentration. The relaxation time was also found to be independent of solute length.

Determination of trace nickel in hydrogenated cottonseed oil by electrothermal atomic absorption spectrometry after microwave-assisted digestion.

PubMed

Zhang, Gai

2012-01-01

Microwave digestion of hydrogenated cottonseed oil prior to trace nickel determination by electrothermal atomic absorption spectrometry (ETAAS) is proposed here for the first time. Currently, the methods outlined in U.S. Pharmacopeia 28 (USP28) or British Pharmacopeia (BP2003) are recommended as the official methods for analyzing nickel in hydrogenated cottonseed oil. With these methods the samples may be pre-treated by a silica or a platinum crucible. However, the samples were easily tarnished during sample pretreatment when using a silica crucible. In contrast, when using a platinum crucible, hydrogenated cottonseed oil acting as a reducing material may react with the platinum and destroy the crucible. The proposed microwave-assisted digestion avoided tarnishing of sample in the process of sample pretreatment and also reduced the cycle of analysis. The programs of microwave digestion and the parameters of ETAAS were optimized. The accuracy of the proposed method was investigated by analyzing real samples. The results were compared with the ones by pressurized-PTFE-bomb acid digestion and ones obtained by the U.S. Pharmacopeia 28 (USP28) method. The new method involves a relatively rapid matrix destruction technique compared with other present methods for the quantification of metals in oil. © 2011 Institute of Food Technologists®

Broadband and tunable high-performance microwave absorption of an ultralight and highly compressible graphene foam.

PubMed

Zhang, Yi; Huang, Yi; Zhang, Tengfei; Chang, Huicong; Xiao, Peishuang; Chen, Honghui; Huang, Zhiyu; Chen, Yongsheng

2015-03-25

The broadband and tunable high-performance microwave absorption properties of an ultralight and highly compressible graphene foam (GF) are investigated. Simply via physical compression, the microwave absorption performance can be tuned. The qualified bandwidth coverage of 93.8% (60.5 GHz/64.5 GHz) is achieved for the GF under 90% compressive strain (1.0 mm thickness). This mainly because of the 3D conductive network. © 2015 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Microwave absorption properties of reduced graphene oxide strontium hexaferrite/poly(methyl methacrylate) composites

NASA Astrophysics Data System (ADS)

Acharya, Sanghamitra; Ray, J.; Patro, T. U.; Alegaonkar, Prashant; Datar, Suwarna

2018-03-01

The key factors to consider when designing microwave absorber materials for eradication of electromagnetic (EM) pollution are absorption of incident EM waves and good impedance matching. By keeping these things in mind, flexible microwave absorber composite films can be fabricated by simple gel casting techniques using reduced graphene oxide (RGO) and strontium ferrite (SF) in a poly(methyl methacrylate) (PMMA) matrix. SF nanoparticles are synthesized by the well known sol-gel method. Subsequently, reduced graphene oxide (RGO) and SF nanocomposite (RGOSF) are prepared through a chemical reduction method using hydrazine. The structure, morphology, chemical composition, thermal stability and magnetic properties of the nanocomposite are characterized in detail by various techniques. The SF particles are found to be nearly 500 nm and decorated on RGO sheets as revealed by field emission scanning electron microscopy and transmission electron microscopy analysis. Fourier transform infrared and and Raman spectroscopy clearly show the presence of SF in the graphene sheet by the lower peak positions. Finally, ternary polymer composites of RGO/SF/PMMA are prepared by an in situ polymerization method. Magnetic and dielectric studies of the composite reveal that the presence of RGO/SF/PMMA lead to polarization effects contributing to dielectric loss. Also, RGO surrounding SF provides a conductive network in the polymer matrix which is in turn responsible for the magnetic loss in the composite. Thus, the permittivity as well as the permeability of the composite can be controlled by an appropriate combination of RGO and SF in PMMA. More than 99% absorption efficiency is achieved by a suitable combination of magneto-dielectric coupling in the X-band frequency range by incorporating 9 wt% of RGO and 1 wt% of SF in the polymer matrix.

A microwave pressure sounder. [for remote measurement of atmospheric pressure

NASA Technical Reports Server (NTRS)

Peckham, G. E.; Flower, D. A.

1981-01-01

A technique for the remote measurement of atmospheric surface pressure will be described. Such measurements could be made from a satellite in polar orbit and would cover many areas for which conventional meteorological data are not available. An active microwave instrument is used to measure the strength of return echoes from the ocean surface at a number of frequencies near the 60 GHz oxygen absorption band. Factors which affect the accuracy with which surface pressure can be deduced from these measurements will be discussed and an instrument designed to test the method by making measurements from an aircraft will be described.

BMFO-PVDF electrospun fiber based tunable metamaterial structures for electromagnetic interference shielding in microwave frequency region

NASA Astrophysics Data System (ADS)

Revathi, Venkatachalam; Dinesh Kumar, Sakthivel; Subramanian, Venkatachalam; Chellamuthu, Muthamizhchelvan

2015-11-01

Metamaterial structures are artificial structures that are useful in controlling the flow of electromagnetic radiation. In this paper, composite fibers of sub-micron thickness of barium substituted magnesium ferrite (Ba0.2Mg0.8Fe2O4) - polyvinylidene fluoride obtained by electrospinning is used as a substrate to design electromagnetic interference shielding structures. While electrospinning improves the ferroelectric properties of the polyvinylidene fluoride, the presence of barium magnesium ferrite modifies the magnetic property of the composite fiber. The dielectric and magnetic properties at microwave frequency measured using microwave cavity perturbation technique are used to design the reflection as well as absorption based tunable metamaterial structures for electromagnetic interference shielding in microwave frequency region. For one of the structures, the simulation indicates that single negative metamaterial structure becomes a double negative metamaterial under the external magnetic field.

Microwave absorption properties of carbon nanocoils coated with highly controlled magnetic materials by atomic layer deposition.

PubMed

Wang, Guizhen; Gao, Zhe; Tang, Shiwei; Chen, Chaoqiu; Duan, Feifei; Zhao, Shichao; Lin, Shiwei; Feng, Yuhong; Zhou, Lei; Qin, Yong

2012-12-21

In this work, atomic layer deposition is applied to coat carbon nanocoils with magnetic Fe(3)O(4) or Ni. The coatings have a uniform and highly controlled thickness. The coated nanocoils with coaxial multilayer nanostructures exhibit remarkably improved microwave absorption properties compared to the pristine carbon nanocoils. The enhanced absorption ability arises from the efficient complementarity between complex permittivity and permeability, chiral morphology, and multilayer structure of the products. This method can be extended to exploit other composite materials benefiting from its convenient control of the impedance matching and combination of dielectric-magnetic multiple loss mechanisms for microwave absorption applications.

Design of Miniaturized Double-Negative Material for Specific Absorption Rate Reduction in Human Head

PubMed Central

Faruque, Mohammad Rashed Iqbal; Islam, Mohammad Tariqul

2014-01-01

In this study, a double-negative triangular metamaterial (TMM) structure, which exhibits a resounding electric response at microwave frequency, was developed by etching two concentric triangular rings of conducting materials. A finite-difference time-domain method in conjunction with the lossy-Drude model was used in this study. Simulations were performed using the CST Microwave Studio. The specific absorption rate (SAR) reduction technique is discussed, and the effects of the position of attachment, the distance, and the size of the metamaterials on the SAR reduction are explored. The performance of the double-negative TMMs in cellular phones was also measured in the cheek and the tilted positions using the COMOSAR system. The TMMs achieved a 52.28% reduction for the 10 g SAR. These results provide a guideline to determine the triangular design of metamaterials with the maximum SAR reducing effect for a mobile phone. PMID:25350398

A quasi-classical mechanism for microwave induced resistance oscillations in high mobility GaAs/AlGaAs 2DEG samples

NASA Astrophysics Data System (ADS)

Studenikin, S. A.; Fedorych, O. N.; Maude, D. K.; Potemski, M.; Sachrajda, A. S.; Wasilewski, Z. R.; Gupta, J. A.; Magarill, L. I.

2008-03-01

In this work we investigate microwave induced resistance oscillations (MIROs) in a GaAs/AlGaAs heterostructure containing a high mobility two-dimensional electron gas (2DEG). We show that MIROs can be explained within a purely classical mechanism based on the Boltzmann equation [L.I. Magarill, I.A. Panaev, S.A. Studenikin, Condens. Matter 7 (1995) 1101]. The MIRO-related transitions can be observed in absorption and we demonstrate it experimentally for the first time using EPR-cavity absorption technique. Next we investigate MIROs and Shubnikov-de Haas (SdH) oscillations at milli-Kelvin temperatures. We find that MIROs persist to approximately three times lower magnetic field as compared with the SdH oscillations, which at temperatures below 50 mK are defined purely by the quantum relaxation time. This finding indicates a possible quasi-classical origin of MIROs.

Design of miniaturized double-negative material for specific absorption rate reduction in human head.

PubMed

Faruque, Mohammad Rashed Iqbal; Islam, Mohammad Tariqul

2014-01-01

In this study, a double-negative triangular metamaterial (TMM) structure, which exhibits a resounding electric response at microwave frequency, was developed by etching two concentric triangular rings of conducting materials. A finite-difference time-domain method in conjunction with the lossy-Drude model was used in this study. Simulations were performed using the CST Microwave Studio. The specific absorption rate (SAR) reduction technique is discussed, and the effects of the position of attachment, the distance, and the size of the metamaterials on the SAR reduction are explored. The performance of the double-negative TMMs in cellular phones was also measured in the cheek and the tilted positions using the COMOSAR system. The TMMs achieved a 52.28% reduction for the 10 g SAR. These results provide a guideline to determine the triangular design of metamaterials with the maximum SAR reducing effect for a mobile phone.

Full-time response of starch subjected to microwave heating.

PubMed

Fan, Daming; Wang, Liyun; Zhang, Nana; Xiong, Lei; Huang, Luelue; Zhao, Jianxin; Wang, Mingfu; Zhang, Hao

2017-06-21

The effect of non-ionizing microwave radiation on starch is due to a gelatinization temperature range that changes starch structure and properties. However, the changes in starch upon microwave heating are observable throughout the heating process. We compared the effects on starch heating by microwaves to the effects by rapid and regular conventional heating. Our results show that microwave heating promotes the rapid rearrangement of starch molecules at low temperatures; starch showed a stable dielectric response and a high dielectric constant. Microwave heating changed the Cole-Cole curve and the polarization of starch suspension at low temperatures. A marked transition at 2.45 GHz resulted in a double-polarization phenomenon. At temperatures below gelatinization, microwave-induced dielectric rearrangement and changes in the polarization characteristics of starch suspensions reduced the absorption properties; at temperatures above gelatinization, these characteristics became consistent with conventional heating. Throughout the heating process, microwaves change the electrical response and polarization characteristics of the starch at low temperatures, but on the macro level, there is no enhancement of the material's microwave absorption properties. In contrast, with the warming process, the starch exhibited a "blocking effect", and the absorption properties of the starch quickly returned to the level observed in conductive heating after gelatinization.

A theoretical study of microwave beam absorption by a Rectenna

NASA Technical Reports Server (NTRS)

Ott, J. H.; Rice, J. S.; Thorn, D. C.

1980-01-01

The results of a theoretical study of microwave beam absorption by a rectenna is given. Total absorption of power beam is shown to be theoretically possible. Several improvements in the rectenna design are indicated as a result of analytic modeling. The nature of rectenna scattering and atmospheric effects is discussed.

A theoretical study of microwave beam absorption by a rectenna

NASA Technical Reports Server (NTRS)

Ott, J. H.; Rice, J. S.; Thorn, D. C.

1981-01-01

The results of a theoretical study of microwave beam absorption by a Rectenna are given. Total absorption of the power beam is shown to be theoretically possible. Several improvements in the Rectenna design are indicated as a result of analytic modeling. The nature of Rectenna scattering and atmospheric effects are discussed.

Microwave absorption properties of gold nanoparticle doped polymers

NASA Astrophysics Data System (ADS)

Jiang, C.; Ouattara, L.; Ingrosso, C.; Curri, M. L.; Krozer, V.; Boisen, A.; Jakobsen, M. H.; Johansen, T. K.

2011-03-01

This paper presents a method for characterizing microwave absorption properties of gold nanoparticle doped polymers. The method is based on on-wafer measurements at the frequencies from 0.5 GHz to 20 GHz. The on-wafer measurement method makes it possible to characterize electromagnetic (EM) property of small volume samples. The epoxy based SU8 polymer and SU8 doped with gold nanoparticles are chosen as the samples under test. Two types of microwave test devices are designed for exciting the samples through electrical coupling and magnetic coupling, respectively. Measurement results demonstrate that the nanocomposites absorb a certain amount of microwave energy due to gold nanoparticles. Higher nanoparticle concentration results in more significant absorption effect.

Dielectric Characteristics and Microwave Absorption of Graphene Composite Materials

PubMed Central

Rubrice, Kevin; Castel, Xavier; Himdi, Mohamed; Parneix, Patrick

2016-01-01

Nowadays, many types of materials are elaborated for microwave absorption applications. Carbon-based nanoparticles belong to these types of materials. Among these, graphene presents some distinctive features for electromagnetic radiation absorption and thus microwave isolation applications. In this paper, the dielectric characteristics and microwave absorption properties of epoxy resin loaded with graphene particles are presented from 2 GHz to 18 GHz. The influence of various parameters such as particle size (3 µm, 6–8 µm, and 15 µm) and weight ratio (from 5% to 25%) are presented, studied, and discussed. The sample loaded with the smallest graphene size (3 µm) and the highest weight ratio (25%) exhibits high loss tangent (tanδ = 0.36) and a middle dielectric constant ε′ = 12–14 in the 8–10 GHz frequency range. As expected, this sample also provides the highest absorption level: from 5 dB/cm at 4 GHz to 16 dB/cm at 18 GHz. PMID:28773948

Microwave absorbance properties of zirconium–manganese substituted cobalt nanoferrite as electromagnetic (EM) wave absorbers

DOE Office of Scientific and Technical Information (OSTI.GOV)

Khan, Kishwar, E-mail: kknano@hotmail.com; Rehman, Sarish

2014-02-01

Highlights: • Good candidates for EM materials with low reflectivity. • Good candidates for broad bandwidth at microwave frequency. • Microwave absorbing bandwidth was modulated simply by manipulating the Zr–Mn. • Higher the Zr–Mn content, the higher absorption rates for the electromagnetic radiation. • The predicted reflection loss shows that this can be used for thin ferrite absorber. - Abstract: Nanocrystalline Zr–Mn (x) substituted Co ferrite having chemical formula CoFe{sub 2−2x}Zr{sub x}Mn{sub x}O{sub 4} (x = 0.1–0.4) was prepared by co-precipitation technique. Combining properties such as structural, electrical, magnetic and reflection loss characteristics. Crystal structure and surface morphology of themore » calcined samples were characterized by X-ray diffraction analysis (XRD) and scanning electron microscopy (SEM). By using two point probe homemade resistivity apparatus to find resistivity of the sample. Electromagnetic (EM) properties are measured through RF impedance/materials analyzer over 1 MHz–3 GHz. The room-temperature dielectric measurements show dispersion behavior with increasing frequency from 100 Hz to 3 MHz. Magnetic properties confirmed relatively strong dependence of saturation magnetization on Zr–Mn composition. Curie temperature is also found to decrease linearly with addition of Zr–Mn. Furthermore, comprehensive analysis of microwave reflection loss (RL) is carried out as a function of substitution, frequency, and thickness. Composition accompanying maximum microwave absorption is suggested.« less

Broadening microwave absorption via a multi-domain structure

NASA Astrophysics Data System (ADS)

Liu, Zhengwang; Che, Renchao; Wei, Yong; Liu, Yupu; Elzatahry, Ahmed A.; Dahyan, Daifallah Al.; Zhao, Dongyuan

2017-04-01

Materials with a high saturation magnetization have gained increasing attention in the field of microwave absorption; therefore, the magnetization value depends on the magnetic configuration inside them. However, the broad-band absorption in the range of microwave frequency (2-18 GHz) is a great challenge. Herein, the three-dimensional (3D) Fe/C hollow microspheres are constructed by iron nanocrystals permeating inside carbon matrix with a saturation magnetization of 340 emu/g, which is 1.55 times as that of bulk Fe, unexpectedly. Electron tomography, electron holography, and Lorentz transmission electron microscopy imaging provide the powerful testimony about Fe/C interpenetration and multi-domain state constructed by vortex and stripe domains. Benefiting from the unique chemical and magnetic microstructures, the microwave minimum absorption is as strong as -55 dB and the bandwidth (<-10 dB) spans 12.5 GHz ranging from 5.5 to 18 GHz. Morphology and distribution of magnetic nano-domains can be facilely regulated by a controllable reduction sintering under H2/Ar gas and an optimized temperature over 450-850 °C. The findings might shed new light on the synthesis strategies of the materials with the broad-band frequency and understanding the association between multi-domain coupling and microwave absorption performance.

Resonance lamp absorption technique for simultaneous determination of the OH concentration and temperature at 10 spatial positions in combustion environments

NASA Technical Reports Server (NTRS)

Shirinzadeh, B.; Gregory, Ray W.

1994-01-01

A rugged, easy to implement, line-of-sight absorption instrument which utilizes a low pressure water vapor microwave discharge cell as the light source, has been developed to make simultaneous measurements of the OH concentration and temperature at 10 spatial positions. The design, theory, and capability of the instrument are discussed. Results of the measurements obtained on a methane/air flat flame burner are compared with those obtained using a single-frequency, tunable dye laser system.

Electromagnetic interference attenuation and shielding effect of quaternary Epoxy-PPy/Fe3O4-ZnO nanocomposite as a broad band microwave-absorber

NASA Astrophysics Data System (ADS)

Olad, Ali; Shakoori, Sahar

2018-07-01

An increase in the electromagnetic wave pollution generated from wireless telecommunication devices has devoted to a great request for exploiting microwave absorbing materials for themselves. The combination of inherently conducting polymers such as polypyrrole (PPy) with metal oxides has led to design ideal microwave absorbing materials which benefit both advantage effects of ICPs and metal oxide nanoparticles. Herein, the quaternary nanocomposite of Epoxy-PPy/Fe3O4-ZnO was prepared and tested for the absorption of X-band microwaves. Simultaneous application of metal oxides and conducting polypyrrole in the epoxy matrix was evaluated in order to increase the absorption intensity and broadness of microwaves in X-band region. The morphology, microstructure, and phase structure of Fe3O4, ZnO, and PPy, as well as quaternary nanocomposite were characterized and studied using FTIR, XRD, FESEM and TEM techniques. The presence of nanoparticles in the quaternary nanocomposite was confirmed by EDS. The magnetization of iron oxide was studied by VSM. The synergetic effect of iron oxide and zinc oxide nanoparticles in different weight ratios (Fe3O4/ZnO) on the electromagnetic wave absorption was evaluated. The electromagnetic parameters have been evaluated by the vector network analyzer in the frequency range of 8.2-12.4 GHz which is named as X-band region and is adequate for radar applications. The electromagnetic wave absorbing outcomes indicated that Epoxy-PPy/Fe3O4-ZnO quaternary nanocomposite has wide absorption area and high attenuation, which is believed to be due to dielectric loss properties related to the polypyrrole, magnetic loss factor of Fe3O4, and synergetic effects of components. The maximum reflection loss reached to -32.53 dB at 9.96 GHz with a nanocomposite thickness of 2 mm which is dedicated to the Epoxy-PPy/Fe3O4-ZnO with iron oxide to zinc oxide ratio of 2:1. The absorption bandwidth with the reflection loss lower than -10 dB (90% attenuation) was up to 4.2 GHz that covering a frequency range of 8.2-12.4 GHz. Results showed that absorber having %15 (w/w) polypyrrole/epoxy resin in Epoxy-PPy/Fe3O4-ZnO nanocomposite with iron oxide to zinc oxide ratio of 2:1 displays the best reflection loss properties. The loss curves illustrated the values of dielectric loss tangent and magnetic loss tangent of prepared nanocomposites which are in the range of 0.25-0.7 and -0.08 to 0.09 respectively. Therefore, microwave absorption mechanism is probably attributed to dielectric loss.

Micro-quantity tissue digestion for metal measurements by use of a microwave acid-digestion bomb.

PubMed

Nicholson, J R; Savory, M G; Savory, J; Wills, M R

1989-03-01

We describe a simple and convenient method for processing small amounts of tissue samples for trace-metal measurements by atomic absorption spectrometry, by use of a modified Parr microwave digestion bomb. Digestion proceeds rapidly (less than or equal to 90 s) in a sealed Teflon-lined vessel that eliminates contamination or loss from volatilization. Small quantities of tissue (5-100 mg dry weight) are digested in high-purity nitric acid, yielding concentrations of analyte that can be measured directly without further sample manipulation. We analyzed National Institute of Standards and Technology bovine liver Standard Reference Material to verify the accuracy of the technique. We assessed the applicability of the technique to analysis for aluminum in bone by comparison with a dry ashing procedure.

Influence of Reduced Graphene Oxide on Effective Absorption Bandwidth Shift of Hybrid Absorbers.

PubMed

Ameer, Shahid; Gul, Iftikhar Hussain

2016-01-01

The magnetic nanoparticle composite NiFe2O4 has traditionally been studied for high-frequency microwave absorption with marginal performance towards low-frequency radar bands (particularly L and S bands). Here, NiFe2O4 nanoparticles and nanohybrids using large-diameter graphene oxide (GO) sheets are prepared via solvothermal synthesis for low-frequency wide bandwidth shielding (L and S radar bands). The synthesized materials were characterized using XRD, SEM, FTIR and microwave magneto dielectric spectroscopy. The dimension of these solvothermally synthesized pristine particles and hybrids lies within 30-58 nm. Microwave magneto-dielectric spectroscopy was performed in the low-frequency region in the 1 MHz-3 GHz spectrum. The as-synthesized pristine nanoparticles and hybrids were found to be highly absorbing for microwaves throughout the L and S radar bands (< -10 dB from 1 MHz to 3 GHz). This excellent microwave absorbing property induced by graphene sheet coupling shows application of these materials with absorption bandwidth which is tailored such that these could be used for low frequency. Previously, these were used for high frequency absorptions (typically > 4 GHz) with limited selective bandwidth.

Dependency of magnetic microwave absorption on surface architecture of Co20Ni80 hierarchical structures studied by electron holography

NASA Astrophysics Data System (ADS)

Liu, Qinhe; Xu, Xianhui; Xia, Weixing; Che, Renchao; Chen, Chen; Cao, Qi; He, Jingang

2015-01-01

To design and fabricate rational surface architecture of individual particles is one of the key factors that affect their magnetic properties and microwave absorption capability, which is still a great challenge. Herein, a series of Co20Ni80 hierarchical structures with different surface morphologies, including flower-, urchin-, ball-, and chain-like morphologies, were obtained using structure-directing templates via a facile one-step solvothermal treatment. The microwave reflection loss (RL) of urchin-like Co20Ni80 hierarchical structures reaches as high as -33.5 dB at 3 GHz, with almost twice the RL intensity of the ball- and chain-like structures, and the absorption bandwidth (<-10 dB) is about 5.5 GHz for the flower-like morphology, indicating that the surface nanospikes and nanoflakes on the Co20Ni80 microsphere surfaces have great influences on their magnetic microwave absorption properties. Electron holography analysis reveals that the surface nanospikes and nanoflakes could generate a high density of stray magnetic flux lines and contribute a large saturation magnetization (105.62 emu g-1 for urchin-like and 96.41 emu g-1 for flower-like morphology), leading the urchin-like and flower-like Co20Ni80 to possess stronger microwave RL compared with the ball-like and chain-like Co20Ni80 alloys. The eddy-current absorption mechanism μ''(μ')-2(f)-1 is dominant in the frequency region above 8 GHz, implying that eddy-current loss is a vital factor for microwave RL in the high frequency range. It can be supposed from our findings that different surface morphologies of magnetic hierarchical structures might become an effective path to achieve high-performance microwave absorption for electromagnetic shielding and stealth camouflage applications.To design and fabricate rational surface architecture of individual particles is one of the key factors that affect their magnetic properties and microwave absorption capability, which is still a great challenge. Herein, a series of Co20Ni80 hierarchical structures with different surface morphologies, including flower-, urchin-, ball-, and chain-like morphologies, were obtained using structure-directing templates via a facile one-step solvothermal treatment. The microwave reflection loss (RL) of urchin-like Co20Ni80 hierarchical structures reaches as high as -33.5 dB at 3 GHz, with almost twice the RL intensity of the ball- and chain-like structures, and the absorption bandwidth (<-10 dB) is about 5.5 GHz for the flower-like morphology, indicating that the surface nanospikes and nanoflakes on the Co20Ni80 microsphere surfaces have great influences on their magnetic microwave absorption properties. Electron holography analysis reveals that the surface nanospikes and nanoflakes could generate a high density of stray magnetic flux lines and contribute a large saturation magnetization (105.62 emu g-1 for urchin-like and 96.41 emu g-1 for flower-like morphology), leading the urchin-like and flower-like Co20Ni80 to possess stronger microwave RL compared with the ball-like and chain-like Co20Ni80 alloys. The eddy-current absorption mechanism μ''(μ')-2(f)-1 is dominant in the frequency region above 8 GHz, implying that eddy-current loss is a vital factor for microwave RL in the high frequency range. It can be supposed from our findings that different surface morphologies of magnetic hierarchical structures might become an effective path to achieve high-performance microwave absorption for electromagnetic shielding and stealth camouflage applications. Electronic supplementary information (ESI) available: EDS analysis data, SEM images, electron holography schematic diagram, electron holography and magnetic hysteresis loops. See DOI: 10.1039/c4nr05547k

CaCu3Ti4O12 particles and MWCNT-filled microwave absorber with improved microwave absorption by FSS incorporation

NASA Astrophysics Data System (ADS)

Qing, Yuchang; Yang, Zhaoning; Wen, Qinlong; Luo, Fa

2016-07-01

Multi-walled carbon nanotube (MWCNTs)- and CaCu3Ti4O12 (CCTO) particle-filled epoxy microwave absorbing coatings were prepared, and their electromagnetic properties and reflection loss (RL) were investigated in the frequency range 8.2-12.4 GHz. The microstructures of these coatings exhibit a uniform dispersion of MWCNTs and CCTO particles in the matrix. The value and frequency dependency of complex permittivity of such coatings enhanced with increasing MWCNT content. Frequency-selective surface was used to improve their microwave absorption (both the operating bandwidth and minimum RL) without increasing the absorber thickness. Such absorber showed high microwave absorbing performance, and the bandwidth of the RL below -8 dB (more than 84.1 % absorption) can be obtained in the whole X-band with a thickness of 1.5 mm.

A new method for the preparation of a Fe{sub 3}O{sub 4}/graphene hybrid material and its applications in electromagnetic wave absorption

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wu, Tsung-Yung; Lu, Kai-Tai; Peng, Cheng-Hsiung

2015-10-15

Graphical abstract: A microwave-assisted solvothermal process was used to prepare Fe{sub 3}O{sub 4} nanoparticles/graphene hybrids, which could be applied as an electromagnetic (EM) radiation absorbent. The absorber, composed of 20 wt% Fe{sub 3}O{sub 4}/graphene–epoxy, exhibited a dual-frequency reflection characteristic covering the C and Ku bands with maximum reflection losses of less than −20 dB at thicknesses of 4 and 5 mm. - Highlights: • Fe{sub 3}O{sub 4}/graphene composites were prepared by a microwave-assisted solvothermal route. • Uniform loading of Fe{sub 3}O{sub 4} nanoparticles on graphene was obtained. • The products as-synthesized show great promise as a microwave absorption material. •more » Synergistic effects of Fe{sub 3}O{sub 4} and graphene caused improved absorption efficiency. • The Fe{sub 3}O{sub 4}/graphene product possessed a dual-frequency reflection characteristic. - Abstract: A rapid, simple, and inexpensive process combining a microwave-assisted technique and a solvothermal method has been developed using graphene sheets and FeCl{sub 3}·6H{sub 2}O as the reactant to prepare graphene/Fe{sub 3}O{sub 4} nanoparticle hybrids, which can be applied as an electromagnetic radiation absorbent. The experimental factors (i.e., composition ratio, microwave power, and irradiation time) on the products’ characteristics were examined. Under optimal conditions, the morphological analysis revealed that the graphene sheet was homogeneously covered with Fe{sub 3}O{sub 4} nanoparticles (∼50 nm). The electromagnetic parameters of the composites made from 20 wt% Fe{sub 3}O{sub 4}/graphene–epoxy were measured by a vector network analyzer. It was found that the 4- and 5 mm-thick composites could attain a reflection loss below −20 dB in the dual-ranges of 4–8 and 12–18 GHz.« less

Facile synthesis of Fe3O4/C composites for broadband microwave absorption properties

NASA Astrophysics Data System (ADS)

Liu, Xiang; Ma, Yating; Zhang, Qinfu; Zheng, Zhiming; Wang, Lai-Sen; Peng, Dong-Liang

2018-07-01

Rod-like and flower-like Fe3O4/C composites were successfully synthesized via a facile approach in aqueous phase. The morphologies, structures and static magnetic properties of as-prepared rod-like and flower-like Fe3O4/C composites were characterized thoroughly. The relative complex permittivity and permeability of Fe3O4/C/paraffin composites were recorded by a vector network analyzer (VNA) in the range of 1-18 GHz. The resonant-antiresonant electromagnetic behavior was observed simultaneously in both rod-like and flower-like Fe3O4/C composites. Moreover, the resonant-antiresonant behavior was explained using displacement current lag at the "core/shell" interface. The flower-like Fe3O4/C/paraffin composites show superior microwave absorption performance with minimum reflection loss (RL) of up to -18.73 dB at 15.37 GHz. Comparatively, the rod-like Fe3O4/C/paraffin composites have uncommon continuous trinal absorption peaks at a thickness of 2.5 mm that effectively broadens the absorption bandwidth which is from 8.0 to 13.4 GHz. Furthermore, the microwave absorption mechanism has been discussed to provide a novel design for microwave absorption materials.

Change in Dielectric Properties in the Microwave Frequency Region of Polypyrrole–Coated Textiles during Aging

PubMed Central

Hakansson, Eva; Kaynak, Akif; Kouzani, Abbas

2016-01-01

Complex permittivity of conducting polypyrrole (PPy)-coated Nylon-Lycra textiles is measured using a free space transmission measurement technique over the frequency range of 1–18 GHz. The aging of microwave dielectric properties and reflection, transmission and absorption for a period of 18 months is demonstrated. PPy-coated fabrics are shown to be lossy over the full frequency range. The levels of absorption are shown to be higher than reflection in the tested samples. This is attributed to the relatively high resistivity of the PPy-coated fabrics. Both the dopant concentration and polymerisation time affect the total shielding effectiveness and microwave aging behaviour. Distinguishing either of these two factors as being exclusively the dominant mechanism of shielding effectiveness is shown to be difficult. It is observed that the PPy-coated Nylon-Lycra samples with a p-toluene sulfonic acid (pTSA) concentration of 0.015 M and polymerisation times of 60 min and 180 min have 37% and 26% decrease in total transmission loss, respectively, upon aging for 72 weeks at room temperature (20 °C, 65% Relative humidity (RH)). The concentration of the dopant also influences the microwave aging behaviour of the PPy-coated fabrics. The samples with a higher dopant concentration of 0.027 mol/L pTSA are shown to have a transmission loss of 32.6% and 16.5% for short and long polymerisation times, respectively, when aged for 72 weeks. The microwave properties exhibit better stability with high dopant concentration and/or longer polymerization times. High pTSA dopant concentrations and/or longer polymerisation times result in high microwave insertion loss and are more effective in reducing the transmission and also increasing the longevity of the electrical properties. PMID:28773729

Change in Dielectric Properties in the Microwave Frequency Region of Polypyrrole-Coated Textiles during Aging.

PubMed

Hakansson, Eva; Kaynak, Akif; Kouzani, Abbas

2016-07-22

Complex permittivity of conducting polypyrrole (PPy)-coated Nylon-Lycra textiles is measured using a free space transmission measurement technique over the frequency range of 1-18 GHz. The aging of microwave dielectric properties and reflection, transmission and absorption for a period of 18 months is demonstrated. PPy-coated fabrics are shown to be lossy over the full frequency range. The levels of absorption are shown to be higher than reflection in the tested samples. This is attributed to the relatively high resistivity of the PPy-coated fabrics. Both the dopant concentration and polymerisation time affect the total shielding effectiveness and microwave aging behaviour. Distinguishing either of these two factors as being exclusively the dominant mechanism of shielding effectiveness is shown to be difficult. It is observed that the PPy-coated Nylon-Lycra samples with a p -toluene sulfonic acid ( p TSA) concentration of 0.015 M and polymerisation times of 60 min and 180 min have 37% and 26% decrease in total transmission loss, respectively, upon aging for 72 weeks at room temperature (20 °C, 65% Relative humidity (RH)). The concentration of the dopant also influences the microwave aging behaviour of the PPy-coated fabrics. The samples with a higher dopant concentration of 0.027 mol/L p TSA are shown to have a transmission loss of 32.6% and 16.5% for short and long polymerisation times, respectively, when aged for 72 weeks. The microwave properties exhibit better stability with high dopant concentration and/or longer polymerization times. High p TSA dopant concentrations and/or longer polymerisation times result in high microwave insertion loss and are more effective in reducing the transmission and also increasing the longevity of the electrical properties.

Antenna design for microwave hepatic ablation using an axisymmetric electromagnetic model

PubMed Central

Bertram, John M; Yang, Deshan; Converse, Mark C; Webster, John G; Mahvi, David M

2006-01-01

Background An axisymmetric finite element method (FEM) model was employed to demonstrate important techniques used in the design of antennas for hepatic microwave ablation (MWA). To effectively treat deep-seated hepatic tumors, these antennas should produce a highly localized specific absorption rate (SAR) pattern and be efficient radiators at approved generator frequencies. Methods and results As an example, a double slot choked antenna for hepatic MWA was designed and implemented using FEMLAB™ 3.0. Discussion This paper emphasizes the importance of factors that can affect simulation accuracy, which include boundary conditions, the dielectric properties of liver tissue, and mesh resolution. PMID:16504153

Nonlinear optical behavior of two tetrathiafulvalene derivatives in the picosecond regime

NASA Astrophysics Data System (ADS)

Marcovicz, Crislaine; Ferreira, Rudson C.; Santos, Arthur B. S.; Reyna, Albert S.; de Araújo, Cid B.; Malvestiti, Ivani; Falcão, Eduardo H. L.

2018-06-01

We report the microwave-assisted synthesis of two symmetrical tetrathiafulvalene (TTF) derivatives via trialkyl phosphite-promoted coupling of a DMIT precursor. The microwave irradiation led to an increase in the reaction yield and significantly reduced the reaction time, affording the 2,3,6,7-tetrakis(2‧-methylacetatethio)tetrathiafulvalene (4) in 74% isolated yield. Hydrolysis of 4 yielded the tetraacid 5 in excellent yield. The nonlinear optical properties of both TTF compounds at 532 nm were studied by using the Z-scan technique in the picosecond regime exhibiting large third-order refractive index and saturated nonlinear absorption with promising applications in optical limiting devices.

Efficiency of Microwave Heating of Weakly Loaded Polymeric Nanocomposites (Postprint)

DTIC Science & Technology

2012-05-10

shielding and radar absorption [5]. Interaction of carbon nanotubes with microwaves is a subject of active ongoing research, 2 and the...mechanism of the microwave absorption by carbon nanotubes is still poorly understood [6-8]. Low thermal conductivity materials with controlled...and RAS design simulation. Composites Science and Technology. 70(2): p. 400‐409. 6. Vázquez, E. and M. Prato, Carbon Nanotubes and

Broadband superior electromagnetic absorption of a discrete-structure microwave coating

NASA Astrophysics Data System (ADS)

Duan, Yuping; Xi, Qun; Liu, Wei; Wang, Tongmin

2016-10-01

A method of improving the electromagnetic (EM) absorption property of conventional microwave absorber (CMA) is proposed here. The structural design process was mainly concerned with systematic analysis and research into the impedance matching characteristic and induced current. By processing a CMA-carbonyl-iron powder (CIP) coating into many isolated regions, the discrete-structure microwave absorber (DMA) had a much better absorption property than the corresponding CMA. When the thickness was only 2.0 mm and the component content was 33 wt%, the loss of reflection was less than -10 dB shifted from 6-7 GHz to 7-13 GHz and the loss of minimum reflection decreased from 12.5 dB lost to 32 dB lost through a discrete-structure process. The microwave absorption properties of coatings with different component contents and thicknesses were investigated. The minimum reflection peaks tended to shift towards the lower frequency region as CIP content or coating thickness increased. By adjusting these three factors, a high-performance broadband absorber was produced.

Remote microwave monitoring of magnetization switching in CoFeB/Ta/CoFeB spin logic device

NASA Astrophysics Data System (ADS)

Morgunov, R.; L'vova, G.; Talantsev, A.; Koplak, O.; Petit-Watelot, S.; Devaux, X.; Migot, S.; Lu, Y.; Mangin, S.

2017-05-01

Stable magnetic states of the MgO/CoFeB/Ta/CoFeB/MgO/Ta spin valve as well as transitions between the states were detected by microwave magnetoresistance (MMR) measured in the cavity of an electron spin resonance spectrometer. Advantages of this experimental technique are the possibility to study the orientation dependence of the MMR, the absence of the additional contact/sample interfaces, the wireless control of the spin valves, and the compatibility of the MMR measurements with ferromagnetic resonance experiments. The magnetic field dependence of the first derivation of the microwave absorption allows one to judge about the negative magnetoresistance of the layers and positive interlayer giant magnetoresistance. The obtained experimental results could be used for engineering of the microwave high sensitive sensors available for remote identification of the stable magnetic and logic states of the spin valves needful in medical spintronics to detect biological objects labeled with nanoparticles.

Microwave Absorption Properties of Co@C Nanofiber Composite for Normal and Oblique Incidence

NASA Astrophysics Data System (ADS)

Zhang, Junming; Wang, Peng; Chen, Yuanwei; Wang, Guowu; Wang, Dian; Qiao, Liang; Wang, Tao; Li, Fashen

2018-05-01

Co@C nanofibers have been prepared by an electrospinning technique. Uniform morphology of the nanofibers and good dispersion of the magnetic cobalt nanoparticles in the carbon fiber frame were confirmed by field-emission scanning electron microscopy and high-resolution transmission electron microscopy. The electromagnetic parameters of a composite absorber composed of Co@C nanofibers/paraffin were measured from 2 GHz to 15 GHz. The electromagnetic wave absorption properties were simulated and investigated in the case of normal and oblique incidence. In the normal case, the absorber achieved absorption performance of - 40 dB at 7.1 GHz. When the angle of incidence was increased to 60°, the absorption effect with reflection loss (RL) exceeding - 10 dB could still be obtained. These results demonstrate that the reported Co@C nanofiber absorber exhibits excellent absorption performance over a wide range of angle of incidence.

Ultra-wideband microwave absorber by connecting multiple absorption bands of two different-sized hyperbolic metamaterial waveguide arrays.

PubMed

Yin, Xiang; Long, Chang; Li, Junhao; Zhu, Hua; Chen, Lin; Guan, Jianguo; Li, Xun

2015-10-19

Microwave absorbers have important applications in various areas including stealth, camouflage, and antenna. Here, we have designed an ultra-broadband light absorber by integrating two different-sized tapered hyperbolic metamaterial (HMM) waveguides, each of which has wide but different absorption bands due to broadband slow-light response, into a unit cell. Both the numerical and experimental results demonstrate that in such a design strategy, the low absorption bands between high absorption bands with a single-sized tapered HMM waveguide array can be effectively eliminated, resulting in a largely expanded absorption bandwidth ranging from 2.3 to 40 GHz. The presented ultra-broadband light absorber is also insensitive to polarization and robust against incident angle. Our results offer a further step in developing practical artificial electromagnetic absorbers, which will impact a broad range of applications at microwave frequencies.

Laboratory evaluation and application of microwave absorption properties under simulated conditions for planetary atmospheres

NASA Technical Reports Server (NTRS)

Steffes, Paul G.

1987-01-01

Laboratory measurements were conducted to evaluate properties of atmospheric gases under simulated conditions for the outer planets. A significant addition to this effort was the capability to make such measurements at millimeter wavelengths. Measurements should soon be completed on the millimeter wave absorption from ammonia under Jovian conditions. Also studied will be the feasibility of measuring the microwave and millimeter wave properties of phosphine (PH3) under simulated Jovian conditions. Further analysis and application of the laboratory results to microwave and millimeter wave absorption data for the outer planet, such as Voyager Radio Occultation experiments, will be pursued.

Effects of rain and fog on the Shuttle Ku-band microwave scanning beam landing system range and accuracy performance

NASA Technical Reports Server (NTRS)

Butler, D.

1981-01-01

The microwave Scanning Beam Landing System's (MSBLS) performance in fog and rain was studied. The fog and rain effects on the Shuttle Ku-band system were determined. Specifically, microwave attenuation, beam distortion, and coordinate errors resulting from operation of the MSBLS in poor weather conditions were evaluated. The main physical processes giving rise to microwave attenuation were found to be absorption and scattering by water droplets. The general theory of scattering and absorption used is discussed and a listing of applicable computer programs is provided.

Microwave Absorption Characteristics of Tire

NASA Astrophysics Data System (ADS)

Zhang, Yuzhe; Hwang, Jiann-Yang; Peng, Zhiwei; Andriese, Matthew; Li, Bowen; Huang, Xiaodi; Wang, Xinli

The recycling of waste tires has been a big environmental problem. About 280 million waste tires are produced annually in the United States and more than 2 billion tires are stockpiled, which cause fire hazards and health issues. Tire rubbers are insoluble elastic high polymer materials. They are not biodegradable and may take hundreds of years to decompose in the natural environment. Microwave irradiation can be a thermal processing method for the decomposition of tire rubbers. In this study, the microwave absorption properties of waste tire at various temperatures are characterized to determine the conditions favorable for the microwave heating of waste tires.

Microwave-induced direct spin-flip transitions in mesoscopic Pd/Co heterojunctions

NASA Astrophysics Data System (ADS)

Pietsch, Torsten; Egle, Stefan; Keller, Martin; Fridtjof-Pernau, Hans; Strigl, Florian; Scheer, Elke

2016-09-01

We experimentally investigate the effect of resonant microwave absorption on the magneto-conductance of tunable Co/Pd point contacts. At the interface a non-equilibrium spin accumulation is created via microwave absorption and can be probed via point contact spectroscopy. We interpret the results as a signature of direct spin-flip excitations in Zeeman-split spin-subbands within the Pd normal metal part of the junction. The inverse effect, which is associated with the emission of a microwave photon in a ferromagnet/normal metal point contact, can also be detected via its unique signature in transport spectroscopy.

Properties of water vapor relevant to its measurement in the stratosphere and mesosphere

NASA Technical Reports Server (NTRS)

Longbothum, R. L.

1974-01-01

The literature on the concentrations of water vapor in the stratosphere and mesosphere was studied. It is estimated that the concentrations in these lie in the range from 0.1 ppm to 10 ppm. A survey was made of the scattering and radiative transfer properties of water vapor and the background constituents to determine the physical properties of importance to measurements of concentrations. It was determined that absorption and emission properties provide significant increases in sensitivity compared with the various scattering phenomena considered. Microwave absorption in the region of 22 GHz and 183 GHz and infrared absorption in the vibrational rotational band systems seem to be the most attractive techniques. Various experimental configurations are analyzed and compared.

Response of a 2DEG to Microwave Irradiation

NASA Astrophysics Data System (ADS)

Moreau, S.; Fedorych, O. M.; Sadowski, M. L.; Potemski, M.; Studenikin, S.; Austing, G.; Sachrajda, A. S.; Saku, T.; Hirayama, Y.

In this paper, we study the behavior of a high mobility two dimensional electron gas under microwave irradiation by means of magneto-photoluminescence (PL) and absorption measurements. The high mobility sample investigated is a 15nm wide GaAs/AlGaAs quantum well with an electron concentration between 1-2×1011cm-2, tunable by visible-light illumination. Structures in the microwave absorption at 40-60GHz are identified as geometrically confined magneto-plasmons.

Constructing Two-, Zero-, and One-Dimensional Integrated Nanostructures: an Effective Strategy for High Microwave Absorption Performance.

PubMed

Sun, Yuan; Xu, Jianle; Qiao, Wen; Xu, Xiaobing; Zhang, Weili; Zhang, Kaiyu; Zhang, Xing; Chen, Xing; Zhong, Wei; Du, Youwei

2016-11-23

A novel "201" nanostructure composite consisting of two-dimensional MoS 2 nanosheets, zero-dimensional Ni nanoparticles and one-dimensional carbon nanotubes (CNTs) was prepared successfully by a two-step method: Ni nanopaticles were deposited onto the surface of few-layer MoS 2 nanosheets by a wet chemical method, followed by chemical vapor deposition growth of CNTs through the catalysis of Ni nanoparticles. The as-prepared 201-MoS 2 -Ni-CNTs composites exhibit remarkably enhanced microwave absorption performance compared to Ni-MoS 2 or Ni-CNTs. The minimum reflection loss (RL) value of 201-MoS 2 -Ni-CNTs/wax composites with filler loading ratio of 30 wt % reached -50.08 dB at the thickness of 2.4 mm. The maximum effective microwave absorption bandwidth (RL< -10 dB) of 6.04 GHz was obtained at the thickness of 2.1 mm. The excellent absorption ability originates from appropriate impedance matching ratio, strong dielectric loss and large surface area, which are attributed to the "201" nanostructure. In addition, this method could be extended to other low-dimensional materials, proving to be an efficient and promising strategy for high microwave absorption performance.

Spatially resolved measurement of singlet delta oxygen by radar resonance-enhanced multiphoton ionization.

PubMed

Wu, Yue; Zhang, Zhili; Ombrello, Timothy M

2013-07-01

Coherent microwave Rayleigh scattering (Radar) from resonance-enhanced multiphoton ionization (REMPI) was demonstrated to directly and nonintrusively measure singlet delta oxygen, O(2)(a(1)Δ(g)), with high spatial resolution. Two different approaches, photodissociation of ozone and microwave discharge plasma in an argon and oxygen flow, were utilized for O(2)(a(1)Δ(g)) generation. The d(1)Π(g)←a(1)Δ(g) (3-0) and d(1)Π(g)←a(1)Δ(g) (1-0) bands of O(2)(a(1)Δ(g)) were detected by Radar REMPI for two different flow conditions. Quantitative absorption measurements using sensitive off-axis integrated cavity output spectroscopy (ICOS) was used simultaneously to evaluate the accuracy and sensitivity of the Radar REMPI technique. The detection limit of Radar REMPI was found to be comparable to the ICOS technique with a detection threshold of approximately 10(14) molecules/cm(3) but with a spatial resolution that was 8 orders of magnitude smaller than the ICOS technique.

Synthesis of fluorescent carbon dots by a microwave heating process: structural characterization and cell imaging applications

NASA Astrophysics Data System (ADS)

Stefanakis, Dimitrios; Philippidis, Aggelos; Sygellou, Labrini; Filippidis, George; Ghanotakis, Demetrios; Anglos, Demetrios

2014-10-01

Two types of highly fluorescent carbon dots (C-dots) were prepared by a single-step procedure based on microwave heating citric acid and 6-aminocaproic acid or citric acid and urea in an aqueous solution. The small size of the isolated carbon dots along with their strong absorption in the UV and their excitation wavelength-dependent fluorescence render them ideal nanomaterials for biomedical applications (imaging and sensing). The structure and properties of the two types of C-dot materials were studied using a series of spectroscopic techniques. The ability of the C-dots to be internalized by HeLa cells was demonstrated via 3-photon fluorescence microscopy imaging.

Investigations on structural and optical properties of starch capped ZnS nanoparticles synthesized by microwave irradiation method

NASA Astrophysics Data System (ADS)

Lalithadevi, B.; Mohan Rao, K.; Ramananda, D.

2018-05-01

Following a green synthesis method, zinc sulfide (ZnS) nanoparticles were prepared by chemical co-precipitation technique using starch as capping agent. Microwave irradiation was used as heating source. X-ray diffraction studies indicated that nanopowders obtained were polycrystalline possessing ZnS simple cubic structure. Transmission electron microscopic studies indicated that starch limits the agglomeration by steric stabilization. Interaction between ZnS and starch was confirmed by Fourier transform infrared spectroscopy as well as Raman scattering studies. Quantum size effects were observed in optical absorption studies while quenching of defect states on nanoparticles was improved with increase in starch addition as indicated by photoluminescence spectra.

Microwave-assisted cationic polymerization of palm olein and their urea inclusion products

NASA Astrophysics Data System (ADS)

Soegijono, Bambang; Farid, Muhamad; Alim Mas'ud, Zainal

2018-01-01

Cationic polymerization is affected by the relative amount of unsaturated bond (C=C) in the compound. The enrichment of an unsaturated triglyceride fraction from oils may be performed using urea inclusion techniques. In this study, palm olein was enriched-unsaturated fraction using urea-methanol system. The palm olein and its urea-inclusion products were cationic polymerized with ethereal boron trifluoride catalyst and followed by irradiation using a commercial microwave (microwave-assisted). The microwave irradiated products were cured at 110 °C for 24 hours. Fatty acid composition of the palm olein and its urea-inclusion products were analyzed by gas chromatography. Iodine numbers, functional groups, and ultraviolet absorption spectra of all palm olein origin, urea inclusion products and polymerization products were analyzed using titrimetric, ultraviolet spectrophotometric, and Fourier Transform infrared spectrophotometric methods. Differential scanning calorimetric (DSC) was used to observe the thermal characteristics of the polymer. Urea-inclusion process increased the unsaturated fatty acid components as indicated by the increased iodine number, intensity of alkene band absorptions in the infrared spectra, and the absorbance of the ultraviolet spectra. The polymer formation is converting the C=C group to C-C, which is indicated by the opposite of the urea inclusion process. The curing process results in reformation of new C=C bonds that were similar to that of the urea inclusion process. The DSC thermogram curve shows that the enrichment process improves the thermal stability of the polymer formed.

Preparation of Oxidation-Resistant Ultra High Melting Temperature Materials and Structures Using Laser Method

DTIC Science & Technology

2009-06-06

sample within a small ceramic muffle. The microwave absorption coefficient of most ceramics is low, but increases with temperature. Thus, as the...increased using additives with higher absorption 7 coefficients . Silicon carbide has a higher loss tangent at 2.4 GHz than most ceramics, and thus...electron beam sintering. Microwave heating works well for large volumes, but ceramics normally have a low dielectric absorption constant at room

Highly precise stabilization of intracavity prism-based Er:fiber frequency comb using optical-microwave phase detector.

PubMed

Zhang, Shuangyou; Wu, Jiutao; Leng, Jianxiao; Lai, Shunnan; Zhao, Jianye

2014-11-15

In this Letter, we demonstrate a fully stabilized Er:fiber frequency comb by using a fiber-based, high-precision optical-microwave phase detector. To achieve high-precision and long-term phase locking of the repetition rate to a microwave reference, frequency control techniques (tuning pump power and cavity length) are combined together as its feedback. Since the pump power has been used for stabilization of the repetition rate, we introduce a pair of intracavity prisms as a regulator for carrier-envelope offset frequency, thereby phase locking one mode of the comb to the rubidium saturated absorption transition line. The stabilized comb performs the same high stability as the reference for the repetition rate and provides a residual frequency instability of 3.6×10(-13) for each comb mode. The demonstrated stabilization scheme could provide a high-precision comb for optical communication, direct frequency comb spectroscopy.

Flexible thin broadband microwave absorber based on a pyramidal periodic structure of lossy composite.

PubMed

Huang, Yixing; Yuan, Xujin; Wang, Changxian; Chen, Mingji; Tang, Liqun; Fang, Daining

2018-06-15

Microwave absorber with broadband absorption and thin thickness is one of the main research interests in this field. A flexible ultrathin and broadband microwave absorber comprising multiwall carbon nanotubes, spherical carbonyl iron, and silicone rubber is fabricated in a newly proposed pyramidal spatial periodic structure (SPS). The SPS with equivalent thickness of 3.73 mm covers the -10  dB and -15  dB absorption bandwidth in the frequency range 2-40 GHz and 10-40 GHz, respectively. The excellent absorption performance is achieved by concentration and dissipation of the electromagnetic field inside different parts of the magnetic-dielectric lossy protrusions in different frequency ranges.

Microwave absorption properties of Ni/(C, silicides) nanocapsules

PubMed Central

2012-01-01

The microwave absorption properties of Ni/(C, silicides) nanocapsules prepared by an arc discharge method have been studied. The composition and the microstructure of the Ni/(C, silicides) nanocapsules were determined by means of X-ray diffraction, X-ray photoelectric spectroscopy, and transmission electron microscope observations. Silicides, in the forms of SiOx and SiC, mainly exist in the shells of the nanocapsules and result in a large amount of defects at the ‘core/shell’ interfaces as well as in the shells. The complex permittivity and microwave absorption properties of the Ni/(C, silicides) nanocapsules are improved by the doped silicides. Compared with those of Ni/C nanocapsules, the positions of maximum absorption peaks of the Ni/(C, silicides) nanocapsules exhibit large red shifts. An electric dipole model is proposed to explain this red shift phenomenon. PMID:22548846

Adjustable 3-D structure with enhanced interfaces and junctions towards microwave response using FeCo/C core-shell nanocomposites.

PubMed

Li, Daoran; Liang, Xiaohui; Liu, Wei; Ma, Jianna; Zhang, Yanan; Ji, Guangbin; Meng, Wei

2017-12-01

In this work, the 3-D honeycomb-like FeCo/C nanocomposites were synthesized through the carbon thermal reduction under an inert atmosphere. The enhanced microwave absorption properties of the composites were mainly attributed to the unique three dimensional structure of the FeCo/C nanocomposites, abundant interfaces and junctions, and the appropriate impedance matching. The Cole-Cole semicircles proved the sufficient dielectric relaxation process. The sample calcinated at 600°C for 4h showed the best microwave absorption properties. A maximum reflection loss of -54.6dB was achieved at 10.8GHz with a thickness of 2.3mm and the frequency bandwidth was as large as 5.3GHz. The results showed that the as-prepared FeCo/C nanocomposite could be a potential candidate for microwave absorption. Copyright © 2017 Elsevier Inc. All rights reserved.

Microwave propagation and absorption and its thermo-mechanical consequences in heterogeneous rocks.

PubMed

Meisels, R; Toifl, M; Hartlieb, P; Kuchar, F; Antretter, T

2015-02-10

A numerical analysis in a two-component model rock is presented including the propagation and absorption of a microwave beam as well as the microwave-induced temperature and stress distributions in a consistent way. The analyses are two-dimensional and consider absorbing inclusions (discs) in a non-absorbing matrix representing the model of a heterogeneous rock. The microwave analysis (finite difference time domain - FDTD) is performed with values of the dielectric permittivity typical for hard rocks. Reflections at the discs/matrix interfaces and absorption in the discs lead to diffuse scattering with up to 20% changes of the intensity in the main beam compared to a homogeneous model rock. The subsequent thermo-mechanical finite element (FE) analysis indicates that the stresses become large enough to initiate damage. The results are supported by preliminary experiments on hard rock performed at 2.45 GHz.

Very high S-band microwave absorption of carbon nanotube buckypapers with Mn nanoparticle interlayers

NASA Astrophysics Data System (ADS)

Lu, Shaowei; Bai, Yaoyao; Wang, Jijie; Zhang, Lu; Tian, Caijiao; Ma, Keming; Wang, Xiaoqiang

2018-03-01

Flexible and high-performance electromagnetic absorbing materials of multi-walled carbon nanotube (MWCNT) buckypapers with Mn nanoparticles (NPSs) interlayer were fabricated via monodisperse solutions through layer by layer vacuum filtration method. The morphology and element composition of buckypapers were characterized by scanning electron microscopy, energy dispersive spectrometer, and X-ray diffraction. The formation of flexible MWCNT buckypapers with Mn NPS (0-30 wt. %) interlayer was attributed to nanostructure and morphology of the samples. When the blended Mn NPS content in buckypapers is 20 wt. %, there are evidently two larger absorption peaks (-13.2 dB at 3.41 GHz, -15.6 dB at 3.52 GHz) of the buckypaper with an absorbing thickness of 0.1 mm. The fundamental microwave absorption mechanism of the buckypapers is discussed. This work opens a new pathway towards tuning microwave absorbers performance and this method can be extended to exploit other excellent microwave absorbers with interlayer.

Laboratory evaluation and application of microwave absorption properties under simulated conditions for planetary atmospheres

NASA Technical Reports Server (NTRS)

Steffes, Paul G.

1988-01-01

Radio absorptivity data for planetary atmospheres obtained from spacecraft radio occultation experiments and earth-based radio astronomical observations can be used to infer abundances of microwave absorbing atmospheric constituents in those atmospheres, as long as reliable information regarding the microwave absorbing properties of potential constituents is available. The key activity for this grant year has continued to be laboratory measurements of the microwave and millimeter-wave properties of the simulated atmospheres of the outer planets and their satellites. A Fabry-Perot spectrometer system capable of operation from 32 to 41 GHz was developed. Initially this spectrometer was used to complete laboratory measurements of the 7.5 to 9.3 mm absorption spectrum of ammonia. Laboratory measurements were begun at wavelengths near 3.2 mm, where a large number of observations of the emission from the outer planets were made. A description of this system is presented.

Non-resonant microwave absorption in high-T c thin films

NASA Astrophysics Data System (ADS)

Durny, R.; Dulcic, A.; Crepeau, R. H.; Freed, J. H.; Kus, P.

1990-11-01

Magnetic-field-dependent non-resonant microwave absorption in thin film samples of various high- Tc superconductors is reported. Complex types of signals were observed as the temperature was lowered from Tc to ≈ 10 K. Possible correlation between the thin film quality and the occurrence of the signals is suggested.

Superior microwave absorption properties of ultralight reduced graphene oxide/black phosphorus aerogel.

PubMed

Hao, Chunxue; Wang, Bochong; Wen, Fusheng; Mu, Congpu; Xiang, Jianyong; Li, Lei; Liu, Zhongyuan

2018-06-08

Through a facile self-assembled process, an ultralight reduced graphene oxide/black phosphorus (rGO/BP) composite aerogel was successfully fabricated. The BP nanosheets were homogeneously distributed throughout the rGO 3D framework, and the interfaces between rGO and BP possessed four kinds of interconnections, such as wrapping, wearing, bridging and weak linking. As an ultralight composite, the rGO/BP aerogel could easily stand on the stamen of a flower. Compared with pure rGO aerogel, the rGO/BP composite aerogel exhibited enhanced microwave absorption ability. The minimum reflection loss value of -46.9 dB with a thickness of 2.53 mm was obtained, and a wide absorption band of 6.1 GHz (RL < -10 dB) was achieved. The superior microwave absorption property was demonstrated to stem from the interfacial polarization loss mechanism in which the multiform interface interactions between the rGO skeleton and BP nanosheets played critical roles. The rGO/BP aerogel has great potential to be used as an ultralight microwave absorber.

Superior microwave absorption properties of ultralight reduced graphene oxide/black phosphorus aerogel

NASA Astrophysics Data System (ADS)

Hao, Chunxue; Wang, Bochong; Wen, Fusheng; Mu, Congpu; Xiang, Jianyong; Li, Lei; Liu, Zhongyuan

2018-06-01

Through a facile self-assembled process, an ultralight reduced graphene oxide/black phosphorus (rGO/BP) composite aerogel was successfully fabricated. The BP nanosheets were homogeneously distributed throughout the rGO 3D framework, and the interfaces between rGO and BP possessed four kinds of interconnections, such as wrapping, wearing, bridging and weak linking. As an ultralight composite, the rGO/BP aerogel could easily stand on the stamen of a flower. Compared with pure rGO aerogel, the rGO/BP composite aerogel exhibited enhanced microwave absorption ability. The minimum reflection loss value of ‑46.9 dB with a thickness of 2.53 mm was obtained, and a wide absorption band of 6.1 GHz (RL < ‑10 dB) was achieved. The superior microwave absorption property was demonstrated to stem from the interfacial polarization loss mechanism in which the multiform interface interactions between the rGO skeleton and BP nanosheets played critical roles. The rGO/BP aerogel has great potential to be used as an ultralight microwave absorber.

Laboratory evaluation and application of microwave absorption properties under simulated conditions for planetary atmospheres

NASA Technical Reports Server (NTRS)

Steffes, P. G.

1985-01-01

Radio absorptivity data for planetary atmospheres obtained from spacecraft radio occultation experiments and Earth-based radio astronomical observations can be used to infer abundances of microwave absorbing atmospheric constituents in those atmospheres, as long as reliable information regarding the microwave absorbing properties of potential constituents is available. The use of theoretically-derived microwave absorption properties for such atmospheric constituents, or laboratory measurements of such properties under environmental conditions which are significantly different than those of the planetary atmosphere being studied, often lead to significant misinterpretation of available opacity data. Steffes and Eshleman showed that under environmental conditions corresponding to the middle atmosphere of Venus, the microwave absorption due to atmospheric SO2 was 50 percent greater than that calculated from Van Vleck-Weiskopff theory. Similarly, the opacity from gaseous H2SO4 was found to be a factor of 7 greater than theoretically predicted for conditions of the Venus middle atmosphere. The recognition of the need to make such measurements over a range of temperatures and pressures which correspond to the periapsis altitudes of radio occultation experiments, and over a range of frequencies which correspond to both radio occultation experiments and radio astronomical observations, has led to the development of a facility at Georgia Tech which is capable of making such measurements.

Low content Ag-coated poly(acrylonitrile) microspheres and graphene for enhanced microwave absorption performance epoxy composites

NASA Astrophysics Data System (ADS)

Zhang, Bin; Wang, Jun; Chen, Xiaocheng; Su, Xiaogang; Zou, Yi; Huo, Siqi; Chen, Wei; Wang, Junpeng

2018-04-01

Silver nanoparticles was uniformly anchored on the surface of hollow poly(acrylonitrile) microspheres with a facile chemical method using hydrazine hydrate as reductant. Integrating these conducting hollow spheres (PANS@Ag) with chemical reduced graphene oxide (RGO) dispersed in epoxy resin, a lightweight microwave absorber was successfully prepared with enhanced microwave absorption performance. The chemical constitution and surface morphology of as-synthesized RGO and PANS@Ag powders were characterized by XRD, XPS, FE-SEM and SAED, while the electromagnetic properties of these different proportion PANS@Ag-RGO/EP samples were analyzed through vector network analyzer (VNA). The minimum reflection loss (RL) could reach up to ‑28.1 dB at 8.8 GHz with a layer thickness of 2 mm, and the corresponding effective absorption bandwidth (RL values less than ‑10 dB) was from 7.9 GHz to 9.8 GHz. However, the dosage of PANS@Ag and RGO was merely 3 wt% and 1 wt%, respectively. As the content of PANS@Ag powders decreased to 1 wt%, the PANS@Ag-RGO/EP samples still retained effective microwave absorption performance and the optimal RL was ‑14.7 dB. The density of as-prepared absorbers was in the range of 0.49 ∼ 0.87 g cm‑3. The low content, low density and enhanced microwave absorption performance endow the hybrid composites with competitive application prospect in stealth technology field.

Water-based metamaterial absorbers for optical transparency and broadband microwave absorption

NASA Astrophysics Data System (ADS)

Pang, Yongqiang; Shen, Yang; Li, Yongfeng; Wang, Jiafu; Xu, Zhuo; Qu, Shaobo

2018-04-01

Naturally occurring water is a promising candidate for achieving broadband absorption. In this work, by virtue of the optically transparent character of the water, the water-based metamaterial absorbers (MAs) are proposed to achieve the broadband absorption at microwave frequencies and optical transparence simultaneously. For this purpose, the transparent indium tin oxide (ITO) and polymethyl methacrylate (PMMA) are chosen as the constitutive materials. The water is encapsulated between the ITO backed plate and PMMA, serving as the microwave loss as well as optically transparent material. Numerical simulations show that the broadband absorption with the efficiency over 90% in the frequency band of 6.4-30 GHz and highly optical transparency of about 85% in the visible region can be achieved and have been well demonstrated experimentally. Additionally, the proposed water-based MA displays a wide-angle absorption performance for both TE and TM waves and is also robust to the variations of the structure parameters, which is much desired in a practical application.

Physics of the Microwave Oven

ERIC Educational Resources Information Center

Vollmer, Michael

2004-01-01

This is the first of two articles about the physics of microwave ovens. This article deals with the generation of microwaves in the oven and includes the operation of the magnetrons, waveguides and standing waves in resonant cavities. It then considers the absorption of microwaves by foods, discussing the dielectric relaxation of water,…

Preparation and microwave absorption properties of honeycomb core structures coated with composite absorber

NASA Astrophysics Data System (ADS)

Luo, Hui; Chen, Fu; Wang, Fang; Wang, Xian; Dai, Weiyong; Hu, Sheng; Gong, Rongzhou

2018-05-01

Honeycomb structure coated with paraffin filled with composite of graphene and flaky carbonyl iron powder (FCIP) as lossy filler have been studied. The composite of graphene/FCIP with different weight ratio were synthesized via mechanical milling, the electromagnetic properties of the samples were measured by transmission/reflection method in the frequency range of 8-12 GHz. The microwave absorbing properties of the microwave absorbing honeycomb structure (MAHS) and microwave absorbing honeycomb sandwich structure (MAHSS) were studied based on the Finite Element Method with periodical boundary conditions. The matching layer on the top of the honeycomb sandwich structure can enhanced the microwave absorption properties. It was shown that a light weight and broadband MAHSS could be implemented with the use of the magnetic material and dielectric material.

Ultrathin microwave absorber based on metamaterial

NASA Astrophysics Data System (ADS)

Kim, Y. J.; Yoo, Y. J.; Hwang, J. S.; Lee, Y. P.

2016-11-01

We suggest that ultrathin broadband metamaterial is a perfect absorber in the microwave regime by utilizing the properties of a resistive sheet and metamaterial. Meta-atoms are composed of four-leaf clover-shape metallic patterns and a metal plane separated by three intermediate resistive sheet layers between four dielectric layers. We interpret the absorption mechanism of the broadband by using the distribution of surface currents at specific frequencies. The simulated absorption was over 99% in 1.8-4.2 GHz. The corresponding experimental absorption was also over 99% in 2.62-4.2 GHz; however, the absorption was slightly lower than 99% in 1.8-2.62 GHz because of the sheet resistance and the changed values for the dielectric constant. Furthermore, it is independent of incident angle. The results of this research indicate the possibility of applications, due to the suppression of noxious exposure, in cell phones, computers and microwave equipments.

Electromagnetic and Microwave Absorption Properties of Carbonyl Tetrapod-Shaped Zno Nanostructures Composite Coatings

NASA Astrophysics Data System (ADS)

Yu, Haibo; Qin, Hui; Huang, Yunhua

2012-08-01

CIP/T-ZnO/EP composite coatings with carbonyl iron powders (CIP) and tetrapodshaped ZnO (T-ZnO) nanostructures as absorbers, and epoxy resin (EP) as matrix were prepared. The complex permittivity, permeability and microwave absorption properties of the coatings were investigated in the frequency range of 2-18 GHz. The effects of the weight ratio (CIP/T-ZnO/EP), the thickness and the solidification temperature on microwave absorption properties were discussed. When the weight ratio (CIP/TZnO/ EP), the thickness and the solidification temperature is 28:2:22, 1.8 mm, and 10°C, respectively, the optimal wave absorption with the minimum reflection loss (RL) value of -22.38 dB at 15.67 GHz and the bandwidth (RL<-10 dB) of 5.74 GHz was obtained, indicating that the composite coatings may have a promising application in Ku-band (12-18 GHz).

Transfer of thermal microwaves in the atmosphere, volume 1

NASA Technical Reports Server (NTRS)

Paris, J. F.

1971-01-01

The Mie theory is used to determine the absorption and scattering properties of liquid hydrometeors at 27 microwave frequencies from 500 MHz to 60 GHz. Based on the Marshall-Palmer distribution of drop sizes, regression equations are developed for the volume absorption coefficient of rain as a function of its temperature and content of liquid water.

Microwave Kinetic Inductance Detector with Selective Polarization Coupling

NASA Technical Reports Server (NTRS)

Wollack, Edward; U-yen, Kongpop; Stevenson, Thomas; Brown, Ari; Moseley, Samuel; Hsieh, Wen-Ting

2013-01-01

A conventional low-noise detector requires a technique to both absorb incident power and convert it to an electrical signal at cryogenic temperatures. This innovation combines low-noise detector and readout functionality into one device while maintaining high absorption, controlled polarization sensitivity, and broadband detection capability. The resulting far-infrared detectors can be read out with a simple approach, which is compact and minimizes thermal loading. The proposed microwave kinetic inductance detector (MKID) consists of three basic elements. The first is the absorptive section in which the incident power is coupled to a superconducting resonator at far-infrared frequency above its superconducting critical frequency (where superconductor becomes normal conductor). This absorber's shape effectively absorbs signals in the desired polarization state and is resonant at the radio frequency (RF) used for readout of the device. Control over the metal film used in the absorber allows realization of structures with either a 50% broadband or 100% resonance absorptance over a 30% fractional bandwidth. The second element is a microwave resonator - which is realized from the thin metal films used to make the absorber as transmission lines - whose resonance frequency changes due to a variation in its kinetic inductance. The resonator's kinetic inductance is a function of the power absorbed by the device. A low-loss dielectric (mono-crystalline silicon) is used in a parallel-plate transmission line structure to realize the desired superconducting resonators. There is negligible coupling among the adjacent elements used to define the polarization sensitivity of each detector. The final component of the device is a microwave transmission line, which is coupled to the resonator, and allows detection of changes in resonance frequency for each detector in the focal plane array. The spiral shape of the detector's absorber allows incident power with two polarizations to couple to the detector equally. A stepped impedance resonator was used that allows the incident power absorbed in the detecting membrane area to be uniformly distributed in the detector's transmission line at the RF readout frequency. This maximizes the sensitivity of the detector. The signal is read out via a frequency multiplexing technique that requires a minimum number of interface transmission lines for readout. This reduces the packaging complexity and coupling to the device's thermal environment.

Quantitative analysis of time-resolved microwave conductivity data

DOE Office of Scientific and Technical Information (OSTI.GOV)

Reid, Obadiah G.; Moore, David T.; Li, Zhen

Flash-photolysis time-resolved microwave conductivity (fp-TRMC) is a versatile, highly sensitive technique for studying the complex photoconductivity of solution, solid, and gas-phase samples. The purpose of this paper is to provide a standard reference work for experimentalists interested in using microwave conductivity methods to study functional electronic materials, describing how to conduct and calibrate these experiments in order to obtain quantitative results. The main focus of the paper is on calculating the calibration factor, K, which is used to connect the measured change in microwave power absorption to the conductance of the sample. We describe the standard analytical formulae that havemore » been used in the past, and compare them to numerical simulations. This comparison shows that the most widely used analytical analysis of fp-TRMC data systematically under-estimates the transient conductivity by ~60%. We suggest a more accurate semi-empirical way of calibrating these experiments. However, we emphasize that the full numerical calculation is necessary to quantify both transient and steady-state conductance for arbitrary sample properties and geometry.« less

Quantitative analysis of time-resolved microwave conductivity data

DOE PAGES

Reid, Obadiah G.; Moore, David T.; Li, Zhen; ...

2017-11-10

Flash-photolysis time-resolved microwave conductivity (fp-TRMC) is a versatile, highly sensitive technique for studying the complex photoconductivity of solution, solid, and gas-phase samples. The purpose of this paper is to provide a standard reference work for experimentalists interested in using microwave conductivity methods to study functional electronic materials, describing how to conduct and calibrate these experiments in order to obtain quantitative results. The main focus of the paper is on calculating the calibration factor, K, which is used to connect the measured change in microwave power absorption to the conductance of the sample. We describe the standard analytical formulae that havemore » been used in the past, and compare them to numerical simulations. This comparison shows that the most widely used analytical analysis of fp-TRMC data systematically under-estimates the transient conductivity by ~60%. We suggest a more accurate semi-empirical way of calibrating these experiments. However, we emphasize that the full numerical calculation is necessary to quantify both transient and steady-state conductance for arbitrary sample properties and geometry.« less

Microwave measurements of the absolute values of absorption by water vapour in the atmosphere.

PubMed

Hogg, D C; Guiraud, F O

1979-05-31

MEASUREMENT of the absolute value of absorption by water vapour at microwave frequencies is difficult because the effect is so small. Far in the wings of the absorption lines, in the so-called 'windows' of the spectrum, it is especially difficult to achieve high accuracy in the free atmosphere. But it is in these windows that the behaviour of the absorption is important from both applied and scientific points of view. Satellite communications, remote sensing of the atmosphere, and radioastronomy, are all influenced by this behaviour. Measurements on an Earth-space path are reported here; the results indicate a nonlinear relationship between absorption and water-vapour content.

Microwave Enhancement of Autocatalytic Growth of Nanometals.

PubMed

Ashley, Bridgett; Vakil, Parth N; Lynch, Brian B; Dyer, Christopher M; Tracy, Joseph B; Owens, Jeffery; Strouse, Geoffrey F

2017-10-24

The desire for designing efficient synthetic methods that lead to industrially important nanomaterials has led a desire to more fully understand the mechanism of growth and how modern synthetic techniques can be employed. Microwave (MW) synthesis is one such technique that has attracted attention as a green, sustainable method. The reports of enhancement of formation rates and improved quality for MW driven reactions are intriguing, but the lack of understanding of the reaction mechanism and how coupling to the MW field leads to these observations is concerning. In this manuscript, the growth of a metal nanoparticles (NPs) in a microwave cavity is spectroscopically analyzed and compared with the classical autocatalytic method of NP growth to elucidate the underpinnings for the observed enhanced growth behavior for metal NPs prepared in a MW field. The study illustrates that microwave synthesis of nickel and gold NPs below saturation conditions follows the Finke-Watzky mechanism of nucleation and growth. The enhancement of the reaction arises from the size-dependent increase in MW absorption cross section for the metal NPs. For Ni, the presence of oxides is considered via theoretical computations and compared to dielectric measurements of isolated nickel NPs. The study definitively shows that MW growth can be modeled by an autocatalytic mechanism that directly leads to the observed enhanced rates and improved quality widely reported in the nanomaterial community when MW irradiation is employed.

Application of fluorescent dyes for some problems of bioelectromagnetics

NASA Astrophysics Data System (ADS)

Babich, Danylo; Kylsky, Alexandr; Pobiedina, Valentina; Yakunov, Andrey

2016-04-01

Fluorescent organic dyes solutions are used for non-contact measurement of the millimeter wave absorption in liquids simulating biological tissue. There is still not any certain idea of the physical mechanism describing this process despite the widespread technology of microwave radiation in the food industry, biotechnology and medicine. For creating adequate physical model one requires an accurate command of knowledge concerning to the relation between millimeter waves and irradiated object. There were three H-bonded liquids selected as the samples with different coefficients of absorption in the millimeter range like water (strong absorption), glycerol (medium absorption) and ethylene glycol (light absorption). The measurements showed that the greatest response to the action of microwaves occurs for glycerol solutions: R6G (building-up luminescence) and RC (fading luminescence). For aqueous solutions the signal is lower due to lower quantum efficiency of luminescence, and for ethylene glycol — due to the low absorption of microwaves. In the area of exposure a local increase of temperature was estimated. For aqueous solutions of both dyes the maximum temperature increase is about 7° C caused with millimeter waves absorption, which coincides with the direct radio physical measurements and confirmed by theoretical calculations. However, for glycerol solution R6G temperature equivalent for building-up luminescence is around 9° C, and for the solution of ethylene glycol it's about 15°. It is assumed the possibility of non-thermal effect of microwaves on the different processes and substances. The application of this non-contact temperature sensing is a simple and novel method to detect temperature change in small biological objects.

The synergistic effects of carbon coating and micropore structure on the microwave absorption properties of Co/CoO nanoparticles.

PubMed

Xie, Xiubo; Pang, Yu; Kikuchi, Hiroaki; Liu, Tong

2016-11-09

25 nm carbon-coated microporous Co/CoO nanoparticles (NPs) were synthesized by integrating chemical de-alloying and chemical vapor deposition (CVD) methods. The NPs possess micropores of 0.8-1.5 nm and display a homogeneous carbon shell of about 4 nm in thickness with a low graphitization degree. The saturation magnetization (M S ) and coercivity (H C ) of the NPs were 70.3 emu g -1 and 398.4 Oe, respectively. The microporous Co/CoO/C NPs exhibited enhanced microwave absorption performance with a minimum reflection coefficient (RC) of -78.4 dB and a wide absorption bandwidth of 8.1 GHz (RC ≤ -10 dB), larger than those of the nonporous counterparts of -68.3 dB and 5.8 GHz. The minimum RC values of the microporous Co/CoO/C NPs at different thicknesses were much smaller than the nonporous counterparts. The high microwave absorption mechanism of the microporous Co/CoO/C nanocomposite can be interpreted in terms of the interfacial polarization relaxation of the core/shell and micropore structures, the effective permittivity modification of the air in the micropores and the polarization relaxation of the defects in the low-graphitization carbon shell and the porous Co NPs. Our study demonstrates that the microporous Co/CoO/C nanocomposite is an efficient microwave absorber with high absorption intensity and wide absorption bandwidth.

Characterization of Alq3 thin films by a near-field microwave microprobe.

PubMed

Hovsepyan, Artur; Lee, Huneung; Sargsyan, Tigran; Melikyan, Harutyun; Yoon, Youngwoon; Babajanyan, Arsen; Friedman, Barry; Lee, Kiejin

2008-09-01

We observed tris-8-hydroxyquinoline aluminum (Alq3) thin films dependence on substrate heating temperatures by using a near-field microwave microprobe (NFMM) and by optical absorption at wavelengths between 200 and 900 nm. The changes of absorption intensity at different substrate heating temperatures are correlated to the changes in the sheet resistance of Alq3 thin films.

Ultra-broadband microwave metamaterial absorber based on resistive sheets

NASA Astrophysics Data System (ADS)

Kim, Y. J.; Yoo, Y. J.; Hwang, J. S.; Lee, Y. P.

2017-01-01

We investigate a broadband perfect absorber for microwave frequencies, with a wide incident angle, using resistive sheets, based on both simulation and experiment. The absorber uses periodically-arranged meta-atoms, consisting of snake-shape metallic patterns and metal planes separated by three resistive sheet layers between four dielectric layers. We demonstrate the mechanism of the broadband by impedance matching with free space, and the distribution of surface currents at specific frequencies. In simulation, the absorption was over 96% in 1.4-6.0 GHz. The corresponding experimental absorption band over 96% was 1.4-4.0 GHz, however, the absorption was lower than 96% in the 4.0-6.0 GHz range because of the rather irregular thickness of the resistive sheets. Furthermore, it works for wide incident angles and is relatively independent of polarization. The design is scalable to smaller sizes in the THz range. The results of this study show potential for real applications in prevention of microwave frequency exposure, with devices such as cell phones, monitors, and microwave equipment.

Improved high-intensity microwave discharge lamp for atomic resonance absorption and fluorescence spectrometry.

PubMed

Lifshitz, A; Skinner, G B; Wood, D R

1978-09-01

An unusually good combination of high intensity and narrow line has been achieved in a microwave discharge lamp by placing the optical window in the center of the microwave cavity. Construction details and performance characteristics are described.

Synthesis and microwave absorption property of graphene oxide/carbon nanotubes modified with cauliflower-like Fe3O4 nanospheres

NASA Astrophysics Data System (ADS)

Yan, Shaojiu; Wang, Lina; Wang, Tihong; Zhang, Liqiang; Li, Yongfeng; Dai, Shenglong

2016-03-01

We report a simple procedure to fabricate graphene oxide/carbon nanotube hybrids coated with cauliflower-like Fe3O4 sphere. Characterizations have been carried out to investigate the morphology, crystalline structure of the composites by scanning electron microscopy, transmission electron microscopy and X-ray diffraction. Fe3O4 particles have the morphologies of multi-lacuna; moreover, some spheres are hollow. As a kind of potential microwave absorption material, the composites are lightweight and exhibit excellent microwave absorbing ability in the range of 2-16 GHz.

Experimental study of microwave-induced thermoacoustic imaging

NASA Astrophysics Data System (ADS)

Jacobs, Ryan T.

Microwave-Induced Thermoacoustic Imaging (TAI) is a noninvasive hybrid modality which improves contrast by using thermoelastic wave generation induced by microwave absorption. Ultrasonography is widely used in medical practice as a low-cost alternative and supplement to magnetic resonance imaging (MRI). Although ultrasonography has relatively high image resolution (depending on the ultrasonic wavelength at diagnostic frequencies), it suffers from low image contrast of soft tissues. In this work samples are irradiated with sub-microsecond electromagnetic pulses inducing acoustic waves in the sample that are then detected with an unfocused transducer. The advantage of this hybrid modality is the ability to take advantage of the microwave absorption coefficients which provide high contrast in tissue samples. This in combination with the superior spatial resolution of ultrasound waves is important to providing a low-cost alternative to MRI and early breast cancer detection methods. This work describes the implementation of a thermoacoustic experiment using a 5 kW peak power microwave source.

Thermoacoustic and photoacoustic characterizations of few-layer graphene by pulsed excitations

DOE Office of Scientific and Technical Information (OSTI.GOV)

Wang, Xiong; Department of Medical Imaging, The University of Arizona, Tucson, Arizona 85724; School of Information Science and Technology, ShanghaiTech University, Shanghai 200031

2016-04-04

We characterized the thermoacoustic and photoacoustic properties of large-area, few-layer graphene by pulsed microwave and optical excitations. Due to its high electric conductivity and low heat capacity per unit area, graphene lends itself to excellent microwave and optical energy absorption and acoustic signal emanation due to the thermoacoustic effect. When exposed to pulsed microwave or optical radiation, distinct thermoacoustic and photoacoustic signals generated by the few-layer graphene are obtained due to microwave and laser absorption of the graphene, respectively. Clear thermoacoustic and photoacoustic images of large-area graphene sample are achieved. A numerical model is developed and the simulated results aremore » in good accordance with the measured ones. This characterization work may find applications in ultrasound generator and detectors for microwave and optical radiation. It may also become an alternative characterization approach for graphene and other types of two-dimensional materials.« less

Spectral shape deformation in inverse spin Hall voltage in Y{sub 3}Fe{sub 5}O{sub 12}|Pt bilayers at high microwave power levels

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lustikova, J., E-mail: lustikova@imr.tohoku.ac.jp; Shiomi, Y.; Handa, Y.

2015-02-21

We report on the deformation of microwave absorption spectra and of the inverse spin Hall voltage signals in thin film bilayers of yttrium iron garnet (YIG) and platinum at high microwave power levels in a 9.45-GHz TE{sub 011} cavity. As the microwave power increases from 0.15 to 200 mW, the resonance field shifts to higher values, and the initially Lorentzian spectra of the microwave absorption intensity as well as the inverse spin Hall voltage signals become asymmetric. The contributions from opening of the magnetization precession cone and heating of YIG cannot well reproduce the data. Control measurements of inverse spinmore » Hall voltages on thin-film YIG|Pt systems with a range of line widths underscore the role of spin-wave excitations in spectral deformation.« less

Flower-like BiOI microsphere/Ni@C nanocapsule hybrid composites and their efficient microwave absorbing activity

NASA Astrophysics Data System (ADS)

Liu, Xianguo; Yu, Jieyi; Cui, Caiyun; Sun, Yuping; Li, Xiaolong; Li, Zhenxing

2018-07-01

At present, microwave absorbers are prepared by dispersing absorbing nanomaterials in a binder, which can lead to the aggregation of nanomaterials in the binder and further affect the optimization of the absorption performances. Hybrid micro/nano-scale structures are beneficial for buffering agglomeration phenomena and the construction of multiple interfaces. Here, Ni@C nanocapsules are conjugated onto flower-like BiOI microspheres, forming micro/nano-scale hybrid composites. The multiple interfaces between BiOI microspheres and Ni@C nanocapsules can bring enhanced dielectric loss and increased attenuation constant, resulting in the enhancement of absorption capacity (the optimal reflection loss reaches  ‑61.35 dB), increased width of the effective absorption band (the maximum effective bandwidth, f Emax , is 5.86 GHz) and the reduction of absorption thickness (the thickness corresponding to f Emax is 1.7 mm). This study highlights a simple idea for the optimization of electromagnetic absorbing performance, which is of great significance in the development of microwave absorbers.

Microwave absorption properties of a wave-absorbing coating employing carbonyl-iron powder and carbon black

NASA Astrophysics Data System (ADS)

Liu, Lidong; Duan, Yuping; Ma, Lixin; Liu, Shunhua; Yu, Zhen

2010-11-01

To prevent serious electromagnetic interference, a single-layer wave-absorbing coating employing complex absorbents composed of carbonyl-iron powder (CIP) and carbon black (CB) with epoxy resin as matrix was prepared. The morphologies of CIP and CB were characterized by scanning electron microscope (SEM) and transmission electron microscope (TEM), respectively. The electromagnetic parameters of CIP and CB were measured in the frequency range of 2-18 GHz by transmission/reflection technology, and the electromagnetic loss mechanisms of the two particles were discussed, respectively. The microwave absorption properties of the coatings were investigated by measuring reflection loss (RL) using arch method. The effects of CIP ratio, CB content and thickness on the microwave absorption properties were discussed, respectively. The results showed that the higher thickness, CIP or CB content could make the absorption band shift towards the lower frequency range. Significantly, the wave-absorbing coating could be applied in different frequency ranges according to actual demand by controlling the content of CIP or CB in composites.

The feasibility of using microwave-induced thermoacoustic tomography for detection and evaluation of renal calculi.

PubMed

Cao, Caijun; Nie, Liming; Lou, Cunguang; Xing, Da

2010-09-07

Imaging of renal calculi is important for patients who suffered a urinary calculus prior to treatment. The available imaging techniques include plain x-ray, ultrasound scan, intravenous urogram, computed tomography, etc. However, the visualization of a uric acid calculus (radiolucent calculi) is difficult and often impossible by the above imaging methods. In this paper, a new detection method based on microwave-induced thermoacoustic tomography was developed to detect the renal calculi. Thermoacoustic images of calcium oxalate and uric acid calculus were compared with their x-ray images. The microwave absorption differences among the calcium oxalate calculus, uric acid calculus and normal kidney tissue could be evaluated by the amplitude of the thermoacoustic signals. The calculi hidden in the swine kidney were clearly imaged with excellent contrast and resolution in the three orthogonal thermoacoustic images. The results indicate that thermoacoustic imaging may be developed as a complementary method for detecting renal calculi, and its low cost and effective feature shows high potential for clinical applications.

Design of lightweight broadband microwave absorbers in the X-band based on (polyaniline/MnNiZn ferrite) nanocomposites

NASA Astrophysics Data System (ADS)

Ali, Nassim Nasser; Al-Qassar Bani Al-Marjeh, Rama; Atassi, Yomen; Salloum, Akil; Malki, Adnan; Jafarian, Mojtaba

2018-05-01

We present the design of novel, lightweight, broadband microwave absorbers based on polyaniline/Mn0.1Ni0.45Zn0.45Fe2O4 (PANI/MnNiZn ferrite) nanocomposites. The ferrite is synthesized by sol-gel technique. Then, the polymer is deposited by in-situ chemical oxidative polymerization. The structural and morphological characterizations of the composites are investigated by SEM, XRD, FT-IR and UV-vis spectroscopy. The functional characterization is performed by measuring the dc-conductivity and microwave absorption characteristics in the X-band. The absorbers exhibit broad bandwidths under -10 dB ranging from 2.60 to 3.74 GHz and low surface density ranging from 2.5 to 3.1 kg/m2. The absorber of 3.74 GHz bandwidth has a minimum reflection loss of -31.32 dB at 11.13 GHz with a matching thickness of 3 mm and a low loading in paraffin of only 25% w/w.

Water vapor profiling using microwave radiometry

NASA Technical Reports Server (NTRS)

Wang, J. R.; Wilheit, T. T.

1988-01-01

Water vapor is one of the most important constituents in the Earth's atmosphere. Its spatial and temporal variations affect a wide spectrum of meteorological phenomena ranging from the formation of clouds to the development of severe storms. The passive microwave technique offers an excellent means for water vapor measurements. It can provide both day and night coverage under most cloud conditions. Two water vapor absorption features, at 22 and 183 GHz, were explored in the past years. The line strengths of these features differ by nearly two orders of magnitude. As a consequence, the techniques and the final products of water vapor measurements are also quite different. The research effort in the past few years was to improve and extend the retrieval algorithm to the measurements of water vapor profiles under cloudy conditions. In addition, the retrieval of total precipitable water using 183 GHz measurements, but in a manner analogous to the use of 22 GHz measurements, to increase measurement sensitivity for atmospheres of very low moisture content was also explored.

Preparation and characterization of Ba0.2Sr0.2La0.6MnO3 nanoparticles and investigation of size & shape effect on microwave absorption

NASA Astrophysics Data System (ADS)

Peymanfar, Reza; Javanshir, Shahrzad

2017-06-01

In this paper, the design and characterization of a radar absorbing material (RAM) was investigated at microwave frequency. Ba0.2Sr0.2La0.6MnO3 magnetic nanoparticles was synthesized thru a facile hydrothermal method in the presence of polymethyl methacrylate (PMMA) and the possibility of shape and size-controlled synthesis of nanoparticles (NPs) over the range 15-50 Nm was also explored. Afterward, the effect of shape and size of the synthesized Ba0.2Sr0.2La0.6MnO3 NPs on microwave absorption properties was investigated in KU-band. The crystal structures and morphology of as-synthesized nanoparticles were characterized and confirmed by FESEM, XRD, VSM, FTIR analysis. The RAM samples were prepared by dispersion of magnetic NPs in silicone rubber in an ultrasonic bath. The maximum reflection loss (RL) values NPs were 12.04 dB at 14.82 GHz and a broad absorption band (over 1.22 GHz) with RL values <-10 dB are obtained and the maximum reflection loss (RL) values of decrease and shaped NPs were 22.36 dB at 14.78 GHz and a broad absorption band (over 2.67 GHz) with RL values <-10 dB are obtained. The results indicated that the particle size and shape play a major role on the absorption properties of the composites in the 12.4-18 GHz frequency range. It is observed that microwave absorption properties increased with the decrease in average particle size of NPs.

Laboratory evaluation and application of microwave absorption properties under simulated conditions for planetary atmospheres

NASA Technical Reports Server (NTRS)

Steffes, P. G.

1986-01-01

After long arduous work with the simulator, measurements of the refractivity and absorptivity of nitrogen under conditions similar to those for Titan were completed. The most significant measurements, however, were those of the microwave absorption from gaseous ammonia under simulated conditions for the Jovian atmospheres over wavelengths from 1.3 to 22 cm. The results of these measurements are critical in that they confirm the theoretical calculation of the ammonia opacity using the Ben-Reuven lineshape. The application of both these results, and results obtained previously, to planetary observations at microwave frequencies were especially rewarding. Applications of the results for ammonia to radio astronomical observations of Jupiter in the 1.3 to 20 cm wavelength range and the application of results for gaseous H2SO4 under simulated Venus conditions are discussed.

Optimization of microwire/glass-fibre reinforced polymer composites for wind turbine application

NASA Astrophysics Data System (ADS)

Qin, F. X.; Peng, H. X.; Chen, Z.; Wang, H.; Zhang, J. W.; Hilton, G.

2013-11-01

We here report a comprehensive study of glass-fibre reinforced polymers (GFRP) incorporating ferromagnetic microwires for microwave absorption applications. With wire addition, a remarkable dependence of microwave absorption performance appears on the local properties of wires such as wire geometry and the mesostructure such as inter-wire spacing, as well as the embedded depth of the wires layer. The impact testing further demonstrates that the metallic microwires can to some extent improve the impact performance. Based on both the absorption and impact behavior, we propose an optimized design of the microwire/GFRP composites to achieve simultaneous best possible absorption and impact performance for multifunctional applications in aeronautical structures and wind turbines.

Effects of Natural Rubber on Microwave Absorption Characteristics of Some Li-Ni-Zn Ferrite-Thermoplastic Natural Rubber Composites

NASA Astrophysics Data System (ADS)

Abdul Hamid, Siti Atkah; Abdullah, Mustaffa Hj.; Ahmad, Sahrim Hj.; Mansor, Abdul Aziz; Yusoff, Ahmad Nazlim

2002-09-01

A microwave (Li0.5Fe0.5)0.4Ni0.3Zn0.3Fe2O4 (LNZ) ferrite was prepared by a conventional sintering method in air. Thermoplastic natural rubber (TPNR) was prepared from polypropylene (PP) and natural rubber (NR) in the ratios of 80:20, 70:30, 60:40, 50:50 and 40:60 with liquid natural rubber as a compatibilizer by a melt blending technique. LNZ ferrite-TPNR composites with 20 wt% ferrite filler were prepared using a Brabender plasticorder internal mixer. The microwave electromagnetic properties of the composites were studied in the frequency range of 0.3-13.5 GHz using a microwave vector network analyzer (MVNA). The real and imaginary components of the relative complex dielectric permittivity (\\varepsilonr*=\\varepsilonr\\prime-j\\varepsilonr\\prime\\prime) and magnetic permeability (μr*=μr\\prime-jμr\\prime\\prime) were calculated from the measured complex scattering parameters (S11* and S12*) using the Nicolson-Ross model. The dielectric and magnetic properties were found to depend on the NR and PP content in the composites. The minimum reflection loss (RL) under the matching conditions increases with increasing NR content.

Microwave-assisted extraction coupled online with derivatization, restricted access material cleanup, and high-performance liquid chromatography for determination of formaldehyde in aquatic products.

PubMed

Chen, Ligang; Jin, Haiyan; Xu, Haoyan; Sun, Lei; Yu, Aimin; Zhang, Hanqi; Ding, Lan

2009-05-27

A rapid technique based on microwave-assisted extraction (MAE) coupled online with derivatization, restricted access material cleanup, and high-performance liquid chromatography (HPLC) was developed for the determination of formaldehyde in aquatic products. Formaldehyde was first extracted with water under the action of microwaves and then directly introduced into a derivatization reservoir containing 2,4-dinitrophenylhydrazine (DNPH). The formaldehyde-DNPH derivative (100 μL) was loaded into a restricted access material (RAM) precolumn for online cleanup. Subsequently, the analyte was transferred from the precolumn to an analytical column and determined by UV absorption spectrum at 352 nm. The limit of detection (LOD) was 0.27 mg kg(-1). The intraday and interday precisions expressed as RSDs were 3.5% and 5.0%, respectively. This method was applied to determine the presence of formaldehyde in various aquatic products. The results were in agreement with those obtained by the state standard method (steam-distillation and offline HPLC analysis) used in China and higher than those obtained by the online ultrasound-assisted extraction (UAE) method. The recoveries obtained by analyzing 11 spiked aquatic products were in the range of 70.0%-105.0%. The online technique was demonstrated to be rapid with little consumption of samples and reagents.

Absorption Characterization of Mn-Zr-Substituted La-Sr Hexaferrite Using Open-Circuit and Short-Circuit Approaches in 8.2-18 GHz Frequency Range

NASA Astrophysics Data System (ADS)

Narang, Sukhleen Bindra; Kaur, Pawandeep; Bahel, Shalini; Pubby, Kunal

2018-01-01

The present study reports on the microwave absorption characterization of Mn2+-Zr4+ substituted lanthanum strontium ferrites, Sr0.85La0.15(MnZr) x Fe12-2 x O19, where x = 0.0, 0.25, 0.50, 0.75 and 1.0 in the X- and Ku-band. The synthesized ferrites are characterized with regard to their electromagnetic properties such as complex permittivity ( {ɛ^' - jɛ^'' ) and complex permeability ( {μ^' - jμ^'' ) using vector network analysis in the 8.2-18 GHz frequency range. Real and imaginary parts of permittivity decrease with the increase in Mn-Zr concentration due to a reduction in electron hopping conduction and eddy current losses, respectively. Microwave permeability spectra are also affected by the doping. The amplitude of magnetic loss peak increases with the increase in doping except for the x = 1.0 composition. Two commonly used approaches, open-circuit and short-circuit, have been employed for the absorption analysis. The difference in the results of these two techniques is justified on the basis of the reflection mechanism. The presented experimental findings underline the potential of the synthesized compositions with Mn-Zr concentrations x = 0.25, 0.5 and 0.75 in the suppression of electromagnetic reflections and radar signatures.

A Theoretical Study of Microwave Beam Absorption by a Rectenna

NASA Technical Reports Server (NTRS)

Ott, J. H.; Rice, J. S.; Thorn, D. C.

1981-01-01

The theoretical operational parameters for the workable satellite power system were examined. The system requirements for efficient transmission and reception of an environmentally benign microwave beam were determined.

Microwave heating of a high-Tc YBa2Cu3O6.9 superconductor through a Josephson-junction system

NASA Astrophysics Data System (ADS)

Stankowski, J.; Czyak, B.; Martinek, J.

1990-12-01

An overheating of a Josephson-junction system (JJS) in ceramic YBa2Cu3O6.9 samples was induced by microwave irradiation in a microwave cavity. The amplitude of the Josephson microwave absorption (JMA) was used as a monitor of the local JJS temperature. The difference between the JJS temperature and a sample temperature depends linearly on the power of the microwave field. A thermal hysteresis of Tc for heating and cooling is proportional to the microwave power applied in the JMA experiment.

Bandwidth enhancement in microwave absorption of binary nanocomposite ferrites hollow microfibers.

PubMed

Song, Fuzhan; Shen, Xiangqian; Yang, Xinchun; Meng, Xianfeng; Xiang, Jun; Liu, Ruijiang; Dong, Mingdong

2013-04-01

The binary Ba0.5Sr0.5Fe12O19 (BSFO)/Ni0.5Zn0.5Fe2O4 (NZFO) nanocomposite ferrites hollow microfibers with high aspect ratios have been prepared by the gel precursor transformation process. These microfibers possess a high specific surface area about 45.2 m2 g(-1), and a ratio of the hollow diameter to the fiber diameter estimated about 5/7. The binary nanocomposite ferrites are formed after the precursor calcined at 750 degrees C for 3 h. Their minimum reflection loss (RL) is -38.1 dB at 10.4 GHz. The microwave absorption bandwidth with RL value exceeding -20 dB covers the whole X-band (8.2-12.4 GHz) and Ku-band (12.4-18 GHz). This enhancement in microwave absorption can be attributed to the exchange-coupling interaction, interfacial polarization and small size effect in nanocomposite hollow microfibers.

Ultrathin and lightweight microwave absorbers made of mu-near-zero metamaterials

PubMed Central

Zhong, Shuomin; He, Sailing

2013-01-01

We present a theory of perfect absorption in a bilayer model composed of a mu-near-zero (MNZ) metamaterial (MM) absorbing layer on a metallic substrate. Our analytical solutions reveal that a MM layer with a large purely imaginary permeability and a moderate permittivity backed by a metallic plane has a zero reflection at normal incidence when the thickness is ultrathin. The impedance-mismatched metamaterial absorber (MA) can be 77.3% thinner than conventional impedance-matched MAs with the same material loss in order to get the same absorption. A microwave absorber using double-layered spiral MMs with a thickness of only about one percent of the operating wavelength is designed and realized. An absorption efficiency above 93% at 1.74 GHz is demonstrated experimentally at illumination angles up to 60 degrees. Our absorber is 98% lighter than traditional microwave absorbers made of natural materials working at the same frequencies. PMID:23803861

Measurement of dielectric properties of whole and ground chicken breast meat over the frequency range from 500 MHz to 50 GHz

USDA-ARS?s Scientific Manuscript database

The dielectric properties of food greatly influence its interaction with RF and MW electromagnetic fields and subsequently determine the absorption of microwave energy and consequent heating behavior of food materials in microwave heating and processing applications. Microwave heating is usually re...

Enhanced Microwave Absorption Properties of Carbon Black/Silicone Rubber Coating by Frequency-Selective Surface

NASA Astrophysics Data System (ADS)

Yang, Zhaoning; Luo, Fa; Gao, Lu; Qing, Yuchang; Zhou, Wancheng; Zhu, Dongmei

2016-10-01

A square frequency-selective surface (FSS) design has been employed to improve the microwave absorption properties of carbon black/silicone rubber (CBSR) composite coating. The FSS is placed on the surface of the CBSR coating. The effects of FSS design parameters on the microwave absorption properties of the CBSR coating have been investigated, including the size and period of the FSS design, and the thickness and permittivity of the coating. Simulation results indicate that the absorption peak for the CBSR coating alone is related to its thickness and electromagnetic parameters, while the combination of the CBSR coating with a FSS can exhibit a new absorption peak in the reflection curve; the frequency of the new absorption peak is determined by the resonance of the square FSS design and tightly depends on the size of the squares, with larger squares in the FSS design leading to a lower frequency of the new absorption peak. The enhancement of the absorption performance depends on achievement of a new absorption peak using a suitable size and period of the FSS design. In addition, the FSS design has a stable frequency response for both transverse electromagnetic (TE) and transverse magnetic (TM) polarizations as the incident angle varies from 0° to 40°. The optimized results indicate that the bandwidth with reflection loss below -5 dB can encompass the whole frequency range from 8 GHz to 18 GHz for thickness of the CBSR coating of only 1.8 mm. The simulation results are confirmed by experiments.

High Temperature Microwave Dielectric Properties of JSC-1AC Lunar Simulant

NASA Technical Reports Server (NTRS)

Allan, Shawn M.; Merritt, Brandon J.; Griffin, Brittany F.; Hintze, Paul E.; Shulman, Holly S.

2011-01-01

Microwave heating has many potential lunar applications including sintering regolith for lunar surface stabilization and heating regolith for various oxygen production reactors. The microwave properties of lunar simulants must be understood so this technology can be applied to lunar operations. Dielectric properties at microwave frequencies for a common lunar simulant, JSC-1AC, were measured up to 1100 C, which is approximately the melting point. The experimentally determined dielectric properties included real and imaginary permittivity (epsilon', epsilon"), loss tangent (tan delta), and half-power depth, the di stance at which a material absorbs 50% of incident microwave energy. Measurements at 2.45 GHz revealed tan delta of JSC-1A increases from 0.02 at 25 C to 0.31 at 110 C. The corresponding half-power depth decreases from a peak of 286 mm at 110 C, to 13 mm at 1100 C. These data indicate that JSC-1AC becomes more absorbing, and thus a better microwave heater as temperature increases. A half-power depth maximum at 100-200 C presents a barrier to direct microwave heating at low temperatures. Microwave heating experiments confirm the sluggish heating effect of weak absorption below 200 C, and increasingly strong absorption above 200 C, leading to rapid heating and melting of JSC-1AC.

Improved passive microwave sounding of the atmosphere

NASA Technical Reports Server (NTRS)

Staelin, D. H.; Rosenkranz, P. W.; Schwartz, M. J.

1996-01-01

The effort this year focused primarily on 118-GHz transmittance experiments. The data analyzed here was collected with the Microwave Temperature Sounder (MTS) radiometer package during the CAMEX deployment of 1993 with the aim of validating current models of atmospheric microwave absorption in the O2 bands near 54 and 118 GHz. Particular attention has been paid to data collected during four flights when the MTS scanned zenith while profiles of downwelling radiances were collected through ascents and descents. These radiances, in conjunction with radiosonde temperature data, permit the retrieval of band-averaged absorption profiles for each channel. The Millimeter-wave Propagation Model (MPM92) provides theoretical expressions for the absorption of microwaves by oxygen and water vapor and accounts for the interference of pressure-broadened spectral lines'. This model is a good fit to laboratory measurements at temperatures ranging from 279-327 K, but it has been suggested that extrapolation to the conditions of the atmospheric tropopause may result in underestimation of absorption by as much as 15 percent. Preliminary results of the analysis of MTS data appear to be in general agreement with the predictions of the MPM model to within the accuracy of the measurements, which through the coldest parts of the atmosphere ranges from less than plus or minus 5 percent in the most opaque channels to greater than plus or minus 10 percent in the most transparent channels. At those altitudes where each channel is most sensitive to changes in absorption, there is some indication that the modeled absorption may be biased low relative to the observations. Accurate instrument calibration provided challenges, particularly when observed radiances were as much as 260 K below the temperatures of the cold calibration load.

Microwave absorption properties of polypyrrole-SrFe12O19-TiO2-epoxy resin nanocomposites: Optimization using response surface methodology

NASA Astrophysics Data System (ADS)

Seyed Dorraji, M. S.; Rasoulifard, M. H.; Amani-Ghadim, A. R.; Khodabandeloo, M. H.; Felekari, M.; Khoshrou, M. R.; hajimiri, I.

2016-10-01

At a few works are discussed about formation of heterogeneous composites with different distribution of particle shape and size that are used for electromagnetic absorption purposes. In this study a novel heterogeneous nanocpmposites is investigated. The nanocomposite has been successfully prepared based on epoxy resin including various nano-metal oxides (TiO2, SrFe12O19) and polypyrrole (PPy) by sol-gel and the solution chemistry method, respectively. The performance of prepared nanocomposite in absorption of microwave in X-band range was investigated and transmission line method by X-band waveguide straight was used to measure EM parameters of nanocomposites. The Response surface methodology (RSM) with central composite design (CCD) was utilized to study the effects of the wt.% TiO2 in SrFe12O19, wt.% Tio2-SrFe12O19 in PPy and wt.% TiO2-SrFe12O19-PPy in epoxy resin, on the microwave absorption properties with the absorber thickness of only 2 mm. The proposed quadratic model was in accordance with the experimental results with correlation coefficient of 96.5%. The optimum condition for maximum microwave absorption efficiency were wt.% TiO2 in SrFe12O19 of 70, wt.% TiO2-SrFe12O19 in PPy of 10 and wt.% TiO2-SrFe12O19-PPy in epoxy of 25. The sample prepared in optimal conditions indicated reflection loss of -15 dB corresponding to 97% absorption, at the range of 9.2-10.8 GHz.

Protection layers on a superconducting microwave resonator toward a hybrid quantum system

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lee, Jongmin, E-mail: jongmin.lee@sandia.gov; Sandia National Laboratories, Albuquerque, New Mexico 87123; Park, Dong Hun, E-mail: leomac@umd.edu

2015-10-07

We propose a protection scheme of a superconducting microwave resonator to realize a hybrid quantum system, where cold neutral atoms are coupled with a single microwave photon through magnetic dipole interaction at an interface inductor. The evanescent field atom trap, such as a waveguide/nanofiber atom trap, brings both surface-scattered photons and absorption-induced broadband blackbody radiation which result in quasiparticles and a low quality factor at the resonator. A proposed multiband protection layer consists of pairs of two dielectric layers and a thin nanogrid conductive dielectric layer above the interface inductor. We show numerical simulations of quality factors and reflection/absorption spectra,more » indicating that the proposed multilayer structure can protect a lumped-element microwave resonator from optical photons and blackbody radiation while maintaining a reasonably high quality factor.« less

Preparation and high-performance microwave absorption of hierarchical dendrite-like Co superstructures self-assembly of nanoflakes

NASA Astrophysics Data System (ADS)

Yu, Miao; Wang, Lirui; Yang, Pingan; Fu, Jie

2017-12-01

Dendritic-like Co superstructures based on the self-assembly of nanoflakes that could efficiently suppress the eddy current were successfully synthesized via a facile, rapid, and energy-saving chemical reduction method. Since crystal structure, size, and special geometrical morphology, magnetism have a vital influence on microwave absorption properties, the as-obtained products were characterized by x-ray diffraction, scanning electron microscopy, vibrating sample magnetometry, and vector network analysis. The prepared dendritic Co possesses abundant secondary branches that extend to the 3D space. Their dimensions, spacing, sheet-like blocks, and high-ordering microstructures all contribute to the penetration, scattering, and attenuation of EM waves. The composites present attractive microwave absorption performances in the X band, as well as in the whole S band (2-4 GHz). This work investigates the mechanism of absorption for the as-obtained Co, offers a promising strategy for the fabrication of hierarchical Co microstructure assemblies by multi-leaf flakes and introduces the application of dendritic-like Co as a highly efficient absorber in the S band and X band.

[Determination of metals in waste bag filter of steel works by microwave digestion-flame atomic absorption spectrometry].

PubMed

Ning, Xun-An; Zhou, Yun; Liu, Jing-Yong; Wang, Jiang-Hui; Li, Lei; Ma, Xiao-Guo

2011-09-01

A method of microwave digestion technique-flame atomic absorption spectrometry was proposed to determine the total contents of Cu, Zn, Pb, Cd, Cr and Ni in five different kinds of waste bag filters from a steel plant. The digestion effects of the six acid systems on the heavy metals digestion were studied for the first time. The relative standard deviation (RSD) of the method was between 1.02% and 9.35%, and the recovery rates obtained by standard addition method ranged from 87.7% to 105.6%. The results indicated that the proposed method exhibited the advantages of simplicity, speediness, accuracy and repeatability, and it was suitable for determining the metal elements of the waste bag filter. The results also showed that different digestion systems should be used according to different waste bag filters. The waste bag filter samples from different production processes had different metal elements content. The Pb and Zn were the highest in the waste bag filters, while the Cu, Ni, Cd and Cr were relatively lower. These determination results provided the scientific data for further treatment and disposal of the waste bag filter.

High microwave attenuation performance of planar carbonyl iron particles with orientation of shape anisotropy field

NASA Astrophysics Data System (ADS)

Guo, Cheng; Yang, Zhihong; Shen, Shile; Liang, Juan; Xu, Guoyue

2018-05-01

Planar anisotropy carbonyl iron (PACI) particles were prepared from commercial spherical carbonyl iron particles through a high performance ball-milling technique. The paraffin composites with orientation of shape anisotropy field for these PACI particles were obtained by applying an external magnetic field during the fabrication process. The frequency-dependent complex permeability values of these prepared paraffin composites have been investigated in the frequency range of 1-18 GHz. The results demonstrate that the orientation of shape anisotropy field for these PACI particles can effectively increase the complex permeability and decrease the complex permittivity values. Benefit from the enhancement in the complex permeability and reduction in the complex permittivity, the better impedance matching condition can be obtained and thus the good microwave absorption performance can be achieved for the samples with enough magnetic field orientation time.

Co7Fe3 and Co7Fe3@SiO2 Nanospheres with Tunable Diameters for High-Performance Electromagnetic Wave Absorption.

PubMed

Chen, Na; Jiang, Jian-Tang; Xu, Cheng-Yan; Yuan, Yong; Gong, Yuan-Xun; Zhen, Liang

2017-07-05

Ferromagnetic metal/alloy nanoparticles have attracted extensive interest for electromagnetic wave-absorbing applications. However, ferromagnetic nanoparticles are prone to oxidization and producing eddy currents, leading to the deterioration of electromagnetic properties. In this work, a simple and scalable liquid-phase reduction method was employed to synthesize uniform Co 7 Fe 3 nanospheres with diameters ranging from 350 to 650 nm for high-performance microwave absorption application. Co 7 Fe 3 @SiO 2 core-shell nanospheres with SiO 2 shell thicknesses of 30 nm were then fabricated via a modified Stöber method. When tested as microwave absorbers, bare Co 7 Fe 3 nanospheres with a diameter of 350 nm have a maximum reflection loss (RL) of 78.4 dB and an effective absorption with RL > 10 dB from 10 to 16.7 GHz at a small thickness of 1.59 mm. Co 7 Fe 3 @SiO 2 nanospheres showed a significantly enhanced microwave absorption capability for an effective absorption bandwidth and a shift toward a lower frequency, which is ascribed to the protection of the SiO 2 shell from direct contact among Co 7 Fe 3 nanospheres, as well as improved crystallinity and decreased defects upon annealing. This work illustrates a simple and effective method to fabricate Co 7 Fe 3 and Co 7 Fe 3 @SiO 2 nanospheres as promising microwave absorbers, and the design concept can also be extended to other ferromagnetic alloy particles.

Rapid analysis of the essential oil components of dried Zanthoxylum bungeanum Maxim by Fe2O3-magnetic-microsphere-assisted microwave distillation and simultaneous headspace single-drop microextraction followed by GC-MS.

PubMed

Ye, Qing

2013-06-01

In this work, microwave distillation assisted by Fe2 O3 magnetic microspheres (FMMS) and headspace single-drop microextraction were combined, and developed for determination of essential oil compounds in dried Zanthoxylum bungeanum Maxim (ZBM). The FMMS were used as microwave absorption solid medium for dry distillation of dried ZBM. Using the proposed method, isolation, extraction, and concentration of essential oil compounds can be carried out in a single step. The experimental parameters including extraction solvent, solvent volume, microwave power, irradiation time, and the amount of added FMMS, were studied. The optimal analytical conditions were: 2.0 μL decane as the extraction solvent, microwave power of 300 W, irradiation time of 2 min, and the addition of 0.1 g FMMS to ZBM. The method precision was from 4 to 10%. A total of 52 compounds were identified by the proposed method. The conventional steam distillation method was also used for the analysis of essential oil in dried ZBM and only 31 compounds were identified by steam distillation method. It was found that the proposed method is a simple, rapid, reliable, and solvent-free technique for the determination of volatile compounds in Chinese herbs. © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Study on preparation and microwave absorption property of the core-nanoshell composite materials doped with La.

PubMed

Wei, Liqiu; Che, Ruxin; Jiang, Yijun; Yu, Bing

2013-12-01

Microwave absorbing material plays a great role in electromagnetic pollution controlling, electromagnetic interference shielding and stealth technology, etc. The core-nanoshell composite materials doped with La were prepared by a solid-state reaction method, which is applied to the electromagnetic wave absorption. The core is magnetic fly-ash hollow cenosphere, and the shell is the nanosized ferrite doped with La. The thermal decomposition process of the sample was investigated by thermogravimetry and differential thermal analysis. The morphology and components of the composite materials were investigated by the X-ray diffraction analysis, the microstructure was observed by scanning electron microscope and transmission electron microscope. The results of vibrating sample magnetometer analysis indicated that the exchange-coupling interaction happens between ferrite of magnetic fly-ash hollow cenosphere and nanosized ferrite coating, which caused outstanding magnetic properties. The microwave absorbing property of the sample was measured by reflectivity far field radar cross section of radar microwave absorbing material with vector network analyzer. The results indicated that the exchange-coupling interaction enhanced magnetic loss of composite materials. Therefore, in the frequency of 5 GHz, the reflection coefficient can achieve -24 dB. It is better than single material and is consistent with requirements of the microwave absorbing material at the low-frequency absorption. Copyright © 2013 The Research Centre for Eco-Environmental Sciences, Chinese Academy of Sciences. Published by Elsevier B.V. All rights reserved.

Achieving the interfacial polarization on C/Fe3C heterojunction structures for highly efficient lightweight microwave absorption.

PubMed

Zhang, Yanan; Liu, Wei; Quan, Bin; Ji, Guangbin; Ma, Jianna; Li, Daoran; Meng, Wei

2017-12-15

Design of dielectric/magnetic heterostructure and multiple interfaces is a challenge for the microwave absorption. Thus, in this study, a novel C/Fe 3 C nanocomposites have been fabricated by annealing the precursors obtained by the facile chemical blowing of polyvinyl pyrrolidone (PVP) and Fe(NO 3 ) 3 ·9H 2 O. By changing the content of Fe(NO 3 ) 3 ·9H 2 O, the honeycomb-like structure with scads of pores and electromagnetic parameters could be successfully tailored. When the addition of Fe(NO 3 ) 3 ·9H 2 O is ranging from 1 to 2g, honeycomb-structured nanocomposites possess high performance microwave absorption when mixed with 90wt% paraffin. The minimal reflection loss is -37.4dB at 13.6GHz and effective bandwidth can reach to 5.6GHz when the thickness is 2.0mm, indicating its great potential in microwave absorbing field. Its outstanding microwave performance is tightly related to the porous structure and substantial interface such as carbon/air and carbon/Fe 3 C, which are in favor of the impedance matching and interfacial polarization. Thus, our study may provide a good reference for the facile synthesis of light-weight carbon-based nanocomposites with effective interfacial polarization. Copyright © 2017 Elsevier Inc. All rights reserved.

Microwave Induced Direct Bonding of Single Crystal Silicon Wafers

NASA Technical Reports Server (NTRS)

Budraa, N. K.; Jackson, H. W.; Barmatz, M.

1999-01-01

We have heated polished doped single-crystal silicon wafers in a single mode microwave cavity to temperatures where surface to surface bonding occurred. The absorption of microwaves and heating of the wafers is attributed to the inclusion of n-type or p-type impurities into these substrates. A cylindrical cavity TM (sub 010) standing wave mode was used to irradiate samples of various geometry's at positions of high magnetic field. This process was conducted in vacuum to exclude plasma effects. This initial study suggests that the inclusion of impurities in single crystal silicon significantly improved its microwave absorption (loss factor) to a point where heating silicon wafers directly can be accomplished in minimal time. Bonding of these substrates, however, occurs only at points of intimate surface to surface contact. The inclusion of a thin metallic layer on the surfaces enhances the bonding process.

Reducing microwave absorption with fast frequency modulation.

PubMed

Qin, Juehang; Hubler, A

2017-05-01

We study the response of a two-level quantum system to a chirp signal, using both numerical and analytical methods. The numerical method is based on numerical solutions of the Schrödinger solution of the two-level system, while the analytical method is based on an approximate solution of the same equations. We find that when two-level systems are perturbed by a chirp signal, the peak population of the initially unpopulated state exhibits a high sensitivity to frequency modulation rate. We also find that the aforementioned sensitivity depends on the strength of the forcing, and weaker forcings result in a higher sensitivity, where the frequency modulation rate required to produce the same reduction in peak population would be lower. We discuss potential applications of this result in the field of microwave power transmission, as it shows applying fast frequency modulation to transmitted microwaves used for power transmission could decrease unintended absorption of microwaves by organic tissue.

Multi-band microwave metamaterial absorber based on coplanar Jerusalem crosses

NASA Astrophysics Data System (ADS)

Wang, Guo-Dong; Liu, Ming-Hai; Hu, Xi-Wei; Kong, Ling-Hua; Cheng, Li-Li; Chen, Zhao-Quan

2014-01-01

The influence of the gap on the absorption performance of the conventional split ring resonator (SRR) absorber is investigated at microwave frequencies. Our simulated results reveal that the geometry of the square SRR can be equivalent to a Jerusalem cross (JC) resonator and its corresponding metamaterial absorber (MA) is changed to a JC absorber. The JC MA exhibits an experimental absorption peak of 99.1% at 8.72 GHz, which shows an excellent agreement with our simulated results. By simply assembling several JCs with slightly different geometric parameters next to each other into a unit cell, a perfect multi-band absorption can be effectively obtained. The experimental results show that the MA has four distinct and strong absorption peaks at 8.32 GHz, 9.8 GHz, 11.52 GHz and 13.24 GHz. Finally, the multi-reflection interference theory is introduced to interpret the absorption mechanism.

Synthesis and characterization of some metal oxide nanocrystals by microwave irradiation

DOE Office of Scientific and Technical Information (OSTI.GOV)

Rashad, M.; Gaber, A.; Abdelrahim, M. A.

2013-12-16

Copper oxide and cobalt oxide (CuO, Co3O4) nanocrystals (NCs) have been successfully prepared in a short time using microwave irradiation. The resulted powders of nanocrystals (NCs) were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). Thermogravimetric analysis (TGA) measurements are also studied. Fourier-transform infrared (FT-IR) and UV–visible absorption spectroscopy of both kind of nanoparticels are illustrated. Optical absorption analysis indicated the direct band gap for both kinds of nanocrystals.

Electromagnetic interference shielding and microwave absorption properties of cobalt ferrite CoFe2O4/polyaniline composite

NASA Astrophysics Data System (ADS)

Ismail, Mukhils M.; Rafeeq, Sewench N.; Sulaiman, Jameel M. A.; Mandal, Avinandan

2018-05-01

Improvement of microwave-absorbing materials (MAMs) is the most important research area in various applications, such as in communication, radiation medical exposure, electronic warfare, air defense, and different civilian applications. Conducting polymer, polyaniline doped with para toluene sulphonic acid (PANI-PTSA) as well as cobalt ferrite (CoFe2O4) is synthesized by sol-gel method and intensely blends in different ratios. The characterization of the composite materials, CoFe2O4/PANI-PTSA (CFP1, CFP2, CFP3 and CFP4), was performed by X-ray diffraction (XRD), atomic force microscopy (AFM) and vibrating sample magnetometry (VSM). The microwave-absorbing properties' reflection loss (dB) and important parameters, such as complex relative permittivity ( ɛ r '- jɛ r ″) and complex relative permeability ( µ r '- jµ r ″) were measured in different microwave frequencies in the X-band (8.2-12.4 GHz) region. The composite material CFP3 showed a wider absorption frequency range and maximum reflection loss of - 28.4 dB (99.8% power absorption) at 8.1 GHz and - 9.6 dB (> 90% power absorption) at 11.2 GHz, and so the composite can be used as a microwave absorber; however, it can be more suitable for application in daily life for making cell phones above 9 GHz. Also the results showed that the thicker composites like CFP3 (4 mm) exhibit obviously better EMI SE as compared with the thinner ones (0.19, 0.19, 0.3 mm); this may be related to the low transmission of the EM wave from the composites.

On-chip dual-comb source for spectroscopy.

PubMed

Dutt, Avik; Joshi, Chaitanya; Ji, Xingchen; Cardenas, Jaime; Okawachi, Yoshitomo; Luke, Kevin; Gaeta, Alexander L; Lipson, Michal

2018-03-01

Dual-comb spectroscopy is a powerful technique for real-time, broadband optical sampling of molecular spectra, which requires no moving components. Recent developments with microresonator-based platforms have enabled frequency combs at the chip scale. However, the need to precisely match the resonance wavelengths of distinct high quality-factor microcavities has hindered the development of on-chip dual combs. We report the simultaneous generation of two microresonator combs on the same chip from a single laser, drastically reducing experimental complexity. We demonstrate broadband optical spectra spanning 51 THz and low-noise operation of both combs by deterministically tuning into soliton mode-locked states using integrated microheaters, resulting in narrow (<10 kHz) microwave beat notes. We further use one comb as a reference to probe the formation dynamics of the other comb, thus introducing a technique to investigate comb evolution without auxiliary lasers or microwave oscillators. We demonstrate high signal-to-noise ratio absorption spectroscopy spanning 170 nm using the dual-comb source over a 20-μs acquisition time. Our device paves the way for compact and robust spectrometers at nanosecond time scales enabled by large beat-note spacings (>1 GHz).

Floquet theory of microwave absorption by an impurity in the two-dimensional electron gas

NASA Astrophysics Data System (ADS)

Chepelianskii, Alexei D.; Shepelyansky, Dima L.

2018-03-01

We investigate the dynamics of a two-dimensional electron gas (2DEG) under circular polarized microwave radiation in the presence of dilute localized impurities. Inspired by recent developments on Floquet topological insulators we obtain the Floquet wave functions of this system which allow us to predict the microwave absorption and charge density responses of the electron gas; we demonstrate how these properties can be understood from the underlying semiclassical dynamics even for impurities with a size of around a magnetic length. The charge density response takes the form of a rotating charge density vortex around the impurity that can lead to a significant renormalization of the external microwave field which becomes strongly inhomogeneous on the scale of a cyclotron radius around the impurity. We show that this inhomogeneity can suppress the circular polarization dependence which is theoretically expected for microwave induced resistance oscillations but which was not observed in experiments on semiconducting 2DEGs. Our explanation for this so far unexplained polarization independence has close similarities with the Azbel'-Kaner effect in metals where the interaction length between the microwave field and conduction electrons is much smaller than the cyclotron radius due to skin effect generating harmonics of the cyclotron resonance.

MICROWAVE RESONANCES IN DNA

EPA Science Inventory

This report describes spectroscopic studies of DNA which were undertaken to better understand a physical basis for microwave absorption by this molecule. hree types of studies are described. ) The low frequency scattered light spectrum of DNA was studied by two methods. irst, Ram...

Laser heterodyne detection techniques. [for atmospheric monitoring applications

NASA Technical Reports Server (NTRS)

Menzies, R. T.

1976-01-01

The principles of heterodyne radiometry are examined, taking into account thermal radiation, the Dicke microwave radiometer, photomixing in the infrared, and signal-to-noise considerations. The passive heterodyne radiometer is considered and a description is presented of heterodyne techniques in active monitoring systems. Attention is given to gas emissivities in the infrared, component requirements, experimental heterodyne detection of gases, a comparison of the passive heterodyne radiometer with the Michelson interferometer-spectrometer, airborne monitoring applications, turbulence effects on passive heterodyne radiometry, sensitivity improvements with heterodyning, atmosphere-induced degradation of bistatic system performance, pollutant detection experiments with a bistatic system, and the airborne laser absorption spectrometer. Future improvements in spectral flexibility are also discussed.

Laboratory evaluation and application of microwave absorption properties under simulated conditions for planetary atmospheres

NASA Technical Reports Server (NTRS)

Steffes, P. G.

1986-01-01

The recognition of the need to make laboratory measurements of simulated planetary atmospheres over a range of temperatures and pressure which correspond to the altitudes probed by radio occultation experiments, and over a range of frequencies which correspond to both radio occultation experiments and radio astronomical observations, has led to the development of a facility at Georgia Tech which is capable of making such measurements. Construction was completed of the outer planets simulator and measurements were conducted of the microwave absorption and refraction from nitrogen under simulated Titan conditions. The results of these and previous laboratory measurements were applied to a wide range of microwave opacity measurements, in order to derive constituent densities and distributions in planetary atmospheres such as Venus.

Ultrabroadband Microwave Metamaterial Absorber Based on Electric SRR Loaded with Lumped Resistors

NASA Astrophysics Data System (ADS)

Zhao, Jingcheng; Cheng, Yongzhi

2016-10-01

An ultrabroadband microwave metamaterial absorber (MMA) based on an electric split-ring resonator (ESRR) loaded with lumped resistors is presented. Compared with an ESRR MMA, the composite MMA (CMMA) loaded with lumped resistors offers stronger absorption over an extremely extended bandwidth. The reflectance simulated under different substrate loss conditions indicates that incident electromagnetic (EM) wave energy is mainly consumed by the lumped resistors. The simulated surface current and power loss density distributions further illustrate the mechanism underlying the observed absorption. Further simulation results indicate that the performance of the CMMA can be tuned by adjusting structural parameters of the ESRR and lumped resistor parameters. We fabricated and measured MMA and CMMA samples. The CMMA yielded below -10 dB reflectance from 4.4 GHz to 18 GHz experimentally, with absorption bandwidth and relative bandwidth of 13.6 GHz and 121.4%, respectively. This ultrabroadband microwave absorber has potential applications in the electromagnetic energy harvesting and stealth fields.

VUV absorption spectroscopy measurements of the role of fast neutral atoms in a high-power gap breakdown

NASA Astrophysics Data System (ADS)

Filuk, A. B.; Bailey, J. E.; Cuneo, M. E.; Lake, P. W.; Nash, T. J.; Noack, D. D.; Maron, Y.

2000-12-01

The maximum power achieved in a wide variety of high-power devices, including electron and ion diodes, z pinches, and microwave generators, is presently limited by anode-cathode gap breakdown. A frequently discussed hypothesis for this effect is ionization of fast neutral atoms injected throughout the anode-cathode gap during the power pulse. We describe a newly developed diagnostic tool that provides a direct test of this hypothesis. Time-resolved vacuum-ultraviolet absorption spectroscopy is used to directly probe fast neutral atoms with 1-mm spatial resolution in the 10-mm anode-cathode gap of the SABRE 5 MV, 1 TW applied-B ion diode. Absorption spectra collected during Ar RF glow discharges and with CO2 gas fills confirm the reliability of the diagnostic technique. Throughout the 50-100 ns ion diode pulses no measurable neutral absorption was seen, setting upper limits of (0.12-1.5)×1014 cm-3 for ground-state fast neutral atom densities of H, C, N, O, and F. The absence of molecular absorption bands also sets upper limits of (0.16-1.2)×1015 cm-3 for common simple molecules. These limits are low enough to rule out ionization of fast neutral atoms as a breakdown mechanism. Breakdown due to ionization of molecules is also found to be unlikely. This technique can now be applied to quantify the role of neutral atoms in other high-power devices.

VUV absorption spectroscopy measurements of the role of fast neutral atoms in high-power gap breakdown

DOE Office of Scientific and Technical Information (OSTI.GOV)

FILUK,A.B.; BAILEY,JAMES E.; CUNEO,MICHAEL E.

The maximum power achieved in a wide variety of high-power devices, including electron and ion diodes, z pinches, and microwave generators, is presently limited by anode-cathode gap breakdown. A frequently-discussed hypothesis for this effect is ionization of fast neutral atoms injected throughout the anode-cathode gap during the power pulse. The authors describe a newly-developed diagnostic tool that provides the first direct test of this hypothesis. Time-resolved vacuum-ultraviolet absorption spectroscopy is used to directly probe fast neutral atoms with 1 mm spatial resolution in the 10 mm anode-cathode gap of the SABRE 5 MV, 1 TW applied-B ion diode. Absorption spectramore » collected during Ar RF glow discharges and with CO{sub 2} gas fills confirm the reliability of the diagnostic technique. Throughout the 50--100 ns ion diode pulses no measurable neutral absorption is seen, setting upper limits of 0.12--1.5 x 10{sup 14} cm{sup {minus}3} for ground state fast neutral atom densities of H, C, N, O, F. The absence of molecular absorption bands also sets upper limits of 0.16--1.2 x 10{sup 15} cm{sup {minus}3} for common simple molecules. These limits are low enough to rule out ionization throughout the gap as a breakdown mechanism. This technique can now be applied to quantify the role of neutral atoms in other high-power devices.« less

Digital communications: Microwave applications

NASA Astrophysics Data System (ADS)

Feher, K.

Transmission concepts and techniques of digital systems are presented; and practical state-of-the-art implementation of digital communications systems by line-of-sight microwaves is described. Particular consideration is given to statistical methods in digital transmission systems analysis, digital modulation methods, microwave amplifiers, system gain, m-ary and QAM microwave systems, correlative techniques and applications to digital radio systems, hybrid systems, digital microwave systems design, diversity and protection switching techniques, measurement techniques, and research and development trends and unsolved problems.

Microwave Resonant Cavity and Loaded Carbon Nanotubes -- A Sensor to Detect Toxins like Methamphetamine

NASA Astrophysics Data System (ADS)

Anand, Aman; Robert, James; Henley, Don; Dahiya, Jai

2006-10-01

A resonant cavity operating in TM010 mode was used to study the absorption response of Single Walled Carbon Nanotubes and other Nanomaterials for different types of gas molecules. The range of the frequency signal as a probe was chosen arbitrarily between 9.1 -9.8 GHz. A highly specific range will be studied for further experiments. It was found that for different pressures of different gases and different types of Nanomaterials, there was a different response in the shifts of the probe signal for each cycle of gassing and degassing of the cavity. The preliminary work done so far suggests that Microwave spectroscopy of the complex medium of gases and Carbon Nanotubes can be used as a highly sensitive technique in studying the complex dielectric response of different polar as well as non-polar gases when subjected to intense electromagnetic fields within the Cavity.

Microwave-assisted synthesis and characterization of nickel ferrite nanoparticles

DOE Office of Scientific and Technical Information (OSTI.GOV)

Carpenter, Gopal; Sen, Ravindra; Gupta, Nitish, E-mail: nitish.nidhi75@gmail.com

2015-08-28

Nickel ferrite nanoparticles (NiFe{sub 2}O{sub 4}) were successfully prepared by microwave-assisted combustion method (MWAC) using citric Electron acid as a chelating agent. NiFe{sub 2}O{sub 4} nanoparticles were characterized by X-ray diffraction (XRD) pattern, Scanning Microscopy (SEM), Fourier transform infrared (FTIR) and UV-Visible techniques. XRD analysis revealed that NiFe{sub 2}O{sub 4} nanoparticles have spinel cubic structure with the average crystalline size of 26.38 nm. SEM analysis revealed random and porous structural morphology of particles and FTIR showed absorption bands related to octahedral and tetrahedral sites, in the range 400–600cm{sup −1} which strongly favor the formation of NiFe{sub 2}O{sub 4} nanoparticles. The opticalmore » band gap is determined by UV Visible method and found to be 5.4 eV.« less

Evaluation of methods for trace-element determination with emphasis on their usability in the clinical routine laboratory.

PubMed

Bolann, B J; Rahil-Khazen, R; Henriksen, H; Isrenn, R; Ulvik, R J

2007-01-01

Commonly used techniques for trace-element analysis in human biological material are flame atomic absorption spectrometry (FAAS), graphite furnace atomic absorption spectrometry (GFAAS), inductively coupled plasma atomic emission spectrometry (ICP-AES) and inductively coupled plasma mass spectrometry (ICP-MS). Elements that form volatile hydrides, first of all mercury, are analysed by hydride generation techniques. In the absorption techniques the samples are vaporized into free, neutral atoms and illuminated by a light source that emits the atomic spectrum of the element under analysis. The absorbance gives a quantitative measure of the concentration of the element. ICP-AES and ICP-MS are multi-element techniques. In ICP-AES the atoms of the sample are excited by, for example, argon plasma at very high temperatures. The emitted light is directed to a detector, and the optical signals are processed to values for the concentrations of the elements. In ICP-MS a mass spectrometer separates and detects ions produced by the ICP, according to their mass-to-charge ratio. Dilution of biological fluids is commonly needed to reduce the effect of the matrix. Digestion using acids and microwave energy in closed vessels at elevated pressure is often used. Matrix and spectral interferences may cause problems. Precautions should be taken against trace-element contamination during collection, storage and processing of samples. For clinical problems requiring the analysis of only one or a few elements, the use of FAAS may be sufficient, unless the higher sensitivity of GFAAS is required. For screening of multiple elements, however, the ICP techniques are preferable.

Emission, absorption and group delay of microwaves in the atmosphere in relation to water vapour content over the Indian subcontinent

NASA Technical Reports Server (NTRS)

Sen, A. K.; Gupta, A. K. D.; Karmakar, P. K.; Barman, S. D.; Bhattacharya, A. B.; Purkait, N.; Gupta, M. K. D.; Sehra, J. S.

1985-01-01

The advent of satellite communication for global coverage has apparently indicated a renewed interest in the studies of radio wave propagation through the atmosphere, in the VHF, UHF and microwave bands. The extensive measurements of atmosphere constituents, dynamics and radio meterological parameters during the Middle Atmosphere Program (MAP) have opened up further the possibilities of studying tropospheric radio wave propagation parameters, relevant to Earth/space link design. The three basic parameters of significance to radio propagation are thermal emission, absorption and group delay of the atmosphere, all of which are controlled largely by the water vapor content in the atmosphere, particular at microwave bands. As good emitters are also good absorbers, the atmospheric emission as well as the absorption attains a maximum at the frequency of 22.235 GHz, which is the peak of the water vapor line. The group delay is practically independent of frequency in the VHF, UHF and microwave bands. However, all three parameters exhibit a similar seasonal dependence originating presumably from the seasonal dependence of the water vapor content. Some of the interesting results obtained from analyses of radiosonde data over the Indian subcontinent collected by the India Meteorological Department is presented.

Microwave electromagnetic and absorption properties of SiO2/C core/shell composites plated with metal cobalt

NASA Astrophysics Data System (ADS)

Shen, Guozhu; Fang, Xumin; Wu, Hongyan; Wei, Hongyu; Li, Jingfa; Li, Kaipeng; Mei, Buqing; Xu, Yewen

2017-04-01

A facile method has been developed to fabricate magnetic core/shell SiO2/C/Co sub-microspheres via the pyrolysis of SiO2/PANI (polyaniline) and electroless plating method. The electromagnetic parameters of these SiO2/C and SiO2/C/Co composites were measured and the microwave reflection loss properties were evaluated in the frequency range of 2-18 GHz. The results show that the dielectric loss of SiO2/C composite increases with the increase of carbonization temperature and the magnetic loss enhances due to the deposition of cobalt on the SiO2/C sub-microspheres. The reflection loss results exhibit that the microwave absorption properties of the SiO2/C/Co composites are more excellent than those of SiO2/C composites for each thickness. The maximum effective absorption bandwidth (reflection loss ≤ -10 dB) arrives at 5.0 GHz (13.0-18 GHz) for SiO2/C/Co composite with 1.5 mm of thickness and the minimum reflection loss value is -24.0 dB at 5.0 GHz with 4.0 mm of thickness. The microwave loss mechanism of the SiO2/C/Co composites was also discussed in this paper.

Laboratory evaluation and application of microwave absorption properties under simulated conditions for planetary atmospheres

NASA Technical Reports Server (NTRS)

Steffes, Paul G.

1992-01-01

Radio absorptivity data for planetary atmospheres obtained from spacecraft radio occultation experiments and earth-based radio astronomical observations can be used to infer abundances of microwave absorbing atmospheric constituents in those atmospheres, as long as reliable information regarding the microwave absorbing properties of potential constituents is available. The use of theoretically derived microwave absorption properties for such atmospheric constituents, or using laboratory measurements of such properties under environmental conditions which are significantly different than those of the planetary atmosphere being studied, often leads to significant misinterpretation of available opacity data. The recognition of the need to make such laboratory measurements of simulated planetary atmospheres over a range of temperatures and pressures which correspond to the altitudes probed by both radio occultation experiments and radio astronomical observations, and over a range of frequencies which correspond to those used in both radio occultation experiments and radio astronomical observations, has led to the development of a facility at Georgia Tech which is capable of making such measurements. The goal of this investigation was to conduct such measurements and to apply the results to a wide range of planetary observations, both spacecraft and earth-based, in order to determine the identity and abundance profiles of constituents in those planetary atmospheres.

Absorption and Reflection Experiments on High-Mobility 2DEGs in the Regime of Microwave-Induced Resistance Oscillations

NASA Astrophysics Data System (ADS)

Studenikin, S. A.; Potemski, M.; Sachrajda, A. S.; Hilke, M.; Pfeiffer, L. N.; West, K. W.

2005-04-01

We have performed microwave absorption and near-field reflection experiments on a high mobility GaAs/AlGaAs heterostructure for the same conditions for which Microwave-Induced Resistance Oscillations (MIROs) are observed. It is shown that the electrodynamic aspect of the problem is important in these experiments. In the absorption experiments a broad CR line was observed due to a large reflection from the highly conductive electron gas. There were no additional features observed related to absorption at harmonics of the cyclotron resonance. In near-field reflection experiments a very different oscillation pattern was revealed when compared to MIROs. The oscillation pattern observed in the reflection experiments is probably due to plasma effects occurring in a finite-size sample. The whole microscopic picture of MIROs is more complicated than simply a resonant absorption at harmonics of the cyclotron resonance. Nevertheless, the experimental observations are in good agreement with the model by Durst et al. involving the photo-assisted scattering in the presence of a crossed magnetic field and dc bias. The observed damping factor of MIROs may be attributed to a change in the electron mobility as a function of temperature. MIROs may be considered as a light-induced drift effect, a broad class of phenomena associated with a light-induced asymmetry in the velocity distribution function.

Absorption and Reflection Experiments on High-Mobility 2DEGs in the Regime of Microwave-Induced Resistance Oscillations

NASA Astrophysics Data System (ADS)

Studenikin, S. A.; Potemski, M.; Sachrajda, A. S.; Hilke, M.; Pfeiffer, L. N.; West, K. W.

We have performed microwave absorption and near-field reflection experiments on a high mobility GaAs/AlGaAs heterostructure for the same conditions for which Microwave-Induced Resistance Oscillations (MIROs) are observed. It is shown that the electrodynamic aspect of the problem is important in these experiments. In the absorption experiments a broad CR line was observed due to a large reflection from the highly conductive electron gas. There were no additional features observed related to absorption at harmonics of the cyclotron resonance. In near-field reflection experiments a very different oscillation pattern was revealed when compared to MIROs. The oscillation pattern observed in the reflection experiments is probably due to plasma effects occurring in a finite-size sample. The whole microscopic picture of MIROs is more complicated than simply a resonant absorption at harmonics of the cyclotron resonance. Nevertheless, the experimental observations are in good agreement with the model by Durst et al. involving the photo-assisted scattering in the presence of a crossed magnetic field and dc bias. The observed damping factor of MIROs may be attributed to a change in the electron mobility as a function of temperature. MIROs may be considered as a light-induced drift effect, a broad class of phenomena associated with a light-induced asymmetry in the velocity distribution function.

Time-dependent low field microwave absorption in the high temperature superconductors

NASA Astrophysics Data System (ADS)

Owens, F. J.; Iqbal, Z.

1990-11-01

It is observed that the hysteresis in the applied magnetic field position and the intensity at the peak of the low field non-resonant microwave absorption (recorded in an EPR experiment with a modulation amplitude of ∼ 10 G) in the superconducting state of the cuprate superconductors, is time-dependent after the removal of a DC magnetic field sizably greater than the lower critical field. This intrinsic time-dependence, which we attribute to flux creep, is reported here for two copper oxide-based high temperature superconductors.

ESR and nonresonant microwave absorption of ErBa2Cu3O(7-delta) and HoBa2Cu3O(7-delta) single crystals

NASA Astrophysics Data System (ADS)

Tagaya, Kimihito; Fukuoka, Nobuo; Nakanishi, Shigemitsu

1990-12-01

ESR measurements were performed for ErBa2Cu3O(7-delta) and HoBa2Cu3O(7-delta) single crystals from 77 K to room temperature. The ESR signals of Er2BaCuO5 and Ho2BaCuO5 were observed, and their temperature variations were investigated. Nonresonant microwave absorption was also observed below the superconducting critical temperature of 93 K. The principal values of lower critical field were determined.

FDTD chiral brain tissue model for specific absorption rate determination under radiation from mobile phones at 900 and 1800 MHz

NASA Astrophysics Data System (ADS)

Zamorano, M.; Torres-Silva, H.

2006-04-01

A new electrodynamics model formed by chiral bioplasma, which represents the human head inner structure and makes it possible to analyse its behaviour when it is irradiated by a microwave electromagnetic field from cellular phones, is presented. The finite-difference time-domain (FDTD) numeric technique is used, which allows simulation of the electromagnetic fields, deduced with Maxwell's equations, and allows us to simulate the specific absorption rate (SAR). The results show the SAR behaviour as a function of the input power and the chirality factor. In considering the chiral brain tissue in the proposed human head model, the two more important conclusions of our work are the following: (a) the absorption of the electromagnetic fields from cellular phones is stronger, so the SAR coefficient is higher than that using the classical model, when values of the chiral factor are of order of 1; (b) 'inverse skin effect' shows up at 1800 MHz, with respect to a 900 MHz source.

Study on the characteristics of magneto-sensitive electromagnetic wave-absorbing properties of magnetorheological elastomers

NASA Astrophysics Data System (ADS)

Yu, Miao; Yang, Pingan; Fu, Jie; Liu, Shuzhi; Qi, Song

2016-08-01

Magnetorheological (MR) materials are a class of materials whose mechanical and electrical properties can be reversible controlled by the magnetic field. In this study, we pioneered research on the effect of a uniform magnetic field with different strengths and directions on the microwave-absorbing properties of magnetorheological elastomers (MREs), in which the ferromagnetic particles are flower-like carbonyl iron powders (CIPs) prepared by an in situ reduction method. The electromagnetic (EM) absorbing properties of the composites have been analyzed by vector network analysis with the coaxial reflection/transmission technique. Under the magnetic field, the columnar or chainlike structures were formed, which allows EM waves to penetrate. Meanwhile, stronger Debye dipolar relaxation and attenuation constant have been obtained when changing the direction of the applied magnetic field. Compared with untreated MREs, not only have the minimum reflection loss (RL) and the effective absorption bandwidth (below -20 dB) greatly increased, the frequencies of the absorbing peaks shift about 15%. This suggests that MREs are a magnetic-field-sensitive electromagnetic wave-absorbing material and have great potential in applications such as in anti-radar camouflage, due to the fact that radar can continuously conduct detection at many electromagnetic frequencies, while the MR materials can adjust the microwave-absorption peak according to the radar frequency.

Magnetic field effects on microwave absorbing materials

NASA Technical Reports Server (NTRS)

Goldberg, Ira; Hollingsworth, Charles S.; Mckinney, Ted M.

1991-01-01

The objective of this program was to gather information to formulate a microwave absorber that can work in the presence of strong constant direct current (DC) magnetic fields. The program was conducted in four steps. The first step was to investigate the electrical and magnetic properties of magnetic and ferrite microwave absorbers in the presence of strong magnetic fields. This included both experimental measurements and a literature survey of properties that may be applicable to finding an appropriate absorbing material. The second step was to identify those material properties that will produce desirable absorptive properties in the presence of intense magnetic fields and determine the range of magnetic field in which the absorbers remain effective. The third step was to establish ferrite absorber designs that will produce low reflection and adequate absorption in the presence of intense inhomogeneous static magnetic fields. The fourth and final step was to prepare and test samples of such magnetic microwave absorbers if such designs seem practical.

Characterization of M-type barium hexagonal ferrite-based wide band microwave absorber

NASA Astrophysics Data System (ADS)

Meshram, M. R.; Agrawal, Nawal K.; Sinha, Bharoti; Misra, P. S.

2004-05-01

This paper present the design, development and characterization of the hexagonal ferrite powder [BaCo 0.5δTi 0.5δMn 0.1Fe (11.87-δ)O 19] and [Ba(MnTi) δFe (12-2δ)O 19] at δ=1.6 as a microwave absorber. The hexagonal ferrite powder has been developed by dry attrition and sintering procedure. The developed ferrite powder 60% by weight has been mixed in epoxy resin to form a microwave-absorbing paint. This paint was coated on a conducting aluminum sheet to study the absorption characteristics of a linearly polarized TE wave at X band. The results for single- and two-layer microwave absorbers for different coating thicknesses have been reported. It has been found that it shows the broadband characteristics with minimum absorption of 8 dB from 8 to 12 GHz for a coating thickness of 2 mm.These paints are very useful in military applications such as RCS reduction, camouflaging of the target and prevention of EMI, etc.

Observation of ultrahigh-energy electrons by resonance absorption of high-power microwaves in a pulsed plasma.

PubMed

Rajyaguru, C; Fuji, T; Ito, H; Yugami, N; Nishida, Y

2001-07-01

The interaction of high power microwave with collisionless unmagnetized plasma is studied. Investigation on the generation of superthermal electrons near the critical layer, by the resonance absorption phenomenon, is extended to very high microwave power levels (eta=E(2)(0)/4 pi n(e)kT(e) approximately 0.3). Here E0, n(e), and T(e) are the vacuum electric field, electron density, and electron temperature, respectively. Successive generation of electron bunches having maximum energy of about 2 keV, due to nonlinear wave breaking, is observed. The electron energy epsilon scales as a function of the incident microwave power P, according to epsilon proportional to P0.5 up to 250 kW. The two-dimensional spatial distribution of high energy electrons reveals that they are generated near the critical layer. However, the lower energy component is again produced in the subcritical density region indicating the possibility of other electron heating mechanisms.

EPR and ENDOR Studies of Point Defects in Lithium Tetraborate Crystals

DTIC Science & Technology

2012-12-14

the US and its allies. Terrorist groups have shown interest in seeking and deploying weapons of mass destruction and mass disruption--weapons that...5]. Lithium tetraborate, has been grown pure and doped with many different elements including transition metals, actinides , and rare earth...microwave cavity is said to be “ critically coupled” when there is no reflected microwave power. Absorption of microwaves, which occurs when the magnetic

Embedded dielectric water "atom" array for broadband microwave absorber based on Mie resonance

NASA Astrophysics Data System (ADS)

Gogoi, Dhruba Jyoti; Bhattacharyya, Nidhi Saxena

2017-11-01

A wide band microwave absorber at X-band frequency range is demonstrated numerically and experimentally by embedding a simple rectangular structured dielectric water "atom" in flexible silicone substrate. The absorption peak of the absorber is tuned by manipulating the size of the dielectric water "atom." The frequency dispersive permittivity property of the water "atom" shows broadband absorption covering the entire X-band above 90% efficiency with varying the size of the water "atom." Mie resonance of the proposed absorber provides the desired impedance matching condition at the air-absorber interface across a wide frequency range in terms of electric and magnetic resonances. Multipole decomposition of induced current densities is used to identify the nature of observed resonances. Numerical absorptivity verifies that the designed absorber is polarization insensitive for normal incidence and can maintain an absorption bandwidth of more than 2 GHz in a wide-angle incidence. Additionally, the tunability of absorption property with temperature is shown experimentally.

In-orbit verification of MHS spectral channels co-registration using the moon

NASA Astrophysics Data System (ADS)

Bonsignori, Roberto

2017-09-01

In-orbit verification of the co-registration of channels in a scanning microwave or infrared radiometer can in principle be done during normal in-orbit operation, by using the regular events of lunar intrusion in the instrument cold space calibration view. A technique of data analysis based on best fit of data across lunar intrusions has been used to check the mutual alignment of the spectral channels of the MHS instrument. MHS (Microwave Humidity Sounder) is a cross-track scanning radiometer in the millimetre-wave range flying on EUMETSAT and NOAA polar satellites, used operationally for the retrieval of atmospheric parameters in numerical weather prediction and nowcasting. This technique does not require any special operation or manoeuvre and only relies on analysis of data from the nominal scanning operation. The co-alignment of sounding channels and window channels can be evaluated by this technique, which would not be possible by using earth landmarks, due to the absorption effect of the atmosphere. The analysis reported in this paper shows an achievable accuracy below 0.5 mrad against a beam width at 3dB and spatial sampling interval of about 20 mrad. In-orbit results for the MHS instrument on Metop-B are also compared with the pre-launch instrument characterisation, showing a good correlation.

Water-injected all-dielectric ultra-wideband and prominent oblique incidence metamaterial absorber in microwave regime

NASA Astrophysics Data System (ADS)

Huang, Xiaojun; Yang, Helin; Shen, Zhaoyang; Chen, Jiao; Lin, Hail; Yu, Zetai

2017-09-01

We present a water-injected all-dielectric metamaterial that can offer an extremely wide bandwidth of electromagnetic absorption and prominent wide incident angle range. Different from conventional metal-dielectric based metamaterial absorbers, the absorption mechanism of the proposed all-dielectric metamaterial absorber is to take advantage of the dispersion of water, rather than electric or/and magnetic resonance, which thoroughly overcomes the defects of narrow bandwidth and oblique incidence from metal-dielectric based metamaterial absorber. The simulated absorption was over 90% in 8.1-22.9 GHz with the relative bandwidth of 95.5% when the incident angle reaches 60°, and the corresponding microwave experiment is performed to support the simulations. The obtained excellent absorption performance reveals a possible application of the proposed absorber, which can be exploited for electromagnetic stealth purposes, especially for electromagnetic stealth of sea targets.

Review of Microwave Photonics Technique to Generate the Microwave Signal by Using Photonics Technology

NASA Astrophysics Data System (ADS)

Raghuwanshi, Sanjeev Kumar; Srivastav, Akash

2017-12-01

Microwave photonics system provides high bandwidth capabilities of fiber optic systems and also contains the ability to provide interconnect transmission properties, which are virtually independent of length. The low-loss wide bandwidth capability of optoelectronic systems makes them attractive for the transmission and processing of microwave signals, while the development of high-capacity optical communication systems has required the use of microwave techniques in optical transmitters and receivers. These two strands have led to the development of the research area of microwave photonics. So, we can considered microwave photonics as the field that studies the interaction between microwave and optical waves for applications such as communications, radars, sensors and instrumentations. In this paper we have thoroughly reviewed the microwave generation techniques by using photonics technology.

[Application of microwave irradiation technology to the field of pharmaceutics].

PubMed

Zhang, Xue-Bing; Shi, Nian-Qiu; Yang, Zhi-Qiang; Wang, Xing-Lin

2014-03-01

Microwaves can be directly transformed into heat inside materials because of their ability of penetrating into any substance. The degree that materials are heated depends on their dielectric properties. Materials with high dielectric loss are more easily to reach a resonant state by microwaves field, then microwaves can be absorbed efficiently. Microwave irradiation technique with the unique heating mechanisms could induce drug-polymer interaction and change the properties of dissolution. Many benefits such as improving product quality, increasing energy efficiency and reducing times can be obtained by microwaves. This paper summarized characteristics of the microwave irradiation technique, new preparation techniques and formulation process in pharmaceutical industry by microwave irradiation technology. The microwave technology provides a new clue for heating and drying in the field of pharmaceutics.

Probing dynamics of micro-magnets with multi-mode superconducting resonator

NASA Astrophysics Data System (ADS)

Golovchanskiy, I. A.; Abramov, N. N.; Stolyarov, V. S.; Shchetinin, I. V.; Dzhumaev, P. S.; Averkin, A. S.; Kozlov, S. N.; Golubov, A. A.; Ryazanov, V. V.; Ustinov, A. V.

2018-05-01

In this work, we propose and explore a sensitive technique for investigation of ferromagnetic resonance and corresponding magnetic properties of individual micro-scaled and/or weak ferromagnetic samples. The technique is based on coupling the investigated sample to a high-Q transmission line superconducting resonator, where the response of the sample is studied at eigen frequencies of the resonator. The high quality factor of the resonator enables sensitive detection of weak absorption losses at multiple frequencies of the ferromagnetic resonance. Studying the microwave response of individual micro-scaled permalloy rectangles, we have confirmed the superiority of fluxometric demagnetizing factor over the commonly accepted magnetometric one and have depicted the demagnetization of the sample, as well as magnetostatic standing wave resonance.

Laboratory Measurement of the Temperature Dependence of Gaseous Sulfur Dioxide (SO2) Microwave Absorption with Application to the Venus Atmosphere

NASA Technical Reports Server (NTRS)

Suleiman, Shady H.; Kolodner, Marc A.; Steffes, Paul G.

1996-01-01

High-accuracy laboratory measurements of the temperature dependence of the opacity from gaseous sulfur dioxide (SO2) in a carbon dioxide (CO2) atmosphere at temperatures from 290 to 505 K and at pressures from 1 to 4 atm have been conducted at frequencies of 2.25 GHz (13.3 cm), 8.5 GHz (3.5 cm), and 21.7 GHz (1.4 cm). Based on these absorptivity measurements, a Ben-Reuven (BR) line shape model has been developed that provides a more accurate characterization of the microwave absorption of gaseous S02 in the Venus atmosphere as compared with other formalisms. The developed BR formalism is incorporated into a radiative transfer model. The resulting microwave emission spectrum of Venus is then used to set an upper limit on the disk-averaged abundance of gaseous S02 below the main cloud layer. It is found that gaseous S02 has an upper limit of 150 ppm, which compares well with previous spacecraft in situ measurements and Earth-based radio astronomical observations.

Ultra-thin Low-Frequency Broadband Microwave Absorber Based on Magnetic Medium and Metamaterial

NASA Astrophysics Data System (ADS)

Cheng, Yongzhi; He, Bo; Zhao, Jingcheng; Gong, Rongzhou

2017-02-01

An ultra-thin low-frequency broadband microwave absorber (MWA) based on a magnetic rubber plate (MRP) and cross-shaped structure (CSS) metamaterial (MM) was presented numerically and experimentally. The designed composite MWA is consisted of the MRP, CSS resonator, dielectric substrate and metallic background plane. The low-frequency absorption can be easily adjusted by tuning the geometric parameter of the CSS MM and the thickness of MPR. A bandwidth (i.e. the reflectance is below -10 dB) from 2.5 GHz to 5 GHz can be achieved with the total thickness of about 2 mm in experiments. The broadband absorption is attributed to the overlap of two resonant absorption peaks originated from MRP and CSS MM, respectively. More importantly, the thickness of the composite WMA is much thinner ( λ/40; λ is the operation center frequency), which could operate well at wide incidence angles for both transverse electric and transverse magnetic waves. Thus, it can be expected that our design will be applicable in the area of eliminating microwave energy and electromagnetic stealth.

Microwave thermal radiation effects on skin tissues

NASA Astrophysics Data System (ADS)

Yoon, Hargsoon; Song, Kyo D.; Lee, Uhn; Choi, Sang H.

2012-10-01

Microwave/RF energy has been used for wireless power transmission including many therapeutic applications, such as transurethral microwave therapy (TUMT). For safe uses of RF power, it is important to know how to deliver microwave energy on focused area and control the temperature changes not to drastically increase on adjacent areas. Graphical analysis of thermal loading factor is important to understand how to achieve effective transmission of microwave through the tissue. The loss mechanism while transmission often appears as thermal effects due to absorption of microwave, especially for materials such as human skin, muscles, and other organic parts including brain. In this paper, microwave thermal effects are investigated to measure temperatures, penetration depth through animal skins in terms of input power and various frequencies. This result will be compare with the case of human applications.

Catalysis by Single Atoms: Water Gas Shift and Ethylene Hydrogenation

DTIC Science & Technology

2009-04-20

addition to other microscopic phenomena at region of coefficients . Silicon carbide has a higher loss tangent at 2.4 GHz than most ceramics, and thus...Si 50 35 30 20 Ni 50 — — D. Sample holder and preparation: * The remainder is ZrB2. Graphite sheet ( McMaster -Carr, USA) is cut into different...results. 19 B. Microwave hybrid processing i. Microwave heating: 1. Volumetric Microwave absorption is proportional to the loss

Influence of multi-walled carbon nanotubes (MWCNTs) volume percentage on the magnetic and microwave absorbing properties of BaMg{sub 0.5}Co{sub 0.5}TiFe{sub 10}O{sub 19}/MWCNTs nanocomposites

DOE Office of Scientific and Technical Information (OSTI.GOV)

Alam, Reza Shams; Moradi, Mahmood, E-mail: moradi@susc.ac.ir; Institute of Nanotechnology, Shiraz University, Shiraz 71454

2016-01-15

Graphical abstract: Reflection losses of (a) doped barium hexaferrite, BaMg{sub 0.5}Co{sub 0.5}TiFe{sub 10}O{sub 19}, sample and their nanocomposites with (b) 4 vol. (c) 8 vol. and (d) 12 vol.% of MWCNTs are presented. - Highlights: • BaMg{sub 0.5}Co{sub 0.5}TiFe{sub 10}O{sub 19}/MWCNTs nanocomposites were synthesized. • The structural, magnetic and microwave absorption properties were investigated. • The microwave absorption is strongly influenced by volume percentage of MWCNTs. • The nanocomposite with 8 vol.% of MWCNTs can be proposed as a wideband absorber. - Abstract: In this study BaMg{sub 0.5}Co{sub 0.5}TiFe{sub 10}O{sub 19}/MWCNTs nanocomposites with different amount of MWCNTs (0, 4, 8more » and 12 vol.%) were synthesized. Here, the X-ray diffraction (XRD), Fourier transform spectroscopy (FTIR) and scanning electron microscopy (SEM) were used to demonstrate the structural and morphological characteristics of the prepared samples. XRD along with FTIR examinations exhibited that the nanocomposites were successfully synthesized. Vibrating sample magnetometer (VSM) showed the relatively strong dependence of saturation magnetization and coercivity on the volume percentage of MWCNTs. The microwave evaluation also confirmed that the complex permittivity of nanocomposites could be enhanced by adding MWCNTs. Finally, the nanocomposite with 8% vol. of MWCNTs exhibited the best microwave absorption performance among the samples.« less

In situ construction of g-C3N4/TiO2 heterojunction films with enhanced photocatalytic activity over magnetic-driven rotating frame

NASA Astrophysics Data System (ADS)

Pan, Chao; Jia, Jia; Hu, Xiaoyun; Fan, Jun; Liu, Enzhou

2018-02-01

Corn-shaped TiO2 nanofilms were fabricated by a glycerol-assisted hydrothermal method, and then g-C3N4 was deposited on the surface of TiO2 films using melamine as precursor under air atmosphere by an in site microwave-heating technique. The investigations indicate that microwave-heating process is a facile strategy to obtain g-C3N4 by thermal polymerization of melamine, which can achieve in situ constructing of g-C3N4/TiO2 heterojunction films with high stability. The as-prepared TiO2 films with crack and holes have visible light scattering capability, and the scattering light overlaps with the intrinsic absorption of g-C3N4, leading to an absorption plateau in the range of 400-550 nm. Besides, a magnetic-driven rotating frame was developed to enhance the mass transfer processes during the photocatalytic water splitting. The result shows that g-C3N4/TiO2 films exhibit excellent activities under simulated-sunlight irradiation, in addition to the enhanced mass transfer, the overlapped visible light absorption, stable contact and effective charge transfer between g-C3N4 and TiO2 can facilitate the hydrogen production and light utilization efficiency as well. The hydrogen production rate can reach 13.8 mmol h-1 m-2 over g-C3N4/TiO2 films prepared using 0.5 g of melamine and 16.0 cm2 of TiO2.

Microwave Atmospheric-Pressure Sensor

NASA Technical Reports Server (NTRS)

Flower, D. A.; Peckham, G. E.; Bradford, W. J.

1986-01-01

Report describes tests of microwave pressure sounder (MPS) for use in satellite measurements of atmospheric pressure. MPS is multifrequency radar operating between 25 and 80 GHz. Determines signal absorption over vertical path through atmosphere by measuring strength of echoes from ocean surface. MPS operates with cloud cover, and suitable for use on current meteorological satellites.

Graphene/Poly(aniline-co-pyrrole) Nanocomposite: Potential Candidate for Supercapacitor and Microwave Absorbing Applications.

PubMed

Sahoo, Sumanta; Bhattacharya, Pallab; Dhibar, Saptarshi; Hatui, Goutam; Das, Tanya; Das, Chapal Kumar

2015-09-01

A simple and cost-effective in-situ chemical route to prepare the nanocomposites based on graphene and Poly(aniline-co-pyrrole) [PPP] has been proposed. Introduction of graphene changes the morphology of copolymer from spherical to fiber like. Graphene/Poly(aniline-co-pyrrole) [GPPP] nanocomposite achieved highest specific capacitance of 351 F/g and energy density of 124.8 Wh/Kg at 10 mV/s scan rate. The composite also obtained moderate specific capacitance retention of 66% after 500 cycles, which establish its potentiality as supercapacitor electrode materials. The composite also exhibited high electrical conductivity and superior microwave absorbing properties (maximum reflection loss is -29.97 dB). The absorption range corresponding to ≥ 90% absorption (or -10 dB) is 2.72 GHz which is excellent for the microwave absorbing applications.

Behavioral effects of microwaves: relationship of total dose and dose rate

DOE Office of Scientific and Technical Information (OSTI.GOV)

O'Connor, M.E.; Strattan, R.

1988-10-01

The goal of the research was to compare the relationship of whole-body averaged specific absorption rate (SAR) and specific absorption (SA) to determine whether dose rate or dose was the better predictor of biological effects. Sperm-positive Long-Evans female rats were exposed to 2450-MHz CW microwave radiation for 1-3 hours at approximately 10 W/kg. The maternal subjects were then observed for natural delivery of their litters. Sensitivity to thermally induced seizures and huddling were studied in the offspring. Analyses revealed that there were no statistically significant differences between exposed and control offspring on the behavioral indices. The behavior did not appearmore » to be affected by prenatal exposure to microwave radiation at this level. The huddle sizes became smaller as the pups aged both in exposed and control offspring.« less

Microwave absorption performance of Ni(OH)2 decorating biomass carbon composites from Jackfruit peel

NASA Astrophysics Data System (ADS)

Guan, Hongtao; Wang, Huiya; Zhang, Yanlin; Dong, Chengjun; Chen, Gang; Wang, Yude; Xie, Jianbin

2018-07-01

The composite material of Ni(OH)2/biomass carbon have been prepared by a facile "carbonization-activation" procedure from Jackfruit peel and a subsequent water-bathing precipitation process. The biomass carbon material after activation (AC) is constituted of small particles and achieves a large specific surface area of 1602 m2/g. After decoration of Ni(OH)2 nanosheets, the Ni(OH)2/AC composites were investigated the microwave absorption performances in 2-18 GHz. The maximum reflection loss of the Ni(OH)2/AC composites reached -23.6 dB at 15.48 GHz with a thickness of 6 mm. Moreover, the fundamental mechanism based on conductivity, the polarization and defects is discussed. The present investigation offers a new possibility for the biomass based fabrication of potential microwave absorbing materials.

Unraveling the mysteries of microwave chemistry using silicon carbide reactor technology.

PubMed

Kappe, C Oliver

2013-07-16

In the past few years, the use of microwave energy to heat chemical reactions has become an increasingly popular theme in the scientific community. This nonclassical heating technique has slowly progressed from a laboratory curiosity to an established method commonly used both in academia and in industry. Because of its efficiency, microwave heating dramatically reduces reaction times (from days and hours to minutes and seconds) and improves product purities or material properties among other advantages. Since the early days of microwave chemistry, researchers have observed rate-accelerations and, in some cases, altered product distributions as compared with reactions carried out using classical oil-bath heating. As a result, researchers have speculated that so-called specific or nonthermal microwave effects could be responsible for these differences. Much of the debate has centered on the question of whether the electromagnetic field can exert a direct influence on a chemical transformation outside of the simple macroscopic change in bulk reaction temperature. In 2009, our group developed a relatively simple "trick" that allows us to rapidly evaluate whether an observed effect seen in a microwave-assisted reaction results from a purely thermal phenomenon, or involves specific or nonthermal microwave effects. We use a microwave reaction vessel made from silicon carbide (SiC) ceramic. Because of its high microwave absorptivity, the vessel shields its contents from the electromagnetic field. As a result, we can easily mimic a conventionally heated autoclave experiment inside a microwave reactor under carefully controlled reaction conditions. The switch from an almost microwave transparent glass (Pyrex) to a strongly microwave absorbing SiC reaction vial under otherwise identical reaction conditions (temperature profiles, pressure, stirring speed) then allows us to carefully evaluate the influence of the electromagnetic field on the particular chemical transformation. Over the past five years we have subjected a wide variety of chemical transformations, including organic reactions, preparations of inorganic nanoparticles, and the hydrolysis of proteins, to the "SiC test." In nearly all of the studied examples, we obtained identical results from reactions carried out in Pyrex vials and those carried out in SiC vials. The data obtained from these investigations confirm that in the overwhelming majority of cases a bulk temperature phenomenon drives the enhancements in microwave chemistry and that the electromagnetic field has no direct influence on the reaction pathway.

Mobile system for microwave removal of concrete surfaces

DOEpatents

White, Terry L.; Bigelow, Timothy S.; Schaich, Charles R.; Foster, Jr., Don

1997-01-01

A method and apparatus for the microwave removal of contaminated concrete surfaces. The apparatus comprises a housing adapted to pass over a support surface. The housing includes a waveguide for directing microwave energy to the surface at an angle maximizing absorption of microwave energy by the surface. The apparatus is further provided with a source of microwave energy operably associated with the waveguide, wherein the microwave energy has a frequency of between about 10.6 GHz and about 24 GHz and acts to remove the uppermost layer from the surface. The apparatus further includes a debris containment assembly comprising a vacuum assembly operably associated with the housing. The vacuum assembly is adapted to remove debris from the area adjacent the surface.

Mobile system for microwave removal of concrete surfaces

DOEpatents

White, T.L.; Bigelow, T.S.; Schaich, C.R.; Foster, D. Jr.

1997-06-03

A method and apparatus are disclosed for the microwave removal of contaminated concrete surfaces. The apparatus comprises a housing adapted to pass over a support surface. The housing includes a waveguide for directing microwave energy to the surface at an angle maximizing absorption of microwave energy by the surface. The apparatus is further provided with a source of microwave energy operably associated with the waveguide, wherein the microwave energy has a frequency of between about 10.6 GHz and about 24 GHz and acts to remove the uppermost layer from the surface. The apparatus further includes a debris containment assembly comprising a vacuum assembly operably associated with the housing. The vacuum assembly is adapted to remove debris from the area adjacent the surface. 7 figs.

Microwave Technique for Detecting and Locating Concealed Weapons

DOT National Transportation Integrated Search

1971-12-01

The subject of this report is the evaluation of a microwave technique for detecting and locating weapons concealed under clothing. The principal features of this technique are: persons subjected to search are not exposed to 'objectional' microwave ra...

Chemoselectivity-induced multiple interfaces in MWCNT/Fe3O4@ZnO heterotrimers for whole X-band microwave absorption.

PubMed

Wang, Zhijiang; Wu, Lina; Zhou, Jigang; Jiang, Zhaohua; Shen, Baozhong

2014-11-07

A chemoselective route to induce Fe3O4@ZnO core-shell nanoparticles decorating carbon nanotubes to form MWCNT/Fe3O4@ZnO heterotrimers has been developed. Charges are redistributed in the heterotrimers through C-O-Zn, C-O-Fe and Fe-O-Zn bondings, giving rise to multiple electronic phases. The generated significant interfacial polarization and synergetic interaction between dielectric and magnetic absorbers result in the MWCNT/Fe3O4@ZnO heterotrimers with high-performance microwave absorption in an entire X band.

VUV absorption spectroscopy measurements of the role of fast neutral atoms in a high-power gap breakdown

DOE Office of Scientific and Technical Information (OSTI.GOV)

Filuk, A. B.; Bailey, J. E.; Cuneo, M. E.

The maximum power achieved in a wide variety of high-power devices, including electron and ion diodes, z pinches, and microwave generators, is presently limited by anode-cathode gap breakdown. A frequently discussed hypothesis for this effect is ionization of fast neutral atoms injected throughout the anode-cathode gap during the power pulse. We describe a newly developed diagnostic tool that provides a direct test of this hypothesis. Time-resolved vacuum-ultraviolet absorption spectroscopy is used to directly probe fast neutral atoms with 1-mm spatial resolution in the 10-mm anode-cathode gap of the SABRE 5 MV, 1 TW applied-B ion diode. Absorption spectra collected duringmore » Ar RF glow discharges and with CO{sub 2} gas fills confirm the reliability of the diagnostic technique. Throughout the 50--100 ns ion diode pulses no measurable neutral absorption was seen, setting upper limits of (0.12--1.5)x10{sup 14}cm{sup -3} for ground-state fast neutral atom densities of H, C, N, O, and F. The absence of molecular absorption bands also sets upper limits of (0.16--1.2)x10{sup 15}cm{sup -3} for common simple molecules. These limits are low enough to rule out ionization of fast neutral atoms as a breakdown mechanism. Breakdown due to ionization of molecules is also found to be unlikely. This technique can now be applied to quantify the role of neutral atoms in other high-power devices.« less

Improving the Electromagnetic Wave Absorption Properties of the Layered MoS2 by Cladding with Ni Nanoparticles

NASA Astrophysics Data System (ADS)

Zhang, Zilong; Wang, Zilin; Heng, Liuyang; Wang, Shuai; Chen, Xiqiao; Fu, Xiquan; Zou, Yanhong; Tang, Zhixiang

2018-05-01

MoS2 is a promising material with microwave absorption performance due to its high dielectric properties and low density. However, pure MoS2 is non-magnetic and has a bad impedance matching characteristic. In this study we prepared the Ni/MoS2 nanocomposites by cladding the MoS2 micrometer slices with magnetic Ni nanoparticles. Our results show that the microwave absorption properties of Ni/MoS2 nanocomposites have been improved obviously compared with the pure MoS2. Because of the introduction of Ni particles, the permeability of the nanocomposites has been turned from one to a complex, indicating a newly added magnetic loss. Meanwhile, the big gap between the permittivity and permeability of the Ni/MoS2 nanocomposites has been properly narrowed, which suggests an improved impedance matching. Moreover, the dielectric Cole-Cole semicircle shows that there are more Debye relaxation processes for the Ni/MoS2 nanocomposites, which further enhances the dielectric loss. Due to its improved electromagnetic properties, the minimum reflection loss (RL) value of the Ni/MoS2 nanocomposites with 60 wt % loading reaches -55 dB and the absorption bandwidth (<-10 dB) is up to 4.0 GHz (10.8-14.8 GHz) with a matching thickness of 1.5 mm. The results provide an excellent candidate for microwave absorbing materials with a broad effective absorption bandwidth at thin thicknesses.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Takahashi, Masayuki, E-mail: m.takahashi@al.t.u-tokyo.ac.jp; Ohnishi, Naofumi

A filamentary plasma is reproduced based on a fully kinetic model of electron and ion transports coupled with electromagnetic wave propagation. The discharge plasma transits from discrete to diffusive patterns at a 110-GHz breakdown, with decrease in the ambient pressure, because of the rapid electron diffusion that occurs during an increase in the propagation speed of the ionization front. A discrete plasma is obtained at low pressures when a low-frequency microwave is irradiated because the ionization process becomes more dominant than the electron diffusion, when the electrons are effectively heated by the low-frequency microwave. The propagation speed of the plasmamore » increases with decrease in the incident microwave frequency because of the higher ionization frequency and faster plasma diffusion resulting from the increase in the energy-absorption rate. An external magnetic field is applied to the breakdown volume, which induces plasma filamentation at lower pressures because the electron diffusion is suppressed by the magnetic field. The thrust performance of a microwave rocket is improved by the magnetic fields corresponding to the electron cyclotron resonance (ECR) and its higher-harmonic heating, because slower propagation of the ionization front and larger energy-absorption rates are obtained at lower pressures. It would be advantageous if the fundamental mode of ECR heating is coupled with a lower frequency microwave instead of combining the higher-harmonic ECR heating with the higher frequency microwave. This can improve the thrust performance with smaller magnetic fields even if the propagation speed increases because of the decrease in the incident microwave frequency.« less

High power water load for microwave and millimeter-wave radio frequency sources

DOEpatents

Ives, R. Lawrence; Mizuhara, Yosuke M.; Schumacher, Richard V.; Pendleton, Rand P.

1999-01-01

A high power water load for microwave and millimeter wave radio frequency sources has a front wall including an input port for the application of RF power, a cylindrical dissipation cavity lined with a dissipating material having a thickness which varies with depth, and a rear wall including a rotating reflector for the reflection of wave energy inside the cylindrical cavity. The dissipation cavity includes a water jacket for removal of heat generated by the absorptive material coating the dissipation cavity, and this absorptive material has a thickness which is greater near the front wall than near the rear wall. Waves entering the cavity reflect from the rotating reflector, impinging and reflecting multiple times on the absorptive coating of the dissipation cavity, dissipating equal amounts of power on each internal reflection.

On-chip dual-comb source for spectroscopy

PubMed Central

Dutt, Avik; Joshi, Chaitanya; Ji, Xingchen; Cardenas, Jaime; Okawachi, Yoshitomo; Luke, Kevin; Gaeta, Alexander L.; Lipson, Michal

2018-01-01

Dual-comb spectroscopy is a powerful technique for real-time, broadband optical sampling of molecular spectra, which requires no moving components. Recent developments with microresonator-based platforms have enabled frequency combs at the chip scale. However, the need to precisely match the resonance wavelengths of distinct high quality-factor microcavities has hindered the development of on-chip dual combs. We report the simultaneous generation of two microresonator combs on the same chip from a single laser, drastically reducing experimental complexity. We demonstrate broadband optical spectra spanning 51 THz and low-noise operation of both combs by deterministically tuning into soliton mode-locked states using integrated microheaters, resulting in narrow (<10 kHz) microwave beat notes. We further use one comb as a reference to probe the formation dynamics of the other comb, thus introducing a technique to investigate comb evolution without auxiliary lasers or microwave oscillators. We demonstrate high signal-to-noise ratio absorption spectroscopy spanning 170 nm using the dual-comb source over a 20-μs acquisition time. Our device paves the way for compact and robust spectrometers at nanosecond time scales enabled by large beat-note spacings (>1 GHz). PMID:29511733

Shell thickness-dependent microwave absorption of core-shell Fe3O4@C composites.

PubMed

Du, Yunchen; Liu, Wenwen; Qiang, Rong; Wang, Ying; Han, Xijiang; Ma, Jun; Xu, Ping

2014-08-13

Core-shell composites, Fe3O4@C, with 500 nm Fe3O4 microspheres as cores have been successfully prepared through in situ polymerization of phenolic resin on the Fe3O4 surface and subsequent high-temperature carbonization. The thickness of carbon shell, from 20 to 70 nm, can be well controlled by modulating the weight ratio of resorcinol and Fe3O4 microspheres. Carbothermic reduction has not been triggered at present conditions, thus the crystalline phase and magnetic property of Fe3O4 micropsheres can be well preserved during the carbonization process. Although carbon shells display amorphous nature, Raman spectra reveal that the presence of Fe3O4 micropsheres can promote their graphitization degree to a certain extent. Coating Fe3O4 microspheres with carbon shells will not only increase the complex permittivity but also improve characteristic impedance, leading to multiple relaxation processes in these composites, thus the microwave absorption properties of these composites are greatly enhanced. Very interestingly, a critical thickness of carbon shells leads to an unusual dielectric behavior of the core-shell structure, which endows these composites with strong reflection loss, especially in the high frequency range. By considering good chemical homogeneity and microwave absorption, we believe the as-fabricated Fe3O4@C composites can be promising candidates as highly effective microwave absorbers.

A passive and active microwave-vector radiative transfer (PAM-VRT) model

NASA Astrophysics Data System (ADS)

Yang, Jun; Min, Qilong

2015-11-01

A passive and active microwave vector radiative transfer (PAM-VRT) package has been developed. This fast and accurate forward microwave model, with flexible and versatile input and output components, self-consistently and realistically simulates measurements/radiation of passive and active microwave sensors. The core PAM-VRT, microwave radiative transfer model, consists of five modules: gas absorption (two line-by-line databases and four fast models); hydrometeor property of water droplets and ice (spherical and nonspherical) particles; surface emissivity (from Community Radiative Transfer Model (CRTM)); vector radiative transfer of successive order of scattering (VSOS); and passive and active microwave simulation. The PAM-VRT package has been validated against other existing models, demonstrating good accuracy. The PAM-VRT not only can be used to simulate or assimilate measurements of existing microwave sensors, but also can be used to simulate observation results at some new microwave sensors.

Continuous microwave regeneration apparatus for absorption media

DOEpatents

Smith, Douglas D.

1999-01-01

A method and apparatus for continuously drying and regenerating ceramic beads for use in process gas moisture drying operations such as glove boxes. A microwave energy source is coupled to a process chamber to internally heat the ceramic beads and vaporize moisture contained therein. In a preferred embodiment, the moisture laden ceramic beads are conveyed toward the microwave source by a screw mechanism. The regenerated beads flow down outside of the screw mechanism and are available to absorb additional moisture.

Microwave Magnetochiral Dichroism in the Chiral-Lattice Magnet Cu2OSeO3

NASA Astrophysics Data System (ADS)

Okamura, Y.; Kagawa, F.; Seki, S.; Kubota, M.; Kawasaki, M.; Tokura, Y.

2015-05-01

Through broadband microwave spectroscopy in Faraday geometry, we observe distinct absorption spectra accompanying magnetoelectric (ME) resonance for oppositely propagating microwaves, i.e., directional dichroism, in the multiferroic chiral-lattice magnet Cu2OSeO3. The magnitude of the directional dichroism critically depends on the magnetic-field direction. Such behavior is well accounted for by considering the relative direction of the oscillating electric polarizations induced via the ME effect with respect to microwave electric fields. Directional dichroism in a system with an arbitrary form of ME coupling can be also discussed in the same manner.

Optically transparent microwave screens based on engineered graphene layers.

PubMed

Grande, M; Bianco, G V; Vincenti, M A; de Ceglia, D; Capezzuto, P; Petruzzelli, V; Scalora, M; Bruno, G; D'Orazio, A

2016-10-03

We propose an innovative approach for the realization of a microwave absorber fully transparent in the optical regime. This device is based on the Salisbury screen configuration, which consists of a lossless spacer, sandwiched between two graphene sheets whose sheet resistances are different and properly engineered. Experimental results show that it is possible to achieve near-perfect electromagnetic absorption in the microwave X-band. These findings are fully supported by an analytical approach based on an equivalent circuital model. Engineering and integration of graphene sheets could facilitate the realization of innovative microwave absorbers with additional electromagnetic and optical functionalities that could circumvent some of the major limitations of opaque microwave absorbers.

Headspace single drop microextraction coupled with microwave extraction of essential oil from plant materials.

PubMed

Zhai, Yujuan; Sun, Shuo; Wang, Ziming; Zhang, Yupu; Liu, He; Sun, Ye; Zhang, Hanqi; Yu, Aimin

2011-05-01

Headspace single drop microextraction (HS-SDME) coupled with microwave extraction (ME) was developed and applied to the extraction of the essential oil from dried Syzygium aromaticum (L.) Merr. et Perry and Cuminum cyminum L. The operational parameters, such as microdrop volume, microwave absorption medium (MAM), extraction time, and microwave power were optimized. Ten microliters of decane was used as the microextraction solvent. Ionic liquid and carbonyl iron powder were used as MAM. The extraction time was less than 7 min at the microwave power of 440 W. The proposed method was compared with hydrodistillation (HD). There were no obvious differences in the constituents of essential oils obtained by the two methods.

Exchange coupling and microwave absorption in core/shell-structured hard/soft ferrite-based CoFe2O4/NiFe2O4 nanocapsules

NASA Astrophysics Data System (ADS)

Feng, Chao; Liu, Xianguo; Or, Siu Wing; Ho, S. L.

2017-05-01

Core/shell-structured, hard/soft spinel-ferrite-based CoFe2O4/NiFe2O4 (CFO/NFO) nanocapsules with an average diameter of 17 nm are synthesized by a facile two-step hydrothermal process using CFO cores of ˜15 nm diameter as the hard magnetic phase and NFO shells of ˜1 nm thickness as the soft magnetic phase. The single-phase-like hysteresis loop with a high remnant-to-saturation magnetization ratio of 0.7, together with a small grain size of ˜16 nm, confirms the existence of exchange-coupling interaction between the CFO cores and the NFO shells. The effect of hard/soft exchange coupling on the microwave absorption properties is studied. Comparing to CFO and NFO nanoparticles, the finite-size NFO shells and the core/shell structure enable a significant reduction in electric resistivity and an enhancement in dipole and interfacial polarizations in the CFO/NFO nanocapsules, resulting in an obvious increase in dielectric permittivity and loss in the whole S-Ku bands of microwaves of 2-18 GHz, respectively. The exchange-coupling interaction empowers a more favorable response of magnetic moment to microwaves, leading to enhanced exchange resonances in magnetic permeability and loss above 10 GHz. As a result, strong absorption, as characterized by a large reflection loss (RL) of -20.1 dB at 9.7 GHz for an absorber thickness of 4.5 mm as well as a broad effective absorption bandwidth (for RL<-10 dB) of 8.4 GHz (7.8-16.2 GHz) at an absorber thickness range of 3.0-4.5 mm, is obtained.

Laboratory Evaluation and Application of Microwave Absorption Properties Under Simulated Conditions for Planetary Atmospheres

NASA Technical Reports Server (NTRS)

Steffes, Paul G.

1998-01-01

Radio absorptivity data for planetary atmospheres obtained from spacecraft radio occultation experiments, entry probe radio signal absorption measurements, and earth-based radio astronomical observations can be used to infer abundances of microwave absorbing constituents in those atmospheres, as long as reliable information regarding the microwave absorbing properties of potential constituents is available. The use of theoretically-derived microwave absorption properties for such atmospheric constituents, or using laboratory measurements of such properties taken under environmental conditions which are significantly different than those of the planetary atmosphere being studied, often leads to significant misinterpretation of available opacity data. For example, laboratory measurements completed recently by Kolodner and Steffes (ICARUS 132, pp. 151-169, March 1998, attached as Appendix A) under this grant (NAGS-4190), have shown that the opacity from gaseous H2SO4 under simulated Venus conditions is best described by a different formalism than was previously used. The recognition of the need to make such laboratory measurements of simulated planetary atmospheres over a range of temperatures and pressures which correspond to the altitudes probed by both spacecraft entry probe and orbiter radio occultation experiments and by radio astronomical observations, and over a range of frequencies which correspond to those used in such experiments, has led to the development of a facility at Georgia Tech which is capable of making such measurements. It has been the goal of this investigation to conduct such measurements and to apply the results to a wide range of planetary observations, both spacecraft and earth-based, in order to determine the identity and abundance profiles of constituents in those planetary atmospheres.

Formaldehyde monitor for automobile exhausts

NASA Technical Reports Server (NTRS)

Easley, W. C.

1973-01-01

Device makes use of microwave spectral absorption in low-Q resonant Stark cell, and indications are that ultimate sensitivity of instrument is within 100 parts per billion of formaldehyde. Microwave source is very small and requires only six-volt dc bias for operation. Coarse tuning is accomplished mechanically and fine tuning by adjusting dc-bias voltage.

Uniform Fe3O4 coating on flower-like ZnO nanostructures by atomic layer deposition for electromagnetic wave absorption.

PubMed

Wan, Gengping; Wang, Guizhen; Huang, Xianqin; Zhao, Haonan; Li, Xinyue; Wang, Kan; Yu, Lei; Peng, Xiange; Qin, Yong

2015-11-21

An elegant atomic layer deposition (ALD) method has been employed for controllable preparation of a uniform Fe3O4-coated ZnO (ZnO@Fe3O4) core-shell flower-like nanostructure. The Fe3O4 coating thickness of the ZnO@Fe3O4 nanostructure can be tuned by varying the cycle number of ALD Fe2O3. When serving as additives for microwave absorption, the ZnO@Fe3O4-paraffin composites exhibit a higher absorption capacity than the ZnO-paraffin composites. For ZnO@500-Fe3O4, the effective absorption bandwidth below -10 dB can reach 5.2 GHz and the RL values below -20 dB also cover a wide frequency range of 11.6-14.2 GHz when the coating thickness is 2.3 mm, suggesting its potential application in the treatment of the electromagnetic pollution problem. On the basis of experimental observations, a mechanism has been proposed to understand the enhanced microwave absorption properties of the ZnO@Fe3O4 composites.

Dataset used to improve liquid water absorption models in the microwave

DOE Data Explorer

Turner, David

2015-12-14

Two datasets, one a compilation of laboratory data and one a compilation from three field sites, are provided here. These datasets provide measurements of the real and imaginary refractive indices and absorption as a function of cloud temperature. These datasets were used in the development of the new liquid water absorption model that was published in Turner et al. 2015.

Determination of gold and cobalt dopants in advanced materials based on tin oxide by slurry sampling high-resolution continuum source graphite furnace atomic absorption spectrometry

NASA Astrophysics Data System (ADS)

Filatova, Daria G.; Eskina, Vasilina V.; Baranovskaya, Vasilisa B.; Vladimirova, Svetlana A.; Gaskov, Alexander M.; Rumyantseva, Marina N.; Karpov, Yuri A.

2018-02-01

A novel approach is developed for the determination of Co and Au dopants in advanced materials based on tin oxide using high-resolution continuum source graphite furnace atomic absorption spectrometry (HR CS GFAAS) with direct slurry sampling. Sodium carboxylmethylcellulose (Na-CMC) is an effective stabilizer for diluted suspensions. Use Na-CMC allows to transfer the analytes into graphite furnace completely and reproducibly. The relative standard deviation obtained by HR CS GFAAS was not higher than 4%. Accuracy was proven by means inductively coupled plasma mass spectrometry (ICP-MS) in solutions after decomposition as a comparative technique. To determine Au and Co in the volume of SnO2, the acid decomposition conditions (HCl, HF) of the samples were suggested by means of an autoclave in a microwave oven.

A feasibility study of a microwave water vapor measurement from a space probe along an occultation path

NASA Technical Reports Server (NTRS)

Longbothum, R. L.

1975-01-01

Stratospheric and mesospheric water vapor measurements were taken using the microwave lines at 22 GHz (22.235 GHz) and 183 GHz (183.31 GHz). The resonant cross sections for both the 22 GHz and the 183 GHz lines were used to model the optical depth of atmospheric water vapor. The range of optical depths seen by a microwave radiometer through the earth's limb was determined from radiative transfer theory. Radiometer sensitivity, derived from signal theory, was compared with calculated optical depths to determine the maximum height to which water vapor can be measured using the following methods: passive emission, passive absorption, and active absorption. It was concluded that measurements using the 22 GHz line are limited to about 50 km whereas the 183 GHz line enables measurements up to and above 100 km for water vapor mixing ratios as low as 0.1 ppm under optimum conditions.

Enhanced microwave absorption properties of Fe3O4-modified flaky FeSiAl

NASA Astrophysics Data System (ADS)

He, Jun; Deng, Lianwen; Liu, Sheng; Yan, Shuoqing; Luo, Heng; Li, Yuhan; He, Longhui; Huang, Shengxiang

2017-12-01

The magnetic insulator Fe3O4-modified flaky Fe85Si9.5Al5.5 (FeSiAl) powders with significantly enhanced electromagnetic wave absorption properties in the frequency range of 2-8 GHz were prepared by chemical co-precipitation. X-ray diffraction (XRD) and scanning electron microscopy (SEM) have confirmed the formation of nanoparticles Fe3O4 precipitated on the flake-shaped FeSiAl. The electromagnetic measurements of the modified flakes presents a nearly invariable complex permeability and decreased complex permittivity in the 2-8 GHz, as well as improved impedance matching performance. More importantly, an excellent microwave absorbing performance with the bandwidth (RL <-10 dB) of 5.36 GHz is achieved in modified sample with the thickness of 1.5 mm, which is a promising microwave absorbing material in 2-8 GHz.

Intercomparison of atmospheric water vapour measurements at a Canadian High Arctic site

NASA Astrophysics Data System (ADS)

Weaver, Dan; Strong, Kimberly; Schneider, Matthias; Rowe, Penny M.; Sioris, Chris; Walker, Kaley A.; Mariani, Zen; Uttal, Taneil; McElroy, C. Thomas; Vömel, Holger; Spassiani, Alessio; Drummond, James R.

2017-08-01

Water vapour is a critical component of the Earth system. Techniques to acquire and improve measurements of atmospheric water vapour and its isotopes are under active development. This work presents a detailed intercomparison of water vapour total column measurements taken between 2006 and 2014 at a Canadian High Arctic research site (Eureka, Nunavut). Instruments include radiosondes, sun photometers, a microwave radiometer, and emission and solar absorption Fourier transform infrared (FTIR) spectrometers. Close agreement is observed between all combination of datasets, with mean differences ≤ 1.0 kg m-2 and correlation coefficients ≥ 0.98. The one exception in the observed high correlation is the comparison between the microwave radiometer and a radiosonde product, which had a correlation coefficient of 0.92.A variety of biases affecting Eureka instruments are revealed and discussed. A subset of Eureka radiosonde measurements was processed by the Global Climate Observing System (GCOS) Reference Upper Air Network (GRUAN) for this study. Comparisons reveal a small dry bias in the standard radiosonde measurement water vapour total columns of approximately 4 %. A recently produced solar absorption FTIR spectrometer dataset resulting from the MUSICA (MUlti-platform remote Sensing of Isotopologues for investigating the Cycle of Atmospheric water) retrieval technique is shown to offer accurate measurements of water vapour total columns (e.g. average agreement within -5.2 % of GRUAN and -6.5 % of a co-located emission FTIR spectrometer). However, comparisons show a small wet bias of approximately 6 % at the high-latitude Eureka site. In addition, a new dataset derived from Atmospheric Emitted Radiance Interferometer (AERI) measurements is shown to provide accurate water vapour measurements (e.g. average agreement was within 4 % of GRUAN), which usefully enables measurements to be taken during day and night (especially valuable during polar night).

Electromagnetic-radiation absorption by water

NASA Astrophysics Data System (ADS)

Lunkenheimer, P.; Emmert, S.; Gulich, R.; Köhler, M.; Wolf, M.; Schwab, M.; Loidl, A.

2017-12-01

Why does a microwave oven work? How does biological tissue absorb electromagnetic radiation? Astonishingly, we do not have a definite answer to these simple questions because the microscopic processes governing the absorption of electromagnetic waves by water are largely unclarified. This absorption can be quantified by dielectric loss spectra, which reveal a huge peak at a frequency of the exciting electric field of about 20 GHz and a gradual tailing off toward higher frequencies. The microscopic interpretation of such spectra is highly controversial and various superpositions of relaxation and resonance processes ascribed to single-molecule or molecule-cluster motions have been proposed for their analysis. By combining dielectric, microwave, THz, and far-infrared spectroscopy, here we provide nearly continuous temperature-dependent broadband spectra of water. Moreover, we find that corresponding spectra for aqueous solutions reveal the same features as pure water. However, in contrast to the latter, crystallization in these solutions can be avoided by supercooling. As different spectral contributions tend to disentangle at low temperatures, this enables us to deconvolute them when approaching the glass transition under cooling. We find that the overall spectral development, including the 20 GHz feature (employed for microwave heating), closely resembles the behavior known for common supercooled liquids. Thus water's absorption of electromagnetic waves at room temperature is not unusual but very similar to that of glass-forming liquids at elevated temperatures, deep in the low-viscosity liquid regime, and should be interpreted along similar lines.

Two-gigawatt burst-mode operation of the intense microwave prototype (IMP) free-electron laser (FEL) for the microwave tokamak experiment (MTX)

DOE Office of Scientific and Technical Information (OSTI.GOV)

Felker, B.; Allen, S.; Bell, H.

1993-10-06

The MTX explored the plasma heating effects of 140 GHz microwaves from both Gyrotrons and from the IMP FEL wiggler. The Gyrotron was long pulse length (0.5 seconds maximum) and the FEL produced short-pulse length, high-peak power, single and burst modes of 140 GHZ microwaves. Full-power operations of the IMP FEL wiggler were commenced in April of 1992 and continued into October of 1992. The Experimental Test Accelerator H (ETA-II) provided a 50-nanosecond, 6-MeV, 2--3 kAmp electron beam that was introduced co-linear into the IMP FEL with a 140 GHz Gyrotron master oscillator (MO). The FEL was able to amplifymore » the MO signal from approximately 7 kW to peaks consistently in the range of 1--2 GW. This microwave pulse was transmitted into the MTX and allowed the exploration of the linear and non-linear effects of short pulse, intense power in the MTX plasma. Single pulses were used to explore and gain operating experience in the parameter space of the IMP FEL, and finally evaluate transmission and absorption in the MTX. Single-pulse operations were repeatable. After the MTX was shut down burst-mode operations were successful at 2 kHz. This paper will describe the IMP FEL, Microwave Transmission System to MTX, the diagnostics used for calorimetric measurements, and the operations of the entire Microwave system. A discussion of correlated and uncorrelated errors that affect FEL performance will be made Linear and non-linear absorption data of the microwaves in the MTX plasma will be presented.« less

Ultrasound-assisted fabrication of nanoporous CdS films.

PubMed

Singh, R S; Sanagapalli, S; Jayaraman, V; Singh, V P

2004-01-01

A new method for fabricating nanoporous CdS films is reported. It involves exposing the CdS solution with ultrasound waves during the process of dip coating. Indium tin oxide (ITO)-coated glass and plastic (commercial transparency) were used as substrates. In each case three different precursors were used for dip coating. The precursors used were CdCl2 and thiourea in one case and CdS nanoparticles prepared by sonochemical and microwave-assisted methods in the other two cases. X-ray diffraction studies performed on these powders show a phase corresponding to cubic CdS. The Field Emission Scanning Electron Microscopy (FE-SEM) images of the films on plastic showed uniform pores with a diameter of 80 nm for all three methods. Optical absorption measurements indicated a blue shift and multiple peaks in the absorption curve. The FE-SEM observations of the films on an ITO/glass substrate indicated a crystalline film with voids. The UV-vis absorption results indicated a blue shift in the absorption with an absorption edge at 435, 380, and 365 nm for CdS films made by solution growth, sonochemical, and microwave routes, respectively. The magnitude of the absorption is dependent on film thickness, and the observed blue shift in the absorption can be explained on the basis of quantum confinement effects.

Microwave Permittivity and Permeability Measurement on Lunar Soils

NASA Technical Reports Server (NTRS)

Barmatz, Martin; Steinfeld, David; Begley, Shelley B.; Winterhalter, Daniel; Allen, Carlton

2011-01-01

There has been interest in finding ways to process the lunar regolith since the early analyses of lunar samples returned from the Apollo moon missions. This fact has led to proposals for using microwaves to perform in-situ processing of the lunar soil to support future colonization of the moon. More recently, there has been speculation that the excellent microwave absorption of lunar soil came from the nanophase iron content in the regolith. The motivation for the present study was to begin obtaining a more fundamental understanding of the dielectric and magnetic properties of the regolith at microwave frequencies. A major objective of this study was to obtain information that would help answer the question about whether nanophase iron plays a major role in heating lunar soils. These new measurements over a wide frequency range can also determine the magnitude of the dielectric and magnetic absorption and if there are any resonant features that could be used to enhance processing of the regolith in the future. In addition, these microwave measurements would be useful in confirming that new simulants being developed, particularly those containing nanophase iron, would have the correct composition to simulate the lunar regolith. The results of this study suggest that nanophase iron does not play a major role in heating lunar regolith.

Utilizing commercial microwave for rapid and effective immunostaining.

PubMed

Owens, Katrina; Park, Ji H; Kristian, Tibor

2013-09-30

There is an accumulating literature demonstrating the application of microwaves across a wide spectrum of histological techniques. Although exposure to microwaves for short periods resulted in substantial acceleration of all procedures this technique still is not adopted widely. In part, this may be due to concerns over solutions that will avoid induction of thermal damage to the tissue when using standard microwave. Here, we offer a cooling setup that can be used with conventional microwave ovens. We utilized dry ice for effective cooling during microwave irradiation of tissue samples. To prevent overheating, the cups with tissue during exposure to microwaves were surrounded with powdered dry ice. Since the dry ice does not touch the walls of the cups, freezing is prevented. Overheating is avoided by alternating the microwave treatment with 1-2 min time periods when the cups are cooled outside of the microwave oven. This technique was used on mouse brain sections that were immunostained with microglia-specific CD68 antiserum and astrocyte labeling GFAP antibody. Both standard and microwave-assisted immonolabeling gave comparable results visualizing cells with fine processes and low background signal. Short incubation time in the microwave requires high concentrations of antibody for tissue immunostaining. We show that by prolonging the microwaving procedure we were able to reduce the antibody concentration to the levels used in standard immunostaining protocol. In summary, our technique gives a possibility to use a conventional microwave for rapid and effective immunolabeling resulting in reduced amount of antibody required for satisfactory immunostaining. Published by Elsevier B.V.

The microwave induced plasma with optical emission spectrometry (MIP-OES) in 23 elements determination in geological samples.

PubMed

Niedzielski, P; Kozak, L; Wachelka, M; Jakubowski, K; Wybieralska, J

2015-01-01

The article presents the optimisation, validation and application of the microwave induced plasma optical emission spectrometry (MIP-OES) dedicated for a routine determination of Ag, Al, B, Ba, Bi, Ca, Cd, Cr, Cu, Fe, Ga, In, K, Li, Mg, Mn, Mo, Na, Ni, Pb, Sr, Tl, Zn, in the geological samples. The three procedures of sample preparation has been proposed: sample digestion with the use of hydrofluoric acid for determination of total concentration of elements, extraction by aqua regia for determination of the quasi-total element concentration and extraction by hydrochloric acid solution to determine contents of the elements in acid leachable fraction. The detection limits were on the level 0.001-0.121 mg L(-1) (from 0.010-0.10 to 1.2-12 mg kg(-1) depend on the samples preparation procedure); the precision: 0.20-1.37%; accuracy 85-115% (for recovery for certified standards materials analysis and parallel analysis by independent analytical techniques: X-ray fluorescence (XRF) and flame absorption spectrometry (FAAS)). The conformity of the results obtained by MIP-OES analytical procedures with the results obtained by XRF and FAAS analysis allows to propose the procedures for studies of elemental composition of the fraction of the geological samples. Additionally, the MIP-OES technique is much less expensive than ICP techniques and much less time-consuming than AAS techniques. Copyright © 2014 Elsevier B.V. All rights reserved.

Inverse spin Hall effect from pulsed spin current in organic semiconductors with tunable spin-orbit coupling.

PubMed

Sun, Dali; van Schooten, Kipp J; Kavand, Marzieh; Malissa, Hans; Zhang, Chuang; Groesbeck, Matthew; Boehme, Christoph; Valy Vardeny, Z

2016-08-01

Exploration of spin currents in organic semiconductors (OSECs) induced by resonant microwave absorption in ferromagnetic substrates is appealing for potential spintronics applications. Owing to the inherently weak spin-orbit coupling (SOC) of OSECs, their inverse spin Hall effect (ISHE) response is very subtle; limited by the microwave power applicable under continuous-wave (cw) excitation. Here we introduce a novel approach for generating significant ISHE signals in OSECs using pulsed ferromagnetic resonance, where the ISHE is two to three orders of magnitude larger compared to cw excitation. This strong ISHE enables us to investigate a variety of OSECs ranging from π-conjugated polymers with strong SOC that contain intrachain platinum atoms, to weak SOC polymers, to C60 films, where the SOC is predominantly caused by the curvature of the molecule's surface. The pulsed-ISHE technique offers a robust route for efficient injection and detection schemes of spin currents at room temperature, and paves the way for spin orbitronics in plastic materials.

Superficial heat reduction technique for a hybrid microwave-optical device.

PubMed

Al-Armaghany, A; Tong, K; Leung, T S

2013-01-01

Microwave applicator in the form of a circularly polarized microstrip patch antenna is proposed to provide localized deep heating in biological tissue, which causes blood vessels to dilate leading to changes in tissue oxygenation. These changes are monitored by an integrated optical system for studying thermoregulation in different parts of the human body. Using computer simulations, this paper compares circularly and linearly polarized antennas in terms of the efficiency of depositing electromagnetic (EM) energy and the heating patterns. The biological model composes of the skin, fat and muscle layers with appropriate dielectric and thermal properties. The results show that for the same specific absorption rate (SAR) in the muscle, the circularly polarized antenna results in a lower SAR in the skin-fat interface than the linearly polarized antenna. The thermal distribution is also presented based on the biological heat equation. The proposed circularly polarized antenna shows heat reduction in the superficial layers in comparison to the linearly polarized antenna.

Experimental Quasi-Microwave Whole-Body Averaged SAR Estimation Method Using Cylindrical-External Field Scanning

NASA Astrophysics Data System (ADS)

Kawamura, Yoshifumi; Hikage, Takashi; Nojima, Toshio

The aim of this study is to develop a new whole-body averaged specific absorption rate (SAR) estimation method based on the external-cylindrical field scanning technique. This technique is adopted with the goal of simplifying the dosimetry estimation of human phantoms that have different postures or sizes. An experimental scaled model system is constructed. In order to examine the validity of the proposed method for realistic human models, we discuss the pros and cons of measurements and numerical analyses based on the finite-difference time-domain (FDTD) method. We consider the anatomical European human phantoms and plane-wave in the 2GHz mobile phone frequency band. The measured whole-body averaged SAR results obtained by the proposed method are compared with the results of the FDTD analyses.

ARTICLES: Microwave Assisted Synthesis of a New Triplet Iridium(III) Pyrazine Complex

NASA Astrophysics Data System (ADS)

Wu, Qiu-hua; Wang, Chuan-hong; Song, Xi-ming; Zhang, Guo-lin

2010-06-01

A new cyclometalated iridium(III) complex Ir(DPP)3 (DPP = 2,3-diphenylpyrazine) was prepared by reaction of DPP with iridium trichloride hydrate under microwave irradiation. The structure of the complex was confirmed by elemental analysis, 1H NMR, and mass spectroscopy. The UV-Vis absorption and photoluminescent properties of the complex were investigated. The complex shows strong 1MLCT (singlet metal to ligand charge-transfer) and 3MLCT (triplet metal to ligand charge-transfer) absorption at 382 and 504 nm, respectively. The complex also shows strong photoluminescence at 573 nm at room temperature. These results suggest the complex to be a promising phosphorescent material.

Physicochemical and Nonlinear Optical Properties of Novel Environmentally Benign Heterocyclic Azomethine Dyes: Experimental and Theoretical Studies

PubMed Central

Afzal, S. M.; Razvi, M. A. N.; Khan, Salman A.; Osman, Osman I.; Bakry, Ahmed H.; Asiri, Abdullah M.

2016-01-01

Novel heterocyclic azomethine dyes were prepared by the reaction of anthracene-9-carbaldehyde with different heterocyclic amines under microwave irradiation. Structures of the azomethine dyes were confirmed by the elemental analysis, mass spectrometry and several spectroscopic techniques. We studied absorbance and fluorescence spectra of the azomethine dyes in various solvents. They are found to be good absorbers and emitters. We also report photophysical properties like, extinction coefficient, oscillator strength, stokes shift and transition dipole moment. This reflects physicochemical behaviors of synthesized dyes. In addition, their intramolecular charge transfer and nonlinear optical properties, supported by natural bond orbital technique, were also studied computationally by density functional theory. The negative nonlinear refractive index and nonlinear absorption coefficient were measured for these dyes using the closed and open aperture Z-scan technique with a continuous wave helium-neon laser. These are found to vary linearly with solution concentration. PMID:27631371

Octahedron Fe3O4 particles supported on 3D MWCNT/graphene foam: In-situ method and application as a comprehensive microwave absorption material

NASA Astrophysics Data System (ADS)

Shi, Luolin; Zhao, Yan; Li, Ye; Han, Xiao; Zhang, Tong

2017-09-01

In this work, we used in-situ method to directly prepare a novel structure consisting of well-distributed octahedron Fe3O4 particles, porous graphene foam (GF) and fibrous multiwalled carbon nanotube (MWCNT): started with an intense stir to anchor Fe3+ on the surfaces of graphene oxide and oxided MWCNT, followed by solvothermal reaction to synthesize 3D lightweight Fe3O4/MWCNT/GF hybrids with high performance microwave absorption (MA). The maximum Reflection Loss (RL) value of -35.30 dB and 9.01 GHz bandwidth with RL below -10 dB detected with the thickness of 3.0 mm are achieved by Fe3O4/MWCNT/GF with an ultralow bulk density of 5.0 mg cm-3, of which the Specific Microwave Absorption Performance is much higher than most available MA materials reported. Impedance matching, high loss characteristic, interfacial polarization and polarization relaxation significantly improve MA properties, which serves as a guide for fabricating comprehensive MA materials enjoying numerous advantages of high RL value, broad bandwidth, low density and thin thickness.

Laminated and Two-Dimensional Carbon-Supported Microwave Absorbers Derived from MXenes.

PubMed

Han, Meikang; Yin, Xiaowei; Li, Xinliang; Anasori, Babak; Zhang, Litong; Cheng, Laifei; Gogotsi, Yury

2017-06-14

Microwave absorbers with layered structures that can provide abundant interfaces are highly desirable for enhancing electromagnetic absorbing capability and decreasing the thickness. The atomically thin layers of two-dimensional (2D) transition-metal carbides (MXenes) make them a convenient precursor for synthesis of other 2D and layered structures. Here, laminated carbon/TiO 2 hybrid materials composed of well-aligned 2D carbon sheets with embedded TiO 2 nanoparticles were synthesized and showed excellent microwave absorption. Disordered 2D carbon layers with an unusual structure were obtained by annealing multilayer Ti 3 C 2 MXene in a CO 2 atmosphere. The minimum reflection coefficient of laminated carbon/TiO 2 composites reaches -36 dB, and the effective absorption bandwidth ranges from 3.6 to 18 GHz with the tunable thickness from 1.7 to 5 mm. The effective absorption bandwidth covers the whole Ku band (12.4-18 GHz) when the thickness of carbon/TiO 2 /paraffin composite is 1.7 mm. This study is expected to pave the way to the synthesis of carbon-supported absorbing materials using a large family of 2D carbides.

Microwave Resonator Measurements of Atmospheric Absorption Coefficients: A Preliminary Design Study

NASA Technical Reports Server (NTRS)

Walter, Steven J.; Spilker, Thomas R.

1995-01-01

A preliminary design study examined the feasibility of using microwave resonator measurements to improve the accuracy of atmospheric absorption coefficients and refractivity between 18 and 35 GHz. Increased accuracies would improve the capability of water vapor radiometers to correct for radio signal delays caused by Earth's atmosphere. Calibration of delays incurred by radio signals traversing the atmosphere has applications to both deep space tracking and planetary radio science experiments. Currently, the Cassini gravity wave search requires 0.8-1.0% absorption coefficient accuracy. This study examined current atmospheric absorption models and estimated that current model accuracy ranges from 5% to 7%. The refractivity of water vapor is known to 1% accuracy, while the refractivity of many dry gases (oxygen, nitrogen, etc.) are known to better than 0.1%. Improvements to the current generation of models will require that both the functional form and absolute absorption of the water vapor spectrum be calibrated and validated. Several laboratory techniques for measuring atmospheric absorption and refractivity were investigated, including absorption cells, single and multimode rectangular cavity resonators, and Fabry-Perot resonators. Semi-confocal Fabry-Perot resonators were shown to provide the most cost-effective and accurate method of measuring atmospheric gas refractivity. The need for accurate environmental measurement and control was also addressed. A preliminary design for the environmental control and measurement system was developed to aid in identifying significant design issues. The analysis indicated that overall measurement accuracy will be limited by measurement errors and imprecise control of the gas sample's thermodynamic state, thermal expansion and vibration- induced deformation of the resonator structure, and electronic measurement error. The central problem is to identify systematic errors because random errors can be reduced by averaging. Calibrating the resonator measurements by checking the refractivity of dry gases which are known to better than 0.1% provides a method of controlling the systematic errors to 0.1%. The primary source of error in absorptivity and refractivity measurements is thus the ability to measure the concentration of water vapor in the resonator path. Over the whole thermodynamic range of interest the accuracy of water vapor measurement is 1.5%. However, over the range responsible for most of the radio delay (i.e. conditions in the bottom two kilometers of the atmosphere) the accuracy of water vapor measurements ranges from 0.5% to 1.0%. Therefore the precision of the resonator measurements could be held to 0.3% and the overall absolute accuracy of resonator-based absorption and refractivity measurements will range from 0.6% to 1.

The Ionization History of The Intergalactic Medium:

NASA Technical Reports Server (NTRS)

Madau, Piero

2003-01-01

The funded project seeked a unified description of the ionization, physical structure, and evolution of the intergalactic medium (IGM) and quasar intervening absorption systems. We proposed to conduct theoretical studies of the IGM and QSO absorbers in the context of current theories of galaxy formation, developing and using numerical and analytical techniques aimed at a detailed modeling of cosmological radiative transfer, gas dynamics, and thermal and ionization evolution. The ionization history of the IGM has important implications for the metagalactic UV background, intergalactic helium absorption 21-cm tomography, metal absorption systems, fluctuations in the microwave background, and the cosmic rate of structure and star formation. All the original objectives of our program have been achieved, and the results widely used and quoted by the community. Indeed, they remain relevant as the level and complexity of research in this area has increased substantially since our proposal was submitted, due to new discoveries on galaxy formation and evolution, a flood of high-quality data on the distant universe, new theoretical ideas and direct numerical simulations of structure formation in hierarchical clustering theories.

Selective coherent perfect absorption in metamaterials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Nie, Guangyu; Shi, Quanchao; Zhu, Zheng

2014-11-17

We show multi-band coherent perfect absorption (CPA) in simple bilayered asymmetrically split ring metamaterials. The selectivity of absorption can be accomplished by separately excited electric and magnetic modes in a standing wave formed by two coherent counterpropagating beams. In particular, each CPA can be completely switched on/off by the phase of a second coherent wave. We propose a practical scheme for realizing multi-band coherent perfect absorption of 100% that is allowed to work from microwave to optical frequency.

ACCURATE: Greenhouse Gas Profiles Retrieval from Combined IR-Laser and Microwave Occultation Measurements

NASA Astrophysics Data System (ADS)

Proschek, Veronika; Kirchengast, Gottfried; Schweitzer, Susanne; Fritzer, Johannes

2010-05-01

The new climate satellite concept ACCURATE (Atmospheric Climate and Chemistry in the UTLS Region And climate Trends Explorer) enables simultaneous measurement of profiles of greenhouse gases, isotopes, wind and thermodynamic variables from Low Earth Orbit (LEO) satellites. The measurement principle applied is a combination of the novel LEO-LEO infrared laser occultation (LIO) technique and the already better studied LEO-LEO microwave occultation (LMO) technique. Resulting occultation events are evenly distributed around the world, have high vertical resolution and accuracy and are stable over long time periods. The LIO uses near-monochromatic signals in the short-wave infrared range (~2-2.5 μm for ACCURATE). These signals are absorbed by various trace species in the Earth's atmosphere. Profiles of the concentration of the absorbing species can be derived from signal transmission measurements. Accurately known temperature, pressure and humidity profiles derived from simultaneously measured LMO signals are essential pre-information for the retrieval of the trace species profiles. These LMO signals lie in the microwave band region from 17-23 GHz and, optionally, 178-195 GHz. The current ACCURATE mission design is arranged for the measurement of six greenhouse gases (GHG) (H2O, CO2, CH4, N2O, O3, CO) and four isotopes (13CO2, C18OO, HDO, H218O), with focus on the upper troposphere/lower stratosphere region (UTLS, 5-35 km). Wind speed in line-of-sight can be derived from a line-symmetric transmission difference which is caused by wind-induced Doppler shift. By-products are information on cloud layering, aerosol extinction, and scintillation strength. We introduce the methodology to retrieve GHG profiles from quasi-realistic forward-simulated intensities of LIO signals and thermodynamic profiles retrieved in a preceding step from LMO signals. Key of the retrieval methodology is the differencing of two LIO transmission signals, one being GHG sensitive on a target absorption line and one being a close-by reference outside of any absorption lines. The reference signal is used to remove atmospheric broadband" effects by this differential absorption" approach. Refractivity and impact parameter of the LIO signals, needed for the retrieval, can be computed from the LMO-derived thermodynamic profiles. An Abel Transform converts the differential LIO log-transmission profile to the absorption coefficient. Based on the absorption coefficient and the absorption cross section of the GHG under investigation, that can as well be computed from the LMO-derived profiles, the number density profile or volume mixing ratio of the desired GHG can be finally derived. When using several LIO signals, best sensitive to the same GHG at different heights, a joint optimal GHG profile can be constructed by combining the individual profiles in an inverse-variance-weighted manner (practically used for H2O, obtained from 3-4 signals, and for CO2, obtained from 2 isotope signals). The thermodynamic parameters (temperature, pressure and humidity) derived from LMO as basis for the LIO retrieval are found to be accurate to better than 0.5 K for temperature, 0.2% for pressure, and 10% for humidity. The accuracy of retrieved trace species profiles is found better than 1% to 4% for single profiles in the UTLS region (outside clouds which block infrared) and the profiles are essentially unbiased (biases

Laboratory Evaluation and Application of Microwave Absorption Properties Under Simulated Conditions for Planetary Atmospheres

NASA Technical Reports Server (NTRS)

Steffes, Paul G.

1997-01-01

Radio absorptivity data for planetary atmospheres obtained from spacecraft radio occultation experiments and earth-based radio astronomical observations can be used to infer abundances of microwave absorbing constituents in those atmospheres, as long as reliable information regarding the microwave absorbing properties of potential constituents is available. The use of theoretically-derived microwave absorption properties for such atmospheric constituents, or using laboratory measurements of such properties under environmental conditions which are significantly different than those of the planetary atmosphere being studied, often leads to significant misinterpretation of available opacity data. Laboratory measurements completed under this grant (NAGW-533), have shown that the opacity from, SO2 under simulated Venus conditions is best described by a different lineshape than was previously used in theoretical predictions. The recognition of the need to make such laboratory measurements of simulated planetary atmospheres over a range of temperatures and pressures which correspond to the altitudes probed by both radio occultation experiments and radio astronomical observations, and over a range of frequencies which correspond to those used in both radio occultation experiments and radio astronomical observations, has led to the development of a facility at Georgia Tech which is capable of making such measurements. It has been the goal of this investigation to conduct such measurements and to apply the results to a wide range of planetary observations, both spacecraft and earth-based, in order to determine the identity and abundance profiles of constituents in those planetary atmospheres.

Enhanced microwave absorption property of epoxy nanocomposites based on PANI@Fe3O4@CNFs nanoparticles with three-phase heterostructure

NASA Astrophysics Data System (ADS)

Yang, Lingfeng; Cai, Haopeng; Zhang, Bin; Huo, Siqi; Chen, Xi

2018-02-01

Novel electromagnetic functionalized carbon nanofibers (CNFs) have been synthesized by coating with Fe3O4 magnetite nanoparticles and conducting polymers polyaniline (PANI) on CNFs through a layer by layer assembly. The Fe3O4@CNFs were first prepared by coating nano-Fe3O4 particles on CNFs via co-precipitation method; Then the PANI was coated on Fe3O4@CNFs using an in situ polymerization process to obtain PANI@Fe3O4@CNFs nanoparticles. The prepared PANI@Fe3O4@CNFs nanoparticles were dispersed in the epoxy matrix to fabricate microwave absorbing nanocomposites. Compared with the Fe3O4@CNFs/epoxy nanocomposites, the PANI@Fe3O4@CNFs/epoxy nanocomposites exhibit better microwave absorbing properties. The composite containing 15 wt% of PANI@Fe3O4@CNFs with the thickness of 2 mm showed a minimum reflection loss (RL) value of -23.7 dB with an effective absorption bandwidth which is about 3.7 GHz (11.9-15.6 GHz) in the frequency range of 1-18 GHz, indicating that it is an attractive candidate for efficient microwave absorber. A potential absorption mechanism was proposed for enhancement of the impedance-matching condition and electromagnetic wave-attenuation characteristic of materials. Specifically, the impedance-matching condition was improved by the combination of conductive polymers and magnetic nanoparticles with CNFs. The electromagnetic wave attenuation characteristic was enhanced by multiple reflections, due to the increased propagation paths.

A comparison of essential oils obtained from lavandin via different extraction processes: Ultrasound, microwave, turbohydrodistillation, steam and hydrodistillation.

PubMed

Périno-Issartier, Sandrine; Ginies, Christian; Cravotto, Giancarlo; Chemat, Farid

2013-08-30

A total of eight extraction techniques ranging from conventional methods (hydrodistillation (HD), steam distillation (SD), turbohydrodistillation (THD)), through innovative techniques (ultrasound assisted extraction (US-SD) and finishing with microwave assisted extraction techniques such as In situ microwave-generated hydrodistillation (ISMH), microwave steam distillation (MSD), microwave hydrodiffusion and gravity (MHG), and microwave steam diffusion (MSDf)) were used to extract essential oil from lavandin flowers and their results were compared. Extraction time, yield, essential oil composition and sensorial analysis were considered as the principal terms of comparison. The essential oils extracted using the more innovative processes were quantitatively (yield) and qualitatively (aromatic profile) similar to those obtained from the conventional techniques. The method which gave the best results was the microwave hydrodiffusion and gravity (MHG) method which gave reduced extraction time (30min against 220min for SD) and gave no differences in essential oil yield and sensorial perception. Copyright © 2013 Elsevier B.V. All rights reserved.

Detection of chemical contraband using spectroscopic microwave imaging

NASA Astrophysics Data System (ADS)

Falconer, David G.; Watters, David G.

1994-02-01

We have developed and demonstrated a microwave technique for detecting high explosives, illegal drugs, and other chemical contraband in checked airline baggage. Our technique isolates suspicious materials using microwave tomography and identifies chemical contraband using microwave spectroscopy. Measurements in the frequency range 2 - 18 GHz indicate that microwave energy will penetrate nonmetallic suitcases and that contraband materials feature distinct dielectric spectra at these wavelengths. We have also formed microwave images of a soft-sided suitcase and its contents. After manually segmenting the microwave imagery, we successfully identified chemical simulants for both high explosives and illegal drugs.

Optimization of microwave digestion for mercury determination in marine biological samples by cold vapour atomic absorption spectrometry.

PubMed

Cardellicchio, Nicola; Di Leo, Antonella; Giandomenico, Santina; Santoro, Stefania

2006-01-01

Optimization of acid digestion method for mercury determination in marine biological samples (dolphin liver, fish and mussel tissues) using a closed vessel microwave sample preparation is presented. Five digestion procedures with different acid mixtures were investigated: the best results were obtained when the microwave-assisted digestion was based on sample dissolution with HNO3-H2SO4-K2Cr2O7 mixture. A comparison between microwave digestion and conventional reflux digestion shows there are considerable losses of mercury in the open digestion system. The microwave digestion method has been tested satisfactorily using two certified reference materials. Analytical results show a good agreement with certified values. The microwave digestion proved to be a reliable and rapid method for decomposition of biological samples in mercury determination.

Effects of Pulsed 2.856 GHz Microwave Exposure on BM-MSCs Isolated from C57BL/6 Mice

PubMed Central

Wang, Changzhen; Wang, Xiaoyan; Zhou, Hongmei; Dong, Guofu; Guan, Xue; Wang, Lifeng; Xu, Xinping; Wang, Shuiming; Chen, Peng; Peng, Ruiyun; Hu, Xiangjun

2015-01-01

The increasing use of microwave devices over recent years has meant the bioeffects of microwave exposure have been widely investigated and reported. However the exact biological fate of bone marrow MSCs (BM-MSCs) after microwave radiation remains unknown. In this study, the potential cytotoxicity on MSC proliferation, apoptosis, cell cycle, and in vitro differentiation were assayed following 2.856 GHz microwave exposure at a specific absorption rate (SAR) of 4 W/kg. Importantly, our findings indicated no significant changes in cell viability, cell division and apoptosis after microwave treatment. Furthermore, we detected no significant effects on the differentiation ability of these cells in vitro, with the exception of reduction in mRNA expression levels of osteopontin (OPN) and osteocalcin (OCN). These findings suggest that microwave treatment at a SAR of 4 W/kg has undefined adverse effects on BM-MSCs. However, the reduced-expression of proteins related to osteogenic differentiation suggests that microwave can the influence at the mRNA expression genetic level. PMID:25658708

Fluorinated graphene oxide for enhanced S and X-band microwave absorption

DOE Office of Scientific and Technical Information (OSTI.GOV)

Sudeep, P. M.; TIFR-Centre for Interdisciplinary Sciences, Tata Institute of Fundamental Research, Hyderabad 500075; Vinayasree, S.

2015-06-01

Here we report the microwave absorbing properties of three graphene derivatives, namely, graphene oxide (GO), fluorinated GO (FGO, containing 5.6 at. % Fluorine (F)), and highly FGO (HFGO, containing 23 at. % F). FGO is known to be exhibiting improved electrochemical and electronic properties when compared to GO. Fluorination modifies the dielectric properties of GO and hence thought of as a good microwave absorber. The dielectric permittivities of GO, FGO, and HFGO were estimated in the S (2 GHz to 4 GHz) and X (8 GHz to 12 GHz) bands by employing cavity perturbation technique. For this, suspensions containing GO/FGO/HFGO were made in N-Methylmore » Pyrrolidone (NMP) and were subjected to cavity perturbation. The reflection loss was then estimated and it was found that −37 dB (at 3.2 GHz with 6.5 mm thickness) and −31 dB (at 2.8 GHz with 6 mm thickness) in the S band and a reflection loss of −18 dB (at 8.4 GHz with 2.5 mm thickness) and −10 dB (at 11 GHz with 2 mm thickness) in the X band were achieved for 0.01 wt. % of FGO and HFGO in NMP, respectively, suggesting that these materials can serve as efficient microwave absorbers even at low concentrations.« less

A newly-designed magnetic/dielectric [Fe3O4/BaTiO3@MWCNT] nanocomposite system for modern electromagnetic absorption applications

NASA Astrophysics Data System (ADS)

Sardarian, Pouria; Naffakh-Moosavy, Homam; Afghahi, Seyyed Salman Seyyed

2017-11-01

Developments in electronic industries for telecommunications and demands for decreasing electromagnetic radiation pollution result in developing researches on microwave absorption materials. The target of the present study is to design materials with high absorption properties for electromagnetic waves in the 12-18 GHz range. Thus, Fe3O4 magnetic nanoparticles were syntheses through chemical co-precipitation reinforced by ultrasonic. Then, BaTiO3 nanocrystalline powder was synthesized by the hydrothermal sol-gel method under atmospheric oxygen. Next, nano-particles of barium titanate were deposited on the multi-walled carbon nanotubes (BaTiO3@CNT). It was concluded that a magnetic-dielectric nanocomposite has superior microwave absorption properties in comparison to individual magnetic or dielectric absorbers. Also, in order to obtain an optimum absorption in a wide frequency band, dielectric-CNT nanocomposites represents higher properties than magnetic-CNT composites. It is concluded that composites with more magnetic percentage showed better absorption in low frequency band (12 GHz), whereas composites with more dielectric percentage exhibited superior absorption for high frequency band (18 GHz). 80-93% absorption was obtained in the frequency range of 16.7-18 GHz by composite 40M.20F.40C (40% paraffin, 20% magnetite, 40% multi-walled carbon nanotubes). Also, composite 40M.20B.40B@C (40% paraffin, 20% barium titanate, 40% barium titanate deposited on multi-walled carbon nanotubes) showed the absorption of 80-90%.

One-step microwave-assisted colloidal synthesis of hybrid silver oxide/silver nanoparticles: characterization and catalytic study

NASA Astrophysics Data System (ADS)

Prakoso, S. P.; Taufik, A.; Saleh, R.

2017-04-01

This study reports the characterization and catalytic activities of silver-oxide/silver nanoparticles (Ag2O/Ag NPs) synthesized by microwave-assisted colloidal method in the presence of anionic sodium dodecyl sulfate (SDS) surfactant. To promote different contents of silver in silver oxide, the volume ratio (VR) of ethylene glycol (EG) was varied (VR: 10% to 14%) in relation to the total volume of distilled water solvent. The plasmonic resonance of Ag2O/Ag NPs could be detected around a wavelength of 350 nm, and it is suggested that Ag2O/Ag NPs were successfully formed in the colloid solution following exposure to microwaves. Additionally, the growth rate for each crystal phase within Ag2O and Ag was influenced by an increase of EG as revealed by x-ray diffraction patterns. The morphology, average diameter, and uniformity of Ag2O/Ag NPs were studied simultaneously by transmission electron microscopy. Infrared absorption measurement of Ag2O/Ag NPs confirmed the existence of SDS surfactant as a protective agent. Based on the characterization data, Ag2O/Ag NPs synthesized using this technique exhibited good properties, with high-yield production of NPs. The photocatalytic experiments demonstrate the key role of the crystal phase of Ag2O/Ag NPs in photocatalytic efficiency.

Synergistic Enhancement of Microwave Absorption Using Hybridized Polyaniline@helical CNTs with Dual Chirality.

PubMed

Tian, Xin; Meng, Fanbin; Meng, Fanchen; Chen, Xiangnan; Guo, Yifan; Wang, Ying; Zhu, Wenjun; Zhou, Zuowan

2017-05-10

In this study, we designed a dual-chirality hierarchical structure to achieve a synergistically enhanced effect in microwave absorption via the hybridization of nanomaterials. Herein, polyaniline (PANi) nanorods with tunable chirality are grown on helical carbon nanotubes (HCNTs), a typical nanoscale chiral structure, through in situ polymerization. The experimental results show that the hierarchical hybrids (PANi@HCNTs) exhibit distinctly dual chirality and a significant enhancement in electromagnetic (EM) losses compared to those of either pure PANi or HCNTs. The maximum reflection loss of the as-prepared hybrids can reach -32.5 dB at 8.9 GHz. Further analysis demonstrates that combinations of chiral acid-doped PANi and coiled HCNTs with molecular and nanoscale chirality lead to synergistic effects resulting from the dual chirality. The so-called cross-polarization may result in additional interactions with induced EM waves in addition to multiscaled relaxations from functional groups and interfacial polarizations, which can benefit EM absorption.

Templated synthesis of highly ordered mesoporous cobalt ferrite and its microwave absorption properties

NASA Astrophysics Data System (ADS)

Li, Guo-Min; Wang, Lian-Cheng; Xu, Yao

2014-08-01

Based on the nanocasting strategy, highly ordered mesoporous CoFe2O4 is synthesized via the ‘two-solvent’ impregnation method using a mesoporous SBA-15 template. An ordered two-dimensional (P6mm) structure is preserved for the CoFe2O4/SBA-15 composite after the nanocasting. After the SBA-15 template is dissolved by NaOH solution, a mesoporous structure composed of aligned nanoparticles can be obtained, and the P6mm structure of the parent SBA-15 is preserved. With a high specific surface area (above 90 m2/g) and ferromagnetic behavior, the obtained material shows potential in light weight microwave absorption application. The minimum reflection loss (RL) can reach -18 dB at about 16 GHz with a thickness of 2 mm and the corresponding absorption bandwidth is 4.5 GHz.

Ultrathin microwave metamaterial absorber utilizing embedded resistors

NASA Astrophysics Data System (ADS)

Kim, Young Ju; Hwang, Ji Sub; Yoo, Young Joon; Khuyen, Bui Xuan; Rhee, Joo Yull; Chen, Xianfeng; Lee, YoungPak

2017-10-01

We numerically and experimentally studied an ultrathin and broadband perfect absorber by enhancing the bandwidth with embedded resistors into the metamaterial structure, which is easy to fabricate in order to lower the Q-factor and by using multiple resonances with the patches of different sizes. We analyze the absorption mechanism in terms of the impedance matching with the free space and through the distribution of surface current at each resonance frequency. The magnetic field, induced by the antiparallel surface currents, is formed strongly in the direction opposite to the incident electromagnetic wave, to cancel the incident wave, leading to the perfect absorption. The corresponding experimental absorption was found to be higher than 97% in 0.88-3.15 GHz. The agreement between measurement and simulation was good. The aspects of our proposed structure can be applied to future electronic devices, for example, advanced noise-suppression sheets in the microwave regime.

Comparison of global cloud liquid water path derived from microwave measurements with CERES-MODIS

NASA Astrophysics Data System (ADS)

Yi, Y.; Minnis, P.; Huang, J.; Lin, B.; Ayers, K.; Sun-Mack, S.; Fan, A.

Cloud liquid water path LWP is a crucial parameter for climate studies due to the link that it provides between the atmospheric hydrological and radiative budgets Satellite-based visible infrared techniques such as the Visible Infrared Solar Split-Window Technique VISST can retrieve LWP for water clouds assumes single-layer over a variety of surfaces If the water clouds are overlapped by ice clouds the LWP of the underlying clouds can not be retrieved by such techniques However microwave techniques may be used to retrieve the LWP underneath ice clouds due to the microwave s insensitivity to cloud ice particles LWP is typically retrieved from satellite-observed microwave radiances only over ocean due to variations of land surface temperature and emissivity Recently Deeter and Vivekanandan 2006 developed a new technique for retrieving LWP over land In order to overcome the sensitivity to land surface temperature and emissivity their technique is based on a parameterization of microwave polarization-difference signals In this study a similar regression-based technique for retrieving LWP over land and ocean using Advanced Microwave Scanning Radiometer - EOS AMSR-E measurements is developed Furthermore the microwave surface emissivities are also derived using clear-sky fields of view based on the Clouds and Earth s Radiant Energy System Moderate-resolution Imaging Spectroradiometer CERES-MODIS cloud mask These emissivities are used in an alternate form of the technique The results are evaluated using independent measurements such

Excellent microwave response derived from the construction of dielectric-loss 1D nanostructure.

PubMed

Dai, Sisi; Quan, Bin; Liang, Xiaohui; Lv, Jing; Yang, Zhihong; Ji, Guangbin; Du, Youwei

2018-05-11

Increasing efforts have recently been devoted to the artificial design and function of nanostructures for their application prospects in catalysis, drug delivery, energy storage, and microwave absorption. With the advantages of natural abundance, low cost, and environment friendliness, a one-dimensional (1D) MnO 2 nanowire (MW) is the representative dielectric-loss absorber for its special morphology and crystalline structure. However, its low reflection loss (RL) value due to its thin thickness limits its wide development and application in the microwave absorption field. In this work, artificially designed MnO 2 @AIR@C (MCs), namely, 1D hollow carbon nanotubes filled with nano-MnO 2 , were designed and synthesized. It is found that the RL value of the MC is almost lower than -10 dB. Furthermore, the RL value was able to achieve -18.9 dB with an effective bandwidth (-10 dB) of 5.84 GHz at 2.25 mm. Simultaneously, the dielectric and interfacial polarization became stronger while the impedance matching was much better than in the single MWs. Hence, the rational design and fabrication of micro-architecture are essential and MC has great potential to be an outstanding microwave absorber.

Excellent microwave response derived from the construction of dielectric-loss 1D nanostructure

NASA Astrophysics Data System (ADS)

Dai, Sisi; Quan, Bin; Liang, Xiaohui; Lv, Jing; Yang, Zhihong; Ji, Guangbin; Du, Youwei

2018-05-01

Increasing efforts have recently been devoted to the artificial design and function of nanostructures for their application prospects in catalysis, drug delivery, energy storage, and microwave absorption. With the advantages of natural abundance, low cost, and environment friendliness, a one-dimensional (1D) MnO2 nanowire (MW) is the representative dielectric-loss absorber for its special morphology and crystalline structure. However, its low reflection loss (RL) value due to its thin thickness limits its wide development and application in the microwave absorption field. In this work, artificially designed MnO2@AIR@C (MCs), namely, 1D hollow carbon nanotubes filled with nano-MnO2, were designed and synthesized. It is found that the RL value of the MC is almost lower than -10 dB. Furthermore, the RL value was able to achieve -18.9 dB with an effective bandwidth (-10 dB) of 5.84 GHz at 2.25 mm. Simultaneously, the dielectric and interfacial polarization became stronger while the impedance matching was much better than in the single MWs. Hence, the rational design and fabrication of micro-architecture are essential and MC has great potential to be an outstanding microwave absorber.

Preliminary studies: far-field microwave dosimetric measurements of a full-scale model of man.

PubMed

Olsen, R G

1979-12-01

Measurements of microwave heating were made in a full-size, upright human model. The 75-Kg model, composed of electrically simulated muscle, was placed in the far-zone of a standard-gain horn inside an absorber-lined chamber. Pulsed energy at 1.29 GHz was obtained from a military radar transmitter (AN/TPS-1G) and produced radiation at 6-14 mW/cm2 average power density at the location of the model. Microwave heating at the front surface was measured at nine locations on the phantom. Measurements at several depths within the phantom were also made at a central location to gain information on the depth-of-penetration of the microwave energy. Results of the frontal surface measurements and of the penetration study permitted a calculation of the approximate whole-body average specific absorption rate (SAR) when the model's long axis was parallel to the E-field vector. For a normalized power density of 1 mW/cm2 at a frequency of 1.29 GHz, the whole-body average SAR approximated 0.03 W/Kg. This result agrees well with theoretical predictions based on absorption in prolate spheroidal models of man.

Electromagnetic-radiation absorption by water.

PubMed

Lunkenheimer, P; Emmert, S; Gulich, R; Köhler, M; Wolf, M; Schwab, M; Loidl, A

2017-12-01

Why does a microwave oven work? How does biological tissue absorb electromagnetic radiation? Astonishingly, we do not have a definite answer to these simple questions because the microscopic processes governing the absorption of electromagnetic waves by water are largely unclarified. This absorption can be quantified by dielectric loss spectra, which reveal a huge peak at a frequency of the exciting electric field of about 20 GHz and a gradual tailing off toward higher frequencies. The microscopic interpretation of such spectra is highly controversial and various superpositions of relaxation and resonance processes ascribed to single-molecule or molecule-cluster motions have been proposed for their analysis. By combining dielectric, microwave, THz, and far-infrared spectroscopy, here we provide nearly continuous temperature-dependent broadband spectra of water. Moreover, we find that corresponding spectra for aqueous solutions reveal the same features as pure water. However, in contrast to the latter, crystallization in these solutions can be avoided by supercooling. As different spectral contributions tend to disentangle at low temperatures, this enables us to deconvolute them when approaching the glass transition under cooling. We find that the overall spectral development, including the 20 GHz feature (employed for microwave heating), closely resembles the behavior known for common supercooled liquids. Thus water's absorption of electromagnetic waves at room temperature is not unusual but very similar to that of glass-forming liquids at elevated temperatures, deep in the low-viscosity liquid regime, and should be interpreted along similar lines.

Novel "203" type of heterostructured MoS2-Fe3O4-C ternary nanohybrid: Synthesis, and enhanced microwave absorption properties

NASA Astrophysics Data System (ADS)

Yang, Erqi; Qi, Xiaosi; Xie, Ren; Bai, Zhongchen; Jiang, Yang; Qin, Shuijie; Zhong, Wei; Du, Youwei

2018-06-01

It is widely recognized that constructing multiple interface structures to enhance interface polarization is very good for the attenuation of electromagnetic (EM) wave. Here, a novel "203" type of heterostructured nanohybrid consisting of two-dimensional (2D) MoS2 nanosheets, zero-dimensional (0D) Fe3O4 nanoparticles and three-dimensional (3D) carbon layers was elaborately designed and successfully synthesized by a two-step method: Fe3O4 nanoparticles were deposited onto the surface of few-layer MoS2 nanosheets by a hydrothermal method, followed by the carbonation process by a chemical vapor deposition method. Compared to that of "20" type MoS2-Fe3O4, the as-prepared heterostructured "203" type MoS2-Fe3O4-C ternary nanohybrid exhibited remarkably enhanced EM and microwave absorption properties. And the minimum reflection loss (RL) value of the obtained MoS2-Fe3O4-C ternary nanohybrid could reach -53.03 dB at 14.4 GHz with a matching thickness of 7.86 mm. Moreover, the excellent EM wave absorption property of the as-prepared ternary nanohybrid was proved to be attributed to the quarter-wavelength matching model. Therefore, a simple and effective route was proposed to produce MoS2-based mixed-dimensional van der Waals heterostructure, which provided a new platform for the designing and production of high performance microwave absorption materials.

Measurement of xenon plasma properties in an ion thruster using laser Thomson scattering technique

DOE Office of Scientific and Technical Information (OSTI.GOV)

Yamamoto, N.; Tomita, K.; Sugita, K.

2012-07-15

This paper reports on the development of a method for measuring xenon plasma properties using the laser Thomson scattering technique, for application to ion engine system design. The thresholds of photo-ionization of xenon plasma were investigated and the number density of metastable atoms, which are photo-ionized by a probe laser, was measured using laser absorption spectroscopy, for several conditions. The measured threshold energy of the probe laser using a plano-convex lens with a focal length of 200 mm was 150 mJ for a xenon mass flow rate of 20 {mu}g/s and incident microwave power of 6 W; the probe lasermore » energy was therefore set as 80 mJ. Electron number density was found to be (6.2 {+-} 0.4) Multiplication-Sign 10{sup 17} m{sup -3} and electron temperature was found to be 2.2 {+-} 0.4 eV at a xenon mass flow rate of 20 {mu}g/s and incident microwave power of 6 W. The threshold of the probe laser intensity against photo-ionization in a miniature xenon ion thruster is almost constant for various mass flow rates, since the ratio of population of the metastable atoms to the electron number density is little changed.« less

Review on Photonic Generation of Chirp Arbitrary Microwave Waveforms for Remote Sensing Application

NASA Astrophysics Data System (ADS)

Raghuwanshi, Sanjeev Kumar; Srivastav, Akash; Athokpam, Bidhanshel Singh

2017-12-01

A novel technique to generate an arbitrary chirped waveform by harnessing features of lithium niobate (LiNb O_3) Mach-Zehnder modulator is proposed and demonstrated. The most important application of chirped microwave waveform is that, it improves the range resolution of radar. Microwave photonics system provides high bandwidth capabilities of fiber-optic systems and also contains the ability to provide interconnect transmission properties, which are virtually independent of length. The low-loss wide bandwidth capability of optoelectronic systems makes them attractive for the transmission and processing of microwave signals, while the development of high-capacity optical communication systems has required the use of microwave techniques in optical transmitters and receivers. These two strands have led to the development of the research area of microwave photonics. So, it should be consider that microwave photonics as the field that studies the interaction between microwave and optical waves for applications such as communications, radars, sensors and instrumentations. In this paper, we have thoroughly reviewed the arbitrary chirped microwave generation techniques by using photonics technology.

1990 MTT-S International Microwave Symposium and Exhibition and Microwave and Millimeter-Wave Monolithic IC Symposium, Dallas, TX, May 7-10, 1990, Proceedings

NASA Astrophysics Data System (ADS)

McQuiddy, David N., Jr.; Sokolov, Vladimir

1990-12-01

The present conference discusses microwave filters, lightwave technology for microwave antennas, planar and quasi-planar guides, mixers and VCOs, cavity filters, discontinuity and coupling effects, control circuits, power dividers and phase shifters, microwave ICs, biological effects and medical applications, CAD and modeling for MMICs, directional couplers, MMIC design trends, microwave packaging and manufacturing, monolithic ICs, and solid-state devices and circuits. Also discussed are microwave and mm-wave superconducting technology, MICs for communication systems, the merging of optical and microwave technologies, microwave power transistors, ferrite devices, network measurements, advanced transmission-line structures, FET devices and circuits, field theory of IC discontinuities, active quasi-optical techniques, phased-array techniques and circuits, nonlinear CAD, sub-mm wave devices, and high power devices.

[Determination of heavy metals for RoHS compliance by ICP-OES spectrometry coupled with microwave extraction system].

PubMed

Hua, Li; Wu, Yi-Ping; An, Bing; Lai, Xiao-Wei

2008-11-01

The harm of heavy metals contained in electronic and electrical equipment (EEE) on environment is of high concern by human. Aiming to handle the great challenge of RoHS compliance, the determinations of trace or ultratrace chromium (Cr), cadmium (Cd), mercury (Hg) and lead (Pb) by inductively coupled plasma optical emission spectrometry (ICP-OES) was performed in the present paper, wherein, microwave extraction technology was used to prepare the sample solutions. In addition, the precision, recovery, repeatability and interference issues of this method were also discussed. The results exhibited that using the microwave extraction system to prepare samples is more quick, lossless, contamination-free in comparison with the conventional extraction methods such as dry ashing, wet-oven extraction etc. By analyzing the recoveries of these four heavy metals over different working time and wavelengths, the good recovery range between 85% and 115% showed that there was only tiny loss or contamination during the process of microwave extraction, sample introduction and ICP detection. Repeatability experiments proved that ICP plasma had a good stability during the working time and the matrix effect was small. Interference was a problem troublesome for atomic absorption spectrometry (AAS), however, the techniques of standard additions or inter-element correction (IEC) method can effectively eliminated the interferences of Ni, As, Fe etc. with the Cd determination. By employing the multi-wavelengths and two correction point methods, the issues of background curve sloping shift and spectra overlap were successfully overcome. Besides, for the determinations of trace heavy metal elements, the relative standard deviation (RSD) was less than 3% and the detection limits were less than 1 microg x L(-10 (3sigma, n = 5) for samples, standard solutions, and standard additions, which proved that ICP-OES has a good precision and high reliability. This provided a reliable technique support for electronic and electrical (EE) industries to comply with RoHS directive.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Klingler, S., E-mail: stefan.klingler@wmi.badw.de; Maier-Flaig, H.; Weiler, M.

Microfocused Brillouin light scattering (BLS) and microwave absorption (MA) are used to study magnon-photon coupling in a system consisting of a split-ring microwave resonator and an yttrium iron garnet (YIG) film. The split-ring resonator is defined by optical lithography and loaded with a 1 μm-thick YIG film grown by liquid phase epitaxy. BLS and MA spectra of the hybrid system are simultaneously recorded as a function of the applied magnetic field magnitude and microwave excitation frequency. Strong coupling of the magnon and microwave resonator modes is found with a coupling strength of g{sub eff} /2π = 63 MHz. The combined BLS and MA datamore » allow us to study the continuous transition of the hybridized modes from a purely magnonic to a purely photonic mode by varying the applied magnetic field and microwave frequency. Furthermore, the BLS data represent an up-conversion of the microwave frequency coupling to optical frequencies.« less

Microwave techniques for measuring complex permittivity and permeability of materials

DOE Office of Scientific and Technical Information (OSTI.GOV)

Guillon, P.

1995-08-01

Different materials are of fundamental importance to the aerospace, microwave, electronics and communications industries, and include for example microwave absorbing materials, antennas lenses and radomes, substrates for MMIC and microwave components and antennaes. Basic measurements for the complex permittivity and permeability of those homogeneous solid materials in the microwave spectral region are described including hardware, instrumentation and analysis. Elevated temperature measurements as well as measurements intercomparisons, with a discussion of the strengths and weaknesses of each techniques are also presented.

Laboratory evaluation and application of microwave absorption properties under simulated conditions for planetary atmospheres

NASA Technical Reports Server (NTRS)

Steffes, Paul G.

1988-01-01

In the first half of this grant year, laboratory measurements were conducted on the millimeter-wave properties of atmospheric gases under simulated conditions for the outer planet. Significant improvements in the current system have made it possible to accurately characterize the opacity from gaseous NH3 at longer millimeter wavelengths (7 to 10 mm) under simulated Jovian conditions. In the second half of the grant year, it is hoped to extend such measurements to even shorter millimeter-wavelengths. Further analysis and application of the laboratory results to microwave and millimeter-wave absorption data for the outer planets, such as results from Voyager Radio Occultation experiments and earth-based radio astronomical observations will be continued. The analysis of available multispectral microwave opacity data from Venus, including data from the most recent radio astronomical ovservations in the 1.3 to 3.6 cm wavelength range and newly obtained Pioneer-Venus Radio Occulatation measurements at 13 cm, using the laboratory measurements as an interpretative tool will be pursued.

Microwave absorption enhancement, magnetic coupling and ab initio electronic structure of monodispersed (Mn1-xCox)3O4 nanoparticles

NASA Astrophysics Data System (ADS)

Zhao, Pengfei; Liang, Chongyun; Gong, Xiwen; Gao, Ran; Liu, Jiwei; Wang, Min; Che, Renchao

2013-08-01

Monodispersed manganese oxide (Mn1-xCox)3O4 (0 <= x <= 0.5) nanoparticles, less than 10 nm size, are respectively synthesized via a facile thermolysis method at a rather low temperature, ranging from 90 to 100 °C, without any inertia gas for protection. The influences of the Co dopant content on the critical reaction temperature required for the nanoparticle formation, electronic band structures, magnetic properties, and the microwave absorption capability of (Mn1-xCox)3O4 are comprehensively investigated by means of both experimental and theoretical approaches including powder X-ray diffraction (XRD), electron energy loss spectroscopy (EELS), super conductivity quantum interference device (SQUID) examination, and first-principle simulations. Co is successfully doped into the Mn atomic sites of the (Mn1-xCox)3O4 lattice, which is further confirmed by EELS data acquired from one individual nanoparticle. Therefore, continuous solid solutions of well-crystallized (Mn1-xCox)3O4 products are achieved without any impurity phase or phase separation. With increases in the Co dopant concentration x from 0 to 0.5, the lattice parameters change systemically, where the overall saturation magnetization at 30 K increases due to the more intense coupling of the 3d electrons between Mn and Co, as revealed by simulations. The microwave absorption properties of the (Mn1-xCox)3O4 nanoparticles are examined between 2 and 18 GHz. The maximum absorption peak -11.0 dB of the x = 0 sample is enhanced to -11.5 dB for x = 0.2, -12.7 dB for x = 0.25, -15.6 dB for x = 0.33, and -24.0 dB for x = 0.5 respectively, suggesting the Co doping effects. Our results might provide novel insights into the understanding of the influences of metallic ion doping on the electromagnetic properties of metallic oxide nanomaterials.Monodispersed manganese oxide (Mn1-xCox)3O4 (0 <= x <= 0.5) nanoparticles, less than 10 nm size, are respectively synthesized via a facile thermolysis method at a rather low temperature, ranging from 90 to 100 °C, without any inertia gas for protection. The influences of the Co dopant content on the critical reaction temperature required for the nanoparticle formation, electronic band structures, magnetic properties, and the microwave absorption capability of (Mn1-xCox)3O4 are comprehensively investigated by means of both experimental and theoretical approaches including powder X-ray diffraction (XRD), electron energy loss spectroscopy (EELS), super conductivity quantum interference device (SQUID) examination, and first-principle simulations. Co is successfully doped into the Mn atomic sites of the (Mn1-xCox)3O4 lattice, which is further confirmed by EELS data acquired from one individual nanoparticle. Therefore, continuous solid solutions of well-crystallized (Mn1-xCox)3O4 products are achieved without any impurity phase or phase separation. With increases in the Co dopant concentration x from 0 to 0.5, the lattice parameters change systemically, where the overall saturation magnetization at 30 K increases due to the more intense coupling of the 3d electrons between Mn and Co, as revealed by simulations. The microwave absorption properties of the (Mn1-xCox)3O4 nanoparticles are examined between 2 and 18 GHz. The maximum absorption peak -11.0 dB of the x = 0 sample is enhanced to -11.5 dB for x = 0.2, -12.7 dB for x = 0.25, -15.6 dB for x = 0.33, and -24.0 dB for x = 0.5 respectively, suggesting the Co doping effects. Our results might provide novel insights into the understanding of the influences of metallic ion doping on the electromagnetic properties of metallic oxide nanomaterials. Electronic supplementary information (ESI) available: Fig. S1. A digital photo showing the large-scale synthesis of our monodispersed (Mn1-xCox)3O4 Fig. S2. Microwave absorption measurements; Fig. S3. Schematic diagram of the microwave absorption mechanism of the (Mn1-xCox)3O4. See DOI: 10.1039/c3nr02287k

ABSORPTION OF MICROWAVE RADIATION BY THE ANESTHETIZED RAT: ELECTROMAGNETIC AND THERMAL HOTSPOTS IN BODY AND TAIL

EPA Science Inventory

Anatomic variability in the deposition of radio frequency electromagnetic energy in mammals as been well documented. ecent study [D'Andrea et al. 1985] reported specific absorption rat (SAR) hotspots in the brain, rectum, and tail of rat carcasses exposed to 360- and to 2,450-MHz...

Conformal dual-band near-perfectly absorbing mid-infrared metamaterial coating.

PubMed

Jiang, Zhi Hao; Yun, Seokho; Toor, Fatima; Werner, Douglas H; Mayer, Theresa S

2011-06-28

Metamaterials offer a new approach to create surface coatings with highly customizable electromagnetic absorption from the microwave to the optical regimes. Thus far, efficient metamaterial absorbers have been demonstrated at microwave frequencies, with recent efforts aimed at much shorter terahertz and infrared wavelengths. The present infrared absorbers have been constructed from arrays of nanoscale metal resonators with simple circular or cross-shaped geometries, which provide a single band response. In this paper, we demonstrate a conformal metamaterial absorber with a narrow band, polarization-independent absorptivity of >90% over a wide ±50° angular range centered at mid-infrared wavelengths of 3.3 and 3.9 μm. The highly efficient dual-band metamaterial was realized by using a genetic algorithm to identify an array of H-shaped nanoresonators with an effective electric and magnetic response that maximizes absorption in each wavelength band when patterned on a flexible Kapton and Au thin film substrate stack. This conformal metamaterial absorber maintains its absorption properties when integrated onto curved surfaces of arbitrary materials, making it attractive for advanced coatings that suppress the infrared reflection from the protected surface.

Electromagnetic and Microwave Absorption Properties of the Flake-Shaped Pr-Ho-Fe Alloys in the C-Band

NASA Astrophysics Data System (ADS)

Luo, Jialiang; Pan, Shunkang; Qiao, Ziqiang; Cheng, Lichun; Wang, Zhenzhong; Lin, Peihao; Chang, Junqing

2018-01-01

The polycrystalline samples Pr x Ho2- x Fe17 ( x = 0.0, 0.1, 0.2, 0.3, 0.4) were prepared by arc melting and high-energy ball milling method. The influences of Pr substitution on phase structure, morphology, saturation magnetization and electromagnetic parameters were investigated by x-ray diffraction, scanning electron microscopy, vibrating-sample magnetometry and vector network analyzer, respectively. The results show that the particle size increased and the saturation magnetization decreased with increasing Pr content. The minimum absorption peak frequency shifted towards a lower-frequency region with increasing Pr concentration. The minimum RL of Pr0.3Ho1.7Fe17 powder was -41.03 dB at 6.88 GHz with a coating thickness of 2.0 mm. With different thickness of 1.8-2.8 mm, the minimum reflection loss (RL) of Pr0.3Ho1.7Fe17 powder was less than -20 dB in the whole C-band (4-8 GHz). The microwave-absorbing properties of the composite with different weight ratios of Pr0.3Ho1.7Fe17/Co were researched. The microwave-absorbing peaks of the composites shifted to a lower frequency with increasing Co content. The minimum RL of Pr0.3Ho1.7Fe17/Co(10%) was -42.51 dB at 4.72 GHz with a coating thickness of 2.6 mm. This suggests that the Pr-Ho-Fe will be a promising microwave absorption material in higher-gigahertz frequency, especially in the C-band.

Microwave bale moisture sensing: Field trial continued

USDA-ARS?s Scientific Manuscript database

A microwave moisture measurement technique was developed at the USDA, ARS Cotton Production and Processing Research Unit for moisture sensing of cotton bales after the bale press. The technique measures the propagation delay of a microwave signal that is transmitted through the cotton bale. This res...

Microwave bale moisture sensing: Field trial

USDA-ARS?s Scientific Manuscript database

A microwave moisture measurement technique was developed for moisture sensing of cotton bales after the bale press. The technique measures the propagation delay of a microwave signal that is transmitted through the cotton bale. This research conducted a field trial to test the sensor in a commercial...

What band rocks the MTB? (Invited)

NASA Astrophysics Data System (ADS)

Kind, J.; García-Rubio, I.; Gehring, A. U.

2013-12-01

Magnetotactic bacteria (MTB) are a polyphyletic group of bacteria that have been found in marine and lacustrine environments and soils [e.g. 1]. The hallmark of MTB is their intracellular formation of magnetosomes, single-domain ferrimagnetic particles that are aligned in chains. The chain configuration generates a strong magnetic dipole, which is used as magnetic compass to move the MTB into their favorable habit. The term band corresponds to a frequency window of microwaves in the gigahertz (GHz) range. Ferromagnetic resonance (FMR) spectroscopy uses the microwave absorption in a magnetic field to analyze the anisotropy properties and the domain state of magnetic materials. Specific microwave frequency causes absorption in a characteristic magnetic field range. For the investigation of MTB we use S-band (4.02 GHz), X-band (9.47 GHz), and Q-band (34.16 GHz). Experiments on cultured MTB and on sediment samples of Holocene age showed that absorption in X- and Q-band occurs when the sample is in a saturated or nearly saturated state [2, 3]. By contrast, absorption in the S-band appears in lower magnetic fields, where the sample is far from saturation. All FMR spectra show two distinct low-field features that can be assigned to magnetite particles in chains, aligned parallel and perpendicular to the external magnetic field. The detailed separation of the parallel and perpendicular components in the bulk samples is hampered, because of the random orientation of the chains in the sample. The comparison of S-, X-, and Q-band shows that the lower the frequency the better the separation of the components. In the S-band FMR spectroscopy, the separation of chains parallel to the external magnetic field is supported by the internal field of the sample. This field is caused by the remanence that contributes to the external magnetic field to fulfill the resonance condition [3,4]. Considering the different FMR responses, it can be postulated that a lower microwave frequency generally leads to a better resolution of the chain configuration. Finally, for the investigation of geological samples, the application of S-band can be a powerful tool to complement the commonly used X-band FMR spectroscopy, i.e. multiple band rock the MTB. [1] Blakemore R.P., 1975, Magnetotactic bacteria, Science, 190, 377-379 [2] Mastogiacomo G., Fischer H., Garcia-Rubio I., and Gehring A. U., 2010, Ferromagnetic resonance spectroscopic response of magnetic chains in a biological matrix, J. Magn. Magn. Matter, 322, 661-663, doi: 10.1016/j.jmmm.2009.10.035 [3] Gehring A. U., Kind. J., Charilaou M., Garcia-Rubio I., 2011, S-band ferromagnetic resonance spectroscopy and the detection of magnetofossils, J. R. Soc. Interface, 10(80), doi: 10.1098/rsif.2012.0790 [4] Kind J., van Raden U., Garcia-Rubio I., and Gehring A. U., 2012, Rock magnetic techniques complemented by ferromagnetic resonance spectroscopy to analyse a sediment record, Geophys. J. Int., 191, 51-61, doi: 10.1111/j.1365-246X.2012.05620.x

Physical quality characteristics of the microwave-dried breadfruit powders due to different processing conditions

NASA Astrophysics Data System (ADS)

Taruna, I.; Hakim, A. L.; Sutarsi

2018-03-01

Production of breadfruit powder has been an option to make easy its uses in various food processing. Accordingly, there is a need recently to apply advanced drying method, i.e. microwave drying, for improving quality since conventional methods produced highly variable product quality and required longer process. The present work was aimed to study the effect of microwave power and grinding time on physical quality of breadfruit powders. The experiment was done initially by drying breadfruit slices in a microwave dryer at power level of 420, 540, and 720 W and then grinding for 3, 5, and 7 min to get powdery product of less than 80 mesh. The physical quality of breadfruit powders were measured in terms of fineness modulus (FM), average particle size (D), whiteness (WI), total color difference (ΔE), water absorption (Wa), oil absorption (La), bulk density (ρb) and consistency gel (Gc). The results showed that physical quality of powders and its ranged-values included the FM (2.08-2.62), D (0.44-0.68 mm), WI (75.2-77.9), ΔE (7.4-10.5), Wa (5.5-6.2 ml/g), La (0.7-0.9 ml/g), ρb (0.62-0.70 g/cm3) and Gc (41.3-46.8 mm). The experiment revealed that variation of microwave power and grinding time affected significantly the quality of the breadfruit powders. However, microwave power was more dominant factor to affect quality of breadfruit powder in comparison to the grinding time.

Laboratory Evaluation and Application of Microwave Absorption Properties under Simulated Conditions for Planetary Atmospheres

NASA Technical Reports Server (NTRS)

Steffes, Paul G.

2002-01-01

Radio absorptivity data for planetary atmospheres obtained from spacecraft radio occultation experiments, entry probe radio signal absorption measurements, and earth-based or spacecraft-based radio astronomical (emission) observations can be used to infer abundances of microwave absorbing constituents in those atmospheres, as long as reliable information regarding the microwave absorbing properties of potential constituents is available. The use of theoretically-derived microwave absorption properties for such atmospheric constituents, or the use of laboratory measurements of such properties taken under environmental conditions that are significantly different than those of the planetary atmosphere being studied, often leads to significant misinterpretation of available opacity data. Laboratory measurements have shown that the centimeter-wavelength opacity from gaseous phosphine (PH3) under simulated conditions for the outer planets far exceeds that predicted from theory over a wide range of temperatures and pressures. This fundamentally changed the resulting interpretation of Voyager radio occultation data at Saturn and Neptune. It also directly impacts planning and scientific goals for study of Saturn's atmosphere with the Cassini Radio Science Experiment and the Rossini RADAR instrument. The recognition of the need to make such laboratory measurements of simulated planetary atmospheres over a range of temperatures and pressures which correspond to the altitudes probed by both radio occultation experiments and radio astronomical observations, and over a range of frequencies which correspond to those used in both spacecraft entry probe and orbiter (or flyby) radio occultation experiments and radio astronomical observations, has led to the development of a facility at Georgia Tech which is capable of making such measurements. It has been the goal of this investigation to conduct such measurements and to apply the results to a wide range of planetary observations, both spacecraft- and earth-based, in order to determine the identity and abundance profiles of constituents in those planetary atmospheres,

Low-Cost Carbothermal Reduction Preparation of Monodisperse Fe3O4/C Core-Shell Nanosheets for Improved Microwave Absorption.

PubMed

Liu, Yun; Fu, Yiwei; Liu, Lin; Li, Wei; Guan, Jianguo; Tong, Guoxiu

2018-05-16

This paper demonstrates a facile and low-cost carbothermal reduction preparation of monodisperse Fe 3 O 4 /C core-shell nanosheets (NSs) for greatly improved microwave absorption. In this protocol, the redox reaction between sheet-like hematite (α-Fe 2 O 3 ) precursors and acetone under inert atmosphere and elevated temperature generates Fe 3 O 4 /C core-shell NSs with the morphology inheriting from α-Fe 2 O 3 . Thus, Fe 3 O 4 /C core-shell NSs of different sizes ( a) and Fe 3 O 4 /C core-shell nanopolyhedrons are obtained by using different precursors. Benefited from the high crystallinity of the Fe 3 O 4 core and the thin carbon layer, the resultant NSs exhibit high specific saturation magnetization larger than 82.51 emu·g -1 . Simultaneously, the coercivity enhances with the increase of a, suggesting a strong shape anisotropy effect. Furthermore, because of the anisotropy structure and the complementary behavior between Fe 3 O 4 and C, the as-obtained Fe 3 O 4 /C core-shell NSs exhibit strong natural magnetic resonance at a high frequency, enhanced interfacial polarization, and improved impedance matching, ensuring the enhancement of the microwave absorption. The 250 nm NSs-paraffin composites exhibit reflection loss (RL) lower than -20 dB (corresponding to 99% absorption) in a large frequency ( f) range of 2.08-16.40 GHz with a minimum RL of -43.95 dB at f = 3.92 GHz when the thickness is tuned from 7.0 to 1.4 mm, indicating that the Fe 3 O 4 /C core-shell NSs are a good candidate to manufacture high-performance microwave absorbers. Moreover, the as-developed carbothermal reduction method could be applied for the fabrication of other composites based on ferrites and carbon.

Microwave, Millimeter, Submillimeter, and Far Infrared Spectral Databases

NASA Technical Reports Server (NTRS)

Pearson, J. C.; Pickett, H. M.; Drouin, B. J.; Chen, P.; Cohen, E. A.

2002-01-01

The spectrum of most known astrophysical molecules is derived from transitions between a few hundred to a few hundred thousand energy levels populated at room temperature. In the microwave and millimeter wave regions. spectroscopy is almost always performed with traditional microwave techniques. In the submillimeter and far infrared microwave technique becomes progressively more technologically challenging and infrared techniques become more widely employed as the wavelength gets shorter. Infrared techniques are typically one to two orders of magnitude less precise but they do generate all the strong features in the spectrum. With microwave technique, it is generally impossible and rarely necessary to measure every single transition of a molecular species, so careful fitting of quantum mechanical Hamiltonians to the transitions measured are required to produce the complete spectral picture of the molecule required by astronomers. The fitting process produces the most precise data possible and is required in the interpret heterodyne observations. The drawback of traditional microwave technique is that precise knowledge of the band origins of low lying excited states is rarely gained. The fitting of data interpolates well for the range of quantum numbers where there is laboratory data, but extrapolation is almost never precise. The majority of high resolution spectroscopic data is millimeter or longer in wavelength and a very limited number of molecules have ever been studied with microwave techniques at wavelengths shorter than 0.3 millimeters. The situation with infrared technique is similarly dire in the submillimeter and far infrared because the black body sources used are competing with a very significant thermal background making the signal to noise poor. Regardless of the technique used the data must be archived in a way useful for the interpretation of observations.

Resonance of electromagnetic absorption in a dielectric composite based on a high temperature superconductor

NASA Astrophysics Data System (ADS)

Grishin, A. M.; D'Iakonov, V. P.; Mezin, N. I.; Shapovalov, V. A.; Starostiuk, N. Iu.; Iarosh, G. S.

1992-10-01

A dielectric composite has been produced which is characterized by a sufficiently strong dependence of its microwave properties on weak magnetic fields. The composite is based on highly dispersed YBa2Cu3O(7-x) superconducting powder, with paraffin used as the matrix material. Results of a study of the magnetic and microwave properties of the composite are presented.

Activation of boron and recrystallization in Ge preamorphization implant structure of ultra shallow junctions by microwave annealing

NASA Astrophysics Data System (ADS)

Tsai, Ming Han; Wu, Chi-Ting; Lee, Wen-His

2014-04-01

In this study, high-current and low-energy (400 eV) ion implantation and low-temperature microwave annealing were employed to achieve ultra shallow junctions. To use the characteristic of microwave annealing more effectively, two-step microwave annealing was also employed. In the first step annealing, a high-power (2400 W; ˜500 °C) microwave was used to achieve solid-state epitaxial regrowth (SPER) and enhance microwave absorption. In the second step of annealing, unlike in conventional thermal annealing, which requires a higher energy to activate the dopant, a 600 W (˜250 °C) microwave was used to achieve low sheet resistance. The device subjected to two-step microwave annealing at 2400 W for 300 s + 600 W for 600 s has the lowest Vth. It also has the lowest subthreshold swing (SS), which means that it has the highest cap ability to control sub threshold current. In these three devices, the largest Ion/Ioff ratio is 2.203 × 106, and the smallest Ion/Ioff ratio is 2.024 × 106.

[Determination of benzo(alpha)pyrene in food with microwave-assisted extraction].

PubMed

Zhou, Na; Luo, He-Dong; Li, Na; Li, Yao-Qun

2014-03-01

Coupling derivative technique and constant-energy synchronous fluorescence scanning technique, a method of determining benzo[alpha] pyrene in foods by second derivative constant-energy synchronous spectrofluorimetry after microwave-assisted treatment of samples was established using domestic microwave oven. The main factors of influencing the efficiency of microwave extraction were discussed, including the extraction solvent types and amounts, the microwave extraction time, microwave radiation power and cooling time. And the comparison with ultrasonic extraction was made. Low-fat food samples, which were just microwave-extracted with mixed-solvents, could be analyzed immediately by the spectrofluorimetric technique. For high-fat food samples, microwave-assisted saponification and extraction were made at the same time, thus simplifying operation steps and reducing sample analysis time. So the whole sample analysis process could be completed within one hour. This method was simple, rapid and inexpensive. In consequence, it was applied to determine benzo(a)pyrene in food with good reproducibility and the recoveries of benzo(alpha) pyrene ranged from 90.0% to 105.0% for the low fat samples and 83.3% to 94.6% for high-fat samples.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Li, Sucheng; Duan, Qian; Li, Shuo

We experimentally demonstrate that perfect electromagnetic absorption can be realized in the one-atom thick graphene. Employing coherent illumination in the waveguide system, the absorbance of the unpatterned graphene monolayer is observed to be greater than 94% over the microwave X-band, 7–13 GHz, and to achieve a full absorption, >99% in experiment, at ∼8.3 GHz. In addition, the absorption characteristic manifests equivalently a wide range of incident angle. The experimental results agree very well with the theoretical calculations. Our work accomplishes the broadband, wide-angle, high-performance absorption in the thinnest material with simple configuration.

The Cassini mission: Infrared and microwave spectroscopic measurements

NASA Technical Reports Server (NTRS)

Kunde, V. G.

1989-01-01

The Cassini Orbiter and Titan Probe model payloads include a number of infrared and microwave instruments. This document describes: (1) the fundamental scientific objectives for Saturn and Titan which can be addressed by infrared and microwave instrumentation, (2) the instrument requirements and the accompanying instruments, and (3) the synergism resulting from the comprehensive coverage of the total infrared and microwave spectrum by the complement of individual instruments. The baseline consists of four instruments on the orbiter and two on the Titan probe. The orbiter infrared instruments are: (1) a microwave spectrometer and radiometer; (2) a far to mid-infrared spectrometer; (3) a pressure modulation gas correlation spectrometer, and (4) a near-infrared grating spectrometer. The two Titan probe infrared instruments are: (1) a near-infrared instrument, and (2) a tunable diode laser infrared absorption spectrometer and nephelometer.

Microwave-field-driven acoustic modes in DNA.

PubMed Central

Edwards, G S; Davis, C C; Saffer, J D; Swicord, M L

1985-01-01

The direct coupling of a microwave field to selected DNA molecules is demonstrated using standard dielectrometry. The absorption is resonant with a typical lifetime of 300 ps. Such a long lifetime is unexpected for DNA in aqueous solution at room temperature. Resonant absorption at fundamental and harmonic frequencies for both supercoiled circular and linear DNA agrees with an acoustic mode model. Our associated acoustic velocities for linear DNA are very close to the acoustic velocity of the longitudinal acoustic mode independently observed on DNA fibers using Brillouin spectroscopy. The difference in acoustic velocities for supercoiled circular and linear DNA is discussed in terms of solvent shielding of the nonbonded potentials in DNA. Images FIGURE 5 FIGURE 6 FIGURE 7 PMID:3893557

Enhanced microwave absorbing performance of CoNi alloy nanoparticles anchored on a spherical carbon monolith.

PubMed

Li, Na; Hu, Changwen; Cao, Minhua

2013-05-28

CoNi alloy nanoparticles anchored on a spherical carbon monolith (CoNi-C) were prepared by a solvothermal route and subsequent heat treatment without any templates. Their permittivity and permeability behaviors were studied in the frequency range of 2-18 GHz. The CoNi-C composites showed the best microwave absorbing performances compared to those of Co-C and Ni-C. The maximum reflection loss of the CoNi-C nanocomposites can reach -50.2 dB at 7.7 GHz with samples of 4 mm in thickness, better than that of the Ni-C composites, while the Co-C composites showed almost no absorption at all. The absorption mechanism of the three absorbents was also discussed.

An ultralight and thin metasurface for radar-infrared bi-stealth applications

NASA Astrophysics Data System (ADS)

Zhang, C.; Yang, J.; Yuan, W.; Zhao, J.; Dai, J. Y.; Guo, T. C.; Liang, J.; Xu, G. Y.; Cheng, Q.; Cui, T. J.

2017-11-01

We present a thin metasurface with large microwave absorptivity and low infrared emissivity simultaneously. By properly tuning the resonance peaks and impedance of the meta-atom, broadband microwave absorptivity greater than 90% from 8.2 to 16.0 GHz is achieved. In the meantime, owing to large coverage of periodic metal patches on the top surface, low infrared emissivity is exhibited in the infrared region (IR) of 8 µm-14 µm. The excellent agreement between numerical simulation and experimental result demonstrates the good performance of the proposed metasurface. Due to the usage of polymethacrylimide (PMI) and polyethylene terephthalate (PET) as the substrate, the metasurface is especially advantageous for the light weight, making it a favorite in real engineering applications.

Classical scattering calculations for diatomic molecules: A general procedure and application to the microwave spectrum O2

NASA Technical Reports Server (NTRS)

Mingelgrin, U.

1972-01-01

Many properties of gaseous systems such as electromagnetic absorption and emission, sound dispersion and absorption, may be elucidated if the nature of collisions between the particles in the system is understood. A procedure for the calculation of the classical trajectories of two interacting diatomic molecules is described. The dynamics of the collision will be assumed to be that of two rigid rotors moving in a specified potential. The actual outcome of a representative sample of many trajectories at 298K was computed, and the use of these values at any temperature for calculations of various molecular properties will be described. Calculations performed for the O2 microwave spectrum are given to demonstrate the use of the procedure described.

Double-negative metamaterial for mobile phone application

NASA Astrophysics Data System (ADS)

Hossain, M. I.; Faruque, M. R. I.; Islam, M. T.

2017-01-01

In this paper, a new design and analysis of metamaterial and its applications to modern handset are presented. The proposed metamaterial unit-cell design consists of two connected square spiral structures, which leads to increase the effective media ratio. The finite instigation technique based on Computer Simulation Technology Microwave Studio is utilized in this investigation, and the measurement is taken in an anechoic chamber. A good agreement is observed among simulated and measured results. The results indicate that the proposed metamaterial can successfully cover cellular phone frequency bands. Moreover, the uses of proposed metamaterial in modern handset antennas are also analyzed. The results reveal that the proposed metamaterial attachment significantly reduces specific absorption rate values without reducing the antenna performances.

A Brief Review of Recent Superconductivity Research at NIST

PubMed Central

Lundy, D. R.; Swartzendruber, L. J.; Bennett, L. H.

1989-01-01

A brief overview of recent superconductivity research at NIST is presented. Emphasis is placed on the new high-temperature oxide superconductors, though mention is made of important work on low-temperature superconductors, and a few historical notes are included. NIST research covers a wide range of interests. For the new high-temperature superconductors, research activities include determination of physical properties such as elastic constants and electronic structure, development of new techniques such as magnetic-field modulated microwave-absorption and determination of phase diagrams and crystal structure. For the low-temperature superconductors, research spans studying the effect of stress on current density to the fabrication of a new Josephson junction voltage standard. PMID:28053408

Numerical 3D modeling of heat transfer in human tissues for microwave radiometry monitoring of brown fat metabolism

NASA Astrophysics Data System (ADS)

Rodrigues, Dario B.; Maccarini, Paolo F.; Salahi, Sara; Colebeck, Erin; Topsakal, Erdem; Pereira, Pedro J. S.; Limão-Vieira, Paulo; Stauffer, Paul R.

2013-02-01

Background: Brown adipose tissue (BAT) plays an important role in whole body metabolism and could potentially mediate weight gain and insulin sensitivity. Although some imaging techniques allow BAT detection, there are currently no viable methods for continuous acquisition of BAT energy expenditure. We present a non-invasive technique for long term monitoring of BAT metabolism using microwave radiometry. Methods: A multilayer 3D computational model was created in HFSSTM with 1.5 mm skin, 3-10 mm subcutaneous fat, 200 mm muscle and a BAT region (2-6 cm3) located between fat and muscle. Based on this model, a log-spiral antenna was designed and optimized to maximize reception of thermal emissions from the target (BAT). The power absorption patterns calculated in HFSSTM were combined with simulated thermal distributions computed in COMSOL® to predict radiometric signal measured from an ultra-low-noise microwave radiometer. The power received by the antenna was characterized as a function of different levels of BAT metabolism under cold and noradrenergic stimulation. Results: The optimized frequency band was 1.5-2.2 GHz, with averaged antenna efficiency of 19%. The simulated power received by the radiometric antenna increased 2-9 mdBm (noradrenergic stimulus) and 4-15 mdBm (cold stimulus) corresponding to increased 15-fold BAT metabolism. Conclusions: Results demonstrated the ability to detect thermal radiation from small volumes (2-6 cm3) of BAT located up to 12 mm deep and to monitor small changes (0.5 °C) in BAT metabolism. As such, the developed miniature radiometric antenna sensor appears suitable for non-invasive long term monitoring of BAT metabolism.

Spin-Label CW Microwave Power Saturation and Rapid Passage with Triangular Non-Adiabatic Rapid Sweep (NARS) and Adiabatic Rapid Passage (ARP) EPR Spectroscopy

PubMed Central

Kittell, Aaron W.; Hyde, James S.

2015-01-01

Non-adiabatic rapid passage (NARS) electron paramagnetic resonance (EPR) spectroscopy was introduced by Kittell, A.W., Camenisch, T.G., Ratke, J.J. Sidabras, J.W., Hyde, J.S., 2011 as a general purpose technique to collect the pure absorption response. The technique has been used to improve sensitivity relative to sinusoidal magnetic field modulation, increase the range of inter-spin distances that can be measured under near physiological conditions, and enhance spectral resolution in copper (II) spectra. In the present work, the method is extended to CW microwave power saturation of spin-labeled T4 Lysozyme (T4L). As in the cited papers, rapid triangular sweep of the polarizing magnetic field was superimposed on slow sweep across the spectrum. Adiabatic rapid passage (ARP) effects were encountered in samples undergoing very slow rotational diffusion as the triangular magnetic field sweep rate was increased. The paper reports results of variation of experimental parameters at the interface of adiabatic and non-adiabatic rapid sweep conditions. Comparison of the forward (up) and reverse (down) triangular sweeps is shown to be a good indicator of the presence of rapid passage effects. Spectral turning points can be distinguished from spectral regions between turning points in two ways: differential microwave power saturation and differential passage effects. Oxygen accessibility data are shown under NARS conditions that appear similar to conventional field modulation data. However, the sensitivity is much higher, permitting, in principle, experiments at substantially lower protein concentrations. Spectral displays were obtained that appear sensitive to rotational diffusion in the range of rotational correlation times of 10−3 to 10−7 s in a manner that is analogous to saturation transfer spectroscopy. PMID:25917132

Numerical 3D modeling of heat transfer in human tissues for microwave radiometry monitoring of brown fat metabolism

PubMed Central

Rodrigues, Dario B.; Maccarini, Paolo F.; Salahi, Sara; Colebeck, Erin; Topsakal, Erdem; Pereira, Pedro J. S.; Limão-Vieira, Paulo; Stauffer, Paul R.

2013-01-01

Background Brown adipose tissue (BAT) plays an important role in whole body metabolism and could potentially mediate weight gain and insulin sensitivity. Although some imaging techniques allow BAT detection, there are currently no viable methods for continuous acquisition of BAT energy expenditure. We present a non-invasive technique for long term monitoring of BAT metabolism using microwave radiometry. Methods A multilayer 3D computational model was created in HFSS™ with 1.5 mm skin, 3–10 mm subcutaneous fat, 200 mm muscle and a BAT region (2–6 cm3) located between fat and muscle. Based on this model, a log-spiral antenna was designed and optimized to maximize reception of thermal emissions from the target (BAT). The power absorption patterns calculated in HFSS™ were combined with simulated thermal distributions computed in COMSOL® to predict radiometric signal measured from an ultra-low-noise microwave radiometer. The power received by the antenna was characterized as a function of different levels of BAT metabolism under cold and noradrenergic stimulation. Results The optimized frequency band was 1.5–2.2 GHz, with averaged antenna efficiency of 19%. The simulated power received by the radiometric antenna increased 2–9 mdBm (noradrenergic stimulus) and 4–15 mdBm (cold stimulus) corresponding to increased 15-fold BAT metabolism. Conclusions Results demonstrated the ability to detect thermal radiation from small volumes (2–6 cm3) of BAT located up to 12 mm deep and to monitor small changes (0.5 °C) in BAT metabolism. As such, the developed miniature radiometric antenna sensor appears suitable for non-invasive long term monitoring of BAT metabolism. PMID:24244831

Numerical 3D modeling of heat transfer in human tissues for microwave radiometry monitoring of brown fat metabolism.

PubMed

Rodrigues, Dario B; Maccarini, Paolo F; Salahi, Sara; Colebeck, Erin; Topsakal, Erdem; Pereira, Pedro J S; Limão-Vieira, Paulo; Stauffer, Paul R

2013-02-26

Brown adipose tissue (BAT) plays an important role in whole body metabolism and could potentially mediate weight gain and insulin sensitivity. Although some imaging techniques allow BAT detection, there are currently no viable methods for continuous acquisition of BAT energy expenditure. We present a non-invasive technique for long term monitoring of BAT metabolism using microwave radiometry. A multilayer 3D computational model was created in HFSS™ with 1.5 mm skin, 3-10 mm subcutaneous fat, 200 mm muscle and a BAT region (2-6 cm 3 ) located between fat and muscle. Based on this model, a log-spiral antenna was designed and optimized to maximize reception of thermal emissions from the target (BAT). The power absorption patterns calculated in HFSS™ were combined with simulated thermal distributions computed in COMSOL® to predict radiometric signal measured from an ultra-low-noise microwave radiometer. The power received by the antenna was characterized as a function of different levels of BAT metabolism under cold and noradrenergic stimulation. The optimized frequency band was 1.5-2.2 GHz, with averaged antenna efficiency of 19%. The simulated power received by the radiometric antenna increased 2-9 mdBm (noradrenergic stimulus) and 4-15 mdBm (cold stimulus) corresponding to increased 15-fold BAT metabolism. Results demonstrated the ability to detect thermal radiation from small volumes (2-6 cm 3 ) of BAT located up to 12 mm deep and to monitor small changes (0.5 °C) in BAT metabolism. As such, the developed miniature radiometric antenna sensor appears suitable for non-invasive long term monitoring of BAT metabolism.

Quantitative analyses of tartaric acid based on terahertz time domain spectroscopy

NASA Astrophysics Data System (ADS)

Cao, Binghua; Fan, Mengbao

2010-10-01

Terahertz wave is the electromagnetic spectrum situated between microwave and infrared wave. Quantitative analysis based on terahertz spectroscopy is very important for the application of terahertz techniques. But how to realize it is still under study. L-tartaric acid is widely used as acidulant in beverage, and other food, such as soft drinks, wine, candy, bread and some colloidal sweetmeats. In this paper, terahertz time-domain spectroscopy is applied to quantify the tartaric acid. Two methods are employed to process the terahertz spectra of different samples with different content of tartaric acid. The first one is linear regression combining correlation analysis. The second is partial least square (PLS), in which the absorption spectra in the 0.8-1.4THz region are used to quantify the tartaric acid. To compare the performance of these two principles, the relative error of the two methods is analyzed. For this experiment, the first method does better than the second one. But the first method is suitable for the quantitative analysis of materials which has obvious terahertz absorption peaks, while for material which has no obvious terahertz absorption peaks, the second one is more appropriate.

Metasurface Salisbury screen: achieving ultra-wideband microwave absorption.

PubMed

Zhou, Ziheng; Chen, Ke; Zhao, Junming; Chen, Ping; Jiang, Tian; Zhu, Bo; Feng, Yijun; Li, Yue

2017-11-27

The metasurfaces have recently been demonstrated to provide full control of the phase responses of electromagnetic (EM) wave scattering over subwavelength scales, enabling a wide range of practical applications. Here, we propose a comprehensive scheme for the efficient and flexible design of metasurface Salisbury screen (MSS) capable of absorbing the impinging EM wave in an ultra-wide frequency band. We show that properly designed reflective metasurface can be used to substitute the metallic ground of conventional Salisbury screen for generating diverse resonances in a desirable way, thus providing large controllability over the absorption bandwidth. Based on this concept, we establish an equivalent circuit model to qualitatively analysis the resonances in MSS and design algorithms to optimize the overall performance of the MSS. Experiments have been carried out to demonstrate that the absorption bandwidth from 6 GHz to 30 GHz with an efficiency higher than 85% can be achieved by the proposal, which is apparently much larger than that of conventional Salisbury screen (7 GHz - 17 GHz). The proposed concept of MSS could offer opportunities for flexibly designing thin electromagnetic absorbers with simultaneously ultra-wide bandwidth, polarization insensitivity, and wide incident angle, exhibiting promising potentials for many applications such as in EM compatibility, stealth technique, etc.

Magnetic graphene enabled tunable microwave absorber via thermal control.

PubMed

Quan, L; Qin, F X; Li, Y H; Estevez, D; Fu, G J; Wang, H; Peng, H-X

2018-06-15

By synthesizing nitrogen-doped graphene (NG) via a facile thermal annealing method, a fine control of the amount and location of doped nitrogen as well as the oxygen-containing functional groups is achieved with varying annealing temperature. The favorable magnetic properties have been achieved for N-doped rGO samples obtained at two temperatures of all NG samples, i.e., 500 °C and 900 °C with saturation magnetization of 0.63 emu g -1 and 0.67 emu g -1 at 2 K, respectively. This is attributed to the optimized competition of the N-doping and reduction process at 500 °C and the dominated reduction process at 900 °C. NG obtained at 300 °C affords the best overall absorbing performance: when the absorber thickness is 3.0 mm, the maximum absorption was -24.6 dB at 8.51 GHz, and the absorption bandwidth was 4.89 GHz (7.55-12.44 GHz) below -10 dB. It owes its large absorbing intensity to the good impedance match and significant dielectric loss. The broad absorption bandwidth benefits from local fluctuations of dielectric responses contributed by competing mechanisms. Despite the significant contribution from materials loss to the absorption, the one quarter-wavelength model is found to be responsible for the reflection loss peak positions. Of particular significance is that an appropriate set of electromagnetic parameters associated with reasonable reduction is readily accessible by convenient control of annealing temperature to modulate the microwave absorbing features of graphene. Thus, NG prepared by thermal annealing promises to be a highly efficient microwave absorbent.

Magnetic graphene enabled tunable microwave absorber via thermal control

NASA Astrophysics Data System (ADS)

Quan, L.; Qin, F. X.; Li, Y. H.; Estevez, D.; Fu, G. J.; Wang, H.; Peng, H.-X.

2018-06-01

By synthesizing nitrogen-doped graphene (NG) via a facile thermal annealing method, a fine control of the amount and location of doped nitrogen as well as the oxygen-containing functional groups is achieved with varying annealing temperature. The favorable magnetic properties have been achieved for N-doped rGO samples obtained at two temperatures of all NG samples, i.e., 500 °C and 900 °C with saturation magnetization of 0.63 emu g‑1 and 0.67 emu g‑1 at 2 K, respectively. This is attributed to the optimized competition of the N-doping and reduction process at 500 °C and the dominated reduction process at 900 °C. NG obtained at 300 °C affords the best overall absorbing performance: when the absorber thickness is 3.0 mm, the maximum absorption was ‑24.6 dB at 8.51 GHz, and the absorption bandwidth was 4.89 GHz (7.55–12.44 GHz) below ‑10 dB. It owes its large absorbing intensity to the good impedance match and significant dielectric loss. The broad absorption bandwidth benefits from local fluctuations of dielectric responses contributed by competing mechanisms. Despite the significant contribution from materials loss to the absorption, the one quarter-wavelength model is found to be responsible for the reflection loss peak positions. Of particular significance is that an appropriate set of electromagnetic parameters associated with reasonable reduction is readily accessible by convenient control of annealing temperature to modulate the microwave absorbing features of graphene. Thus, NG prepared by thermal annealing promises to be a highly efficient microwave absorbent.

Microwave Heating of Synthetic Skin Samples for Potential Treatment of Gout Using the Metal-Assisted and Microwave-Accelerated Decrystallization Technique

PubMed Central

2016-01-01

Physical stability of synthetic skin samples during their exposure to microwave heating was investigated to demonstrate the use of the metal-assisted and microwave-accelerated decrystallization (MAMAD) technique for potential biomedical applications. In this regard, optical microscopy and temperature measurements were employed for the qualitative and quantitative assessment of damage to synthetic skin samples during 20 s intermittent microwave heating using a monomode microwave source (at 8 GHz, 2–20 W) up to 120 s. The extent of damage to synthetic skin samples, assessed by the change in the surface area of skin samples, was negligible for microwave power of ≤7 W and more extensive damage (>50%) to skin samples occurred when exposed to >7 W at initial temperature range of 20–39 °C. The initial temperature of synthetic skin samples significantly affected the extent of change in temperature of synthetic skin samples during their exposure to microwave heating. The proof of principle use of the MAMAD technique was demonstrated for the decrystallization of a model biological crystal (l-alanine) placed under synthetic skin samples in the presence of gold nanoparticles. Our results showed that the size (initial size ∼850 μm) of l-alanine crystals can be reduced up to 60% in 120 s without damage to synthetic skin samples using the MAMAD technique. Finite-difference time-domain-based simulations of the electric field distribution of an 8 GHz monomode microwave radiation showed that synthetic skin samples are predicted to absorb ∼92.2% of the microwave radiation. PMID:27917407

High quality Y-type hexaferrite thick films for microwave applications by an economical and environmentally benign crystal growth technique

DOE Office of Scientific and Technical Information (OSTI.GOV)

Hu, Bolin; Chen, Yajie, E-mail: y.chen@neu.edu; Gillette, Scott

2014-02-17

Thick barium hexaferrite Ba{sub 2}Zn{sub 2}Fe{sub 12}O{sub 22} (i.e., Zn{sub 2}Y) films having thicknesses of ∼100 μm were epitaxially grown on MgO (111) substrates using an environmentally benign ferrite-salt mixture by vaporizing the salt. X-ray diffraction pole figure analyses showed (00l) crystallographic alignment with little in plane dispersion confirming epitaxial growth. Saturation magnetization, 4πM{sub s}, was measured for as-grown films to be 2.51 ± 0.1 kG with an out of plane magnetic anisotropy field H{sub A} of 8.9 ± 0.1 kOe. Ferromagnetic resonance linewidth, as the peak-to-peak power absorption derivative at 9.6 GHz, was measured to be 62 Oe. These properties demonstrate a rapid, convenient, cost-effective, and nontoxic methodmore » of growing high quality thick crystalline ferrite films which could be used widely for microwave device applications.« less

Synthesis, structure and electromagnetic properties of Mn-Zn ferrite by sol-gel combustion technique

NASA Astrophysics Data System (ADS)

Wang, Wenjie; Zang, Chongguang; Jiao, Qingjie

2014-01-01

The electromagnetic absorbing behaviors of a thin coating fabricated by mixing Mn-Zn ferrite with epoxy resin (EP) were studied. The spinel ferrites Mn1-xZnxFe2O4 (x=0.2, 0.5 and 0.8) were synthesized with citrate acid as complex agent by sol-gel combustion method. The microstructure and surface morphology of Mn-Zn ferrite powders were characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM). The complex permittivity and complex permeability of the fabricated ferrite/EP composites were investigated in terms of their contributions to the absorbing properties in the low frequency (10 MHz to 1 GHz). The microwave absorption of the prepared ferrite/EP composites could be tailored by matching the dielectric loss and magnetic loss and by controlling the doped metal ratio. The composites with the ferrite composition x=0.2 are found to show higher reflection loss compared with the composites with other compositions. It is proposed that the prepared composites can potentially be applied in electromagnetic microwave absorbing field.

Observation of electromagnetically induced transparency and absorption in Yttrium Iron Garnet loaded split ring resonator

NASA Astrophysics Data System (ADS)

Tay, Z. J.; Soh, W. T.; Ong, C. K.

2018-04-01

In this paper, we propose a new method of controlling microwave transmission from Electromagnetically Induced Absorption (EIA) to Electromagnetically Induced Transparency (EIT). EIA describes the state where the system strongly absorbs microwaves, whereas EIT describes the state in which the system is transparent to microwaves. Control is achieved via coupling of the 3 GHz photon mode of a metamaterial Split Ring Resonator (SRR) to the spin wave magnon modes of a Yttrium Iron Garnet (YIG) bulk. The system is described by a 2-body interaction matrix with an additional fitting parameter τ which takes into account the fact that the microstrip feed line could excite the SRR as well as the YIG. The parameter τ reveals the effect of geometry and shielding on the coupling behaviour and gives rise to unique physics. In low τ (τ ⩽ 2) configurations, only EIT is reported. However, in high τ (τ ≈ 10) configurations, EIA is reported. Furthermore, we report that the system can be easily changed from a low τ to high τ configuration by shielding the SRR from the microstrip with a thin metal piece. Varying the τ parameter through shielding is thus proposed as a new method of controlling the microwave transmission at the coupling region.

Determination of total arsenic in fish by hydride-generation atomic absorption spectrometry: method validation, traceability and uncertainty evaluation

NASA Astrophysics Data System (ADS)

Nugraha, W. C.; Elishian, C.; Ketrin, R.

2017-03-01

Fish containing arsenic compound is one of the important indicators of arsenic contamination in water monitoring. The high level of arsenic in fish is due to absorption through food chain and accumulated in their habitat. Hydride generation (HG) coupled with atomic absorption spectrometric (AAS) detection is one of the most popular techniques employed for arsenic determination in a variety of matrices including fish. This study aimed to develop a method for the determination of total arsenic in fish by HG-AAS. The method for sample preparation from American of Analytical Chemistry (AOAC) Method 999.10-2005 was adopted for acid digestion using microwave digestion system and AOAC Method 986.15 - 2005 for dry ashing. The method was developed and validated using Certified Reference Material DORM 3 Fish Protein for trace metals for ensuring the accuracy and the traceability of the results. The sources of uncertainty of the method were also evaluated. By using the method, it was found that the total arsenic concentration in the fish was 45.6 ± 1.22 mg.Kg-1 with a coverage factor of equal to 2 at 95% of confidence level. Evaluation of uncertainty was highly influenced by the calibration curve. This result was also traceable to International Standard System through analysis of Certified Reference Material DORM 3 with 97.5% of recovery. In summary, it showed that method of preparation and HG-AAS technique for total arsenic determination in fish were valid and reliable.

Electrical, Magnetic and Microwave Absorption Properties of M-type Barium Hexaferrites (BaFe12-2x CoxNixO19)

NASA Astrophysics Data System (ADS)

Susilawati; Doyan, A.; Khair, H.; Taufik, M.; Wahyudi

2018-04-01

M-type barium hexaferrites synthesis with Co-Ni doping ion (BaFe12-2x CoxNixO19) based on natural iron sand of Loang Balok beach, Lombok, Indonesia, to be applied as a microwave absorbent material using co-precipitation method. The materials used in the synthesis process are magnetite minerals (Fe2O3 and Fe3O4), 12M HCl, NH4OH 37%, CoCl2.6H2O and NiCl2.6H2O. This research to investigate the effect of doping ion concentration variation (x = 0.0, 0.6 and 1.0) and calcination temperature (T = 80, 600, and 800°C) on electrical and magnetic properties and microwave absorption as well. The samples were characterized using Vibrating Sample Magnetometer (VSM) and Network Vector Analyzer (VNA). The result from VSM showed that the coercivity value decreased when doping ion concentration and calcination temperature increased (0.151 Tesla at 600°C for x = 0.0 and 0.044 Tesla at 800°C for x = 1.0. The value of magnetic saturation and the magnetic remanence increased with increasing ion concentration (Ms = 0.327 emu/g at x = 0.0 increased to 35.4 emu/g at x = 1.0) and Mr = 0.148 emu/g for x = 0.0 increased to 15.6 emu/g at x=1.0, this indicates that the sample has been soft magnetic. The result from VNA showed that the electrical conductivity values measured in the range 8.0-15.0 GHz indicate that the sample is a semiconductor (6.149 x 10-6 -5.975 x 10-4 S/cm). It also showed that the microwave absorption properties increased at higher concentration of doping ions and the calcination temperature would increase the value of Reflection Loss (RL). The maximum RL value of the sample is -14.47 dB at 12.38 GHz, and the absorption coefficient of 96.43%. These results indicate that the BaFe12-2x CoxNixO19 sample can be applied as a microwave absorbent material on X-band to Ku-band frequency.

Feasibility of reading LiF thermoluminescent dosimeters by electron spin resonance

NASA Astrophysics Data System (ADS)

Breen, S. L.; Battista, J. J.

1999-08-01

Lithium fluoride is a commonly used solid state dosimeter. During irradiation, electrons and holes become trapped in crystal imperfections; thermoluminescence dosimetry measures their thermally induced recombination. Electron paramagnetic resonance (EPR) spectroscopy can be used to measure the resonant absorption of microwaves by the unpaired electrons trapped in LiF. In an effort to extend the use of LiF dosimeters to smaller sizes and to the harsh environments encountered in internal dosimetry, EPR was evaluated as an alternative technique to read the radiation dose delivered to TLD-100 dosimeters. TLD-100 rods were irradiated with a 60Co source to doses of 10 Gy to 100 Gy. A radiation-induced signal (with a g-value of 2.002) could be detected only at liquid nitrogen temperatures at doses above 20 Gy. The EPR spectrum of irradiated LiF contains three components, one of which correlates positively with dose. However, the low sensitivity of the technique, and difficulty in interpreting the EPR spectrum from polycrystalline dosimeters, preclude its use as a dosimetry technique.

Feasibility of reading LiF thermoluminescent dosimeters by electron spin resonance.

PubMed

Breen, S L; Battista, J J

1999-08-01

Lithium fluoride is a commonly used solid state dosimeter. During irradiation, electrons and holes become trapped in crystal imperfections; thermoluminescence dosimetry measures their thermally induced recombination. Electron paramagnetic resonance (EPR) spectroscopy can be used to measure the resonant absorption of microwaves by the unpaired electrons trapped in LiF. In an effort to extend the use of LiF dosimeters to smaller sizes and to the harsh environments encountered in internal dosimetry, EPR was evaluated as an alternative technique to read the radiation dose delivered to TLD-100 dosimeters. TLD-100 rods were irradiated with a 60Co source to doses of 10 Gy to 100 Gy. A radiation-induced signal (with a g-value of 2.002) could be detected only at liquid nitrogen temperatures at doses above 20 Gy. The EPR spectrum of irradiated LiF contains three components, one of which correlates positively with dose. However, the low sensitivity of the technique, and difficulty in interpreting the EPR spectrum from polycrystalline dosimeters, preclude its use as a dosimetry technique.

Safety and quality of food contact materials. Part 1: evaluation of analytical strategies to introduce migration testing into good manufacturing practice.

PubMed

Feigenbaum, A; Scholler, D; Bouquant, J; Brigot, G; Ferrier, D; Franzl, R; Lillemarktt, L; Riquet, A M; Petersen, J H; van Lierop, B; Yagoubi, N

2002-02-01

The results of a research project (EU AIR Research Programme CT94-1025) aimed to introduce control of migration into good manufacturing practice and into enforcement work are reported. Representative polymer classes were defined on the basis of chemical structure, technological function, migration behaviour and market share. These classes were characterized by analytical methods. Analytical techniques were investigated for identification of potential migrants. High-temperature gas chromatography was shown to be a powerful method and 1H-magnetic resonance provided a convenient fingerprint of plastic materials. Volatile compounds were characterized by headspace techniques, where it was shown to be essential to differentiate volatile compounds desorbed from those generated during the thermal desorption itself. For metal trace analysis, microwave mineralization followed by atomic absorption was employed. These different techniques were introduced into a systematic testing scheme that is envisaged as being suitable both for industrial control and for enforcement laboratories. Guidelines will be proposed in the second part of this paper.

H-modulated microwave absorption and resistive transition in the high- Tc superconductor YBa 2Cu 3O 7

NASA Astrophysics Data System (ADS)

Buluggiu, E.; Vera, A.; Amoretti, G.

1990-11-01

The derivative microwave absorption near Tc in presence of a sufficiently high field ( H⩾1 kOe) is related to the temperature variation of resistivity. This idea, originally proposed by Kim et al. (1988), is extended to take into account the effects of the anomalous resistive tail by using the thermoactivated flux-creep model proposed by Tinkham (1988). This gives a simple explanation for some relevant features observed in the temperature behaviour of the ESR absorption, as the asymmetry of the peak at Tc, with the long tail extending toward low temperatures, and the field dependence of height and linewidth, for which the model provides H-1 and H2/3 behaviour, respectively, ESR data on YBa 2Cu 3O 7 powder are in satisfactory agreement with this picture, when the role of the intrinsic 2D-character of this compound is properly taken into account. This allows us to deduce consistent values for the parameters a‖ and a⊥ of the anisotropic resistivity.

Enhanced absorption of microwave radiations through flexible polyvinyl alcohol-carbon black/barium hexaferrite composite films

NASA Astrophysics Data System (ADS)

Kumar, Sushil; Datt, Gopal; Santhosh Kumar, A.; Abhyankar, A. C.

2016-10-01

Flexible microwave absorber composite films of carbon black (CB)/barium hexaferrite nano-discs (BaF) in polyvinyl alcohol (PVA) matrix, fabricated by gel casting, exhibit ˜99.5% attenuation of electromagnetic waves in the entire 8-18 GHz (X and Ku-band) range. The X-ray diffraction and Raman spectroscopy studies confirm the formation of CB-BaF-PVA composite films. The electromagnetic absorption properties of composite films are found to be enhanced with CB content due to the synergetic effect of multiple dielectric and magnetic losses. The 25 wt. % CB grafted PVA-BaF flexible composite films with a thickness of ˜ 2 mm exhibit effective electromagnetic shielding of 23.6 dB with a dominant contribution from absorption mechanism (SEA ˜ 21 dB). The dielectric properties of composite films are further discussed by using the Debye model. The detailed analysis reveals that major contribution to dielectric losses is from dipolar and interfacial polarizations, whereas magnetic losses are predominantly from domain wall displacement.

Ultra-Thin Multi-Band Polarization-Insensitive Microwave Metamaterial Absorber Based on Multiple-Order Responses Using a Single Resonator Structure

PubMed Central

Cheng, Zheng Ze; Mao, Xue Song; Gong, Rong Zhou

2017-01-01

We design an ultra-thin multi-band polarization-insensitive metamaterial absorber (MMA) using a single circular sector resonator (CSR) structure in the microwave region. Simulated results show that the proposed MMA has three distinctive absorption peaks at 3.35 GHz, 8.65 GHz, and 12.44 GHz, with absorbance of 98.8%, 99.7%, and 98.3%, respectively, which agree well with an experiment. Simulated surface current distributions of the unit-cell structure reveal that the triple-band absorption mainly originates from multiple-harmonic magnetic resonance. The proposed triple-band MMA can remain at a high absorption level for all polarization of both transverse-electric (TE) and transverse-magnetic (TM) modes under normal incidence. Moreover, by further optimizing the geometric parameters of the CSRs, four-band and five-band MMAs can also be obtained. Thus, our design will have potential application in detection, sensing, and stealth technology. PMID:29077036

Spectroscopic Studies on the Effect of Some Ferrocene Derivatives in the Formation of Silver Nanoparticles.

PubMed

Sanyal, Manik Kumar; Biswas, Bipul; Chowdhury, Avijit; Mallik, Biswanath

2016-06-01

Silver nanoparticles were prepared by microwave assisted method using silver nitrate as precursor in the presence of some ferrocene derivatives. The formation of the silver nanoparticles was monitored using UV-Vis spectroscopy. The UV-Vis spectroscopy revealed the formation of silver nanoparticles by exhibiting typical surface plasmon absorption band. The position of plasmon band (406-429 nm) was observed to depend on the nature of a particular ferrocene derivative used. TEM images indicated that the nanoparticles were spherical in shape and well-dispersed. Quantum dots (3.2 nm) were prepared by using ferrocenecarboxylic acid. The surface plasmon absorption band has shown red shift with increasing concentration of ferrocene derivative. For different duration of microwave heating time, intensity of absorption spectra in general was found to increase except in presence of ferrocene carbaldehyde where it decreased. Time-dependent spectra have indicated almost stable position of the surface plasmon band with increasing time of observation confirming that the as prepared silver nanoparticles did not aggregate with lapse of time.

Porous Graphene Microflowers for High-Performance Microwave Absorption

NASA Astrophysics Data System (ADS)

Chen, Chen; Xi, Jiabin; Zhou, Erzhen; Peng, Li; Chen, Zichen; Gao, Chao

2018-06-01

Graphene has shown great potential in microwave absorption (MA) owing to its high surface area, low density, tunable electrical conductivity and good chemical stability. To fully realize graphene's MA ability, the microstructure of graphene should be carefully addressed. Here we prepared graphene microflowers (Gmfs) with highly porous structure for high-performance MA filler material. The efficient absorption bandwidth (reflection loss ≤ -10 dB) reaches 5.59 GHz and the minimum reflection loss is up to -42.9 dB, showing significant increment compared with stacked graphene. Such performance is higher than most graphene-based materials in the literature. Besides, the low filling content (10 wt%) and low density (40-50 mg cm-3) are beneficial for the practical applications. Without compounding with magnetic materials or conductive polymers, Gmfs show outstanding MA performance with the aid of rational microstructure design. Furthermore, Gmfs exhibit advantages in facile processibility and large-scale production compared with other porous graphene materials including aerogels and foams.

EBG Based Microstrip Patch Antenna for Brain Tumor Detection via Scattering Parameters in Microwave Imaging System.

PubMed

Inum, Reefat; Rana, Md Masud; Shushama, Kamrun Nahar; Quader, Md Anwarul

2018-01-01

A microwave brain imaging system model is envisaged to detect and visualize tumor inside the human brain. A compact and efficient microstrip patch antenna is used in the imaging technique to transmit equivalent signal and receive backscattering signal from the stratified human head model. Electromagnetic band gap (EBG) structure is incorporated on the antenna ground plane to enhance the performance. Rectangular and circular EBG structures are proposed to investigate the antenna performance. Incorporation of circular EBG on the antenna ground plane provides an improvement of 22.77% in return loss, 5.84% in impedance bandwidth, and 16.53% in antenna gain with respect to the patch antenna with rectangular EBG. The simulation results obtained from CST are compared to those obtained from HFSS to validate the design. Specific absorption rate (SAR) of the modeled head tissue for the proposed antenna is determined. Different SAR values are compared with the established standard SAR limit to provide a safety regulation of the imaging system. A monostatic radar-based confocal microwave imaging algorithm is applied to generate the image of tumor inside a six-layer human head phantom model. S -parameter signals obtained from circular EBG loaded patch antenna in different scanning modes are utilized in the imaging algorithm to effectively produce a high-resolution image which reliably indicates the presence of tumor inside human brain.

EBG Based Microstrip Patch Antenna for Brain Tumor Detection via Scattering Parameters in Microwave Imaging System

PubMed Central

Rana, Md. Masud; Shushama, Kamrun Nahar; Quader, Md. Anwarul

2018-01-01

A microwave brain imaging system model is envisaged to detect and visualize tumor inside the human brain. A compact and efficient microstrip patch antenna is used in the imaging technique to transmit equivalent signal and receive backscattering signal from the stratified human head model. Electromagnetic band gap (EBG) structure is incorporated on the antenna ground plane to enhance the performance. Rectangular and circular EBG structures are proposed to investigate the antenna performance. Incorporation of circular EBG on the antenna ground plane provides an improvement of 22.77% in return loss, 5.84% in impedance bandwidth, and 16.53% in antenna gain with respect to the patch antenna with rectangular EBG. The simulation results obtained from CST are compared to those obtained from HFSS to validate the design. Specific absorption rate (SAR) of the modeled head tissue for the proposed antenna is determined. Different SAR values are compared with the established standard SAR limit to provide a safety regulation of the imaging system. A monostatic radar-based confocal microwave imaging algorithm is applied to generate the image of tumor inside a six-layer human head phantom model. S-parameter signals obtained from circular EBG loaded patch antenna in different scanning modes are utilized in the imaging algorithm to effectively produce a high-resolution image which reliably indicates the presence of tumor inside human brain. PMID:29623087

Structural and optical properties of Ag-doped copper oxide thin films on polyethylene napthalate substrate prepared by low temperature microwave annealing

NASA Astrophysics Data System (ADS)

Das, Sayantan; Alford, T. L.

2013-06-01

Silver doped cupric oxide thin films are prepared on polyethylene naphthalate (flexible polymer) substrates. Thin films Ag-doped CuO are deposited on the substrate by co-sputtering followed by microwave assisted oxidation of the metal films. The low temperature tolerance of the polymer substrates led to the search for innovative low temperature processing techniques. Cupric oxide is a p-type semiconductor with an indirect band gap and is used as selective absorption layer solar cells. X-ray diffraction identifies the CuO phases. Rutherford backscattering spectrometry measurements confirm the stoichiometry of each copper oxide formed. The surface morphology is determined by atomic force microscopy. The microstructural properties such as crystallite size and the microstrain for (-111) and (111) planes are calculated and discussed. Incorporation of Ag led to the lowering of band gap in CuO. Consequently, it is determined that Ag addition has a strong effect on the structural, morphological, surface, and optical properties of CuO grown on flexible substrates by microwave annealing. Tauc's plot is used to determine the optical band gap of CuO and Ag doped CuO films. The values of the indirect and direct band gap for CuO are found to be 2.02 eV and 3.19 eV, respectively.

High-Power Microwave Transmission and Mode Conversion Program

DOE Office of Scientific and Technical Information (OSTI.GOV)

Vernon, Ronald J.

2015-08-14

This is a final technical report for a long term project to develop improved designs and design tools for the microwave hardware and components associated with the DOE Plasma Fusion Program. We have developed basic theory, software, fabrication techniques, and low-power measurement techniques for the design of microwave hardware associated gyrotrons, microwave mode converters and high-power microwave transmission lines. Specifically, in this report we discuss our work on designing quasi-optical mode converters for single and multiple frequencies, a new method for the analysis of perturbed-wall waveguide mode converters, perturbed-wall launcher design for TE0n mode gyrotrons, quasi-optical traveling-wave resonator design formore » high-power testing of microwave components, and possible improvements to the HSX microwave transmission line.« less

Fault tolerance analysis and applications to microwave modules and MMIC's

NASA Astrophysics Data System (ADS)

Boggan, Garry H.

A project whose objective was to provide an overview of built-in-test (BIT) considerations applicable to microwave systems, modules, and MMICs (monolithic microwave integrated circuits) is discussed. Available analytical techniques and software for assessing system failure characteristics were researched, and the resulting investigation provides a review of two techniques which have applicability to microwave systems design. A system-level approach to fault tolerance and redundancy management is presented in its relationship to the subsystem/element design. An overview of the microwave BIT focus from the Air Force Integrated Diagnostics program is presented. The technical reports prepared by the GIMADS team were reviewed for applicability to microwave modules and components. A review of MIMIC (millimeter and microwave integrated circuit) program activities relative to BIT/BITE is given.

Synthesis of (azelaic-co-dodecanedioic) polyanhydride by microwave technique

NASA Astrophysics Data System (ADS)

Gutiérrez, M.; Sierra, C.; Acevedo Morantes, M.; Herrera, A. P.

2016-02-01

A polyanhydride was synthesized through microwave radiation using azelaic acid and dodecanedioic dicarboxylic acid at concentrations of 75:25, 50:50, and 25:75%w/w with acetic anhydride as crosslinking agent. Polymerization was carried out during 3 and 5 minutes. The copolymer with the highest molecular weight was selected using the intrinsic viscometry technique and by Huggin/Kraemer and Solomon/Ciuta methods. Based on these measurements, the 50:50 copolymer was selected with a polymerization time of 3 minutes in the microwave. This sample displayed the highest intrinsic viscosity (41.82cm3/g), demonstrating the relevance of the microwave technique for the synthesis of biopolymers.

A promising diagnostic method: Terahertz pulsed imaging and spectroscopy

PubMed Central

Sun, Yiwen; Sy, Ming Yiu; Wang, Yi-Xiang J; Ahuja, Anil T; Zhang, Yuan-Ting; Pickwell-MacPherson, Emma

2011-01-01

The terahertz band lies between the microwave and infrared regions of the electromagnetic spectrum. This radiation has very low photon energy and thus it does not pose any ionization hazard for biological tissues. It is strongly attenuated by water and very sensitive to water content. Unique absorption spectra due to intermolecular vibrations in this region have been found in different biological materials. These unique features make terahertz imaging very attractive for medical applications in order to provide complimentary information to existing imaging techniques. There has been an increasing interest in terahertz imaging and spectroscopy of biologically related applications within the last few years and more and more terahertz spectra are being reported. This paper introduces terahertz technology and provides a short review of recent advances in terahertz imaging and spectroscopy techniques, and a number of applications such as molecular spectroscopy, tissue characterization and skin imaging are discussed. PMID:21512652

Fundamental experiment of ion thruster using ECR discharge

NASA Astrophysics Data System (ADS)

Yasui, Toshiaki; Kitayama, Jiro; Tahara, Hirokazu; Onoe, Ken-Ichi; Yoshikawa, Takao

A microwave ion thruster has the potential to overcome a lifetime problem of electric propulsion by eliminating electrodes. Two types of microwave ion thruster have been investigated to examine the operational characteristics. The one is the thruster using cavity-resonance microwave discharge, and the other is the thruster using Electron Cyclotron Resonance (ECR) discharge. Cavity-resonance microwave discharge produced plasmas by strong electric field in the resonant cavity and sustained plasmas at argon mass flow rates above 10 sccm. However, ECR discharge was capable of sustaining plasmas at lower mass flow rate, because ECR discharge efficiently produced plasmas by resonance absorption. From these generated microwave plasmas, ions were electrostatically extracted by two multiaperture grids. In ECR discharge, the maximum ion beam current of 75 mA and the highest mass utilization efficiency of 18.7% were achieved at a total extraction voltage of 950 V.

Electron cyclotron resonance plasma reactor for production of carbon stripper foil

NASA Astrophysics Data System (ADS)

Faith Romero, Camille; Kanamori, Keita; Kinsho, Michikazu; Yoshimoto, Masahiro; Wada, Motoi

2018-01-01

A graphite antenna for the production of carbon-containing hydrogen plasmas is being developed to prepare impurity-free charge exchange foils for high-energy synchrotrons. Microwave power at 2.45 GHz frequency drives a coaxial structure antenna with a 12-mm-diameter central graphite cylinder and a tapered surrounding cylinder serving as the ground electrode. The antenna was placed in a linear magnetic field to investigate how it performs under an electron cyclotron resonance (ECR) condition. A clear resonance phenomenon was observed in plasma luminosity, microwave power absorption, and microwave power reflection when the induction current used to produce a linear magnetic field was changed. The antenna realized the best microwave coupling to the plasma with the ECR zone formed 5 mm from the end of the center electrode. The antenna realized stable operation for more than 5 h with 100 W input microwave power and with operating hydrogen pressure from 0.5 to 50 Pa.

Microwave modification of surface hydroxyl density for g-C3N4 with enhanced photocatalytic activity

NASA Astrophysics Data System (ADS)

An, Na; Zhao, Yang; Mao, Zhiyong; Agrawal, Dinesh Kumar; Wang, Dajian

2018-03-01

Microwave modification was performed on graphitic carbon nitride (g-C3N4) photocatalysts to tail the surface hydroxyl content for enhanced photocatalytic activity in this work. The influence of microwave heating on the surface hydroxyl density was investigated by a suite of characterization methods. The microwave treated g-C3N4 (MT-g-C3N4) delivered a higher photocatalytic activity in degradation of Rhodamine B (RhB) under visible light irradiation than pristine g-C3N4 due to its improved separation efficiency of photogenerated charge carries and promoted absorption capacity of RhB reactants on surface, which resulted from the increased surface hydroxyl density induced by microwave treatment. This study provides a simple and convenient method to modify g-C3N4 materials with enhanced photocatalytic activity for the potential application in photocatalytic elimination of environmental pollutants.

Feasibility study of microwave modulation DIAL system for global CO II monitoring

NASA Astrophysics Data System (ADS)

Hirano, Yoshihito; Kameyama, Shumpei; Ueno, Shinichi; Sugimoto, Nobuo; Kimura, Toshiyoshi

2006-12-01

A new concept of DIAL (DIfferential Absorption Lidar) system for global CO II monitoring using microwave modulation is introduced. This system uses quasi-CW lights which are intensity modulated in microwave region and receives a backscattered light from the ground. In this system, ON/OFF wavelength laser lights are modulated with microwave frequencies, and received lights of two wavelengths are able to be discriminated by modulation frequencies in electrical signal domain. Higher sensitivity optical detection can be realized compared with the conventional microwave modulation lidar by using direct down conversion of modulation frequency. The system also has the function of ranging by using pseudo-random coding in modulation. Fiber-based optical circuit using wavelength region of 1.6 micron is a candidate for the system configuration. After the explanation of this configuration, feasibility study of this system on the application to global CO II monitoring is introduced.

Microwave Cooking: Knowledge, Attitudes, and Practices of California Foods Teachers.

ERIC Educational Resources Information Center

Stalder, Laura D.; And Others

1990-01-01

A survey of 500 California secondary foods teachers (172 responses) indicated their understanding of microwave cooking principles and techniques and positive attitudes toward microwave cooking and safety. A majority used microwave instruction in their classrooms, although many indicated a need for ovens and microwave educational materials. (SK)

Intermixing optical and microwave signals in GaAs microstrip circuits for phase-locking applications

NASA Astrophysics Data System (ADS)

Li, Ming G.; Chauchard, Eve A.; Lee, Chi H.; Hung, Hing-Loi A.

1990-12-01

The microwave modulation of the interference generated by optical beams that are reflected from the top and bottom surfaces of GaAs substrate adjacent to a microstrip line is studied. The detected modulation is used to directly characterize the electrooptic effect. This optical-microwave intermixing technique is applied to phase-lock a free-running microwave oscillator with picosecond laser pulses. One potential application of this technique is for the optical on-wafer characterization of MMICs.

Chemical Ni-C Bonding in Ni-Carbon Nanotube Composite by a Microwave Welding Method and Its Induced High-Frequency Radar Frequency Electromagnetic Wave Absorption.

PubMed

Sha, Linna; Gao, Peng; Wu, Tingting; Chen, Yujin

2017-11-22

In this work, a microwave welding method has been used for the construction of chemical Ni-C bonding at the interface between carbon nanotubes (CNTs) and metal Ni to provide a different surface electron distribution, which determined the electromagnetic (EM) wave absorption properties based on a surface plasmon resonance mechanism. Through a serial of detailed examinations, such as X-ray diffraction, scanning electron microscopy, transmission electron microscopy, high-resolution transmission electron microscopy, X-ray photoelectron spectroscopy, and Raman spectrum, the as-expected chemical Ni-C bonding between CNTs and metal Ni has been confirmed. And the Brunauer-Emmett-Teller and surface zeta potential measurements uncovered the great evolution of structure and electronic density compared with CNTs, metal Ni, and Ni-CNT composite without Ni-C bonding. Correspondingly, except the EM absorption due to CNTs and metal Ni in the composite, another wide and strong EM absorption band ranging from 10 to 18 GHz was found, which was induced by the Ni-C bonded interface. With a thinner thickness and more exposed Ni-C interfaces, the Ni-CNT composite displayed less reflection loss.

Simple and Low-Cost Dual-Band Printed Microwave Absorber for 2.4- and 5-GHz-Band Applications

NASA Astrophysics Data System (ADS)

Khoomwong, Ekajit; Phongcharoenpanich, Chuwong

2017-10-01

In this research, a dual-band thin printed-circuit-board (PCB) microwave absorber has been proposed for applications in 2.4 and 5 GHz frequency bands. Each unit cell of the absorber consists of a square ring and a thick cross-dipole, augmented with the tuning elements. In the design process, numerical simulations were performed for the optimal characteristics of the absorber and an absorber prototype was fabricated using the simple print-transferring and etching process. The measured absorption bandwidths (50 %) of 170 MHz (2.36-2.53 GHz) and 830 MHz (5.09-5.92 GHz) were achieved for the first and second bands, respectively, with the wideband characteristic at the second operating band. The absorption rates near the center frequencies (2.45 and 5.5 GHz) were respectively 97.85 % and 97.76 %. The simulation and measured results are in good agreement. Furthermore, the incidence-angle dependencies of the absorber were of moderately wide angles with the absorption capacity of at least 50 % for both operating bands. The proposed absorber is suitable for a variety of applications requiring absorption in the 2.4/5 GHz bands.

1D Magnetic Materials of Fe3O4 and Fe with High Performance of Microwave Absorption Fabricated by Electrospinning Method

PubMed Central

Han, Rui; Li, Wei; Pan, Weiwei; Zhu, Minggang; Zhou, Dong; Li, Fa-shen

2014-01-01

Fe3O4 and Fe nanowires are successfully fabricated by electrospinning method and reduction process. Wiry microstructures were achieved with the phase transformation from α-Fe2O3 to Fe3O4 and Fe by partial and full reduction, while still preserving the wire morphology. The diameters of the Fe3O4 and Fe nanowires are approximately 50–60 nm and 30–40 nm, respectively. The investigation of microwave absorption reveals that the Fe3O4 nanowires exhibit excellent microwave absorbing properties. For paraffin-based composite containing 50% weight concentration of Fe3O4 nanowires, the minimum reflection loss reaches −17.2 dB at 6.2 GHz with the matching thickness of 5.5 mm. Furthermore, the calculation shows that the modulus of the ratio between the complex permittivity and permeability |ε/μ| is far away from unity at the minimum reflection loss point, which is quite different from the traditional opinions. PMID:25510415

Coupled high performance liquid chromatography-microwave digestion-hydride generation-atomic absorption spectrometry for inorganic and organic arsenic speciation in fish tissue.

PubMed

Villa-Lojo, M C; Alonso-Rodríguez, E; López-Mahía, P; Muniategui-Lorenzo, S; Prada-Rodríguez, D

2002-06-10

A high performance liquid chromatography-microwave digestion-hydride generation-atomic absorption spectrometry (HPLC-MW-HG-AAS) coupled method is described for As(III), As(V), monomethylarsonic acid (MMA), dimethylarsinic acid (DMA), arsenobetaine (AsB) and arsenocholine (AsC) determination. A Hamilton PRP-X100 anion-exchange column is used for carrying out the arsenic species separation. As mobile phase 17 mM phosphate buffer (pH 6.0) is used for As(III), As(V), MMA and DMA separation, and ultrapure water (pH 6.0) for AsB and AsC separation. Prior to injection into the HPLC system AsB and AsC are isolated from the other arsenic species using a Waters Accell Plus QMA cartridge. A microwave digestion with K(2)S(2)O(8) as oxidizing agent is used for enhancing the efficiency of conversion of AsB and AsC into arsenate. Detection limits achieved were between 0.3 and 1.1 ng for all species. The method was applied to arsenic speciation in fish samples.

Photophysical Behavior and Computational Investigation of Novel 1,4-Bis(2-(2-Phenylpyrimido[1,2-a]Benzimidazol-4-Yl)Phenoxy)Butan (BPPB) Macromolecule.

PubMed

Saleh, Tamer S; Hussein, Mahmoud A; Osman, Osman I; Alamry, Khalid A; Mekky, Ahmed E M; Asiri, Abdullah M; El-Daly, Samy A

2016-09-01

A new macromolecule pyrimido[l,2-a]benzimidazole derivative named 1,4-bis(2-(2-phenylpyrimido[1,2-a]benzimidazol-4-yl)phenoxy)butan (BPPB) has been synthesized in accepted yield using microwave assistance. The new compound BPPB has been formed by the interaction of 3,3'-((butane-1,4-diylbis(oxy))bis(2,1-phenylene))bis(1-phenylprop-2-en-1-one) (3) with 2- aminobenzimidazole (4) in the presence of potassium hydroxide as a basic catalyst in dimethylformamide (DMF) under microwave radiation for 20 min. The chemical structure of this novel compound was elucidated by elemental and spectral techniques including: FT-IR, (1)H-NMR, (13)C-NMR and mass spectra. The electronic absorption and emission spectra of BPPB were measured in different solvents. BPPB displayed a solvatochromic effect of the emission spectrum that is reflected by red shifts of its fluorescence emission maxima on increasing the solvent polarity, indicating a change of electronic charge distribution upon excitation. BPPB crystalline solids gave excimer-like emission at 535 nm with a bandwidth of ca. 60 nm. Ground and excited states electronic geometry optimizations using density functional theory (DFT) and time-dependent density functional theory (TD-DFT), respectively, complemented these spectral findings. The intramolecular charge transfer was investigated by natural bond orbital (NBO) technique.

NEUTRON FLUX INTENSITY DETECTION

DOEpatents

Russell, J.T.

1964-04-21

A method of measuring the instantaneous intensity of neutron flux in the core of a nuclear reactor is described. A target gas capable of being transmuted by neutron bombardment to a product having a resonance absorption line nt a particular microwave frequency is passed through the core of the reactor. Frequency-modulated microwave energy is passed through the target gas and the attenuation of the energy due to the formation of the transmuted product is measured. (AEC)

Heating of tissues by microwaves: a model analysis.

PubMed

Foster, K R; Lozano-Nieto, A; Riu, P J; Ely, T S

1998-01-01

We consider the thermal response times for heating of tissue subject to nonionizing (microwave or infrared) radiation. The analysis is based on a dimensionless form of the bioheat equation. The thermal response is governed by two time constants: one (tau1) pertains to heat convection by blood flow, and is of the order of 20-30 min for physiologically normal perfusion rates; the second (tau2) characterizes heat conduction and varies as the square of a distance that characterizes the spatial extent of the heating. Two idealized cases are examined. The first is a tissue block with an insulated surface, subject to irradiation with an exponentially decreasing specific absorption rate, which models a large surface area of tissue exposed to microwaves. The second is a hemispherical region of tissue exposed at a spatially uniform specific absorption rate, which models localized exposure. In both cases, the steady-state temperature increase can be written as the product of the incident power density and an effective time constant tau(eff), which is defined for each geometry as an appropriate function of tau1 and tau2. In appropriate limits of the ratio of these time constants, the local temperature rise is dominated by conductive or convective heat transport. Predictions of the block model agree well with recent data for the thresholds for perception of warmth or pain from exposure to microwave energy. Using these concepts, we developed a thermal averaging time that might be used in standards for human exposure to microwave radiation, to limit the temperature rise in tissue from radiation by pulsed sources. We compare the ANSI exposure standards for microwaves and infrared laser radiation with respect to the maximal increase in tissue temperature that would be allowed at the maximal permissible exposures. A historical appendix presents the origin of the 6-min averaging time used in the microwave standard.

Densification and Electrical Properties of Zinc Oxide Varistors Microwave-Sintered Under Different Oxygen Partial Pressures

NASA Astrophysics Data System (ADS)

Lin, Cong; Wang, Bo; Xu, Zheng; Peng, Hu

2012-11-01

ZnO varistors were prepared by microwave sintering under different oxygen partial pressures. The temperature profile and the densification behavior in different atmospheres were investigated. It was found that the density of ZnO varistors during sintering was the key factor affecting the absorption of microwave energy. The electrical properties, including the nonlinear properties and capacitance-voltage ( C- V) characteristics, were also carefully studied. The results showed that the oxygen partial pressure has significant effects on the electrical properties of ZnO varistors by changing the concentration of defects through a series of reactions involving oxygen during sintering.

New NOAA-15 Advanced Microwave Sounding Unit (AMSU) Datasets for Stratospheric Research

NASA Technical Reports Server (NTRS)

Spencer, Roy W.; Braswell, William D.

1999-01-01

The NOAA-15 spacecraft launched in May 1998 carried the first Advanced Microwave Sounding Unit (AMSU). The AMSU has eleven oxygen absorption channels with weighting functions peaking from near the surface to 2 mb. Twice-daily, limb-corrected I degree gridded datasets of layer temperatures have been constructed since the AMSU went operational in early August 1998. Examples of AMSU imagery will be shown, as will preliminary analyses of daily fluctuations in tropical stratospheric temperatures and their relationship to daily variations in tropical-average rainfall measured by the Special Sensor Microwave Imager (SSM/I). The AMSU datasets are now available for other researchers to utilize.

Microwave remote sensing: Active and passive. Volume 1 - Microwave remote sensing fundamentals and radiometry

NASA Technical Reports Server (NTRS)

Ulaby, F. T.; Moore, R. K.; Fung, A. K.

1981-01-01

The three components of microwave remote sensing (sensor-scene interaction, sensor design, and measurement techniques), and the applications to geoscience are examined. The history of active and passive microwave sensing is reviewed, along with fundamental principles of electromagnetic wave propagation, antennas, and microwave interaction with atmospheric constituents. Radiometric concepts are reviewed, particularly for measurement problems for atmospheric and terrestrial sources of natural radiation. Particular attention is given to the emission by atmospheric gases, clouds, and rain as described by the radiative transfer function. Finally, the operation and performance characteristics of radiometer receivers are discussed, particularly for measurement precision, calibration techniques, and imaging considerations.

RF Testing Of Microwave Integrated Circuits

NASA Technical Reports Server (NTRS)

Romanofsky, R. R.; Ponchak, G. E.; Shalkhauser, K. A.; Bhasin, K. B.

1988-01-01

Fixtures and techniques are undergoing development. Four test fixtures and two advanced techniques developed in continuing efforts to improve RF characterization of MMIC's. Finline/waveguide test fixture developed to test submodules of 30-GHz monolithic receiver. Universal commercially-manufactured coaxial test fixture modified to enable characterization of various microwave solid-state devices in frequency range of 26.5 to 40 GHz. Probe/waveguide fixture is compact, simple, and designed for non destructive testing of large number of MMIC's. Nondestructive-testing fixture includes cosine-tapered ridge, to match impedance wavequide to microstrip. Advanced technique is microwave-wafer probing. Second advanced technique is electro-optical sampling.

The application of microwave digestion in decomposing some refractory ore samples with solid fusion agent.

PubMed

Lu, Yan; Li, Gang; Liu, Wei; Yuan, Hongyan; Xiao, Dan

2018-08-15

It is known that most of the refractory ore are the basis of national economy and widely applied in various fields, however, the complexity of the chemical composition and the diversity of the crystallinity in the mineral phases make the sample pre-treatment of refractory ore still remains a challenge. In this work, the complete decomposition of the refractory ore sample can be achieved just by exposing the solid fusion agent and the refractory ore sample in the microwave irradiation environment for a few minutes, and induced by a drop of water. A digestion time of 15 min for 3.0 g solid fusion agent mixture of sodium peroxide/sodium carbonate (Na 2 O 2 /Na 2 CO 3 ) in a corundum crucible via microwave heating is sufficient to decompose 0.1 g refractory ore sample. An excellent microwave digestion solid agent should meet the following conditions, a good decomposition ability, an outstanding ability of absorbing microwave energy and converting it into heat quickly, a higher melting point than the decomposing temperature of the ore sample. In the research, the induction effect of water plays an important role for the microwave digestion. The energy which is released by the reaction of water and the solid fusion agent (Na 2 O 2 ) is the key to decompose refractory ore samples with solid fusion agent, which replenished the total energy required for the microwave digestion and made the microwave digestion completed successfully. This microwave digestion technique has good reproducibility and precision, RSD % for Mo, Fe, Ti, Cr and W in the refractory ore samples were all better than 6, except RSD % for Be of about 8 because of the influence of matrix-effect. Meanwhile, the analysis results of the elements in the refractory ore samples provided by the microwave digestion technique were all in good agreement with the analysis results provided by the traditional fusion method except for Cr in the mixture ore samples. In the study, the non-linear dependence of the electromagnetic and thermal properties of the solid fusion agent on temperature under microwave irradiation and the selective heating of microwave are fully applied in this simple microwave technique. Comparing to the traditional fusion decomposition method, this microwave digestion technique is a simple, economical, fast and energy-saving sample pre-treatment technique. Copyright © 2018 Elsevier B.V. All rights reserved.

Master Equation Analysis of Thermal and Nonthermal Microwave Effects.

PubMed

Ma, Jianyi

2016-10-11

Master equation is a successful model to describe the conventional heating reaction, it is expanded to capture the "microwave effect" in this work. The work equation of "microwave effect" included master equation presents the direct heating, indirect heating, and nonthermal effect about the microwave field. The modified master equation provides a clear physics picture to the nonthermal microwave effect: (1) The absorption and the emission of the microwave, which is dominated by the transition dipole moment between two corresponding states and the intensity of the microwave field, provides a new path to change the reaction rate constants. (2) In the strong microwave field, the distribution of internal states of the molecules will deviate from the equilibrium distribution, and the system temperature defined in the conventional heating reaction is no longer available. According to the general form of "microwave effect" included master equation, a two states model for unimolecular dissociation is proposed and is used to discuss the microwave nonthermal effect particularly. The average rate constants can be increased up to 2400 times for some given cases without the temperature changed in the two states model. Additionally, the simulation of a model system was executed using our State Specified Master Equation package. Three important conclusions can be obtained in present work: (1) A reasonable definition of the nonthermal microwave effect is given in the work equation of "microwave effect" included master equation. (2) Nonthermal microwave effect possibly exists theoretically. (3) The reaction rate constants perhaps can be changed obviously by the microwave field for the non-RRKM and the mode-specified reactions.

Theoretical Analysis of Microwave Propagation.

DTIC Science & Technology

1984-04-01

effects of the turbulent atmosphere on wave propagation, US Department of Commerce, NTIS, Springfield, VA. * VanVleck, J.H. (1947), "The absorption of... turbulent atmosphere on wave propagation, US Department of Commerce, NTIS, Sprinifield, VA. -. A. Vigants (1975), "Space diversity engineering," BSTJ, Vol... Turbulence ., ...... 2-26 2.5 ATMOSPHERIC ABSORPTION. 2-26 2 .6 RAIN ATTENUATION ....... 2-29 3 TROPOSCATTER PROPAGATION .................... 3-1 3.1

Microwave quantum illumination.

PubMed

Barzanjeh, Shabir; Guha, Saikat; Weedbrook, Christian; Vitali, David; Shapiro, Jeffrey H; Pirandola, Stefano

2015-02-27

Quantum illumination is a quantum-optical sensing technique in which an entangled source is exploited to improve the detection of a low-reflectivity object that is immersed in a bright thermal background. Here, we describe and analyze a system for applying this technique at microwave frequencies, a more appropriate spectral region for target detection than the optical, due to the naturally occurring bright thermal background in the microwave regime. We use an electro-optomechanical converter to entangle microwave signal and optical idler fields, with the former being sent to probe the target region and the latter being retained at the source. The microwave radiation collected from the target region is then phase conjugated and upconverted into an optical field that is combined with the retained idler in a joint-detection quantum measurement. The error probability of this microwave quantum-illumination system, or quantum radar, is shown to be superior to that of any classical microwave radar of equal transmitted energy.

Proceedings of Microwaves and Thermoregulation Held at New Haven, Connecticut on 26-27 October 1981

DTIC Science & Technology

1981-01-01

uneven. When radiobiological data indicate a threshold of effective heat for killing tumor cells that lies within a narrow range of temperatures, the...and orientation effects of whole animal absorption of electromagnetic waves. IEEE Trans. Biomed. Eng. 22 :536. Gandhi, O.P. (1975b). Conditions of...S., Szmigl.elski, S., and Moneta, J. (1974). Effects of microwave irradiation in vitro on cell mem- brane permeability. In Czerski (1974), p. 173

GFAAS determination of selenium in infant formulas using a microwave digestion method.

PubMed

Alegria, A; Barbera, R; Farré, R; Moreno, A

1994-01-01

A method for determining the selenium content of infant formulas is proposed. It includes wet digestion with nitric acid and hydrogen peroxide in medium pressure teflon bombs in a microwave oven and determination by graphite furnace atomic absorption spectrometry (GFAAS). The absence of interferences is checked. Values obtained for the limit of detection (19.4 ng/g), precision (RSD = 2.2%) and accuracy by analysis of a reference material show that the method is reliable.

Lightweight NiFe2O4 with controllable 3D network structure and enhanced microwave absorbing properties

NASA Astrophysics Data System (ADS)

Wang, Fen; Wang, Xing; Zhu, Jianfeng; Yang, Haibo; Kong, Xingang; Liu, Xiao

2016-11-01

3D network structure NiFe2O4 was successfully synthesized by a templated salt precipitation method using PMMA colloid crystal as templates. The morphology, phase composition and microwave absorbing properties of as-prepared samples were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), vector network analyzer (VNA), and so on. The results revealed that the 3D network structure was configurated with smooth spherical walls composed of NiFe2O4 nanocrystals and their pore diameters being in the range of 80-250 nm. The microwave absorption properties of the 3D network structure NiFe2O4 were crucially determined by the special structure. The synergy of intrinsic magnetic loss of magnetic NiFe2O4 and the interfacial polarization enhanced by 3D network structure and the interaction of multiple mechanisms endowed the sample with the feature of strong absorption, broad bandwidth and lightweight. There is more than one valley in the reflection loss curves and the maximum reflection loss is 27.5 dB with a bandwidth of 4 GHz. Moreover, the 3D network structure NiFe2O4 show a greater reflection loss with the same thickness comparing to the ordinary NiFe2O4 nanoparticles, which could achieve the feature of lightweight of the microwave absorbing materials.

Lightweight NiFe2O4 with controllable 3D network structure and enhanced microwave absorbing properties

PubMed Central

Wang, Fen; Wang, Xing; Zhu, Jianfeng; Yang, Haibo; Kong, Xingang; Liu, Xiao

2016-01-01

3D network structure NiFe2O4 was successfully synthesized by a templated salt precipitation method using PMMA colloid crystal as templates. The morphology, phase composition and microwave absorbing properties of as-prepared samples were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), vector network analyzer (VNA), and so on. The results revealed that the 3D network structure was configurated with smooth spherical walls composed of NiFe2O4 nanocrystals and their pore diameters being in the range of 80–250 nm. The microwave absorption properties of the 3D network structure NiFe2O4 were crucially determined by the special structure. The synergy of intrinsic magnetic loss of magnetic NiFe2O4 and the interfacial polarization enhanced by 3D network structure and the interaction of multiple mechanisms endowed the sample with the feature of strong absorption, broad bandwidth and lightweight. There is more than one valley in the reflection loss curves and the maximum reflection loss is 27.5 dB with a bandwidth of 4 GHz. Moreover, the 3D network structure NiFe2O4 show a greater reflection loss with the same thickness comparing to the ordinary NiFe2O4 nanoparticles, which could achieve the feature of lightweight of the microwave absorbing materials. PMID:27897209

A time domain based method for the accurate measurement of Q-factor and resonance frequency of microwave resonators

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gyüre, B.; Márkus, B. G.; Bernáth, B.

2015-09-15

We present a novel method to determine the resonant frequency and quality factor of microwave resonators which is faster, more stable, and conceptually simpler than the yet existing techniques. The microwave resonator is pumped with the microwave radiation at a frequency away from its resonance. It then emits an exponentially decaying radiation at its eigen-frequency when the excitation is rapidly switched off. The emitted microwave signal is down-converted with a microwave mixer, digitized, and its Fourier transformation (FT) directly yields the resonance curve in a single shot. Being a FT based method, this technique possesses the Fellgett (multiplex) and Connesmore » (accuracy) advantages and it conceptually mimics that of pulsed nuclear magnetic resonance. We also establish a novel benchmark to compare accuracy of the different approaches of microwave resonator measurements. This shows that the present method has similar accuracy to the existing ones, which are based on sweeping or modulating the frequency of the microwave radiation.« less

Snow wetness measurements for melt forecasting

NASA Technical Reports Server (NTRS)

Linlor, W. I.; Clapp, F. D.; Meier, M. F.; Smith, J. L.

1975-01-01

A microwave technique for directly measuring snow pack wetness in remote installations is described. The technique, which uses satellite telemetry for data gathering, is based on the attenuation of a microwave beam in transmission through snow.

An accurate automated technique for quasi-optics measurement of the microwave diagnostics for fusion plasma

NASA Astrophysics Data System (ADS)

Hu, Jianqiang; Liu, Ahdi; Zhou, Chu; Zhang, Xiaohui; Wang, Mingyuan; Zhang, Jin; Feng, Xi; Li, Hong; Xie, Jinlin; Liu, Wandong; Yu, Changxuan

2017-08-01

A new integrated technique for fast and accurate measurement of the quasi-optics, especially for the microwave/millimeter wave diagnostic systems of fusion plasma, has been developed. Using the LabVIEW-based comprehensive scanning system, we can realize not only automatic but also fast and accurate measurement, which will help to eliminate the effects of temperature drift and standing wave/multi-reflection. With the Matlab-based asymmetric two-dimensional Gaussian fitting method, all the desired parameters of the microwave beam can be obtained. This technique can be used in the design and testing of microwave diagnostic systems such as reflectometers and the electron cyclotron emission imaging diagnostic systems of the Experimental Advanced Superconducting Tokamak.

Enhanced conductive loss in nickel–cobalt sulfide nanostructures for highly efficient microwave absorption and shielding

NASA Astrophysics Data System (ADS)

Li, Wanrong; Zhou, Min; Lu, Fei; Liu, Hongfei; Zhou, Yuxue; Zhu, Jun; Zeng, Xianghua

2018-06-01

Microwave-absorbing materials with light weight and high efficiency are desirable in addressing electromagnetic interference (EMI) problems. Herein, a nickel–cobalt sulfide (NCS) nanostructure was employed as a robust microwave absorber, which displayed an optimized reflection loss of  ‑49.1 dB in the gigahertz range with a loading of only 20 wt% in an NCS/paraffin wax composite. High electrical conductivity was found to contribute prominent conductive loss in NCS, leading to intense dielectric loss within a relatively low mass loading. Furthermore, owing to its high electrical conductivity and remarkable dielectric loss to microwaves, the prepared NCS exhibited excellent performance in EMI shielding. The EMI shielding efficiency of the 50 wt% NCS/paraffin composite exceeded 55 dB at the X-band, demonstrating NCS is a versatile candidate for solving EMI problems.

Remote sensing of atmospheric chemistry; Proceedings of the Meeting, Orlando, FL, Apr. 1-3, 1991

NASA Technical Reports Server (NTRS)

Mcelroy, James L. (Editor); Mcneal, Robert J. (Editor)

1991-01-01

The present volume on remote sensing of atmospheric chemistry discusses special remote sensing space observations and field experiments to study chemical change in the atmosphere, network monitoring for detection of stratospheric chemical change, stratospheric chemistry studies, and the combining of model, in situ, and remote sensing in atmospheric chemistry. Attention is given to the measurement of tropospheric carbon monoxide using gas filter radiometers, long-path differential absorption measurements of tropospheric molecules, air quality monitoring with the differential optical absorption spectrometer, and a characterization of tropospheric methane through space-based remote sensing. Topics addressed include microwave limb sounder experiments for UARS and EOS, an overview of the spectroscopy of the atmosphere using an FIR emission experiment, the detection of stratospheric ozone trends by ground-based microwave observations, and a FIR Fabry-Perot spectrometer for OH measurements.

Dynamics of the formation and loss of boron atoms in a H2/B2H6 microwave plasma

NASA Astrophysics Data System (ADS)

Duluard, C. Y.; Aubert, X.; Sadeghi, N.; Gicquel, A.

2016-09-01

For further improvements in doped-diamond deposition technology, an understanding of the complex chemistry in H2/CH4/B2H6 plasmas is of general importance. In this context, a H2/B2H6 plasma ignited by microwave power in a near resonant cavity at high pressure (100-200 mbar) is studied to measure the B-atom density in the ground state. The discharge is ignited in the gas mixture (0-135 ppm B2H6 in H2) by a 2.45 GHz microwave generator, leading to the formation of a hemispheric plasma core, surrounded by a faint discharge halo filling the remaining reactor volume. Measurements with both laser induced fluorescence and resonant absoption with a boron hollow cathode lamp indicate that the B-atom density is higher in the halo than in the plasma core. When the absorption line-of-sight is positioned in the halo, the absorption is so strong that the upper detection limit is reached. To understand the mechanisms of creation and loss of boron atoms, time-resolved absorption measurements have been carried out in a pulsed plasma regime (10 Hz, duty cycle 50%). The study focuses on the influence of the total pressure, the partial pressure of B2H6, as well as the source power, on the growth and decay rates of boron atoms when the plasma is turned off.

Field study of in situ remediation of petroleum hydrocarbon contaminated soil on site using microwave energy.

PubMed

Chien, Yi-Chi

2012-01-15

Many laboratory-scale studies strongly suggested that remediation of petroleum hydrocarbon contaminated soil by microwave heating is very effective; however, little definitive field data existed to support the laboratory-scale observations. This study aimed to evaluate the performance of a field-scale microwave heating system to remediate petroleum hydrocarbon contaminated soil. A constant microwave power of 2 kW was installed directly in the contaminated area that applied in the decontamination process for 3.5h without water input. The C10-C40 hydrocarbons were destroyed, desorbed or co-evaporated with moisture from soil by microwave heating. The moisture may play an important role in the absorption of microwave and in the distribution of heat. The success of this study paved the way for the second and much larger field test in the remediation of petroleum hydrocarbon contaminated soil by microwave heating in place. Implemented in its full configuration for the first time at a real site, the microwave heating has demonstrated its robustness and cost-effectiveness in cleaning up petroleum hydrocarbon contaminated soil in place. Economically, the concept of the microwave energy supply to the soil would be a network of independent antennas which powered by an individual low power microwave generator. A microwave heating system with low power generators shows very flexible, low cost and imposes no restrictions on the number and arrangement of the antennas. Copyright © 2011 Elsevier B.V. All rights reserved.

An absorbing microwave micro-solid-phase extraction device used in non-polar solvent microwave-assisted extraction for the determination of organophosphorus pesticides.

PubMed

Wang, Ziming; Zhao, Xin; Xu, Xu; Wu, Lijie; Su, Rui; Zhao, Yajing; Jiang, Chengfei; Zhang, Hanqi; Ma, Qiang; Lu, Chunmei; Dong, Deming

2013-01-14

A single-step extraction-cleanup method, including microwave-assisted extraction (MAE) and micro-solid-phase extraction (μ-SPE), was developed for the extraction of ten organophosphorus pesticides in vegetable and fruit samples. Without adding any polar solvent, only one kind of non-polar solvent (hexane) was used as extraction solvent in the whole extraction step. Absorbing microwave μ-SPE device, was prepared by packing activated carbon with microporous polypropylene membrane envelope, and used as not only the sorbent in μ-SPE, but also the microwave absorption medium. Some experimental parameters effecting on extraction efficiency was investigated and optimized. 1.0 g of sample, 8 mL of hexane and three absorbing microwave μ-SPE devices were added in the microwave extraction vessel, the extraction was carried out under 400 W irradiation power at 60°C for 10 min. The extracts obtained by MAE-μ-SPE were directly analyzed by GC-MS without any clean-up process. The recoveries were in the range of 93.5-104.6%, and the relative standard deviations were lower than 8.7%. Copyright © 2012 Elsevier B.V. All rights reserved.

On the importance of simultaneous infrared/fiber-optic temperature monitoring in the microwave-assisted synthesis of ionic liquids.

PubMed

Obermayer, David; Kappe, C Oliver

2010-01-07

The temperature profiles obtained from both an external infrared and internal fiber-optic sensor were compared for heating and synthesizing the ionic liquid 1-butyl-3-methylimidazolium bromide (bmimBr) under microwave conditions. Utilizing a single-mode microwave reactor that allows simultaneous infrared/fiber-optic temperature measurements, significant differences between the two methods of temperature monitoring were revealed. Due to the strong microwave absorptivity of ionic liquids and the delay experienced in monitoring temperature on the outer surface of a heavy-walled glass vial, external infrared temperature sensors can not be used to accurately control the temperature in the heating of ionic liquids under microwave conditions. The use of internal fiber-optic probes allows the monitoring and control of the heating behavior in a much better way. In order to prevent the strong exotherm in the synthesis of bmimBr under microwave conditions the use of a reaction vessel made out of silicon carbide is the method of choice. Because of the high thermal conductivity and effusivity of silicon carbide, the heat generated during the ionic liquid formation is efficiently exchanged with the comparatively cool air in the microwave cavity via the silicon carbide ceramic.

Green synthesis, structure and fluorescence spectra of new azacyanine dyes

NASA Astrophysics Data System (ADS)

Enchev, Venelin; Gadjev, Nikolai; Angelov, Ivan; Minkovska, Stela; Kurutos, Atanas; Markova, Nadezhda; Deligeorgiev, Todor

2017-11-01

A series of symmetric and unsymmetric monomethine azacyanine dyes (monomethine azacyanine and merocyanine sulfobetaines) were synthesized with moderate to high yields via a novel method using microwave irradiation. The compounds are derived from a condensation reaction between 2-thiomethylbenzotiazolium salts and 2-imino-3-methylbenzothiazolines proceeded under microwave irradiation. The synthetic approach involves the use of green solvent and absence of basic reagent. TD-DFT calculations were performed to simulate absorption and fluorescent spectra of synthesized dyes. Absorption maxima, λmax, of the studied dyes were found in the range 364-394 nm. Molar absorbtivities were evaluated in between 40300 and 59200 mol-1 dm3 cm-1. Fluorescence maxima, λfl, were registered around 418-448 nm upon excitation at 350 nm. A slight displacements of theoretically estimated absorption maxima according to experimental ones is observed. The differences are most probably due to the fact that the DFT calculations were carried out without taking into account the solvent effect. In addition, the merocyanine sulfobetaines also fluorescence in blue optical range (420-480 nm) at excitation in red range (630-650 nm).

Emerging Trends in Microwave Processing of Spices and Herbs.

PubMed

Rahath Kubra, Ismail; Kumar, Devender; Jagan Mohan Rao, Lingamallu

2016-10-02

Today, spices are integral part of our food as they provide sensory attributes such as aroma, color, flavour and taste to food. Further their antimicrobial, antioxidant, pharmaceutical and nutritional properties are also well known. Since spices are seasonal so their availability can be extended year round by adopting different preservation techniques. Drying and extraction are most important methods for preservation and value addition to spices. There are different techniques for drying of spices with their own advantages and limitations. A novel, non-conventional technique for drying of spices is use of microwave radiation. This technique proved to be very rapid, and also provide a good quality product. Similarly, there are a number of non-conventional extraction methods in use that are all, in principle, solid-liquid extractions but which introduce some form of additional energy to the process in order to facilitate the transfer of analytes from sample to solvent. This paper reviews latest advances in the use of microwave energy for drying of spices and herbs. Also, the review describes the potential application of microwave energy for extraction of essential oil/bioactive components from spices and herbs and the advantages of microwave-assisted process over the other extraction processes generally employed for extraction. It also showcases some recent research results on microwave drying/extraction from spices and herbs.

Microwave electromagnetic properties of carbonyl iron particles and Si/C/N nano-powder filled epoxy-silicone coating

NASA Astrophysics Data System (ADS)

Qing, Yuchang; Zhou, Wancheng; Luo, Fa; Zhu, Dongmei

2010-02-01

The electromagnetic characteristics of carbonyl iron particles and Si/C/N nano-powder filled epoxy-silicone coatings were studied. The reflection loss of the coatings exceeds -10 dB at 8-18 GHz and -9 dB at 2-18 GHz when the coating thickness is 1 and 3 mm, respectively. The dielectric and magnetic absorbers filled coatings possess excellent microwave absorption, which could be attributed to the proper incorporate of the multi-polarization mechanisms as well as strong natural resonance. It is feasible to develop the thin and wideband microwave absorbing coatings using carbonyl iron particles and Si/C/N nano-powder.

Effect of microwave radiation on inactivation of Clostridium sporogenes (PA 3679) spores.

PubMed Central

Welt, B A; Tong, C H; Rossen, J L; Lund, D B

1994-01-01

Three techniques for studying effects of microwave radiation on microorganisms were introduced. Spores of Clostridium sporogenes (PA 3679) were chosen as a test organism because the kinetic parameters for thermal inactivation are well known and because of the importance of the genus Clostridium to the food industry. For the first technique, a specially designed kinetics vessel was used to compare inactivation rates of microwave-heated and conventionally heated spores at steady-state temperatures of 90, 100, and 110 degrees C. Rates were found to be similar at the 95% confidence level. The second and third techniques were designed to study the effect of relatively high power microwave exposure at sublethal temperatures. In the second approach, the suspension was continuously cooled via direct contact with a copper cooling coil in a well-mixed vessel, outside the microwave oven. The suspension was pumped through a Teflon loop in the oven, where it continuously absorbed approximately 400 W of microwave power. Inactivation occurred in both irradiated and unirradiated samples. It was suspected that copper ions entered the suspension from the copper coil and were toxic to the spores. The fact that the results were similar, however, implied the absence of nonthermal microwave effects. In the third approach, the copper coil was replaced with a silicone tubing loop in a microwave transparent vessel. The suspension was continuously irradiated at 150 W of microwave power. No detectable inactivation occurred. Results indicated that the effect of microwave energy on viability of spores was indistinguishable from the effect of conventional heating. PMID:8135512

Behavioral and autonomic thermoregulation in hamsters during microwave-induced heat exposure

DOE Office of Scientific and Technical Information (OSTI.GOV)

Gordon, C.J.; Long, M.D.; Fehlner, K.S.

1984-01-01

Preferred ambient temperature (Ta) and ventilatory frequency were measured in free-moving hamsters exposed to 2450-MHz microwaves. A waveguide exposure system that permits continuous monitoring of the absorbed heat load accrued from microwave exposure was imposed with a longitudinal temperature gradient which allowed hamsters to select their preferred Ta. Ventilatory frequency was monitored remotely by analysing the rhythmic shifts in unabsorbed microwave energy passing down the waveguide. Without microwave exposure hamsters selected an average T2 of 30.2 C. This preferred Ta did not change until the rate of heat absorption (SAR) from microwave exposure exceeded approx. 2 W kg-1. In amore » separate experiment, a SAR of 2.0 W kg-1 at a Ta of 30C was shown to promote an average 0.5 C increase in colonic temperature. Hamsters maintained their ventilatory frequency at baseline levels by selecting a cooler Ta during microwave exposure. These data support previous studies suggesting that during thermal stress behavioral thermo-regulation (i.e. preferred Ta) takes prescedence over autonomic thermoregulation (i.e. ventilatory frequency). It is apparent that selecting a cooler Ta is a more efficient and/or effective than autonomic thermoregulation for dissipating a heat load accrued from microwave exposure.« less

MICROWAVE TECHNOLOGY CHEMICAL SYNTHESIS APPLICATIONS

EPA Science Inventory

Microwave-accelerated chemical syntheses in various solvents as well as under solvent-free conditions have witnessed an explosive growth. The technique has found widespread application predominantly exploiting the inexpensive unmodified household microwave (MW) ovens although th...

Asymmetric Shock Wave Generation in a Microwave Rocket Using a Magnetic Field

NASA Astrophysics Data System (ADS)

Takahashi, Masayuki

2017-10-01

A plasma pattern is reproduced by coupling simulations between a particle-in- cell with Monte Carlo collisions model and a finite-difference time-domain simulation for an electromagnetic wave propagation when an external magnetic field is applied to the breakdown volume inside a microwave-rocket nozzle. The propagation speed and energy-absorption rate of the plasma are estimated based on the breakdown simulation, and these are utilized to reproduce shock wave propagation, which provides impulsive thrust for the microwave rocket. The shock wave propagation is numerically reproduced by solving the compressible Euler equation with an energy source of the microwave heating. The shock wave is asymmetrically generated inside the nozzle when the electron cyclotron resonance region has a lateral offset, which generates lateral and angular impulses for postural control of the vehicle. It is possible to develop an integrated device to maintain beaming ight of the microwave rocket, achieving both axial thrust improvement and postural control, by controlling the spatial distribution of the external magnetic field.

Abatement of Perfluorinated Compounds Using Cylindrical Microwave Plasma Source at Low Pressure

NASA Astrophysics Data System (ADS)

Kim, Seong Bong; Park, S.; Park, Y.; Youn, S.; Yoo, S. J.

2016-10-01

Microwave plasma source with a cylindrical cavity has been proposed to abate the perfluorinated compounds (PFCs). This plasma source was designed to generate microwave plasma with the cylindrical shape and to be easily installed in existing exhaust line. The microwave frequency is 2.45 GHz and the operating pressure range is 0.1 Torr to 0.3 Torr. The plasma characteristic of the cylindrical microwave plasma source was measured using the optical spectrometer, and tunable diode laser absorption spectroscopy (TDLAS). The destruction and removal efficiency (DRE) of CF4 and CHF3 were measured by a quadrupole mass spectroscopy (QMS) with the various operation conditions. The effect of the addition of the oxygen gas were tested and also the correlation between the plasma parameters and the DRE are presented in this study. This work was supported by R&D Program of ``Plasma Advanced Technology for Agriculture and Food (Plasma Farming)'' through the National Fusion Research Institute of Korea (NFRI) funded by the Government funds.

Thermoregulation in intense microwave fields

DOE Office of Scientific and Technical Information (OSTI.GOV)

Michaelson, S.M.

1981-10-01

These studies clearly indicate the thermoregulatory capacity of the dog to withstand exposure to high microwave fields at specific absorption rates (SAR) of 3.7 and 6.1 W/kg. It appears that adequate thermoregulation takes place at an SAR of 3.7 W/kg but only transiently at 6.1 W/kg. These values, compared with the standardized resting metabolic rate of 3.29 W/kg (0.75), provide a basis for assessing the relationship of the thermal burden and thermo-regulatory disruption by microwaves in the dog. To elucidate the thermal potential of microwave exposure, it was helpful to conduct these exposures at various ambient temperatures in which themore » normal body temperature remained stable, thus permitting comparison of heat production and dissipation with our without microwaves. The zone of the thermal neutrality or thermoneutral zone of vasomotor activity, 22-26.5 deg C, where body temperature is regulated by changes in vasomotor tonus, fulfilled this requirement.« less

A method for combining passive microwave and infrared rainfall observations

NASA Technical Reports Server (NTRS)

Kummerow, Christian; Giglio, Louis

1995-01-01

Because passive microwave instruments are confined to polar-orbiting satellites, rainfall estimates must interpolate across long time periods, during which no measurements are available. In this paper the authors discuss a technique that allows one to partially overcome the sampling limitations by using frequent infrared observations from geosynchronous platforms. To accomplish this, the technique compares all coincident microwave and infrared observations. From each coincident pair, the infrared temperature threshold is selected that corresponds to an area equal to the raining area observed in the microwave image. The mean conditional rainfall rate as determined from the microwave image is then assigned to pixels in the infrared image that are colder than the selected threshold. The calibration is also applied to a fixed threshold of 235 K for comparison with established infrared techniques. Once a calibration is determined, it is applied to all infrared images. Monthly accumulations for both methods are then obtained by summing rainfall from all available infrared images. Two examples are used to evaluate the performance of the technique. The first consists of a one-month period (February 1988) over Darwin, Australia, where good validation data are available from radar and rain gauges. For this case it was found that the technique approximately doubled the rain inferred by the microwave method alone and produced exceptional agreement with the validation data. The second example involved comparisons with atoll rain gauges in the western Pacific for June 1989. Results here are overshadowed by the fact that the hourly infrared estimates from established techniques, by themselves, produced very good correlations with the rain gauges. The calibration technique was not able to improve upon these results.

A New Remote-Sensing Method for Mine Detection using HPM Irradiation and IR Detection.

DTIC Science & Technology

1999-12-01

absorption of microwave energy by the mine. This signature appears at the soil surface after a brief time-delay from the start of HPM illumination. At...detection de cible, l’operation de teledetection, la capacite de detecter des cibles sous un ciel couvert avec peu de dependance du cycle solaire et la...the temperature of the sample depends on the microwave energy absorbed by the sample and varies inversely with the sample thermal heat capacity. The

High Pressure Microwave Powered UV Light Sources

NASA Astrophysics Data System (ADS)

Cekic, M.; Frank, J. D.; Popovic, S.; Wood, C. H.

1997-10-01

Industrial microwave powered (*electrodeless*) light sources have been limited to quiescent pressures of 300 Torr of buffer gas and metal- halide fills. Recently developed multi-atmospheric electronegative bu lb fills (noble gas-halide excimers, metal halide) require electric field s for ionization that are often large multiples of the breakdown voltage for air. For these fills an auxiliary ignition system is necessary. The most successful scheme utilizes a high voltage pulse power supply and a novel field emission source. Acting together they create localized condition of pressure reduction and high free electron density. This allows the normal microwave fields to drive this small region into avalanche, ignite the bulb, and heat the plasma to it's operating poin t Standard diagnostic techniques of high density discharges are inapplicable to the excimer bulbs, because of the ionic molecular exci ted state structure and absence of self-absorption. The method for temperature determination is based on the equilibrium population of certain vibrational levels of excimer ionic excited states. Electron d ensity was determined from the measurements of Stark profiles of H_β radiation from a small amount of hydrogen mixed with noble gas and halogens. At the present time, high pressure (Te 0.5eV, ne 3 x 10^17 cm-3) production bulbs produce over 900W of radiation in a 30nm band, centered at 30nm. Similarly, these prototypes when loaded with metal-halide bulb fills produce 1 kW of radiation in 30nm wide bands, centered about the wavelength of interest.

Microwave-assisted microemulsion technique for production of miconazole nitrate- and econazole nitrate-loaded solid lipid nanoparticles.

PubMed

Shah, Rohan M; Eldridge, Daniel S; Palombo, Enzo A; Harding, Ian H

2017-08-01

The microwave-assisted production of solid lipid nanoparticles (SLNs) is a novel technique reported recently by our group. The small particle size, solid nature and use of physiologically well-tolerated lipid materials make SLNs an interesting and potentially efficacious drug carrier. The main purpose of this research work was to investigate the suitability of microwave-assisted microemulsion technique to encapsulate selected ionic drug substances such as miconazole nitrate and econazole nitrate. The microwave-produced SLNs had a small size (250-300nm), low polydispersity (<0.20), high encapsulation efficiency (72-87%) and loading capacity (3.6-4.3%). Differential scanning calorimetry (DSC) and X-ray diffraction (XRD) studies suggested reduced crystallinity of stearic acid in SLNs. The release studies demonstrated a slow, sustained but incomplete release of drugs (<60% after 24h) from microwave-produced SLNs. Data fitting of drug release data revealed that the release of both drugs from microwave-produced SLNs was governed by non-Fickian diffusion indicating that drug release was both diffusion- and dissolution- controlled. Anti-fungal efficacy of drug-loaded SLNs was evaluated on C. albicans. The cell viability studies showed that cytotoxicity of SLNs was concentration-dependent. These encouraging results suggest that the microwave-assisted procedure is suitable for encapsulation of ionic drugs and that microwave-produced SLNs can act as potential carriers of antifungal drugs. Copyright © 2017 Elsevier B.V. All rights reserved.

Thermal tolerance reduces hyperthermia-induced disruption of working memory: a role for endogenous opiates?

PubMed

Mickley, G A; Cobb, B L

1998-03-01

Previous reports indicate that microwave-induced hyperthermia can impair learning and memory. Here, we report that preexposure to a single 20-min period of hyperthermia can produce thermal tolerance and, thereby, attenuate future physiological and behavioral reactions to heating. Because endogenous opioids have been implicated in thermoregulation and reactions to microwave exposure, we also determined how opioid receptor antagonism might modulate these effects. In an initial experiment, rats were exposed daily, over 5 successive days, to 600-MHz microwaves (at a whole-body specific absorption rate of 9.3 W/kg) or sham exposed. In animals exposed to microwaves, thermal tolerance was evidenced by declining rectal temperatures over time. Temperature reductions following microwave exposure were prominent after a single previous exposure. Therefore, in a second study, a single hyperthermic episode was used to induce thermal tolerance. On Day 1, rats were either exposed, over a 20-min period, to 600-MHz microwaves (at a whole-body specific absorption rate of 9.3 W/kg) or sham exposed. Just prior to radiation/sham-radiation treatment, rats received either saline or naltrexone (0.1 or 10 mg/kg, intraperitoneally (i.p.)). The following day (Day 2), rats were either microwave or sham exposed and tested on a task which measures the relative time subjects explore a familiar versus a novel stimulus object. Normothermic rats spend significantly more time in contact with new environmental components and less time with familiar objects. Brain (dura) and rectal temperatures were recorded on both days of the study. Microwave exposure produced a reliable hyperthermia which was significantly lower (on Day 2) in rats receiving repeated treatments (tolerant group). On the behavioral test, rats exposed only once to microwave-induced hyperthermia (nontolerant group) exhibited significantly different patterns of object discrimination than did tolerant or sham-exposed animals. Sham-exposed and tolerant animals showed a distinct preference for the new object whereas the nontolerant animals did not. Naltrexone (10 mg/kg) antagonized the hyperthermia-induced disruption of the object discrimination task (in nontolerant rats) and produced patterns of object exploration that were similar to those of sham-irradiated and thermal-tolerant rats, suggesting that endogenous opioids play a role in the organism's response to heating. Taken together, these data are consistent with the conclusions that 1) microwave-induced hyperthermia can cause a dose-dependent disruption of the normal discrimination between new and familiar objects, 2) physiological reactions to a single hyperthermic episode can produce a thermotolerance that expresses itself in both reduced levels of hyperthermia and attenuated behavioral disruptions following microwave exposure, and 3) opioid antagonism can partially reverse some of the behavioral effects of microwave-induced hyperthermia.

Prospects for Finite-Difference Time-Domain (FDTD) Computational Electrodynamics

NASA Astrophysics Data System (ADS)

Taflove, Allen

2002-08-01

FDTD is the most powerful numerical solution of Maxwell's equations for structures having internal details. Relative to moment-method and finite-element techniques, FDTD can accurately model such problems with 100-times more field unknowns and with nonlinear and/or time-variable parameters. Hundreds of FDTD theory and applications papers are published each year. Currently, there are at least 18 commercial FDTD software packages for solving problems in: defense (especially vulnerability to electromagnetic pulse and high-power microwaves); design of antennas and microwave devices/circuits; electromagnetic compatibility; bioelectromagnetics (especially assessment of cellphone-generated RF absorption in human tissues); signal integrity in computer interconnects; and design of micro-photonic devices (especially photonic bandgap waveguides, microcavities; and lasers). This paper explores emerging prospects for FDTD computational electromagnetics brought about by continuing advances in computer capabilities and FDTD algorithms. We conclude that advances already in place point toward the usage by 2015 of ultralarge-scale (up to 1E11 field unknowns) FDTD electromagnetic wave models covering the frequency range from about 0.1 Hz to 1E17 Hz. We expect that this will yield significant benefits for our society in areas as diverse as computing, telecommunications, defense, and public health and safety.

High temperature acoustic and hybrid microwave/acoustic levitators for materials processing

NASA Technical Reports Server (NTRS)

Barmatz, Martin

1990-01-01

The physical acoustics group at the Jet Propulsion Laboratory developed a single mode acoustic levitator technique for advanced containerless materials processing. The technique was successfully demonstrated in ground based studies to temperatures of about 1000 C in a uniform temperature furnace environment and to temperatures of about 1500 C using laser beams to locally heat the sample. Researchers are evaluating microwaves as a more efficient means than lasers for locally heating a positioned sample. Recent tests of a prototype single mode hybrid microwave/acoustic levitator successfully demonstrated the feasibility of using microwave power as a heating source. The potential advantages of combining acoustic positioning forces and microwave heating for containerless processing investigations are presented in outline form.

Enhanced microwave absorption properties of epoxy composites containing graphite nanosheets@Fe3O4 decorated comb-like MnO2 nanoparticles

NASA Astrophysics Data System (ADS)

Su, Xiaogang; Wang, Jun; Zhang, Bin; Chen, Wei; Wu, Qilei; Dai, Wei; Zou, Yi

2018-05-01

Recently, owing to the radiation and interference from electromagnetic wave (EMW), the requirements of EMW absorbing materials have been increasing. Herein, a novel absorber composed of graphite nanosheets@Fe3O4 composites decorated comb-like MnO2 (GNFM) has been successfully synthesized via a facile two steps, characterized using x-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), x-ray photoelectron spectroscopy (XPS), Raman spectroscopy, vibrating sample magnetometry (VSM) and vector network analyzer (VNA). The ternary composites with enhanced microwave absorption performance are due to the complementary effects of electroconductive material (graphite nanosheets), dielectric materials (MnO2) and magnetic material (Fe3O4 nanospheres). Hence, the maximum reflection loss of GNFM/epoxy composites is up to ‑31.7 dB at 5.85 GHz with absorbing thickness of 4.5 mm, and the efficient frequency bandwidth below ‑10 dB can reach up to 4.47 GHz (11.87–16.34 GHz) at matching thickness of 2 mm. The results demonstrate that GNFM could be regarded as a novel type of microwave absorbing material.

Influence of SiO2 Addition on Properties of PTFE/TiO2 Microwave Composites

NASA Astrophysics Data System (ADS)

Yuan, Ying; Wang, Jie; Yao, Minghao; Tang, Bin; Li, Enzhu; Zhang, Shuren

2018-01-01

Composite substrates for microwave circuit applications have been fabricated by filling polytetrafluoroethylene (PTFE) polymer matrix with ceramic powder consisting of rutile TiO2 ( D 50 ≈ 5 μm) partially substituted with fused amorphous SiO2 ( D 50 ≈ 8 μm) with composition x vol.% SiO2 + (50 - x) vol.% TiO2 ( x = 0, 3, 6, 9, 12), and the effects of SiO2 addition on characteristics such as the density, moisture absorption, microwave dielectric properties, and thermal properties systematically investigated. The results show that the filler was well distributed throughout the matrix. High dielectric constant ( ɛ r > 7.19) and extremely low moisture absorption (<0.02%) were obtained, resulting from the relatively high density of the composites. The ceramic particles served as barriers and improved the thermal stability of the PTFE polymer, retarding its decomposition. The temperature coefficient of dielectric constant ( τ ɛ ) of the composites shifted toward the positive direction (from - 309 ppm/°C to - 179 ppm/°C) as the SiO2 content was increased, while the coefficient of thermal expansion remained almost unchanged (˜ 35 ppm/°C).

The flaky porous Fe3O4 with tunable dimensions for enhanced microwave absorption performance in X and C bands

NASA Astrophysics Data System (ADS)

Zhao, Huanqin; Cheng, Yan; Liu, Wei; Yang, Zhihong; Zhang, Baoshan; Ji, Guangbin; Du, Youwei

2018-07-01

Special electric and magnetic characteristics make Fe3O4 widely applied in the electromagnetic (EM) wave absorption region. However, for pure Fe3O4, it is still a challenge to simultaneously obtain high absorption intensity and broadband absorption at a low thickness, owing to its low dielectric property. As we realized, flake configuration and the porous structure have obviously promote the EM wave absorption property. Because the former can lead to multi-reflection between flakes and the latter is conductive to interface polarization, flaky Fe3O4 with a porous and coarse surface was designed to overcome the deficiency of traditional Fe3O4 particles. The experimental results demonstrate that the flaky configuration is conductive to enhancing the dielectric coefficient and optimizing impedance matching. Moreover, the complex permittivity rises with the aspect ratio of the sheet. Under a suitable dimension, the flaky Fe3O4 could acquire targeted EM wave absorption capacity in the X band (8–12 GHz). In detail, the maximum reflection loss (RL) could reach a strong intensity of ‑49 dB at 2.05 mm. The effective absorption bandwidth (EAB) with RL below ‑10 dB is 4.32 (7.52–11.84) GHz, which is almost equivalent to the whole X band (8–12 GHz). Even more exciting, when regulating the thickness between 2.05 and 3.05 mm, the EAB could cover the entire C and X bands (4–12 GHz). This study provides a good reference for the future development of other ferromagnetic materials toward specific microwave bands.

The flaky porous Fe3O4 with tunable dimensions for enhanced microwave absorption performance in X and C bands.

PubMed

Zhao, Huanqin; Cheng, Yan; Liu, Wei; Yang, Zhihong; Zhang, Baoshan; Ji, Guangbin; Du, Youwei

2018-07-20

Special electric and magnetic characteristics make Fe 3 O 4 widely applied in the electromagnetic (EM) wave absorption region. However, for pure Fe 3 O 4 , it is still a challenge to simultaneously obtain high absorption intensity and broadband absorption at a low thickness, owing to its low dielectric property. As we realized, flake configuration and the porous structure have obviously promote the EM wave absorption property. Because the former can lead to multi-reflection between flakes and the latter is conductive to interface polarization, flaky Fe 3 O 4 with a porous and coarse surface was designed to overcome the deficiency of traditional Fe 3 O 4 particles. The experimental results demonstrate that the flaky configuration is conductive to enhancing the dielectric coefficient and optimizing impedance matching. Moreover, the complex permittivity rises with the aspect ratio of the sheet. Under a suitable dimension, the flaky Fe 3 O 4 could acquire targeted EM wave absorption capacity in the X band (8-12 GHz). In detail, the maximum reflection loss (RL) could reach a strong intensity of -49 dB at 2.05 mm. The effective absorption bandwidth (EAB) with RL below -10 dB is 4.32 (7.52-11.84) GHz, which is almost equivalent to the whole X band (8-12 GHz). Even more exciting, when regulating the thickness between 2.05 and 3.05 mm, the EAB could cover the entire C and X bands (4-12 GHz). This study provides a good reference for the future development of other ferromagnetic materials toward specific microwave bands.

ORGANIC SYNTHESES USING MICROWAVES AND SUPPORTED REAGENTS

EPA Science Inventory

Microwave-accelerated chemical syntheses under solvent-free conditions have witnessed an explosive growth. The technique has found widespread application predominantly exploiting the inexpensive unmodified household microwave (MW) ovens although the use of dedicated MW equipment...

Modeling and prediction of extraction profile for microwave-assisted extraction based on absorbed microwave energy.

PubMed

Chan, Chung-Hung; Yusoff, Rozita; Ngoh, Gek-Cheng

2013-09-01

A modeling technique based on absorbed microwave energy was proposed to model microwave-assisted extraction (MAE) of antioxidant compounds from cocoa (Theobroma cacao L.) leaves. By adapting suitable extraction model at the basis of microwave energy absorbed during extraction, the model can be developed to predict extraction profile of MAE at various microwave irradiation power (100-600 W) and solvent loading (100-300 ml). Verification with experimental data confirmed that the prediction was accurate in capturing the extraction profile of MAE (R-square value greater than 0.87). Besides, the predicted yields from the model showed good agreement with the experimental results with less than 10% deviation observed. Furthermore, suitable extraction times to ensure high extraction yield at various MAE conditions can be estimated based on absorbed microwave energy. The estimation is feasible as more than 85% of active compounds can be extracted when compared with the conventional extraction technique. Copyright © 2013 Elsevier Ltd. All rights reserved.

Suitability of microwave drying for mealworms (Tenebrio molitor) as alternative to freeze drying: Impact on nutritional quality and colour.

PubMed

Lenaerts, S; Van Der Borght, M; Callens, A; Van Campenhout, L

2018-07-15

Freeze drying represents the current practice to stabilize mealworms, even though it is an energy demanding technique. Therefore, it was examined in the present study whether microwave drying could be a proper alternative. To this end, the impact of both drying techniques on the proximate composition, vitamin B 12 content, fatty acid profile, oxidation status and colour parameters of mealworms was investigated. Furthermore, the influence of the application of vacuum during microwave drying was studied. The different drying technologies resulted in small differences in the proximate composition, while the vitamin B 12 content was only reduced by microwave drying. The fat fraction of freeze dried mealworms showed a higher oxidation status than the fat of microwave dried mealworms. Application of a vacuum during the microwave drying process did not appear to offer advantages. This research shows that for mealworms microwave drying can be a proper alternative to freeze drying. Copyright © 2018 Elsevier Ltd. All rights reserved.

Addendum to Site Assessment and Feasibility of a New Operations Base on the Greenland Ice Sheet: Addendum to Preliminary Report

DTIC Science & Technology

2015-11-01

National Guard PLR Division of Polar Programs SMM /I Special Sensor Microwave/Imager SMMR Scanning Multi-channel Microwave Radiometer ERDC/CRREL...and the Special Sensor Microwave/Imager ( SMM /I). The satellite-based technique uses a difference in the passive microwave brightness temperatures

Evaluation of microwave cavity gas sensor for in-vessel monitoring of dry cask storage systems

NASA Astrophysics Data System (ADS)

Bakhtiari, S.; Gonnot, T.; Elmer, T.; Chien, H.-T.; Engel, D.; Koehl, E.; Heifetz, A.

2018-04-01

Results are reported of research activities conducted at Argonne to assess the viability of microwave resonant cavities for extended in-vessel monitoring of dry cask storage system (DCSS) environment. One of the gases of concern to long-term storage in canisters is water vapor, which appears due to evaporation of residual moisture from incompletely dried fuel assembly. Excess moisture could contribute to corrosion and deterioration of components inside the canister, which would in turn compromise maintenance and safe transportation of such systems. Selection of the sensor type in this work was based on a number of factors, including good sensitivity, fast response time, small form factor and ruggedness of the probing element. A critical design constraint was the capability to mount and operate the sensor using the existing canister penetrations-use of existing ports for thermocouple lances. Microwave resonant cavities operating at select resonant frequency matched to the rotational absorption line of the molecule of interest offer the possibility of highly sensitive detection. In this study, two prototype K-band microwave cylindrical cavities operating at TE01n resonant modes around the 22 GHz water absorption line were developed and tested. The sensors employ a single port for excitation and detection and a novel dual-loop inductive coupling for optimized excitation of the resonant modes. Measurement of the loaded and unloaded cavity quality factor was obtained from the S11 parameter. The acquisition and real-time analysis of data was implemented using software based tools developed for this purpose. The results indicate that the microwave humidity sensors developed in this work could be adapted to in-vessel monitoring applications that require few parts-per-million level of sensitivity. The microwave sensing method for detection of water vapor can potentially be extended to detection of radioactive fission gases leaking into the interior of the canister through cracks in fuel cladding.

Evaluation of the effects of varying moisture contents on microwave thermal emissions from agriculture fields

NASA Technical Reports Server (NTRS)

Burke, H. H. K.

1980-01-01

Three tasks related to soil moisture sensing at microwave wavelengths were undertaken: (1) analysis of data at L, X and K sub 21 band wavelengths over bare and vegetated fields from the 1975 NASA sponsored flight experiment over Phoenix, Arizona; (2) modeling of vegetation canopy at microwave wavelengths taking into consideration both absorption and volume scattering effects; and (3) investigation of overall atmospheric effects at microwave wavelengths that can affect soil moisture retrieval. Data for both bare and vegetated fields are found to agree well with theoretical estimates. It is observed that the retrieval of surface and near surface soil moisture information is feasible through multi-spectral and multi-temporal analysis. It is also established that at long wavelengths, which are optimal for surface sensing, atmospheric effects are generally minimal. At shorter wavelengths, which are optimal for atmosheric retrieval, the background surface properties are also established.

Microwave properties of Ni-based ferromagnetic inverse opals

NASA Astrophysics Data System (ADS)

Kostylev, M.; Stashkevich, A. A.; Roussigné, Y.; Grigoryeva, N. A.; Mistonov, A. A.; Menzel, D.; Sapoletova, N. A.; Napolskii, K. S.; Eliseev, A. A.; Lukashin, A. V.; Grigoriev, S. V.; Samarin, S. N.

2012-11-01

Investigations of microwave properties of Ni-based inverse ferromagnetic opal-like film with the [111] axis of the fcc structure along the normal direction to the film have been carried out in the 2-18 GHz frequency band. We observed multiple spin wave resonances for the magnetic field applied perpendicular to the film, i.e., along the [111] axis of this artificial crystal. For the field applied in the film plane, a broad band of microwave absorption is observed, which does not contain a fine structure. The field ranges of the responses observed are quite different for these two magnetization directions. This suggests a collective magnetic ground state or shape anisotropy and collective microwave dynamics for this foam-like material. This result is in agreement with SQUID measurements of hysteresis loops for the material. Two different models for this collective behavior are suggested that satisfactorily explain the major experimental results.

Microwave Palaeointensity Experiments On Terrestrial and Martian Material

NASA Astrophysics Data System (ADS)

Shaw, J.; Hill, M.; Gratton, M.

The microwave palaeointensity technique was developed in Liverpool University (Walton et al 1996) and has successfully been applied to archaeological ceramics and recent lavas (Shaw et al 1996, 1999.; Hill et al 1999,2000). These published results show that microwave analysis provides accurate palaeointensity determinations com- bined with a very high success rate. Most recently the technique has been successfully applied to Martian material (Shaw et al, 2001) to look for the existence of an internal Martian dynamo early in Martian history. New experiments have been carried out us- ing microwaves to demagnetise synthetic muti-component TRM's and new palaeoin- tensity experiments providing a comparison between microwave analysis of laboratory TRM's and conventional thermal Thellier analysis of microwave generated mTRM's. These experiments demonstrate the equivalence of microwave and thermally gener- ated TRM's. D. Walton, S Snape, T.C. Rolph, J. Shaw and J.A. Share, Application of ferromagnetic resonance heating to palaeointensity determinations.1996, Phys Earth Planet Int,94, 183-186. J. Shaw, D. Walton, S Yang, T.C.Rolph, and J.A. Share. Microwave Archaeointensities from Peruvian Ceramics. 1996, Geophys. J. Int,124,241-244 J. Shaw, S. Yang, T. C. Rolph, and F. Y. Sun. A comparison of archaeointensity results from Chinese ceramics using Microwave and conventional ThellierSs and ShawSs methods.,1999, G J Int.136, 714-718 M. Hill, and J. Shaw, 1999, Palaeointensity results for Historic Lavas from Mt. Etna using microwave demagnetisation/remagnetisation in a modified Thellier type exper- iment. G. J. Int, 139, 583-590 M. J. Hill, and J. Shaw, 2000. Magnetic field intensity study of the 1960 Kilauea lava flow, Hawaii, using the microwave palaeointensity technique, Geophys. J. Int., 142, 487-504. J. Shaw, M. Hill, and S. J. Openshaw, 2001, Investigating the ancient Martian magnetic field using microwaves, Earth and Planetary Science Letters 190 (2001) 103-109

Dynamic Self-Locking of an OEO Containing a VCSEL

NASA Technical Reports Server (NTRS)

Strekalov, Dmitry; Matsko, Andrey; Yu, Nan; Savchenkov, Anatoliy; Maleki, Lute

2009-01-01

A method of dynamic self-locking has been demonstrated to be effective as a means of stabilizing the wavelength of light emitted by a vertical-cavity surface-emitting laser (VCSEL) that is an active element in the frequency-control loop of an optoelectronic oscillator (OEO) designed to implement an atomic clock based on an electromagnetically- induced-transparency (EIT) resonance. This scheme can be considered an alternative to the one described in Optical Injection Locking of a VCSEL in an OEO (NPO-43454), NASA Tech Briefs, Vol. 33, No. 7 (July 2009), page 33. Both schemes are expected to enable the development of small, low-power, high-stability atomic clocks that would be suitable for use in applications involving precise navigation and/or communication. To recapitulate from the cited prior article: In one essential aspect of operation of an OEO of the type described above, a microwave modulation signal is coupled into the VCSEL. Heretofore, it has been well known that the wavelength of light emitted by a VCSEL depends on its temperature and drive current, necessitating thorough stabilization of these operational parameters. Recently, it was discovered that the wavelength also depends on the microwave power coupled into the VCSEL. This concludes the background information. From the perspective that led to the conception of the optical injection-locking scheme described in the cited prior article, the variation of the VCSEL wavelength with the microwave power circulating in the frequency-control loop is regarded as a disadvantage and optical injection locking is a solution of the problem of stabilizing the wavelength in the presence of uncontrolled fluctuations in the microwave power. The present scheme for dynamic self-locking emerges from a different perspective, in which the dependence of VCSEL wavelength on microwave power is regarded as an advantageous phenomenon that can be exploited as a means of controlling the wavelength. The figure schematically depicts an atomic-clock OEO of the type in question, wherein (1) the light from the VCSEL is used to excite an EIT resonance in selected atoms in a gas cell (e.g., 87Rb atoms in a low-pressure mixture of Ar and Ne) and (2) the power supplied to the VCSEL is modulated by a microwave signal that includes components at beat frequencies among the VCSEL wavelength and modulation sidebands. As the VCSEL wavelength changes, it moves closer to or farther from a nearby absorption spectral line, and the optical power transmitted through the cell (and thus the loop gain) changes accordingly. A change in the loop gain causes a change in the microwave power and, thus, in the VCSEL wavelength. It is possible to choose a set of design and operational parameters (most importantly, the electronic part of the loop gain) such that the OEO stabilizes itself in the sense that an increase in circulating microwave power causes the VCSEL wavelength to change in a direction that results in an increase in optical absorption and thus a decrease in circulating microwave power. Typically, such an appropriate choice of operational parameters involves setting the nominal VCSEL wavelength to a point on the shorter-wavelength wing of an absorption spectral line.

The Expected Impacts of NPOESS Microwave and Infrared Sounder Radiances on Operational Numerical Weather Prediction and Data Assimilation Systems

NASA Astrophysics Data System (ADS)

Swadley, S. D.; Baker, N.; Derber, J.; Collard, A.; Hilton, F.; Ruston, B.; Bell, W.; Candy, B.; Kleespies, T. J.

2009-12-01

The NPOESS atmospheric sounding functionality will be accomplished using two separate sensor suites, the combined infrared (IR) and microwave (MW) sensor suite (CrIMSS), and the Microwave Imager/Sounder (MIS) instrument. CrIMSS consists of the Cross Track Infrared Sounder (CrIS) and the cross track Advanced Technology Microwave Sounder (ATMS), and is scheduled to fly on the NPOESS Preparatory Project (NPP), and NPOESS operational flight units C1 and C3. The MIS is a conical scanning polarimetric imager and sounder patterned after the heritage WindSat, and DMSP Special Sensor Microwave Imagers and Sounders (SSMI and SSMIS), and is scheduled for flight units C2, C3 and C4. ATMS combines the current operational Advanced Microwave Sounding Unit (AMSU) and the Microwave Humidity Sounder (MHS), but with an additional channel in the 51.76 GHz oxygen absorption region and 3 additional channels in the 165.5 and 183 GHz water vapor absorption band. CrIS is a Fourier Transform Spectrometer and will provide 159 shortwave IR channels, 433 mid-range IR channels, and 713 longwave IR channels. The heritage sensors for CrIS are the NASA Advanced Infrared Sounder (AIRS) and the MetOp-A Infrared Atmospheric Sounding Interferometer (IASI). Both AIRS and IASI are high quality, high spectral resolution sounders which represent a significant improvement in the effective vertical resolution over previous IR sounders. This presentation will give an overview of preparations underway for day-1 monitoring of NPP/NPOESS radiances, and subsequent operational radiance assimilation. These preparations capitalize on experience gained during the pre-launch preparations, sensor calibration/validation and operational assimilation for the heritage sensors. One important step is to use pre-flight sensor channel specifications, noise estimates and knowledge of the antenna patterns, to generate and test proxy NPP/NPOESS sensor observations in existing assimilation systems. Other critical factors for successful radiance assimilation include low noise measurements, channel sets that span the vertical space defined within the NWP model, a fast and accurate radiative transfer model, and bias correction schemes designed to remove systematic biases in the departures between the observed versus calculated radiances.

Microwave absorption studies of magnetic sublattices in microwave sintered Cr3+ doped SrFe12O19

NASA Astrophysics Data System (ADS)

Praveena, K.; Sadhana, K.; Liu, Hsiang-Lin; Bououdina, M.

2017-03-01

The partial substitution of Fe3+ by Cr3+ in strontium hexaferrite has shown to be an effective method to tailor anisotropy for many novel microwave applications. Some basic studies have revealed that this substitution leads to unusual interactions among the magnetic sublattices of the hexaferrite. In order to investigate these interactions, Cr3+ doped SrCrxFe12-xO19 (x=0.0, 0.1, 0.3, 0.5, 0.7 and 0.9) (m-type) hexaferrites were prepared by microwave-hydrothermal (m-H) method and subsequently sintered at 950 °C/90 min using microwave furnace. The magnetic hysteresis (m-H) loops revealed the ferromagnetic nature of nanoparticles (NPs). The coercive field was increasing from 3291 Oe to 7335 Oe with increasing chromium content. This resulting compacts exhibited high squareness ratio (Mr/Ms-80%). The intrinsic coercivity (Hci) above 1,20,000 Oe and high values of magnetocrystalline anisotropy revealed that all samples are magnetically hard materials. A material with high loss as well as high dielectric constant may be desired in applications such as electromagnetic (EM) wave absorbing coatings. The room temperature complex dielectric and magnetic properties (ε‧, ε‧‧, μ‧ and μ‧‧) of Cr3+ doped SrFe12O19 were measured in X-band region. The frequency dependent dielectric and magnetic losses were increasing to large extent. The reflection coefficient varied from -16 to -33 dB at 10.1 GHz as Cr3+ concentration increased from x=0.0 to x=0.9. Ferromagnetic resonance spectra (FMR) were measured in the X-band (9.4 GHz), linewidth decreases with chromium concentration from 1368 to 752 Oe from x=0.0 to x=0.9, which is quite low compared to commercial samples. We also have detailed origins of the FMR linewidth broadenings in terms of some important theoretical models. These results show that chromium doped strontium hexaferrites are useful for microwave absorption in the X-band frequency and also have potential for use in low frequency self-biased microwave/millimeter devices such as circulators and isolators.

Rational Construction of Uniform CoNi-Based Core-Shell Microspheres with Tunable Electromagnetic Wave Absorption Properties.

PubMed

Chen, Na; Jiang, Jian-Tang; Xu, Cheng-Yan; Yan, Shao-Jiu; Zhen, Liang

2018-02-16

Core-shell particles with integration of ferromagnetic core and dielectric shell are attracting extensive attention for promising microwave absorption applications. In this work, CoNi microspheres with conical bulges were synthesized by a simple and scalable liquid-phase reduction method. Subsequent coating of dielectric materials was conducted to acquire core-shell structured CoNi@TiO 2 composite particles, in which the thickness of TiO 2 is about 40 nm. The coating of TiO 2 enables the absorption band of CoNi to effectively shift from K u to S band, and endows CoNi@TiO 2 microspheres with outstanding electromagnetic wave absorption performance along with a maximum reflection loss of 76.6 dB at 3.3 GHz, much better than that of bare CoNi microspheres (54.4 dB at 17.8 GHz). The enhanced EMA performance is attributed to the unique core-shell structures, which can induce dipole polarization and interfacial polarization, and tune the dielectric properties to achieve good impedance matching. Impressively, TiO 2 coating endows the composites with better microwave absorption capability than CoNi@SiO 2 microspheres. Compared with SiO 2 , TiO 2 dielectric shells could protect CoNi microspheres from merger and agglomeration during annealed. These results indicate that CoNi@TiO 2 core-shell microspheres can serve as high-performance absorbers for electromagnetic wave absorbing application.

Cell membrane as a possible site of Fröhlich's coherent oscillations

NASA Astrophysics Data System (ADS)

Blinowska, K. J.; Lech, W.; Wittlin, A.

1985-05-01

The microwave absorption spectra of erythrocytes and their ghosts have a resonant structure and reveal a close resemblance, indicating that the cell membrane is the primary site of Fröhlich's coherent oscillations.

A Microwave Pressure Sounder

NASA Technical Reports Server (NTRS)

Flower, D. A.; Peckham, G. E.

1978-01-01

An instrument to measure atmospheric pressure at the earth's surface from an orbiting satellite would be a valuable addition to the expanding inventory of remote sensors. The subject of this report is such an instrument - the Microwave Pressure Sounder (MPS). It is shown that global-ocean coverage is attainable with sufficient accuracy, resolution and observational frequency for meteorological, oceanographic and climate research applications. Surface pressure can be deduced from a measurement of the absorption by an atmospheric column at a frequency in the wing of the oxygen band centered on 60 GHz. An active multifrequency instrument is needed to make this measurement with sufficient accuracy. The selection of optimum operating frequencies is based upon accepted models of surface reflection, oxygen, water vapor and cloud absorption. Numerical simulation using a range of real atmospheres defined by radiosonde observations were used to validate the frequency selection procedure. Analyses are presented of alternative system configurations that define the balance between accuracy and achievable resolution.

Theoretical Analysis and Design of Ultrathin Broadband Optically Transparent Microwave Metamaterial Absorbers

PubMed Central

Deng, Ruixiang; Li, Meiling; Muneer, Badar; Zhu, Qi; Shi, Zaiying; Song, Lixin; Zhang, Tao

2018-01-01

Optically Transparent Microwave Metamaterial Absorber (OTMMA) is of significant use in both civil and military field. In this paper, equivalent circuit model is adopted as springboard to navigate the design of OTMMA. The physical model and absorption mechanisms of ideal lightweight ultrathin OTMMA are comprehensively researched. Both the theoretical value of equivalent resistance and the quantitative relation between the equivalent inductance and equivalent capacitance are derived for design. Frequency-dependent characteristics of theoretical equivalent resistance are also investigated. Based on these theoretical works, an effective and controllable design approach is proposed. To validate the approach, a wideband OTMMA is designed, fabricated, analyzed and tested. The results reveal that high absorption more than 90% can be achieved in the whole 6~18 GHz band. The fabricated OTMMA also has an optical transparency up to 78% at 600 nm and is much thinner and lighter than its counterparts. PMID:29324686

Theoretical Analysis and Design of Ultrathin Broadband Optically Transparent Microwave Metamaterial Absorbers.

PubMed

Deng, Ruixiang; Li, Meiling; Muneer, Badar; Zhu, Qi; Shi, Zaiying; Song, Lixin; Zhang, Tao

2018-01-11

Optically Transparent Microwave Metamaterial Absorber (OTMMA) is of significant use in both civil and military field. In this paper, equivalent circuit model is adopted as springboard to navigate the design of OTMMA. The physical model and absorption mechanisms of ideal lightweight ultrathin OTMMA are comprehensively researched. Both the theoretical value of equivalent resistance and the quantitative relation between the equivalent inductance and equivalent capacitance are derived for design. Frequency-dependent characteristics of theoretical equivalent resistance are also investigated. Based on these theoretical works, an effective and controllable design approach is proposed. To validate the approach, a wideband OTMMA is designed, fabricated, analyzed and tested. The results reveal that high absorption more than 90% can be achieved in the whole 6~18 GHz band. The fabricated OTMMA also has an optical transparency up to 78% at 600 nm and is much thinner and lighter than its counterparts.

Sequential ultrasound-microwave assisted acid extraction (UMAE) of pectin from pomelo peels.

PubMed

Liew, Shan Qin; Ngoh, Gek Cheng; Yusoff, Rozita; Teoh, Wen Hui

2016-12-01

This study aims to optimize sequential ultrasound-microwave assisted extraction (UMAE) on pomelo peel using citric acid. The effects of pH, sonication time, microwave power and irradiation time on the yield and the degree of esterification (DE) of pectin were investigated. Under optimized conditions of pH 1.80, 27.52min sonication followed by 6.40min microwave irradiation at 643.44W, the yield and the DE value of pectin obtained was respectively at 38.00% and 56.88%. Based upon optimized UMAE condition, the pectin from microwave-ultrasound assisted extraction (MUAE), ultrasound assisted extraction (UAE) and microwave assisted extraction (MAE) were studied. The yield of pectin adopting the UMAE was higher than all other techniques in the order of UMAE>MUAE>MAE>UAE. The pectin's galacturonic acid content obtained from combined extraction technique is higher than that obtained from sole extraction technique and the pectin gel produced from various techniques exhibited a pseudoplastic behaviour. The morphological structures of pectin extracted from MUAE and MAE closely resemble each other. The extracted pectin from UMAE with smaller and more regular surface differs greatly from that of UAE. This has substantiated the highest pectin yield of 36.33% from UMAE and further signified their compatibility and potentiality in pectin extraction. Copyright © 2016 Elsevier B.V. All rights reserved.

Water metamaterial for ultra-broadband and wide-angle absorption.

PubMed

Xie, Jianwen; Zhu, Weiren; Rukhlenko, Ivan D; Xiao, Fajun; He, Chong; Geng, Junping; Liang, Xianling; Jin, Ronghong; Premaratne, Malin

2018-02-19

A subwavelength water metamaterial is proposed and analyzed for ultra-broadband perfect absorption at microwave frequencies. We experimentally demonstrate that this metamaterial shows over 90% absorption within almost the entire frequency band of 12-29.6 GHz. It is also shown that the proposed metamaterial exhibits a good thermal stability with its absorption performance almost unchanged for the temperature range from 0 to 100°C. The study of the angular tolerance of the metamaterial absorber shows its ability of working at wide angles of incidence. Given that the proposed water metamaterial absorber is low-cost and easy for manufacture, we envision it may find numerous applications in electromagnetics such as broadband scattering reduction and electromagnetic energy harvesting.

Varied absorption peaks of dual-band metamaterial absorber analysis by using reflection theory

NASA Astrophysics Data System (ADS)

Xiong, Han; Yu, Yan-Tao; Tang, Ming-Chun; Chen, Shi-Yong; Liu, Dan-Ping; Ou, Xiang; Zeng, Hao

2016-03-01

Cross-resonator metamaterial absorbers (MMA) have been widely investigated from microwave to optical frequencies. However, only part of the factors influencing the absorption properties were analyzed in previous works at the same time. In order to completely understand how the spacer thickness, dielectric parameter and incidence angle affect the absorption properties of the dual-band MMA, two sets of simulation were performed. It was found that with increasing incident angles, the low-frequency absorption peak showed a blue shift, while the high-frequency absorption peaks showed a red shift. However, with the increase in spacer thickness, both of the absorption peaks showed a red shift. By using the reflection theory expressions, the physical mechanism of the cross-resonator MMA was well explained. This method provides an effective way to analyze multi-band absorber in technology.

Microwave Remote Sensing Modeling of Ocean Surface Salinity and Winds Using an Empirical Sea Surface Spectrum

NASA Technical Reports Server (NTRS)

Yueh, Simon H.

2004-01-01

Active and passive microwave remote sensing techniques have been investigated for the remote sensing of ocean surface wind and salinity. We revised an ocean surface spectrum using the CMOD-5 geophysical model function (GMF) for the European Remote Sensing (ERS) C-band scatterometer and the Ku-band GMF for the NASA SeaWinds scatterometer. The predictions of microwave brightness temperatures from this model agree well with satellite, aircraft and tower-based microwave radiometer data. This suggests that the impact of surface roughness on microwave brightness temperatures and radar scattering coefficients of sea surfaces can be consistently characterized by a roughness spectrum, providing physical basis for using combined active and passive remote sensing techniques for ocean surface wind and salinity remote sensing.

Carbon dioxide crystals: An examination of their size, shape, and scattering properties at 37 GHz and comparisons with water ice (snow) measurements

NASA Astrophysics Data System (ADS)

Foster, J. L.; Chang, A. T. C.; Hall, D. K.; Wergin, W. P.; Erbe, E. F.; Barton, J.

1998-11-01

On Earth, the temperature regime is such that water is generally fairly close to its freezing point, and thus relatively small differences in climate affect how much snow and ice are present and whether or not the snow covering will be seasonal or last from one year to the next. On Mars, as on Earth, the presence of ice also plays a role in large-scale climate processes and it is important in controlling the abundance of atmospheric carbon dioxide (CO2) and water vapor. Passive microwave radiometry has been used to derive snow extent and snow depth on Earth, where scattering by snow (H2O) crystals is the dominant effect on the microwave radiation emanating from the ground and emerging from the snowpack. Microwave remote sensing may also prove to be useful for assessing the coverage and thickness of the frozen H2O and CO2 on Mars, but more exact information is needed on how both H2O crystals and frozen CO2 crystals scatter and absorb passive microwave radiation. In this study, CO2 crystals have been produced in a laboratory cold chamber with temperature conditions similar to those found on the polar caps of Mars, and detailed three-dimensional images of their size and shape have been made with a low-temperature scanning electron microscope. Unlike the much larger H2O snow crystals found on Earth, which typically range in size between 0.1 mm and 1.0 mm (radius), CO2 crystals are differently shaped and considerably smaller. Bipyramid crystals (base to base four-sided pyramids) are commonly observed, some as small as 1.0 μm. A discrete dipole model was employed to calculate the passive microwave radiation scattered and absorbed by crystals of various sizes and shapes. Modeling results indicate that the shape of the crystal, whether for frozen CO2 or H2O, is of little consequence in affecting extinction efficiency. However, owing to their smaller size, frozen CO2 crystals are more emissive than the H2O crystals in the 37 GHz region of the microwave spectrum. For the larger sizes of the modeled crystals, scattering dominates over absorption since the particles approach the size of the wavelength. The scattering values are 2 orders of magnitude larger than absorption for the 900 μm size snow particles. For CO2 crystals of 3.0 μm in size, absorption is 7 orders of magnitude greater than scattering.

Evolution of microwave sea ice signatures during early summer and midsummer in the marginal ice zone

NASA Technical Reports Server (NTRS)

Onstott, R. G.; Grenfell, T. C.; Matzler, C.; Luther, C. A.; Svendsen, E. A.

1987-01-01

Emissivities at frequencies from 5 to 94 GHz and backscatter at frequencies from 1 to 17 GHz were measured from sea ice in Fram Strait during the marginal Ice Zone Experiment in June and July of 1983 and 1984. The ice observed was primarily multiyear; the remainder, first-year ice, was often deformed. Results from this active and passive microwave study include the description of the evolution of the sea ice during early summer and midsummer; the absorption properties of summer snow; the interrelationship between ice thickness and the state and thickness of snow; and the modulation of the microwave signature, especially at the highest frequencies, by the freezing of the upper few centimeters of the ice.

Synthesis of Ag@TiO2 core-shells using a rapid microwave irradiation and study of their nonlinear optical properties

NASA Astrophysics Data System (ADS)

Karimipour, M.; Ebrahimi, M.; Abafat, Z.; Molaei, M.

2016-07-01

Ag@TiO2 core-shells were synthesized by employing oleylamine as capping agent and using a rapid microwave method. The shell growth was optimized first based on the variation of oleylamine content in the reaction solution. Thereafter the shell thickness was varied just by varying titanium isopropoxide (TiTP) with 25, 50, 100 and 200 μl as TiO2 precursor. The prepared core-shells were characterized by means of XRD, FTIR spectroscopy, transmission electron microscopy, and UV-Vis spectroscopy. XRD analysis revealed a cubic crystal structure for Ag and Anatase phase for TiO2. TEM images clearly indicated that the size of Ag core is roughly 15 nm and with the increase of TiTP, the shell thickness increases and varies between 5 nm and 15 nm. UV-Vis spectroscopy indicated that the plasmon resonance of Ag nanoparticles shifts from 407 nm up to 454 nm with the increase of TiTP precursor. Using a low power laser diode at a 532 nm wavelength, the magnitude and the sign of the nonlinear refractive index were determined by the Z-scan technique and Sheik-Bahae model. The results show that the enhancement of nonlinear optical properties originates from the quality of TiO2 shell growth. The highest nonlinearity belongs to the sample synthesized with 100 μlit TiTP. Generally all the prepared Ag@TiO2 core-shells show both saturable and reverse saturable absorption. They exhibit also a considerable nonlinear absorption and nonlinear refractive index ranging from -4.21 × 10-7 to -3.51 × 10-6 which are comparable to the sole Ag and TiO2 nanoparticles.

Brillouin Amplification--A Powerful New Scheme for Microwave Photonic Communications

NASA Technical Reports Server (NTRS)

Yao, S.; Maleki, L.

1997-01-01

We introduce the Brillouin selective sideband amplification technique and demonstrate many important applications of this technique in photonic microwave systems, including efficient phase modulation to amplitude modulation conversion, photonic frequency multiplication, photonic signal mixing with gain, and frequency multiplied signal up conversion.

In vivo microwave-based thermoacoustic tomography of rats (Conference Presentation)

NASA Astrophysics Data System (ADS)

Lin, Li; Zhou, Yong; Wang, Lihong V.

2016-03-01

Microwave-based thermoacoustic tomography (TAT), based on the measurement of ultrasonic waves induced by microwave pulses, can reveal tissue dielectric properties that may be closely related to the physiological and pathological status of the tissues. Using microwaves as the excitation source improved imaging depth because of their deep penetration into biological tissues. We demonstrate, for the first time, in vivo microwave-based thermoacoustic imaging in rats. The transducer is rotated around the rat in a full circle, providing a full two-dimensional view. Instead of a flat ultrasonic transducer, we used a virtual line detector based on a cylindrically focused transducer. A 3 GHz microwave source with 0.6 µs pulse width and an electromagnetically shielded transducer with 2.25 MHz central frequency provided clear cross-sectional images of the rat's body. The high imaging contrast, based on the tissue's rate of absorption, and the ultrasonically defined spatial resolution combine to reveal the spine, kidney, muscle, and other deeply seated anatomical features in the rat's abdominal cavity. This non-invasive and non-ionizing imaging modality achieved an imaging depth beyond 6 cm in the rat's tissue. Cancer diagnosis based on information about tissue properties from microwave band TAT can potentially be more accurate than has previously been achievable.

Optimization of enzymes-microwave-ultrasound assisted extraction of Lentinus edodes polysaccharides and determination of its antioxidant activity.

PubMed

Yin, Chaomin; Fan, Xiuzhi; Fan, Zhe; Shi, Defang; Gao, Hong

2018-05-01

Enzymes-microwave-ultrasound assisted extraction (EMUE) method had been used to extract Lentinus edodes polysaccharides (LEPs). The enzymatic temperature, enzymatic pH, microwave power and microwave time were optimized by response surface methodology. The yields, properties and antioxidant activities of LEPs from EMUE and other extraction methods including hot-water extraction, enzymes-assisted extraction, microwave-assisted extraction and ultrasound-assisted extraction were evaluated. The results showed that the highest LEPs yield of 9.38% was achieved with enzymatic temperature of 48°C, enzymatic pH of 5.0, microwave power of 440W and microwave time of 10min, which correlated well with the predicted value of 9.79%. Additionally, LEPs from different extraction methods possessed typical absorption peak of polysaccharides, which meant different extraction methods had no significant effects on type of glycosidic bonds and sugar ring of LEPs. However, SEM images of LEPs from different extraction methods were significantly different. Moreover, the different LEPs all showed antioxidant activities, but LEPs from EMUE showed the highest reducing power when compared to other LEPs. The results indicated LEPs from EMUE can be used as natural antioxidant component in the pharmaceutical and functional food industries. Copyright © 2018 Elsevier B.V. All rights reserved.

The impact of frequency on the performance of microwave ablation.

PubMed

Sawicki, James F; Shea, Jacob D; Behdad, Nader; Hagness, Susan C

2017-02-01

The use of higher frequencies in percutaneous microwave ablation (MWA) may offer compelling interstitial antenna design advantages over the 915 MHz and 2.45 GHz frequencies typically employed in current systems. To evaluate the impact of higher frequencies on ablation performance, we conducted a comprehensive computational and experimental study of microwave absorption and tissue heating as a function of frequency. We performed electromagnetic and thermal simulations of MWA in ex vivo and in vivo porcine muscle at discrete frequencies in the 1.9-26 GHz range. Ex vivo ablation experiments were performed in the 1.9-18 GHz range. We tracked the size of the ablation zone across frequency for constant input power and ablation duration. Further, we conducted simulations to investigate antenna feed line heating as a function of frequency, input power, and cable diameter. As the frequency was increased from 1.9 to 26 GHz the resulting ablation zone dimensions decreased in the longitudinal direction while remaining relatively constant in the radial direction; thus at higher frequencies the overall ablation zone was more spherical. However, cable heating at higher frequencies became more problematic for smaller diameter cables at constant input power. Comparably sized ablation zones are achievable well above 1.9 GHz, despite increasingly localised power absorption. Specific absorption rate alone does not accurately predict ablation performance, particularly at higher frequencies where thermal diffusion plays an important role. Cable heating due to ohmic losses at higher frequencies may be controlled through judicious choices of input power and cable diameter.

Monodisperse NixFe3-xO4 nanospheres: Metal-ion-steered size/composition control mechanism, static magnetic and enhanced microwave absorbing properties

NASA Astrophysics Data System (ADS)

Jiang, Kedan; Liu, Yun; Pan, Yefei; Wang, Ru; Hu, Panbing; He, Rujia; Zhang, Lingli; Tong, Guoxiu

2017-05-01

An easy metal-ion-steered solvothermal method was developed for the one-step synthesis of monodisperse, uniform NixFe3-xO4 polycrystalline nanospheres with tunable sphere diameter (40-400 nm) and composition (0 ≤ x ≤ 0.245) via changing just Ni2+/Fe3+ molar ratio (γ). With g increased from 0:1 to 2:1, sphere diameter gradually decreased and crystal size exhibited an inversed U-shaped change tendency, followed by increased Ni/Fe atom ratio from 0% to 0.0888%. An in situ-reduction, coordination-precipitation transformation mechanism was proposed to interpret the metal-ion-steered growth. Size- and composition-dependent static magnetic and microwave absorbing properties were systematically investigated. Saturation magnetization declines with g in a Boltzmann model due to the changes of crystal size, sphere diameter, and Ni content. The coercivity reaches a maximum at γ = 0.75:1 because of the critical size of Fe3O4 single domain (25 nm). Studies on microwave absorption reveal that 150-400 nm Fe3O4 nanospheres mainly obey the quarter-wavelength cancellation model with the single-band absorption; 40-135 nm NixFe3-xO4 nanospheres (0 ≤ x ≤ 0.245) obey the one and three quarter-wavelength cancellation model with the multi-band absorption. 150 nm Fe3O4 nanospheres exhibit the optimal EM wave-absorbing property with an absorbing band of 8.94 GHz and the maximum RL of -50.11 dB.

Prediction of microwave absorption properties of tetrapod-needle zinc oxide whisker radar absorbing material without prior knowledge

NASA Astrophysics Data System (ADS)

Zhao, Yu-Chen; Wang, Jie; Liu, Jiang-Fan; Song, Zhong-Guo; Xi, Xiao-Li

2017-07-01

The radar absorbing material (RAM) containing a tetrapod-needle zinc oxide whisker (T-ZnOw) has been proved to have good efficiency of microwave absorption. However, the available theoretical models, which are intended to predict the microwave absorbing properties of such an interesting composite, still cannot work well without some prior knowledge, like the measured effective electromagnetic parameters of the prepared T-ZnOw composite. Hence, we propose a novel predictive method here to calculate the reflectivity of T-ZnOw RAM without prior knowledge. In this method, the absorbing ability of this kind of material is divided into three main aspects: the unstructured background, the conductive network, and the nanostructured particle. Then, the attenuation properties of these three parts are represented, respectively, by three different approaches: the equivalent spherical particle and the static strong fluctuation theory, the equivalent circuit model obtained from the complex impedance spectra technology, and the combination of four different microscopic electromagnetic responses. The operational calculation scheme can be obtained by integrating these three absorption effects into the existing theoretical attenuation model. The reasonable agreement between the theoretical and experimental data of a T-ZnON/SiO2 composite in the range of 8-14 GHz shows that the proposed scheme can predict the microwave absorption properties of the T-ZnOw RAM. Furthermore, a detailed analysis of these three mechanisms indicates that, on the one hand, the background plays a dominant role in determining the real part of the effective permittivity of the T-ZnOw composite while the network and the particle are the decisive factors of its material loss; on the other hand, an zero-phase impedance, i.e., a pure resistance, with appropriate resonance characteristic might be a rational physical description of the attenuation property of the conductive network, but it is difficult to realize such an impedance property by the traditional resistance and capacitance network. As a result, a series resonant circuit with a relatively low quality factor is introduced to approximate the material loss caused by the network. Finally, the different combinations of these three absorbing mechanisms are analyzed to further display their roles in the overall absorbing performance.

Effect of Manganese Addition on the Structure, Magnetic Properties and Microwave Absorption of La0.8Ba0.2MnxFe½(1-x)Ti½(1-x)O3

NASA Astrophysics Data System (ADS)

Adi, W. A.; Indro, M. N.; Kusumastuti, A. A.

2017-03-01

We have carried out modification of La0.8Ba0.2MnxFe½(1-x)Ti½(1-x)O3 (x = 0.1 - 0.8) magnetic materials by wet milling method. Raw materials of La2O3, BaCO3, Fe2O3, TiO2 and MnCO3 were mixed according to stoichiometry calculation for each composition. The mixture was milled for 5 hours and then sintered at 1000 °C for 5 hours. The refinement results by X-ray diffraction pattern shows that the increasing Mn composition enhances the mass fraction of La0.8Ba0.2MnxFe½(1-x)Ti½(1-x)O3 phase which has the same structure as LaMnO3. For x = 0.8 a single phase of LaMnO3 was formed. The single phase has a crystal monoclinic crystal structure with space group of I 1 2 / a 1, with lattice parameters given by a = 5.519(5) Å, b = 5.5537(5) Å and c = 7.8176(9) Å, α = γ = 90o and β = 90.345(6)o, V = 239.64(3) Å3, ρ = 6.463 gr.cm-3, wRp = 5.96, and χ2 (chi-squared) = 1.17. The hysteresis curve shows that the sample with composition x = 0.8 produces ferromagnetic behaviour at room temperature. The ferromagnetic properties arise due to the mixed valence of Mn3+ and Mn4+ ions through a double exchange mechanism. The results of the microwave absorption indicated that there was a broadening of absorption peak frequency at 9.9 GHz. The reflection loss (RL) increases with the increasing of LaMnO3 phase. For x = 0.8 we have the best of RL where the microwave absorption was calculated reaching 95% at the highest peak frequency with a thickness of 1.5 mm. Thus we have been successful in creating a single phase of La0.8Ba0.2MnxFe½(1-x)Ti½(1-x)O3 with application as a microwave absorber.

The Role of Engineering Principles in the Medical Utilization of Electromagnetic Energies from kHz to Visible Light - Examples

NASA Astrophysics Data System (ADS)

Rosen, Arye; Rosen, Harel D.

2009-12-01

The use of RF/microwaves in medicine has increased dramatically over the last ten years. RF and microwave therapies for the treatment of cancer in humans are well documented, and are presently used in many cancer centers. RF treatment for supra ventricular arrhythmias, and more recently for the treatment of ventricular tachycardia, are currently employed by major hospitals. RF/microwave are also used in human subjects for the treatment of benign prostatic hyperplasia (BPH). In the last few years, several otolaryngological centers have been utilizing RF to treat upper airway obstruction and to alleviate sleep apnea. Many centers also utilize RF for the treatment of gastro-esophageal disease (GERD), for pain management, and for endometrial ablation. Balloon microwave catheters for ablating solid tumors, then forming cavities in those tumors for the local delivery of therapeutic agents, are currently being investigated. New modalities are being studied, such as RF/microwave for the enhancement of drug absorption and microwave septic wound treatment, microwave imaging for the detection of breast cancer, epidemiological studies on the effects of rats’ exposure to microwave, as well as tissue regeneration using electromagnetic fields. In addition, technology is presently being developed that allows for permanent implantation of microwave wireless sensors in humans. A permanently implantable intra-cranial pressure monitor is one such application of the latter technology. Many more areas of research are currently being investigated, a partial list of which is summarized here.

DOE Office of Scientific and Technical Information (OSTI.GOV)

Tereshchenko, M. A., E-mail: maxt@inbox.ru

A study is made of the microwave beam evolution due to passing through the stagnation zone, where the group velocity vanishes, thus making the paraxial approximation for the wavefield inappropriate. An extension to the standard beam tracing technique is suggested that allows one to calculate the microwave beam parameters on either branch of its path apart from the stagnation zone, omitting the calculation of the wavefield inside it. Application examples of the extended technique are presented for the case of microwave reflection from the upper hybrid resonance layer in a tokamak plasma.

Microwave holographic metrology for antenna diagnosis

NASA Astrophysics Data System (ADS)

Rahmat-Samii, Y.

1990-11-01

Advances in antenna diagnostic methodologies have been very significant in recent years. In particular, microwave holographic diagnostic techniques have been applied very successfully in improving the performance of reflector and array antennas. These techniques use the knowledge of the measured amplitude and phase of the antenna radiated fields and then take advantage of the existing Fourier transform relationships between the radiated fields and the effective aperture or current distribution to eventually determine the reflector surface or array excitation coefficients anomalies. In this paper an overview of the recent developments in applying microwave holography is presented. The theoretical, numerical and measurement aspects of this technique is detailed by providing representative results.

Theoretical Calculation and Validation of the Water Vapor Continuum Absorption

NASA Technical Reports Server (NTRS)

Ma, Qiancheng; Tipping, Richard H.

1998-01-01

The primary objective of this investigation is the development of an improved parameterization of the water vapor continuum absorption through the refinement and validation of our existing theoretical formalism. The chief advantage of our approach is the self-consistent, first principles, basis of the formalism which allows us to predict the frequency, temperature and pressure dependence of the continuum absorption as well as provide insights into the physical mechanisms responsible for the continuum absorption. Moreover, our approach is such that the calculated continuum absorption can be easily incorporated into satellite retrieval algorithms and climate models. Accurate determination of the water vapor continuum is essential for the next generation of retrieval algorithms which propose to use the combined constraints of multispectral measurements such as those under development for EOS data analysis (e.g., retrieval algorithms based on MODIS and AIRS measurements); current Pathfinder activities which seek to use the combined constraints of infrared and microwave (e.g., HIRS and MSU) measurements to improve temperature and water profile retrievals, and field campaigns which seek to reconcile spectrally-resolved and broad-band measurements such as those obtained as part of FIRE. Current widely used continuum treatments have been shown to produce spectrally dependent errors, with the magnitude of the error dependent on temperature and abundance which produces errors with a seasonal and latitude dependence. Translated into flux, current water vapor continuum parameterizations produce flux errors of order 10 W/sq m, which compared to the 4 W/sq m magnitude of the greenhouse gas forcing and the 1-2 W/sq m estimated aerosol forcing is certainly climatologically significant and unacceptably large. While it is possible to tune the empirical formalisms, the paucity of laboratory measurements, especially at temperatures of interest for atmospheric applications, preclude tuning, the empirical continuum models over the full spectral range of interest for remote sensing and climate applications. Thus, we propose to further develop and refine our existing, far-wing formalism to provide an improved treatment applicable from the near-infrared through the microwave. Based on the results of this investigation, we will provide to the remote sensing/climate modeling community a practical and accurate tabulation of the continuum absorption covering the near-infrared through the microwave region of the spectrum for the range of temperatures and pressures of interest for atmospheric applications.

Theoretical Calculation and Validation of the Water Vapor Continuum Absorption

NASA Technical Reports Server (NTRS)

Ma, Qiancheng; Tipping, Richard H.

1998-01-01

The primary objective of this investigation is the development of an improved parameterization of the water vapor continuum absorption through the refinement and validation of our existing theoretical formalism. The chief advantage of our approach is the self-consistent, first principles, basis of the formalism which allows us to predict the frequency, temperature and pressure dependence of the continuum absorption as well as provide insights into the physical mechanisms responsible for the continuum absorption. Moreover, our approach is such that the calculated continuum absorption can be easily incorporated into satellite retrieval algorithms and climate models. Accurate determination of the water vapor continuum is essential for the next generation of retrieval algorithms which propose to use the combined constraints of multi-spectral measurements such as those under development for EOS data analysis (e.g., retrieval algorithms based on MODIS and AIRS measurements); current Pathfinder activities which seek to use the combined constraints of infrared and microwave (e.g., HIRS and MSU) measurements to improve temperature and water profile retrievals, and field campaigns which seek to reconcile spectrally-resolved and broad-band measurements such as those obtained as part of FIRE. Current widely used continuum treatments have been shown to produce spectrally dependent errors, with the magnitude of the error dependent on temperature and abundance which produces errors with a seasonal and latitude dependence. Translated into flux, current water vapor continuum parameterizations produce flux errors of order 10 W/ml, which compared to the 4 W/m' magnitude of the greenhouse gas forcing and the 1-2 W/m' estimated aerosol forcing is certainly climatologically significant and unacceptably large. While it is possible to tune the empirical formalisms, the paucity of laboratory measurements, especially at temperatures of interest for atmospheric applications, preclude tuning the empirical continuum models over the full spectral range of interest for remote sensing and climate applications. Thus, we propose to further develop and refine our existing far-wing formalism to provide an improved treatment applicable from the near-infrared through the microwave. Based on the results of this investigation, we will provide to the remote sensing/climate modeling community a practical and accurate tabulation of the continuum absorption covering the near-infrared through the microwave region of the spectrum for the range of temperatures and pressures of interest for atmospheric applications.

Microwave Three-Wave Mixing Experiments for Chirality Determination: Current Status

NASA Astrophysics Data System (ADS)

Perez, Cristobal; Shubert, V. Alvin; Schmitz, David; Medcraft, Chris; Krin, Anna; Schnell, Melanie

2015-06-01

Microwave three-wave mixing experiments have been shown to provide a novel and sensitive way to generate and measure enantiomer-specific molecular signatures. The handedness of the sample can be obtained from the phase of the molecular free induction decay whereas the enantiomeric excess can be determined by the amplitude of the chiral signal. After the introduction of this technique by Patterson et al. remarkable improvements have been realized and experimental strategies for both absolute phase determination and enantiomeric excess have been presented. This technique has been also successfully implemented at higher microwave frequencies. Here we present the current status of this technique as well future directions and perspectives. This will be illustrated through our systematic study of chiral terpenes as well as preliminary results in molecular clusters. Patterson, D.; Schnell, M.; Doyle, J. M. Enantiomer-Specific Detection of Chiral Molecules via Microwave Spectroscopy. Nature 2013, 497, 475-477. Patterson, D.; Doyle, J. M. Sensitive Chiral Analysis via Microwave Three-Wave Mixing. Phys. Rev. Lett. 2013, 111, 023008. Shubert, V. A.; Schmitz, D.; Patterson, D.; Doyle, J. M.; Schnell, M. Identifying Enantiomers in Mixtures of Chiral Molecules with Broadband Microwave Spectroscopy. Angew. Chem. Int. Ed. 2014, 53, 1152-1155. Lobsiger, S.; Perez, C.; Evangelisti, L.; Lehmann, K. K.; Pate, B. H. Molecular Structure and Chirality Detection by Fourier Transform Microwave Spectroscopy. J. Phys. Chem. Lett. 2014, 6, 196-200.

Use of a microwave diagnostics technique to measure the temperature of an axisymmetric ionized gas flow

NASA Astrophysics Data System (ADS)

Tsel'Sov, Iu. G.; Kondrat'ev, A. S.

1990-12-01

A method is developed for determining the temperature of an ionized gas on the basis of electron-density sounding. This technique is used to measure the cross-sectional temperature distribution of an axisymmetric ionized gas flow using microwave diagnostics.

Determination of multi-walled carbon nanotube bioaccumulation in earthworms measured by a microwave-based detection technique

EPA Science Inventory

Reliable quantification techniques for carbon nanotubes (CNTs) are limited. In this study, a new procedure was developed for quantifying multi-walled carbon nanotubes (MWNTs) in earthworms (Eisenia fetida) based on freeze drying and microwave-induced heating. Specifically, earthw...

The free jet microwave spectrum of 2-phenylethylamine-water.

PubMed

Melandri, Sonia; Maris, Assimo; Giuliano, Barbara M; Favero, Laura B; Caminati, Walther

2010-09-21

We observed the rotational spectrum of the 1:1 molecular adduct between 2-phenylethylamine and water (normal and H(2)(18)O species) by free jet absorption microwave spectroscopy in the frequency region 60-78 GHz. The dominant spectrum belongs to the structure where the PEA moiety is in the most stable gauche conformation and the water molecule is hydrogen bound to the nitrogen lone pair. The orientation of the water molecule is such that the oxygen atom is almost equidistant (ca. 2.5 A) from the closest methylenic and aromatic hydrogen atoms.

Omni-directional selective shielding material based on amorphous glass coated microwires.

PubMed

Ababei, G; Chiriac, H; David, V; Dafinescu, V; Nica, I

2012-01-01

The shielding effectiveness of the omni-directional selective shielding material based on CoFe-glass coated amorphous wires in 0.8 GHz-3 GHz microwave frequency range is investigated. The measurements were done in a controlled medium using a TEM cell and in the free space using horn antennas, respectively. Experimental results indicate that the composite shielding material can be developed with desired shielding effectiveness and selective absorption of the microwave frequency range by controlling the number of the layers and the length of microwires.

Characterization of weakly ionized argon flows for radio blackout mitigation experiments

NASA Astrophysics Data System (ADS)

Steffens, L.; Koch, U.; Esser, B.; Gülhan, A.

2017-06-01

For reproducing the so-called E × B communication blackout mitigation scheme inside the L2K arc heated facility of the DLR in weakly ionized argon §ows, a §at plate model has been equipped with a superconducting magnet, electrodes, and a setup comprising microwave plasma transmission spectroscopy (MPTS). A thorough characterization of the weakly ionized argon §ow has been performed including the use of microwave interferometry (MWI), Langmuir probe measurements, Pitot probe pro¦les, and spectroscopic methods like diode laser absorption spectroscopy (DLAS) and emission spectroscopy.

Atmospheric influences on infrared-laser signals used for occultation measurements between Low Earth Orbit satellites

NASA Astrophysics Data System (ADS)

Schweitzer, S.; Kirchengast, G.; Proschek, V.

2011-10-01

LEO-LEO infrared-laser occultation (LIO) is a new occultation technique between Low Earth Orbit (LEO) satellites, which applies signals in the short wave infrared spectral range (SWIR) within 2 μm to 2.5 μm. It is part of the LEO-LEO microwave and infrared-laser occultation (LMIO) method that enables to retrieve thermodynamic profiles (pressure, temperature, humidity) and altitude levels from microwave signals and profiles of greenhouse gases and further variables such as line-of-sight wind speed from simultaneously measured LIO signals. Due to the novelty of the LMIO method, detailed knowledge of atmospheric influences on LIO signals and of their suitability for accurate trace species retrieval did not yet exist. Here we discuss these influences, assessing effects from refraction, trace species absorption, aerosol extinction and Rayleigh scattering in detail, and addressing clouds, turbulence, wind, scattered solar radiation and terrestrial thermal radiation as well. We show that the influence of refractive defocusing, foreign species absorption, aerosols and turbulence is observable, but can be rendered small to negligible by use of the differential transmission principle with a close frequency spacing of LIO absorption and reference signals within 0.5%. The influences of Rayleigh scattering and terrestrial thermal radiation are found negligible. Cloud-scattered solar radiation can be observable under bright-day conditions, but this influence can be made negligible by a close time spacing (within 5 ms) of interleaved laser-pulse and background signals. Cloud extinction loss generally blocks SWIR signals, except very thin or sub-visible cirrus clouds, which can be addressed by retrieving a cloud layering profile and exploiting it in the trace species retrieval. Wind can have a small influence on the trace species absorption, which can be made negligible by using a simultaneously retrieved or a moderately accurate background wind speed profile. We conclude that the set of SWIR channels proposed for implementing the LMIO method (Kirchengast and Schweitzer, 2011) provides adequate sensitivity to accurately retrieve eight trace species of key importance to climate and atmospheric chemistry (H2O, CO2, 13CO2, C18OO, CH4, N2O, O3, CO) in the upper troposphere/lower stratosphere region outside clouds under all atmospheric conditions. Two further species (HDO, H218O) can be retrieved in the upper troposphere.

ADVANCES IN GREEN CHEMISTRY: CHEMICAL SYNTHESES USING MICROWAVE IRRADIATION, ISBN 81-901238-5-8

EPA Science Inventory

16. Abstract Advances in Green Chemistry: Chemical Syntheses Using Microwave Irradiation
Microwave-accelerated chemical syntheses in solvents as well as under solvent-free conditions have witnessed an explosive growth. The technique has found widespread application predomi...

Microwave-Assisted Organic Synthesis and Transformations using Benign Reaction Media

EPA Science Inventory

The nonclassical heating technique using microwaves, termed as 'Bunsen burner of the 21st century, is rapidly becoming popular and is dramatically reducing the reaction times. The significant outcomes of microwave (MW)-assisted green chemistry endeavors are summarized that have r...

Microwave signatures of ice hydrometeors from ground-based observations above Summit, Greenland

DOE PAGES

Pettersen, Claire; Bennartz, Ralf; Kulie, Mark S.; ...

2016-04-15

Multi-instrument, ground-based measurements provide unique and comprehensive data sets of the atmosphere for a specific location over long periods of time and resulting data compliment past and existing global satellite observations. Our paper explores the effect of ice hydrometeors on ground-based, high-frequency passive microwave measurements and attempts to isolate an ice signature for summer seasons at Summit, Greenland, from 2010 to 2013. Furthermore, data from a combination of passive microwave, cloud radar, radiosonde, and ceilometer were examined to isolate the ice signature at microwave wavelengths. By limiting the study to a cloud liquid water path of 40 g m -2more » or less, the cloud radar can identify cases where the precipitation was dominated by ice. These cases were examined using liquid water and gas microwave absorption models, and brightness temperatures were calculated for the high-frequency microwave channels: 90, 150, and 225GHz. By comparing the measured brightness temperatures from the microwave radiometers and the calculated brightness temperature using only gas and liquid contributions, any residual brightness temperature difference is due to emission and scattering of microwave radiation from the ice hydrometeors in the column. The ice signature in the 90, 150, and 225 GHz channels for the Summit Station summer months was isolated. Then, this measured ice signature was compared to an equivalent brightness temperature difference calculated with a radiative transfer model including microwave single-scattering properties for several ice habits. Furthermore, initial model results compare well against the 4 years of summer season isolated ice signature in the high-frequency microwave channels.« less

Preface to the special issue on "Integrated Microwave Photonic Signal Processing"

NASA Astrophysics Data System (ADS)

Azaña, José; Yao, Jianping

2016-08-01

As Guest Editors, we are pleased to introduce this special issue on ;Integrated Microwave Photonic Signal Processing; published by the Elsevier journal Optics Communications. Microwave photonics is a field of growing importance from both scientific and practical application perspectives. The field of microwave photonics is devoted to the study, development and application of optics-based techniques and technologies aimed to the generation, processing, control, characterization and/or distribution of microwave signals, including signals well into the millimeter-wave frequency range. The use of photonic technologies for these microwave applications translates into a number of key advantages, such as the possibility of dealing with high-frequency, wide bandwidth signals with minimal losses and reduced electromagnetic interferences, and the potential for enhanced reconfigurability. The central purpose of this special issue is to provide an overview of the state of the art of generation, processing and characterization technologies for high-frequency microwave signals. It is now widely accepted that the practical success of microwave photonics at a large scale will essentially depend on the realization of high-performance microwave-photonic signal-processing engines in compact and integrated formats, preferably on a chip. Thus, the focus of the issue is on techniques implemented using integrated photonic technologies, with the goal of providing an update of the most recent advances toward realization of this vision.

Evaluation of nondestructive testing techniques for the space shuttle nonmetallic thermal protection system

NASA Technical Reports Server (NTRS)

Tiede, D. A.

1972-01-01

A program was conducted to evaluate nondestructive analysis techniques for the detection of defects in rigidized surface insulation (a candidate material for the Space Shuttle thermal protection system). Uncoated, coated, and coated and bonded samples with internal defects (voids, cracks, delaminations, density variations, and moisture content), coating defects (holes, cracks, thickness variations, and loss of adhesion), and bondline defects (voids and unbonds) were inspected by X-ray radiography, acoustic, microwave, high-frequency ultrasonic, beta backscatter, thermal, holographic, and visual techniques. The detectability of each type of defect was determined for each technique (when applicable). A possible relationship between microwave reflection measurements (or X-ray-radiography density measurements) and the tensile strength was established. A possible approach for in-process inspection using a combination of X-ray radiography, acoustic, microwave, and holographic techniques was recommended.

Enhanced microwave absorption properties of CTAB assisted Pr-Cu substituted nanomaterial

NASA Astrophysics Data System (ADS)

Sadiq, Imran; Naseem, Shahzad; Riaz, Saira; Khan, Hasan M.; Ashiq, Muhammad Naeem; Hussain, S. Sajjad; Rana, Mazhar

2016-09-01

In this study, the rare earth Pr3+and divalent Cu2+ elements substituted Sr1-xPrxMn2Fe16-yCuyO27 (x=0, 0.02, 0.06, 0.1 and y=0, 0.1, 0.3, 0.5) W-type hexagonal ferrites were prepared by Sol-Gel method. TGA and DSC analysis of as prepared material was carried out to confirm the temperature at which required phase can be obtained. The XRD patterns exhibit the single phase for all the samples and the lattice parameters were changed with the additives. The absorption bands at wave number 636 and 554 cm-1 in FTIR spectrum indicate the stretching vibration of metal-oxygen ions which also ratifies the single phase for the prepared material. Microstructural analysis confirms the agglomeration of nanograins which leads to formation of platelet like structure which cause in the enhancement of the microwave absorption properties of material. The minimum reflection loss of -59.8 dB at 9.34 GHz frequency was observed makes the prepared material good candidate to be used in super high frequency application. The attenuation constant and reflectivity results are also in good agreement with minimum reflection losses results.

Core@shell@shell structured carbon-based magnetic ternary nanohybrids: Synthesis and their enhanced microwave absorption properties

NASA Astrophysics Data System (ADS)

Yang, Erqi; Qi, Xiaosi; Xie, Ren; Bai, Zhongchen; Jiang, Yang; Qin, Shuijie; Zhong, Wei; Du, Youwei

2018-05-01

High encapsulation efficiency of core@shell@shell structured carbon-based magnetic ternary nanohybrids have been synthesized in high yield by chemical vapor deposition of acetylene directly over octahedral-shaped Fe2O3 nanoparticles. By controlling the pyrolysis temperature, Fe3O4@Fe3C@carbon nanotubes (CNTs) and Fe@Fe3C@CNTs ternary nanohybrids could be selectively produced. The optimal RL values for the as-prepared ternary nanohybrids could reach up to ca. -46.7, -52.7 and -29.5 dB, respectively. The excellent microwave absorption properties of the obtaiend ternary nanohybrids were proved to ascribe to the quarter-wavelength matching model. Moreover, the as-prepared Fe@Fe3C@CNTs ternary nanohybrids displayed remarkably enhanced EM wave absorption capabilities compared to Fe3O4@Fe3C@CNTs due to their excellent dielectric loss abilities, good complementarities between the dielectric loss and the magnetic loss, and high attenuation constant. Generally, this strategy can be extended to explore other categories of core@shell or core@shell@shell structured carbon-based nanohybrids, which is very beneficial to accelerate the advancements of high performance MAMs.

Electromagnetic-wave propagation in unmagnetized plasmas

NASA Astrophysics Data System (ADS)

Gregoire, D. J.; Santoru, J.; Schumacher, R. W.

1992-03-01

This final report describes an investigation of electromagnetic-wave propagation in unmagnetized plasmas and its application to the reduction of the radar cross section (RCS) of a plasma-filled enclosure. We have demonstrated RCS reduction of 20 to 25 dB with a prototype system at the radar range at Hughes Aircraft's Microwave Products Division in Torrance. The prototype consists of a sealed ceramic enclosure with a microwave reflector and a plasma generator inside it. When the plasma is present, the RCS is significantly reduced over a frequency range of 4 to 14 GHz. As part of the program, we also investigated the basic-plasma-physics issues relating to the absorption and refraction of electromagnetic (EM) waves in collisional plasmas. We demonstrated absorption as high as 63 dB in a section of plasma-loaded C-band rectangular waveguide. We also developed a theoretical model for the plasma cloaking process that includes scattering contributions from the plasma-vacuum interface, partial reflections from the plasma, and collisional absorption in the plasma. The theoretical model is found to be in reasonable agreement with the experimental results and can be used to confidently design future plasma cloaking systems.

Asymmetric absorption and emission of energy by a macroscopic mechanical oscillator in a microwave circuit optomechanical system

NASA Astrophysics Data System (ADS)

Harlow, Jennifer; Palomaki, Tauno; Kerckhoff, Joseph; Teufel, John; Simmonds, Raymond; Lehnert, Konrad

2012-02-01

We measure the asymmetry in rates for emission and absorption of mechanical energy in an electromechanical system composed of a macroscopic suspended membrane coupled to a high-Q, superconducting microwave resonant circuit. This asymmetry is inherently quantum mechanical because it arises from the inability to annihilate the mechanical ground state. As such, it is only appreciable when the average mechanical occupancy approaches one. This measurement is now possible due to the recent achievement of ground state cooling of macroscopic mechanical oscillators [1,2]. Crucially, we measure the thermal cavity photon occupancy and account for it in our analysis. Failure to correctly account for the interference of these thermal photons with the mechanical signal can lead to a misinterpretation of the data and an overestimate of the emission/absorption asymmetry. [4pt] [1] J. D. Teufel, T. Donner, Dale Li, J. W. Harlow, M. S. Allman, K. Cicak, A. J. Sirois, J. D. Whittaker, K. W. Lehnert, R. W. Simmonds, ``Sideband Cooling Micromechanical Motion to the Quantum Ground State,'' Nature, 475, 359-363 (2011).[0pt] [2] Jasper Chan, et al, ``Laser cooling of a nanomechanical oscillator into its quantum ground state,'' Nature, 478, 89-92 (2011).

Microwave absorptivity by sulfuric acid in the Venus atmosphere derived from the Venus Express Radio Science Experiment VeRa

NASA Astrophysics Data System (ADS)

Oschlisniok, J.; Pätzold, M.; Häusler, B.; Tellmann, S.; Bird, M.; Andert, T.; Remus, S.; Krüger, C.; Mattei, R.

2011-10-01

Earth's nearest planetary neighbour Venus is shrouded within a roughly 22 km thick three-layered cloud deck, which is located approximately 48 km above the surface and extends to an altitude of about 70 km. The clouds are mostly composed of sulfuric acid. The latter is responsible for a strong absorption of radio signals at microwaves, which is observed in radio occultation experiments. The absorption of the radio signal intensity is used to determine the abundance of H2SO4. This way a detailed study of the H2SO4 height distribution within the cloud deck is possible. The Venus Express spacecraft is orbiting Venus since 2006. The Radio Science Experiment VeRa onboard probes the atmosphere with radio signals at 3.4 cm (X-Band) and 13 cm (S-Band). Absorptivity profiles of the 3.4 cm radio wave and the resulting vertical sulfuric acid profiles in the cloud region of Venus' atmosphere are presented. The three-layered structure and a distinct latitudinal variation of H2SO4 are observed. Convective atmospheric motions within the equatorial latitudes, which transport absorbing material from lower to higher altitudes, are clearly visible. Results of the Venus Monitoring Camera (VMC) and the Visible and Infrared Thermal Imaging Spectrometer (VIRTIS) are compared with the VeRa results.

Observation of microwave absorption and emission from incoherent electron tunneling through a normal-metal-insulator-superconductor junction.

PubMed

Masuda, Shumpei; Tan, Kuan Y; Partanen, Matti; Lake, Russell E; Govenius, Joonas; Silveri, Matti; Grabert, Hermann; Möttönen, Mikko

2018-03-02

We experimentally study nanoscale normal-metal-insulator-superconductor junctions coupled to a superconducting microwave resonator. We observe that bias-voltage-controllable single-electron tunneling through the junctions gives rise to a direct conversion between the electrostatic energy and that of microwave photons. The measured power spectral density of the microwave radiation emitted by the resonator exceeds at high bias voltages that of an equivalent single-mode radiation source at 2.5 K although the phonon and electron reservoirs are at subkelvin temperatures. Measurements of the generated power quantitatively agree with a theoretical model in a wide range of bias voltages. Thus, we have developed a microwave source which is compatible with low-temperature electronics and offers convenient in-situ electrical control of the incoherent photon emission rate with a predetermined frequency, without relying on intrinsic voltage fluctuations of heated normal-metal components or suffering from unwanted losses in room temperature cables. Importantly, our observation of negative generated power at relatively low bias voltages provides a novel type of verification of the working principles of the recently discovered quantum-circuit refrigerator.

Miniature modular microwave end-to-end receiver

NASA Technical Reports Server (NTRS)

Sukamto, Lin M. (Inventor); Cooley, Thomas W. (Inventor); Janssen, Michael A. (Inventor); Parks, Gary S. (Inventor)

1993-01-01

An end-to-end microwave receiver system contained in a single miniature hybrid package mounted on a single heatsink is presented. It includes an input end connected to a microwave receiver antenna and an output end which produces a digital count proportional to the amplitude of a signal of a selected microwave frequency band received at the antenna and corresponding to one of the water vapor absorption lines near frequencies of 20 GHz or 30 GHz. The hybrid package is on the order of several centimeters in length and a few centimeters in height and width. The package includes an L-shaped carrier having a base surface, a vertical wall extending up from the base surface and forming a corner therewith, and connection pins extending through the vertical wall. Modular blocks rest on the base surface against the vertical wall and support microwave monolithic integrated circuits on top surfaces thereof connected to the external connection pins. The modular blocks lie end-to-end on the base surface so as to be modularly removable by sliding along the base surface beneath the external connection pins away from the vertical wall.

Electro-optic modulation of a laser at microwave frequencies for interferometric purposes

NASA Astrophysics Data System (ADS)

Specht, Paul E.; Jilek, Brook A.

2017-02-01

A multi-point microwave interferometer (MPMI) concept was previously proposed by the authors for spatially-resolved, non-invasive tracking of a shock, reaction, or detonation front in energetic media [P. Specht et al., AIP Conf. Proc. 1793, 160010 (2017).]. The advantage of the MPMI concept over current microwave interferometry techniques is its detection of Doppler shifted microwave signals through electro-optic (EO) modulation of a laser. Since EO modulation preserves spatial variations in the Doppler shift, collecting the EO modulated laser light into a fiber array for recording with an optical heterodyne interferometer yields spatially-resolved velocity information. This work demonstrates the underlying physical principle of the MPMI diagnostic: the monitoring of a microwave signal with nanosecond temporal resolution using an optical heterodyne interferometer. For this purpose, the MPMI concept was simplified to a single-point construction using two tunable 1550 nm lasers and a 35.2 GHz microwave source. A (110) ZnTe crystal imparted the microwave frequency onto a laser, which was combined with a reference laser for determination of the microwave frequency in an optical heterodyne interferometer. A single, characteristic frequency associated with the microwave source was identified in all experiments, providing a means to monitor a microwave signal on nanosecond time scales. Lastly, areas for improving the frequency resolution of this technique are discussed, focusing on increasing the phase-modulated signal strength.

Electro-optic modulation of a laser at microwave frequencies for interferometric purposes.

PubMed

Specht, Paul E; Jilek, Brook A

2017-02-01

A multi-point microwave interferometer (MPMI) concept was previously proposed by the authors for spatially-resolved, non-invasive tracking of a shock, reaction, or detonation front in energetic media [P. Specht et al., AIP Conf. Proc. 1793, 160010 (2017).]. The advantage of the MPMI concept over current microwave interferometry techniques is its detection of Doppler shifted microwave signals through electro-optic (EO) modulation of a laser. Since EO modulation preserves spatial variations in the Doppler shift, collecting the EO modulated laser light into a fiber array for recording with an optical heterodyne interferometer yields spatially-resolved velocity information. This work demonstrates the underlying physical principle of the MPMI diagnostic: the monitoring of a microwave signal with nanosecond temporal resolution using an optical heterodyne interferometer. For this purpose, the MPMI concept was simplified to a single-point construction using two tunable 1550 nm lasers and a 35.2 GHz microwave source. A (110) ZnTe crystal imparted the microwave frequency onto a laser, which was combined with a reference laser for determination of the microwave frequency in an optical heterodyne interferometer. A single, characteristic frequency associated with the microwave source was identified in all experiments, providing a means to monitor a microwave signal on nanosecond time scales. Lastly, areas for improving the frequency resolution of this technique are discussed, focusing on increasing the phase-modulated signal strength.

Microwave-assisted synthesis of water-soluble, fluorescent gold nanoclusters capped with small organic molecules and a revealing fluorescence and X-ray absorption study

NASA Astrophysics Data System (ADS)

Helmbrecht, C.; Lützenkirchen-Hecht, D.; Frank, W.

2015-03-01

Colourless solutions of blue light-emitting, water-soluble gold nanoclusters (AuNC) were synthesized from gold colloids under microwave irradiation using small organic molecules as ligands. Stabilized by 1,3,5-triaza-7-phosphaadamantane (TPA) or l-glutamine (GLU), fluorescence quantum yields up to 5% were obtained. AuNC are considered to be very promising for biological labelling, optoelectronic devices and light-emitting materials but the structure-property relationships have still not been fully clarified. To expand the knowledge about the AuNC apart from their fluorescent properties they were studied by X-ray absorption spectroscopy elucidating the oxidation state of the nanoclusters' gold atoms. Based on curve fitting of the XANES spectra in comparison to several gold references, optically transparent fluorescent AuNC are predicted to be ligand-stabilized Au5+ species. Additionally, their near edge structure compared with analogous results of polynuclear clusters known from the literature discloses an increasing intensity of the feature close to the absorption edge with decreasing cluster size. As a result, a linear relationship between the cluster size and the X-ray absorption coefficient can be established for the first time.Colourless solutions of blue light-emitting, water-soluble gold nanoclusters (AuNC) were synthesized from gold colloids under microwave irradiation using small organic molecules as ligands. Stabilized by 1,3,5-triaza-7-phosphaadamantane (TPA) or l-glutamine (GLU), fluorescence quantum yields up to 5% were obtained. AuNC are considered to be very promising for biological labelling, optoelectronic devices and light-emitting materials but the structure-property relationships have still not been fully clarified. To expand the knowledge about the AuNC apart from their fluorescent properties they were studied by X-ray absorption spectroscopy elucidating the oxidation state of the nanoclusters' gold atoms. Based on curve fitting of the XANES spectra in comparison to several gold references, optically transparent fluorescent AuNC are predicted to be ligand-stabilized Au5+ species. Additionally, their near edge structure compared with analogous results of polynuclear clusters known from the literature discloses an increasing intensity of the feature close to the absorption edge with decreasing cluster size. As a result, a linear relationship between the cluster size and the X-ray absorption coefficient can be established for the first time. Electronic supplementary information (ESI) available: The deconvoluted reference spectra are given in ESI Fig. 1-9. See DOI: 10.1039/c4nr07051h

Computer-Aided Design of Low-Noise Microwave Circuits

NASA Astrophysics Data System (ADS)

Wedge, Scott William

1991-02-01

Devoid of most natural and manmade noise, microwave frequencies have detection sensitivities limited by internally generated receiver noise. Low-noise amplifiers are therefore critical components in radio astronomical antennas, communications links, radar systems, and even home satellite dishes. A general technique to accurately predict the noise performance of microwave circuits has been lacking. Current noise analysis methods have been limited to specific circuit topologies or neglect correlation, a strong effect in microwave devices. Presented here are generalized methods, developed for computer-aided design implementation, for the analysis of linear noisy microwave circuits comprised of arbitrarily interconnected components. Included are descriptions of efficient algorithms for the simultaneous analysis of noisy and deterministic circuit parameters based on a wave variable approach. The methods are therefore particularly suited to microwave and millimeter-wave circuits. Noise contributions from lossy passive components and active components with electronic noise are considered. Also presented is a new technique for the measurement of device noise characteristics that offers several advantages over current measurement methods.

Determination of solid-propellant transient regression rates using a microwave Doppler shift technique

NASA Technical Reports Server (NTRS)

Strand, L. D.; Schultz, A. L.; Reedy, G. K.

1972-01-01

A microwave Doppler shift system, with increased resolution over earlier microwave techniques, was developed for the purpose of measuring the regression rates of solid propellants during rapid pressure transients. A continuous microwave beam is transmitted to the base of a burning propellant sample cast in a metal waveguide tube. A portion of the wave is reflected from the regressing propellant-flame zone interface. The phase angle difference between the incident and reflected signals and its time differential are continuously measured using a high resolution microwave network analyzer and related instrumentation. The apparent propellant regression rate is directly proportional to this latter differential measurement. Experiments were conducted to verify the (1) spatial and time resolution of the system, (2) effect of propellant surface irregularities and compressibility on the measurements, and (3) accuracy of the system for quasi-steady-state regression rate measurements. The microwave system was also used in two different transient combustion experiments: in a rapid depressurization bomb, and in the high-frequency acoustic pressure environment of a T-burner.

Microwave absorption property of the diatomite coated by Fe-CoNiP films

NASA Astrophysics Data System (ADS)

Yan, Zhenqiang; Cai, Jun; Xu, Yonggang; Zhang, Deyuan

2015-08-01

A bio-absorbent of Fe-CoNiP coated on the diatomite was fabricated by way of electroless plating of CoNiP and subsequent chemical vapor deposition of Fe. The surface morphology and composition of the above-mentioned diatomite particles at different stage were characterized with the scanning electron microscopy and the energy spectrum analysis respectively, and the results showed that the diatomite was successfully coated with CoNoP and Fe (carbony iron). The complex permittivity and permeability of composites filled with the bio-absorbent and paraffin was measured in frequency range of 2-18 GHz, and then the microwave reflection loss (RL) and the shielding effectiveness (SE) were calculated. The results showed that the permittivity and the permeability were both enlarged as Fe films were coated onto the CoNiP-coated diatomite, which was attributed to the excellent electromagnetic property of carbonyl irons. The composites made with the Fe-CoNiP diatomite had a better absorbing property (minimum RL -11.0 dB) as well as the shielding property (maximum SE 5.6 dB) at thickness 2 mm. It indicated the absorption property was mainly due to the attenuation on the microwave, and the Fe-CoNiP diatomite could be an effective absorbent with low-density.

Laboratory evaluation and application of microwave absorption properties under simulated conditions for planetary atmospheres

NASA Technical Reports Server (NTRS)

Steffes, Paul G.

1989-01-01

Radio absorptivity data for planetary atmospheres obtained from spacecraft radio occultation experiments and earth-based radio astronomical observations can be used to infer abundances of microwave absorbing atmospheric constituents in those atmospheres, as long as reliable information regarding the microwave absorbing properties of potential constituents is available. Work performed has shown that laboratory measurements of the millimeter-wave opacity of ammonia between 7.5 mm and 9.3 mm and also at the 3.2 mm wavelength require a different lineshape to be used in the theoretical prediction for millimeter-wave ammonia opacity than was previously used. The recognition of the need to make such laboratory measurements of simulated planetary atmospheres over a range of temperatures and pressures which correspond to the altitudes probed by both radio occultation experiments and radio astronomical observations, and over a range of frequencies which correspond to those used in both radio occultation experiments and radio astronomical observations, has led to the development of a facility at Georgia Tech which is capable of making such measurements. It has been the goal of this investigation to conduct such measurements and to apply the results to a wide range of planetary observations, both spacecraft and earth-based, in order to determine the identity and abundance profiles of constituents in those planetary atmospheres.

Using x-ray mammograms to assist in microwave breast image interpretation.

PubMed

Curtis, Charlotte; Frayne, Richard; Fear, Elise

2012-01-01

Current clinical breast imaging modalities include ultrasound, magnetic resonance (MR) imaging, and the ubiquitous X-ray mammography. Microwave imaging, which takes advantage of differing electromagnetic properties to obtain image contrast, shows potential as a complementary imaging technique. As an emerging modality, interpretation of 3D microwave images poses a significant challenge. MR images are often used to assist in this task, and X-ray mammograms are readily available. However, X-ray mammograms provide 2D images of a breast under compression, resulting in significant geometric distortion. This paper presents a method to estimate the 3D shape of the breast and locations of regions of interest from standard clinical mammograms. The technique was developed using MR images as the reference 3D shape with the future intention of using microwave images. Twelve breast shapes were estimated and compared to ground truth MR images, resulting in a skin surface estimation accurate to within an average Euclidean distance of 10 mm. The 3D locations of regions of interest were estimated to be within the same clinical area of the breast as corresponding regions seen on MR imaging. These results encourage investigation into the use of mammography as a source of information to assist with microwave image interpretation as well as validation of microwave imaging techniques.

Free radical propulsion concept

NASA Technical Reports Server (NTRS)

Hawkins, C. E.; Nakanishi, S.

1981-01-01

A free radical propulsion concept utilizing the recombination energy of dissociated low molecular weight gases to produce thrust was examined. The concept offered promise of a propulsion system operating at a theoretical impulse, with hydrogen, as high as 2200 seconds at high thrust to power ratio, thus filling the gas existing between chemical and electrostatic propulsion capabilities. Microwave energy used to dissociate a continuously flowing gas was transferred to the propellant via three body recombination for conversion to propellant kinetic energy. Power absorption by the microwave plasma discharge was in excess of 90 percent over a broad range of pressures. Gas temperatures inferred from gas dynamic equations showed much higher temperatures from microwave heating than from electrothermal heating. Spectroscopic analysis appeared to corroborate the inferred temperatures of one of the gases tested.

Water-soluble loratadine inclusion complex: analytical control of the preparation by microwave irradiation.

PubMed

Nacsa, A; Ambrus, R; Berkesi, O; Szabó-Révész, P; Aigner, Z

2008-11-04

The majority of active pharmaceutical ingredients are poorly soluble in water. The rate-determining step of absorption is the dissolution of these drugs. Inclusion complexation with cyclodextrin derivatives can lead to improved aqueous solubility and bioavailability of pharmacons due to the formation of co-crystals through hydrogen-bonding between the components. Inclusion complexes of loratadine were prepared by a convenient new method involving microwave irradiation and the products were compared with those of a conventional preparation method. Dissolution studies demonstrated that the solubility and rate of dissolution of loratadine increased in both of the methods used. The interactions between the components were investigated by thermal analysis and Fourier Transform Infrared studies. The microwave treatment did not cause any chemical changes in the loratadine molecule.

Microwave-assisted incorporation of silver nanoparticles in paper for point-of-use water purification

PubMed Central

Dankovich, Theresa A.

2014-01-01

This work reports an environmentally benign method for the in situ preparation of silver nanoparticles (AgNPs) in paper using microwave irradiation. Through thermal evaporation, microwave heating with an excess of glucose relative to the silver ion precursor yields nanoparticles on the surface of cellulose fibers within three minutes. Paper sheets were characterized by electron microscopy, UV-Visible reflectance spectroscopy, and atomic absorption spectroscopy. Antibacterial activity and silver release from the AgNP sheets were assessed for model Escherichia coli and Enterococci faecalis bacteria in deionized water and in suspensions that also contained with various influent solution chemistries, i.e. with natural organic matter, salts, and proteins. The paper sheets containing silver nanoparticles were effective in inactivating the test bacteria as they passed through the paper. PMID:25400935

ARTS, the Atmospheric Radiative Transfer Simulator - version 2.2, the planetary toolbox edition

NASA Astrophysics Data System (ADS)

Buehler, Stefan A.; Mendrok, Jana; Eriksson, Patrick; Perrin, Agnès; Larsson, Richard; Lemke, Oliver

2018-04-01

This article describes the latest stable release (version 2.2) of the Atmospheric Radiative Transfer Simulator (ARTS), a public domain software for radiative transfer simulations in the thermal spectral range (microwave to infrared). The main feature of this release is a planetary toolbox that allows simulations for the planets Venus, Mars, and Jupiter, in addition to Earth. This required considerable model adaptations, most notably in the area of gaseous absorption calculations. Other new features are also described, notably radio link budgets (including the effect of Faraday rotation that changes the polarization state) and the treatment of Zeeman splitting for oxygen spectral lines. The latter is relevant, for example, for the various operational microwave satellite temperature sensors of the Advanced Microwave Sounding Unit (AMSU) family.

High resolution spectroscopy in the microwave and far infrared

NASA Technical Reports Server (NTRS)

Pickett, Herbert M.

1990-01-01

High resolution rotational spectroscopy has long been central to remote sensing techniques in atmospheric sciences and astronomy. As such, laboratory measurements must supply the required data to make direct interpretation of data for instruments which sense atmospheres using rotational spectra. Spectral measurements in the microwave and far infrared regions are also very powerful tools when combined with infrared measurements for characterizing the rotational structure of vibrational spectra. In the past decade new techniques were developed which have pushed high resolution spectroscopy into the wavelength region between 25 micrometers and 2 mm. Techniques to be described include: (1) harmonic generation of microwave sources, (2) infrared laser difference frequency generation, (3) laser sideband generation, and (4) ultrahigh resolution interferometers.

Three-phase heterostructures f-NiFe2O4/PANI/PI EMI shielding fabric with high Microwave Absorption Performance

NASA Astrophysics Data System (ADS)

Wang, Yu; Wang, Wei; Yu, Dan

2017-12-01

In this work, a three-phase heterostructures f-NiFe2O4/PANI/PI EMI shielding fabric with a layer by layer structure was designed and prepared to obtain excellent microwave attenuation performance. Firstly, PANI/PI fabric was prepared via in-situ deposition method. Then, the NiFe2O4 nanoparticles functionalized by oleic acid were uniformly dispersed in epoxy resin and coated on the top and bottom of PANI/PI fabric with 0.041 mm total thickness. The investigation of chemical structure and surface morphologies indicated the composite structure of f-NiFe2O4/PANI/PI fabric. Various parameters like magnetic property, reflection loss and attenuation constant were used to evaluate its microwave attenuation performance. The results demonstrated that the 30f-NiFe2O4/PANI/PI fabric had a highest attenuation effectiveness with the minimum reflection loss value of -42.5 dB (>90% attenuation) at 12.5 GHz and the effective absorption bandwidth was 3.4 GHz. The study of attenuation mechanism indicated that the dielectric loss from PANI, the magnetic loss caused by f-NiFe2O4 and the layer by layer structure effectively improved microwave attenuation performance of composite fabric. Furthermore, the favorable flexibility and dimensional stability of this resultant fabric would allow the composite fabric for a long time service under pressure or foldable conditions. In sum, the study clearly indicated that three-phase heterostructures f-NiFe2O4/PANI/PI fabric was a good candidate as electromagnetic shielding materials in many fields.

Efficacy and survival analysis of percutaneous radiofrequency versus microwave ablation for hepatocellular carcinoma: an Egyptian multidisciplinary clinic experience.

PubMed

Abdelaziz, Ashraf; Elbaz, Tamer; Shousha, Hend Ibrahim; Mahmoud, Sherif; Ibrahim, Mostafa; Abdelmaksoud, Ahmed; Nabeel, Mohamed

2014-12-01

Hepatocellular carcinoma (HCC) is a primary tumor of the liver with poor prognosis. For early stage HCC, treatment options include surgical resection, liver transplantation, and percutaneous ablation. Percutaneous ablative techniques (radiofrequency and microwave techniques) emerged as best therapeutic options for nonsurgical patients. We aimed to determine the safety and efficacy of radiofrequency and microwave procedures for ablation of early stage HCC lesions and prospectively follow up our patients for survival analysis. One Hundred and 11 patients with early HCC are managed in our multidisciplinary clinic using either radiofrequency or microwave ablation. Patients are assessed for efficacy and safety. Complete ablation rate, local recurrence, and overall survival analysis are compared between both procedures. Radiofrequency ablation group (n = 45) and microwave ablation group (n = 66) were nearly comparable as regards the tumor and patients characteristics. Complete ablation was achieved in 94.2 and 96.1% of patients managed by radiofrequency and microwave ablation techniques, respectively (p value 0.6) with a low rate of minor complications (11.1 and 3.2, respectively) including subcapsular hematoma, thigh burn, abdominal wall skin burn, and pleural effusion. Ablation rates did not differ between ablated lesions ≤ 3 and 3-5 cm. A lower incidence of local recurrence was observed in microwave group (3.9 vs. 13.5% in radiofrequency group, p value 0.04). No difference between both groups as regards de novo lesions, portal vein thrombosis, and abdominal lymphadenopathy. The overall actuarial probability of survival was 91.6% at 1 year and 86.1% at 2 years with a higher survival rates noticed in microwave group but still without significant difference (p value 0.49). Radiofrequency and microwave ablations led to safe and equivalent ablation and survival rates (with superiority for microwave ablation as regards the incidence of local recurrence).

Broadband polarization-independent and low-profile optically transparent metamaterial absorber

NASA Astrophysics Data System (ADS)

Li, Long; Xi, Rui; Liu, Haixia; Lv, Zhiyong

2018-05-01

A transparent metamaterial absorber with simultaneously high optical transparency and broadband microwave absorption is presented in this paper. Consisting of a two-layer soda-lime glass substrate and three-layer patch-shaped indium tin oxide (ITO) films, the proposed absorber has advantages of broadband absorption with an absorptivity higher than 85% in the range from 6.1 to 22.1 GHz, good polarization insensitiveness, a high transparency, a low profile, and wide-incident-angle stability. A prototype of the proposed absorber is fabricated and experimentally measured to demonstrate its excellent performance. The measured results agree well with the theoretical design and numerical simulations.

Efficient atom localization via probe absorption in an inverted-Y atomic system

NASA Astrophysics Data System (ADS)

Wu, Jianchun; Wu, Bo; Mao, Jiejian

2018-06-01

The behaviour of atom localization in an inverted-Y atomic system is theoretically investigated. For the atoms interacting with a weak probe field and several orthogonal standing-wave fields, their position information can be obtained by measuring the probe absorption. Compared with the traditional scheme, we couple the probe field to the transition between the middle and top levels. It is found that the probe absorption sensitively depends on the detuning and strength of the relevant light fields. Remarkably, the atom can be localized at a particular position in the standing-wave fields by coupling a microwave field to the transition between the two ground levels.

Effects of the morphology of CIPs on microwave absorption behaviors

NASA Astrophysics Data System (ADS)

Woo, Soobin; Yoo, Chan-Sei; Kim, Hwijun; Lee, Mijung; Quevedo-Lopez, Manuel; Choi, Hyunjoo

2017-11-01

Electromagnetic (EM) wave absorption properties are affected by the thickness and surface area of absorbing materials. In this study, a facile ball-milling process was introduced to effectively reduce the diameter and increase the aspect ratio of carbonyl iron powder (CIP), which is one of the most commercially available EM-absorbing materials. The size, aspect ratio, and consequent surface area of CIP were manipulated by controlling the milling parameters to investigate their effects on EM absorption properties. The results indicated that ball-milled CIPs exhibited better EM wave absorption ability when compared with that of pristine CIPs. However, significant differences in minimum reflection loss values were not observed between CIPs with different morphologies and similar specific surface areas. Hence, both fine and flaky CIPs were considered as beneficial for EM wave absorption.[Figure not available: see fulltext.

Determination of tropical cyclone surface pressure and winds from satellite microwave data

NASA Technical Reports Server (NTRS)

Kidder, S. Q.

1979-01-01

An approach to the problem of deducing wind speed and pressure around tropical cyclones is presented. The technique, called the Surface Wind Inference from Microwave data (SWIM technique, uses satellites microwave sounder data to measure upper tropospheric temperature anomalies which may then be related to surface pressure anomalies through the hydrostatic and radiative transfer equations. Surface pressure gradients outside of the radius of maximum wind are estimated for the first time. Future instruments may be able to estimate central pressure with + or - 0/1 kPa accuracy.

Assimilation of all-weather GMI and ATMS observations into HWRF

NASA Astrophysics Data System (ADS)

Moradi, I.; Evans, F.; McCarty, W.; Marks, F.; Eriksson, P.

2017-12-01

We propose a novel Bayesian Monte Carlo Integration (BMCI) technique to retrieve the profiles of temperature, water vapor, and cloud liquid/ice water content from microwave cloudy measurements in the presence of TCs. These retrievals then can either be directly used by meteorologists to analyze the structure of TCs or be assimilated to provide accurate initial conditions for the NWP models. The technique is applied to the data from the Advanced Technology Microwave Sounder (ATMS) onboard Suomi National Polar-orbiting Partnership (NPP) and Global Precipitation Measurement (GPM) Microwave Imager (GMI).

Microwave-Assisted Hydro-Distillation of Essential Oil from Rosemary: Comparison with Traditional Distillation

PubMed Central

Moradi, Sara; Fazlali, Alireza; Hamedi, Hamid

Background: Hydro-distillation (HD) method is a traditional technique which is used in most industrial companies. Microwave-assisted Hydro-distillation (MAHD) is an advanced HD technique utilizing a microwave oven in the extraction process. Methods: In this research, MAHD of essential oils from the aerial parts (leaves) of rosemary (Rosmarinus officinalis L.) was studied and the results were compared with those of the conventional HD in terms of extraction time, extraction efficiency, chemical composition, quality of the essential oils and cost of the operation. Results: Microwave hydro-distillation was superior in terms of saving energy and extraction time (30 min, compared to 90 min in HD). Chromatography was used for quantity analysis of the essential oils composition. Quality of essential oil improved in MAHD method due to an increase of 17% in oxygenated compounds. Conclusion: Consequently, microwave hydro-distillation can be used as a substitute of traditional hydro-distillation. PMID:29296263

Microwave-Assisted Hydro-Distillation of Essential Oil from Rosemary: Comparison with Traditional Distillation.

PubMed

Moradi, Sara; Fazlali, Alireza; Hamedi, Hamid

2018-01-01

Hydro-distillation (HD) method is a traditional technique which is used in most industrial companies. Microwave-assisted Hydro-distillation (MAHD) is an advanced HD technique utilizing a microwave oven in the extraction process. In this research, MAHD of essential oils from the aerial parts (leaves) of rosemary ( Rosmarinus officinalis L. ) was studied and the results were compared with those of the conventional HD in terms of extraction time, extraction efficiency, chemical composition, quality of the essential oils and cost of the operation. Microwave hydro-distillation was superior in terms of saving energy and extraction time (30 min , compared to 90 min in HD). Chromatography was used for quantity analysis of the essential oils composition. Quality of essential oil improved in MAHD method due to an increase of 17% in oxygenated compounds. Consequently, microwave hydro-distillation can be used as a substitute of traditional hydro-distillation.

Comparison of microwave hydrodistillation and solvent-free microwave extraction of essential oil from Melaleuca leucadendra Linn

NASA Astrophysics Data System (ADS)

Ismanto, A. W.; Kusuma, H. S.; Mahfud, M.

2017-12-01

The comparison of solvent-free microwave extraction (SFME) and microwave hydrodistillation (MHD) in the extraction of essential oil from Melaleuca leucadendra Linn. was examined. Dry cajuput leaves were used in this study. The purpose of this study is also to determine optimal condition (microwave power). The relative electric consumption of SFME and MHD methods are both showing 0,1627 kWh/g and 0,3279 kWh/g. The results showed that solvent-free microwave extraction methods able to reduce energy consumption and can be regarded as a green technique for extraction of cajuput oil.

Impedance Matched Absorptive Thermal Blocking Filters

NASA Technical Reports Server (NTRS)

Wollack, E. J.; Chuss, D. T.; U-Yen, K.; Rostem, K.

2014-01-01

We have designed, fabricated and characterized absorptive thermal blocking filters for cryogenic microwave applications. The transmission line filter's input characteristic impedance is designed to match 50 Omega and its response has been validated from 0-to-50GHz. The observed return loss in the 0-to-20GHz design band is greater than 20 dB and shows graceful degradation with frequency. Design considerations and equations are provided that enable this approach to be scaled and modified for use in other applications.

Impedance Matched Absorptive Thermal Blocking Filters

NASA Technical Reports Server (NTRS)

Wollack, E. J.; Chuss, D. T.; Rostem, K.; U-Yen, K.

2014-01-01

We have designed, fabricated and characterized absorptive thermal blocking filters for cryogenic microwave applications. The transmission line filter's input characteristic impedance is designed to match 50O and its response has been validated from 0-to-50GHz. The observed return loss in the 0-to-20GHz design band is greater than 20 dB and shows graceful degradation with frequency. Design considerations and equations are provided that enable this approach to be scaled and modified for use in other applications.

Frequency band justifications for passive sensors 10.0 to 385 GHz, chapter 2. [for monitoring earth resources and the environment

NASA Technical Reports Server (NTRS)

1976-01-01

Sensitivity requirements of the various measurements obtained by microwave sensors, and radiometry techniques are described. Analytical techniques applied to detailed sharing analyses are discussed. A bibliography of publications pertinent to the scientific justification of frequency requirements for passive microwave remote sensing is included.

Microwave-Induced Interfacial Nanobubbles.

PubMed

Wang, Lei; Miao, Xiaojun; Pan, Gang

2016-11-01

A new method for generating nanobubbles via microwave irradiation was verified and quantified. AFM measurement showed that nanobubbles with diameters ranging from 200 to 600 nm were generated at a water-HOPG surface by applying microwave radiation to aqueous solutions with 9.0-30.0 mg/L dissolved oxygen. Graphite displays strong microwave absorption and transmits high thermal energy to the surface. Because of the high dielectric constant (20 °C, 80 F/m) and dielectric loss factor, water molecules have a strong ability to absorb microwave radiation. The thermal and nonthermal effects of microwave radiation made contributions to decreasing the gas solubility, thus facilitating nanobubble nucleation. The yield of nanobubbles increased about 10-fold when the irradiation time increased from 60 to 120 s at 200 W of microwave radiation. The nanobubble density increased from 0.8 to 15 μm -2 by improving the working power from 200 to 600 W. An apparent improvement in nanobubbles yield was obtained between 300 and 400 W, and the resulting temperature was 34-52 °C. When the initial dissolved oxygen increased from 11.3 to 30.0 mg/L, the density of nanobubbles increased from 1.2 to 13 μm -2 . The generation of nanobubbles could be well controlled by adjusting the gas concentration, microwave power, or irradiation time. The method may be valuable in preparing surface nanobubbles quickly and conveniently for various applications, such as catalysis, hypoxia/anoxia remediation, and templates for preparing nanoscale materials.

Nuke 'Em! Library Pest Control Using a Microwave.

ERIC Educational Resources Information Center

Brezner, Jerome; Luner, Philip

1989-01-01

Discusses the threats to books and periodicals posed by such insects as book lice, termites, cockroaches, silverfish, firebrats, and beetles; reviews past methods of pest control; and describes a technique for insect control using microwaves. The results of tests of microwave effects on publications are reported, necessary precautions are…

High Temperature Superconductor/Semiconductor Hybrid Microwave Devices and Circuits

NASA Technical Reports Server (NTRS)

Romanofsky, Robert R.; Miranda, Felix A.

1999-01-01

Contents include following: film deposition technique; laser ablation; magnetron sputtering; sequential evaporation; microwave substrates; film characterization at microwave frequencies; complex conductivity; magnetic penetration depth; surface impedance; planar single-mode filters; small antennas; antenna arrays phase noise; tunable oscillations; hybrid superconductor/semiconductor receiver front ends; and noise modeling.

Embedded solution for a microwave moisture meter

USDA-ARS?s Scientific Manuscript database

In this paper, the conversion of a PC or laptop-controlled microwave moisture meter to a stand-alone meter hosting its own embedded system is discussed. The moisture meter is based on the free-space transmission measurement technique and uses low-intensity microwaves to measure the attenuation and p...

Microwave-Assisted Synthesis of "N"-Phenylsuccinimide

ERIC Educational Resources Information Center

Shell, Thomas A.; Shell, Jennifer R.; Poole, Kathleen A.; Guetzloff, Thomas F.

2011-01-01

A microwave-assisted synthesis of "N"-phenylsuccinimide has been developed for the second-semester organic teaching laboratory. Utilizing this procedure, "N"-phenylsuccinimide can be synthesized in moderate yields (40-60%) by heating a mixture of aniline and succinic anhydride in a domestic microwave oven for four minutes. This technique reduces…

Detection of Low Level Microwave Radiation Induced Deoxyribonucleic Acid Damage Vis-à-vis Genotoxicity in Brain of Fischer Rats

PubMed Central

Deshmukh, Pravin Suryakantrao; Megha, Kanu; Banerjee, Basu Dev; Ahmed, Rafat Sultana; Chandna, Sudhir; Abegaonkar, Mahesh Pandurang; Tripathi, Ashok Kumar

2013-01-01

Background: Non-ionizing radiofrequency radiation has been increasingly used in industry, commerce, medicine and especially in mobile phone technology and has become a matter of serious concern in present time. Objective: The present study was designed to investigate the possible deoxyribonucleic acid (DNA) damaging effects of low-level microwave radiation in brain of Fischer rats. Materials and Methods: Experiments were performed on male Fischer rats exposed to microwave radiation for 30 days at three different frequencies: 900, 1800 and 2450 MHz. Animals were divided into 4 groups: Group I (Sham exposed): Animals not exposed to microwave radiation but kept under same conditions as that of other groups, Group II: Animals exposed to microwave radiation at frequency 900 MHz at specific absorption rate (SAR) 5.953 × 10−4 W/kg, Group III: Animals exposed to 1800 MHz at SAR 5.835 × 10−4 W/kg and Group IV: Animals exposed to 2450 MHz at SAR 6.672 × 10−4 W/kg. At the end of the exposure period animals were sacrificed immediately and DNA damage in brain tissue was assessed using alkaline comet assay. Results: In the present study, we demonstrated DNA damaging effects of low level microwave radiation in brain. Conclusion: We concluded that low SAR microwave radiation exposure at these frequencies may induce DNA strand breaks in brain tissue. PMID:23833433

Abnormal cardiovascular responses induced by localized high power microwave exposure

DOE Office of Scientific and Technical Information (OSTI.GOV)

Lu, S.-T; Brown, D.O.; Johnson, C.E.

1992-05-01

A hypothesis of microwave-induced circulatory under perfusion was tested in ketamine anesthetized rats whose heart rate, mean arterial pressure, pulse pressure, respiration rate, and body temperatures were monitored continuously. Fifty-eight ventral head and neck exposures in a waveguide consisted of sham-exposure and exposure to continuous wave (CW) and pulsed 1.25 GHz microwaves for 5 min. The 0.5 Hz and 16 Hz pulsemodulated microwaves were delivered at 400 kW peak power. The CW microwaves were 2 and 6.4 W. The average specific absorption rate was 4.75 W/kg per watt transmitted in the brain and 17.15 W/kg per watt transmitted in themore » neck. Respiration rate and mean arterial pressure were not altered. Changes in heart rate and pulse pressure were observed in rats exposed to higher power but not to the lower average power microwaves. Depression of pulse pressure, an indication of a decrease in stroke volume, and increased or decreased heart rate were noted in presence of whole-body hyperthermia. The cardiac output of those animals exposed to higher average power microwaves was considered to be below normal as hypothesized. Decreased cardiac output and normal mean arterial pressure resulted in an increase in the total peripheral resistance which was contrary to the anticipated thermal response of animals.« less

DOE Office of Scientific and Technical Information (OSTI.GOV)

Pettersen, Claire; Bennartz, Ralf; Kulie, Mark S.

Multi-instrument, ground-based measurements provide unique and comprehensive data sets of the atmosphere for a specific location over long periods of time and resulting data compliment past and existing global satellite observations. Our paper explores the effect of ice hydrometeors on ground-based, high-frequency passive microwave measurements and attempts to isolate an ice signature for summer seasons at Summit, Greenland, from 2010 to 2013. Furthermore, data from a combination of passive microwave, cloud radar, radiosonde, and ceilometer were examined to isolate the ice signature at microwave wavelengths. By limiting the study to a cloud liquid water path of 40 g m -2more » or less, the cloud radar can identify cases where the precipitation was dominated by ice. These cases were examined using liquid water and gas microwave absorption models, and brightness temperatures were calculated for the high-frequency microwave channels: 90, 150, and 225GHz. By comparing the measured brightness temperatures from the microwave radiometers and the calculated brightness temperature using only gas and liquid contributions, any residual brightness temperature difference is due to emission and scattering of microwave radiation from the ice hydrometeors in the column. The ice signature in the 90, 150, and 225 GHz channels for the Summit Station summer months was isolated. Then, this measured ice signature was compared to an equivalent brightness temperature difference calculated with a radiative transfer model including microwave single-scattering properties for several ice habits. Furthermore, initial model results compare well against the 4 years of summer season isolated ice signature in the high-frequency microwave channels.« less

Microwave radiation (2.45 GHz)-induced oxidative stress: Whole-body exposure effect on histopathology of Wistar rats.

PubMed

Chauhan, Parul; Verma, H N; Sisodia, Rashmi; Kesari, Kavindra Kumar

2017-01-01

Man-made microwave and radiofrequency (RF) radiation technologies have been steadily increasing with the growing demand of electronic appliances such as microwave oven and cell phones. These appliances affect biological systems by increasing free radicals, thus leading to oxidative damage. The aim of this study was to explore the effect of 2.45 GHz microwave radiation on histology and the level of lipid peroxide (LPO) in Wistar rats. Sixty-day-old male Wistar rats with 180 ± 10 g body weight were used for this study. Animals were divided into two groups: sham exposed (control) and microwave exposed. These animals were exposed for 2 h a day for 35 d to 2.45 GHz microwave radiation (power density, 0.2 mW/cm 2 ). The whole-body specific absorption rate (SAR) was estimated to be 0.14 W/kg. After completion of the exposure period, rats were sacrificed, and brain, liver, kidney, testis and spleen were stored/preserved for determination of LPO and histological parameters. Significantly high level of LPO was observed in the liver (p < 0.001), brain (p < 0.004) and spleen (p < 0.006) in samples from rats exposed to microwave radiation. Also histological changes were observed in the brain, liver, testis, kidney and spleen after whole-body microwave exposure, compared to the control group. Based on the results obtained in this study, we conclude that exposure to microwave radiation 2 h a day for 35 d can potentially cause histopathology and oxidative changes in Wistar rats. These results indicate possible implications of such exposure on human health.

Photoluminescence study of carbon dots from ginger and galangal herbs using microwave technique

NASA Astrophysics Data System (ADS)

Isnaeni; Rahmawati, I.; Intan, R.; Zakaria, M.

2018-03-01

Carbon dots are new type of fluorescent nanoparticle that can be synthesis easily from natural sources. We have synthesized carbon dots from ginger and galangal herbs using microwave technique and studied their optical properties. We synthesized colloidal carbon dots in water solvent by varying microwave processing time. UV-Vis absorbance, photoluminescence, time-resolved photoluminescence, and transmission electron microscope were utilized to study properties of carbon dots. We found that microwave processing time significantly affect optical properties of synthesized carbon dots. UV-Vis absorbance spectra and time-resolved photoluminescence results show that luminescent of carbon dots is dominated by recombination process from n-π* surface energy level. With further development, these carbon dots are potential for several applications.

Evaluation of the color stability of two techniques for reproducing artificial irides after microwave polymerization

PubMed Central

GOIATO, Marcelo Coelho; dos SANTOS, Daniela Micheline; MORENO, Amália; GENNARI-FILHO, Humberto; PELLIZZER, Eduardo Piza

2011-01-01

The use of ocular prostheses for ophthalmic patients aims to rebuild facial aesthetics and provide an artificial substitute to the visual organ. Natural intemperate conditions promote discoloration of artificial irides and many studies have attempted to produce irides with greater chromatic paint durability using different paint materials. Objectives The present study evaluated the color stability of artificial irides obtained with two techniques (oil painting and digital image) and submitted to microwave polymerization. Material and Methods Forty samples were fabricated simulating ocular prostheses. Each sample was constituted by one disc of acrylic resin N1 and one disc of colorless acrylic resin with the iris interposed between the discs. The irides in brown and blue color were obtained by oil painting or digital image. The color stability was determined by a reflection spectrophotometer and measurements were taken before and after microwave polymerization. Statistical analysis of the techniques for reproducing artificial irides was performed by applying the normal data distribution test followed by 2-way ANOVA and Tukey HSD test (α=.05). Results Chromatic alterations occurred in all specimens and statistically significant differences were observed between the oil-painted samples and those obtained by digital imaging. There was no statistical difference between the brown and blue colors. Independently of technique, all samples suffered color alterations after microwave polymerization. Conclusion The digital imaging technique for reproducing irides presented better color stability after microwave polymerization. PMID:21625733

Method And Apparatus For Launching Microwave Energy Into A Plasma Processing Chamber

DOEpatents

DOUGHTY, FRANK C.; [et al

2001-05-01

A method and apparatus for launching microwave energy to a plasma processing chamber in which the required magnetic field is generated by a permanent magnet structure and the permanent magnet material effectively comprises one or more surfaces of the waveguide structure. The waveguide structure functions as an impedance matching device and controls the field pattern of the launched microwave field to create a uniform plasma. The waveguide launcher may comprise a rectangular waveguide, a circular waveguide, or a coaxial waveguide with permanent magnet material forming the sidewalls of the guide and a magnetization pattern which produces the required microwave electron cyclotron resonance magnetic field, a uniform field absorption pattern, and a rapid decay of the fields away from the resonance zone. In addition, the incorporation of permanent magnet material as a portion of the waveguide structure places the magnetic material in close proximity to the vacuum chamber, allowing for a precisely controlled magnetic field configuration, and a reduction of the amount of permanent magnet material required.

Dynamic microwave assisted extraction coupled with dispersive micro-solid-phase extraction of herbicides in soybeans.

PubMed

Li, Na; Wu, Lijie; Nian, Li; Song, Ying; Lei, Lei; Yang, Xiao; Wang, Kun; Wang, Zhibing; Zhang, Liyuan; Zhang, Hanqi; Yu, Aimin; Zhang, Ziwei

2015-09-01

Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (D-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and D-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00 μg kg(-1). The relative recoveries of the herbicides were in the range of 91.1-106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Copyright © 2015 Elsevier B.V. All rights reserved.

Preparation and microwave absorbing properties of carbon/cobalt ferromagnetic composites.

PubMed

Li, Wangchang; Qiao, Xiaojing; Zhao, Hui; Wang, Shuman; Ren, Qingguo

2013-02-01

Carbon/cobalt ferromagnetic light composites with high performance of microwave absorbing properties were prepared by hydrothermal method using starch and hollow cobalt ferrites. It was concluded that after carbonization the spinel structure ferrites changed to Co3Fe7 alloys and the temperature of graphitization was significantly decreased for the catalytic of CoFe2O4/Co3Fe7. The increase of carbon content, and exist of CoFe2O4/Co3Fe7 heightened the microwave absorbing properties. Electromagnetic parameters were tested with 40% of the titled materials and 60% of paraffin wax composites by using HP8722ES vector network analyzer. The reflection was also simulated through transmission line theory. The microwave absorbers exhibited a maximum reflection loss -43 dB and the electromagnetic wave absorption less than -10 dB was found to exceed 3.0 GHz between 11.6 GHz and 15 GHz for an absorber thickness of 2 mm.

Microwave Photon Detector in Circuit QED

NASA Astrophysics Data System (ADS)

Garcia-Ripoll, Juan Jose; Romero, Guillermo; Solano, Enrique

2009-03-01

In this work we propose a design for a microwave photodetector based on elements from circuit QED such as the ones used in qubit designs. Our proposal consists on a microwave guide in which we embed circuital elements that can absorb photons and irreversibly change state. These incoherent absorption processes constitute the measurement itself. We first model this design using a general master equation for the propagating photons and the absorbing elements. We find that the detection efficiency for a single absorber is limited to 50%, and that this efficiency can be quickly increased by adding more elements with a moderate separation, obtaining 80% and 90% for two and three absorbers. Our abstract design has at least one possible implementation in which the absorbers are current biased Josephson junction. We demonstrate that the coupling between the guide and the junctions is strong enough, irrespectively of the microwave guide size, and derivate realistic parameters for high fidelity operation with current experiments. Patent pending No. 200802933, Oficina Espanola de Patentes y Marcas, 17/10/2008.

Temperature distribution analysis of tissue water vaporization during microwave ablation: experiments and simulations.

PubMed

Ai, Haiming; Wu, Shuicai; Gao, Hongjian; Zhao, Lei; Yang, Chunlan; Zeng, Yi

2012-01-01

The temperature distribution in the region near a microwave antenna is a critical factor that affects the entire temperature field during microwave ablation of tissue. It is challenging to predict this distribution precisely, because the temperature in the near-antenna region varies greatly. The effects of water vaporisation and subsequent tissue carbonisation in an ex vivo porcine liver were therefore studied experimentally and in simulations. The enthalpy and high-temperature specific absorption rate (SAR) of liver tissues were calculated and incorporated into the simulation process. The accuracy of predictions for near-field temperatures in our simulations has reached the level where the average maximum error is less than 5°C. In addition, a modified thermal model that accounts for water vaporisation and the change in the SAR distribution pattern is proposed and validated with experiment. The results from this study may be useful in the clinical practice of microwave ablation and can be applied to predict the temperature field in surgical planning.

Structural, Magnetic and Microwave Absorption Properties of Hydrothermally Synthesized (Gd, Mn, Co) Substituted Ba-Hexaferrite Nanoparticles

NASA Astrophysics Data System (ADS)

Torabi, Z.; Arab, A.; Ghanbari, F.

2018-02-01

Gd, Mn and Co substituted barium hexagonal ferrite nanoparticles, according to the formula Ba1- x Gd x Fe12-2 y (MnCo) y O19 and the proportion of y = x/2 (and x = 0, 0.1, 0.3, 0.5, 0.7, 0.9, 1), have been prepared by hydrothermal method. Structural, magnetic and absorption microwave properties of the compositions were evaluated by x-ray diffraction (XRD), field-emission scanning electron microscopy (FE-SEM), vibrating sample magnetometry, and vector network analysis. Studying the XRDs data showed the single-phase structure of all samples without any impurities at 900°C calcination temperature. FE-SEM micrographs demonstrated that the morphology of the nanoparticles has planar and nearly hexagonal morphology. The nanoparticles size calculated within the range of 62-85 nm. Study of the room temperature hysteresis loops of calcined samples indicated that maximum magnetizations and coercivities decreased compared to undoped composite with respect to x. The alterations of magnetizations and coercivities are related to the site occupation of substituted ions, change in grain growth inhibition and the effect of spin canting. Moreover, the results of microwave absorption measurements demonstrated that the maximum reflection loss of substituted Ba-hexaferrite equivalent to - 47 dB in sample x = 0.5 with thickness 5.6 mm at a frequency about 17.2 GHz and a bandwidth of 2 GHz greater than - 10 dB. The results showed that Gd has good potential for use as a rare-earth substitution in permanent magnet hexaferrites and these composites can be employed as absorbers in the gigahertz frequency range.

Flow injection for the determination of Se(IV) and Se(VI) by hydride generation atomic absorption spectrometry with microwave oven on-line prereduction of Se(VI) to Se(IV)

NASA Astrophysics Data System (ADS)

Burguera, J. L.; Carrero, P.; Burguera, M.; Rondon, C.; Brunetto, M. R.; Gallignani, M.

1996-12-01

An on-line flow injection system has been developed for the selective determination of Se(IV) and Se(VI) in citric fruit juices and geothermal waters by hydride generation atomic absorption spectrometry with microwave-aided heating prereduction of Se(VI) to Se(IV). The samples and the prereductant solutions (4 mol l -1 HCl for Se(IV) and 12 mol l -1 HCl for Se(VI)) which circulated in a closed-flow circuit were injected by means of a time-based injector. This mixture was displaced by a carrier solution of 1% v/v of hydrochloric acid through a PTFE coil located inside the focused microwave oven and mixed downstream with a borohydride solution to generate the hydride. The linear ranges were 0-120 and 0-100 μg l -1 of Se(IV) and Se(VI), respectively. The detection limits were 1.0 μg l -1 for Se(IV) and 1.5 μg l -1 for Se(VI). The precision (about 2.0-2.5% RSD) and recoveries (96-98% for Se(IV) and 94-98% for Se(VI)) were good. Total selenium values were also obtained by electrothermal atomic absorption spectrometry which agreed with the content of both selenium species. The sample throughput was about 50 measurements per hour. The main advantage of the method is that the selective determination of Se(IV) and Se(VI) in citric fruit juices and geothermal waters is performed in a closed system with a minimum sample manipulation, exposure to the environment, minimum sample waste and operator attention.

Electromagnetic and thermal properties of three-dimensional printed multilayered nano-carbon/poly(lactic) acid structures

DOE Office of Scientific and Technical Information (OSTI.GOV)

Paddubskaya, A.; Center for Physical Sciences and Technology, A. Goštauto 11, LT-01108 Vilnius; Valynets, N.

A new type of light-weight material produced by 3D printing consisting of nano-carbon doped polymer layer followed by a dielectric polymer layer is proposed. We performed temperature dependent characterization and measured the electromagnetic (EM) response of the samples in the GHz and THz range. The temperature dependent structural characteristics, crystallization, and melting were observed to be strongly affected by the presence and the number of nano-carbon doped layers in the sandwich structure. The electromagnetic measurements show a great potential of such a type of periodic material for electromagnetic compatibility applications in microwave frequency range. Sandwich structures containing only two nano-carbonmore » layers already become not transparent to the microwaves, giving an electromagnetic interference shielding efficiency at the level of 8–15 dB. A sandwich consisting of one nano-carbon doped and one polymer layer is opaque for THz radiation, because of 80% of absorption. These studies serve as a basis for design and realization of specific optimal geometries of meta-surface type with the 3D printing technique, in order to reach a high level of electromagnetic interference shielding performance for real world EM cloaking and EM ecology applications.« less

Paramagnetism of cobalt-doped ZnO nanoparticles obtained by microwave solvothermal synthesis.

PubMed

Wojnarowicz, Jacek; Kusnieruk, Sylwia; Chudoba, Tadeusz; Gierlotka, Stanislaw; Lojkowski, Witold; Knoff, Wojciech; Lukasiewicz, Malgorzata I; Witkowski, Bartlomiej S; Wolska, Anna; Klepka, Marcin T; Story, Tomasz; Godlewski, Marek

2015-01-01

Zinc oxide nanopowders doped with 1-15 mol % cobalt were produced by the microwave solvothermal synthesis (MSS) technique. The obtained nanoparticles were annealed at 800 °C in nitrogen (99.999%) and in synthetic air. The material nanostructure was investigated by means of the following techniques: X-ray diffraction (XRD), helium pycnometry density, specific surface area (SSA), inductively coupled plasma optical emission spectrometry (ICP-OES), extended X-ray absorption fine structure (EXAFS) spectroscopy, scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS) and with magnetometry using superconducting quantum interference device (SQUID). Irrespective of the Co content, nanoparticles in their initial state present a similar morphology. They are composed of loosely agglomerated spherical particles with wurtzite-type crystal structure with crystallites of a mean size of 30 nm. Annealing to temperatures of up to 800 °C induced the growth of crystallites up to a maximum of 2 μm in diameter. For samples annealed in high purity nitrogen, the precipitation of metallic α-Co was detected for a Co content of 5 mol % or more. For samples annealed in synthetic air, no change of phase structure was detected, except for precipitation of Co3O4 for a Co content of 15 mol %. The results of the magentometry investigation indicated that all as-synthesized samples displayed paramagnetic properties with a contribution of anti-ferromagnetic coupling of Co-Co pairs. After annealing in synthetic air, the samples remained paramagnetic and samples annealed under nitrogen flow showed a magnetic response under the influences of a magnetic field, likely related to the precipitation of metallic Co in nanoparticles.

Characterization of lunar ferromagnetic phases by the effective linewidth method

NASA Technical Reports Server (NTRS)

Patton, C. E.; Schmidt, H.

1978-01-01

The effective line-width technique, first developed to study the physics of microwave relaxation in ferrites, has been successfully applied to lunar matter. Effective line-width measurements have been made on two selected samples containing disperse spherical metallic iron particles below 40 microns in diam. The data were obtained for fields from 7 to 12 kOe and a temperature range 125 - 300 K. The effective line width was field-independent and temperature-independent at 650 - 750 Oe. The high-field tails of the ferromagnetic resonance absorption were highly Lorentzian. From the relatively large and temperature-independent high-field effective line widths, it appears that (1) the metallic iron phases in lunar soil are rather impure; (2) the impurities are passive, in that there is no evidence for a temperature peak process; and (3) these samples contain no appreciable magnetite.

Hazardous materials in aquatic environments of the Mississippi River basin. Quarterly project status report, April 1, 1993--June 30, 1993

DOE Office of Scientific and Technical Information (OSTI.GOV)

Not Available

1993-08-01

During this quarter, the Review Panel made its final recommendations regarding which of the proposals should be funded. Included in this report is a brief status report of each of the research and education projects that are currently funded in this project. The Coordinated Instrumentation Facility (CIF) sponsored 3 seminars on Environmental Sample Preparation Techniques. These seminars were designed to educate the investigators on the use of microwave digestion systems for sample preparation and the use of Inductively Coupled Plasma and Atomic Absorption Specrtroscopy for analyses. During this period, Tulane and Xavier Universities have worked closely with Oak Ridge Nationalmore » Laboratories (ORNL) to develop a long term relationship that will encourage interaction and collaborations among the investigators at all of the institutions.« less

RT-CW: widely tunable semiconductor THz QCL sources

NASA Astrophysics Data System (ADS)

Razeghi, M.; Lu, Q. Y.

2016-09-01

Distinctive position of Terahertz (THz) frequencies (ν 0.3 -10 THz) in the electromagnetic spectrum with their lower quantum energy compared to IR and higher frequency compared to microwave range allows for many potential applications unique to them. Especially in the security side of the THz sensing applications, the distinct absorption spectra of explosives and related compounds in the range of 0.1-5 THz makes THz technology a competitive technique for detecting hidden explosives. A compact, high power, room temperature continuous wave terahertz source emitting in a wide frequency range will greatly boost the THz applications for the diagnosis and detection of explosives. Here we present a new strong-coupled strain-balanced quantum cascade laser design for efficient THz generation based intracavity DFG. Room temperature continuous wave operation with electrical frequency tuning range of 2.06-4.35 THz is demonstrated.

The influence of continuum radiation fields on hydrogen radio recombination lines

NASA Astrophysics Data System (ADS)

Prozesky, Andri; Smits, Derck P.

2018-05-01

Calculations of hydrogen departure coefficients using a model with the angular momentum quantum levels resolved that includes the effects of external radiation fields are presented. The stimulating processes are important at radio frequencies and can influence level populations. New numerical techniques with a solid mathematical basis have been incorporated into the model to ensure convergence of the solution. Our results differ from previous results by up to 20 per cent. A direct solver with a similar accuracy but more efficient than the iterative method is used to evaluate the influence of continuum radiation on the hydrogen population structure. The effects on departure coefficients of continuum radiation from dust, the cosmic microwave background, the stellar ionising radiation, and free-free radiation are quantified. Tables of emission and absorption coefficients for interpreting observed radio recombination lines are provided.

Graphene, microscale metallic mesh, and transparent dielectric hybrid structure for excellent transparent electromagnetic interference shielding and absorbing

NASA Astrophysics Data System (ADS)

Lu, Zhengang; Ma, Limin; Tan, Jiubin; Wang, Heyan; Ding, Xuemei

2017-06-01

A high-performance transparent electromagnetic interference (EMI) shielding material based on a graphene/metallic mesh/transparent dielectric (GMTD) hybrid structure is designed and characterized. It consists of stacked graphene and metallic mesh layers, with neighboring layers separated by a quartz-glass substrsate. The GMTD hybrid structure combines the microwave-reflecting characteristics of the metallic mesh and the microwave-absorbing characteristics of graphene to achieve simultaneously high visible transmittance, strong microwave shielding effectiveness (SE), and low microwave reflection. Experiments show that a double-graphene and double-metallic mesh GMTD hybrid structure with a mesh periodicity of 160 µm provides microwave SE exceeding 47.79 dB in the K u-band, and an SE exceeding 32.12 dB in the K a-band, with a maximum value of 37.78 dB at 26.5 GHz. SE by absorption exceeds 30.78 dB in the K a-band, with a maximum value of 34.55 dB at 26.5 GHz, while maintaining a normalized visible transmittance of ~85% at 700 nm. This remarkable performance favors the application of the proposed structure as a transparent microwave shield and absorber, and offers a new strategy for transparent EMI shielding.

Microwave Assisted Grafting of Gums and Extraction of Natural Materials.

PubMed

Singh, Inderbir; Rani, Priya; Kumar, Pradeep

2017-01-01

Microwave assisted modification of polymers has become an established technique for modifying the functionality of polymers. Microwave irradiation reduces reaction time as well as the use of toxic solvents with enhanced sensitivity and yields of quality products. In this review article instrumentation and basic principles of microwave activation have been discussed. Microwave assisted grafting of natural gums, characterization of grafted polymers and their toxicological parameters have also been listed. Pharmaceutical applications viz. drug release retardant, mucoahesion and tablet superdisintegrant potential of microwave assisted gums has also been discussed. An overview of microwave assisted extraction of plant based natural materials has also been presented. Copyright© Bentham Science Publishers; For any queries, please email at epub@benthamscience.org.

Constraining Microwave Emission from Extensive Air Showers via the MIDAS Experiment

NASA Astrophysics Data System (ADS)

Richardson, Matthew; Privitera, Paolo

2017-01-01

Ultra high energy cosmic rays (UHECRs) are accelerated by the most energetic processes in the universe. Upon entering Earth’s atmosphere they produce particle showers known as extensive air showers (EASs). Observatories like the Pierre Auger Observatory sample the particles and light produced by the EASs through large particle detector arrays or nitrogen fluorescence detectors to ascertain the fundamental properties of UHECRs. The large sample of high quality data provided by the Pierre Auger Observatory can be attributed to the hybrid technique which utilizes the two aforementioned techniques simultaneously; however, the limitation of only being able to observe nitrogen fluorescence from EASs on clear moonless nights yields a limited 10% duty cycle for the hybrid technique. One proposal for providing high quality data at increased statistics is the observation of isotropic microwave emission from EASs, as such emission would be observed with a 100% duty cycle. Measurements of microwave emission from laboratory air plasmas conducted by Gorham et al. (2008) produced promising results indicating that the microwave emission should be observable using inexpensive detectors. The Microwave Detection of Air Showers (MIDAS) experiment was built at the University of Chicago to characterize the isotropic microwave emission from EASs and has collected 359 days of observational data at the location of the Pierre Auger experiment. We have performed a time coincidence analysis between this data and data from Pierre Auger and we report a null result. This result places stringent limits on microwave emission from EASs and demonstrates that the laboratory measurements of Gorham et al. (2008) are not applicable to EASs, thus diminishing the feasibility of using isotropic microwave emission to detect EASs.

Characterization of target camouflage structures by means of different microwave imaging procedures

NASA Astrophysics Data System (ADS)

Inaebnit, Christian; John, Marc-Andre; Aulenbacher, Uwe; Akyol, Zeynrep; Hueppi, Rudolf; Wellig, Peter

2009-05-01

This paper presents two different test methods for camouflage layers (CL) like nets or foam based structures. The effectiveness of CL in preventing radar detection and recognition of targets depends on the interaction of CL properties as absorption and diffuse scattering with target specific scattering properties. This fact is taken into account by representing target backscattering as interference of different types of GTD contributions and evaluating the impact of CL onto these individual contributions separately. The first method investigates how a CL under test alters these individual scattering contributions and which "new" contributions are produced by "self-scattering" at the CL. This information is gained by applying ISAR imaging technique to a test structure with different types of scattering contributions. The second test method aims for separating the effects of absorption and "diffuse scattering" in case of a planar metallic plate covered by CL. For this, the equivalent source distribution in the plane of the CL is reconstructed from bistatic scattering data. Both test methods were verified by experimental results obtained from X-band measurements at different CL and proved to be well suited for an application specific evaluation of camouflage structures from different manufacturers.

Realization of single-phase BaSi2 films by vacuum evaporation with suitable optical properties and carrier lifetime for solar cell applications

NASA Astrophysics Data System (ADS)

Hara, Kosuke O.; Nakagawa, Yoshihiko; Suemasu, Takashi; Usami, Noritaka

2015-07-01

We have realized BaSi2 films by a simple vacuum evaporation technique for solar cell applications. X-ray diffraction analysis shows that single-phase BaSi2 films are formed on alkali-free glass substrates at 500 and 600 °C while impurity phases coexist on quartz or soda-lime glass substrates or at a substrate temperature of 400 °C. The mechanism of film growth is discussed by analyzing the residue on the evaporation boat. An issue on the fabricated films is cracking due to thermal mismatch, as observed by secondary electron microscopy. Optical characterizations by transmittance and reflectance spectroscopy show that the evaporated films have high absorption coefficients, reaching 2 × 104 cm-1 for a photon energy of 1.5 eV, and have indirect absorption edges of 1.14-1.21 eV, which are suitable for solar cells. The microwave-detected photoconductivity decay measurement reveals that the carrier lifetime is approximately 0.027 µs, corresponding to the diffusion length of 0.84 µm, which suggests the potential effective usage of photoexcited carriers.

Aircraft and satellite measurement of ocean wave directional spectra using scanning-beam microwave radars

NASA Technical Reports Server (NTRS)

Jackson, F. C.; Walton, W. T.; Baker, P. L.

1982-01-01

A microwave radar technique for remotely measuring the vector wave number spectrum of the ocean surface is described. The technique, which employs short-pulse, noncoherent radars in a conical scan mode near vertical incidence, is shown to be suitable for both aircraft and satellite application, the technique was validated at 10 km aircraft altitude, where we have found excellent agreement between buoy and radar-inferred absolute wave height spectra.

The Effects of Electromagnetic Fields on The Nervous System,

DTIC Science & Technology

Superior Cervical Ganglia: Design of Waveguide Apparatus, and Calculation of Specific Absorption Rate; Effects of Electromagnetic Fields on Muscle ... Contraction ; Effects of Electromagnetic Fields on Auditory System: Effect of Noise Masking on Threshold of Evoked Auditory Responses, Microwave-induced Cochlear Microphonics in Guinea Pigs.

Effect of Electromagnetic Interactions on the Undulatory Temperature Dependent Behaviour of Non-Resonant Microwave Absorption Signal Amplitude in Bi2Sr2CaCu2O8+x

NASA Astrophysics Data System (ADS)

Padam, Gursharan K.; Ekbote, Shrikant N.; Sharma, Mukul; Tripathy, Malay R.; Srivastava, Ganesh P.; Das, Bijoy K.

2006-01-01

Variation of non-resonant microwave absorption (NRMA) signal amplitude in single-phase Bi-2212 (5 wt % Ag) sintered pellets (Tc\\circ ˜ 96 K) while increasing temperature from 15 to 105 K has been investigated and discussed. These studies show an undulatory behavior of an initial fall in the amplitude (15-71.8 K) with a subsequent narrow weak temperature independent region (71.8-75.6 K) and then a rise peaking at ˜82.5 K followed by a final exponential fall (82.5-105 K). A detailed discussion on earlier reported data has suggested that this undulatory behavior cannot be understood in terms of existing approaches involving effect of Josephson interactions (JI) alone among vortices. In our opinion, the entire undulatory behavior observed in the present samples can be explained with the inclusion of electromagnetic interaction (EMI) along with JI.

New laboratory measurements on ammonia's inversion spectrum, with implications for planetary atmospheres

NASA Technical Reports Server (NTRS)

Spilker, Thomas R.

1993-01-01

Microwave spectral measurements have been performed on pure room-temperature gaseous ammonia at frequencies from 1.75 to 18 GHz (1.7-17 cm), at 50-, 100-, and 300-torr pressures. These measurements are part of a laboratory program to measure the microwave absorption spectrum of ammonia, under conditions applicable to giant planet atmospheres, now in progress at the Jet Propulsion Laboratory. The pure ammonia data reported here agree well with previous data by Bleaney and Loubser (1950) at 100 and 300 torrs, and with predictions of the absorptivity formalism published by Berge and Gulkis. Success with pure ammonia but failure with mixtures of ammonia in hydrogen and helium (Spilker, 1990) indicates that the Berge and Gulkis formalism does not correctly handle foreign-gas effects on ammonia inversion lines. This may require modifying conclusions of radio astronomical and radio occultation studies that used this formalism. Notably, a suggested depletion of ammonia and superabundance of hydrogen sulfide may have been exaggerated as a result of inaccuracies in the Berge and Gulkis formalism.

Microwave Absorption Properties of La0.8Ca0.2-xAgxMnO3 (x=0.05; x=0.15) Synthesized by Sol-Gel Method

NASA Astrophysics Data System (ADS)

Kurniawan, B.; Laksmi, W.; Sahara, N. A.

2018-04-01

Microwave absorption properties of La0.8Ca0.2-xAgxMnO3 (x= 0.05; 0.15) is reported in this paper. Lanthanum manganite materials was reported as a potential absorber material [1][2][3]. In this paper, the material was synthesized by sol-gel method, calcined at 550°C, and sintered at 900°C. The material was characterized by X-Ray Diffractometer (XRD), and we found that the materials were single phased. Through SEM-EDS characterization it is found that the materials have compositional purity. The resistivity of the materials is obtained by four point probe method, and it is shown that Ag doped decreases the resistivity of the materials. Reflection loss of La0.8Ca0.15Ag0.05MnO3 reaches -4.470 dB and La0.8Ca0.05Ag0.15MnO3 reaches - 7.953 dB.

Measurement of the dipole moments of excited states and photochemical transients by microwave dielectric absorption

DOE Office of Scientific and Technical Information (OSTI.GOV)

Fessenden, R.W.; Carton, P.M.; Shimamori, H.

1982-09-16

Time-resolved changes in microwave dielectric absorption have been used to study transients formed by laser flash photolysis. Details of the method and apparatus are given. Applications both to the measurements of the dipole moments of transients and to decay kinetics are given. The dipole moments of the lowest triplet states of a number of aromatic compounds (mostly ketones) have been measured in benzene solution at room temperature. States of n..pi..* character generally possess smaller dipole moments than the corresponding ground states while states of ..pi pi..* character (for example, fluorenone) have larger values than the ground state. The triplets ofmore » 4-(dimethylamino)benzaldehyde and 4,4'-bis(dimethylamino)benzophenone have rather high values of dipole moment (10.5 and 8.4 D, respectively) showing their charge-transfer character. The triplet state of benzil was found to have zero or near-zero dipole moment, thus confirming that the triplet state is of a transstructure. 7 figures, 1 table.« less

Ultrasound assisted biogas production from co-digestion of wastewater sludges and agricultural wastes: Comparison with microwave pre-treatment.

PubMed

Aylin Alagöz, B; Yenigün, Orhan; Erdinçler, Ayşen

2018-01-01

This study investigates the effect of ultrasonication and microwave sludge disintegration/pre-treatment techniques on the anaerobic co-digestion efficiency of wastewater sludges with olive and grape pomaces. The effects of both co-digestion and sludge pre-treatment techniques were evaluated in terms of the organic removal efficiency and the biogas production. The "co-digestion" of wastewater sludge with both types of pomaces was revealed to be a much more efficient way for the biogas production compared to the single (mono) sludge digestion. The ultrasonication and microwave pre-treatments applied to the sludge samples caused to a further increase in biogas and methane yields. Based on applied specific energies, ultrasonication pre-treatment was found much more effective than microwave irradiation. The specific energy applied in microwave pre-treatment (87,000kj/kgTS) was almost 9 times higher than that of used in ultrasonication (10,000kj/kgTS), resulting only 10-15% increases in biogas/methane yield. Co-digestion of winery and olive industry residues with pre-treated wastewater sludges appears to be a suitable technique for waste management and energy production. Copyright © 2017 Elsevier B.V. All rights reserved.

Microwave heating synthesis and formation mechanism of chalcopyrite structured CuInS{sub 2} nanorods in deep eutectic solvent

DOE Office of Scientific and Technical Information (OSTI.GOV)

Zhang, Jianjun, E-mail: zhangjianjun7110@163.com; Chen, Jun; Li, Qiang

2015-03-15

Graphical abstract: Chalcopyrite structured CuInS{sub 2} nanorods were synthesized by an environmentally friendly microwave heating method in deep eutectic solvent. Results show that microwave heating time plays an important role in the formation of CuInS{sub 2} nanostructure phase. The SEM results indicated that the obtained CuInS{sub 2} nanostructures display rod-like morphology with diameters of about 40 nm and lengths of about 400 nm. The UV–vis spectrum results indicated that the CuInS{sub 2} nanorods exhibit strong absorption from the entire visible light region to the near-infrared region beyond 1100 nm. The possible growth mechanism of CuInS{sub 2} nanorods was discussed. -more » Abstract: Chalcopyrite structured CuInS{sub 2} nanorods were synthesized by an environmentally friendly microwave heating method in deep eutectic solvent. The as-synthesized CuInS{sub 2} nanorods were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS), respectively. The results indicated that the obtained CuInS{sub 2} nanostructures display rod-like morphology with diameters of about 40 nm and lengths of about 400 nm. The influences of microwave heating time on the formation of CuInS{sub 2} phase were discussed. Ultraviolet–visible (UV–vis) and photoluminescence (PL) spectra were utilized to investigate the optical properties of CuInS{sub 2} nanorods. The results showed that the as-synthesized CuInS{sub 2} nanorods exhibit strong absorption from the entire visible light region to the near-infrared region beyond 1100 nm. PL spectrum of the as-synthesized CuInS{sub 2} nanorods displays an emission peak centered at 580 nm under excitation wavelength of 366 nm at room temperature. The possible growth mechanism of CuInS{sub 2} nanorods was discussed.« less

Controlled Microwave Heating Accelerates Rolling Circle Amplification.

PubMed

Yoshimura, Takeo; Suzuki, Takamasa; Mineki, Shigeru; Ohuchi, Shokichi

2015-01-01

Rolling circle amplification (RCA) generates single-stranded DNAs or RNA, and the diverse applications of this isothermal technique range from the sensitive detection of nucleic acids to analysis of single nucleotide polymorphisms. Microwave chemistry is widely applied to increase reaction rate as well as product yield and purity. The objectives of the present research were to apply microwave heating to RCA and indicate factors that contribute to the microwave selective heating effect. The microwave reaction temperature was strictly controlled using a microwave applicator optimized for enzymatic-scale reactions. Here, we showed that microwave-assisted RCA reactions catalyzed by either of the four thermostable DNA polymerases were accelerated over 4-folds compared with conventional RCA. Furthermore, the temperatures of the individual buffer components were specifically influenced by microwave heating. We concluded that microwave heating accelerated isothermal RCA of DNA because of the differential heating mechanisms of microwaves on the temperatures of reaction components, although the overall reaction temperatures were the same.

A Melting Layer Model for Passive/Active Microwave Remote Sensing Applications. Part 1; Model Formulation and Comparison with Observations

NASA Technical Reports Server (NTRS)

Olson, William S.; Bauer, Peter; Viltard, Nicolas F.; Johnson, Daniel E.; Tao, Wei-Kuo

2000-01-01

In this study, a 1-D steady-state microphysical model which describes the vertical distribution of melting precipitation particles is developed. The model is driven by the ice-phase precipitation distributions just above the freezing level at applicable gridpoints of "parent" 3-D cloud-resolving model (CRM) simulations. It extends these simulations by providing the number density and meltwater fraction of each particle in finely separated size categories through the melting layer. The depth of the modeled melting layer is primarily determined by the initial material density of the ice-phase precipitation. The radiative properties of melting precipitation at microwave frequencies are calculated based upon different methods for describing the dielectric properties of mixed phase particles. Particle absorption and scattering efficiencies at the Tropical Rainfall Measuring Mission Microwave Imager frequencies (10.65 to 85.5 GHz) are enhanced greatly for relatively small (approx. 0.1) meltwater fractions. The relatively large number of partially-melted particles just below the freezing level in stratiform regions leads to significant microwave absorption, well-exceeding the absorption by rain at the base of the melting layer. Calculated precipitation backscatter efficiencies at the Precipitation Radar frequency (13.8 GHz) increase in proportion to the particle meltwater fraction, leading to a "bright-band" of enhanced radar reflectivities in agreement with previous studies. The radiative properties of the melting layer are determined by the choice of dielectric models and the initial water contents and material densities of the "seeding" ice-phase precipitation particles. Simulated melting layer profiles based upon snow described by the Fabry-Szyrmer core-shell dielectric model and graupel described by the Maxwell-Garnett water matrix dielectric model lead to reasonable agreement with radar-derived melting layer optical depth distributions. Moreover, control profiles that do not contain mixed-phase precipitation particles yield optical depths that are systematically lower than those observed. Therefore, the use of the melting layer model to extend 3-D CRM simulations appears justified, at least until more realistic spectral methods for describing melting precipitation in high-resolution, 3-D CRM's are implemented.

Microwave-Assisted Organic Synthesis in the Organic Teaching Lab: A Simple, Greener Wittig Reaction

ERIC Educational Resources Information Center

Martin, Eric; Kellen-Yuen, Cynthia

2007-01-01

A greener, microwave-assisted Wittig reaction has been developed for the second-semester organic teaching laboratory. Utilizing this microwave technique, a variety of styrene derivatives have been successfully synthesized from aromatic aldehydes in good yields (41-68%). The reaction not only occurs under neat reaction conditions, but also employs…

[Microwave stimulated cell marker analysis. Possibilities for more rapid immune diagnosis].

PubMed

Ebener, U; Wehner, S

1993-01-01

We describe a successful rapid APAAP-complex technique using innovative application of microwave irradiation (MIWI) on Ficoll separated peripheral blood mononuclear cell smears of healthy donors. The typing with several monoclonal antibodies (MoAbs) against different cell surface antigens is compared with the conventional APAAP procedure. The commercial domestic microwave oven was operated at 2.45 GHz. Fifteen second irradiation at 350 W during all incubation steps, e.g. primary antibody, bridging antibody and APAAP-complexes produced excellent color reactions with Fast Red TR, Fast Blue BB, New Fuchsin or NBT similar with the conventional immunoenzyme procedure. The routinely usage of a Silicon-Chamber-System developed by us is applicable without limitation under microwave conditions. The results till now have shown that the application of microwave-technique (MIWI) eliminated the need for much longer incubation periods without lost of sensitivity. All immunological markers could be detected in the same degree as observed with the conventional method. We could demonstrate that an immunological diagnosis is possible within 30 minutes using air dried smears in an microwave oven.

Brillouin Selective Sideband Amplification of Microwave Photonic Signals

NASA Technical Reports Server (NTRS)

Yao, S.

1997-01-01

We introduce a powerful Brillouin selective sideband amplification technique and demonstrate its application for achieving gain in photonix signal up- and down- conversions in microwave photonic systems.