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Sample records for mode ii fracture

  1. Combined mode I and mode II fracture of monolithic ceramics

    NASA Technical Reports Server (NTRS)

    Tikare, Veena; Choi, Sung R.

    1993-01-01

    The mode I, mode II, and combined mode I-mode II fracture behaviors of a coarse-grained silicon nitride, a fine-grained silicon nitride, and an alumina were investigated. These ceramics were fractured from two types of fracture initiating flaws: small surface flaws and large single edge precracks. The small surface flaws were introduced by Knoop indentation in flexural samples at various angles to the tensile stress direction and fractured in four-point bending. The samples with large precracks were fractured in the asymmetric four-point-bend geometry. The mixed-mode fracture toughness values obtained from the two flaw configurations were in good agreement with each other. All three ceramics displayed very similar mixed-mode fracture behavior, although their microstructures were not similar. Comparison of experimental data to mixed-mode fracture theories revealed that the minimum strain energy density theory best described the mixed-mode fracture behavior of all three ceramics.

  2. Fracture toughness of polycrystalline ceramics in combined mode I and mode II loading

    NASA Technical Reports Server (NTRS)

    Singh, Dileep; Shetty, Dinesh K.

    1989-01-01

    The present investigation of the fracture of alumina and zirconia polycrystalline ceramic specimens of precracked-disk type, in diametral compression, evaluated fracture toughness in pure mode I, combined mode I/mode II, and pure mode II, depending on the alignment of the center crack relative to the loading diameter. The mixed-mode fracture-toughness envelope thus obtained exhibits significant deviation to higher fracture toughness in mode II, relative to the predictions of linear elastic fracture mechanics theory. Crack-surface resistance due to grain-interlocking and abrasion are identified as the primary sources of increased fracture resistance in mode II loading of the polycrystalline ceramics.

  3. Microstructural effects on fracture toughness of polycrystalline ceramics in combined mode I and mode II loading

    NASA Technical Reports Server (NTRS)

    Singh, D.; Shetty, D. K.

    1988-01-01

    Fracture toughness of polycrystalline alumina and ceria partially-stabilized tetragonal zirconia (CeO2-TZP) ceramics were assessed in combined mode I and mode II loading using precracked disk specimens in diametral compression. Stress states ranging from pure mode I, combined mode I and mode II, and pure mode II were obtained by aligning the center crack at specific angles relative to the loading diameter. The resulting mixed-mode fracture toughness envelope showed significant deviation to higher fracture toughness in mode II relative to the predictions of the linear elastic fracture mechanics theory. Critical comparison with corresponding results on soda-lime glass and fracture surface observations showed that crack surface resistance arising from grain interlocking and abrasion was the main source of the increased fracture toughness in mode II loading of the polycrystalline ceramics. The normalized fracture toughness for pure mode II loading, (KII/KIc), increased with increasing grain size for the CeO2-TZP ceramics. Quantitative fractography confirmed an increased percentage of transgranular fracture of the grains in mode II loading.

  4. Combined Mode I and Mode II Fracture of Plasma-Sprayed Thermal Barrier Coatings at Ambient and Elevated Temperatures

    NASA Technical Reports Server (NTRS)

    Choi, Sung R.; Zhu, Dongming; Miller, Robert A.

    2003-01-01

    The mode I, mode II, and combined mode I-mode II fracture behavior of ZrO2- 8wt%Y2O3 thermal barrier coatings was determined in asymmetric flexure loading at both ambient and elevated temperatures. Precracks were introduced in test specimens using the single-edge-v-notched beam (SEVNB) method incorporated with final diamond polishing to achieve sharp crack tips. A fracture envelope of KI versus KII was determined for the coating material at ambient and elevated temperatures. Propagation angles of fracture as a function of K(sub I)/K(sub II) were also determined. The mixed-mode fracture behaviors of the coating material were compared with those of monolithic advanced ceramics determined previously. The mixed-mode fracture behavior of the plasma-sprayed thermal barrier coating material was predicted in terms of fracture envelope and propagation angle using mixed-mode fracture theories.

  5. Combined Mode I and Mode II Fracture of Plasma-Sprayed Thermal Barrier Coatings at Ambient and Elevated Temperatures

    NASA Technical Reports Server (NTRS)

    Choi, Sung R.; Zhu, Dongming; Miller, Robert A.

    2003-01-01

    The mode I, mode II, and combined mode I-mode II fracture behavior of ZrO2 - 8wt%Y2O3 thermal barrier coatings was determined in asymmetric flexure loading at both ambient and elevated temperatures. Precracks were introduced in test specimens using the single-edge-v-notched beam (SEVNB) method incorporated with final diamond polishing to achieve sharp crack tips. A fracture envelope of KI versus KII was determined for the coating material at ambient and elevated temperatures. Propagation angles of fracture as a function of KI/KII were also determined. The mixed-mode fracture behaviors of the coating material were compared with those of monolithic advanced ceramics determined previously. The mixed-mode fracture behavior of the plasma- sprayed thermal barrier coating material was predicted in terms of fracture envelope and propagation angle using mixed-mode fracture theories.

  6. Mode II Interlaminar Fracture Toughness and Fatigue Characterization of a Graphite Epoxy Composite Material

    NASA Technical Reports Server (NTRS)

    O'Brien, T. Kevin; Johnston, William M.; Toland, Gregory J.

    2010-01-01

    Mode II interlaminar fracture toughness and delamination onset and growth characterization data were generated for IM7/8552 graphite epoxy composite materials from two suppliers for use in fracture mechanics analyses. Both the fracture toughness testing and the fatigue testing were conducted using the End-notched Flexure (ENF) test. The ENF test for mode II fracture toughness is currently under review by ASTM as a potential standard test method. This current draft ASTM protocol was used as a guide to conduct the tests on the IM7/8552 material. This report summarizes the test approach, methods, procedures and results of this characterization effort.

  7. Mode II interlaminar fracture toughness of carbon fabric composite laminates with carbon nanotube oriented by magnet

    NASA Astrophysics Data System (ADS)

    Xu, Xinguang; Zhou, Zhenggang

    2017-03-01

    Inspired by the residual iron nanoparticles wrapped in the CNTs tips, we developed a method to induce efficient orientation of multiwalled CNTs bundles by relatively low magnetic fields. Laminates were fabricated to investigate the effect of magnet oriented CNTs on GIIC properties. Microstructure anisotropy of nanotube bundles demonstrated the orientation of CNT bundles by magnet. Furthermore, the application of magnet increased mode II interlaminar fracture toughness by 29% compared to plain laminates.

  8. Ductile fracture in HY100 steel under mixed mode I/mode II loading

    SciTech Connect

    Bhattacharjee, D. . Dept. of Materials Science and Metallurgy); Knott, J.F. . School of Metallurgy and Materials)

    1994-05-01

    A number of criteria have been proposed which predict the direction of cracking under mixed Mode 1/Mode 2 loading. All have been evaluated for brittle materials, in which a crack subjected to tension and shear propagates normal to the maximum tensile stress (i.e. fracture is of the Mode 1 type). In a ductile material, however, a notch subjected to mixed Mode 1/Mode 2 loading may initiate a crack in the direction of maximum shear. This paper shows that the profile of the notch tip changes with increasing mixed mode load in such a way that one side of the tip blunts while the other sharpens. Various specimens, subjected to the same mixed mode ratio, were unloaded from different points on the load-displacement curves to study the change in notch-tip profile. Studies under the Scanning Electron Microscope (SEM) have shown that cracks initiate at the sharpened end, along a microscopic shear band. Using a dislocation pile-up model for decohesion of the carbide-matrix interface, a micromechanical model has been proposed for crack initiation in the shear band. It is shown that a theoretical prediction of the shear strain required for decohesion gives a result that is, of magnitude, similar to that of the shear strain at crack initiation measured in the experiments.

  9. Mixed-mode I+II fracture characterization of human cortical bone using the Single Leg Bending test.

    PubMed

    Silva, F G A; de Moura, M F S F; Dourado, N; Xavier, J; Pereira, F A M; Morais, J J L; Dias, M I R

    2016-02-01

    Mixed-mode I+II fracture characterization of human cortical bone was analyzed in this work. A miniaturized version of the Single Leg Bending test (SLB) was used owing to its simplicity. A power law criterion was verified to accurately describe the material fracture envelop under mixed-mode I+II loading. The crack tip opening displacements measured by digital image correlation were used in a direct method to determine the cohesive law mimicking fracture behavior of cortical bone. Cohesive zone modeling was used for the sake of validation. Several fracture quantities were compared with the experimental results and the good agreement observed proves the appropriateness of the proposed procedure for fracture characterization of human bone under mixed-mode I+II loading.

  10. Effects of Temperature on Mode II Fracture Toughness of Multidirectional CFRP Laminates

    NASA Astrophysics Data System (ADS)

    Kim, Hyoung Soo; Wang, Wen Xue; Takao, Yoshihiro; Ben, Goichi

    End notched flexure (ENF) tests were performed to investigate the effects of temperature and fiber orientation on Mode II interlaminar fracture behavior, GIIC (GII at the crack initiation), of carbon fiber-reinforced epoxy composites, T800H/#3631. The values of GIIC for three kinds of laminates, [012//012], [22.5/-22.5/08/-22.5/22.5//-22.5/22.5/08/22.5/-22.5] and [45/-45/08/-45/45//-45/45/08/45/-45], with a pre-cracked interface, that is // in each laminate, were obtained at three temperatures, i.e. -100°C, 25°C and 150°C. It is shown that GIIC is obviously affected by the temperature and fiber orientation. The scanning electron microscope (SEM) observation was also carried out to investigate the fracture surface. SEM analysis suggested that the decreased Mode II interlaminar fracture toughness for all kinds of specimens at high temperature could be attributed to temperature-induced matrix property change or fiber-matrix interfacial weakening.

  11. A Mixed-Mode (I-II) Fracture Criterion for AS4/8552 Carbon/Epoxy Composite Laminate

    NASA Astrophysics Data System (ADS)

    Karnati, Sidharth Reddy

    A majority of aerospace structures are subjected to bending and stretching loads that introduce peel and shear stresses between the plies of a composite laminate. These two stress components cause a combination of mode I and II fracture modes in the matrix layer of the composite laminate. The most common failure mode in laminated composites is delamination that affects the structural integrity of composite structures. Damage tolerant designs of structures require two types of materials data: mixed-mode (I-II) delamination fracture toughness that predicts failure and delamination growth rate that predicts the life of the structural component. This research focuses determining mixed-mode (I-II) fracture toughness under a combination of mode I and mode II stress states and then a fracture criterion for AS4/8552 composite laminate, which is widely used in general aviation. The AS4/8552 prepreg was supplied by Hexcel Corporation and autoclave fabricated into a 20-ply unidirectional laminate with an artificial delamination by a Fluorinated Ethylene Propylene (FEP) film at the mid-plane. Standard split beam specimens were prepared and tested in double cantilever beam (DCB) and end notched flexure modes to determine mode I (GIC) and II (GIIC) fracture toughnesses, respectively. The DCB specimens were also tested in a modified mixed-mode bending apparatus at GIIm /GT ratios of 0.18, 0.37, 0.57 and 0.78, where GT is total and GIIm is the mode II component of energy release rates. The measured fracture toughness, GC, was found to follow the locus a power law equation. The equation was validated for the present and literature experimental data.

  12. Electron radiation effects on Mode II interlaminar fracture toughness of GFRP and CFRP composites

    SciTech Connect

    Takeda, N.; Tohdoh, M.; Takahashi, K.

    1989-01-01

    The degradation properties of epoxy-based fiber-reinforced-plastics (FRP) composites irradiated by high-energy electrons were studied using the Mode II interlaminar fracture toughness G/sub IIc/, measured by end-notched flexure tests. The radiation-induced degradation mechanisms were investigated through G/sub IIc/ and the scanning electron micrographs of fracture surfaces. For GFRP, the significant decrease in G/sub IIc/ was found. Debonding of glass fibers and epoxy matrix (or degradation of silane coupling agents) plays an important role in degradation in addition to resin degradation. Thus, the improvement of the radiation resistance of fiber-resin interfaces as well as matrix itself is of supreme importance in order to increase the radiation resistance of GFRP. For CFRP, on the other hand, no degradation in fiber-resin interfaces was found and the slight decrease in G/sub IIc/ seems to be due to the resin degradation. 18 references, 6 figures.

  13. In-plane response and mode II fracture response of Z-pin woven laminates

    NASA Astrophysics Data System (ADS)

    Huang, Hseng-Ji

    Textile composites are proven to be an attractive choice over traditional pre-preg based composites because of reduced manufacturing costs and improved transverse mechanical properties. However, similar to traditional pre-preg composites, 2D laminates consisting of multiple layers of laminae still suffer from delamination under impact or transverse loads. Z-pin (carbon fiber of small diameter inserted in the thickness direction-z) composites are a means to provide higher through-thethickness stiffness and strength that 2D woven composites lack. In this thesis, The influences of Z-pin density and Z-pin diameter on the response of Z-pin under in-plane loads (compression) and transverse loads (mode II fracture) are examined. Both experiments and numerical simulations were performed to address the problems. Compression tests were conducted first and failure mechanism in each loading scenario was identified, through optical and mechanical measurements, during and after the tests. This was followed by the development of different numerical models of varying degree of sophistication, which include in-plane 2D models, (used to study fiber distortion and damage due to Z-pin insertion), multi-layer 2D models, (used to provide an inexpensive multi-layer model to study the effect of phase difference due to stacking consolidation), and multi-layer-multi-cell models (used to provide a full 3D multi-layer and multi-representative unit cell description). The second part of this thesis investigates the mode II fracture response under static and dynamic loading. Discrete Cohesive Zone Model (DCZM) was adopted to obtain the fracture toughness in conjunction with experimental data. In dynamic test, a crack advance gage (CAG) was designed to capture the exact time when the crack begins to propagate. By use of these CAGs, the corresponding crack propagation speed between different CAGs can be computed accordingly. These observations are supplemented through high speed optical images

  14. Mode I, Mode II, and Mixed-Mode Fracture of Plasma-sprayed Thermal Barrier Coatings at Ambient and Elevated Temperatures

    NASA Technical Reports Server (NTRS)

    Choi, Sung R.; Zhu, Dongming; Miller, Robert A.

    2003-01-01

    The mixed-mode fracture behavior of plasma-sprayed ZrO2-8 wt% Y2O3 thermal barrier coatings was determined in air at 25 and 1316 C in asymmetric four-point flexure with single edge v-notched beam (SEVNB) test specimens. The mode I fracture toughness was found to be K(sub Ic) = 1.15 plus or minus 0.07 and 0.98 plus or minus 0.13 MPa the square root of m, respectively, at 25 and 1316 C. The respective mode II fracture toughness values were K(sub IIc) = 0.73 plus or minus 0.10 and 0.65 plus or minus 0.04 MPa the square root of m. Hence, there was an insignificant difference in either K(sub Ic or K(sub IIc) between 25 and 1316 C for the coating material, whereas there was a noticeable distinction between K(sub Ic) and K(sub IIc), resulting in K(sub IIc) per K(sub Ic) = 0.65 at both temperatures. The empirical mixed-mode fracture criterion best described the coatings' mixed-mode fracture behavior among the four mixed-mode fracture theories considered. The angle of crack propagation was in reasonable agreement with the minimum strain energy density criterion. The effect of the directionality of the coating material in on K(sub Ic) was observed to be insignificant, while its sintering effect at 1316 C on K(sub Ic) was significant.

  15. Fracture characterization of human cortical bone under mode II loading using the end-notched flexure test.

    PubMed

    Silva, F G A; de Moura, M F S F; Dourado, N; Xavier, J; Pereira, F A M; Morais, J J L; Dias, M I R; Lourenço, P J; Judas, F M

    2016-10-25

    Fracture characterization of human cortical bone under mode II loading was analyzed using a miniaturized version of the end-notched flexure test. A data reduction scheme based on crack equivalent concept was employed to overcome uncertainties on crack length monitoring during the test. The crack tip shear displacement was experimentally measured using digital image correlation technique to determine the cohesive law that mimics bone fracture behavior under mode II loading. The developed procedure was validated by finite element analysis using cohesive zone modeling considering a trapezoidal with bilinear softening relationship. Experimental load-displacement curves, resistance curves and crack tip shear displacement versus applied displacement were used to validate the numerical procedure. The excellent agreement observed between the numerical and experimental results reveals the appropriateness of the proposed test and procedure to characterize human cortical bone fracture under mode II loading. The proposed methodology can be viewed as a novel valuable tool to be used in parametric and methodical clinical studies regarding features (e.g., age, diseases, drugs) influencing bone shear fracture under mode II loading.

  16. Experiments on fracture toughness of thick-wall cylinder for modes I, II, III

    SciTech Connect

    Saegusa, T.; Urabe, N.; Ito, C.; Shirai, K.; Kosaki, A.

    1999-07-01

    There have been few data on fracture toughness for Mode 2 and 3 as compared with those for Mode 1. Experimental data on fracture toughness of plates made of ductile cast iron (ASTM A874-89) and forged steel (ASME SA350 LF5 C1.1) were obtained at a temperature range from 77K to 293K for Mode 1, 2 and 3. The results showed: J{sub IC} < J{sub IIC} < J{sub IIIC}, and K{sub IC} < K{sub IIC} K{sub IIIC}. Integrity of a thick-wall cylinder with artificial flaw was demonstrated against brittle fracture at 233K for Mode 1, 2 and 3, which is one of the design requirements of containers shipping radioactive materials.

  17. A revisit to high-rate mode-II fracture characterization of composites with Kolsky bar techniques.

    SciTech Connect

    Lu, Wei-Yang; Song, Bo; Jin, Huiqing

    2010-03-01

    Nowadays composite materials have been extensively utilized in many military and industrial applications. For example, the newest Boeing 787 uses 50% composite (mostly carbon fiber reinforced plastic) in production. However, the weak delamination strength of fiber reinforced composites, when subjected to external impact such as ballistic impact, has been always potential serious threats to the safety of passengers. Dynamic fracture toughness is a critical indicator of the performance from delamination in such impact events. Quasi-static experimental techniques for fracture toughness have been well developed. For example, end notched flexure (ENF) technique, which is illustrated in Fig. 1, has become a typical method to determined mode-II fracture toughness for composites under quasi-static loading conditions. However, dynamic fracture characterization of composites has been challenging. This has resulted in conflictive and confusing conclusions in regard to strain rate effects on fracture toughness of composites.

  18. Mixed-mode fracture of ceramics

    SciTech Connect

    Petrovic, J.J.

    1985-01-01

    The mixed-mode fracture behavior of ceramic materials is of importance for monolithic ceramics in order to predict the onset of fracture under generalized loading conditions and for ceramic composites to describe crack deflection toughening mechanisms. Experimental data on surface flaw mixed-mode fracture in various ceramics indicate that the flaw-plane normal stress at fracture decreases with increasing in-flaw-plane shear stress, although present data exhibit a fairly wide range in details of this sigma - tau relationship. Fracture from large cracks suggests that Mode II has a greater effect on Mode I fracture than Mode III. A comparison of surface flaw and large crack mixed-mode I-II fracture responses indicated that surface flaw behavior is influenced by shear resistance effects.

  19. An analytical and experimental stress analysis of a practical mode II fracture-test specimen

    NASA Technical Reports Server (NTRS)

    Chisholm, D. B.; Jones, D. L.

    1975-01-01

    A boundary collocation method has been employed to determine the Mode II stress intensity factors for a pair of through-the-thickness edge cracks in a finite isotropic plate. An elastostatic analysis has been carried out in terms of the complete Williams stress function employing both even and odd components. The results of the numerical analysis were verified by a two-step procedure whereby the symmetric and antisymmetric portions of the solution were independently compared with existing solutions. The complete solution was verified by comparison with a photoelastic analysis. A compact shear specimen (CSS) of Hysol epoxy resin was loaded in a photoelastic experiment designed to study the isochromatic fringe patterns resulting from the Mode II crack tip stress distribution. The experiment verified that a pure Mode II stress distribution existed in the neighborhood of the crack tips and confirmed the accuracy of the boundary collocation solution for the Mode II stress intensity factors.

  20. Criterion for mixed mode fracture in composite bonded joints

    NASA Technical Reports Server (NTRS)

    Mall, S.; Kochhar, N. K.

    1986-01-01

    A study was undertaken to characterize the debond growth mechanism of adhesively bonded composite joints under mode I, mixed mode I-II, and mode II static loadings. The bonded system consisted of graphite-epoxy composite adherends bonded with a toughened epoxy adhesive. The mode I, mode II and mixed mode I-II fracture energies of the tested adhesives were found to be equal to each other. The criterion for mixed mode fracture in composite bonded joints was found.

  1. Interlaminar fracture reinforcement under mode-II loading: Post-cure through-thickness reinforcement of graphite epoxy, unidirectional laminates

    NASA Astrophysics Data System (ADS)

    Jacobson, Joel B.

    A novel through-thickness reinforcement method proposed by S. Kravchenko et al., has been static tested under mode II loading using end notched flexure (ENF), unidirectional laminate specimens to determine the impact on the apparent critical fracture toughness (GIIc) for the material tested. Both experimental and numerical methods have been employed in an attempt to characterize and model these effects. Testing and analysis were conducted on two different specimen thickness, 2.34 mm and 3.54 mm nominally. ASTM D7905/7905M -- 14 was followed during the experimental portion of the thick specimens. Multiple reinforcing configurations using the proposed technique were experimentally tested including single, double, and quadruple rows of orthogonal, pultruded carbon/epoxy pins located within the crack and ahead of the crack (pristine material) to determine the effect on the apparent critical fracture toughness for each configuration. Both pre-cracked and no pre-cracked specimens were evaluated. The results of this study indicate that specimens pinned in the crack experienced the highest supportable reaction force such that the crack was completely arrested and most of the specimens failed in flexure. Pre-cracked specimens that were pinned in the body exhibited stable crack growth as well as a shadowing phenomenon. Both pins and the crack surface topography due to this phenomenon are attributed to the increased apparent fracture toughness for these specimens. Similar outcomes were observed through numerical simulations for the models simulated in this study.

  2. Improvement of the mode II interface fracture toughness of glass fiber reinforced plastics/aluminum laminates through vapor grown carbon fiber interleaves

    PubMed Central

    Ning, Huiming; Li, Yuan; Hu, Ning; Cao, Yanping; Yan, Cheng; Azuma, Takesi; Peng, Xianghe; Wu, Liangke; Li, Jinhua; Li, Leilei

    2014-01-01

    The effects of acid treatment, vapor grown carbon fiber (VGCF) interlayer and the angle, i.e., 0° and 90°, between the rolling stripes of an aluminum (Al) plate and the fiber direction of glass fiber reinforced plastics (GFRP) on the mode II interlaminar mechanical properties of GFRP/Al laminates were investigated. The experimental results of an end notched flexure test demonstrate that the acid treatment and the proper addition of VGCF can effectively improve the critical load and mode II fracture toughness of GFRP/Al laminates. The specimens with acid treatment and 10 g m−2 VGCF addition possess the highest mode II fracture toughness, i.e., 269% and 385% increases in the 0° and 90° specimens, respectively compared to those corresponding pristine ones. Due to the induced anisotropy by the rolling stripes on the aluminum plate, the 90° specimens possess 15.3%–73.6% higher mode II fracture toughness compared to the 0° specimens. The improvement mechanisms were explored by the observation of crack propagation path and fracture surface with optical, laser scanning and scanning electron microscopies. Moreover, finite element analyses were carried out based on the cohesive zone model to verify the experimental fracture toughness and to predict the interface shear strength between the aluminum plates and GFRP laminates. PMID:27877680

  3. Improvement of the mode II interface fracture toughness of glass fiber reinforced plastics/aluminum laminates through vapor grown carbon fiber interleaves.

    PubMed

    Ning, Huiming; Li, Yuan; Hu, Ning; Cao, Yanping; Yan, Cheng; Azuma, Takesi; Peng, Xianghe; Wu, Liangke; Li, Jinhua; Li, Leilei

    2014-06-01

    The effects of acid treatment, vapor grown carbon fiber (VGCF) interlayer and the angle, i.e., 0° and 90°, between the rolling stripes of an aluminum (Al) plate and the fiber direction of glass fiber reinforced plastics (GFRP) on the mode II interlaminar mechanical properties of GFRP/Al laminates were investigated. The experimental results of an end notched flexure test demonstrate that the acid treatment and the proper addition of VGCF can effectively improve the critical load and mode II fracture toughness of GFRP/Al laminates. The specimens with acid treatment and 10 g m(-2) VGCF addition possess the highest mode II fracture toughness, i.e., 269% and 385% increases in the 0° and 90° specimens, respectively compared to those corresponding pristine ones. Due to the induced anisotropy by the rolling stripes on the aluminum plate, the 90° specimens possess 15.3%-73.6% higher mode II fracture toughness compared to the 0° specimens. The improvement mechanisms were explored by the observation of crack propagation path and fracture surface with optical, laser scanning and scanning electron microscopies. Moreover, finite element analyses were carried out based on the cohesive zone model to verify the experimental fracture toughness and to predict the interface shear strength between the aluminum plates and GFRP laminates.

  4. Improvement of the mode II interface fracture toughness of glass fiber reinforced plastics/aluminum laminates through vapor grown carbon fiber interleaves

    NASA Astrophysics Data System (ADS)

    Ning, Huiming; Li, Yuan; Hu, Ning; Cao, Yanping; Yan, Cheng; Azuma, Takesi; Peng, Xianghe; Wu, Liangke; Li, Jinhua; Li, Leilei

    2014-06-01

    The effects of acid treatment, vapor grown carbon fiber (VGCF) interlayer and the angle, i.e., 0° and 90°, between the rolling stripes of an aluminum (Al) plate and the fiber direction of glass fiber reinforced plastics (GFRP) on the mode II interlaminar mechanical properties of GFRP/Al laminates were investigated. The experimental results of an end notched flexure test demonstrate that the acid treatment and the proper addition of VGCF can effectively improve the critical load and mode II fracture toughness of GFRP/Al laminates. The specimens with acid treatment and 10 g m-2 VGCF addition possess the highest mode II fracture toughness, i.e., 269% and 385% increases in the 0° and 90° specimens, respectively compared to those corresponding pristine ones. Due to the induced anisotropy by the rolling stripes on the aluminum plate, the 90° specimens possess 15.3%-73.6% higher mode II fracture toughness compared to the 0° specimens. The improvement mechanisms were explored by the observation of crack propagation path and fracture surface with optical, laser scanning and scanning electron microscopies. Moreover, finite element analyses were carried out based on the cohesive zone model to verify the experimental fracture toughness and to predict the interface shear strength between the aluminum plates and GFRP laminates.

  5. On the localization of fracture in highly constrained polymeric layer subjected to mode II loading

    SciTech Connect

    Chiang, M.Y.M.; Chai, H.

    1996-12-31

    The tight spatial constraints imposed on the interlayer by the relatively rigid substrates in adhesive bonding may impede the natural development and growth of damage sources such as voids, kinks and microcracks. This may lead to extensive nonlinear deformations and intense strain localization prior to fracture in ductile or brittle adhesive systems. Moreover, the localized deformation in the bond may be highly triaxial regardless of the nature of the far-field loading. Fracture criteria based on conventional linear elastic fracture mechanics and small-scale yielding condition may not be applicable on large strain. Therefore, the purpose of the authors work is to focus on the local deformation at the crack tip in an effort to demonstrate a fracture criterion, which is independent of the specimen geometry, for the situation in large (or small) plastic deformation.

  6. Non-Linear Analysis of Mode II Fracture in the end Notched Flexure Beam

    NASA Astrophysics Data System (ADS)

    Rizov, V.

    2016-03-01

    Analysis is carried-out of fracture in the End Notched Flex- ure (ENF) beam configuration, taking into account the material nonlin- earity. For this purpose, the J-integral approach is applied. A non-linear model, based on the Classical beam theory is used. The mechanical be- haviour of the ENF configuration is described by the Ramberg-Osgood stress-strain curve. It is assumed that the material possesses the same properties in tension and compression. The influence is evaluated of the material constants in the Ramberg-Osgood stress-strain equation on the fracture behaviour. The effect of the crack length on the J-integral value is investigated, too. The analytical approach, developed in the present paper, is very useful for parametric analyses, since the simple formulae obtained capture the essentials of the non-linear fracture in the ENF con- figuration.

  7. Tests and Interpretation of Mixed Mode I and II Fully Plastic Fracture from Simulated Weld Defects.

    DTIC Science & Technology

    1986-07-31

    0.1). Tis means that with loi %-hardcning (t\\-nicallv highi strength) alloys, the surroiziding structure must be 3 tines stiffe’r :or fracture-stable...9 tauc / a dFxPfax.,)min t ’o a )/i) min (Eq. 7) Svm O.20050. 166 0.258 0.192 Asvm 0.072 .0 v. I 𔃿 0.18 0.215 0.181 Modified Tearing Modulus. T R E

  8. Criterion for mixed mode fracture in composite bonded joints

    NASA Technical Reports Server (NTRS)

    Mall, S.; Kochhar, N. K.

    1986-01-01

    A study was undertaken to characterize the debond growth mechanism of adhesively bonded composite joints under mode I, mixed mode I-II, and mode II static loadings. The bonded system consisted of graphite/epoxy (T300/5208) composite adherends bonded with a toughened epoxy (EC 3445) adhesive. The mode I, mode II and mixed-mode I-II fracture energies of the tested adhesive were found to be equal to each other. Furthermore, the criterion for mixed mode fracture in composite bonded joints was determined.

  9. Role of large-scale slip in mode II fracture of bimaterial interface produced by diffusion bonding

    NASA Astrophysics Data System (ADS)

    Fox, M. R.; Ghosh, A. K.

    2001-08-01

    Bimaterial interfaces present in diffusion-bonded (and in-situ) composites are often not flat interfaces. The unevenness of the interface can result not only from interface reaction products but also from long-range waviness associated with the surfaces of the component phases bonded together. Experimental studies aimed at determining interface mechanical properties generally ignore the departure in the local stress due to waviness and assume a theoretically flat interface. Furthermore, the commonly used testing methods involving superimposed tension often renders the interface so extremely brittle that if microplastic effects were present it becomes impossible to perceive them. This article examines the role of waviness of the interface and microplastic effects on crack initiation. To do this, a test was selected that provides significant stability against crack growth by superimposing compressive stresses. Mode II interface fracture was studied for NiAl/Mo model laminates using a recently developed asymmetrically loaded shear (ALS) interface shear test. The ALS test may be viewed as opposite of the laminate bend test. In the bend test, shear at the interface is created via tension on one surface of the bend, while in the ALS test, shear is created by compression on one side of the interface relative to the other. Normal to the interface, near the crack tip, an initially compressive state is replaced by slight tension due to Poisson’s expansion of the unbonded part of the compressed beam.

  10. 3-D Mixed Mode Delamination Fracture Criteria - An Experimentalist's Perspective

    NASA Technical Reports Server (NTRS)

    Reeder, James R.

    2006-01-01

    Many delamination failure criteria based on fracture toughness have been suggested over the past few decades, but most only covered the region containing mode I and mode II components of loading because that is where toughness data existed. With new analysis tools, more 3D analyses are being conducted that capture a mode III component of loading. This has increased the need for a fracture criterion that incorporates mode III loading. The introduction of a pure mode III fracture toughness test has also produced data on which to base a full 3D fracture criterion. In this paper, a new framework for visualizing 3D fracture criteria is introduced. The common 2D power law fracture criterion was evaluated to produce unexpected predictions with the introduction of mode III and did not perform well in the critical high mode I region. Another 2D criterion that has been shown to model a wide range of materials well was used as the basis for a new 3D criterion. The new criterion is based on assumptions that the relationship between mode I and mode III toughness is similar to the relation between mode I and mode II and that a linear interpolation can be used between mode II and mode III. Until mixed-mode data exists with a mode III component of loading, 3D fracture criteria cannot be properly evaluated, but these assumptions seem reasonable.

  11. A la Mode II.

    ERIC Educational Resources Information Center

    Stowe, Richard A.

    This paper describes two modes of educational decision-making: Mode I, in which the instructor makes such decisions as what to teach, to whom, when, in what order, at what pace, and at what complexity level; and Mode II, in which the learner makes the decisions. While Mode I comprises most of what is regarded as formal education, the learner in…

  12. Fracture - An Unforgiving Failure Mode

    NASA Technical Reports Server (NTRS)

    Goodin, James Ronald

    2006-01-01

    During the 2005 Conference for the Advancement for Space Safety, after a typical presentation of safety tools, a Russian in the audience simply asked, "How does that affect the hardware?" Having participated in several International System Safety Conferences, I recalled that most attention is dedicated to safety tools and little, if any, to hardware. The intent of this paper on the hazard of fracture and failure modes associated with fracture is my attempt to draw attention to the grass roots of system safety - improving hardware robustness and resilience.

  13. Mode II fatigue crack propagation.

    NASA Technical Reports Server (NTRS)

    Roberts, R.; Kibler, J. J.

    1971-01-01

    Fatigue crack propagation rates were obtained for 2024-T3 bare aluminum plates subjected to in-plane, mode I, extensional loads and transverse, mode II, bending loads. These results were compared to the results of Iida and Kobayashi for in-plane mode I-mode II extensional loads. The engineering significance of mode I-mode II fatigue crack growth is considered in view of the present results. A fatigue crack growth equation for handling mode I-mode II fatigue crack growth rates from existing mode I data is also discussed.

  14. Growth Kinematics of Opening-Mode Fractures

    NASA Astrophysics Data System (ADS)

    Eichhubl, P.; Alzayer, Y.; Laubach, S.; Fall, A.

    2014-12-01

    Fracture aperture is a primary control on flow in fractured reservoirs of low matrix permeability including unconventional oil and gas reservoirs and most geothermal systems. Guided by principles of linear elastic fracture mechanics, fracture aperture is generally assumed to be a linear function of fracture length and elastic material properties. Natural opening-mode fractures with significant preserved aperture are observed in core and outcrop indicative of fracture opening strain accommodated by permanent solution-precipitation creep. Fracture opening may thus be decoupled from length growth if the material effectively weakens after initial elastic fracture growth by either non-elastic deformation processes or changes in elastic properties. To investigate the kinematics of fracture length and aperture growth, we reconstructed the opening history of three opening-mode fractures that are bridged by crack-seal quartz cement in Travis Peak Sandstone of the SFOT-1 well, East Texas. Similar crack-seal cement bridges had been interpreted to form by repeated incremental fracture opening and subsequent precipitation of quartz cement. We imaged crack-seal cement textures for bridges sampled at varying distance from the tips using scanning electron microscope cathodoluminescence, and determined the number and thickness of crack-seal cement increments as a function of position along the fracture length and height. Observed trends in increment number and thickness are consistent with an initial stage of fast fracture propagation relative to aperture growth, followed by a stage of slow propagation and pronounced aperture growth. Consistent with fluid inclusion observations indicative of fracture opening and propagation occurring over 30-40 m.y., we interpret the second phase of pronounced aperture growth to result from fracture opening strain accommodated by solution-precipitation creep and concurrent slow, possibly subcritical, fracture propagation. Similar deformation

  15. Mixed Mode Fracture of Plasma Sprayed Thermal Barrier Coatings: Effects of Anisotropy and Heterogeneity

    NASA Technical Reports Server (NTRS)

    Zhu, Dongming; Choi, Sung R.; Ghosn, Louis L.

    2008-01-01

    The combined mode I-mode II fracture behavior of anisotropic ZrO2-8wt%Y2O3 thermal barrier coatings was determined in asymmetric flexure loading at both ambient and elevated temperatures. A fracture envelope of KI versus KII was determined for the coating material at ambient and elevated temperatures. Propagation angles of fracture as a function of KI/KII were also determined. The mixed-mode fracture behavior of the microsplat coating material was modeled using Finite Element approach to account for anisotropy and micro cracked structures, and predicted in terms of fracture envelope and propagation angle using mixed-mode fracture theories.

  16. The impact of hygrothermal preconditioning on mode II interlaminar fracture toughness in unidirectional carbon fiber reinforced epoxy composites: An experimental investigation

    NASA Astrophysics Data System (ADS)

    Hempowicz, Michael L.

    The correlation between the interlaminar Mode II fracture toughness (GIIC) of a carbon fiber reinforced epoxy and other material properties across different conditioning regimes was investigated. Specimens were preconditioned using select hygrothermal criteria to evaluate how changes in the material and mechanical properties in a carbon fiber/epoxy composite correlations with changes in GIIC for each regime. An increase in GIIC from baseline values was demonstrated across all conditions from end-notched flexure (ENF) testing. Dynamic mechanical analysis (DMA) and tensile tests had varying responses based on preconditioning environment. Since tensile and some DMA properties rely on fiber strength and show property loss with increased plasticization, fiber strength may not have a large impact on GIIC properties. Test data also implied that the GIIC increased when consolidation of the polymer chains occurred in the arid condition as well as when crosslink density increased in the moisture exposed conditions. From these results it is believed that the chemical and physical changes in matrix cohesion are more important to GIIC behavior prediction than fiber behavior.

  17. Mixed-Mode Fracture Behavior and Related Surface Topography Feature of a Typical Sandstone

    NASA Astrophysics Data System (ADS)

    Ren, L.; Xie, L. Z.; Xie, H. P.; Ai, T.; He, B.

    2016-08-01

    The geo-mechanical properties of reservoirs, especially the morphology of the rock surface and the fracture properties of rocks, are of great importance in the modeling and simulation of hydraulic processes. To better understand these fundamental issues, five groups of mixed-mode fracture tests were conducted on sandstone using edge-cracked semi-circular bend specimens. Accordingly, the fracture loads, growth paths and fracture surfaces for different initial mixities of the mixed-mode loadings from pure mode I to pure mode II were then determined. A surface topography measurement for each rough fracture surface was conducted using a laser profilometer, and the fractal properties of these surfaces were then investigated. The fracture path evolution mechanism was also investigated via optical microscopy. Moreover, the mixed-mode fracture strength envelope and the crack propagation trajectories of sandstone were theoretically modeled using three widely accepted fracture criteria (i.e., the MTS, MSED and MERR criterions). The published test results in Hasanpour and Choupani (World Acad Sci Eng Tech 41:764-769, 2008) for limestone were also theoretically investigated to further examine the effectiveness of the above fracture criteria. However, none of these criteria could accurately predict the fracture envelopes of both sandstone and limestone. To better estimate the fracture strength of mixed-mode fractures, an empirical maximum tensile stress (EMTS) criterion was proposed and found to achieve good agreement with the test results. Finally, a uniformly pressurized fracture model was simulated for low pressurization rates using this criterion.

  18. Fracture of Sn-Ag-Cu Solder Joints on Cu Substrates. II: Fracture Mechanism Map

    NASA Astrophysics Data System (ADS)

    Kumar, P.; Huang, Z.; Dutta, I.; Sidhu, R.; Renavikar, M.; Mahajan, R.

    2012-02-01

    A methodology to construct fracture mechanism maps for Sn-3.8%Ag-0.7%Cu (SAC387) solder joints attached to Cu substrates has been developed. The map, which delineates the operative mechanisms of fracture along with corresponding joint fracture toughness values, is plotted in a space described by two microstructure-dependent parameters, with the abscissa describing the interfacial intermetallic compound (IMC) and the ordinate representing the strain-rate-dependent solder yield strength. The plot space encompasses the three major mechanisms by which joints fail, namely (i) cohesive fracture of solder, (ii) cleavage fracture of interfacial intermetallic compounds (IMC), and (iii) fracture of the solder-IMC interface. Line contours of constant fracture toughness values, as well as constant fraction of each of the above mechanisms, are indicated on the plots. The plots are generated by experimentally quantifying the dependence of the operative fracture mechanism(s) on the two microstructure-dependent parameters (IMC geometry and solder yield strength) as functions of strain rate, reflow parameters, and post-reflow aging. Separate maps are presented for nominally mode I and equi-mixed mode loading conditions (loading angle ϕ = 0° and 45°, respectively). The maps allow rapid assessment of the operative fracture mechanism(s) along with estimation of the expected joint fracture toughness value for a given loading condition (strain rate and loading angle) and joint microstructure without conducting actual tests, and may serve as a tool for both prediction and microstructure design.

  19. Mixed mode fracture of an HSLA-100 steel

    SciTech Connect

    Densley, J.M.; Hirth, J.P.

    1998-09-04

    Traditionally, mode I instability criteria have marked the conservative fracture toughness limit. However, some high-toughness, particle strengthened materials have been shown to have a lower resistance to the onset of stable crack growth under mixed-mode loading. By testing both standard compact tension specimens and modified mixed-mode compact tension specimens, the authors have determined the pure mode I plain strain fracture toughness and mixed-mode I/III fracture toughness for an HSLA 100 steel. Limited mixed-mode I/II tests of the type described by Kamat were also performed. The steel was provided by E. Czyryca of the Naval Research Laboratory and tested in the as received condition. Czyryca found {sigma}{sub ys} = 780 MPa, {sigma}{sub uts} = 800 MPa, and a two specimen average J{sub Ic} = 490 kJ/m{sup 2} for specimens tested in the T-L orientation. The steel was austenitized at 900 C for 40 minutes, water quenched then aged at 665 C for one hour than air cooled. The hardenability provided by manganese, molybdenum and nickel resulted in a mixed ferrite-bainite microstructure with fine carbonitride and copper precipitates. Such a microstructure gives high strength and toughness, improved weldability, lower DBTT as well as lower cost.

  20. Subcritical crack growth in soda-lime glass in combined mode I and mode II loading

    NASA Technical Reports Server (NTRS)

    Singh, Dileep; Shetty, Dinesh K.

    1990-01-01

    Subcritical crack growth under mixed-mode loading was studied in soda-lime glass. Pure mode I, combined mode I and mode II, and pure mode II loadings were achieved in precracked disk specimens by loading in diametral compression at selected angles with respect to the symmetric radial crack. Crack growth was monitored by measuring the resistance changes in a microcircuit grid consisting of parallel, electrically conducting grid lines deposited on the surface of the disk specimens by photolithography. Subcritical crack growth rates in pure mode I, pure mode II, and combined mode I and mode II loading could be described by an exponential relationship between crack growth rate and an effective crack driving force derived from a mode I-mode II fracture toughness envelope. The effective crack driving force was based on an empirical representation of the noncoplanar strain energy release rate. Stress intensities for kinked cracks were assessed using the method of caustics and an initial decrease and a subsequent increase in the subcritical crack growth rates of kinked cracks were shown to correlate with the variations of the mode I and the mode II stress intensities.

  1. Comparison of Mode II and III Monotonic and Fatigue Delamination Onset Behavior for Carbon/Toughened Epoxy Composites

    NASA Technical Reports Server (NTRS)

    Li, Jian; OBrien, T. Kevin; Lee, Shaw Ming

    1997-01-01

    Monotonic and fatigue tests were performed to compare the Mode II and III interlaminar fracture toughness and fatigue delamination onset for Tenax-HTA/R6376 carbon/toughened epoxy composites. The Mode II interlaminar fracture toughness and fatigue delamination onset were characterized using the end-notched flexure (ENF) test while the Mode III interlaminar fracture toughness and fatigue delamination onset were characterized by using the edge crack torsion (ECT) test. Monotonic tests show that the Mode III fracture toughness is higher than the Mode II fracture toughness. Both Mode II and III cyclic loading greatly increases the tendency for a delamination to grow relative to a single monotonically increasing load. Under fatigue loading, the Mode III specimen also has a longer life than the Mode II specimen.

  2. Combined mode I-mode III fracture toughness of a particulate reinforced metal-matrix composite

    NASA Technical Reports Server (NTRS)

    Manoharan, M.; Lewandowski, J. J.

    1991-01-01

    The aim of this investigation was to determine the fracture behavior of a particulate reinfored aluminum alloy composite under combined mode I-mode III loading conditions. A modified three-point bend specimen was used to carry out these tests. It was found that the mode I loading condition was energetically most favorable. Addition of mode III components to the system seems to increase the amount of redundant work during fracture without affecting the critical fracture criterion.

  3. Mixed-mode Mechanism of Hydraulic Fracture Segmentation

    NASA Astrophysics Data System (ADS)

    Hurt, R. S.; Germanovich, L.; Wu, R.

    2006-12-01

    Mixed-mode I+III loading is one of the primary causes of fracture front segmentation. Although such segmented fractures have been observed both in nature and laboratory, we are not aware of direct laboratory experiments on the mode III mechanism of segmentation of hydraulically induced fractures. In this work, we developed a laboratory technique and a theoretical model for studying not only the effect of mode III loading on the onset of hydraulic fracture segmentation, but also the effect of segmentation on the subsequent growth of hydraulic fractures. In quasi-brittle materials, even a small mode III component may cause fracture segmentation due to a tensile stress field induced near the fracture front [Rice, 1968]. Previously, this has been confirmed in experiments with non-hydraulic fractures [Knauss, 1970; Cooke and Pollard, 1996]. In one occasion, quasi-hydraulic fractures propagated in fast, uncontrollable manner [Sommer, 1969]. This is why, we focused on controlled hydraulic fractures with a rather small KIII/KI ratio (1-10 %). For mixed mode I+III experiments, we used transparent, cylindrical PMMA samples with circular internal fractures perpendicular to the sample axis. Fracture orientation was controlled by thermoelastic stresses induced in each sample by preheating it before creating a fracture. In order to apply mode III loading to the initial fracture, a constant torque was applied to the specimen while fluid was injected into the fracture at a constant rate to pressurize it and to induce mode I loading. The velocity of fracture propagation was constrained by controlling the rate of fluid injection. In spite of a small magnitude of the mode III component, we observed segmented fracture fronts in all tested samples. The segments had similar dimensions and shape elongated around the perimeter of the initial fracture. When the fractures were further pressurized by injecting additional fluid into the sample, second-order segments developed along the fronts

  4. Influence of the resin on interlaminar mixed-mode fracture

    NASA Technical Reports Server (NTRS)

    Johnson, W. S.; Mangalgiri, P. D.

    1985-01-01

    Both literature review data and new data on toughness behavior of seven matrix and adhesive systems in four types of tests were studied in order to assess the influence of the resin on interlaminar fracture. Mixed mode (i.e., various combinations of opening mode 1, G sub 1, and shearing mode 2; G sub 2) fracture toughness data showed that the mixed mode relationship for failure appears to be linear in terms of G sub 1 and G sub 2. The study further indicates that fracture of brittle resins is controlled by the G sub 1 component, and that fracture of many tough resins is controlled by total strain-energy release rate, G sub T. Regarding the relation of polymer structure and the mixed mode fracture: high mode 1 toughness requires resin dilatation; dilatation is low in unmodified epoxies at room temperature/dry conditions; dilatation is higher in plasticized epoxies, heated epoxies, and in modified epoxies; modification improves mode 2 toughness only slightly compared with mode 1 improvements. Analytical aspects of the cracked lap shear test specimen were explored.

  5. An equivalent domain integral method for three-dimensional mixed-mode fracture problems

    NASA Technical Reports Server (NTRS)

    Shivakumar, K. N.; Raju, I. S.

    1991-01-01

    A general formulation of the equivalent domain integral (EDI) method for mixed mode fracture problems in cracked solids is presented. The method is discussed in the context of a 3-D finite element analysis. The J integral consists of two parts: the volume integral of the crack front potential over a torus enclosing the crack front and the crack surface integral due to the crack front potential plus the crack face loading. In mixed mode crack problems the total J integral is split into J sub I, J sub II, and J sub III representing the severity of the crack front in three modes of deformations. The direct and decomposition methods are used to separate the modes. These two methods were applied to several mixed mode fracture problems, were analyzed, and results were found to agree well with those available in the literature. The method lends itself to be used as a post-processing subroutine in a general purpose finite element program.

  6. An equivalent domain integral method for three-dimensional mixed-mode fracture problems

    NASA Technical Reports Server (NTRS)

    Shivakumar, K. N.; Raju, I. S.

    1992-01-01

    A general formulation of the equivalent domain integral (EDI) method for mixed mode fracture problems in cracked solids is presented. The method is discussed in the context of a 3-D finite element analysis. The J integral consists of two parts: the volume integral of the crack front potential over a torus enclosing the crack front and the crack surface integral due to the crack front potential plus the crack face loading. In mixed mode crack problems the total J integral is split into J sub I, J sub II, and J sub III representing the severity of the crack front in three modes of deformations. The direct and decomposition methods are used to separate the modes. These two methods were applied to several mixed mode fracture problems, were analyzed, and results were found to agree well with those available in the literature. The method lends itself to be used as a post-processing subroutine in a general purpose finite element program.

  7. Fractographic study of epoxy fractured under mode I loading and mixed mode I/III loading

    SciTech Connect

    Ren, Fei; Wang, Jy-An John; Bertelsen, Williams D.

    2011-01-01

    Fiber reinforced polymeric composite materials are widely used in structural components such as wind turbine blades, which are typically subject to complicated loading conditions. Thus, material response under mixed mode loading is of great significance to the reliability of these structures. Epoxy is a thermosetting polymer that is currently used in manufacturing wind turbine blades. The fracture behavior of epoxy is relevant to the mechanical integrity of the wind turbine composite materials. In this study, a novel fracture testing methodology, the spiral notch torsion test (SNTT), was applied to study the fracture behavior of an epoxy material. SNTT samples were tested using either monotonic loading or cyclic loading, while both mode I and mixed mode I/III loading conditions were used. Fractographic examination indicated the epoxy samples included in this study were prone to mode I failure even when the samples were subject to mixed mode loading. Different fatigue precracks were observed on mode I and mixed mode samples, i.e. precracks appeared as a uniform band under mode I loading, and a semi-ellipse under mixed mode loading. Fracture toughness was also estimated using quantitative fractography.

  8. Dual mode fracture of composite laminates penetrated by spherical projectiles

    NASA Astrophysics Data System (ADS)

    Czarnecki, G. J.

    The basic for delamination initiation and propagation within an impacted laminate was studied, with an explanation provided for the fracture mode transformation along the projectile's path. Post-impact observations of graphite/epoxy (AS4/3501-6) laminates penetrated by steel spheres (0.5-inch diameter) reveal a fracture mode, similar to shear plugging adjacent to the impacted surface. This fracture mode is contrasted with that of delamination adjacent to the rear surface. The sudden transition from shear plugging to delamination is believed to occur when the projectile interacts with the returning impact-generated tensile wave. To demonstrate the transition, results are presented from ballistically impacted laminates containing a series of imbedded carbon stress and constantan strain gages. Results are based on impact velocities of 1300, 1850, and 2380 f/s. Transverse stress waves are shown capable of creating delamination until attenuated by a local zone of compressed material associated with the on-coming projectile. Based on experimental results, the location of the fracture mode transition plane is predicted both graphically and through a simple equation of motion.

  9. Initiation and growth of mode II delamination in toughened composites

    NASA Astrophysics Data System (ADS)

    Russell, Alan J.

    The origins of nonlinearity in the mode-II delamination fracture of three organic-matrix carbon-fiber composite materials was investigated. This was accomplished by testing specimens with different types of starter cracks and by loading and unloading these specimens several times so that the change in nonlinearity as the delaminations grew could be measured. The load at which crack growth initiated was determined by acoustic emission. Slow crack growth as found to be the principal cause of nonlinearity in the materials tested. The crack velocity obeyed the same power law dependence on GII as is observed for slow crack growth in viscoelastic polymers. For the first loading from the end of the starter cracks, plastic deformation at the crack tip also contributed to the nonlinearity. Other sources of nonlinearity included an increasing fracture resistance in one of the materials as well as problems associated with producing a clean starter notch with a straight crack front.

  10. Dynamic deformation and fracture of single crystal silicon: Fracture modes, damage laws, and anisotropy

    SciTech Connect

    Huang, J. Y.; E, J. C.; Huang, J. W.; Sun, T.; Fezzaa, K.; Xu, S. L.; Luo, S. N.

    2016-05-25

    Impact fracture of single-crystal Si is critical to long-term reliability of electronic devices and solar cells for its wide use as components or substrates in semiconductor industry. Single-crystal Si is loaded along two different crystallographic directions with a split Hopkinson pressure bar integrated with an in situ x-ray imaging and diffraction system. Bulk stress histories are measured, simultaneously with x-ray phase contrast imaging (XPCI) and Laue diffraction. Damage evolution is quantified with grayscale maps from XPCI. Single-crystal Si exhibits pronounced anisotropy in fracture modes, and thus fracture strengths and damage evolution. For loading along [11¯ 0] and viewing along [001], (1¯1¯0)[11¯ 0] cleavage is activated and induces horizontal primary cracks followed by perpendicular wing cracks. However, for loading along [011¯] and viewing along [111], random nucleation and growth of shear and tensile-splitting crack networks lead to catastrophic failure of materials with no cleavage. The primary-wing crack mode leads to a lower characteristic fracture strength due to predamage, but a more concentrated strength distribution, i.e., a higher Weibull modulus, compared to the second loading case. Furthermore, the sequential primary cracking, wing cracking and wing-crack coalescence processes result in a gradual increase of damage with time, deviating from theoretical predictions. Particle size and aspect ratios of fragments are discussed with postmortem fragment analysis, which verifies fracture modes observed in XPCI.

  11. Dynamic deformation and fracture of single crystal silicon: Fracture modes, damage laws, and anisotropy

    DOE PAGES

    Huang, J. Y.; E, J. C.; Huang, J. W.; ...

    2016-05-25

    Impact fracture of single-crystal Si is critical to long-term reliability of electronic devices and solar cells for its wide use as components or substrates in semiconductor industry. Single-crystal Si is loaded along two different crystallographic directions with a split Hopkinson pressure bar integrated with an in situ x-ray imaging and diffraction system. Bulk stress histories are measured, simultaneously with x-ray phase contrast imaging (XPCI) and Laue diffraction. Damage evolution is quantified with grayscale maps from XPCI. Single-crystal Si exhibits pronounced anisotropy in fracture modes, and thus fracture strengths and damage evolution. For loading along [11¯ 0] and viewing along [001],more » (1¯1¯0)[11¯ 0] cleavage is activated and induces horizontal primary cracks followed by perpendicular wing cracks. However, for loading along [011¯] and viewing along [111], random nucleation and growth of shear and tensile-splitting crack networks lead to catastrophic failure of materials with no cleavage. The primary-wing crack mode leads to a lower characteristic fracture strength due to predamage, but a more concentrated strength distribution, i.e., a higher Weibull modulus, compared to the second loading case. Furthermore, the sequential primary cracking, wing cracking and wing-crack coalescence processes result in a gradual increase of damage with time, deviating from theoretical predictions. Particle size and aspect ratios of fragments are discussed with postmortem fragment analysis, which verifies fracture modes observed in XPCI.« less

  12. Modified Mode-I Cracked Sandwich Beam (CSB) Fracture Test

    NASA Technical Reports Server (NTRS)

    Smith, S. A.; Shivakumar, K. N.

    2001-01-01

    Five composite sandwich panels were fabricated using vacuum assisted resin transfer molding (VARTM). Four of these panels had E-glass/vinylester facesheets and one had carbon/epoxy facesheets. The sandwich panels had different density PVC foam cores. The four E-glass panels had core densities of 80, 100, 130, 200 kg/cu m. The sandwich with carbon/epoxy 3 facesheets had a core with density of 100 kg/cu m. Fracture tests were conducted using a modified Cracked Sandwich Beam (CSB) test configuration. Load displacement curves were obtained for loading and unloading of the specimens during crack growth. Various increments of crack growth were monitored. Critical Strain Energy Release Rates (SERR) were determined from the tests using the area method. The critical values of SERR can be considered the fracture toughness of the sandwich material. The fracture toughness ranged 367 J/sq m to 1350 J/sq m over the range of core densities. These results are compared to the Mode-I fracture toughness of the PVC foam core materials and values obtained for foam-cored sandwiches using the TSD specimen. Finite-element analyses (FEA) were performed for the test configuration and Strain Energy Release Rates were calculated using the Virtual Crack Closure Technique (VCCT). The SERR values determined from the FEA were scaled to the fracture loads, or critical loads, obtained from the modified CSB tests. These critical loads were in close agreement with the test values.

  13. Salter-Harris II forearm fracture reduction and fixation using a buttress plate

    PubMed Central

    Barnes, Jonathan; Webb, Mark; Fearon, Paul v

    2014-01-01

    Distal radius fractures are common injuries in children. Those that affect the growth plate (physis) need to be managed carefully as inadequate management may lead to long-term deformity and a reduction in function. However, different management strategies all have drawbacks and controversy exists over how best to manage these cases. This is the case of a 13-year-old girl who presented with a Salter Harris II fracture, which was managed using a novel approach of utilising a T plate in a buttress mode to stabilise the fracture after anatomical reduction. This provided effective fracture fixation and should allow good bone healing without causing any iatrogenic growth plate damage and without fixing a plate across the physis, which may need removal in the future. PMID:24488665

  14. Fracture-mode map of brittle coatings: Theoretical development and experimental verification

    NASA Astrophysics Data System (ADS)

    He, Chong; Xie, Zhaoqian; Guo, Zhenbin; Yao, Haimin

    2015-10-01

    Brittle coatings, upon sufficiently high indentation load, tend to fracture through either ring cracking or radial cracking. In this paper, we systematically study the factors determining the fracture modes of bilayer material under indentation. By analyzing the stress field developed in a coating/substrate bilayer under indentation in combination with the application of the maximum-tensile-stress fracture criterion, we show that the fracture mode of brittle coatings due to indentation is determined synergistically by two dimensionless parameters being functions of the mechanical properties of coating and substrate, coating thickness and indenter tip radius. Such dependence can be graphically depicted by a diagram called 'fracture-mode map', whereby the fracture modes can be directly predicated based on these two dimensionless parameters. Experimental verification of the fracture-mode map is carried out by examining the fracture modes of fused quartz/cement bilayer materials under indentation. The experimental observation exhibits good agreement with the prediction by the fracture-mode map. Our finding in this paper may not only shed light on the mechanics accounting for the fracture modes of brittle coatings in bilayer structures but also pave a new avenue to combating catastrophic damage through fracture mode control.

  15. The significance of crack-resistance curves to the mixed-mode fracture toughness of human cortical bone

    SciTech Connect

    Zimmermann, Elizabeth A.; Launey, Maximilien E.; Ritchie, Robert O.

    2010-03-25

    The majority of fracture mechanics studies on the toughness of bone have been performed under tensile loading. However, it has recently been shown that the toughness of human cortical bone in the transverse (breaking) orientation is actually much lower in shear (mode II) than in tension (mode I); a fact that is physiologically relevant as in vivo bone is invariably loaded multiaxially. Since bone is a material that derives its fracture resistance primarily during crack growth through extrinsic toughening mechanisms, such as crack deflection and bridging, evaluation of its toughness is best achieved through measurements of the crack-resistance or R-curve, which describes the fracture toughness as a function of crack extension. Accordingly, in this study, we attempt to measure for the first time the R-curve fracture toughness of human cortical bone under physiologically relevant mixed-mode loading conditions. We show that the resulting mixed-mode (mode I + II) toughness depends strongly on the crack trajectory and is the result of the competition between the paths of maximum mechanical driving force and 'weakest' microstructural resistance.

  16. The significance of crack-resistance curves to the mixed-mode fracture toughness of human cortical bone

    PubMed Central

    Zimmermann, Elizabeth A.; Launey, Maximilien E.; Ritchie, Robert O.

    2011-01-01

    The majority of fracture mechanics studies on the toughness of bone have been performed under tensile loading. However, it has recently been shown that the toughness of human cortical bone in the transverse (breaking) orientation is actually much lower in shear (mode II) than in tension (mode I); a fact that is physiologically relevant as in vivo bone is invariably loaded multiaxially. Since bone is a material that derives its fracture resistance primarily during crack growth through extrinsic toughening mechanisms, such as crack deflection and bridging, evaluation of its toughness is best achieved through measurements of the crack-resistance or R-curve, which describes the fracture toughness as a function of crack extension. Accordingly, in this study, we attempt to measure for the first time the R-curve fracture toughness of human cortical bone under physiologically relevant mixed-mode loading conditions. We show that the resulting mixed-mode (mode I + II) toughness depends strongly on the crack trajectory and is the result of the competition between the paths of maximum mechanical driving force and “weakest” microstructural resistance. PMID:20409579

  17. The significance of crack-resistance curves to the mixed-mode fracture toughness of human cortical bone.

    PubMed

    Zimmermann, Elizabeth A; Launey, Maximilien E; Ritchie, Robert O

    2010-07-01

    The majority of fracture mechanics studies on the toughness of bone have been performed under tensile loading. However, it has recently been shown that the toughness of human cortical bone in the transverse (breaking) orientation is actually much lower in shear (mode II) than in tension (mode I); a fact that is physiologically relevant as in vivo bone is invariably loaded multiaxially. Since bone is a material that derives its fracture resistance primarily during crack growth through extrinsic toughening mechanisms, such as crack deflection and bridging, evaluation of its toughness is best achieved through measurements of the crack-resistance or R-curve, which describes the fracture toughness as a function of crack extension. Accordingly, in this study, we attempt to measure for the first time the R-curve fracture toughness of human cortical bone under physiologically relevant mixed-mode loading conditions. We show that the resulting mixed-mode (mode I+II) toughness depends strongly on the crack trajectory and is the result of the competition between the paths of maximum mechanical driving force and "weakest" microstructural resistance.

  18. Mode-II Crack Problem for a Long Rectangular Slab of Superconductor under an Electromagnetic Force

    NASA Astrophysics Data System (ADS)

    Gao, Zhi-Wen; Zhou, You-He

    2009-02-01

    We present a theoretical analysis to the fracture parameters of the large single domain YBCO superconductor with a tangential line crack under electromagnetic force. The mode-II fracture parameters are obtained due to coupled finite element and infinite element method, and the numerical results are conducted for two activation processes. For a zero-field cooling (ZFC) magnetization process, in the process of magnetic field descent, the larger the applied field is, the larger the stress intensity factors. In the case of field cooling (FC) magnetization process, the stress intensity factors have obvious differences between the two cases of bfc > 1 and bfc >= 1. Additionally, J-integral characteristic is obtained, and according to these results, the mode-II crack growth trend is predicted. These results are benefit for us to understand the fracture mechanism of superconductor both in theory and application.

  19. Numerical Study on Mixed-mode Fracture in Reinforced Concrete

    SciTech Connect

    Yu, Rena C.; Saucedo, Luis; Ruiz, Gonzalo

    2010-05-21

    The object of this work is to model the propagation of fracture in mixed-mode in lightly reinforced concrete beams. When a notched beam does not have enough shear reinforcement, fracture can initiate and propagate unstably and lead to failure through diagonal tension. In order to study this phenomenon numerically, a model capable of dealing with both static and dynamic crack propagation as well as the natural transition of those two regimes is necessary. We adopt a cohesive model for concrete fracture and an interface model for the deterioration between concrete and steel re-bar, both combined with an insertion algorithm. The static process is solved by dynamic relaxation (DR) method together with a modified technique to enhance convergence rate. The same DR method is used to detect a dynamic process and switch to a dynamic calculation. The numerically obtained load-displacement curves, load-CMOD curves and crack patterns fit reasonably well with their experimental counterparts, having in mind that we fed the calculations only with parameters measured experimentally.

  20. Influence of Mixed Mode I-Mode II Loading on Fatigue Delamination Growth Characteristics of a Graphite Epoxy Tape Laminate

    NASA Technical Reports Server (NTRS)

    Ratcliffe, James G.; Johnston, William M., Jr.

    2014-01-01

    Mixed mode I-mode II interlaminar tests were conducted on IM7/8552 tape laminates using the mixed-mode bending test. Three mixed mode ratios, G(sub II)/G(sub T) = 0.2, 0.5, and 0.8, were considered. Tests were performed at all three mixed-mode ratios under quasi-static and cyclic loading conditions, where the former static tests were used to determine initial loading levels for the latter fatigue tests. Fatigue tests at each mixed-mode ratio were performed at four loading levels, Gmax, equal to 0.5G(sub c), 0.4G(sub c), 0.3G(sub c), and 0.2G(sub c), where G(sub c) is the interlaminar fracture toughness of the corresponding mixed-mode ratio at which a test was performed. All fatigue tests were performed using constant-amplitude load control and delamination growth was automatically documented using compliance solutions obtained from the corresponding quasi-static tests. Static fracture toughness data yielded a mixed-mode delamination criterion that exhibited monotonic increase in Gc with mixed-mode ratio, G(sub II)/G(sub T). Fatigue delamination onset parameters varied monotonically with G(sub II)/G(sub T), which was expected based on the fracture toughness data. Analysis of non-normalized data yielded a monotonic change in Paris law exponent with mode ratio. This was not the case when normalized data were analyzed. Fatigue data normalized by the static R-curve were most affected in specimens tested at G(sub II)/G(sub T)=0.2 (this process has little influence on the other data). In this case, the normalized data yielded a higher delamination growth rate compared to the raw data for a given loading level. Overall, fiber bridging appeared to be the dominant mechanism, affecting delamination growth rates in specimens tested at different load levels and differing mixed-mode ratios.

  1. Mixed mode stress field effect in adhesive fracture

    NASA Technical Reports Server (NTRS)

    Anderson, G. P.; Devries, K. L.; Williams, M. L.

    1974-01-01

    Numerical or analytical analyses were performed on seven different test specimens including blister test, 90-degree peel test, torsion test, and various cone tests. These specimens are in general subjected to complex stress fields having various amounts of Mode I, Mode II, and Mode III loads. The specimens were then constructed using polymethyl methacrylate for the adherends and a transparent polyurethane elastomer (Solithane 113) for the adhesive. This combination permitted direct observation of the bondline as load was applied. Although initial debonds as well as bond end termination singularities were present in all specimens, in some cases the debond did not initiate at the singularity points as would normally have been expected. An explanation for this behavior is presented, as well as a comparison of loading mode effect on those specimens for which the debond did propagate from a bond terminus singular point.

  2. Mixed mode fracture characterization of hydroxylapatite-titanium alloy interface.

    PubMed

    Mann, K A; Edidin, A A; Kinoshita, R K; Manley, M T

    1994-01-01

    Cantilever beam and four-point bend specimen geometries were used to experimentally determine the critical energy release rates for a plasma sprayed hydroxylapatite-titanium alloy (HA-Ti alloy) interface. A locus of energy release rates as a function of crack tip phase angle was determined where a 0 degree phase angle represented tensile opening (mode I) loading and a 90 degree phase angle represented in-plane shear (mode II) loading. Energy release rates were found to increase substantially with an increase in phase angle. An energy release rate of 0.108 N/mm was determined for a phase angle of 0 degrees (mode I). Energy release rates of 0.221, 0.686, and 1.212 N/mm were determined for phase angles of 66 degrees, 69 degrees, and 72 degrees, respectively. The experimental data was matched to a phenomenological model for which crack propagation depended on mode I loading alone indicating that crack propagation at the Ha-Ti alloy interface is dominated by the mode I loading component. Therefore, regions of HA coated implants that experience compressive or shear loading across the HA-Ti alloy interface may be much less likely to debond than regions that experience tensile loading.

  3. Patient-reported outcome following nonsurgical management of type II odontoid process fractures in adults

    PubMed Central

    Fam, Maged D; Zeineddine, Hussein A; Nassir, Rafiq Muhammed; Bhatt, Pragnesh; Kamel, Mahmoud H

    2017-01-01

    Background: Transverse (type II) odontoid process fracture is among the most commonly encountered cervical spine fractures. Nonsurgical management through external immobilization is occasionally preferred to surgical management but is criticized for its higher rates of failure and lower patient satisfaction. Our aim is to analyze patient-reported outcomes in patients who underwent nonsurgical treatment for type II odontoid fractures. Methods: We identified patients >18-year-old who underwent external immobilization as a treatment for isolated type II odontoid fracture between 2007 and 2012. We collected demographic parameters, clinical presentation, mode of injury, imaging studies and modality and duration of treatment (soft collar, halo-vest, or both). Patients were contacted by telephone to participate in a 15-min survey addressing their recovery including their subjective rate of return to preinjury level of functioning. Results: Fifteen patients met the inclusion/exclusion criteria and participated in our survey. Patients were followed up for an average of 19 months after injury. Overall mean age was 61 years. Injury followed a mechanical fall or a road traffic accident in 11 and 4 cases, respectively. External immobilization was achieved by halo vest only in nine patients, soft collar only in two patients (13%), and through a sequential combination in the remaining 4 (27%). This was deployed for a mean of 7.8 months. Radiological studies at the last follow-up showed bony healing (27%), fibrous nonunion (60%), and persistent instability (13%). Patients reported gradual recovery of function throughout the 1st year after injury with levels above 70% of preinjury functioning achieved by 13% of patients at 6 months, 33% at 9 months, and 47% at 12 months. Overall satisfaction with nonsurgical management was 68%. Conclusion: In selected patients with type II odontoid fractures, external immobilization represents a good option with acceptable course of recovery. PMID

  4. Hinged external fixation for Regan-Morrey type I and II fractures and fracture-dislocations.

    PubMed

    Castelli, Alberto; D'amico, Salvatore; Combi, Alberto; Benazzo, Francesco

    2016-06-01

    Elbow fracture-dislocation is always demanding to manage due to the considerable soft-tissue swelling or damage involved, which can make an early open approach and ligamentous reconstruction impossible. The purpose of this study was to evaluate the role of elbow hinged external fixation (HEF) as a definitive treatment in patients with elbow dislocations associated with Regan-Morrey (R-M) type I and II coronoid fractures and soft-tissue damage. We treated 11 patients between 2010 and 2012 with HEF. Instability tests and standard X-ray examinations were performed before surgery and 1-3 to 3-6 months after surgery, respectively. All patients underwent a preoperative CT scan. Outcomes were assessed with a functional assessment scale (Mayo Elbow Performance Score, MEPS) that included 4 parameters: pain, ROM, stability, and function. The results were good or excellent in all 11 patients, and no patient complained of residual instability. Radiographic examination showed bone metaplasia involving the anterior and medial sides of the joint in 5 patients. HEF presented several advantages: it improves elbow stability and it avoids long and demanding surgery in particular in cases with large soft tissue damage. We therefore consider elbow HEF to be a viable option for treating R-M type I and II fracture-dislocations.

  5. Identification of modes of fracture in a 2618-T6 aluminum alloy using stereophotogrammetry

    SciTech Connect

    Salas Zamarripa, A.; Mata, M.P. Guerrero; Morales, M. Castillo; Beber-Solano, T.P.

    2011-12-15

    The identification and the development of a quantification technique of the modes of fracture in fatigue fracture surfaces of a 2618-T6 aluminum alloy were developed during this research. Fatigue tests at room and high temperature (230 Degree-Sign C) were carried out to be able to compare the microscopic fractographic features developed by this material under these testing conditions. The overall observations by scanning electron microscopy (SEM) of the fracture surfaces showed a mixture of transgranular and ductile intergranular fracture. The ductile intergranular fracture contribution appears to be more significant at room temperature than at 230 Degree-Sign C. A quantitative methodology was developed to identify and to measure the contribution of these microscopic fractographic features. The technique consisted of a combination of stereophotogrammetry and image analysis. Stereo-pairs were randomly taken along the crack paths and were then analyzed using the profile module of MeX software. The analysis involved the 3-D surface reconstruction, the trace of primary profile lines in both vertical and horizontal directions within the stereo-pair area, the measurements of the contribution of the modes of fracture in each profile, and finally, the calculation of the average contribution in each stereo-pair. The technique results confirmed a higher contribution of ductile intergranular fracture at room temperature than at 230 Degree-Sign C. Moreover, there was no indication of a direct relationship between this contribution and the strain amplitudes range applied during the fatigue testing. - Highlights: Black-Right-Pointing-Pointer Stereophotogrammetry and image analysis as a measuring tool of modes of fracture in fatigue fracture surfaces. Black-Right-Pointing-Pointer A mixture of ductile intergranular and transgranular fracture was identified at room temperature and 230 Degree-Sign C testing. Black-Right-Pointing-Pointer Development of a quantitative methodology to

  6. Experimental and Numerical Investigation of Mixed-Mode Interlaminar Fracture of Carbon-Polyester Laminated Woven Composite by Using Arcan Set-up

    NASA Astrophysics Data System (ADS)

    Heydari, Mohammad Hossein; Choupani, Naghdali; Shameli, Moharram

    2011-12-01

    Composite materials are widely used in marine, aerospace and automobile industries. These materials are often subjected to defects and damages from both in-service and manufacturing process. Delamination is the most important of these defects. This paper reports investigation of mixed-mode fracture toughness in carbon-polyester composite by using numerical and experimental methods. All tests were performed by Arcan set-up. By changing the loading angle, α, from 0° to 90° at 15° intervals, mode-I, mixed-mode and mode-II fracture data were obtained. Correction factors for various conditions were obtained by using ABAQUS software. Effects of the crack length and the loading angle on fracture were also studied. The interaction j-integral method was used to separate the mixed-mode stress intensity factors at the crack tip under different loading conditions. As the result, it can be seen that the shearing mode interlaminar fracture toughness is larger than the opening mode interlaminar fracture toughness. This means that interlaminar cracked specimen is tougher in shear loading condition and weaker in tensile loading condition.

  7. Esthetic and biologic mode of reattaching incisor fracture fragment utilizing glass fiber post

    PubMed Central

    Manju, M.; Shanthraj, Srinivas L.; Savitha, K. C.; Sethi, Ntasha

    2015-01-01

    Trauma to the anterior teeth affects the esthetic and psychological well-being of the patient. Advancement in the adhesive dentistry has facilitated the restoration of the coronal tooth fractures by minimally invasive procedures when the original tooth fragment is available. Reattachment of fractured fragment offers immediate treatment with improved preponderant aesthetics and restoration of function. Here, we describe a case of complicated fracture of the maxillary left immature permanent central incisor, which was treated endodontically followed by esthetic reattachment of the fractured fragment using the glass fiber post. Functional demands and esthetic considerations of the patient were fully met with this biologic mode of fragment reattachment. PMID:26283849

  8. Opening-mode fracture in siliceous mudstone at high homologous temperature—effect of surface forces

    NASA Astrophysics Data System (ADS)

    Eichhubl, Peter; Aydin, Atilla; Lore, Jason

    In analogy to high-temperature sintering of ceramics and metal powder compacts, the formation of opening-mode fractures in siliceous mudstone during natural in-situ combustion of hydrocarbons is attributed to contractile surface forces between mineral grains and an interstitial melt phase. A comparison between bulk density increase during sintering and created fracture space indicates that fracturing resulted from contraction of the rock matrix due to porosity reduction, grain-scale mass transfer, and high-temperature mineral formation. It is suggested that contractile surface forces between mineral grains and between mineral grains and pore fluid contribute to subcritical fracture formation under a wide range of subsurface conditions.

  9. Experimental study on mixed mode fracture in unidirectional fiber reinforced composites

    NASA Astrophysics Data System (ADS)

    Gong, Kezhuang; Li, Zheng; Fu, Bin

    2008-11-01

    Fiber reinforced composites are applied broadly in aeronautic and astronautic fields as a structural material. But the investigation in dynamic fracture behavior of fiber reinforced composite stands in the breach for scientists due to a large number of aircraft disasters. In this paper, the mixed mode fracture problems in fiber reinforced composites under impact are studied. First, based on the theory of the reflective dynamic caustic method for mixed mode fracture, corresponding experiments are carried out to study the dynamic fracture behaviors of unidirectional fiber reinforced composites under two kinds load conditions. By recording and analyzing the shadow spot patterns during the crack propagation process carefully, the dynamic fracture toughness and crack growth velocity of fiber reinforced composites are obtained. Via the observation of the crack growth routes and fracture sections, we further reveal the fracture mechanism of unidirectional fiber reinforced composites. It concludes that opening mode still is the easier fracture type for the pre-crack initiation in fiber reinforced composites, while the interface between fibers and matrix becomes the fatal vulnerability during the crack propagation.

  10. Slow crack growth in glass in combined mode I and mode II loading

    NASA Technical Reports Server (NTRS)

    Shetty, D. K.; Rosenfield, A. R.

    1991-01-01

    Slow crack growth in soda-lime glass under combined mode I and mode II loading was investigated in precracked disk specimens in which pure mode I, pure mode II, and various combinations of mode I and mode II were achieved by loading in diametral compression at selected angles with respect to symmetric radial cracks. It is shown that slow crack growth under these conditions can be described by a simple exponential relationship with elastic strain energy release rate as the effective crack-driving force parameter. It is possible to interpret this equation in terms of theoretical models that treat subcritical crack growth as a thermally activated bond-rupture process with an activation energy dependent on the environment, and the elastic energy release rate as the crack-driving force parameter.

  11. Fracture toughness of the F-82H steel-effect of loading modes, hydrogen, and temperature

    NASA Astrophysics Data System (ADS)

    Li, H.-X.; Jones, R. H.; Hirth, J. P.; Gelles, D. S.

    1996-10-01

    The effects of loading mode, hydrogen, and temperature on fracture toughness and tearing modulus were examined for a ferritic/martensitic steel (F-82H). The introduction of a shear load component, mode III, significantly decreased the initiation and propagation resistance of cracks compared to the opening load, mode I, behavior. Mode I crack initiation and propagation exhibited the highest resistance. A minimum resistance occurred when the mode I and mode III loads were nearly equal. The presence of 4 wppm hydrogen decreased the cracking resistance compared to behavior without H regardless of the loading mode. The minimum mixed-mode fracture toughness with the presence of hydrogen was about 30% of the hydrogen-free mode I fracture toughness. The mixed-mode toughness exhibited a lesser sensitivity to temperature than the mode I toughness. The JIC value was 284 kJ/m 2 at room temperature, but only 60 kJ/m 2 at -55°C and 30 kJ/m 2 at -90°C. The ductile to brittle transition temperature (DBTT) was apparently higher than -55°C.

  12. Standard solar model. II - g-modes

    NASA Technical Reports Server (NTRS)

    Guenther, D. B.; Demarque, P.; Pinsonneault, M. H.; Kim, Y.-C.

    1992-01-01

    The paper presents the g-mode oscillation for a set of modern solar models. Each solar model is based on a single modification or improvement to the physics of a reference solar model. Improvements were made to the nuclear reaction rates, the equation of state, the opacities, and the treatment of the atmosphere. The error in the predicted g-mode periods associated with the uncertainties in the model physics is predicted and the specific sensitivities of the g-mode periods and their period spacings to the different model structures are described. In addition, these models are compared to a sample of published observations. A remarkably good agreement is found between the 'best' solar model and the observations of Hill and Gu (1990).

  13. Vibrational modes of hydraulic fractures: Inference of fracture geometry from resonant frequencies and attenuation

    NASA Astrophysics Data System (ADS)

    Lipovsky, Bradley P.; Dunham, Eric M.

    2015-02-01

    Oscillatory seismic signals arising from resonant vibrations of hydraulic fractures are observed in many geologic systems, including volcanoes, glaciers and ice sheets, and hydrocarbon and geothermal reservoirs. To better quantify the physical dimensions of fluid-filled cracks and properties of the fluids within them, we study wave motion along a thin hydraulic fracture waveguide. We present a linearized analysis, valid at wavelengths greater than the fracture aperture, that accounts for quasi-static elastic deformation of the fracture walls, as well as fluid viscosity, inertia, and compressibility. In the long-wavelength limit, anomalously dispersed guided waves known as crack or Krauklis waves propagate with restoring force from fracture wall elasticity. At shorter wavelengths, the waves become sound waves within the fluid channel. Wave attenuation in our model is due to fluid viscosity, rather than seismic radiation from crack tips or fracture wall roughness. We characterize viscous damping at both low frequencies, where the flow is always fully developed, and at high frequencies, where the flow has a nearly constant velocity profile away from viscous boundary layers near the fracture walls. Most observable seismic signals from resonating fractures likely arise in the boundary layer crack wave limit, where fluid-solid coupling is pronounced and attenuation is minimal. We present a method to estimate the aperture and length of a resonating hydraulic fracture using both the seismically observed quality factor and characteristic frequency. Finally, we develop scaling relations between seismic moment and characteristic frequency that might be useful when interpreting the statistics of hydraulic fracture events.

  14. Fixation of unstable type II clavicle fractures with distal clavicle plate and suture button.

    PubMed

    Johnston, Peter S; Sears, Benjamin W; Lazarus, Mark R; Frieman, Barbara G

    2014-11-01

    This article reports on a technique to treat unstable type II distal clavicle fractures using fracture-specific plates and coracoclavicular augmentation with a suture button. Six patients with clinically unstable type II distal clavicle fractures underwent treatment using the above technique. All fractures demonstrated radiographic union at 9.6 (8.4-11.6) weeks with a mean follow-up of 15.6 (12.4-22.3) months. American Shoulder and Elbow Surgeons, Penn Shoulder Score, and Single Assessment Numeric Evaluation scores were 97.97 (98.33-100), 96.4 (91-99), and 95 (90-100), respectively. One patient required implant removal. Fracture-specific plating with suture-button augmentation for type II distal clavicle fractures provides reliable rates of union without absolute requirement for implant removal.

  15. Rogue Mode Shileding in NSLS-II Multipole Vacuum Chambers

    SciTech Connect

    Ferreira, M.; Blednykh, A.; Bacha, B.; Borrelli, A.; Hseuh, H.-C.; Kosciuk, B.; Krinsky, S.; Singh, O.; Vetter, K.

    2011-03-28

    Modes with transverse electric field (TE-modes) in the NSLS-II multipole vacuum chamber can be generated at frequencies above 450MHz due to its geometric dimensions. Since the NSLS-II BPM system monitors signals within 10 MHz band at RF frequency of 500 MHz, frequencies of higher-order modes (HOM) can be generated within the transmission band of the band pass filter. In order to avoid systematic errors in the NSLS-II BPM system, we introduced frequency shift of HOMs by using RF metal shielding located in the antechamber slot. We demonstrated numerical modeling and experimental studies of the spurious TE modes in the NSLS-II vacuum chambers with antechamber slot. Calculated frequencies of TE-modes in considered chambers with and without RF shielding were verified experimentally. Flexible BeCu RF shielding inside each chamber at proper location shifts frequencies of H{sub 10p}-modes above {approx}900MHz, except chambers S6 odd and even. These chambers need special attention because of synchrotron radiation from downstream magnets. S6 odd multipole vacuum chamber needs to be measured and the RF shielding length has to be optimized. RF shielding looks adequate for baseline design. Fifty percent of open space provides adequate pumping speed.

  16. Characterization of the Edge Crack Torsion (ECT) Test for Mode III Fracture Toughness Measurement of Laminated Composites

    NASA Technical Reports Server (NTRS)

    Ratcliffe, James G.

    2004-01-01

    The edge crack torsion (ECT) test is designed to initiate mode III delamination growth in composite laminates. The test has undergone several design changes during its development. The objective of this paper was to determine the suitability of the current ECT test design a mode III fracture test. To this end, ECT tests were conducted on specimens manufactured from IM7/8552 and S2/8552 tape laminates. Three-dimensional finite element analyses were performed. The analysis results were used to calculate the distribution of mode I, mode II, and mode III strain energy release rate along the delamination front. The results indicated that mode IIIdominated delamination growth would be initiated from the specimen center. However, in specimens of both material types, the measured values of GIIIc exhibited significant dependence on delamination length. Load-displacement response of the specimens exhibited significant deviation from linearity before specimen failure. X-radiographs of a sample of specimens revealed that damage was initiated in the specimens prior to failure. Further inspection of the failure surfaces is required to identify the damage and determine that mode III delamination is initiated in the specimens.

  17. Alternate Operating Modes For NDCX-II

    NASA Astrophysics Data System (ADS)

    Sharp, W. M.; Friedman, A.; Grote, D. P.; Cohen, R. H.; Lund, S. M.; Vay, J.-L.; Waldron, W. L.

    2012-10-01

    NDCX-II is a newly completed accelerator facility at LBNL, built to study ion-heated warm dense matter and aspects of ion-driven targets for inertial-fusion energy. The baseline design calls for using twelve induction cells to accelerate 40 nC of Li+ ions to 1.2 MeV. During commissioning, though, we plan to extend the source lifetime by extracting less total charge. For operational flexibility, the option of using a helium plasma source is also being investigated. Over time, we expect that NDCX-II will be upgraded to substantially higher energies, necessitating the use of heavier ions to keep a suitable deposition range in targets. Each of these options requires development of an alternate acceleration schedule and the associated transverse focusing. The schedules here are first worked out with a fast-running 1-D particle-in-cell code ASP, then 2-D and 3-D Warp simulations are used to verify the 1-D results and to design transverse focusing.

  18. Effect of initial delamination on Mode 1 and Mode 2 interlaminar fracture toughness and fatigue fracture threshold

    NASA Technical Reports Server (NTRS)

    Murri, Gretchen Bostaph; Martin, Roderick H.

    1991-01-01

    Static and fatigue double-cantilever beam (DCB) and end-notch flexure (ENF) tests were conducted to determine the effect of the simulated initial delamination in interlaminar fracture toughness, G(sub c), and fatigue fracture threshold, G(sub th). Unidirectional, 24-ply specimens of S2/SP250 glass/epoxy were tested using Kapton inserts of four different thickness - 13, 25, 75, and 130 microns, at the midplane at one end, or with tension or shear precracks, to simulate an initial delamination. To determine G(sub c), the fatigue fracture threshold below which no delamination growth would occur in less than 1 x 10(exp 6) cycles, fatigue tests were conducted by cyclically loading specimens until delamination growth was detected. Consistent values of model 1 fracture toughness, G(sub Ic), were measured from DCB specimens with inserts of thickness 75 microns or thinner, or with shear precracks. The fatigue DCB tests gave similar values of G(sub Ith) for the 13, 25, and 75 microns specimens. Results for the shear precracked specimens were significantly lower that for specimens without precracks. Results for both the static and fatigue ENF tests showed that measured G(IIc) and G(IIth) values decreased with decreasing insert thickness, so that no limiting thickness could be determined. Results for specimens with inserts of 75 microns or thicker were significantly higher than the results for precracked specimens or specimens with 13 or 25 microns inserts.

  19. Non-universal aperture-length scaling of opening mode fractures

    NASA Astrophysics Data System (ADS)

    Mayrhofer, Franziska; Schöpfer, Martin P. J.; Grasemann, Bernhard

    2014-05-01

    Opening-mode fractures, such as joints, veins and dykes, typically exhibit a power-law aperture-length scaling with a power-law exponent of about 0.5. The fracture aperture is hence proportional to the square root of fracture length, a relation which is in fact predicted by linear elastic fracture mechanics (LEFM) for an isolated Mode I fracture subjected to remote tension. The existence of such a 'universal scaling law' is however a highly debated topic. High quality outcrop data illustrate that fracture aperture-length scaling may be 'non-universal' and indicate that below a certain length-scale scaling is super-linear (power-law exponent > 1). We use a numerical model comprised of a square lattice of breakable elastic beams to investigate the aperture-length scaling that emerges in thin plates subjected to remote tension. Strength heterogeneity is introduced in the regular lattice by randomly assigning beam strengths from a Weibull probability distribution. The model fracture system evolution is characterised by two stages which are separated by the strain at which peak-stress occurs. During the pre-peak stress stage fracture aperture-length scaling is universal with a power-law exponent of about 0.5 as expected from LEFM. Shortly after the material has attained its maximum load bearing capacity, aperture-length scaling becomes non-universal, so that the average aperture-length relation plotted on a log-log graph exhibits a distinct kink. Fractures with a length less than this critical length scale exhibit super-linear aperture-length scaling, whereas fractures with a greater length exhibit sub-linear scaling. The models illustrate that the emergence of non-universal aperture-length scaling is a result of fracture clustering, which occurs after peak-stress in the form of a localised fracture zone. Given that fracture clustering is a common phenomenon in natural fracture systems, we argue that a universal scaling law may be the exception rather than the rule.

  20. Fracture mode control: a bio-inspired strategy to combat catastrophic damage

    PubMed Central

    Yao, Haimin; Xie, Zhaoqian; He, Chong; Dao, Ming

    2015-01-01

    The excellent mechanical properties of natural biomaterials have attracted intense attention from researchers with focus on the strengthening and toughening mechanisms. Nevertheless, no material is unconquerable under sufficiently high load. If fracture is unavoidable, constraining the damage scope turns to be a practical way to preserve the integrity of the whole structure. Recent studies on biomaterials have revealed that many structural biomaterials tend to be fractured, under sufficiently high indentation load, through ring cracking which is more localized and hence less destructive compared to the radial one. Inspired by this observation, here we explore the factors affecting the fracture mode of structural biomaterials idealized as laminated materials. Our results suggest that fracture mode of laminated materials depends on the coating/substrate modulus mismatch and the indenter size. A map of fracture mode is developed, showing a critical modulus mismatch (CMM), below which ring cracking dominates irrespective of the indenter size. Many structural biomaterials in nature are found to have modulus mismatch close to the CMM. Our results not only shed light on the mechanics of inclination to ring cracking exhibited by structural biomaterials but are of great value to the design of laminated structures with better persistence of structural integrity. PMID:25619564

  1. Mode I and Mode III fractures in intermediate zone of full-thickness porcine temporomandibular joint discs.

    PubMed

    Beatty, Mark W; Hohl, Rebecca H; Nickel, Jeffrey C; Iwasaki, Laura R; Pidaparti, Ramana M

    2008-05-01

    The aim of this study was to assess the critical energy required to induce flaw propagation in the temporomandibular joint (TMJ) disc when tensile and shear stresses were applied. J-integrals were measured for Mode I and III fractures because excessive tensile and shear stresses promote disc failure. Single edge notch (Mode I) and trouser tear (Mode III) specimens were constructed with flaws oriented parallel to the predominant anteroposteriorly oriented collagen fibers of the TMJ disc. Disks with and without an impulsive pre-load of 3 N s were studied to compare impact-damaged and healthy tissues. Results demonstrated that impulsive loading stiffened the tissues and significantly increased the Mode I fracture energy (J (IC)) but not Mode III (J (IIIC)) (p < or = 0.05). J (IC) and J (IIIC) values were similar for undamaged tissues, but J (IC) values were 2.3 times higher for impulsively loaded tissues (p < or = 0.05). This suggests that when flaws are introduced through impact, the TMJ disc responds by requiring more energy for tensile flaw extension. This research is a first step towards characterizing the mechanical microenvironment that initiates joint disease. This characterization is essential for successful integration of engineered replacement tissues for damaged TMJs.

  2. Characterization of the Edge Crack Torsion (ECT) Test for Mode III Fracture Toughness Measurement of Laminated Composites

    NASA Technical Reports Server (NTRS)

    Ratcliffe, James G.

    2004-01-01

    The edge crack torsion (ECT) test is designed to initiate mode III delamination growth in composite laminates. An ECT specimen is a rectangular laminate, containing an edge delamination at the laminate mid-plane. Torsion load is applied to the specimens, resulting in relative transverse shear sliding of the delaminated faces. The test data reduction schemes are intended to yield initiation values of critical mode III strain energy release rate, G(sub IIIc), that are constant with delamination length. The test has undergone several design changes during its development. The objective of this paper was to determine the suitability of the current ECT test design as a mode III fracture test. To this end, ECT tests were conducted on specimens manufactured from IM7/8552 and specimens made from S2/8552 tape laminates. Several specimens, each with different delamination lengths are tested. Detailed, three-dimensional finite element analyses of the specimens were performed. The analysis results were used to calculate the distribution of mode I, mode II, and mode III strain energy release rate along the delamination front. The results indicated that mode III-dominated delamination growth would be initiated from the specimen center. However, in specimens of both material types, the measured values of G(sub IIIc) exhibited significant dependence on delamination length. Furthermore, there was a large amount of scatter in the data. Load-displacement response of the specimens exhibited significant deviation from linearity before specimen failure. X-radiographs of a sample of specimens revealed that damage was initiated in the specimens prior to failure. Further inspection of the failure surfaces is required to identify the damage and determine that mode III delamination is initiated in the specimens.

  3. Fracture modes under uniaxial compression in hydroxyapatite scaffolds fabricated by robocasting.

    PubMed

    Miranda, Pedro; Pajares, Antonia; Saiz, Eduardo; Tomsia, Antoni P; Guiberteau, Fernando

    2007-12-01

    The fracture modes of hydroxyapatite (HA) scaffolds fabricated by direct-write assembly (robocasting) are analyzed in this work. Concentrated HA inks with suitable viscoelastic properties were developed to enable the fabrication of prototype structures consisting of a 3-D square mesh of interpenetrating rods. The fracture behavior of these model scaffolds under compressive stresses is determined from in situ uniaxial tests performed in two different directions: perpendicular to the rods and along one of the rod directions. The results are analyzed in terms of the stress field calculated by finite element modeling (FEM). This analysis provides valuable insight into the mechanical behavior of scaffolds for bone tissue engineering applications fabricated by robocasting.

  4. Matrix resin effects in composite delamination - Mode I fracture aspects

    NASA Technical Reports Server (NTRS)

    Hunston, Donald L.; Moulton, Richard J.; Johnston, Norman J.; Bascom, Willard D.

    1987-01-01

    A number of thermoset, toughened thermoset, and thermoplastic resin matrix systems were characterized for Mode I critical strain energy release rates, and their composites were tested for interlaminar critical strain energy release rates using the double cantilever beam method. A clear correlation is found between the two sets of data. With brittle resins, the interlaminar critical strain energy release rates are somewhat larger than the neat resin values due to a full transfer of the neat resin toughness to the composite and toughening mechanisms associated with crack growth. With tougher matrices, the higher critical strain energy release rates are only partially transferred to the composites, presumably because the fibers restrict the crack-tip deformation zones.

  5. Fracture mechanics analyses of ceramic/veneer interface under mixed-mode loading.

    PubMed

    Wang, Gaoqi; Zhang, Song; Bian, Cuirong; Kong, Hui

    2014-11-01

    Few studies have focused on the interface fracture performance of zirconia/veneer bilayered structure, which plays an important role in dental all-ceramic restorations. The purpose of this study was to evaluate the fracture mechanics performance of zirconia/veneer interface in a wide range of mode-mixities (at phase angles ranging from 0° to 90°), and to examine the effect of mechanical properties of the materials and the interface on the fracture initiation and crack path of an interfacial crack. A modified sandwich test configuration with an oblique interfacial crack was proposed and calibrated to choose the appropriate geometry dimensions by means of finite element analysis. The specimens with different interface inclination angles were tested to failure under three-point bending configuration. Interface fracture parameters were obtained with finite element analyses. Based on the interfacial fracture mechanics, three fracture criteria for crack kinking were used to predict crack initiation and propagation. In addition, the effects of residual stresses due to coefficient of thermal expansion mismatch between zirconia and veneer on the crack behavior were evaluated. The crack initiation and propagation were well predicted by the three fracture criteria. For specimens at phase angle of 0, the cracks propagated in the interface; whereas for all the other specimens the cracks kinked into the veneer. Compressive residual stresses in the veneer can improve the toughness of the interface structure. The results suggest that, in zirconia/veneer bilayered structure the veneer is weaker than the interface, which can be used to explain the clinical phenomenon that veneer chipping rate is larger than interface delamination rate. Consequently, a veneer material with larger fracture toughness is needed to decrease the failure rate of all-ceramic restorations. And the coefficient of thermal expansion mismatch of the substrates can be larger to produce larger compressive

  6. NSLS-II BPM System Protection from Rogue Mode Coupling

    SciTech Connect

    Blednykh, A.; Bach, B.; Borrelli, A.; Ferreira, M.; Hseuh, H.-C.; Hetzel, C.; Kosciuk, B.; Krinsky, S.; Singh, O.; Vetter, K.

    2011-03-28

    Rogue mode RF shielding has been successfully designed and implemented into the production multipole vacuum chambers. In order to avoid systematic errors in the NSLS-II BPM system we introduced frequency shift of HOM's by using RF metal shielding located in the antechamber slot of each multipole vacuum chamber. To satisfy the pumping requirement the face of the shielding has been perforated with roughly 50 percent transparency. It stays clear of synchrotron radiation in each chamber.

  7. Mode of action of lipid II-targeting lantibiotics.

    PubMed

    Bauer, R; Dicks, L M T

    2005-05-25

    The antimicrobial action of bacteriocins from Gram-positive bacteria is based on interaction with the cytoplasmic membrane of sensitive bacteria. Models based on studies with artificial membrane systems propose that nisin forms wedge-like poration complexes in the membrane by electrostatic interaction between the positively charged C terminus of the peptide and anionic membrane phospholipids. Nisin can also permeabilise membranes via a targeted mechanism by using lipid II, the bactoprenol-bound precursor of the bacterial cell wall, as a docking molecule. Another consequence of binding with lipid II is the inhibition of peptidoglycan biosynthesis. Mersacidine and actagardine also form a complex with lipid II, but binding only blocks the incorporation of lipid II into peptidoglycan, resulting in slow cell lysis rather than pore formation. Both peptides share a conserved sequence motif with plantaricin C and pediocin PD-1, which is most probably involved in the binding of these bacteriocins to lipid II. Although pediocin PD-1 and plantaricin C may inhibit peptidoglycan biosynthesis, pore formation is rather due to electrostatic interaction between the positively charged unbridged N-terminus and anionic phospholipids in the cytoplasmic membrane of sensitive cells. In the light of increased antibiotic resistance, this review focuses on the mode of action of lantibiotics that involve lipid II, possible candidates for the development of new-generation novel antibiotic drugs.

  8. On the mode I fracture analysis of cracked Brazilian disc using a digital image correlation method

    NASA Astrophysics Data System (ADS)

    Abshirini, Mohammad; Soltani, Nasser; Marashizadeh, Parisa

    2016-03-01

    Mode I of fracture of centrally cracked Brazilian disc was investigated experimentally using a digital image correlation (DIC) method. Experiments were performed on PMMA polymers subjected to diametric-compression load. The displacement fields were determined by a correlation between the reference and the deformed images captured before and during loading. The stress intensity factors were calculated by displacement fields using William's equation and the least square algorithm. The parameters involved in the accuracy of SIF calculation such as number of terms in William's equation and the region of analysis around the crack were discussed. The DIC results were compared with the numerical results available in literature and a very good agreement between them was observed. By extending the tests up to the critical state, mode I fracture toughness was determined by analyzing the image of specimen captured at the moment before fracture. The results showed that the digital image correlation was a reliable technique for the calculation of the fracture toughness of brittle materials.

  9. A Practical Test Method for Mode I Fracture Toughness of Adhesive Joints with Dissimilar Substrates

    SciTech Connect

    Boeman, R.G.; Erdman, D.L.; Klett, L.B.; Lomax, R.D.

    1999-09-27

    A practical test method for determining the mode I fracture toughness of adhesive joints with dissimilar substrates will be discussed. The test method is based on the familiar Double Cantilever Beam (DCB) specimen geometry, but overcomes limitations in existing techniques that preclude their use when testing joints with dissimilar substrates. The test method is applicable to adhesive joints where the two bonded substrates have different flexural rigidities due to geometric and/or material considerations. Two specific features discussed are the use of backing beams to prevent substrate damage and a compliance matching scheme to achieve symmetric loading conditions. The procedure is demonstrated on a modified DCB specimen comprised of SRIM composite and thin-section, e-coat steel substrates bonded with an epoxy adhesive. Results indicate that the test method provides a practical means of characterizing the mode I fracture toughness of joints with dissimilar substrates.

  10. The size effect of crystalline inclusions on the fracture modes in glass-ceramic materials.

    PubMed

    Charitidis, C A; Karakasidis, T E; Kavouras, P; Karakostas, Th

    2007-07-04

    The main parameters influencing the mechanical performance of glass-ceramic materials are the shape and mean size of the ceramic phase, i.e. the crystalline inclusions. The aim of the present work is twofold: first, to study the effect of the above parameters on the modes of fracture in two kinds of glass-ceramic materials by the use of the static microindentation technique; second, to interpret the experimental results by the application of a simple physical model. It was found that reduction in the size of granularly shaped crystallite inclusions or reduction of the width of needle-like crystalline inclusions results in an increase of the extent of crack propagation, while the fracture mode shifts from intergranular to transgranular. These observations were successfully interpreted in terms of energetic arguments related to the size of the crystalline inclusions with respect to the width of a disordered zone acting as an interface between them and the amorphous matrix.

  11. Evaluation of the Edge Crack Torsion (ECT) Test for Mode 3 Interlaminar Fracture Toughness of Laminated Composites

    NASA Technical Reports Server (NTRS)

    Li, Jian; Lee, Edward W.; OBrien, T. Kevin; Lee, Shaw Ming

    1996-01-01

    An analytical and experimental investigation was carried out on G40-800/R6376 graphite epoxy laminates to evaluate the Edge Crack Torsion (ECT) test as a candidate for a standard Mode 3 interlaminar fracture toughness test for laminated composites. The ECT test consists of a (90/(+/- 45)(sub 3)/(+/- 45)(sub 3)/90))(sub s) laminate with a delamination introduced by a non-adhesive film at the mid-plane along one edge and loaded in a special fixture to create torsion along the length of the laminate. Dye penetrate enhanced X-radiograph of failed specimens revealed that the delamination initiated at the middle of the specimen length and propagated in a self similar manner along the laminate mid-plane. A three-dimensional finite element analysis was performed that indicated that a pure Mode 3 delamination exists at the middle of specimen length away from both ends. At the ends near the loading point a small Mode 2 component exists. However, the magnitude of this Mode 2 strain energy release rate at the loading point is small compared to the magnitude of Mode 3 component in the mid-section of the specimen. Hence, the ECT test yielded the desired Mode 3 delamination. The Mode 3 fracture toughness was obtained from a compliance calibration method and was in good agreement with the finite element results. Mode 2 End-Notched Flexure (ENF) tests and Mode 1 Double Cantilever Beam (DCB) tests were also performed for the same composite material. The Mode 1 fracture toughness was much smaller than both the Mode 2 and Mode 3 fracture toughness. The Mode 2 fracture toughness was found to be 75% of the Mode 3 fracture toughness.

  12. Physeal fractures, part II: fate of interposed periosteum in a physeal fracture.

    PubMed

    Gruber, Helen E; Phieffer, Laura S; Wattenbarger, J Michael

    2002-01-01

    This study describes the histologic features of periosteum interposed into a physeal fracture of the rat proximal tibia. Periosteum was introduced into a physeal fracture in two groups of animals: those with an intact physis after fracture, and those with the medial half of the physis surgically ablated. Specimens of the proximal tibia underwent histologic analysis at 2, 4, 6, 10, and 21 days after fracture to determine the histologic features of interposed periosteum in a physeal fracture. In animals with an intact physis, interposed periosteum underwent one of two fates: it was degraded by giant cells in the fracture plane, which allowed cellular infiltration, or if the periosteum was closely surrounded by physeal cartilage, the physis grew around it and appeared to force it toward the metaphysis. In animals whose physis received surgical ablation, physeal bar formation was always present, with poor organization of the remaining lateral growth plate. Histologic evidence from this study also underscores the fact that physeal bar formation occurs from the migration of osteoblasts and osteoclasts along vertical septa.

  13. Improvement of Mode I Interlaminar Fracture Toughness of Stitched Glass/Epoxy Composites

    NASA Astrophysics Data System (ADS)

    Göktaş, D.; Kennon, W. R.; Potluri, P.

    2016-11-01

    This study examines the improvement of Interlaminar Fracture Toughness (IFT) of multilayered 3D glass/epoxy textile composites when through thickness reinforcement is introduced. Three stitching techniques have been examined: Modified Lockstitch (ISO-301), Single-yarn Orthogonal-stitch (ISO-205) and Double-yarn Orthogonal-stitch (ISO-205). It was found that the use of class ISO-205 manual-type stitched reinforcement significantly enhanced the Mode I-IFT, GIC measured using a Double Cantilever Beam technique. Furthermore, in every case, the use of class ISO-205 stitching and high stitch densities offer a significant improvement of 74.5 % on Mode I-IFT against interlaminar delamination.

  14. Improvement of Mode I Interlaminar Fracture Toughness of Stitched Glass/Epoxy Composites

    NASA Astrophysics Data System (ADS)

    Göktaş, D.; Kennon, W. R.; Potluri, P.

    2017-04-01

    This study examines the improvement of Interlaminar Fracture Toughness (IFT) of multilayered 3D glass/epoxy textile composites when through thickness reinforcement is introduced. Three stitching techniques have been examined: Modified Lockstitch (ISO-301), Single-yarn Orthogonal-stitch (ISO-205) and Double-yarn Orthogonal-stitch (ISO-205). It was found that the use of class ISO-205 manual-type stitched reinforcement significantly enhanced the Mode I-IFT, GIC measured using a Double Cantilever Beam technique. Furthermore, in every case, the use of class ISO-205 stitching and high stitch densities offer a significant improvement of 74.5 % on Mode I-IFT against interlaminar delamination.

  15. Opening-mode fracture patterns and their shearing: an assessment of the state of knowledge and prediction capability

    NASA Astrophysics Data System (ADS)

    Aydin, A.

    2012-12-01

    Two common opening-mode fracture patterns include those comprising one set (Figure 1a) and two orthogonal sets (Figure 1b). It is also possible to have three mutually orthogonal opening-mode fractures, but this situation is rare. The prediction of the orientation and dimensional attributes of these simple systems requires a basic knowledge of the medium in which they occur (lithology, bedding, shape and distribution of initial flaws, elastic modulus, subcritical index and other environmental conditions) and the driving stresses or strains responsible for their formation. The issues related to fracture patterns become more complex when initial patterns of predominantly opening-mode fractures were later subjected to shearing. Shearing of a single set of opening-mode fractures (Figure 1c) produces splay fractures whose orientations and lengths show a significant variation. Given the attributes of the initial set and the orientation and relative magnitudes of the new stress components responsible for the shearing, and the mechanical behavoir of the fractures, it is possible to constrain the splay geometry. It turns out that the natural progression of the system is such that the new splays are sheared in a sequential manner to form remarkably consistent fracture domain patterns, which may be called "apparent conjugate." Well-documented case studies, some of which will be used in this presentation as templates, indicate that these fracture domain patterns can be visualized, but mapping their variation (local orientation and geometry of the individual components) is not a trivial task and may require knowledge both of some of the parameters referred to above and of the stress distribution about larger regional structures such as folds and faults. The shearing of orthogonal arrays of opening-mode fractures produces splay fractures diagonal to both orthogonal sets (Figure 1d). New through-going shear fractures, again in apparent conjugate patterns, utilize both members of

  16. Mode and mechanism of fatigue fracture of a pearlitic steel in hydrogen

    NASA Technical Reports Server (NTRS)

    Lo, S. H.; Johnson, H. H.

    1986-01-01

    It is presently suggested that there are two mechanisms that cause fatigue crack initiation in a specimen subjected to a hydrogen environment: either a critical concentration of hydrogen is attained within the specimen, causing Mode I crack initiation, or the presence of some hydrogen (below critical concentration) promotes the early onset of plastic instability at the sites of maximum strain. It is further suggested that in the static loading condition, a high hydrogen concentration may be attained by way of mechanical factors, causing Mode I crack initiation. While cyclic fatigue specimens exhibited Mode II crack initiation in air, only Mode I crack initiation emerged in a hydrogen environment.

  17. Dependence of mode I and mixed mode I/III fracture toughness on temperature for a ferritic/martensitic stainless steel

    SciTech Connect

    Li, H.; Jones, R.H.; Gelles, D.S.

    1995-04-01

    The objective is to investigate the dependence of mode I and mixed mode I/III fracture toughness on temperature in the range of {minus}95{degrees}C to 25{degrees}C for a low activation ferritic/martensitic stainless steel (F82-H). Mode I and mixed Mode I/III fracture toughnesses were investigated in the range of {minus}95 to 25{degree}C for a F82-H steel heat-treated in the following way; 1000{degree}C/20 h/air-cooled (AC), 1100{degree}C/7 min/AC, and 700{degree}C/2 h/AC. The results indicate that crack tip plasticity was increased by mixed mode loading, and suggest that at low temperature, mode I fracture toughness is the critical design parameter, but at temperatures above room temperature, expecially concerning fatigure and creep-fatigue crack growth rate, a mixed mode loading may be more harmful than a mode I loading for this steel because a mixed mode loading results in lower fracture toughness and higher crack tip plasticity (or dislocation activity).

  18. Teriparatide anabolic therapy as potential treatment of type II dens non-union fractures

    PubMed Central

    Pola, Enrico; Pambianco, Virginia; Colangelo, Debora; Formica, Virginia M; Autore, Giovanni; Nasto, Luigi A

    2017-01-01

    Odontoid fractures account for 5% to 15% of all cervical spine injuries and 1% to 2% of all spine fractures. Type II fractures are the most common fracture pattern in elderly patients. Treatment (rigid and non-rigid immobilization, anterior screw fixation of the odontoid and posterior C1-C2 fusion) remains controversial and represents a unique challenge for the treating surgeon. The aims of treatment in the elderly is to quickly restore pre-injury function while decreasing morbidity and mortality associated with inactivity, immobilization with rigid collar and prolonged hospitalization. Conservative treatment of type II odontoid fractures is associated with relatively high rates of non-union and in a few cases delayed instability. Options for treatment of symptomatic non-unions include surgical fixation or prolonged rigid immobilization. In this report we present the case of a 73-year-old woman with post-traumatic odontoid non-union successfully treated with Teriparatide systemic anabolic therapy. Complete fusion and resolution of the symptoms was achieved 12 wk after the onset of the treatment. Several animal and clinical studies have confirmed the potential role of Teriparatide in enhancing fracture healing. Our case suggests that Teriparatide may have a role in improving fusion rates of C2 fractures in elderly patients. PMID:28144584

  19. Imaging appearance of entrapped periosteum within a distal femoral Salter-Harris II fracture.

    PubMed

    Chen, Johnathan; Abel, Mark F; Fox, Michael G

    2015-10-01

    Salter Harris II fractures of the distal femur are associated with a high incidence of complications, especially premature physeal closure. Many risk factors for this high rate of premature physeal closure have been proposed. More recently, entrapment of periosteum within the physis has been suggested as an additional predisposing factor for premature physeal closure. The radiographic diagnosis of entrapped soft tissues, including periosteum, can be suggested in the setting of a Salter-Harris II fracture when the fracture does not reduce and physeal widening >3 mm remains. We report a patient who sustained a distal femoral Salter-Harris II fracture following a valgus injury. The patient had persistent distal medial physeal widening >5 mm following attempted reduction. A subsequent MRI revealed a torn periosteum entrapped within the distal femoral physis. Following removal of the periosteum, the patient developed a leg length discrepancy which required physiodesis of the contralateral distal femur. We present this case to raise awareness of the importance of having a high index of suspicion of periosteal entrapment in the setting of Salter-Harris II fractures since most consider entrapped periosteum an indication for surgery.

  20. Mixed-mode I/III fracture toughness of a ferritic/martensitic stainless steel

    SciTech Connect

    Li, Huaxin; Jones, R.H.; Gelles, D.S.; Hirth, J.P.

    1993-10-01

    The critical J-integrals of mode I (J{sub IC}), mixed-mode I/III (J{sub MC}), and mode III (J{sub IIIC}) were examined for a ferritic stainless steel (F-82H) at ambient temperature. A determination of J{sub MC} was made using modified compact-tension specimens. Different ratios of tension/shear stress were achieved by varying the principal axis of the crack plane between 0 and 55 degrees from the load line. Results showed that J{sub MC} and tearing modulus (T{sub M}) values varied with the crack angles and were lower than their mode I and mode III counterparts. Both the minimum J{sub MC} and T{sub M} values occurred at a crack angle between 40 and 50 degrees, where the load ratio of {sigma}{sub i}/{sigma}{sub iii} was 1.2 to 0.84. The J{sub min} was 240 Kj/M{sup 2}, and ratios of J{sub IC}/J{sub min} and J{sub IIIC}/J{sub min} were 2.1 and 1.9, respectively. The morphology of fracture surfaces was consistent with the change of J{sub MC} and T{sub M} values. While the upper shelf-fracture toughness of F-82H depends on loading mode, the J{sub min} remains very high. Other important considerations include the effect of mixed-mode loading on the DBT temperature, and effects of hydrogen and irradiation on J{sub min}.

  1. Uncommon Variant of Type II Monteggia Fracture with Concomitant Distal Humeral Fracture

    PubMed Central

    Matta, Jihad F.; El Rassi, George S.; Abd El Nour, Hicham G.; El Asmar, Rachel

    2015-01-01

    Monteggia fracture-dislocation, a common injury sustained by pediatric population, is a rare entity in adults. It was first observed by Giovanni Battista Monteggia and later classified by Bado into 4 groups. The term “Monteggia equivalent or variant” was introduced to describe certain injuries with similar radiographic pattern and biomechanism of injury. Since then various types and their variants have been described in the literature. We present a complex fracture pattern in a 55-year-old male not previously described in the literature along with its treatment modality and favorable outcome. PMID:26550509

  2. Kohn-Sham density functional theory prediction of fracture in silicon carbide under mixed mode loading

    NASA Astrophysics Data System (ADS)

    Leung, K. W. K.; Pan, Z. L.; Warner, D. H.

    2016-03-01

    The utility of silicon carbide (SiC) for high temperature structural application has been limited by its brittleness. To improve its ductility, it is paramount to develop a sound understanding of the mechanisms controlling crack propagation. In this manuscript, we present direct ab initio predictions of fracture in SiC under pure mode I and mixed mode loading, utilizing a Kohn-Sham Density Functional Theory (KSDFT) framework. Our results show that in both loading cases, cleavage occurs at a stress intensity factor (SIF) only slightly higher than the Griffith toughness, focusing on a (1 1 1) [1 \\bar{1} 0] crack in the 3C-SiC crystal structure. This lattice trapping effect is shown to decrease with mode mixity, due to the formation of a temporary surface bond that forms during decohesion under shear. Comparing the critical mode I SIF to the value obtained in experiments suggests that some plasticity may occur near a crack tip in SiC even at low temperatures. Ultimately, these findings provide a solid foundation upon which to study the influence of impurities on brittleness, and upon which to develop empirical potentials capable of realistically simulating fracture in SiC.

  3. Analysis of the Numerical and Geometrical Parameters Influencing the Simulation of Mode I and Mode II Delamination Growth in Unidirectional and Textile Composites

    NASA Astrophysics Data System (ADS)

    Jacques, S.; De Baere, I.; Van Paepegem, W.

    2015-12-01

    The reliability of composite structures depends, among other damage mechanisms, on their ability to withstand delaminations. In order to have a better understanding of the cohesive zone method technique for delamination simulations, a complete analysis of the multiple parameters influencing the results is necessary. In this paper the work is concentrated on the cohesive zone method using cohesive elements. First a summary of the theory of the cohesive zone method is given. A numerical investigation on the multiple parameters influencing the numerical simulation of the mode I and mode II delamination tests has been performed. The parameters such as the stabilization method, the output frequency, the friction and the computational efficiency have been taken into account. The results will be compared to an analytical solution obtained by linear elastic fracture mechanics. Additionally the numerical simulation results will be compared to the experimental results of a glass-fibre reinforced composite material for the mode I Double Cantilever Beam (DCB) and to a carbon fibre 5-harness satin weave reinforced polyphenylene sulphide composite for the mode I DCB and mode II End Notched Flexure (ENF).

  4. Fracture resistance of premolars with bonded class II amalgams.

    PubMed

    Dias de Souza, Grace Mendonça; Pereira, Gisele Damiana Silveira; Dias, Carlos Tadeu Santos; Paulillo, Luis Alexandre Maffei Sartini

    2002-01-01

    This study evaluated the fracture resistance of maxillary premolars with MOD cavity preparation and simulated periodontal ligament. The teeth were restored with silver amalgam (G1), Scotchbond Multi-Purpose Plus and silver amalgam (G2) and Panavia F and silver amalgam (G3). After restorations were made, the specimens were stored at 37 degrees C for 24 hours at 100% humidity and submitted to the compression test in the Universal Testing Machine (Instron). The statistical analysis of the results (ANOVA and Tukey Test) revealed that the fracture resistance of group 2 (G2=105.720 kgF) was superior to those of groups 1 (G1=72.433 kgF) and 3 (G3=80.505 kgF) that did not differ between them.

  5. Propagating mode-I fracture in amorphous materials using the continuous random network model

    NASA Astrophysics Data System (ADS)

    Heizler, Shay I.; Kessler, David A.; Levine, Herbert

    2011-08-01

    We study propagating mode-I fracture in two-dimensional amorphous materials using atomistic simulations. We use the continuous random network model of an amorphous material, creating samples using a two-dimensional analog of the Wooten-Winer-Weaire Monte Carlo algorithm. For modeling fracture, molecular-dynamics simulations were run on the resulting samples. The results of our simulations reproduce the main experimental features. In addition to achieving a steady-state crack under a constant driving displacement (which has not yet been achieved by other atomistic models for amorphous materials), the runs show microbranching, which increases with driving, transitioning to macrobranching for the largest drivings. In addition to the qualitative visual similarity of the simulated cracks to experiment, the simulation also succeeds in reproducing qualitatively the experimentally observed oscillations of the crack velocity.

  6. A tension-mode fracture model for bolted joints in laminated composites

    SciTech Connect

    Schulz, K.C.; Packman, P.F.; Eisenmann, J.R.

    1995-06-01

    A failure prediction model for bolted joints in generally orthotropic laminated composite plates that fail in the tension mode under bearing loading conditions has been developed. The plate is analyzed as a bulk orthotropic plate whose material properties are determined through the application of classical lamination theory to facilitate practical application of the model. Ply-by-ply laminated analysis is not required. Fracture mechanics concepts are applied to a pseudo-flaw which is related to the physical cracking of the laminate at the joint. The maximum circumferential stress concept is extended to orthotropic materials where both the fracture toughness and stress intensity vary with orientation. Excellent correlation between experimental tests conducted on single-bolt joints for two laminate layups and analytical prediction was found.

  7. Factors influencing the Mode I interlaminar fracture toughness of a rubber toughened thermoplastic matrix composite

    NASA Technical Reports Server (NTRS)

    Parker, D. S.; Yee, A. F.

    1989-01-01

    The use of a rubber modified thermoplastic resin has been investigated as a method to improve the Mode I interlaminar fracture toughness of a unidirectional continuous carbon fiber composite. Test results show that the improvement in the fracture toughness is less than expected due to rubber particle agglomeration, solvent and molding induced crystallization of the matrix and poor fiber/matrix adhesion. The plastic zone in composites utilizing tough matrices can extend well beyond a single interfibrillar spacing. However, the development of the plastic zone is limited due to the failure of the fiber/matrix interface. In order to fully evaluate the potential of tough composites using toughened matrices, any improvement made in the matrix toughness must be coupled with improvements in the fiber/matrix adhesion.

  8. Results of ASTM round robin testing for mode 1 interlaminar fracture toughness of composite materials

    NASA Technical Reports Server (NTRS)

    Obrien, T. Kevin; Martin, Roderick H.

    1992-01-01

    The results are summarized of several interlaboratory 'round robin' test programs for measuring the mode 1 interlaminar fracture toughness of advanced fiber reinforced composite materials. Double Cantilever Beam (DCB) tests were conducted by participants in ASTM committee D30 on High Modulus Fibers and their Composites and by representatives of the European Group on Fracture (EGF) and the Japanese Industrial Standards Group (JIS). DCB tests were performed on three AS4 carbon fiber reinforced composite materials: AS4/3501-6 with a brittle epoxy matrix; AS4/BP907 with a tough epoxy matrix; and AS4/PEEK with a tough thermoplastic matrix. Difficulties encountered in manufacturing panels, as well as conducting the tests are discussed. Critical issues that developed during the course of the testing are highlighted. Results of the round robin testing used to determine the precision of the ASTM DCB test standard are summarized.

  9. Mixed-mode fracture in unidirectional graphite epoxy composite laminates with central notch

    NASA Technical Reports Server (NTRS)

    Binienda, Wieslaw K.; Reddy, E. S.

    1992-01-01

    Mixed-mode matrix fracture in central notched off-axis unidirectional composite laminates was investigated. A limited number of unidirectional tensile type specimens with a central, horizontal, notch were tested. Crack initiation and propagation were examined under various local stress fields that were controlled by fiber orientations. The tested specimens were simulated using a two dimensional finite element method with constant strain loading. The strain energy release rates along the crack were evaluated via crack closure technique. The variation of critical strain energy rates with off-axis angle was studied. The results from single (one-sided) and double (two-sided) crack simulations were presented and compared.

  10. A model for predicting crack growth rate for mixed mode fracture under biaxial loads

    NASA Astrophysics Data System (ADS)

    Shliannikov, V. N.; Braude, N. Z.

    1992-09-01

    A model for predicting the crack growth rate of an initially angled crack under biaxial loads of arbitrary direction is suggested. The model is based on a combination of both the Manson-Coffin equation for low cycle fatigue and the Paris equation for fatigue crack propagation. The model takes into consideration the change in material plastic properties in the region around the crack tip due to the stress state, together with the initial orientation of the crack and also its trajectory of growth. Predictions of crack growth rate for any mixed mode fracture is based on the results of uniaxial tension experiments.

  11. Subcritical crack growth under mode I, II, and III loading for Coconino sandstone

    NASA Astrophysics Data System (ADS)

    Ko, Tae Young

    of 34 to 38 and the parameter A has the range of 1.02x10-2 to 6.52x10-2 m/s. The effect of confining stress, specimen size, and water saturation on subcritical crack growth under mode II loading has also been investigated. Finally strength parameters for Coconino sandstone were determined experimentally, including tensile strength, uniaxial compressive strength, cohesion, internal friction angle, in-plane/our-of-plane shear strength and the fracture toughness under mode I, II, and III loading.

  12. Outcomes of Nonoperative Treatment of Salter-Harris II Distal Radius Fractures

    PubMed Central

    Larsen, Meredith C.; Bohm, Kyle C.; Rizkala, Amir R.; Ward, Christina M.

    2016-01-01

    Background: Despite the frequent occurrence of these injuries, we know little about the natural history of Salter-Harris II (SH II) distal radius fractures. We conducted a systematic review of studies examining the radiographic and clinical outcomes of nonoperatively managed SH II distal radius fractures. Methods: Systematic searches of the MEDLINE and Cochrane computerized literature databases and manual searches of bibliographies were performed. We reviewed both descriptive and quantitative data. Results: Seven studies including 434 SH II fractures were reviewed. Two studies reported clinical outcomes based on patient age, but neither study described a statistical correlation between patient age and outcome. Two studies discussed the effect of age on radiographic outcome and reported higher rates of anatomic remodeling in children 10 years or younger. Two studies with long-term (average follow-up greater than 8 years) clinical results reported complication rates of 5%. Long-term follow-up of radiographic outcomes appeared in 4 studies with variable results. Five studies reported the frequency of premature physeal arrest after SH II fractures, with results ranging from 0% to 4.3%. Conclusions: Based on this review, no recommendations can be made as to what defines an acceptable reduction or which fractures would benefit from surgical intervention. Angular deformity seems to correct to an acceptable alignment in patients less than 10 years of age, but these younger patients seem to be at higher risk for symptomatic shortening if a growth arrest occurs. Redisplacement after reduction is fairly common, and other more severe complications such as pain, loss of motion, and nerve injury can occur. PMID:27418886

  13. Characterization of Mode I Fracture and Morphological Properties of PLLA Blends with Addition of Lysine Triisocyanate

    NASA Astrophysics Data System (ADS)

    Vannaladsaysy, Vilay; Todo, Mitsugu

    Poly(L-lactic acid) (PLLA) was toughened by blending with three different ductile biopolymers such as poly (ε-caprolactone) (PCL), poly(butylene succinate-co-e-caprolactone) (PBSC), poly (butylene succinate-co-L-lactate) (PBSL). The blend ratio was fixed to 50:50. Lysine triisocyanate (LTI) was added to the blends as a compatibilizer. Characterizations such as Fourier transform infra-red (FT-IR) spectroscopy, field-emission electron microscope (FE-SEM), and mode I fracture test were used to characterize the effectiveness of LTI on the mechanical and morphological properties of various PLLA blends. It was found that PLLA/PCL blend shows the highest toughness energy among the binary blends. On the other hand, addition of LTI in PLLA/PBSC blend exhibits the best toughness property. Based on the FE-SEM observation, fractured surfaces of PLLA blends with LTI indicate ductile fracture with dense elongated fibrils. The largest damage zone is generated in the vicinity of crack-trip, suggesting that high energy dissipation occurred in the crack-trip region. FT-IR analysis also suggested that the NCO groups of LTI were acted as a compatibilizer, as the results of interaction between the two phases of the polymer blends.

  14. Mode I Fracture Toughness Prediction for Multiwalled-Carbon-Nanotube Reinforced Ceramics

    SciTech Connect

    Nguyen, Ba Nghiep; Henager, Charles H.

    2015-08-27

    This article develops a multiscale model to predict fracture toughness of multiwalled-carbon-nanotube (MWCNT) reinforced ceramics. The model bridges different scales from the scale of a MWCNT to that of a composite domain containing a macroscopic crack. From the nano, micro to meso scales, Eshelby-Mori-Tanaka models combined with a continuum damage mechanics approach are explored to predict the elastic damage behavior of the composite as a function of MWCNT volume fraction. MWCNTs are assumed to be randomly dispersed in a ceramic matrix subject to cracking under loading. A damage variable is used to describe matrix cracking that causes reduction of the elastic modulus of the matrix. This damage model is introduced in a modified boundary layer modeling approach to capture damage initiation and development at a tip of a pre-existing crack. Damage and fracture are captured only in a process window containing the crack tip under plane strain Mode I loading. The model is validated against the published experimental fracture toughness data for a MWCNT 3 mol% yttria stabilized zirconia composite system. In addition, crack resistance curves as a function of MWCNT content are predicted and fitted by a power law as observed in the experiments on zirconia.

  15. Effects of pulp capping materials on fracture resistance of Class II composite restorations

    PubMed Central

    Kucukyilmaz, Ebru; Yasa, Bilal; Akcay, Merve; Savas, Selcuk; Kavrik, Fevzi

    2015-01-01

    Objective: The aim of this study was to investigate the effect of cavity design and the type of pulp capping materials on the fracture resistance of Class II composite restorations. Materials and Methods: Sixty freshly extracted, sound molar teeth were selected for the study. A dovetail cavity on the mesio-occlusal and a slot cavity on disto-occlusal surfaces of each tooth were prepared, and the teeth were divided 4 groups which one of them as a control group. The pulp capping materials (TheraCal LC, Calcimol LC, Dycal) applied on pulpo-axial wall of each cavity, and the restoration was completed with composite resin. The teeth were subjected to a compressive load in a universal mechanical testing machine. The surfaces of the tooth and restoration were examined under a stereomicroscope. The data were analyzed using factorial analysis of variance and Tukey's test. Results: For pulp capping materials, the highest fracture load (931.15 ± 203.81 N) and the lowest fracture load (832.28 ± 245.75 N) were calculated for Control and Dycal group, respectively. However, there were no statistically significant differences among all groups (P > 0.05). The fracture load of the dovetail groups was significantly higher than those of the slot cavity groups (P < 0.05). Conclusion: Dovetail cavity design shows better fracture resistance in Class II composite restorations, independent of used or not used pulp capping materials. PMID:26038653

  16. Influence of preparation design and ceramic thicknesses on fracture resistance and failure modes of premolar partial coverage restorations

    PubMed Central

    Guess, Petra C.; Schultheis, Stefan; Wolkewitz, Martin; Zhang; Strub, Joerg R.

    2015-01-01

    Statement of problem Preparation designs and ceramic thicknesses are key factors for the long-term success of minimally invasive premolar partial coverage restorations. However, only limited information is presently available on this topic. Purpose The aim of this in vitro study was to evaluate the fracture resistance and failure modes of ceramic premolar partial coverage restorations with different preparation designs and ceramic thicknesses. Material and methods Caries-free human premolars (n= 144) were divided into 9 groups. Palatal onlay preparation comprised reduction of the palatal cusp by 2 mm (Palatal-Onlay-Standard), 1 mm (Palatal-Onlay-Thin), or 0.5 mm (Palatal-Onlay-Ultra-Thin). Complete-coverage onlay preparation additionally included the buccal cusp (Occlusal-Onlay-Standard; Occlusal-Onlay-Thin; Occlusal-Onlay-Ultra-Thin). Labial surface preparations with chamfer reductions of 0.8 mm (Complete-Veneer-Standard), 0.6 mm (Complete-Veneer-Thin) and 0.4 mm (Complete-Veneer-Ultra-Thin) were implemented for complete veneer restorations. Restorations were fabricated from a pressable lithium-disilicate ceramic (IPS-e.max-Press) and cemented adhesively (Syntac-Classic/Variolink-II). All specimens were subjected to cyclic mechanical loading (F= 49 N, 1.2 million cycles) and simultaneous thermocycling (5°C to 55°C) in a mouth-motion simulator. After fatigue, restorations were exposed to single-load-to-failure. Two-way ANOVA was used to identify statistical differences. Pair-wise differences were calculated and P-values were adjusted by the Tukey–Kramer method (α= .05). Results All specimens survived fatigue. Mean (SD) load to failure values (N) were as follows: 837 (320/Palatal-Onlay-Standard), 1055 (369/Palatal-Onlay-Thin), 1192 (342/Palatal-Onlay-Ultra-Thin), 963 (405/Occlusal-Onlay-Standard), 1108 (340/Occlusal-Onlay-Thin), 997 (331/Occlusal-Onlay-Ultra-Thin), 1361 (333/Complete-Veneer-Standard), 1087 (251/Complete-Veneer-Thin), 883 (311/Complete

  17. Modification of fracture surfaces by dissolution. Part II

    SciTech Connect

    Johnson, B.

    1983-01-01

    This study focuses upon how and to what extent dissolution related fluid/rock interactions modify the morphology and roughness of surfaces on Sioux Quartzite. Dissolution experiments consisted of reacting small discs of Sioux Quartzite in sealed gold capsules containing either distilled water or 0.05 N to 4.0 N aqueous solutions of Na/sub 2/CO/sub 3/. Samples were reacted at 200/sup 0/C and 20 to 30 MPa fluid pressures for 2 to 5 days. Two markedly different starting surface textures were used: polished, optically flat surfaces and tensile fracture surfaces. An exploratory experiment also was performed to assess the occurrence of a pressure solution phenomenon on a polished quartzite surface at contact regions of indenting quartz sand grains. Scanning electron microscopy studies indicate progressive increases in the amount of dissolution produced significant changes of surface roughness for both initial surface textures. Surface roughness increased measurably, with the initially polished surfaces exhibiting the more dramatic changes. The pressure solution experiments did not produce definite results, but several surface features are suggestive of dissolution enhancement at load carrying contacts. 9 refs., 10 figs.

  18. Fracture resistance and failure mode of posterior fixed dental prostheses fabricated with two zirconia CAD/CAM systems

    PubMed Central

    López-Suárez, Carlos; Gonzalo, Esther; Peláez, Jesús; Rodríguez, Verónica

    2015-01-01

    Background In recent years there has been an improvement of zirconia ceramic materials to replace posterior missing teeth. To date little in vitro studies has been carried out on the fracture resistance of zirconia veneered posterior fixed dental prostheses. This study investigated the fracture resistance and the failure mode of 3-unit zirconia-based posterior fixed dental prostheses fabricated with two CAD/CAM systems. Material and Methods Twenty posterior fixed dental prostheses were studied. Samples were randomly divided into two groups (n=10 each) according to the zirconia ceramic analyzed: Lava and Procera. Specimens were loaded until fracture under static load. Data were analyzed using Wilcoxon´s rank sum test and Wilcoxon´s signed-rank test (P<0.05). Results Partial fracture of the veneering porcelain occurred in 100% of the samples. Within each group, significant differences were shown between the veneering and the framework fracture resistance (P=0.002). The failure occurred in the connector cervical area in 80% of the cases. Conclusions All fracture load values of the zirconia frameworks could be considered clinically acceptable. The connector area is the weak point of the restorations. Key words:Fixed dental prostheses, zirconium-dioxide, zirconia, fracture resistance, failure mode. PMID:26155341

  19. Atlanto-axial dislocation complicating a type II odontoid fracture. Reduction and final fixation.

    PubMed

    Riouallon, G; Pascal-Moussellard, H

    2014-05-01

    A case of traumatic posterolateral C1-C2 dislocation associated with odontoid fracture is reported. This is a rare case of traumatic posterolateral C1-C2 dislocation associated with odontoid fracture. Its management is discussed. A traumatic dislocation of atlanto-axial joint associated with an odontoid fracture remains a rare injury. No case of posterior dislocation has been reported so far in the literature with this type of management. The case is of a 25 year-old-man with a primary atlanto-axial posterolateral dislocation associated with a type II displaced odontoid fracture without any neurological complication. The patient underwent gentle traction during 24 hours with a halo frame. An incomplete reduction was achieved. Two days later, a complete reduction was obtained thanks to a preoperative manual traction maintained by a Mayfield (R) modified skull clamp. Anterior C1-C2 fixation was performed according to Vaccaro's technique. The patient wore a cervical collar and underwent physiotherapy during three months. To our best knowledge, this case represents the first traumatic atlanto-axial dislocation associated with an odontoid fracture which was treated through retropaharyngeal approach. This had been rendered possible thanks to the final reduction maneuver in extension.

  20. Effect of thickness and loading mode on the fracture properties of V-4Cr-4Ti at room temperature

    SciTech Connect

    Li, H.; Kurtz, R.J.; Jones, R.H.

    1998-03-01

    The effect of thickness on the room temperature (RT) mode I fracture behavior of V-4Cr-4Ti has been investigated. Mode i fracture properties were measured from J-integral tests of compact tension (CT) specimens ranging in thickness from 6.4 mm to 25.4 mm. All specimens were machined in the T-L orientation and vacuum annealed following final matching. Two heats of V-4Cr-4Ti were tested. Specimens 6.4 mm and 12.7 mm thick were taken from ANL Heat No. 832665. The 25.4 mm thick specimens were obtained from GA Heat No. 832864. J-R curves were generated by the single specimen unload-compliance test technique in accordance with ASTM E813. All tests were performed in laboratory air at 25 C. Fracture of V-4Cr-4Ti under mixed-mode loading conditions showed the same trend observed previously for V-5Cr-5Ti and for other tough materials. For materials which fail by microvoid coalescence, the addition of an out-of-plane shear loading component introduces incompatibility stresses at particle interfaces in the trajectory of the crack. These incompatibility stresses cause particle/matrix decohesion or particle fracture which leads to void formation that limits the mode i plastic flow field. The present results demonstrates that fracture of V-4Cr-4Ti is sensitive to the addition of shear loading components and that model fracture toughness tests may not give the most conservative measure of resistance to ductile fracture.

  1. The influence of microstructure and strength on the fracture mode and toughness of 7XXX series aluminum alloys

    NASA Astrophysics Data System (ADS)

    Ludtka, Gerard M.; Laughlin, David E.

    1982-03-01

    The effects of microstructure and strength on the fracture toughness of ultra high strength aluminum alloys have been investigated. For this study three ultra high purity compositions were chosen and fabricated into 1.60 mm (0.063 inches) sheet in a T6 temper providing a range of yield strengths from 496 MPa (72 ksi) to 614 MPa (89 ksi). These alloys differ only in the volume fraction of the fine matrix strengthening precipitates (G. P. ordered + η' ). Fracture toughness data were generated using Kahn-type tear tests, as well as R-curve and J c analyses performed on data from 102 mm wide center cracked tension panel tests. Consistent with previous studies, it has been demonstrated that the toughness decreases as the yield strength is increased by increasing the solute content. Concomitant with this decrease in toughness, a transition in fracture mode was observed from predominantly transgranular dimpled rupture to predominantly intergranular dimpled rupture. Both quantitative fractography and X-ray microanalysis clearly demonstrate that fracture initiation for the two fracture modes occurred by void formation at the Cr-dispersoids ( E-phase). In the case of intergranular fracture, void coalescence was facilitated by the grain boundary η precipitates. The difference in fracture toughness behavior of these alloys has been shown to be dependent on the coarseness of matrix slip and the strength differential between the matrix and precipitate free zone (σM-σPFZ). A new fracture mechanism has been proposed to explain the development of the large amounts of intergranular fracture observed in the low toughness alloys.

  2. Evaluation of a fracture failure mode in the Space Shuttle hydrogen pressurization system flow control valves

    NASA Astrophysics Data System (ADS)

    Hauver, S. E.; Sueme, D. R.

    1992-07-01

    During acceptance testing of the Space Shuttle Endeavor hydrogen flow control valves, which are used in the Orbiter's fuel tank pressurization system, two of the valves experienced fracture of the poppet flange. The poppets are made of 440 C, a high strength, wear-resistant, low ductility, martensitic stainless steel. The investigation which was initiated to determine the cause of these failures is traced. All aspects of the poppet processing that may have introduced a defect were assessed. This included machining, heat treating, passivation, assembly, and test. In addition, several potential failure modes were investigated. The extensive investigation revealed no obvious cause of the failures, but did result in a recommendation for a different material application.

  3. Fracture toughness of the IEA heat of F82H ferritic/martensitic stainless steel as a function of loading mode

    SciTech Connect

    Li, Huaxin; Gelles, D.S.; Hirth, J.P.

    1997-04-01

    Mode I and mixed-mode I/III fracture toughness tests were performed for the IEA heat of the reduced activation ferritic/martensitic stainless steel F82H at ambient temperature in order to provide comparison with previous measurements on a small heat given a different heat treatment. The results showed that heat to heat variations and heat treatment had negligible consequences on Mode I fracture toughness, but behavior during mixed-mode testing showed unexpected instabilities.

  4. Fractures

    MedlinePlus

    A fracture is a break, usually in a bone. If the broken bone punctures the skin, it is called an open ... falls, or sports injuries. Other causes are low bone density and osteoporosis, which cause weakening of the ...

  5. Simulations of flow mode distributions on rough fracture surfaces using a parallelized Smoothed Particle Hydrodynamics (SPH) model

    NASA Astrophysics Data System (ADS)

    Kordilla, J.; Shigorina, E.; Tartakovsky, A. M.; Pan, W.; Geyer, T.

    2015-12-01

    Under idealized conditions (smooth surfaces, linear relationship between Bond number and Capillary number of droplets) steady-state flow modes on fracture surfaces have been shown to develop from sliding droplets to rivulets and finally (wavy) film flow, depending on the specified flux. In a recent study we demonstrated the effect of surface roughness on droplet flow in unsaturated wide aperture fractures, however, its effect on other prevailing flow modes is still an open question. The objective of this work is to investigate the formation of complex flow modes on fracture surfaces employing an efficient three-dimensional parallelized SPH model. The model is able to simulate highly intermittent, gravity-driven free-surface flows under dynamic wetting conditions. The effect of surface tension is included via efficient pairwise interaction forces. We validate the model using various analytical and semi-analytical relationships for droplet and complex flow dynamics. To investigate the effect of surface roughness on flow dynamics we construct surfaces with a self-affine fractal geometry and roughness characterized by the Hurst exponent. We demonstrate the effect of surface roughness (on macroscopic scales this can be understood as a tortuosity) on the steady-state distribution of flow modes. Furthermore we show the influence of a wide range of natural wetting conditions (defined by static contact angles) on the final distribution of surface coverage, which is of high importance for matrix-fracture interaction processes.

  6. Spacing and aperture of opening-mode fractures in layered materials

    NASA Astrophysics Data System (ADS)

    Bai, Taixu

    This dissertation investigates the mechanical control on spacing and aperture of equally-spaced fractures in layered materials using the Finite Element Method, based on the theories of elasticity and linear fracture mechanics. It also investigates the effects of fracture spacing and aperture on fluid flow through the equally-spaced fractures. The results show that under a remote extension in the direction perpendicular to the fractures the normal stress acting in this direction between adjacent fractures changes from tensile to compressive as the fracture spacing to layer thickness ratio changes from greater than to less than a critical value. This stress transition precludes further infilling of fractures unless they are driven by mechanisms other than an extension, or there are significant flaws between the fractures. Hence, it defines the condition of saturation for fractures formed under extension in flawless layered materials. When flaws are present, further infilling of fractures is possible depending upon the size and locations of the flaws. The aspect ratio of equally-spaced fractures is linearly related to the average strain, the overburden stress, and the internal fluid pressure. The aspect ratio increases nonlinearly with increasing fracture spacing to layer thickness ratio because of the mechanical interaction between adjacent fractures. The interaction becomes insignificant when the spacing to layer thickness ratio is greater than about 6.0. The aspect ratio also depends on the ratio of Young's modulus of the fractured layer to that of the neighboring layers. This dependence is significant when the fracture spacing to layer thickness ratio is less than 1.3, otherwise it is negligibe. The aspect ratio is insensitive to variations in Poisson's ratios. Fluid flow rate through equally-spaced fractures does not always increases with increasing fracture density, i.e., with decreasing spacing to layer thickness ratio. There is an optimum value for the ratio

  7. Notch strengthening or weakening governed by transition of shear failure to normal mode fracture

    PubMed Central

    Lei, Xianqi; Li, Congling; Shi, Xinghua; Xu, Xianghong; Wei, Yujie

    2015-01-01

    It is generally observed that the existence of geometrical discontinuity like notches in materials will lead to strength weakening, as a resultant of local stress concentration. By comparing the influence of notches to the strength of three typical materials, aluminum alloys with intermediate tensile ductility, metallic glasses with no tensile ductility, and brittle ceramics, we observed strengthening in aluminum alloys and metallic glasses: Tensile strength of the net section in circumferentially notched cylinders increases with the constraint quantified by the ratio of notch depth over notch root radius; in contrast, the ceramic exhibit notch weakening. The strengthening in the former two is due to resultant deformation transition: Shear failure occurs in intact samples while samples with deep notches break in normal mode fracture. No such deformation transition was observed in the ceramic, and stress concentration leads to its notch weakening. The experimental results are confirmed by theoretical analyses and numerical simulation. The results reported here suggest that the conventional criterion to use brittleness and/or ductility to differentiate notch strengthening or weakening is not physically sound. Notch strengthening or weakening relies on the existence of failure mode transition and materials exhibiting shear failure while subjected to tension will notch strengthen. PMID:26022892

  8. Notch strengthening or weakening governed by transition of shear failure to normal mode fracture.

    PubMed

    Lei, Xianqi; Li, Congling; Shi, Xinghua; Xu, Xianghong; Wei, Yujie

    2015-05-29

    It is generally observed that the existence of geometrical discontinuity like notches in materials will lead to strength weakening, as a resultant of local stress concentration. By comparing the influence of notches to the strength of three typical materials, aluminum alloys with intermediate tensile ductility, metallic glasses with no tensile ductility, and brittle ceramics, we observed strengthening in aluminum alloys and metallic glasses: Tensile strength of the net section in circumferentially notched cylinders increases with the constraint quantified by the ratio of notch depth over notch root radius; in contrast, the ceramic exhibit notch weakening. The strengthening in the former two is due to resultant deformation transition: Shear failure occurs in intact samples while samples with deep notches break in normal mode fracture. No such deformation transition was observed in the ceramic, and stress concentration leads to its notch weakening. The experimental results are confirmed by theoretical analyses and numerical simulation. The results reported here suggest that the conventional criterion to use brittleness and/or ductility to differentiate notch strengthening or weakening is not physically sound. Notch strengthening or weakening relies on the existence of failure mode transition and materials exhibiting shear failure while subjected to tension will notch strengthen.

  9. A MODEL STUDY OF TRANSVERSE MODE COUPLING INSTABILITY AT NATIONAL SYNCHROTRON LIGHT SOURCE-II (NSLS-II).

    SciTech Connect

    BLEDNYKH, A.; WANG, J.M.

    2005-05-15

    The vertical impedances of the preliminary designs of National Synchrotron Light Source II (NSLS-II) Mini Gap Undulators (MGU) are calculated by means of GdfidL code. The Transverse Mode Coupling Instability (TMCI) thresholds corresponding to these impedances are estimated using an analytically solvable model.

  10. Fracture prediction for the proximal femur using finite element models: Part II--Nonlinear analysis.

    PubMed

    Lotz, J C; Cheal, E J; Hayes, W C

    1991-11-01

    In Part I we reported the results of linear finite element models of the proximal femur generated using geometric and constitutive data collected with quantitative computed tomography. These models demonstrated excellent agreement with in vitro studies when used to predict ultimate failure loads. In Part II, we report our extension of those finite element models to include nonlinear behavior of the trabecular and cortical bone. A highly nonlinear material law, originally designed for representing concrete, was used for trabecular bone, while a bilinear material law was used for cortical bone. We found excellent agreement between the model predictions and in vitro fracture data for both the onset of bone yielding and bone fracture. For bone yielding, the model predictions were within 2 percent for a load which simulated one-legged stance and 1 percent for a load which simulated a fall. For bone fracture, the model predictions were within 1 percent and 17 percent, respectively. The models also demonstrated different fracture mechanisms for the two different loading configurations. For one-legged stance, failure within the primary compressive trabeculae at the subcapital region occurred first, leading to load transfer and, ultimately, failure of the surrounding cortical shell. However, for a fall, failure of the cortical and trabecular bone occurred simultaneously within the intertrochanteric region. These results support our previous findings that the strength of the subcapital region is primarily due to trabecular bone whereas the strength of the intertrochanteric region is primarily due to cortical bone.

  11. A discrete dislocation analysis of mixed mode fracture at bimaterial interfaces

    NASA Astrophysics Data System (ADS)

    O'Day, Michael; Curtin, William

    2004-03-01

    The influence of mode mixity on crack growth and failure at a metal/ceramic bimaterial interface is examined within the discrete dislocation (DD) plasticity framework. In this method, plasticity occurs via the motion of a large number of dislocations embedded in a linearly elastic medium. No plastic constitutive law is required, however a set of rules governing dislocation nucleation, motion and annihilation is necessary. The numerical procedure uses a superposition technique, developed specifically to allow the efficient solution of DD problems with elastic inhomogeneities. An interface crack exists in the unloaded configuration, and a mode independent cohesive zone law characterizes the interface ahead of the crack tip. The influence of mode mixity on crack growth resistance curve (R-curve) behavior is qualitatively similar to continuum plasticity calculations, where increasing mode mixity leads to increasing toughness. However, deviations can arise due to (i) statistical effects, and (ii) the discrete nature of plasticity. Crack blunting, dislocation patterning and the existence of preferential slip planes all emerge naturally from the boundary value problem solution and give insight into observed R-curve trends.

  12. Surgical treatment of intraarticular calcaneous fractures of sanders' types II and III. Systematic review

    PubMed Central

    Pelliccioni, Adriano Augusto Antoniazzi; Bittar, Cíntia Kelly; Zabeu, José Luis Amim

    2012-01-01

    Objective This paper aims to identify the most effective surgical technique for intraarticular calcaneal fractures of Sanders' types II and III. Methods Systematic review of comparative randomized clinical trials on surgical treatment of the intraarticular fractures of the calcaneus (Sanders types II and III) that used the questionnaire of the American Orthopaedic Foot and Ankle Society. The studies were identified and retrieved in the following databases - LILACS, MEDLINE/PubMed, Cochrane Library, SciELO, EMBASE, Science Direct, Scopus, Journals@Ovid, ISI Web of Knowledge, Evidence Based Medicine, besides consulting the references of studies accessed. The keywords used Boolean logic (AND and OR): "calcaneus fracture, calcaneous, calcaneal; surgical treatment, management; open reduction, minimally invasive, percutaneous reduction; internal fixation, external fixation. Results We identified only three randomized comparative trials. Each study compared a different technique (external fixation, percutaneous fixation with Kirchner wires and cannulated screws fixation) to the open reduction with internal fixation using plate and screws (considered the standard technique). Conclusion Comparing the series, percutaneous fixation using Kirschner wires presented the best results, however, evidence is insufficient to assert superiority of this treatment in comparison with other surgical techniques. PMID:24453579

  13. Biomechanical Assessment of Stabilization of Simulated Type II Odontoid Fracture with Case Study

    PubMed Central

    Daniel, Roy T.; Klocke, Noelle; Yandamuri, Soumya S.; Bobinski, Lukas; Duff, John M.; Bucklen, Brandon S.

    2017-01-01

    Study Design Researchers created a proper type II dens fracture (DF) and quantified a novel current posterior fixation technique with spacers at C1–C2. A clinical case study supplements this biomechanical analysis. Purpose Researchers explored their hypothesis that spacers combined with posterior instrumentation (PI) reduce range of motion significantly, possibly leading to better fusion outcomes. Overview of Literature Literature shows that the atlantoaxial joint is unique in allowing segmental rotary motion, enabling head turning. With no intervertebral discs at these joints, multiple ligaments bind the axis to the skull base and to the atlas; an intact odontoid (dens) enhances stability. The most common traumatic injury at these strong ligaments is a type II odontoid fracture. Methods Each of seven specimens (C0–C3) was tested on a custom-built six-degrees-of-freedom spine simulator with constructs of intact state, type II DF, C1–C2 PI, PI with joint capsulotomy (PIJC), PI with spacers (PIS) at C1–C2, and spacers alone (SA). A bending moment of 2.0 Nm (1.5°/sec) was applied in flexion-extension (FE), lateral bending (LB), and axial rotation (AR). One-way analysis of variance with repeated measures was performed. Results DF increased motion to 320%, 429%, and 120% versus intact (FE, LB, and AR, respectively). PI significantly reduced motion to 41%, 21%, and 8%. PIJC showed negligible changes from PI. PIS reduced motion to 16%, 14%, and 3%. SA decreased motion to 64%, 24%, and 54%. Reduced motion facilitated solid fusion in an 89-year-old female patient within 1 year. Conclusions Type II odontoid fractures can lead to acute or chronic instability. Current fixation techniques use C1–C2 PI or an anterior dens screw. Addition of spacers alongside PI led to increased biomechanical rigidity over intact motion and may offer an alternative to established surgical fixation techniques. PMID:28243364

  14. Comparison of Intralaminar and Interlaminar Mode-I Fracture Toughness of Unidirectional IM7/8552 Graphite/Epoxy Composite

    NASA Technical Reports Server (NTRS)

    Czabaj, Michael W.; Ratcliffe, James

    2012-01-01

    The intralaminar and interlaminar mode-I fracture-toughness of a unidirectional IM7/8552 graphite/epoxy composite were measured using compact tension (CT) and double cantilever beam (DCB) test specimens, respectively. Two starter crack geometries were considered for both the CT and DCB specimen configurations. In the first case, starter cracks were produced by 12.5 micron thick, Teflon film inserts. In the second case, considerably sharper starter cracks were produced by fatigue precracking. For each specimen configuration, use of the Teflon film starter cracks resulted in initially unstable crack growth and artificially high initiation fracture-toughness values. Conversely, specimens with fatigue precracks exhibited stable growth onset and lower initiation fracture toughness. For CT and DCB specimens with fatigue precracks, the intralaminar and interlaminar initiation fracture toughnesses were approximately equal. However, during propagation, the CT specimens exhibited more extensive fiber bridging, and rapidly increasing R-curve behavior as compared to the DCB specimens. Observations of initiation and propagation of intralaminar and interlaminar fracture, and the measurements of fracture toughness, were supported by fractographic analysis using scanning electron microscopy.

  15. Nonsurgical treatment of Mason type II radial head fractures in athletes. A retrospective study

    PubMed Central

    GUZZINI, M.; VADALÀ, A.; AGRÒ, A.; DI SANZO, V.; PIRONI, D.; REDLER, A.; SERLORENZI, P.; PROIETTI, L.; CIVITENGA, C.; MAZZA, D.; LANZETTI, R.M.; FERRETTI, A.

    2016-01-01

    Objective The best treatment for moderately displaced radial head fractures (Mason type II) still remains controversial. In cases of isolated fractures, there is no evidence that a fragment displacement of ≥ 2 mm gives poor results in conservatively treated fractures. Patients and methods We retrospectively reviewed 52 patients (31M, 21F) affected by an isolated Mason type II fracture, treated with a long arm cast for two weeks between 2008 and 2013. All patients had practiced sports before being injured. They were all either bicyclists, or baseball, boxers, basketball, rugby, tennis or football players. The mean follow-up was 36 months. Elbow and forearm range of motion were measured. The Mayo Elbow Performance Score, the Broberg and Morrey rating system and the Disabilities of the Arm, Shoulder and Hand Score (DASH score) were analyzed. Follow-up radiographs were examined for evidence of consolidation, late displacement, early arthritis and non-unions. Results Flexion was slightly impaired in the injured limb when compared to the uninjured limb (137°± 6° versus 139°±5°) as were extension (–3°±6° versus 1°±4°, p < 0.05), supination (86°±6° versus 88°±3°), pronation (87°±4° versus 88°±6°) and valgus deviation (10°±4° versus 8°±3°, p < 0.05). 40 patients had no elbow complaints; 9 patients experienced occasional pain, 2 a mild instability of the elbow, and 4 a mild loss of grip strength. The DASH score was excellent in 48 patients (92.31%). In only 6 cases (11.53%) degenerative changes were greater in formerly injured elbows than in uninjured elbows. All patients returned to their previous sports activities. Conclusions Isolated Mason type II fractures can have a good or excellent mid-term functional outcome even when treated conservatively. PMID:28098055

  16. Interlaminar fracture toughness: Three-dimensional finite element modeling for end-notch and mixed-mode flexure

    NASA Technical Reports Server (NTRS)

    Murthy, P. L. N.; Chamis, C. C.

    1985-01-01

    A computational procedure is described for evaluating End-Notch-Flexure (ENF) and Mixed-Mode-Flexure (MMF) interlaminar fracture toughness in unidirectional fiber composites. The procedure consists of a three-dimensional finite element analysis in conjunction with the strain energy release rate concept and with composite micromechanics. The procedure is used to analyze select cases of ENF and MMF. The strain energy release rate predicted by this procedure is in good agreement with limited experimental data. The procedure is used to identify significant parameters associated with interlaminar fracture toughness. It is also used to determine the critical strain energy release rate and its attendant crack length in ENF and/or MMF. This computational procedure has considerable versatility/generality and provides extensive information about interlaminar fracture toughness in fiber composites.

  17. An Acoustic Plate Mode Sensor for Biowarfare Toxins, Phase II

    DTIC Science & Technology

    1997-10-01

    Biological agents -- such as bacteria , bacterial toxins and viruses -- must be detected rapidly to allow their neutralization or the quick treatment of...Mode Sensor for Biowarfare Toxins PRINCIPAL INVESTIGATOR: Douglas J. McAllister, Ph.D. CONTRACTING ORGANIZATION: Biode, Incorporated Bangor, Maine...OF PAGES Acoustic Plate Mode, Biowarfare Toxins 54 16. PRICE CODE 17. SECURITY CLASSIFICATION 18. SECURITY CLASSIFICATION 19. SECURITY CLASSIFICATION

  18. Effets de l'humidite sur la propagation du delaminage dans un composite carbone/epoxy sollicite en mode mixte I/II

    NASA Astrophysics Data System (ADS)

    LeBlanc, Luc R.

    In industries such as aerospace, motorsports, and even sporting equipment, composite materials are used more than ever, primarily due to their high stiffness and strength to weight ratios. Studies have shown that moisture exposure on carbon/epoxy composite materials can affect their delamination toughness, initiation and growth rate. Of these studies, only a few demonstrated the effects of moisture on delamination toughness and initiation with mixed mode I/II loadings, while none have investigated the effects of moisture exposure of composites on delamination growth rate with mixed mode I/II loadings. The first part of this thesis studies the effects of moisture exposure on delamination growth in a carbon/epoxy composite using mixed mode I/II loadings. Coupons were cut from plates of unidirectional carbon/epoxy (040-800/5276-1) and were submerged in a 70°C distilled water bath until they reached saturation. Quasi -static experimental tests were performed using a range of mode mixities (0%, 25%, 50%, 75% and 1 00%) on dry and conditioned coupons to determine the effects of humidity on delamination toughness. Fatigue tests with the same mode mixities were performed to determine the effects of moisture on delamination initiation and growth rate. Results from tests with quasi-static loadings demonstrated that delamination toughness decreased for all loading modes studied except for mode I after composites are exposed to moisture. When a conditioned composite is subject to mode I loadings, its delamination toughness increases compared to non-conditioned composites. Composites exposed to moisture showed accelerated delamination initiation and growth rates for all mixed mode I/II fatigue loadings. Experimental data was used to determine which fracture criterion and growth rate model for mixed mode I/II delamination better represented the studied composite. A regression curve and regression surface was used to fit the experimental data to the delamination fracture

  19. Influence of injection mode on transport properties in kilometer-scale three-dimensional discrete fracture networks

    DOE PAGES

    Hyman, Jeffrey De'Haven; Painter, S. L.; Viswanathan, H.; ...

    2015-09-12

    We investigate how the choice of injection mode impacts transport properties in kilometer-scale three-dimensional discrete fracture networks (DFN). The choice of injection mode, resident and flux-weighted, is designed to mimic different physical phenomena. It has been hypothesized that solute plumes injected under resident conditions evolve to behave similarly to solutes injected under flux-weighted conditions. Previously, computational limitations have prohibited the large-scale simulations required to investigate this hypothesis. We investigate this hypothesis by using a high-performance DFN suite, dfnWorks, to simulate flow in kilometer-scale three-dimensional DFNs based on fractured granite at the Forsmark site in Sweden, and adopt a Lagrangian approachmore » to simulate transport therein. Results show that after traveling through a pre-equilibrium region, both injection methods exhibit linear scaling of the first moment of travel time and power law scaling of the breakthrough curve with similar exponents, slightly larger than 2. Lastly, the physical mechanisms behind this evolution appear to be the combination of in-network channeling of mass into larger fractures, which offer reduced resistance to flow, and in-fracture channeling, which results from the topology of the DFN.« less

  20. Influence of injection mode on transport properties in kilometer-scale three-dimensional discrete fracture networks

    SciTech Connect

    Hyman, Jeffrey De'Haven; Painter, S. L.; Viswanathan, H.; Makedonska, N.; Karra, S.

    2015-09-12

    We investigate how the choice of injection mode impacts transport properties in kilometer-scale three-dimensional discrete fracture networks (DFN). The choice of injection mode, resident and flux-weighted, is designed to mimic different physical phenomena. It has been hypothesized that solute plumes injected under resident conditions evolve to behave similarly to solutes injected under flux-weighted conditions. Previously, computational limitations have prohibited the large-scale simulations required to investigate this hypothesis. We investigate this hypothesis by using a high-performance DFN suite, dfnWorks, to simulate flow in kilometer-scale three-dimensional DFNs based on fractured granite at the Forsmark site in Sweden, and adopt a Lagrangian approach to simulate transport therein. Results show that after traveling through a pre-equilibrium region, both injection methods exhibit linear scaling of the first moment of travel time and power law scaling of the breakthrough curve with similar exponents, slightly larger than 2. Lastly, the physical mechanisms behind this evolution appear to be the combination of in-network channeling of mass into larger fractures, which offer reduced resistance to flow, and in-fracture channeling, which results from the topology of the DFN.

  1. Correlation of Fracture Mode Transition of Ceramic Particle with Critical Velocity for Successful Deposition in Vacuum Kinetic Spraying Process

    NASA Astrophysics Data System (ADS)

    Park, Hyungkwon; Kim, Jinyoung; Lee, Sung Bo; Lee, Changhee

    2017-02-01

    Vacuum kinetic spraying (VKS) is a promising room-temperature process to fabricate dense ceramic films. However, unfortunately, the deposition mechanism is still not clearly understood. In this respect, the critical conditions for successful deposition were investigated. Based on simulation and microstructural analysis, it was found that as the particle velocity increased, fracture mode transition from tensile fracture to shear fracture occurred and particle did not bounce off anymore above a certain velocity. Simultaneously, particle underwent shock-induced plasticity and dynamic fragmentation. The plasticity assisted to prevent the fragments from rebounding by spending the excessive kinetic energy and fragmentation is essential for fragment bonding and film growth considering that the deposition rate increased as the fraction of fragmentation increased. Accordingly, plasticity and fragmentation take a crucial role for particle deposition. In this respect, the velocity that fracture mode transition occurs is newly defined as critical velocity. Consequently, for successful deposition, the particle should at least exceed the critical velocity and thus it is very crucial for film fabrication in VKS process at room temperature.

  2. Correlation of Fracture Mode Transition of Ceramic Particle with Critical Velocity for Successful Deposition in Vacuum Kinetic Spraying Process

    NASA Astrophysics Data System (ADS)

    Park, Hyungkwon; Kim, Jinyoung; Lee, Sung Bo; Lee, Changhee

    2016-12-01

    Vacuum kinetic spraying (VKS) is a promising room-temperature process to fabricate dense ceramic films. However, unfortunately, the deposition mechanism is still not clearly understood. In this respect, the critical conditions for successful deposition were investigated. Based on simulation and microstructural analysis, it was found that as the particle velocity increased, fracture mode transition from tensile fracture to shear fracture occurred and particle did not bounce off anymore above a certain velocity. Simultaneously, particle underwent shock-induced plasticity and dynamic fragmentation. The plasticity assisted to prevent the fragments from rebounding by spending the excessive kinetic energy and fragmentation is essential for fragment bonding and film growth considering that the deposition rate increased as the fraction of fragmentation increased. Accordingly, plasticity and fragmentation take a crucial role for particle deposition. In this respect, the velocity that fracture mode transition occurs is newly defined as critical velocity. Consequently, for successful deposition, the particle should at least exceed the critical velocity and thus it is very crucial for film fabrication in VKS process at room temperature.

  3. Shear Fracture of Dual Phase AHSS in the Process of Stamping: Macroscopic Failure Mode and Micro-level Metallographical Observation

    NASA Astrophysics Data System (ADS)

    Wang, Wurong; Wei, Xicheng; Yang, Jun; Shi, Gang

    2011-08-01

    Due to its excellent strength and formability combinations, dual phase (DP) steels offer the potential to improve the vehicle crashworthiness performance without increasing car body weight and have been increasingly used into new vehicles. However, a new type of crack mode termed as shear fracture is accompanied with the application of these high strength DP steel sheets. With the cup drawing experiment to identify the limit drawing ratio (LDR) of three DP AHSS with strength level from 600 MPa to 1000 MPa, the study compared and categorized the macroscopic failure mode of these three types of materials. The metallographical observation along the direction of crack was conducted for the DP steels to discover the micro-level propagation mechanism of the fracture.

  4. Magnetic antenna excitation of whistler modes. II. Antenna arrays

    SciTech Connect

    Stenzel, R. L.; Urrutia, J. M.

    2014-12-15

    The excitation of whistler modes from magnetic loop antennas has been investigated experimentally. The field topology of the excited wave driven by a single loop antenna has been measured for different loop orientations with respect to the uniform background field. The fields from two or more antennas at different locations are then created by superposition of the single-loop data. It is shown that an antenna array can produce nearly plane waves which cannot be achieved with single antennas. By applying a phase shift along the array, oblique wave propagation is obtained. This allows a meaningful comparison with plane wave theory. The Gendrin mode and oblique cyclotron resonance are demonstrated. Wave helicity and polarization in space and time are demonstrated and distinguished from the magnetic helicity of the wave field. The superposition of two oblique plane whistler modes produces in a “whistler waveguide” mode whose polarization and helicity properties are explained. The results show that single point measurements cannot properly establish the wave character of wave packets. The laboratory observations are relevant for excitation and detection of whistler modes in space plasmas.

  5. Magnetic antenna excitation of whistler modes. II. Antenna arrays

    NASA Astrophysics Data System (ADS)

    Stenzel, R. L.; Urrutia, J. M.

    2014-12-01

    The excitation of whistler modes from magnetic loop antennas has been investigated experimentally. The field topology of the excited wave driven by a single loop antenna has been measured for different loop orientations with respect to the uniform background field. The fields from two or more antennas at different locations are then created by superposition of the single-loop data. It is shown that an antenna array can produce nearly plane waves which cannot be achieved with single antennas. By applying a phase shift along the array, oblique wave propagation is obtained. This allows a meaningful comparison with plane wave theory. The Gendrin mode and oblique cyclotron resonance are demonstrated. Wave helicity and polarization in space and time are demonstrated and distinguished from the magnetic helicity of the wave field. The superposition of two oblique plane whistler modes produces in a "whistler waveguide" mode whose polarization and helicity properties are explained. The results show that single point measurements cannot properly establish the wave character of wave packets. The laboratory observations are relevant for excitation and detection of whistler modes in space plasmas.

  6. Resistive wall modes in the Reversatron II RFP

    SciTech Connect

    Barrick, G.; Greene, P.; Robertson, S.

    1990-01-01

    The Reversatron 2 RFP (R/a=50cm/8cm) has been operated with interchangeable shells to investigate resistive wall modes. Shell penetration times are 610, 100, and 4 {mu}sec (no shell). With the 610 {mu}sec shell, the plasma current is {le} 65 kA and the duration {le} 550 {mu}sec. With no shell, helium discharges are more resistive and hydrogen discharges cannot be sustained. An m=1, n=-6 mode resonant on axis grows to a relative amplitude of 20% during the setting-up phase. With the 100{mu}sec shell, deuterium discharges can be sustained but are degraded due to a broad spectrum of modes. The increased plasma resistance can be correlated with the flux intersecting the wall. 21 refs., 12 figs.

  7. Development of fracture facets from a crack loaded in mode I+III: Solution and application of a model 2D problem

    NASA Astrophysics Data System (ADS)

    Leblond, Jean-Baptiste; Frelat, Joël

    2014-03-01

    It is experimentally well-known that a crack loaded in mode I+III propagates through formation of discrete fracture facets inclined at a certain tilt angle on the original crack plane, depending on the ratio of the mode III to mode I initial stress intensity factors. Pollard et al. (1982) have proposed to calculate this angle by considering the tractions on all possible future infinitesimal facets and assuming shear tractions to be zero on that which will actually develop. In this paper we consider the opposite case of well-developed facets; the stress field near the lateral fronts of such facets becomes independent of the initial crack and essentially 2D in a plane perpendicular to the main direction of crack propagation. To determine this stress field, we solve the model 2D problem of an infinite plate containing an infinite periodic array of cracks inclined at some angle on a straight line, and loaded through uniform stresses at infinity. This is done first analytically, for small values of this angle, by combining Muskhelishvili's (1953) formalism and a first-order perturbation procedure. The formulae found for the 2D stress intensity factors are then extended in an approximate way to larger angles by using another reference solution, and finally assessed through comparison with some finite element results. To finally illustrate the possible future application of these formulae to the prediction of the stationary tilt angle, we introduce the tentative assumption that the 2D mode II stress intensity factor is zero on the lateral fronts of the facets. An approximate formula providing the tilt angle as a function of the ratio of the mode III to mode I stress intensity factors of the initial crack is deduced from there. This formula, which slightly depends on the type of loading imposed, predicts somewhat smaller angles than that of Pollard et al. (1982).

  8. Vibrational relaxation pathways of amide I and amide II modes in N-methylacetamide.

    PubMed

    Piatkowski, L; Bakker, H J

    2012-04-28

    We studied the vibrational energy relaxation mechanisms of the amide I and amide II modes of N-methylacetamide (NMA) monomers dissolved in bromoform using polarization-resolved femtosecond two-color vibrational spectroscopy. The results show that the excited amide I vibration transfers its excitation energy to the amide II vibration with a time constant of 8.3 ± 1 ps. In addition to this energy exchange process, we observe that the excited amide I and amide II vibrations both relax to a final thermal state. For the amide I mode this latter process dominates the vibrational relaxation of this mode. We find that the vibrational relaxation of the amide I mode depends on frequency which can be well explained from the presence of two subbands with different vibrational lifetimes (~1.1 ps on the low frequency side and ~2.7 ps on the high frequency side) in the amide I absorption spectrum.

  9. Effect of loading mode on the fracture toughness of a reduced activation ferritic/martensitic stainless steel

    SciTech Connect

    Li, H.; Hirth, J.P.; Jones, R.H.; Gelles, D.S.

    1993-09-01

    The critical J integrals of mode I (J{sub IC}), mixed-mode I/III (J{sub MC}), and mode III (J{sub IIIC}) were examined for a ferritic stainless steel (F-82H) at ambient temperature. A determination of J{sub MC} was made using modified compact-tension specimens. Different ratios of tension/shear stress were achieved by varying the principal axis of the crack plane between 0 and 55 degrees from the load line. The results showed that J{sub MC}s and tearing moduli (T{sub M}) varied with the crack angles and were lower than their mode I and mode III counterparts. Both the minimum J{sub MC} and T{sub M} occurred at a crack angle between 40 and 50 degrees, where {sigma}{sub i}/{sigma}{sub iii} was 1.2 to 0.84. The J{sub min} was 240 kJ/m{sup 2}, and ratios of J{sub IC}/J{sub min} and J{sub IIIC}/J{sub min} were about 2.1 and 1.9, respectively. Morphology of fracture surfaces was consistent with the change of J{sub MC} and T{sub M} values. While the upper shelf-fracture toughness of F-82H depends on loading mode, the J{sub min} remains very high. Other important considerations include the effect of mixed-mode loading on the DBT temperature, and effects of hydrogen and irradiation on J{sub min}.

  10. Physeal fractures of the distal tibia and fibula (Salter-Harris Type I, II, III, and IV fractures).

    PubMed

    Podeszwa, David A; Mubarak, Scott J

    2012-06-01

    Physeal fractures of the distal tibia and fibula are common and can be seen at any age, although most are seen in the adolescent. An understanding of the unique anatomy of the skeletally immature ankle in relation to the mechanism of injury will help one understand the injury patterns seen in this population. A thorough clinical exam is critical to the diagnosis and treatment of these injuries and the avoidance of potentially catastrophic complications. Nondisplaced physeal fractures of the distal tibia and fibula can be safely treated nonoperatively. Displaced fractures should undergo a gentle reduction with appropriate anesthesia while multiple reduction attempts should be avoided. Gapping of the physis >3 mm after reduction should raise the suspicion of entrapped periosteum that will increase the risk of premature physeal closure. Open reduction of displaced Salter-Harris type III and IV fractures is critical to maintain joint congruity and minimize the risk of physeal arrest.

  11. Atomistic study on mixed-mode fracture mechanisms of ferrite iron interacting with coherent copper and nickel nanoclusters

    NASA Astrophysics Data System (ADS)

    Al-Motasem, Ahmed Tamer; Mai, Nghia Trong; Choi, Seung Tae; Posselt, Matthias

    2016-04-01

    The effect of copper and/or nickel nanoclusters, generally formed by neutron irradiation, on fracture mechanisms of ferrite iron was investigated by using molecular statics simulation. The equilibrium configuration of nanoclusters was obtained by using a combination of an on-lattice annealing based on Metropolis Monte Carlo method and an off-lattice relaxation by molecular dynamics simulation. Residual stress distributions near the nanoclusters were also calculated, since compressive or tensile residual stresses may retard or accelerate, respectively, the propagation of a crack running into a nanocluster. One of the nanoclusters was located in front of a straight crack in ferrite iron with a body-centered cubic crystal structure. Two crystallographic directions, of which the crack plane and crack front direction are (010)[001] and (111) [ 1 bar 10 ] , were considered, representing cleavage and non-cleavage orientations in ferrite iron, respectively. Displacements corresponding to pure opening-mode and mixed-mode loadings were imposed on the boundary region and the energy minimization was performed. It was observed that the fracture mechanisms of ferrite iron under the pure opening-mode loading are strongly influenced by the presence of nanoclusters, while under the mixed-mode loading the nanoclusters have no significant effect on the crack propagation behavior of ferrite iron.

  12. Mode I and Mode II Interlaminar Crack Growth Resistances of Ceramic Matrix Composites at Ambient Temperature

    DTIC Science & Technology

    2007-03-02

    Sci. Proc., 25[4] 71-78 (2004). 9. L. P. Zawada , “Longitudinal and Transthickness Tensile Behavior of Several Oxide/Oxide Composites,” Ceram. Eng...Unidirectional C-C Composite,” J. Nucl. Mater., 230 226-232 (1996). 11. S. Mall, R. P. Vozzola, and L. Zawada , “Characterization of Fracture in Fiber...Behavior of a Unidirectional C-C Composite,” J. Nucl. Mater., 230 226-232 (1996). 34. L. P. Zawada , “Longitudinal and Transthickness Tensile Behavior

  13. Failure modes and fracture origins of porcelain veneers on bilayer dental crowns.

    PubMed

    Liu, Yihong; Liu, Guanghua; Wang, Yong; Shen, James Zhijian; Feng, Hailan

    2014-01-01

    The aims of this study were to determine the fracture origins and crack paths in the porcelain of clinically failed bilayer ceramic restorations and to reveal the correlation between the porcelain failures and material properties. Three clinically failed crowns of each material (bilayer zirconia crowns, galvano-ceramic crowns, and porcelain-fused-to-metal crowns) were collected and underwent failure analysis. The fractures found in porcelain veneers showed several characteristics including wear, Hertzian cone crack, chipping off, and delamination. The results indicated that the fracture origins and features of the porcelain in bilayer ceramic restorations might be affected by the rigidity of core materials and thickness of copings.

  14. Salter-Harris type II fracture of the femoral bone in a 14-year-old boy – case report

    PubMed Central

    Kuleta-Bosak, Elżbieta; Bożek, Paweł; Kluczewska, Ewa; Tomaszewski, Ryszard; Machnik-Broncel, Joanna

    2010-01-01

    Summary Background: Distal femoral physis fractures with displacement are rare injuries seen in adolescents related with high incidence of complication. They may lead to premature physeal closure consequently, to growth arrest and bone deformity. Case Report: The case of a 14-year-old boy with Salter-Harris type II displaced fracture underwent surgery with open reduction has been described. CT examination with multiplanar reconstruction was used in pre-operative assessment of distal femur growth plate fracture. Conclusions: Knowledge of classification, prognosis and methods of treatment is necessary in accurate pre- and postoperative assessment of physial fractures in adolescents. CT and multiplanar reconstruction improve the understanding of patterns of injury, relative prevalence and accuracy of pre-operative planning. PMID:22802768

  15. The effects of glass ionomer and flowable composite liners on the fracture resistance of open-sandwich class II restorations.

    PubMed

    Güray Efes, Begüm; Yaman, Batu Can; Gümüştaş, Burak; Tıryakı, Murat

    2013-01-01

    This in vitro study aimed to investigate the effects of glass-ionomer and flowable composite liners on the fracture resistance of Class II amalgam and composite restorations. Group 1 cavities were restored with amalgam and Group 4 cavities with nanofill composite after the application of a dentin-bonding agent. For the remaining groups, light-cured-glass-ionomer liner was used in a gingival floor proximal box (Groups 2, 5) or flowable composite was used as a liner (Groups 3, 6), the remainder of the cavity was restored with amalgam (Groups 2, 3) or composite (Groups 5, 6). The restorations were loaded in compression to failure. The data was analyzed using Tukey's multiple comparison test. The fracture resistance was significantly higher (p<0.05) in Group 3 than in all other groups, except Group 2 (p>0.05). Flowable composite, glass-ionomer liners increased the fracture resistance of open-sandwich Class II amalgam restorations.

  16. EFFECT OF RADIUS OF LOADING NOSE AND SUPPORTS IN SHORT BEAM TEST FIXTURE ON FRACTURE MODE AND INTERLAMINAR SHEAR STRENGTH OF GFRP AT 77 K

    SciTech Connect

    Nishimura, A.

    2008-03-03

    A short beam test is useful to evaluate interlaminar shear strength of glass fiber reinforced plastics, especially for material selection. However, effect of test fixture configuration on interlaminar shear strength has not been clarified. This paper describes dependence of fracture mode and interlaminar shear strength on the fixture radius using the same materials and procedure. In addition, global understanding of the role of the fixture is discussed. When small loading nose and supports are used for the tests, bending fracture or translaminar fracture happens and the interlaminar shear strength would become smaller. By adopting the large radius loading nose and supports (6 mm radius is recommended), it is newly recognized that some stress concentration is able to be reduced, and the interlaminar fracture tends to occur and the other fracture modes will be suppressed. The interlaminar shear strength of 2.5 mm thick GFRP plate of G-10CR is evaluated as 130-150 MPa at 77 K.

  17. A Computational and Experimental Investigation of Mode 1 Fracture in an Elastomer

    DTIC Science & Technology

    1990-09-01

    Fu.kahori, Y. and Andrews. E. H.. Fracture surface roughness in highly deformable polymers . J. Mat. Sct. 13 (1978) 777 .......... 178 3.31 Proposed tearing... polymers , consisting of long flexible chainlike molecules, intercon- nected by crossbonds, a phenomenon referred to as crosslinking. Their mechanical...failure of metals [1] and certain ductile polymers [2] has been documented, suggesting that thickness may also influence fracture in elas- tomers. This

  18. Cooperative binding modes of Cu(II) in prion protein

    NASA Astrophysics Data System (ADS)

    Hodak, Miroslav; Chisnell, Robin; Lu, Wenchang; Bernholc, Jerry

    2007-03-01

    The misfolding of the prion protein, PrP, is responsible for a group of neurodegenerative diseases including mad cow disease and Creutzfeldt-Jakob disease. It is known that the PrP can efficiently bind copper ions; four high-affinity binding sites located in the octarepeat region of PrP are now well known. Recent experiments suggest that at low copper concentrations new binding modes, in which one copper ion is shared between two or more binding sites, are possible. Using our hybrid Thomas-Fermi/DFT computational scheme, which is well suited for simulations of biomolecules in solution, we investigate the geometries and energetics of two, three and four binding sites cooperatively binding one copper ion. These geometries are then used as inputs for classical molecular dynamics simulations. We find that copper binding affects the secondary structure of the PrP and that it stabilizes the unstructured (unfolded) part of the protein.

  19. Facial fractures.

    PubMed Central

    Carr, M. M.; Freiberg, A.; Martin, R. D.

    1994-01-01

    Emergency room physicians frequently see facial fractures that can have serious consequences for patients if mismanaged. This article reviews the signs, symptoms, imaging techniques, and general modes of treatment of common facial fractures. It focuses on fractures of the mandible, zygomaticomaxillary region, orbital floor, and nose. Images p520-a p522-a PMID:8199509

  20. Pulsatile Support Mode of BJUT-II Ventricular Assist Device (VAD) has Better Hemodynamic Effects on the Aorta than Constant Speed Mode: A Primary Numerical Study

    PubMed Central

    Gu, Kaiyun; Gao, Bin; Chang, Yu; Zeng, Yi

    2016-01-01

    Background BJUT-II VAD is a novel left ventricular assist device (LVADs), directly implanted into the ascending aorta. The pulsatile support mode is proposed to achieve better unloading performance than constant speed mode. However, the hemodynamic effects of this support mode on the aorta are still unclear. The aim of this study was to clarify the hemodynamic effects BJUT-II VAD under pulsatile support mode on the aorta. Material/Methods Computational fluid dynamics (CFD) studies, based on a patient-specific aortic geometric model, were conducted. Wall shear stress (WSS), averaged WSS (avWSS), oscillatory shear index (OSI), and averaged helicity density (Ha) were calculated to compare the differences in hemodynamic effects between pulsatile support mode and constant speed mode. Results The results show that avWSS under pulsatile support mode is significantly higher than that under constant speed mode (0.955Pa vs. 0.675Pa). Similarly, the OSI value under pulsatile mode is higher than that under constant speed mode (0.104 vs. 0.057). In addition, Ha under pulsatile mode for all selected cross-sections is larger than that under constant mode. Conclusions BJUT-II VAD, under pulsatile control mode, may prevent atherosclerosis lesions and aortic remodeling. The precise effects of pulsatile support mode on atherosclerosis and aortic remodeling need to be further studied in animal experiments. PMID:27363758

  1. Pulsatile Support Mode of BJUT-II Ventricular Assist Device (VAD) has Better Hemodynamic Effects on the Aorta than Constant Speed Mode: A Primary Numerical Study.

    PubMed

    Gu, Kaiyun; Gao, Bin; Chang, Yu; Zeng, Yi

    2016-07-01

    BACKGROUND BJUT-II VAD is a novel left ventricular assist device (LVADs), directly implanted into the ascending aorta. The pulsatile support mode is proposed to achieve better unloading performance than constant speed mode. However, the hemodynamic effects of this support mode on the aorta are still unclear. The aim of this study was to clarify the hemodynamic effects BJUT-II VAD under pulsatile support mode on the aorta. MATERIAL AND METHODS Computational fluid dynamics (CFD) studies, based on a patient-specific aortic geometric model, were conducted. Wall shear stress (WSS), averaged WSS (avWSS), oscillatory shear index (OSI), and averaged helicity density (Ha) were calculated to compare the differences in hemodynamic effects between pulsatile support mode and constant speed mode. RESULTS The results show that avWSS under pulsatile support mode is significantly higher than that under constant speed mode (0.955Pa vs. 0.675Pa). Similarly, the OSI value under pulsatile mode is higher than that under constant speed mode (0.104 vs. 0.057). In addition, Ha under pulsatile mode for all selected cross-sections is larger than that under constant mode. CONCLUSIONS BJUT-II VAD, under pulsatile control mode, may prevent atherosclerosis lesions and aortic remodeling. The precise effects of pulsatile support mode on atherosclerosis and aortic remodeling need to be further studied in animal experiments.

  2. Acoustic mode driven by fast electrons in TJ-II Electron Cyclotron Resonance plasmas

    NASA Astrophysics Data System (ADS)

    Sun, B. J.; Ochando, M. A.; López-Bruna, D.

    2016-08-01

    Intense harmonic oscillations in radiation signals (δ I/I∼ 5{%}) are commonly observed during Electron Cyclotron Resonance (ECR) heating in TJ-II stellarator plasmas at low line-averaged electron density, 0.15 < \\bar{n}e < 0.6 ×1019 \\text{m}-3 . The frequency agrees with acoustic modes. The poloidal modal structure is compatible with Geodesic Acoustic Modes (GAM) but an n \

  3. Characterization of Mode I and Mode II delamination growth and thresholds in AS4/PEEK composites

    NASA Technical Reports Server (NTRS)

    Martin, Roderick H.; Murri, Gretchen Bostaph

    1990-01-01

    Composite materials often fail by delamination. The onset and growth of delamination in AS4/PEEK, a tough thermoplastic matrix composite, was characterized for mode 1 and mode 2 loadings, using the Double Cantilever Beam (DCB) and the End Notched Flexure (ENF) test specimens. Delamination growth per fatigue cycle, da/dN, was related to strain energy release rate, G, by means of a power law. However, the exponents of these power laws were too large for them to be adequately used as a life prediction tool. A small error in the estimated applied loads could lead to large errors in the delamination growth rates. Hence strain energy release rate thresholds, G sub th, below which no delamination would occur were also measured. Mode 1 and 2 threshold G values for no delamination growth were found by monitoring the number of cycles to delamination onset in the DCB and ENF specimens. The maximum applied G for which no delamination growth had occurred until at least 1,000,000 cycles was considered the threshold strain energy release rate. Comments are given on how testing effects, facial interference or delamination front damage, may invalidate the experimental determination of the constants in the expression.

  4. Fracture modes in tubular LSFCO ceramic membranes under graded reducing conditions

    SciTech Connect

    Nagendra, N.; Biswas, S.; Nithyanantham, T.; Bandopadhyay, S.

    2013-06-01

    Highlights: ► Microstructural evolution in LSFCO membranes under graded environment is reported. ► The role of chemically induced stresses and oxygen deficiency is evaluated. ► The stress distribution is modeled by a point defect model. - Abstract: Chromium (III) oxide (Cr{sub 2}O{sub 3})-doped LaSrFeO{sub 3} perovskite, La{sub 0.2}Sr{sub 0.8}Fe{sub 0.8}Cr{sub 0.2}O{sub 3−δ} (LSFCO), is being considered as a potential material for applications in solid oxide fuel cells, gas separation membranes, and electrochemical reactors because of its high electro-catalytic activity. Similar to other perovskites, the performance and mechanical strength of LSFCO materials are significantly affected by environment and temperature. Here, we report a fracture gradient phenomenon in tubular C-ring-shaped LSFCO ceramic membranes under graded reducing conditions. The graded reducing condition was produced by flushing N{sub 2} on the outer side of the C-ring membranes at 1000 °C while keeping the inner side untreated. The rings were then diametrically compressed to fracture, and the resultant fracture morphology was analyzed with a scanning electron microscope (SEM). A fracture gradient with three distinct regions across the thickness of the membranes was identified on the split surfaces. In the outer region of the C-ring specimen exposed to N{sub 2}, a mixed inter/transgranular fracture with a predominant intergranular pattern was observed. In the middle section of the fracture surface, a characteristic transgranular fracture of the perovskite grains was found. At the inner region of the ring, a mixed inter/transgranular fracture with a predominant transgranular pattern occurred. The mechanism of gradient fractures was attributed both to chemically induced stresses caused by oxygen diffusion and to the formation of a separate phase of oxygen-deficient perovskite in the parent perovskite. The stresses generated were modeled by a point defect model. This work provides

  5. Mode-specific vibrational energy relaxation of amide I' and II' modes in N-methylacetamide/water clusters: intra- and intermolecular energy transfer mechanisms.

    PubMed

    Zhang, Yong; Fujisaki, Hiroshi; Straub, John E

    2009-04-02

    The mode-specific vibrational energy relaxation of the amide I' and amide II' modes in NMA-d(1)/(D(2)O)(n) (n = 0-3) clusters were studied using the time-dependent perturbation theory at the B3LYP/aug-cc-pvdz level. The amide modes were identified for each cluster based on the potential energy distribution of each mode. The vibrational population relaxation time constants were derived for the amide I' and II' modes. Results for the amide I' mode relaxation of NMA-d(1)/(D(2)O)(3) agree well with previous experimental results. The energy relaxation pathways were identified, and both intra- and intermolecular mechanisms were found to be important. The amide II' mode was identified in the energy transfer pathways from the excited amide I' mode of NMA-d(1)/(D(2)O)(n) (n = 1-3) clusters. The modes associated with methyl group deformation were found to play a role in the mechanism of energy transfer from both excited amide I' and II' modes. The kinetics of energy flow in the cluster were examined by solving a master equation describing the vibrational energy relaxation process from excited system mode as a multistep reaction with the third order Fermi resonance parameters as the reaction rate constants. The intramolecular energy transfer mechanism was found to dominate the short time energy flow dynamics, whereas the intermolecular mechanism was found to be dominant at longer times.

  6. A pentanuclear lead(II) complex based on a strapped porphyrin with three different coordination modes.

    PubMed

    Le Gac, Stéphane; Furet, Eric; Roisnel, Thierry; Hijazi, Ismail; Halet, Jean-François; Boitrel, Bernard

    2014-10-06

    We have previously described Pb(II) and Bi(III) bimetallic complexes with overhanging carboxylic acid strapped porphyrins in which one metal ion is bound to the N-core ("out-of-plane", OOP), whereas the second one is bound to the strap ("hanging-atop", HAT). In such complexes, the hemidirected coordination sphere of a HAT Pb(II) cation provides sufficient space for an additional binding of a neutral ligand (e.g., DMSO). Interestingly, investigations of the HAT metal coordination mode in a single strap porphyrin show that a HAT Pb(II) can also interact via intermolecular coordination bonds, allowing the self-assembly of two bimetallic complexes. In the pentanuclear Pb(II) complex we are describing in this Article, three different coordination modes were found. The OOP Pb(II) remains inert toward the supramolecular assembling process, whereas the HAT Pb(II) cation, in addition to its intramolecular carboxylate and regular exogenous acetate groups, coordinates an additional exogenous acetate. These two acetates are shared with a third lead(II) cation featuring a holo-directed coordination sphere, from which a centro-symmetric complex is assembled. Density functional theory calculations show some electron-density pockets in the vicinity of the hemidirected HAT Pb(II) atoms, which are associated with the presence of a stereochemically active lone pair of electrons. On the basis of the comparison with other HAT Pb(II) and Bi(III) systems, the "volume" of this lone pair correlates well with the bond distance distributions and the number of the proximal oxygen atoms tethered to the post-transition metal cation. It thus follows the order 6-coordinate Bi(III) > 6-coordinate Pb(II) > 5-coordinate Pb(II).

  7. Selection of stirling engine parameter and modes of joint operation with the Topaz II

    SciTech Connect

    Kirillov, E.Y.; Ogloblin, B.G.; Shalaev, A.I.

    1996-03-01

    In addition to a high-temperature thermionic conversion cycle, application of a low-temperature machine cycle, such as the Stirling engine, is being considered. To select the optimum mode for joint operation of the Topaz II system and Stirling engine, output electric parameters are obtained as a function of thermal power released in the TFE fuel cores. The hydraulic diagram used for joint operation of the Topaz II and the Stirling engine is considered. Requirements to hydraulic characteristics of the Stirling engine heat exchanges are formulated. Scope of necessary modifications to mount the Stirling Engine on the Topaz II is estimated. {copyright} {ital 1996 American Institute of Physics.}

  8. Effect of Interface Control on Mode I Interlaminar Fracture Toughness of Woven C/C Composite Laminates

    NASA Astrophysics Data System (ADS)

    Hojo, Masaki; Yamao, Taketoshi; Tanaka, Mototsugu; Ochiai, Shojiro; Iwashita, Norio; Sawada, Yoshihiro

    Effects of fiber/matrix interface and matrix microstructure on the mode I interlaminar fracture toughness of C/C composite materials were investigated by coating bismaleimide-triazine co-polymer (BT-resin) on the surface of carbon fiber and changing the heat-treatment temperature (HTT). For the case of laminates with HTT of 1600°C (carbonized C/C composites), the initial fracture toughness, GIC, was insensitive to BT-resin coating. Moreover, the fracture toughness during crack propagation, GIR, increased by coating BT-resin. On the other hand, both GIC and GIR decreased with BT-resin coating for the laminates with HTT of 2500°C. While both GIC and GIR are insensitive to HTT for laminates without BT-resin coating, they both decreased by increasing HTT for laminates with BT-resin coating. The difference of the effects of interface control and HTT was discussed on the basis of microscopic mechanism consideration. Comparison between in-plane and interlaminar strength indicated the possibility to optimize the interface control.

  9. Current concepts in the treatment of Anderson Type II odontoid fractures in the elderly in Germany, Austria and Switzerland.

    PubMed

    Löhrer, L; Raschke, M J; Thiesen, D; Hartensuer, R; Surke, C; Ochman, S; Vordemvenne, T

    2012-04-01

    Although currently there are many different recommendations and strategies in the therapy of odontoid fractures in the elderly, there are still no generally accepted guidelines for a structured and standardised treatment. Moreover, the current opinion of spine surgeons regarding the optimal treatment of odontoid fractures Type II of the elderly is unknown. In order to have an objective insight into the diverging strategies for the management of Anderson Type II odontoid fractures and form a basis for future comparisons, this study investigated the current concepts and preferences of orthopaedic, neuro- and trauma surgeons. Spine surgeons from 34 medical schools and 8 hospitals in Germany, 4 university hospitals in Austria and 5 in Switzerland were invited to participate in an online survey using a 12-item 1-sided questionnaire. A total of 44 interviewees from 34 medical institutions participated in the survey, consisting of trauma (50%), orthopaedic (20.5%) and neurosurgeons (27.3%). Out of these, 70.5% treated 1-20 fractures per year; 63.6% favoured the anterior screw fixation as therapy for Type II odontoid fractures, the open posterior Magerl transarticular C1/C2 fusion, the posterior Harms C1/C2 fusion, and conservative immobilisation by cervical orthosis was preferred by 9.1% in each case. 59.1% preferred the anterior odontoid screw fixation as an appropriate treatment of Anderson Type II odontoid fractures in the elderly. 79.5% chose cervical orthosis for postsurgical treatment. Following operative treatment, nonunion rates were reported to be <10% and <20% by 40.9% and 70% of the surgeons, respectively. 56.8% reported changing from primary conservative to secondary operative treatment in <10% of cases. The most favoured technique in revision surgery of nonunions was the open posterior Magerl transarticular fusion technique, chosen by 38.6% of respondents. 18.2% preferred the posterior Harms C1/C2 fusion technique, 11.4% the percutaneous posterior Magerl

  10. C2-fractures: part II. A morphometrical analysis of computerized atlantoaxial motion, anatomical alignment and related clinical outcomes.

    PubMed

    Koller, Heiko; Acosta, Frank; Forstner, Rosemarie; Zenner, Juliane; Resch, Herbert; Tauber, Mark; Lederer, Stefan; Auffarth, Alexander; Hitzl, Wolfgang

    2009-08-01

    Knowledge on the outcome of C2-fractures is founded on heterogenous samples with cross-sectional outcome assessment focusing on union rates, complications and technical concerns related to surgical treatment. Reproducible clinical and functional outcome assessments are scant. Validated generic and disease specific outcome measures were rarely applied. Therefore, the aim of the current study is to investigate the radiographic, functional and clinical outcome of a patient sample with C2-fractures. Out of a consecutive series of 121 patients with C2 fractures, 44 met strict inclusion criteria and 35 patients with C2-fractures treated either nonsurgically or surgically with motion-preserving techniques were surveyed. Outcome analysis included validated measures (SF-36, NPDI, CSOQ), and a functional CT-scanning protocol for the evaluation of C1-2 rotation and alignment. Mean follow-up was 64 months and mean age of patients was 52 years. Classification of C2-fractures at injury was performed using a detailed morphological description: 24 patients had odontoid fractures type II or III, 18 patients had fracture patterns involving the vertebral body and 11 included a dislocated or a burst lateral mass fracture. Thirty-one percent of patients were treated with a halo, 34% with a Philadelphia collar and 34% had anterior odontoid screw fixation. At follow-up mean atlantoaxial rotation in left and right head position was 20.2 degrees and 20.6 degrees, respectively. According to the classification system of posttreatment C2-alignment established by our group in part I of the C2-fracture study project, mean malunion score was 2.8 points. In 49% of patients the fractures healed in anatomical shape or with mild malalignment. In 51% fractures healed with moderate or severe malalignment. Self-rated outcome was excellent or good in 65% of patients and moderate or poor in 35%. The raw data of varying nuances allow for comparison in future benchmark studies and metaanalysis. Detailed

  11. The radiation swelling effect on fracture properties and fracture mechanisms of irradiated austenitic steels. Part II. Fatigue crack growth rate

    NASA Astrophysics Data System (ADS)

    Margolin, B.; Minkin, A.; Smirnov, V.; Sorokin, A.; Shvetsova, V.; Potapova, V.

    2016-11-01

    The experimental data on the fatigue crack growth rate (FCGR) have been obtained for austenitic steel of 18Cr-10Ni-Ti grade (Russian analog of AISI 321 steel) irradiated up to neutron dose of 150 dpa with various radiation swelling. The performed study of the fracture mechanisms for cracked specimens under cyclic loading has explained why radiation swelling affects weakly FCGR unlike its effect on fracture toughness. Mechanical modeling of fatigue crack growth has been carried out and the dependencies for prediction of FCGR in irradiated austenitic steel with and with no swelling are proposed and verified with the obtained experimental results. As input data for these dependencies, FCGR for unirradiated steel and the tensile mechanical properties for unirradiated and irradiated steels are used.

  12. Method for measuring the mode-I fracture toughness in lead zirconate titanate (PZT)

    NASA Astrophysics Data System (ADS)

    Karastamatis, Thomas; Lynch, Christopher S.

    2000-06-01

    Previous measurements of the fracture toughness of PZT have relied on Vicker's indentations, bend specimens, and compact tension specimens. Vicker's indentations are qualitative and are not suitable for toughness measurements. Recent work has clearly shown that non-linear material behavior induces a non-linear stress gradient through other specimen geometries that must be accounted for to accurately determine the fracture toughness. This work describes the development of a measurement technique for the R-curve behavior of unpoled ferroelastic ceramics using 4-point bend specimens with semi-elliptical surface cracks. The model material is a soft, transparent composition of 8/65/35 lead lanthanum zirconate titanate. The aspect ratio is measured during crack growth. The non-linear stress gradient through the cross section calculated from strain gage data. A parametric study based on the analysis of Newman and Raju is used to elucidate the restrictions on application of this technique.

  13. Far-field stress dependency of the failure mode of damage-zone fractures in fault zones: Results from laboratory tests and field observations of siliceous mudstone

    NASA Astrophysics Data System (ADS)

    Ishii, Eiichi

    2016-01-01

    The macroscopic failure mode (tensile/hybrid/shear) of damage-zone fractures in fault zones may influence the hydrogeological properties of the fault zone. Application of the Griffith-Coulomb failure criterion, combined with the simple assumption that failures are predominantly induced by an increase in differential stresses and/or a decrease in effective normal stresses resulting from stress concentrations generated at the asperities/tips of faults, suggests that (1) only tensile fractures propagate from faults when the effective mean stress is less than the rock tensile strength, (2) tensile/hybrid fractures form when the effective mean stress is less than twice the rock tensile strength, and (3) shear fractures can develop when the effective mean stress is more than twice the rock tensile strength, which suppresses the formation of tensile/hybrid fractures. In this study, thin slots were precut in siliceous mudstone samples and mechanical experiments were conducted under a range of effective confining pressures using core samples with and without precut slots. A comparison of fractures formed in the samples at different applied effective mean stresses gave results consistent with the proposed model. The correspondence of model predictions and results was also corroborated by observations of natural damage-zone fractures observed in the field, in boreholes penetrating the same siliceous mudstone as used in the experiments. The results indicate that fault zones containing numerous tensile/hybrid fractures are limited to domains that have experienced effective mean stresses of less than twice the rock tensile strength.

  14. Damping Higher Order Modes in the PEP-II B-Factory Vertex Bellows

    SciTech Connect

    Weathersby, S.; Langton, J.; Novokhatski, A.; Seeman, J.; /SLAC

    2005-06-30

    Higher stored currents and shorter bunch lengths are requirements for increasing luminosity in colliding storage rings. As a result, more HOM power is generated in the IP region. This HOM power propagates to sensitive components causing undesirable heating, thus becoming a limiting issue for the PEP-II B-factory. HOM field penetration through RF shielding fingers has been shown to cause heating in bellows structures. To overcome these limitations, a proposal to incorporate ceramic absorbers within the bellows cavity to damp these modes is presented. Results show that the majority of modes of interest are damped, the effectiveness depending on geometrical considerations. An optimal configuration is presented for the PEP-II B-factory IR bellows component utilizing commercial grade ceramics with consideration for heat transfer requirements.

  15. Sliding mode control of the space nuclear reactor system TOPAZ II

    SciTech Connect

    Shtessel, Y.B.; Wyant, F.J.

    1996-03-01

    The Automatic Control System (ACS) of the space nuclear reactor power system TOPAZ II that generates electricity from nuclear heat using in-core thermionic converters is considered. Sliding Mode Control Technique was applied to the reactor system controller design in order to provide the robust high accuracy following of a neutron (thermal) power reference profile in a start up regime and a payload electric power (current) reference profile following in an operation regime. Extensive simulations of the TOPAZ II reactor system with the designed sliding mode controllers showed improved accuracy and robustness of the reactor system performances in a start up regime and in an electric power supply regime as well. {copyright} {ital 1996 American Institute of Physics.}

  16. Fracture Analysis of Competing Failure Modes of Aluminum-CFRP Joints Using Three-Layer Titanium Laminates as Transition

    NASA Astrophysics Data System (ADS)

    Woizeschke, P.; Vollertsen, F.

    2015-09-01

    The structural properties of lightweight constructions can be adapted to specific local requirements using multi-material designs. Aluminum alloys and carbon fiber-reinforced plastics (CFRP) are materials of great interest requiring suitable joining techniques in order to transfer the advantages of combining the materials to structural benefits. Thus, the research group "Schwarz-Silber" investigates novel concepts to enable frontal aluminum-CFRP joints using transition structures. In the foil concept titanium foils are used as transition elements. Specimens have been produced using three-layer titanium laminates. In tensile tests, three failure locations have been observed: (1) Al-Ti seam, (2) Ti-CFRP hybrid laminate, and (3) CFRP laminate. In this paper, the fracture mechanisms of these failure modes are investigated by analyzing metallographic micrographs and fracture surfaces as well as by correlating load-displacement curves to video imaging of tensile tests. The results show that the cracking of the CFRP layers can be traced back to an assembly error. The laminate character of the titanium part tends to reduce the Al-Ti seam strength. However, two sub-joint tests demonstrate that the Al-Ti seam can endure loads up to 9.5 kN. The ductile failure behavior of the Ti-CFRP hybrid laminates is caused by plastic deformations of the titanium laminate liners.

  17. Mode I fracture toughness behavior of hydro-thermally aged carbon fibre reinforced DGEBA-HHPA-PES systems

    NASA Astrophysics Data System (ADS)

    Alessi, Sabina; Pitarresi, Giuseppe; Spadaro, Giuseppe; Tumino, Davide

    2012-07-01

    In this work the Mode I fracture toughness behavior of unidirectional CFRP laminates is investigated by means of Double Cantilever Beam (DCB) tests. The composite samples were manufactured by thermal curing after impregnation of a Carbon fabric with a DGEBA epoxy and anhydride HHPA curing agent. One resin batch was also mixed with a PES thermoplastic monomer to enhance the matrix toughness. Two lots of samples, toughened and untoughened, were then left to soak in hot water to achieve various degrees of aging. The influence of matrix toughening and hydrothermal aging on the delamination behavior of the composite have then been assessed and correlated with characterization data from Dynamic Mechanical Thermal Analysis (DMTA) and Scanning Electron Microscopy (SEM).

  18. Determination of the Mode I Interlaminar Fracture Toughness by Using a Nonlinear Double-Cantilever Beam Specimen

    NASA Astrophysics Data System (ADS)

    Pavelko, V.; Lapsa, K.; Pavlovskis, P.

    2016-07-01

    The aim of this study is estimation of the effect of large deflections of a double-cantilever beam (DCB) on the accuracy of determination of the mode I interlaminar fracture toughness GIc of layered composites by using the nonlinear theory of bending of beams. The differential equation of the deflection curve of arm of the DCB specimen in the natural form was used to analyze the strain energy of the specimen and its strain energy release rate GI upon propagation of delamination under the action of cleavage forces at the ends of cantilevers. An algorithm for calculating the strain energy and its release rate in the DCB specimens is realized in the form of a MATLAB code. An experimental study was carried out on DCB specimens of a highly flexible carbon/epoxy laminate. The validity of the nonlinear model developed is demonstrated. The standard methods used to determine GIc are refined for the case of highly flexible specimens.

  19. Stress corrosion-controlled rates of mode I fracture propagation in calcareous bedrock

    NASA Astrophysics Data System (ADS)

    Voigtlaender, Anne; Leith, Kerry; Krautblatter, Michael

    2014-05-01

    Surface bedrock on natural rock slopes is subject to constant and cyclic environmental stresses (wind, water, wave, ice, seismic or gravitational). Studies indicate that these stresses range up to several hundred kPa, generally too low to cause macroscopic changes in intact rock, although clear evidence of fracture generation, crack propagation and weathering of bedrock illustrates the effect of environmental stresses at the Earth's surface. We suggest that material degradation and its extent, is likely to be controlled by the rate of stress corrosion cracking (SCC). Stress corrosion is a fluid-material reaction, where fluids preferentially react with strained atomic bonds at the tip of developing fractures. Stress corrosion in ferrous and siliceous materials is often accepted as the fracture propagation and degradation rate-controlling process where materials are subject to stresses and fluids. Although evidence for chemical weathering in propagating bedrock fractures is clear in natural environments, the physical system and quantification of stress corrosion in natural rocks is yet to be addressed. Here, we present preliminary data on the relationship between stresses at levels commonly present on natural rock slopes, and material damage resulting from stress corrosion under constant or cyclic tensile loading. We undertake single notch three-point bending tests (SNBT) on fresh calcareous bedrock specimens (1100x100x100mm) over a two-month period. Two beams containing an artificial notch are stressed to 75% of their ultimate strength, and a constant supply of weak acid is applied at the notch tip to enhance chemical reactions. A third, unloaded, beam is also exposed to weak acid in order to elucidate the contribution of stress corrosion cracking to the material degradation. Stresses at the tip of propagating cracks affect the kinetics of the chemical reaction in the specimen exposed to both loading and corrosion, leading to an increase in degradation, and greater

  20. Condylar restoration after early TMJ fractures and functional appliance therapy. Part II: Muscle evaluation.

    PubMed

    Kahl-Nieke, B; Fischbach, R

    1999-01-01

    The aim of this study was to analyze and to describe the condition of the lateral pterygoid muscle during and after functional appliance therapy in children who had sustained condylar fractures. The treatment group consisted of 19 patients with an average age of 13.4 years, who had sustained a unilateral fracture at an average age of 8.4 years and had been treated functionally for 6 to 8 months. Muscle condition was assessed through axial soft tissue description. The volume and density of the lateral pterygoid muscle were measured in both groups and were compared on the basis of sex, age and fracture type. 74% of the patients in the follow-up group showed muscle differences of more than 10% between the 2 sides. In 2/3 of these patients the lateral pterygoid of the fracture side was 13 to 69% smaller. The volumes of the contralateral pterygoid muscles in the 2 patient groups differed by 10% on the basis of sex. Both in the treatment group and in the follow-up group the volume difference between the healthy and fractured side was as high as 70% depending on localization and type of fracture. Deep fractures and fractures with complete dislocation of the condyle evoked the most serious reduction in muscle volume.

  1. Measurements and Analysis of Longitudinal HOM Driven Coupled Bunch Modes in PEP-II Rings

    SciTech Connect

    Mastorides, T; Rivetta, C.; Fox, J.D.; Winkle, D.Van; /SLAC

    2008-07-07

    The growth rates of the longitudinal higher-order impedance-driven beam modes have greatly increased since the initial PEP-II design and commissioning. This increase is attributed to the addition of 6 1.2MW RF stations with 8 accelerating cavities in the HER and 2 1.2MW RF stations with 4 accelerating cavities in the LER, which allowed operations at twice the design current and almost four times the luminosity. As a result, the damping requirements for the longitudinal feedback have greatly increased since the design, and the feedback filters and control schemes have evolved during PEP-II operations. In this paper, growth and damping rate data for the higher-order mode (HOM) driven coupled-bunch modes are presented from various PEP-II runs and are compared with historical estimates during commissioning. The effect of noise in the feedback processing channel is also studied. Both the stability and performance limits of the system are analyzed.

  2. Experimental and Numerical Study on the Cracked Chevron Notched Semi-Circular Bend Method for Characterizing the Mode I Fracture Toughness of Rocks

    NASA Astrophysics Data System (ADS)

    Wei, Ming-Dong; Dai, Feng; Xu, Nu-Wen; Liu, Jian-Feng; Xu, Yuan

    2016-05-01

    The cracked chevron notched semi-circular bending (CCNSCB) method for measuring the mode I fracture toughness of rocks combines the merits (e.g., avoidance of tedious pre-cracking of notch tips, ease of sample preparation and loading accommodation) of both methods suggested by the International Society for Rock Mechanics, which are the cracked chevron notched Brazilian disc (CCNBD) method and the notched semi-circular bend (NSCB) method. However, the limited availability of the critical dimensionless stress intensity factor (SIF) values severely hinders the widespread usage of the CCNSCB method. In this study, the critical SIFs are determined for a wide range of CCNSCB specimen geometries via three-dimensional finite element analysis. A relatively large support span in the three point bending configuration was considered because the fracture of the CCNSCB specimen in that situation is finely restricted in the notch ligament, which has been commonly assumed for mode I fracture toughness measurements using chevron notched rock specimens. Both CCNSCB and NSCB tests were conducted to measure the fracture toughness of two different rock types; for each rock type, the two methods produce similar toughness values. Given the reported experimental results, the CCNSCB method can be reliable for characterizing the mode I fracture toughness of rocks.

  3. Mixed Mode Stable Tearing of Thin Sheet Al 6061-T6 Specimens: Experimental Measurements and Finite Element Simulations using a Modified Mohr-Coulomb Fracture Criterion

    DTIC Science & Technology

    2010-11-01

    grounding. Oliver (1996a,b), Teng (2008) andXue (2007a) reported on successful application of contin- uum damage mechanics in simulating initiation and...the accumulated damage should reach the critical value and the load carrying capacity must vanish in the post-initiate range. It should be noted that...specimen using fracture coupled with damage plastic- ity approach. Different from Mode I, little thickness reduction is observed for Mode III loading, as

  4. Kinetics of fracture in Fe-3Si steel under mode I loading

    NASA Technical Reports Server (NTRS)

    Bessendorf, Michael H.

    1989-01-01

    This paper deals with experimental studies of fatigue crack propagation (FCP) in Fe-3Si steel. The FCP experiments were performed on single-edge crack specimens. Results show that an extensive damage zone consisting of slip bands surrounds and precedes the propagating crack. The system of the crack and the damage zone constitutes the crack layer (CL). The results demonstrate that fracture propagates by the translation, expansion, and distortion of the part of CL called the active zone. The contours of the damage distribution show that different loading stresses may cause significantly different shapes of damage. Application of the stability criteria is demonstrated. It was shown that the critical energy release rate depends on the history of loading.

  5. A boundary element alternating method for two-dimensional mixed-mode fracture problems

    NASA Technical Reports Server (NTRS)

    Raju, I. S.; Krishnamurthy, T.

    1992-01-01

    A boundary element alternating method, denoted herein as BEAM, is presented for two dimensional fracture problems. This is an iterative method which alternates between two solutions. An analytical solution for arbitrary polynomial normal and tangential pressure distributions applied to the crack faces of an embedded crack in an infinite plate is used as the fundamental solution in the alternating method. A boundary element method for an uncracked finite plate is the second solution. For problems of edge cracks a technique of utilizing finite elements with BEAM is presented to overcome the inherent singularity in boundary element stress calculation near the boundaries. Several computational aspects that make the algorithm efficient are presented. Finally, the BEAM is applied to a variety of two dimensional crack problems with different configurations and loadings to assess the validity of the method. The method gives accurate stress intensity factors with minimal computing effort.

  6. Effective representation of amide III, II, I, and A modes on local vibrational modes: Analysis of ab initio quantum calculation results

    NASA Astrophysics Data System (ADS)

    Hahn, Seungsoo

    2016-10-01

    The Hamiltonian matrix for the first excited vibrational states of a protein can be effectively represented by local vibrational modes constituting amide III, II, I, and A modes to simulate various vibrational spectra. Methods for obtaining the Hamiltonian matrix from ab initio quantum calculation results are discussed, where the methods consist of three steps: selection of local vibrational mode coordinates, calculation of a reduced Hessian matrix, and extraction of the Hamiltonian matrix from the Hessian matrix. We introduce several methods for each step. The methods were assessed based on the density functional theory calculation results of 24 oligopeptides with four different peptide lengths and six different secondary structures. The completeness of a Hamiltonian matrix represented in the reduced local mode space is improved by adopting a specific atom group for each amide mode and reducing the effect of ignored local modes. The calculation results are also compared to previous models using C=O stretching vibration and transition dipole couplings. We found that local electric transition dipole moments of the amide modes are mainly bound on the local peptide planes. Their direction and magnitude are well conserved except amide A modes, which show large variation. Contrary to amide I modes, the vibrational coupling constants of amide III, II, and A modes obtained by analysis of a dipeptide are not transferable to oligopeptides with the same secondary conformation because coupling constants are affected by the surrounding atomic environment.

  7. Effective representation of amide III, II, I, and A modes on local vibrational modes: Analysis of ab initio quantum calculation results.

    PubMed

    Hahn, Seungsoo

    2016-10-28

    The Hamiltonian matrix for the first excited vibrational states of a protein can be effectively represented by local vibrational modes constituting amide III, II, I, and A modes to simulate various vibrational spectra. Methods for obtaining the Hamiltonian matrix from ab initio quantum calculation results are discussed, where the methods consist of three steps: selection of local vibrational mode coordinates, calculation of a reduced Hessian matrix, and extraction of the Hamiltonian matrix from the Hessian matrix. We introduce several methods for each step. The methods were assessed based on the density functional theory calculation results of 24 oligopeptides with four different peptide lengths and six different secondary structures. The completeness of a Hamiltonian matrix represented in the reduced local mode space is improved by adopting a specific atom group for each amide mode and reducing the effect of ignored local modes. The calculation results are also compared to previous models using C=O stretching vibration and transition dipole couplings. We found that local electric transition dipole moments of the amide modes are mainly bound on the local peptide planes. Their direction and magnitude are well conserved except amide A modes, which show large variation. Contrary to amide I modes, the vibrational coupling constants of amide III, II, and A modes obtained by analysis of a dipeptide are not transferable to oligopeptides with the same secondary conformation because coupling constants are affected by the surrounding atomic environment.

  8. A Modified Edge Crack Torsion Test for Measurement of Mode III Fracture Toughness of Laminated Tape Composites

    NASA Technical Reports Server (NTRS)

    Czabaj, Michael W.; Davidson, Barry D.; Ratcliffe, James G.

    2016-01-01

    Modifications to the edge crack torsion (ECT) test are studied to improve the reliability of this test for measuring the mode-III fracture toughness, G (sub IIIc), of laminated tape fiber-reinforced polymeric (FRP) composites. First, the data reduction methods currently used in the ECT test are evaluated and deficiencies in their accuracy are discussed. An alternative data reduction technique, which uses a polynomial form to represent ECT specimen compliance solution, is evaluated and compared to FEA (finite element analysis) results. Second, seven batches of ECT specimens are tested, each batch containing specimens with a preimplanted midplane edge delamination and midplane plies with orientations of plus theta divided by minus theta, with theta ranging from 0 degrees to 90 degrees in 15-degree increments. Tests on these specimens show that intralaminar cracking occurs in specimens from all batches except for which theta = 15 degrees and 30 degrees. Tests on specimens of these two batches are shown to result in mode-III delamination growth at the intended ply interface. The findings from this study are encouraging steps towards the use of the ECT test as a standardized method for measuring G (sub IIIc), although further modification to the data reduction method is required to make it suitable for use as part of a standardized test method.

  9. A kinetic model for type I and II IP3R accounting for mode changes.

    PubMed

    Siekmann, Ivo; Wagner, Larry E; Yule, David; Crampin, Edmund J; Sneyd, James

    2012-08-22

    Based upon an extensive single-channel data set, a Markov model for types I and II inositol trisphosphate receptors (IP(3)R) is developed. The model aims to represent accurately the kinetics of both receptor types of IP(3)R depending on the concentrations of inositol trisphosphate (IP(3)), adenosine trisphosphate (ATP), and intracellular calcium (Ca(2+)). In particular, the model takes into account that for some combinations of ligands the IP(3)R switches between extended periods of inactivity alternating with intervals of bursting activity (mode changes). In a first step, the inactive and active modes are modeled separately. It is found that, within modes, both receptor types are ligand-independent. In a second step, the submodels are connected by transition rates. Ligand-dependent regulation of the channel activity is achieved by modulating these transitions between active and inactive modes. As a result, a compact representation of the IP(3)R is obtained that accurately captures stochastic single-channel dynamics including mode changes in a model with six states and 10 rate constants, only two of which are ligand-dependent.

  10. Quantifying voids effecting delamination in carbon/epoxy composites: static and fatigue fracture behavior

    NASA Astrophysics Data System (ADS)

    Hakim, I.; May, D.; Abo Ras, M.; Meyendorf, N.; Donaldson, S.

    2016-04-01

    On the present work, samples of carbon fiber/epoxy composites with different void levels were fabricated using hand layup vacuum bagging process by varying the pressure. Thermal nondestructive methods: thermal conductivity measurement, pulse thermography, pulse phase thermography and lock-in-thermography, and mechanical testing: modes I and II interlaminar fracture toughness were conducted. Comparing the parameters resulted from the thermal nondestructive testing revealed that voids lead to reductions in thermal properties in all directions of composites. The results of mode I and mode II interlaminar fracture toughness showed that voids lead to reductions in interlaminar fracture toughness. The parameters resulted from thermal nondestructive testing were correlated to the results of mode I and mode II interlaminar fracture toughness and voids were quantified.

  11. Predicting the occurrence of mixed mode failure associated with hydraulic fracturing, part 2 water saturated tests

    SciTech Connect

    Bauer, Stephen J.; Broome, Scott Thomas; Choens, Charles; Barrow, Perry Carl

    2015-09-14

    Seven water-saturated triaxial extension experiments were conducted on four sedimentary rocks. This experimental condition was hypothesized more representative of that existing for downhole hydrofracture and thus it may improve our understanding of the phenomena. In all tests the pore pressure was 10 MPa and confirming pressure was adjusted to achieve tensile and transitional failure mode conditions. Using previous work in this LDRD for comparison, the law of effective stress is demonstrated in extension using this sample geometry. In three of the four lithologies, no apparent chemo-mechanical effect of water is apparent, and in the fourth lithology test results indicate some chemo-mechanical effect of water.

  12. Effect of Embedded Piezoelectric Sensors on Fracture Toughness and Fatigue Resistance of Composite Laminates Under Mode I Loading

    NASA Technical Reports Server (NTRS)

    Murri, Gretchen B.

    2006-01-01

    Double-cantilevered beam (DCB) specimens of a glass/epoxy composite material with embedded piezoelectric sensors were tested both statically and under fatigue loading to determine the effect of the embedded material on the Mode I fracture toughness and fatigue resistance compared to baseline data without the embedded elements. A material known as LaRC-Macrofiber Composite (LaRC-MFC (TradeMark)), or MFC, was embedded at the midplane of the specimen during the layup. Specimens were manufactured with the embedded MFC material either at the loaded end of the specimen to simulate an initial delamination; or with the MFC material located at the delaminating interface, with a Teflon film at the loaded end to simulate an initial delamination. There were three types of specimens with the embedded material at the delaminating interface: co-cured with no added adhesive; cured with a paste adhesive applied to the embedded element; or cured with a film adhesive added to the embedded material. Tests were conducted with the sensors in both the passive and active states. Results were compared to baseline data for the same material without embedded elements. Interlaminar fracture toughness values (G(sub Ic)) for the passive condition showed little change when the MFC was at the insert end. Passive results varied when the MFC was at the delaminating interface. For the co-cured case and with the paste adhesive, G(sub Ic) decreased compared to the baseline toughness, whereas, for the film adhesive case, G(sub Ic) was significantly greater than the baseline toughness, but the failure was always catastrophic. When the MFC was in the active state, G(sub Ic) was generally lower compared to the passive results. Fatigue tests showed little effect of the embedded material whether it was active or passive compared to baseline values.

  13. Trapped modes in the PEP-II B-Factory Interaction Region

    SciTech Connect

    Henestroza, E.; Heifets, S.; Zolotorev, M.

    1995-04-01

    The design of the PEP-II B-Factory Interaction Region is based primarily on beam-stay-clear requirements and on synchrotron radiation background considerations (masks are required to shield the detector beam pipe from all sources of synchrotron radiation). A complicated 3-dimensional structure results from these requirements. A high intensity beam traversing this structure will generate wake fields that lead to energy deposition on the beam pipe, as well as to decelerating and deflecting forces acting back on the beam. Computation of wake fields and impedances in frequency-domain and time-domain using 2-D and 3-D electromagnetic codes revealed the existence of trapped modes in the interaction region, which if not controlled could enhance the higher order model heating of the beam pipe. We will present the simulation results and the design strategy to avoid resonant conditions between these trapped modes and the bunch train frequency.

  14. Mixed-mode fatigue fracture of adhesive joints in harsh environments and nonlinear viscoelastic modeling of the adhesive

    NASA Astrophysics Data System (ADS)

    Arzoumanidis, Alexis Gerasimos

    A four point bend, mixed-mode, reinforced, cracked lap shear specimen experimentally simulated adhesive joints between load bearing composite parts in automotive components. The experiments accounted for fatigue, solvent and temperature effects on a swirled glass fiber composite adherend/urethane adhesive system. Crack length measurements based on compliance facilitated determination of da/dN curves. A digital image processing technique was also utilized to monitor crack growth from in situ images of the side of the specimen. Linear elastic fracture mechanics and finite elements were used to determine energy release rate and mode-mix as a function of crack length for this specimen. Experiments were conducted in air and in a salt water bath at 10, 26 and 90°C. Joints tested in the solvent were fully saturated. In air, both increasing and decreasing temperature relative to 26°C accelerated crack growth rates. In salt water, crack growth rates increased with increasing temperature. Threshold energy release rate is shown to be the most appropriate design criteria for joints of this system. In addition, path of the crack is discussed and fracture surfaces are examined on three length scales. Three linear viscoelastic properties were measured for the neat urethane adhesive. Dynamic tensile compliance (D*) was found using a novel extensometer and results were considerably more accurate and precise than standard DMTA testing. Dynamic shear compliance (J*) was determined using an Arcan specimen. Dynamic Poisson's ratio (nu*) was extracted from strain gage data analyzed to include gage reinforcement. Experiments spanned three frequency decades and isothermal data was shifted by time-temperature superposition to create master curves spanning thirty decades. Master curves were fit to time domain Prony series. Shear compliance inferred from D* and nu* compared well with measured J*, forming a basis for finding the complete time dependent material property matrix for this

  15. Normal Modes for Dynamic Motions of a Topoisomerase II enzyme upon DNA-Binding and Bending

    NASA Astrophysics Data System (ADS)

    Mentes, Ahmet

    We have used Molecular Dynamics (MD) simulation methods and two analytical approaches (the Gaussian Network Model (GNM) and Anisotropic Network Model (ANM)) to investigate the internal dynamic motions of the S. cerevisiae Topoisomerase (TopoII) during the first step of its catalytic cycle. At the initial state of the first step of its catalytic cycle, the protein and a 34 bp straight-DNA structure have no interaction. At the final state of the cycle, we have the bended-DNA/TopoII complex where the protein binds to DNA and, at this stage, the protein binds and bends the DNA, just before the DNA cleavage by TopoII. Normal mode analysis is used to characterize the functional flexibility of the protein, especially the C-gate domain closing/opening during the DNA binding/bending process and before DNA cleavage. Because of its clinical importance, our study might be helpful to better understand the next steps of its catalytic cycle and may provide new insight into the dynamics and structure of other TopoII-DNA complexes.

  16. Temporary space maintainers retained with composite resin. Part II: Fracture load in vitro.

    PubMed

    Grajower, R; Stern, N; Zamir, S T; Kohavi, D

    1981-01-01

    The average fracture load during occlusal loading of pontics which were bonded to natural abutment teeth in vitro was found to be 56.1, 57.5 and 74.2 kg for natural, acrylic resin, and Restodent pontics, respectively. Coating the roots of the abutment teeth with a thin layer of silicone rubber before embedding them in stone slightly reduced the strength of the fixed partial dentures. Thermocycling the specimens with coated roots caused a considerable decrease in strength to fracture loads of 33.0, 17.9, and 37.3 kg for natural, acrylic resin, and Restodent pontics, respectively. Fracture of the enamel of natural tooth pontics was observed in a few specimens. The superior strength of the fixed partial dentures with natural tooth and Restodent pontics would indicate that these pontics are superior for clinical trials rather than acrylic resin pontics.

  17. Application of the J integral to fracture under mixed-mode loading. [MMJINT; 4330V steel

    SciTech Connect

    Riddle, R.A.

    1981-06-01

    The calculation of the J integral proved to be a successful method for characterizing the stress and displacement fields around a crack tip under mixed mode loading. A computer program was written to determine the symmetric and antisymmetric J integral quantities. The stress intensity factors from these J integral calculations were in excellent agreement with other calculations. The compact shear specimen used contains three loading holes, the load applied at the center hole being the opposite direction to the load applied at the two outer holes. For 7075-T6 aluminum, K/sub IIc/ was 1.9 times larger than K/sub Ic/. In the brittle photoelastic material K/sub IIc/ was less than K/sub Ic/. Failure of the 4330V steel compact shear specimens came as a result of the average shear stress in the region ahead of the crack tip exceeding the material flow shear stress. The experimental results suggest that the angle of crack growth is best predicted by the maximum tangential stress theory.

  18. Fracture strength and elastic modulus as a function of porosity for hydroxyapatite and other brittle materials, Part II

    SciTech Connect

    Fan, Xiaofeng; Case, Eldon D; Ren, Fei; Shu, Yutian; Baumann, Melissa

    2012-01-01

    Part I of this paper discussed the Weibull modulus m, versus porosity P behavior of brittle materials, including HA. While the Weibull modulus m deals with the scatter in fracture strength data, this paper (Part II) focuses on two additional key mechanical properties of porous materials, namely the average fracture strength f , and Young s modulus E, for P in the interval from P zero to P PG (the porosity of the unfired compacts). The f versus P data for HA from this study and the literature data for alumina, yttria stabilized zirconia (YSZ) and silicon nitride are describedwell by functions of , where = 1 P/PG = the degree of densification. A similar function of applies to the E versus P behavior of HA from this study and data from the literature for alumina, titanium and YSZ. All of the data analyzed in this study (Part II) are based on partially and fully sintered powder compacts (excluding green powder compacts), thus the f / 0 versus and E /E0 versus relationships may apply only to such specimens.

  19. Stimuli Responsive/Rheoreversible Hydraulic Fracturing Fluids for Enhanced Geothermal Energy Production (Part II)

    SciTech Connect

    Bonneville, Alain; Jung, Hun Bok; Shao, Hongbo; Kabilan, Senthil; Um, Wooyong; Carroll, Kenneth C.; Varga, Tamas; Suresh, Niraj; Stephens, Sean A.; Fernandez, Carlos A.

    2014-12-14

    We have used an environmentally friendly and recyclable hydraulic fracturing fluid - diluted aqueous solutions of polyallylamine or PAA – for reservoir stimulation in Enhanced Geothermal System (EGS). This fluid undergoes a controlled and large volume expansion with a simultaneous increase in viscosity triggered by CO2 at EGS temperatures. We are presenting here the results of laboratory-scale hydraulic fracturing experiment using the fluid on small cylindrical rock cores (1.59 cm in diameter and 5.08 cm in length) from the Coso geothermal field in California. Rock samples consisted of Mesozoic diorite metamorphosed to greenschist facies. The experiments were conducted on 5 samples for realistic ranges of pressures (up to 275 bar) and temperatures (up to 210 °C) for both the rock samples and the injected fluid. After fracturing, cores were subjected to a CO2 leakage test, injection of KI solution, and X-ray microtomography (XMT) scanning to examine the formation and distribution of fractures. The design and conduct of these experiments will be presented and discussed in details. Based on the obtained XMT images, Computational Fluid Dynamics (CFD) simulations were then performed to visualize hydraulic fractures and compute the bulk permeability. OpenFOAM (OpenCFD Ltd., Reading, UK), was used to solve the steady state simulation. The flow predictions, based upon the laminar, 3-D, incompressible Navier-Stokes equations for fluid mass and momentum, show the remarkable stimulation of the permeability in the core samples and demonstrate the efficiency of such a CO2 triggered fluid in EGS.

  20. Linear growth rates of types I and II convective modes within the rotating-cone boundary layer

    NASA Astrophysics Data System (ADS)

    Garrett, S. J.

    2010-04-01

    Experimental observations have shown that the transition characteristics of the boundary-layer flow over rotating cones depends on the cone half-angle. In particular, pairs of counter-rotating Görtler-type vortices are observed over cones with slender half-angles and co-rotating vortices are observed over broad cones. Garrett et al (2009 J. Fluid Mech. 622 209-32) have hypothesized the existence of a centrifugal instability mode over slender cones that is more dangerous than the types I (crossflow) and II (streamline curvature) modes which dominate over rotating disks and broad cones. Work is currently underway to clarify this alternative mode; however, a clear understanding of the growth rates of types I and II modes is crucial to the ultimate understanding of how the dominant mode changes with half-angle. In this paper, we demonstrate that the maximum growth rate for types I and II modes decreases with reduced half-angle, which clears the way for the dominance of the alternative instability mode. Furthermore, it is suggested that vortices travelling at 75% of the cone surface speed will be selected over smooth, clean rotating cones with half-angle such that the type I mode is dominant. Interestingly, this vortex speed has been experimentally observed by Kobayashi and Arai within the rotating-sphere boundary layer.

  1. Macro- and Micro-Mechanics of Mixed-Mode Dynamic Fracture of Concrete. Part 1. Micro-Mechanic Analysis

    DTIC Science & Technology

    1993-02-14

    fracture energy density of concrete were discussed by Hillerborg and Mindess [55-57]. The total external energy needed to quasi-statically fracture a...Composites.: Strzin Rate Effects on Fracture, eds. S. Mindess and S.P Shah, Materials Research Society Symposia Proceeding Vol. 64, 1986 18 S. Mindess ...Nijhoff Publishers, 1985, pp. 617-636. I 1 9 A. Benton, S. Mindess , and N. Benthur, "The Behavior of Concrete Under Impact Loading: Experimental

  2. Some recent theoretical and experimental developments in fracture mechanics

    NASA Technical Reports Server (NTRS)

    Liebowitz, H.; Eftis, J.; Hones, D. L.

    1978-01-01

    Recent theoretical and experimental developments in four distinct areas of fracture mechanics research are described. These are as follows: experimental comparisons of different nonlinear fracture toughness measures, including the nonlinear energy, R curve, COD and J integral methods; the singular elastic crack-tip stress and displacement equations and the validity of the proposition of their general adequacy as indicated, for example, by the biaxially loaded infinite sheet with a flat crack; the thermodynamic nature of surface energy induced by propagating cracks in relation to a general continuum thermodynamic description of brittle fracture; and analytical and experimental aspects of Mode II fracture, with experimental data for certain aluminum, steel and titanium alloys.

  3. Effect of TE Mode Power on the PEP II LER BPM System

    SciTech Connect

    Ng, Cho-K

    2011-08-26

    The beam chamber of the PEP-II B-Factory Low Energy Ring (LER) arc sections is connected to an antechamber for the absorption of synchrotron radiation on discrete photon stops. The presence of the antechamber substantially reduces the cutoff frequency of the vacuum chamber and, in particular, allows the propagation of higher-order-mode (HOM) TE power generated by beamline components at the BPM signal processing frequency. Calculations of the transmission properties of the TE mode in different sections of the vacuum chamber show that the power is trapped between widely separated bellows in the arc sections. Because of the narrow signal bandwidth and weak coupling of the TE mode to the BPM buttons, the noise contributed by the HOM TE power will not produce a noticeable effect on the BPM position signal voltage. The LER arc vacuum chamber employs an antechamber with a discrete photon stop for absorption of synchrotron radiation and with pumps for maintaining pressure below 10 nTorr [1]. The horizontal dimensions of the antechambers at the pumping chamber section and the magnet chamber section are larger or comparable to that of the beam chamber. Because of the increase in the horizontal dimension, the cutoff frequency of the TE10-like mode (in rectangular coordinates) of the vacuum chamber is considerably reduced and, in particular, is less than the BPM signal processing frequency at 952 MHz. TE power propagating in the vacuum chamber will penetrate through the BPM buttons and will affect the pickup signal if its magnitude is not properly controlled. It is the purpose of this note to clarify various issues pertaining to this problem. TE power is generated when the beam passes a noncylindrically symmetric beamline component such as the RF cavity, the injection region, the IR crotch and the IP region. The beampipes connected to these components have TE cutoff frequencies greater than 952 MHz (for example, the TE cutoff frequency of the RF cavity beampipe is 1.8 GHz

  4. Characterization of debond growth mechanism in adhesively bonded composites under mode II static and fatigue loadings

    NASA Technical Reports Server (NTRS)

    Mall, S.; Kochhar, N. K.

    1988-01-01

    An experimental investigation of adhesively bonded composite joint was conducted to characterize the debond growth mechanism under mode II static and fatigue loadings. For this purpose, end-notched flexure specimens of graphite/epoxy (T300/5208) adherends bonded with EC 3445 adhesive were tested. In all specimen tested, the fatigue failure occurred in the form of cyclic debonding. The present study confirmed the result of previous studies that total strain-energy-release rate is the driving parameter for cyclic debonding. Further, the debond growth resistance under cyclic loading with full shear reversal (i.e., stress ratio, R = -1) is drastically reduced in comparison to the case when subjected to cyclic shear loading with no shear reversal (i.e., R = 0.1).

  5. Damping higher order modes in the PEP-II B-Factory storage ring collider

    NASA Astrophysics Data System (ADS)

    Weathersby, Stephen

    2007-05-01

    The PEP-II B-Factory storage ring collider at SLAC provides crucial experimental evidence for the physics of CP violation. To investigate rare B-meson decays requires high luminosity which comes mainly from increasing bunch currents and reducing bunch sizes. Electromagnetic effects of intense bunch fields in the form of wake fields couple into accelerator components, inducing Joule heating at levels detrimental to vacuum chamber components. Additionally, wake fields contribute to beam instability, decreasing luminosity. These effects are limiting B-factory performance. Computer simulations and experimental evidence indicate that beam collimators produce wake fields in the form of dipole and quadrupole waveguide modes which can propagate tens of meters from their source before depositing energy at remote locations. Simulations confirm that coupling through narrow slots into bellows cavities occurs for beam pipe modes. Two proposals are set forth to mitigate wake field effects. The first proposal is to reduce the quality factor of resonant structures with a water cooled dielectric lossy material. Electromagnetic energy coupling into resonant structures can be isolated and safely dissipated. Prototype devices have been built and have been shown to reduce resistive heating in large pumping chambers coupled to the beam chamber. Designs and simulations which incorporate such techiques into bellows devices are presented. The second proposal incorporates novel devices introduced in the accelerator vacuum chamber which selectively traps dipole and quadrupole propagating wake fields before they can couple into sensitive beam line components without introducing impedance to the beam. Scattering parameter analysis is used to tailor device response to specific modes. Dangerous modes are extracted from the beam chamber, trapped and dissipated in a water cooled lossy material. Modes which represent an impedance to the beam are not affected. After design optimization, production

  6. A fatal iatrogenic right vertebral injury after transoral odontoidectomy and posterior cervical stabilization for a type II odontoid fracture.

    PubMed

    Scalici, Edoardo; Indorato, Francesca; Portelli, Francesca; Savì, Tommaso; Maresi, Emiliano; Busardò, Francesco P

    2014-02-01

    The authors present a singular case of an iatrogenic right vertebral artery injury, involving a 67 year-old man, who reported a type II odontoid fracture (Anderson and D'Alonzo Classification) and posterior atlantoaxial dislocation following a road traffic accident. A small injury involving the right vertebral artery occurred as a consequence of transoral odontoidectomy and posterior cervical stabilization. It was caused by bone spicules of spinal origin and their presence was confirmed by the histological section of the right vertebral artery at the level of C1-C2. The case confirms how iatrogenic vertebral artery injuries during cervical spine surgery may be potentially lethal, especially where complications arise some days after surgery.

  7. A compendium of sources of fracture toughness and fatigue crack growth data for metallic alloys. II

    NASA Technical Reports Server (NTRS)

    Hudson, C. M.; Seward, S. K.

    1982-01-01

    A compendium is presented of sources for metallic alloy fracture toughness and fatigue crack growth data, which concentrates on technical reports as the primary source of references and updates the previous Hudson and Seward (1978) compendium references on technical journals. Where available, the accession numbers which are used as code numbers for the ordering of the reports from their publishers are given. The sources of these reports include the AIAA Technical Information Service, the Defense Technical Information Center, the National Technical Information Service, and NASA.

  8. Pseudo-type-II tuning behavior and mode identification in whispering gallery optical parametric oscillators.

    PubMed

    Meisenheimer, Sarah-Katharina; Fürst, Josef Urban; Schiller, Annelie; Holderied, Florian; Buse, Karsten; Breunig, Ingo

    2016-06-27

    Wavelength tuning of conventional mirror-based optical parametric oscillators (OPOs) exhibits parabolically-shaped tuning curves (type-0 and type-I phase matching) or tuning branches that cross each other with a finite slope (type-II phase matching). We predict and experimentally prove that whispering gallery OPOs based on type-0 phase matching show both tuning behaviors, depending on whether the mode numbers of the generated waves coincide or differ. We investigate the wavelength tuning of optical parametric oscillation in a millimeter-sized radially-poled lithium niobate disk pumped at 1 μm wavelength generating signal and idler waves between 1.7 and 2.6 μm wavelength. Our experimental findings excellently coincide with the theoretical predictions. The investigated whispering gallery optical parametric oscillator combines the employment of the highest nonlinear-optical coefficient of the material with a controlled type-II-like wavelength tuning and with the possibility of self-phase locking.

  9. The effect of incomplete crown ferrules on fracture resistance and failure modes of endodontically treated maxillary incisors restored with quartz fiber post, composite core, and crowns

    PubMed Central

    Muangamphan, Panorjit; Sattapan, Boonrat; Kukiattrakoon, Boonlert; Thammasitboon, Kewalin

    2015-01-01

    Aim: To investigate the fracture resistance of restored endodontically treated teeth (RETT) with fiber posts, cores, and crowns with limited ferrules. Materials and Methods: Sixty maxillary anterior teeth were endodontically treated and decoronated 2 mm above the cemento-enamel junction, and then divided into 6 groups of 10 teeth each; Group circumferential ferrule (2FR), Group ferrule in the labial, mesial, and palatal region (2FR-LaMPa), Group ferrule in the labial, and palatal region (2FR-LaPa), Group 2FR-Pa and 2FR-La respectively, and Group 0FR (no ferrule). All 60 prepared teeth were then restored with quartz fiber posts, resin composite cores, and metal crowns. The specimens were subjected to load until failure occurred. Data were analyzed using one-way analysis of variance and Tukey's tests (α = 0.05). The mode of failure was determined under a stereoscope. Results: A statistical significant difference was found among groups 2FR-LaMPa, 2FR-Pa, 2FR-LaPa, and 2FR from the group 2FR-La, and from the group 0FR (P < 0.01). The predominant mode of failure was an oblique palatal to labial root fracture for the groups with remaining ferrules. Conclusion: For RETT that have incomplete crown ferrules, the location of the ferrules may affect their fracture resistance. PMID:26069401

  10. Geothermal fracture stimulation technology. Volume II. High-temperature proppant testing

    SciTech Connect

    Not Available

    1980-07-01

    Data were obtained from a newly built proppant tester, operated at actual geothermal temperatures. The short term test results show that most proppants are temperature sensitive, particularly at the higher closure stresses. Many materials have been tested using a standard short-term test, i.e., fracture-free sand, bauxite, and a resin-coated sand retained good permeability at the high fluid temperatures in brine over a range of closure stresses. The tests were designed to simulate normal closure stress ranges for geothermal wells which are estimated to be from 2000 to 6000 psi. Although the ultra high closure stresses in oil and gas wells need not be considered with present geothermal resources, there is a definite need for chemically inert proppants that will retain high permeability for long time periods in the high temperature formations.

  11. Topical report on subsurface fracture mapping from geothermal wellbores. Phase I. Pulsed radar techniques. Phase II. Conventional logging methods. Phase III. Magnetic borehole ranging

    SciTech Connect

    Hartenbaum, B.A.; Rawson, G.

    1980-09-01

    To advance the state-of-the-art in Hot Dry Rock technology, an evaluation is made of (i) the use of radar to map far-field fractures, (ii) the use of more than twenty different conventional well logging tools to map borehole-fracture intercepts, and (iii) the use of magnetic dipole ranging to determine the relative positions of the injection well and the production well within the fractured zone. It is found that according to calculations, VHF backscatter radar has the potential for mapping fractures within a distance of 50 +- 20 meters from the wellbore. A new technique for improving fracture identification is presented. Analyses of extant data indicate that when used synergistically the (1) caliper, (2) resistivity dipmeter, (3) televiewer, (4) television, (5) impression packer, and (6) acoustic transmission are useful for mapping borehole-fracture intercepts. Improvements in both data interpretation techniques and high temperature operation are required. The surveying of one borehole from another appears feasible at ranges of up to 200 to 500 meters by using a low frequency magnetic field generated by a moderately strong dipole source (a solenoid) located in one borehole, a sensitive B field detector that traverses part of the second borehole, narrow band filtering, and special data inversion techniques.

  12. Commentary on the management of type II odontoid process fractures in octogenarians: Article by Graffeo et al. and Editorial by Falavigna (J Neurosurgery Spine August 19, 2016)

    PubMed Central

    Epstein, Nancy E.

    2016-01-01

    Background: Establishing a clear treatment paradigm for octogenarians with type II odontoid fractures in hampered by a literature replete with level III articles. Methods: In the study by Graffeo et al., the authors evaluated 111 patients over the age of 79 (average age: 87) with type II odontoid fractures undergoing nonoperative (94 patients) vs. operative intervention (17 total; 15 posterior and 2 anterior). They studied multiple variables and utilized several scales [abbreviated injury scale (AIS), injury severity score (ISS), and the Glasgow coma scale (GCS)] to determine the outcomes of nonoperative vs. operative management. Results: Graffeo et al. concluded that there were no significant differences between nonoperative and operative management for type II odontoid fractures in octogenarians. They found similar frequencies of additional cervical fractures, mechanisms of injury, GCS of 8 or under, AIS/ISS scores, and disposition to “nonhome” facilities. Furthermore, both appeared to have increased mortality rates at 1-year post injury; 13% during hospitalization, 26% within the first post-injury month, and 41% at 1 year. Conclusions: In the editorial by Falavigna, his major criticism of Graffeo's article was the marked disparity in the number of patients in the operative (17 patients) vs. the nonoperative group (94 patients), making it difficult to accept any conclusions as “significant”. He further noted that few prior studies provided level I evidence, and that most, like this one, were level III analyses that did not “significantly” advance our knowledge as to whether to treat octogenarians with type II odontoid fractures operatively vs. nonoperatively. PMID:28028444

  13. A Protocol for Percutaneous Transarticular Fixation of Sanders Type II and III Calcaneal Fractures With or Without an Added Mini-Open Approach.

    PubMed

    Gamal, Osama; Shams, Ahmed; El-Sayed Semaya, Ahmad

    Intra-articular fracture of the calcaneus is one of the most displeasing fractures if not properly managed. Open reduction and internal fixation have been associated with a high incidence of postoperative soft tissue complications. Closed reduction and percutaneous fixation have resulted in a greater incidence of postoperative subtalar osteoarthritis with improper reduction of the articular surface. In the present study, a mini-open approach was used in cases of failure of articular surface restoration with closed reduction. A total of 64 feet in 57 consecutive patients with an intra-articular calcaneal fracture underwent the proposed minimally invasive surgical protocol. Of the 57 patients, 7 (12.3%) had bilateral fractures. According to Sanders classification, 33 (51.6%) fractures were type II and 31 (48.4%) were type III. Seven (12.3%) patients had wedge fractures of the dorsolumbar spine without neurologic manifestations. The postoperative evaluation included radiographs and completion of the Maryland Foot Score and visual analog scale for pain. The mean follow-up period was 16 (range 12 to 36) months. The mean operative time was 42 (range 35 to 60) minutes. The mean period until union of the fracture was 12 (range 10 to 16) weeks. The clinical results according to the Maryland Foot Score revealed 52 (81%) with satisfactory (27 excellent and 25 good) and 12 (19%) with unsatisfactory (10 fair and 2 poor) results. The mean visual analog scale score was 1.5 ± 0.3 when radiographic fracture healing was observed. Six patients (9.4%) developed superficial pin tract infections that responded to local care and parenteral antibiotic therapy and resolved completely after removal of the Kirschner wires. In conclusion, the presented surgical protocol combining closed reduction with or without an added mini-open approach and percutaneous fixation improves the functional outcome and minimizes the incidence of complications.

  14. Nose fracture

    MedlinePlus

    Fracture of the nose; Broken nose; Nasal fracture; Nasal bone fracture; Nasal septal fracture ... A fractured nose is the most common fracture of the face. It ... with other fractures of the face. Sometimes a blunt injury can ...

  15. Particle simulation of radio frequency stabilization of the flute mode in a tandem mirror. II. Perpendicular antenna

    SciTech Connect

    Abe, H.; Kadoya, Y.

    1988-10-01

    A two-and-a-half-dimensional electromagnetic particle code PS2M (J. Phys. Soc. Jpn. 56, 3899 (1987)) is used to study how an electric field applied perpendicularly to the magnetic field affects the radio frequency stabilization of flute modes in a tandem mirror plasma. The electric field perpendicular to the magnetic field stabilizes or destabilizes the flute mode through the mechanism of the ponderomotive force acting on electrons and ions and through the mechanism of sideband coupling. In the simulations two typical examples have been shown: (i) when the sideband coupling effects (in which the electron terms are dominant) stabilize the flute modes and (ii) when the perpendicular ponderomotive force acting on the electrons destabilizes the flute modes.

  16. Flow visualization of flow into 8 point-source fractures II: The effect of fracture non-uniformity and fluid crosslinking

    SciTech Connect

    Clark, P.E.; Zhu, Q.

    1994-12-31

    Recently, the flow of fluids into a fracture from a point source has been the subject of several different papers. Cleary and Fonseca first suggested that convective transport should play a major role in the placement of proppant when the flow into a fracture was from a point source. Clark and Courington presented data showing that for non-viscosified fluids convection was the dominant mechanism of transport. However, they showed, that for uniform fractures, viscosifying the fluid made a large difference in the transport mechanism. In a later paper, Clark and Zhu presented data for nonuniform fractures and viscosified fluids weighted with either salt or silica flour that showed that the presence of minor non-uniformities serve to negate the effect of convection even more than viscosifying the fluids. In this work, the authors have extended the work presented in the previous two papers to high viscosity Newtonian fluids and crosslinked fluids. The experiments have all been done with various concentrations of silica flour to simulate added proppant. Both changing the nature of the non-uniformities and crosslinking the polymer solution have a profound affect on the flow into the fracture and the convective process.

  17. Investigation of the mechanical properties and failure modes of hybrid natural fiber composites for potential bone fracture fixation plates.

    PubMed

    Manteghi, Saeed; Mahboob, Zia; Fawaz, Zouheir; Bougherara, Habiba

    2017-01-01

    The purpose of this study is to investigate the mechanical feasibility of a hybrid Glass/Flax/Epoxy composite material for bone fracture fixation such as fracture plates. These hybrid composite plates have a sandwich structure in which the outer layers are made of Glass/Epoxy and the core from Flax/Epoxy. This configuration resulted in a unique structure compared to prior composites proposed for similar clinical applications. In order to evaluate the mechanical properties of this hybrid composite, uniaxial tension, compression, three-point bending and Rockwell Hardness tests were conducted. In addition, water absorption tests were performed to investigate the rate of water absorption for the specimens. This study confirms that the proposed hybrid composite plates are significantly more flexible axially compared to conventional metallic plates. Furthermore, they have considerably higher ultimate strength in tension, compression and flexion. Such high strength will ensure good stability of bone-implant construct at the fracture site, immobilize adjacent bone fragments and carry clinical-type forces experienced during daily normal activities. Moreover, this sandwich structure with stronger and stiffer face sheets and more flexible core can result in a higher stiffness and strength in bending compared to tension and compression. These qualities make the proposed hybrid composite an ideal candidate for the design of an optimized fracture fixation system with much closer mechanical properties to human cortical bone.

  18. Fracture channel waves

    NASA Astrophysics Data System (ADS)

    Nihei, Kurt T.; Yi, Weidong; Myer, Larry R.; Cook, Neville G. W.; Schoenberg, Michael

    1999-03-01

    The properties of guided waves which propagate between two parallel fractures are examined. Plane wave analysis is used to obtain a dispersion equation for the velocities of fracture channel waves. Analysis of this equation demonstrates that parallel fractures form an elastic waveguide that supports two symmetric and two antisymmetric dispersive Rayleigh channel waves, each with particle motions and velocities that are sensitive to the normal and tangential stiffnesses of the fractures. These fracture channel waves degenerate to shear waves when the fracture stiffnesses are large, to Rayleigh waves and Rayleigh-Lamb plate waves when the fracture stiffnesses are low, and to fracture interface waves when the fractures are either very closely spaced or widely separated. For intermediate fracture stiffnesses typical of fractured rock masses, fracture channel waves are dispersive and exhibit moderate to strong localization of guided wave energy between the fractures. The existence of these waves is examined using laboratory acoustic measurements on a fractured marble plate. This experiment confirms the distinct particle motion of the fundamental antisymmetric fracture channel wave (A0 mode) and demonstrates the ease with which a fracture channel wave can be generated and detected.

  19. Effect of magnetic configuration on frequency of NBI-driven Alfvén modes in TJ-II

    NASA Astrophysics Data System (ADS)

    Melnikov, A. V.; Ochando, M.; Ascasibar, E.; Castejon, F.; Cappa, A.; Eliseev, L. G.; Hidalgo, C.; Krupnik, L. I.; Lopez-Fraguas, A.; Liniers, M.; Lysenko, S. E.; de Pablos, J. L.; Perfilov, S. V.; Sharapov, S. E.; Spong, D. A.; Jimenez, J. A.; Ufimtsev, M. V.; Breizman, B. N.; HIBP Group; the TJ-II Team

    2014-12-01

    Excitation of modes in the Alfvénic frequency range, 30 kHz < fAE < 300 kHz, was observed in hydrogen plasma heated by hydrogen neutral beam injection (NBI) in the TJ-II heliac. Co-field and counter-field NBI were injected, and the components of the poloidal magnetic field were varied one by one and in combinations, in order to investigate the beam-driven modes over an extended range of the rotational transform values, 1.51<\\unicode{7548} (0)<1.67 . Taking advantage of the unique TJ-II capabilities, a dynamic magnetic configuration experiment with \\unicode{7548} (ρ , t) variation during discharges has shown strong effects on the mode frequency via both vacuum \\unicode{7548} changes and induced net plasma current. A drastic frequency increase from ˜50 to ˜250 kHz was observed for some modes when plasma current as low as ±2 kA was induced by small (10%) changes in the vertical field. A comprehensive set of diagnostics including a heavy ion beam probe, magnetic probes and a multi-chord bolometer made it possible to identify the spatial spread of the modes and deduce the internal amplitudes of their plasma density and magnetic field perturbations. A simple analytical model for fAE, based on the local Alfvén eigenmode (AE) dispersion relation, was proposed to characterize the observation. It was shown that all the observations, including vacuum iota and plasma current variations, may be fitted by the model, so the linear mode frequency dependence on \\unicode{7548} (plasma current) and one over square root density dependence present the major features of the NBI-induced AEs in TJ-II, and provide the framework for further experiment-to-theory comparison.

  20. Saturation of the f -mode instability in neutron stars. II. Applications and results

    NASA Astrophysics Data System (ADS)

    Pnigouras, Pantelis; Kokkotas, Kostas D.

    2016-07-01

    We present the first results on the saturation of the f -mode instability in neutron stars due to nonlinear mode coupling. Emission of gravitational waves drives the f -mode (fundamental mode) unstable in fast-rotating, newborn neutron stars. The initial growth phase of the mode is followed by its saturation, because of energy leaking to other modes of the star. The saturation point determines the strain of the generated gravitational-wave signal, which can then be used to extract information about the neutron star's equation of state. The parent (unstable) mode couples via parametric resonances with pairs of daughter modes, with the triplets' evolution exhibiting a rich variety of behaviors. We study both supernova- and merger-derived neutron stars, simply modeled as polytropes in a Newtonian context, and show that the parent may couple to many different daughter pairs during the star's evolution through the instability window, with the saturation amplitude changing by orders of magnitude.

  1. Spectral estimation of plasma fluctuations. II. Nonstationary analysis of edge localized mode spectra

    SciTech Connect

    Riedel, K.S.; Sidorenko, A. ); Bretz, N. ); Thomson, D.J. )

    1994-03-01

    Several analysis methods for nonstationary fluctuations are described and applied to the edge localized mode (ELM) instabilities of limiter H-mode plasmas. The microwave scattering diagnostic observes poloidal [ital k][sub [theta

  2. Composite materials: Fatigue and fracture. Vol. 3

    NASA Technical Reports Server (NTRS)

    O'Brien, T. K. (Editor)

    1991-01-01

    The present volume discusses topics in the fields of matrix cracking and delamination, interlaminar fracture toughness, delamination analysis, strength and impact characteristics, and fatigue and fracture behavior. Attention is given to cooling rate effects in carbon-reinforced PEEK, the effect of porosity on flange-web corner strength, mode II delamination in toughened composites, the combined effect of matrix cracking and free edge delamination, and a 3D stress analysis of plain weave composites. Also discussed are the compression behavior of composites, damage-based notched-strength modeling, fatigue failure processes in aligned carbon-epoxy laminates, and the thermomechanical fatigue of a quasi-isotropic metal-matrix composite.

  3. Effect of fast electrons on the stability of resistive interchange modes in the TJ-II stellarator

    NASA Astrophysics Data System (ADS)

    García, L.; Ochando, M. A.; Carreras, B. A.; Carralero, D.; Hidalgo, C.; van Milligen, B. Ph.

    2016-06-01

    In this paper, we report on electromagnetic phenomena in low-β plasmas at the TJ-II stellarator, controlled by external heating. To understand the observations qualitatively, we introduce a simple modification of the standard resistive MHD equations, to include the potential impact of fast electrons on instabilities. The dominant instabilities of the modeling regime are resistive interchange modes, and calculations are performed in a configuration with similar characteristics as the TJ-II stellarator. The main effect of the trapping of fast electrons by magnetic islands induced by MHD instabilities is to increase the magnetic component of the fluctuations, changing the character of the instability to tearing-like and modifying the frequency of the modes. These effects seem to be consistent with some of the experimental observations.

  4. ELECTROMAGNETIC FIELD MEASUREMENT OF FUNDAMENTAL AND HIGHER-ORDER MODES FOR 7-CELL CAVITY OF PETRA-II

    SciTech Connect

    Kawashima, Y.; Blednykh, A.; Cupolo, J.; Davidsaver, M.; Holub, B.; Ma, H.; Oliva, J.; Rose, J.; Sikora, R.; Yeddulla, M.

    2011-03-28

    The booster synchrotron for NSLS-II will include a 7-cell PETRA cavity, which was manufactured for the PETRA-II project at DESY. The cavity fundamental frequency operates at 500 MHz. In order to verify the impedances of the fundamental and higher-order modes (HOM), which were calculated by computer code, we measured the magnitude of the electromagnetic field of the fundamental acceleration mode and HOM using the bead-pull method. To keep the cavity body temperature constant, we used a chiller system to supply cooling water at 20 degrees C. The bead-pull measurement was automated with a computer. We encountered some issues during the measurement process due to the difficulty in measuring the electromagnetic field magnitude in a multi-cell cavity. We describe the method and apparatus for the field measurement, and the obtained results.

  5. Effects of proof loads and combined mode loadings on fracture and flaw growth characteristics of aerospace alloys

    NASA Technical Reports Server (NTRS)

    Shah, R. C.

    1974-01-01

    This experimental program was undertaken to determine the effects of (1) combined tensile and bending loadings, (2) combined tensile and shear loadings, and (3) proof overloads on fracture and flaw growth characteristics of aerospace alloys. Tests were performed on four alloys: 2219-T87 aluminum, 5Al-2.5Sn (ELl) titanium, 6Al-4V beta STA titanium and high strength 4340 steel. Tests were conducted in room air, gaseous nitrogen at -200F (144K), liquid nitrogen and liquid hydrogen. Flat center cracked and surface flawed specimens, cracked tube specimens, circumferentially notched round bar and surface flawed cylindrical specimens were tested. The three-dimensional photoelastic technique of stress freezing and slicing was used to determine stress intensity factors for surface flawed cylindrical specimens subjected to tension or torsion. Results showed that proof load/temperature histories used in the tests have a small beneficial effect or no effect on subsequent fracture strength and flaw growth rates.

  6. Asteroseismology of the nearby SN II Progenitor Rigel. II. epsilon-mechanism Triggering Gravity-mode Pulsations?

    NASA Astrophysics Data System (ADS)

    Moravveji, Ehsan; Moya, Andres; Guinan, Edward F.

    2012-04-01

    The cores of luminous B- and A-type (BA) supergiant stars are the seeds of later core-collapse supernovae. Thus, constraining the near-core conditions in this class of stars can place tighter constraints on the size, mass, and chemical composition of supernova remnants. Asteroseismology of these massive stars is one possible approach into such investigations. Recently, Moravveji et al. in 2012 (hereafter Paper I) extracted 19 significant frequencies from a 6-year radial velocity monitoring of Rigel (β Ori, B8 Ia). The periods they determined broadly range from 1.22 to 74.74 days. Based on our differentially rotating stellar structure and evolution model, Rigel, at its current evolutionary state, is undergoing core He burning and shell H burning. Linear fully non-adiabatic non-radial stability analyses result in the excitation of a dense spectrum of non-radial gravity-dominated mixed modes. The fundamental radial mode (l = 0) and its overtones are all stable. When the hydrogen-burning shell is located even partially in the radiative zone, a favorable condition for destabilization of g-modes through the so-called epsilon-mechanism becomes viable. Only those g-modes that have high relative amplitudes in the hydrogen-burning (radiative) zone can survive the strong radiative damping. From the entire observed range of variability periods of Rigel (found in Paper I), and based on our model, only those modes with periods ranging between 21 and 127 days can be theoretically explained by the epsilon-mechanism. The origin of the short-period variations (found in Paper I) still remains unexplained. Because Rigel is similar to other massive BA supergiants, we believe that the epsilon-mechanism may be able to explain the long-period variations in α Cygni class of pulsating stars.

  7. Solar seismology. II - The stochastic excitation of the solar p-modes by turbulent convection

    NASA Technical Reports Server (NTRS)

    Goldreich, P.; Keeley, D. A.

    1977-01-01

    We test the hypothesis that the solar p-modes are stabilized by damping due to turbulent viscosity in the convective zone. Starting from the assumption that the modes are stable, we calculate expectation values for the modal energies. We find that the interaction between a p-mode and the turbulent convection is such that the modal energy tends toward equipartition with the kinetic energy of turbulent eddies whose lifetimes are comparable to the modal period. From the calculated values of the modal energies, we compute rms surface velocity amplitudes. Our predicted rms surface velocities range from 0.01 cm/sec for the fundamental radial mode to 0.6 cm/sec for the radial mode whose period is approximately 5 minutes. The predicted surface velocities for the low order p-modes are much smaller than the velocities inferred from recent observations.

  8. VCD Robustness of the Amide-I and Amide-II Vibrational Modes of Small Peptide Models.

    PubMed

    Góbi, Sándor; Magyarfalvi, Gábor; Tarczay, György

    2015-09-01

    The rotational strengths and the robustness values of amide-I and amide-II vibrational modes of For(AA)n NHMe (where AA is Val, Asn, Asp, or Cys, n = 1-5 for Val and Asn; n = 1 for Asp and Cys) model peptides with α-helix and β-sheet backbone conformations were computed by density functional methods. The robustness results verify empirical rules drawn from experiments and from computed rotational strengths linking amide-I and amide-II patterns in the vibrational circular dichroism (VCD) spectra of peptides with their backbone structures. For peptides with at least three residues (n ≥ 3) these characteristic patterns from coupled amide vibrational modes have robust signatures. For shorter peptide models many vibrational modes are nonrobust, and the robust modes can be dependent on the residues or on their side chain conformations in addition to backbone conformations. These robust VCD bands, however, provide information for the detailed structural analysis of these smaller systems.

  9. Oscillations of a vertically stratified dissipative atmosphere. II. Low frequency trapped modes

    NASA Astrophysics Data System (ADS)

    Rudenko, G. V.; Dmitrienko, I. S.

    2016-05-01

    Trapped atmosphere waves, such as IGW waveguide modes and Lamb modes, are described using dissipative solution above source (DSAS) (Dmitrienko and Rudenko, 2016). According to this description, the modes are disturbances penetrating without limit in the upper atmosphere and dissipating their energy throughout the atmosphere; leakage from a trapping region to the upper atmosphere is taken into consideration. The DSAS results are compared to those based on both accurate and WKB approximated dissipationless equations. It is shown that the spatial and frequency characteristics of modes in the upper atmosphere calculated by any of the methods are close to each other and are in good agreement with the observed characteristics of traveling ionospheric disturbances.

  10. Fracture mechanics; Proceedings of the Seventeenth National Symposium, Albany, NY, August 7-9, 1984

    NASA Technical Reports Server (NTRS)

    Underwood, J. M. (Editor); Chait, R. (Editor); Smith, C. W. (Editor); Wilhem, D. P. (Editor); Andrews, W. A. (Editor); Newman, J. C. (Editor)

    1986-01-01

    The present conference gives attention to topics in the application of fracture mechanics, subcritical crack growth phenomena, fracture testing methods, ductile fracture behavior, and fracture mechanisms and their analysis. Specific papers treat the resistance curve approach to composite materials characterization, fracture toughness in ductile iron and cast steel, hold-time effects in elevated temperature fatigue crack propagation, creep crack growth under nonsteady conditions, viscoplastic fatigue in a superalloy at elevated temperatures, fracture testing with arc bend specimens, one-point bend impact test application, and a compact mode II fracture specimen. Also discussed are the computation of stable crack growth using the J-integral, the use of plastic energy dissipation to characterize crack growth, the extension of surface cracks under cyclic loading, the minimum time criterion for crack instability in structural materials, dynamic crack propagation and branching under biaxial loading, and boundary layer effects in cracked bodies.

  11. Fractures in anisotropic media

    NASA Astrophysics Data System (ADS)

    Shao, Siyi

    Rocks may be composed of layers and contain fracture sets that cause the hydraulic, mechanical and seismic properties of a rock to be anisotropic. Coexisting fractures and layers in rock give rise to competing mechanisms of anisotropy. For example: (1) at low fracture stiffness, apparent shear-wave anisotropy induced by matrix layering can be masked or enhanced by the presence of a fracture, depending on the fracture orientation with respect to layering, and (2) compressional-wave guided modes generated by parallel fractures can also mask the presence of matrix layerings for particular fracture orientations and fracture specific stiffness. This report focuses on two anisotropic sources that are widely encountered in rock engineering: fractures (mechanical discontinuity) and matrix layering (impedance discontinuity), by investigating: (1) matrix property characterization, i.e., to determine elastic constants in anisotropic solids, (2) interface wave behavior in single-fractured anisotropic media, (3) compressional wave guided modes in parallel-fractured anisotropic media (single fracture orientation) and (4) the elastic response of orthogonal fracture networks. Elastic constants of a medium are required to understand and quantify wave propagation in anisotropic media but are affected by fractures and matrix properties. Experimental observations and analytical analysis demonstrate that behaviors of both fracture interface waves and compressional-wave guided modes for fractures in anisotropic media, are affected by fracture specific stiffness (controlled by external stresses), signal frequency and relative orientation between layerings in the matrix and fractures. A fractured layered medium exhibits: (1) fracture-dominated anisotropy when the fractures are weakly coupled; (2) isotropic behavior when fractures delay waves that are usually fast in a layered medium; and (3) matrix-dominated anisotropy when the fractures are closed and no longer delay the signal. The

  12. An engineering treatise on the CARE II dual mode and coverage models

    NASA Technical Reports Server (NTRS)

    1976-01-01

    A mathematical model used to calculate the reliability of any dual-mode, spare-switching computer system was described, and some illustrative examples were presented. The possibility of extending the resultant computer program further was also examined, enabling it, in particular, to accommodate computer configurations involving more than two modes of operation.

  13. Rossby normal modes in nonuniform background configurations. I Simple fields. II - Equinox and solstice conditions

    NASA Technical Reports Server (NTRS)

    Salby, M. L.

    1981-01-01

    An investigation is conducted regarding the influence of mean field variations on the realization of planetary normal modes, taking into account the mode response and structure in the presence of simple background nonuniformities. It is found that mean field variations have the combined effect of depressing, shifting, and broadening the characteristic response of Rossby normal modes. While nonuniformities in both the mean wind and temperature fields contribute to the reduction in peak response, the former are primarily responsible for translation and spectral broadening. An investigation is conducted to determine which modes may be realized in actual atmospheric configurations and which may be identified. For both the equinox and solstice configurations, response peaks corresponding to all of the first four modes of wavenumbers 1, 2, and 3 are readily visible above the noise.

  14. Physiological state, growth mode, and oxidative stress play a role in Cd(II)-mediated inhibition of Nitrosomonas europaea 19718.

    PubMed

    Chandran, Kartik; Love, Nancy G

    2008-04-01

    The goal of this study was to determine the impact of physiological growth states (batch exponential and batch stationary growth) and growth modes (substrate-limited chemostat, substrate-sufficient exponential batch, and substrate-depleted stationary batch growth) on several measures of growth and responses to Cd(II)-mediated inhibition of Nitrosomonas europaea strain 19718. The specific oxygen uptake rate (sOUR) was the most sensitive indicator of inhibition among the different responses analyzed, including total cell abundance, membrane integrity, intracellular 16S rRNA/DNA ratio, and amoA expression. This observation remained true irrespective of the physiological state, the growth mode, or the mode of Cd(II) exposure. Based on the sOUR, a strong time-dependent exacerbation of inhibition (in terms of an inhibition coefficient [K(i)]) in exponential batch cultures was observed. Long-term inhibition levels (based on K(i) estimates) in metabolically active chemostat and exponential batch cultures were also especially severe and comparable. In contrast, the inhibition level in stationary-phase cultures was 10-fold lower and invariable with exposure time. Different strategies for surviving substrate limitation (a 10-fold increase in amoA expression) and starvation (the retention of 16S rRNA levels) in N. europaea cultures were observed. amoA expression was most negatively impacted by Cd(II) exposure in the chemostat cultures, was less impacted in exponential batch cultures, and was least impacted in stationary batch cultures. Although the amoA response was consistent with that of the sOUR, the amoA response was not as strong. The intracellular 16S rRNA/DNA ratio, as determined by fluorescence in situ hybridization, also did not uniformly correlate with the sOUR under conditions of inhibition or no inhibition. Finally, Cd(II)-mediated inhibition of N. europaea was attributed partially to oxidative stress.

  15. Two-mode squeezed light source for quantum illumination and quantum imaging II

    NASA Astrophysics Data System (ADS)

    Masada, Genta

    2016-09-01

    Two-mode squeezed light is a macroscopic quantum entangled state of electro-magnetic fields and shows non-classical correlation between quadrature phase amplitudes in each optical mode. In this work the author is developing a high-quality two-mode squeezed light source for exploring the possibility of a quantum radar system based on a quantum illumination method and also expecting to apply it to quantum imaging. Two-mode squeezed light can be generated by combining two independent single-mode squeezed light beams using a beam splitter with a relative optical phase of 90 degrees between them. In current experimental progress the author developed two sub-threshold optical parametric oscillators to generate single-mode squeezed light beams. In the actual quantum radar or quantum imaging system, a turbulent atmosphere degrades quantum entanglement of a light source and affects performance of target detection. An optical loss is one of the simplest and most probable examples of environmental factors. In this work an evaluation method for quantum entanglement of two-mode squeezed light source is developed with consideration for the optical loss based on Duan's inseparability criteria.

  16. Fracture toughness of silicon

    NASA Technical Reports Server (NTRS)

    Chen, C. P.; Leipold, M. H.

    1980-01-01

    The paper presents a study to determine the fracture toughness and to characterize fracture modes of silicon as a function of the orientation of single-crystal and polycrystalline material. It is shown that bar specimens cracked by Knoop microhardness indentation and tested to fracture under four-point bending at room temperature were used to determine the fracture toughness values. It is found that the lowest fracture toughness value of single crystal silicon was 0.82 MN/m to the 3/2 in the 111 plane type orientation, although the difference in values in the 111, 110, and 100 planes was small.

  17. Tidal interactions of a Maclaurin spheroid - II. Resonant excitation of modes by a close, misaligned orbit

    NASA Astrophysics Data System (ADS)

    Braviner, Harry J.; Ogilvie, Gordon I.

    2015-02-01

    We model a tidally forced star or giant planet as a Maclaurin spheroid, decomposing the motion into the normal modes found by Bryan. We first describe the general prescription for this decomposition and the computation of the tidal power. Although this formalism is very general, forcing due to a companion on a misaligned, circular orbit is used to illustrate the theory. The tidal power is plotted for a variety of orbital radii, misalignment angles, and spheroid rotation rates. Our calculations are carried out including all modes of degree l ≤ 4, and the same degree of gravitational forcing. Remarkably, we find that for close orbits (a/R* ≈ 3) and rotational deformations that are typical of giant planets (e ≈ 0.4) the l = 4 component of the gravitational potential may significantly enhance the dissipation through resonance with surface gravity modes. There are also a large number of resonances with inertial modes, with the tidal power being locally enhanced by up to three orders of magnitude. For very close orbits (a/R* ≈ 3), the contribution to the power from the l = 4 modes is roughly the same magnitude as that due to the l = 3 modes.

  18. Geomechanical Parameters in Fracturing Process of Layered Rocks

    NASA Astrophysics Data System (ADS)

    Mighani, S.; Sondergeld, C. H.; Rai, C. S.

    2013-12-01

    Hydraulic fracturing is crucial to geothermal and hydrocarbon recovery. Predicting performance based on rock characteristics (micro and macro) is essential to effective stimulation. We studied two extreme rock types: 1) Lyons sandstone, a brittle, low porosity, low permeability, weakly anisotropic material and 2) pyrophyllite, a strongly anisotropic metamorphic rock similar chemically and mechanically to shale, having extremely low porosity and permeability. Mineralogy, porosity, permeability, mercury capillary pressure, grain size, μ-CT imaging and elastic anisotropy analysis describe these rocks. Brazilian disk tests were carried to observe the fracture initiation and propagation under tension. Fracture propagation velocity is measured using a high speed digital camera. Strain gauges and acoustic emission (AE) sensors recorded deformation leading to and during failure. SEM imaging and surface profilometry were used to study the post-failure fracture systems and failed surface topology. The fracture process zone (FPZ) is mapped and evaluated using a mosaic of stitched SEM images. The fracture permeability was measured as a function of effective stress and compared to fracture permeability models. The effect of anisotropy on fracturing (Mode I and Mode II fractures) was also investigated rotating the fabric direction of the tested disks relative to the loading axis through increments of 15 degrees. Results indicate differences in fracturing process of these two rock types. Pyrophyllite displays a localized ductile behavior in the process zone resulting in a narrower fracture with a higher propagation velocity and far less AE activity. Pyrophyllite shows 70 % higher tensile strength compared to Lyons sandstone even though it becomes ductile at much lower pressures. The sandstone shows a wide brittle fracture with larger FPZ and better permeability at elevated effective pressures. The greater number of AE activity associated with higher energy events confirms the

  19. Structure of the human angiotensin II type 1 (AT1) receptor bound to angiotensin II from multiple chemoselective photoprobe contacts reveals a unique peptide binding mode.

    PubMed

    Fillion, Dany; Cabana, Jérôme; Guillemette, Gaétan; Leduc, Richard; Lavigne, Pierre; Escher, Emanuel

    2013-03-22

    Breakthroughs in G protein-coupled receptor structure determination based on crystallography have been mainly obtained from receptors occupied in their transmembrane domain core by low molecular weight ligands, and we have only recently begun to elucidate how the extracellular surface of G protein-coupled receptors (GPCRs) allows for the binding of larger peptide molecules. In the present study, we used a unique chemoselective photoaffinity labeling strategy, the methionine proximity assay, to directly identify at physiological conditions a total of 38 discrete ligand/receptor contact residues that form the extracellular peptide-binding site of an activated GPCR, the angiotensin II type 1 receptor. This experimental data set was used in homology modeling to guide the positioning of the angiotensin II (AngII) peptide within several GPCR crystal structure templates. We found that the CXC chemokine receptor type 4 accommodated the results better than the other templates evaluated; ligand/receptor contact residues were spatially grouped into defined interaction clusters with AngII. In the resulting receptor structure, a β-hairpin fold in extracellular loop 2 in conjunction with two extracellular disulfide bridges appeared to open and shape the entrance of the ligand-binding site. The bound AngII adopted a somewhat vertical binding mode, allowing concomitant contacts across the extracellular surface and deep within the transmembrane domain core of the receptor. We propose that such a dualistic nature of GPCR interaction could be well suited for diffusible linear peptide ligands and a common feature of other peptidergic class A GPCRs.

  20. An animal model for open femur fracture and osteomyelitis--Part II: Immunomodulation with systemic IL-12.

    PubMed

    Lindsey, Brock A; Clovis, Nina B; Smith, E Suzanne; Salihu, Sydha; Hubbard, David F

    2010-01-01

    Infection resulting from open fracture is a common problem in orthopedics. The purpose of this project was to study the effect of Interleukin-12 (IL-12) systemic therapy on a previously established open fracture model. One hundred seven male Sprague-Dawley rats were assigned to five groups: (1) normal (baseline), (2) control (controlled for anesthesia), (3) fracture, (4) staph, and (5) staph and IL-12 (SIL). Each group was divided into four time periods: 6, 10, 14, and 21 days after injury and fixation. The operative groups had a standardized femur fracture and fixation using a Kirschner wire as an intramedullary device. The two infection groups (staph and SIL) were inoculated with Staphylococcus aureus following fracture and fixed with an identical technique. The SIL group was treated with systemic IL-12 for a total of 10 doses over 10 days. Significantly decreased serum IL-12 levels were noted at day 10 in the operative groups compared to the normal and control groups. The SIL group showed significantly higher macrophage activation levels and total platelet counts at day 21 compared to all the other groups. The overall infection rate was not changed by IL-12 supplementation; however, bacterial qualitative growth scores were significantly lower in the SIL group at day 10, which corresponded to the lowest level of systemic IL-12 in the fracture group.

  1. Novel fracture technology proves marginal Viking prospect economic, part II: Well clean-up, flowback and testing

    SciTech Connect

    Haidar, S.; Rylance, M.; Tybero, G.

    1996-12-31

    Having completed both fracture treatments as discussed in a companion paper, this paper continues on to describe the post fracture shut-in, clean-up and well testing operations that took place on the Viking Wx exploration well 49/17-12. These operations involved the removal of Resin Coated Proppant (RCP) from the wellbore, via Coiled Tubing (CT), through the use of a specially designed jetting nozzle. The RCP pack stability at a concentration of 3.0 lb/ft{sup 2} (as per planned design) had already been tested in a flowback cell. The use of a Surface Read-Out (SRO) gauge, combined with gas, water and proppant flow rates as well as the viscosity of fracturing fluids returns, enabled real time calculation of the drag forces, on the proppant pack, during clean-up. The flow rate, in the field, was controlled such that the calculated drag forces remained below those observed in the laboratory. Following the clean-up a flow and build-up test was conducted, to evaluate the fracture half length and fracture conductivity, from which a Pseudo-radial skin was calculated. The Non-Darcy effects in the fracture were also evaluated, and finally the short term and long term well deliverabilities were assessed.

  2. Development and Application of Benchmark Examples for Mixed-Mode I/II Quasi-Static Delamination Propagation Predictions

    NASA Technical Reports Server (NTRS)

    Krueger, Ronald

    2012-01-01

    The development of benchmark examples for quasi-static delamination propagation prediction is presented and demonstrated for a commercial code. The examples are based on finite element models of the Mixed-Mode Bending (MMB) specimen. The examples are independent of the analysis software used and allow the assessment of the automated delamination propagation prediction capability in commercial finite element codes based on the virtual crack closure technique (VCCT). First, quasi-static benchmark examples were created for the specimen. Second, starting from an initially straight front, the delamination was allowed to propagate under quasi-static loading. Third, the load-displacement relationship from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. Good agreement between the results obtained from the automated propagation analysis and the benchmark results could be achieved by selecting input parameters that had previously been determined during analyses of mode I Double Cantilever Beam and mode II End Notched Flexure specimens. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Overall the results are encouraging, but further assessment for mixed-mode delamination fatigue onset and growth is required.

  3. Seismic transmission operator reciprocity - II: impedance-operator symmetry via elastic lateral modes

    NASA Astrophysics Data System (ADS)

    Thomson, C. J.

    2015-08-01

    The properties of the overburden transmission response are of particular interest for the analysis of reflectivity illumination or blurring in seismic depth imaging. The first step to showing a transmission-operator reciprocity property is to identify the symmetry of the so-called displacement-to-traction operators. The latter are analogous to Dirichlet-to-Neumann operators and they may also be called impedance operators. Their symmetry is deduced here after development of a formal spectral or modal theory of lateral wavefunctions in a laterally heterogeneous generally anisotropic elastic medium. The elastic lateral modes are displacement-traction 6-vectors and they are built from two auxiliary 3-vector lateral-mode bases. These auxiliary modes arise from Hermitian and anti-Hermitian operators, so they have familiar properties such as orthogonality. There is no assumption of down/up symmetry of the elasticity tensor, but basic assumptions are made about the existence and completeness of the elastic modes. A point-symmetry property appears and plays a central role. The 6-vector elastic modes have a symplectic orthogonality property, which facilitates the development of modal expansions for 6-vector functions of the lateral coordinates when completeness is assumed. While the elastic modal theory is consistent with the laterally homogeneous case, numerical work would provide confidence that it is correct in general. An appendix contains an introductory overview of acoustic lateral modes that were studied by other authors, given from the perspective of this new work. A distinction is drawn between unit normalization of scalar auxiliary modes and a separate energy-flux normalization of 2-vector acoustic modes. Neither is crucial to the form of acoustic pressure-to-velocity or impedance operators. This statement carries over to the elastic case for the 3-vector auxiliary- and 6-vector elastic-mode normalizations. The modal theory is used to construct the kernel of the

  4. [Fracture toughness of cortical bone in tension, shear, and tear--a comparison of longitudinal and transverse fracture].

    PubMed

    Feng, Z

    1997-09-01

    The fracture toughness at crack initiation was determined for bovine cortical bone under tension (mode I), shear (mode II), and tear (mode III). A total of 130 compact tension specimens, compact shear specimens and triple pantleg specimens were used for the measurement of fracture toughness under tension, shear, and tear, respectively. Multiple-sample compliance method was utilized to measure the critical strain energy release rate (Gc) at the a/W = 0.55 (crack length, a, to specimen width, W, ratio). The critical stress intensity factor (Kc) was also calculated from the critical loading (PQ) of the specimens at the a/W = 0.55. The effect of the anisotropy of bone on its resistance to crack initiation under shear and tear loading was investigated as well. The fracture toughness of bone with precrack orientations parallel(designed as longitudinal fracture) to and that with precrack orientations normal (designed as transverse fracture) to the longitudinal axis of bone were compared. In longitudinal fracture, the critical strain energy release rates(Gc) of cortical bone under tension, shear, and tear were 644 +/- 102, 2430 +/- 836, and 1723 +/- 486 N/m, respectively. In transverse fracture, the critical strain energy release rates(Gc) of cortical bone under tesion, shear, and tear were 1374 +/- 183, 4710 +/- 1284, and 4016 +/- 948 N/m, respectively. An analysis of variance demonstrated that the crack initiation fracture toughness of bone under shear and tear loading is significantly greater than that under tensile loading in both longitudinal and transverse fracture. Our results also suggest that cortical bone has been "designed" to prevent crack initiation in transverse fracture under tension, shear, and tesar.

  5. Fracture in the Elderly Multidisciplinary Rehabilitation (FEMuR): a phase II randomised feasibility study of a multidisciplinary rehabilitation package following hip fracture

    PubMed Central

    Williams, Nefyn H; Roberts, Jessica L; Din, Nafees Ud; Totton, Nicola; Charles, Joanna M; Hawkes, Claire A; Morrison, Val; Hoare, Zoe; Williams, Michelle; Pritchard, Aaron W; Alexander, Swapna; Lemmey, Andrew; Woods, Robert T; Sackley, Catherine; Logan, Pip; Edwards, Rhiannon T; Wilkinson, Clare

    2016-01-01

    Objective To conduct a rigorous feasibility study for a future definitive parallel-group randomised controlled trial (RCT) and economic evaluation of an enhanced rehabilitation package for hip fracture. Setting Recruitment from 3 acute hospitals in North Wales. Intervention delivery in the community. Participants Older adults (aged ≥65) who received surgical treatment for hip fracture, lived independently prior to fracture, had mental capacity (assessed by clinical team) and received rehabilitation in the North Wales area. Intervention Remote randomisation to usual care (control) or usual care+enhanced rehabilitation package (intervention), including six additional home-based physiotherapy sessions delivered by a physiotherapist or technical instructor, novel information workbook and goal-setting diary. Primary and secondary outcome measures Primary: Barthel Activities of Daily Living (BADL). Secondary measures included Nottingham Extended Activities of Daily Living scale (NEADL), EQ-5D, ICECAP capability, a suite of self-efficacy, psychosocial and service-use measures and costs. Outcome measures were assessed at baseline and 3-month follow-up by blinded researchers. Results 62 participants were recruited, 61 randomised (control 32; intervention 29) and 49 (79%) completed 3-month follow-up. Minimal differences occurred between the 2 groups for most outcomes, including BADL (adjusted mean difference 0.5). The intervention group showed a medium-sized improvement in the NEADL relative to the control group, with an adjusted mean difference between groups of 3.0 (Cohen's d 0.63), and a trend for greater improvement in self-efficacy and mental health, but with small effect sizes. The mean cost of delivering the intervention was £231 per patient. There was a small relative improvement in quality-adjusted life year in the intervention group. No serious adverse events relating to the intervention were reported. Conclusions The trial methods were feasible in terms of

  6. Characterization and modelling of naturally fractured granites in the Redang Island, Terengganu, Malaysia

    NASA Astrophysics Data System (ADS)

    Abd Kadir, Askury; Rahman, Mohd Razlan Abdul; Chee Meng, Choong; Jamaludin, Fathiyah; Talib, Jasmi Ab

    2015-04-01

    The Redang Island is situated in the east coast of Peninsular Malaysia, in the state of Terengganu. Geologically, it is mainly composed of medium- to coarse-grained biotite-hornblend granite and overlain by sedimentary and metamorphic rocks. The close-spaced fractured pattern gave an indicator for the active tectonic, which create a fractured basement in Anding Utara that situated 200km SE of the study area. The main primary objective is to characterize the fracture orientation, fracture density as well as to create the static DFN model based on the surface outcrops. A systematic and accurate data collection is crucial for a proper statistical analysis of fracture parameters for fracture modeling. A total of five scan-lines at different length was captured to represent the area. The mode I (extension) and mode II (sheared) fractures are identified during the data aquisition. Hence, the maximum stresses (α1) were interpreted from rose diagram and stereoplots, which are trending towards NE-SW and ENE-WSW. The regional stresses obtained is almost identical to FMI data from the Malay Basin (Anding). Hence, this study suggests that the fracture networking are genetically correlated between fractured basement in the Malay Basin and the Redang Island. Therefore, it can become a good analogue for in-depth studies for better understanding of fracture reservoir.

  7. Interlaminar Fracture Toughness of CF/PEI and GF/PEI Composites at Elevated Temperatures

    NASA Astrophysics Data System (ADS)

    Kim, Ki-Young; Ye, Lin; Phoa, Kim-Meng

    2004-05-01

    An experimental study has been conducted to assess temperature effects on mode-I and mode-II interlaminar fracture toughness of carbon fibre/polyetherimide (CF/PEI) and glass fibre/polyetherimide (GF/PEI) thermoplastic composites. Mode-I double cantilever beam (DCB) and mode-II end notched flexure (ENF) tests were carried out in a temperature range from 25 to 130°C. For both composite systems, the initiation toughness, G IC, ini and G IIC, ini, of mode-I and mode-II interlaminar fracture decreased with an increase in temperature, while the propagation toughness, G IC, prop and G IIC, prop, displayed a reverse trend. Three main mechanisms were identified to contribute to the interlaminar fracture toughness, namely matrix deformation, fibre/matrix interfacial failure and fibre bridging during the delamination process. At delamination initiation, the weakened fibre/matrix interface at elevated temperatures plays an overriding role with the delamination growth initiating at the fibre/matrix interface, rather than from a blunt crack tip introduced by the insert film, leading to low values of G IC, ini and G IIC, ini. On the other hand, during delamination propagation, enhanced matrix deformation at elevated temperatures and fibre bridging promoted by weakened fibre/matrix interface result in greater G IC, prop values. Meanwhile enhanced matrix toughness and ductility at elevated temperatures also increase the stability of mode-II crack growth.

  8. SIF-based fracture criterion for interface cracks

    NASA Astrophysics Data System (ADS)

    Ji, Xing

    2016-06-01

    The complex stress intensity factor K governing the stress field of an interface crack tip may be split into two parts, i.e., hat{K} and s^{-iɛ}, so that K=hat{K}s^{-iɛ}, s is a characteristic length and ɛ is the oscillatory index. hat{K} has the same dimension as the classical stress intensity factor and characterizes the interface crack tip field. That means a criterion for interface cracks may be formulated directly with hat{K}, as Irwin (ASME J. Appl. Mech. 24:361-364, 1957) did in 1957 for the classical fracture mechanics. Then, for an interface crack, it is demonstrated that the quasi Mode I and Mode II tip fields can be defined and distinguished from the coupled mode tip fields. Built upon SIF-based fracture criteria for quasi Mode I and Mode II, the stress intensity factor (SIF)-based fracture criterion for mixed mode interface cracks is proposed and validated against existing experimental results.

  9. Single-mode tapered optical fiber loop immunosensor II: assay of anti-cholera toxin immunoglobulins

    NASA Astrophysics Data System (ADS)

    Marks, Robert S.; Hale, Zoe M.; Levine, Myron M.; Lowe, C. R.; Payne, Frank P.

    1994-07-01

    An evanescent wave immunoassay for cholera antitoxin immunoglobulins was performed using a single mode tapered optical fiber loop sensor. The transducer was silanized with 3- glycidoxypropyltrimethoxysilane and chemically modified to link covalently either cholera toxin B subunit or a synthetic peptide derived from it, CTP3. The sensor was exposed to seral fluids, obtained from human volunteers having been exposed to live virulent Vibrio cholerae 01 and shown to produce rice-water stools. Other toxins of interest, such as Clostridium botulinum toxin A, have been tested on similar systems. The bound unlabelled immunoglobulins were then exposed to a mixture of FITC-anti-IgG and TRITC-anti-IgA, without requirement for a separation step. The emanating fluorescent emissions of fluorescein and rhodamine, excited by the input laser light, were coupled back into the guided mode of the tapered fiber, and used to determine the concentrations of the complementary antigens.

  10. Development and Application of Benchmark Examples for Mixed-Mode I/II Quasi-Static Delamination Propagation Predictions

    NASA Technical Reports Server (NTRS)

    Krueger, Ronald

    2012-01-01

    The development of benchmark examples for quasi-static delamination propagation prediction is presented. The example is based on a finite element model of the Mixed-Mode Bending (MMB) specimen for 50% mode II. The benchmarking is demonstrated for Abaqus/Standard, however, the example is independent of the analysis software used and allows the assessment of the automated delamination propagation prediction capability in commercial finite element codes based on the virtual crack closure technique (VCCT). First, a quasi-static benchmark example was created for the specimen. Second, starting from an initially straight front, the delamination was allowed to propagate under quasi-static loading. Third, the load-displacement as well as delamination length versus applied load/displacement relationships from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Overall, the results are encouraging, but further assessment for mixed-mode delamination fatigue onset and growth is required.

  11. Measurements of higher-order mode damping in the PEP-II low-power test cavity

    SciTech Connect

    Rimmer, R.A.; Goldberg, D.A.

    1993-05-01

    The paper describes the results of measurements of the Higher-Order Mode (HOM) spectrum of the low-power test model of the PEP-II RF cavity and the reduction in the Q`s of the modes achieved by the addition of dedicated damping waveguides. All the longitudinal (monopole) and deflecting (dipole) modes below the beam pipe cut-off are identified by comparing their measured frequencies and field distributions with calculations using the URMEL code. Field configurations were determined using a perturbation method with an automated bead positioning system. The loaded Q`s agree well with the calculated values reported previously, and the strongest HOMs are damped by more than three orders of magnitude. This is sufficient to reduce the coupled-bunch growth rates to within the capability of a reasonable feedback system. A high power test cavity will now be built to validate the thermal design at the 150 kW nominal operating level, as described elsewhere at this conference.

  12. Strength, Fracture Toughness, Fatigue, and Standardization Issues of Free-standing Thermal Barrier Coatings

    NASA Technical Reports Server (NTRS)

    Choi, Sung R.; Zhu, Dong-Ming; Miller, Robert A.

    2003-01-01

    Strength, fracture toughness and fatigue behavior of free-standing thick thermal barrier coatings of plasma-sprayed ZrO2-8wt % Y2O3 were determined at ambient and elevated temperatures in an attempt to establish a database for design. Strength, in conjunction with deformation (stress-strain behavior), was evaluated in tension (uniaxial and trans-thickness), compression, and uniaxial and biaxial flexure; fracture toughness was determined in various load conditions including mode I, mode II, and mixed modes I and II; fatigue or slow crack growth behavior was estimated in cyclic tension and dynamic flexure loading. Effect of sintering was quantified through approaches using strength, fracture toughness, and modulus (constitutive relations) measurements. Standardization issues on test methodology also was presented with a special regard to material's unique constitutive relations.

  13. Experimental investigation of CNT effect on curved beam strength and interlaminar fracture toughness of CFRP laminates

    NASA Astrophysics Data System (ADS)

    Arca, M. A.; Coker, D.

    2014-06-01

    High mechanical properties and light weight structures of composite materials and advances in manufacturing processes have increased the use of composite materials in the aerospace and wind energy industries as a primary load carrying structures in complex shapes. However, use of composite materials in complex geometries such as L-shaped laminates creates weakness at the radius which causes delamination. Carbon nanotubes (CNTs) is preferred as a toughening materials in composite matrices due to their high mechanical properties and aspect ratios. However, effect of CNTs on curved beam strength (CBS) is not investigated in literature comprehensively. The objective of this study is to investigate the effect of CNT on Mode I and Mode II fracture toughness and CBS. L-shaped beams are fabric carbon/epoxy composite laminates manufactured by hand layup technique. Curved beam composite laminates were subjected to four point bending loading according to ASTM D6415/D6415M-06a. Double cantilever beam (DCB) tests and end notch flexure (ENF) tests were conducted to determine mode-I and mode-II fracture toughness, respectively. Preliminary results show that 3% CNT addition to the resin increased the mode-I fracture toughness by %25 and mode-II fracture toughness by %10 compared to base laminates. In contrast, no effect on curved beam strength was found.

  14. Nucleosynthesis Modes in the High-Entropy-Wind Scenario of Type II Supernovae

    SciTech Connect

    Farouqi, K.; Kratz, K.-L.; Cowan, J. J.; Mashonkina, L. I.; Pfeiffer, B.; Sneden, C.; Thielemann, F.-K.; Truran, J. W.

    2008-03-11

    In an attempt to constrain the astrophysical conditions for the nucleosynthesis of the classical r-process elements beyond Fe, we have performed large-scale dynamical network calculations within the model of an adiabatically expanding high- entropy wind (HEW) of type II supernovae (SN II). A superposition of several entropy-components (S) with model-inherent weightings results in an excellent reproduction of the overall Solar System (SS) isotopic r-process residuals (N{sub r,{center_dot}}), as well as the more recent observations of elemental abundances of metal-poor, r-process rich halo stars in the early Galaxy. For the heavy r-process elements beyond Sn, our HEW model predicts a robust abundance pattern up to the Th, U r-chronometer region. For the lighter neutron-capture region, an S-dependent superposition of (i) a normal {alpha}-component directly producing stable nuclei, including s-only isotopes, and (ii) a component from a neutron-rich {alpha}-freezeout followed by the rapid recapture of {beta}-delayed neutrons ({beta}dnrpar; emitted from the far-unstable seed nuclei is indicated. In agreement with several recent halo-star observations in the 60

  15. Phase effects in guided mode resonances II: measuring the angular phase of a surface plasmon polariton

    NASA Astrophysics Data System (ADS)

    Theisen, M. J.; Brown, T. G.

    2015-02-01

    We show how the phase of a resonant interaction between a focused beam and a guided mode can be directly observed in a pupil imaging experiment, in which the irradiance leaving the pupil of a standard microscope is relayed to an image sensor through a combination Wollaston prism, calcite beam splitter and polarizer. We apply the method to the observation of a surface plasmon polariton resonance excited in a corrugated silver film fabricated using electron beam lithography. We discuss how this particular imaging configuration could be adapted for applications in plasmonic optical sensing.

  16. Comparison of fracture resistance and failure pattern of endodontically treated premolars with different esthetic onlay systems: An in vitro study

    PubMed Central

    Mynampati, Praffulla; Babu, Mandava Ramesh; Saraswathi, Devabhaktuni Disha; Kumar, Janga Ravi; Gudugunta, Leneena; Gaddam, Divya

    2015-01-01

    Aim: To compare the fracture resistance and modes of failures of three different aesthetic MOD onlays on endodontically treated premolars. Materials and Methods: Forty sound maxillary premolars were selected of which 10 untreated teeth were taken as control (Group I). The other thirty premolars were subjected to standardized MOD onlay preparations and root canal treatments and divided into 3 equal groups. Onlays were prepared in Group II- Indirect composite, Group III- Lithium Disilicate ceramic and Group IV- Full Zirconia. All onlays were cemented using Multilink Automix. All the 40 samples were subjected to fracture resistance testing on Universal testing machine. Also fractured specimens were observed under stereo-microscope for modes of failure. Results: Group IV presented the highest fracture resistance. Groups II and III presented no significant difference in fracture resistance from each other (P > 0.05). Group II and Group III showed significantly lower fracture resistance values than Group I. Coming to modes of failure, only Group IV had showed no cracks in any of the restorations. Conclusion: Full Zirconia MOD onlays increased the fracture resistance of endodontically treated premolars to a significantly higher level than the sound teeth. PMID:25829694

  17. Strain energy release rates of composite interlaminar end-notch and mixed-mode fracture: A sublaminate/ply level analysis and a computer code

    NASA Technical Reports Server (NTRS)

    Valisetty, R. R.; Chamis, C. C.

    1987-01-01

    A computer code is presented for the sublaminate/ply level analysis of composite structures. This code is useful for obtaining stresses in regions affected by delaminations, transverse cracks, and discontinuities related to inherent fabrication anomalies, geometric configurations, and loading conditions. Particular attention is focussed on those layers or groups of layers (sublaminates) which are immediately affected by the inherent flaws. These layers are analyzed as homogeneous bodies in equilibrium and in isolation from the rest of the laminate. The theoretical model used to analyze the individual layers allows the relevant stresses and displacements near discontinuities to be represented in the form of pure exponential-decay-type functions which are selected to eliminate the exponential-precision-related difficulties in sublaminate/ply level analysis. Thus, sublaminate analysis can be conducted without any restriction on the maximum number of layers, delaminations, transverse cracks, or other types of discontinuities. In conjunction with the strain energy release rate (SERR) concept and composite micromechanics, this computational procedure is used to model select cases of end-notch and mixed-mode fracture specimens. The computed stresses are in good agreement with those from a three-dimensional finite element analysis. Also, SERRs compare well with limited available experimental data.

  18. Effect of argon purity on mechanical properties, microstructure and fracture mode of commercially pure (cp) Ti and Ti-6Al-4V alloys for ceramometal dental prostheses.

    PubMed

    Bauer, José; Cella, Suelen; Pinto, Marcelo M; Filho, Leonardo E Rodrigues; Reis, Alessandra; Loguercio, Alessandro D

    2009-12-01

    Provision of an inert gas atmosphere with high-purity argon gas is recommended for preventing titanium castings from contamination although the effects of the level of argon purity on the mechanical properties and the clinical performance of Ti castings have not yet been investigated. The purpose of this study was to evaluate the effect of argon purity on the mechanical properties and microstructure of commercially pure (cp) Ti and Ti-6Al-4V alloys. The castings were made using either high-purity and/or industrial argon gas. The ultimate tensile strength (UTS), proportional limit (PL), elongation (EL) and microhardness (VHN) at different depths were evaluated. The microstructure of the alloys was also revealed and the fracture mode was analyzed by scanning electron microscopy. The data from the mechanical tests and hardness were subjected to a two-and three-way ANOVA and Tukey's test (alpha = 0.05). The mean values of mechanical properties were not affected by the argon gas purity. Higher UTS, PL and VHN, and lower EL were observed for Ti-6Al-4V. The microhardness was not influenced by the argon gas purity. The industrial argon gas can be used to cast cp Ti and Ti-6Al-4V.

  19. Fractional Diffusion Analysis of the Electromagnetic Field In Fractured Media Part II: 2.5-D Approach

    NASA Astrophysics Data System (ADS)

    Ge, J.; Everett, M. E.; Weiss, C. J.

    2012-12-01

    A 2.5D finite difference (FD) frequency-domain modeling algorithm based on the theory of fractional diffusion of electromagnetic (EM) fields generated by a loop source lying above a fractured geological medium is addressed in this paper. The presence of fractures in the subsurface, usually containing highly conductive pore fluids, gives rise to spatially hierarchical flow paths of induced EM eddy currents. The diffusion of EM eddy currents in such formations is anomalous, generalizing the classical Gaussian process described by the conventional Maxwell equations. Based on the continuous time random walk (CTRW) theory, the diffusion of EM eddy currents in a rough medium is governed by the fractional Maxwell equations. Here, we model the EM response of a 2D subsurface containing fractured zones, with a 3D loop source, which results the so-called 2.5D model geometry. The governing equation in the frequency domain is converted using Fourier transform into k domain along the strike direction (along which the model conductivity doesn't vary). The resulting equation system is solved by the multifrontal massively parallel solver (MUMPS). The data obtained is then converted back to spatial domain and the time domain. We find excellent agreement between the FD and analytic solutions for a rough halfspace model. Then FD solutions are calculated for a 2D fault zone model with variable conductivity and roughness. We compare the results with responses from several classical models and explore the relationship between the roughness and the spatial density of the fracture distribution.

  20. Measurement of higher-order mode losses in SPEAR II by shift in synchrotron phase and increase in net cavity power

    SciTech Connect

    Not Available

    1988-01-01

    It has been estimated that the loss to higher-order cavity modes in SPEAR II will be 135 keV per cavity at 100 mA for a 10-cm bunch (sigma/sub z/ = 5 cm). This corresponds to a loss of 10 MeV for a 50-m PEP structure. The power lost to higher modes in each SPEAR II cavity at 100 mA would be 13.5 kW. A loss of this order can be measured by calorimetry. This loss is also large enough to cause a significant increase in the net rf power input into the cavities over the power input with no higher-mode excitation. In addition, the higher-mode loss can also produce a measurable shift in the synchronous phase angle. Numbers for these effects are computed in this paper.

  1. An assessment of BWR (boiling water reactor) Mark-II containment challenges, failure modes, and potential improvements in performance

    SciTech Connect

    Kelly, D.L.; Jones, K.R.; Dallman, R.J. ); Wagner, K.C. )

    1990-07-01

    This report assesses challenges to BWR Mark II containment integrity that could potentially arise from severe accidents. Also assessed are some potential improvements that could prevent core damage or containment failure, or could mitigate the consequences of such failure by reducing the release of fission products to the environment. These challenges and improvements are analyzed via a limited quantitative risk/benefit analysis of a generic BWR/4 reactor with Mark II containment. Point estimate frequencies of the dominant core damage sequences are obtained and simple containment event trees are constructed to evaluate the response of the containment to these severe accident sequences. The resulting containment release modes are then binned into source term release categories, which provide inputs to the consequence analysis. The output of the consequences analysis is used to construct an overall base case risk profile. Potential improvements and sensitivities are evaluated by modifying the event tree spilt fractions, thus generating a revised risk profile. Several important sensitivity cases are examined to evaluate the impact of phenomenological uncertainties on the final results. 75 refs., 25 figs., 65 tabs.

  2. Development and Application of Benchmark Examples for Mode II Static Delamination Propagation and Fatigue Growth Predictions

    NASA Technical Reports Server (NTRS)

    Krueger, Ronald

    2011-01-01

    The development of benchmark examples for static delamination propagation and cyclic delamination onset and growth prediction is presented and demonstrated for a commercial code. The example is based on a finite element model of an End-Notched Flexure (ENF) specimen. The example is independent of the analysis software used and allows the assessment of the automated delamination propagation, onset and growth prediction capabilities in commercial finite element codes based on the virtual crack closure technique (VCCT). First, static benchmark examples were created for the specimen. Second, based on the static results, benchmark examples for cyclic delamination growth were created. Third, the load-displacement relationship from a propagation analysis and the benchmark results were compared, and good agreement could be achieved by selecting the appropriate input parameters. Fourth, starting from an initially straight front, the delamination was allowed to grow under cyclic loading. The number of cycles to delamination onset and the number of cycles during delamination growth for each growth increment were obtained from the automated analysis and compared to the benchmark examples. Again, good agreement between the results obtained from the growth analysis and the benchmark results could be achieved by selecting the appropriate input parameters. The benchmarking procedure proved valuable by highlighting the issues associated with choosing the input parameters of the particular implementation. Selecting the appropriate input parameters, however, was not straightforward and often required an iterative procedure. Overall the results are encouraging, but further assessment for mixed-mode delamination is required.

  3. The ice nucleating ability of pollen:. Part II. Laboratory studies in immersion and contact freezing modes

    NASA Astrophysics Data System (ADS)

    Diehl, K.; Matthias-Maser, S.; Jaenicke, R.; Mitra, S. K.

    Laboratory tests were conducted of the ice nucleating ability of four kinds of pollen in the immersion and the contact freezing modes. The diameters of the selected pollen were between 25 and 70 μm. The experiments were carried out at the Mainz vertical wind tunnel with freely suspended supercooled droplets at temperatures down to -28 °C. The immersion freezing experiments were conducted with drops of radii between 250 and 375 μm formed from distilled water with a defined amount of pollen added. The drops were freely floated in the wind tunnel while being supercooled. For the contact freezing experiments, a short burst of pollen was allowed to collide with freely suspended, supercooled pure water drops of 360-μm radius. The results showed that particle-free water drops in particle-free air in the wind tunnel did not freeze at temperatures above -28 °C while water drops containing pollen froze at temperatures as high as -9 °C, and water drops colliding with pollen froze at temperatures -5 °C and lower. Combined with earlier results about the ice nucleating ability of some bacteria, marine plankton, and leaf litters, the present results confirm the importance of biological aerosol particles as potential ice nuclei at relatively warm temperatures.

  4. Effects of ammonium sulfate aerosols on vegetation—II. Mode of entry and responses of vegetation

    NASA Astrophysics Data System (ADS)

    Gmur, Nicholas F.; Evans, Lance S.; Cunningham, Elizabeth A.

    These experiments were designed to provide information on the rates of aerosol deposition, mode of entry, and effects of deposition of submicrometer ammonium sulfate aerosols on foliage of Phaseolus vulgaris L. A deposition velocity of 3.2 × 10 3cms-1 was constant during 3-week exposures of plants to aerosol concentrations of 26mg m -3 (i.e. about two orders of magnitude above ambient episode concentrations). Mean deposition rate on foliage was 4.1 × 10 -11 μg cm -2s -1. Visible injury symptoms included leaf chlorosis, necrosis and loss of turgor. Chlorosis was most frequent near leaf margins causing epinasty and near major veins. Internal injury occurred initially in spongy mesophyll cells. Eventually abaxial epidermal and palisade parenchyma cells were injured. These results suggest that submicrometer aerosols enter abaxial stomata and affect more internal cells before affecting leaf surface cells. Exposure to aerosols decreased both abaxial and adaxial leaf resistances markedly. Although visible injury to foliage occurred, no changes in dry mass of roots and shoots or leaf area occurred. These results suggest that for the plant developmental stage studied, while leaf resistances decreased and cellular injury occurred in foliage, these factors were not significantly related to plant growth and development.

  5. Transit time instabilities in an inverted fireball. II. Mode jumping and nonlinearities

    SciTech Connect

    Stenzel, R. L.; Gruenwald, J.; Fonda, B.; Ionita, C.; Schrittwieser, R.

    2011-01-15

    A fireball is formed inside a highly transparent spherical grid immersed in a dc discharge plasma. The ambient plasma acts as a cathode and the positively biased grid as an anode. A strong nearly current-free double layer separates the two plasmas. Electrons are accelerated into the fireball, ionize, and establish a discharge plasma with plasma potential near the grid potential. Ions are ejected from the fireball. Since electrons are lost at the same rate as ions, most electrons accelerated into the fireball just pass through it. Thus, the electron distribution contains radially counterstreaming electrons. High-frequency oscillations are excited with rf period given by the electron transit time through the fireball. Since the frequency is well below the electron plasma frequency, no eigenmodes other than a beam space-charge wave exists. The instability is an inertial transit-time instability similar to the sheath-plasma instability or the reflex vircator instability. In contrast to vircators, there is no electron reflection from a space-charge layer but counterstreaming arises from spherical convergence and divergence of electrons. While the basic instability properties have been presented in a companion paper [R. L. Stenzel et al., Phys. Plasmas 18, 012104 (2011)], the present paper focuses on observed mode jumping and nonlinear effects. The former produce frequency jumps and different potential profiles, the latter produce harmonics associated with electron bunching at large amplitudes. In situ probe measurements are presented and interpreted.

  6. FORWARD MODELING OF STANDING KINK MODES IN CORONAL LOOPS. II. APPLICATIONS

    SciTech Connect

    Yuan, Ding; Doorsselaere, Tom Van

    2016-04-15

    Magnetohydrodynamic waves are believed to play a significant role in coronal heating, and could be used for remote diagnostics of solar plasma. Both the heating and diagnostic applications rely on a correct inversion (or backward modeling) of the observables into the thermal and magnetic structures of the plasma. However, due to the limited availability of observables, this is an ill-posed issue. Forward modeling is designed to establish a plausible mapping of plasma structuring into observables. In this study, we set up forward models of standing kink modes in coronal loops and simulate optically thin emissions in the extreme ultraviolet bandpasses, and then adjust plasma parameters and viewing angles to match three events of transverse loop oscillations observed by the Solar Dynamics Observatory/Atmospheric Imaging Assembly. We demonstrate that forward models could be effectively used to identify the oscillation overtone and polarization, to reproduce the general profile of oscillation amplitude and phase, and to predict multiple harmonic periodicities in the associated emission intensity and loop width variation.

  7. Concentration-dependent mode of interaction of angiotensin II receptor blockers with uric acid transporter.

    PubMed

    Iwanaga, Takashi; Sato, Masanobu; Maeda, Tomoji; Ogihara, Toshio; Tamai, Ikumi

    2007-01-01

    Serum uric acid (SUA) is currently recognized as a risk factor for cardiovascular disease. It has been reported that an angiotensin II receptor blocker (ARB), losartan, decreases SUA level, whereas other ARBs, such as candesartan, have no lowering effect. Because the renal uric acid transporter (URAT1) is an important factor controlling the SUA level, we examined the involvement of URAT1 in those differential effects of various ARBs on SUA level at clinically relevant concentrations. This study was done by using URAT1-expressing Xenopus oocytes. Losartan, pratosartan, and telmisartan exhibited cis-inhibitory effects on the uptake of uric acid by URAT1, whereas at higher concentrations, only telmisartan did, and these ARBs reduced the uptake in competitive inhibition kinetics. On the other hand, candesartan, EXP3174 [2-n-butyl-4-chloro-1-[(2'-(1H-tetrazol-5-yl)biphenyl-4-yI)methyl]imidazole-5-carboxylic acid] (a major metabolite of losartan), olmesartan, and valsartan were not inhibitory. Preloading of those ARBs in the oocytes enhanced the URAT1-mediated uric acid uptake, showing a trans-stimulatory effect. The present study is a first demonstration of the differential effects of ARBs on URAT1 that some ARBs are both cis-inhibitory and trans-stimulatory, depending on concentration, whereas others exhibit either a trans-stimulatory or cis-inhibitory effect alone, which could explain the clinically observed differential effects of ARBs on SUA level. Furthermore, it was found that such differential effects of ARBs on URAT1 could be predicted from the partial chemical structures of ARBs, which will be useful information for the appropriate use and development of ARBs without an increase of SUA.

  8. Crack Extension in Hydraulic Fracturing of Shale Cores Using Viscous Oil, Water, and Liquid Carbon Dioxide

    NASA Astrophysics Data System (ADS)

    Bennour, Ziad; Ishida, Tsuyoshi; Nagaya, Yuya; Chen, Youqing; Nara, Yoshitaka; Chen, Qu; Sekine, Kotaro; Nagano, Yu

    2015-07-01

    We performed hydraulic fracturing experiments on cylindrical cores of anisotropic shale obtained by drilling normal to the sedimentary plane. Experiments were conducted under ambient condition and uniaxial stresses, using three types of fracturing fluid: viscous oil, water, and liquid carbon dioxide (L-CO2). In the experiments using water and oil, cracks extended along the loading direction normal to the sedimentary plane under the uniaxial loading and extended along the sedimentary plane without loading. These results suggest that the direction of crack extension is strongly affected by in situ stress conditions. Fluorescent microscopy revealed that hydraulic fracturing with viscous oil produced linear cracks with few branches, whereas that with water produced cracks with many branches inclining from the loading axis. Statistical analysis of P wave polarity of acoustic emission waveforms showed that viscous oil tended to induce Mode I fracture, whereas both water and L-CO2 tended to induce Mode II fracture. Crack extension upon injection of L-CO2 was independent of loading condition unlike extension for the other two fluids. This result seemed attributable to the low viscosity of L-CO2 and was consistent with previous observations for granite specimens that low-viscosity fluids like CO2 tend to induce widely extending cracks with many branches, with Mode II fractures being dominant. These features are more advantageous for shale gas production than those induced by injection of conventional slick water.

  9. Anterior single odontoid screw placement for type II odontoid fractures: our modified surgical technique and initial results in a cohort study of 15 patients

    PubMed Central

    Munakomi, Sunil; Tamrakar, Karuna; Chaudhary, Pramod Kumar; Bhattarai, Binod

    2016-01-01

    Objective: Anterior odontoid screw fixation for type II odontoid fracture is the ideal management option. However in the context of unavailability of an O-arm or neuro-navigation and poor images from the available C-arm may be an obstacle to ideal trajectory and placement of the odontoid screw. We herein detail  our surgical technique so as to ensure a correct trajectory and subsequent good fusion in Type II odontoid fractures. This may be advantageous  in clinical set ups lacking state of the art facilities.  Methods and Results: In this cohort study we included 15 consecutive patients who underwent anterior odontoid screw placement. We routinely dissect the longus colli to completely visualize the entire width of C3 body. We then perform a median C2-C3 disectomy followed by creating a gutter in the superior end of C3 body. We then guide the Kirchsner (K) wire purchasing adequate anterior cortex of C2. Rest of the procedure follows the similar steps as described for odontoid screw placement. We achieved 100% correct trajectory and screw placement in our study. There were no instances of screw break out, pull out or nonunion. There was one patient mortality following myocardial infarction in our study. Conclusion: Preoperative imaging details, proper patient positioning, meticulous dissection, thorough anatomical knowledge and few added surgical nuances are the cornerstones in ideal odontoid screw placement. This may be pivotal in managing  patients in developing nations having rudimentary neurosurgical set up. PMID:27990259

  10. Preoperative posterior tilt of at least 20° increased the risk of fixation failure in Garden-I and -II femoral neck fractures

    PubMed Central

    Dolatowski, Filip C; Adampour, Mina; Frihagen, Frede; Stavem, Knut; Erik Utvåg, Stein; Hoelsbrekken, Sigurd Erik

    2016-01-01

    Background and purpose It has been suggested that preoperative posterior tilt of the femoral head may increase the risk of fixation failure in Garden-I and -II femoral neck fractures. To investigate this association, we studied a cohort of 322 such patients. Patients and methods Patients treated with internal fixation between 2005 and 2012 were retrospectively identified using hospital records and the digital image bank. 2 raters measured the preoperative posterior tilt angle and categorized it into 3 groups: < 10°, 10–20°, and ≥ 20°. The inter-rater reliability (IRR) was determined. Patients were observed until September 2013 (with a minimum follow-up of 18 months) or until failure of fixation necessitating salvage arthroplasty. The risk of fixation failure was assessed using competing-risk regression analysis, adjusting for time to surgery. Results Patients with a posterior tilt of ≥ 20° had a higher risk of fixation failure: 19% (8/43) as compared to 11% (14/127) in the 10–20° category and 6% (9/152) in the < 10° category (p = 0.03). Posterior tilt of ≥ 20° increased the risk of fixation failure, with an adjusted hazard ratio of 3.4 (95% CI: 1.3–8.9; p = 0.01). The interclass correlation coefficient for angular measurements of posterior tilt was 0.90 (95% CI: 0.87–0.92), and the IRR for the categorization of posterior tilt into 3 groups was 0.76 (95% CI: 0.69–0.81). Interpretation Preoperative posterior tilt of ≥ 20° in Garden-I and -II femoral neck fractures increased the risk of fixation failure necessitating salvage arthroplasty. The reliability of the methods that we used to measure posterior tilt ranged from good to excellent. PMID:26937557

  11. Size effect law and fracture mechanics of the triggering of dry snow slab avalanches

    NASA Astrophysics Data System (ADS)

    Bažant, ZdeněK. P.; Zi, Goangseup; McClung, David

    2003-02-01

    A size effect law for fracture triggering in dry snow slabs of high enough length-to-thickness ratio is formulated, based on simplified one-dimensional analysis by equivalent linear elastic fracture mechanics. Viscoelastic effects during fracture are neglected. The derived law, which is analogous to Bažant's energetic size effect law developed for concrete and later for sea ice, fiber composites, rocks, and ceramics, is shown to agree with two-dimensional finite element analysis of mode II cohesive crack model with a finite residual shear stress. Fitting the proposed size effect law to fracture data for various slab thicknesses permits identifying the material fracture parameters. The value of preexisting shear stress in a thin weak zone of finite length is shown to have significant effect. There exists a certain critical snow depth, depending on the preexisting stress value, below which the size effect disappears. Practical applications require considering that the material properties (particularly the mode II fracture toughness or fracture energy) at the snow slab base are not constant but depend strongly on the slab thickness. This means that one must distinguish the material size effect from the structural size effect, and the combined size effect law must be obtained by introducing into the structural size effect law dependence of its parameters on snow thickness. The thickness dependence of these parameters can be obtained by matching the combined law to avalanche observations. Matching Perla's field data on 116 avalanches suggests that the mode II fracture toughness is approximately proportional to 1.8 power of snow thickness.

  12. Investigation of Explosively Driven Fragmentation of Metals - Two Dimensional Fracture and Fragmentation of Metal Shells: Progress Report II

    SciTech Connect

    Grady, D

    2003-02-01

    High explosive enclosed by a metal case qualitatively describes an essential component of high energy systems of importance to the Department of Energy. Detonation of the high explosive causes intense transient pressure loading of the metal following arrival of normal or obliquely incident explosive detonation wave. Subsequent expansion and deformation of the metal case leads to eventual rupture and the opening of fractures and fissures. Details of the rupture process are critical to performance of the system. Consequently, it is essential that the material and kinematic issues governing the processes of dynamic loading and subsequent failure of an explosive-metal case component within a functioning system be adequately understood. Among the reasons are to quantify existing performance, characterize potential degradation of performance resulting from system aging, and optimizing or maintaining system performance through implementation of structural or material changes. The physical and engineering issues underlying this dynamic response and failure phenomena are not adequately understood. The purpose of the present program is to identify the key issues and develop theoretical, computational and experimental models needed to achieve a satisfactory theoretical and analysis framework for analysis of metal case failure in the explosive environment. Specific tasks within the present program include: (1) Models and theories currently being pursued based on physical principles of both the statistical fragmentation concepts of Mott and the energy-based concept of others show promise of providing the analytic and computational methodology capable of predicting explosion-induced fracture and fragmentation of metal components. Experimental studies initiated in the earlier effort offer promise to provide critical test data for validation. The present task shall involve the further refinement and development of the dynamic failure and fragmentation models and theories, and the

  13. Multiaxial loading fracture of A1/sub 2/O/sub 3/ tubes: II. Weibull theory and analysis

    SciTech Connect

    Petrovic, J.J.; Stout, M.G.

    1984-01-01

    The Weibull statistical fracture theory for multiaxial loading was developed for thick- and thin-walled tube geometries subjected to multiaxial loading in tension-internal pressure, compression-internal pressure, and pure torsion. As compared to uniaxial tension, lower strengths are predicted for tension-tension stress states and higher strengths for tension-compression stress states. Comparison to experimental results for A1/sub 2/O/sub 3/ tubes indicates a reasonable agreement with Weibull theory predictions for tension-internal pressure and compression-internal pressure conditions, but an underestimation of stress state effects in pure torsion. Results indicate a weakening effect of in-flaw-plane tensile stresses, with no observed influence of in-plane compressive stresses.

  14. Analytic modeling of instabilities driven by higher-order modes in the HLS II RF system with a higher-harmonic cavity

    NASA Astrophysics Data System (ADS)

    Zhao, Yu-Ning; Li, Wei-Min; Wu, Cong-Feng; Wang, Lin

    2013-08-01

    The utility of a passive fourth-harmonic cavity plays a key role in suppressing longitudinal beam instabilities in the electron storage ring and lengthens the bunch by a factor of 2.6 for the phase II project of the Hefei Light Source (HLS II). Meanwhile, instabilities driven by higher-order modes (HOM) may limit the performance of the higher-harmonic cavity. In this paper, the parasitic coupled-bunch instability, which is driven by narrow band parasitic modes, and the microwave instability, which is driven by broadband HOM, are both modeled analytically. The analytic modeling results are in good agreement with those of our previous simulation study and indicate that the passive fourth-harmonic cavity suppresses parasitic coupled-bunch instabilities and microwave instability. The modeling suggests that a fourth-harmonic cavity may be successfully used at the HLS II.

  15. Progressive Fracture of Composite Structures

    NASA Technical Reports Server (NTRS)

    Chamis, Christos C.; Minnetyan, Levon

    2008-01-01

    A new approach is described for evaluating fracture in composite structures. This approach is independent of classical fracture mechanics parameters like fracture toughness. It relies on computational simulation and is programmed in a stand-alone integrated computer code. It is multiscale, multifunctional because it includes composite mechanics for the composite behavior and finite element analysis for predicting the structural response. It contains seven modules; layered composite mechanics (micro, macro, laminate), finite element, updating scheme, local fracture, global fracture, stress based failure modes, and fracture progression. The computer code is called CODSTRAN (Composite Durability Structural ANalysis). It is used in the present paper to evaluate the global fracture of four composite shell problems and one composite built-up structure. Results show that the composite shells and the built-up composite structure global fracture are enhanced when internal pressure is combined with shear loads.

  16. Shoulder Fractures

    MedlinePlus

    ... Journal of Hand Surgery (JHS) Home Anatomy Shoulder Fractures Email to a friend * required fields From * To * ... create difficulty with its function. Types of Shoulder Fractures The type of fracture varies by age. Most ...

  17. Stress Fractures

    MedlinePlus

    Stress fractures Overview By Mayo Clinic Staff Stress fractures are tiny cracks in a bone. They're caused by ... up and down or running long distances. Stress fractures can also arise from normal use of a ...

  18. Greenstick Fractures

    MedlinePlus

    Greenstick fractures Overview By Mayo Clinic Staff A greenstick fracture occurs when a bone bends and cracks, instead of breaking completely into separate pieces. The fracture looks similar to what happens when you try ...

  19. Viscoelastic-damage interface model formulation with friction to simulate the delamination growth in mode II shear

    NASA Astrophysics Data System (ADS)

    Goodarzi, Mohammad Saeed; Hosseini-Toudeshky, Hossein

    2017-02-01

    In this paper a formulation of a viscoelastic-damage interface model with friction in mode-II is presented. The cohesive constitutive law contains elastic and damage regimes. It has been assumed that the shear stress in the elastic regime follows the viscoelastic properties of the matrix material. The three element Voigt model has been used for the formulation of relaxation modulus of the material. Damage evolution proceeds according to the bilinear cohesive constitutive law combined with friction stress consideration. Combination of damage and friction is based on the presumption that the damaged area, related to an integration point, can be dismembered into the un-cracked area with the cohesive damage and cracked area with friction. Samples of a one element model have been presented to see the effect of parameters on the cohesive constitutive law. A comparison between the predicted results with available results of end-notched flexure specimens in the literature is also presented to verify the model. Transverse crack tension specimens are also simulated for different applied displacement velocities.

  20. 3D-RISM-MP2 Approach to Hydration Structure of Pt(II) and Pd(II) Complexes: Unusual H-Ahead Mode vs Usual O-Ahead One.

    PubMed

    Aono, Shinji; Mori, Toshifumi; Sakaki, Shigeyoshi

    2016-03-08

    Solvation of transition metal complexes with water has been one of the fundamental topics in physical and coordination chemistry. In particular, Pt(II) complexes have recently attracted considerable interest for their relation to anticancer activity in cisplatin and its analogues, yet the interaction of the water molecule and the metal center has been obscured. The challenge from a theoretical perspective remains that both the microscopic solvation effect and the dynamical electron correlation (DEC) effect have to be treated simultaneously in a reasonable manner. In this work we derive the analytical gradient for the three-dimensional reference interaction site model Møller-Plesset second order (3D-RISM-MP2) free energy. On the basis of the three-regions 3D-RISM self-consistent field (SCF) method recently proposed by us, we apply a new layer of the Z-vector method to the CP-RISM equation as well as point-charge approximation to the derivatives with respect to the density matrix elements in the RISM-CPHF equation to remarkably reduce the computational cost. This method is applied to study the interaction of H2O with the d(8) square planar transition metal complexes in aqueous solution, trans-[Pt(II)Cl2(NH3)(glycine)] (1a), [Pt(II)(NH3)4](2+) (1b), [Pt(II)(CN)4](2-) (1c), and their Pd(II) analogues 2a, 2b, and 2c, respectively, to elucidate whether the usual H2O interaction through O atom (O-ahead mode) or unusual one through H atom (H-ahead mode) is stable in these complexes. We find that the interaction energy of the coordinating water and the transition metal complex changes little when switching from gas to aqueous phase, but the solvation free energy differs remarkably between the two interaction modes, thereby affecting the relative stability of the H-ahead and O-ahead modes. Particularly, in contrast to the expectation that the O-ahead mode is preferred due to the presence of positive charges in 1b, the H-ahead mode is also found to be more stable. The O

  1. Surface enhanced Raman scattering, natural bond orbitals and Mulliken atomic charge distribution in the normal modes of diethyldithiocarbamate cadmium (II) complex, [Cd(DDTC)2

    NASA Astrophysics Data System (ADS)

    Téllez Soto, C. A.; Costa, A. C.; Versiane, O.; Lemma, T.; Machado, N. C. F.; Mondragón, M. A.; Martin, A. A.

    2015-07-01

    Theoretical and experimental bands have been assigned to the Fourier Transform Infrared (FT-IR) and FT-Raman spectra of the bis(diethyldithiocarbamate)Cd(II) complex, abbreviated as ([Cd(DDTC)2]). The calculations and spectral interpretation have been based on the DFT/B3LYP method, infrared and Raman second derivative spectra, and band deconvolution analysis to assist in the assignment of observed fundamentals. This study validated the unusual pseudo tetrahedral molecular structure formed around the Cd(II) cation. Surface-enhanced Raman scattering (SERS) was used to determine the interactions of the normal-modes of the diethyldithiocarbamate cadmium (II) complex on nano-structured silver surfaces. Natural bond orbital (NBO) analysis was also carried out to study the Cd(II) hybridization causing the pseudo tetrahedral geometry of the framework of the [Cd(DDTC)2] complex, and to confirm the charge transfer mechanisms through second order perturbation theory analysis of the Fox Matrix. In order to find out the electronic dispersion of the Mulliken atomic charges (MAC) in the normal modes, we calculated the MAC for each normal mode and correlated these values with the SERS effect. Experimental UV-Vis spectra were obtained and charge transfer bands were assigned. Good agreement between the calculated and experimental values for the vibrational and UV-Vis spectra was obtained.

  2. Binding mode and thermodynamic studies on the interaction of the anticancer drug dacarbazine and dacarbazine-Cu(II) complex with single and double stranded DNA.

    PubMed

    Temerk, Yassien; Ibrahim, Hossieny

    2014-07-01

    The binding mode and thermodynamic characteristics of the anticancer drug dacarbazine (Dac) with double and single stranded DNA were investigated in the absence and presence of Cu(II) using cyclic voltammetry, square wave voltammetry and fluorescence spectroscopy. The interaction of Dac and Dac-Cu(II) complex with dsDNA indicated their intercalation into the base stacking domain of dsDNA double helix and the strength of interaction is independent on the ionic strength. The interaction of Dac with dsDNA in the presence of Cu(II) leads to a much stronger intercalation. The interaction mode of Dac molecules with ssDNA is electrostatic attraction via negative phosphate on the exterior of the ssDNA with Dac. The binding constants, stoichiometric coefficients and thermodynamic parameters of Dac and Dac-Cu(II) complex with dsDNA and ssDNA were evaluated. Comparison of the mode interaction of Dac with dsDNA and ssDNA was discussed. The decrease of peak current of Dac was proportional to DNA concentration, which was applied for determination of dsDNA and ssDNA concentration.

  3. Mathematical and numerical analysis of non-planer static mode-II crack in a two-layered medium

    NASA Astrophysics Data System (ADS)

    Hirano, S.; Yamashita, T.

    2009-12-01

    A crack in an infinite homogeneous medium is widely assumed as a model for earthquake fault. It is, however, well known that the earth's crust is heterogeneous and its structure is approximated well by a layered medium. Hence, such structure should be taken into account to model earthquake fault reasonably. We mathematically analyze the behavior of a 2-D static mode-II non-planar crack in a two-layered elastic medium in order to understand the effect of layer boundary on earthquake faulting. Although Rani and Singh (1993) and Rivalta et al.(2002) studied similar problems, focuses of their studies were quite narrow probably because of inherent mathematical difficulty. Actually the former assumed a planar crack with uniform slip and the latter assumed a planar crack perpendicular to the layer boundary. While a serious difficulty of the analysis of mode-II crack lies in the derivation of stress distribution due to point source as a kernel function, we first overcome the difficulty by writing its expression in a sequence of complex functions in the real (not the Fourier) domain. A very important characteristic in the sequence is that it has recursive property, which makes possible to derive the kernel function explicitly and to integrate it by parts; the integration by parts is required before the boundary integral equation method (BIEM) is applied. Our kernel function is much easier to treat than the expression given by Rani and Singh (1993). This enables us to analyze arbitrarily oriented non-planar crack in a two-layered medium. Next, we calculate the spatial distribution of stress due to crack that does not intersect the layer boundary using the above derived kernel function. We find in the calculation that the existence of layer boundary amplifies or reduces the stress at the crack tip when the crack is located close to the boundary; the stress is amplified when the crack exists in the layer with lower rigidity. Our method of analysis can easily be applied to the

  4. Crustal magnetization and accretion at the Southwest Indian Ridge near the Atlantis II fracture zone, 0-25 Ma

    USGS Publications Warehouse

    Hosford, A.; Tivey, M.; Matsumoto, T.; Dick, H.; Schouten, Hans; Kinoshita, H.

    2003-01-01

    We analyze geophysical data that extend from 0 to 25-Myr-old seafloor on both flanks of the Southwest Indian Ridge (SWIR). Lineated marine magnetic anomalies are consistent and identifiable within the study area, even over seafloor lacking a basaltic upper crust. The full spreading rate of 14 km/Myr has remained nearly constant since at least 20 Ma, but crustal accretion has been highly asymmetric, with half rates of 8.5 and 5.5 km/Myr on the Antarctic and African flanks, respectively. This asymmetry may be unique to a ???400 km wide corridor between large-offset fracture zones of the SWIR. In contrast to the Mid-Atlantic Ridge, crustal magnetization amplitudes correlate directly with seafloor topography along the present-day rift valleys. This pattern appears to be primarily a function of along-axis variations in crustal thickness, rather than magnetic mineralogy. Off-axis, magnetization amplitudes at paleo-segment ends are more positive than at paleo-segment midpoints, suggesting the presence of an induced component of magnetization within the lower crust or serpentinized upper mantle. Alteration of the magnetic source layer at paleo-segment midpoints reduces magnetization amplitudes by 70-80% within 20 Myr of accretion. Magnetic and Ocean Drilling Program (ODP) Hole 735B data suggest that the lower crust cooled quickly enough to lock in a primary thermoremanent magnetization that is in phase with that of the overlying upper crust. Thus magnetic polarity boundaries within the intrusive lower crust may be steeper than envisioned in prior models of ocean crustal magnetization. As the crust ages, the lower crust becomes increasingly important in preserving marine magnetic stripes.

  5. DAMPING THE HIGH ORDER MODES IN THE PUMPING CHAMBER OF THE PEP-II LOW ENERGY RING

    SciTech Connect

    Novokhatski, A

    2004-06-30

    The Low Energy Ring of the PEP-II B-factory operates with extremely high currents of short positron bunches. Any discontinuity in the vacuum chamber can excite a broad-band spectrum of high order modes (HOM). A temperature rise has been found in the vacuum chamber elements in one junction of straight and arc chambers. The power in the wake fields was high enough to char beyond use the feed-through for the titanium sublimation pump (TSP). This pumping section is 5.5 m long and consists of the beam chamber and an ante-chamber. Electromagnetic fields, excited in the beam chamber penetrate to the ante-chamber and then through the heater feed-through come out. To be sure that these electromagnetic fields are present a small ceramic tile with a high loss tangent was placed near the TSP feed-through outside of the pumping chamber. A thermocouple that was attached to this tile showed a strong temperature rise. A short wire antenna was also placed there. The antenna was connected directly to a spectrum analyzer. Measurements show a wide frequency HOM spectrum with a maximum in the 2-3 GHz region. Based on these measurements a special water cooled HOM absorber was designed and installed in the vacuum chamber. As a result, the HOM power in the section decreased and the temperature rise went down. The power loss in the absorber reaches 1200 W for a positron beam current of 2.4 A. The absorber helped to find the source of HOM. Steering the beam on the vertical collimators upstream of the absorber resulted in the significant HOM power change in the absorber.

  6. Near infra-red emission from a mer-Ru(II) complex: consequences of strong σ-donation from a neutral, flexible ligand with dual binding modes.

    PubMed

    Pal, Amlan K; Zaccheroni, Nelsi; Campagna, Sebastiano; Hanan, Garry S

    2014-07-04

    A rare example of dual coordination modes by a novel tridentate ligand gives rise to unique fac-and mer-Ru((II/III)) complexes. The mer-Ru(II)-complex displays the farthest red-shift of a triplet metal-to-ligand charge transfer ((3)MLCT) emission with a tridentate ligand for a mononuclear complex. This observation is a consequence of large bite angle and strong σ-donation by the ligand, the combined effect of which helps to separate the energy of the (3)MLCT and (3)MC states.

  7. The fracture behaviour of dental enamel.

    PubMed

    Bechtle, Sabine; Habelitz, Stefan; Klocke, Arndt; Fett, Theo; Schneider, Gerold A

    2010-01-01

    Enamel is the hardest tissue in the human body covering the crowns of teeth. Whereas the underlying dental material dentin is very well characterized in terms of mechanical and fracture properties, available data for enamel are quite limited and are apart from the most recent investigation mainly based on indentation studies. Within the current study, stable crack-growth experiments in bovine enamel have been performed, to measure fracture resistance curves for enamel. Single edge notched bending specimens (SENB) prepared out of bovine incisors were tested in 3-point bending and subsequently analysed using optical and environmental scanning electron microscopy. Cracks propagated primarily within the protein-rich rod sheaths and crack propagation occurred under an inclined angle to initial notch direction not only due to enamel rod and hydroxyapatite crystallite orientation but potentially also due to protein shearing. Determined mode I fracture resistance curves ranged from 0.8-1.5 MPa*m(1/2) at the beginning of crack propagation up to 4.4 MPa*m(1/2) at 500 microm crack extension; corresponding mode II values ranged from 0.3 to 1.5 MPa*m(1/2).

  8. Fracture Mechanisms of Layer-By-Layer Polyurethane/Poly(Acrylic Acid) Nanocomposite

    NASA Astrophysics Data System (ADS)

    Kheng, Eugene R.

    A layer-by-layer(LBL) manufactured material is examined in detail in this thesis. Improvements are made to the method of its manufacture. Efforts are made to understand its fracture mechanisms and take advantage of these fracture mechanisms in the absorption of impact energy. A novel series of experiments has been performed on LBL manufactured thin films to demonstrate their unique fracture mechanisms. Polyurethane/Poly(Acrylic Acid) (PU/PAA) and PU/PAA/(PU/Clay)5 nanocomposite films readily undergo Interlaminar mode II fracture, because of the relatively weak elctrostatic bonds between monolayers. Tensile tests performed while under observation by a scanning electron microscope demonstrate the tendency of these nanocomposite films to undergo interlaminar mode II fracture even when loads are applied in the plane of nanocomposite film. It is concluded that these mechanisms of energy dissipation are responsible for the enhanced toughness of these films when used as layers between glass blocks in the prevention of impact damage to the glass. A novel automated manufacturing facility has been designed and built to deposit large sheets of Layer-by-Layer nanocomposite film. These large sheets are incorporated into a borosillicate glass composite in order to compare the ballistic characteristics of LBL PU based nanocomposite films to a single cast layer of polyurethane. It is demonstrated that shear fracture is the mode of failure in the blocks containing the nanocomposite film. The shear fracture surface in the nanocomposite after it has undergone a ballistic impact is characterized. Additional experiments are performed to characterize the interlaminar fracture stresses and toughnesses of the nanocomposite LBL layers, to assist in the implementation of a numerical crack band model that describes the nanocomposite film. The computational model predicts the failure of the ballistic nanocomposite samples, and the predicted V50 velocity is found to be in good agreement with

  9. Rock fracture processes in chemically reactive environments

    NASA Astrophysics Data System (ADS)

    Eichhubl, P.

    2015-12-01

    Rock fracture is traditionally viewed as a brittle process involving damage nucleation and growth in a zone ahead of a larger fracture, resulting in fracture propagation once a threshold loading stress is exceeded. It is now increasingly recognized that coupled chemical-mechanical processes influence fracture growth in wide range of subsurface conditions that include igneous, metamorphic, and geothermal systems, and diagenetically reactive sedimentary systems with possible applications to hydrocarbon extraction and CO2 sequestration. Fracture processes aided or driven by chemical change can affect the onset of fracture, fracture shape and branching characteristics, and fracture network geometry, thus influencing mechanical strength and flow properties of rock systems. We are investigating two fundamental modes of chemical-mechanical interactions associated with fracture growth: 1. Fracture propagation may be aided by chemical dissolution or hydration reactions at the fracture tip allowing fracture propagation under subcritical stress loading conditions. We are evaluating effects of environmental conditions on critical (fracture toughness KIc) and subcritical (subcritical index) fracture properties using double torsion fracture mechanics tests on shale and sandstone. Depending on rock composition, the presence of reactive aqueous fluids can increase or decrease KIc and/or subcritical index. 2. Fracture may be concurrent with distributed dissolution-precipitation reactions in the hostrock beyond the immediate vicinity of the fracture tip. Reconstructing the fracture opening history recorded in crack-seal fracture cement of deeply buried sandstone we find that fracture length growth and fracture opening can be decoupled, with a phase of initial length growth followed by a phase of dominant fracture opening. This suggests that mechanical crack-tip failure processes, possibly aided by chemical crack-tip weakening, and distributed

  10. Crack path determination for non-proportional mixed-mode fatigue

    NASA Astrophysics Data System (ADS)

    Highsmith, Shelby, Jr.

    Turbine engine components such as fan and compressor blades experience complex combinations of steady and vibratory loads that lead to in-service cracking in directions that cannot be predicted by current fracture criteria. Accurate crack path predictions are required in order to characterize the risk and extent of damage resulting from liberation of a fractured ligament from rotating components. Under proportional in-phase mixed Mode I/Mode II loading conditions, crack growth direction has been observed in some materials to shift from tensile-dominated Mode I to shear-dominated Mode II or mixed-mode crack growth at higher proportions of initial Mode II loading, but non-proportional loads are not well-characterized. An extensive database of crack growth direction under non-proportional 2-D mixed-mode loading conditions is required to expand crack path prediction models, which are likely to vary between alloys. An approach based on linear elastic fracture mechanics (LEFM) is desired in order to implement the model in crack growth software such as the boundary element-based fracture analysis package FRANC3D. A novel specimen configuration has been designed and analyzed for generation of wide ranges of mixed-mode loading conditions in a single test. This specimen and a more conventional thin-walled tubular specimen have been used to test polycrystalline nickel-base superalloy Inconel 718 under proportional in-phase and 3 kinds of non-proportional fatigue loading. Stress intensity factors for the various configurations have been analyzed with FRANC3D. Modal transition from Mode I (tensile) to Mode II (shear) crack branching has been observed in several load cases. Qualitative microscopy of fracture surfaces was used to characterize the crack growth behavior. An LEFM approach based on an effective stress intensity factor range, which incorporates the maximum value and range of each appropriate stress intensity (Mode I or Mode II), has been used to successfully predict

  11. Experimental study of stable imbibition displacements in a model open fracture. II. Scale-dependent avalanche dynamics.

    PubMed

    Clotet, Xavier; Santucci, Stéphane; Ortín, Jordi

    2016-01-01

    We report the results of an experimental investigation of the spatiotemporal dynamics of stable imbibition fronts in a disordered medium, in the regime of capillary disorder, for a wide range of experimental conditions. We have used silicone oils of various viscosities μ and nearly identical oil-air surface tension, and forced them to slowly invade a model open fracture at very different flow rates v. In this second part of the study we have carried out a scale-dependent statistical analysis of the front dynamics. We have specifically analyzed the influence of μ and v on the statistical properties of the velocity V_{ℓ}, the spatial average of the local front velocities over a window of lateral size ℓ. We have varied ℓ from the local scale defined by our spatial resolution up to the lateral system size L. Even though the imposed flow rate is constant, the signals V_{ℓ}(t) present very strong fluctuations which evolve systematically with the parameters μ, v, and ℓ. We have verified that the non-Gaussian fluctuations of the global velocity V_{ℓ}(t) are very well described by a generalized Gumbel statistics. The asymmetric shape and the exponential tail of those distributions are controlled by the number of effective degrees of freedom of the imbibition fronts, given by N_{eff}=ℓ/ℓ_{c} (the ratio of the lateral size of the measuring window ℓ to the correlation length ℓ_{c}∼1/sqrt[μv]). The large correlated excursions of V_{ℓ}(t) correspond to global avalanches, which reflect extra displacements of the imbibition fronts. We show that global avalanches are power-law distributed, both in sizes and durations, with robustly defined exponents-independent of μ, v, and ℓ. Nevertheless, the exponential upper cutoffs of the distributions evolve systematically with those parameters. We have found, moreover, that maximum sizes ξ_{S} and maximum durations ξ_{T} of global avalanches are not controlled by the same mechanism. While ξ_{S} are also

  12. Molecular interactions of DNA-topoisomerase I and II inhibitor with DNA and topoisomerases and in ternary complexes: binding modes and biological effects for intoplicine derivatives.

    PubMed

    Nabiev, I; Chourpa, I; Riou, J F; Nguyen, C H; Lavelle, F; Manfait, M

    1994-08-02

    Molecular interactions of intoplicine, dual DNA-topoisomerases (Topo) I and II inhibitor, with topoisomerases, plasmid DNA, in ternary cleavable complexes with enzymes and plasmid DNA, and in the reversed cleavable complexes were examined by means of surface-enhanced Raman scattering (SERS) and CD spectroscopy and by biochemical techniques. Detailed spectral analysis of intoplicine derivatives allowed us to assign SERS vibrational modes of chromophores and to propose the models for these complexes. Intoplicine was found to be able to interact specifically with the Topo II alone, but with Topo I only when in the presence of DNA. It shows at least two modes of binding to the DNA: the first was found to be dominant for its derivative 1c (most potent Topo I inhibitor), and the second was dominant for derivative 2a (most potent Topo II inhibitor). The possibility of forming these two types of complexes simultaneously is suggested to be one of the main factors enabling the drug to be a dual Topo I and Topo II inhibitor. The "deep intercalation mode" of the drug from the DNA minor groove with the long axis of the chromophore oriented roughly parallel to the dyad axis has been suggested to be responsible for induction of distortions of the DNA structure by the intercalating drug. Being involved in the formation of Topo I-mediated cleavable ternary complex, the molecules participating in the deep intercalation mode within the DNA do not change their molecular interactions as compared with their complex with the DNA alone. The stabilization of the Topo I-mediated cleavable complex was shown to be followed by the local denaturation of DNA in the AT-rich regions of the helix. When the ternary cleavable complex was reversed, the drug was shown to be in the complex with the plasmid. The "outside binding mode" from the DNA major groove via the hydroxyl group of the A-ring of the chromophore has been suggested to be responsible for Topo II inhibition. These molecules did not

  13. Improving the accuracy of derivation of the Williams’ series parameters under mixed (I+II) mode loading by compensation of measurement bias in the stress field components data

    NASA Astrophysics Data System (ADS)

    Lychak, Oleh V.; Holyns'kiy, Ivan S.

    2016-12-01

    A new method for compensation of bias in the stress field components measurement data used for Williams’ series parameters derivation was presented. Essential increase of accuracy of derivation of SIF-related leading terms in series under mixed (I+II) mode loading was demonstrated. It was shown that a relatively low value of bias in the stress field components data error could result in the essential deviation of the values of derived Williams’ coefficients and the crack tip coordinates.

  14. Application of the Pegasus II Pulsed-Power Facility to the Study of Inertial Instability and Fracture of Cylindrical Tubes of Solid Aluminum

    SciTech Connect

    Chandler, E.A.; Stokes, J.; Fulton, R.D.; Morgan, D.V.; Obst, A.W.; Oro, D.M.; Oona, H.; Anderson, W.E.

    1999-06-23

    Understanding the surface stability of metals undergoing dynamic fracture at shock breakout is important to several applications in metals processing. The advantages of using the Pegasus II facility to investigate the phenomena occurring at shock break out are described. As an example of the data collected, we concentrate on brief descriptions of two experiments that compared the tensile failure, i.e. ''spall'', patterns in the presence of sinusoidal perturbations seeded on the free inner surface of cylindrical samples of 3 types of Al. These samples were composed variously of soft Al 1100-O, structural grade Al 6061-T6, and ultra-pure 99.99% Al and were subjected to Taylor waves with shock pressures of 14 GPa. We show that the material behind the exiting surface undergoes a type of failure termed here ''microspall'', resulting in the production of a significant volume of low-density, probably granular, material. The failure mechanism, combined with the forces that cause inertial instability, leads to rapid pattern growth in the failed material and subsequent pattern growth on the surface. Pattern growth was studied as a function of perturbation wavelength and amplitude. The different Al samples vary by an order of magnitude in yield strength, and some increase in pattern instability was observed at lower yield strength. The ultra-pure Al has exceptionally large grain size, in the mm range. No appreciable variation of spall pattern was observed due to grain size.

  15. In-Situ Study of the Tensile Deformation and Fracture Modes in Peak-Aged Cast Mg-11Y-5Gd-2Zn-0.5Zr (Weight Percent)

    NASA Astrophysics Data System (ADS)

    Yin, D. D.; Wang, Q. D.; Boehlert, C. J.; Chen, Z.; Li, H. M.; Mishra, R. K.; Chakkedath, A.

    2016-12-01

    Tensile deformation and fracture modes in peak-aged cast Mg-11Y-5Gd-2Zn-0.5Zr (wt pct) (WGZ1152) samples at temperatures between 298 K [25 °C, room temperature (RT)] and 623 K (350 °C) (0.33 to 0.69 T m) were studied in situ inside a scanning electron microscope (SEM) using electron backscatter diffraction (EBSD) and slip trace analysis. The ultimate tensile strength (UTS) (265 MPa) and yield strength (YS) (193 MPa) at 523 K (250 °C) were 91 and 80 pct of those at RT, respectively. The observed dominant slip mode transitioned from basal slip (100 pct) to basal slip (81 pct) combined with prismatic slip (12 pct) from RT to 473 K (200 °C). As the temperature increased to 623 K (350 °C), basal slip (67 pct) and pyramidal slip (25 pct) became the dominant slip modes. The estimated critical resolved shear stress (CRSS) ratio of pyramidal slip/basal slip (7.3) was lower than that of prismatic slip/basal slip (12.7) at temperatures above 573 K (300 °C). Prismatic slip and pyramidal slip were more active at higher strains for moderate temperatures [473 K to 523 K (200 °C to 250 °C)] and at high temperatures [573 K to 623 K (300 °C to 350 °C)], respectively. A transition in the dominant fracture mode occurred from transgranular cracking (40 pct) combined with intergranular cracking (60 pct) to intergranular cracking as temperatures increased from RT to 623 K (350 °C). The intergranular crack nucleation sites tended to be located at grain boundaries and the interface between the Mg matrix and the large intermetallic grain boundary X phase. Slip bands were associated with transgranular crack nucleation.

  16. A theoretical analysis of the coordination modes of CuII with penicillins: activation of the beta-lactam C-N bond.

    PubMed

    Campomanes, Pablo; Menéndez, M Isabel; López, Ramón; Sordo, Tomás L

    2005-02-01

    The interaction of CuII with 6-formylamino-3alpha-carboxypenam and 6-acetylamino-3alpha-carboxypenam was investigated by means of DFT calculations with the UB3LYP functional. Nine different modes of complexation between CuII and 6-formylamino-3alpha-carboxypenam were located. When two water molecules directly bonded to CuII are included in the calculations on 6-acetylamino-3alpha-carboxypenam as penicillin model, only six CuII(H2O)2-6-acetylamino-3alpha-carboxypenam complexes (1S-6S) are found. In solution the four most stable complexes obtained from our calculations, 6S, 1S, 2S, and 3S, exhibit CuII in square-planar coordination with at least one bond to the carboxylate group, in agreement with experimental evidence. Complexes 6S, 1S, and 3S were previously suggested by available experimental evidence. In three of the most stable complexes (6S, 2S, and 3S) the beta-lactam C-N bond is remarkably activated and displays C-N bond lengths similar to those found in some tetrahedral intermediates located for the hydrolysis of 2-azetidinones. This suggests that these kinds of complexes belong to the reaction coordinate for the degradation of beta-lactam antibiotics in the presence of CuII.

  17. Diesel Fuels Hydraulic Fracturing (DFHF)

    EPA Pesticide Factsheets

    This webpage provides information on how hydraulic fracturing is regulated by the Underground Injection Control Program. It includes information about what owners and operators need to do to be in compliance and guidance for EPA Class II permit writers.

  18. Numerical Modeling of Fracture Propagation in Naturally Fractured Formations

    NASA Astrophysics Data System (ADS)

    Wang, W.; Prodanovic, M.; Olson, J. E.; Schultz, R.

    2015-12-01

    Hydraulic fracturing consists of injecting fluid at high pressure and high flowrate to the wellbore for the purpose of enhancing production by generating a complex fracture network. Both tensile failure and shear failure occur during the hydraulic fracturing treatment. The shear event can be caused by slip on existing weak planes such as faults or natural fractures. From core observation, partially cemented and fully cemented opening mode natural fractures, often with considerable thickness are widely present. Hydraulic fractures can propagate either within the natural fracture (tensile failure) or along the interface between the natural fracture and the rock matrix (tensile/shear failure), depending on the relative strength of cement and rock matrix materials, the bonding strength of interface, as well as the presence of any heterogeneities. In this study, we evaluate the fracture propagation both experimentally and numerically. We embed one or multiple inclusions of different mechanical properties within synthetic hydrostone samples in order to mimic cemented natural fractures and rock. A semi-circular bending test is performed for each set of properties. A finite element model built with ABAQUS is used to mimic the semi-circular bending test and study the fracture propagation path, as well as the matrix-inclusion bonding interface status. Mechanical properties required for the numerical model are measured experimentally. The results indicate that the match between experiment and modeling fracture path are extremely sensitive to the chosen interface (bonding) model and related parameters. The semi-circular bending test is dry and easily conducted, providing a good platform for validating numerical approaches. A validated numerical model will enable us to add pressurized fluid within the crack and simulate hydraulic fracture-natural fracture interaction in the reservoir conditions, ultimately providing insights into the extent of the fracture network.

  19. [Atlas fractures].

    PubMed

    Schären, S; Jeanneret, B

    1999-05-01

    Fractures of the atlas account for 1-2% of all vertebral fractures. We divide atlas fractures into 5 groups: isolated fractures of the anterior arch of the atlas, isolated fractures of the posterior arch, combined fractures of the anterior and posterior arch (so-called Jefferson fractures), isolated fractures of the lateral mass and fractures of the transverse process. Isolated fractures of the anterior or posterior arch are benign and are treated conservatively with a soft collar until the neck pain has disappeared. Jefferson fractures are divided into stable and unstable fracture depending on the integrity of the transverse ligament. Stable Jefferson fractures are treated conservatively with good outcome while unstable Jefferson fractures are probably best treated operatively with a posterior atlanto-axial or occipito-axial stabilization and fusion. The authors preferred treatment modality is the immediate open reduction of the dislocated lateral masses combined with a stabilization in the reduced position using a transarticular screw fixation C1/C2 according to Magerl. This has the advantage of saving the atlanto-occipital joints and offering an immediate stability which makes immobilization in an halo or Minerva cast superfluous. In late instabilities C1/2 with incongruency of the lateral masses occurring after primary conservative treatment, an occipito-cervical fusion is indicated. Isolated fractures of the lateral masses are very rare and may, if the lateral mass is totally destroyed, be a reason for an occipito-cervical fusion. Fractures of the transverse processes may be the cause for a thrombosis of the vertebral artery. No treatment is necessary for the fracture itself.

  20. The onset of mixed-mode intralaminar cracking in a cross-ply composite laminate

    NASA Astrophysics Data System (ADS)

    Andersons, J.; Spārniņš, E.; Joffe, R.

    2008-12-01

    The intralaminar fracture toughness of a unidirectionally reinforced glass/epoxy composite is determined experimentally at several mode I and mode II loading ratios. The crack propagation criterion, expressed as a quadratic form in terms of single-mode stress intensity factors (alternatively, linear in terms of energy release rates), approximates the test results reasonably well. The mixed-mode cracking criterion obtained is used to predict the intralaminar crack on set in a cross-ply glass/epoxy composite under off-axis tensile loading.

  1. Sensitivity of the active fracture model parameter to fracture network orientation and injection scenarios

    NASA Astrophysics Data System (ADS)

    Başağaoğlu, Hakan; Succi, Sauro; Manepally, Chandrika; Fedors, Randall; Wyrick, Danielle Y.

    2009-09-01

    Active fractures refer to the portions of unsaturated, connected fractures that actively conduct water. The active fracture model parameter accounts for the reduction in the number of fractures carrying water and in the fracture-matrix interface area in field-scale simulations of flow and transport in unsaturated fractured rocks. One example includes the numerical analyses of the fault test results at the Yucca Mountain site, Nevada (USA). In such applications, the active fracture model parameter is commonly used as a calibration parameter without relating it to fracture network orientations and infiltration rates. A two-dimensional, multiphase lattice-Boltzmann model was used in this study to investigate the sensitivity of the active fracture model parameter to fracture network orientation and injection scenarios for an unsaturated, variable dipping, and geometrically simple fracture network. The active fracture model parameter differed by as much as 0.11-0.44 when the effects of fracture network orientation, injection rate, and injection mode were included in the simulations. Hence, the numerical results suggest that the sensitivity of the active fracture model parameter to fracture network orientation, injection rates, and injection modes should be explored at the field-scale to strengthen the technical basis and range of applicability of the active fracture model.

  2. The effects of radiation on the interlaminar fracture toughness of a graphite/epoxy composite

    NASA Technical Reports Server (NTRS)

    Funk, J. G.; Sykes, G. F.

    1986-01-01

    An experimental study is made of the effect of electron irradiation (10 to the 10th rad), simulating a 30-year geosynchronous orbit exposure, on the fracture toughness of a graphite/epoxy composite, T300/934. The double cantilever beam (DBC) test is used to determine Mode I (peel) critical strain energy release rate and the edge delamination tension (EDT) test is used to determine mixed Mode I and II (peel and shear) critical strain energy release rate. It is found that the electron interaction of the epoxy matrix material enhances the fracture toughness properties of the composite and that the test temperature has a significant effect on the fracture toughness of both baseline and irradiated material.

  3. Computation of Anisotropic Bi-Material Interfacial Fracture Parameters and Delamination Creteria

    NASA Technical Reports Server (NTRS)

    Chow, W-T.; Wang, L.; Atluri, S. N.

    1998-01-01

    This report documents the recent developments in methodologies for the evaluation of the integrity and durability of composite structures, including i) the establishment of a stress-intensity-factor based fracture criterion for bimaterial interfacial cracks in anisotropic materials (see Sec. 2); ii) the development of a virtual crack closure integral method for the evaluation of the mixed-mode stress intensity factors for a bimaterial interfacial crack (see Sec. 3). Analytical and numerical results show that the proposed fracture criterion is a better fracture criterion than the total energy release rate criterion in the characterization of the bimaterial interfacial cracks. The proposed virtual crack closure integral method is an efficient and accurate numerical method for the evaluation of mixed-mode stress intensity factors.

  4. Skull fracture

    MedlinePlus

    ... compress the underlying brain tissue (subdural or epidural hematoma). A simple fracture is a break in the bone without damage ... Causes of skull fracture can include: Head trauma Falls, automobile accidents, physical assault, and sports

  5. Rib Fractures

    MedlinePlus

    ... From Brain Injury Additional Content Medical News Rib Fractures By Thomas G. Weiser, MD, MPH, Department of ... Hemothorax Injury to the Aorta Pulmonary Contusion Rib Fractures Tension Pneumothorax Traumatic Pneumothorax (See also Introduction to ...

  6. Hand Fractures

    MedlinePlus

    ... Thumb Arthritis Thumb Sprains Trigger Finger Tumors Wrist Fracture Hand Safety Fireworks Safety Lawnmower Safety Snowblower safety ... Tunnel Ganglion Cysts Thumb Arthritis Trigger Finger Wrist Fracture Hand Safety Fireworks Safety Lawnmower Safety Snowblower safety ...

  7. Improving the fracture toughness and the strength of epoxy using nanomaterials - a review of the current status

    NASA Astrophysics Data System (ADS)

    Domun, N.; Hadavinia, H.; Zhang, T.; Sainsbury, T.; Liaghat, G. H.; Vahid, S.

    2015-06-01

    The incorporation of nanomaterials in the polymer matrix is considered to be a highly effective technique to improve the mechanical properties of resins. In this paper the effects of the addition of different nanoparticles such as single-walled CNT (SWCNT), double-walled CNT (DWCNT), multi-walled CNT (MWCNT), graphene, nanoclay and nanosilica on fracture toughness, strength and stiffness of the epoxy matrix have been reviewed. The Young's modulus (E), ultimate tensile strength (UTS), mode I (GIC) and mode II (GIIC) fracture toughness of the various nanocomposites at different nanoparticle loadings are compared. The review shows that, depending on the type of nanoparticles, the integration of the nanoparticles has a substantial effect on mode I and mode II fracture toughness, strength and stiffness. The critical factors such as maintaining a homogeneous dispersion and good adhesion between the matrix and the nanoparticles are highlighted. The effect of surface functionalization, its relevancy and toughening mechanism are also scrutinized and discussed. A large variety of data comprised of the mechanical properties of nanomaterial toughened composites reported to date has thus been compiled to facilitate the evolution of this emerging field, and the results are presented in maps showing the effect of nanoparticle loading on mode I fracture toughness, stiffness and strength.

  8. Numerical investigations with a hybrid isentropic-sigma model. I - Normal-mode characteristics. II - The inclusion of moist processes

    NASA Technical Reports Server (NTRS)

    Pierce, R. B.; Johnson, Donald R.; Reames, Fred M.; Zapotocny, Tom H.; Wolf, Bart J.

    1991-01-01

    The normal-mode characteristics of baroclinically amplifying disturbances were numerically investigated in a series of adiabatic simulations by a hybrid isentropic-sigma model, demonstrating the effect of coupling an isentropic-coordinate free atmospheric domain with a sigma-coordinate PBL on the normal-mode characteristics. Next, the normal-mode model was modified by including a transport equation for water vapor and adiabatic heating by condensation. Simulations with and without a hydrological component showed that the overall effect of latent heat release is to markedly enhance cyclogenesis and frontogenesis.

  9. Failure modes and materials design for biomechanical layer structures

    NASA Astrophysics Data System (ADS)

    Deng, Yan

    Ceramic materials are finding increasing usage in the area of biomechanical replacements---dental crowns, hip and bone implants, etc.---where strength, wear resistance, biocompatibility, chemical durability and even aesthetics are critical issues. Aesthetic ceramic crowns have been widely used in dentistry to replace damaged or missing teeth. However, the failure rates of ceramic crowns, especially all-ceramic crowns, can be 1%˜6% per year, which is not satisfactory to patients. The materials limitations and underlying fracture mechanisms of these prostheses are not well understood. In this thesis, fundamental fracture and damage mechanisms in model dental bilayer and trilayer structures are studied. Principle failure modes are identified from in situ experimentation and confirmed by fracture mechanics analysis. In bilayer structures of ceramic/polycarbonate (representative of ceramic crown/dentin structure), three major damage sources are identified: (i) top-surface cone cracks or (ii) quasiplasticity, dominating in thick ceramic bilayers; (iii) bottom-surface radial cracks, dominating in thin ceramic bilayers. Critical load P for each damage mode are measured in six dental ceramics: Y-TZP zirconia, glass-infiltrated zirconia and alumina (InCeram), glass-ceramic (Empress II), Porcelain (Mark II and Empress) bonded to polymer substrates, as a function of ceramic thickness d in the range of 100 mum to 10 mm. P is found independent of d for mode (i) and (ii), but has a d 2 relations for mode (iii)---bottom surface radial cracking. In trilayer structures of glass/core-ceramic/polycarbonate (representing veneer porcelain/core/dentin structures), three inner fracture origins are identified: radial cracks from the bottom surface in the (i) first and (ii) second layers; and (iii) quasiplasticity in core-ceramic layer. The role of relative veneer/core thickness, d1/d 2 and materials properties is investigated for three core materials with different modulus (114--270GPa

  10. Pore- and fracture-filling gas hydrate reservoirs in the Gulf of Mexico Gas Hydrate Joint Industry Project Leg II Green Canyon 955 H well

    USGS Publications Warehouse

    Lee, M.W.; Collett, T.S.

    2012-01-01

    High-quality logging-while-drilling (LWD) downhole logs were acquired in seven wells drilled during the Gulf of MexicoGasHydrateJointIndustryProjectLegII in the spring of 2009. Well logs obtained in one of the wells, the GreenCanyon Block 955Hwell (GC955-H), indicate that a 27.4-m thick zone at the depth of 428 m below sea floor (mbsf; 1404 feet below sea floor (fbsf)) contains gashydrate within sand with average gashydrate saturations estimated at 60% from the compressional-wave (P-wave) velocity and 65% (locally more than 80%) from resistivity logs if the gashydrate is assumed to be uniformly distributed in this mostly sand-rich section. Similar analysis, however, of log data from a shallow clay-rich interval between 183 and 366 mbsf (600 and 1200 fbsf) yielded average gashydrate saturations of about 20% from the resistivity log (locally 50-60%) and negligible amounts of gashydrate from the P-wave velocity logs. Differences in saturations estimated between resistivity and P-wave velocities within the upper clay-rich interval are caused by the nature of the gashydrate occurrences. In the case of the shallow clay-rich interval, gashydrate fills vertical (or high angle) fractures in rather than fillingpore space in sands. In this study, isotropic and anisotropic resistivity and velocity models are used to analyze the occurrence of gashydrate within both the clay-rich and sand dominated gas-hydrate-bearing reservoirs in the GC955-Hwell.

  11. Posterior C1-C2 Fixation Using Absorbable Suture for Type II Odontoid Fracture in 2-Year-Old Child: Description of a New Technique and Literature Review.

    PubMed

    Labbe, Jean L; Peres, Olivier; Leclair, Olivier; Goulon, Renaud; Scemama, Patrice; Jourdel, François; Bertrou, Véronique; Murgier, Jerome

    2016-12-01

    Odontoid synchondrosis fractures are rare in children, even though they are the more common cervical fracture in children less than 7 years old. Nonoperative treatment with external orthosis immobilization is the treatment of choice for stable undisplaced or minimally displaced injuries. In unstable fractures, when reduction cannot be achieved or maintained, surgical fixation is recommended. We report a 2-year-old boy with an unstable fracture of the odontoid treated surgically using an absorbable monofilament suture for C1-C2 interlaminar fixation without bone grafting. This suture was strong enough to provide the stability necessary to allow healing of the synchondrosis and the delayed resorption of the suture was followed by complete restoration of the mobility between C1 and C2. This case illustrates that surgical stabilization using an absorbable suture in young children with an unstable odontoid fracture is a safe and effective alternative to other surgical techniques.

  12. Study of NBI-driven chirping mode properties and radial location by the heavy ion beam probe in the TJ-II stellarator

    NASA Astrophysics Data System (ADS)

    Melnikov, A. V.; Eliseev, L. G.; Castejón, F.; Hidalgo, C.; Khabanov, P. O.; Kozachek, A. S.; Krupnik, L. I.; Liniers, M.; Lysenko, S. E.; de Pablos, J. L.; Sharapov, S. E.; Ufimtsev, M. V.; Zenin, V. N.; HIBP Group; TJ-II Team

    2016-11-01

    Alfvén eigenmodes (AEs) were studied in low magnetic shear flexible heliac TJ-II (B 0  =  0.95 T, R 0  =  1.5 m, < a>   =  0.22 m) neutral beam injection (NBI) heated plasmas (P NBI  ⩽  1.1 MW, E NBI  =  32 keV) using the heavy ion beam probe (HIBP). L-mode hydrogen plasmas heated with co-, counter- and balanced-NBI and electron cyclotron resonance heating (ECRH) were investigated in various magnetic configurations with rotational transform ι(a)/2π  =  1/q ~ 1.5-1.6. The HIBP diagnostic is capable of simultaneously measuring the oscillations of the plasma electric potential, density and poloidal magnetic field. In earlier studies chirping modes have been observed with 250 kHz  <  f AE  <  380 kHz in combined ECR and NBI heated plasmas at low density {{\\bar{n}}\\text{e}}   =  (0.3-1.5)  ×  1019 m-3. In this paper we report the observation of chirping modes obtained with NBI only in plasmas with densities similar to those of earlier studies and obtained after lithium evaporation in the vacuum vessel. The absence of ECRH in the discharges studied here shows that ECRH is not a necessary ingredient to obtain chirping modes in TJ-II but rather a tool for obtaining low-density discharges. Using the HIBP we deduce that the location of the AE chirping mode is  -0.8  <  ρ  <  0.8. Chirping modes have a specific spatial structure: electric potential perturbations have a ballooning character, while the density and B pol perturbations are nearly symmetric for both ECRH  +  NBI and NBI-only plasmas. On TJ-II, the dominant effect on the nonlinear evolution of the AE from the chirping state to the steady-frequency state is the magnetic configuration, determined by the vacuum ι and plasma current I pl.

  13. Interlaminar fracture characterization: A current review

    NASA Technical Reports Server (NTRS)

    Martin, Roderick H.

    1991-01-01

    Interlaminar fracture characterization has been investigated for several years. Only now is it well enough understood for standardization organizations to attempt to write standard test methods. A review of the current philosophies in characterizing interlaminar fracture is presented. First, the mode 1, double cantilever beam test (DCB) for measuring G(sub 1c) and the end notched flexure (ENF) test for measuring G(sub 2c) are discussed. These tests have undergone the most extensive research throughout the years and are furthest towards standardization. In addition, the mode 2, end loaded split (ELS) specimen is discussed. Mixed mode fracture is also discussed and the recently developed mixed mode bending (MMB) test is detailed. Then, tests for evaluating mode 3 fracture toughness, including the split cantilever beam (SCB), are reviewed. Finally, the work done on interlaminar fracture characterization in fatigue is reviewed.

  14. Fracture toughness testing data: A technology survey and bibliography

    NASA Technical Reports Server (NTRS)

    Stuhrke, W. F.; Carpenter, J. L., Jr.; Moya, N.; Mandel, G.

    1975-01-01

    Announced survey includes reports covering fracture toughness testing for various structural materials including information on plane strain and developing areas of mixed mode and plane strain test conditions. Bibliography references cite work and conclusions in fracture toughness testing and application of fracture toughness test data, and in fracture mechanics analysis.

  15. Interfacial fracture toughness of synthetic bone-cement interface

    PubMed Central

    Tong, J

    2008-01-01

    Conventionally, the bonding strength of bone-cement interface is obtained by mechanical strength testing which tends to produce large variability between specimens and test methods. In this work, interfacial fracture toughness of synthetic bone-cement interface has been determined using sandwiched Brazilian disk specimens. Experiments were carried out under selected loading angles from 0 to 25 degrees to achieve full loading conditions from mode I to mode II. Solutions for complex stress intensity factors as well as strain energy release rates were obtained for a sandwich disk with a finite interlayer using the finite element method. Phase angles were obtained at a fixed distance to the crack tip. The fracture loads were obtained from the load displacement curves and the values of interfacial fracture toughness were calculated from the fracture loads and the finite element J-integral solutions. The implication of this information on the assessment of fixation in acetabular replacements was discussed in the light of in-vitro fatigue testing of implanted acetabula. PMID:19325935

  16. Interfacial fracture toughness of synthetic bone-cement interface.

    PubMed

    Tong, J

    2006-06-15

    Conventionally, the bonding strength of bone-cement interface is obtained by mechanical strength testing which tends to produce large variability between specimens and test methods. In this work, interfacial fracture toughness of synthetic bone-cement interface has been determined using sandwiched Brazilian disk specimens. Experiments were carried out under selected loading angles from 0 to 25 degrees to achieve full loading conditions from mode I to mode II. Solutions for complex stress intensity factors as well as strain energy release rates were obtained for a sandwich disk with a finite interlayer using the finite element method. Phase angles were obtained at a fixed distance to the crack tip. The fracture loads were obtained from the load displacement curves and the values of interfacial fracture toughness were calculated from the fracture loads and the finite element J-integral solutions. The implication of this information on the assessment of fixation in acetabular replacements was discussed in the light of in-vitro fatigue testing of implanted acetabula.

  17. Effects of fracture reactivation and diagenesis on fracture network evolution: Cambrian Eriboll Formation, NW Scotland

    NASA Astrophysics Data System (ADS)

    Hooker, J. N.; Eichhubl, P.; Xu, G.; Ahn, H.; Fall, A.; Hargrove, P.; Laubach, S.; Ukar, E.

    2011-12-01

    The Cambrian Eriboll Formation quartzarenites contain abundant fractures with varying degrees of quartz cement infill. Fractures exist that are entirely sealed; are locally sealed by bridging cements but preserve pore space among bridges; are mostly open but lined with veneers of cement; or are devoid of cement. Fracture propagation in the Eriboll Formation is highly sensitive to the presence of pre-existing fractures. Fracture reactivation occurs in opening mode as individual fractures repeatedly open and are filled or bridged by syn-kinematic cements. As well, reactivation occurs in shear as opening of one fracture orientation coincides with shear displacement along pre-existing fractures of different orientations. The tendency for pre-existing fractures to slip varies in part by the extent of cement infill, yet we observe shear and opening-mode reactivation even among sealed fractures. Paleotemperature analysis of fluid inclusions within fracture cements suggests some fractures now in outcrop formed deep in the subsurface. Fractures within the Eriboll Formation may therefore affect later fracture propagation throughout geologic time. With progressive strain, fault zones develop within fracture networks by a sequence of opening-mode fracture formation, fracture reactivation and linkage, fragmentation, cataclasis, and the formation of slip surfaces. Cataclasite within fault zones is commonly more thoroughly cemented than fractures in the damage zone or outside the fault zone. This variance of cement abundance is likely the result of (1) continued exposure of freshly broken quartz surfaces within cataclasite, promoting quartz precipitation, and (2) possibly more interconnected pathways for mass transfer within the fault zone. Enhanced cementation of cataclasite results in strengthening or diagenetic strain hardening of the evolving fault zone. Further slip is accommodated by shear localization along discrete slip surfaces. With further linkage of fault segments

  18. Wave Propagation in Isotropic Media with Two Orthogonal Fracture Sets

    NASA Astrophysics Data System (ADS)

    Shao, S.; Pyrak-Nolte, L. J.

    2016-10-01

    Orthogonal intersecting fracture sets form fracture networks that affect the hydraulic and mechanical integrity of a rock mass. Interpretation of elastic waves propagated through orthogonal fracture networks is complicated by guided modes that propagate along and between fractures, by multiple internal reflections, as well as by scattering from fracture intersections. The existence of some or all of these potentially overlapping modes depends on local stress fields that can preferentially close or open either one or both sets of fractures. In this study, an acoustic wave front imaging system was used to examine the effect of bi-axial loading conditions on acoustic wave propagation in isotropic media containing two orthogonal fracture sets. From the experimental data, orthogonal intersecting fracture sets support guided waves that depend on fracture spacing and fracture-specific stiffnesses. In addition, fracture intersections have stronger effects on propagating wave fronts than merely the superposition of the effects of two independent fractures because of energy partitioning among transmitted/reflected waves, scattered waves and guided modes. Interpretation of the properties of fractures or fracture sets from seismic measurements must consider non-uniform fracture stiffnesses within and among fracture sets, as well as considering the striking effects of fracture intersections on wave propagation.

  19. Risk Factors for Severity and Type of the Hip Fracture

    PubMed Central

    Cauley, Jane A.; Lui, Li-Yung; Genant, Harry K.; Salamone, Loran; Browner, Warren; Fink, Howard A.; Cohen, Peter; Hillier, Teresa; Bauer, Doug C.; Cummings, Steven R.

    2009-01-01

    More severe hip fractures such as displaced femoral neck (FN) fractures and unstable intertrochanteric (IT) fractures lead to poorer outcomes, but risk factors for severe fractures have not been studied. To identify risk factors for severe types of hip fracture, we performed a prospective cohort study and obtained preoperative hip radiographs from women who sustained an incident hip fracture (excluding traumatic fractures). A single radiologist scored the severity of FN fractures by the Garden System: grades I and II, undisplaced; grades III and IV, displaced. The severity of IT hip fractures was rated by the Kyle System: grades I and II, stable; grades III and IV, unstable. A total of 249 women had FN fractures: 75 (30%) were undisplaced. A total of 213 women had IT fractures: 59 (28%) were stable. Both types of hip fracture increased with age, but older age was even more strongly associated with more severe hip fractures. Low BMD was more strongly related to undisplaced FN fractures (p interaction BMD × FN type, p = 0.0008) and stable IT fractures (p interaction BMD × IT type, p = 0.04). Similar findings were observed for estimated volumetric BMD and hip geometric parameters. Corticosteroid use was only associated with displaced FN fractures, and Parkinson's disease was only associated with stable IT fractures. Little difference was reported in the self-reported circumstances surrounding each type of fracture. In conclusion, the lower the BMD, the greater the likelihood of experiencing a hip fracture that is less displaced and more stable. PMID:19113930

  20. 10 CFR Appendix G to Part 50 - Fracture Toughness Requirements

    Code of Federal Regulations, 2013 CFR

    2013-01-01

    ... 10 Energy 1 2013-01-01 2013-01-01 false Fracture Toughness Requirements G Appendix G to Part 50..., App. G Appendix G to Part 50—Fracture Toughness Requirements I. Introduction and scope. II. Definitions. III. Fracture toughness tests. IV. Fracture toughness requirements. I. Introduction and...

  1. 10 CFR Appendix G to Part 50 - Fracture Toughness Requirements

    Code of Federal Regulations, 2014 CFR

    2014-01-01

    ... 10 Energy 1 2014-01-01 2014-01-01 false Fracture Toughness Requirements G Appendix G to Part 50..., App. G Appendix G to Part 50—Fracture Toughness Requirements I. Introduction and scope. II. Definitions. III. Fracture toughness tests. IV. Fracture toughness requirements. I. Introduction and...

  2. Lunar floor-fractured craters as magmatic intrusions: Geometry, modes of emplacement, associated tectonic and volcanic features, and implications for gravity anomalies

    NASA Astrophysics Data System (ADS)

    Jozwiak, Lauren M.; Head, James W.; Wilson, Lionel

    2015-03-01

    Lunar floor-fractured craters are a class of 170 lunar craters with anomalously shallow, fractured floors. Two end-member processes have been proposed for the floor formation: viscous relaxation, and subcrater magmatic intrusion and sill formation. Recent morphometric analysis with new Lunar Reconnaissance Orbiter Laser Altimeter (LOLA) and image (LROC) data supports an origin related to shallow magmatic intrusion and uplift. We find that the distribution and characteristics of the FFC population correlates strongly with crustal thickness and the predicted frequency distribution of overpressurization values of magmatic dikes. For a typical nearside lunar crustal thickness, dikes with high overpressurization values favor surface effusive eruptions, medium values favor intrusion and sill formation, and low values favor formation of solidified dikes concentrated lower in the crust. We develop a model for this process, make predictions for the morphologic, morphometric, volcanic, and geophysical consequences of the process and then compare these predictions with the population of observed floor-fractured craters. In our model, the process of magmatic intrusion and sill formation begins when a dike propagates vertically towards the surface; as the dike encounters the underdense brecciated region beneath the crater, the magmatic driving pressure is insufficient to continue vertical propagation, but pressure in the stalled dike exceeds the local lithostatic pressure. The dike then begins to propagate laterally forming a sill which does not propagate past the crater floor region because increased overburden pressure from the crater wall and rim crest pinch off the dike at this boundary; the sill then continues to inflate, further raising and fracturing the brittle crater floor. When the intrusion diameter to intrusion depth ratio is smaller than a critical value, the intrusion assumes a laccolith shape with a domed central region. When the ratio exceeds a critical value

  3. The versatile binding mode of transition-state analogue inhibitors of tyrosinase towards dicopper(II) model complexes: experimental and theoretical investigations.

    PubMed

    Orio, Maylis; Bochot, Constance; Dubois, Carole; Gellon, Gisèle; Hardré, Renaud; Jamet, Hélène; Luneau, Dominique; Philouze, Christian; Réglier, Marius; Serratrice, Guy; Belle, Catherine

    2011-11-25

    We describe 2-mercaptopyridine-N-oxide (HSPNO) as a new and efficient competitive inhibitor of mushroom tyrosinase (K(IC) =3.7 μM). Binding studies of HSPNO and 2-hydroxypyridine-N-oxide (HOPNO) on dinuclear copper(II) complexes [Cu(2)(BPMP)(μ-OH)](ClO(4))(2) (1; HBPMP=2,6-bis[bis(2-pyridylmethyl)aminomethyl]-4-methylphenol) and [Cu(2)(BPEP)(μ-OH)](ClO(4))(2)) (2; HBPEP=2,6-bis{bis[2-(2-pyridyl)ethyl]aminomethyl}-4-methylphenol), known to be functional models for the tyrosinase diphenolase activity, have been performed. A combination of structural data, spectroscopic studies, and DFT calculations evidenced the adaptable binding mode (bridging versus chelating) of HOPNO in relation to the geometry and chelate size of the dicopper center. For comparison, binding studies of HSPNO and kojic acid (5-hydroxy-2-(hydroxymethyl)-4-pyrone) on dinuclear complexes were performed. A theoretical approach has been developed and validated on HOPNO adducts to compare the binding mode on the model complexes. It has been applied for HSPNO and kojic acid. Although results for HSPNO were in line with those obtained with HOPNO, thus reflecting their chemical similarity, we showed that the bridging mode was the most preferential binding mode for kojic acid on both complexes.

  4. Out-of-plane deviation of a mode I+III crack encountering a tougher obstacle

    NASA Astrophysics Data System (ADS)

    Leblond, Jean-Baptiste; Ponson, Laurent

    2016-07-01

    One possible explanation of out-of-plane deviations of cracks loaded in mode I+III was suggested by Gao and Rice in 1986. These authors noted that small in-plane undulations of the crack front, arising from fluctuations of the fracture toughness, should generate a small local mode-II component, causing the crack to depart from planarity. Their analysis is completed here by explicitly calculating the evolution in time of the out-of-plane deviation of a mode-I+III crack encountering a tougher obstacle. The calculation is based on (i) first-order formulae for the stress intensity factors of a crack slightly perturbed within and out of its plane; and (ii) a "double" propagation criterion combining a Griffith condition on the local energy-release rate and a Goldstein-Salganik condition on the local stress intensity factor of mode II. It is predicted that the crack must evolve toward a stationary state, wherein the orthogonal distance from the average fracture plane to the perturbed crack front is constant outside the obstacle and varies linearly across it. We hope that this theoretical prediction will encourage comparison with experiments, and propose a fracture test involving propagation of a mode-I+III crack through a 3D-printed specimen containing some designed obstacle. xml:lang="fr"

  5. Scalable High-Performance Algorithm for the Simulation of Exciton Dynamics. Application to the Light-Harvesting Complex II in the Presence of Resonant Vibrational Modes.

    PubMed

    Kreisbeck, Christoph; Kramer, Tobias; Aspuru-Guzik, Alán

    2014-09-09

    The accurate simulation of excitonic energy transfer in molecular complexes with coupled electronic and vibrational degrees of freedom is essential for comparing excitonic system parameters obtained from ab initio methods with measured time-resolved spectra. Several exact methods for computing the exciton dynamics within a density-matrix formalism are known but are restricted to small systems with less than 10 sites due to their computational complexity. To study the excitonic energy transfer in larger systems, we adapt and extend the exact hierarchical equation of motion (HEOM) method to various high-performance many-core platforms using the Open Compute Language (OpenCL). For the light-harvesting complex II (LHC II) found in spinach, the HEOM results deviate from predictions of approximate theories and clarify the time scale of the transfer process. We investigate the impact of resonantly coupled vibrations on the relaxation and show that the transfer does not rely on a fine-tuning of specific modes.

  6. Comparative internal kinematics of the H II regions in interacting and isolated galaxies: implications for massive star formation modes

    NASA Astrophysics Data System (ADS)

    Zaragoza-Cardiel, Javier; Beckman, John E.; Font, Joan; García-Lorenzo, Begoña; Camps-Fariña, Artemi; Fathi, Kambiz; James, Philip A.; Erroz-Ferrer, Santiago; Barrera-Ballesteros, Jorge; Cisternas, Mauricio

    2015-08-01

    We have observed 12 interacting galaxy pairs using the Fabry-Perot interferometer GH αFaS (Galaxy H α Fabry-Perot system) on the 4.2-m William Herschel Telescope at the Observatorio del Roque de los Muchachos, La Palma. We present here the Hα surface brightness, velocity and velocity dispersion maps for the 10 systems we have not previously observed using this technique, as well as the physical properties (sizes, Hα luminosities and velocity dispersion) of 1259 H II regions from the full sample. We also derive the physical properties of 1054 H II regions in a sample of 28 isolated galaxies observed with the same instrument in order to compare the two populations of H II regions. We find a population of the brightest H II regions for which the scaling relations, for example the relation between the Hα luminosity and the radius, are clearly distinct from the relations for the regions of lower luminosity. The regions in this bright population are more frequent in the interacting galaxies. We find that the turbulence, and also the star formation rate (SFR), are enhanced in the H II regions in the interacting galaxies. We have also extracted the Hα equivalent widths for the H II regions of both samples, and we have found that the distribution of H II region ages coincides for the two samples of galaxies. We suggest that the SFR enhancement is brought about by gas flows induced by the interactions, which give rise to gravitationally bound gas clouds which grow further by accretion from the flowing gas, producing conditions favourable to star formation.

  7. Bulk filling of Class II cavities with a dual-cure composite: Effect of curing mode and enamel etching on marginal adaptation

    PubMed Central

    Bortolotto, Tissiana; Roig, Miguel; Krejci, Ivo

    2014-01-01

    Objectives: This study attempted to find a simple adhesive restorative technique for class I and II cavities on posterior teeth. Study Design: The tested materials were a self-etching adhesive (Parabond, Coltène/Whaledent) and a dual-cure composite (Paracore, Coltène/Whaledent) used in bulk to restore the cavities. Class II MO cavities were performed and assigned to 4 groups depending on the orthophosphoric acid (H3PO4) conditioning of enamel and polymerization method used (chemical or dual). Specimens were subjected to quantitative marginal analysis before and after thermo-mechanical loading. Results: Higher percentages of marginal adaptation at the total margin length, both before and after thermo-mechanical loading, were found in groups in which enamel was etched with phosphoric acid, without significant differences between the chemically and dual-cured modes. The restorations performance was similar on enamel and dentin, obtaining low results of adaptation on occlusal enamel in the groups without enamel etching, the lowest scores were on cervical dentin in the group with no ortophosphoric acid and self-cured. Conclusions: A dual-cure composite applied in bulk on acid etched enamel obtained acceptable marginal adaptation results, and may be an alternative technique for the restoration of class II cavities. Key words:Dual-cure composite, bulk technique, class II restoration, selective enamel etching, marginal adaptation. PMID:25674316

  8. Modeling interfacial fracture in Sierra.

    SciTech Connect

    Brown, Arthur A.; Ohashi, Yuki; Lu, Wei-Yang; Nelson, Stacy A. C.; Foulk, James W.,; Reedy, Earl David,; Austin, Kevin N.; Margolis, Stephen B.

    2013-09-01

    This report summarizes computational efforts to model interfacial fracture using cohesive zone models in the SIERRA/SolidMechanics (SIERRA/SM) finite element code. Cohesive surface elements were used to model crack initiation and propagation along predefined paths. Mesh convergence was observed with SIERRA/SM for numerous geometries. As the funding for this project came from the Advanced Simulation and Computing Verification and Validation (ASC V&V) focus area, considerable effort was spent performing verification and validation. Code verification was performed to compare code predictions to analytical solutions for simple three-element simulations as well as a higher-fidelity simulation of a double-cantilever beam. Parameter identification was conducted with Dakota using experimental results on asymmetric double-cantilever beam (ADCB) and end-notched-flexure (ENF) experiments conducted under Campaign-6 funding. Discretization convergence studies were also performed with respect to mesh size and time step and an optimization study was completed for mode II delamination using the ENF geometry. Throughout this verification process, numerous SIERRA/SM bugs were found and reported, all of which have been fixed, leading to over a 10-fold increase in convergence rates. Finally, mixed-mode flexure experiments were performed for validation. One of the unexplained issues encountered was material property variability for ostensibly the same composite material. Since the variability is not fully understood, it is difficult to accurately assess uncertainty when performing predictions.

  9. Anticancer Activity and Modes of Action of (arene) ruthenium(II) Complexes Coordinated to C-, N-, and O-ligands.

    PubMed

    Biersack, Bernhard

    2016-01-01

    An overview of anticancer active (arene)ruthenium(II) complexes coordinated to period 2 element-based ligand systems, i.e., carbon-, nitrogen-, and oxygen-coordinated ligands, is provided in this mini-review. A bridge is forged from the large group of anticancer active ruthenium compounds with monodentate and chelating nitrogen ligands via complexes of O,O-chelating ligands to organometallic ruthenium derivatives coordinated to carbon. (Arene)ruthenium(II) complexes with reduced side-effects and enhanced efficacy against cancer are highlighted. Pertinent literature is covered up to 2014.

  10. Interlaminar Fracture toughness in Glass-Cellulose Reinforced Epoxy hybrid composites

    NASA Astrophysics Data System (ADS)

    Uppin, Vinayak S.; Ashok; AnanthJoshi; Sridhar, I.; Shivakumar Gouda, P. S.

    2016-09-01

    Laminates of fibre reinforced compositesare weak in through thicknessbut strong in fibre direction, this lead to development of hybridizationconcept in polymer composites. In this work a new method of disperssing cellulose micro particleson unidirectional (UD) Glass fibre epoxy composite using semi-automated draw down coating technique was adopted to enhance fracture toughness.Test results show that by adding cellulose increases the load carrying competency by 32% in mode-I as compare to Glass- Epoxy composite samples. Imrovement in interlaminar critical energy release rates (GiC and GnC) up to 55% in Mode -I and 19 %in Mode -II respectively was also observed. This enahancement in fracture toughnees is due to the amount of fiber bridging seen during crack initiation and propagation.

  11. An Evaluation of the Mode of Action Framework for MutagenicCarcinogens Case Study II: Chromium (VI).

    EPA Science Inventory

    In response to the 2005 revised U.S Environmental Protection Agency’s (EPA) Cancer Guidelines, a strategy is being developed to include all mutagenicity and other genotoxicity data with any additional information to determine whether a carcinogen operates through a mutagenic mode...

  12. Mechanistic fracture criteria for the failure of human cortical bone

    SciTech Connect

    Nalla, Ravi K.; Kinney, John H.; Ritchie, Robert O.

    2002-12-13

    A mechanistic understanding of fracture in human bone is critical to predicting fracture risk associated with age and disease. Despite extensive work, a mechanistic framework for describing how the underlying microstructure affects the failure mode in bone is lacking.

  13. Outcome by mode of anaesthesia for hip fracture surgery. An observational audit of 65 535 patients in a national dataset.

    PubMed

    White, S M; Moppett, I K; Griffiths, R

    2014-03-01

    Large observational studies of accurate data can provide similar results to more arduous and expensive randomised controlled trials. In 2012, the National Hip Fracture Database extended its dataset to include 'type of anaesthesia' data fields. We analysed 65 535 patient record sets to determine differences in outcome. Type of anaesthesia was recorded in 59 191 (90%) patients. Omitting patients who received both general and spinal anaesthesia or in whom an uncertain type of anaesthesia was recorded, there was no significant difference in either cumulative five-day (2.8% vs 2.8%, p = 0.991) or 30-day (7.0% vs 7.5%, p = 0.053) mortality between 30 130 patients receiving general anaesthesia and 22 999 patients receiving spinal anaesthesia, even when 30-day mortality was adjusted for age and ASA physical status (p = 0.226). Mortality within 24 hours after surgery was significantly higher among patients receiving cemented compared with uncemented hemiarthroplasty (1.6% vs 1.2%, p = 0.030), suggesting excess early mortality related to bone cement implantation syndrome. If these data are accurate, then either there is no difference in 30-day mortality between general and spinal anaesthesia after hip fracture surgery per se, and therefore future research should focus on how to make both types of anaesthesia safer, or there is a difference, but mortality is not the correct outcome to measure after anaesthesia, and therefore future research should focus on differences between general and spinal anaesthesia. These could include more anaesthesia-sensitive outcomes, such as hypotension, pain, postoperative confusion, respiratory infection and mobilisation.

  14. Shear-flow trapped-ion-mode interaction revisited. II. Intermittent transport associated with low-frequency zonal flow dynamics

    SciTech Connect

    Ghizzo, A.; Palermo, F.

    2015-08-15

    We address the mechanisms underlying low-frequency zonal flow generation in turbulent system and the associated intermittent regime of ion-temperature-gradient (ITG) turbulence. This model is in connection with the recent observation of quasi periodic zonal flow oscillation at a frequency close to 2 kHz, at the low-high transition, observed in the ASDEX Upgrade [Conway et al., Phys. Rev. Lett. 106, 065001 (2011)] and EAST tokamak [Xu et al., Phys. Rev. Lett 107, 125001 (2011)]. Turbulent bursts caused by the coupling of Kelvin-Helmholtz (KH) driven shear flows with trapped ion modes (TIMs) were investigated by means of reduced gyrokinetic simulations. It was found that ITG turbulence can be regulated by low-frequency meso-scale zonal flows driven by resonant collisionless trapped ion modes (CTIMs), through parametric-type scattering, a process in competition with the usual KH instability.

  15. Microstructural effects in foam fracture

    NASA Astrophysics Data System (ADS)

    Stewart, Peter; Davis, Stephen; Hilgenfeldt, Sascha

    2015-11-01

    We examine the fracture of a quasi two-dimensional aqueous foam under an applied driving pressure, using a network modelling approach developed for metallic foams by Stewart & Davis (J. Rheol., vol. 56, 2012, p. 543). In agreement with experiments, we observe two distinct mechanisms of failure analogous to those observed in a crystalline solid: a slow ductile mode when the driving pressure is applied slowly, where the void propagates as bubbles interchange neighbours through the T1 process, and a rapid brittle mode for faster application of pressures, where the void advances by successive rupture of liquid films driven by Rayleigh-Taylor instability. The simulations allow detailed insight into the mechanics of the fracturing medium and the role of its microstructure. In particular, we examine the stress distribution around the crack tip and investigate how brittle fracture localizes into a single line of breakages. We also confirm that pre-existing microstructural defects can alter the course of fracture.

  16. Multiscale Multifunctional Progressive Fracture of Composite Structures

    NASA Technical Reports Server (NTRS)

    Chamis, C. C.; Minnetyan, L.

    2012-01-01

    A new approach is described for evaluating fracture in composite structures. This approach is independent of classical fracture mechanics parameters like fracture toughness. It relies on computational simulation and is programmed in a stand-alone integrated computer code. It is multiscale, multifunctional because it includes composite mechanics for the composite behavior and finite element analysis for predicting the structural response. It contains seven modules; layered composite mechanics (micro, macro, laminate), finite element, updating scheme, local fracture, global fracture, stress based failure modes, and fracture progression. The computer code is called CODSTRAN (Composite Durability Structural ANalysis). It is used in the present paper to evaluate the global fracture of four composite shell problems and one composite built-up structure. Results show that the composite shells. Global fracture is enhanced when internal pressure is combined with shear loads. The old reference denotes that nothing has been added to this comprehensive report since then.

  17. The AO Pediatric Comprehensive Classification of Long Bone Fractures (PCCF)

    PubMed Central

    Joeris, Alexander; Lutz, Nicolas; Blumenthal, Andrea; Slongo, Theddy; Audigé, Laurent

    2017-01-01

    Background and purpose To achieve a common understanding when dealing with long bone fractures in children, the AO Pediatric Comprehensive Classification of Long Bone Fractures (AO PCCF) was introduced in 2007. As part of its final validation, we present the most relevant fracture patterns in the upper extremities of a representative population of children classified according to the PCCF. Patients and methods We included children and adolescents (0–17 years old) diagnosed with 1 or more long bone fractures between January 2009 and December 2011 at the university hospitals in Bern and Lausanne (Switzerland). Patient charts were retrospectively reviewed and fractures were classified from standard radiographs. Results Of 2,292 upper extremity fractures in 2,203 children and adolescents, 26% involved the humerus and 74% involved the forearm. In the humerus, 61%, and in the forearm, 80% of single distal fractures involved the metaphysis. In adolescents, single humerus fractures were more often epiphyseal and diaphyseal fractures, and among adolescents radius fractures were more often epiphyseal fractures than in other age groups. 47% of combined forearm fractures were distal metaphyseal fractures. Only 0.7% of fractures could not be classified within 1 of the child-specific fracture patterns. Of the single epiphyseal fractures, 49% were Salter-Harris type-II (SH II) fractures; of these, 94% occurred in schoolchildren and adolescents. Of the metaphyseal fractures, 58% showed an incomplete fracture pattern. 89% of incomplete fractures affected the distal radius. Of the diaphyseal fractures, 32% were greenstick fractures. 24 Monteggia fractures occurred in pre-school children and schoolchildren, and 2 occurred in adolescents. Interpretation The pattern of pediatric fractures in the upper extremity can be comprehensively described according to the PCCF. Prospective clinical studies are needed to determine its clinical relevance for treatment decisions and prognostication

  18. The AO Pediatric Comprehensive Classification of Long Bone Fractures (PCCF).

    PubMed

    Joeris, Alexander; Lutz, Nicolas; Blumenthal, Andrea; Slongo, Theddy; Audigé, Laurent

    2017-04-01

    Background and purpose - To achieve a common understanding when dealing with long bone fractures in children, the AO Pediatric Comprehensive Classification of Long Bone Fractures (AO PCCF) was introduced in 2007. As part of its final validation, we present the most relevant fracture patterns in the upper extremities of a representative population of children classified according to the PCCF. Patients and methods - We included children and adolescents (0-17 years old) diagnosed with 1 or more long bone fractures between January 2009 and December 2011 at the university hospitals in Bern and Lausanne (Switzerland). Patient charts were retrospectively reviewed and fractures were classified from standard radiographs. Results - Of 2,292 upper extremity fractures in 2,203 children and adolescents, 26% involved the humerus and 74% involved the forearm. In the humerus, 61%, and in the forearm, 80% of single distal fractures involved the metaphysis. In adolescents, single humerus fractures were more often epiphyseal and diaphyseal fractures, and among adolescents radius fractures were more often epiphyseal fractures than in other age groups. 47% of combined forearm fractures were distal metaphyseal fractures. Only 0.7% of fractures could not be classified within 1 of the child-specific fracture patterns. Of the single epiphyseal fractures, 49% were Salter-Harris type-II (SH II) fractures; of these, 94% occurred in schoolchildren and adolescents. Of the metaphyseal fractures, 58% showed an incomplete fracture pattern. 89% of incomplete fractures affected the distal radius. Of the diaphyseal fractures, 32% were greenstick fractures. 24 Monteggia fractures occurred in pre-school children and schoolchildren, and 2 occurred in adolescents. Interpretation - The pattern of pediatric fractures in the upper extremity can be comprehensively described according to the PCCF. Prospective clinical studies are needed to determine its clinical relevance for treatment decisions and

  19. Coordination modes of a schiff base pentadentate derivative of 4-aminoantipyrine with cobalt(II), nickel(II) and copper(II) metal ions: synthesis, spectroscopic and antimicrobial studies.

    PubMed

    Chandra, Sulekh; Jain, Deepali; Sharma, Amit Kumar; Sharma, Pratibha

    2009-01-01

    Transition metal complexes of Co(II), Ni(II) and Cu(II) metal ions with general stoichiometry [M(L)X]X and [M(L)SO(4)], where M = Co(II), Ni(II) and Cu(II), L = 3,3'-thiodipropionic acid bis(4-amino-5-ethylimino-2,3-dimethyl-1-phenyl-3-pyrazoline) and X = NO(3)(-), Cl(-) and OAc(-), have been synthesized and structurally characterized by elemental analyses, molar conductance measurements, magnetic susceptibility measurements and spectral techniques like IR, UV and EPR. The nickel(II) complexes were found to have octahedral geometry, whereas cobalt(II) and copper(II) complexes were of tetragonal geometry. The covalency factor (beta) and orbital reduction factor (k) suggest the covalent nature of the complexes. The ligand and its complexes have been screened for their antifungal and antibacterial activities against three fungi, i.e. Alternaria brassicae, Aspergillus niger and Fusarium oxysporum and two bacteria, i.e. Xanthomonas compestris and Pseudomonas aeruginosa.

  20. TOXIC SUBSTANCES FROM COAL COMBUSTION--A COMPREHENSIVE ASSESSMENT, PHASE II: ELEMENT MODES OF OCCURRENCE FOR THE OHIO 5/6/7, WYODAK AND NORTH DAKOTA COAL SAMPLES

    SciTech Connect

    Allan Kolker; Stanley J. Mroczkowski; Curtis A. Palmer; Kristen O. Dennen; Robert B. Finkelman; John H. Bullock Jr.

    2002-05-30

    This study reports on the second phase (Phase II) of USGS research activities in support of DOE contract DE-AC22-95PC95101 ''Toxic Substances From Coal Combustion--A Comprehensive Assessment'', funded under DOE Interagency Agreement DE-AI22-95PC95145. The purpose of the study was to provide a quantitative and semi-quantitative characterization of the modes of occurrence of trace elements in coal samples investigated under Phase II, including (1) Ohio 5/6/7, an Ohio bituminous coal sample blended from the No.5, No.6, and No.7 beds; (2) North Dakota, a lignite sample from the Falkirk Mine, Underwood, ND, and (3) Wyodak, a sub-bituminous coal sample from the Cordero Mine, Gillette, WY. Samples from these coal beds were selected for their range in rank and commercial applicability. Results of this research provide basic information on the distribution of elements in Phase II coal samples, information needed for development of a commercial predictive model for trace-element behavior during coal combustion.

  1. Vibrational investigation on the copper(II) binding mode of carcinine and its pH dependence

    NASA Astrophysics Data System (ADS)

    Torreggiani, Armida; Reggiani, Matteo; Manco, Immacolata; Tinti, Anna

    2007-05-01

    A comparative FT-Raman and FT-IR study of Carcinine (Carc), a natural imidazole dipeptide, and its complexes with Cu(II) ions was performed at different pH's. Both Raman and IR spectra present marker bands useful for the identification of the predominant complexes; in particular, Raman spectroscopy appears useful for identifying the metal-coordination site of the imidazole ring (N π or N τ atoms) of Carc. Free Carc shows a strong network of H-bonds and tautomer I (N τ-H) is the preferred form of the imidazolic ring (bands at 1578, 1292 and 988 cm -1). The presence of Cu(II) does not affect the tautomeric equilibrium at pH 7, whereas the deprotonation of both N-imidazolic nitrogens is strongly induced at higher pH. Under neutral and alkaline conditions the primary amino group takes part to the Cu(II) chelation, whereas all the peptidic moieties are involved in coordination only at pH 7. Thus, Carc acts as a tri-dentate ligand at neutral pH, mainly giving a monomeric complex, [CuLH -1], containing tautomer I, whereas an oligonuclear complex, probably [Cu 4L 4H -8], where metal-imidazolate ions connect different ligand molecules, predominates at alkaline pH.

  2. Structures of mammalian ER α-glucosidase II capture the binding modes of broad-spectrum iminosugar antivirals

    PubMed Central

    Alonzi, Dominic S.; Marti, Lucia; Reca, Ida-Barbara; Kiappes, J. L.; Struwe, Weston B.; Cross, Alice; Basu, Souradeep; Lowe, Edward D.; Darlot, Benoit; Santino, Angelo; Zitzmann, Nicole

    2016-01-01

    The biosynthesis of enveloped viruses depends heavily on the host cell endoplasmic reticulum (ER) glycoprotein quality control (QC) machinery. This dependency exceeds the dependency of host glycoproteins, offering a window for the targeting of ERQC for the development of broad-spectrum antivirals. We determined small-angle X-ray scattering (SAXS) and crystal structures of the main ERQC enzyme, ER α-glucosidase II (α-GluII; from mouse), alone and in complex with key ligands of its catalytic cycle and antiviral iminosugars, including two that are in clinical trials for the treatment of dengue fever. The SAXS data capture the enzyme’s quaternary structure and suggest a conformational rearrangement is needed for the simultaneous binding of a monoglucosylated glycan to both subunits. The X-ray structures with key catalytic cycle intermediates highlight that an insertion between the +1 and +2 subsites contributes to the enzyme’s activity and substrate specificity, and reveal that the presence of d-mannose at the +1 subsite renders the acid catalyst less efficient during the cleavage of the monoglucosylated substrate. The complexes with iminosugar antivirals suggest that inhibitors targeting a conserved ring of aromatic residues between the α-GluII +1 and +2 subsites would have increased potency and selectivity, thus providing a template for further rational drug design. PMID:27462106

  3. Solute transport in a synthetic fracture with one porous wall: fracture-matrix interaction

    NASA Astrophysics Data System (ADS)

    Michel, L.; Meheust, Y.; Caudal, J.; de Bremond D'Ars, J.; de Dreuzy, J.; Davy, P.

    2007-12-01

    Contaminant transport in heterogeneous fractured aquifers occurs mostly through the networks of intersecting fractures. The physical mechanisms of solute transport in a single fracture with impermeable walls are well identified (Dronfield and Silliman 1993; Roux, Plouraboué et al. 1998; Keller, Roberts et al. 1999; Detwiler and Rajaram 2000): advection, Taylor-Aris dispersion, roughness dispersion, aperture-variation dispersion and molecular diffusion. However, when the permeability of the surrounding rock matrix cannot be neglected, there is, to our knowledge, no fundamental description of the mass transfert coefficient between the region of high permeability (the fracture) and that of low permeability (the surrounding matrix). We address here solute transport through a synthetic fracture with a porous wall. We present an analog experimental model setup in which we can focus on specific dispersion mechanisms, neglecting molecular diffusion, in order to extract descriptive laws that will be integrated in future numerical models. The planar horizontal fracture is 1 m long, 5 cm wide and its mean aperture is 5 mm. It is bounded by either two smooth parallel Plexiglass plates (impermeable walls configuration), or by one such plate and a porous medium consisting of 1 mm glass beads ("semi-permeable" configuration). A permanent laminar water flow is forced through the fracture at controlled mean velocity (~ 1mm/s), and a dye (patent blue) injection system simulates a point source of contaminant along the center plane of the fracture. The tracer plume is tracked using a visualization system based on (i) lasers illuminating a series of vertical linear optical sensor arrays, and (ii) 4 cameras positioned side by side and providing a composite image of the fracture viewed from the side. The two measurement systems yield consistent quantitative temporal descriptions of the tracer concentration, integrated over the fracture width and at several positions along the fracture

  4. Studies on effect of pre-crack length variation on Inter-laminar fracture toughness of a Glass Epoxy laminated composite

    NASA Astrophysics Data System (ADS)

    Huddhar, Arun; Desai, Abilash; Sharanaprabhu, C. M.; Kudari, Shashidhar K.; Shivakumar Gouda, P. S.

    2016-09-01

    Laminates of fiber reinforced polymer composites are good in in-plane properties and inherently weak in through thickness direction. To address this through thickness properties, the inter-laminar fracture toughness (GIc and GIIc) of a unidirectional (UD) Glass epoxy composite laminates were subjected to Mode-I and Mode-II loadings. Experiments were conducted using Double cantilever beam (DCB) and End notch flexure (ENF) specimens with varying pre-crack lengths. Mode I energy release rate (GIc) were also evaluated with modified beam and modified compliance theories. The experimental results reveal that, GIc fracture toughness increases with increasing in pre-crack length, where as in GIIc the effect of increase in pre-crack length exhibits reduced fracture toughness.

  5. Treatment of fractures in avian species.

    PubMed

    MacCoy, D M

    1992-01-01

    External fixation, with coaptation or Kirschner-Ehmer splints, is a viable treatment for many fractures in captive and wild birds. Important considerations in selecting a device are the weight and size of the device, location of the fracture relative to joints, and prognosis associated with location of the fracture(s). A variety of materials, not limited to traditional medical materials, may be used in coaptation splinting. Straws, plastic spoons, and rubber balls can serve as effective splints. Type I and II Kirschner splints are typically used in birds, although large birds may require a type III splint on leg fractures. The most useful configuration for wing fractures is the type Ia single bar splint using epoxy or acrylic for the connecting bar. This splint is lightweight, positioned close to the patient, and stable for most fractures. The type II splint is an excellent choice for leg fractures at the level of the tibiotarsus and below. The destructive character of psittacines requires all splints be protected from the beak of the bird. Clavicular-furcular and coracoid fractures in small birds may be effectively managed with coaptation splinting. In birds over 400 g body weight, open reduction is needed for best results. Since fractures of the foramen triosseum are usually not surgically repairable, they can be stabilized with coaptation splints. Although humeral fractures may be managed with coaptation in some circumstances, firm stabilization with a type I Kirschner-Ehmer splint or internal fixation is best. Single bone fracture(s) of the radius or ulna can usually be managed with minimal treatment, brailling, or figure-of-eight wraps. Fractures of both the radius and the ulna require a type I Kirschner-Ehmer splint for internal fixation. Coaptation splinting alone is usually indicated for carpal or carpometacarpal injuries. Femoral fractures in small birds may be managed with coaptation splinting, although fractures in large birds or unstable fractures

  6. Geomechanical Simulation of Fluid-Driven Fractures

    SciTech Connect

    Makhnenko, R.; Nikolskiy, D.; Mogilevskaya, S.; Labuz, J.

    2012-11-30

    The project supported graduate students working on experimental and numerical modeling of rock fracture, with the following objectives: (a) perform laboratory testing of fluid-saturated rock; (b) develop predictive models for simulation of fracture; and (c) establish educational frameworks for geologic sequestration issues related to rock fracture. These objectives were achieved through (i) using a novel apparatus to produce faulting in a fluid-saturated rock; (ii) modeling fracture with a boundary element method; and (iii) developing curricula for training geoengineers in experimental mechanics, numerical modeling of fracture, and poroelasticity.

  7. Wilsonville SRC-I pilot plant: I. Fractionation area corrosion studies; II. Hot vs. normal separation mode of operation

    SciTech Connect

    Lee, J.M.

    1981-04-01

    Extensive corrosion studies in solvent recovery columns have been done with different coals (mainly Kentucky number 9 Lafayette, Dotiki and Fies). Sodium carbonate (0.1 to 1.1% of coal) was added as neutralizer to control corrosion rate. Chloride balance runs were made for isolation of corrosive streams with high chlorine content. A caustic wash program of inlet streams has been developed for selective treatment of corrosive streams as an alternative means for possible replacement of sodium carbonate addition. High chlorine content coals such as Kentucky number 9 Lafayette and Dotiki (0.2 to 0.3%) were very corrosive, compared to low chlorine content coal, Kentucky number 9 Fies (< 0.1%). Sodium carbonate addition (0.6 to 0.7% of coal) reduced corrosion rate from 500 MPY to an insignificant level of less than 5 MPY. Caustic wash of solvents could reduce corrosion rate by 50%, removing most corrosive compounds present in the 440 to 480/sup 0/F boiling fraction. Extensive studies for the hot separator mode of operation have been done as a means of saving substantial energy by elimination of dissolver slurry cooling (0.3 MM Btu/hr) and reheating for solvent recovery (1 MM Btu/h). Impacts of the hot separator mode on plant operability, product quality and Kerr-McGee CSD Unit recovery have been studied. The hot separator mode of operation was carried out by controlling the V103 temperature to 740/sup 0/F. It was observed that preasphaltene contents increased in the SRC products such as V110 L/F SRC and CSD feed; CSD unit recovery was not affected significantly; solvent quality was not affected significantly.

  8. Motions in the interiors and atmospheres of Jupiter and Saturn. II - Barotropic instabilities and normal modes of an adiabatic planet

    NASA Technical Reports Server (NTRS)

    Ingersoll, A. P.; Miller, R. L.

    1986-01-01

    A rotating and adiabatic inviscid fluid planet possesses low frequency motions that are barotropic, quasi-geostrophic and quasi-columnar. The limiting curvature at which flow becomes unstable upon projection onto the planetary surface is negative, with an amplitude that is 3-4 times that for thin atmospheres, in planets in which density linearly decreases to zero at the surface. This result is shown to hold for all quasi-columnar perturbations. Both the phase speed of the normal mode oscillations and the barotropic stability criterion have features in common with Saturn and Jupiter oscillations.

  9. Sintering and Fracture Behavior of Plasma-sprayed Thermal Barrier Coatings

    NASA Technical Reports Server (NTRS)

    Zhu, Dongming; Choi, Sung R.; Miller, Robert A.

    2004-01-01

    Thermal barrier coatings will be more aggressively designed to protect gas turbine engine hot-section components in order to meet future engine higher fuel efficiency and lower emission goals. There is a need to characterize the fundamental sintering and fracture behavior of the current ZrO2-(7 to 8)wt%Y2O3 coating, in order to fully take advantage of the coating capability. In addition, a thorough evaluation of the coating behavior and temperature limits will be useful for more accurately assessing the benefit gained from future advanced coating systems. In this study, the sintering behavior of plasma-sprayed ZrO2-8wt%Y2O3 coatings was systematically investigated as a function of temperature and time using a dilatometer in the temperature range of 1200-1500 C. The coating sintering kinetics obtained by dilatometry were compared with the coating thermal conductivity increase kinetics, determined by a steady-state laser heat-flux testing approach, under high temperature and thermal gradient sintering conditions. The mode I, mode II, and mixed mode I-mode II fracture behavior of as-processed and sintering-annealed coatings was determined in asymmetric flexure loading at ambient and elevated temperatures in order to evaluate the coating sintering effects on the fracture envelope of K(sub I) versus K(sub II). The coating thermal conductivity cyclic response associated with the interface delamination of the coating systems under simulated engine heat-flux conditions will be discussed in conjunction with the sintering and fracture testing results.

  10. Ankle fracture - aftercare

    MedlinePlus

    Malleolar fracture; Tri-malleolar; Bi-malleolar; Distal tibia fracture; Distal fibula fracture; Malleolus fracture ... Some ankle fractures may require surgery when: The ends of the bone are out of line with each other (displaced). The ...

  11. Observing Exoplanets with High-dispersion Coronagraphy. II. Demonstration of an Active Single-mode Fiber Injection Unit

    NASA Astrophysics Data System (ADS)

    Mawet, D.; Ruane, G.; Xuan, W.; Echeverri, D.; Klimovich, N.; Randolph, M.; Fucik, J.; Wallace, J. K.; Wang, J.; Vasisht, G.; Dekany, R.; Mennesson, B.; Choquet, E.; Delorme, J.-R.; Serabyn, E.

    2017-04-01

    High-dispersion coronagraphy (HDC) optimally combines high-contrast imaging techniques such as adaptive optics/wavefront control plus coronagraphy to high spectral resolution spectroscopy. HDC is a critical pathway toward fully characterizing exoplanet atmospheres across a broad range of masses from giant gaseous planets down to Earth-like planets. In addition to determining the molecular composition of exoplanet atmospheres, HDC also enables Doppler mapping of atmosphere inhomogeneities (temperature, clouds, wind), as well as precise measurements of exoplanet rotational velocities. Here, we demonstrate an innovative concept for injecting the directly imaged planet light into a single-mode fiber, linking a high-contrast adaptively corrected coronagraph to a high-resolution spectrograph (diffraction-limited or not). Our laboratory demonstration includes three key milestones: close-to-theoretical injection efficiency, accurate pointing and tracking, and on-fiber coherent modulation and speckle nulling of spurious starlight signal coupling into the fiber. Using the extreme modal selectivity of single-mode fibers, we also demonstrated speckle suppression gains that outperform conventional image-based speckle nulling by at least two orders of magnitude.

  12. Nonaxisymmetric Dynamic Instabilities of Rotating Polytropes. II. Torques, Bars, and Mode Saturation with Applications to Protostars and Fizzlers

    NASA Astrophysics Data System (ADS)

    Imamura, James N.; Durisen, Richard H.; Pickett, Brian K.

    2000-01-01

    Dynamic nonaxisymmetric instabilities in rapidly rotating stars and protostars have a range of potential applications in astrophysics, including implications for binary formation during protostellar cloud collapse and for the possibility of aborted collapse to neutron star densities at late stages of stellar evolution (``fizzlers''). We have recently presented detailed linear analyses for polytropes of the most dynamically unstable global modes, the barlike modes. These produce bar distortions in the regions near the rotation axis but have trailing spiral arms toward the equator. In this paper, we use our linear eigenfunctions to predict the early nonlinear behavior of the dynamic instability and compare these ``quasi-linear'' predictions with several fully nonlinear hydrodynamics simulations. The comparisons demonstrate that the nonlinear saturation of the barlike instability is due to the self-interaction gravitational torques between the growing central bar and the spiral arms, where angular momentum is transferred outward from bar to arms. We also find a previously unsuspected resonance condition that accurately predicts the mass of the bar regions in our own simulations and in those published by other researchers. The quasi-linear theory makes other accurate predictions about consequences of instability, including properties of possible end-state bars and increases in central density, which can be large under some conditions. We discuss in some detail the application of our results to binary formation during protostellar collapse and to the formation of massive rotating black holes.

  13. Unbound position II in MXCXXC metallochaperone model peptides impacts metal binding mode and reactivity: Distinct similarities to whole proteins.

    PubMed

    Shoshan, Michal S; Dekel, Noa; Goch, Wojciech; Shalev, Deborah E; Danieli, Tsafi; Lebendiker, Mario; Bal, Wojciech; Tshuva, Edit Y

    2016-06-01

    The effect of position II in the binding sequence of copper metallochaperones, which varies between Thr and His, was investigated through structural analysis and affinity and oxidation kinetic studies of model peptides. A first Cys-Cu(I)-Cys model obtained for the His peptide at acidic and neutral pH, correlated with higher affinity and more rapid oxidation of its complex; in contrast, the Thr peptide with the Cys-Cu(I)-Met coordination under neutral conditions demonstrated weaker and pH dependent binding. Studies with human antioxidant protein 1 (Atox1) and three of its mutants where S residues were replaced with Ala suggested that (a) the binding affinity is influenced more by the binding sequence than by the protein fold (b) pH may play a role in binding reactivity, and (c) mutating the Met impacted the affinity and oxidation rate more drastically than did mutating one of the Cys, supporting its important role in protein function. Position II thus plays a dominant role in metal binding and transport.

  14. Ilizarov hybrid external fixation for fractures of the distal radius: Part II. Internal fixation versus Ilizarov hybrid external fixation: Stability as assessed by cadaveric simulated motion testing.

    PubMed

    Dunning, C E; Lindsay, C S; Bicknell, R T; Johnson, J A; King, G J; Patterson, S D

    2001-03-01

    The in vitro stability of an Ilizarov hybrid external fixator was compared with that of a dorsal 3.5-mm AO T-plate in 8 unpaired, fresh-frozen upper extremities. A specially designed testing device that used computer-controlled pneumatic actuators was used to simulate active finger, wrist, and forearm motions by applying loads to relevant tendons. A comminuted extra-articular distal radius fracture was modelled using a dorsally based wedge osteotomy. Fracture stability was assessed using an electromagnetic tracking device to measure motion across the fracture site after randomized application of the plate and the hybrid fixator. During simulated finger and wrist motions with the forearm pronated or supinated, motion of the distal fragment with the hybrid fixator applied was comparable to or statistically less than with the AO plate applied. During simulated forearm rotation, the stability provided by the 2 fixation types was similar, although the plate allowed statistically less radial-ulnar deviation of the fragment. In this model of a 2-part extra-articular distal radius fracture, the clinically meaningful stability of the Ilizarov hybrid external fixator was comparable to that of the dorsal AO plate.

  15. Fundamental parameters of RR Lyrae stars from multicolour photometry and Kurucz atmospheric models - II. Adaptation to double-mode stars

    NASA Astrophysics Data System (ADS)

    Barcza, S.; Benkő, J. M.

    2012-02-01

    Our photometric-hydrodynamic method is generalized to determine the fundamental parameters of multiperiodic radially pulsating stars. We report 302 UBV(RI)C Johnson-Kron-Cousins observations of GSC 4868-0831. Using these and the published photometric data of V372 Ser, we determine the metallicity, reddening, distance, mass, radius, equilibrium luminosity and effective temperature. The results underline the necessity of using multicolour photometry, including an ultraviolet band, to classify the subgroups of RR Lyrae stars properly. Our U observations might reveal that GSC 4868-0831 is a subgiant star pulsating in two radial modes and that V372 Ser is a giant star with the size and mass of an RRd star.

  16. Integrating a DNA Strand Displacement Reaction with a Whispering Gallery Mode Sensor for Label-Free Mercury (II) Ion Detection

    PubMed Central

    Wu, Fengchi; Wu, Yuqiang; Niu, Zhongwei; Vollmer, Frank

    2016-01-01

    Mercury is an extremely toxic chemical pollutant of our environment. It has attracted the world’s attention due to its high mobility and the ease with which it accumulates in organisms. Sensitive devices and methods specific for detecting mercury ions are, hence, in great need. Here, we have integrated a DNA strand displacement reaction with a whispering gallery mode (WGM) sensor for demonstrating the detection of Hg2+ ions. Our approach relies on the displacement of a DNA hairpin structure, which forms after the binding of mercury ions to an aptamer DNA sequence. The strand displacement reaction of the DNA aptamer provides highly specific and quantitative means for determining the mercury ion concentration on a label-free WGM sensor platform. Our approach also shows the possibility for manipulating the kinetics of a strand displacement reaction with specific ionic species. PMID:27483277

  17. DNA binding, DNA cleavage and cytotoxicity studies of a new water soluble copper(II) complex: The effect of ligand shape on the mode of binding

    NASA Astrophysics Data System (ADS)

    Kashanian, Soheila; Khodaei, Mohammad Mehdi; Roshanfekr, Hamideh; Shahabadi, Nahid; Mansouri, Ghobad

    2012-02-01

    The interaction of native calf thymus DNA (CT-DNA) with [Cu(ph 2phen)(phen-dione)Cl]Cl was studied at physiological pH by spectrophotometric, spectrofluorometric, circular dichroism, and viscometric techniques. Considerable hypochromicity and red shift are observed in the UV absorption band of the Cu complex. Binding constants ( Kb) of DNA with the complex were calculated at different temperatures. Thermodynamic parameters, enthalpy and entropy changes were calculated according to Van't Hoff equation, which indicated that reaction is predominantly enthalpically driven. All these results indicate that Cu(II) complex interacts with CT-DNA via intercalative mode. Also, this new complex induced cleavage in pUC18 plasmid DNA as indicated in gel electrophoresis and showed excellent antitumor activity against K562 (human chronic myeloid leukemia) and human T lymphocyte carcinoma-Jurkat cell lines.

  18. Coronal loop seismology using damping of standing kink oscillations by mode coupling. II. additional physical effects and Bayesian analysis

    NASA Astrophysics Data System (ADS)

    Pascoe, D. J.; Anfinogentov, S.; Nisticò, G.; Goddard, C. R.; Nakariakov, V. M.

    2017-04-01

    Context. The strong damping of kink oscillations of coronal loops can be explained by mode coupling. The damping envelope depends on the transverse density profile of the loop. Observational measurements of the damping envelope have been used to determine the transverse loop structure which is important for understanding other physical processes such as heating. Aims: The general damping envelope describing the mode coupling of kink waves consists of a Gaussian damping regime followed by an exponential damping regime. Recent observational detection of these damping regimes has been employed as a seismological tool. We extend the description of the damping behaviour to account for additional physical effects, namely a time-dependent period of oscillation, the presence of additional longitudinal harmonics, and the decayless regime of standing kink oscillations. Methods: We examine four examples of standing kink oscillations observed by the Atmospheric Imaging Assembly (AIA) onboard the Solar Dynamics Observatory (SDO). We use forward modelling of the loop position and investigate the dependence on the model parameters using Bayesian inference and Markov chain Monte Carlo (MCMC) sampling. Results: Our improvements to the physical model combined with the use of Bayesian inference and MCMC produce improved estimates of model parameters and their uncertainties. Calculation of the Bayes factor also allows us to compare the suitability of different physical models. We also use a new method based on spline interpolation of the zeroes of the oscillation to accurately describe the background trend of the oscillating loop. Conclusions: This powerful and robust method allows for accurate seismology of coronal loops, in particular the transverse density profile, and potentially reveals additional physical effects.

  19. Crystallographic studies of metal ion-DNA interactions: different binding modes of cobalt(II), copper(II) and barium(II) to N7 of guanines in Z-DNA and a drug-DNA complex.

    PubMed Central

    Gao, Y G; Sriram, M; Wang, A H

    1993-01-01

    Metal ion coordination to nucleic acids is not only required for charge neutralization, it is also essential for the biological function of nucleic acids. The structural impact of different metal ion coordinations of DNA helices is an open question. We carried out X-ray diffraction analyses of the interactions of the two transition metal ions Co(II) and Cu(II) and an alkaline earth metal ion Ba(II), with DNA of different conformations. In crystals, Co(II) ion binds exclusively at the N7 position of guanine bases by direct coordination. The coordination geometry around Co(II) is octahedral, although some sites have an incomplete hydration shell. The averaged Co-N7 bond distance is 2.3 A. The averaged Co-N7-C8 angle is 121 degrees, significantly smaller than the value of 128 degrees if the Co-N7 vector were to bisect the C5-N7-C8 bond angle. Model building of Co(II) binding to guanine N7 in B-DNA indicates that the coordinated waters in the axial positions would have a van der Waals clash with the neighboring base on the 5' side. In contrast, the major groove of A-DNA does not have enough room to accommodate the entire hydration shell. This suggests that Co(II) binding to either B-DNA or A-DNA may induce significant conformational changes. The Z-DNA structure of Cu(II)-soaked CGCGTG crystal revealed that the Cu(II) ion is bis-coordinated to N7 position of G10 and #G12 (# denotes a symmetry-related position) bases with a trigonal bipyramid geometry, suggesting a possible N7-Cu-N7 crosslinking mechanism. A similar bis-coordination to two guanines has also been seen in the interaction of Cu(II) in m5CGUAm5CG Z-DNA crystal and of Ba(II) with two other Z-DNA crystals. PMID:8371984

  20. Mode of opening of an oceanic pull-apart: The 20°N Basin along the Owen Fracture Zone (NW Indian Ocean)

    NASA Astrophysics Data System (ADS)

    Rodriguez, Mathieu; Chamot-Rooke, Nicolas; Fournier, Marc; Huchon, Philippe; Delescluse, Matthias

    2013-09-01

    basins are common features observed at releasing bends along major strike-slip faults. The formation and structural evolution of such basins have mostly been investigated in the continental domain and by sandbox laboratory experiments or numerical models. Here we present recently acquired multibeam bathymetry, 3.5 kHz echo sounder, and seismic profiles across the 20°N pull-apart Basin along the India-Arabia transform boundary, known as the Owen Fracture Zone (OFZ). Using nearby oceanic drilling (Deep Sea Drilling Project 222), we constrain the structural evolution of the basin since opening some 3 Myr ago. The 20°N Basin is large (90 km long and 35 km wide) despite limited transcurrent motion (~10 km). The first stage involved the formation of a step over along the OFZ and the subsequent isolation of a subsiding half graben. Extension and subsidence were further partitioned over three distinct subbasins separated by complex sets of transverse faults. The size of the basin was enhanced by gravity-driven collapse. The 20°N Basin has been a catchment for Indus turbidites since its opening, which provide a good record of syn-sedimentary deformation. The deformation related to the subsidence of the half graben mimics rollover structures commonly encountered in salt tectonics, suggesting that subsidence was accommodated by one or several décollement layers at depth. Despite a different rheological context, the subsurface structure of the nascent oceanic 20°N Basin is very similar to the more mature continental Dead Sea Basin along the Levant Fault, which also displays subbasins separated by transverse faults.

  1. Sharply notch cylindrical tension specimen for screening plane-strain fracture toughness. I - Influence of fundamental testing variables on notch strength. II Applications in aluminum alloy quality assurance of fracture toughness

    NASA Technical Reports Server (NTRS)

    Jones, M. H.; Bubsey, R. T.; Brown, W. F., Jr.; Bucci, R. J.; Collis, S. F.; Kohm, R. F.; Kaufman, J. G.

    1977-01-01

    A description is presented of studies which have been conducted to establish an improved technology base for a use of the sharply notched cylindrical specimen in quality assurance tests of aluminum alloy products. The results are presented of an investigation of fundamental variables associated with specimen preparation and testing, taking into account the influence of the notch root radius, the eccentricity of loading, the specimen diameter, and the notch depth on the sharp notch strength. Attention is given to the statistical procedures which are necessary to establish correlations between the sharp notch strength and the plane-strain fracture toughness for high-strength aluminum alloys.

  2. Interlaminar shear fracture toughness and fatigue thresholds for composite materials

    NASA Technical Reports Server (NTRS)

    Obrien, T. Kevin; Murri, Gretchen B.; Salpekar, Satish A.

    1987-01-01

    Static and cyclic end notched flexure tests were conducted on a graphite epoxy, a glass epoxy, and graphite thermoplastic to determine their interlaminar shear fracture toughness and fatigue thresholds for delamination in terms of limiting values of the mode II strain energy release rate, G-II, for delamination growth. The influence of precracking and data reduction schemes are discussed. Finite element analysis indicated that the beam theory calculation for G-II with the transverse shear contribution included was reasonably accurate over the entire range of crack lengths. Cyclic loading significantly reduced the critical G-II for delamination. A threshold value of the maximum cyclic G-II below which no delamination occurred after one million cycles was identified for each material. Also, residual static toughness tests were conducted on glass epoxy specimens that had undergone one million cycles without delamination. A linear mixed-mode delamination criteria was used to characterize the static toughness of several composite materials; however, a total G threshold criterion appears to characterize the fatigue delamination durability of composite materials with a wide range of static toughness.

  3. Interlaminar shear fracture toughness and fatigue thresholds for composite materials

    NASA Technical Reports Server (NTRS)

    O'Brien, T. Kevin; Murri, Gretchen B.; Salpekar, Satish A.

    1989-01-01

    Static and cyclic end notched flexure tests were conducted on a graphite epoxy, a glass epoxy, and graphite thermoplastic to determine their interlaminar shear fracture toughness and fatigue thresholds for delamination in terms of limiting values of the mode II strain energy release rate, G-II, for delamination growth. The influence of precracking and data reduction schemes are discussed. Finite element analysis indicated that the beam theory calculation for G-II with the transverse shear contribution included was reasonably accurate over the entire range of crack lengths. Cyclic loading significantly reduced the critical G-II for delamination. A threshold value of the maximum cyclic G-II below which no delamination occurred after one million cycles was identified for each material. Also, residual static toughness tests were conducted on glass epoxy specimens that had undergone one million cycles without delamination. A linear mixed-mode delamination criteria was used to characterize the static toughness of several composite materials; however, a total G threshold criterion appears to characterize the fatigue delamination durability of composite materials with a wide range of static toughness.

  4. Fractal patterns of fractures in granites

    USGS Publications Warehouse

    Velde, B.; Dubois, J.; Moore, D.; Touchard, G.

    1991-01-01

    Fractal measurements using the Cantor's dust method in a linear one-dimensional analysis mode were made on the fracture patterns revealed on two-dimensional, planar surfaces in four granites. This method allows one to conclude that: 1. (1)|The fracture systems seen on two-dimensional surfaces in granites are consistent with the part of fractal theory that predicts a repetition of patterns on different scales of observation, self similarity. Fractal analysis gives essentially the same values of D on the scale of kilometres, metres and centimetres (five orders of magnitude) using mapped, surface fracture patterns in a Sierra Nevada granite batholith (Mt. Abbot quadrangle, Calif.). 2. (2)|Fractures show the same fractal values at different depths in a given batholith. Mapped fractures (main stage ore veins) at three mining levels (over a 700 m depth interval) of the Boulder batholith, Butte, Mont. show the same fractal values although the fracture disposition appears to be different at different levels. 3. (3)|Different sets of fracture planes in a granite batholith, Central France, and in experimental deformation can have different fractal values. In these examples shear and tension modes have the same fractal values while compressional fractures follow a different fractal mode of failure. The composite fracture patterns are also fractal but with a different, median, fractal value compared to the individual values for the fracture plane sets. These observations indicate that the fractal method can possibly be used to distinguish fractures of different origins in a complex system. It is concluded that granites fracture in a fractal manner which can be followed at many scales. It appears that fracture planes of different origins can be characterized using linear fractal analysis. ?? 1991.

  5. DNA interaction studies of a copper (II) complex containing an antiviral drug, valacyclovir: the effect of metal center on the mode of binding.

    PubMed

    Shahabadi, Nahid; Fatahi, Parvin

    2012-07-01

    The water-soluble complex, [Cu(Val)(2)(NO(3))(2)]; in which Val = valacyclovir, an antiviral drug, has been synthesized and characterized by elemental analysis, furier transfer-infrared, hydrogen nuclear magnetic resonance (H NMR), and UV-Vis techniques. The binding of this Cu (II) complex to calf thymus DNA was investigated using fluorimetry, spectrophotometry, circular dichroism, and viscosimetry. In fluorimetric studies, the enthalpy and entropy of the reaction between the complex and calf-thymus DNA (CT-DNA) showed that the reaction is endothermic (ΔH = 208.22 kJ mol(-1); ΔS = 851.35 J mol(-1)K(-1)). The complex showed the absorption hyperchromism in its ultra violet-visible (UV-Vis) spectrum with DNA. The calculated binding constant, K(b), obtained from UV-Vis absorption studies was 2 × 10(5) M(-1). Moreover, the complex induced detectable changes in the circular dichroism spectrum of CT-DNA, as well as changes in its viscosity. The results suggest that this copper (II) complex interacts with CT-DNA via a groove-binding mode.

  6. Percutaneous screw fixation of fractures of the iliac wing and fracture-dislocations of the sacro-iliac joint (OTA Types 61-B2.2 and 61-B2.3, or Young-Burgess "lateral compression type II" pelvic fractures).

    PubMed

    Starr, Adam J; Walter, James C; Harris, Robert W; Reinert, Charles M; Jones, Alan L

    2002-02-01

    A technique for closed reduction and percutaneous screw fixation of fractures of the iliac wing and fracture-dislocations of the sacro-iliac joint is presented. Twenty-seven pelvic fractures were treated with attempted closed reduction followed by percutaneous screw fixation. Closed reduction failed in two patients. In the other twenty-five, closed reduction to within one centimeter of residual displacement was obtained, and was followed by stabilization with percutaneously placed cannulated screws. Complications included dislodgment of a screw from the superior pubic ramus in one patient, and partial cut-out of a screw along the inner cortex of the iliac wing in another. Two patients were lost to follow-up before fracture union occurred. The remaining twenty-three patients were followed-up for an average of twenty-seven months (range, 18-48 months). All of the fractures healed in the twenty-three patients who were not lost to follow-up. All but two of the patients who were working before injury returned to work. All but one of the patients was satisfied with the outcome of their pelvic fracture treatment. Closed reduction and percutaneous screw fixation of fractures of the posterior portion of the iliac wing yields acceptable reductions, with minimal blood loss and limited damage to the surrounding soft tissues.

  7. Fracture Management

    MedlinePlus

    ... to hold the fracture in the correct position. • Fiberglass casting is lighter and stronger and the exterior ... with your physician if this occurs. • When a fiberglass cast is used in conjunction with a GORE- ...

  8. Hip Fracture

    MedlinePlus

    ... make older people more likely to trip and fall — one of the most common causes of hip ... Taking steps to maintain bone density and avoid falls can help prevent hip fracture. Signs and symptoms ...

  9. CAD-II: the second version current-mode readout ASIC for high-resolution timing measurements

    NASA Astrophysics Data System (ADS)

    Yuan, Z. X.; Deng, Z.; Wang, Y.; Liu, Y. N.

    2016-07-01

    This paper presents the second version of a fully current-mode front-end ASIC, CAD (Current Amplifier and Discriminator), for MRPC detectors for TOF applications. Several upgrades have been made in this new version, including: 1). Using differential input stages with input impedance down to 30 Ω and LVDS compatible outputs; 2). Much higher current gain and bandwidth of 4.5 A/A and 380 MHz 3). Fabricated in 0.18 μ m CMOS process instead of 0.35 μ m CMOS technology used in CAD-I. The detailed design of the ASIC will be described as well as the measurement results. The single-ended input impedance could be as low as 32 Ω and the power consumption was measured to be 15 mW per channel. Input referred RMS noise current was about 0.56 μ A. The threshold could be set as low as 4.5 μ A referred to input, corresponding to 9 fC for the typical MRPC detector signal with 2 ns width. Sub-10 ps resolution has been measured for input signal above 200 μ A.

  10. Effects of Different Modes of Hot Cross-Rolling in 7010 Aluminum Alloy: Part II. Mechanical Properties Anisotropy

    NASA Astrophysics Data System (ADS)

    Mondal, Chandan; Singh, A. K.; Mukhopadhyay, A. K.; Chattopadhyay, K.

    2013-06-01

    The influence of microstructure and texture developed by different modes of hot cross-rolling on in-plane anisotropy ( A IP) of yield strength, work hardening behavior, and anisotropy of Knoop hardness (KHN) yield locus has been investigated. The A IP and work hardening behavior are evaluated by tensile testing at 0 deg, 45 deg, and 90 deg to the rolling direction, while yield loci have been generated by directional KHN measurements. It has been observed that specimens especially in the peak-aged temper, in spite of having a strong, rotated Brass texture, show low A IP. The results are discussed on the basis of Schmid factor analyses in conjunction with microstructural features, namely grain morphology and precipitation effects. For the specimen having a single-component texture, the yield strength variation as a function of orientation can be rationalized by the Schmid factor analysis of a perfectly textured material behaving as a quasi-single crystal. The work hardening behavior is significantly affected by the presence of solute in the matrix and the state of precipitation rather than texture, while yield loci derived from KHN measurements reiterate the low anisotropy of the materials. Theoretic yield loci calculated from the texture data using the visco-plastic self-consistent model and Hill's anisotropic equation are compared with that obtained experimentally.

  11. A Tropical Ocean Recharge Mechanism for Climate Variability. Part II: A Unified Theory for Decadal and ENSO Modes.

    NASA Astrophysics Data System (ADS)

    Wang, Xiaochun; Jin, Fei-Fei; Wang, Yuqing

    2003-11-01

    Decadal to interdecadal timescale variability in the Pacific region, commonly referred to as the Pacific decadal oscillation (PDO), is studied in this research using analytical and numerical models. A coupled analytical model is formulated to analyze the physical mechanism of both the PDO and ENSO. It has the equatorial β-plane dynamics of a reduced-gravity model coupled with the wind stress of fixed spatial patterns. The amplitude of the latter is proportional to the sea surface temperature (SST) anomaly in the eastern equatorial Pacific. The SST anomaly is governed by a simple thermal dynamic equation used for ENSO modeling. It is found that when a warm SST is coupled with cyclonic wind stress patterns in the eastern subtropical Pacific, an oscillation with a timescale of around 10 15 yr could be generated. In contrast, when a warm SST is coupled with only a westerly wind stress in the central equatorial Pacific, an ENSO-like oscillation could be generated with a timescale of around 3 5 yr. Thus the present research is potentially relevant to aspects of the PDO and the mechanism of the PDO may be understood as a weakly coupled decadal recharge oscillator similar to the recharge oscillator dynamics of ENSO. The sensitivity of these two kinds of coupled modes to different parameters is tested. Numerical integrations with the reduced-gravity shallow-water model in a rectangular basin and a similar coupled framework confirm the results of the analytical model.

  12. Lisfranc fractures.

    PubMed

    Wright, Amanda; Gerhart, Ann E

    2009-01-01

    Injuries of the tarsometatarsal, or Lisfranc, joint are rarely seen. Lisfranc fractures and fracture dislocations are among the most frequently misdiagnosed foot injuries in the emergency department. A misdiagnosed injury may have severe consequences including chronic pain and loss of foot biomechanics. Evaluation of a foot injury should include a high level of suspicion of a Lisfranc injury, and a thorough work-up is needed for correct diagnosis.

  13. Colles' fracture.

    PubMed

    Altizer, Linda L

    2008-01-01

    Many people "slip and fall", especially in the icy areas of the winter season. To prevent an injury to the head, most people put their hand out to hit the ground first, so the wrist usually gets injured. The most frequent injury from this type of "intervention" is a fracture to the distal radius and/or ulna, which is frequently called a "Colles' fracture."

  14. Reduction of RF accelerating voltage of Pohang Light Source-II superconducting RF cavity for stable top-up mode operation

    NASA Astrophysics Data System (ADS)

    Joo, Y.; Yu, I.; Park, I.; Chun, M. H.; Sohn, Y.

    2017-03-01

    The Pohang Light Source-II (PLS-II) is currently providing a top-up mode user-service operation with maximum available beam current of 400 mA and a beam emittance of below 10 nm-rad. The dimension of the beam bunch shortened to accomplish a low beam emittance of below 10 nm-rad from a high beam current of 400 mA increases the bunch charge density. As a result, the electron beam lifetime is significantly degraded and a high gradient of power is lost in the vacuum components of the storage ring. A study on how to reduce the bunch charge density without degrading beam emittance found that reducing the RF accelerating voltage (Vacc) can lower the bunch charge density by lengthening the bunch in the longitudinal direction. In addition, the Vacc required for stable operation with beam current of 400 mA can be reduced by lowering the external cavity quality factors (Qext values) of the superconducting cavities (SCs). To control the Qext values of SCs gradually without accessing the accelerator tunnel, a remote control motorized three-probe-tuner was installed in the transmission line of each SC. The optimum installation position of the three-probe-tuner was determined by using a finite-difference time-domain (FDTD) simulation and by experimenting on various installation positions of the three-probe-tuner. The Qext values of all the SCs were lowered to 1.40 × 105, and then, the Vacc required to store the beam current of 400 mA was decreased from 4.8 MV to 4.2 MV, which corresponds to 10% lengthening of the beam bunches. The stable operation with the reduced Vacc was confirmed during a 400 mA ten-day top-up mode user-service. Currently, the RF system of the PLS-II storage ring delivers the user-service operation with lowered Qext values to reduce the power loss at the vacuum components as well as the cryogenic heat load of SCs, and no significant problems have been found. This method of reducing the Vacc may also be applied in other synchrotron facilities.

  15. Boxer's fracture.

    PubMed

    Altizer, Linda

    2006-01-01

    Boxer's fracture is a common name for a fracture of the distal fifth metacarpal and received its name from one of its most common causes, punching an object with a closed fist. It can occur from a fistfight or from punching a hard object. The injury of a "Boxer's Fracture" earned the name from the way in which the injury occurred, punching an immovable object with a closed fist and no boxing mitt (Figure 1). Naturally, a "Boxer" usually punches his fist into his opponent's face or body. An angry person may perform the same action into a person, or into the wall. The third person may be performing a task and strike something with his fist with forceful action accidentally. In any event, if the closed fist "punches" into an immovable or firm object with force, the most frequent injury sustained would be a fracture of the fifth metacarpal neck. Some caregivers would also call a fourth metacarpal neck fracture a boxer's fracture.

  16. A Nitroxide-Tagged Platinum(II) Complex Enables the Identification of DNA G-Quadruplex Binding Mode

    PubMed Central

    Zhou, Yi-Wei; Wang, Hanqiang; Cao, Qian; Shen, Yong; Ji, Liang-Nian; Mao, Zong-Wan; Qin, Peter Z.

    2016-01-01

    We reported a novel strategy for investigating small molecule binding to G-quadruplexes (GQs). A newly synthesized dinuclear platinum(II) complex (Pt2L) containing a nitroxide radical was shown to selectively bind a GQ-forming sequence derived from human telomere (hTel). Using the nitroxide moiety as a spin label, electron paramagnetic resonance (EPR) spectroscopy was carried out to investigate binding between Pt2L and hTel GQ. Measurements indicated that two molecules of Pt2L bind with one molecule of hTel GQ. The inter-spin distance measured between the two bound Pt2L, together with molecular docking analyses, revealed that Pt2L predominately binds to the neighboring narrow and wide grooves of the G-tetrads as hTel adopts the antiparallel conformation. The design and synthesis of nitroxide tagged GQ binders, and the use of spin-labeling/EPR to investigate their interactions with GQs, will aid the development of small molecules for manipulating GQs involved in crucial biological processes. PMID:26845489

  17. An evaluation of mixed-mode delamination failure criteria

    NASA Technical Reports Server (NTRS)

    Reeder, J. R.

    1992-01-01

    Many different failure criteria have been suggested for mixed mode delamination toughness, but few sets of mixed mode data exist that are consistent over the full mode I opening to mode II shear load range. The mixed mode bending (MMB) test was used to measure the delamination toughness of a brittle epoxy composite, a state of the art toughened epoxy composite, and a tough thermoplastic composite over the full mixed mode range. To gain insight into the different failure responses of the different materials, the delamination fracture surfaces were also examined. An evaluation of several failure criteria which have been reported in the literature was performed, and the range of responses modeled by each criterion was analyzed. A new bilinear failure criterion was analyzed. A new bilinear failure criterion was developed based on a change in the failure mechanism observed from the delamination surfaces. The different criteria were compared to the failure criterion. The failure response of the tough thermoplastic composite could be modeled well with the bilinear criterion but could also be modeled with the more simple linear failure criterion. Since the materials differed in their mixed mode failure response, mixed mode delamination testing will be needed to characterize a composite material. A critical evaluation is provided of the mixed mode failure criteria and should provide general guidance for selecting an appropriate criterion for other materials.

  18. The Effects of Targeted Deliveries of Lovastatin and Tocotrienol on Ossification-Related Gene Expressions in Fracture Healing in an Osteoporosis Rat Model

    PubMed Central

    Ibrahim, Nurul ‘Izzah; Mohamed, Norazlina; Soelaiman, Ima Nirwana; Shuid, Ahmad Nazrun

    2015-01-01

    Osteoporotic drugs are used to prevent fragility fractures, but their role in fracture healing still remains unknown. Thus, alternative agents with suitable mode of delivery are needed to promote fracture healing. This study was performed to investigate the effects of direct deliveries of lovastatin and tocotrienol to fracture sites on ossification-related gene expression in fracture healing in a postmenopausal osteoporosis model. Forty-eight Sprague Dawley female rats were divided into six groups. Group I comprised the sham-operated rats, while Groups II–VI were ovariectomized rats. After 8 weeks, the right tibiae of all rats were fractured and stabilized. Group I and Group II were given two single injections of lovastatin and tocotrienol carriers. Group III was given an estrogen preparation at 64.5 µg/kg daily via oral gavages. Group IV was injected with lovastatin particles (750 µg/kg), while Group V was injected with tocotrienol particles (60 mg/kg). Group VI received two single injections of 750 µg/kg lovastatin particles and 60 mg/kg tocotrienol particles. After 4 weeks, the gene expressions were measured. Group VI showed significantly higher gene expressions of osteocalcin, BMP-2, VEGF-α, and RUNX-2 compared to Group II. In conclusion, combined treatment of lovastatin and tocotrienol upregulated the expression of genes related to fracture healing. PMID:26501302

  19. Mode-coupling approach to polymer diffusion in an unentangled melt. II. The effect of viscoelastic hydrodynamic interactions

    NASA Astrophysics Data System (ADS)

    Farago, J.; Meyer, H.; Baschnagel, J.; Semenov, A. N.

    2012-05-01

    A mode-coupling theory (MCT) version (called hMCT thereafter) of a recently presented theory [Farago, Meyer, and Semenov, Phys. Rev. Lett.PRLTAO0031-900710.1103/PhysRevLett.107.178301 107, 178301 (2011)] is developed to describe the diffusional properties of a tagged polymer in a melt. The hMCT accounts for the effect of viscoelastic hydrodynamic interactions (VHIs), that is, a physical mechanism distinct from the density-based MCT (dMCT) described in the first paper of this series. The two versions of the MCT yield two different contributions to the asymptotic behavior of the center-of-mass velocity autocorrelation function (c.m. VAF). We show that in most cases the VHI mechanism is dominant; for long chains and prediffusive times it yields a negative tail ∝-N-1/2t-3/2 for the c.m. VAF. The case of non-momentum-conserving dynamics (Langevin or Monte Carlo) is discussed as well. It generally displays a distinctive behavior with two successive relaxation stages: first -N-1t-5/4 (as in the dMCT approach), then -N-1/2t-3/2. Both the amplitude and the duration of the first t-5/4 stage crucially depend on the Langevin friction parameter γ. All results are also relevant for the early time regime of entangled melts. These slow relaxations of the c.m. VAF, thus account for the anomalous subdiffusive regime of the c.m. mean square displacement widely observed in numerical and experimental works.

  20. Microstructure and fracture behavior of F82H steel under different irradiation and tensile test conditions

    NASA Astrophysics Data System (ADS)

    Wang, K.; Dai, Y.; Spätig, P.

    2016-01-01

    Specimens of martensitic steel F82H were irradiated to doses ranging from 10.7 dpa/850 appm He to 19.6 dpa/1740 appm He at temperatures between 165 and 305 °C in the second experiment of SINQ Target Irradiation Program (STIP-II). Tensile tests were conducted at different temperatures and various fracture modes were observed. Microstructural changes including irradiation-induced defect clusters, dislocation loops and helium bubbles under different irradiation conditions were investigated using transmission electron microscopy (TEM). The deformation microstructures of tensile tested specimens were carefully examined to understand the underlying deformation mechanisms. Deformation twinning was for the first time observed in irradiated martensitic steels. A change of deformation mechanism from dislocation channeling to deformation twinning was observed when the fracture mode changed from rather ductile (quasi-cleavage) to brittle (intergranular or cleavage and intergranular mixed).

  1. Characterizing the dynamic behavior of hydraulically-induced fracture networks associated with hydraulic fracture stimulations (Invited)

    NASA Astrophysics Data System (ADS)

    Urbancic, T.; Baig, A. M.

    2013-12-01

    Seismic Moment Tensor Inversion (SMTI) analysis of microseismicity recorded with multi-well multi-array configurations allows for the potential determination of fracture growth, both spatially and temporally away from a treatment well, as well as the identification of fracture interactions within the reservoir. Based on these analyses, it may be possible to identify the role of pre-existing fracture networks in fracture development as well as, for example, failure type, fracture connectivity, and fracture intensity. Here, we present our observations based on evaluating event sequences associated with multiple injection programs in shale plays throughout North America. In our analysis we identify that, generally, local hydraulically induced variations in the stress-strain field during stimulation result in mixed-mode shear/tensile failures along predominantly pre-existing fractures/joints emplaced during current- and paleo-stress regimes rather than in the creation of new fractures. Away from treatment intervals, failures tend to be dominated by shear and are heavily influenced by the regional stress conditions. Utilizing Hudson plots (k-T), it appears that the fracture process can be further broken down into four types of activity relative to the treatment well and the start of the injection, namely initiation/reactivation of fractures (k ~ 0, double couple dominated), breakout into formation (explosive isotropic), progression of fracture from the treatment well (mostly explosive isotropic), and fracture infill behind the fracture front (decreasing k with treatment time, i.e., explosive to implosive). Breakout events comprised of crack-opening type failures followed by closure events close to the treatment well could be considered to be a canonical fracture, and that the observed behavior can be thought of as the superposition of many of these canonical fractures. Based on our observations, we suggest that by mapping these mechanisms, we can begin to delineate the

  2. Illuminating heterogeneous anisotropic upper mantle: testing a new anisotropic teleseismic body-wave tomography code - part II: Inversion mode

    NASA Astrophysics Data System (ADS)

    Munzarova, Helena; Plomerova, Jaroslava; Kissling, Edi

    2015-04-01

    necessary step before AniTomo is applied to real datasets. We examine various aspects coming along with anisotropic tomography such as setting a starting anisotropic model and parameters controlling the inversion, and particularly influence of a ray coverage on resolvability of individual anisotropic parameters. Synthetic testing also allows investigation of the well-known trade-off between effects of P-wave anisotropy and isotropic heterogeneities. Therefore, the target synthetic models are designed to represent schematically different heterogeneous anisotropic structures of the upper mantle. Testing inversion mode of the AniTomo code, considering an azimuthally quasi-equal distribution of rays and teleseismic P-wave incidences, shows that a separation of seismic anisotropy and isotropic velocity heterogeneities is plausible and that the correct orientation of the symmetry axes in a model can be found within three iterations for well-tuned damping factors.

  3. Deformation and fracture of a particle-reinforced aluminum alloy composite: Part I. Experiments

    NASA Astrophysics Data System (ADS)

    Pandey, A. B.; Majumdar, B. S.; Miracle, D. B.

    2000-03-01

    Mechanical tests were performed on a powder-metallurgically processed 7093/SiC/15p discontinuously reinforced aluminum (DRA) composite in different heat-treatment conditions, to determine the influence of matrix characteristics on the composite response. The work-hardening exponent and the strain to failure varied inversely to the strength, similar to monolithic Al alloys, and this dependence was independent of the dominant damage mode. The damage consisted of SiC particle cracks, interface and near-interface debonds, and matrix rupture inside intense slip bands. Fracture surfaces revealed particle fracture-dominated damage for most of the heat-treatment conditions, including an overaged (OA) condition that exhibited a combination of precipitates at the interface and a precipitate-free zone (PFZ) in the immediate vicinity. In the highly OA conditions and in a 450°C as-rolled condition, when the composite strength became less than 400 MPa, near-interface matrix rupture became dominant. A combination of a relatively weak matrix and a weak zone around the particle likely contributed to this damage mode over that of particle fracture. Fracture-toughness tests show that it is important to maintain a proper geometry and testing procedure to obtain valid fracture-toughness data. Overaged microstructures did reveal a recovery of fracture toughness as compared to the peak-aged (PA) condition, unlike the lack of toughness recovery reported earlier for a similar 7XXX (Al-Zn-Cu-Mg)—based DRA. The PA material exhibited extensive localization of damage and plasticity. The low toughness of the DRA in this PA condition is explored in detail, using fractography and metallography. The damage and fracture micromechanisms formed the basis for modeling the strength, elongation, toughness, and damage, which are described in Part II of this work.

  4. Fracture toughness anisotropy in shale

    NASA Astrophysics Data System (ADS)

    Chandler, Michael R.; Meredith, Philip G.; Brantut, Nicolas; Crawford, Brian R.

    2016-03-01

    The use of hydraulic fracturing to recover shale gas has focused attention on the fundamental fracture properties of gas-bearing shales, but there remains a paucity of available experimental data on their mechanical and physical properties. Such shales are strongly anisotropic, so that their fracture propagation trajectories depend on the interaction between their anisotropic mechanical properties and the anisotropic in situ stress field in the shallow crust. Here we report fracture toughness measurements on Mancos shale determined in all three principal fracture orientations: Divider, Short Transverse, and Arrester, using a modified short-rod methodology. Experimental results for a range of other sedimentary and carbonate rocks are also reported for comparison purposes. Significant anisotropy is observed in shale fracture toughness measurements at ambient conditions, with values, as high as 0.72 MPa m1/2 where the crack plane is normal to the bedding, and values as low as 0.21 MPa m1/2 where the crack plane is parallel to the bedding. For cracks propagating nonparallel to bedding, we observe a tendency for deviation toward the bedding-parallel orientation. Applying a maximum energy release rate criterion, we determined the conditions under which such deviations are more or less likely to occur under more generalized mixed-mode loading conditions. We find for Mancos shale that the fracture should deviate toward the plane with lowest toughness regardless of the loading conditions.

  5. Effects of through-the-thickness stitching on impact and interlaminar fracture properties of textile graphite/epoxy laminates

    NASA Technical Reports Server (NTRS)

    Sharma, Suresh K.; Sankar, Bhavani V.

    1995-01-01

    This study investigated the effects of through-the-thickness stitching on impact damage resistance, impact damage tolerance, and mode I and mode II fracture toughness of textile graphite/epoxy laminates. Uniweave resin-transfer-molded 48 ply graphite/epoxy (AS4/3501-6) laminates were stitched with Kevlar and glass yarns of different linear densities and stitch spacings. Delaminations were implanted during processing to simulate impact damage. Sublaminate buckling tests were performed to determine the effects of stitching on the compressive strength. The results showed outstanding improvements of up to 400 percent in the compression strength over the unstitched laminates. In impact and static indentation tests the onset of damage occurred at the same level, but the extent of damage was less in stitched laminates. Mode I fracture toughness of 24 ply Uniweave unidirectional (AS4/3501-6) stitched laminates was measured by conducting double-cantilever-beam tests. The critical strain energy release rate (G(sub Ic)) was found to be up to 30 times higher than the unstitched laminates. Mode II fracture toughness of the Uniweave laminates was measured by performing end-notched-flexure tests. Two new methods to compute the apparent G(sub IIc) are presented. The apparent G(sub IIc) was found to be at least 5-15 times higher for the stitched laminates.

  6. Modeling fracture porosity evolution in dolostone

    NASA Astrophysics Data System (ADS)

    Gale, Julia F. W.; Lander, Robert H.; Reed, Robert M.; Laubach, Stephen E.

    2010-09-01

    Opening-mode fractures in dolostones buried to depths of ˜1-5 km contain synkinematic dolomite cement, the amount and internal structure of which has a systematic relationship to fracture size. Narrow fractures (<0.01 mm) typically seal completely with either massive cement or cement with a crack-seal texture that indicates multiple incremental openings. Wider fractures can preserve considerable effective porosity, but anomalously thick dolomite cement bridges are commonly present in fractures that are otherwise lined with a thin veneer of cement. Dolomite bridges resemble quartz bridges that are common in fractured sandstones. We developed a geometric crystal growth model for synkinematic dolomite fracture fill in fractured dolostones, where periodic incremental fracture-opening events are introduced with concurrent cement growth. We assumed constant temperature and supersaturation with respect to dolomite. A key assumption in the model is that rapid dolomite accumulation within bridges is governed by high cement-growth rates on repeatedly broken grain surfaces during the process of crack seal. Slower cement-growth rates occur on euhedral crystals. This assumption is made on the basis of a comparison with quartz cement growth in fractured sandstones. Simulations with different fracture-opening rates mimic bridge and lining cement morphologies, including characteristic rhombic shapes of dolomite bridges.

  7. Fracture types (1) (image)

    MedlinePlus

    ... fracture which goes at an angle to the axis Comminuted - a fracture of many relatively small fragments Spiral - a fracture which runs around the axis of the bone Compound - a fracture (also called ...

  8. Hydraulic fracturing-1

    SciTech Connect

    Not Available

    1990-01-01

    This book contains papers on hydraulic fracturing. Topics covered include: An overview of recent advances in hydraulic fracturing technology; Containment of massive hydraulic fracture; and Fracturing with a high-strength proppant.

  9. Molecular recognition modes between adenine or adeniniun(1+) ion and binary M(II)(pdc) chelates (MCoZn; pdc=pyridine-2,6-dicarboxylate(2-) ion).

    PubMed

    Del Pilar Brandi-Blanco, María; Choquesillo-Lazarte, Duane; Domínguez-Martín, Alicia; Matilla-Hernández, Antonio; González-Pérez, Josefa María; Castiñeiras, Alfonso; Niclós-Gutiérrez, Juan

    2013-10-01

    Mixed ligand M(II)-complexes (MCoZn) with pyridine-2,6-dicarboxylate(2-) chelator (pdc) and adenine (Hade) have been synthesized and studied by X-ray diffraction and other spectral and thermal methods: [Cu(pdc)(H(N9)ade)(H2O)] (1), [Cu2(pdc)2(H2O)2(μ2-N3,N7-H(N9)ade)]·3H2O (2), trans-[M(pdc)(H(N9)ade)(H2O)2]·nH2O for MCo (3-L, 3-M, 3-H) or Zn (4-L, 4-H), where n is 0, 1 or 3 for the 'lowest' (L), 'medium' (M) and 'highest' (H) hydrated forms, and the salt trans-[Ni(pdc)(H2(N1,N9)ade)(H2O)2]Cl·2H2O (5). In all the nine compounds, both neutral and cationic adenine exist as their most stable tautomer and the molecular recognition pattern between the metal-pdc chelates and the adenine or adeninium(1+) ligands involves the MN7 bond in cooperation with an intra-molecular N6H⋯O(coordinated carboxylate) interligand interaction. In addition the dinuclear copper(II) compound (2) has the CuN3 bond and the N9H⋯O(coord. carboxylate) interaction. The structures of mononuclear ternary complexes proved that the molecular recognition pattern is the same irrespective of (a) the coordination geometry of the complex molecule, (b) the different hydrated forms of crystals with Co or Zn, and (c) the neutral of cationic form of the adenine ligand. These features are related to the mer-NO2 chelating ligand conformation (imposed by the planar rigidity of pdc) as a driving force for the observed metal binding mode.

  10. Ferrocene and (arene)ruthenium(II) complexes of the natural anticancer naphthoquinone plumbagin with enhanced efficacy against resistant cancer cells and a genuine mode of action.

    PubMed

    Spoerlein-Guettler, Cornelia; Mahal, Katharina; Schobert, Rainer; Biersack, Bernhard

    2014-09-01

    A series of ferrocene and (arene)ruthenium(II) complexes attached to the naturally occurring anticancer naphthoquinones plumbagin and juglone was tested for efficacy against various cancer cell lines and for alterations in the mode of action. The plumbagin ferrocene and (p-cymene)Ru(II) conjugates 1c and 2a overcame the multi-drug drug resistance of KB-V1/Vbl cervix carcinoma cells and showed IC50 (72 h) values around 1 μM in growth inhibition assays using 3-(4,5-dimethyl-2-yl)-2,5-diphenyltetrazolium bromide (MTT). They were further investigated for their influence on the cell cycle of KB-V1/Vbl and HCT-116 colon carcinoma cells, on the generation of reactive oxygen species (ROS) by the latter cell line, for their substrate character for the P-glycoprotein drug eflux pump via the calcein-AM efflux assays, and for DNA affinity by the electrophoretic mobility shift assay (EMSA). The derivatives 1c and 2a increased the number of dead cancer cells (sub-G0/G1 fraction) in a dose- and time-dependent manner. ROS levels were significantly increased upon treatment with 1c and 2a. These compounds also showed a greater affinity to linear DNA than plumbagin. While plumbagin did not affect calcein-AM transport by P-glycoprotein the derivatives 1c and 2a exhibited a 50% or 80% inhibition of the P-glycoprotein-mediated calcein-AM efflux relative to the clinically established sensitizer verapamil.

  11. The influence of mode of delivery, obstetric analgesia and anaesthesia on the response of isolated human chorionic plate arteries to angiotensin II.

    PubMed

    Odum, C U; Pipkins, F B

    1989-01-01

    A six point concentration: response curved of the contractile effect of angiotensin II (AII) on helically-cut strips of human chorionic plate artery strips were established at final concentrations of between 10(-14) to 10(-9) M. The tissues were obtained from the placentae of primigravid patients who had normal pregnancy, and also from those with pregnancy induced hypertension (PIH). The tissue response were then related to mode of delivery, obstetric analgesia, and anaesthesia. A total of 36 chorionic plate arteries from 12 primigravid patients were studied. i) The overall initial EC50s of the tissues ranged from 8.0 x 10(-13) M and 4.5 x 10(-13) M. The tissues from PIH patients were significantly more sensitive to AII, when compared with tissues from the normotensive subjects (P greater than or equal to 0.01 less than or equal to 0.05). ii) The tissues from epidural vaginal deliveries were also significantly more sensitive to AII, than those from both normal vaginal deliveries and caesarean deliveries respectively. The median gradients of the semi-log transformed concentration response curved were 2.4 +/- 0.18; 1.27 +/- 0.37, and 1.5 +/- 0.49, for epidural, Caeserean and normal vaginal deliveries respectively. iii) It is suggested that whilst Lumbar epidural analgesia may be of great value in pain relief in labour and in the control of intrapartum hypertension in pre-eclampsia, this procedure may be associated with hypersensitivity and perhaps vasospasm of the placental vasculature to vasoactive agents invivo.

  12. FRACTURED PETROLEUM RESERVOIRS

    SciTech Connect

    Abbas Firoozabadi

    1999-06-11

    The four chapters that are described in this report cover a variety of subjects that not only give insight into the understanding of multiphase flow in fractured porous media, but they provide also major contribution towards the understanding of flow processes with in-situ phase formation. In the following, a summary of all the chapters will be provided. Chapter I addresses issues related to water injection in water-wet fractured porous media. There are two parts in this chapter. Part I covers extensive set of measurements for water injection in water-wet fractured porous media. Both single matrix block and multiple matrix blocks tests are covered. There are two major findings from these experiments: (1) co-current imbibition can be more efficient than counter-current imbibition due to lower residual oil saturation and higher oil mobility, and (2) tight fractured porous media can be more efficient than a permeable porous media when subjected to water injection. These findings are directly related to the type of tests one can perform in the laboratory and to decide on the fate of water injection in fractured reservoirs. Part II of Chapter I presents modeling of water injection in water-wet fractured media by modifying the Buckley-Leverett Theory. A major element of the new model is the multiplication of the transfer flux by the fractured saturation with a power of 1/2. This simple model can account for both co-current and counter-current imbibition and computationally it is very efficient. It can be orders of magnitude faster than a conventional dual-porosity model. Part II also presents the results of water injection tests in very tight rocks of some 0.01 md permeability. Oil recovery from water imbibition tests from such at tight rock can be as high as 25 percent. Chapter II discusses solution gas-drive for cold production from heavy-oil reservoirs. The impetus for this work is the study of new gas phase formation from in-situ process which can be significantly

  13. Intubation Biomechanics: Laryngoscope Force and Cervical Spine Motion during Intubation in Cadavers—Cadavers vs. Patients, the Effect of Repeated Intubations, and the Effect of Type II Odontoid Fracture on C1-C2 Motion

    PubMed Central

    Hindman, Bradley J.; From, Robert P.; Fontes, Ricardo B.; Traynelis, Vincent C.; Todd, Michael M.; Zimmerman, M. Bridget; Puttlitz, Christian M.; Santoni, Brandon G.

    2015-01-01

    Introduction The aims of this study were to characterize: 1) cadaver intubation biomechanics, including the effect of repeated intubations; and 2) the relationship between intubation force and the motion of an injured cervical segment. Methods Fourteen cadavers were serially intubated using force-sensing Macintosh and Airtraq laryngoscopes in random order, with simultaneous cervical spine motion recorded with lateral fluoroscopy. Motion of the C1-C2 segment was measured in the intact and injured state (Type II odontoid fracture). Injured C1-C2 motion was proportionately corrected for changes in intubation forces that occurred with repeated intubations. Results Cadaver intubation biomechanics were comparable to those of patients in all parameters other than C2-C5 extension. In cadavers, intubation force (Set 2/Set1 force ratio = 0.61 [95% CI: 0.46, 0.81]; P=0.002) and Oc-C5 extension (Set 2 –Set 1 difference = −6.1 degrees [95% CI: −11.4, −0.9]; P=0.025) decreased with repeated intubations. In cadavers, C1-C2 extension did not differ: 1) between intact and injured states; or 2) in the injured state, between laryngoscopes (with and without force correction). With force correction, in the injured state, C1-C2 subluxation was greater with the Airtraq (mean difference 2.8 mm [95% CI: 0.7, 4.9 mm]; P=0.004). Discussion With limitations, cadavers may be clinically relevant models of intubation biomechanics and cervical spine motion. In the setting of a Type II odontoid fracture, C1-C2 motion during intubation with either the Macintosh or Airtraq does not appear to greatly exceed physiologic values or to have a high likelihood of hyperextension or direct cord compression. PMID:26288267

  14. Fracture healing in osteoporotic bone.

    PubMed

    Cheung, Wing Hoi; Miclau, Theodore; Chow, Simon Kwoon-Ho; Yang, Frank F; Alt, Volker

    2016-06-01

    As the world population rises, osteoporotic fracture is an emerging global threat to the well-being of elderly patients. The process of fracture healing by intramembranous ossification or/and endochondral ossification involve many well-orchestrated events including the signaling, recruitment and differentiation of mesenchymal stem cells (MSCs) during the early phase; formation of a hard callus and extracellular matrix, angiogenesis and revascularization during the mid-phase; and finally callus remodeling at the late phase of fracture healing. Through clinical and animal research, many of these factors are shown to be impaired in osteoporotic bone. Animal studies related to post-menopausal estrogen deficient osteoporosis (type I) have shown healing to be prolonged with decreased levels of MSCs and decreased levels of angiogenesis. Moreover, the expression of estrogen receptor (ER) was shown to be delayed in ovariectomy-induced osteoporotic fracture. This might be related to the observed difference in mechanical sensitivity between normal and osteoporotic bones, which requires further experiments to elucidate. In mice fracture models related to senile osteoporosis (type II), it was observed that chondrocyte and osteoblast differentiation were impaired; and that transplantation of juvenile bone marrow would result in enhanced callus formation. Other factors related to angiogenesis and vasculogenesis have also been noted to be impaired in aged models, affecting the degradation of cartilaginous matrixes and vascular invasion; the result is changes in matrix composition and growth factors concentrations that ultimately impairs healing during age-related osteoporosis. Most osteoporotic related fractures occur at metaphyseal sites clinically, and reports have indicated that differences exist between diaphyseal and metaphyseal fractures. An animal model that satisfies three main criteria (metaphyseal region, plate fixation, osteoporosis) is suggested for future research for

  15. Control over the Self-Assembly Modes of Pt(II) Complexes by Alkyl Chain Variation: From Slipped to Parallel π-Stacks.

    PubMed

    Allampally, Naveen Kumar; Mayoral, María José; Chansai, Sarayute; Lagunas, María Cristina; Hardacre, Christopher; Stepanenko, Vladimir; Albuquerque, Rodrigo Q; Fernández, Gustavo

    2016-06-01

    We report the self-assembly of a new family of hydrophobic, bis(pyridyl) Pt(II) complexes featuring an extended oligophenyleneethynylene-derived π-surface appended with six long (dodecyloxy (2)) or short (methoxy (3)) side groups. Complex 2, containing dodecyloxy chains, forms fibrous assemblies with a slipped arrangement of the monomer units (dPt⋅⋅⋅Pt ≈14 Å) in both nonpolar solvents and the solid state. Dispersion-corrected PM6 calculations suggest that this organization is driven by cooperative π-π, C-H⋅⋅⋅Cl and π-Pt interactions, which is supported by EXAFS and 2D NMR spectroscopic analysis. In contrast, nearly parallel π-stacks (dPt⋅⋅⋅Pt ≈4.4 Å) stabilized by multiple π-π and C-H⋅⋅⋅Cl contacts are obtained in the crystalline state for 3 lacking long side chains, as shown by X-ray analysis and PM6 calculations. Our results reveal not only the key role of alkyl chain length in controlling self-assembly modes but also show the relevance of Pt-bound chlorine ligands as new supramolecular synthons.

  16. Condylar fractures.

    PubMed

    Sawhney, Raja; Brown, Ryan; Ducic, Yadranko

    2013-10-01

    The purpose of this article is to review the basic indications for different treatments of condylar and subcondylar fractures. It also reviews the steps of different surgical approaches to access the surgical area and explains the pros and cons of each procedure.

  17. Type IIA Monteggia Fracture Dislocation with Ipsilateral Distal Radius Fracture in Adult – A Rare Association

    PubMed Central

    James, Boblee

    2016-01-01

    Monteggia fracture constitutes about 5-10% of the forearm fractures. Monteggia fracture by definition is proximal ulnar fracture with disruption of proximal radioulnar joint. Bado classified Monteggia fracture dislocation into four types and Jupiter subclassified type II Bado’s fractures into four types. The associated injury in the form of distal radial fractures and distal humerus fractures are rare though many cases of distal radial physeal injuries have been reported in paediatric population. Hereby we report a rare association of type IIA Monteggia fracture dislocation with ipsilateral distal radius fracture in an adult patient. This case report also highlights on proper examination and full length radiographs of forearm to avoid missing injury at wrist in cases of elbow injuries. Management of such complex injuries included open reduction and internal fixation of olecronon fracture, distal radius fracture and radial head resection. Functional outcome at six months was good at wrist whereas at elbow, stiffness was a major concern with elbow range of movement from 40°-110°. PMID:27656518

  18. [Triple fracture of the shoulder suspensory complex].

    PubMed

    Tamimi Mariño, I; Martin Rodríguez, I; Mora Villadeamigo, J

    2013-01-01

    The superior suspensory complex of the shoulder (SSCS) is a ring shaped structure composed of bones and soft tissues that play a fundamental role in the stability of the shoulder joint. Isolated injuries of the SSCS are relatively common, but injuries that affect 3 components are extremely unusual. We present a triple injury of the SSCS in a 26 year old patient with a Neer type ii clavicular fracture, a Kuhn type iii acromion fracture and an Ogawa type i coracoid fracture. An open reduction and stabilization of the clavicle was performed with 2 Kirschner nails. The acromial fracture was synthesized with 2 cannulated screws, and the coracoid fracture was treated conservatively. After 24 months of follow up the patient had an excellent functional outcome according to the Constat-Murley shoulder score and QuickDASH scoring system, and all the fractures healed correctly.

  19. Posterior talar fracture with dislocation of both talo-navicular and subtalar joints: a variant type II of the Sneppens classification

    PubMed Central

    Galanopoulos, Ilias; Fogg, Quentin; Ashwood, Neil

    2012-01-01

    A 63-year-old man fell from a ladder, thus causing an axial compression injury to the right ankle. Severe deformity was evident and the ankle could not be reduced by simple manipulation. The skin was tented and appearing critically contused. Radiographs revealed an oblique fracture of the posterior aspect of the talar body with dislocation of both the talo-navicular and subtalar joints, an injury previously not described in the literature. The fracture–dislocation was anatomically reduced within 3 h of presentation and stability achieved with two headless buried compression screws. CT scan confirmed anatomical reduction and the patient remained non-weight bearing in a cast for 6 weeks. One year postoperatively, the patient remains pain-free with no radiological signs of avascular necrosis of the talus. This injury is unique and despite its severity and soft tissue compromise good quality reduction and internal fixation resulted in an excellent clinical outcome. PMID:22847568

  20. Traitement chirurgical d'une luxation fracture parcellaire de la tete femorale pipkin II irreductible: à propos d'un cas

    PubMed Central

    Abid, Hatim; Mechchat, Atif; El Idrissi, Mohammed; Shimi, Mohammed; El Ibrahimi, Abdelhalim; El Mrini, Abdelmajid

    2014-01-01

    L'irréductibilité d'une luxation-fracture parcellaire de la tête fémorale est une entité pathologique rare dont le traitement est chirurgical. Dans la littérature, les avis des auteurs divergent concernant le choix de la voie d'abord, mais la conservation du fragment céphalique est la règle. Indépendamment de la qualité de la prise en charge, les résultats mauvais et passables sont très importants estimés à 50% au bout de 10 ans, et l’évolution arthrosique à long terme semble être inéluctable. PMID:25489358

  1. Fracture behaviour of polycrystalline tungsten

    NASA Astrophysics Data System (ADS)

    Gaganidze, Ermile; Rupp, Daniel; Aktaa, Jarir

    2014-03-01

    Fracture behaviour of round blank polycrystalline tungsten was studied by means of three point bending Fracture-Mechanical (FM) tests at temperatures between RT and 1000 °C and under high vacuum. To study the influence of the anisotropic microstructure on the fracture toughness (FT) and ductile-to-brittle transition (DBT) the specimens were extracted in three different, i.e. longitudinal, radial and circumferential orientations. The FM tests yielded distinctive fracture behaviour for each specimen orientation. The crack propagation was predominantly intergranular for longitudinal orientation up to 600 °C, whereas transgranular cleavage was observed at low test temperatures for radial and circumferentially oriented specimens. At intermediate test temperatures the change of the fracture mode took place for radial and circumferential orientations. Above 800 °C all three specimen types showed large ductile deformation without noticeable crack advancement. For longitudinal specimens the influence of the loading rate on the FT and DBT was studied in the loading rate range between 0.06 and 18 MPa m1/2/s. Though an increase of the FT was observed for the lowest loading rate, no resolvable dependence of the DBT on the loading rate was found partly due to loss of FT validity. A Master Curve approach is proposed to describe FT vs. test temperature data on polycrystalline tungsten. Fracture safe design space was identified by analysis compiled FT data.

  2. Optimizing Shear Stresses at the Tip of a Hydraulic Fracture - What Is the Ideal Orientation of Natural Fractures with respect to Hydraulic Fracture?

    NASA Astrophysics Data System (ADS)

    Sheibani, F.; Hager, B. H.

    2015-12-01

    While many shale and unconventional plays are naturally fractured (or contain planes of weakness), these are often cemented and effectively impermeable to flow. Stress shadow behind the tip of a hydraulic fracture stablizes natural fractures. It essentially means that if impermeable natural fractures and weakness planes are not opened when the hydraulic fracture tip passes, they will remain closed and impermeable to flow. In this work a detailed and comprehensive evaluation of tip shear stresses and associated natural fracture or weakness plane shear is presented. From analytical work, the theoretical shear stresses from a fracture tip are first presented. The effect of fracture length, in-situ pore pressure, maximum horizontal remote stress, net pressure, natural fracture friction coefficient and the direction of natural fracture with respect to the hydraulic fracture on shear stimulation at the tip are calculated using the plane strain analytical solution of a 2-D fracture, and assuming simple linear coulomb friction law. Since slippage along natural fractures will locally violate the assumptions used in the analytical solutions and to incorporate the effect of weakness planes on stress-strain and displacement field, 2-D and 3-D finite element model (FEM) simulations are presented that build upon both the analytical and continuum solutions. FEM models are capable of numerically simulating the slippage through weakness planes by using contact elements. This advantage makes FEM tools very appropriate for synthetically generating microseismicity, which can then be evaluated for mode, focal mechanism, and magnitude. The results of the simulations highlight the critical parameters involved in shearing and opening cemented natural fractures in unconventionals - which is a critical component of stimulation and production optimization for these plays. According to the results, the ideal orientation of natural fractures with respect to hydraulic fracture from shear

  3. Fracture Interface Waves in an Anisotropic Medium

    NASA Astrophysics Data System (ADS)

    Pyrak-Nolte, L. J.; Shao, S.; Abell, B.

    2011-12-01

    The detection of fractures in an anisotropic medium is complicated by discreet modes that are guided or confined by fractures and that travel with velocities close (~92%) to the shear wave velocity. For instance, fractures can mask the presence of textural anisotropy in a rock, and can increase the apparent shear wave velocity anisotropy. In this study, we examine how fracture interface waves affect the interpretation of shear wave velocities for two orthogonal polarizations propagating parallel to the layers. Samples with textural anisotropy measuring 100 x 100 x 100 mm were fabricated from garolite, an epoxy - cloth laminate, with layer thickness on the order of 0.5 mm. Three fracture samples were created with: (1) a fracture oriented parallel to layering, (2) a fracture oriented perpendicular to layering, and (3) two intersecting orthogonal fractures. An intact sample without fractures was used a standard. A seismic array, consisting of source and receiver arrays, was used to perform full waveform measurements. Each array contained two compressional and five shear wave piezoelectric contact transducers with a central frequency of 1 MHz. Shear wave transducers were polarized both perpendicular and parallel to the layering as well as to the fracture. Measurements were made for a range of stresses (0.4 - 4MPa). When the shear wave was polarized parallel to a fracture, the shear wave traveled at the bulk shear velocity respective to the layering. However, when the shear wave was polarized perpendicular to a fracture, the measured velocity ranged between the Rayleigh wave velocity at low stress and the bulk shear wave at high stress. The shear wave velocities perpendicular and parallel to the layering (propagation direction parallel to the layers) were ~1500 m/s and ~1600 m/s, respectively, in the intact sample. However, in the fractured samples, the observed shear wave anisotropy depended on the stress and fracture orientation relative to the layering. When the

  4. Are Carotid Stent Fractures Clinically Significant?

    SciTech Connect

    Garcia-Toca, Manuel; Rodriguez, Heron E.; Naughton, Peter A.; Keeling, Aiofee; Phade, Sachin V.; Morasch, Mark D.; Kibbe, Melina R.; Eskandari, Mark K.

    2012-04-15

    Purpose: Late stent fatigue is a known complication after carotid artery stenting (CAS) for cervical carotid occlusive disease. The purpose of this study was to determine the prevalence and clinical significance of carotid stent fractures. Materials and Methods: A single-center retrospective review of 253 carotid bifurcation lesions treated with CAS and mechanical embolic protection from April 2001 to December 2009 was performed. Stent integrity was analyzed by two independent observers using multiplanar cervical plain radiographs with fractures classified into the following types: type I = single strut fracture; type II = multiple strut fractures; type III = transverse fracture; and type IV = transverse fracture with dislocation. Mean follow-up was 32 months. Results: Follow-up imaging was completed on 106 self-expanding nitinol stents (26 closed-cell and 80 open-cell stents). Eight fractures (7.5%) were detected (type I n = 1, type II n = 6, and type III n = 1). Seven fractures were found in open-cell stents (Precise n = 3, ViVEXX n = 2, and Acculink n = 2), and 1 fracture was found in a closed-cell stent (Xact n = 1) (p = 0.67). Only a previous history of external beam neck irradiation was associated with fractures (p = 0.048). No associated clinical sequelae were observed among the patients with fractures, and only 1 patient had an associated significant restenosis ({>=}80%) requiring reintervention. Conclusions: Late stent fatigue after CAS is an uncommon event and rarely clinically relevant. Although cell design does not appear to influence the occurrence of fractures, lesion characteristics may be associated risk factors.

  5. Frequency-Dependent Fracture Specific Stiffness

    NASA Astrophysics Data System (ADS)

    Pyrak-Nolte, L. J.; Folz, M. A.; Acosta-Colon, A.

    2003-12-01

    Monitoring the hydraulic properties of fractures remotely through their seismic signatures is an important goal for field hydrology. Empirical studies have shown that the hydraulic properties of a fracture are implicitly related to the fracture specific stiffness through the amount and distribution of contact area and apertures that arise from two rough surfaces in contact. Complicating this simple picture are seismic measurements that indicate frequency-dependent stiffness, i.e., a scale-dependent fracture stiffness where the scale is set by the wavelength. Thus relating the hydraulic properties of fractures to seismic measurements becomes a scale dependent problem. We have performed laboratory experiments to examine the phenomenon of frequency dependent fracture specific stiffness to aid in the assessment of the hydraulic properties of a fracture using seismic techniques. To this end, we have developed a photolithographic technique with which we can construct synthetic fractures of known fracture geometry with feature sizes controlled over several orders of magnitude. The synthetic fracture (and the control non-fractured samples) are made from acrylic cylinders that measure 15.0 cm in diameter by 7.7 cm in height. The diameter of the samples enables us to sample the acoustic properties of the fracture using acoustic lens over regions that range in scale from 10 mm to 60 mm. A confinement cell controls the normal stress on the fracture. Seismic measurements were made with broadband compressional-mode piezoelectric transducers enabling one-order of magnitude in frequency. We found that when the wavelength is smaller than the asperity size, a linear dependence of fracture specific stiffness on frequency occurs. In this geometric ray regime the asymptotic value of the transmission function provides a direct measure of the contact area of the fracture. On the other hand, when the asperity spacing is less than an eighth of a wavelength, the fracture behaves as a

  6. Facial Fractures

    PubMed Central

    White, Lawrence M.; Marotta, Thomas R.; McLennan, Michael K.; Kassel, Edward E.

    1992-01-01

    Appropriate clinical radiographic investigation, together with an understanding of the normal radiographic anatomy of the facial skeleton, allows for precise delineation of facial fracutres and associated soft tissue injuries encountered in clinical practice. A combination of multiple plain radiographic views and coronal and axial computed tomographic images allow for optimal delineation of fracture patterns. This information is beneficial in the clinical and surgical management patients with facial injuries

  7. Electron Microscopy Used for Fracture Mode Identification,

    DTIC Science & Technology

    1980-06-01

    joint from the Infantry Fighting Vehicle (IFV). The U-Joint was case carburized and was in service for a total of 474 miles when failure occurred...device provides etching-cleaning of samples by immersing the work in a charged plasma field. Organic material is removed as is some of the base

  8. Damage mechanisms and failure modes of cortical bone under components of physiological loading.

    PubMed

    George, W T; Vashishth, D

    2005-09-01

    Fatigue damage development in cortical bone was investigated in vitro under different mechanical components of physiological loading including tension, compression, and torsion. During each test, stress and strain data were collected continuously to monitor and statistically determine the occurrence of the primary, secondary, and tertiary stages associated with fatigue and/or creep failure of bone. The resultant microdamage and failure modes were identified by histological and fractographic analysis, respectively. The tensile group demonstrated Mode I cracking and the three classic stages of fatigue and creep suggesting a low crack initiation threshold, steady crack propagation and final failure by coalescence of microcracks. In contrast, the compressive group displayed Mode II cracking and a two-stage fatigue behavior with limited creep suggesting a high crack initiation threshold followed by a sudden fracture. The torsion group also displayed a two-stage fatigue profile but demonstrated extensive damage from mixed mode (Modes II and III) microcracking and predominant time-dependent damage. Thus, fatigue behavior of bone was found to be uniquely related to the individual mechanical components of physiological loading and the latter determined the specific damage mechanisms associated with fatigue fracture.

  9. Low Cycle Fatigue Behavior of 316LN Stainless Steel Alloyed with Varying Nitrogen Content. Part II: Fatigue Life and Fracture Behavior

    NASA Astrophysics Data System (ADS)

    Prasad Reddy, G. V.; Sandhya, R.; Sankaran, S.; Mathew, M. D.

    2014-10-01

    Influence of nitrogen content on low cycle fatigue life and fracture behavior of 316LN stainless steel (SS) alloyed with 0.07 to 0.22 wt pct nitrogen is presented in this paper over a range of total strain amplitudes ( ±0.25 to 1.0 pct) in the temperature range from 773 K to 873 K (500 °C to 600 °C). The combined effect of nitrogen and strain amplitude on fatigue life is observed to be complex i.e., fatigue life either decreases/increases with increase in nitrogen content or saturates/peaks at 0.14 wt pct N depending on strain amplitude and temperature. Coffin-Manson plots (CMPs) revealed both single-slope and dual-slope strain-life curves depending on the test temperature and nitrogen content. 316LN SS containing 0.07 and 0.22 wt pct N showed nearly single-slope CMP at all test temperatures, while 316LN SS with 0.11 and 0.14 wt pct N exhibited marked dual-slope behavior at 773 K (500 °C) that changes to single-slope behavior at 873 K (600 °C). The changes in slope of CMP are found to be in good correlation with deformation substructural changes.

  10. Fracture surfaces of irradiated composites

    NASA Technical Reports Server (NTRS)

    Milkovich, Scott M.; Sykes, George F., Jr.; Herakovich, Carl T.

    1987-01-01

    Electron microscopy was used to analyze the fracture surfaces of T300/934 graphite/epoxy unidirectional off-axis tensile coupons which were subjected to 1.0-MeV electron radiation at a rate of 50 Mrad/h for a total dose of 10 Grad. Fracture surfaces from irradiated and nonirradiated specimens tested at 116 K, room temperature, and 394 K were analyzed to assess the influence of radiation and temperature on the mode of failure and variations in constituent material as a function of environmental exposure. Micrographs of fracture surfaces indicate that irradiated specimens are more brittle than nonirradiated specimens at low temperatures. However, at elevated temperatures the irradiated specimens exhibit significantly more plasticity than nonirradiated specimens.

  11. Fracture toughness and the effects of stress state on fracture of nickel aluminides

    NASA Technical Reports Server (NTRS)

    Lewandowski, John J.; Michal, Gary M.; Locci, Ivan; Rigney, Joseph D.

    1991-01-01

    The effects of stress state on the fracture behavior of Ni3Al, Ni3Al + B, and NiAl were determined using either notched or fatigue-precracked bend bars tested to failure at room temperature, in addition to testing specimens in tension under superposed hydrostatic pressure. Although Ni3Al is observed to fail in a macroscopically brittle intergranular manner in tension tests conducted at room temperature, the fracture toughnesses presently obtained on Ni3Al exceeded 20 MPam, and R-curve behavior was exhibited. In situ monitoring of the fracture experiments was utilized to aid in interpreting the source(s) of the high toughness in Ni3Al, while SEM fractography was utilized to determine the operative fracture modes. The superposition by hydrostatic pressure during tensile testing of NiAl specimens was observed to produce increased ductility without changing the fracture mode.

  12. Influence of ceramic thickness and ceramic materials on fracture resistance of posterior partial coverage restorations.

    PubMed

    Bakeman, E M; Rego, N; Chaiyabutr, Y; Kois, J C

    2015-01-01

    This study evaluated the influence of ceramic thickness and ceramic materials on fracture resistance of posterior partial coverage ceramic restorations. Forty extracted molars were allocated into four groups (n=10) to test for two variables: 1) the thickness of ceramic (1 mm or 2 mm) and 2) the ceramic materials (a lithium disilicate glass-ceramic [IPS e.max] or leucite-reinforced glass ceramic [IPS Empress]). All ceramic restorations were luted with resin cement (Variolink II) on the prepared teeth. These luted specimens were loaded to failure in a universal testing machine, in the compression mode, with a crosshead speed of 1.0 mm/min. The data were analyzed using two-way analysis of variance and the Tukey Honestly Significantly Different multiple comparison test (α =0.05). The fracture resistance revealed a significant effect for materials (p<0.001); however, the thickness of ceramic was not significant (p=0.074), and the interaction between the thickness of ceramic and the materials was not significant (p=0.406). Mean (standard deviation) fracture resistance values were as follows: a 2-mm thickness of a lithium disilicate bonded to tooth structure (2505 [401] N) revealed a significantly higher fracture resistance than did a 1-mm thickness of leucite-reinforced (1569 [452] N) and a 2-mm thickness of leucite-reinforced ceramic bonded to tooth structure (1716 [436] N) (p<0.05). There was no significant difference in fracture resistance values between a lithium disilicate ceramic at 1-mm thickness (2105 [567] N) and at 2-mm thickness. Using a lithium disilicate glass ceramic for partial coverage restoration significantly improved fracture resistance compared to using a leucite-reinforced glass ceramic. The thickness of ceramic had no significant effect on fracture resistance when the ceramics were bonded to the underlying tooth structure.

  13. Aspects of the Fracture Toughness of Carbon Nanotube Modified Epoxy Polymer Composites

    NASA Astrophysics Data System (ADS)

    Mirjalili, Vahid

    .% of Single Walled CNT (SWNT). Finally, the CNT-modified epoxy resin was used to manufacture carbon fibre laminates by resin film infusion and prepreg technologies. The Mode I and Mode II delamination properties of the CNT-modified composite increased by 140% and 127%, respectively. In contrast, this improvement was not observed for the base CNT-modified polymers, used to manufacture the composite laminates. A qualitative analysis of the fractured surface using a Scanning Electron Microscope revealed a good dispersion in the composites samples, confirming the importance of processing to harness the full potential of carbon nanotubes for toughening polymer composites.

  14. Fracture Mechanics

    DTIC Science & Technology

    1974-01-31

    2219 -T851 aluminum (fractures at low stresses). The parameter KF is alloy compact specimens 1 2 and demonstrate consistent a function of specimen...Congress of 20. Walker, E. K., "The Effect of Stress Ratio Applied Mechanics, 1924. During Crack Propagation and Fatigue for 2024-T3 and 7015- T6 Aluminum ...34Stress- Corrosion Cracking in 12. Kaufman, J. G., and Nelson, F. G., "More Ti-6A1-4V Titanium Alloy in Nitrogen Tetroxide," on Specimen Size Effect in 2219

  15. Radial head fracture - aftercare

    MedlinePlus

    Elbow fracture - radial head - aftercare ... to 2 weeks. If you have a small fracture and your bones did not move around much, ... to see a bone doctor (orthopedic surgeon). Some fractures require surgery to: Insert pins and plates to ...

  16. Hand fracture - aftercare

    MedlinePlus

    ... this page: //medlineplus.gov/ency/patientinstructions/000552.htm Hand fracture - aftercare To use the sharing features on ... need to be repaired with surgery. Types of Hand Fractures Your fracture may be in one of ...

  17. Chopart fractures.

    PubMed

    Klaue, Kaj

    2004-09-01

    The Chopart articular space was described by François Chopart (1743-1795) as a practical space for amputations in cases of distal foot necrosis. It corresponds to the limit between the anatomical hind-foot and the mid-foot. The bones involved are the talus and the calcaneus proximally, and the navicular and the cuboid distally. This space thus holds two functionally distinct entities, the anterior part of the coxa pedis (an essential functional joint) and the calcaneo-cuboidal joint,which can be considered to be an "adaptive joint" within a normal foot. Trauma to this region may cause fractures and/or dislocations and, in high energy trauma,compartment syndromes. Principles of treatment are immediate reduction of dislocations and realignment of the medial and lateral column of the foot in length and orientation. Open reduction and internal fixation of talus and navicular fractures are often indicated to restore the "coxa pedis". Open reconstruction or fusion in correct length of the calcaneo-cuboidal joint is occasionally indicated. Salvage procedures in malunions include navicular osteotomies and calcaneo-cuboidal bone block fusions. Treatment of joint destructions, especially involving the talo-navicular joint, include triple arthrodesis.

  18. Optimal scaling in ductile fracture

    NASA Astrophysics Data System (ADS)

    Fokoua Djodom, Landry

    This work is concerned with the derivation of optimal scaling laws, in the sense of matching lower and upper bounds on the energy, for a solid undergoing ductile fracture. The specific problem considered concerns a material sample in the form of an infinite slab of finite thickness subjected to prescribed opening displacements on its two surfaces. The solid is assumed to obey deformation-theory of plasticity and, in order to further simplify the analysis, we assume isotropic rigid-plastic deformations with zero plastic spin. When hardening exponents are given values consistent with observation, the energy is found to exhibit sublinear growth. We regularize the energy through the addition of nonlocal energy terms of the strain-gradient plasticity type. This nonlocal regularization has the effect of introducing an intrinsic length scale into the energy. We also put forth a physical argument that identifies the intrinsic length and suggests a linear growth of the nonlocal energy. Under these assumptions, ductile fracture emerges as the net result of two competing effects: whereas the sublinear growth of the local energy promotes localization of deformation to failure planes, the nonlocal regularization stabilizes this process, thus resulting in an orderly progression towards failure and a well-defined specific fracture energy. The optimal scaling laws derived here show that ductile fracture results from localization of deformations to void sheets, and that it requires a well-defined energy per unit fracture area. In particular, fractal modes of fracture are ruled out under the assumptions of the analysis. The optimal scaling laws additionally show that ductile fracture is cohesive in nature, i.e., it obeys a well-defined relation between tractions and opening displacements. Finally, the scaling laws supply a link between micromechanical properties and macroscopic fracture properties. In particular, they reveal the relative roles that surface energy and microplasticity

  19. Mechanical behavior and fracture characteristics of off-axis fiber composites. 1: Experimental investigation. [at the Lewis Research Center

    NASA Technical Reports Server (NTRS)

    Sinclair, J. H.; Chamis, C. C.

    1977-01-01

    The mechanical behavior, fracture surfaces, and fracture modes of unidirectional high-modulus graphite-fiber/epoxy composites subjected to off-axis tensile loads were investigated experimentally. The investigation included the generation of stress-strain-to-fracture data and scanning electron microscope studies of the fractured surfaces. The results led to the identification of fracture modes and distinct fracture surface characteristics for off-axis tensile loading. The results also led to the formulation of critical for identifying and characterizing these fracture modes and their associated fracture surfaces. The results presented and discussed herein were used in the theoretical investigation and comparisons described in Part 2. These results should also provide a good foundation for identifying, characterizing, and quantifying fracture modes in both off-axis and angle-plied laminates.

  20. Energy Partitioning of Seismic Waves in Fractured Rocks

    SciTech Connect

    1997-08-31

    Advances in locating and characterizes fractures in oil and gas reservoirs, and at waste isolation sites from seismic surveys requires improved interpretation methods. Experimental and theoretical results from this work have lead to an understanding of diagnostic signatures of energy that is partitioned into body waves and guided modes by fractures. Compressional waves and shear waves (i.e., shear waves with particle motion perpendicular to the fracture plane) are sensitive to changes in shear stress on a pre-existing fracture and to the formation of a fracture in a previously intact specimen. Both types of waves exhibit a shift in frequency content and a change in the amplitude of the wave as a fracture is formed or a pre-existing fracture is closed. The dispersion characteristics of interfact waves that propagate along a fracture enable quantification of fracture specific stiffness. A new compressional-mode interface wave was measured that has the potential for becoming a diagnostic tool for changes in stress in a fracture. The results of this research provide the basis for the development of seismic imaging techniques and analyses tools for locating and characterizing fractures on the field scale.

  1. Mechanics and fracture of hybrid material interface bond

    NASA Astrophysics Data System (ADS)

    Wang, Jialai

    Considering current and future applications of hybrid materials and structures in civil engineering, the strength and durability of interface bond between the conventional materials and composites are critical to development of such products. Conventional methods mostly used for analysis of isotropic materials may not be well suitable or accurate enough for a system made of anisotropic materials with relatively low shear stiffness. A need exists for developing more accurate and explicit analytical solutions for hybrid material interface analysis and related novel experimental characterization techniques. In this study, a combined analytical and experimental approach to characterize hybrid material interface bond is developed. Using a shear deformable plate theory and an elastic interface model, a mechanics approach for interface analysis of hybrid material bond under general loading is first proposed. The resulting closed-form solution of interface stress distribution is used to compute strain energy release rate (SERB) and stress intensity factor (SIF) of the interface with or without adhesive bond. This approach is then extended to delamination of composite structures under generic loading conditions. Second, novel experimental approaches for characterization of hybrid material bonded interfaces are presented. To account for the crack tip deformations, a tapered beam on elastic foundation (TBEF) is developed. Based on the TBEF model, analysis and design of two novel fracture specimens, Tapered Double Cantilever Beam (TDCB) and Tapered End Notched Flexure (TENF), are proposed, and they are effectively used in fracture toughness tests of bonded interface under Mode-I and Mode-II loadings, respectively. A constant compliance rate change over certain crack length range is achieved for the TDCB and TENF specimens, and it alleviates the necessity of experimental compliance calibration tests. The fracture toughness data obtained from the experiments are useful to

  2. Fracture Toughness Determination of Cracked Chevron Notched Brazilian Disc Rock Specimen via Griffith Energy Criterion Incorporating Realistic Fracture Profiles

    NASA Astrophysics Data System (ADS)

    Xu, Yuan; Dai, Feng; Zhao, Tao; Xu, Nu-wen; Liu, Yi

    2016-08-01

    The cracked chevron notched Brazilian disc (CCNBD) specimen has been suggested by the International Society for Rock Mechanics to measure the mode I fracture toughness of rocks, and has been widely adopted in laboratory tests. Nevertheless, a certain discrepancy has been observed in results when compared with those derived from methods using straight through cracked specimens, which might be due to the fact that the fracture profiles of rock specimens cannot match the straight through crack front as assumed in the measuring principle. In this study, the progressive fracturing of the CCNBD specimen is numerically investigated using the discrete element method (DEM), aiming to evaluate the impact of the realistic cracking profiles on the mode I fracture toughness measurements. The obtained results validate the curved fracture fronts throughout the fracture process, as reported in the literature. The fracture toughness is subsequently determined via the proposed G-method originated from Griffith's energy theory, in which the evolution of the realistic fracture profile as well as the accumulated fracture energy is quantified by DEM simulation. A comparison between the numerical tests and the experimental results derived from both the CCNBD and the semi-circular bend (SCB) specimens verifies that the G-method incorporating realistic fracture profiles can contribute to narrowing down the gap between the fracture toughness values measured via the CCNBD and the SCB method.

  3. Numerical Investigation of Fracture Propagation in Geomaterials

    NASA Astrophysics Data System (ADS)

    Newell, P.; Borowski, E.; Major, J. R.; Eichhubl, P.

    2015-12-01

    Fracture in geomaterials is a critical behavior that affects the long-term structural response of geosystems. The processes involving fracture initiation and growth in rocks often span broad time scales and size scales, contributing to the complexity of these problems. To better understand fracture behavior, the authors propose an initial investigation comparing the fracture testing techniques of notched three-point bending (N3PB), short rod (SR), and double torsion (DT) on geomaterials using computational analysis. Linear softening cohesive fracture modeling (LCFM) was applied using ABAQUS to computationally simulate the three experimental set-ups. By applying material properties obtained experimentally, these simulations are intended to predict single-trace fracture growth. The advantages and limitations of the three testing techniques were considered for application to subcritical fracture propagation taking into account the accuracy of constraints, load applications, and modes of fracture. This work is supported as part of the Geomechanics of CO2 Reservoir Seals, a DOE-NETL funded under Award Number DE-FOA-0001037. Sandia National Laboratories is a multi-program laboratory managed and operated by Sandia Corporation, a wholly owned subsidiary of Lockheed Martin Corporation, for the U.S. Department of Energy's National Nuclear Security Administration under contract DE-AC04-94AL85000.

  4. Studies in interactive communication. II - The effects of four communication modes on the linguistic performance of teams during cooperative problem solving

    NASA Technical Reports Server (NTRS)

    Chapanis, A.; Parrish, R. N.; Ochsman, R. B.; Weeks, G. D.

    1977-01-01

    Two-man teams solved credible, 'real world' problems for which computer assistance has been or could be useful. Conversations were carried on in one of four modes of communication: typewriting, handwriting, voice, and natural unrestricted communication. Performance was assessed on three classes of dependent measures: time to solution, behavioral measures of activity, and linguistic measures. Significant differences among the communication modes were found in each of the three classes. This paper is concerned mainly with the results of the linguistic analyses. Linguistic performance was assessed with 182 measures, most of which turned out to be redundant and some of which were useless or meaningless. Those that remain show that although problems can be solved faster in the oral modes than in the hard-copy modes, the oral modes are characterized by many more messages, sentences, words, and unique words; much higher communication rates; but lower type-token ratios. Although a number of significant problem and job-role effects were found, there were relatively few significant interactions of modes with thsse variables. It appears, therefore, that the mode effects hold for both problems and for both job roles assigned to the subjects.

  5. Dynamical response of the Galileo Galilei on the ground rotor to test the equivalence principle: Theory, simulation, and experiment. II. The rejection of common mode forces

    NASA Astrophysics Data System (ADS)

    Comandi, G. L.; Toncelli, R.; Chiofalo, M. L.; Bramanti, D.; Nobili, A. M.

    2006-03-01

    "Galileo Galilei on the ground" (GGG) is a fast rotating differential accelerometer designed to test the equivalence principle (EP). Its sensitivity to differential effects, such as the effect of an EP violation, depends crucially on the capability of the accelerometer to reject all effects acting in common mode. By applying the theoretical and simulation methods reported in Part I of this work, and tested therein against experimental data, we predict the occurrence of an enhanced common mode rejection of the GGG accelerometer. We demonstrate that the best rejection of common mode disturbances can be tuned in a controlled way by varying the spin frequency of the GGG rotor.

  6. Dynamical response of the Galileo Galilei on the ground rotor to test the equivalence principle: Theory, simulation, and experiment. II. The rejection of common mode forces

    SciTech Connect

    Comandi, G.L.; Toncelli, R.; Chiofalo, M.L.; Bramanti, D.; Nobili, A.M.

    2006-03-15

    'Galileo Galilei on the ground' (GGG) is a fast rotating differential accelerometer designed to test the equivalence principle (EP). Its sensitivity to differential effects, such as the effect of an EP violation, depends crucially on the capability of the accelerometer to reject all effects acting in common mode. By applying the theoretical and simulation methods reported in Part I of this work, and tested therein against experimental data, we predict the occurrence of an enhanced common mode rejection of the GGG accelerometer. We demonstrate that the best rejection of common mode disturbances can be tuned in a controlled way by varying the spin frequency of the GGG rotor.

  7. Effect of Natural Fractures on Hydraulic Fracturing

    NASA Astrophysics Data System (ADS)

    Ben, Y.; Wang, Y.; Shi, G.

    2012-12-01

    Hydraulic Fracturing has been used successfully in the oil and gas industry to enhance oil and gas production in the past few decades. Recent years have seen the great development of tight gas, coal bed methane and shale gas. Natural fractures are believed to play an important role in the hydraulic fracturing of such formations. Whether natural fractures can benefit the fracture propagation and enhance final production needs to be studied. Various methods have been used to study the effect of natural fractures on hydraulic fracturing. Discontinuous Deformation Analysis (DDA) is a numerical method which belongs to the family of discrete element methods. In this paper, DDA is coupled with a fluid pipe network model to simulate the pressure response in the formation during hydraulic fracturing. The focus is to study the effect of natural fractures on hydraulic fracturing. In particular, the effect of rock joint properties, joint orientations and rock properties on fracture initiation and propagation will be analyzed. The result shows that DDA is a promising tool to study such complex behavior of rocks. Finally, the advantages of disadvantages of our current model and future research directions will be discussed.

  8. The effect of low-intensity therapeutic ultrasound in induced fracture of rat tibiae

    PubMed Central

    Fontes-Pereira, Aldo José; Teixeira, Renato da Costa; de Oliveira, Antônio Jorge Barbosa; Pontes, Roberto Waldesmand Farias; de Barros, Rui Sérgio Monteiro; Negrão, José Nazareno Cunha

    2013-01-01

    OBJECTIVE: To analyze the possible effects of low-intensity ultrasound on induced tibia fracture of rats in a dose commonly used in physical therapy treatments. METHODS: Twenty male Wistar rats were divided into two groups with 10 animals each. In the ultrasound group (USG), the animals were submitted to bone fracture and treatment with therapeutic ultrasound (TUS). Ultrasonic parameters are: frequency of 1.0 MHz, intensity of 0.2 W/cm2, pulsed mode at 20%, applied in stationary form during 10 minutes on the fracture region, for five weeks. The control group (CG) was submitted to bone fracture but not treated with ultrasound. RESULTS: The radiographies showed better consolidation in USG compared to CG. The statistical tests for alkaline phosphatase and serum calcium did not show significant difference between groups. CONCLUSION: According to this study, TUS, applied with these parameters (not commonly used for bone therapy) accelerates bone healing, confirmed by radiography, yet the biochemical analysis was not conclusive. One reason for this inconsistency may have been some inadequacy of the biochemical protocol, currently under investigation. Level of Evidence II, Prospective comparative study. PMID:24453637

  9. Tibial spine fractures: an analysis of outcome in surgically treated type III injuries.

    PubMed

    Mulhall, K J; Dowdall, J; Grannell, M; McCabe, J P

    1999-05-01

    We analysed the outcome of open reduction and internal fixation of type III tibial spine fractures, assessing treatment and determining a treatment protocol. A total of 10 patients presented over 3 years to our institution with a mean age of 15 years (range 10-21), a male-to-female ratio of 8:2. left to right 6:4 and anterior to posterior spine fracture 9:1. Only one patient had associated meniscal injury noted at arthroscopy (no treatment required). The mode of injury was road traffic accidents four, sports injuries three and falls three. The mean follow-up was 9 months. There were seven excellent results and three good results. Those patients with good results exhibited either minimal quadriceps weakness, extensor lag (< 10 degrees) or antero-posterior laxity. This reflects the experience of other authors in dealing with these injuries in younger patients. There is widespread agreement that types I and II should be treated by plaster cast alone and that is also the policy at our institution. We recommend a routine treatment protocol in type III injuries of (1) examination under anaesthesia, (2) arthroscopy (evaluating the fracture, cruciate integrity and other associated injuries), (3) open reduction and screw fixation and (4) vigorous physiotherapy/rehabilitation of all type III fractures, as we feel this provides the best possible outcome in these injuries.

  10. In vitro study to compare impact fracture resistance of intact root-treated teeth.

    PubMed

    McDonald, A V; King, P A; Setchell, D J

    1990-11-01

    The aim of this in vitro study was to determine the effect on impact fracture resistance of three methods for restoration of root-treated lower incisor teeth with otherwise intact natural crowns. In a control group (Group I) laterally condensed gutta-percha filled the entire root canal, whereas part of the root filling was removed to enable insertion of a 1 mm diameter post in the other two groups. Stainless steel posts were placed in Group II and experimental carbon fibre reinforced carbon (CFRC) in Group III. A composite resin luting agent was used to lute the posts, and standardized composite resin restorations were placed in each access cavity. Fifteen specimens of each group were tested to failure with a single impact force applied at 90 degrees to the mid-point inciso-cervically on the labial surface. The peak force, peak energy, and first peak total energy required to fracture each specimen were recorded. The results showed no significant difference between the three groups, nor was a difference in the mode or site of fracture observed. The results suggested that there is no advantage from the point of view of fracture mechanics in 'restoring' intact root-treated teeth with either stainless steel or carbon fibre reinforced carbon rods.

  11. The copper(II) and zinc(II) coordination mode of HExxH and HxxEH motif in small peptides: the role of carboxylate location and hydrogen bonding network.

    PubMed

    Grasso, Giuseppe; Magrì, Antonio; Bellia, Francesco; Pietropaolo, Adriana; La Mendola, Diego; Rizzarelli, Enrico

    2014-01-01

    Copper(II) and zinc(II) complexes with two hexapeptides encompassing HExxH and HxxEH motif were characterized by means of a combined experimental and theoretical approach. Parallel tempering and density functional theory (DFT) investigations show the presence of different hydrogen bonding networks between the copper(II) and zinc(II) complexes with the two peptides, suggesting a significant contribution of these non-covalent interactions to the stability constant values. The glutamate carboxylate group has a direct role in metal ion binding. The location of this amino acid along the sequence of the investigated peptides is critical to determine thermodynamic and spectroscopic features of the copper(II) complex species, whereas is less relevant in the zinc(II) complexes formation. Electrospray ionization mass spectrometry (ESI-MS) characterization of the zinc(II) complex species show that in the [ZnH-2L] two deprotonated amide nitrogen atoms are involved in the metal coordination environment, an uncommon behavior in zinc(II) complexes for multi-histidine ligands.

  12. Coordination mode of pentadentate ligand derivative of 5-amino-1,3,4-thiadiazole-2-thiol with nickel(II) and copper(II) metal ions: Synthesis, spectroscopic characterization, molecular modeling and fungicidal study

    NASA Astrophysics Data System (ADS)

    Chandra, Sulekh; Gautam, Seema; Kumar, Amit; Madan, Molly

    2015-02-01

    Complexes of nickel(II), and copper(II) were synthesized with pantadentate ligand i.e. 3,3‧-thiodipropionicacid-bis(5-amino-1,3,4-thiadiazole-2-thiol) (L). The ligand was synthesized by the condensation of thiodipropionic acid and 5-amino-1,3,4-thiadiazole-2-thiol in 1:2 ratio, respectively. Synthesized ligand was characterized by elemental analysis, mass, 1H NMR, IR, and molecular modeling. All the complexes were characterized by elemental analysis, molar conductance, magnetic moment, IR, electronic spectra, ESR, and molecular modeling. The newly synthesized complexes possessed general composition [M(L)X2] where M = Ni(II), Cu(II), L = pantadentate ligand and X = Cl-, CH3COO-. The IR spectral data indicated that the ligand behaved as a pantadentate ligand and coordinated to the metal ion through N2S3 donor atoms. The molar conductance value of Ni(II), and Cu(II) complexes in DMSO corresponded to their electrolytic behavior. On the basis of spectral study, octahedral and tetragonal geometry was assigned for Ni(II) and Cu(II) complexes, respectively. In vitro fungicidal study of ligand and its complexes was investigated against fungi Candida albicans, Candida parapsilosis, Candidia krusei, and Candida tropicalis by means of well diffusion method.

  13. Coordination mode of pentadentate ligand derivative of 5-amino-1,3,4-thiadiazole-2-thiol with nickel(II) and copper(II) metal ions: synthesis, spectroscopic characterization, molecular modeling and fungicidal study.

    PubMed

    Chandra, Sulekh; Gautam, Seema; Kumar, Amit; Madan, Molly

    2015-02-05

    Complexes of nickel(II), and copper(II) were synthesized with pantadentate ligand i.e. 3,3'-thiodipropionicacid-bis(5-amino-1,3,4-thiadiazole-2-thiol) (L). The ligand was synthesized by the condensation of thiodipropionic acid and 5-amino-1,3,4-thiadiazole-2-thiol in 1:2 ratio, respectively. Synthesized ligand was characterized by elemental analysis, mass, (1)H NMR, IR, and molecular modeling. All the complexes were characterized by elemental analysis, molar conductance, magnetic moment, IR, electronic spectra, ESR, and molecular modeling. The newly synthesized complexes possessed general composition [M(L)X2] where M = Ni(II), Cu(II), L = pantadentate ligand and X = Cl(-), CH3COO(-). The IR spectral data indicated that the ligand behaved as a pantadentate ligand and coordinated to the metal ion through N2S3 donor atoms. The molar conductance value of Ni(II), and Cu(II) complexes in DMSO corresponded to their electrolytic behavior. On the basis of spectral study, octahedral and tetragonal geometry was assigned for Ni(II) and Cu(II) complexes, respectively. In vitro fungicidal study of ligand and its complexes was investigated against fungi Candida albicans, Candida parapsilosis, Candidia krusei, and Candida tropicalis by means of well diffusion method.

  14. Determination of interfacial fracture toughness of bone–cement interface using sandwich Brazilian disks

    PubMed Central

    Tong, J.; Wong, K.Y.; Lupton, C.

    2007-01-01

    The long-term stability of cemented total hip replacements critically depends on the lasting integrity of the bond between bone and bone cement. Conventionally, the bonding strength of bone–cement is obtained by mechanical tests that tend to produce a large variability between specimens and test methods. In this work, interfacial fracture toughness of synthetic bone–cement interface has been studied using sandwiched Brazilian disk specimens. Experiments were carried out using polyurethane foams as substrates and a common bone cement as an interlayer. Selected loading angles from 0° to 25° were used to achieve full loading conditions from mode I to mode II. Finite element analyses were carried out to obtain the solutions for strain energy release rates at given phase angles associated with the experimental models. The effects of crack length on the measured interfacial fracture toughness were examined. Microscopic studies were also carried out to obtain the morphology of the fractured interfaces at selected loading angles. The implication of the results on the assessment of fixation in acetabular replacements is discussed in the light of preliminary work on bovine cancellous bone–cement interface. PMID:19330043

  15. A new, model-free calculation method to determine the coordination modes and distribution of copper(II) among the metal binding sites of multihistidine peptides using circular dichroism spectroscopy.

    PubMed

    Osz, Katalin

    2008-12-01

    A new calculation method to determine microscopic protonation processes from CD spectra measured at different pH and Cu(II):ligand ratios was developed and used to give the relative binding strengths for the three histidines of hsPrP(84-114), a 31-mer polypeptide modeling the N-terminal copper(II) binding region of human (homo sapiens) prion protein. Mutants of hsPrP(84-114) with two or one histidyl residues have also been synthesized and their copper(II) complexes studied by CD spectroscopy. The 1-His models were analyzed first, and the molar CD spectra for the different coordination modes on the different histidines were calculated using the general computational program PSEQUAD. These spectra were deconvoluted into the sum of Gaussian curves and used as a first parameter set to calculate the molar spectra for the different coordination modes (3N and 4N coordination) and coordination positions (His85, His96 and His111) of the 2-His peptides. The calculation method therefore does not require the direct use of CD spectra measured in the smaller peptide models. This is a significant improvement over earlier calculation methods. In the same runs, the stepwise deprotonation pK(mic) values were refined and the pH-dependent distribution of copper(II) between the two histidines was determined. The results revealed the high, but different copper(II) binding affinities of the three separate histidines in the following order: His85 < His96His111. The calculation also showed that molar CD spectra which belong to the same coordination mode and coordination position in different ligands have very similar transition energies but different intensities. For this reason, direct transfer of molar CD spectra between different ligands may be a source of error, but the pK(mic) values and the copper(II) binding preferences are transferable from the 2-His peptides to the 3-His hsPrP(84-114).

  16. Achondrogenesis type II (Langer-Saldino)--a case report.

    PubMed

    Swar, M O; Srikrishna, B V

    1995-09-01

    Achondrogenesis is a lethal form of congenital chondrodystophy characterised by extreme micromelia. Definitive clinical and radiographic criteria have been established to differentiate Type II Achondrogenesis (Langer-Saldino) from type I Achondrogenesis (Parenti-Fraccaro). The mode of inheritance is autosomal recessive for both types. We are presenting a case of Type II Achondrogenesis, a still born male to consanguinous parents. The clinical features included an enlarged head, protuberant abdomen and short stubby limbs. The mother had earlier delivered two still born males presumably with similar features. Radiographic characteristics of absence of rib fractures and well ossified iliac bones with concave medial margins and absent or deficient ossification of the sacrum, ischiae, and pubic bones differentiated Type II Achondrogenesis from Type I Achondrogenesis.

  17. Can the spinal instability neoplastic score prior to spinal radiosurgery predict compression fractures following stereotactic spinal radiosurgery for metastatic spinal tumor?: a post hoc analysis of prospective phase II single-institution trials.

    PubMed

    Lee, Sun-Ho; Tatsui, Claudio E; Ghia, Amol J; Amini, Behrang; Li, Jing; Zavarella, Salvatore M; Tannir, Nizar M; Brown, Paul D; Rhines, Laurence D

    2016-02-01

    The aim of this study was to determine the predictability of vertebral compression fracture (VCF) development applying the spinal instability neoplastic score (SINS) prior to delivery of stereotactic spinal radiosurgery (SSRS) for spinal metastases. From two prospective cohorts of SSRS for spinal metastases, we selected patients with a low degree of cord compression or cauda equine from C3 to S1 and analyzed 79 patients enrolled according to binary SINS criteria. The primary endpoint was the development of a de novo VCF or progression of an existing fracture after SSRS. We identified 32 fractures (40.5%): 19 de novo and 13 progressive. The mean time to fracture after SSRT was 3.3 months (range, 0.4-34.1 months). In 41 patients with low SINS (0-6), 7 patients (17.1%) developed a fracture after SSRS. In 38 patients with high SINS (7-12), 25 (65.8%) developed a fracture. Among the 32 fractures, 15 were symptomatic. Patients with high SINS were more likely to experience symptomatic fractures (31.6%) than were patients with lower SINS (7.4%). On univariate and multivariate analysis, 24-month fracture-free rates were 78.7 and 33.7% in low and high SINS group, respectively and high SINS was found to be a significant risk factor for VCFs and symptomatic fractures (respectively, HR 5.6, p = 0.04; HR 5.3, p = 0.01). SINS is a useful tool for predicting the development of VCF after SSRS for spinal metastases. Prophylactic cement augmentation should not be considered for patients with lower SINS, since the risk of fracture is low.

  18. [Periprosthetic Acetabulum Fractures].

    PubMed

    Schreiner, A J; Stuby, F; de Zwart, P M; Ochs, B G

    2016-12-01

    In contrast to periprosthetic fractures of the femur, periprosthetic fractures of the acetabulum are rare complications - both primary fractures and fractures in revision surgery. This topic is largely under-reported in the literature; there are a few case reports and no long term results. Due to an increase in life expectancy, the level of patients' activity and the number of primary joint replacements, one has to expect a rise in periprosthetic complications in general and periprosthetic acetabular fractures in particular. This kind of fracture can be intra-, peri- or postoperative. Intraoperative fractures are especially associated with insertion of cementless press-fit acetabular components or revision surgery. Postoperative periprosthetic fractures of the acetabulum are usually related to osteolysis, for example, due to polyethylene wear. There are also traumatic fractures and fractures missed intraoperatively that lead to some kind of insufficiency fracture. Periprosthetic fractures of the acetabulum are treated conservatively if the implant is stable and the fracture is not dislocated. If surgery is needed, there are many possible different surgical techniques and challenging approaches. That is why periprosthetic fractures of the acetabulum should be treated by experts in pelvic surgery as well as revision arthroplasty and the features specific to the patient, fracture and prosthetic must always be considered.

  19. Peculiar double-periodic pulsation in RR Lyrae stars of the OGLE collection - II. Short-period stars with a dominant radial fundamental mode

    NASA Astrophysics Data System (ADS)

    Prudil, Z.; Smolec, R.; Skarka, M.; Netzel, H.

    2017-03-01

    We report the discovery of a new group of double-periodic stars in the OGLE Galactic bulge photometry. In 38 stars identified as fundamental-mode RR Lyrae and four classified as first-overtone RR Lyrae, we detected an additional shorter periodicity. The periods of the dominant variability in the newly discovered group are 0.28 < PD < 0.41 d. Period ratios (0.68-0.72) are smaller than the period ratios of the Galactic bulge RRd stars. The typical amplitude ratio (of the additional to the dominant periodicity) is 20 per cent for the stars identified as fundamental-mode RR Lyrae and 50 per cent for stars classified as first-overtone RR Lyrae. 10 stars from our sample exhibit equidistant peaks in the frequency spectrum, which suggests the Blazhko-type modulation of the main pulsation frequency and/or additional periodicity. The Fourier coefficients R21 and R31 are some of the lowest among fundamental-mode RR Lyrae stars, but among the highest for the first-overtone pulsators. For the phase Fourier coefficients φ21 and φ31, our stars lie between RRab and RRc stars. The stars discussed were compared with radial linear pulsation models. Their position in the Petersen diagram cannot be reproduced by assuming that two radial modes are excited and their physical parameters are like those characteristic of RR Lyrae stars. The non-radial-mode scenario also faces difficulties. We conclude that the dominant variability is most likely due to pulsation in the radial fundamental mode, which applies to stars classified as first-overtone mode pulsators. At this point, we cannot explain the nature of the additional periodicity. Even more, the classification of the stars as RR Lyrae should be treated as tentative.

  20. Analysis of the structural parameters that influence gas production from the Devonian shale. Annual progress report, 1979-1980. Volume II. Data repository and reports published during fiscal year 1979-1980: regional structure, surface structure, surface fractures, hydrology

    SciTech Connect

    Negus-De Wys, J.; Dixon, J. M.; Evans, M. A.; Lee, K. D.; Ruotsala, J. E.; Wilson, T. H.; Williams, R. T.

    1980-10-01

    This volume comprises appendices giving regional structure data, surface structure data, surface fracture data, and hydrology data. The fracture data covers oriented Devonian shale cores from West Virginia, Ohio, Virginia, Pennsylvania, and Kentucky. The subsurface structure of the Eastern Kentucky gas field is also covered. (DLC)

  1. Multiscale rotational mechanism of fracture propagation in geomaterials

    NASA Astrophysics Data System (ADS)

    Dyskin, Arcady; Pasternak, Elena; Esin, Maxim

    2015-10-01

    We consider rotational mechanism of macrocrack propagation based on breakage of the bonds between mutually rotating grains. The mechanism is multiscale with the macroscopic scale corresponding to the macrocrack, the next, smaller scale corresponding to the grain rotations and the smallest scale corresponding to the microcracks formed in the bonds whose propagation causes the bond breakage. The bond breakage is initiated by their bending or twisting caused by the corresponding moments. The sign of the moments only affects the side of the bond where the microfracturing starts. The independence of the microfracturing of the sign of the moment stresses provides a unified way of describing such apparently different types of fractures as tensile (Mode I) cracks, compaction bands (Mode I anticracks) and shear bands (Mode II and III). Modelling of this mechanism is based on the Cosserat theory. The bending/twisting moments are controlled by the corresponding components of moment stress. In the cases, when the Cosserat characteristic lengths are comparable with the grain sizes, the Cosserat theory is reduced to the couple-stress theory. It is found that the stress exhibits the square root singularity that coincides with the conventional ones, while the moment stress has singularity of the power -3/2. The J-integral, however, reflects only stress singularities, while the moment stress singularities do not contribute to the energy release rate. Subsequently, the energy criterion of macrofracture propagation can be based on the conventional J-integral and is not affected by the strong moment stress singularity.

  2. Summary of Research through Phase II/Year 2 of Initially Approved 3 Phase/3 Year Project - Establishing the Relationship between Fracture-Related Dolomite and Primary Rock Fabric on the Distribution of Reservoirs in the Michigan Basin

    SciTech Connect

    G. Grammer

    2007-09-30

    This final scientific/technical report covers the first 2 years (Phases I and II of an originally planned 3 Year/3 Phase program). The project was focused on evaluating the relationship between fracture-related dolomite and dolomite constrained by primary rock fabric in the 3 most prolific reservoir intervals in the Michigan Basin. The characterization of select dolomite reservoirs was the major focus of our efforts in Phases I and II of the project. Structural mapping and log analysis in the Dundee (Devonian) and Trenton/Black River (Ordovician) suggest a close spatial relationship among gross dolomite distribution and regional-scale, wrench fault-related NW-SE and NE-SW structural trends. A high temperature origin for much of the dolomite in these 2 studied intervals (based upon fluid inclusion homogenization temperatures and stable isotopic analyses,) coupled with persistent association of this dolomite in reservoirs coincident with wrench fault-related features, is strong evidence for these reservoirs being influenced by hydrothermal dolomitization. In the Niagaran (Silurian), there is a general trend of increasing dolomitization shelfward, with limestone predominant in more basinward positions. A major finding is that facies types, when analyzed at a detailed level, are directly related to reservoir porosity and permeability in these dolomites which increases the predictability of reservoir quality in these units. This pattern is consistent with our original hypothesis of primary facies control on dolomitization and resulting reservoir quality at some level. The identification of distinct and predictable vertical stacking patterns within a hierarchical sequence and cycle framework provides a high degree of confidence at this point that the results should be exportable throughout the basin. Much of the data synthesis and modeling for the project was scheduled to be part of Year 3/Phase III, but the discontinuation of funding after Year 2 precluded those efforts

  3. Paratrooper's Ankle Fracture: Posterior Malleolar Fracture

    PubMed Central

    Young, Ki Won; Cho, Jae Ho; Kim, Hyung Seuk; Cho, Hun Ki; Lee, Kyung Tai

    2015-01-01

    Background We assessed the frequency and types of ankle fractures that frequently occur during parachute landings of special operation unit personnel and analyzed the causes. Methods Fifty-six members of the special force brigade of the military who had sustained ankle fractures during parachute landings between January 2005 and April 2010 were retrospectively analyzed. The injury sites and fracture sites were identified and the fracture types were categorized by the Lauge-Hansen and Weber classifications. Follow-up surveys were performed with respect to the American Orthopedic Foot and Ankle Society ankle-hindfoot score, patient satisfaction, and return to preinjury activity. Results The patients were all males with a mean age of 23.6 years. There were 28 right and 28 left ankle fractures. Twenty-two patients had simple fractures and 34 patients had comminuted fractures. The average number of injury and fractures sites per person was 2.07 (116 injuries including a syndesmosis injury and a deltoid injury) and 1.75 (98 fracture sites), respectively. Twenty-three cases (41.07%) were accompanied by posterior malleolar fractures. Fifty-five patients underwent surgery; of these, 30 had plate internal fixations. Weber type A, B, and C fractures were found in 4, 38, and 14 cases, respectively. Based on the Lauge-Hansen classification, supination-external rotation injuries were found in 20 cases, supination-adduction injuries in 22 cases, pronation-external rotation injuries in 11 cases, tibiofibular fractures in 2 cases, and simple medial malleolar fractures in 2 cases. The mean follow-up period was 23.8 months, and the average follow-up American Orthopedic Foot and Ankle Society ankle-hindfoot score was 85.42. Forty-five patients (80.36%) reported excellent or good satisfaction with the outcome. Conclusions Posterior malleolar fractures occurred in 41.07% of ankle fractures sustained in parachute landings. Because most of the ankle fractures in parachute injuries were

  4. Constitutive modeling of fracture waves

    NASA Astrophysics Data System (ADS)

    Resnyansky, A. D.; Romensky, E. I.; Bourne, N. K.

    2003-02-01

    A fracture wave (FW) in a brittle material is a narrow transition region (border) of a continuous fracture zone, which may be associated with the damage accumulation process initiated by propagation of shock waves. In multidimensional structures the fracture wave may behave in an unusual way. The high-speed photography of penetration of a borosilicate (Pyrex) glass block [N. K. Bourne, L. Forde, and J. E. Field, Proc. SPIE 2869, 626 (1997)] shows a visible fracture zone with an apparent flat front although the projectile is a hemispherically nosed rod. A strain-rate-sensitive model is being developed and employed for analysis of the role of the complex stress state and kinetic description of the damage accumulation to describe the process of the impact. Numerical analysis is conducted with a one-dimensional wave propagation code employing the model and with the LS-DYNA2D hydrocode in which the model has been implemented. The analysis demonstrates that (i) the second (plastic) shock wave is superseded by quicker FW relaxing stress behind the elastic precursor, and (ii) the FW front flattening is apparently caused by the change in the acoustic directional properties. This change is associated with the phase-like transition due to the damage accumulation within the FW. In particular, the FW transition separates a highly anisotropic zone of material characterized acoustically by longitudinal and shear waves in front of the FW from a nearly isotropic region of the material characterized only by bulk waves behind the FW.

  5. Copper complexes relevant to the catalytic cycle of copper nitrite reductase: electrochemical detection of NO(g) evolution and flipping of NO2 binding mode upon Cu(II) → Cu(I) reduction.

    PubMed

    Maji, Ram Chandra; Barman, Suman Kumar; Roy, Suprakash; Chatterjee, Sudip K; Bowles, Faye L; Olmstead, Marilyn M; Patra, Apurba K

    2013-10-07

    Copper complexes of the deprotonated tridentate ligand, N-2-methylthiophenyl-2'-pyridinecarboxamide (HL1), were synthesized and characterized as part of our investigation into the reduction of copper(II) o-nitrito complexes into the related copper nitric oxide complexes and subsequent evolution of NO(g) such as occurs in the enzyme copper nitrite reductase. Our studies afforded the complexes [(L1)Cu(II)Cl]n (1), [(L1)Cu(II)(ONO)] (2), [(L1)Cu(II)(H2O)](ClO4)·H2O (3·H2O), [(L1)Cu(II)(CH3OH)](ClO4) (4), [(L1)Cu(II)(CH3CO2)]·H2O (5·H2O), and [Co(Cp)2][(L1)Cu(I)(NO2)(CH3CN)] (6). X-ray crystal structure determinations revealed distorted square-pyramidal coordination geometry around Cu(II) ion in 1-5. Substitution of the H2O of 3 by nitrite quantitatively forms 2, featuring the κ(2)-O,O binding mode of NO2(-) to Cu(II). Reduction of 2 generates two Cu(I) species, one with κ(1)-O and other with the κ(1)-N bonded NO2(-) group. The Cu(I) analogue of 2, compound 6, was synthesized. The FTIR spectrum of 6 reveals the presence of κ(1)-N bonded NO2(-). Constant potential electrolysis corresponding to Cu(II) → Cu(I) reduction of a CH3CN solution of 2 followed by reaction with acids, CH3CO2H or HClO4 generates 5 or 3, and NO(g), identified electrochemically. The isolated Cu(I) complex 6 independently evolves one equivalent of NO(g) upon reaction with acids. Production of NO(g) was confirmed by forming [Co(TPP)NO] in CH2Cl2 (λ(max) in CH2Cl2: 414 and 536 nm, ν(NO) = 1693 cm(-1)).

  6. Dynamic fracture of adhesively bonded composite structures using cohesive zone models

    NASA Astrophysics Data System (ADS)

    Makhecha, Dhaval P.

    Using experimental data obtained from standard fracture test configurations, theoretical and numerical tools are developed to mathematically describe non-self-similar progression of cracks without specifying an initial crack. A cohesive-decohesive zone model, similar to the cohesive zone model known in the fracture mechanics literature as the Dugdale-Barenblatt model, is adopted to represent the degradation of the material ahead of the crack tip. This model unifies strength-based crack initiation and fracture-mechanics-based crack progression. The cohesive-decohesive zone model is implemented with an interfacial surface material that consists of an upper and a lower surface that are connected by a continuous distribution of normal and tangential nonlinear elastic springs that act to resist either Mode I opening, Mode II sliding, Mode III sliding, or a mixed anode. The initiation of fracture is determined by the interfacial strength and the progression of the crack is determined by the critical energy release rate. The adhesive is idealized with an interfacial surface material to predict interfacial fracture. The interfacial surface material is positioned within the bulk material to predict discrete cohesive cracks. The interfacial surface material is implemented through an interface element, which is incorporated in ABAQUS using the user defined element (UEL) option. A procedure is established to formulate a rate dependent model based on experiments carried out on compact tension test specimens. The rate dependent model is incorporated into the interface element approach to capture the unstable crack growth observed in experiments under quasi-static loading conditions. The compact tension test gives the variation of the fracture toughness with the rate of loading, this information is processed and a relationship between the fracture toughness and the rate of the opening displacement is established. The cohesive-decohesive zone model is implemented through a

  7. [Fractures of the forefoot].

    PubMed

    Richter, M

    2011-10-01

    Fractures of the forefoot are common and comprise approximately two thirds of all foot fractures. Forefoot fractures are caused by direct impact or the effect of indirect force. The forces exerted can range from repetitive minor load (stress fractures) to massive destructive forces (complex trauma). The clinical course in forefoot fractures is typically more favourable than in fractures of the mid- and hindfoot. The incidence of complications like infection or pseudarthrosis is low. Exceptions are rare fractures of the proximal shaft of the fifth metatarsal and the sesamoids with higher pseudarthrosis rates. Malunited metatarsal fractures can cause painful conditions that should even be treated operatively. Differences in structure and function of the different forefoot areas and specific fracture types require an adapted management of these special injuries.

  8. Management of metacarpal fractures.

    PubMed

    McNemar, Thomas B; Howell, Julianne Wright; Chang, Eric

    2003-01-01

    Fractures of the hand are the most common fractures of the human skeleton. Metacarpal fractures account for 30% to 50% of all of hand fractures. The mechanisms of these injuries vary from axial loading forces to direct blows to the dorsal hand. Resulting deformities include malrotation, angulation, and shortening. Treatment modalities vary from nonoperative reduction to open reduction and internal fixation. The treatment algorithm is guided by the location of the fracture, the stability of the fracture, and the resultant deformity. Operative procedures, although they may lead to excellent radiographic reduction of fractures, often lead to debilitating stiffness from the inflammatory reaction of the surgical procedure. Operative fixation must be employed judiciously and offered only when confident that non-operative therapy can be improved on with operative intervention. This article reviews the various types of metacarpal fractures, with the treatment options available for each fracture. The indications for each treatment modality, postoperative care, and rehabilitation are presented.

  9. Fracture characteristics of balloon films

    NASA Technical Reports Server (NTRS)

    Portanova, Marc A.

    1989-01-01

    An attempt was made to determine the failure modes of high altitude scientific balloons through an investigation of the fracture characteristics of the thin polyethylene films. Two films were the subject of the evaluation, Winzen Int.'s Stratafilm SF-85 and Raven Industries' Astro-E. Research began with an investigation of the film's cold brittleness point and it's effect on the ultimate strength and elasticity of the polyethylene film. A series of preliminary investigations were conducted to develop an understanding of the material characteristics. The primary focus of this investigation was on the notch sensitivity of the films. Simple stress strain tests were also conducted to enable analysis employing fracture toughness parameters. Studies were conducted on both film types at 23 C (room temperature), -60 C, -90 C, and -120 C.

  10. Un mode de découverte inhabituel d'hyperparathyroïdie primaire: fractures multiples sur tumeurs brunes secondaires à un adénome parathyroïdien ectopique médiastinal

    PubMed Central

    Yassine, Asmaa; Guerboub, Ahmed Anas; Arsalane, Adil; Biyi, Abdelhamid; Moussaoui, Souad El; Belmejdoub, Ghizlaine

    2015-01-01

    La tumeur brune est une entité clinique bénigne apparaissant comme une manifestation squelettique rare de l'hyperparathyroïdie primaire. Il s'agit d'une cause inhabituelle de fractures pathologiques. Nous rapportons ici le cas clinique d'un patient âgé de 20 ans chez qui l'hyperparathyroïdie primitive a été découverte devant des tumeurs brunes multiples. PMID:26966486

  11. On material fracture criteria

    NASA Astrophysics Data System (ADS)

    Kremnev, L. S.

    2017-01-01

    Based on the nonlinear mechanics of material fracture, a model of the fracture of materials with actual (discrete) structures has been constructed. The model is supported by proofs that crack resistance K 1 c and fracture toughness G 1 c obtained from the energy conservation law without using the assumptions adopted in the linear material fracture mechanics serve as the force and energy criteria in the nonlinear fracture mechanics. It has been shown that energy criterion G 1 c in the nonlinear mechanics is much greater than G 1 c in the linear fracture mechanics.

  12. Fracture-Based Mesh Size Requirements for Matrix Cracks in Continuum Damage Mechanics Models

    NASA Technical Reports Server (NTRS)

    Leone, Frank A.; Davila, Carlos G.; Mabson, Gerald E.; Ramnath, Madhavadas; Hyder, Imran

    2017-01-01

    This paper evaluates the ability of progressive damage analysis (PDA) finite element (FE) models to predict transverse matrix cracks in unidirectional composites. The results of the analyses are compared to closed-form linear elastic fracture mechanics (LEFM) solutions. Matrix cracks in fiber-reinforced composite materials subjected to mode I and mode II loading are studied using continuum damage mechanics and zero-thickness cohesive zone modeling approaches. The FE models used in this study are built parametrically so as to investigate several model input variables and the limits associated with matching the upper-bound LEFM solutions. Specifically, the sensitivity of the PDA FE model results to changes in strength and element size are investigated.

  13. Mode of death and hospitalization from the Second Follow-up Serial Infusions of Nesiritide (FUSION II) trial and comparison of clinical events committee adjudicated versus investigator reported outcomes.

    PubMed

    O'Connor, Christopher M; Fiuzat, Mona; Lindenfeld, Joann; Miller, Alan; Lombardi, Carlo; Carson, Peter; Shaw, Linda K; Wang, Li-Joy; Connolly, Patricia; Mills, Roger; Yancy, Clyde; Mahaffey, Kenneth

    2011-11-15

    The aim of this study was to evaluate the mode of death and hospitalizations in advanced heart failure (HF) patients with renal dysfunction and to examine the rate of concordance between events reported by the clinical events committee and site investigators (using case report forms) in the Second Follow-Up Serial Infusions of Nesiritide (FUSION II) trial. Little is known about the cause of death and hospitalization in patients with advanced HF. FUSION II was a randomized, double-blind, placebo-controlled trial evaluating outpatient nesiritide infusions versus placebo, with 911 patients with advanced HF (New York Heart Association class III or IV) and renal dysfunction enrolled. There were 151 deaths and 1,041 hospitalizations at 24 weeks. The clinical events committee classified events as cardiac, renal, cardiorenal, other or noncardiovascular, or unknown. Kappa statistics and McNemar tests were used to assess agreement (overall and by individual modes of death and hospitalization indications). In conclusion, the most common cause of death or hospitalization was cardiac related, with 70% of deaths and 60% of hospitalizations due to cardiac causes. There was 74% agreement (26% disagreement) on cardiac cause of death (κ = 0.40, McNemar p = 0.001) and 75% agreement (25% disagreement) between the investigators and the clinical events committee on cardiac classification for hospitalization (κ = 0.49, McNemar p <0.0001).

  14. [Emergy value evaluation on rice-duck organic farming mode].

    PubMed

    Xi, Yunguan; Qin, Pei

    2006-02-01

    Employing emergy value evaluation method, this paper compared the ecological and economic benefits of rice-duck organic farming system (mode I) and conventional rice-wheat rotation system (mode II) in Shanghai suburb. The results showed that mode I had better emergy benefits, higher self-organizing ability and sustainability, and higher product safety. The net emergy yield ratio (EYR), feedback ratio of yield emergy (FYE), and emergy sustainable index (ESI) of mode I were respectively 1.57, 14.1, and 8.71 times as much as those of mode II, and the emergy index of product safety (EIPS) was 0 in mode I but -0.66 in mode II. The emergy investment ratio (EIR) and environmental loading ratio (ELR) of mode I were 40.1% and 18.3% of mode II, respectively, suggesting that mode I had less environmental pressure than mode II. Mode I had lower economic benefits than mode II. The economic output, gross income, and net income of mode I were 15.7%, 9.6%, and 29.6% less than those of mode II , respectively. As for Em dollars, the output, gross income, and net income of mode I were respectively 50%, 102.6%, and 136.4% higher than those of mode II. With the system optimization and the development of organic food market, mode I had the potential to improve its economic benefits.

  15. A locked hip screw-intramedullary nail (cephalomedullary nail) for the treatment of fractures of the proximal part of the femur combined with fractures of the femoral shaft.

    PubMed

    Alho, A; Ekeland, A; Grøgaard, B; Dokke, J R

    1996-01-01

    Twenty-seven patients with complex femoral fractures (combined shaft and proximal femoral fractures) were treated with a modified Grosse-Kempf slotted locking nail (cephalomedullary nail), wherein two screws were inserted in the hip. Four types of complex, multifocal femoral fractures were represented in the series. Eleven of the femoral shaft fractures were secondary to a previous, internally fixed, not yet united hip fracture (type I). Ten comminuted peritrochanteric fractures occurred in normal bone (type II). Three similar fractures were pathologic because of metastasis. Two patients had an ipsilateral fracture of the femoral shaft and the trochanteric area (type III), and one of the shaft and the femoral neck (type IV). Locking was made static in 24 cases. Additional cerclage wiring was used in three type II fractures. Five complications were as follows: one cutting out of a screw in the femoral head, two fractures of the nail, one deep venous thrombosis, and one wound hematoma. Reoperations were two salvage operations using a new nail and one evacuation of hematoma. One patient with multiple injuries and four elderly patients died within 2 months. Eighteen patients with fractures in normal bone were followed for a median of 20 (6 to 37) months. All fractures united. Two nails were removed. The end result was excellent in ten patients, good in seven, and fair in one (2-cm shortening and 20-degree external rotation). We conclude that a locked intramedullary construct with locking screws in femoral neck and distal femur controls a complex fracture situation well.

  16. Wavefront Imaging in Fractured Transversely-Isotropic Media

    NASA Astrophysics Data System (ADS)

    Shao, S.; Pyrak-Nolte, L. J.

    2013-12-01

    Fractures in the Earth's crust are a source of stress-dependent mechanical anisotropy that affect seismic wave attenuation and velocity. While many theoretical and experimental studies have investigated seismic wave propagation in single or multi- fractured isotropic rocks, few studies have examined the seismic response of a fractured anisotropic medium. Fractures and layering each contribute to the mechanical anisotropy of the crust. The coexistence of these two sources of anisotropy complicates the interpretation of the seismic properties of crustal rock. In this study, laboratory wavefront imaging was performed to capture the seismic response of layered media containing multiple parallel fractures. We determined that whether the observed anisotropy is dominated by the matrix anisotropy or by the fracture orientation depends on the applied stress and that late-arriving guided-modes provide information on the orientation of the fractures. Four cubic garolite samples (~102 mm on edge) each containing 5 parallel fractures were used in this study. The fractures were oriented normal, parallel or at acute angles (30 degrees, 60 degrees) to the layering. The fracture and layer spacing were approximately 10mm and 0.5mm, respectively. An intact sample containing no fractures was used as a standard orthorhombic medium for reference. Stress was applied to the samples with a servo-controlled loading machine. Two spherically-focused water-coupled transducers (central frequency 1MHz) were used; one as a fixed-source and the other as a translating receiver. Each sample was scanned over a 60mm×60mm region in 1 mm increments to map out the arriving wavefront (i.e. 3600 signals were recorded) as a function of time. The measured wavefront in the intact reference sample (which contained no fractures) was elliptical with the major axis parallel to the layers as expected and was stress-independent. When the fracture samples were subjected to low stress (<4 MPa), the observed seismic

  17. Interface fracture and composite deformation of model laminates

    NASA Astrophysics Data System (ADS)

    Fox, Matthew R.

    Model laminates were studied to improve the understanding of composite mechanical behavior. NiAl/Mo and NiAl/Cr model laminates, with a series of interfaces, were bonded at 1100°C. Reaction layers were present in all laminates, varying in thickness with bonding conditions. Interface fracture strengths and resistances were determined under primarily mode II loading conditions using a novel technique, the asymmetrically-loaded shear (ALS) test, in which one layer of the laminate was loaded in compression, producing a stable interface crack. The NiAl/Mo interface was also fractured in four-point bending. A small amount of plasticity was found to play a role in crack initiation. During steady-state mode II interface fracture of NiAl/Mo model laminates, large-scale slip was observed near the crack tip in the NiAl adjacent to the interface. After testing, the local slope and curvature of the interface were characterized at intervals along the interface and at slip locations to qualitatively describe local stresses present at and just ahead of the crack tip. The greatest percentage of slip occurred where closing forces on the crack tip were below the maximum value and were decreasing with crack growth. A mechanism for crack propagation is presented describing the role of large-scale slip in crack propagation. The mechanical response of structural laminates in 3-D stress states, as would be present in a polycrystalline aggregate composed of lamellar grains, are lacking. In order to understand the response of laminates composed of hard and soft phases, Pb/Zn laminates were prepared and tested in compression with varying lamellar orientation relative to the loading axis. A model describing the mechanical response in a general state assuming elastic-perfectly plastic isotropic layers was developed. For the 90° laminate, a different approach was applied, using the friction hill concepts used in forging analyses. With increasing ratios of cross-sectional radius to layer

  18. Metatarsal stress fractures - aftercare

    MedlinePlus

    ... page: //medlineplus.gov/ency/patientinstructions/000553.htm Metatarsal stress fractures - aftercare To use the sharing features on ... that connect your ankle to your toes. A stress fracture is a break in the bone that ...

  19. Infant skull fracture (image)

    MedlinePlus

    Skull fractures may occur with head injuries. Although the skull is both tough and resilient and provides excellent ... or blow can result in fracture of the skull and may be accompanied by injury to the ...

  20. Rib fracture - aftercare

    MedlinePlus

    ... page: //medlineplus.gov/ency/patientinstructions/000539.htm Rib fracture - aftercare To use the sharing features on this page, please enable JavaScript. A rib fracture is a crack or break in one or ...

  1. Forearm Fractures in Children

    MedlinePlus

    .org Forearm Fractures in Children The forearm is the part of the arm between the wrist and the elbow. It is ... two bones: the radius and the ulna. Forearm fractures are common in childhood, accounting for more than ...

  2. Pediatric Thighbone (Femur) Fracture

    MedlinePlus

    .org Thighbone (Femur) Fractures In Children Page ( 1 ) The thighbone (femur) is the largest and strongest bone in the body. It can break ... Cause Statistics The most common cause of thighbone fractures in infants under 1 year old is child ...

  3. Nasal fracture (image)

    MedlinePlus

    A nasal fracture is a break in the bone over the ridge of the nose. It usually results from a blunt ... and is one of the most common facial fracture. Symptoms of a broken nose include pain, blood ...

  4. Bone fracture repair - slideshow

    MedlinePlus

    ... page: //medlineplus.gov/ency/presentations/100077.htm Bone fracture repair - series—Indications To use the sharing features ... Go to slide 4 out of 4 Overview Fractures of the bones are classified in a number ...

  5. Femur fracture repair - discharge

    MedlinePlus

    ... page: //medlineplus.gov/ency/patientinstructions/000166.htm Femur fracture repair - discharge To use the sharing features on this page, please enable JavaScript. You had a fracture (break) in the femur in your leg. It ...

  6. Lisfranc (Midfoot) Fractures

    MedlinePlus

    ... that disrupts multiple different joints and includes multiple fractures. Lisfranc injuries tend to damage the cartilage of ... include ligament strains and tears, as well as fractures and dislocations of bone (far right). (Le ) This ...

  7. Growth Plate Fractures

    MedlinePlus

    .org Growth Plate Fractures Page ( 1 ) The bones of children and adults share many of the same risks for injury. But because they ... to a unique injury called a growth plate fracture. Growth plates are areas of cartilage located near ...

  8. Hip fracture surgery

    MedlinePlus

    ... neck fracture repair; Trochanteric fracture repair; Hip pinning surgery; Osteoarthritis-hip ... You may receive general anesthesia before this surgery. This means ... spinal anesthesia. With this kind of anesthesia, medicine is ...

  9. Transients from initial conditions based on Lagrangian perturbation theory in N-body simulations II: the effect of the transverse mode

    SciTech Connect

    Tatekawa, Takayuki

    2014-04-01

    We study the initial conditions for cosmological N-body simulations for precision cosmology. In general, Zel'dovich approximation has been applied for the initial conditions of N-body simulations for a long time. These initial conditions provide incorrect higher-order growth. These error caused by setting up the initial conditions by perturbation theory is called transients. We investigated the impact of transient on non-Gaussianity of density field by performing cosmological N-body simulations with initial conditions based on first-, second-, and third-order Lagrangian perturbation theory in previous paper. In this paper, we evaluates the effect of the transverse mode in the third-order Lagrangian perturbation theory for several statistical quantities such as power spectrum and non-Gaussianty. Then we clarified that the effect of the transverse mode in the third-order Lagrangian perturbation theory is quite small.

  10. FTIR spectra and normal-mode analysis of a tetranuclear Manganese adamantane-like complex in two electrochemically prepared oxidation states: Relevance to the oxygen-evolving complex of Photosystem II

    SciTech Connect

    Visser, Hendrik; Dube, Christopher E.; Armstrong, William H.; Sauer, Kenneth; Yachandra, Vittal K.

    2002-03-19

    The IR spectra and normal-mode analysis of the adamantane-like compound [Mn4O6(bpea)4]n+ in two oxidation states, MnIV4 and MnIIIMnIV3, that are relevant to the oxygen-evolving complex of photosystem II are presented. Mn-O vibrational modes are identified with isotopic exchange, 16O->18O, of the mono-(mu)-oxo bridging atoms in the complex. IR spectra of the MnIIIMnIV3 species are obtained by electrochemical reduction of the MnIV4 species using a spectroelectrochemical cell, based on attenuated total reflection [Visser et al. Anal Chem 2001, 73, 4374-4378]. A novel method of subtraction is used to reduce background contributions from solvent and ligand modes, and the difference and double-difference spectra are used in identifying Mn-O bridging modes that are sensitive to oxidation state change. Two strong IR bands are observed for the MnIV4 species at 745 and 707 cm-1 and a weaker band at 510 cm-1. Upon reduction, the MnIIIMnIV3 species exhibits two strong IR bands at 745 and 680 cm-1, and several weaker bands are observed in the 510 - 425 cm-1 range. A normal mode analysis is performed to assign all the relevant bridging modes in the oxidized MnIV4 and reduced MnIIIMnIV3 species. The calculated force constants for the MnIV4 species are = 3.15 mdynAngstrom, = 0.55 mdyn/Angstrom, and = 0.20 mdyn/Angstrom. The force constants for the MnIIIMnIV3 species are = 3.10 mdyn/Angstrom, = 2.45 mdyn/Angstrom, = 0.40, and = 0.15 mdyn/Angstrom. This study provides insights for the identification of Mn-O modes in the IR spectra of the photosynthetic oxygen-evolving complex during its catalytic cycle.

  11. FTIR Spectra and Normal-Mode Analysis of a Tetranuclear Manganese Adamantane-like Complex in Two Electrochemically Prepared Oxidation States: Relevance to the Oxygen-Evolving Complex of Photosystem II

    PubMed Central

    Visser, Hendrik; Dubé, Christopher E.; Armstrong, William H.; Sauer, Kenneth; Yachandra, Vittal K.

    2014-01-01

    The IR spectra and normal-mode analysis of the adamantane-like compound [Mn4O6(bpea)4]n+ (bpea = N,N-bis(2-pyridylmethyl)ethylamine) in two oxidation states, MnIV4 and MnIIIMnIV3, that are relevant to the oxygen-evolving complex of photosystem II are presented. Mn–O vibrational modes are identified with isotopic exchange, 16O→18O, of the mono-μ-oxo bridging atoms in the complex. IR spectra of the MnIIIMnIV3 species are obtained by electrochemical reduction of the MnIV4 species using a spectroelectrochemical cell, based on attenuated total reflection [Visser, H.; et al. Anal. Chem. 2001, 73, 4374–4378]. A novel method of subtraction is used to reduce background contributions from solvent and ligand modes, and the difference and double-difference spectra are used in identifying Mn–O bridging modes that are sensitive to oxidation state change. Two strong IR bands are observed for the MnIV4 species at 745 and 707 cm−1, and a weaker band is observed at 510 cm−1. Upon reduction, the MnIIIMnIV3 species exhibits two strong IR bands at 745 and 680 cm−1, and several weaker bands are observed in the 510–425 cm−1 range. A normal-mode analysis is performed to assign all the relevant bridging modes in the oxidized MnIV4 and reduced MnIIIMnIV3 species. The calculated force constants for the MnIV4 species are frIV = 3.15 mdyn/Å, frOr = 0.55 mdyn/Å, and frMnr = 0.20 mdyn/Å. The force constants for the MnIIIMnIV3 species are frIV = 3.10 mdyn/Å, frIII = 2.45 mdyn/Å, frOr = 0.40 mdyn/Å, and frMnr = 0.15 mdyn/Å. This study provides insights for the identification of Mn–O modes in the IR spectra of the photosynthetic oxygen-evolving complex during its catalytic cycle. PMID:12224948

  12. FTIR spectra and normal-mode analysis of a tetranuclear manganese adamantane-like complex in two electrochemically prepared oxidation states: relevance to the oxygen-evolving complex of photosystem II.

    PubMed

    Visser, Hendrik; Dubé, Christopher E; Armstrong, William H; Sauer, Kenneth; Yachandra, Vittal K

    2002-09-18

    The IR spectra and normal-mode analysis of the adamantane-like compound [Mn(4)O(6)(bpea)(4)](n+) (bpea = N,N-bis(2-pyridylmethyl)ethylamine) in two oxidation states, Mn(IV)(4) and Mn(III)Mn(IV)(3), that are relevant to the oxygen-evolving complex of photosystem II are presented. Mn-O vibrational modes are identified with isotopic exchange, (16)O-->(18)O, of the mono-micro-oxo bridging atoms in the complex. IR spectra of the Mn(III)Mn(IV)(3) species are obtained by electrochemical reduction of the Mn(IV)(4) species using a spectroelectrochemical cell, based on attenuated total reflection [Visser, H.; et al. Anal. Chem. 2001, 73, 4374-4378]. A novel method of subtraction is used to reduce background contributions from solvent and ligand modes, and the difference and double-difference spectra are used in identifying Mn-O bridging modes that are sensitive to oxidation state change. Two strong IR bands are observed for the Mn(IV)(4) species at 745 and 707 cm(-1), and a weaker band is observed at 510 cm(-1). Upon reduction, the Mn(III)Mn(IV)(3) species exhibits two strong IR bands at 745 and 680 cm(-1), and several weaker bands are observed in the 510-425 cm(-1) range. A normal-mode analysis is performed to assign all the relevant bridging modes in the oxidized Mn(IV)(4) and reduced Mn(III)Mn(IV)(3) species. The calculated force constants for the Mn(IV)(4) species are f(r)(IV)= 3.15 mdyn/A, f(rOr) = 0.55 mdyn/A, and f(rMnr) = 0.20 mdyn/A. The force constants for the Mn(III)Mn(IV)(3) species are f(r)(IV)= 3.10 mdyn/A, f(r)(III)= 2.45 mdyn/A, f(rOr) = 0.40 mdyn/A, and f(rMnr) = 0.15 mdyn/A. This study provides insights for the identification of Mn-O modes in the IR spectra of the photosynthetic oxygen-evolving complex during its catalytic cycle.

  13. Orbital fractures: a review

    PubMed Central

    Joseph, Jeffrey M; Glavas, Ioannis P

    2011-01-01

    This review of orbital fractures has three goals: 1) to understand the clinically relevant orbital anatomy with regard to periorbital trauma and orbital fractures, 2) to explain how to assess and examine a patient after periorbital trauma, and 3) to understand the medical and surgical management of orbital fractures. The article aims to summarize the evaluation and management of commonly encountered orbital fractures from the ophthalmologic perspective and to provide an overview for all practicing ophthalmologists and ophthalmologists in training. PMID:21339801

  14. [Epidemiological view of fracture risk].

    PubMed

    Fujiwara, Saeko

    2010-09-01

    Incidence of hip fracture increases exponentially with age. Women had two times higher hip fracture incidence than men. Major risk factors for the hip fracture are age, sex, bone mineral density, and previous fracture and others, but each risk factor contributes differently to development of the fracture by sites. Factors related to fall are important role in developing hip fracture.

  15. [Osteoporosis and Colles' fracture].

    PubMed

    Hindsø, K; Lauritzen, J B

    2001-10-01

    We describe the connection between osteoporosis and Colles' fractures of the distal radius from an epidemiological and aetiological point of view. In addition, the value of these fractures as markers of osteoporosis and future risk of fracture is assessed. Several studies have clearly shown an epidemiological association between osteoporosis and fractures of the distal radius, with the association strongest for women up to 65 years of age and for osteoporosis located in the forearm. The association weakens for other locations and for older women. Osteoporosis may have some aetiologic significance for the development of Colles' fractures, but several extraskeletal factors are of equal or further importance. The occurrence of a Colles' fracture in the first 10-15 years after the postmenopause indicates an increased relative risk of sustaining another fracture in the future. However the relative risk approaches one after a few years and, because of the comparatively low absolute risk in this age-group, Colles' fracture as a risk factor contributes little to an assessment of the lifetime fracture risk. In a few longitudinal studies, Colles' fractures could not predict the long-term risk of osteoporosis. The presence of a Colles' fracture should lead to considerations concerning the skeletal and extraskeletal causes of the fracture for the purpose of initiating preventive and therapeutic measures.

  16. Elbow fractures and dislocations.

    PubMed

    Little, Kevin J

    2014-07-01

    Elbow fractures are common in pediatric patients. Most injuries to the pediatric elbow are stable and require simple immobilization; however, more severe fractures can occur, often requiring operative stabilization and/or close monitoring. This article highlights the common fractures and dislocations about the pediatric elbow and discusses the history, evaluation, and treatment options for specific injuries.

  17. Two coordination modes of CuII in a binuclear complex with N-(pyridin-2-yl­carbon­yl)pyridine-2-carboxamidate ligands

    PubMed Central

    Campos-Gaxiola, José J.; Morales-Morales, David; Höpfl, Herbert; Parra-Hake, Miguel; Reyes-Martínez, Reyna

    2012-01-01

    In the title dinuclear complex, (acetonitrile-1κN)[μ-N-(pyri­din-2-ylcarbonyl)pyridine-2-carboxamidato-1:2κ5 N,N′,N′′:O,O′][N-(pyridin-2-ylcarbonyl)pyridine-2-carboxamidato-2κ3 N,N′,N′′]bis(trifluoromethanesulfonato-1κO)dicopper(II), [Cu2(C12H8N3O2)2(CF3O3S)2(CH3CN)], one of the CuII ions is five-coordinated in a distorted square-pyramidal N3O2 environment provided by two N-(pyridin-2-ylcarbon­yl)pyridine-2-carboxamidate (bpca) ligands, while the second CuII ion is six-coordinated in a distorted octa­hedral N4O2 environment provided by one bpca ligand, two trifluoro­methansulfonate ligands and one acetonitrile mol­ecule. Weak inter­molecular C—H⋯O and C—H⋯F hydrogen bonds and π–π stacking inter­actions with centroid–centroid distances of 3.6799 (15) and 3.8520 (16) Å stabilize the crystal packing and lead to a three-dimensional network. PMID:23125602

  18. Two coordination modes of Cu(II) in a binuclear complex with N-(pyridin-2-yl-carbon-yl)pyridine-2-carboxamidate ligands.

    PubMed

    Campos-Gaxiola, José J; Morales-Morales, David; Höpfl, Herbert; Parra-Hake, Miguel; Reyes-Martínez, Reyna

    2012-10-01

    In the title dinuclear complex, (acetonitrile-1κN)[μ-N-(pyri-din-2-ylcarbonyl)pyridine-2-carboxamidato-1:2κ(5)N,N',N'':O,O'][N-(pyridin-2-ylcarbonyl)pyridine-2-carboxamidato-2κ(3)N,N',N'']bis(trifluoromethanesulfonato-1κO)dicopper(II), [Cu(2)(C(12)H(8)N(3)O(2))(2)(CF(3)O(3)S)(2)(CH(3)CN)], one of the Cu(II) ions is five-coordinated in a distorted square-pyramidal N(3)O(2) environment provided by two N-(pyridin-2-ylcarbon-yl)pyridine-2-carboxamidate (bpca) ligands, while the second Cu(II) ion is six-coordinated in a distorted octa-hedral N(4)O(2) environment provided by one bpca ligand, two trifluoro-methansulfonate ligands and one acetonitrile mol-ecule. Weak inter-molecular C-H⋯O and C-H⋯F hydrogen bonds and π-π stacking inter-actions with centroid-centroid distances of 3.6799 (15) and 3.8520 (16) Å stabilize the crystal packing and lead to a three-dimensional network.

  19. Influence of the temperature and strain rate on the structure and fracture mode of high-strength steels upon the simulation of the thermal cycle of welding and post-welding tempering

    NASA Astrophysics Data System (ADS)

    Pazilova, U. A.; Il'in, A. V.; Kruglova, A. A.; Motovilina, G. D.; Khlusova, E. I.

    2015-06-01

    Structural changes and the main features of the fracture of the base metal and the coarse-grained region of the heat-affected zone of the welded joints of high-strength steels have been studied by simulating the thermal cycle of welding and post-welding heat treatment. The effects of the simultaneous action of heating for high-temperature tempering and of deformation allowing the estimation of the impact of residual welding stresses have been studied. The probable reasons of the formation of cracks in welds upon the postwelding tempering have been determined.

  20. Fracture Behavior of Ceramic Composites.

    DTIC Science & Technology

    1983-08-01

    AD-R158 810 FRACTURE BEHAVIOR OF CERAMIC COMPOSITES(U) MATERIALS i/i SCIENCES CORP SPRING HOUSE PH K W BUESKING ET AL. AUG 83 MSC/TFR/’i482/i583...the U.S. Government . D T IC ELECTEF C01 AIR FORCE OFFICE OF SCIENTIFIC RESEARCH MSC TFR 1402/1503 Bolling Air Force Base, DC August, 1983 q Ippreved...Bethlehem Pike, Spring House , PA * 215-542-8400 ." -- . ". ’- , ,,- . ..O TTr.AqRTTpf SECURITY CLASSIFICATION OF THIS PAGE (When Date Enteredl REPORT

  1. Proximal humerus fractures.

    PubMed

    Price, Matthew C; Horn, Pamela L; Latshaw, James C

    2013-01-01

    Proximal humerus fractures are among the most common fractures associated with osteoporosis. With an aging population, incidence of these fractures will only increase. The proximal humerus not only forms the lateral portion of the shoulder articulation but also has significant associations with musculoskeletal and neurovascular structures. As a result, fractures of the proximal humerus can significantly impact not only the function of the shoulder joint, but the health and function of the entire upper extremity as well. Understanding of these fractures, the management options, and associated nursing care, can help reduce morbidity rate and improve functional outcomes.

  2. Stress fractures in runners.

    PubMed

    McCormick, Frank; Nwachukwu, Benedict U; Provencher, Matthew T

    2012-04-01

    Stress fractures are a relatively common entity in athletes, in particular, runners. Physicians and health care providers should maintain a high index of suspicion for stress fractures in runners presenting with insidious onset of focal bone tenderness associated with recent changes in training intensity or regimen. It is particularly important to recognize “high-risk” fractures, as these are associated with an increased risk of complication. A patient with confirmed radiographic evidence of a high-risk stress fracture should be evaluated by an orthopedic surgeon. Runners may benefit from orthotics, cushioned sneakers, interval training, and vitamin/calcium supplementation as a means of stress fracture prevention.

  3. [Rarely seen fractures].

    PubMed

    Subaşi, M; Kapukaya, A; Kesemenli, C; Coban, V

    2001-10-01

    Rarely seen fractures are presented in this study. One case was a calcaneal spur, 2 cases osteochondroma pedicule fractures and talus posteromedial tubercle fracture due to direct trauma. Calcaneal spur and osteochondromas were removed surgically and posteromedial tubercle was treated by short-leg cast immobilization. In conclusion, we think that fractures of osteochondroma and calcaneal spur may be treated by surgical removal which do not cause any functional disorders after this operation, but fractures like the talus posteromedial tubercle should be treated conservatively by short-leg immobilization in the early period.

  4. structured exploratory data analysis (SEDA) for determining mode of inheritance of quantitative traits. II. simulation studies on the effect of ascertaining families through high-valued probands.

    PubMed Central

    Karlin, S; Williams, P T

    1981-01-01

    An understanding of the effect of selecting families through a high-valued proband on the major gene index (MGI), the offspring between parents function (OBP), and the pairwise midparental correlation coefficient (MPCC) is developed. It is shown that the interpretations of these statistics must be carefully modified to adjust for the biases created by the selection criteria. Computer simulations are used to examine sporadic, multifactorial, and major gene models, under moderate (85%) and extreme (95%) proband selection. Additional insights may be acquired into the nature of mode of inheritance by comparing and contrasting selected and unselected of populations. PMID:7211842

  5. structured exploratory data analysis (SEDA) for determining mode of inheritance of quantitative traits. II. simulation studies on the effect of ascertaining families through high-valued probands.

    PubMed

    Karlin, S; Williams, P T

    1981-03-01

    An understanding of the effect of selecting families through a high-valued proband on the major gene index (MGI), the offspring between parents function (OBP), and the pairwise midparental correlation coefficient (MPCC) is developed. It is shown that the interpretations of these statistics must be carefully modified to adjust for the biases created by the selection criteria. Computer simulations are used to examine sporadic, multifactorial, and major gene models, under moderate (85%) and extreme (95%) proband selection. Additional insights may be acquired into the nature of mode of inheritance by comparing and contrasting selected and unselected of populations.

  6. Development of an isothermal titration microcalorimetric system with digital control and dynamic power peltier compensation. II. Characterization and operation mode. Myoglobin adsorption onto polymeric latex particles

    NASA Astrophysics Data System (ADS)

    Velázquez-Campoy, A.; López-Mayorga, O.; Cabrerizo-Vílchez, M. A.

    2000-04-01

    In a previous article a comprehensive description of an isothermal titration microcalorimeter with Peltier compensation was reported. This work deals with the characterization procedure and the operation mode. The transfer function parameters (time constants, calibration constants, and thermal properties of the system components) have been determined using a rigorous physical model for the microcalorimeter. To check the good performance of the instrument, titration experiments of cytidine and adenosine protonation have been carried out. Finally, as an example of the instrument applicability, differential heat measurements of myoglobin adsorption onto polymeric (polystyrene) latex particles are presented.

  7. Long-term regional bond strength of three MMA-based adhesive resins in simulated vertical root fracture.

    PubMed

    Nurrohman, Hamid; Nikaido, Toru; Sadr, Alireza; Takagaki, Tomohiro; Kitayama, Shuzo; Ikeda, Masaomi; Waidyasekera, Kanchana; Tagami, Junji

    2011-01-01

    The purpose of this study was to investigate bond durability of MMA-based adhesives to root dentin in a simulated complete vertical root fracture (CVRF). The fractured fragments of human premolar root were reattached using Super-Bond C&B (SB; Sun Medical), M-Bond or M-Bond II (MB or MB II; Tokuyama Dental). After storage for 1 day, 1 month, 6 months and 1 year, the reattached specimens were subjected to microtensile bond strength (µTBS) test at cervical and apical regions. Results showed that µTBS was significantly higher to cervical dentin than to apical dentin in MB and MB II, but not SB (p<0.05). Significant decrease in µTBS was found for MB and MB II after 1 year, whereas no significant difference was found for SB (p<0.05). Analysis of failure mode by SEM indicated differences over time. In conclusion, significant differences were found in the regional bond durability among MMA-based adhesives used to restore CVRF, that may lead to different clinical performances.

  8. Subsurface fracture spacing

    SciTech Connect

    Lorenz, J.C. ); Hill, R.E. )

    1991-01-01

    This study was undertaken in order to document and analyze the unique set of data on subsurface fracture characteristics, especially spacing, provided by the US Department of Energy's Slant Hole Completion Test well (SHCT-1) in the Piceance Basin, Colorado. Two hundred thirty-six (236) ft (71.9 m) of slant core and 115 ft (35.1 m) of horizontal core show irregular, but remarkably close, spacings for 72 natural fractures cored in sandstone reservoirs of the Mesaverde Group. Over 4200 ft (1280 m) of vertical core (containing 275 fractures) from the vertical Multiwell Experiment wells at the same location provide valuable information on fracture orientation, termination, and height, but only data from the SHCT-1 core allow calculations of relative fracture spacing. Within the 162-ft (49-m) thick zone of overlapping core from the vertical and deviated wellbores, only one fracture is present in vertical core whereas 52 fractures occur in the equivalent SHCT-1 core. The irregular distribution of regional-type fractures in these heterogeneous reservoirs suggests that measurements of average fracture spacing'' are of questionable value as direct input parameters into reservoir engineering models. Rather, deviated core provides data on the relative degree of fracturing, and confirms that cross fractures can be rare in the subsurface. 13 refs., 11 figs.

  9. Numerical Experiments on Ductile Fracture in Granites

    NASA Astrophysics Data System (ADS)

    Regenauer-Lieb, K.; Weinberg, R. F.

    2006-12-01

    Ceramics and, by analogy rocks, are brittle at low temperatures, however, at high temperature and high pressure a second ductile mode of fracture based on dislocation and/or diffusion processes predominates. For ceramics 0.5-0.7 times the melting temperature suffice to create creep/ductile fracture which occurs typically after long time of deformation 104-1010 s (1). Ductile creep fractures make up for the low stress by profiting from accumulated strain and diffusion during slow creep deformation. Creep fractures typically nucleate on grain or phase boundaries, rigid or soft inclusions. Ultimately, the localized inhomogeneous damaged zone, begin to spread laterally and coalesce to create or follow a propagating shear band. The creep fracture sequence of crack nucleation, growth and coalescence relies on a mechanism of self-organization of fluids into a shear band during deformation and converts macroscopically to the crack like propagation of localized shear zones. Numerical experiments are used to test the ductile fracture hypothesis for the segregation and transfer of melts in granites. Ref: (1) C. Ghandi, M. F. Ashby, Acta Metallurgica 27, 1565 (1979).

  10. Atraumatic sternum fracture

    PubMed Central

    Abrahamsen, Sebastian Ørskov; Madsen, Christina Friis

    2014-01-01

    The spine, pelvic bones and long bones of the lower extremities are common sites for insufficiency fractures. Cases of sternum insufficiency fractures have rarely been reported among elderly patients. Insufficiency fractures tend to occur in bones with decreased mechanical strength especially among elderly patients, in postmenopausal women and patients with underlying diseases. We describe a case of spontaneous sternum insufficiency fracture in a healthy man, with no known risk factors to fracture, or previous history of fractures. Sternum insufficiency fracture is a rare cause of chest pain. This case serves to remind the emergency physician to remain vigilant for other non-cardiac, non-pulmonary and non-traumatic causes of chest pain, especially among patients with known risk factors such as osteoporosis, chronic obstructive pulmonary disease, rheumatoid arthritis, systemic lupus erythematosus and patients on long-term steroid treatment. If diagnosed correctly, these patients can be discharged and treated as outpatients as this case emphasises. PMID:25326566

  11. Mechanics of Hydraulic Fractures

    NASA Astrophysics Data System (ADS)

    Detournay, Emmanuel

    2016-01-01

    Hydraulic fractures represent a particular class of tensile fractures that propagate in solid media under pre-existing compressive stresses as a result of internal pressurization by an injected viscous fluid. The main application of engineered hydraulic fractures is the stimulation of oil and gas wells to increase production. Several physical processes affect the propagation of these fractures, including the flow of viscous fluid, creation of solid surfaces, and leak-off of fracturing fluid. The interplay and the competition between these processes lead to multiple length scales and timescales in the system, which reveal the shifting influence of the far-field stress, viscous dissipation, fracture energy, and leak-off as the fracture propagates.

  12. Prediction of Petermann I and II Spot Sizes for Single-mode Dispersion-shifted and Dispersion-flattened Fibers by a Simple Technique

    NASA Astrophysics Data System (ADS)

    Kamila, Kiranmay; Panda, Anup Kumar; Gangopadhyay, Sankar

    2013-09-01

    Employing the series expression for the fundamental modal field of dispersion-shifted trapezoidal and dispersion-flattened graded and step W fibers, we present simple but accurate analytical expressions for Petermann I and II spot sizes of such kind of fibers. Choosing some typical dispersion-shifted trapezoidal and dispersion-flattened graded and step W fibers as examples, we show that our estimations match excellently with the exact numerical results. The evaluation of the concerned propagation parameters by our formalism needs very little computations. This accurate but simple formalism will benefit the system engineers working in the field of all optical technology.

  13. Atomic simulation of cracks under mixed mode loading

    NASA Technical Reports Server (NTRS)

    Mullins, M.

    1984-01-01

    A discrete atomic model of a crack tip in iron under mixed mode loads is examined. The results indicate that the behavior of the crack at the atomic scale as a function of the ratio of mode I to mode II component of load is quite complex. In general, crack tip plasticity appears to increase as the mode II component of load increases.

  14. Fracture Strength of Endodontically Treated Teeth Restored with Casting Post and Core and Glass-Fiber with Composite Core

    PubMed Central

    Saatian, Sedigheh

    2006-01-01

    INTRODUCTION: Prefabricated metal and ceramic posts can be used with different kinds of core materials as an alternative to the conventional casting post and cores. It is unclear how these post and core systems can withstand different kind of forces in the mouth. The purpose of this study was to compare the fracture strength of endodontically treated, crowned maxillary incisors restored with casting post and cores and glass- fiber post with composite core and to evaluate their mode of fractures. MATERIALS AND METHODS: Thirty caries free, human maxillary central incisors with incisoapical length of 23 ± 1 mm were divided into two groups. After root canal treatment procedures and decronation of teeth 2mm above cementoenamel junction, Grope 1 was restored with glass- fiber posts and composite cores and group 2 received casting post and cores. Teeth were prepared with a circumferential shoulder including a 1-2 mm ferrule and 0.5 mm bevel; all posts were cemented with an adhesive resin and teeth were restored with complete coverage crowns. Loads were applied at an angle of 135 degrees using a universal testing machine. Compression force was applied until the specimens fractured. RESULTS: The median fracture strengths of groups 1 and 2 were 459 and 686 respectively (p<0.5). In group I, all fractures occurred in incisal third of roots. In groups II, 40% of fractures were in apical third and middle of roots. CONCLUSION: Within the limitation of this study, the results suggested that glass fiber with composite cores can be used as an alternative to cast posts and cores in anterior teeth when creating 2mm ferrule effect was possible in normal occlusion. Clinical trial is required to verify these in vitro results. PMID:24470803

  15. Effect of interposed periosteum in an animal physeal fracture model.

    PubMed

    Phieffer, L S; Meyer, R A; Gruber, H E; Easley, M; Wattenbarger, J M

    2000-07-01

    To study the effect of interposed periosteum on physeal fracture healing, 52 skeletally immature female Harlan Sprague-Dawley rats, 4 to 5 weeks of age, were randomized to one of three cohort groups. All animals underwent surgical dissection of the left proximal medial tibia; dissection consisted of superficial exposure and incision of a standard periosteal flap. Animals in Group I (fracture alone) underwent physeal fracture; those in Group II (fracture and periosteum) underwent physeal fracture with interposition of periosteum in the fracture site, and those in Group III (positive control) underwent physeal fracture, excision of 1/2 of the growth plate, and interposition of periosteum in the defect. After histologic examination of serial sections, fracture alone resulted in physeal injury frequently associated with small bar formation without a reduction in leg length. With the addition of interposition of periosteum into the fracture site, a small, but statistically significant, increase in leg length discrepancy frequently associated with small histologic bar formation occurred when compared with fracture alone.

  16. Anisotropic mode-dependent damage of cortical bone using the extended finite element method (XFEM).

    PubMed

    Feerick, Emer M; Liu, Xiangyi Cheryl; McGarry, Patrick

    2013-04-01

    Anisotropic damage initiation criteria were developed for extended finite element method (XFEM) prediction of crack initiation and propagation in cortical bone. This anisotropic damage model was shown to accurately predict the dependence of crack propagation patterns and fracture toughness on mode mixity and on osteon orientations, as observed experimentally. Four in